3412_OldSalisburyRdCDLF_GWMR_20180104

This page intentionally left blank.

ASSESSMENT
MONITORING
REPORT
Including the November 2017
Groundwater Sampling Event
Old Salisbury Road Landfill
NCDEQ Permit NO. 34-12
HDR Project No. 10043322
Forsyth County, North Carolina
January 2018

This page intentionally left blank.

Winston-Salem City/County Utilities | Assessment Monitoring Report Table of Contents
i
Table of Contents
Table of Contents ........................................................................................................................... i
List of Tables .......................................................................................................................... i
List of Figures ......................................................................................................................... i
Appendices ............................................................................................................................ ii
List of Acronyms .................................................................................................................... ii
1.0 General .............................................................................................................................. 1
1.1. Facility Background ........................................................................................................ 1
1.2. Regulatory Authority ....................................................................................................... 1
1.3. Assessment Monitoring .................................................................................................. 1
1.4. Geologic Characteristics ................................................................................................. 3
1.4.1. Regional Geologic and Hydrogeologic Setting ........................................................ 3
1.4.2. Site Specific Topography and Drainage .................................................................. 3
1.4.3. Site Specific Hydrogeology ..................................................................................... 3
2.0 Monitoring Network ............................................................................................................ 5
3.0 Data Collection ................................................................................................................... 7
4.0 Results ............................................................................................................................... 9
4.1. Detected Groundwater Constituents .............................................................................. 9
4.2. Landfill Gas ................................................................................................................... 10
5.0 Summary & Recommendations ....................................................................................... 11

List of Tables
Table 1 - Existing Groundwater Monitoring Well Details ............................................................... 5
Table 2 - Sampling Schedule ........................................................................................................ 6
Table 3 - Recent Water Level Readings ....................................................................................... 7
Table 4 - Hydraulic Gradient & Flow Velocity ............................................................................... 8
Table 5 - Methane Gas Readings ............................................................................................... 10
Table 6 - Event Lab Summary – November 2017 ....................................................................... 13
Table 7 - Event Field Summary – November 2017 ..................................................................... 14

List of Figures
Figure 1 - Groundwater Contours and Sample Locations – January 2018 ................................... 2
Figure 2 - Historic Groundwater Elevations .................................................................................. 7
Figure 3 - Selected Groundwater Detections in MW-2R ............................................................... 9

Winston-Salem City/County Utilities | Assessment Monitoring Report Table of Contents
ii
Appendices
Appendix A – Summary of Groundwater Monitoring Results
Appendix B – Laboratory Groundwater Report
Appendix C – Field Data
Appendix D – Electronic Files

List of Acronyms
2L 15A NCAC Subchapter 02L - Groundwater Classification and Standards
µg/L micrograms per liter
EPA United States Environmental Protection Agency
MCL Maximum Contaminant Level
MDL method detction limit
NC DENR North Carolina Department of Environment and Natural Resources1
NCDEQ North Carolina Department of Environmental Quality1
ND not detected in sample
NE standard not established
NS not sampled
NTU Nephelometric turbidity units
PCB polychlorinated biphenyl
PCE tetrachloroethene
PRL practical reporting limit
PVC polyvinyl chloride
SWSL solid waste section limits
SVOC semi-volatile organic compound
VOC volatile organic compound
USGS U.S. Geological Survey
1Prior to September 18, 2015, the NCDEQ was referred to as the NC DENR. Both naming conventions are used in this report, as appropriate.

Winston-Salem City/County Utilities | Assessment Monitoring Report General
1
1.0 General
HDR Engineering, Inc. of the Carolinas (HDR), on behalf of the Winston-Salem City/County
Utility Commission (the City), is hereby submitting assessment monitoring results for
groundwater at the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North
Carolina. The assessment monitoring is being conducted to address the detection of benzene
and tetrachloroethene (PCE) above the groundwater monitoring standards in groundwater
monitoring well MW-2R that were initially detected during the May 2011 and June 2011 events.
1.1. Facility Background
The OSR landfill covers approximately 56 acres and is situated within a 140-acre tract north of
Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The
site is accessed via Old Salisbury Road (State Road 3011). The Forsyth/Davidson County line
borders the site to the south. Figure 1 illustrates the location of the OSR landfill. The facility was
originally issued a permit to operate on July 3, 1996 and opened in August of the same year.
1.2. Regulatory Authority
The site is currently operated under NC DENR facility permit number 34-12 dated April 6, 2015
(DIN 23258). The groundwater monitoring and reporting requirements are addressed in items
36 to 45 of the permit. NC Solid Waste Management Rules 15A NCAC 13B .0544(b) and
.0544(c) define the requirements for the site’s groundwater and surface water monitoring plans,
respectively. The current Groundwater Monitoring Plan was approved as noted, by NC DENR
on March 5, 2015 (DIN 23910).
1.3. Assessment Monitoring
The site is currently in assessment monitoring due to detections in MW-2R. An Assessment
Monitoring Plan for MW-2R was submitted in accordance with 15A NCAC 13B .0545 by HDR on
December 9, 2011. This plan was approved with two exceptions on January 17, 2012. The first
exception required the location of MW-15 to be in the same flow path as MW-2R; the second
required all wells to be sampled for Appendix II constituents. In February of 2014 the City
requested, and NC DENR approved, the following modifications to the facility’s assessment
monitoring plan.
• Groundwater monitoring wells MW-1R, MW-2R, MW-4R and MW-15 will be sampled
semiannually for the previously detected Appendix II constituents, in addition to
Appendix I constituents; and
• All groundwater monitoring wells will be sampled during every other Fall event (odd
years) for the entire Appendix II constituent list.
• Additional Appendix II constituents detected will be added to the sampling program for
subsequent semiannual events.
In January 2016 (the Fall 2015 Report), HDR recommended changes to the semi-annual
sampling schedule. NCDEQ approved sampling for additional detected parameters. No
parameters were approved by NCDEQ to be removed from the sampling schedule.
FORSYTH COUNTY
DAVIDSON COUNTY FORSYTH COUNTY
DAVIDSON COUNTY
V
IV
VI
III
II
I
SHEET TITLE
PROJECT TITLE
PROJECT MANAGER
DATE
PROJECT NUMBER
REFERENCE DOCUMENT
EXHIBIT NUMBER
REFERENCE SHEET
SHEET TITLE
PROJECT TITLE
GROUNDWATER CONTOURS
AND SAMPLE LOCATIONS
FALL 2017
Winston-Salem City/County Utilities | Assessment Monitoring Report General
3
1.4. Geologic Characteristics
This section paraphrases the descriptions in the original July 2003 Ground Water Monitoring
Plan and the 2003 Design Hydrogeologic Investigation Report.
1.4.1. Regional Geologic and Hydrogeologic Setting
The 1985 Geologic Map of North Carolina locates OSR in the Charlotte belt of the Piedmont
Physiographic Province. This Province contains metamorphic and igneous plutonic rocks, which
in some areas have been extensively weathered and eroded forming an undulating and well-
dissected topography.
Subsurface conditions generally consist of a veneer of topsoil underlain by residual soils,
saprolite, partially weathered rock, and fractured rock. There is generally a gradual transition
from one material type to the next with varying thickness of each.
The area is underlain by granite rock. The bedrock is typically fractured and is overlain by highly
weathered bedrock called saprolite. The saprolite varies in thickness from a few feet near
bedrock outcrops to over 100 feet. The saprolite material retains some of the original (relict)
structural features of the parent rock. The nearer surface residual soils are formed by the in-
place physical and chemical weathering of the saprolite and usually do not retain the relict
structural features.
In the Piedmont Physiographic Province, groundwater is present within the openings created by
fractures and joints within the bedrock and within the pore spaces of the overlying-saprolite. The
saprolite/bedrock aquifers are primarily recharged by precipitation in the interstream areas,
which infiltrates through the unsaturated zone to the water table. The depth to groundwater is
generally deeper beneath uplands than beneath valleys. The water table is commonly close to
the top of bedrock and is more often than not, located within the saprolite. Groundwater
generally moves laterally and downward through the saprolite and bedrock toward streams, and
surface water bodies. The water table surface is generally a subdued reflection of the surface
topography.
1.4.2. Site Specific Topography and Drainage
Surface drainage at the subject site is primarily controlled by a north-northwesterly trending
ridge within the property. Surface runoff is directed by a ridge within the site. Construction of the
landfill generally mimics and replaced the natural ridge that existed prior to the landfill. This
ridge directs runoff northeast, west and southwest into tributaries of South Fork Muddy Creek.
The majority of surface runoff within this site is directed to South Fork Muddy Creek on the
north. A small area in the extreme southeasterly section of the site appears to drain south into
Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow to the west where they
converge with Muddy Creek. Muddy Creek flows to the south and converges with the Yadkin
River.
1.4.3. Site Specific Hydrogeology
As documented in the Design Hydrogeological Investigation Report submitted by HDR on
December 2, 2003, the uppermost aquifer underlying the facility is comprised of three
stratigraphic units. The stratigraphic downward progression of the three units is saprolite
Winston-Salem City/County Utilities | Assessment Monitoring Report General
4
transitioning into partially weather bedrock, then competent bedrock. Groundwater flow through
the saprolite and partially weathered bedrock is through the soil matrix, while groundwater flow
through the bedrock is primarily fracture flow.
The average effective porosity of the saprolite stratum is 17 (unitless), while the saprolite
transition zone has an effective porosity of 25. The effective porosity of the bedrock is
significantly less at 2.
The historical hydraulic conductivity (K) calculated for the saprolite is 0.259 feet per day (ft./day)
(9.1 x 10-5 cm/sec). The historical average hydraulic conductivity for the transition zone is 0.466
ft./day (1.65 x 10-4 cm/sec). The historic hydraulic conductivity of the bedrock aquifer was
considerably less than either the saprolite or transition zone units with a K value of 0.043 ft./day
(1.5 x 10-5 cm/sec). Detailed calculations of the hydraulic conductivity, flow rates, and porosity
were provided in the 2003 Design Hydrogeologic Investigation Report.
Based on historical field observations (i.e., soil boring records) and laboratory test results from
the 2003 Design Hydrogeologic Investigation Report, the uppermost aquifer beneath the facility
predominantly exists within the unconsolidated saprolite soil and transition zone units that have
been classified as micaceous silty sands and sandy silts produced by the in-situ weathering of
the granodiorite parent rock. Groundwater flow within the uppermost aquifer is predominantly
porous flow through the unconsolidated units. There is no evidence of discrete flow patterns
within the saprolite and transition zones of the uppermost aquifer resulting from relict quartz
veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In
general, the flow of groundwater occurs for the facility is from higher elevations onsite to lower
elevations onsite under unconfined (water table) conditions regardless of the stratigraphic unit in
which it resides. As such, the static water table generally mimics the topography.

Winston-Salem City/County Utilities | Assessment Monitoring Report Monitoring Network
5
2.0 Monitoring Network
Sampling occurs semiannually for the site monitoring wells and four surface water monitoring
locations. The groundwater monitoring locations are depicted on the Figure 1. Table 1 provides
location and construction details for the existing monitoring wells.
Groundwater monitoring well MW-1R is located hydraulically upgradient of the landfill and is
considered as the background well for the site. Upstream surface water (SW-1) and
downstream surface water (SW-2) samples are obtained from the adjacent stream to the east.
Surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity
of MW-2R. SW-3 is located south of the entrance road near MW-2R; SW-4 is located on the
north side of the entrance road, downstream of SW-3.
Table 1 - Existing Groundwater Monitoring Well Details

The sampled locations were evaluated by the methods and for the analytical parameters listed
in Table 2, except that the full round of Appendix II parameters were not sampled for at all wells.
The wells were resampled for the missing parameters on December 28, 2017. The results of the
December sampling will be presented after they are reported by the laboratory.
Samples were collected from each of the landfill groundwater wells using the dedicated QEDTM
MicroPurge ® pumps that were installed in August 2004, except at MW-15, which is sampled
with a bailer.

OSR LF
WELL Installed
NC Sate
Plane
Northing
NC Sate
Plane
Easting
Well
Diameter
(inches)
Well
Depth
(below
ground)
Depth:
Ground to
Top of
Screen
Screened
Interval
(ft)
Screened Interval
Geology
Top Of
Casing
Elevation
(ft MSL)
Ground
Elevation
(ft MSL)
MW-1R 12/27/1995 820,411 1,622,983 2 60.0 45 15 Granitic saprolite 836.42 833.40MW-2R 12/29/1995 820,974 1,622,722 2 23.0 8 15 Granitic saprolite 785.22 781.81MW-3R 7/7/1999 821,237 1,621,463 2 27.0 12 15 Granitic saprolite 776.60 772.90MW-4R 12/28/1995 820,435 1,621,428 2 20.0 5 15 Granitic saprolite 767.96 765.70MW-5R 12/29/1995 820,137 1,622,130 2 32.0 17 15 Granitic saprolite 784.36 782.30MW-7 12/28/1995 820,886 1,621,424 2 48.0 33 15 Granitic saprolite 803.66 802.10MW-8 7/7/1999 821,930 1,621,485 2 27.0 12 15 Granitic saprolite 762.50 759.80MW-9 8/11/2004 822,311 1,621,986 2 60.0 45 15 Sand 790.28 788.04MW-10 8/10/2004 822,626 1,622,699 2 21.0 6 15 Sand 738.21 735.70MW-11 8/10/2004 822,307 1,622,838 2 20.0 5 15 Sand 732.59 730.35
MW-12 8/9/2004 821,844 1,622,955 2 16.0 6 10 Silt 739.07 736.41MW-13 8/9/2004 821,500 1,622,915 2 20.0 5 15 Sand 751.23 749.19MW-14 8/11/2004 822,420 1,622,260 2 60.0 45 15 Sand 783.88 781.44MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58
Winston-Salem City/County Utilities | Assessment Monitoring Report Monitoring Network
6
Table 2 - Sampling Schedule
Method Parameter(s) Frequency Monitoring Wells Surface Water
EPA 300.0 Sulfate 2x/year All All
EPA 6010 Trace Metals 2x/year All All
EPA 7470 Mercury 2x/year All All
EPA 8081
Pesticides Fall of odd years (2017) All None
4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, delta-BHC, Endosulfan I, Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Heptachlor epoxide & Methoxychlor
(Pesticides recently detected)
2x/year MW-1R, MW-2R, MW-4, MW-7, MW-10 & MW-15 None
EPA 8082 PCB’s Fall of odd years (2017) All None
EPA 8151
Herbicides Fall of odd years (2017) All None
2,4,5-TP (Silvex), 2,4-D
(Herbicides previously detected) 2x/year MW-1R, MW-2R, MW-4R & MW-15 None
EPA 8260
App I VOCs + Tetrahydrofuran 2x/year All All
Appendix II VOCs Fall of odd years (2017) All None
Dichlorodifluoromethane
(Appendix II VOC
recently detected)
2x/year All None
EPA 8270
SVOCs Fall of odd years (2017) All None
Benzo(a)anthracene, Bis(2-ethylhexyl)phthalate, Chrysene Dibenz(a,h)anthracene &
Indeno(1,2,3-cd)pyrene
(SVOCs recently detected)
2x/year MW-1R, MW-2R, MW-4R , MW-3R & MW-15 SW-2
SM 2320B Alkalinity 2x/year All All
SM 2540C Total Dissolved Solids 2x/year All All
SM 4500 Chloride, Cyanide, Sulfide 2x/year All All
Field Temperature, Specific conductance, Dissolved Oxygen, Redox, Turbidity, pH 2x/year All All
Field Total well depth and static water level 2x/year All NA

Winston-Salem City/County Utilities | Assessment Monitoring Report Data Collection
7
3.0 Data Collection
The monitoring program consists of collection and analysis of groundwater samples from 14
wells. The sampling event occurred over two days (November 16-17, 2017). Pace Analytical
Laboratories, Inc. (Pace) of Huntersville, North Carolina (NC Cert. # 5342), on behalf of HDR,
sampled the groundwater monitoring wells for this report. Synoptic groundwater elevations were
measured at all wells on November 16, 2017.
The depth from the top of the PVC casing to groundwater is measured to the nearest 0.01 foot
prior to purging each well. This depth to water, when subtracted from the reference datum,
provides a groundwater surface elevation. Table 3 provides the recent water level readings as
well as depicted in Figure 1. Figure 2 depicts the relative groundwater elevations in the on-site
monitoring wells over time.
Table 3 - Recent Water Level Readings

Figure 2 - Historic Groundwater Elevations

720
730
740
750
760
770
780
790
800
810
Groundwater Surface Elevation (feet above msl)Sample Date
MW-1R
MW-2R
MW-5R
MW-6R
MW-7
MW-15
MW-4R
MW-3R
MW-8
MW-13
MW-9
MW-12
MW-14
MW-11
MW-10
MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8
11/16/2017 801.59 777.00 756.20 759.04 772.94 767.01 744.95
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
11/16/2017 737.45 726.09 728.22 733.77 742.19 731.91 763.48
Winston-Salem City/County Utilities | Assessment Monitoring Report Data Collection
8
A variable speed micro-purge pump (or bailer in the case of MW-15) was used to purge
groundwater from each well until stabilization of measured field parameters (pH, conductivity,
redox, temperature, turbidity, and dissolved oxygen) occurred. Following completion of purging
activities, the wells were sampled using the same pump and field parameters (pH, specific
conductance, redox, turbidity, dissolved oxygen, and temperature) were recorded on field
sampling logs. Copies of these logs are provided in Appendix C.
Table 3 illustrates the hydraulic gradients calculated between representative well pairs and the
corresponding flow velocities. The flow velocities have been calculated based on the values for
historic hydraulic conductivity (0.466 ft./day) and effective porosity (25%), as presented in Table
2-9 of the December 2003 OSR Design Hydrogeologic Investigation Report for the landfill.
The minimum and maximum values are based on the historic data collected from the site
beginning in May 2003. HDR estimates a travel time of about four years between MW-2R and
MW-15, based on the estimated flow rate of 49 ft./yr. and a distance of 195 feet.
Table 4 - Hydraulic Gradient & Flow Velocity
Hydraulic Gradient (ft./ft.)
Flow Velocity (ft./yr.)
Based on Historic Record
Minimum Maximum May 2015 Nov 2015 May 2016 Nov 2016 May 2017 Nov 2017
MW-1R to
MW-4R
0.024
17
0.028
19
0.027
18
0.027
19
0.026
18
0.028
19
0.027
18
0.027
19
MW-1R to
MW-2R
0.032
22
0.040
27
0.038
26
0.037
25
0.037
25
0.040
27
0.038
26
0.040
27
MW-2R to
MW-13
0.060
41
0.064
44
0.062
42
0.062
42
0.064
43
0.062
42
0.062
42
0.062
42
MW-13 to
MW-10
0.013
9
0.014
10
0.014
9
0.014
10
0.013
9
0.014
9
0.014
9
0.014
10
MW-2R to
MW-15
0.068
46
0.072
49
0.069
47
0.070
48
0.072
49
0.068
47
0.069
47
0.069
47

Winston-Salem City/County Utilities | Assessment Monitoring Report Results
9
4.0 Results
4.1. Detected Groundwater Constituents
Detections of benzene and PCE above the groundwater standards triggered assessment
monitoring for well MW-2R. The trends of selected containments detected in MW-2R above the
SWSL are shown on Figure 3.

Figure 3 - Selected Groundwater Detections in MW-2R
A summary of the constituents detected during this period, along with the NCDEQ solid waste
section limits (SWSL) and applicable North Carolina state maximum concentration levels, are
provided in Table 6. There were twenty-nine detections above the 2L standard; these detections
comprised seven parameters in twelve locations during this event. Methylene chloride was only
detected above the SWSL at MW-7 during this event. Barium, cobalt, mercury, and
trichloroflouromethane were also detected between the two standards. Three herbicides were
detected by method EPA 8151 below the PRL in the samples from MW-2R, MW-15 and the
equipment blank.
Appendix A contains historical summaries of detections by well and by parameter. The complete
laboratory analyses are provided in Appendix B. A Microsoft Excel file containing the analysis
data in NCDEQ electronic data deliverable format is include as part of Appendix D.
0.1
1
10
100
1000
10000
100000
1000000
1-Jan-09 1-Jan-10 1-Jan-11 1-Jan-12 1-Jan-13 1-Jan-14 1-Jan-15 1-Jan-16 1-Jan-17 1-Jan-18 1-Jan-19Detected Concentration (ug/L)Date Sample Collected
MW-2R Groundwater Detections
OSR Construction & Demolition Landfill Permit 34-12
Total Dissolved Solids
Sulfate
Chloride
Manganese
Iron
Barium
Selenium
Chromium
Methylene Chloride
Lead
Benzene
bis(2-Ethylhexyl)phthalate
Heptachlor
delta-BHC
Chloromethane
alpha-BHC
4,4'-DDT
Winston-Salem City/County Utilities | Assessment Monitoring Report Results
10
The constituents detected above 2L groundwater standards for this event are as follows.
• Appendix I constituents
o Iron in MW-2R, MW-3R, MW-4R, MW-10, MW-11, MW-15 and all four surface
water samples.
o Manganese in MW-2R, MW-3R, MW-4R, MW-10, MW-11, MW-12, MW-15 and
all four surface water samples.
o Benzene in MW-2R.
o Tetrachloroethene in MW-2R.
o Vinyl Chloride in MW-2R.
o Total dissolved solids in MW-2R, MW-4R, MW-10 and SW-3
• All SVOCs, Herbicides and Pesticides were non detect or below the PRL during this
sampling event.
4.2. Landfill Gas
Landfill gas is measured at MW-2R and wells in the vicinity of MM-1 during each groundwater
event. These results do not indicate the presence of methane gas in these wells. The results do
indicate the presence of carbon dioxide above ambient levels in MM-1 and MW-13. The City is
responsible for quarterly sampling of all methane monitoring wells and the related reporting,
which is not included in this document.
Table 5 - Methane Gas Readings
Date Time ID # CH4 (%) CO2 (%) O2 (%) Balance (%)
30-May-17 10:29 MM-1 0.0% 4.3% 16.4% 79.3%
30-May-17 10:47 MW-13 0.0% 0.3% 21.0% 78.7%
30-May-17 10:38 MW-15 0.0% 0.4% 20.9% 78.7%
30-May-17 10:20 MW-1R 0.0% 0.2% 21.3% 78.5%
30-May-17 10:32 MW-2R 0.0% 0.5% 21.1% 78.3%
16-Nov-17 09:45 MM-1 0.0% 5.2% 16.8% 78.0%
16-Nov-17 09:00 MW-13 0.0% 4.3% 17.9% 77.8%
16-Nov-17 09:41 MW-15 0.0% 0.3% 20.9% 78.8%
16-Nov-17 09:54 MW-1R 0.0% 0.1% 20.7% 79.2%
16-Nov-17 09:48 MW-2R 0.0% 0.5% 20.6% 78.9%
Highlighted cells are outside of normal atmospheric ranges

Winston-Salem City/County Utilities | Assessment Monitoring Report Summary & Recommendations
11
5.0 Summary & Recommendations
The full round of Appendix II parameters were not sampled for at all wells. The wells were
resampled for the missing parameters on December 28, 2017. The results of the December
sampling will be presented after they are reported by the laboratory.
The level of detections from this event are generally consistent with previous events. No
Appendix II constituents have been detected above the 2L standard since the November 2016
event. The two herbicides detected in November, were below the SWSL. No pesticides or semi-
volatile organic compounds were detected in 2017. The pesticides, heptachlor and heptachlor
epoxide that were last detected during the November 2016 sampling event were not detected in
this current November 2017 event.
Table 6 and Table 7 depict a summary of exceedances and field parameters for the November
2017 Sampling Event.

Winston-Salem City/County Utilities | Assessment Monitoring Report Summary & Recommendations
12

This page intentionally left blank.

Winston-Salem City/County Utilities | Assessment Monitoring Report Summary & Recommendations
13
Table 6 - Event Lab Summary – November 2017
SWSL 2L units Row Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4 Equipment Blank
EPA 300.0
250000 250000 µg/L Sulfate 122000 179000 7830 13400 4740 64100 16200 62400 4960 59600 2730 9920 33800 26700
EPA 6010
10 10 µg/L Arsenic 9
100 700 µg/L Barium 260 323 278 198 53.2 152 46.5 196 106 89.8 84.2 116 214 17.1 47.5 65.4 217 110
1 4000 µg/L Beryllium 0.52 0.54
10 10 µg/L Chromium 4 2.7 3.2 10.2 4.9 7.2 4.6 3.8 3.8 4.7 3.2
10 1000 µg/L Cobalt 23.5 9.4 93 22.5 7.2
300 300 µg/L Iron 43.1 3010 78700 365 37.9 25 37.6 166 3270 29300 125 193 93.9 1050 4900 1740 1720 802
10 15 µg/L Lead 3.4
50 50 µg/L Manganese 11.8 10600 5440 1050 4.2 43 3.6 10.6 13800 1590 169 17.9 18.4 317 461 196 7340 1020
50 100 µg/L Nickel 20.3 7.5 7.6 5.5
NE NE µg/L Sodium 15200 77600 2380 65500 13500 15300 9860 14900 138000 12300 13200 9740 17100 19800 17000 11600 35500 25600 539
25 300 µg/L Vanadium 4.9 3.6
10 1000 µg/L Zinc 5.8 5 5.3 7.1 8.3
EPA 7470
0.2 1 µg/L Mercury 0.23
EPA 8151
2 50 µg/L 2,4,5-TP (Silvex) 0.072
2 70 µg/L 2,4-D 0.27
25 0.3 µg/L Pentachlorophenol 0.018
EPA 8260
5 6 µg/L 1,1-Dichloroethane 0.48 1.4
1 6 µg/L 1,4-Dichlorobenzene 0.46
100 NE µg/L 4-Methyl-2-pentanone (MIBK) 1.1
100 6000 µg/L Acetone 12.1
1 1 µg/L Benzene 2.6 0.38 0.52
5 70 µg/L Chloroform 0.44
1 3 µg/L Chloromethane 0.12
5 70 µg/L cis-1,2-Dichloroethene 0.62 0.6 1.1 0.23
5 1000 µg/L Dichlorodifluoromethane 1.2 3.9
5 500 µg/L m&p-Xylene 1.4 1.1
1 5 µg/L Methylene Chloride 4.6
NE NE µg/L o-Xylene 0.68 0.97
1 0.7 µg/L Tetrachloroethene 1.8
NE NE µg/L Tetrahydrofuran 28 20.1 131
1 3 µg/L Trichloroethene 0.93
1 2000 µg/L Trichlorofluoromethane 1.5 1.6 1.2 0.52 0.87 0.71 0.32
1 0.03 µg/L Vinyl chloride 1.4
SM 2320B
NE NE µg/L Alkalinity, Total as CaCO3 71400 670000 78900 461000 33500 80400 28200 27900 520000 130000 73800 44600 63500 110000 43600 57600 477000 192000
SM 4500-Cl-E
NE 250000 µg/L Chloride 9290 47600 2650 49200 16200 7390 3860 4430 163000 13000 10400 4770 3620 89800 35700 15200 33800 36800
SM 4500-S2D
1000 NE µg/L Sulfide 127
SM 2540C
NE 500000 µg/L Total Dissolved Solids 153000 918000 164000 862000 144000 175000 82000 136000 1430000 218000 219000 90000 142000 370000 123000 125000 600000 317000
Note - To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks.

Winston-Salem City/County Utilities | Assessment Monitoring Report Summary & Recommendations
14
Table 7 - Event Field Summary – November 2017
Field Parameters MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
µmhos/cm
Field Specific Conductance 208.3 1393 394.2 1209 176.8 288.4 77.4 160 1989 348.3 299.8 111.4 172.7 624 211 181 959 509.1
mg/L
Oxygen, Dissolved 0.6 2.09 0.3 0.23 5.95 0.5 4.2 6.3 0.1 0.1 0.34 4.3 3.3 4.36 6.6 7.8 3 7.5
mV
REDOX 158.6 -10.1 -109.6 48.5 70.4 135.5 166.3 206.8 -44.7 -43 60.9 182.2 215.5 65.2 -121.9 -50.3 -19 -2.7
NTU
Turbidity 1.1 11.87 7.6 8.94 0.92 0.1 0.4 7.9 9.3 8.9 1.61 2.8 2.4 98.53 4.96 8.66 14.79 3.5
Std. Units
Field pH 5.6 6.3 6.4 6.2 6.1 5.6 5.6 5.5 6.3 6.1 6.1 5.6 5.5 6.4 7.4 7.1 6.7 7.1
feet
Static Water Level 34.72 8.22 20.34 8.92 11.42 36.61 17.73 52.89 12.12 4.33 5.31 8.96 51.95 39.37
Total Well Depth 60 21 27 20 30 48 27 60 21 20 15.7 20 60 50.85
deg C
Field Temperature 17.2 13.1 15.5 16.2 16.5 16.3 16.3 15.3 16.3 16.4 16.5 17.2 16.1 16 8 10.3 7.9 8.1

Winston-Salem City/County Utilities | Assessment Monitoring Report Appendix A – Summary of Groundwater Monitoring Results

A
Appendix A – Summary of
Groundwater Monitoring Results
A-1 Appendix II Detections (8 pages)
A-2 Detections by Well Location (15 pages)
A-3 Detections by Date (43 pages)

This page intentionally left blank.
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11Herbicides2 50 µg/L 2,4,5-TP (Silvex)2 50 µg/L MW-2R 0.072 0.14 0.232 70 µg/L 2,4-D2 70 µg/L MW-2R 0.43 1.12 70 µg/L MW-15 0.27Pesticides0.1 0.1 µg/L 4,4'-DDD0.1 0.1 µg/L MW-70.130.1 0.1 µg/L MW-150.0620.1 0.1 µg/L SW-30.0790.1 0.1 µg/L SW-40.110.0620.1 0.1 µg/L 4,4'-DDT0.1 0.1 µg/L MW-2R0.540.1 0.1 µg/L MW-4R0.140.1 0.1 µg/L MW-110.050.1 0.1 µg/L SW-30.090.1 0.1 µg/L SW-40.0540.05 2 µg/L Aldrin0.05 2 µg/L MW-2R0.120.05 0.006 µg/L alpha-BHC0.05 0.006 µg/L MW-2R0.120.05 0.019 µg/L beta-BHC0.05 0.019 µg/L MW-70.10.05 0.019 µg/L delta-BHC0.05 0.019 µg/L MW-2R0.180.05 0.019 µg/L MW-4R0.0690.002 0.002 µg/L Dieldrin0.002 0.002 µg/L MW-70.11 0.0810.1 40 µg/L Endosulfan I0.1 40 µg/L MW-7 0.150.1 40 µg/L MW-10 0.17MCLc:\pwworking\tpa\d0269489\W-S GW Revised.xlsb1 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL0.1 42 µg/L Endosulfan II0.1 42 µg/L MW-4R0.120.1 42 µg/L SW-30.071 0.0850.1 42 µg/L SW-40.0660.1 2 µg/L Endrin0.1 2 µg/L MW-2R0.270.1 2 µg/L SW-10.080.1 2 µg/L Endrin aldehyde0.1 2 µg/L MW-2R0.23 0.280.1 2 µg/L SW-40.0610.05 0.008 µg/L Heptachlor0.05 0.008 µg/L MW-2R0.480.05 0.008 µg/L MW-100.21 0.120.075 0.004 µg/L Heptachlor epoxide0.075 0.004 µg/L MW-70.12 0.0660.075 0.004 µg/L MW-100.17 0.0931 40 µg/L Methoxychlor1 40 µg/L MW-2R0.83SemiVOCs10 NE µg/L 2,4-Dinitrotoluene10 NE µg/L MW-2R 5.910 NE µg/L 2,6-Dinitrotoluene10 NE µg/L MW-2R 8.110 40 µg/L 3&4-Methylphenol(m&p Cresol)10 40 µg/L SW-33.620 NE µg/L 3,3'-Dichlorobenzidine20 NE µg/L SW-23.610 NE µg/L 3-Methylcholanthrene10 NE µg/L SW-22.910 0.05 µg/L Benzo(a)anthracene10 0.05 µg/L MW-1R1.410 0.05 µg/L SW-21.1c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb2 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL10 0.005 µg/L Benzo(a)pyrene10 0.005 µg/L MW-131.110 0.005 µg/L SW-22.510 0.05 µg/L Benzo(b)fluoranthene10 0.05 µg/L MW-13110 0.05 µg/L SW-22.810 200 µg/L Benzo(g,h,i)perylene10 200 µg/L MW-3R 110 200 µg/L MW-111.310 200 µg/L MW-121.210 200 µg/L MW-131.510 200 µg/L SW-21.810 0.5 µg/L Benzo(k)fluoranthene10 0.5 µg/L SW-22.515 3 µg/L bis(2-Ethylhexyl)phthalate15 3 µg/L MW-1R2.415 3 µg/L MW-2R1.115 3 µg/L MW-3R5.515 3 µg/L MW-5R115 3 µg/L MW-91315 3 µg/L MW-149.815 3 µg/L SW-21.110 5 µg/L Chrysene10 5 µg/L MW-1R1.510 5 µg/L SW-21.110 0.005 µg/L Dibenz(a,h)anthracene10 0.005 µg/L MW-3R110 0.005 µg/L MW-131.210 0.005 µg/L SW-22.110 100 µg/L Di-n-octylphthalate10 100 µg/L MW-8 5.610 100 µg/L MW-12 5.6c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb3 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL10 0.05 µg/L Indeno(1,2,3-cd)pyrene10 0.05 µg/L MW-3R1.110 0.05 µg/L MW-121.210 0.05 µg/L MW-131.510 0.05 µg/L SW-22.2VOCs1 200 µg/L 1,1,1-Trichloroethane1 200 µg/L MW-70.825 6 µg/L 1,1-Dichloroethane5 6 µg/L MW-2R 0.48 0.48 0.53 0.49 1.1 0.83 1.3 1.2 1.2 1.1 1.2 1.15 6 µg/L MW-7 1.4 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.84 1.2 1.2 1.9 3.85 350 µg/L 1,1-Dichloroethene5 350 µg/L MW-2R36.6 38.75 350 µg/L MW-153.15 350 µg/L SW-40.581 0.4 µg/L 1,2-Dichloroethane1 0.4 µg/L MW-2R 0.241 6 µg/L 1,4-Dichlorobenzene1 6 µg/L MW-2R 0.46 0.39 0.38 0.450 NE µg/L 2-Hexanone50 NE µg/L MW-2R0.4850 NE µg/L MW-10 0.69 0.9650 NE µg/L SW-2 1.850 NE µg/L SW-4 3.1100 NE µg/L 4-Methyl-2-pentanone (MIBK)100 NE µg/L MW-10 1.1 2.8 2.5 2.6 5.6 2.2c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb4 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL100 6000 µg/L Acetone100 6000 µg/L Equipment Blank 18.35.5100 6000 µg/L GP-B-1 (12-16)3.6100 6000 µg/L MW-2R 10.3 20.3 3.7100 6000 µg/L MW-3R 21.4100 6000 µg/L MW-4R 11100 6000 µg/L MW-5R 18.4100 6000 µg/L MW-7 15.7100 6000 µg/L MW-8 15.83.8100 6000 µg/L MW-10 12.1 22.5 14.1 11.8100 6000 µg/L MW-11 21.1100 6000 µg/L MW-12 12.1100 6000 µg/L MW-13 17.3100 6000 µg/L MW-14 14.7100 6000 µg/L MW-15 13.2100 6000 µg/L SW-1 11.22.2100 6000 µg/L SW-24100 6000 µg/L SW-3 16.2100 6000 µg/L SW-4 161 1 µg/L Benzene1 1 µg/L MW-2R2.6 2.1 2.2 1.7 1.5 1.7 2.5 1.8 1.9 1.4 1.3 1.5 2 1.6 1.31 1 µg/L MW-4R 0.38 0.42 0.28 0.271 1 µg/L MW-7 0.38 0.43 0.42 0.26 0.291 1 µg/L MW-10 0.52 0.83 0.46 0.441 1 µg/L SW-3 0.42 0.54 0.32 0.88 0.34 0.25100 700 µg/L Carbon disulfide100 700 µg/L MW-10 2 5.210 3000 µg/L Chloroethane10 3000 µg/L MW-2R 2.110 3000 µg/L MW-71.3c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb5 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL5 70 µg/L Chloroform5 70 µg/L GP-B-1 (12-16)0.985 70 µg/L MW-2R0.16 0.26 0.365 70 µg/L MW-15 0.44 0.4 0.44 0.7 0.44 0.26 0.49 0.77 0.63 0.49 1.45 70 µg/L SW-40.971 3 µg/L Chloromethane1 3 µg/L MW-2R 0.251 3 µg/L MW-4R0.151 3 µg/L MW-7 0.131 3 µg/L MW-11 0.231 3 µg/L MW-120.211 3 µg/L MW-140.241 3 µg/L SW-2 0.125 70 µg/L cis-1,2-Dichloroethene5 70 µg/L MW-1R 0.62 0.38 0.25 70 µg/L MW-2R 0.6 0.51 0.47 0.26 0.5 0.38 0.41 0.26 0.25 0.33 0.46 0.265 70 µg/L MW-7 1.1 1.1 1.1 0.77 0.8 0.73 0.73 0.37 0.54 0.72 0.62 0.5 0.67 0.715 70 µg/L MW-10 0.23 0.2 0.33 0.355 70 µg/L SW-3 0.265 1000 µg/L Dichlorodifluoromethane5 1000 µg/L MW-2R 0.265 1000 µg/L MW-7 0.62 15 1000 µg/L MW-9 1.2 1.5 0.88 0.76 0.28 0.285 1000 µg/L MW-12 0.235 1000 µg/L MW-14 3.9 3.6 2.3 3.6 2.11 600 µg/L Ethylbenzene1 600 µg/L MW-1R 0.381 600 µg/L MW-10 0.53 0.55 0.4 1 0.735 500 µg/L m&p-Xylene5 500 µg/L MW-2R0.66 0.745 500 µg/L MW-7 1.4 1.2 2.2 1.8 0.84 1.5 1.1 0.96 1.45 500 µg/L MW-10 1.1 1.2 2.1 0.68 1.2 1.1c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb6 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL1 5 µg/L Methylene Chloride1 5 µg/L Equipment Blank61.1 1.8 3.21 5 µg/L MW-1R 2.31 5 µg/L MW-2R 4.4 1.3 2.3 3.7 3.7 3 4.2 4.5 3.2 3.5 4.11 5 µg/L MW-3R 3.4 2.31 5 µg/L MW-4R 2.91 5 µg/L MW-5R 3.21 5 µg/L MW-7 4.6 3.1 4.2 3.79.53.9 2.1 2.91 5 µg/L MW-8 1.11 5 µg/L MW-10 2.8 1.21 5 µg/L MW-11 1.41 5 µg/L MW-12 2 21 5 µg/L MW-14 1.61 5 µg/L MW-15 2.41 5 µg/L SW-1 21 5 µg/L SW-2 3.11 5 µg/L SW-3 11 5 µg/L SW-4 1.210 6 µg/L Naphthalene10 6 µg/L MW-2R0.86 1.3 1.6 1.9NE NE µg/L o-XyleneNE NE µg/L MW-2R 0.33 0.31 0.54 0.54 0.63 1 1.2 0.84NE NE µg/L MW-7 0.68 0.46 0.63 0.47 0.27 0.4 0.36 0.27 0.39NE NE µg/L MW-10 0.97 1 2.1 0.43 0.85 0.651 0.7 µg/L Tetrachloroethene1 0.7 µg/L MW-2R1.81.8 1.3 0.95 1.2 2 1.8 2.2 1.5 1.8 1.71.8 1.6 1.41 0.7 µg/L MW-70.481 0.7 µg/L MW-140.61NE NE µg/L TetrahydrofuranNE NE µg/L Equipment Blank3.2NE NE µg/L MW-2R 28 36.3 39.1 49.6 35.8 34.6 79.2 72.6 99.6 111 93.2 152197 274 226NE NE µg/L MW-4R9.3 13.6 3.5 7 5.8 15.9 11.8 11.7 8.5 13.5 8.8NE NE µg/L MW-7 20.132 21.7 13.5 17.7 14.1 8.8 5.2 13.7 24.2 26 18.9c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb7 of 8
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsNov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCLNE NE µg/L MW-10 131 182 237 6.1 120 145 106 18.6 5NE NE µg/L MW-11 4.54.4 12.1NE NE µg/L MW-12 11.4 26.8 12.4NE NE µg/L MW-1318.6NE NE µg/L MW-15 12 16.8 27.3 19.8 16.9 15.5 21.4 14.7 7.4 6.3NE NE µg/L SW-2 18.4NE NE µg/L SW-3 6.3 3.3 10.2 9.7 18.9 5.1 4.8 4.5NE NE µg/L SW-4 3.5 3.6 4.1 4.41 600 µg/L Toluene1 600 µg/L MW-2R0.271 600 µg/L MW-100.270.631 600 µg/L SW-20.521 3 µg/L Trichloroethene1 3 µg/L MW-2R 0.93 1 1.2 0.71 0.66 0.79 0.85 0.71 0.89 0.68 0.77 0.820.88 0.651 2000 µg/L Trichlorofluoromethane1 2000 µg/L GP-A-7 (20.5-24.5)0.251 2000 µg/L MW-2R 1.50.71 1 1.5 2.4 3.7 12 12.1 16.9 20.920.1 31.61 2000 µg/L MW-7 1.6 0.91 1.5 0.92 1.4 0.79 1.2 0.62 0.47 0.25 0.290.34 0.481 2000 µg/L MW-9 1.2 1.4 1 1.3 1.1 0.98 0.96 0.47 0.69 0.36 0.490.42 0.261 2000 µg/L MW-100.2 0.33 0.38 0.490.68 0.521 2000 µg/L MW-12 0.521 2.8 1.4 0.82 0.22 0.321 2000 µg/L MW-14 0.87 0.75 0.58 1.1 0.54 0.59 0.57 0.341 2000 µg/L MW-15 0.71 2.1 4.4 5.1 4.8 4.4 3.9 5.3 7.6 4.3 8.1 7.31 2000 µg/L SW-4 0.320.27 0.251.41 0.03 µg/L Vinyl chloride1 0.03 µg/L MW-2R1.41 0.72 0.75 0.7 1.2 0.955 500 µg/L Xylenes (Total)5 500 µg/L MW-2R0.98 1.65 500 µg/L MW-71.2 0.79c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb8 of 8
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14µg/L
MW-1R
NE NE µg/L Alkalinity, Total as CaCO3 71400 68600 64300 54900 48100 39600 37600
10 10 µg/L Arsenic
100 700 µg/L Barium 260 272 241 228 207 164 142
10 0.05 µg/L Benzo(a)anthracene
15 3 µg/L bis(2-Ethylhexyl)phthalate
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 9290 8860 9630 9000 8510 7640 7090
10 10 µg/L Chromium 4
10 5 µg/L Chrysene
5 70 µg/L cis-1,2-Dichloroethene 0.62 0.38 0.2
10 70 µg/L Cyanide 4.4
1 600 µg/L Ethylbenzene 0.38
300 300 µg/L Iron 43.1 54.8 96.2 78.8 82.8 85.8
10 15 µg/L Lead
50.0 50.0 µg/L Manganese 11.8 12.5 7.3 7.2 2.8 2.9
0.2 1 µg/L Mercury 0.23
1 5 µg/L Methylene Chloride 2.3
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 15200 15800 14600 13300 13200 11600 10600
250000 250000 µg/L Sulfate 1380 1080 1070 1700 1720
1 600 µg/L Toluene
NE 500000 µg/L Total Dissolved Solids 2E+05 165000 154000 138000 78000 133000 120000
10 1000 µg/L Zinc 5.5 5.7 5.6
MW-2R
5 6 µg/L 1,1-Dichloroethane 0.48 0.48 0.53 0.49 1.1
5 350 µg/L 1,1-Dichloroethene
1 0.4 µg/L 1,2-Dichloroethane 0.24
1 6 µg/L 1,4-Dichlorobenzene 0.46 0.39 0.38 0.4
2 50 µg/L 2,4,5-TP (Silvex)0.072 0.14
270µg/L2,4-D 0.43
10 NE µg/L 2,4-Dinitrotoluene 5.9
10 NE µg/L 2,6-Dinitrotoluene 8.1
100 4000 µg/L 2-Butanone (MEK)
50 NE µg/L 2-Hexanone
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 10.3
0.05 2 µg/L Aldrin
NE NE µg/L Alkalinity, Total as CaCO3 7E+05 587000 571000 482000 440000 358000 453000
0.05 0.006 µg/L alpha-BHC
6 1000 µg/L Antimony 4.7
10 10 µg/L Arsenic
100 700 µg/L Barium 323 323 272 324 279 287 339
1 1 µg/L Benzene 2.6 2.1 2.2 1.7 1.5 1.7 2.5
15 3 µg/L bis(2-Ethylhexyl)phthalate
1 2 µg/L Cadmium
NE 250000 µg/L Chloride 47600 50400 47600 47700 48700 44200 49800
10 3000 µg/L Chloroethane 2.1
5 70 µg/L Chloroform
1 3 µg/L Chloromethane 0.25
10 10 µg/L Chromium 2.7 2.8 2.6 3.4
MCL
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
µg/L
MW-1R
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
bis(2-Ethylhexyl)phthalate
Carbon disulfide
Chloride
Chromium
Chrysene
cis-1,2-Dichloroethene
Cyanide
Ethylbenzene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Toluene
Total Dissolved Solids
Zinc
MW-2R
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
1,4-Dichlorobenzene
2,4,5-TP (Silvex)
2,4-D
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Butanone (MEK)
2-Hexanone
4,4'-DDT
Acetone
Aldrin
Alkalinity, Total as CaCO3
alpha-BHC
Antimony
Arsenic
Barium
Benzene
bis(2-Ethylhexyl)phthalate
Cadmium
Chloride
Chloroethane
Chloroform
Chloromethane
Chromium
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-0930000 28100 29800 26300 27100 27500
124 106 109 91.7 93.8 82.6 84.7 85.4 85.3 92.8 74.3
1.4
2.4
5600 5880 5910 5320 5350
1.4 0.96 1.4 2 0.88
1.5
52.9
0.51 0.29 0.48
10800 9940 9080 9180 9440 7670
91000 103000 84000 95000 93000 95000
0.83 1.3 1.2 1.2 1.1 1.2 1.1
36.6 38.7
0.23
1.1
0.48
0.54
20.3 3.7
0.12
344000 349000 363000 277000 196000 219000 165000
0.12
5.4
324 311 324 335 366 351 273 223 103 80.7 88.5
1.8 1.9 1.4 1.3 1.5 2 1.6 1.3
1.1
50500 56700 50000 64000 61500 62400 39900
0.16 0.26 0.36
5.4 0.49 1.2 1.6
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
µg/L
MW-1R
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
bis(2-Ethylhexyl)phthalate
Carbon disulfide
Chloride
Chromium
Chrysene
cis-1,2-Dichloroethene
Cyanide
Ethylbenzene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Toluene
Total Dissolved Solids
Zinc
MW-2R
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
1,4-Dichlorobenzene
2,4,5-TP (Silvex)
2,4-D
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Butanone (MEK)
2-Hexanone
4,4'-DDT
Acetone
Aldrin
Alkalinity, Total as CaCO3
alpha-BHC
Antimony
Arsenic
Barium
Benzene
bis(2-Ethylhexyl)phthalate
Cadmium
Chloride
Chloroethane
Chloroform
Chloromethane
Chromium
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-015.8
85 90.3 105 81 94 82 78 48 95 96.3 460 120 100 130 280
0.64 0.49 2 3.5 4.3 2.3 5 22
22 10
5.5
0.62 0.43
21
98.8 102 107 79 90 52 62 43 52 55 60 56 140 100 160
1.9
3.4
0.5 0.79 2.2 2.1 16
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
µg/L
MW-1R
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
bis(2-Ethylhexyl)phthalate
Carbon disulfide
Chloride
Chromium
Chrysene
cis-1,2-Dichloroethene
Cyanide
Ethylbenzene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Toluene
Total Dissolved Solids
Zinc
MW-2R
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
1,4-Dichlorobenzene
2,4,5-TP (Silvex)
2,4-D
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Butanone (MEK)
2-Hexanone
4,4'-DDT
Acetone
Aldrin
Alkalinity, Total as CaCO3
alpha-BHC
Antimony
Arsenic
Barium
Benzene
bis(2-Ethylhexyl)phthalate
Cadmium
Chloride
Chloroethane
Chloroform
Chloromethane
Chromium
Old Salisbury Road Landfill (C&D)Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-9687 150 110 130 150 160 100 290 100 180 224
28 23
6.6 6.6 5.2 7.8 12 49 11 36
12 6
0.2 1.8
13
86
11
280 61 180 120 150 1100 190 340 200 160 350
3
16 3.9 3 14 7.8 210 34 43 4912
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
5 70 µg/L cis-1,2-Dichloroethene 0.6 0.51 0.47 0.26 0.5
10 1000 µg/L Cobalt 23.5 20.6 16.5 18 17.4 20.3 25
10 1000 µg/L Copper 6.3 9.6
10 70 µg/L Cyanide 5.1 7.5 4.2
0.05 0.019 µg/L delta-BHC
5 1000 µg/L Dichlorodifluoromethane 0.26
0.1 2 µg/L Endrin
0.1 2 µg/L Endrin aldehyde
0.05 0.008 µg/L Heptachlor
300 300 µg/L Iron 3010 3870 1780 4360 3080 9560 2580
10 15 µg/L Lead 3.3
5 500 µg/L m&p-Xylene
50 50 µg/L Manganese 10600 9200 8570 10900 9010 11900 9880
0.2 1 µg/L Mercury
NS NS µg/L Methane
1 40 µg/L Methoxychlor
1 5 µg/L Methylene Chloride 4.4 1.3 2.3 3.7
10 6 µg/L Naphthalene
50 100 µg/L Nickel 20.3 17 18.5 17.9 18 17 25.9
NS NS µg/L Nitrogen, Ammonia
NE NE µg/L o-Xylene 0.33
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 77600 72400 70200 61500 61400 51400 58300
250000 250000 µg/L Sulfate 1E+05 110000 121000 115000 115000 98400 117000
1 0.7 µg/L Tetrachloroethene 1.8 1.8 1.3 0.95 1.2 2
NE NE µg/L Tetrahydrofuran 28 36.3 39.1 49.6 35.8 34.6 79.2
5.5 200 µg/L Thallium 5.1
1 600 µg/L Toluene 0.27
NE 500000 µg/L Total Dissolved Solids 9E+05 796000 831000 769000 806000 632000 769000
1 3 µg/L Trichloroethene 0.93 1 1.2 0.71 0.66 0.79 0.85
1 2000 µg/L Trichlorofluoromethane 1.5 0.71 1 1.5 2.4
25 300 µg/L Vanadium 11.9 11.4
1 0.03 µg/L Vinyl chloride 1.4 1 0.72 0.75 0.7 1.2
5 500 µg/L Xylenes (Total)
10 1000 µg/L Zinc 5.8 8.7 16.8
MW-3R
100 6000 µg/L Acetone 21.4
NE NE µg/L Alkalinity, Total as CaCO3 78900 114000 133000 87800 102000 107000 177000
10 10 µg/L Arsenic 9 5.5 3.9 3.3
100 700 µg/L Barium 278 309 297 278 271 214 221
10 200 µg/L Benzo(g,h,i)perylene 1
15 3 µg/L bis(2-Ethylhexyl)phthalate
1 2 µg/L Cadmium
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 2650 2520 2050 2470 2990 2990 2940
10 10 µg/L Chromium
10 1000 µg/L Cobalt 9.4 11.5 9.8 10.2 9.1 10.1 13.3
10 1000 µg/L Copper 6.2
10 70 µg/L Cyanide 4.4 4.7 10.4
10 0.005 µg/L Dibenz(a,h)anthracene 1
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.1
300 300 µg/L Iron 78700 89300 86400 77200 68200 56000 49700
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
delta-BHC
Dichlorodifluoromethane
Endrin
Endrin aldehyde
Heptachlor
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methane
Methoxychlor
Methylene Chloride
Naphthalene
Nickel
Nitrogen, Ammonia
o-Xylene
Selenium
Silver
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Thallium
Toluene
Total Dissolved Solids
Trichloroethene
Trichlorofluoromethane
Vanadium
Vinyl chloride
Xylenes (Total)
Zinc
MW-3R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-090.38 0.41 0.26 0.25 0.33 0.46 0.26
22.8 19.2 18.2 15.2 14.8 11.8
0.18
0.27
0.23 0.28
0.48
1650 766 877 1730 3190 2980
0.66 0.74
7950 8710 7880 8400 8280 7920
1280
0.83
3.7 3 4.2 4.5 3.2 3.5 4.1 4.2
0.86 1.3 1.6 1.9
20.6 27.1 20.7 21.8 22.3 20.9
0.12
0.31 0.54 0.54 0.63 1 1.2 0.84
16.5
5.2 5 2.5 0.85 0.67 0.68 0.58
59700 46200 45700 43400 38400 31800 27200
136000 128000 115000 79500 95000 96300
1.8 2.2 1.5 1.8 1.7 1.8 1.6 1.4
72.6 99.6 111 93.2 152 197 274 226
549000 654000 589000 564000 531000 498000
0.71 0.89 0.68 0.77 0.82 0.88 0.65
3.7 12 12.1 16.9 20.9 20.1 31.6 36.1 21.9 22.2
5.5
0.95
0.98 1.6
12.2 21.1 24.5 35.2 33.3
155000 155000 175000 142000 150000 155000
8.9 4
205 201 216 173 228 237 301 302 314 289 252
5.5
0.82
26.1 3.3
3260 3620 3860 3920
53.5 64.1 16.4
7.1 8.1 9.1 6.5
38200 31300 34100 25300 41500 40300
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
delta-BHC
Dichlorodifluoromethane
Endrin
Endrin aldehyde
Heptachlor
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methane
Methoxychlor
Methylene Chloride
Naphthalene
Nickel
Nitrogen, Ammonia
o-Xylene
Selenium
Silver
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Thallium
Toluene
Total Dissolved Solids
Trichloroethene
Trichlorofluoromethane
Vanadium
Vinyl chloride
Xylenes (Total)
Zinc
MW-3R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-017
0.34
1.2 0.93
7.4 8.4
231 293 273 310 230 290 300 300 340 270 200 220 13 370 400
2
0.63 2.3 3.7 2.3 15 19
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
delta-BHC
Dichlorodifluoromethane
Endrin
Endrin aldehyde
Heptachlor
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methane
Methoxychlor
Methylene Chloride
Naphthalene
Nickel
Nitrogen, Ammonia
o-Xylene
Selenium
Silver
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Thallium
Toluene
Total Dissolved Solids
Trichloroethene
Trichlorofluoromethane
Vanadium
Vinyl chloride
Xylenes (Total)
Zinc
MW-3R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Old Salisbury Road Landfill (C&D)Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-968.9 6.5 6.9 68 19 31 14 8 26
0.4
13
6
18 31 5.9
950 1500 300 52 1400 860 620 800 790 1230
50 100 24 77 25 16 28 20 9
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
10 15 µg/L Lead 3.4 3.4 3.5 3.8 2.7 2.7
50 50 µg/L Manganese 5440 6460 5920 6800 7100 7980 9380
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 3.4 2.3
10 20 µg/L Selenium 5 5.5
10 20 µg/L Silver
NE NE µg/L Sodium 2380 2240 2450 2310 2590 2770
250000 250000 µg/L Sulfate 1530 1800 2200 3000 3740
100 2000000 µg/L Tin
NE 500000 µg/L Total Dissolved Solids 2E+05 133000 168000 188000 137000 182000 191000
25 300 µg/L Vanadium 9.9 8.8 2.8
10 1000 µg/L Zinc 8.7
MW-4R
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 11
NE NE µg/L Alkalinity, Total as CaCO3 5E+05 315000 454000 99000 144000 117000 286000
10 10 µg/L Arsenic
100 700 µg/L Barium 198 343 255 210 184 306 305
1 1 µg/L Benzene 0.38 0.42
Butylbenzylphthalate 1.7
1 2 µg/L Cadmium
NE 250000 µg/L Chloride 49200 35800 58400 13800 16900 22200 50500
1 3 µg/L Chloromethane
10 10 µg/L Chromium 3.2 3.2
10 1000 µg/L Cobalt 93 59.9 100 10.5 28.3 15.2 82
10 1000 µg/L Copper 2.8
10 70 µg/L Cyanide 4.2 4.3
0.05 0.019 µg/L delta-BHC
0.1 42 µg/L Endosulfan II
300 300 µg/L Iron 365 302 214 1550 312 292 126
10 15 µg/L Lead
50 50 µg/L Manganese 1050 801 1320 515 407 315 1040
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 2.9
50 100 µg/L Nickel 7.5 5.8 8 3.2 3.7 2.8 7.2
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 65500 42100 71000 14500 23800 23000 55400
250000 250000 µg/L Sulfate 2E+05 125000 193000 48700 70300 72700 143000
NE NE µg/L Tetrahydrofuran 9.3 13.6 3.5 7 5.8 15.9
NE 500000 µg/L Total Dissolved Solids 9E+05 552000 824000 241000 161000 304000 692000
25 300 µg/L Vanadium 4.2 2.7
10 1000 µg/L Zinc 5.8 8.6 8.4 17.8 5.9 7.5 7.2
MW-5R
100 6000 µg/L Acetone 18.4
NE NE µg/L Alkalinity, Total as CaCO3 33500 32300 32700 30800 32300 28600 24000
10 10 µg/L Arsenic
100 700 µg/L Barium 53.2 57.1 55.9 55.9 92.7 54 58.2
15 3 µg/L bis(2-Ethylhexyl)phthalate
1 2 µg/L Cadmium
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 16200 15100 16400 15300 16200 15700 15500
1 3 µg/L Chloromethane
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Tin
Total Dissolved Solids
Vanadium
Zinc
MW-4R
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Butylbenzylphthalate
Cadmium
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
delta-BHC
Endosulfan II
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Vanadium
Zinc
MW-5R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chloromethane
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-099260 9990 9630 11600 9310 7310
0.6 0.45 1 0.29
4230 3400 5070 5420 6860
5.8
187000 193000 175000 172000 168000 180000
10.5
0.14
222000 224000 203000 174000 64300 143000
264 296 375 400 407 328 126 335 55.9 334 58.3
0.28 0.27
29700 36500 33700 34500 33200 29200
0.15
1.3 0.68 1.3 5.4 1.2
46.6 49.4 35.3 35.5 21.5 15
5.9
0.069
0.12
89.5 158 344 145 368
4.8
641 688 496 541 370 257
5.3
11.5
0.88 1.3 2.4
39700 42600 42600 43600 40400 35300
85200 113000 97600 73600 98700 61800
11.8 11.7 8.5 13.5 8.8
445000 496000 413000 435000 374000 345000
13.6
31900 31700 34800 31200 134000 32800
4.2
54.4 53.9 57.7 53.4 57.5 85.2 63.7 53 54.3 66.8 52.6
1
13900 15200 16200 16100 16100 16400
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Tin
Total Dissolved Solids
Vanadium
Zinc
MW-4R
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Butylbenzylphthalate
Cadmium
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
delta-BHC
Endosulfan II
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Vanadium
Zinc
MW-5R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chloromethane
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-0114 21 35
11.8 4.9 18.1 24
1.5 0.87
9.2 12
263 172 287 200 220 220 180 150 140 380 97 94 86 61 900
0.58 0.4 14 2.6 5.5 5 95
18 5.3 6 36
2.6 0.94
5.1 5 7
56.157.570.6585857 545380 76657265150610
2.7
5.4
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Tin
Total Dissolved Solids
Vanadium
Zinc
MW-4R
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Butylbenzylphthalate
Cadmium
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
delta-BHC
Endosulfan II
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Vanadium
Zinc
MW-5R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chloromethane
Old Salisbury Road Landfill (C&D)Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-9653 80 40 39 32 26 27 15 15
0.2 0.7
5.6 7.5
550 350 570 860 950 2000 850 650 280 720 595
7
38 28 60 110 300 130 55 47 21
14 8.1 9.5 40 50 76 43 29 12 16 17
0.36 0.21 0.3 1.7
10
6
150
55
270 400 200 200 240 480 820 610 330 620 1000
25
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
10 10 µg/L Chromium 10.2 4.6 5.8 5.1 4.8 4.8
10 1000 µg/L Cobalt 2.5
10 70 µg/L Cyanide 4.4 5.1
300 300 µg/L Iron 37.9 68.4 87.8 32600 113 221
10 15 µg/L Lead
50 50 µg/L Manganese 4.2 1890 2.6
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 3.2
10 20 µg/L Silver
NE NE µg/L Sodium 13500 13900 14200 13100 11300 13100 13700
250000 250000 µg/L Sulfate 7830 7740 8450 7620 7430 8000 8180
NE 500000 µg/L Total Dissolved Solids 1E+05 156000 145000 154000 104000 166000 163000
25 300 µg/L Vanadium 4.9 4.4 5 4.2 3.7 4.3 5.6
10 1000 µg/L Zinc 7.3
MW-6R
10 10 µg/L Arsenic
100 700 µg/L Barium
10 10 µg/L Chromium
10 15 µg/L Lead
0.2 1 µg/L Mercury
MW-7
1 200 µg/L 1,1,1-Trichloroethane
5 6 µg/L 1,1-Dichloroethane 1.4 1.3 1.5 1.2 0.91 1.1 1.3
0.1 0.1 µg/L 4,4'-DDD
100 6000 µg/L Acetone 15.7
NE NE µg/L Alkalinity, Total as CaCO3 80400 85000 80100 71700 67300 64100 62400
10 10 µg/L Arsenic
100 700 µg/L Barium 152 163 140 129 140 122 111
1 1 µg/L Benzene 0.38 0.43 0.42 0.26 0.29
1 4000 µg/L Beryllium 0.58
0.05 0.019 µg/L beta-BHC
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 7390 5290 4820 4430 6050 4340 4300
10 3000 µg/L Chloroethane
1 3 µg/L Chloromethane 0.13
10 10 µg/L Chromium
5 70 µg/L cis-1,2-Dichloroethene 1.1 1.1 1.1 0.77 0.8 0.73 0.73
10 70 µg/L Cyanide
5 1000 µg/L Dichlorodifluoromethane 0.62 1
0.002 0.002 µg/L Dieldrin
0.1 40 µg/L Endosulfan I 0.15
0.075 0.004 µg/L Heptachlor epoxide
300 300 µg/L Iron 25 25.2 76.5
10 15 µg/L Lead
5 500 µg/L m&p-Xylene 1.4 1.2 2.2 1.8 0.84 1.5 1.1
50 50 µg/L Manganese 43 51.9 35.6 28.8 33.6 27.1 22.9
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 4.6 3.1 4.2 3.7 9.5 3.9 2.1 2.9
NE NE µg/L o-Xylene 0.68 0.46 0.63 0.47 0.27 0.4 0.36
10 20 µg/L Silver
NE NE µg/L Sodium 15300 17800 16200 16400 15700 16300 16600
250000 250000 µg/L Sulfate 13400 6720 3800 2930 10100 1850 1360
1 0.7 µg/L Tetrachloroethene 0.48
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Chromium
Cobalt
Cyanide
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
MW-6R
Arsenic
Barium
Chromium
Lead
Mercury
MW-7
1,1,1-Trichloroethane
1,1-Dichloroethane
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
beta-BHC
Carbon disulfide
Chloride
Chloroethane
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cyanide
Dichlorodifluoromethane
Dieldrin
Endosulfan I
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
o-Xylene
Silver
Sodium
Sulfate
Tetrachloroethene
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-095.6 5.2 14.7 7.6 5.8 5 8.6 5.2
123 126 102 209 3540
6.1 43.5
0.57 0.16 0.46 0.6 0.28
13600 13800 13000 14500 14200 13300
8060 8310 11200 8400 7910 7020
167000 154000 131000 157000 149000 139000
13
11.4 15.3
0.82
0.81 0.9 0.84 1.2 1.2 1.9 3.8
0.13
51900 51600 63500 51900 50200 47700
3.4
90.8 98.8 115 95.1 100 97.1 104 100 99.3 104 86.9
0.1
12.5
3600 5160 5340 3810
1.3
0.55 0.65
0.37 0.54 0.72 0.62 0.5 0.67 0.71
5
0.11 0.081
0.12 0.066
0.96 1.4
15.5 19.4 24.9 17.4 10.2 12.7
0.27 0.39
0.84 0.23 0.56 0.88 0.42
14200 13000 14300 13900 13700 12000
2090
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Chromium
Cobalt
Cyanide
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
MW-6R
Arsenic
Barium
Chromium
Lead
Mercury
MW-7
1,1,1-Trichloroethane
1,1-Dichloroethane
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
beta-BHC
Carbon disulfide
Chloride
Chloroethane
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cyanide
Dichlorodifluoromethane
Dieldrin
Endosulfan I
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
o-Xylene
Silver
Sodium
Sulfate
Tetrachloroethene
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-015.3 5.6 8.4 6.4 6.2 6.2 3.5 5.6 14 7.3 8.7 9.5 7.4 23 140
5.1 13
0.4
0.78 0.56
16
28 25 24 41 180 530
2.2 2.4 3.2 26 95
7.6 38
8.6 17
99 95.7 101 89 76 74 60 53 63 180 820 130 210 84 1300
0.91 7.3 4.4 26 150 17 32 6.8 270
24 5.3 6 36
0.24
0.96 0.66 2.6
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Chromium
Cobalt
Cyanide
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
MW-6R
Arsenic
Barium
Chromium
Lead
Mercury
MW-7
1,1,1-Trichloroethane
1,1-Dichloroethane
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
beta-BHC
Carbon disulfide
Chloride
Chloroethane
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cyanide
Dichlorodifluoromethane
Dieldrin
Endosulfan I
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
o-Xylene
Silver
Sodium
Sulfate
Tetrachloroethene
Old Salisbury Road Landfill (C&D)Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-9649 82 8.1 29 38 96 170 16 70 43 96
7.6 7.6 8.2 16 29 69 31 14 20 19
0.8
10
62 41 82 59 160 360 260 300 590 1400
4.1 2.6 2.8 12 33 14 21 10 12
5.8 20 14 14 11 18
1.4
16 45 9.8
1300 2600 360 390 960 1300 1200 1800 750 970 1930
9
210 580 2.5 62 190 350 430 410 180 21 28
26 65 8.7 12 30 36 38 53 23 6 17
0.2 0.4 1.4
10
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
NE NE µg/L Tetrahydrofuran 20.1 32 21.7 13.5 17.7 14.1 8.8
NE 500000 µg/L Total Dissolved Solids 2E+05 175000 153000 137000 78000 145000 138000
1 2000 µg/L Trichlorofluoromethane 1.6 0.91 1.5 0.92 1.4 0.79 1.2
5 500 µg/L Xylenes (Total)
10 1000 µg/L Zinc 5 8.9 5.7 5.2 6.8
MW-8
100 6000 µg/L Acetone 15.8
NE NE µg/L Alkalinity, Total as CaCO3 28200 20800 25800 24800 23200 20000 22800
10 10 µg/L Arsenic 2.6
100 700 µg/L Barium 46.5 42.9 44 38.3 34.4 30 38
NE 250000 µg/L Chloride 3860 3060 2670 1960 2040 1960 1350
10 10 µg/L Chromium 4.9 4.1
10 70 µg/L Cyanide 9.9 4.3 5.1
10 100 µg/L Di-n-octylphthalate 5.6
300 300 µg/L Iron 37.6 48.6 54 529
10 15 µg/L Lead
50 50 µg/L Manganese 3.6 3 2.7 2.9 3.3 3.4 19.9
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 1.1
10 20 µg/L Silver
NE NE µg/L Sodium 9860 9240 9700 8280 7940 6940 7810
250000 250000 µg/L Sulfate 4740 2700 4090 1630 1350 1860
NE 500000 µg/L Total Dissolved Solids 82000 67000 67000 87000 79000 61000 64000
10 1000 µg/L Zinc 5.3 7.1
MW-9
NE NE µg/L Alkalinity, Total as CaCO3 27900 25400 23300 21200 23400 18900 18300
10 10 µg/L Arsenic 3.5
100 700 µg/L Barium 196 207 195 197 186 182 193
15 3 µg/L bis(2-Ethylhexyl)phthalate
NE 250000 µg/L Chloride 4430 4610 4360 6850 4710 4290 3610
10 10 µg/L Chromium 7.2
10 70 µg/L Cyanide 4.7
5 1000 µg/L Dichlorodifluoromethane 1.2 1.5 0.88 0.76
300 300 µg/L Iron 166 149 128 55.9
10 15 µg/L Lead
50 50 µg/L Manganese 10.6 4.6 8.5 6.3 4 3.5 7.6
10 20 µg/L Silver
NE NE µg/L Sodium 14900 15400 15700 14200 14500 14500 14600
250000 250000 µg/L Sulfate 960 3440 1110 2030 2100
NE 500000 µg/L Total Dissolved Solids 1E+05 141000 135000 103000 142000 134000 141000
1 2000 µg/L Trichlorofluoromethane 1.2 1.4 1 1.3 1.1 0.98 0.96
10 1000 µg/L Zinc 5.1 5.3
MW-10
50 NE µg/L 2-Hexanone 0.69 0.96
100 NE µg/L 4-Methyl-2-pentanone (MIBK 1.1 2.8 2.5 2.6 5.6 2.2
100 6000 µg/L Acetone 12.1 22.5 14.1 11.8
NE NE µg/L Alkalinity, Total as CaCO3 5E+05 446000 626000 29000 48200 47300 42200
10 10 µg/L Arsenic 2.6 5.2
100 700 µg/L Barium 106 221 148 292 241 660 262
1 1 µg/L Benzene 0.52 0.83 0.46 0.44
1 4000 µg/L Beryllium 3.2 1.9 2.8 1.4
100 700 µg/L Carbon disulfide 2 5.2
NE 250000 µg/L Chloride 2E+05 318000 202000 9640 47400 51800 2220
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Xylenes (Total)
Zinc
MW-8
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chromium
Cyanide
Di-n-octylphthalate
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Zinc
MW-9
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Chloride
Chromium
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Silver
Sodium
Sulfate
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-10
2-Hexanone
4-Methyl-2-pentanone (MIBK
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
Carbon disulfide
Chloride
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-095.2 13.7 24.2 26 18.9
126000 116000 108000 111000 109000 124000
0.62 0.47 0.25 0.29 0.34 0.48
1.2 0.79
3.8
21300 19700 22800 19500 20100 19600
30.7 25.4 28.5 26.9 27.5 24.4 27.3 26.8 28.8 27.2 25
1800 1510 2070 1860
0.96 0.62 1.4 0.78
136 61.5 60.8 57.8 151
6.8 7
0.1 0.16
6160 5580 6120 6980 6250 5410
2100
50000 61000 51000 58000 52000 81000
15.2 45.4
18300 18400 21700 17200 20100 17400
168 170 174 142 142 141 153 157 134 128 173
13
3610 3950 4300 3560
7.6
0.28 0.28
136 867
6.9 16.6
0.43 0.27 0.32 0.18
12400 13500 12900 13100 12600 11900
3200
107000 124000 100000 118000 123000 128000
0.47 0.69 0.36 0.49 0.42 0.26
31400 26700 32100 25500 413000 21700
132 112 115 101 96.5 91.3 80.7 38.9 46.6 39.1 38.9
13
1820 1790 2040 1800
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Xylenes (Total)
Zinc
MW-8
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chromium
Cyanide
Di-n-octylphthalate
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Zinc
MW-9
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Chloride
Chromium
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Silver
Sodium
Sulfate
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-10
2-Hexanone
4-Methyl-2-pentanone (MIBK
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
Carbon disulfide
Chloride
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-016 36
32.8 24 26.6 30 29 29 26 25 30 480 52 77 48 150 2700
0.97 0.42 2.4 28 3.2 3.8 2 23 94
41 6.7 150
0.1 0.26
0.15 0.13 0.16
124 124 117 140 140 100 100 85 95 240
0.47 14
14
0.36 0.22 0.32
41.9 4240.8527148 46825598
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Xylenes (Total)
Zinc
MW-8
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chromium
Cyanide
Di-n-octylphthalate
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Zinc
MW-9
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Chloride
Chromium
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Silver
Sodium
Sulfate
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-10
2-Hexanone
4-Methyl-2-pentanone (MIBK
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
Carbon disulfide
Chloride
Old Salisbury Road Landfill (C&D)Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-9646 89
2600 4200
92 240
210 400
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
10 10 µg/L Chromium 4.6 4.2 6.4 9.1 3.5 6.7
5 70 µg/L cis-1,2-Dichloroethene 0.23 0.2 0.33 0.35
10 1000 µg/L Cobalt 22.5 21.8 39.5 3.1 3.1 4.8
10 1000 µg/L Copper 16.4 6.3 3.8
10 70 µg/L Cyanide 5.4 4.1 9.8
0.1 40 µg/L Endosulfan I 0.17
1 600 µg/L Ethylbenzene 0.53 0.55 0.4 1 0.73
0.05 0.008 µg/L Heptachlor 0.21 0.12
0.075 0.004 µg/L Heptachlor epoxide 0.17 0.093
300 300 µg/L Iron 3270 2400 2430 11800 3690 3650 1160
10 15 µg/L Lead 4.1 2.6 19.1 8.5 11.6 4.1
5 500 µg/L m&p-Xylene 1.1 1.2 2.1 0.68 1.2 1.1
50 50 µg/L Manganese 13800 8390 12300 530 587 736 130
0.2 1 µg/L Mercury 0.12 0.12 0.29 0.33
1 5 µg/L Methylene Chloride 2.8 1.2
50 100 µg/L Nickel 7.6 6.9 10.7 4.7 3.9 5.9
NE NE µg/L o-Xylene 0.97 1 2.1 0.43 0.85 0.65
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 1E+05 123000 184000 10300 19800 14100 6860
250000 250000 µg/L Sulfate 64100 333000 555000 15800 63600 8770
1000 NE µg/L Sulfide 127 260
NE NE µg/L Tetrahydrofuran 131 182 237 6.1 120 145 106
5.5 200 µg/L Thallium 0.043
100 2000000 µg/L Tin 3.1 8.5
1 600 µg/L Toluene 0.27 0.63
NE 500000 µg/L Total Dissolved Solids 1E+06 1150000 2040000 311000 403000 279000 86000
1 2000 µg/L Trichlorofluoromethane
25 300 µg/L Vanadium 2.7 20 5.6 4.9
10 1000 µg/L Zinc 5.4 5.1 34 27.2 21.2 6.2
MW-11
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 21.1
NE NE µg/L Alkalinity, Total as CaCO3 1E+05 135000 107000 104000 127000 132000 143000
100 700 µg/L Barium 89.8 102 93.1 103 97.2 93.7 96.8
10 200 µg/L Benzo(g,h,i)perylene
NE 250000 µg/L Chloride 13000 13500 14500 14500 14900 14400 15000
1 3 µg/L Chloromethane 0.23
10 10 µg/L Chromium
10 1000 µg/L Cobalt 2.9 2.5 2.6
10 1000 µg/L Copper 2.8
10 70 µg/L Cyanide 4.1 4.2
300 300 µg/L Iron 29300 26700 32400 29400 34600 31400 35700
10 15 µg/L Lead 2.9 3.6
50 50 µg/L Manganese 1590 1720 1670 1820 2020 1990 2030
1 5 µg/L Methylene Chloride 1.4
10 20 µg/L Selenium 5.6
10 20 µg/L Silver
NE NE µg/L Sodium 12300 11700 12000 11200 12000 9460 10000
250000 250000 µg/L Sulfate 16200 14100 17100 15200 19100 15300 12800
1000 NE µg/L Sulfide 130
NE NE µg/L Tetrahydrofuran 4.5
5.5 200 µg/L Thallium 8.8
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
Endosulfan I
Ethylbenzene
Heptachlor
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
Nickel
o-Xylene
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Tin
Toluene
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-11
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Benzo(g,h,i)perylene
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
Iron
Lead
Manganese
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-090.63 0.65
84.3 92.8 218 55.1 424
10.9 7.9 5.1 6.8
0.51
0.12 0.19
5280
18.6 5
63000 66000 46000 63000 49000 89000
0.2 0.33 0.38 0.49 0.68 0.52
0.05
175000 161000 189000 153000 120000 122000
94.3 87.8 87 76.8 70.3 57.5 56.2 48.1 37.6 31.8 28.4
1.3
12400 14000 14200 12900 10800 8480
47.5 65.1
33400 32100 30700 29000 26300 23000
1960 1920 1890 1740 1580 1250
1.2 0.48 0.5
8490 9070 8290 8770 7460 6480
10700 10400 11000 10400 9700 7590
4.4 12.1
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
Endosulfan I
Ethylbenzene
Heptachlor
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
Nickel
o-Xylene
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Tin
Toluene
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-11
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Benzo(g,h,i)perylene
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
Iron
Lead
Manganese
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-0113
6.8
0.2
6.2
28.629.223.1252426 27242847
3.9 3.3
8.7
0.79 0.41 0.39
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
NE 500000 µg/L Total Dissolved Solids 2E+05 226000 189000 236000 281000 239000 228000
25 300 µg/L Vanadium 3.5 3.2 3.6
10 1000 µg/L Zinc
MW-12
100 6000 µg/L Acetone 12.1
NE NE µg/L Alkalinity, Total as CaCO3 73800 64500 72900 55900 41000 19200 40500
10 10 µg/L Arsenic
100 700 µg/L Barium 84.2 113 144 190 95.7 60.9 59.2
10 200 µg/L Benzo(g,h,i)perylene
NE 250000 µg/L Chloride 10400 19700 23300 26000 9000 8070 8240
1 3 µg/L Chloromethane
10 10 µg/L Chromium
10 70 µg/L Cyanide 5.3
5 1000 µg/L Dichlorodifluoromethane 0.23
10 100 µg/L Di-n-octylphthalate 5.6
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
300 300 µg/L Iron 125 714 274 312 523 524 758
50 50 µg/L Manganese 169 134 148 90.8 49.6 9.7 199
1 5 µg/L Methylene Chloride 2 2
50 100 µg/L Nickel 4.4 6.2 5.5 3.2 4.1
10 20 µg/L Silver
NE NE µg/L Sodium 13200 16200 19200 19200 13700 11200 12800
250000 250000 µg/L Sulfate 62400 86100 129000 169000 70800 73600 32800
NE NE µg/L Tetrahydrofuran 11.4 26.8 12.4
5.5 200 µg/L Thallium 0.021
NE 500000 µg/L Total Dissolved Solids 2E+05 288000 286000 382000 234000 163000 135000
1 2000 µg/L Trichlorofluoromethane 0.52 1 2.8 1.4 0.82 0.22
10 1000 µg/L Zinc
MW-13
5 350 µg/L 1,1-Dichloroethene
100 6000 µg/L Acetone 17.3
NE NE µg/L Alkalinity, Total as CaCO3 44600 42400 42300 41000 37100 36900 36200
10 10 µg/L Arsenic 2.6
100 700 µg/L Barium 116 120 91.6 210 71.5 89.3 130
10 0.005 µg/L Benzo(a)pyrene
10 0.05 µg/L Benzo(b)fluoranthene
10 200 µg/L Benzo(g,h,i)perylene
1 4000 µg/L Beryllium 0.52 2.2 0.68 0.66 1.2
NE 250000 µg/L Chloride 4770 4310 4100 4590 3270 3760 5870
10 10 µg/L Chromium 3.8 13.6 2.9 3
10 1000 µg/L Cobalt
10 1000 µg/L Copper 8.5 3.8
10 70 µg/L Cyanide 5
10 0.005 µg/L Dibenz(a,h)anthracene
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
300 300 µg/L Iron 193 58 343 11000 790 1400 2720
10 15 µg/L Lead 8 2.9 5.4
50 50 µg/L Manganese 17.9 9.7 26.7 284 62.1 41.2 55.6
50 100 µg/L Nickel 6.4
10 20 µg/L Silver
NE NE µg/L Sodium 9740 10000 9380 9420 12200 10700 10700
250000 250000 µg/L Sulfate 4960 5670 5390 7280 10100 9330 8660
1000 NE µg/L Sulfide 151
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Total Dissolved Solids
Vanadium
Zinc
MW-12
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
Chloride
Chloromethane
Chromium
Cyanide
Dichlorodifluoromethane
Di-n-octylphthalate
Indeno(1,2,3-cd)pyrene
Iron
Manganese
Methylene Chloride
Nickel
Silver
Sodium
Sulfate
Tetrahydrofuran
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-13
1,1-Dichloroethene
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Beryllium
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Nickel
Silver
Sodium
Sulfate
Sulfide
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09207000 236000 228000 220000 161000 165000
92
45500 39300 29600 40200 37200 40200
2.7
61.1 47.6 50.1 50.5 46.9 60.1 39.1 44.9 40.6 38 34.5
1.2
6180 6230 5820 4900 8200 8030
0.21
2.6 1.1 2.4 2
1.2
348 253 324 1430 539 3030
14.6 86.1 13.2 33.6 15.7 58.3
0.7 0.2 0.39
11000 10500 11100 11000 11600 9980
48000 27400 51800 24200 20500 15300
149000 126000 138000 127000 130000 124000
0.32
30.8
19.8
46400 43200 58700 43900 52200 44500
77.1 106 176 279 144 139 164 176 126 117 79.2
1.1
1
1.5
2.4 3.5 1.4 2.3
3880 5700 3820 6150 5380
7.1 11.8 5.5 3.9 4 1.7 0.8 1.6
6.6
7.6 6.9 6.1
1.2
1.5
232 1330 8610 11300 3760 6140
6.5 7.5 6.4 4.3
34.1 48.8 158 301 91.5 140
0.72 0.4 0.41
11200 11700 19100 14600 16700 20200
8680 9360 7820 9770 9420 9460
106 178
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Total Dissolved Solids
Vanadium
Zinc
MW-12
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
Chloride
Chloromethane
Chromium
Cyanide
Dichlorodifluoromethane
Di-n-octylphthalate
Indeno(1,2,3-cd)pyrene
Iron
Manganese
Methylene Chloride
Nickel
Silver
Sodium
Sulfate
Tetrahydrofuran
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-13
1,1-Dichloroethene
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Beryllium
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Nickel
Silver
Sodium
Sulfate
Sulfide
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-0157.960.547.3316655 77507774
1.8 4 2.1
0.37 0.15 0.26
88.7 64.6 85.6 79 62 65 59 46 57 160
2.2 1.1 2 4.8 9.2
11
0.44 0.21
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
NE NE µg/L Tetrahydrofuran
100 2000000 µg/L Tin 2.5
NE 500000 µg/L Total Dissolved Solids 90000 89000 79000 145000 110000 107000 119000
1 2000 µg/L Trichlorofluoromethane
25 300 µg/L Vanadium 22.6 2.6 3.4 7.1
10 1000 µg/L Zinc 5.7 12.8 40.5 8.6 7.9 13.7
MW-14
100 6000 µg/L Acetone 14.7
NE NE µg/L Alkalinity, Total as CaCO3 63500 55300 59700 50400 51500 45200 42300
10 10 µg/L Arsenic
100 700 µg/L Barium 214 221 188 188 183 179 193
1 4000 µg/L Beryllium 0.54 0.6 0.57 0.83 0.63 0.54 0.6
15 3 µg/L bis(2-Ethylhexyl)phthalate
NE 250000 µg/L Chloride 3620 3260 3410 3470 3930 3510 3720
1 3 µg/L Chloromethane
10 10 µg/L Chromium 4.5
10 1000 µg/L Copper 4.8
10 70 µg/L Cyanide 4.3 5.3
5 1000 µg/L Dichlorodifluoromethane 3.9 3.6 2.3 3.6 2.1
300 300 µg/L Iron 93.9 134 123 312 466 695 2620
10 15 µg/L Lead
50 50 µg/L Manganese 18.4 18.1 13.7 21.6 69.3 25.7 120
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 1.6
50 100 µg/L Nickel 2.7 2.8 2.8 5.3
10 20 µg/L Silver
NE NE µg/L Sodium 17100 16900 16200 15400 15800 14500 14400
250000 250000 µg/L Sulfate 663 1400 1080 1790
1 0.7 µg/L Tetrachloroethene 0.61
5.5 200 µg/L Thallium 0.048
NE 500000 µg/L Total Dissolved Solids 1E+05 130000 118000 85000 135000 131000 119000
1 2000 µg/L Trichlorofluoromethane 0.87 0.75 0.58 1.1 0.54 0.59 0.57
25 300 µg/L Vanadium 5.5
10 1000 µg/L Zinc 6.3 13.3
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Tetrahydrofuran
Tin
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-14
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Beryllium
bis(2-Ethylhexyl)phthalate
Chloride
Chloromethane
Chromium
Copper
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Silver
Sodium
Sulfate
Tetrachloroethene
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-0918.6
113000 114000 87000 144000 110000 159000
18.6
14.6 18.7 7.2 10.8
17.2 37.3 51 20 31.6
37400 32800 35600 28900 30100 30400
163 140 254 160 122 143 125 129 130 242 97.9
9.8
3630 4100 4290 4790
0.24
6.6 6 1.8 2.3 3 10.7 0.4
9.5 5.8
6
142 915 5820 4520 1140 2050
7.2
40.2 110 240 251 170 71
8.6 13.7 12.5
0.74 0.39 0.54
12800 12300 13500 15000 14300 12700
124000 123000 102000 127000 145000 138000
0.34
9.9 8
11.7 27.4 23 12
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Tetrahydrofuran
Tin
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-14
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Beryllium
bis(2-Ethylhexyl)phthalate
Chloride
Chloromethane
Chromium
Copper
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Silver
Sodium
Sulfate
Tetrachloroethene
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-017.3 8.3
583 186 130 210 460 250 120 69 66 170
40.2 4.1 1.7 6.6 35 15 3.9 3.2
26.2 5.2 23 13 5.9 8
0.098 0.44
0.46 0.56 0.48
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
MW-15
5 350 µg/L 1,1-Dichloroethene
2 70 µg/L 2,4-D 0.27
0.1 0.1 µg/L 4,4'-DDD
100 6000 µg/L Acetone 13.2
NE NE µg/L Alkalinity, Total as CaCO3 1E+05 98100 101000 104000 103000 91500 54700
10 10 µg/L Arsenic 4.5
100 700 µg/L Barium 17.1 22.7 14 11 74 105 41.5
NE 250000 µg/L Chloride 89800 104000 98000 94000 113000 98200 146000
5 70 µg/L Chloroform 0.44 0.4 0.44 0.7 0.44 0.26
10 10 µg/L Chromium 5.4 7.6
10 1000 µg/L Copper 2.6 7.1 8.8
10 70 µg/L Cyanide
300 300 µg/L Iron 1050 1740 781 227 8180 10600 233
10 15 µg/L Lead 66.8
50 50 µg/L Manganese 317 359 259 116 297 271 33
1 5 µg/L Methylene Chloride 2.4
50 100 µg/L Nickel 2.7 3.9 4.3
NE NE µg/L Sodium 19800 21600 20200 20100 21800 20300 24000
250000 250000 µg/L Sulfate 59600 58300 58700 63700 70000 65400 43800
1000 NE µg/L Sulfide
NE NE µg/L Tetrahydrofuran 12 16.8 27.3 19.8 16.9 15.5
5.5 200 µg/L Thallium 0.049
NE 500000 µg/L Total Dissolved Solids 4E+05 410000 371000 418000 362000 360000 464000
1 2000 µg/L Trichlorofluoromethane 0.71 2.1 4.4 5.1 4.8 4.4 3.9
25 300 µg/L Vanadium 3.6 5 18.9 24.7
10 1000 µg/L Zinc 7.1 16.2 6.3 5.9 35.4 49 5.3
SW-1
100 6000 µg/L Acetone 11.2
NE NE µg/L Alkalinity, Total as CaCO3 43600 33200 57400 27700 35100 44500 63700
10 10 µg/L Arsenic 3.6 5.9
100 700 µg/L Barium 47.5 86.8 65.9 69.5 65 72.2 276
1 4000 µg/L Beryllium 1.1
1 2 µg/L Cadmium 0.7
NE 250000 µg/L Chloride 35700 49200 26800 26000 21600 31500 19500
10 10 µg/L Chromium 13
10 1000 µg/L Cobalt
10 1000 µg/L Copper 8.6 3.9 16.4
10 70 µg/L Cyanide 4.4 4.7
0.1 2 µg/L Endrin
300 300 µg/L Iron 4900 5040 5660 5520 9830 8870 155000
10 15 µg/L Lead 18.3
50 50 µg/L Manganese 461 804 1050 465 688 1160 1760
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 2
50 100 µg/L Nickel 8.7
10 20 µg/L Selenium 7
10 20 µg/L Silver
NE NE µg/L Sodium 17000 23000 14200 13000 12800 16000 12500
250000 250000 µg/L Sulfate 2730 2530 3410 4320 4460 3690 3130
NE 500000 µg/L Total Dissolved Solids 1E+05 143000 116000 118000 113000 140000 122000
25 300 µg/L Vanadium 4.3 37
10 1000 µg/L Zinc 10.1 7.2 7.5 69.8
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
MW-15
1,1-Dichloroethene
2,4-D
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chloroform
Chromium
Copper
Cyanide
Iron
Lead
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
SW-1
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Beryllium
Cadmium
Chloride
Chromium
Cobalt
Copper
Cyanide
Endrin
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-093.1
0.062
96600 64300 78900 77600 75300
7.1 5.7
8.6 23.8 59.6 143 115
83400 124000 124000 143000 60600
0.49 0.77 0.63 0.49 1.4
6.7 7.2
10.5
5.2
292 239 4140 12300 10000
9.5 7.6
34.7 14 160 317 327
24200 25300 26700 21200 16300
59500 53200 41200 35600 25800
100
21.4 14.7 7.4 6.3
373000 410000 442000 298000 260000
5.3 7.6 4.3 8.1 7.3
8.6 28.6 23.4
17.1 22.7 45.6 51.1
2.2
45200 72700 58000 79700 47200 19600
3.7
65.8 71.1 58.9 63.3 70.4 42.5 69.9 61.9 92.5 77.7 45.6
23700 18100 20600 19700 25300 19100
0.61
9 14.6
0.08
8210 22800 6900 25500 11400 2290
17.5
749 1530 855 1720 1040 130
0.4 0.28 0.62
14500 13000 12400 15500 14300 9390
2820 2190 2700 2090
126000 125000 104000 131000 98000 140000
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
MW-15
1,1-Dichloroethene
2,4-D
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chloroform
Chromium
Copper
Cyanide
Iron
Lead
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
SW-1
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Beryllium
Cadmium
Chloride
Chromium
Cobalt
Copper
Cyanide
Endrin
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-0122.7
23 20
78.2 79.7 70.3 88 54 120 73 750 53 500
0.67 1.2 0.61 4.2 52 3.2 36
57 38
1.1
0.39 0.37 0.51
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
SW-2
50 NE µg/L 2-Hexanone 1.8
20 NE µg/L 3,3'-Dichlorobenzidine
10 NE µg/L 3-Methylcholanthrene
100 6000 µg/L Acetone
NE NE µg/L Alkalinity, Total as CaCO3 57600 46200 58800 32300 43200 33200 2390
10 10 µg/L Arsenic 3.7 17 6.2
100 700 µg/L Barium 65.4 77.5 108 73.1 70 700 171
10 0.05 µg/L Benzo(a)anthracene
10 0.005 µg/L Benzo(a)pyrene
10 0.05 µg/L Benzo(b)fluoranthene
10 200 µg/L Benzo(g,h,i)perylene
10 0.5 µg/L Benzo(k)fluoranthene
1 4000 µg/L Beryllium 3.7 0.64
15 3 µg/L bis(2-Ethylhexyl)phthalate
NE 250000 µg/L Chloride 15200 13800 6190 9720 12500 4050 28200
1 3 µg/L Chloromethane 0.12
10 10 µg/L Chromium 3.8 40.3 3.2
10 5 µg/L Chrysene
10 1000 µg/L Cobalt 5.9 4.4
10 1000 µg/L Copper 81.6 3.2
10 0.005 µg/L Dibenz(a,h)anthracene
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
300 300 µg/L Iron 1740 1790 29900 1510 2070 226000 75000
10 15 µg/L Lead 2.7 75 7.4
50 50 µg/L Manganese 196 304 1160 317 291 1020 1010
0.2 1 µg/L Mercury 0.2
1 5 µg/L Methylene Chloride 3.1
50 100 µg/L Nickel 16.4 3.1
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 11600 11600 10200 8420 11300 8390 17600
250000 250000 µg/L Sulfate 9920 10900 6270 17100 11600 7280 5620
1000 NE µg/L Sulfide 142
NE NE µg/L Tetrahydrofuran 18.4
1 600 µg/L Toluene 0.52
NE 500000 µg/L Total Dissolved Solids 1E+05 129000 106000 113000 105000 125000 117000
25 300 µg/L Vanadium 127 11.6
10 1000 µg/L Zinc 249 28
SW-3
10 40 µg/L 3&4-Methylphenol(m&p Cresol)
0.1 0.1 µg/L 4,4'-DDD
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 16.2
NE NE µg/L Alkalinity, Total as CaCO3 5E+05 251000 520000 161000 210000 118000 389000
100 700 µg/L Barium 217 173 270 114 152 105 206
1 1 µg/L Benzene 0.42 0.54
NE 250000 µg/L Chloride 33800 18400 34000 10500 16300 27000 27000
10 10 µg/L Chromium 3.4
5 70 µg/L cis-1,2-Dichloroethene 0.26
10 1000 µg/L Cobalt 7.2 3 6.8 3.4
10 1000 µg/L Copper 4.4
10 70 µg/L Cyanide 4.6 6
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
SW-2
2-Hexanone
3,3'-Dichlorobenzidine
3-Methylcholanthrene
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Beryllium
bis(2-Ethylhexyl)phthalate
Chloride
Chloromethane
Chromium
Chrysene
Cobalt
Copper
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Toluene
Total Dissolved Solids
Vanadium
Zinc
SW-3
3&4-Methylphenol(m&p Cre
4,4'-DDD
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Benzene
Chloride
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-093.6
2.9
4
41300 48900 48600 44700 44200 26100
59.7 50.1 51.7 46.5 53.4 81 49.2 57.6 59.4 52.1 46.3
1.1
2.5
2.8
1.8
2.5
1.1
10700 11600 10800 10300 11300 10900
0.42
1.1
2.1
2.2
2130 3360 1400 1280 1720 4170
219 152 153 106 157 280
0.081
0.2 0.2 0.36
9840 10300 9160 9990 9890 8650
12700 5490 5090 4240 6180 38300
120000 114000 91000 101000 101000 189000
7.5
13.5
3.6
0.079
0.09
259000 516000 293000 317000 221000 160000
181 348 185 315 179 123
0.32 0.88 0.34 0.25
16900 34800 20000 24300 22800 20900
14.8 14.4 25.3 13 5.5
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
SW-2
2-Hexanone
3,3'-Dichlorobenzidine
3-Methylcholanthrene
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Beryllium
bis(2-Ethylhexyl)phthalate
Chloride
Chloromethane
Chromium
Chrysene
Cobalt
Copper
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Toluene
Total Dissolved Solids
Vanadium
Zinc
SW-3
3&4-Methylphenol(m&p Cre
4,4'-DDD
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Benzene
Chloride
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
Old Salisbury Road Landfill (C&D)Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04Nov-03May-03Dec-02Apr-02Nov-015.5
50.6 50.6 49.4 300 44 150 51 47 65 63
17 4.7
11 7.6
21
0.5 0.26 0.26
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections
Value Column Labels
SWSL 2L units Row Labels Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14MCL
0.1 42 µg/L Endosulfan II
300 300 µg/L Iron 1720 8240 10500 3390 4160 4940 5270
10 15 µg/L Lead 2.7
50 50 µg/L Manganese 7340 4750 8350 2310 3860 1420 5080
1 5 µg/L Methylene Chloride 1
50 100 µg/L Nickel 5.5 3.6 6.8 2.8 2.8 4.8
NE NE µg/L Sodium 35500 24600 38400 14700 20900 18200 29900
250000 250000 µg/L Sulfate 33800 15200 18500 11400 27000 17000 16800
NE NE µg/L Tetrahydrofuran 6.3 3.3 10.2
100 2000000 µg/L Tin 2.8
NE 500000 µg/L Total Dissolved Solids 6E+05 321000 623000 231000 300000 233000 473000
25 300 µg/L Vanadium 5.6 9.7
10 1000 µg/L Zinc 9.6 13.6
SW-4
5 350 µg/L 1,1-Dichloroethene
50 NE µg/L 2-Hexanone 3.1
0.1 0.1 µg/L 4,4'-DDD
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 16
NE NE µg/L Alkalinity, Total as CaCO3 2E+05 187000 240000 148000 187000 242000 140000
100 700 µg/L Barium 110 121 128 113 115 187 82.8
NE 250000 µg/L Chloride 36800 27400 27900 20300 19800 19000 24300
5 70 µg/L Chloroform
10 10 µg/L Chromium 4.7
10 1000 µg/L Cobalt 5.9
10 70 µg/L Cyanide 5.6
0.1 42 µg/L Endosulfan II
0.1 2 µg/L Endrin aldehyde
300 300 µg/L Iron 802 1480 1520 1520 2240 9220 638
50 50 µg/L Manganese 1020 2900 2930 1930 2550 5050 739
1 5 µg/L Methylene Chloride 1.2
50 100 µg/L Nickel 2.5 3.6
NE NE µg/L Sodium 25600 23400 26000 16900 20200 23800 17800
250000 250000 µg/L Sulfate 26700 18200 28600 16600 24900 23500 17600
NE NE µg/L Tetrahydrofuran 3.5 3.6 4.1
NE 500000 µg/L Total Dissolved Solids 3E+05 289000 325000 229000 267000 371000 222000
1 2000 µg/L Trichlorofluoromethane 0.32 0.27
25 300 µg/L Vanadium 3.5 5.9
10 1000 µg/L Zinc 8.3 7.3
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb
Appendix A2
Facility Permit
Historic Detections
Value
Row Labels
Endosulfan II
Iron
Lead
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Tetrahydrofuran
Tin
Total Dissolved Solids
Vanadium
Zinc
SW-4
1,1-Dichloroethene
2-Hexanone
4,4'-DDD
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Chloride
Chloroform
Chromium
Cobalt
Cyanide
Endosulfan II
Endrin aldehyde
Iron
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)May-14Nov-13May-13Nov-12Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-090.071 0.085
8890 11700 9560 16500 9370 3230
4320 8930 3990 5200 3760 1890
12
29900 41100 25000 33800 21300 18500
26300 62500 20100 36400 26400 19800
9.7 18.9 5.1 4.8 4.5
319000 705000 327000 432000 329000 237000
9.8
10.8
0.58
0.11 0.062
0.054
158000 152000 147000 220000 158000 131000
126 101 106 151 136 105
30800 31000 26900 28800 30900 23600
0.97
10.4
0.066
0.061
2520 1790 4180 1640 2140 1060
2250 1080 1650 2430 2420 1290
24400 20100 18200 29000 20000 17900
23500 23000 13200 32300 23600 19500
4.4
257000 270000 255000 349000 272000 234000
0.25 1.4
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb

This page intentionally left blank.
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankNovember-17EPA 300.0µg/L250000 250000 µg/L Sulfate 122000 179000 7830 13400 4740 64100 16200 62400 4960 59600 2730 9920 33800 26700EPA 6010µg/L10 10 µg/LArsenic9100 700 µg/LBarium260 323 278 198 53.2 152 46.5 196 106 89.8 84.2 116 214 17.1 47.5 65.4 217 1101 4000 µg/LBeryllium0.52 0.5410 10 µg/LChromium4 2.73.210.24.9 7.2 4.63.83.84.73.210 1000 µg/LCobalt23.5 9.4 9322.57.2300 300 µg/LIron43.13010 78700 36537.925 37.6 1663270 29300125 193 93.91050 4900 1740 1720 80210 15 µg/LLead3.450 50 µg/LManganese11.810600 5440 10504.243 3.6 10.613800 1590 16917.9 18.4317 461 196 7340 102050 100 µg/LNickel20.37.57.65.5NE NE µg/LSodium15200 77600 2380 65500 13500 15300 9860 14900 138000 12300 13200 9740 17100 19800 17000 11600 35500 2560053925 300 µg/LVanadium4.93.610 1000 µg/LZinc5.85 5.37.18.3EPA 7470µg/L0.2 1 µg/LMercury0.23EPA 8151µg/L2 50 µg/L2,4,5-TP (Silvex)0.0722 70 µg/L2,4-D0.2725 0.3 µg/LPentachlorophenol0.018EPA 8260µg/L5 6 µg/L1,1-Dichloroethane0.481.41 6 µg/L1,4-Dichlorobenzene0.46100 NE µg/L4-Methyl-2-pentanone (MIBK)1.1100 6000 µg/LAcetone12.11 1 µg/LBenzene2.60.380.525 70 µg/LChloroform0.441 3 µg/LChloromethane0.125 70 µg/Lcis-1,2-Dichloroethene0.62 0.61.10.235 1000 µg/LDichlorodifluoromethane1.23.95 500 µg/Lm&p-Xylene1.41.11 5 µg/LMethylene Chloride4.6NE NE µg/Lo-Xylene0.680.971 0.7 µg/LTetrachloroethene1.8NE NE µg/LTetrahydrofuran2820.11311 3 µg/LTrichloroethene0.931 2000 µg/LTrichlorofluoromethane1.51.61.20.520.87 0.710.321 0.03 µg/LVinyl chloride1.4EPA 8270µg/LButylbenzylphthalate1.7SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 71400 670000 78900 461000 33500 80400 28200 27900 520000 130000 73800 44600 63500 110000 43600 57600 477000 192000MCL1/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLSM 2540Cµg/LNE 500000 µg/L Total Dissolved Solids 153000918000164000862000144000 175000 82000 1360001430000218000 219000 90000 142000 370000 123000 125000600000317000SM 4500-Cl-Eµg/LNE 250000 µg/L Chloride 9290 47600 2650 49200 16200 7390 3860 4430 163000 13000 10400 4770 3620 89800 35700 15200 33800 36800SM 4500-S2Dµg/L1000 NE µg/LSulfide127FieldfeetStatic Water Level34.72 8.22 20.34 8.92 11.42 36.61 17.73 52.89 12.12 4.33 5.31 8.96 51.95 39.37Total Well Depth60 21 27 20 3048 27 60 21 20 15.7 20 60 50.85mg/LOxygen, Dissolved0.6 2.09 0.3 0.23 5.950.5 4.2 6.3 0.1 0.1 0.34 4.3 3.3 4.36 6.6 7.8 3 7.5NTUTurbidity1.1 11.87 7.6 8.94 0.920.1 0.4 7.9 9.3 8.9 1.61 2.8 2.4 98.53 4.96 8.66 14.79 3.5Std. UnitsField pH5.6 6.3 6.4 6.2 6.15.6 5.6 5.5 6.3 6.1 6.1 5.6 5.5 6.4 7.4 7.1 6.7 7.1mVREDOX158.6 -10.1 -109.6 48.5 70.4 135.5 166.3 206.8 -44.7 -43 60.9 182.2 215.5 65.2 -121.9 -50.3 -19 -2.7µmhos/cmField Specific Conductance 208.3 1393 394.2 1209 176.8 288.4 77.4 160 1989 348.3 299.8 111.4 172.7 624 211 181 959 509.1°CField Temperature17.2 13.1 15.5 16.2 16.5 16.3 16.3 15.3 16.3 16.4 16.5 17.2 16.1 16 8 10.3 7.9 8.1June-17EPA 300.0µg/L250000 250000 µg/LSulfate110000 12500033300014100EPA 6010µg/L100 700 µg/LBarium323343221 10210 10 µg/LChromium4.210 1000 µg/LCobalt20.659.921.8300 300 µg/LIron38703022400 2670010 15 µg/LLead4.150 50 µg/LManganese92008018390 172050 100 µg/LNickel175.86.9NE NE µg/LSodium72400 42100123000 117005.5 200 µg/LThallium0.04325 300 µg/LVanadium2.710 1000 µg/LZinc8.65.4EPA 8260µg/L5 6 µg/L1,1-Dichloroethane0.481 0.4 µg/L1,2-Dichloroethane0.24100 NE µg/L4-Methyl-2-pentanone (MIBK)2.8100 6000 µg/LAcetone10.31122.5 21.11 1 µg/LBenzene2.1100 700 µg/LCarbon disulfide21 3 µg/LChloromethane0.235 70 µg/Lcis-1,2-Dichloroethene0.510.21 600 µg/LEthylbenzene0.531/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL5 500 µg/Lm&p-Xylene1.2NE NE µg/Lo-Xylene1NE NE µg/LTetrahydrofuran36.39.3182 4.51 600 µg/LToluene0.271 3 µg/LTrichloroethene1SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3587000 315000446000 135000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids796000 5520001150000226000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride50400 3580031800013500FieldfeetStatic Water Level7.888.111.39 3.92Total Well Depth212021 20mg/LOxygen, Dissolved1.90.10.6 0.3NTUTurbidity3.49.9334.3 8.58Std. UnitsField pH6.166.1 5.9mVREDOX-62.6154.4-58.5 -10.4µmhos/cmField Specific Conductance12467561714 354.9°CField Temperature24.314.823 16.6May-17EPA 300.0µg/L250000 250000 µg/LSulfate7740 6720 2700 96086100 5670 663 58300 2530 10900 15200 18200EPA 6010µg/L10 10 µg/LArsenic5.5100 700 µg/LBarium27230957.1 163 42.9 207113 120 221 22.7 86.8 77.5 173 1211 4000 µg/LBeryllium0.610 10 µg/LChromium4.610 1000 µg/LCobalt11.5310 1000 µg/LCopper2.6761300 300 µg/LIron54.88930068.4 25.271458 1341740 5040 1790 8240 148027.110 15 µg/LLead3.418.250 50 µg/LManganese12.5646051.93 4.61349.7 18.1359 804 304 4750 290050 100 µg/LNickel4.42.73.6NE NE µg/LSodium158002240 13900 17800 9240 1540016200 10000 16900 21600 23000 11600 24600 234005.5 200 µg/LThallium0.0210.048 0.049100 2000000 µg/LTin425 300 µg/LVanadium4.4510 1000 µg/LZinc5.58.95.15.716.2 10.14551/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLEPA 8260µg/L5 6 µg/L 1,1-Dichloroethane 1.3100 6000 µg/L Acetone 21.4 18.4 15.7 15.8 12.1 17.3 14.7 13.2 11.2 16.2 16 18.7 18.31 1 µg/LBenzene0.435 70 µg/LChloroform0.45 70 µg/Lcis-1,2-Dichloroethene0.381.15 1000 µg/LDichlorodifluoromethane1.53.65 500 µg/Lm&p-Xylene1.21 5 µg/LMethylene Chloride3.1NE NE µg/Lo-Xylene0.461 0.7 µg/LTetrachloroethene0.61NE NE µg/LTetrahydrofuran3211.4123.51 2000 µg/LTrichlorofluoromethane0.911.410.75 2.1SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 68600 114000 32300 85000 20800 2540064500 42400 55300 98100 33200 46200 251000 187000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 165000 133000 156000 175000 67000 141000288000 89000 130000 410000 143000 129000 321000 289000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride88602520 15100 5290 3060 461019700 4310 3260 104000 49200 13800 18400 27400SM 4500-CN-Eµg/L10 70 µg/LCyanide4.44.49.94.34.44.6FieldfeetStatic Water Level35.0518.4310.6 36.56 15.16 52.824.64 8.7 51.86 38.85Total Well Depth60275048 27 6015.7 20 60 50.85mg/LOxygen, Dissolved1.30.55.40.4 5.4 6.510.3 4.03 3.28 3.06 4.7 6.3 4.3 6NTUTurbidity3.55.33.14.2 1.16 0.49.26 1.75 5.42 23.24 15.12 14.72 7.94 7.13Std. UnitsField pH5.56.35.95.5 5.6 5.55.9 5.6 5.5 6.3 6.5 6.8 6.6 7.3mVREDOX179.6-60182.6 210.2 195 178.8107.5 138.8 147 121 -7.1 -15.2 -49.6 -38.5µmhos/cmField Specific Conductance 209.7392.9175.5 220.7 68.1 159367.4 116.5 173.7 690 250.9 172 549 461°CField Temperature20.320.421.2 19.7 17 19.817.4 16.9 18.4 17.6 21 21 21.2 20.4November-16EPA 300.0µg/L250000 250000 µg/LSulfate1380 121000 1530 193000 8450 3800 4090 344055500017100 129000 5390 1400 58700 3410 6270 18500 28600EPA 6010µg/L10 10 µg/LArsenic3.92.63.6 3.7100 700 µg/LBarium241 272 297 255 55.9 140 44 195 148 93.1 144 91.6 188 14 65.9 108 270 1281 4000 µg/LBeryllium0.580.5710 10 µg/LChromium2.85.84.16.410 1000 µg/LCobalt16.5 9.8 10039.56.81/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL300 300 µg/LIron96.21780 864002141492430 32400274343123781 5660 29900 10500 152010 15 µg/LLead3.52.62.750 50 µg/LManganese7.38570 5920 132035.6 2.7 8.512300 1670 14826.7 13.7259 1050 1160 8350 293050 100 µg/LNickel18.5810.76.26.810 20 µg/LSelenium5NE NE µg/LSodium14600 70200 2450 71000 14200 16200 9700 15700 184000 12000 19200 9380 16200 20200 14200 10200 38400 2600025 300 µg/LVanadium510 1000 µg/LZinc5.78.4 7.35.75.112.86.3EPA 8081µg/L0.05 0.008 µg/LHeptachlor0.210.075 0.004 µg/LHeptachlor epoxide0.17EPA 8260µg/L5 6 µg/L1,1-Dichloroethane0.531.51 6 µg/L1,4-Dichlorobenzene0.39100 NE µg/L4-Methyl-2-pentanone (MIBK)2.5100 6000 µg/LAcetone14.125.41 1 µg/LBenzene2.20.380.420.830.42100 700 µg/LCarbon disulfide5.25 70 µg/LChloroform0.441 3 µg/LChloromethane0.45 70 µg/Lcis-1,2-Dichloroethene0.2 0.471.10.330.265 1000 µg/LDichlorodifluoromethane0.620.882.31 600 µg/LEthylbenzene0.380.555 500 µg/Lm&p-Xylene2.22.11 5 µg/LMethylene Chloride4.2NE NE µg/Lo-Xylene0.632.11 0.7 µg/LTetrachloroethene1.80.48NE NE µg/LTetrahydrofuran39.113.621.723726.816.86.3 3.61 600 µg/LToluene0.521 3 µg/LTrichloroethene1.21 2000 µg/LTrichlorofluoromethane1.512.80.58 4.41 0.03 µg/LVinyl chloride1SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000 72900 42300 59700 101000 57400 58800 520000 240000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 154000831000168000824000145000 153000 67000 1350002040000189000 286000 79000 118000 371000 116000 106000623000325000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride9630 47600 2050 58400 16400 4820 2670 4360 202000 14500 23300 4100 3410 98000 26800 6190 34000 27900SM 4500-CN-Eµg/L10 70 µg/LCyanide5.4FieldfeetStatic Water Level34.35 8.32 20.47 8.88 11.08 36.41 17.1 52.04 12.07 4.37 5.38 9.22 51.5 39.3Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved1.52 1.18 2.9 3.5 5.731.2 7.7 8.26 1.16 4.39 1.34 4.6 4 3.19 3.25 1.91 2.81 6.331/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLNTUTurbidity 0.72 1.51 5.3 7.03 0.31 0.25 0.31 4.61 6.38 5.81 2.97 7.23 1.95 44.5 19.33 34.84 13.52 6.16Std. UnitsField pH 5.6 6.2 6.3 6.1 5.9 5.6 5.7 5.5 6.2 6 5.9 5.7 5.6 6.4 6.4 6.5 6.5 7.2mVREDOX 137.2 24.1 -61.4 176.7 242.9 152 217.5 272 62.3 16.7 175.1 241.4 270.5 177.6 14.7 -57 -23.6 -72.6µmhos/cmField Specific Conductance 202.8 1262 380.4 1204 176 203.1 73.7 167.8 2535 355 463.1 106.2 158.6 609.9 208.3 208.7 1006 549.9°CField Temperature16.6 15.9 15 16 16.3 15.3 16.5 17.1 17.2 16.1 16.7 16.4 17.1 15.2 17.2 21.5 15.6 17June-16EPA 8260µg/L1 5 µg/LMethylene Chloride3.7FieldfeetStatic Water Level34.657.6836.15Total Well Depth602048mg/LOxygen, Dissolved1.70.20.3NTUTurbidity1.44.260.42Std. UnitsField pH5.465.6mVREDOX242.6212.4257.5µmhos/cmField Specific Conductance 194.3981198.4°CField Temperature2215.917May-16EPA 300.0µg/L250000 250000 µg/LSulfate1080 115000 1800 48700 7620 2930 163015800 15200 169000 7280 63700 4320 17100 11400 16600EPA 6010µg/L6 1000 µg/LAntimony4.710 10 µg/LArsenic3.35.2100 700 µg/LBarium228 324 278 210 55.9 129 38.3 197 292 103 190 210 188 11 69.5 73.1 114 1131 4000 µg/LBeryllium3.22.2 0.8310 10 µg/LChromium2.63.2 5.19.113.610 1000 µg/LCobalt18 10.2 10.53.110 1000 µg/LCopper2.816.48.58.6300 300 µg/LIron78.84360 77200 155087.812811800 29400 312 11000 3122275520 1510 3390 152010 15 µg/LLead19.1850 50 µg/LManganese7.210900 6800 51528.8 2.9 6.3530 1820 90.8 28421.6116 465 317 2310 193050 100 µg/LNickel17.93.24.75.5 6.4 2.72.510 20 µg/LSelenium5.5NE NE µg/LSodium13300 61500 2310 14500 13100 16400 8280 14200 10300 11200 19200 9420 15400 20100 13000 8420 14700 16900100 2000000 µg/LTin3.12.52.82.825 300 µg/LVanadium4.2 4.22022.610 1000 µg/LZinc17.85.23440.55.9 7.29.6 7.361/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLEPA 7470µg/L0.2 1 µg/L Mercury0.12EPA 8081µg/L0.1 40 µg/L Endosulfan I0.15EPA 8260µg/L5 6 µg/L 1,1-Dichloroethane 1.21 1 µg/L Benzene1.70.265 70 µg/L Chloroform0.75 70 µg/L cis-1,2-Dichloroethene 0.775 1000 µg/L Dichlorodifluoromethane3.65 500 µg/L m&p-Xylene1.81 5 µg/L Methylene Chloride 2.3 4.4 3.4 2.9 3.29.51.1 2.8 1.4 2 1.6 2.4 2 3.1 1 1.2 2.36NE NE µg/L o-Xylene0.471 0.7 µg/L Tetrachloroethene1.3NE NE µg/L Tetrahydrofuran 49.6 3.5 13.5 6.1 12.4 27.3 3.7 3.21 3 µg/L Trichloroethene 0.711 2000 µg/L Trichlorofluoromethane 0.71 0.92 1.3 1.4 1.1 5.11 0.03 µg/L Vinyl chloride0.72SM 2320Bµg/LNE NE µg/L Alkalinity, Total as CaCO3 54900 482000 87800 99000 30800 71700 24800 21200 29000 104000 55900 41000 50400 104000 27700 32300 161000 148000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 138000769000188000 241000 154000 137000 87000 103000 311000 236000 382000 145000 85000 418000 118000 113000 231000 229000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride9000 47700 2470 13800 15300 4430 1960 6850 9640 14500 26000 4590 3470 94000 26000 9720 10500 20300SM 4500-CN-Eµg/L10 70 µg/LCyanide5.1 4.7 4.24.34.1 4.14.76 5.6December-15FieldfeetStatic Water Level20.86Total Well Depth27mg/LOxygen, Dissolved1NTUTurbidity7.8Std. UnitsField pH6mVREDOX-71.6µmhos/cmField Specific Conductance365.6°CField Temperature13.61/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLNovember-15EPA 300.0µg/L250000 250000 µg/L Sulfate 1070 115000 2200 70300 7430 10100 1350 1110 63600 19100 70800 10100 1080 70000 4460 11600 27000 24900EPA 6010µg/L10 10 µg/LArsenic2.64.5100 700 µg/LBarium207 279 271 184 92.7 140 34.4 186 241 97.2 95.7 71.5 183 74 65 70 152 1151 4000 µg/LBeryllium1.90.68 0.6310 10 µg/LChromium3.55.410 1000 µg/LCobalt17.4 9.1 28.3 2.53.1 2.910 1000 µg/LCopper6.26.3 2.87.1 3.9300 300 µg/LIron82.83080 68200 312 3260048.63690 34600 523 790 466 8180 9830 2070 4160 224010 15 µg/LLead3.88.5650 50 µg/LManganese2.89010 7100 407 189033.6 3.3 4587 202049.662.1 69.3 297 688 291 3860 255050 100 µg/LNickel183.73.93.22.8 3.92.810 20 µg/LSelenium5.6NE NE µg/LSodium13200 61400 2590 23800 11300 15700 7940 14500 19800 12000 13700 12200 15800 21800 12800 11300 20900 202005.5 200 µg/LThallium8.8100 2000000 µg/LTin8.525 300 µg/LVanadium11.9 9.93.75.6 3.52.618.9 4.35.6 3.510 1000 µg/LZinc5.6 5.8 8.7 5.97.127.28.6 6.3 35.4 7.5EPA 7470µg/L0.2 1 µg/LMercury0.12EPA 8081µg/L0.1 40 µg/LEndosulfan I0.170.05 0.008 µg/LHeptachlor0.120.075 0.004 µg/LHeptachlor epoxide0.093EPA 8260µg/L5 6 µg/L1,1-Dichloroethane0.911 6 µg/L1,4-Dichlorobenzene0.3850 NE µg/L2-Hexanone0.69100 NE µg/L4-Methyl-2-pentanone (MIBK)2.6100 6000 µg/LAcetone11.81 1 µg/LBenzene1.55 70 µg/LChloroform0.441 3 µg/LChloromethane0.255 70 µg/Lcis-1,2-Dichloroethene0.260.85 1000 µg/LDichlorodifluoromethane0.2610.760.232.11 600 µg/LEthylbenzene0.45 500 µg/Lm&p-Xylene0.840.681 5 µg/LMethylene Chloride1.3 2.33.91.221.1NE NE µg/Lo-Xylene0.270.431 0.7 µg/LTetrachloroethene0.95NE NE µg/LTetrahydrofuran35.8717.712019.83.31 600 µg/LToluene0.271 3 µg/LTrichloroethene0.661 2000 µg/LTrichlorofluoromethane11.41.10.820.54 4.81 0.03 µg/LVinyl chloride0.751/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLEPA 8270µg/L10 NE µg/L2,4-Dinitrotoluene5.910 NE µg/L2,6-Dinitrotoluene8.110 200 µg/LBenzo(g,h,i)perylene110 0.005 µg/LDibenz(a,h)anthracene110 100 µg/LDi-n-octylphthalate5.65.610 0.05 µg/LIndeno(1,2,3-cd)pyrene1.1SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 35100 43200 210000 187000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 78000806000137000 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 113000 105000 300000 267000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride8510 48700 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 21600 12500 16300 19800SM 4500-CN-Eµg/L10 70 µg/LCyanide7.55.1 4.7 9.8 4.2 5.3 5 5.3FieldfeetStatic Water Level72.25 16.3 43.76 20.31 23.2 76.9 36.73 107.71 24.15 7.17 9.51 17.47 104.89 78.88Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved2.2 2 0.2 3.3 5.90.7 4.4 6.3 0.2 0.1 3.4 1.2 4.8 2.8 5.5 3.5 3.2 7.6NTUTurbidity1 5.6 3 9.6 11 1.6 2.6 295 9.3 8.9 51.6 5.9 154.9 48.7 20.5 9.1 3.2Std. UnitsField pH5.4 6.1 6.3 5.8 5.85.5 5.4 5.3 5.4 5.9 5.8 5.5 5.4 6.2 6.7 6.6 6.4 7mVREDOX34.8 -35.2 -91.6 48.8 52.6 30.9 4 54.3 -77.7 -38.7 -23.3 5.2 49.6 34.8 -78.3 -84.6 -90 -87.1µmhos/cmField Specific Conductance 163.2 1044 211.4 395.9 164.5 196.6 58.4 151.5 365.1 400.8 281.5 108.9 152.1 596.2 92.6 88.6 274.8 247.9°CField Temperature16 15.9 15.2 15.5 15.9 15.3 15.6 15.9 16.5 15.8 16.2 16.2 16.3 15.6 9.4 11.9 8.2 9May-15EPA 300.0µg/L250000 250000 µg/LSulfate1700 98400 3000 72700 8000 1850 1860 2030 8770 15300 73600 9330 1790 65400 3690 7280 17000 23500EPA 6010µg/L10 10 µg/LArsenic17100 700 µg/LBarium164 287 214 306 54 122 30 182 660 93.7 60.9 89.3 179 105 72.2700105 1871 4000 µg/LBeryllium2.80.66 0.543.710 10 µg/LChromium4.86.72.97.640.33.410 1000 µg/LCobalt20.3 10.1 15.24.8 2.55.95.910 1000 µg/LCopper6.33.88.881.6 4.4300 300 µg/LIron9560 56000292 113543650 31400 524 1400 695 10600 8870 226000 4940 922010 15 µg/LLead3.3 2.711.6 2.92.96.8752.750 50 µg/LManganese11900 7980 31527.1 3.4 3.5736 19909.7 41.2 25.7271 1160 1020 1420 505050 100 µg/LNickel172.85.92.8 4.316.4 2.8 3.6NE NE µg/LSodium11600 51400 23000 13100 16300 6940 14500 14100 9460 11200 10700 14500 20300 16000 8390 18200 238001/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL5.5 200 µg/LThallium5.125 300 µg/LVanadium11.4 8.84.34.9 3.23.424.7127 9.7 5.910 1000 µg/LZinc8.77.56.821.27.949249 13.6EPA 7470µg/L0.2 1 µg/LMercury0.290.2EPA 8151µg/L2 50 µg/L2,4,5-TP (Silvex)0.142 70 µg/L2,4-D0.43EPA 8260µg/L5 6 µg/L1,1-Dichloroethane0.491.150 NE µg/L2-Hexanone0.961.83.1100 NE µg/L4-Methyl-2-pentanone (MIBK)5.61 1 µg/LBenzene1.70.290.465 70 µg/LChloroform0.261 3 µg/LChloromethane0.135 70 µg/Lcis-1,2-Dichloroethene0.731 600 µg/LEthylbenzene15 500 µg/Lm&p-Xylene1.51.21 5 µg/LMethylene Chloride2.32.11.5 1.8NE NE µg/Lo-Xylene0.40.851 0.7 µg/LTetrachloroethene1.2NE NE µg/LTetrahydrofuran34.65.814.114516.94.11 600 µg/LToluene0.631 3 µg/LTrichloroethene0.791 2000 µg/LTrichlorofluoromethane1.50.790.980.220.59 4.41 0.03 µg/LVinyl chloride0.7SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 39600 358000 107000 117000 28600 64100 20000 18900 47300 132000 19200 36900 45200 91500 44500 33200 118000 242000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 133000632000182000 304000 166000 145000 61000 134000 279000 239000 163000 107000 131000 360000 140000 125000 233000 371000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride7640 44200 2990 22200 15700 4340 1960 4290 51800 14400 8070 3760 3510 98200 31500 4050 27000 19000FieldfeetStatic Water Level71.44 16.32 42.18 18.28 21.85 75.46 16.85 53.36 23.35 8.07 9.8 8.98 52.23 39.21Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved4.5 1.6 2 2.5 6.80.4 5.7 6.3 1.5 0.3 5.4 2.7 5.2 2 4.5 0.2 6.9 3.5NTUTurbidity1.2 8.8 6.2 12.2 2.21.2 2.3 1.4 246.4 8 7.7 32.7 26.1 81.7 26.5 385.5 42.7 18.6Std. UnitsField pH5.5 6.1 6.1 5.9 5.95.6 5.7 5.5 5.2 6 6 5.7 5.6 6.2 6.3 6.5 6.9 6.5mVREDOX265.1 15.4 -1.1 262.8 244.4 228.8 255.2 206.8 244.7 -34.3 230.6 218.9 221.2 176 11 -79.4 -15.8 -25.5µmhos/cmField Specific Conductance 153.1 985 363.4 422 175.1 194.8 50.9 148.3 297.2 407.8 234.3 115 150.1 611 228.7 185.9 364.2 6031/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL°CField Temperature 18 13.7 15 13.3 14.7 16.7 16.1 17.5 17.1 13.4 14.9 18.7 17.1 17.3 20.4 19.7 17.5 18.2November-14EPA 300.0µg/L250000 250000 µg/LSulfate1720 117000 3740 143000 8180 1360 210012800 32800 8660 43800 3130 5620 16800 17600EPA 6010µg/L10 10 µg/LArsenic2.6 3.55.9 6.2100 700 µg/LBarium142 339 221 305 58.2 111 38 193 262 96.8 59.2 130 193 41.5 276 171 206 82.81 4000 µg/LBeryllium1.41.2 0.61.1 0.641 2 µg/LCadmium0.710 10 µg/LChromium3.44.83 4.5133.210 1000 µg/LCobalt25 13.3 822.64.4 3.410 1000 µg/LCopper9.63.8 4.816.4 3.2300 300 µg/LIron85.82580 49700126 221 76.552955.91160 35700 758 2720 2620233155000 75000 5270 63810 15 µg/LLead2.74.1 3.65.418.37.450 50 µg/LManganese2.99880 9380 10402.6 22.9 19.9 7.6130 2030 199 55.6 120331760 1010 5080 73950 100 µg/LNickel25.97.24.15.38.7 3.1 4.810 20 µg/LSelenium7NE NE µg/LSodium10600 58300 2770 55400 13700 16600 7810 14600 6860 10000 12800 10700 14400 24000 12500 17600 29900 1780025 300 µg/LVanadium2.8 2.7 5.63.67.1 5.537 11.610 1000 µg/LZinc16.87.25.3 6.213.7 13.3 5.3 69.8 28EPA 7470µg/L0.2 1 µg/LMercury0.33EPA 8260µg/L5 6 µg/L1,1-Dichloroethane1.11.31 6 µg/L1,4-Dichlorobenzene0.4100 NE µg/L4-Methyl-2-pentanone (MIBK)2.21 1 µg/LBenzene2.50.420.440.5410 3000 µg/LChloroethane2.15 70 µg/Lcis-1,2-Dichloroethene0.50.730.351 600 µg/LEthylbenzene0.735 500 µg/Lm&p-Xylene1.11.11 5 µg/LMethylene Chloride3.72.9NE NE µg/Lo-Xylene0.330.360.651 0.7 µg/LTetrachloroethene2NE NE µg/LTetrahydrofuran79.215.98.810615.518.4 10.21 3 µg/LTrichloroethene0.851 2000 µg/LTrichlorofluoromethane2.41.20.960.57 3.90.271 0.03 µg/LVinyl chloride1.2SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000 40500 36200 42300 54700 63700 2390 389000 140000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 120000769000191000692000163000 138000 64000 141000 86000 228000 135000 119000 119000 464000 122000 117000 473000 222000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride7090 49800 2940 50500 15500 4300 1350 3610 2220 15000 8240 5870 3720 146000 19500 28200 27000 243001/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLSM 4500-CN-Eµg/L10 70 µg/LCyanide4.4 4.2 10.4 4.3 5.1SM 4500-S2Dµg/L1000 NE µg/LSulfide260 130151142FieldfeetStatic Water Level69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4 10.76 18.48 103.8 79Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved1 0.5 6.3 0.5 50.5 2.3 8.30.5 0.5 0.5 3.8 1.25 0.5 2.11 4.5 8.18NTUTurbidity1.7 3.53 5.2 10 3.61.2 9.1 2 98 9.9 5.2 152 7.8 20.1 363.9 136.9 16.6 28.3Std. UnitsField pH5.6 6.1 6 5.9 65.6 5.7 5.5 5.1 5.9 5.9 5.6 5.6 6.2 6.1 6.3 6.6 6.7mVREDOX194 38 13 158 198 184 224 252 198 -61 101 232 242 182 7 -36 -45 27µmhos/cmField Specific Conductance 138 1150 363 971 184 186 59 161 106 440 203 120 159 647 247 324 885 344°CField Temperature14.8 13.2 13.2 13.7 12.9 13.7 13 12.4 15.3 15.4 15.4 13.8 11.9 16.7 10.8 11.2 12.5 10May-14EPA 300.0µg/L250000 250000 µg/LSulfate136000 4230 85200 806010700 48000 8680 59500 2820 12700 26300 23500EPA 6010µg/L6 1000 µg/LAntimony5.410 10 µg/LArsenic8.9100 700 µg/LBarium124 324 205 264 54.4 90.8 30.7 168 132 94.3 61.1 77.1 163 8.6 65.8 59.7 181 12610 10 µg/LChromium5.610 1000 µg/LCobalt22.846.6914.8300 300 µg/LIron52.91650 3820012333400 348232 142 2928210 2130 8890 252050 50 µg/LManganese7950 9260 6416.1 15.510.9196014.6 34.1 40.2 34.7749 219 4320 225050 100 µg/LNickel20.610 20 µg/LSelenium16.511.5NE NE µg/LSodium10800 59700 39700 13600 14200 6160 124008490 11000 11200 12800 24200 14500 9840 29900 2440010 1000 µg/LZinc11.417.2 11.7EPA 7470µg/L0.2 1 µg/LMercury0.51EPA 8260µg/L5 6 µg/L1,1-Dichloroethane0.830.811 1 µg/LBenzene1.80.280.325 70 µg/LChloroform0.495 70 µg/Lcis-1,2-Dichloroethene0.380.371 5 µg/LMethylene Chloride3.71.1NE NE µg/Lo-Xylene0.311 0.7 µg/LTetrachloroethene1.8NE NE µg/LTetrahydrofuran72.611.85.218.621.49.7 4.41 3 µg/LTrichloroethene0.711/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL1 2000 µg/LTrichlorofluoromethane3.70.620.47 0.20.320.34 5.3SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000 45500 46400 37400 96600 45200 41300 259000 158000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 91000549000187000 445000 167000 126000 50000 107000 63000 207000 149000 113000 124000 373000 126000 120000 319000 257000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride5600 50500 3260 29700 13900 3600 1800 3610 1820 12400 6180 3880 3630 83400 23700 10700 16900 30800FieldfeetStatic Water Level70.78 14.24 37.86 14.47 20.22 74.12 26.82 52.72 11.34 8.55 9.77 17.91 103.61 76.95Total Well Depth60 21 27 20 30 37.05 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved5.3 4.8 6.3 6.2 8.63.8 8.4 8.7 8.3 7.5 8.4 6.8 8.1 5.4 5.5 7.3 2.9 7NTUTurbidity3 11 6 17 106 8 5 4 22 15 147 118 50 51 23 14 33Std. UnitsField pH5.6 5.8 6 5.7 5.75.3 5 5.2 5 6 5.9 5.6 5.5 6.3 6.4 6.8 6.5 6.8mVREDOX411 243 146 374 389 363 389 436 436 27 315 367 437 406 284 252 127 262µmhos/cmField Specific Conductance 137 1040 367 715 194 171 64 155 86 430 243 149 156 623 205 183 649 478°CField Temperature18.4 19.6 18.7 14.8 14.7 17.2 16 17.7 15 14.4 15 16.6 17.7 17.8 21.2 19.7 18.9 19.3November-13EPA 300.0µg/L250000 250000 µg/LSulfate128000 3400 113000 831010400 27400 9360 53200 2190 5490 62500 23000EPA 6010µg/L100 700 µg/LBarium106 311 201 296 53.9 98.8 25.4 170 112 87.8 47.6 106 140 23.8 71.1 50.1 348 10110 1000 µg/LCobalt19.2 53.5 49.447.514.4300 300 µg/LIron766 3130089.5136 136 84.3321002531330 91523922800 3360 11700 179050 50 µg/LManganese8710 9990 68819.4 6.8 6.9 7.91920 86.148.8110141530 152 8930 108050 100 µg/LNickel27.15.312NE NE µg/LSodium9940 46200 42600 13800 13000 5580 135009070 10500 11700 12300 25300 13000 10300 41100 2010025 300 µg/LVanadium5.59.810 1000 µg/LZinc12.217.110.8EPA 8151µg/L2 50 µg/L2,4,5-TP (Silvex)0.232 70 µg/L2,4-D1.1EPA 8260µg/L5 6 µg/L1,1-Dichloroethane1.30.91 1 µg/LBenzene1.90.270.885 70 µg/LChloroform0.775 70 µg/Lcis-1,2-Dichloroethene0.410.545 1000 µg/LDichlorodifluoromethane0.281 5 µg/LMethylene Chloride310 6 µg/LNaphthalene0.861/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLNE NE µg/Lo-Xylene0.541 0.7 µg/LTetrachloroethene2.2NE NE µg/LTetrahydrofuran99.611.713.7514.718.91 3 µg/LTrichloroethene0.891 2000 µg/LTrichlorofluoromethane120.470.69 0.337.60.251 0.03 µg/LVinyl chloride0.95EPA 8270µg/L10 40 µg/L3&4-Methylphenol(m&p Cresol3.6SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 28100 349000 155000 224000 31700 51600 19700 18400 26700 161000 39300 43200 32800 64300 72700 48900 516000 152000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 103000654000193000 496000 154000 116000 61000 124000 66000 236000 126000 114000 123000 410000 125000 114000705000270000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride5880 56700 3620 36500 15200 5160 1510 3950 1790 14000 6230 5700 4100 124000 18100 11600 34800 31000SM 4500-CN-Eµg/L10 70 µg/LCyanide7.1 5.96 5.2FieldfeetStatic Water Level71.87 16.65 45.08 18.63 22.73 76.44 36.08 106.03 24.77 9.1 10.56 18.83 104.66 79.28Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved8.7 0.9 0.7 7.5 5.60.5 10.2 9.2 2.2 0.5 6.5 1.3 6.5 2.8 3 4 2.5 4.3NTUTurbidity1 3 1 12 32 5 11 4 8 9 123 250 21 35 2 57 4Std. UnitsField pH5.6 5.6 5.9 5.8 5.95.5 5.4 5.2 5.2 5.9 5.8 5.4 5.4 6.2 6.2 6.7 6.2 6.8mVREDOX228 68 -8 207 239 200 357 363 327 -66 189 280 355 241 -31 -12 -15 61µmhos/cmField Specific Conductance 104 840 316 678 168 144 48 138 63 385 153 115 123 614 246 134 899 369°CField Temperature18.3 13.8 15.9 17.2 17.4 16.5 15.1 16.3 16.7 16.7 17.1 14.8 16.7 17 13.7 12.7 15.1 12.8May-13EPA 300.0µg/L250000 250000 µg/LSulfate115000 5070 97600 112002100 320011000 51800 7820 41200 2700 5090 20100 13200EPA 6010µg/L100 700 µg/LBarium109 324 216 375 57.7 115 28.5 174 115 87 50.1 176 254 59.6 58.9 51.7 185 1061 4000 µg/LBeryllium2.410 10 µg/LChromium7.1 6.610 1000 µg/LCobalt18.2 64.1 35.365.16.614.625.3 10.410 1000 µg/LCopper7.6 9.5300 300 µg/LIron877 34100158 12661.586792.830700 324 8610 5820 4140 6900 1400 9560 418010 15 µg/LLead6.550 50 µg/LManganese7880 9630 49624.916.6189013.2158 240 160 855 153 3990 165050 100 µg/LNickel20.78.6NE NE µg/LSodium9080 45700 42600 13000 14300 6120 129008290 11100 19100 13500 26700 12400 9160 25000 182001/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL100 2000000 µg/LTin5.825 300 µg/LVanadium14.6 9.9 8.610 1000 µg/LZinc21.1 10.5 13.637.3 27.4 22.7EPA 8260µg/L5 6 µg/L1,1-Dichloroethane1.20.8450 NE µg/L2-Hexanone0.48100 6000 µg/LAcetone20.31 1 µg/LBenzene1.45 70 µg/LChloroform0.635 70 µg/Lcis-1,2-Dichloroethene0.260.725 500 µg/Lm&p-Xylene0.961 5 µg/LMethylene Chloride4.210 6 µg/LNaphthalene1.3NE NE µg/Lo-Xylene0.540.271 0.7 µg/LTetrachloroethene1.5NE NE µg/LTetrahydrofuran1118.524.27.45.11 3 µg/LTrichloroethene0.681 2000 µg/LTrichlorofluoromethane12.10.250.36 0.384.35 500 µg/LXylenes (Total)1.2SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 29800 363000 175000 203000 34800 63500 22800 21700 32100 189000 29600 58700 35600 78900 58000 48600 293000 147000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 84000589000175000 413000 131000 108000 51000 100000 46000 228000 138000 87000 102000 442000 104000 91000 327000 255000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride5910 50000 3860 33700 16200 5340 2070 4300 2040 14200 5820 3820 4290 124000 20600 10800 20000 26900SM 4500-CN-Eµg/L10 70 µg/LCyanide8.15FieldfeetStatic Water Level73 15.54 21.94 17.53 21.44 38.62 31.43 106.24 23.65 8.13 9.59 17.62 104.48 78.61Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved8.3 1.9 6 2.7 7.10.9 7.2 7.4 3.1 6.4 9.3 1.3 6.4 2.5 5 9.5 1.9 5.8NTUTurbidity1 1 1 36 11 1 44 1 6 5 587 446 190 45 11 13 15Std. UnitsField pH5.6 5.8 5.8 5.6 65.3 5.5 5 5.2 6.2 5.8 5.6 5.5 6.1 6.4 7 6.3 6.9mVREDOX263 10 21 246 274 211 260 282 267 -22 185 204 254 224 -13 -10 -53 -31µmhos/cmField Specific Conductance 68 802 217 382 116 106 31 88 43 400 197 136 81 403 208 144 575 367°CField Temperature20.9 19.7 15.7 15.6 15.2 16.3 17.5 18.1 16.3 14.7 14.7 16.5 18.2 17.9 22.4 23 22.4 23.3November-12EPA 300.0µg/L250000 250000 µg/LSulfate79500 5420 73600 8400 209010400 24200 9770 35600 2090 4240 36400 323001/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLEPA 6010µg/L10 10 µg/LArsenic7.1100 700 µg/LBarium91.7 335 173 400 53.4 95.1 26.9 142 101 76.8 50.5 279 160 143 63.3 46.5 315 1511 4000 µg/LBeryllium3.510 10 µg/LChromium11.86 6.710 1000 µg/LCobalt15.235.51310 1000 µg/LCopper6.9 5.8 10.5300 300 µg/LIron1730 25300 34410260.821829000 1430 11300 4520 12300 25500 1280 16500 164010 15 µg/LLead7.59.550 50 µg/LManganese8400 11600 54117.45.1174033.6301 251 317 1720 106 5200 243050 100 µg/LNickel21.813.7NE NE µg/LSodium9180 43400 43600 14500 13900 6980 13100 5280 8770 11000 14600 15000 21200 15500 9990 33800 2900025 300 µg/LVanadium18.7 8 28.610 1000 µg/LZinc24.515.292 30.8 51 23 45.6EPA 8081µg/L0.1 0.1 µg/L4,4'-DDD0.0620.0790.110.002 0.002 µg/LDieldrin0.110.1 42 µg/LEndosulfan II0.120.0710.1 2 µg/LEndrin0.270.080.1 2 µg/LEndrin aldehyde0.230.075 0.004 µg/LHeptachlor epoxide0.12EPA 8260µg/L5 6 µg/L1,1-Dichloroethane1.21.21 1 µg/LBenzene1.30.3410 3000 µg/LChloroethane1.35 70 µg/LChloroform0.160.495 70 µg/Lcis-1,2-Dichloroethene0.250.625 1000 µg/LDichlorodifluoromethane0.281 5 µg/LMethylene Chloride4.510 6 µg/LNaphthalene1.6NE NE µg/Lo-Xylene0.631 0.7 µg/LTetrachloroethene1.8NE NE µg/LTetrahydrofuran93.213.5266.34.81 3 µg/LTrichloroethene0.771 2000 µg/LTrichlorofluoromethane16.90.290.49 0.498.15 500 µg/LXylenes (Total)0.980.79EPA 8270µg/L10 0.05 µg/LBenzo(a)anthracene1.415 3 µg/Lbis(2-Ethylhexyl)phthalate 2.4 1.11139.810 5 µg/LChrysene1.5SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 26300 277000 142000 174000 31200 51900 19500 17200 25500 153000 40200 43900 28900 77600 79700 44700 317000 220000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 95000564000172000 435000 157000 111000 58000 118000 63000 220000 127000 144000 127000 298000 131000 101000 432000 349000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride5320 64000 3920 34500 16100 3810 1860 3560 1800 12900 4900 6150 4790 143000 19700 10300 24300 288001/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLSM 4500-CN-Eµg/L10 70 µg/LCyanide9.1SM 4500-S2Dµg/L1000 NE µg/LSulfide106100FieldfeetStatic Water Level72.24 17.78 45.36 19.26 22.81 77.49 37.56 105.53 25.13 8.94 10.71 18.71 104.68 79.91Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved5.5 1.5 1.2 2.3 6.41.8 9.8 7.3 4.4 0.9 3 2.3 6.4 2.3 8.7 6.7 2.1 6.7NTUTurbidity1 1 25 14 147 1 1 1 25 1 605 329 456 3 1 14 92Std. UnitsField pH5.7 5.8 5.6 5.7 5.85.4 5.7 5.5 5 6.1 5.9 5.5 5.5 6.5 6.1 6.7 6.2 6.8mVREDOX236 77 16 181 245 197 260 352 366 -61 150 246 365 160 -21 -21 -26 83µmhos/cmField Specific Conductance 100 842 283 655 175 147 49 134 63 354 158 136 137 434 261 135 700 523°CField Temperature16 14 15.2 13.3 15.9 14.5 15.6 16 16.3 16 16.1 15.8 15.8 15.5 14.7 12.7 10 12.4April-12EPA 300.0µg/L250000 250000 µg/LSulfate95000 6860 98700 79109700 20500 9420 258006180 26400 23600EPA 6010µg/L10 10 µg/LArsenic5.7100 700 µg/LBarium93.8 366 228 407 57.5 100 27.5 142 96.5 70.3 46.9 144 122 115 70.4 53.4 179 1361 4000 µg/LBeryllium1.410 10 µg/LChromium5.27.210 1000 µg/LCobalt14.8 16.4 21.55.5300 300 µg/LIron3190 41500145 20957.855.126300 539 3760 1140 10000 11400 1720 9370 214010 15 µg/LLead7.650 50 µg/LManganese8280 9310 37010.2158015.791.5 170 327 1040 157 3760 242050 100 µg/LNickel22.312.510 20 µg/LSilver5.2NE NE µg/LSodium9440 38400 40400 14200 13700 6250 126007460 11600 16700 14300 16300 14300 9890 21300 2000025 300 µg/LVanadium7.223.410 1000 µg/LZinc35.22051.1EPA 8081µg/L0.1 0.1 µg/L4,4'-DDD0.130.0620.1 0.1 µg/L4,4'-DDT0.540.140.050.09 0.0540.05 2 µg/LAldrin0.120.05 0.006 µg/Lalpha-BHC0.120.05 0.019 µg/Lbeta-BHC0.10.05 0.019 µg/Ldelta-BHC0.180.0690.002 0.002 µg/LDieldrin0.0810.1 42 µg/LEndosulfan II0.085 0.0660.1 2 µg/LEndrin aldehyde0.280.0610.05 0.008 µg/LHeptachlor0.481/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL0.075 0.004 µg/LHeptachlor epoxide0.0661 40 µg/LMethoxychlor0.83EPA 8260µg/L5 6 µg/L1,1-Dichloroethane1.11.25 350 µg/L1,1-Dichloroethene36.63.11 1 µg/LBenzene1.50.255 70 µg/LChloroform1.40.975 70 µg/Lcis-1,2-Dichloroethene0.330.51 5 µg/LMethylene Chloride3.210 6 µg/LNaphthalene1.9NE NE µg/Lo-Xylene11 0.7 µg/LTetrachloroethene1.7NE NE µg/LTetrahydrofuran1528.818.94.44.51 3 µg/LTrichloroethene0.821 2000 µg/LTrichlorofluoromethane20.97.31.45 500 µg/LXylenes (Total)1.6EPA 8270µg/L20 NE µg/L3,3'-Dichlorobenzidine3.610 NE µg/L3-Methylcholanthrene2.910 0.05 µg/LBenzo(a)anthracene1.110 0.005 µg/LBenzo(a)pyrene1.12.510 0.05 µg/LBenzo(b)fluoranthene12.810 200 µg/LBenzo(g,h,i)perylene1.3 1.2 1.51.810 0.5 µg/LBenzo(k)fluoranthene2.515 3 µg/Lbis(2-Ethylhexyl)phthalate5.51.110 5 µg/LChrysene1.110 0.005 µg/LDibenz(a,h)anthracene1.22.110 0.05 µg/LIndeno(1,2,3-cd)pyrene1.2 1.52.2SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 27100 196000 150000 64300 134000 50200 20100 20100 413000 120000 37200 52200 30100 75300 47200 44200 221000 158000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 93000531000168000 374000 149000 109000 52000 123000 49000 161000 130000 110000 145000 260000 98000 101000 329000 272000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride5350 61500 33200 1610010800 8200 5380 60600 25300 11300 22800 30900SM 4500-CN-Eµg/L10 70 µg/LCyanide6.5SM 4500-S2Dµg/L1000 NE µg/LSulfide178FieldfeetStatic Water Level36.43 7.99 21.01 8.24 10.55 38.23 15.03 52.4 11.92 4.13 5.04 8.92 52.03 39.39Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60 50.85mg/LOxygen, Dissolved5 2.9 0.8 0.7 8.70.8 6.7 7.2 4.8 0.5 5.4 1.6 6.9 2.5 7.1 8.5 4.1 7.7NTUTurbidity14372 172 214815032112211612101/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLStd. UnitsField pH 5.2 5.8 5.8 5.5 5.4 5.5 5.5 5.2 5.2 5.5 6.1 5.9 5.8 6.4 6.5 7.1 6.4 6.5mVREDOX 166 43 -24 156 189 185 176 180 196 -78 166 189 177 121 -6 -36 -62 -23µmhos/cmField Specific Conductance 102 809 329 568 182 149 52 140 66 325 176 144 150 404 194 142 570 454°CField Temperature16.7 15.2 13.8 13 13.9 14.7 14.4 16 14.5 14.2 15.1 15 16.4 16.7 19.9 18 18.5 18.9December-11EPA 300.0µg/L250000 250000 µg/LSulfate61800 702019800 19500EPA 6010µg/L100 700 µg/LBarium82.6328 85.2123 10510 10 µg/LChromium14.710 1000 µg/LCobalt15300 300 µg/LIron368 35403230 106050 50 µg/LManganese25743.51890 1290NE NE µg/LSodium767035300 1330018500 1790025 300 µg/LVanadium1310 1000 µg/LZinc15.3EPA 8260µg/L5 350 µg/L1,1-Dichloroethene0.58SM 2320Bµg/LNE NE µg/LAlkalinity, Total as CaCO3 27500143000 32800160000 131000SM 2540Cµg/LNE 500000 µg/LTotal Dissolved Solids 95000345000 139000237000 234000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride29200 1640020900 23600FieldfeetStatic Water Level36.89.33 11.2Total Well Depth6020 30mg/LOxygen, Dissolved5.42.3 6.25.1 8.3NTUTurbidity240 9014 7Std. UnitsField pH5.85.9 5.76.4 6.7mVREDOX218175 200-1 66µmhos/cmField Specific Conductance 97490 177415 370°CField Temperature15.412.5 15.211.4 11.51/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLNovember-11EPA 300.0µg/L250000 250000 µg/L Sulfate 96300 7590 15300 9460 38300EPA 6010µg/L100 700 µg/L Barium 351 237 97.1 24.4 141 91.3 57.5 60.1 139 143 42.5 811 4000 µg/L Beryllium2.310 10 µg/L Chromium5.510 1000 µg/L Cobalt 11.810 1000 µg/L Copper6.1300 300 µg/L Iron2980 40300151424 23000 3030 6140 2050 2290 417010 15 µg/L Lead6.450 50 µg/L Manganese7920 731012.7 7 6.81250 58.3 140 71 130 28050 100 µg/L Nickel 20.910 20 µg/L Silver 5NE NE µg/L Sodium 31800 12000 5410 11900 6480 9980 20200 12700 9390 865025 300 µg/L Vanadium10.8 7.510 1000 µg/L Zinc 33.3 45.4 31.6 12 13.5EPA 8260µg/L5 6 µg/L 1,1-Dichloroethane 1.2 1.95 350 µg/L 1,1-Dichloroethene 38.7100 6000 µg/L Acetone 3.72.2 4 6.6 5.51 1 µg/L Benzene25 70 µg/L Chloroform 0.265 70 µg/L cis-1,2-Dichloroethene 0.46 0.675 500 µg/L m&p-Xylene 0.661 5 µg/L Methylene Chloride 3.53.2NE NE µg/L o-Xylene 1.21 0.7 µg/L Tetrachloroethene1.8NE NE µg/L Tetrahydrofuran 1971 3 µg/L Trichloroethene 0.881 2000 µg/L Trichlorofluoromethane 20.1 0.34 0.42 0.68SM 2320Bµg/LNE NE µg/L Alkalinity, Total as CaCO3 219000 155000 47700 19600 17400 21700 122000 40200 44500 30400 19600 26100SM 2540Cµg/LNE 500000 µg/L Total Dissolved Solids 498000 180000 124000 81000 128000 89000 165000 124000 159000 138000 140000 189000SM 4500-Cl-Eµg/LNE 250000 µg/LChloride624008480 803019100 10900FieldfeetStatic Water Level36.52 16.58 44.06 9.04 11.1 77.6 17.03 52.19 12.24 7.38 9.19 17.83 52.08Total Well Depth21 2748 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved1.7 3.14 5.8 6.8 4.5 0.6 2 6.9 6.27.7 7.3NTUTurbidity1 43 4 1 2 37 54 223 15436 103Std. UnitsField pH5.9 65.8 5.6 5.6 5.6 6.3 6 5.9 5.86.4 6.61/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLmVREDOX 95 71 207 206 205 223 -148 216 239 218 112 88µmhos/cmField Specific Conductance 762 306 158 48 141 58 289 155 127 139 116 177°CField Temperature 12.7 13.8 12.3 15.2 14.9 14.2 13.5 13 13.3 14.3 10.9 11.5June-11EPA 350.1µg/LNS NS µg/L Nitrogen, Ammonia 0.12EPA 6010µg/LNE NE µg/L Sodium 27200EPA 8260µg/L1 1 µg/L Benzene1.61 0.7 µg/L Tetrachloroethene1.6NE NE µg/L Tetrahydrofuran 274RSK 175µg/LNS NS µg/L Methane 1280SM 2320Bµg/LNE NE µg/L Alkalinity, Total as CaCO3 165000SM 4500-Cl-Eµg/LNE 250000 µg/L Chloride 39900FieldfeetStatic Water Level 8.31Total Well Depth 21mg/LOxygen, Dissolved 4.2NTUTurbidity 3Std. UnitsField pH 5.8mVREDOX 88µmhos/cmField Specific Conductance 698°CField Temperature 19.1May-11EPA 6010µg/L100 700 µg/L Barium 84.7 273 301 126 63.7 104 27.3 153 80.7 56.2 39.1 164 125 69.9 49.210 10 µg/LChromium1.4 5.41.3 7.60.960.632.6 3.9 1.810 20 µg/LSilver0.51 2.5 0.6 0.88 0.57 0.84 0.1 0.43 0.12 1.2 0.7 0.72 0.740.4 0.2EPA 8260µg/L1 200 µg/L1,1,1-Trichloroethane0.825 6 µg/L1,1-Dichloroethane1.13.81/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL100 6000 µg/LAcetone3.81 1 µg/LBenzene1.35 70 µg/LChloroform0.361 3 µg/LChloromethane0.150.210.245 70 µg/Lcis-1,2-Dichloroethene0.260.715 500 µg/Lm&p-Xylene0.741.41 5 µg/LMethylene Chloride4.1NE NE µg/Lo-Xylene0.840.391 0.7 µg/LTetrachloroethene1.4NE NE µg/LTetrahydrofuran22612.118.61 3 µg/LTrichloroethene0.651 2000 µg/LTrichlorofluoromethane31.60.480.26 0.52FieldfeetStatic Water Level35.93 8.17 20.56 8.34 10.44 37.99 15.08 51.11 11.72 4 4.91 8.85 51.45Total Well Depth60 21 27 20 19.5648 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved6.3 3.9 6.3 5.3 93.2 8.7 7.3 7.1 4.3 7.4 5.2 7.86.6 9.1NTUTurbidity55 57 70 96 8540 18 1 4 23 25 177 3950 52Std. UnitsField pH5.8 5.9 6.2 5.7 6.15.6 5.1 5.6 5.5 6.2 6 5.6 5.56.4 6.5mVREDOX263 71 -43 271 141 245 272 265 279 -36 188 245 272-15 23µmhos/cmField Specific Conductance 110 687 409 174 208 193 10 153 55 321 179 171 140295 129°CField Temperature17 16 14.6 14.3 15.5 16.2 16.6 18.7 16.6 15.6 15 15 17.119.7 18.6November-10EPA 6010µg/L100 700 µg/LBarium85.4 223 302 335 53 100 26.8 157 38.9 48.1 44.9 176 12961.9 57.610 10 µg/LChromium0.96 0.490.68 5.8 0.55 0.621.1 4 2.310 15 µg/LLead4.310 20 µg/LSilver0.851.3 0.16 0.23EPA 8260µg/L1 5 µg/LMethylene Chloride4.21 2000 µg/LTrichlorofluoromethane36.1FieldfeetStatic Water Level35.62 8.39 19.97 8.49 10.5 37.48 16.12 50.02 12.04 4.03 4.97 9.04 51Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved6.8 4.3 4.8 3.6 8.14 7.9 7.8 7.8 5.1 4.9 5.2 7.76.7 8.8NTUTurbidity3 6 99 40 31.5 1 1 0.5 80 7 200 247 8Std. UnitsField pH5.13 5.05 5.22 6.16 5.13 5.81 5.56 5.38 5.31 5.91 5.82 5.45 5.426.37 6.09mVREDOX282 99 -14 260 212 261 329 334 329 -27 183 251 3359 60µmhos/cmField Specific Conductance 109 543 369 562 204 191 60 193 42 267 183 168 167307 1831/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL°CField Temperature 16.8 16.3 15.9 16.4 16.2 15.1 17.5 16.2 18.5 17 18.1 17.2 17.214 13.4April-10EPA 8260µg/L1 2000 µg/LTrichlorofluoromethane21.9FieldfeetStatic Water Level7.15Total Well Depth21mg/LOxygen, Dissolved2.7NTUTurbidity2Std. UnitsField pH5.46mVREDOX-7µmhos/cmField Specific Conductance255°CField Temperature14.3March-10EPA 6010µg/L10 10 µg/LArsenic44.23.42.73.7100 700 µg/LBarium85.3 103 314 55.9 54.3 99.3 28.8 134 46.6 37.6 40.6 126 13092.5 59.41 2 µg/LCadmium0.8210 10 µg/LChromium1.4 1.21.3 51.42.4 1.7 310 20 µg/LSilver0.29 0.67 0.450.46 0.560.270.48 0.2 0.4 0.390.28 0.2EPA 8260µg/L1 2000 µg/LTrichlorofluoromethane22.2FieldfeetStatic Water Level36.62 7.16 18.22 8.22 9.99 38.71 13.23 51.31 11.18 3.55 4.15 8.05 51.21Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved5.9 4.8 3.7 4.4 6.12.2 7.2 8.5 7.4 1.9 6.8 5.4 7.96.8 8.8NTUTurbidity2 4 6 45 32 7 6 2 13 31 11 298 13Std. UnitsField pH5.74 5.31 5.61 5.56 5.96 5.55 5.21 5.32 5.18 5.97 5.73 5.5 5.357.05 6.77mVREDOX262 191 31 262 260 213 303 309 300 -60 197 237 29253 82µmhos/cmField Specific Conductance 90 230 330 90 170 160 60 140 40 190 140 120 150230 170°CField Temperature20.7 14.8 16.4 14.6 19.2 16.8 13.7 14.6 17.1 13.4 13 13.6 14.417.1 17.91/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLNovember-09FieldfeetStatic Water Level8.55Total Well Depth20mg/LOxygen, Dissolved2.6NTUTurbidity65Std. UnitsField pH5.23mVREDOX386µmhos/cmField Specific Conductance105°CField Temperature15.9September-09EPA 6010µg/L100 700 µg/L Barium 92.8 80.7 289 334 66.8 104 27.2 128 39.1 31.8 38 117 242 77.7 52.110 10 µg/LChromium25.4 8.6 0.650.810.710 15 µg/LLead4.87.217.510 20 µg/LSilver0.48 0.68 1 2.4 0.6 0.88 0.16 0.32 0.19 0.5 0.39 0.41 0.540.62 0.36EPA 7470µg/L0.2 1 µg/LMercury0.081EPA 8260µg/L5 350 µg/L1,1-Dichloroethene19.8100 700 µg/LCarbon disulfide26.112.5131 5 µg/LMethylene Chloride2.61 2000 µg/LTrichlorofluoromethane18.6FieldfeetStatic Water Level37.16 8.89 22.73 9.59 11.33 39.87 16.7 51.52 12.36 4.48 4.85 9.35 51.28Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved3.6 1 0.5 1.8 6.31 5.4 6.1 6.9 1 2.4 4.1 60.6 8.4NTUTurbidity38 12 40 247 6221 27 28 2 13 19 63 59865 30Std. UnitsField pH5.61 5.65 5.88 5.77 6.11 5.47 5.43 5.45 5.35 6.15 5.83 5.56 5.536.16 6.55mVREDOX334 175 37 259 362 292 342 353 371 -22 197 290 36428 111µmhos/cmField Specific Conductance 107 228 366 391 195 170 60 141 42 171 139 124 147255 148°CField Temperature18.1 18.8 17.6 19.2 16.6 18.9 16.1 16.9 18.9 19.3 19.5 17.9 16.819.8 20.91/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLMarch-09EPA 6010µg/L100 700 µg/L Barium 74.3 88.5 252 58.3 52.6 86.9 25 173 38.9 28.4 34.5 79.2 97.945.6 46.310 10 µg/L Chromium 0.88 1.6 1.2 5.2 0.78 7.6 0.65 2 1.6 0.4 0.61 0.4210 20 µg/L Silver 0.58 0.29 0.28 0.42 0.18EPA 8260µg/L100 700 µg/L Carbon disulfide 3.3FieldfeetStatic Water Level 38.27 8.14 22.29 10.07 11.14 40.61 15.86 52.36 11.7 3.73 4.13 8.34 51.52Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved4.5 2.6 1.3 4.9 6.60.9 7.8 6.4 7.2 2.4 7.1 4.2 8.36.4 8.6Std. UnitsField pH5.7 5.59 5.92 5.51 6.01 5.62 5.38 5.37 5.58 5.84 5.79 5.4 5.56.07 7.01mVREDOX585 198 1 433 517 355 523 466 353 -122 181 241 39053 117µmhos/cmField Specific Conductance 94 222 349 60 175 152 54 115 37 137 114 89 140146 126°CField Temperature15.4 13 14.7 11 13.615 14.8 15.5 13.9 13.5 12.4 12.8 1515.5 15.9December-08EPA 6010µg/L10 10 µg/LArsenic7.3100 700 µg/LBarium85 98.8 231 263 56.199 32.8 124 41.9 28.6 57.9 88.7 58378.2 50.610 10 µg/LChromium0.64 0.50.58 5.3 0.91 0.97 0.472.240.20.6710 15 µg/LLead26.210 20 µg/LSelenium11.88.710 20 µg/LSilver0.62 1.2 1.5 2.6 0.78 0.96 0.15 0.360.79 0.37 0.44 0.460.39 0.5EPA 8260µg/L5 70 µg/LChloroform3.4FieldfeetStatic Water Level38.39 9.13 22.72 11.18 11.78 40.61 17.8 52.11 12.33 4.24 4.51 8.91 51.81Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved4.43 0.64 0.62 0.81 6.83 1.88 6.01 6.19 6.73 0.35 2.52 4.2 6.685.58 8.4Std. UnitsField pH5.79 5.76 5.79 5.88 6.08 5.64 5.85 5.7 5.73 6.33 5.98 5.68 5.815.04 6.19mVREDOX217 185 45 178 197 220 199 203 222 -79 -30 190 215145 88µmhos/cmField Specific Conductance 93 218 268 422 176 152 53 117 35 133 118 84 135196 130°CField Temperature14.8 13.3 14.6 14.7 15 12.8 15.3 15 15.6 14.7 14.3 14.5 14.88.1 71/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLMarch-08EPA 6010µg/L100 700 µg/L Barium 90.3 102 293 172 57.5 95.7 24 124 42 29.2 60.5 64.6 186 79.7 50.610 10 µg/LChromium0.49 0.79 0.63 0.4 5.67.3 0.421.8 1.1 4.11.210 20 µg/LSelenium4.910 20 µg/LSilver0.43 0.93 0.87 0.94 0.56 0.66 0.13 0.220.41 0.15 0.21 0.560.37 0.26EPA 7470µg/L0.2 1 µg/LMercury0.10.26EPA 8260µg/L100 4000 µg/L2-Butanone (MEK)4.6100 6000 µg/LAcetone15FieldfeetStatic Water Level38.28 8.83 22.71 10.49 11.13 40.6 15.22 51.33 11.77 4.08 4.47 8.78 51.11Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved4.61 1.46 3.08 3.69 6.77 3.04 6.44 7.8 7.08 0.33 5.27 5.85 6.697.5 7.28Std. UnitsField pH6.04 6.14 6.08 6.75 6.56 5.84 7.39 5.66 6.81 7.12 7.22 6.45 5.827.69 8.54mVREDOX56 29 -43 24 3352 50 191 123 -172 18 74 124197 195µmhos/cmField Specific Conductance 91 234 258 254 172 141 51 123 36 125 99 72 136194 122°CField Temperature16.62 16.47 14.41 11.87 14.15 15.59 14 17.68 14.52 13.95 12.86 15.63 16.4714.74 13.5November-07(blank)µg/L100 6000 µg/LAcetone22.7100 700 µg/LBarium105 107 273 287 70.6 101 26.6 117 40.8 23.1 47.3 85.6 13070.3 49.410 10 µg/LChromium8.41.70.610.2 1 µg/LMercury0.09810 20 µg/LSelenium18.110 20 µg/LSilver0.16 0.320.39 0.260.480.51 0.26FieldfeetStatic Water Level38.12 9.32 22.72 10.65 11.65 40.4 16.78 50.38 12.34 4.33 4.95 9.27 50.78Total Well Depth60 21 27 20 3048 27 60 21 20 15.58 20 60mg/LOxygen, Dissolved5.08 0.72 1.69 1.32 6.5 0.85 7.12 7.32 6.59 1.02 2.01 5.16 7.335 6.93Std. UnitsField pH6.52 6.67 6.21 6.35 7 6.07 6.27 5.73 5.95 6.67 6.48 6.83 5.826.18 7.35mVREDOX59 61 66 43 6153 66 56 73 -80 21 73 5834 48µmhos/cmField Specific Conductance 85 176 217 394 161 126 51 121 36 121 114 65 140218 112°CField Temperature15.42 14.08 13.22 16.04 14.9 14.16 15.48 15.75 16.38 16.33 16.3 15.32 15.7515.64 17.531/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLApril-07(blank)µg/L100 4000 µg/L 2-Butanone (MEK)1110 10 µg/L Arsenic5.5100 700 µg/L Barium 81 79 310 200 58 89 30 140 52 25 31 79 210 88 30010 10 µg/L Chromium 6.46.61710 15 µg/L Lead5.2 1110 20 µg/L Selenium2421FieldfeetStatic Water Level 37.43 8.58 20.12 8.71 10.33 39.81 14.14 49.98 11.43 2.66 4.21 8.67 49.43Total Well Depth60 21 27 20 3048 27 60 21 20 15.7 20 60mg/LOxygen, Dissolved3.82 0.48 290 1.07 5.55 0.67 5.14 5.35 5.53 280 6.57 4.59 5.75.5 6.16Std. UnitsField pH5.86 5.59 5.81 6 6.17 5.66 5.03 5.86 5.62 5.96 6.02 5.72 5.796.63 6.32mVREDOX58 50 -3 -8 3630 48 90 124 -114 87 110 9927 86µmhos/cmField Specific Conductance 91 151 324 333 171 139 52 115 39 125 105 72 140314 130°CField Temperature15.4 12.4 14.2 12.1 13.5 15.4 14.3 15.5 14 13.9 13.5 12.9 15.422.3 20.8November-06(blank)µg/L10 10 µg/LArsenic8.3100 700 µg/LBarium94 90 230 220 5876 29 140 71 24 66 62 46054 441 2 µg/LCadmium210 10 µg/LChromium6.23510 15 µg/LLead23FieldfeetStatic Water Level38.17 8.74 22.3 9.81 11.17 40.13 16.19 49.85 11.94 3.41 4.65 8.92 40.93Total Well Depth60 21 27 20 3048 27 60 21 20 15.6 20 60mg/LOxygen, Dissolved4.28 0.31 1.15 0.42 5.88 1.21 6.2 5.44 5.67 0.31 0.85 4.54 6.417.91 5.26Std. UnitsField pH6.29 5.97 5.94 6.16 6.49 5.94 6.15 5.94 5.84 6.64 6.24 5.84 67.28 6.65mVREDOX-13 114 160 59 5995 35 90 221 67 132 235 171130 233µmhos/cmField Specific Conductance 104 235 266 196 196 155 60 136 45 145 127 80 15266 140°FField Temperature58.8 59.3 59.5 59.9 60.2 58.1 59.9 59.7 60.7 60.4 60.3 60.7 59.255.4 62.2April-06(blank)µg/L100 700 µg/LBarium82 52 290 220 5774 29 100 48 26 55 65 250120 15010 10 µg/LChromium6.24 2154.2 4.710 15 µg/LLead137.61/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLNovember-05EPA 6010µg/L100 700 µg/L Barium 78 62 300 180 54 60 26 100 46 27 77 59 120 73 5110 10 µg/L Chromium 3.53.910 15 µg/L Lead5.9EPA 7470µg/L0.2 1 µg/L Mercury 0.34 0.4 0.24 0.26 0.2 0.441.1EPA 8260µg/L1 3 µg/L Chloromethane5.4June-05(blank)µg/L10 10 µg/LArsenic23100 700 µg/LBarium48 43 300 150 5353 25 85 82 24 50 46 697504710 10 µg/LChromium5.65210 15 µg/LLead5710 20 µg/LSelenium5.5November-04(blank)µg/L10 10 µg/LArsenic5.1100 700 µg/LBarium95 52 340 140 8063 30 95 55 28 77 57 6653 6510 10 µg/LChromium22.3144.4 2.43.9 2.1 4.83.2August-04(blank)µg/L10 10 µg/LArsenic20100 700 µg/LBarium240 98 47 74 160 170500 6310 10 µg/LChromium14 133.39.2 3.23610 15 µg/LLead14 6.811 83810 20 µg/LSelenium6.2May-04(blank)µg/L10 10 µg/LArsenic9.2 56100 700 µg/LBarium96.3 55 270 380 76 28 180 48010 10 µg/LChromium3.53.7147.3 2.226 2810 15 µg/LLead14185.141November-03(blank)µg/L10 10 µg/LArsenic8.6100 700 µg/LBarium460 60 200 97 65 258205210 10 µg/LChromium2.2 2.3 2.6 8.7 2.41503.210 15 µg/LLead2224May-03(blank)µg/L100 700 µg/LBarium120 56 220 94 72 24 130 771 2 µg/LCadmium2.71/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCL10 10 µg/LChromium4.35.5 9.5173.810 15 µg/LLead5.35.3 6.7December-02(blank)µg/L100 700 µg/LBarium100 140 13 86 65 41 210 481 2 µg/LCadmium1.910 10 µg/LChromium2.3 2.15 7.4 3.232210 15 µg/LLead66April-02(blank)µg/L10 10 µg/LArsenic7.4100 700 µg/LBarium130 100 370 61 150 180 84 15010 10 µg/LChromium51523 266.82310 15 µg/LLead217.610 20 µg/LSilver2.6November-01(blank)µg/L10 10 µg/LArsenic5.88.412716 17 36100 700 µg/LBarium280 160 400900610 5301300 270010 10 µg/LChromium22 16 19 95 140 95 270 9410 15 µg/LLead10 735 361338 36 1501 600 µg/LToluene21July-01(blank)µg/L10 10 µg/LArsenic185.616 46100 700 µg/LBarium87 280950550 270 621300 260010 10 µg/LChromium6.616 50 38 494.1210 9210 15 µg/LLead8.95314 7.626 210December-00(blank)µg/L10 10 µg/LArsenic31545 89100 700 µg/LBarium150 611500350 400 412600 420010 10 µg/LChromium6.6 3.9100 28 822.6580 24010 15 µg/LLead808.1 7.665 400June-00(blank)µg/L100 700 µg/LBarium110 180 300 570 200 82 36010 10 µg/LChromium38.12.510 15 µg/LLead6.59.55.8 8.7November-99(blank)µg/L10 10 µg/LArsenic5.9 7.5100 700 µg/LBarium130 120 52860200 59 39010 10 µg/LChromium5.214 24 60 292.86210 15 µg/LLead6.940 408.2120.21µg/LMercury0.361/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLJune-99(blank)µg/L10 10 µg/LArsenic9.8100 700 µg/LBarium150 15095024096010 10 µg/LChromium7.8 7.8110 38 19010 15 µg/LLead50 16301 5 µg/LMethylene Chloride13 1310 1010November-98(blank)µg/L100 6000 µg/LAcetone15010 10 µg/LArsenic11100 700 µg/LBarium1601100 1400 2000480 1601300100 700 µg/LCarbon disulfide2825910 10 µg/LChromium12 210 77 300 96 12 35010 15 µg/LLead68 39 76 29360.2 1 µg/LMercury0.21May-98(blank)µg/L10 10 µg/LArsenic5100 700 µg/LBarium100 190860 850 820360120010 10 µg/LChromium49 34 25 130 170 33 43010 15 µg/LLead19 32 43 69 20 38October-97(blank)µg/L100 700 µg/LBarium290 340 620 650 610 260180010 10 µg/LChromium11 43 16 55 16 14 41010 15 µg/LLead1231 26 29 3114530.2 1 µg/LMercury0.20.2May-97(blank)µg/L100 700 µg/LBarium100 200800280 330 3007501 2 µg/LCadmium310 10 µg/LChromium3 42870 21 18010 15 µg/LLead142712 14 142310 20 µg/LSilver66October-96(blank)µg/L100 700 µg/LBarium180 160790 720620 59097010 10 µg/LChromium6 920 47 43 10 2110 15 µg/LLead815 16 2011 60.2 1 µg/LMercury0.20.30.41/3/2018
Appendix A3Summary of Detected Constituents Facility Permit34-12Old Salisbury Road Landfill (C&D)Qualifier(Multiple Items)SWSL2L UnitsConcentrationMW-1RMW-2R MW-3R MW-4R MW-5RMW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4Trip BlankEquipment BlankMCLJanuary-96(blank)µg/L100 4000 µg/L 2-Butanone (MEK) 86100 700 µg/L Barium 224 35012305951000 1400 19301 2 µg/L Cadmium7100 700 µg/L Carbon disulfide 2310 10 µg/L Chromium12921 96 12 2810 15 µg/L Lead 626 15 17 19 18 170.2 1 µg/L Mercury1.80.4 0.71.70.81.4 1.41/3/2018
This page intentionally left blank.
Winston-Salem City/County Utilities | Assessment Monitoring Report Appendix B – Laboratory Groundwater Report

B
Appendix B – Laboratory
Groundwater Report

This page intentionally left blank.
#=CL#
December 28, 2017
LIMS USE: FR - SEAN QUARRY
LIMS OBJECT ID: 92363879
92363879
Project:
Pace Project No.:
RE:
Sean QuarryHDR Engineering440 South Church StreetSuite 1000Charlotte, NC 28202
OSR
Dear Sean Quarry:
Enclosed are the analytical results for sample(s) received by the laboratory on November 17, 2017.
The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
Per client request, report revised 12/28/17 to include APP 2 compounds.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin for
[e-mail]
HORIZON Database Administrator
Kevin Herring
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 87
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92363879
OSR
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 87
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92363879
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92363879001 3412-EQUIPMENT BLANK EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8151 6 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92363879002 3412-MW1R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8151 6 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92363879003 3412-MW4R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8151 6 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 87
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92363879
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-CN-E 1 PASI-AAES2
92363879004 3412-MW15 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8151 6 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92363879005 3412-MW3R EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92363879006 3412-MW5R EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92363879007 3412-MW13 EPA 6010 18 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 87
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92363879
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92363879008 3412-MW14 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92363879009 3412-MW7 EPA 8081 21 PASI-CPKS
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-EQUIPMENT BLANK Lab ID: 92363879001 Collected: 11/16/17 07:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/26/17 03:26 309-00-211/22/17 11:360.050 1
alpha-BHC ND ug/L 11/26/17 03:26 319-84-611/22/17 11:360.050 1
beta-BHC ND ug/L 11/26/17 03:26 319-85-711/22/17 11:360.050 1
delta-BHC ND ug/L 11/26/17 03:26 319-86-811/22/17 11:360.050 1
gamma-BHC (Lindane)ND ug/L 11/26/17 03:26 58-89-911/22/17 11:360.050 1
Chlordane (Technical)ND ug/L 11/26/17 03:26 57-74-911/22/17 11:360.20 1
4,4'-DDD ND ug/L 11/26/17 03:26 72-54-811/22/17 11:360.050 1
4,4'-DDE ND ug/L 11/26/17 03:26 72-55-911/22/17 11:360.050 1
4,4'-DDT ND ug/L 11/26/17 03:26 50-29-311/22/17 11:360.050 1
Dieldrin ND ug/L 11/26/17 03:26 60-57-111/22/17 11:360.050 1
Endosulfan I ND ug/L 11/26/17 03:26 959-98-811/22/17 11:360.050 1
Endosulfan II ND ug/L 11/26/17 03:26 33213-65-911/22/17 11:360.050 1
Endosulfan sulfate ND ug/L 11/26/17 03:26 1031-07-811/22/17 11:360.050 1
Endrin ND ug/L 11/26/17 03:26 72-20-811/22/17 11:360.050 1
Endrin aldehyde ND ug/L 11/26/17 03:26 7421-93-411/22/17 11:360.050 1
Heptachlor ND ug/L 11/26/17 03:26 76-44-811/22/17 11:360.050 1
Heptachlor epoxide ND ug/L 11/26/17 03:26 1024-57-311/22/17 11:360.050 1
Methoxychlor ND ug/L 11/26/17 03:26 72-43-511/22/17 11:360.15 1
Toxaphene ND ug/L 11/26/17 03:26 8001-35-211/22/17 11:360.20 1
Surrogates
Tetrachloro-m-xylene (S)82 %11/26/17 03:26 877-09-811/22/17 11:3620-130 1
Decachlorobiphenyl (S)49 %11/26/17 03:26 2051-24-311/22/17 11:3620-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/29/17 17:58 12674-11-211/27/17 13:140.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/29/17 17:58 11104-28-211/27/17 13:140.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/29/17 17:58 11141-16-511/27/17 13:140.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/29/17 17:58 53469-21-911/27/17 13:140.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/29/17 17:58 12672-29-611/27/17 13:140.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/29/17 17:58 11097-69-111/27/17 13:140.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/29/17 17:58 11096-82-511/27/17 13:140.50 1
Surrogates
Decachlorobiphenyl (S)37 %11/29/17 17:58 2051-24-311/27/17 13:1410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/29/17 01:26 94-75-7 1g11/21/17 23:280.99 1
Dinoseb ND ug/L 11/29/17 01:26 88-85-7 1g11/21/17 23:280.20 1
Pentachlorophenol 0.018J ug/L 11/29/17 01:26 87-86-5 1g11/21/17 23:280.030 1
2,4,5-T ND ug/L 11/29/17 01:26 93-76-5 1g11/21/17 23:280.20 1
2,4,5-TP (Silvex)ND ug/L 11/29/17 01:26 93-72-1 1g11/21/17 23:280.20 1
Surrogates
2,4-DCAA (S)105 %11/29/17 01:26 19719-28-911/21/17 23:2839-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 01:46 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 01:46 7440-38-211/21/17 12:0010.0 1
Barium ND ug/L 12/07/17 01:46 7440-39-311/21/17 12:005.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-EQUIPMENT BLANK Lab ID: 92363879001 Collected: 11/16/17 07:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Beryllium ND ug/L 12/07/17 01:46 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 01:46 7440-43-911/21/17 12:001.0 1
Chromium 3.2J ug/L 12/07/17 01:46 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 01:46 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 01:46 7440-50-811/21/17 12:005.0 1
Iron ND ug/L 12/07/17 01:46 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 01:46 7439-92-111/21/17 12:005.0 1
Manganese ND ug/L 12/07/17 01:46 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 01:46 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 01:46 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 01:46 7440-22-411/21/17 12:005.0 1
Sodium 539J ug/L 12/07/17 01:46 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 01:46 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 01:46 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 01:46 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:28 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:14 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 10:51 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 10:51 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 10:51 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 10:51 120-12-711/23/17 05:4110.0 1
Benzo(a)anthracene ND ug/L 11/28/17 10:51 56-55-311/23/17 05:4110.0 1
Benzo(a)pyrene ND ug/L 11/28/17 10:51 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 10:51 205-99-211/23/17 05:4110.0 1
Benzo(g,h,i)perylene ND ug/L 11/28/17 10:51 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 10:51 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 10:51 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 10:51 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate ND ug/L 11/28/17 10:51 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 10:51 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 10:51 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 10:51 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 10:51 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 10:51 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 10:51 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 10:51 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 10:51 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 10:51 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 10:51 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 10:51 91-94-111/23/17 05:4120.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-EQUIPMENT BLANK Lab ID: 92363879001 Collected: 11/16/17 07:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
2,4-Dichlorophenol ND ug/L 11/28/17 10:51 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 10:51 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 10:51 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 10:51 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 10:51 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 10:51 534-52-1 L211/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 10:51 51-28-5 L211/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 10:51 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 10:51 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 10:51 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 10:51 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 10:51 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 10:51 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 10:51 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 10:51 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 10:51 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 10:51 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 10:51 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 10:51 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 10:51 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 10:51 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 10:51 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 10:51 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 10:51 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 10:51 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 10:51 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 10:51 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 10:51 100-02-711/23/17 05:4150.0 1
N-Nitrosodimethylamine ND ug/L 11/28/17 10:51 62-75-911/23/17 05:4110.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 10:51 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 10:51 86-30-611/23/17 05:4110.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 10:51 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 10:51 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 10:51 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 10:51 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 10:51 95-95-4 L211/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 10:51 88-06-2 L211/23/17 05:4110.0 1
SurrogatesNitrobenzene-d5 (S)60 %11/28/17 10:51 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)54 %11/28/17 10:51 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)73 %11/28/17 10:51 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)44 %11/28/17 10:51 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)50 %11/28/17 10:51 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)66 %11/28/17 10:51 118-79-611/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 03:34 67-64-125.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-EQUIPMENT BLANK Lab ID: 92363879001 Collected: 11/16/17 07:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetonitrile ND ug/L 11/26/17 03:34 75-05-850.0 1
Acrolein ND ug/L 11/26/17 03:34 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 03:34 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 03:34 107-05-12.0 1
Benzene ND ug/L 11/26/17 03:34 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 03:34 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 03:34 75-27-41.0 1
Bromoform ND ug/L 11/26/17 03:34 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 03:34 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 03:34 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 03:34 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 03:34 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 03:34 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 03:34 75-00-31.0 1
Chloroform ND ug/L 11/26/17 03:34 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 03:34 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 03:34 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 03:34 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 03:34 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 03:34 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 03:34 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 03:34 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 03:34 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 03:34 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 03:34 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 03:34 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 03:34 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 03:34 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 03:34 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 03:34 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 03:34 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 03:34 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 03:34 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 03:34 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 03:34 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 03:34 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 03:34 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 03:34 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 03:34 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 03:34 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 03:34 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 03:34 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 03:34 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 03:34 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 03:34 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 03:34 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 03:34 108-10-15.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-EQUIPMENT BLANK Lab ID: 92363879001 Collected: 11/16/17 07:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Naphthalene ND ug/L 11/26/17 03:34 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 03:34 107-12-020.0 1
Styrene ND ug/L 11/26/17 03:34 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 03:34 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 03:34 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 03:34 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 03:34 109-99-910.0 1
Toluene ND ug/L 11/26/17 03:34 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 03:34 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 03:34 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 03:34 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 03:34 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 03:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 03:34 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 03:34 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 03:34 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 03:34 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 03:34 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/26/17 03:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %11/26/17 03:34 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 03:34 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 12:56 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW1R Lab ID: 92363879002 Collected: 11/16/17 13:00 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 13:00 12/13/17 14:081
Field pH 5.6 Std. Units 12/13/17 14:080.10 1
Field Temperature 17.2 deg C 12/13/17 14:080.50 1
Static Water Level 34.72 feet 12/13/17 14:081
Field Specific Conductance 208.3 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 0.6 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 60 feet 12/13/17 14:081
REDOX 158.6 mV 12/13/17 14:081
Turbidity 1.1 NTU 12/13/17 14:081.0 1
Odor NONE 12/13/17 14:081
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/29/17 15:06 309-00-211/22/17 17:100.050 1
alpha-BHC ND ug/L 11/29/17 15:06 319-84-611/22/17 17:100.050 1
beta-BHC ND ug/L 11/29/17 15:06 319-85-711/22/17 17:100.050 1
delta-BHC ND ug/L 11/29/17 15:06 319-86-811/22/17 17:100.050 1
gamma-BHC (Lindane)ND ug/L 11/29/17 15:06 58-89-911/22/17 17:100.050 1
Chlordane (Technical)ND ug/L 11/29/17 15:06 57-74-911/22/17 17:100.20 1
4,4'-DDD ND ug/L 11/29/17 15:06 72-54-811/22/17 17:100.050 1
4,4'-DDE ND ug/L 11/29/17 15:06 72-55-911/22/17 17:100.050 1
4,4'-DDT ND ug/L 11/29/17 15:06 50-29-311/22/17 17:100.050 1
Dieldrin ND ug/L 11/29/17 15:06 60-57-111/22/17 17:100.050 1
Endosulfan I ND ug/L 11/29/17 15:06 959-98-811/22/17 17:100.050 1
Endosulfan II ND ug/L 11/29/17 15:06 33213-65-911/22/17 17:100.050 1
Endosulfan sulfate ND ug/L 11/29/17 15:06 1031-07-811/22/17 17:100.050 1
Endrin ND ug/L 11/29/17 15:06 72-20-811/22/17 17:100.050 1
Endrin aldehyde ND ug/L 11/29/17 15:06 7421-93-411/22/17 17:100.050 1
Heptachlor ND ug/L 11/29/17 15:06 76-44-811/22/17 17:100.050 1
Heptachlor epoxide ND ug/L 11/29/17 15:06 1024-57-311/22/17 17:100.050 1
Methoxychlor ND ug/L 11/29/17 15:06 72-43-511/22/17 17:100.15 1
Toxaphene ND ug/L 11/29/17 15:06 8001-35-211/22/17 17:100.20 1
Surrogates
Tetrachloro-m-xylene (S)78 %11/29/17 15:06 877-09-811/22/17 17:1020-130 1
Decachlorobiphenyl (S)63 %11/29/17 15:06 2051-24-311/22/17 17:1020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/29/17 18:38 12674-11-211/27/17 13:140.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/29/17 18:38 11104-28-211/27/17 13:140.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/29/17 18:38 11141-16-511/27/17 13:140.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/29/17 18:38 53469-21-911/27/17 13:140.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/29/17 18:38 12672-29-611/27/17 13:140.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/29/17 18:38 11097-69-111/27/17 13:140.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/29/17 18:38 11096-82-511/27/17 13:140.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW1R Lab ID: 92363879002 Collected: 11/16/17 13:00 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)65 %11/29/17 18:38 2051-24-311/27/17 13:1410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/29/17 01:50 94-75-7 1g11/21/17 23:280.99 1
Dinoseb ND ug/L 11/29/17 01:50 88-85-7 1g11/21/17 23:280.20 1
Pentachlorophenol ND ug/L 11/29/17 01:50 87-86-5 1g11/21/17 23:280.030 1
2,4,5-T ND ug/L 11/29/17 01:50 93-76-5 1g11/21/17 23:280.20 1
2,4,5-TP (Silvex)ND ug/L 11/29/17 01:50 93-72-1 1g11/21/17 23:280.20 1
Surrogates
2,4-DCAA (S)116 %11/29/17 01:50 19719-28-911/21/17 23:2839-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:06 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:06 7440-38-211/21/17 12:0010.0 1
Barium 260 ug/L 12/07/17 02:06 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:06 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:06 7440-43-911/21/17 12:001.0 1
Chromium 4.0J ug/L 12/07/17 02:06 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:06 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:06 7440-50-811/21/17 12:005.0 1
Iron 43.1J ug/L 12/07/17 02:06 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:06 7439-92-111/21/17 12:005.0 1
Manganese 11.8 ug/L 12/07/17 02:06 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:06 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:06 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:06 7440-22-411/21/17 12:005.0 1
Sodium 15200 ug/L 12/07/17 02:06 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:06 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:06 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 02:06 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:36 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.23 ug/L 11/29/17 13:22 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 11:45 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 11:45 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 11:45 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 11:45 120-12-711/23/17 05:4110.0 1
Benzo(a)anthracene ND ug/L 11/28/17 11:45 56-55-311/23/17 05:4110.0 1
Benzo(a)pyrene ND ug/L 11/28/17 11:45 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 11:45 205-99-211/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW1R Lab ID: 92363879002 Collected: 11/16/17 13:00 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Benzo(g,h,i)perylene ND ug/L 11/28/17 11:45 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 11:45 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 11:45 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 11:45 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate ND ug/L 11/28/17 11:45 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 11:45 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 11:45 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 11:45 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 11:45 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 11:45 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 11:45 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 11:45 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 11:45 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 11:45 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 11:45 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 11:45 91-94-111/23/17 05:4120.0 1
2,4-Dichlorophenol ND ug/L 11/28/17 11:45 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 11:45 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 11:45 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 11:45 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 11:45 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 11:45 534-52-111/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 11:45 51-28-511/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 11:45 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 11:45 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 11:45 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 11:45 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 11:45 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 11:45 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 11:45 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 11:45 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 11:45 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 11:45 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 11:45 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 11:45 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 11:45 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 11:45 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 11:45 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 11:45 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 11:45 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 11:45 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 11:45 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 11:45 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 11:45 100-02-711/23/17 05:4150.0 1
N-Nitrosodimethylamine ND ug/L 11/28/17 11:45 62-75-911/23/17 05:4110.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 11:45 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 11:45 86-30-611/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW1R Lab ID: 92363879002 Collected: 11/16/17 13:00 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 11:45 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 11:45 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 11:45 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 11:45 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 11:45 95-95-411/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 11:45 88-06-211/23/17 05:4110.0 1
SurrogatesNitrobenzene-d5 (S)68 %11/28/17 11:45 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)64 %11/28/17 11:45 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)70 %11/28/17 11:45 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)42 %11/28/17 11:45 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)39 %11/28/17 11:45 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)47 %11/28/17 11:45 118-79-611/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 03:52 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 03:52 75-05-850.0 1
Acrolein ND ug/L 11/26/17 03:52 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 03:52 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 03:52 107-05-12.0 1
Benzene ND ug/L 11/26/17 03:52 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 03:52 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 03:52 75-27-41.0 1
Bromoform ND ug/L 11/26/17 03:52 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 03:52 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 03:52 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 03:52 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 03:52 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 03:52 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 03:52 75-00-31.0 1
Chloroform ND ug/L 11/26/17 03:52 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 03:52 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 03:52 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 03:52 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 03:52 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 03:52 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 03:52 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 03:52 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 03:52 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 03:52 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 03:52 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 03:52 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 03:52 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 03:52 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 03:52 75-35-41.0 1
cis-1,2-Dichloroethene 0.62J ug/L 11/26/17 03:52 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 03:52 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW1R Lab ID: 92363879002 Collected: 11/16/17 13:00 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 11/26/17 03:52 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 03:52 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 03:52 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 03:52 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 03:52 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 03:52 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 03:52 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 03:52 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 03:52 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 03:52 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 03:52 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 03:52 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 03:52 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 03:52 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 03:52 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 03:52 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 03:52 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 03:52 107-12-020.0 1
Styrene ND ug/L 11/26/17 03:52 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 03:52 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 03:52 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 03:52 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 03:52 109-99-910.0 1
Toluene ND ug/L 11/26/17 03:52 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 03:52 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 03:52 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 03:52 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 03:52 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 03:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 03:52 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 03:52 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 03:52 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 03:52 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 03:52 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/26/17 03:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %11/26/17 03:52 17060-07-070-130 1
Toluene-d8 (S)110 %11/26/17 03:52 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 71400 ug/L 11/27/17 23:205000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 153000 ug/L 11/20/17 23:4225000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW1R Lab ID: 92363879002 Collected: 11/16/17 13:00 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 11/27/17 19:14 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 9290 ug/L 11/22/17 23:58 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 12:57 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW4R Lab ID: 92363879003 Collected: 11/16/17 13:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 13:10 12/13/17 14:081
Field pH 6.2 Std. Units 12/13/17 14:080.10 1
Field Temperature 16.2 deg C 12/13/17 14:080.50 1
Static Water Level 8.92 feet 12/13/17 14:081
Field Specific Conductance 1209 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 0.23 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 20.0 feet 12/13/17 14:081
REDOX 48.5 mV 12/13/17 14:081
Turbidity 8.94 NTU 12/13/17 14:081.0 1
Odor NONE 12/13/17 14:081
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/29/17 15:24 309-00-211/22/17 17:100.050 1
alpha-BHC ND ug/L 11/29/17 15:24 319-84-611/22/17 17:100.050 1
beta-BHC ND ug/L 11/29/17 15:24 319-85-711/22/17 17:100.050 1
delta-BHC ND ug/L 11/29/17 15:24 319-86-811/22/17 17:100.050 1
gamma-BHC (Lindane)ND ug/L 11/29/17 15:24 58-89-911/22/17 17:100.050 1
Chlordane (Technical)ND ug/L 11/29/17 15:24 57-74-911/22/17 17:100.20 1
4,4'-DDD ND ug/L 11/29/17 15:24 72-54-811/22/17 17:100.050 1
4,4'-DDE ND ug/L 11/29/17 15:24 72-55-911/22/17 17:100.050 1
4,4'-DDT ND ug/L 11/29/17 15:24 50-29-311/22/17 17:100.050 1
Dieldrin ND ug/L 11/29/17 15:24 60-57-111/22/17 17:100.050 1
Endosulfan I ND ug/L 11/29/17 15:24 959-98-811/22/17 17:100.050 1
Endosulfan II ND ug/L 11/29/17 15:24 33213-65-911/22/17 17:100.050 1
Endosulfan sulfate ND ug/L 11/29/17 15:24 1031-07-811/22/17 17:100.050 1
Endrin ND ug/L 11/29/17 15:24 72-20-811/22/17 17:100.050 1
Endrin aldehyde ND ug/L 11/29/17 15:24 7421-93-411/22/17 17:100.050 1
Heptachlor ND ug/L 11/29/17 15:24 76-44-811/22/17 17:100.050 1
Heptachlor epoxide ND ug/L 11/29/17 15:24 1024-57-311/22/17 17:100.050 1
Methoxychlor ND ug/L 11/29/17 15:24 72-43-511/22/17 17:100.15 1
Toxaphene ND ug/L 11/29/17 15:24 8001-35-211/22/17 17:100.20 1
Surrogates
Tetrachloro-m-xylene (S)79 %11/29/17 15:24 877-09-811/22/17 17:1020-130 1
Decachlorobiphenyl (S)64 %11/29/17 15:24 2051-24-311/22/17 17:1020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/29/17 19:18 12674-11-211/27/17 13:140.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/29/17 19:18 11104-28-211/27/17 13:140.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/29/17 19:18 11141-16-511/27/17 13:140.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/29/17 19:18 53469-21-911/27/17 13:140.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/29/17 19:18 12672-29-611/27/17 13:140.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/29/17 19:18 11097-69-111/27/17 13:140.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/29/17 19:18 11096-82-511/27/17 13:140.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW4R Lab ID: 92363879003 Collected: 11/16/17 13:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)50 %11/29/17 19:18 2051-24-311/27/17 13:1410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/29/17 02:15 94-75-7 1g11/21/17 23:280.98 1
Dinoseb ND ug/L 11/29/17 02:15 88-85-7 1g11/21/17 23:280.20 1
Pentachlorophenol ND ug/L 11/29/17 02:15 87-86-5 1g11/21/17 23:280.029 1
2,4,5-T ND ug/L 11/29/17 02:15 93-76-5 1g11/21/17 23:280.20 1
2,4,5-TP (Silvex)ND ug/L 11/29/17 02:15 93-72-1 1g11/21/17 23:280.20 1
Surrogates
2,4-DCAA (S)96 %11/29/17 02:15 19719-28-911/21/17 23:2839-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:10 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:10 7440-38-211/21/17 12:0010.0 1
Barium 198 ug/L 12/07/17 02:10 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:10 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:10 7440-43-911/21/17 12:001.0 1
Chromium 3.2J ug/L 12/07/17 02:10 7440-47-311/21/17 12:005.0 1
Cobalt 93.0 ug/L 12/07/17 02:10 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:10 7440-50-811/21/17 12:005.0 1
Iron 365 ug/L 12/07/17 02:10 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:10 7439-92-111/21/17 12:005.0 1
Manganese 1050 ug/L 12/07/17 02:10 7439-96-511/21/17 12:005.0 1
Nickel 7.5 ug/L 12/07/17 02:10 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:10 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:10 7440-22-411/21/17 12:005.0 1
Sodium 65500 ug/L 12/07/17 02:10 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:10 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:10 7440-62-211/21/17 12:005.0 1
Zinc 5.8J ug/L 12/07/17 02:10 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:38 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:24 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 12:12 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 12:12 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 12:12 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 12:12 120-12-711/23/17 05:4110.0 1
Benzo(a)anthracene ND ug/L 11/28/17 12:12 56-55-311/23/17 05:4110.0 1
Benzo(a)pyrene ND ug/L 11/28/17 12:12 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 12:12 205-99-211/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW4R Lab ID: 92363879003 Collected: 11/16/17 13:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Benzo(g,h,i)perylene ND ug/L 11/28/17 12:12 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 12:12 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 12:12 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 12:12 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate 1.7J ug/L 11/28/17 12:12 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 12:12 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 12:12 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 12:12 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 12:12 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 12:12 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 12:12 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 12:12 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 12:12 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 12:12 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 12:12 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 12:12 91-94-111/23/17 05:4120.0 1
2,4-Dichlorophenol ND ug/L 11/28/17 12:12 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 12:12 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 12:12 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 12:12 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 12:12 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 12:12 534-52-111/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 12:12 51-28-511/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 12:12 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 12:12 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 12:12 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 12:12 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 12:12 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 12:12 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 12:12 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 12:12 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 12:12 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 12:12 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 12:12 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 12:12 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 12:12 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 12:12 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 12:12 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 12:12 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 12:12 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 12:12 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 12:12 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 12:12 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 12:12 100-02-711/23/17 05:4150.0 1
N-Nitrosodimethylamine ND ug/L 11/28/17 12:12 62-75-911/23/17 05:4110.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 12:12 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 12:12 86-30-611/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW4R Lab ID: 92363879003 Collected: 11/16/17 13:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 12:12 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 12:12 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 12:12 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 12:12 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 12:12 95-95-411/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 12:12 88-06-211/23/17 05:4110.0 1
SurrogatesNitrobenzene-d5 (S)68 %11/28/17 12:12 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)59 %11/28/17 12:12 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)64 %11/28/17 12:12 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)50 %11/28/17 12:12 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)52 %11/28/17 12:12 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)73 %11/28/17 12:12 118-79-611/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 04:09 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 04:09 75-05-850.0 1
Acrolein ND ug/L 11/26/17 04:09 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 04:09 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 04:09 107-05-12.0 1
Benzene ND ug/L 11/26/17 04:09 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 04:09 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 04:09 75-27-41.0 1
Bromoform ND ug/L 11/26/17 04:09 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 04:09 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 04:09 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 04:09 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 04:09 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 04:09 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 04:09 75-00-31.0 1
Chloroform ND ug/L 11/26/17 04:09 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 04:09 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 04:09 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 04:09 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 04:09 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 04:09 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 04:09 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 04:09 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 04:09 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 04:09 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 04:09 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 04:09 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 04:09 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 04:09 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 04:09 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 04:09 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 04:09 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW4R Lab ID: 92363879003 Collected: 11/16/17 13:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 11/26/17 04:09 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 04:09 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 04:09 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 04:09 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 04:09 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 04:09 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 04:09 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 04:09 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 04:09 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 04:09 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 04:09 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 04:09 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 04:09 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 04:09 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 04:09 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 04:09 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 04:09 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 04:09 107-12-020.0 1
Styrene ND ug/L 11/26/17 04:09 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 04:09 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 04:09 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 04:09 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 04:09 109-99-910.0 1
Toluene ND ug/L 11/26/17 04:09 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 04:09 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 04:09 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 04:09 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 04:09 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 04:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 04:09 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 04:09 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 04:09 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 04:09 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 04:09 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/26/17 04:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %11/26/17 04:09 17060-07-070-130 1
Toluene-d8 (S)106 %11/26/17 04:09 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 461000 ug/L 11/28/17 12:155000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 862000 ug/L 11/20/17 23:4250000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW4R Lab ID: 92363879003 Collected: 11/16/17 13:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 179000 ug/L 11/28/17 06:27 14808-79-83000 3
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 49200 ug/L 11/23/17 02:25 16887-00-62000 2
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 12:58 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW15 Lab ID: 92363879004 Collected: 11/16/17 16:35 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 16:35 12/13/17 14:081
Field pH 6.4 Std. Units 12/13/17 14:080.10 1
Field Temperature 16.0 deg C 12/13/17 14:080.50 1
Static Water Level 39.37 feet 12/13/17 14:081
Field Specific Conductance 624 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 4.36 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 50.85 feet 12/13/17 14:081
REDOX 65.2 mV 12/13/17 14:081
Turbidity 98.53 NTU 12/13/17 14:081.0 1
Odor NONE 12/13/17 14:081
Appearance MURKY 12/13/17 14:081
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/29/17 15:42 309-00-211/22/17 17:100.050 1
alpha-BHC ND ug/L 11/29/17 15:42 319-84-611/22/17 17:100.050 1
beta-BHC ND ug/L 11/29/17 15:42 319-85-711/22/17 17:100.050 1
delta-BHC ND ug/L 11/29/17 15:42 319-86-811/22/17 17:100.050 1
gamma-BHC (Lindane)ND ug/L 11/29/17 15:42 58-89-911/22/17 17:100.050 1
Chlordane (Technical)ND ug/L 11/29/17 15:42 57-74-911/22/17 17:100.20 1
4,4'-DDD ND ug/L 11/29/17 15:42 72-54-811/22/17 17:100.050 1
4,4'-DDE ND ug/L 11/29/17 15:42 72-55-911/22/17 17:100.050 1
4,4'-DDT ND ug/L 11/29/17 15:42 50-29-311/22/17 17:100.050 1
Dieldrin ND ug/L 11/29/17 15:42 60-57-111/22/17 17:100.050 1
Endosulfan I ND ug/L 11/29/17 15:42 959-98-811/22/17 17:100.050 1
Endosulfan II ND ug/L 11/29/17 15:42 33213-65-911/22/17 17:100.050 1
Endosulfan sulfate ND ug/L 11/29/17 15:42 1031-07-811/22/17 17:100.050 1
Endrin ND ug/L 11/29/17 15:42 72-20-811/22/17 17:100.050 1
Endrin aldehyde ND ug/L 11/29/17 15:42 7421-93-411/22/17 17:100.050 1
Heptachlor ND ug/L 11/29/17 15:42 76-44-811/22/17 17:100.050 1
Heptachlor epoxide ND ug/L 11/29/17 15:42 1024-57-311/22/17 17:100.050 1
Methoxychlor ND ug/L 11/29/17 15:42 72-43-511/22/17 17:100.15 1
Toxaphene ND ug/L 11/29/17 15:42 8001-35-211/22/17 17:100.20 1
Surrogates
Tetrachloro-m-xylene (S)94 %11/29/17 15:42 877-09-811/22/17 17:1020-130 1
Decachlorobiphenyl (S)64 %11/29/17 15:42 2051-24-311/22/17 17:1020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/29/17 19:38 12674-11-211/27/17 13:140.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/29/17 19:38 11104-28-211/27/17 13:140.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/29/17 19:38 11141-16-511/27/17 13:140.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/29/17 19:38 53469-21-911/27/17 13:140.50 1
PCB-1248 (Aroclor 1248)ND ug/L 11/29/17 19:38 12672-29-611/27/17 13:140.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/29/17 19:38 11097-69-111/27/17 13:140.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/29/17 19:38 11096-82-511/27/17 13:140.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW15 Lab ID: 92363879004 Collected: 11/16/17 16:35 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)47 %11/29/17 19:38 2051-24-311/27/17 13:1410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D 0.27J ug/L 11/29/17 02:40 94-75-7 1g11/21/17 23:280.99 1
Dinoseb ND ug/L 11/29/17 02:40 88-85-7 1g11/21/17 23:280.20 1
Pentachlorophenol ND ug/L 11/29/17 02:40 87-86-5 1g11/21/17 23:280.030 1
2,4,5-T ND ug/L 11/29/17 02:40 93-76-5 1g11/21/17 23:280.20 1
2,4,5-TP (Silvex)ND ug/L 11/29/17 02:40 93-72-1 1g11/21/17 23:280.20 1
Surrogates
2,4-DCAA (S)104 %11/29/17 02:40 19719-28-911/21/17 23:2839-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:15 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:15 7440-38-211/21/17 12:0010.0 1
Barium 17.1 ug/L 12/07/17 02:15 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:15 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:15 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 02:15 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:15 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:15 7440-50-811/21/17 12:005.0 1
Iron 1050 ug/L 12/07/17 02:15 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:15 7439-92-111/21/17 12:005.0 1
Manganese 317 ug/L 12/07/17 02:15 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:15 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:15 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:15 7440-22-411/21/17 12:005.0 1
Sodium 19800 ug/L 12/07/17 02:15 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:15 7440-31-511/21/17 12:005.0 1
Vanadium 3.6J ug/L 12/07/17 02:15 7440-62-211/21/17 12:005.0 1
Zinc 7.1J ug/L 12/07/17 02:15 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:41 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:26 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 12:39 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 12:39 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 12:39 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 12:39 120-12-711/23/17 05:4110.0 1
Benzo(a)anthracene ND ug/L 11/28/17 12:39 56-55-311/23/17 05:4110.0 1
Benzo(a)pyrene ND ug/L 11/28/17 12:39 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 12:39 205-99-211/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW15 Lab ID: 92363879004 Collected: 11/16/17 16:35 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Benzo(g,h,i)perylene ND ug/L 11/28/17 12:39 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 12:39 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 12:39 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 12:39 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate ND ug/L 11/28/17 12:39 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 12:39 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 12:39 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 12:39 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 12:39 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 12:39 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 12:39 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 12:39 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 12:39 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 12:39 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 12:39 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 12:39 91-94-111/23/17 05:4120.0 1
2,4-Dichlorophenol ND ug/L 11/28/17 12:39 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 12:39 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 12:39 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 12:39 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 12:39 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 12:39 534-52-111/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 12:39 51-28-511/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 12:39 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 12:39 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 12:39 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 12:39 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 12:39 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 12:39 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 12:39 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 12:39 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 12:39 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 12:39 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 12:39 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 12:39 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 12:39 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 12:39 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 12:39 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 12:39 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 12:39 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 12:39 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 12:39 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 12:39 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 12:39 100-02-711/23/17 05:4150.0 1
N-Nitrosodimethylamine ND ug/L 11/28/17 12:39 62-75-911/23/17 05:4110.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 12:39 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 12:39 86-30-611/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW15 Lab ID: 92363879004 Collected: 11/16/17 16:35 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 12:39 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 12:39 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 12:39 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 12:39 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 12:39 95-95-411/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 12:39 88-06-211/23/17 05:4110.0 1
SurrogatesNitrobenzene-d5 (S)68 %11/28/17 12:39 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)62 %11/28/17 12:39 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)67 %11/28/17 12:39 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)50 %11/28/17 12:39 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)53 %11/28/17 12:39 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)73 %11/28/17 12:39 118-79-611/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 04:26 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 04:26 75-05-850.0 1
Acrolein ND ug/L 11/26/17 04:26 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 04:26 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 04:26 107-05-12.0 1
Benzene ND ug/L 11/26/17 04:26 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 04:26 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 04:26 75-27-41.0 1
Bromoform ND ug/L 11/26/17 04:26 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 04:26 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 04:26 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 04:26 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 04:26 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 04:26 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 04:26 75-00-31.0 1
Chloroform 0.44J ug/L 11/26/17 04:26 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 04:26 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 04:26 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 04:26 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 04:26 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 04:26 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 04:26 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 04:26 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 04:26 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 04:26 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 04:26 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 04:26 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 04:26 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 04:26 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 04:26 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 04:26 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 04:26 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW15 Lab ID: 92363879004 Collected: 11/16/17 16:35 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 11/26/17 04:26 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 04:26 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 04:26 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 04:26 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 04:26 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 04:26 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 04:26 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 04:26 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 04:26 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 04:26 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 04:26 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 04:26 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 04:26 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 04:26 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 04:26 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 04:26 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 04:26 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 04:26 107-12-020.0 1
Styrene ND ug/L 11/26/17 04:26 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 04:26 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 04:26 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 04:26 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 04:26 109-99-910.0 1
Toluene ND ug/L 11/26/17 04:26 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 04:26 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 04:26 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 04:26 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 04:26 79-01-61.0 1
Trichlorofluoromethane 0.71J ug/L 11/26/17 04:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 04:26 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 04:26 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 04:26 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 04:26 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 04:26 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/26/17 04:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %11/26/17 04:26 17060-07-070-130 1
Toluene-d8 (S)106 %11/26/17 04:26 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 110000 ug/L 11/28/17 00:035000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 370000 ug/L 11/20/17 23:4225000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW15 Lab ID: 92363879004 Collected: 11/16/17 16:35 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 59600 ug/L 11/27/17 19:49 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 89800 ug/L 11/23/17 00:00 16887-00-65000 5
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 12:59 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW3R Lab ID: 92363879005 Collected: 11/16/17 10:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 10:30 12/13/17 14:081
Field pH 6.4 Std. Units 12/13/17 14:080.10 1
Field Temperature 15.5 deg C 12/13/17 14:080.50 1
Static Water Level 20.34 feet 12/13/17 14:081
Field Specific Conductance 394.2 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 0.3 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 27 feet 12/13/17 14:081
REDOX -109.6 mV 12/13/17 14:081
Turbidity 7.6 NTU 12/13/17 14:081.0 1
Odor NONE 12/13/17 14:081
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:19 7440-36-011/21/17 12:005.0 1
Arsenic 9.0J ug/L 12/07/17 02:19 7440-38-211/21/17 12:0010.0 1
Barium 278 ug/L 12/07/17 02:19 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:19 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:19 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 02:19 7440-47-311/21/17 12:005.0 1
Cobalt 9.4 ug/L 12/07/17 02:19 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:19 7440-50-811/21/17 12:005.0 1
Iron 78700 ug/L 12/07/17 02:19 7439-89-611/21/17 12:0050.0 1
Lead 3.4J ug/L 12/07/17 02:19 7439-92-111/21/17 12:005.0 1
Manganese 5440 ug/L 12/07/17 02:19 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:19 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:19 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:19 7440-22-411/21/17 12:005.0 1
Sodium 2380J ug/L 12/07/17 02:19 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:19 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:19 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 02:19 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:43 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:29 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 13:07 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 13:07 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 13:07 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 13:07 120-12-711/23/17 05:4110.0 1
Benzo(a)anthracene ND ug/L 11/28/17 13:07 56-55-311/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW3R Lab ID: 92363879005 Collected: 11/16/17 10:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Benzo(a)pyrene ND ug/L 11/28/17 13:07 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 13:07 205-99-211/23/17 05:4110.0 1
Benzo(g,h,i)perylene ND ug/L 11/28/17 13:07 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 13:07 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 13:07 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 13:07 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate ND ug/L 11/28/17 13:07 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 13:07 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 13:07 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 13:07 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 13:07 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 13:07 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 13:07 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 13:07 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 13:07 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 13:07 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 13:07 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 13:07 91-94-111/23/17 05:4120.0 1
2,4-Dichlorophenol ND ug/L 11/28/17 13:07 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 13:07 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 13:07 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 13:07 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 13:07 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 13:07 534-52-111/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 13:07 51-28-511/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 13:07 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 13:07 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 13:07 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 13:07 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 13:07 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 13:07 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 13:07 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 13:07 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 13:07 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 13:07 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 13:07 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 13:07 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 13:07 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 13:07 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 13:07 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 13:07 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 13:07 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 13:07 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 13:07 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 13:07 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 13:07 100-02-711/23/17 05:4150.0 1
N-Nitrosodimethylamine ND ug/L 11/28/17 13:07 62-75-911/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW3R Lab ID: 92363879005 Collected: 11/16/17 10:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 13:07 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 13:07 86-30-611/23/17 05:4110.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 13:07 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 13:07 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 13:07 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 13:07 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 13:07 95-95-411/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 13:07 88-06-211/23/17 05:4110.0 1
Surrogates
Nitrobenzene-d5 (S)68 %11/28/17 13:07 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)63 %11/28/17 13:07 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)73 %11/28/17 13:07 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)54 %11/28/17 13:07 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)57 %11/28/17 13:07 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)73 %11/28/17 13:07 118-79-611/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 04:44 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 04:44 75-05-850.0 1
Acrolein ND ug/L 11/26/17 04:44 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 04:44 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 04:44 107-05-12.0 1
Benzene ND ug/L 11/26/17 04:44 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 04:44 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 04:44 75-27-41.0 1
Bromoform ND ug/L 11/26/17 04:44 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 04:44 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 04:44 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 04:44 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 04:44 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 04:44 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 04:44 75-00-31.0 1
Chloroform ND ug/L 11/26/17 04:44 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 04:44 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 04:44 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 04:44 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 04:44 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 04:44 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 04:44 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 04:44 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 04:44 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 04:44 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 04:44 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 04:44 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 04:44 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 04:44 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 04:44 75-35-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW3R Lab ID: 92363879005 Collected: 11/16/17 10:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,2-Dichloroethene ND ug/L 11/26/17 04:44 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 04:44 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 04:44 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 04:44 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 04:44 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 04:44 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 04:44 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 04:44 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 04:44 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 04:44 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 04:44 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 04:44 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 04:44 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 04:44 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 04:44 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 04:44 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 04:44 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 04:44 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 04:44 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 04:44 107-12-020.0 1
Styrene ND ug/L 11/26/17 04:44 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 04:44 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 04:44 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 04:44 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 04:44 109-99-910.0 1
Toluene ND ug/L 11/26/17 04:44 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 04:44 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 04:44 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 04:44 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 04:44 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 04:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 04:44 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 04:44 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 04:44 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 04:44 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 04:44 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)102 %11/26/17 04:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %11/26/17 04:44 17060-07-070-130 1
Toluene-d8 (S)112 %11/26/17 04:44 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 78900 ug/L 11/28/17 00:445000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 164000 ug/L 11/20/17 23:4225000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW3R Lab ID: 92363879005 Collected: 11/16/17 10:30 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 11/27/17 20:06 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2650 ug/L 11/23/17 00:01 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:00 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW5R Lab ID: 92363879006 Collected: 11/16/17 14:20 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 14:20 12/13/17 14:081
Field pH 6.1 Std. Units 12/13/17 14:080.10 1
Field Temperature 16.5 deg C 12/13/17 14:080.50 1
Static Water Level 11.42 feet 12/13/17 14:081
Field Specific Conductance 176.8 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 5.95 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 30 feet 12/13/17 14:081
REDOX 70.4 mV 12/13/17 14:081
Turbidity 0.92 NTU 12/13/17 14:081.0 1
Odor NONE 12/13/17 14:081
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:23 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:23 7440-38-211/21/17 12:0010.0 1
Barium 53.2 ug/L 12/07/17 02:23 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:23 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:23 7440-43-911/21/17 12:001.0 1
Chromium 10.2 ug/L 12/07/17 02:23 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:23 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:23 7440-50-811/21/17 12:005.0 1
Iron 37.9J ug/L 12/07/17 02:23 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:23 7439-92-111/21/17 12:005.0 1
Manganese 4.2J ug/L 12/07/17 02:23 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:23 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:23 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:23 7440-22-411/21/17 12:005.0 1
Sodium 13500 ug/L 12/07/17 02:23 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:23 7440-31-511/21/17 12:005.0 1
Vanadium 4.9J ug/L 12/07/17 02:23 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 02:23 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:46 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:31 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 05:01 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 05:01 75-05-850.0 1
Acrolein ND ug/L 11/26/17 05:01 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 05:01 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 05:01 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW5R Lab ID: 92363879006 Collected: 11/16/17 14:20 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 05:01 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 05:01 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 05:01 75-27-41.0 1
Bromoform ND ug/L 11/26/17 05:01 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 05:01 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 05:01 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 05:01 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 05:01 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 05:01 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 05:01 75-00-31.0 1
Chloroform ND ug/L 11/26/17 05:01 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 05:01 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 05:01 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 05:01 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 05:01 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 05:01 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 05:01 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 05:01 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 05:01 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 05:01 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 05:01 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 05:01 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 05:01 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 05:01 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 05:01 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 05:01 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 05:01 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 05:01 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 05:01 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 05:01 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 05:01 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 05:01 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 05:01 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 05:01 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 05:01 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 05:01 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 05:01 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 05:01 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 05:01 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 05:01 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 05:01 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 05:01 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 05:01 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 05:01 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 05:01 107-12-020.0 1
Styrene ND ug/L 11/26/17 05:01 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 05:01 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW5R Lab ID: 92363879006 Collected: 11/16/17 14:20 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 05:01 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 05:01 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 05:01 109-99-910.0 1
Toluene ND ug/L 11/26/17 05:01 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 05:01 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 05:01 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 05:01 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 05:01 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 05:01 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 05:01 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 05:01 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 05:01 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 05:01 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 05:01 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %11/26/17 05:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %11/26/17 05:01 17060-07-070-130 1
Toluene-d8 (S)108 %11/26/17 05:01 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 33500 ug/L 11/28/17 00:555000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 144000 ug/L 11/20/17 23:4225000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 7830 ug/L 11/27/17 20:57 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 16200 ug/L 11/23/17 00:03 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:02 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW13 Lab ID: 92363879007 Collected: 11/16/17 15:20 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 15:20 12/13/17 14:081
Field pH 5.6 Std. Units 12/13/17 14:080.10 1
Field Temperature 17.2 deg C 12/13/17 14:080.50 1
Static Water Level 8.96 feet 12/13/17 14:081
Field Specific Conductance 111.4 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 4.3 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 20 feet 12/13/17 14:081
REDOX 182.2 mV 12/13/17 14:081
Turbidity 2.8 NTU 12/13/17 14:081.0 1
Odor none 12/13/17 14:081
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:27 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:27 7440-38-211/21/17 12:0010.0 1
Barium 116 ug/L 12/07/17 02:27 7440-39-311/21/17 12:005.0 1
Beryllium 0.52J ug/L 12/07/17 02:27 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:27 7440-43-911/21/17 12:001.0 1
Chromium 3.8J ug/L 12/07/17 02:27 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:27 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:27 7440-50-811/21/17 12:005.0 1
Iron 193 ug/L 12/07/17 02:27 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:27 7439-92-111/21/17 12:005.0 1
Manganese 17.9 ug/L 12/07/17 02:27 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:27 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:27 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:27 7440-22-411/21/17 12:005.0 1
Sodium 9740 ug/L 12/07/17 02:27 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:27 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:27 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 02:27 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:48 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:33 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 05:19 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 05:19 75-05-850.0 1
Acrolein ND ug/L 11/26/17 05:19 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 05:19 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 05:19 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW13 Lab ID: 92363879007 Collected: 11/16/17 15:20 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 05:19 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 05:19 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 05:19 75-27-41.0 1
Bromoform ND ug/L 11/26/17 05:19 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 05:19 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 05:19 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 05:19 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 05:19 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 05:19 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 05:19 75-00-31.0 1
Chloroform ND ug/L 11/26/17 05:19 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 05:19 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 05:19 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 05:19 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 05:19 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 05:19 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 05:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 05:19 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 05:19 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 05:19 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 05:19 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 05:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 05:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 05:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 05:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 05:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 05:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 05:19 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 05:19 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 05:19 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 05:19 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 05:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 05:19 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 05:19 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 05:19 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 05:19 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 05:19 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 05:19 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 05:19 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 05:19 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 05:19 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 05:19 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 05:19 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 05:19 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 05:19 107-12-020.0 1
Styrene ND ug/L 11/26/17 05:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 05:19 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW13 Lab ID: 92363879007 Collected: 11/16/17 15:20 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 05:19 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 05:19 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 05:19 109-99-910.0 1
Toluene ND ug/L 11/26/17 05:19 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 05:19 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 05:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 05:19 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 05:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 05:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 05:19 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 05:19 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 05:19 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 05:19 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 05:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/26/17 05:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %11/26/17 05:19 17060-07-070-130 1
Toluene-d8 (S)109 %11/26/17 05:19 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 44600 ug/L 11/28/17 01:065000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 90000 ug/L 11/20/17 23:4225000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4960 ug/L 11/27/17 22:24 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4770 ug/L 11/23/17 00:06 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:05 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW14 Lab ID: 92363879008 Collected: 11/16/17 16:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 16:10 12/13/17 14:081
Field pH 5.5 Std. Units 12/13/17 14:080.10 1
Field Temperature 16.1 deg C 12/13/17 14:080.50 1
Static Water Level 51.95 feet 12/13/17 14:081
Field Specific Conductance 172.7 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 3.3 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 60 feet 12/13/17 14:081
REDOX 215.5 mV 12/13/17 14:081
Turbidity 2.4 NTU 12/13/17 14:081.0 1
Odor NONE 12/13/17 14:081
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:31 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:31 7440-38-211/21/17 12:0010.0 1
Barium 214 ug/L 12/07/17 02:31 7440-39-311/21/17 12:005.0 1
Beryllium 0.54J ug/L 12/07/17 02:31 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:31 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 02:31 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:31 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:31 7440-50-811/21/17 12:005.0 1
Iron 93.9 ug/L 12/07/17 02:31 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:31 7439-92-111/21/17 12:005.0 1
Manganese 18.4 ug/L 12/07/17 02:31 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:31 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:31 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:31 7440-22-411/21/17 12:005.0 1
Sodium 17100 ug/L 12/07/17 02:31 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:31 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:31 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 02:31 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 21:51 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:36 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 05:36 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 05:36 75-05-850.0 1
Acrolein ND ug/L 11/26/17 05:36 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 05:36 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 05:36 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW14 Lab ID: 92363879008 Collected: 11/16/17 16:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 05:36 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 05:36 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 05:36 75-27-41.0 1
Bromoform ND ug/L 11/26/17 05:36 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 05:36 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 05:36 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 05:36 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 05:36 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 05:36 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 05:36 75-00-31.0 1
Chloroform ND ug/L 11/26/17 05:36 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 05:36 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 05:36 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 05:36 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 05:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 05:36 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 05:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 05:36 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 05:36 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 05:36 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 05:36 110-57-61.0 1
Dichlorodifluoromethane 3.9 ug/L 11/26/17 05:36 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 05:36 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 05:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 05:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 05:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 05:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 05:36 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 05:36 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 05:36 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 05:36 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 05:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 05:36 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 05:36 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 05:36 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 05:36 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 05:36 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 05:36 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 05:36 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 05:36 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 05:36 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 05:36 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 05:36 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 05:36 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 05:36 107-12-020.0 1
Styrene ND ug/L 11/26/17 05:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 05:36 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW14 Lab ID: 92363879008 Collected: 11/16/17 16:10 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 05:36 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 05:36 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 05:36 109-99-910.0 1
Toluene ND ug/L 11/26/17 05:36 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 05:36 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 05:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 05:36 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 05:36 79-01-61.0 1
Trichlorofluoromethane 0.87J ug/L 11/26/17 05:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 05:36 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 05:36 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 05:36 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 05:36 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 05:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/26/17 05:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %11/26/17 05:36 17060-07-070-130 1
Toluene-d8 (S)108 %11/26/17 05:36 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 63500 ug/L 11/28/17 01:185000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 142000 ug/L 11/20/17 23:4225000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 11/27/17 22:41 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3620 ug/L 11/23/17 00:07 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:06 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW7 Lab ID: 92363879009 Collected: 11/16/17 11:45 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:081
Collected Date 11/16/17 12/13/17 14:081
Collected Time 11:45 12/13/17 14:081
Field pH 5.6 Std. Units 12/13/17 14:080.10 1
Field Temperature 16.3 deg C 12/13/17 14:080.50 1
Static Water Level 36.61 feet 12/13/17 14:081
Field Specific Conductance 288.4 umhos/cm 12/13/17 14:081.0 1
Oxygen, Dissolved 0.5 mg/L 12/13/17 14:08 7782-44-71
Total Well Depth 48 feet 12/13/17 14:081
REDOX 135.5 mV 12/13/17 14:081
Turbidity 0.1 NTU 12/13/17 14:081.0 1
Appearance CLEAR 12/13/17 14:081
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/29/17 16:00 309-00-211/22/17 17:100.050 1
alpha-BHC ND ug/L 11/29/17 16:00 319-84-611/22/17 17:100.050 1
beta-BHC ND ug/L 11/29/17 16:00 319-85-711/22/17 17:100.050 1
delta-BHC ND ug/L 11/29/17 16:00 319-86-811/22/17 17:100.050 1
gamma-BHC (Lindane)ND ug/L 11/29/17 16:00 58-89-911/22/17 17:100.050 1
Chlordane (Technical)ND ug/L 11/29/17 16:00 57-74-911/22/17 17:100.20 1
4,4'-DDD ND ug/L 11/29/17 16:00 72-54-811/22/17 17:100.050 1
4,4'-DDE ND ug/L 11/29/17 16:00 72-55-911/22/17 17:100.050 1
4,4'-DDT ND ug/L 11/29/17 16:00 50-29-311/22/17 17:100.050 1
Dieldrin ND ug/L 11/29/17 16:00 60-57-111/22/17 17:100.050 1
Endosulfan I ND ug/L 11/29/17 16:00 959-98-811/22/17 17:100.050 1
Endosulfan II ND ug/L 11/29/17 16:00 33213-65-911/22/17 17:100.050 1
Endosulfan sulfate ND ug/L 11/29/17 16:00 1031-07-811/22/17 17:100.050 1
Endrin ND ug/L 11/29/17 16:00 72-20-811/22/17 17:100.050 1
Endrin aldehyde ND ug/L 11/29/17 16:00 7421-93-411/22/17 17:100.050 1
Heptachlor ND ug/L 11/29/17 16:00 76-44-811/22/17 17:100.050 1
Heptachlor epoxide ND ug/L 11/29/17 16:00 1024-57-311/22/17 17:100.050 1
Methoxychlor ND ug/L 11/29/17 16:00 72-43-511/22/17 17:100.15 1
Toxaphene ND ug/L 11/29/17 16:00 8001-35-211/22/17 17:100.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %11/29/17 16:00 877-09-811/22/17 17:1020-130 1
Decachlorobiphenyl (S)71 %11/29/17 16:00 2051-24-311/22/17 17:1020-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:35 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:35 7440-38-211/21/17 12:0010.0 1
Barium 152 ug/L 12/07/17 02:35 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:35 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:35 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 02:35 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:35 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:35 7440-50-811/21/17 12:005.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW7 Lab ID: 92363879009 Collected: 11/16/17 11:45 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Iron 25.0J ug/L 12/07/17 02:35 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:35 7439-92-111/21/17 12:005.0 1
Manganese 43.0 ug/L 12/07/17 02:35 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:35 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:35 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:35 7440-22-411/21/17 12:005.0 1
Sodium 15300 ug/L 12/07/17 02:35 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:35 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:35 7440-62-211/21/17 12:005.0 1
Zinc 5.0J ug/L 12/07/17 02:35 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:01 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:43 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 05:53 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 05:53 75-05-850.0 1
Acrolein ND ug/L 11/26/17 05:53 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 05:53 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 05:53 107-05-12.0 1
Benzene 0.38J ug/L 11/26/17 05:53 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 05:53 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 05:53 75-27-41.0 1
Bromoform ND ug/L 11/26/17 05:53 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 05:53 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 05:53 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 05:53 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 05:53 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 05:53 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 05:53 75-00-31.0 1
Chloroform ND ug/L 11/26/17 05:53 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 05:53 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 05:53 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 05:53 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 05:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 05:53 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 05:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 05:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 05:53 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 05:53 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 05:53 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 05:53 75-71-81.0 1
1,1-Dichloroethane 1.4 ug/L 11/26/17 05:53 75-34-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW7 Lab ID: 92363879009 Collected: 11/16/17 11:45 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloroethane ND ug/L 11/26/17 05:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 05:53 75-35-41.0 1
cis-1,2-Dichloroethene 1.1 ug/L 11/26/17 05:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 05:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 05:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 05:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 05:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 05:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 05:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 05:53 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 05:53 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 05:53 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 05:53 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 05:53 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 05:53 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 05:53 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 05:53 126-98-710.0 1
Methylene Chloride 4.6 ug/L 11/26/17 05:53 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 11/26/17 05:53 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 05:53 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 05:53 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 05:53 107-12-020.0 1
Styrene ND ug/L 11/26/17 05:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 05:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 05:53 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 05:53 127-18-41.0 1
Tetrahydrofuran 20.1 ug/L 11/26/17 05:53 109-99-910.0 1
Toluene ND ug/L 11/26/17 05:53 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 05:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 05:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 05:53 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 05:53 79-01-61.0 1
Trichlorofluoromethane 1.6 ug/L 11/26/17 05:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 05:53 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 05:53 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 05:53 75-01-41.0 1
m&p-Xylene 1.4J ug/L 11/26/17 05:53 179601-23-12.0 1
o-Xylene 0.68J ug/L 11/26/17 05:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/26/17 05:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %11/26/17 05:53 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 05:53 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 80400 ug/L 11/28/17 01:305000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 87
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92363879
OSR
Sample: 3412-MW7 Lab ID: 92363879009 Collected: 11/16/17 11:45 Received: 11/17/17 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 175000 ug/L 11/20/17 23:4225000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/21/17 22:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 13400 ug/L 11/27/17 22:58 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 7390 ug/L 11/23/17 00:08 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:07 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388398
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154671
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 11/29/17 13:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154672LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154673MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879001
2154674
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 94 75-12597 32.5ND 2.4 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387775
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151277
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
Antimony ug/L ND 5.0 12/07/17 01:38
Arsenic ug/L ND 10.0 12/07/17 01:38
Barium ug/L ND 5.0 12/07/17 01:38
Beryllium ug/L ND 1.0 12/07/17 01:38
Cadmium ug/L ND 1.0 12/07/17 01:38
Chromium ug/L ND 5.0 12/07/17 11:47
Cobalt ug/L ND 5.0 12/07/17 01:38
Copper ug/L ND 5.0 12/07/17 01:38
Iron ug/L ND 50.0 12/07/17 01:38
Lead ug/L ND 5.0 12/07/17 01:38
Manganese ug/L ND 5.0 12/07/17 01:38
Nickel ug/L ND 5.0 12/07/17 01:38
Selenium ug/L ND 10.0 12/07/17 01:38
Silver ug/L ND 5.0 12/07/17 01:38
Sodium ug/L ND 5000 12/07/17 01:38
Tin ug/L ND 5.0 12/07/17 01:38
Vanadium ug/L ND 5.0 12/07/17 01:38
Zinc ug/L ND 10.0 12/07/17 01:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151278LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 479500 96 80-120
Arsenic ug/L 460500 92 80-120
Barium ug/L 479500 96 80-120
Beryllium ug/L 468500 94 80-120
Cadmium ug/L 471500 94 80-120
Chromium ug/L 467500 93 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 486500 97 80-120
Iron ug/L 46705000 93 80-120
Lead ug/L 470500 94 80-120
Manganese ug/L 463500 93 80-120
Nickel ug/L 468500 94 80-120
Selenium ug/L 448500 90 80-120
Silver ug/L 234250 93 80-120
Sodium ug/L 4780J5000 96 80-120
Tin ug/L 477500 95 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151278LABORATORY CONTROL SAMPLE:
LCSSpike
Vanadium ug/L 478500 96 80-120
Zinc ug/L 470500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879001
2151280
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-125101 5500ND483 507
Arsenic ug/L 500 94 75-12598 4500ND470 490
Barium ug/L 500 99 75-125101 2500ND496 509
Beryllium ug/L 500 98 75-125100 2500ND490 500
Cadmium ug/L 500 95 75-125100 5500ND478 501
Chromium ug/L 500 101 75-125101 05003.2J 506 507
Cobalt ug/L 500 99 75-125102 4500ND494 512
Copper ug/L 500 97 75-125102 5500ND485 511
Iron ug/L 5000 99 75-125100 15000ND4960 5020
Lead ug/L 500 97 75-125101 4500ND485 503
Manganese ug/L 500 100 75-125100 0500ND500 499
Nickel ug/L 500 97 75-125101 4500ND483 503
Selenium ug/L 500 89 75-12593 5500ND449 470
Silver ug/L 250 97 75-12599 3250ND242 249
Sodium ug/L 5000 98 75-125100 25000539J5440 5560
Tin ug/L 500 99 75-125103 4500ND494 514
Vanadium ug/L 500 102 75-125102 0500ND511 511
Zinc ug/L 500 99 75-125102 3500ND498 511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387486
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2149919
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
Thallium ug/L ND 0.10 11/21/17 21:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2149920LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 93.1100 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2149921MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879001
2149922
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-125101 1100ND100 101
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2149923MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018002
2149924
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-125102 2100ND100 102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388168
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153766
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/26/17 01:33
1,1,1-Trichloroethane ug/L ND 1.0 11/26/17 01:33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/26/17 01:33
1,1,2-Trichloroethane ug/L ND 1.0 11/26/17 01:33
1,1-Dichloroethane ug/L ND 1.0 11/26/17 01:33
1,1-Dichloroethene ug/L ND 1.0 11/26/17 01:33
1,1-Dichloropropene ug/L ND 1.0 11/26/17 01:33
1,2,3-Trichloropropane ug/L ND 1.0 11/26/17 01:33
1,2,4-Trichlorobenzene ug/L ND 1.0 11/26/17 01:33
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/26/17 01:33
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/26/17 01:33
1,2-Dichlorobenzene ug/L ND 1.0 11/26/17 01:33
1,2-Dichloroethane ug/L ND 1.0 11/26/17 01:33
1,2-Dichloropropane ug/L ND 1.0 11/26/17 01:33
1,3-Dichlorobenzene ug/L ND 1.0 11/26/17 01:33
1,3-Dichloropropane ug/L ND 1.0 11/26/17 01:33
1,4-Dichlorobenzene ug/L ND 1.0 11/26/17 01:33
2,2-Dichloropropane ug/L ND 1.0 11/26/17 01:33
2-Butanone (MEK)ug/L ND 5.0 11/26/17 01:33
2-Hexanone ug/L ND 5.0 11/26/17 01:33
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/26/17 01:33
Acetone ug/L ND 25.0 11/26/17 01:33
Acetonitrile ug/L ND 50.0 11/26/17 01:33
Acrolein ug/L ND 10.0 11/26/17 01:33
Acrylonitrile ug/L ND 10.0 11/26/17 01:33
Allyl chloride ug/L ND 2.0 11/26/17 01:33
Benzene ug/L ND 1.0 11/26/17 01:33
Bromochloromethane ug/L ND 1.0 11/26/17 01:33
Bromodichloromethane ug/L ND 1.0 11/26/17 01:33
Bromoform ug/L ND 1.0 11/26/17 01:33
Bromomethane ug/L ND 2.0 11/26/17 01:33
Carbon disulfide ug/L ND 2.0 11/26/17 01:33
Carbon tetrachloride ug/L ND 1.0 11/26/17 01:33
Chlorobenzene ug/L ND 1.0 11/26/17 01:33
Chloroethane ug/L ND 1.0 11/26/17 01:33
Chloroform ug/L ND 1.0 11/26/17 01:33
Chloromethane ug/L ND 1.0 11/26/17 01:33
Chloroprene ug/L ND 5.0 11/26/17 01:33
cis-1,2-Dichloroethene ug/L ND 1.0 11/26/17 01:33
cis-1,3-Dichloropropene ug/L ND 1.0 11/26/17 01:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153766
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 11/26/17 01:33
Dibromomethane ug/L ND 1.0 11/26/17 01:33
Dichlorodifluoromethane ug/L ND 1.0 11/26/17 01:33
Ethyl methacrylate ug/L ND 1.0 11/26/17 01:33
Ethylbenzene ug/L ND 1.0 11/26/17 01:33
Hexachloro-1,3-butadiene ug/L ND 1.0 11/26/17 01:33
Iodomethane ug/L ND 5.0 11/26/17 01:33
Isobutanol ug/L ND 100 11/26/17 01:33
m&p-Xylene ug/L ND 2.0 11/26/17 01:33
Methacrylonitrile ug/L ND 10.0 11/26/17 01:33
Methyl methacrylate ug/L ND 2.0 11/26/17 01:33
Methylene Chloride ug/L ND 1.0 11/26/17 01:33
Naphthalene ug/L ND 1.0 11/26/17 01:33
o-Xylene ug/L ND 1.0 11/26/17 01:33
Propionitrile ug/L ND 20.0 11/26/17 01:33
Styrene ug/L ND 1.0 11/26/17 01:33
Tetrachloroethene ug/L ND 1.0 11/26/17 01:33
Tetrahydrofuran ug/L ND 10.0 11/26/17 01:33
Toluene ug/L ND 1.0 11/26/17 01:33
trans-1,2-Dichloroethene ug/L ND 1.0 11/26/17 01:33
trans-1,3-Dichloropropene ug/L ND 1.0 11/26/17 01:33
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/26/17 01:33
Trichloroethene ug/L ND 1.0 11/26/17 01:33
Trichlorofluoromethane ug/L ND 1.0 11/26/17 01:33
Vinyl acetate ug/L ND 2.0 11/26/17 01:33
Vinyl chloride ug/L ND 1.0 11/26/17 01:33
1,2-Dichloroethane-d4 (S)%88 70-130 11/26/17 01:33
4-Bromofluorobenzene (S)%101 70-130 11/26/17 01:33
Toluene-d8 (S)%108 70-130 11/26/17 01:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153767LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.450 93 80-125
1,1,1-Trichloroethane ug/L 48.750 97 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 53.850 108 85-125
1,1-Dichloroethane ug/L 49.250 98 73-126
1,1-Dichloroethene ug/L 53.550 107 66-135
1,1-Dichloropropene ug/L 48.250 96 74-135
1,2,3-Trichloropropane ug/L 47.350 95 75-130
1,2,4-Trichlorobenzene ug/L 50.050 100 75-134
1,2-Dibromo-3-chloropropane ug/L 43.550 87 71-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153767LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromoethane (EDB)ug/L 49.650 99 83-124
1,2-Dichlorobenzene ug/L 47.650 95 80-133
1,2-Dichloroethane ug/L 50.850 102 67-128
1,2-Dichloropropane ug/L 53.750 107 75-132
1,3-Dichlorobenzene ug/L 47.850 96 77-130
1,3-Dichloropropane ug/L 50.250 100 76-131
1,4-Dichlorobenzene ug/L 48.150 96 78-130
2,2-Dichloropropane ug/L 31.150 62 40-160
2-Butanone (MEK)ug/L 92.7100 93 61-144
2-Hexanone ug/L 95.5100 96 68-143
4-Methyl-2-pentanone (MIBK)ug/L 89.2100 89 72-135
Acetone ug/L 94.8100 95 48-146
Acetonitrile ug/L 457500 91 62-150
Acrolein ug/L 256250 102 24-160
Acrylonitrile ug/L 228250 91 40-160
Allyl chloride ug/L 46.250 92 66-137
Benzene ug/L 51.050 102 80-125
Bromochloromethane ug/L 52.550 105 71-125
Bromodichloromethane ug/L 52.850 106 78-124
Bromoform ug/L 45.650 91 71-128
Bromomethane ug/L 47.050 94 40-160
Carbon disulfide ug/L 49.850 100 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 49.750 99 81-122
Chloroethane ug/L 51.250 102 39-148
Chloroform ug/L 50.450 101 73-127
Chloromethane ug/L 44.550 89 44-146
Chloroprene ug/L 49.750 99 75-145
cis-1,2-Dichloroethene ug/L 52.750 105 74-124
cis-1,3-Dichloropropene ug/L 47.550 95 72-132
Dibromochloromethane ug/L 47.650 95 78-125
Dibromomethane ug/L 49.550 99 82-120
Dichlorodifluoromethane ug/L 50.850 102 34-157
Ethyl methacrylate ug/L 46.950 94 82-121
Ethylbenzene ug/L 49.150 98 79-121
Hexachloro-1,3-butadiene ug/L 47.350 95 72-131
Iodomethane ug/L 91.9100 92 39-154
Isobutanol ug/L 8761000 88 34-160
m&p-Xylene ug/L 97.5100 97 81-124
Methacrylonitrile ug/L 480500 96 74-134
Methyl methacrylate ug/L 50.750 101 84-124
Methylene Chloride ug/L 46.750 93 64-133
Naphthalene ug/L 49.650 99 73-133
o-Xylene ug/L 49.850 100 79-131
Propionitrile ug/L 519500 104 73-140
Styrene ug/L 49.650 99 84-126
Tetrachloroethene ug/L 51.150 102 78-122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153767LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrahydrofuran ug/L 472500 94 69-148
Toluene ug/L 46.450 93 80-121
trans-1,2-Dichloroethene ug/L 48.850 98 71-127
trans-1,3-Dichloropropene ug/L 43.550 87 69-141
trans-1,4-Dichloro-2-butene ug/L 42.150 84 40-160
Trichloroethene ug/L 54.350 109 78-122
Trichlorofluoromethane ug/L 51.350 103 53-137
Vinyl acetate ug/L 94.9100 95 40-160
Vinyl chloride ug/L 52.750 105 58-137
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153768MATRIX SPIKE SAMPLE:
MSSpike
Result
92363938001
1,1,1,2-Tetrachloroethane ug/L 17.420 87 70-130ND
1,1,1-Trichloroethane ug/L 21.820 109 70-130ND
1,1,2,2-Tetrachloroethane ug/L 17.920 90 70-130ND
1,1,2-Trichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 24.220 121 70-166ND
1,1-Dichloropropene ug/L 21.920 109 70-130ND
1,2,3-Trichloropropane ug/L 18.420 92 70-130ND
1,2,4-Trichlorobenzene ug/L 20.520 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 14.120 71 70-130ND
1,2-Dibromoethane (EDB)ug/L 17.620 88 70-130ND
1,2-Dichlorobenzene ug/L 19.220 96 70-130ND
1,2-Dichloroethane ug/L 21.520 108 70-130ND
1,2-Dichloropropane ug/L 21.220 106 70-130ND
1,3-Dichlorobenzene ug/L 19.120 96 70-130ND
1,3-Dichloropropane ug/L 18.220 91 70-130ND
1,4-Dichlorobenzene ug/L 19.320 97 70-130ND
2,2-Dichloropropane ug/L 18.620 93 70-130ND
2-Butanone (MEK)ug/L 34.140 85 70-130ND
2-Hexanone ug/L 35.140 88 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 86 70-130ND
Acetone ug/L 39.540 99 70-130ND
Acrylonitrile ug/L 105100 105 70-130ND
Benzene ug/L 20.920 105 70-148ND
Bromochloromethane ug/L 23.020 115 70-130ND
Bromodichloromethane ug/L 21.120 106 70-130ND
Bromoform ug/L 16.920 84 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.920 114 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153768MATRIX SPIKE SAMPLE:
MSSpike
Result
92363938001
Carbon tetrachloride ug/L 22.620 113 70-130ND
Chlorobenzene ug/L 20.020 100 70-146ND
Chloroethane ug/L 25.420 127 70-130ND
Chloroform ug/L 21.520 107 70-130ND
Chloromethane ug/L 21.920 109 70-130ND
cis-1,2-Dichloroethene ug/L 22.920 114 70-130ND
cis-1,3-Dichloropropene ug/L 18.220 91 70-130ND
Dibromochloromethane ug/L 17.420 87 70-130ND
Dibromomethane ug/L 20.920 105 70-130ND
Dichlorodifluoromethane ug/L 29.5 M120147 70-130ND
Ethylbenzene ug/L 20.020 100 70-130ND
Hexachloro-1,3-butadiene ug/L 21.220 106 70-130ND
Iodomethane ug/L 37.640 94 70-130ND
m&p-Xylene ug/L 40.140 100 70-130ND
Methylene Chloride ug/L 21.120 106 70-130ND
Naphthalene ug/L 18.820 94 70-130ND
o-Xylene ug/L 20.120 100 70-130ND
Styrene ug/L 19.420 97 70-130ND
Tetrachloroethene ug/L 31.920 107 70-13010.5
Tetrahydrofuran ug/L 179200 89 70-130ND
Toluene ug/L 20.520 103 70-155ND
trans-1,2-Dichloroethene ug/L 23.420 117 70-130ND
trans-1,3-Dichloropropene ug/L 16.020 80 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.920 80 70-130ND
Trichloroethene ug/L 23.520 118 69-151ND
Trichlorofluoromethane ug/L 25.420 127 70-130ND
Vinyl acetate ug/L 33.540 84 70-130ND
Vinyl chloride ug/L 26.5 M120132 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92363938002
2153769SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363938002
2153769SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L 0.72J0.66J
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L 16.2 216.5
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L 6.3 26.2
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363938002
2153769SAMPLE DUPLICATE:
1,2-Dichloroethane-d4 (S)%91 292
4-Bromofluorobenzene (S)%102 0103
Toluene-d8 (S)%108 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387993
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples: 92363879001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2152632
Associated Lab Samples:92363879001
Matrix: Water
Analyzed
4,4'-DDD ug/L ND 0.050 11/25/17 20:42
4,4'-DDE ug/L ND 0.050 11/25/17 20:42
4,4'-DDT ug/L ND 0.050 11/25/17 20:42
Aldrin ug/L ND 0.050 11/25/17 20:42
alpha-BHC ug/L ND 0.050 11/25/17 20:42
beta-BHC ug/L ND 0.050 11/25/17 20:42
Chlordane (Technical)ug/L ND 0.20 11/25/17 20:42
delta-BHC ug/L ND 0.050 11/25/17 20:42
Dieldrin ug/L ND 0.050 11/25/17 20:42
Endosulfan I ug/L ND 0.050 11/25/17 20:42
Endosulfan II ug/L ND 0.050 11/25/17 20:42
Endosulfan sulfate ug/L ND 0.050 11/25/17 20:42
Endrin ug/L ND 0.050 11/25/17 20:42
Endrin aldehyde ug/L ND 0.050 11/25/17 20:42
gamma-BHC (Lindane)ug/L ND 0.050 11/25/17 20:42
Heptachlor ug/L ND 0.050 11/25/17 20:42
Heptachlor epoxide ug/L ND 0.050 11/25/17 20:42
Methoxychlor ug/L ND 0.15 11/25/17 20:42
Toxaphene ug/L ND 0.20 11/25/17 20:42
Decachlorobiphenyl (S)%69 20-130 11/25/17 20:42
Tetrachloro-m-xylene (S)%81 20-130 11/25/17 20:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2152633LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.24.25 98 20-150
4,4'-DDE ug/L 0.23.25 93 20-150
4,4'-DDT ug/L 0.25.25 101 20-150
Aldrin ug/L 0.19.25 78 20-150
alpha-BHC ug/L 0.23.25 94 20-150
beta-BHC ug/L 0.21.25 83 20-150
delta-BHC ug/L 0.25.25 100 20-150
Dieldrin ug/L 0.23.25 94 20-150
Endosulfan I ug/L 0.24.25 97 20-150
Endosulfan II ug/L 0.23.25 95 20-150
Endosulfan sulfate ug/L 0.24.25 96 20-150
Endrin ug/L 0.24.25 98 20-150
Endrin aldehyde ug/L 0.19.25 76 20-150
gamma-BHC (Lindane)ug/L 0.24.25 96 20-150
Heptachlor ug/L 0.20.25 82 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2152633LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.24.25 97 20-150
Methoxychlor ug/L 0.74.74 100 20-150
Decachlorobiphenyl (S)%82 20-130
Tetrachloro-m-xylene (S)%94 20-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2152634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363874006
2152635
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4,4'-DDD ug/L .5 100 20-15097 3.5ND 0.49 0.48
4,4'-DDE ug/L .5 93 20-15089 5.5ND 0.46 0.44
4,4'-DDT ug/L .5 104 20-15099 4.5ND 0.51 0.49
Aldrin ug/L .5 83 20-15072 13.5ND 0.41 0.36
alpha-BHC ug/L .5 88 20-15073 18.5ND 0.43 0.36
beta-BHC ug/L .5 81 20-15074 8.5ND 0.40 0.37
delta-BHC ug/L .5 99 20-15090 9.5ND 0.49 0.45
Dieldrin ug/L .5 93 20-15087 7.5ND 0.46 0.43
Endosulfan I ug/L .5 95 20-15089 7.5ND 0.47 0.44
Endosulfan II ug/L .5 96 20-15087 10.5ND 0.48 0.43
Endosulfan sulfate ug/L .5 96 20-15086 10.5ND 0.47 0.43
Endrin ug/L .5 101 20-15094 7.5ND 0.50 0.47
Endrin aldehyde ug/L .5 77 20-15066 16.5ND 0.38 0.33
gamma-BHC (Lindane)ug/L .5 93 20-15081 14.5ND 0.46 0.40
Heptachlor ug/L .5 83 20-15074 12.5ND 0.41 0.37
Heptachlor epoxide ug/L .5 97 20-15091 6.5ND 0.48 0.45
Methoxychlor ug/L 1.5 103 20-15094 91.5ND 1.5 1.4
Decachlorobiphenyl (S)%67 20-13058
Tetrachloro-m-xylene (S)%84 20-13066
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388080
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples: 92363879002, 92363879003, 92363879004, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153200
Associated Lab Samples:92363879002, 92363879003, 92363879004, 92363879009
Matrix: Water
Analyzed
4,4'-DDD ug/L ND 0.050 11/29/17 19:03
4,4'-DDE ug/L ND 0.050 11/29/17 19:03
4,4'-DDT ug/L ND 0.050 11/29/17 19:03
Aldrin ug/L ND 0.050 11/29/17 19:03
alpha-BHC ug/L ND 0.050 11/29/17 19:03
beta-BHC ug/L ND 0.050 11/29/17 19:03
Chlordane (Technical)ug/L ND 0.20 11/29/17 19:03
delta-BHC ug/L ND 0.050 11/29/17 19:03
Dieldrin ug/L ND 0.050 11/29/17 19:03
Endosulfan I ug/L ND 0.050 11/29/17 19:03
Endosulfan II ug/L ND 0.050 11/29/17 19:03
Endosulfan sulfate ug/L ND 0.050 11/29/17 19:03
Endrin ug/L ND 0.050 11/29/17 19:03
Endrin aldehyde ug/L ND 0.050 11/29/17 19:03
gamma-BHC (Lindane)ug/L ND 0.050 11/29/17 19:03
Heptachlor ug/L ND 0.050 11/29/17 19:03
Heptachlor epoxide ug/L ND 0.050 11/29/17 19:03
Methoxychlor ug/L ND 0.15 11/29/17 19:03
Toxaphene ug/L ND 0.20 11/29/17 19:03
Decachlorobiphenyl (S)%75 20-130 11/29/17 19:03
Tetrachloro-m-xylene (S)%77 20-130 11/29/17 19:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153201LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.23.25 93 20-150
4,4'-DDE ug/L 0.21.25 86 20-150
4,4'-DDT ug/L 0.25.25 100 20-150
Aldrin ug/L 0.20.25 79 20-150
alpha-BHC ug/L 0.21.25 85 20-150
beta-BHC ug/L 0.18.25 73 20-150
delta-BHC ug/L 0.23.25 92 20-150
Dieldrin ug/L 0.21.25 87 20-150
Endosulfan I ug/L 0.22.25 88 20-150
Endosulfan II ug/L 0.23.25 93 20-150
Endosulfan sulfate ug/L 0.24.25 96 20-150
Endrin ug/L 0.24.25 96 20-150
Endrin aldehyde ug/L 0.24.25 95 20-150
gamma-BHC (Lindane)ug/L 0.22.25 87 20-150
Heptachlor ug/L 0.21.25 84 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153201LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.22.25 88 20-150
Methoxychlor ug/L 0.79.74 107 20-150
Decachlorobiphenyl (S)%81 20-130
Tetrachloro-m-xylene (S)%89 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153202MATRIX SPIKE SAMPLE:
MSSpike
Result
92364018001
4,4'-DDD ug/L 0.33.25 133 20-150ND
4,4'-DDE ug/L 0.28.25 112 20-150ND
4,4'-DDT ug/L 0.41 M1.25 167 20-150ND
Aldrin ug/L 0.19.25 78 20-150ND
alpha-BHC ug/L 0.21.25 85 20-150ND
beta-BHC ug/L 0.16.25 63 20-150ND
delta-BHC ug/L 0.23.25 91 20-150ND
Dieldrin ug/L 0.26.25 107 20-150ND
Endosulfan I ug/L 0.26.25 105 20-150ND
Endosulfan II ug/L 0.28.25 111 20-150ND
Endosulfan sulfate ug/L 0.31.25 127 20-150ND
Endrin ug/L 0.30.25 119 20-150ND
Endrin aldehyde ug/L 0.31.25 126 20-150ND
gamma-BHC (Lindane)ug/L 0.21.25 85 20-150ND
Heptachlor ug/L 0.24.25 95 20-150ND
Heptachlor epoxide ug/L 0.24.25 96 20-150ND
Methoxychlor ug/L 1.4 M1.74 184 20-150ND
Decachlorobiphenyl (S)%102 20-130
Tetrachloro-m-xylene (S)%72 20-130
Parameter Units
Dup
Result QualifiersRPDResult
92364340003
2153203SAMPLE DUPLICATE:
4,4'-DDD ug/L NDND
4,4'-DDE ug/L NDND
4,4'-DDT ug/L NDND
Aldrin ug/L NDND
alpha-BHC ug/L NDND
beta-BHC ug/L NDND
Chlordane (Technical)ug/L NDND
delta-BHC ug/L NDND
Dieldrin ug/L NDND
Endosulfan I ug/L NDND
Endosulfan II ug/L NDND
Endosulfan sulfate ug/L NDND
Endrin ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92364340003
2153203SAMPLE DUPLICATE:
Endrin aldehyde ug/L NDND
gamma-BHC (Lindane)ug/L NDND
Heptachlor ug/L NDND
Heptachlor epoxide ug/L NDND
Methoxychlor ug/L NDND
Toxaphene ug/L NDND
Decachlorobiphenyl (S)%59 1367
Tetrachloro-m-xylene (S)%78 1590
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388331
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154375
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004
Matrix: Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 11/29/17 23:18
PCB-1221 (Aroclor 1221)ug/L ND 0.50 11/29/17 23:18
PCB-1232 (Aroclor 1232)ug/L ND 0.50 11/29/17 23:18
PCB-1242 (Aroclor 1242)ug/L ND 0.50 11/29/17 23:18
PCB-1248 (Aroclor 1248)ug/L ND 0.50 11/29/17 23:18
PCB-1254 (Aroclor 1254)ug/L ND 0.50 11/29/17 23:18
PCB-1260 (Aroclor 1260)ug/L ND 0.50 11/29/17 23:18
Decachlorobiphenyl (S)%70 10-132 11/29/17 23:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154376LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 3.45 67 50-150
PCB-1260 (Aroclor 1260)ug/L 4.55 90 50-150
Decachlorobiphenyl (S)%55 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2154377MATRIX SPIKE SAMPLE:
MSSpike
Result
92363879001
PCB-1016 (Aroclor 1016)ug/L 5.05 99 50-150ND
PCB-1260 (Aroclor 1260)ug/L 4.05 79 50-150ND
Decachlorobiphenyl (S)%25 10-132
Parameter Units
Dup
Result QualifiersRPDResult
92363879002
2154378SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L NDND
PCB-1221 (Aroclor 1221)ug/L NDND
PCB-1232 (Aroclor 1232)ug/L NDND
PCB-1242 (Aroclor 1242)ug/L NDND
PCB-1248 (Aroclor 1248)ug/L NDND
PCB-1254 (Aroclor 1254)ug/L NDND
PCB-1260 (Aroclor 1260)ug/L NDND
Decachlorobiphenyl (S)%60 865
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
406966
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2222026
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004
Matrix: Water
Analyzed
2,4,5-T ug/L ND 0.19 11/28/17 22:57
2,4,5-TP (Silvex)ug/L ND 0.19 11/28/17 22:57
2,4-D ug/L ND 0.94 11/28/17 22:57
Dinoseb ug/L ND 0.19 11/28/17 22:57
Pentachlorophenol ug/L ND 0.028 11/28/17 22:57
2,4-DCAA (S)%88 39-139 11/28/17 22:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2222027LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2224113
2,4,5-T ug/L 1.11.2 93 37-133911.1 2 40
2,4,5-TP (Silvex)ug/L 1.21.2 97 53-134951.1 2 40
2,4-D ug/L 5.76 96 35-124935.6 2 40
Dinoseb ug/L 0.631.2 52 13-116500.60 5 40
Pentachlorophenol ug/L 0.18.18 100 39-170970.17 3 40
2,4-DCAA (S)%94 39-13994 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388120
EPA 3510
EPA 8270
8270 Water MSSV RVE
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153602
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005
Matrix: Water
Analyzed
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 11/27/17 09:53
2,4,5-Trichlorophenol ug/L ND 10.0 11/27/17 09:53
2,4,6-Trichlorophenol ug/L ND 10.0 11/27/17 09:53
2,4-Dichlorophenol ug/L ND 10.0 11/27/17 09:53
2,4-Dimethylphenol ug/L ND 10.0 11/27/17 09:53
2,4-Dinitrophenol ug/L ND 50.0 11/27/17 09:53
2,4-Dinitrotoluene ug/L ND 10.0 11/27/17 09:53
2,6-Dinitrotoluene ug/L ND 10.0 11/27/17 09:53
2-Chloronaphthalene ug/L ND 10.0 11/27/17 09:53
2-Chlorophenol ug/L ND 10.0 11/27/17 09:53
2-Methylnaphthalene ug/L ND 10.0 11/27/17 09:53
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/27/17 09:53
2-Nitroaniline ug/L ND 50.0 11/27/17 09:53
2-Nitrophenol ug/L ND 10.0 11/27/17 09:53
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/27/17 09:53
3,3'-Dichlorobenzidine ug/L ND 20.0 11/27/17 09:53
3-Nitroaniline ug/L ND 50.0 11/27/17 09:53
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/27/17 09:53
4-Bromophenylphenyl ether ug/L ND 10.0 11/27/17 09:53
4-Chloro-3-methylphenol ug/L ND 20.0 11/27/17 09:53
4-Chloroaniline ug/L ND 20.0 11/27/17 09:53
4-Chlorophenylphenyl ether ug/L ND 10.0 11/27/17 09:53
4-Nitroaniline ug/L ND 20.0 11/27/17 09:53
4-Nitrophenol ug/L ND 50.0 11/27/17 09:53
Acenaphthene ug/L ND 10.0 11/27/17 09:53
Acenaphthylene ug/L ND 10.0 11/27/17 09:53
Acetophenone ug/L ND 10.0 11/27/17 09:53
Anthracene ug/L ND 10.0 11/27/17 09:53
Benzo(a)anthracene ug/L ND 10.0 11/27/17 09:53
Benzo(a)pyrene ug/L ND 10.0 11/27/17 09:53
Benzo(b)fluoranthene ug/L ND 10.0 11/27/17 09:53
Benzo(g,h,i)perylene ug/L ND 10.0 11/27/17 09:53
Benzo(k)fluoranthene ug/L ND 10.0 11/27/17 09:53
Benzyl alcohol ug/L ND 20.0 11/27/17 09:53
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/27/17 09:53
bis(2-Chloroethyl) ether ug/L ND 10.0 11/27/17 09:53
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/27/17 09:53
Butylbenzylphthalate ug/L ND 10.0 11/27/17 09:53
Chrysene ug/L ND 10.0 11/27/17 09:53
Di-n-butylphthalate ug/L ND 10.0 11/27/17 09:53
Di-n-octylphthalate ug/L ND 10.0 11/27/17 09:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153602
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005
Matrix: Water
Analyzed
Dibenz(a,h)anthracene ug/L ND 10.0 11/27/17 09:53
Dibenzofuran ug/L ND 10.0 11/27/17 09:53
Diethylphthalate ug/L ND 10.0 11/27/17 09:53
Dimethylphthalate ug/L ND 10.0 11/27/17 09:53
Diphenylamine ug/L ND 10.0 11/27/17 09:53
Fluoranthene ug/L ND 10.0 11/27/17 09:53
Fluorene ug/L ND 10.0 11/27/17 09:53
Hexachlorobenzene ug/L ND 10.0 11/27/17 09:53
Hexachlorocyclopentadiene ug/L ND 10.0 11/27/17 09:53
Hexachloroethane ug/L ND 10.0 11/27/17 09:53
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/27/17 09:53
Isophorone ug/L ND 10.0 11/27/17 09:53
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/27/17 09:53
N-Nitrosodimethylamine ug/L ND 10.0 11/27/17 09:53
N-Nitrosodiphenylamine ug/L ND 10.0 11/27/17 09:53
Nitrobenzene ug/L ND 10.0 11/27/17 09:53
Phenanthrene ug/L ND 10.0 11/27/17 09:53
Phenol ug/L ND 10.0 11/27/17 09:53
Pyrene ug/L ND 10.0 11/27/17 09:53
2,4,6-Tribromophenol (S)%49 31-170 11/27/17 09:53
2-Fluorobiphenyl (S)%52 45-139 11/27/17 09:53
2-Fluorophenol (S)%42 13-118 11/27/17 09:53
Nitrobenzene-d5 (S)%56 40-121 11/27/17 09:53
Phenol-d6 (S)%35 18-105 11/27/17 09:53
Terphenyl-d14 (S)%72 48-146 11/27/17 09:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153603LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 28.250 56 18-120
2,4,5-Trichlorophenol ug/L 17.0 L25034 43-113
2,4,6-Trichlorophenol ug/L 17.3 L25035 42-120
2,4-Dichlorophenol ug/L 18.550 37 30-120
2,4-Dimethylphenol ug/L 37.950 76 29-111
2,4-Dinitrophenol ug/L 19.8J L22508 19-132
2,4-Dinitrotoluene ug/L 37.850 76 58-128
2,6-Dinitrotoluene ug/L 38.750 77 54-129
2-Chloronaphthalene ug/L 32.450 65 43-117
2-Chlorophenol ug/L 18.950 38 37-120
2-Methylnaphthalene ug/L 30.450 61 33-120
2-Methylphenol(o-Cresol)ug/L 27.250 54 31-120
2-Nitroaniline ug/L 73.2100 73 48-121
2-Nitrophenol ug/L 16.950 34 25-116
3&4-Methylphenol(m&p Cresol)ug/L 24.950 50 23-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153603LABORATORY CONTROL SAMPLE:
LCSSpike
3,3'-Dichlorobenzidine ug/L 76.5100 77 10-154
3-Nitroaniline ug/L 72.0100 72 43-115
4,6-Dinitro-2-methylphenol ug/L 28.6 L210029 44-124
4-Bromophenylphenyl ether ug/L 34.450 69 34-113
4-Chloro-3-methylphenol ug/L 60.9100 61 31-110
4-Chloroaniline ug/L 69.2100 69 20-120
4-Chlorophenylphenyl ether ug/L 32.650 65 34-116
4-Nitroaniline ug/L 74.0100 74 46-128
4-Nitrophenol ug/L 42.5J250 17 11-120
Acenaphthene ug/L 32.350 65 48-114
Acenaphthylene ug/L 32.650 65 48-112
Acetophenone ug/L 32.4100 32 24-120
Anthracene ug/L 35.750 71 57-118
Benzo(a)anthracene ug/L 39.450 79 56-121
Benzo(a)pyrene ug/L 37.950 76 55-127
Benzo(b)fluoranthene ug/L 38.050 76 53-128
Benzo(g,h,i)perylene ug/L 38.850 78 54-125
Benzo(k)fluoranthene ug/L 37.350 75 51-123
Benzyl alcohol ug/L 63.3100 63 27-120
bis(2-Chloroethoxy)methane ug/L 35.650 71 32-120
bis(2-Chloroethyl) ether ug/L 33.650 67 33-111
bis(2-Ethylhexyl)phthalate ug/L 39.350 79 50-145
Butylbenzylphthalate ug/L 39.750 79 54-138
Chrysene ug/L 40.250 80 58-127
Di-n-butylphthalate ug/L 37.750 75 56-125
Di-n-octylphthalate ug/L 39.550 79 50-134
Dibenz(a,h)anthracene ug/L 38.550 77 53-129
Dibenzofuran ug/L 32.950 66 45-120
Diethylphthalate ug/L 34.850 70 53-120
Dimethylphthalate ug/L 34.550 69 55-116
Diphenylamine ug/L 38.150 76 42-120
Fluoranthene ug/L 36.850 74 57-125
Fluorene ug/L 33.950 68 53-118
Hexachlorobenzene ug/L 36.750 73 49-116
Hexachlorocyclopentadiene ug/L 33.850 68 26-158
Hexachloroethane ug/L 27.250 54 30-114
Indeno(1,2,3-cd)pyrene ug/L 39.550 79 55-128
Isophorone ug/L 35.650 71 31-118
N-Nitroso-di-n-propylamine ug/L 33.650 67 32-119
N-Nitrosodimethylamine ug/L 36.950 74 13-120
N-Nitrosodiphenylamine ug/L 38.150 76 43-120
Nitrobenzene ug/L 37.350 75 33-110
Phenanthrene ug/L 35.250 70 57-117
Phenol ug/L 17.250 34 10-120
Pyrene ug/L 38.450 77 55-122
2,4,6-Tribromophenol (S)%38 31-170
2-Fluorobiphenyl (S)%70 45-139
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153603LABORATORY CONTROL SAMPLE:
LCSSpike
2-Fluorophenol (S)%24 13-118
Nitrobenzene-d5 (S)%67 40-121
Phenol-d6 (S)%29 18-105
Terphenyl-d14 (S)%74 48-146
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153604MATRIX SPIKE SAMPLE:
MSSpike
Result
92364222001
2,2'-Oxybis(1-chloropropane)ug/L 19.7 M15039 50-150ND
2,4,5-Trichlorophenol ug/L 9.2J M05018 19-105ND
2,4,6-Trichlorophenol ug/L 9.6J50 19 13-108ND
2,4-Dichlorophenol ug/L 33.950 68 19-111ND
2,4-Dimethylphenol ug/L 29.450 59 21-103ND
2,4-Dinitrophenol ug/L 61.9250 25 10-109ND
2,4-Dinitrotoluene ug/L 9.4J M15019 27-104ND
2,6-Dinitrotoluene ug/L 8.8J M15018 28-101ND
2-Chloronaphthalene ug/L 7.5J50 15 14-102ND
2-Chlorophenol ug/L 23.050 46 16-110ND
2-Methylnaphthalene ug/L 23.250 46 13-110ND
2-Methylphenol(o-Cresol)ug/L 22.650 45 19-110ND
2-Nitroaniline ug/L 21.5J M110021 26-103ND
2-Nitrophenol ug/L 23.550 47 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 24.250 41 20-1103.47J
3,3'-Dichlorobenzidine ug/L ND M11000 25-112ND
3-Nitroaniline ug/L 6.5J M11007 29-110ND
4,6-Dinitro-2-methylphenol ug/L 56.0100 56 10-117ND
4-Bromophenylphenyl ether ug/L 22.750 45 20-105ND
4-Chloro-3-methylphenol ug/L 32.0100 32 22-110ND
4-Chloroaniline ug/L ND M11006 20-100ND
4-Chlorophenylphenyl ether ug/L 7.3J M15015 19-102ND
4-Nitroaniline ug/L 6.7J M11007 29-110ND
4-Nitrophenol ug/L 33.8J250 14 10-110ND
Acenaphthene ug/L 7.4J M15015 17-100ND
Acenaphthylene ug/L 7.4J M15015 21-100ND
Anthracene ug/L 23.950 48 24-109ND
Benzo(a)anthracene ug/L 22.050 44 22-117ND
Benzo(a)pyrene ug/L 23.650 47 23-104ND
Benzo(b)fluoranthene ug/L 23.750 47 23-103ND
Benzo(g,h,i)perylene ug/L 22.350 45 18-111ND
Benzo(k)fluoranthene ug/L 24.350 49 22-113ND
Benzyl alcohol ug/L 33.2100 33 19-101ND
bis(2-Chloroethoxy)methane ug/L 21.250 42 22-110ND
bis(2-Chloroethyl) ether ug/L 21.850 44 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 27750 75 23-102240
Butylbenzylphthalate ug/L 23.650 47 25-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153604MATRIX SPIKE SAMPLE:
MSSpike
Result
92364222001
Chrysene ug/L 23.650 47 23-115ND
Di-n-butylphthalate ug/L 26.150 49 26-1101.42J
Di-n-octylphthalate ug/L 22.350 45 23-110ND
Dibenz(a,h)anthracene ug/L 22.650 45 21-112ND
Dibenzofuran ug/L 7.6J M15015 19-102ND
Diethylphthalate ug/L 10.7 M15018 29-110ND
Dimethylphthalate ug/L 7.9J M15016 27-110ND
Fluoranthene ug/L 24.450 49 23-112ND
Fluorene ug/L 7.7J M15015 22-104ND
Hexachlorobenzene ug/L 21.950 44 21-116ND
Hexachlorocyclopentadiene ug/L 7.8J50 16 10-110ND
Hexachloroethane ug/L 18.950 38 10-110ND
Indeno(1,2,3-cd)pyrene ug/L 23.250 46 20-113ND
Isophorone ug/L 27.950 56 50-150ND
N-Nitroso-di-n-propylamine ug/L 25.850 52 21-105ND
N-Nitrosodimethylamine ug/L 20.650 41 10-110ND
N-Nitrosodiphenylamine ug/L 25.350 51 23-107ND
Nitrobenzene ug/L 30.150 60 20-110ND
Phenanthrene ug/L 23.750 47 24-106ND
Phenol ug/L 31.250 30 12-11016.0
Pyrene ug/L 22.450 45 24-114ND
2,4,6-Tribromophenol (S)%52 31-170
2-Fluorobiphenyl (S)%S014 45-139
2-Fluorophenol (S)%37 13-118
Nitrobenzene-d5 (S)%53 40-121
Phenol-d6 (S)%33 18-105
Terphenyl-d14 (S)%S037 48-146
Parameter Units
Dup
Result QualifiersRPDResult
92363879001
2153605SAMPLE DUPLICATE:
2,2'-Oxybis(1-chloropropane)ug/L NDND
2,4,5-Trichlorophenol ug/L NDND
2,4,6-Trichlorophenol ug/L NDND
2,4-Dichlorophenol ug/L NDND
2,4-Dimethylphenol ug/L NDND
2,4-Dinitrophenol ug/L NDND
2,4-Dinitrotoluene ug/L NDND
2,6-Dinitrotoluene ug/L NDND
2-Chloronaphthalene ug/L NDND
2-Chlorophenol ug/L NDND
2-Methylnaphthalene ug/L NDND
2-Methylphenol(o-Cresol)ug/L NDND
2-Nitroaniline ug/L NDND
2-Nitrophenol ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363879001
2153605SAMPLE DUPLICATE:
3&4-Methylphenol(m&p Cresol)ug/L NDND
3,3'-Dichlorobenzidine ug/L NDND
3-Nitroaniline ug/L NDND
4,6-Dinitro-2-methylphenol ug/L NDND
4-Bromophenylphenyl ether ug/L NDND
4-Chloro-3-methylphenol ug/L NDND
4-Chloroaniline ug/L NDND
4-Chlorophenylphenyl ether ug/L NDND
4-Nitroaniline ug/L NDND
4-Nitrophenol ug/L NDND
Acenaphthene ug/L NDND
Acenaphthylene ug/L NDND
Acetophenone ug/L NDND
Anthracene ug/L NDND
Benzo(a)anthracene ug/L NDND
Benzo(a)pyrene ug/L NDND
Benzo(b)fluoranthene ug/L NDND
Benzo(g,h,i)perylene ug/L NDND
Benzo(k)fluoranthene ug/L NDND
Benzyl alcohol ug/L NDND
bis(2-Chloroethoxy)methane ug/L NDND
bis(2-Chloroethyl) ether ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Butylbenzylphthalate ug/L NDND
Chrysene ug/L NDND
Di-n-butylphthalate ug/L NDND
Di-n-octylphthalate ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Dibenzofuran ug/L NDND
Diethylphthalate ug/L NDND
Dimethylphthalate ug/L NDND
Diphenylamine ug/L NDND
Fluoranthene ug/L NDND
Fluorene ug/L NDND
Hexachlorobenzene ug/L NDND
Hexachlorocyclopentadiene ug/L NDND
Hexachloroethane ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
Isophorone ug/L NDND
N-Nitroso-di-n-propylamine ug/L NDND
N-Nitrosodimethylamine ug/L NDND
N-Nitrosodiphenylamine ug/L NDND
Nitrobenzene ug/L NDND
Phenanthrene ug/L NDND
Phenol ug/L NDND
Pyrene ug/L NDND
2,4,6-Tribromophenol (S)%64 266
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363879001
2153605SAMPLE DUPLICATE:
2-Fluorobiphenyl (S)%73 3054
2-Fluorophenol (S)%51 250
Nitrobenzene-d5 (S)%78 2560
Phenol-d6 (S)%52 1744
Terphenyl-d14 (S)%76 473
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388262
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007, 92363879008,92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154071
Associated Lab Samples: 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007, 92363879008,92363879009
Matrix: Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 11/27/17 17:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154072LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4790050000 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154073MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364038004
2154074
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 102 80-12096 25000094.7mg/L 146000 143000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154075MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879004
2154076
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 92 80-12088 150000110000156000 154000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387714
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007, 92363879008,92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151040
Associated Lab Samples: 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007, 92363879008,92363879009
Matrix: Water
Analyzed
Total Dissolved Solids ug/L ND 25000 11/20/17 23:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151041LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 246000250000 98 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92363860009
2151042SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 219000 2224 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92363860019
2151043SAMPLE DUPLICATE:
Total Dissolved Solids ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387728
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151104
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
Sulfide ug/L ND 100 11/21/17 22:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151105LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 455500 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151106MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363696009
2151107
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 41 80-12051 145000.12mg/L 322 372
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151108MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879008
2151109
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 106 80-120109 3500ND531 546
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388265
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples: 92363879002, 92363879003, 92363879004, 92363879005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154084
Associated Lab Samples:92363879002, 92363879003, 92363879004, 92363879005
Matrix: Water
Analyzed
Sulfate ug/L ND 1000 11/27/17 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154085LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5020050000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363776001
2154087
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 100 90-110102 15000048.2mg/L 98000 99300
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363874010
2154089
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 93 90-11095 15000068.6mg/L 115000 116000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388266
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples: 92363879006, 92363879007, 92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154090
Associated Lab Samples:92363879006, 92363879007, 92363879008, 92363879009
Matrix: Water
Analyzed
Sulfate ug/L ND 1000 11/27/17 20:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154091LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5050050000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154092MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879006
2154093
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 102 90-110103 150000783058900 59500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154094MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018003
2154095
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 103 90-110106 350000ND51600 53000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388094
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007, 92363879008,92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153405
Associated Lab Samples: 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007, 92363879008,92363879009
Matrix: Water
Analyzed
Chloride ug/L ND 1000 11/22/17 23:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153406LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2100020000 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2153407MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364320001
2153408
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 102 90-110102 0100002.3mg/L 12500 12500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2153409MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879006
2153410
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 102 90-110101 0100001620026500 26400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 87
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92363879
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387705
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151028
Associated Lab Samples: 92363879001, 92363879002, 92363879003, 92363879004, 92363879005, 92363879006, 92363879007,92363879008, 92363879009
Matrix: Water
Analyzed
Cyanide ug/L ND 8.0 11/21/17 12:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151029LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 105100 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151030MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363835001
2151031
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11008780-12078 11100ND88.0 79.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151032MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879005
2151033
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 105 80-12098 7100ND107 99.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 87
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92363879
OSR
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
BATCH QUALIFIERS
Batch: 408387
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[M5]
ANALYTE QUALIFIERS
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.1g
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 87
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92363879
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92363879002 3412-MW1R
92363879003 3412-MW4R
92363879004 3412-MW15
92363879005 3412-MW3R
92363879006 3412-MW5R
92363879007 3412-MW13
92363879008 3412-MW14
92363879009 3412-MW7
92363879001 387993 3881863412-EQUIPMENT BLANK EPA 3510 EPA 8081
92363879002 388080 3886433412-MW1R EPA 3510 EPA 8081
92363879003 388080 3886433412-MW4R EPA 3510 EPA 8081
92363879004 388080 3886433412-MW15 EPA 3510 EPA 8081
92363879009 388080 3886433412-MW7 EPA 3510 EPA 8081
92363879001 388331 3884663412-EQUIPMENT BLANK EPA 3510 EPA 8082
92363879002 388331 3884663412-MW1R EPA 3510 EPA 8082
92363879003 388331 3884663412-MW4R EPA 3510 EPA 8082
92363879004 388331 3884663412-MW15 EPA 3510 EPA 8082
92363879001 406966 4083873412-EQUIPMENT BLANK EPA 8151 EPA 8151
92363879002 406966 4083873412-MW1R EPA 8151 EPA 8151
92363879003 406966 4083873412-MW4R EPA 8151 EPA 8151
92363879004 406966 4083873412-MW15 EPA 8151 EPA 8151
92363879001 387775 3879213412-EQUIPMENT BLANK EPA 3010A EPA 6010
92363879002 387775 3879213412-MW1R EPA 3010A EPA 6010
92363879003 387775 3879213412-MW4R EPA 3010A EPA 6010
92363879004 387775 3879213412-MW15 EPA 3010A EPA 6010
92363879005 387775 3879213412-MW3R EPA 3010A EPA 6010
92363879006 387775 3879213412-MW5R EPA 3010A EPA 6010
92363879007 387775 3879213412-MW13 EPA 3010A EPA 6010
92363879008 387775 3879213412-MW14 EPA 3010A EPA 6010
92363879009 387775 3879213412-MW7 EPA 3010A EPA 6010
92363879001 387486 3875503412-EQUIPMENT BLANK EPA 3010A EPA 6020B
92363879002 387486 3875503412-MW1R EPA 3010A EPA 6020B
92363879003 387486 3875503412-MW4R EPA 3010A EPA 6020B
92363879004 387486 3875503412-MW15 EPA 3010A EPA 6020B
92363879005 387486 3875503412-MW3R EPA 3010A EPA 6020B
92363879006 387486 3875503412-MW5R EPA 3010A EPA 6020B
92363879007 387486 3875503412-MW13 EPA 3010A EPA 6020B
92363879008 387486 3875503412-MW14 EPA 3010A EPA 6020B
92363879009 387486 3875503412-MW7 EPA 3010A EPA 6020B
92363879001 388398 3884203412-EQUIPMENT BLANK EPA 7470 EPA 7470
92363879002 388398 3884203412-MW1R EPA 7470 EPA 7470
92363879003 388398 3884203412-MW4R EPA 7470 EPA 7470
92363879004 388398 3884203412-MW15 EPA 7470 EPA 7470
92363879005 388398 3884203412-MW3R EPA 7470 EPA 7470
92363879006 388398 3884203412-MW5R EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 87
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92363879
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92363879007 388398 3884203412-MW13 EPA 7470 EPA 7470
92363879008 388398 3884203412-MW14 EPA 7470 EPA 7470
92363879009 388398 3884203412-MW7 EPA 7470 EPA 7470
92363879001 388120 3882953412-EQUIPMENT BLANK EPA 3510 EPA 8270
92363879002 388120 3882953412-MW1R EPA 3510 EPA 8270
92363879003 388120 3882953412-MW4R EPA 3510 EPA 8270
92363879004 388120 3882953412-MW15 EPA 3510 EPA 8270
92363879005 388120 3882953412-MW3R EPA 3510 EPA 8270
92363879001 3881683412-EQUIPMENT BLANK EPA 8260
92363879002 3881683412-MW1R EPA 8260
92363879003 3881683412-MW4R EPA 8260
92363879004 3881683412-MW15 EPA 8260
92363879005 3881683412-MW3R EPA 8260
92363879006 3881683412-MW5R EPA 8260
92363879007 3881683412-MW13 EPA 8260
92363879008 3881683412-MW14 EPA 8260
92363879009 3881683412-MW7 EPA 8260
92363879002 3882623412-MW1R SM 2320B
92363879003 3882623412-MW4R SM 2320B
92363879004 3882623412-MW15 SM 2320B
92363879005 3882623412-MW3R SM 2320B
92363879006 3882623412-MW5R SM 2320B
92363879007 3882623412-MW13 SM 2320B
92363879008 3882623412-MW14 SM 2320B
92363879009 3882623412-MW7 SM 2320B
92363879002 3877143412-MW1R SM 2540C
92363879003 3877143412-MW4R SM 2540C
92363879004 3877143412-MW15 SM 2540C
92363879005 3877143412-MW3R SM 2540C
92363879006 3877143412-MW5R SM 2540C
92363879007 3877143412-MW13 SM 2540C
92363879008 3877143412-MW14 SM 2540C
92363879009 3877143412-MW7 SM 2540C
92363879001 3877283412-EQUIPMENT BLANK SM 4500-S2D
92363879002 3877283412-MW1R SM 4500-S2D
92363879003 3877283412-MW4R SM 4500-S2D
92363879004 3877283412-MW15 SM 4500-S2D
92363879005 3877283412-MW3R SM 4500-S2D
92363879006 3877283412-MW5R SM 4500-S2D
92363879007 3877283412-MW13 SM 4500-S2D
92363879008 3877283412-MW14 SM 4500-S2D
92363879009 3877283412-MW7 SM 4500-S2D
92363879002 3882653412-MW1R EPA 300.0
92363879003 3882653412-MW4R EPA 300.0
92363879004 3882653412-MW15 EPA 300.0
92363879005 3882653412-MW3R EPA 300.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 87
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92363879
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92363879006 3882663412-MW5R EPA 300.0
92363879007 3882663412-MW13 EPA 300.0
92363879008 3882663412-MW14 EPA 300.0
92363879009 3882663412-MW7 EPA 300.0
92363879002 3880943412-MW1R SM 4500-Cl-E
92363879003 3880943412-MW4R SM 4500-Cl-E
92363879004 3880943412-MW15 SM 4500-Cl-E
92363879005 3880943412-MW3R SM 4500-Cl-E
92363879006 3880943412-MW5R SM 4500-Cl-E
92363879007 3880943412-MW13 SM 4500-Cl-E
92363879008 3880943412-MW14 SM 4500-Cl-E
92363879009 3880943412-MW7 SM 4500-Cl-E
92363879001 3877053412-EQUIPMENT BLANK SM 4500-CN-E
92363879002 3877053412-MW1R SM 4500-CN-E
92363879003 3877053412-MW4R SM 4500-CN-E
92363879004 3877053412-MW15 SM 4500-CN-E
92363879005 3877053412-MW3R SM 4500-CN-E
92363879006 3877053412-MW5R SM 4500-CN-E
92363879007 3877053412-MW13 SM 4500-CN-E
92363879008 3877053412-MW14 SM 4500-CN-E
92363879009 3877053412-MW7 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 01:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 87
Page 83 of 87
Page 84 of 87
Page 85 of 87
Page 86 of 87
Page 87 of 87
#=CL#
December 28, 2017
LIMS USE: FR - SEAN QUARRY
LIMS OBJECT ID: 92364018
92364018
Project:
Pace Project No.:
RE:
Sean QuarryHDR Engineering440 South Church StreetSuite 1000Charlotte, NC 28202
OSR
Dear Sean Quarry:
Enclosed are the analytical results for sample(s) received by the laboratory on November 17, 2017.
The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
Per client request, report revised 12/28/17 to include APP 2 compounds.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin for
[e-mail]
HORIZON Database Administrator
Kevin Herring
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 90
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92364018
OSR
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 90
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92364018
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92364018001 3412-MW2R EPA 8081 24 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8151 6 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018002 3412-MW8 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018003 3412-MW9 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018004 3412-MW11 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 90
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92364018
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018005 3412-MW12 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018006 3412-SW1 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 53 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018007 3412-SW3 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 53 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 90
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92364018
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92364018008 3412-SW4 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 53 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018009 3412-MW10 EPA 8081 24 PASI-CPKS
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018010 3412-SW2 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 66 PASI-CRES
EPA 8260 69 PASI-CSWB
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AMDW
SM 4500-CN-E 1 PASI-AAES2
92364018011 3412-TRIP BLANK EPA 8260 69 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW2R Lab ID: 92364018001 Collected: 11/17/17 08:45 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 08:45 12/13/17 14:101
Field pH 6.3 Std. Units 12/13/17 14:100.10 1
Field Temperature 13.1 deg C 12/13/17 14:100.50 1
Static Water Level 8.22 feet 12/13/17 14:101
Field Specific Conductance 1393 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 2.09 mg/L 12/13/17 14:10 7782-44-71
Total Well Depth 21 feet 12/13/17 14:101
REDOX -10.1 mV 12/13/17 14:101
Turbidity 11.87 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/29/17 16:17 309-00-211/22/17 17:100.050 1
alpha-BHC ND ug/L 11/29/17 16:17 319-84-611/22/17 17:100.050 1
beta-BHC ND ug/L 11/29/17 16:17 319-85-711/22/17 17:100.050 1
delta-BHC ND ug/L 11/29/17 16:17 319-86-811/22/17 17:100.050 1
gamma-BHC (Lindane)ND ug/L 11/29/17 16:17 58-89-911/22/17 17:100.050 1
Chlordane (Technical)ND ug/L 11/29/17 16:17 57-74-911/22/17 17:100.20 1
4,4'-DDD ND ug/L 11/29/17 16:17 72-54-811/22/17 17:100.050 1
4,4'-DDE ND ug/L 11/29/17 16:17 72-55-911/22/17 17:100.050 1
4,4'-DDT ND ug/L 11/29/17 16:17 50-29-3 M111/22/17 17:100.050 1
Dieldrin ND ug/L 11/29/17 16:17 60-57-111/22/17 17:100.050 1
Endosulfan I ND ug/L 11/29/17 16:17 959-98-811/22/17 17:100.050 1
Endosulfan II ND ug/L 11/29/17 16:17 33213-65-911/22/17 17:100.050 1
Endosulfan sulfate ND ug/L 11/29/17 16:17 1031-07-811/22/17 17:100.050 1
Endrin ND ug/L 11/29/17 16:17 72-20-811/22/17 17:100.050 1
Endrin aldehyde ND ug/L 11/29/17 16:17 7421-93-411/22/17 17:100.050 1
Endrin ketone ND ug/L 11/29/17 16:17 53494-70-511/22/17 17:100.050 1
Heptachlor ND ug/L 11/29/17 16:17 76-44-811/22/17 17:100.050 1
Heptachlor epoxide ND ug/L 11/29/17 16:17 1024-57-311/22/17 17:100.050 1
Hexachlorobenzene ND ug/L 11/29/17 16:17 118-74-111/22/17 17:100.050 1
Methoxychlor ND ug/L 11/29/17 16:17 72-43-5 M111/22/17 17:100.15 1
Mirex ND ug/L 11/29/17 16:17 2385-85-511/22/17 17:100.15 1
Toxaphene ND ug/L 11/29/17 16:17 8001-35-211/22/17 17:100.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %11/29/17 16:17 877-09-811/22/17 17:1020-130 1
Decachlorobiphenyl (S)59 %11/29/17 16:17 2051-24-311/22/17 17:1020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 11/29/17 19:58 12674-11-211/27/17 13:140.50 1
PCB-1221 (Aroclor 1221)ND ug/L 11/29/17 19:58 11104-28-211/27/17 13:140.50 1
PCB-1232 (Aroclor 1232)ND ug/L 11/29/17 19:58 11141-16-511/27/17 13:140.50 1
PCB-1242 (Aroclor 1242)ND ug/L 11/29/17 19:58 53469-21-911/27/17 13:140.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW2R Lab ID: 92364018001 Collected: 11/17/17 08:45 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1248 (Aroclor 1248)ND ug/L 11/29/17 19:58 12672-29-611/27/17 13:140.50 1
PCB-1254 (Aroclor 1254)ND ug/L 11/29/17 19:58 11097-69-111/27/17 13:140.50 1
PCB-1260 (Aroclor 1260)ND ug/L 11/29/17 19:58 11096-82-511/27/17 13:140.50 1
Surrogates
Decachlorobiphenyl (S)47 %11/29/17 19:58 2051-24-311/27/17 13:1410-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 11/29/17 03:04 94-75-7 1g11/21/17 23:280.99 1
Dinoseb ND ug/L 11/29/17 03:04 88-85-7 1g11/21/17 23:280.20 1
Pentachlorophenol ND ug/L 11/29/17 03:04 87-86-5 1g11/21/17 23:280.030 1
2,4,5-T ND ug/L 11/29/17 03:04 93-76-5 1g11/21/17 23:280.20 1
2,4,5-TP (Silvex)0.072J ug/L 11/29/17 03:04 93-72-1 1g11/21/17 23:280.20 1
Surrogates2,4-DCAA (S)110 %11/29/17 03:04 19719-28-911/21/17 23:2839-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:39 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:39 7440-38-211/21/17 12:0010.0 1
Barium 323 ug/L 12/07/17 02:39 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:39 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:39 7440-43-911/21/17 12:001.0 1
Chromium 2.7J ug/L 12/07/17 02:39 7440-47-311/21/17 12:005.0 1
Cobalt 23.5 ug/L 12/07/17 02:39 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:39 7440-50-811/21/17 12:005.0 1
Iron 3010 ug/L 12/07/17 02:39 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:39 7439-92-111/21/17 12:005.0 1
Manganese 10600 ug/L 12/07/17 11:50 7439-96-511/21/17 12:0025.0 5
Nickel 20.3 ug/L 12/07/17 02:39 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:39 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:39 7440-22-411/21/17 12:005.0 1
Sodium 77600 ug/L 12/07/17 02:39 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:39 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:39 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 02:39 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:03 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:45 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 13:34 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 13:34 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 13:34 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 13:34 120-12-711/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW2R Lab ID: 92364018001 Collected: 11/17/17 08:45 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Benzo(a)anthracene ND ug/L 11/28/17 13:34 56-55-311/23/17 05:4110.0 1
Benzo(a)pyrene ND ug/L 11/28/17 13:34 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 13:34 205-99-211/23/17 05:4110.0 1
Benzo(g,h,i)perylene ND ug/L 11/28/17 13:34 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 13:34 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 13:34 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 13:34 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate ND ug/L 11/28/17 13:34 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 13:34 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 13:34 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 13:34 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 13:34 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 13:34 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 13:34 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 13:34 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 13:34 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 13:34 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 13:34 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 13:34 91-94-111/23/17 05:4120.0 1
2,4-Dichlorophenol ND ug/L 11/28/17 13:34 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 13:34 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 13:34 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 13:34 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 13:34 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 13:34 534-52-111/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 13:34 51-28-511/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 13:34 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 13:34 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 13:34 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 13:34 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 13:34 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 13:34 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 13:34 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 13:34 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 13:34 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 13:34 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 13:34 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 13:34 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 13:34 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 13:34 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 13:34 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 13:34 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 13:34 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 13:34 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 13:34 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 13:34 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 13:34 100-02-711/23/17 05:4150.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW2R Lab ID: 92364018001 Collected: 11/17/17 08:45 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
N-Nitrosodimethylamine ND ug/L 11/28/17 13:34 62-75-911/23/17 05:4110.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 13:34 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 13:34 86-30-611/23/17 05:4110.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 13:34 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 13:34 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 13:34 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 13:34 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 13:34 95-95-411/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 13:34 88-06-211/23/17 05:4110.0 1
Surrogates
Nitrobenzene-d5 (S)62 %11/28/17 13:34 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)55 %11/28/17 13:34 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)65 %11/28/17 13:34 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)52 %11/28/17 13:34 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)51 %11/28/17 13:34 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)72 %11/28/17 13:34 118-79-611/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 06:11 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 06:11 75-05-850.0 1
Acrolein ND ug/L 11/26/17 06:11 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 06:11 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 06:11 107-05-12.0 1
Benzene 2.6 ug/L 11/26/17 06:11 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 06:11 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 06:11 75-27-41.0 1
Bromoform ND ug/L 11/26/17 06:11 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 06:11 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 06:11 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 06:11 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 06:11 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 06:11 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 06:11 75-00-31.0 1
Chloroform ND ug/L 11/26/17 06:11 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 06:11 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 06:11 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 06:11 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 06:11 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 06:11 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 06:11 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 06:11 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 06:11 541-73-11.0 1
1,4-Dichlorobenzene 0.46J ug/L 11/26/17 06:11 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 06:11 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 06:11 75-71-81.0 1
1,1-Dichloroethane 0.48J ug/L 11/26/17 06:11 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 06:11 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW2R Lab ID: 92364018001 Collected: 11/17/17 08:45 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 11/26/17 06:11 75-35-41.0 1
cis-1,2-Dichloroethene 0.60J ug/L 11/26/17 06:11 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 06:11 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 06:11 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 06:11 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 06:11 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 06:11 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 06:11 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 06:11 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 06:11 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 06:11 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 06:11 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 06:11 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 06:11 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 06:11 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 06:11 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 06:11 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 06:11 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 06:11 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 06:11 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 06:11 107-12-020.0 1
Styrene ND ug/L 11/26/17 06:11 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 06:11 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 06:11 79-34-51.0 1
Tetrachloroethene 1.8 ug/L 11/26/17 06:11 127-18-41.0 1
Tetrahydrofuran 28.0 ug/L 11/26/17 06:11 109-99-910.0 1
Toluene ND ug/L 11/26/17 06:11 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 06:11 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 06:11 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 06:11 79-00-51.0 1
Trichloroethene 0.93J ug/L 11/26/17 06:11 79-01-61.0 1
Trichlorofluoromethane 1.5 ug/L 11/26/17 06:11 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 06:11 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 06:11 108-05-42.0 1
Vinyl chloride 1.4 ug/L 11/26/17 06:11 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 06:11 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 06:11 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)102 %11/26/17 06:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %11/26/17 06:11 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 06:11 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 670000 ug/L 11/28/17 17:08 M15000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW2R Lab ID: 92364018001 Collected: 11/17/17 08:45 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 918000 ug/L 11/21/17 01:2550000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8 M1,R1100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 122000 ug/L 11/28/17 07:36 14808-79-82000 2
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 47600 ug/L 11/23/17 00:13 16887-00-64000 4
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:09 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW8 Lab ID: 92364018002 Collected: 11/17/17 11:15 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 11:15 12/13/17 14:101
Field pH 5.6 Std. Units 12/13/17 14:100.10 1
Field Temperature 16.3 deg C 12/13/17 14:100.50 1
Static Water Level 17.73 feet 12/13/17 14:101
Field Specific Conductance 77.4 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 4.2 mg/L 12/13/17 14:10 7782-44-71
Total Well Depth 27 feet 12/13/17 14:101
REDOX 166.3 mV 12/13/17 14:101
Turbidity 0.4 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 02:44 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 02:44 7440-38-211/21/17 12:0010.0 1
Barium 46.5 ug/L 12/07/17 02:44 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 02:44 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 02:44 7440-43-911/21/17 12:001.0 1
Chromium 4.9J ug/L 12/07/17 02:44 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 02:44 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 02:44 7440-50-811/21/17 12:005.0 1
Iron 37.6J ug/L 12/07/17 02:44 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 02:44 7439-92-111/21/17 12:005.0 1
Manganese 3.6J ug/L 12/07/17 02:44 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 02:44 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 02:44 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 02:44 7440-22-411/21/17 12:005.0 1
Sodium 9860 ug/L 12/07/17 02:44 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 02:44 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 02:44 7440-62-211/21/17 12:005.0 1
Zinc 5.3J ug/L 12/07/17 02:44 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:06 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:48 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 06:28 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 06:28 75-05-850.0 1
Acrolein ND ug/L 11/26/17 06:28 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 06:28 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 06:28 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW8 Lab ID: 92364018002 Collected: 11/17/17 11:15 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 06:28 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 06:28 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 06:28 75-27-41.0 1
Bromoform ND ug/L 11/26/17 06:28 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 06:28 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 06:28 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 06:28 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 06:28 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 06:28 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 06:28 75-00-31.0 1
Chloroform ND ug/L 11/26/17 06:28 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 06:28 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 06:28 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 06:28 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 06:28 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 06:28 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 06:28 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 06:28 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 06:28 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 06:28 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 06:28 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 06:28 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 06:28 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 06:28 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 06:28 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 06:28 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 06:28 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 06:28 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 06:28 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 06:28 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 06:28 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 06:28 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 06:28 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 06:28 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 06:28 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 06:28 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 06:28 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 06:28 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 06:28 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 06:28 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 06:28 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 06:28 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 06:28 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 06:28 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 06:28 107-12-020.0 1
Styrene ND ug/L 11/26/17 06:28 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 06:28 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW8 Lab ID: 92364018002 Collected: 11/17/17 11:15 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 06:28 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 06:28 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 06:28 109-99-910.0 1
Toluene ND ug/L 11/26/17 06:28 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 06:28 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 06:28 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 06:28 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 06:28 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 06:28 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 06:28 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 06:28 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 06:28 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 06:28 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 06:28 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/26/17 06:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %11/26/17 06:28 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 06:28 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 28200 ug/L 11/28/17 17:455000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 82000 ug/L 11/21/17 01:2525000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4740 ug/L 11/28/17 00:41 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3860 ug/L 11/23/17 00:14 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:10 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW9 Lab ID: 92364018003 Collected: 11/17/17 12:10 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 12:10 12/13/17 14:101
Field pH 5.5 Std. Units 12/13/17 14:100.10 1
Field Temperature 15.3 deg C 12/13/17 14:100.50 1
Static Water Level 52.89 feet 12/13/17 14:101
Field Specific Conductance 160.0 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 6.3 mg/L 12/13/17 14:10 7782-44-71
Total Well Depth 60 feet 12/13/17 14:101
REDOX 206.8 mV 12/13/17 14:101
Turbidity 7.9 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:04 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:04 7440-38-211/21/17 12:0010.0 1
Barium 196 ug/L 12/07/17 03:04 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:04 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 03:04 7440-43-911/21/17 12:001.0 1
Chromium 7.2 ug/L 12/07/17 03:04 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 03:04 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:04 7440-50-811/21/17 12:005.0 1
Iron 166 ug/L 12/07/17 03:04 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:04 7439-92-111/21/17 12:005.0 1
Manganese 10.6 ug/L 12/07/17 03:04 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 03:04 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:04 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:04 7440-22-411/21/17 12:005.0 1
Sodium 14900 ug/L 12/07/17 03:04 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 03:04 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:04 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 03:04 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:13 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:50 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 06:45 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 06:45 75-05-850.0 1
Acrolein ND ug/L 11/26/17 06:45 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 06:45 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 06:45 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW9 Lab ID: 92364018003 Collected: 11/17/17 12:10 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 06:45 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 06:45 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 06:45 75-27-41.0 1
Bromoform ND ug/L 11/26/17 06:45 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 06:45 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 06:45 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 06:45 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 06:45 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 06:45 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 06:45 75-00-31.0 1
Chloroform ND ug/L 11/26/17 06:45 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 06:45 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 06:45 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 06:45 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 06:45 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 06:45 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 06:45 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 06:45 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 06:45 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 06:45 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 06:45 110-57-61.0 1
Dichlorodifluoromethane 1.2 ug/L 11/26/17 06:45 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 06:45 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 06:45 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 06:45 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 06:45 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 06:45 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 06:45 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 06:45 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 06:45 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 06:45 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 06:45 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 06:45 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 06:45 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 06:45 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 06:45 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 06:45 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 06:45 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 06:45 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 06:45 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 06:45 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 06:45 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 06:45 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 06:45 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 06:45 107-12-020.0 1
Styrene ND ug/L 11/26/17 06:45 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 06:45 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW9 Lab ID: 92364018003 Collected: 11/17/17 12:10 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 06:45 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 06:45 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 06:45 109-99-910.0 1
Toluene ND ug/L 11/26/17 06:45 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 06:45 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 06:45 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 06:45 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 06:45 79-01-61.0 1
Trichlorofluoromethane 1.2 ug/L 11/26/17 06:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 06:45 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 06:45 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 06:45 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 06:45 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 06:45 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/26/17 06:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %11/26/17 06:45 17060-07-070-130 1
Toluene-d8 (S)111 %11/26/17 06:45 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 27900 ug/L 11/28/17 17:565000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 136000 ug/L 11/21/17 01:2525000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 11/28/17 01:33 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4430 ug/L 11/23/17 00:15 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:10 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW11 Lab ID: 92364018004 Collected: 11/17/17 12:50 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JSH 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 12:50 12/13/17 14:101
Field pH 6.1 Std. Units 12/13/17 14:100.10 1
Field Temperature 16.4 deg C 12/13/17 14:100.50 1
Static Water Level 4.33 feet 12/13/17 14:101
Field Specific Conductance 348.3 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 0.1 mg/L 12/13/17 14:10 7782-44-71
Total Well Depth 20.0 feet 12/13/17 14:101
REDOX -43.0 mV 12/13/17 14:101
Turbidity 8.9 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:08 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:08 7440-38-211/21/17 12:0010.0 1
Barium 89.8 ug/L 12/07/17 03:08 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:08 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 03:08 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 03:08 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 03:08 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:08 7440-50-811/21/17 12:005.0 1
Iron 29300 ug/L 12/07/17 03:08 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:08 7439-92-111/21/17 12:005.0 1
Manganese 1590 ug/L 12/07/17 03:08 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 03:08 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:08 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:08 7440-22-411/21/17 12:005.0 1
Sodium 12300 ug/L 12/07/17 03:08 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 03:08 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:08 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 03:08 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:16 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:52 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 07:03 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 07:03 75-05-850.0 1
Acrolein ND ug/L 11/26/17 07:03 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 07:03 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 07:03 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW11 Lab ID: 92364018004 Collected: 11/17/17 12:50 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 07:03 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 07:03 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 07:03 75-27-41.0 1
Bromoform ND ug/L 11/26/17 07:03 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 07:03 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 07:03 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 07:03 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 07:03 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 07:03 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 07:03 75-00-31.0 1
Chloroform ND ug/L 11/26/17 07:03 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 07:03 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 07:03 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 07:03 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 07:03 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 07:03 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 07:03 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 07:03 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 07:03 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 07:03 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 07:03 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 07:03 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 07:03 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 07:03 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 07:03 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 07:03 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 07:03 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 07:03 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 07:03 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 07:03 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 07:03 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 07:03 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 07:03 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 07:03 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 07:03 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 07:03 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 07:03 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 07:03 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 07:03 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 07:03 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 07:03 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 07:03 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 07:03 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 07:03 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 07:03 107-12-020.0 1
Styrene ND ug/L 11/26/17 07:03 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 07:03 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW11 Lab ID: 92364018004 Collected: 11/17/17 12:50 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 07:03 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 07:03 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 07:03 109-99-910.0 1
Toluene ND ug/L 11/26/17 07:03 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 07:03 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 07:03 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 07:03 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 07:03 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 07:03 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 07:03 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 07:03 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 07:03 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 07:03 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 07:03 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %11/26/17 07:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %11/26/17 07:03 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 07:03 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 130000 ug/L 11/28/17 18:085000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 218000 ug/L 11/21/17 01:2525000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 16200 ug/L 11/28/17 02:25 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 13000 ug/L 11/23/17 00:16 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:11 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW12 Lab ID: 92364018005 Collected: 11/17/17 13:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 12:52 12/13/17 14:101
Field pH 6.1 Std. Units 12/13/17 14:100.10 1
Field Temperature 16.5 deg C 12/13/17 14:100.50 1
Static Water Level 5.31 feet 12/13/17 14:101
Field Specific Conductance 299.8 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 0.34 mg/L 12/13/17 14:10 7782-44-71
Total Well Depth 15.7 feet 12/13/17 14:101
REDOX 60.9 mV 12/13/17 14:101
Turbidity 1.61 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:12 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:12 7440-38-211/21/17 12:0010.0 1
Barium 84.2 ug/L 12/07/17 03:12 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:12 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 03:12 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 03:12 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 03:12 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:12 7440-50-811/21/17 12:005.0 1
Iron 125 ug/L 12/07/17 03:12 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:12 7439-92-111/21/17 12:005.0 1
Manganese 169 ug/L 12/07/17 03:12 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 03:12 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:12 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:12 7440-22-411/21/17 12:005.0 1
Sodium 13200 ug/L 12/07/17 03:12 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 03:12 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:12 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 03:12 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:18 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:55 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 07:20 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 07:20 75-05-850.0 1
Acrolein ND ug/L 11/26/17 07:20 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 07:20 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 07:20 107-05-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW12 Lab ID: 92364018005 Collected: 11/17/17 13:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 11/26/17 07:20 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 07:20 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 07:20 75-27-41.0 1
Bromoform ND ug/L 11/26/17 07:20 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 07:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 07:20 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 07:20 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 07:20 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 07:20 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 07:20 75-00-31.0 1
Chloroform ND ug/L 11/26/17 07:20 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 07:20 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 07:20 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 07:20 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 07:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 07:20 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 07:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 07:20 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 07:20 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 07:20 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 07:20 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 07:20 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 07:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 07:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 07:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 07:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 07:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 07:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 07:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 07:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 07:20 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 07:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 07:20 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 07:20 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 07:20 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 07:20 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 07:20 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 07:20 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 07:20 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 07:20 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 07:20 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 07:20 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 07:20 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 07:20 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 07:20 107-12-020.0 1
Styrene ND ug/L 11/26/17 07:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 07:20 630-20-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW12 Lab ID: 92364018005 Collected: 11/17/17 13:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 07:20 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 07:20 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 07:20 109-99-910.0 1
Toluene ND ug/L 11/26/17 07:20 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 07:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 07:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 07:20 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 07:20 79-01-61.0 1
Trichlorofluoromethane 0.52J ug/L 11/26/17 07:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 07:20 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 07:20 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 07:20 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 07:20 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 07:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/26/17 07:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %11/26/17 07:20 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 07:20 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 73800 ug/L 11/28/17 18:455000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 219000 ug/L 11/21/17 01:2525000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 62400 ug/L 11/28/17 02:42 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 10400 ug/L 11/23/17 00:17 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 12:45 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW1 Lab ID: 92364018006 Collected: 11/17/17 10:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 10:30 12/13/17 14:101
Field pH 7.4 Std. Units 12/13/17 14:100.10 1
Field Temperature 8.0 deg C 12/13/17 14:100.50 1
Field Specific Conductance 211.0 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 6.60 mg/L 12/13/17 14:10 7782-44-71
REDOX -121.9 mV 12/13/17 14:101
Turbidity 4.96 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:16 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:16 7440-38-211/21/17 12:0010.0 1
Barium 47.5 ug/L 12/07/17 03:16 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:16 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 03:16 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 03:16 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 03:16 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:16 7440-50-811/21/17 12:005.0 1
Iron 4900 ug/L 12/07/17 03:16 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:16 7439-92-111/21/17 12:005.0 1
Manganese 461 ug/L 12/07/17 03:16 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 03:16 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:16 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:16 7440-22-411/21/17 12:005.0 1
Sodium 17000 ug/L 12/07/17 03:16 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 03:16 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:16 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 03:16 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:21 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:57 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 07:38 67-64-125.0 1
Acrylonitrile ND ug/L 11/26/17 07:38 107-13-110.0 1
Benzene ND ug/L 11/26/17 07:38 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 07:38 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 07:38 75-27-41.0 1
Bromoform ND ug/L 11/26/17 07:38 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 07:38 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW1 Lab ID: 92364018006 Collected: 11/17/17 10:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 11/26/17 07:38 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 07:38 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 07:38 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 07:38 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 07:38 75-00-31.0 1
Chloroform ND ug/L 11/26/17 07:38 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 07:38 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 07:38 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 07:38 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 07:38 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 07:38 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 07:38 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 07:38 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 07:38 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 07:38 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 07:38 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 07:38 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 07:38 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 07:38 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 07:38 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 07:38 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 07:38 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 07:38 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 07:38 100-41-41.0 1
2-Hexanone ND ug/L 11/26/17 07:38 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 07:38 74-88-45.0 1
Methylene Chloride ND ug/L 11/26/17 07:38 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 07:38 108-10-15.0 1
Styrene ND ug/L 11/26/17 07:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 07:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 07:38 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 07:38 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 07:38 109-99-910.0 1
Toluene ND ug/L 11/26/17 07:38 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 07:38 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 07:38 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 07:38 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 07:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 07:38 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 07:38 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 07:38 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 07:38 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 07:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/26/17 07:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %11/26/17 07:38 17060-07-070-130 1
Toluene-d8 (S)107 %11/26/17 07:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW1 Lab ID: 92364018006 Collected: 11/17/17 10:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 43600 ug/L 11/28/17 18:595000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 123000 ug/L 11/21/17 01:2525000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2730 ug/L 11/28/17 02:59 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 35700 ug/L 11/23/17 00:21 16887-00-6 M11000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:34 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW3 Lab ID: 92364018007 Collected: 11/17/17 09:50 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 09:50 12/13/17 14:101
Field pH 6.7 Std. Units 12/13/17 14:100.10 1
Field Temperature 7.9 deg C 12/13/17 14:100.50 1
Field Specific Conductance 959 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 3.0 mg/L 12/13/17 14:10 7782-44-71
REDOX -19.0 mV 12/13/17 14:101
Turbidity 14.79 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance MURKY 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:20 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:20 7440-38-211/21/17 12:0010.0 1
Barium 217 ug/L 12/07/17 03:20 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:20 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 03:20 7440-43-911/21/17 12:001.0 1
Chromium ND ug/L 12/07/17 03:20 7440-47-311/21/17 12:005.0 1
Cobalt 7.2 ug/L 12/07/17 03:20 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:20 7440-50-811/21/17 12:005.0 1
Iron 1720 ug/L 12/07/17 03:20 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:20 7439-92-111/21/17 12:005.0 1
Manganese 7340 ug/L 12/07/17 03:20 7439-96-511/21/17 12:005.0 1
Nickel 5.5 ug/L 12/07/17 03:20 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:20 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:20 7440-22-411/21/17 12:005.0 1
Sodium 35500 ug/L 12/07/17 03:20 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 03:20 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:20 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 03:20 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:23 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 13:59 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 07:55 67-64-125.0 1
Acrylonitrile ND ug/L 11/26/17 07:55 107-13-110.0 1
Benzene ND ug/L 11/26/17 07:55 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 07:55 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 07:55 75-27-41.0 1
Bromoform ND ug/L 11/26/17 07:55 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 07:55 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW3 Lab ID: 92364018007 Collected: 11/17/17 09:50 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 11/26/17 07:55 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 07:55 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 07:55 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 07:55 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 07:55 75-00-3 M11.0 1
Chloroform ND ug/L 11/26/17 07:55 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 07:55 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 07:55 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 07:55 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 07:55 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 07:55 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 07:55 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 07:55 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 07:55 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 07:55 75-71-8 M11.0 1
1,1-Dichloroethane ND ug/L 11/26/17 07:55 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 07:55 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 07:55 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 07:55 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 07:55 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 07:55 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 07:55 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 07:55 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 07:55 100-41-41.0 1
2-Hexanone ND ug/L 11/26/17 07:55 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 07:55 74-88-45.0 1
Methylene Chloride ND ug/L 11/26/17 07:55 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 07:55 108-10-15.0 1
Styrene ND ug/L 11/26/17 07:55 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 07:55 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 07:55 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 07:55 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 07:55 109-99-910.0 1
Toluene ND ug/L 11/26/17 07:55 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 07:55 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 07:55 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 07:55 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 07:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 07:55 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 07:55 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 07:55 75-01-4 M11.0 1
m&p-Xylene ND ug/L 11/26/17 07:55 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 07:55 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/26/17 07:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %11/26/17 07:55 17060-07-070-130 1
Toluene-d8 (S)110 %11/26/17 07:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW3 Lab ID: 92364018007 Collected: 11/17/17 09:50 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 477000 ug/L 11/29/17 13:005000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 600000 ug/L 11/21/17 01:2550000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 33800 ug/L 11/28/17 03:16 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 33800 ug/L 11/23/17 00:30 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:35 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW4 Lab ID: 92364018008 Collected: 11/17/17 11:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 11:00 12/13/17 14:101
Field pH 7.1 Std. Units 12/13/17 14:100.10 1
Field Temperature 8.1 deg C 12/13/17 14:100.50 1
Field Specific Conductance 509.1 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 7.50 mg/L 12/13/17 14:10 7782-44-71
REDOX -2.7 mV 12/13/17 14:101
Turbidity 3.50 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance MURKY 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:25 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:25 7440-38-211/21/17 12:0010.0 1
Barium 110 ug/L 12/07/17 03:25 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:25 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 03:25 7440-43-911/21/17 12:001.0 1
Chromium 4.7J ug/L 12/07/17 03:25 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 03:25 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:25 7440-50-811/21/17 12:005.0 1
Iron 802 ug/L 12/07/17 03:25 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:25 7439-92-111/21/17 12:005.0 1
Manganese 1020 ug/L 12/07/17 03:25 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 03:25 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:25 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:25 7440-22-411/21/17 12:005.0 1
Sodium 25600 ug/L 12/07/17 03:25 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 03:25 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:25 7440-62-211/21/17 12:005.0 1
Zinc 8.3J ug/L 12/07/17 03:25 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:33 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 14:02 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 08:12 67-64-125.0 1
Acrylonitrile ND ug/L 11/26/17 08:12 107-13-110.0 1
Benzene ND ug/L 11/26/17 08:12 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 08:12 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 08:12 75-27-41.0 1
Bromoform ND ug/L 11/26/17 08:12 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 08:12 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW4 Lab ID: 92364018008 Collected: 11/17/17 11:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 11/26/17 08:12 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 08:12 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 08:12 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 08:12 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 08:12 75-00-31.0 1
Chloroform ND ug/L 11/26/17 08:12 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 08:12 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 08:12 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 08:12 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 08:12 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 08:12 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 08:12 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 08:12 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 08:12 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 08:12 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 08:12 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 08:12 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 08:12 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 08:12 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 08:12 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 08:12 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 08:12 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 08:12 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 08:12 100-41-41.0 1
2-Hexanone ND ug/L 11/26/17 08:12 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 08:12 74-88-45.0 1
Methylene Chloride ND ug/L 11/26/17 08:12 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 08:12 108-10-15.0 1
Styrene ND ug/L 11/26/17 08:12 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 08:12 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 08:12 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 08:12 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 08:12 109-99-910.0 1
Toluene ND ug/L 11/26/17 08:12 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 08:12 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 08:12 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 08:12 79-01-61.0 1
Trichlorofluoromethane 0.32J ug/L 11/26/17 08:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 08:12 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 08:12 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 08:12 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 08:12 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 08:12 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/26/17 08:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %11/26/17 08:12 17060-07-070-130 1
Toluene-d8 (S)106 %11/26/17 08:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW4 Lab ID: 92364018008 Collected: 11/17/17 11:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 192000 ug/L 11/28/17 19:205000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 317000 ug/L 11/21/17 01:2525000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 26700 ug/L 11/28/17 03:34 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 36800 ug/L 11/23/17 00:31 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:37 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW10 Lab ID: 92364018009 Collected: 11/17/17 11:20 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JSH 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 11:20 12/13/17 14:101
Field pH 6.3 Std. Units 12/13/17 14:100.10 1
Field Temperature 16.3 deg C 12/13/17 14:100.50 1
Static Water Level 12.12 feet 12/13/17 14:101
Field Specific Conductance 1989 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 0.1 mg/L 12/13/17 14:10 7782-44-71
Total Well Depth 21.00 feet 12/13/17 14:101
REDOX -44.7 mV 12/13/17 14:101
Turbidity 9.3 NTU 12/13/17 14:101.0 1
Odor METHANE 12/13/17 14:101
Appearance CLEAR 12/13/17 14:101
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 11/29/17 16:58 309-00-211/22/17 17:100.050 1
alpha-BHC ND ug/L 11/29/17 16:58 319-84-611/22/17 17:100.050 1
beta-BHC ND ug/L 11/29/17 16:58 319-85-711/22/17 17:100.050 1
delta-BHC ND ug/L 11/29/17 16:58 319-86-811/22/17 17:100.050 1
gamma-BHC (Lindane)ND ug/L 11/29/17 16:58 58-89-911/22/17 17:100.050 1
Chlordane (Technical)ND ug/L 11/29/17 16:58 57-74-911/22/17 17:100.20 1
4,4'-DDD ND ug/L 11/29/17 16:58 72-54-811/22/17 17:100.050 1
4,4'-DDE ND ug/L 11/29/17 16:58 72-55-911/22/17 17:100.050 1
4,4'-DDT ND ug/L 11/29/17 16:58 50-29-311/22/17 17:100.050 1
Dieldrin ND ug/L 11/29/17 16:58 60-57-111/22/17 17:100.050 1
Endosulfan I ND ug/L 11/29/17 16:58 959-98-811/22/17 17:100.050 1
Endosulfan II ND ug/L 11/29/17 16:58 33213-65-911/22/17 17:100.050 1
Endosulfan sulfate ND ug/L 11/29/17 16:58 1031-07-811/22/17 17:100.050 1
Endrin ND ug/L 11/29/17 16:58 72-20-811/22/17 17:100.050 1
Endrin aldehyde ND ug/L 11/29/17 16:58 7421-93-411/22/17 17:100.050 1
Endrin ketone ND ug/L 11/29/17 16:58 53494-70-511/22/17 17:100.050 1
Heptachlor ND ug/L 11/29/17 16:58 76-44-811/22/17 17:100.050 1
Heptachlor epoxide ND ug/L 11/29/17 16:58 1024-57-311/22/17 17:100.050 1
Hexachlorobenzene ND ug/L 11/29/17 16:58 118-74-111/22/17 17:100.050 1
Methoxychlor ND ug/L 11/29/17 16:58 72-43-511/22/17 17:100.15 1
Mirex ND ug/L 11/29/17 16:58 2385-85-511/22/17 17:100.15 1
Toxaphene ND ug/L 11/29/17 16:58 8001-35-211/22/17 17:100.20 1
Surrogates
Tetrachloro-m-xylene (S)28 %11/29/17 16:58 877-09-811/22/17 17:1020-130 1
Decachlorobiphenyl (S)46 %11/29/17 16:58 2051-24-311/22/17 17:1020-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 03:29 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 03:29 7440-38-211/21/17 12:0010.0 1
Barium 106 ug/L 12/07/17 03:29 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 03:29 7440-41-711/21/17 12:001.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW10 Lab ID: 92364018009 Collected: 11/17/17 11:20 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Cadmium ND ug/L 12/07/17 03:29 7440-43-911/21/17 12:001.0 1
Chromium 4.6J ug/L 12/07/17 03:29 7440-47-311/21/17 12:005.0 1
Cobalt 22.5 ug/L 12/07/17 03:29 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 03:29 7440-50-811/21/17 12:005.0 1
Iron 3270 ug/L 12/07/17 03:29 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 03:29 7439-92-111/21/17 12:005.0 1
Manganese 13800 ug/L 12/07/17 12:00 7439-96-511/21/17 12:0025.0 5
Nickel 7.6 ug/L 12/07/17 03:29 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 03:29 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 03:29 7440-22-411/21/17 12:005.0 1
Sodium 138000 ug/L 12/07/17 12:00 7440-23-511/21/17 12:0025000 5
Tin ND ug/L 12/07/17 03:29 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 03:29 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 03:29 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:36 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 14:04 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.1J ug/L 11/26/17 08:30 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 08:30 75-05-850.0 1
Acrolein ND ug/L 11/26/17 08:30 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 08:30 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 08:30 107-05-12.0 1
Benzene 0.52J ug/L 11/26/17 08:30 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 08:30 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 08:30 75-27-41.0 1
Bromoform ND ug/L 11/26/17 08:30 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 08:30 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 08:30 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 08:30 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 08:30 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 08:30 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 08:30 75-00-31.0 1
Chloroform ND ug/L 11/26/17 08:30 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 08:30 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 08:30 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 08:30 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 08:30 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 08:30 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 08:30 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 08:30 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 08:30 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW10 Lab ID: 92364018009 Collected: 11/17/17 11:20 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 11/26/17 08:30 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 08:30 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 08:30 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 08:30 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 08:30 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 08:30 75-35-41.0 1
cis-1,2-Dichloroethene 0.23J ug/L 11/26/17 08:30 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 08:30 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 08:30 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 08:30 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 08:30 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 08:30 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 08:30 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 08:30 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 08:30 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 08:30 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 08:30 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 08:30 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 08:30 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 08:30 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 08:30 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 08:30 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 08:30 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)1.1J ug/L 11/26/17 08:30 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 08:30 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 08:30 107-12-020.0 1
Styrene ND ug/L 11/26/17 08:30 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 08:30 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 08:30 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 08:30 127-18-41.0 1
Tetrahydrofuran 131 ug/L 11/26/17 08:30 109-99-910.0 1
Toluene ND ug/L 11/26/17 08:30 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 08:30 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 08:30 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 08:30 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 08:30 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 08:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 08:30 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 08:30 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 08:30 75-01-41.0 1
m&p-Xylene 1.1J ug/L 11/26/17 08:30 179601-23-12.0 1
o-Xylene 0.97J ug/L 11/26/17 08:30 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)104 %11/26/17 08:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %11/26/17 08:30 17060-07-070-130 1
Toluene-d8 (S)108 %11/26/17 08:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-MW10 Lab ID: 92364018009 Collected: 11/17/17 11:20 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 520000 ug/L 11/29/17 13:125000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 1430000 ug/L 11/21/17 01:25125000 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 127 ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 64100 ug/L 11/28/17 08:44 14808-79-87000 7
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 163000 ug/L 11/23/17 02:32 16887-00-65000 5
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:38 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW2 Lab ID: 92364018010 Collected: 11/17/17 11:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 12/13/17 14:101
Collected Date 11/17/17 12/13/17 14:101
Collected Time 11:30 12/13/17 14:101
Field pH 7.1 Std. Units 12/13/17 14:100.10 1
Field Temperature 10.3 deg C 12/13/17 14:100.50 1
Field Specific Conductance 181.0 umhos/cm 12/13/17 14:101.0 1
Oxygen, Dissolved 7.80 mg/L 12/13/17 14:10 7782-44-71
REDOX -50.3 mV 12/13/17 14:101
Turbidity 8.66 NTU 12/13/17 14:101.0 1
Odor NONE 12/13/17 14:101
Appearance MURKY 12/13/17 14:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/07/17 12:03 7440-36-011/21/17 12:005.0 1
Arsenic ND ug/L 12/07/17 12:03 7440-38-211/21/17 12:0010.0 1
Barium 65.4 ug/L 12/07/17 12:03 7440-39-311/21/17 12:005.0 1
Beryllium ND ug/L 12/07/17 12:03 7440-41-711/21/17 12:001.0 1
Cadmium ND ug/L 12/07/17 12:03 7440-43-911/21/17 12:001.0 1
Chromium 3.8J ug/L 12/07/17 12:03 7440-47-311/21/17 12:005.0 1
Cobalt ND ug/L 12/07/17 12:03 7440-48-411/21/17 12:005.0 1
Copper ND ug/L 12/07/17 12:03 7440-50-811/21/17 12:005.0 1
Iron 1740 ug/L 12/07/17 12:03 7439-89-611/21/17 12:0050.0 1
Lead ND ug/L 12/07/17 12:03 7439-92-111/21/17 12:005.0 1
Manganese 196 ug/L 12/07/17 12:03 7439-96-511/21/17 12:005.0 1
Nickel ND ug/L 12/07/17 12:03 7440-02-011/21/17 12:005.0 1
Selenium ND ug/L 12/07/17 12:03 7782-49-211/21/17 12:0010.0 1
Silver ND ug/L 12/07/17 12:03 7440-22-411/21/17 12:005.0 1
Sodium 11600 ug/L 12/07/17 12:03 7440-23-511/21/17 12:005000 1
Tin ND ug/L 12/07/17 12:03 7440-31-511/21/17 12:005.0 1
Vanadium ND ug/L 12/07/17 12:03 7440-62-211/21/17 12:005.0 1
Zinc ND ug/L 12/07/17 12:03 7440-66-611/21/17 12:0010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/21/17 22:38 7440-28-011/19/17 13:000.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/29/17 14:13 7439-97-611/28/17 00:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Acenaphthene ND ug/L 11/28/17 14:01 83-32-911/23/17 05:4110.0 1
Acenaphthylene ND ug/L 11/28/17 14:01 208-96-811/23/17 05:4110.0 1
Acetophenone ND ug/L 11/28/17 14:01 98-86-211/23/17 05:4110.0 1
Anthracene ND ug/L 11/28/17 14:01 120-12-711/23/17 05:4110.0 1
Benzo(a)anthracene ND ug/L 11/28/17 14:01 56-55-311/23/17 05:4110.0 1
Benzo(a)pyrene ND ug/L 11/28/17 14:01 50-32-811/23/17 05:4110.0 1
Benzo(b)fluoranthene ND ug/L 11/28/17 14:01 205-99-211/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW2 Lab ID: 92364018010 Collected: 11/17/17 11:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
Benzo(g,h,i)perylene ND ug/L 11/28/17 14:01 191-24-211/23/17 05:4110.0 1
Benzo(k)fluoranthene ND ug/L 11/28/17 14:01 207-08-911/23/17 05:4110.0 1
Benzyl alcohol ND ug/L 11/28/17 14:01 100-51-611/23/17 05:4120.0 1
4-Bromophenylphenyl ether ND ug/L 11/28/17 14:01 101-55-311/23/17 05:4110.0 1
Butylbenzylphthalate ND ug/L 11/28/17 14:01 85-68-711/23/17 05:4110.0 1
4-Chloro-3-methylphenol ND ug/L 11/28/17 14:01 59-50-711/23/17 05:4120.0 1
4-Chloroaniline ND ug/L 11/28/17 14:01 106-47-811/23/17 05:4120.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/28/17 14:01 111-91-111/23/17 05:4110.0 1
bis(2-Chloroethyl) ether ND ug/L 11/28/17 14:01 111-44-411/23/17 05:4110.0 1
2-Chloronaphthalene ND ug/L 11/28/17 14:01 91-58-711/23/17 05:4110.0 1
2-Chlorophenol ND ug/L 11/28/17 14:01 95-57-811/23/17 05:4110.0 1
4-Chlorophenylphenyl ether ND ug/L 11/28/17 14:01 7005-72-311/23/17 05:4110.0 1
Chrysene ND ug/L 11/28/17 14:01 218-01-911/23/17 05:4110.0 1
Dibenz(a,h)anthracene ND ug/L 11/28/17 14:01 53-70-311/23/17 05:4110.0 1
Dibenzofuran ND ug/L 11/28/17 14:01 132-64-911/23/17 05:4110.0 1
3,3'-Dichlorobenzidine ND ug/L 11/28/17 14:01 91-94-111/23/17 05:4120.0 1
2,4-Dichlorophenol ND ug/L 11/28/17 14:01 120-83-211/23/17 05:4110.0 1
Diethylphthalate ND ug/L 11/28/17 14:01 84-66-211/23/17 05:4110.0 1
2,4-Dimethylphenol ND ug/L 11/28/17 14:01 105-67-911/23/17 05:4110.0 1
Dimethylphthalate ND ug/L 11/28/17 14:01 131-11-311/23/17 05:4110.0 1
Di-n-butylphthalate ND ug/L 11/28/17 14:01 84-74-211/23/17 05:4110.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/28/17 14:01 534-52-111/23/17 05:4120.0 1
2,4-Dinitrophenol ND ug/L 11/28/17 14:01 51-28-511/23/17 05:4150.0 1
2,4-Dinitrotoluene ND ug/L 11/28/17 14:01 121-14-211/23/17 05:4110.0 1
2,6-Dinitrotoluene ND ug/L 11/28/17 14:01 606-20-211/23/17 05:4110.0 1
Di-n-octylphthalate ND ug/L 11/28/17 14:01 117-84-011/23/17 05:4110.0 1
Diphenylamine ND ug/L 11/28/17 14:01 122-39-411/23/17 05:4110.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/28/17 14:01 117-81-711/23/17 05:416.0 1
Fluoranthene ND ug/L 11/28/17 14:01 206-44-011/23/17 05:4110.0 1
Fluorene ND ug/L 11/28/17 14:01 86-73-711/23/17 05:4110.0 1
Hexachlorobenzene ND ug/L 11/28/17 14:01 118-74-111/23/17 05:4110.0 1
Hexachlorocyclopentadiene ND ug/L 11/28/17 14:01 77-47-411/23/17 05:4110.0 1
Hexachloroethane ND ug/L 11/28/17 14:01 67-72-111/23/17 05:4110.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/28/17 14:01 193-39-511/23/17 05:4110.0 1
Isophorone ND ug/L 11/28/17 14:01 78-59-111/23/17 05:4110.0 1
2-Methylnaphthalene ND ug/L 11/28/17 14:01 91-57-611/23/17 05:4110.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/28/17 14:01 95-48-711/23/17 05:4110.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/28/17 14:01 15831-10-411/23/17 05:4110.0 1
2-Nitroaniline ND ug/L 11/28/17 14:01 88-74-411/23/17 05:4150.0 1
3-Nitroaniline ND ug/L 11/28/17 14:01 99-09-211/23/17 05:4150.0 1
4-Nitroaniline ND ug/L 11/28/17 14:01 100-01-611/23/17 05:4120.0 1
Nitrobenzene ND ug/L 11/28/17 14:01 98-95-311/23/17 05:4110.0 1
2-Nitrophenol ND ug/L 11/28/17 14:01 88-75-511/23/17 05:4110.0 1
4-Nitrophenol ND ug/L 11/28/17 14:01 100-02-711/23/17 05:4150.0 1
N-Nitrosodimethylamine ND ug/L 11/28/17 14:01 62-75-911/23/17 05:4110.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/28/17 14:01 621-64-711/23/17 05:4110.0 1
N-Nitrosodiphenylamine ND ug/L 11/28/17 14:01 86-30-611/23/17 05:4110.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW2 Lab ID: 92364018010 Collected: 11/17/17 11:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV RVE Semivol Organic
2,2'-Oxybis(1-chloropropane)ND ug/L 11/28/17 14:01 108-60-111/23/17 05:4110.0 1
Phenanthrene ND ug/L 11/28/17 14:01 85-01-811/23/17 05:4110.0 1
Phenol ND ug/L 11/28/17 14:01 108-95-211/23/17 05:4110.0 1
Pyrene ND ug/L 11/28/17 14:01 129-00-011/23/17 05:4110.0 1
2,4,5-Trichlorophenol ND ug/L 11/28/17 14:01 95-95-411/23/17 05:4110.0 1
2,4,6-Trichlorophenol ND ug/L 11/28/17 14:01 88-06-211/23/17 05:4110.0 1
SurrogatesNitrobenzene-d5 (S)68 %11/28/17 14:01 4165-60-011/23/17 05:4140-121 1
2-Fluorobiphenyl (S)59 %11/28/17 14:01 321-60-811/23/17 05:4145-139 1
Terphenyl-d14 (S)81 %11/28/17 14:01 1718-51-011/23/17 05:4148-146 1
Phenol-d6 (S)26 %11/28/17 14:01 13127-88-311/23/17 05:4118-105 1
2-Fluorophenol (S)15 %11/28/17 14:01 367-12-411/23/17 05:4113-118 1
2,4,6-Tribromophenol (S)24 %11/28/17 14:01 118-79-6 S011/23/17 05:4131-170 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 08:47 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 08:47 75-05-850.0 1
Acrolein ND ug/L 11/26/17 08:47 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 08:47 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 08:47 107-05-12.0 1
Benzene ND ug/L 11/26/17 08:47 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 08:47 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 08:47 75-27-41.0 1
Bromoform ND ug/L 11/26/17 08:47 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 08:47 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 08:47 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 08:47 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 08:47 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 08:47 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 08:47 75-00-31.0 1
Chloroform ND ug/L 11/26/17 08:47 67-66-31.0 1
Chloromethane 0.12J ug/L 11/26/17 08:47 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 08:47 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 08:47 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 08:47 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 08:47 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 08:47 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 08:47 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 08:47 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 08:47 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 08:47 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 08:47 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 08:47 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 08:47 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 08:47 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 08:47 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 08:47 156-60-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW2 Lab ID: 92364018010 Collected: 11/17/17 11:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 11/26/17 08:47 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 08:47 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 08:47 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 08:47 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 08:47 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 08:47 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 08:47 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 08:47 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 08:47 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 08:47 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 08:47 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 08:47 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 08:47 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 08:47 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 08:47 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 08:47 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 08:47 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 08:47 107-12-020.0 1
Styrene ND ug/L 11/26/17 08:47 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 08:47 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 08:47 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 08:47 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 08:47 109-99-910.0 1
Toluene ND ug/L 11/26/17 08:47 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 08:47 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 08:47 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 08:47 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 08:47 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 08:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 08:47 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 08:47 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 08:47 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 08:47 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 08:47 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/26/17 08:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %11/26/17 08:47 17060-07-070-130 1
Toluene-d8 (S)110 %11/26/17 08:47 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 57600 ug/L 11/28/17 19:475000 1
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 125000 ug/L 11/21/17 01:2525000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-SW2 Lab ID: 92364018010 Collected: 11/17/17 11:30 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 11/24/17 20:30 18496-25-8100 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 9920 ug/L 11/28/17 04:08 14808-79-81000 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 15200 ug/L 11/23/17 00:33 16887-00-61000 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 11/21/17 13:39 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-TRIP BLANK Lab ID: 92364018011 Collected: 11/17/17 00:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/26/17 09:05 67-64-125.0 1
Acetonitrile ND ug/L 11/26/17 09:05 75-05-850.0 1
Acrolein ND ug/L 11/26/17 09:05 107-02-810.0 1
Acrylonitrile ND ug/L 11/26/17 09:05 107-13-110.0 1
Allyl chloride ND ug/L 11/26/17 09:05 107-05-12.0 1
Benzene ND ug/L 11/26/17 09:05 71-43-21.0 1
Bromochloromethane ND ug/L 11/26/17 09:05 74-97-51.0 1
Bromodichloromethane ND ug/L 11/26/17 09:05 75-27-41.0 1
Bromoform ND ug/L 11/26/17 09:05 75-25-21.0 1
Bromomethane ND ug/L 11/26/17 09:05 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/26/17 09:05 78-93-35.0 1
Carbon disulfide ND ug/L 11/26/17 09:05 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/26/17 09:05 56-23-51.0 1
Chlorobenzene ND ug/L 11/26/17 09:05 108-90-71.0 1
Chloroethane ND ug/L 11/26/17 09:05 75-00-31.0 1
Chloroform ND ug/L 11/26/17 09:05 67-66-31.0 1
Chloromethane ND ug/L 11/26/17 09:05 74-87-31.0 1
Chloroprene ND ug/L 11/26/17 09:05 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/26/17 09:05 96-12-82.0 1
Dibromochloromethane ND ug/L 11/26/17 09:05 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/26/17 09:05 106-93-41.0 1
Dibromomethane ND ug/L 11/26/17 09:05 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/26/17 09:05 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/26/17 09:05 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/26/17 09:05 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/26/17 09:05 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 11/26/17 09:05 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/26/17 09:05 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/26/17 09:05 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/26/17 09:05 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/26/17 09:05 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/26/17 09:05 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/26/17 09:05 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/26/17 09:05 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/26/17 09:05 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/26/17 09:05 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/26/17 09:05 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/26/17 09:05 10061-02-61.0 1
Ethylbenzene ND ug/L 11/26/17 09:05 100-41-41.0 1
Ethyl methacrylate ND ug/L 11/26/17 09:05 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 11/26/17 09:05 87-68-31.0 1
2-Hexanone ND ug/L 11/26/17 09:05 591-78-65.0 1
Iodomethane ND ug/L 11/26/17 09:05 74-88-45.0 1
Isobutanol ND ug/L 11/26/17 09:05 78-83-1100 1
Methacrylonitrile ND ug/L 11/26/17 09:05 126-98-710.0 1
Methylene Chloride ND ug/L 11/26/17 09:05 75-09-21.0 1
Methyl methacrylate ND ug/L 11/26/17 09:05 80-62-62.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 90
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92364018
OSR
Sample: 3412-TRIP BLANK Lab ID: 92364018011 Collected: 11/17/17 00:00 Received: 11/17/17 17:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
4-Methyl-2-pentanone (MIBK)ND ug/L 11/26/17 09:05 108-10-15.0 1
Naphthalene ND ug/L 11/26/17 09:05 91-20-31.0 1
Propionitrile ND ug/L 11/26/17 09:05 107-12-020.0 1
Styrene ND ug/L 11/26/17 09:05 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/26/17 09:05 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/26/17 09:05 79-34-51.0 1
Tetrachloroethene ND ug/L 11/26/17 09:05 127-18-41.0 1
Tetrahydrofuran ND ug/L 11/26/17 09:05 109-99-910.0 1
Toluene ND ug/L 11/26/17 09:05 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 11/26/17 09:05 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/26/17 09:05 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/26/17 09:05 79-00-51.0 1
Trichloroethene ND ug/L 11/26/17 09:05 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/26/17 09:05 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/26/17 09:05 96-18-41.0 1
Vinyl acetate ND ug/L 11/26/17 09:05 108-05-42.0 1
Vinyl chloride ND ug/L 11/26/17 09:05 75-01-41.0 1
m&p-Xylene ND ug/L 11/26/17 09:05 179601-23-12.0 1
o-Xylene ND ug/L 11/26/17 09:05 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/26/17 09:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %11/26/17 09:05 17060-07-070-130 1
Toluene-d8 (S)110 %11/26/17 09:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388398
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154671
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 11/29/17 13:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154672LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154673MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879001
2154674
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 94 75-12597 32.5ND 2.4 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387775
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151277
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Antimony ug/L ND 5.0 12/07/17 01:38
Arsenic ug/L ND 10.0 12/07/17 01:38
Barium ug/L ND 5.0 12/07/17 01:38
Beryllium ug/L ND 1.0 12/07/17 01:38
Cadmium ug/L ND 1.0 12/07/17 01:38
Chromium ug/L ND 5.0 12/07/17 11:47
Cobalt ug/L ND 5.0 12/07/17 01:38
Copper ug/L ND 5.0 12/07/17 01:38
Iron ug/L ND 50.0 12/07/17 01:38
Lead ug/L ND 5.0 12/07/17 01:38
Manganese ug/L ND 5.0 12/07/17 01:38
Nickel ug/L ND 5.0 12/07/17 01:38
Selenium ug/L ND 10.0 12/07/17 01:38
Silver ug/L ND 5.0 12/07/17 01:38
Sodium ug/L ND 5000 12/07/17 01:38
Tin ug/L ND 5.0 12/07/17 01:38
Vanadium ug/L ND 5.0 12/07/17 01:38
Zinc ug/L ND 10.0 12/07/17 01:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151278LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 479500 96 80-120
Arsenic ug/L 460500 92 80-120
Barium ug/L 479500 96 80-120
Beryllium ug/L 468500 94 80-120
Cadmium ug/L 471500 94 80-120
Chromium ug/L 467500 93 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 486500 97 80-120
Iron ug/L 46705000 93 80-120
Lead ug/L 470500 94 80-120
Manganese ug/L 463500 93 80-120
Nickel ug/L 468500 94 80-120
Selenium ug/L 448500 90 80-120
Silver ug/L 234250 93 80-120
Sodium ug/L 4780J5000 96 80-120
Tin ug/L 477500 95 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151278LABORATORY CONTROL SAMPLE:
LCSSpike
Vanadium ug/L 478500 96 80-120
Zinc ug/L 470500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879001
2151280
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-125101 5500ND483 507
Arsenic ug/L 500 94 75-12598 4500ND470 490
Barium ug/L 500 99 75-125101 2500ND496 509
Beryllium ug/L 500 98 75-125100 2500ND490 500
Cadmium ug/L 500 95 75-125100 5500ND478 501
Chromium ug/L 500 101 75-125101 05003.2J 506 507
Cobalt ug/L 500 99 75-125102 4500ND494 512
Copper ug/L 500 97 75-125102 5500ND485 511
Iron ug/L 5000 99 75-125100 15000ND4960 5020
Lead ug/L 500 97 75-125101 4500ND485 503
Manganese ug/L 500 100 75-125100 0500ND500 499
Nickel ug/L 500 97 75-125101 4500ND483 503
Selenium ug/L 500 89 75-12593 5500ND449 470
Silver ug/L 250 97 75-12599 3250ND242 249
Sodium ug/L 5000 98 75-125100 25000539J5440 5560
Tin ug/L 500 99 75-125103 4500ND494 514
Vanadium ug/L 500 102 75-125102 0500ND511 511
Zinc ug/L 500 99 75-125102 3500ND498 511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387486
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2149919
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Thallium ug/L ND 0.10 11/21/17 21:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2149920LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 93.1100 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2149921MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879001
2149922
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-125101 1100ND100 101
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2149923MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018002
2149924
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-125102 2100ND100 102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388168
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153766
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/26/17 01:33
1,1,1-Trichloroethane ug/L ND 1.0 11/26/17 01:33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/26/17 01:33
1,1,2-Trichloroethane ug/L ND 1.0 11/26/17 01:33
1,1-Dichloroethane ug/L ND 1.0 11/26/17 01:33
1,1-Dichloroethene ug/L ND 1.0 11/26/17 01:33
1,1-Dichloropropene ug/L ND 1.0 11/26/17 01:33
1,2,3-Trichloropropane ug/L ND 1.0 11/26/17 01:33
1,2,4-Trichlorobenzene ug/L ND 1.0 11/26/17 01:33
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/26/17 01:33
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/26/17 01:33
1,2-Dichlorobenzene ug/L ND 1.0 11/26/17 01:33
1,2-Dichloroethane ug/L ND 1.0 11/26/17 01:33
1,2-Dichloropropane ug/L ND 1.0 11/26/17 01:33
1,3-Dichlorobenzene ug/L ND 1.0 11/26/17 01:33
1,3-Dichloropropane ug/L ND 1.0 11/26/17 01:33
1,4-Dichlorobenzene ug/L ND 1.0 11/26/17 01:33
2,2-Dichloropropane ug/L ND 1.0 11/26/17 01:33
2-Butanone (MEK)ug/L ND 5.0 11/26/17 01:33
2-Hexanone ug/L ND 5.0 11/26/17 01:33
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/26/17 01:33
Acetone ug/L ND 25.0 11/26/17 01:33
Acetonitrile ug/L ND 50.0 11/26/17 01:33
Acrolein ug/L ND 10.0 11/26/17 01:33
Acrylonitrile ug/L ND 10.0 11/26/17 01:33
Allyl chloride ug/L ND 2.0 11/26/17 01:33
Benzene ug/L ND 1.0 11/26/17 01:33
Bromochloromethane ug/L ND 1.0 11/26/17 01:33
Bromodichloromethane ug/L ND 1.0 11/26/17 01:33
Bromoform ug/L ND 1.0 11/26/17 01:33
Bromomethane ug/L ND 2.0 11/26/17 01:33
Carbon disulfide ug/L ND 2.0 11/26/17 01:33
Carbon tetrachloride ug/L ND 1.0 11/26/17 01:33
Chlorobenzene ug/L ND 1.0 11/26/17 01:33
Chloroethane ug/L ND 1.0 11/26/17 01:33
Chloroform ug/L ND 1.0 11/26/17 01:33
Chloromethane ug/L ND 1.0 11/26/17 01:33
Chloroprene ug/L ND 5.0 11/26/17 01:33
cis-1,2-Dichloroethene ug/L ND 1.0 11/26/17 01:33
cis-1,3-Dichloropropene ug/L ND 1.0 11/26/17 01:33
Dibromochloromethane ug/L ND 1.0 11/26/17 01:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153766
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006
Matrix: Water
Analyzed
Dibromomethane ug/L ND 1.0 11/26/17 01:33
Dichlorodifluoromethane ug/L ND 1.0 11/26/17 01:33
Ethyl methacrylate ug/L ND 1.0 11/26/17 01:33
Ethylbenzene ug/L ND 1.0 11/26/17 01:33
Hexachloro-1,3-butadiene ug/L ND 1.0 11/26/17 01:33
Iodomethane ug/L ND 5.0 11/26/17 01:33
Isobutanol ug/L ND 100 11/26/17 01:33
m&p-Xylene ug/L ND 2.0 11/26/17 01:33
Methacrylonitrile ug/L ND 10.0 11/26/17 01:33
Methyl methacrylate ug/L ND 2.0 11/26/17 01:33
Methylene Chloride ug/L ND 1.0 11/26/17 01:33
Naphthalene ug/L ND 1.0 11/26/17 01:33
o-Xylene ug/L ND 1.0 11/26/17 01:33
Propionitrile ug/L ND 20.0 11/26/17 01:33
Styrene ug/L ND 1.0 11/26/17 01:33
Tetrachloroethene ug/L ND 1.0 11/26/17 01:33
Tetrahydrofuran ug/L ND 10.0 11/26/17 01:33
Toluene ug/L ND 1.0 11/26/17 01:33
trans-1,2-Dichloroethene ug/L ND 1.0 11/26/17 01:33
trans-1,3-Dichloropropene ug/L ND 1.0 11/26/17 01:33
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/26/17 01:33
Trichloroethene ug/L ND 1.0 11/26/17 01:33
Trichlorofluoromethane ug/L ND 1.0 11/26/17 01:33
Vinyl acetate ug/L ND 2.0 11/26/17 01:33
Vinyl chloride ug/L ND 1.0 11/26/17 01:33
1,2-Dichloroethane-d4 (S)%88 70-130 11/26/17 01:33
4-Bromofluorobenzene (S)%101 70-130 11/26/17 01:33
Toluene-d8 (S)%108 70-130 11/26/17 01:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153767LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.450 93 80-125
1,1,1-Trichloroethane ug/L 48.750 97 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 53.850 108 85-125
1,1-Dichloroethane ug/L 49.250 98 73-126
1,1-Dichloroethene ug/L 53.550 107 66-135
1,1-Dichloropropene ug/L 48.250 96 74-135
1,2,3-Trichloropropane ug/L 47.350 95 75-130
1,2,4-Trichlorobenzene ug/L 50.050 100 75-134
1,2-Dibromo-3-chloropropane ug/L 43.550 87 71-133
1,2-Dibromoethane (EDB)ug/L 49.650 99 83-124
1,2-Dichlorobenzene ug/L 47.650 95 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153767LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 50.850 102 67-128
1,2-Dichloropropane ug/L 53.750 107 75-132
1,3-Dichlorobenzene ug/L 47.850 96 77-130
1,3-Dichloropropane ug/L 50.250 100 76-131
1,4-Dichlorobenzene ug/L 48.150 96 78-130
2,2-Dichloropropane ug/L 31.150 62 40-160
2-Butanone (MEK)ug/L 92.7100 93 61-144
2-Hexanone ug/L 95.5100 96 68-143
4-Methyl-2-pentanone (MIBK)ug/L 89.2100 89 72-135
Acetone ug/L 94.8100 95 48-146
Acetonitrile ug/L 457500 91 62-150
Acrolein ug/L 256250 102 24-160
Acrylonitrile ug/L 228250 91 40-160
Allyl chloride ug/L 46.250 92 66-137
Benzene ug/L 51.050 102 80-125
Bromochloromethane ug/L 52.550 105 71-125
Bromodichloromethane ug/L 52.850 106 78-124
Bromoform ug/L 45.650 91 71-128
Bromomethane ug/L 47.050 94 40-160
Carbon disulfide ug/L 49.850 100 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 49.750 99 81-122
Chloroethane ug/L 51.250 102 39-148
Chloroform ug/L 50.450 101 73-127
Chloromethane ug/L 44.550 89 44-146
Chloroprene ug/L 49.750 99 75-145
cis-1,2-Dichloroethene ug/L 52.750 105 74-124
cis-1,3-Dichloropropene ug/L 47.550 95 72-132
Dibromochloromethane ug/L 47.650 95 78-125
Dibromomethane ug/L 49.550 99 82-120
Dichlorodifluoromethane ug/L 50.850 102 34-157
Ethyl methacrylate ug/L 46.950 94 82-121
Ethylbenzene ug/L 49.150 98 79-121
Hexachloro-1,3-butadiene ug/L 47.350 95 72-131
Iodomethane ug/L 91.9100 92 39-154
Isobutanol ug/L 8761000 88 34-160
m&p-Xylene ug/L 97.5100 97 81-124
Methacrylonitrile ug/L 480500 96 74-134
Methyl methacrylate ug/L 50.750 101 84-124
Methylene Chloride ug/L 46.750 93 64-133
Naphthalene ug/L 49.650 99 73-133
o-Xylene ug/L 49.850 100 79-131
Propionitrile ug/L 519500 104 73-140
Styrene ug/L 49.650 99 84-126
Tetrachloroethene ug/L 51.150 102 78-122
Tetrahydrofuran ug/L 472500 94 69-148
Toluene ug/L 46.450 93 80-121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153767LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,2-Dichloroethene ug/L 48.850 98 71-127
trans-1,3-Dichloropropene ug/L 43.550 87 69-141
trans-1,4-Dichloro-2-butene ug/L 42.150 84 40-160
Trichloroethene ug/L 54.350 109 78-122
Trichlorofluoromethane ug/L 51.350 103 53-137
Vinyl acetate ug/L 94.9100 95 40-160
Vinyl chloride ug/L 52.750 105 58-137
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153768MATRIX SPIKE SAMPLE:
MSSpike
Result
92363938001
1,1,1,2-Tetrachloroethane ug/L 17.420 87 70-130ND
1,1,1-Trichloroethane ug/L 21.820 109 70-130ND
1,1,2,2-Tetrachloroethane ug/L 17.920 90 70-130ND
1,1,2-Trichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 24.220 121 70-166ND
1,1-Dichloropropene ug/L 21.920 109 70-130ND
1,2,3-Trichloropropane ug/L 18.420 92 70-130ND
1,2,4-Trichlorobenzene ug/L 20.520 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 14.120 71 70-130ND
1,2-Dibromoethane (EDB)ug/L 17.620 88 70-130ND
1,2-Dichlorobenzene ug/L 19.220 96 70-130ND
1,2-Dichloroethane ug/L 21.520 108 70-130ND
1,2-Dichloropropane ug/L 21.220 106 70-130ND
1,3-Dichlorobenzene ug/L 19.120 96 70-130ND
1,3-Dichloropropane ug/L 18.220 91 70-130ND
1,4-Dichlorobenzene ug/L 19.320 97 70-130ND
2,2-Dichloropropane ug/L 18.620 93 70-130ND
2-Butanone (MEK)ug/L 34.140 85 70-130ND
2-Hexanone ug/L 35.140 88 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 34.640 86 70-130ND
Acetone ug/L 39.540 99 70-130ND
Acrylonitrile ug/L 105100 105 70-130ND
Benzene ug/L 20.920 105 70-148ND
Bromochloromethane ug/L 23.020 115 70-130ND
Bromodichloromethane ug/L 21.120 106 70-130ND
Bromoform ug/L 16.920 84 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.920 114 70-130ND
Carbon tetrachloride ug/L 22.620 113 70-130ND
Chlorobenzene ug/L 20.020 100 70-146ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153768MATRIX SPIKE SAMPLE:
MSSpike
Result
92363938001
Chloroethane ug/L 25.420 127 70-130ND
Chloroform ug/L 21.520 107 70-130ND
Chloromethane ug/L 21.920 109 70-130ND
cis-1,2-Dichloroethene ug/L 22.920 114 70-130ND
cis-1,3-Dichloropropene ug/L 18.220 91 70-130ND
Dibromochloromethane ug/L 17.420 87 70-130ND
Dibromomethane ug/L 20.920 105 70-130ND
Dichlorodifluoromethane ug/L 29.5 M120147 70-130ND
Ethylbenzene ug/L 20.020 100 70-130ND
Hexachloro-1,3-butadiene ug/L 21.220 106 70-130ND
Iodomethane ug/L 37.640 94 70-130ND
m&p-Xylene ug/L 40.140 100 70-130ND
Methylene Chloride ug/L 21.120 106 70-130ND
Naphthalene ug/L 18.820 94 70-130ND
o-Xylene ug/L 20.120 100 70-130ND
Styrene ug/L 19.420 97 70-130ND
Tetrachloroethene ug/L 31.920 107 70-13010.5
Tetrahydrofuran ug/L 179200 89 70-130ND
Toluene ug/L 20.520 103 70-155ND
trans-1,2-Dichloroethene ug/L 23.420 117 70-130ND
trans-1,3-Dichloropropene ug/L 16.020 80 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.920 80 70-130ND
Trichloroethene ug/L 23.520 118 69-151ND
Trichlorofluoromethane ug/L 25.420 127 70-130ND
Vinyl acetate ug/L 33.540 84 70-130ND
Vinyl chloride ug/L 26.5 M120132 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92363938002
2153769SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363938002
2153769SAMPLE DUPLICATE:
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L 0.72J0.66J
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L 16.2 216.5
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L 6.3 26.2
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%91 292
4-Bromofluorobenzene (S)%102 0103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363938002
2153769SAMPLE DUPLICATE:
Toluene-d8 (S)%108 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388169
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples: 92364018007, 92364018008, 92364018009, 92364018010, 92364018011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153770
Associated Lab Samples:92364018007, 92364018008, 92364018009, 92364018010, 92364018011
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/26/17 01:50
1,1,1-Trichloroethane ug/L ND 1.0 11/26/17 01:50
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/26/17 01:50
1,1,2-Trichloroethane ug/L ND 1.0 11/26/17 01:50
1,1-Dichloroethane ug/L ND 1.0 11/26/17 01:50
1,1-Dichloroethene ug/L ND 1.0 11/26/17 01:50
1,1-Dichloropropene ug/L ND 1.0 11/26/17 01:50
1,2,3-Trichloropropane ug/L ND 1.0 11/26/17 01:50
1,2,4-Trichlorobenzene ug/L ND 1.0 11/26/17 01:50
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/26/17 01:50
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/26/17 01:50
1,2-Dichlorobenzene ug/L ND 1.0 11/26/17 01:50
1,2-Dichloroethane ug/L ND 1.0 11/26/17 01:50
1,2-Dichloropropane ug/L ND 1.0 11/26/17 01:50
1,3-Dichlorobenzene ug/L ND 1.0 11/26/17 01:50
1,3-Dichloropropane ug/L ND 1.0 11/26/17 01:50
1,4-Dichlorobenzene ug/L ND 1.0 11/26/17 01:50
2,2-Dichloropropane ug/L ND 1.0 11/26/17 01:50
2-Butanone (MEK)ug/L ND 5.0 11/26/17 01:50
2-Hexanone ug/L ND 5.0 11/26/17 01:50
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/26/17 01:50
Acetone ug/L ND 25.0 11/26/17 01:50
Acetonitrile ug/L ND 50.0 11/26/17 01:50
Acrolein ug/L ND 10.0 11/26/17 01:50
Acrylonitrile ug/L ND 10.0 11/26/17 01:50
Allyl chloride ug/L ND 2.0 11/26/17 01:50
Benzene ug/L ND 1.0 11/26/17 01:50
Bromochloromethane ug/L ND 1.0 11/26/17 01:50
Bromodichloromethane ug/L ND 1.0 11/26/17 01:50
Bromoform ug/L ND 1.0 11/26/17 01:50
Bromomethane ug/L ND 2.0 11/26/17 01:50
Carbon disulfide ug/L ND 2.0 11/26/17 01:50
Carbon tetrachloride ug/L ND 1.0 11/26/17 01:50
Chlorobenzene ug/L ND 1.0 11/26/17 01:50
Chloroethane ug/L ND 1.0 11/26/17 01:50
Chloroform ug/L ND 1.0 11/26/17 01:50
Chloromethane ug/L ND 1.0 11/26/17 01:50
Chloroprene ug/L ND 5.0 11/26/17 01:50
cis-1,2-Dichloroethene ug/L ND 1.0 11/26/17 01:50
cis-1,3-Dichloropropene ug/L ND 1.0 11/26/17 01:50
Dibromochloromethane ug/L ND 1.0 11/26/17 01:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153770
Associated Lab Samples:92364018007, 92364018008, 92364018009, 92364018010, 92364018011
Matrix: Water
Analyzed
Dibromomethane ug/L ND 1.0 11/26/17 01:50
Dichlorodifluoromethane ug/L ND 1.0 11/26/17 01:50
Ethyl methacrylate ug/L ND 1.0 11/26/17 01:50
Ethylbenzene ug/L ND 1.0 11/26/17 01:50
Hexachloro-1,3-butadiene ug/L ND 1.0 11/26/17 01:50
Iodomethane ug/L ND 5.0 11/26/17 01:50
Isobutanol ug/L ND 100 11/26/17 01:50
m&p-Xylene ug/L ND 2.0 11/26/17 01:50
Methacrylonitrile ug/L ND 10.0 11/26/17 01:50
Methyl methacrylate ug/L ND 2.0 11/26/17 01:50
Methylene Chloride ug/L ND 1.0 11/26/17 01:50
Naphthalene ug/L ND 1.0 11/26/17 01:50
o-Xylene ug/L ND 1.0 11/26/17 01:50
Propionitrile ug/L ND 20.0 11/26/17 01:50
Styrene ug/L ND 1.0 11/26/17 01:50
Tetrachloroethene ug/L ND 1.0 11/26/17 01:50
Tetrahydrofuran ug/L ND 10.0 11/26/17 01:50
Toluene ug/L ND 1.0 11/26/17 01:50
trans-1,2-Dichloroethene ug/L ND 1.0 11/26/17 01:50
trans-1,3-Dichloropropene ug/L ND 1.0 11/26/17 01:50
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/26/17 01:50
Trichloroethene ug/L ND 1.0 11/26/17 01:50
Trichlorofluoromethane ug/L ND 1.0 11/26/17 01:50
Vinyl acetate ug/L ND 2.0 11/26/17 01:50
Vinyl chloride ug/L ND 1.0 11/26/17 01:50
1,2-Dichloroethane-d4 (S)%94 70-130 11/26/17 01:50
4-Bromofluorobenzene (S)%102 70-130 11/26/17 01:50
Toluene-d8 (S)%109 70-130 11/26/17 01:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153771LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.750 89 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 42.950 86 79-124
1,1,2-Trichloroethane ug/L 51.450 103 85-125
1,1-Dichloroethane ug/L 49.550 99 73-126
1,1-Dichloroethene ug/L 49.650 99 66-135
1,1-Dichloropropene ug/L 48.850 98 74-135
1,2,3-Trichloropropane ug/L 42.450 85 75-130
1,2,4-Trichlorobenzene ug/L 49.450 99 75-134
1,2-Dibromo-3-chloropropane ug/L 38.050 76 71-133
1,2-Dibromoethane (EDB)ug/L 45.750 91 83-124
1,2-Dichlorobenzene ug/L 46.850 94 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153771LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 49.850 100 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
1,3-Dichlorobenzene ug/L 47.150 94 77-130
1,3-Dichloropropane ug/L 47.450 95 76-131
1,4-Dichlorobenzene ug/L 47.550 95 78-130
2,2-Dichloropropane ug/L 32.450 65 40-160
2-Butanone (MEK)ug/L 80.5100 80 61-144
2-Hexanone ug/L 79.0100 79 68-143
4-Methyl-2-pentanone (MIBK)ug/L 77.2100 77 72-135
Acetone ug/L 88.4100 88 48-146
Acetonitrile ug/L 429500 86 62-150
Acrolein ug/L 239250 96 24-160
Acrylonitrile ug/L 221250 89 40-160
Allyl chloride ug/L 50.150 100 66-137
Benzene ug/L 50.450 101 80-125
Bromochloromethane ug/L 50.850 102 71-125
Bromodichloromethane ug/L 52.750 105 78-124
Bromoform ug/L 42.250 84 71-128
Bromomethane ug/L 45.650 91 40-160
Carbon disulfide ug/L 48.650 97 50-160
Carbon tetrachloride ug/L 53.450 107 69-131
Chlorobenzene ug/L 48.250 96 81-122
Chloroethane ug/L 48.850 98 39-148
Chloroform ug/L 49.150 98 73-127
Chloromethane ug/L 44.250 88 44-146
Chloroprene ug/L 48.950 98 75-145
cis-1,2-Dichloroethene ug/L 52.150 104 74-124
cis-1,3-Dichloropropene ug/L 46.850 94 72-132
Dibromochloromethane ug/L 45.950 92 78-125
Dibromomethane ug/L 48.250 96 82-120
Dichlorodifluoromethane ug/L 49.650 99 34-157
Ethyl methacrylate ug/L 43.950 88 82-121
Ethylbenzene ug/L 47.550 95 79-121
Hexachloro-1,3-butadiene ug/L 47.850 96 72-131
Iodomethane ug/L 89.3100 89 39-154
Isobutanol ug/L 8131000 81 34-160
m&p-Xylene ug/L 93.4100 93 81-124
Methacrylonitrile ug/L 433500 87 74-134
Methyl methacrylate ug/L 45.650 91 84-124
Methylene Chloride ug/L 49.150 98 64-133
Naphthalene ug/L 47.450 95 73-133
o-Xylene ug/L 48.250 96 79-131
Propionitrile ug/L 436500 87 73-140
Styrene ug/L 47.450 95 84-126
Tetrachloroethene ug/L 48.450 97 78-122
Tetrahydrofuran ug/L 397500 79 69-148
Toluene ug/L 46.650 93 80-121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153771LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,2-Dichloroethene ug/L 52.350 105 71-127
trans-1,3-Dichloropropene ug/L 43.750 87 69-141
trans-1,4-Dichloro-2-butene ug/L 37.650 75 40-160
Trichloroethene ug/L 56.450 113 78-122
Trichlorofluoromethane ug/L 48.750 97 53-137
Vinyl acetate ug/L 91.1100 91 40-160
Vinyl chloride ug/L 51.450 103 58-137
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153772MATRIX SPIKE SAMPLE:
MSSpike
Result
92364018007
1,1,1,2-Tetrachloroethane ug/L 17.920 89 70-130ND
1,1,1-Trichloroethane ug/L 22.320 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.720 98 70-130ND
1,1,2-Trichloroethane ug/L 21.220 106 70-130ND
1,1-Dichloroethane ug/L 22.820 114 70-130ND
1,1-Dichloroethene ug/L 24.520 122 70-166ND
1,2,3-Trichloropropane ug/L 20.120 101 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.420 82 70-130ND
1,2-Dibromoethane (EDB)ug/L 18.920 94 70-130ND
1,2-Dichlorobenzene ug/L 19.520 98 70-130ND
1,2-Dichloroethane ug/L 22.320 111 70-130ND
1,2-Dichloropropane ug/L 21.820 109 70-130ND
1,4-Dichlorobenzene ug/L 20.020 100 70-130ND
2-Butanone (MEK)ug/L 39.840 100 70-130ND
2-Hexanone ug/L 41.040 103 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 70-130ND
Acetone ug/L 49.140 123 70-130ND
Acrylonitrile ug/L 115100 115 70-130ND
Benzene ug/L 21.620 108 70-148ND
Bromochloromethane ug/L 22.820 114 70-130ND
Bromodichloromethane ug/L 22.220 111 70-130ND
Bromoform ug/L 18.420 92 70-130ND
Bromomethane ug/L 22.820 114 70-130ND
Carbon disulfide ug/L 23.620 118 70-130ND
Carbon tetrachloride ug/L 23.820 119 70-130ND
Chlorobenzene ug/L 20.620 103 70-146ND
Chloroethane ug/L 26.6 M120133 70-130ND
Chloroform ug/L 23.020 115 70-130ND
Chloromethane ug/L 21.520 108 70-130ND
cis-1,2-Dichloroethene ug/L 23.820 119 70-130ND
cis-1,3-Dichloropropene ug/L 19.120 96 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153772MATRIX SPIKE SAMPLE:
MSSpike
Result
92364018007
Dibromochloromethane ug/L 18.520 92 70-130ND
Dibromomethane ug/L 22.220 111 70-130ND
Dichlorodifluoromethane ug/L 30.2 M120151 70-130ND
Ethylbenzene ug/L 20.620 103 70-130ND
Iodomethane ug/L 40.440 101 70-130ND
m&p-Xylene ug/L 41.740 104 70-130ND
Methylene Chloride ug/L 21.720 109 70-130ND
o-Xylene ug/L 20.920 105 70-130ND
Styrene ug/L 20.720 103 70-130ND
Tetrachloroethene ug/L 21.420 107 70-130ND
Tetrahydrofuran ug/L 211200 106 70-130ND
Toluene ug/L 21.020 105 70-155ND
trans-1,2-Dichloroethene ug/L 23.520 117 70-130ND
trans-1,3-Dichloropropene ug/L 16.820 84 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.120 91 70-130ND
Trichloroethene ug/L 23.920 119 69-151ND
Trichlorofluoromethane ug/L 26.120 130 70-130ND
Vinyl acetate ug/L 36.240 90 70-130ND
Vinyl chloride ug/L 27.7 M120139 70-130ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92364018008
2153773SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92364018008
2153773SAMPLE DUPLICATE:
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L 0.22J0.32J
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%94 396
4-Bromofluorobenzene (S)%104 1103
Toluene-d8 (S)%106 0106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388080
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples: 92364018001, 92364018009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153200
Associated Lab Samples:92364018001, 92364018009
Matrix: Water
Analyzed
4,4'-DDD ug/L ND 0.050 11/29/17 19:03
4,4'-DDE ug/L ND 0.050 11/29/17 19:03
4,4'-DDT ug/L ND 0.050 11/29/17 19:03
Aldrin ug/L ND 0.050 11/29/17 19:03
alpha-BHC ug/L ND 0.050 11/29/17 19:03
beta-BHC ug/L ND 0.050 11/29/17 19:03
Chlordane (Technical)ug/L ND 0.20 11/29/17 19:03
delta-BHC ug/L ND 0.050 11/29/17 19:03
Dieldrin ug/L ND 0.050 11/29/17 19:03
Endosulfan I ug/L ND 0.050 11/29/17 19:03
Endosulfan II ug/L ND 0.050 11/29/17 19:03
Endosulfan sulfate ug/L ND 0.050 11/29/17 19:03
Endrin ug/L ND 0.050 11/29/17 19:03
Endrin aldehyde ug/L ND 0.050 11/29/17 19:03
Endrin ketone ug/L ND 0.050 11/29/17 19:03
gamma-BHC (Lindane)ug/L ND 0.050 11/29/17 19:03
Heptachlor ug/L ND 0.050 11/29/17 19:03
Heptachlor epoxide ug/L ND 0.050 11/29/17 19:03
Hexachlorobenzene ug/L ND 0.050 11/29/17 19:03
Methoxychlor ug/L ND 0.15 11/29/17 19:03
Mirex ug/L ND 0.15 11/29/17 19:03
Toxaphene ug/L ND 0.20 11/29/17 19:03
Decachlorobiphenyl (S)%75 20-130 11/29/17 19:03
Tetrachloro-m-xylene (S)%77 20-130 11/29/17 19:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153201LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.23.25 93 20-150
4,4'-DDE ug/L 0.21.25 86 20-150
4,4'-DDT ug/L 0.25.25 100 20-150
Aldrin ug/L 0.20.25 79 20-150
alpha-BHC ug/L 0.21.25 85 20-150
beta-BHC ug/L 0.18.25 73 20-150
delta-BHC ug/L 0.23.25 92 20-150
Dieldrin ug/L 0.21.25 87 20-150
Endosulfan I ug/L 0.22.25 88 20-150
Endosulfan II ug/L 0.23.25 93 20-150
Endosulfan sulfate ug/L 0.24.25 96 20-150
Endrin ug/L 0.24.25 96 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153201LABORATORY CONTROL SAMPLE:
LCSSpike
Endrin aldehyde ug/L 0.24.25 95 20-150
Endrin ketone ug/L 0.24.25 96 20-150
gamma-BHC (Lindane)ug/L 0.22.25 87 20-150
Heptachlor ug/L 0.21.25 84 20-150
Heptachlor epoxide ug/L 0.22.25 88 20-150
Hexachlorobenzene ug/L 0.18.25 72 20-150
Methoxychlor ug/L 0.79.74 107 20-150
Mirex ug/L 0.66.74 89 20-150
Decachlorobiphenyl (S)%81 20-130
Tetrachloro-m-xylene (S)%89 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153202MATRIX SPIKE SAMPLE:
MSSpike
Result
92364018001
4,4'-DDD ug/L 0.33.25 133 20-150ND
4,4'-DDE ug/L 0.28.25 112 20-150ND
4,4'-DDT ug/L 0.41 M1.25 167 20-150ND
Aldrin ug/L 0.19.25 78 20-150ND
alpha-BHC ug/L 0.21.25 85 20-150ND
beta-BHC ug/L 0.16.25 63 20-150ND
delta-BHC ug/L 0.23.25 91 20-150ND
Dieldrin ug/L 0.26.25 107 20-150ND
Endosulfan I ug/L 0.26.25 105 20-150ND
Endosulfan II ug/L 0.28.25 111 20-150ND
Endosulfan sulfate ug/L 0.31.25 127 20-150ND
Endrin ug/L 0.30.25 119 20-150ND
Endrin aldehyde ug/L 0.31.25 126 20-150ND
Endrin ketone ug/L 0.34.25 136 20-150ND
gamma-BHC (Lindane)ug/L 0.21.25 85 20-150ND
Heptachlor ug/L 0.24.25 95 20-150ND
Heptachlor epoxide ug/L 0.24.25 96 20-150ND
Hexachlorobenzene ug/L 0.16.25 66 20-150ND
Methoxychlor ug/L 1.4 M1.74 184 20-150ND
Mirex ug/L 0.82.74 110 20-150ND
Decachlorobiphenyl (S)%102 20-130
Tetrachloro-m-xylene (S)%72 20-130
Parameter Units
Dup
Result QualifiersRPDResult
92364340003
2153203SAMPLE DUPLICATE:
4,4'-DDD ug/L NDND
4,4'-DDE ug/L NDND
4,4'-DDT ug/L NDND
Aldrin ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92364340003
2153203SAMPLE DUPLICATE:
alpha-BHC ug/L NDND
beta-BHC ug/L NDND
Chlordane (Technical)ug/L NDND
delta-BHC ug/L NDND
Dieldrin ug/L NDND
Endosulfan I ug/L NDND
Endosulfan II ug/L NDND
Endosulfan sulfate ug/L NDND
Endrin ug/L NDND
Endrin aldehyde ug/L NDND
Endrin ketone ug/L NDND
gamma-BHC (Lindane)ug/L NDND
Heptachlor ug/L NDND
Heptachlor epoxide ug/L NDND
Hexachlorobenzene ug/L NDND
Methoxychlor ug/L NDND
Mirex ug/L NDND
Toxaphene ug/L NDND
Decachlorobiphenyl (S)%59 1367
Tetrachloro-m-xylene (S)%78 1590
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388331
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples: 92364018001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154375
Associated Lab Samples:92364018001
Matrix: Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 11/29/17 23:18
PCB-1221 (Aroclor 1221)ug/L ND 0.50 11/29/17 23:18
PCB-1232 (Aroclor 1232)ug/L ND 0.50 11/29/17 23:18
PCB-1242 (Aroclor 1242)ug/L ND 0.50 11/29/17 23:18
PCB-1248 (Aroclor 1248)ug/L ND 0.50 11/29/17 23:18
PCB-1254 (Aroclor 1254)ug/L ND 0.50 11/29/17 23:18
PCB-1260 (Aroclor 1260)ug/L ND 0.50 11/29/17 23:18
Decachlorobiphenyl (S)%70 10-132 11/29/17 23:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154376LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 3.45 67 50-150
PCB-1260 (Aroclor 1260)ug/L 4.55 90 50-150
Decachlorobiphenyl (S)%55 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2154377MATRIX SPIKE SAMPLE:
MSSpike
Result
92363879001
PCB-1016 (Aroclor 1016)ug/L 5.05 99 50-150ND
PCB-1260 (Aroclor 1260)ug/L 4.05 79 50-150ND
Decachlorobiphenyl (S)%25 10-132
Parameter Units
Dup
Result QualifiersRPDResult
92363879002
2154378SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L NDND
PCB-1221 (Aroclor 1221)ug/L NDND
PCB-1232 (Aroclor 1232)ug/L NDND
PCB-1242 (Aroclor 1242)ug/L NDND
PCB-1248 (Aroclor 1248)ug/L NDND
PCB-1254 (Aroclor 1254)ug/L NDND
PCB-1260 (Aroclor 1260)ug/L NDND
Decachlorobiphenyl (S)%60 865
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
406966
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples: 92364018001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2222026
Associated Lab Samples:92364018001
Matrix: Water
Analyzed
2,4,5-T ug/L ND 0.19 11/28/17 22:57
2,4,5-TP (Silvex)ug/L ND 0.19 11/28/17 22:57
2,4-D ug/L ND 0.94 11/28/17 22:57
Dinoseb ug/L ND 0.19 11/28/17 22:57
Pentachlorophenol ug/L ND 0.028 11/28/17 22:57
2,4-DCAA (S)%88 39-139 11/28/17 22:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2222027LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2224113
2,4,5-T ug/L 1.11.2 93 37-133911.1 2 40
2,4,5-TP (Silvex)ug/L 1.21.2 97 53-134951.1 2 40
2,4-D ug/L 5.76 96 35-124935.6 2 40
Dinoseb ug/L 0.631.2 52 13-116500.60 5 40
Pentachlorophenol ug/L 0.18.18 100 39-170970.17 3 40
2,4-DCAA (S)%94 39-13994 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388120
EPA 3510
EPA 8270
8270 Water MSSV RVE
Associated Lab Samples: 92364018001, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153602
Associated Lab Samples:92364018001, 92364018010
Matrix: Water
Analyzed
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 11/27/17 09:53
2,4,5-Trichlorophenol ug/L ND 10.0 11/27/17 09:53
2,4,6-Trichlorophenol ug/L ND 10.0 11/27/17 09:53
2,4-Dichlorophenol ug/L ND 10.0 11/27/17 09:53
2,4-Dimethylphenol ug/L ND 10.0 11/27/17 09:53
2,4-Dinitrophenol ug/L ND 50.0 11/27/17 09:53
2,4-Dinitrotoluene ug/L ND 10.0 11/27/17 09:53
2,6-Dinitrotoluene ug/L ND 10.0 11/27/17 09:53
2-Chloronaphthalene ug/L ND 10.0 11/27/17 09:53
2-Chlorophenol ug/L ND 10.0 11/27/17 09:53
2-Methylnaphthalene ug/L ND 10.0 11/27/17 09:53
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/27/17 09:53
2-Nitroaniline ug/L ND 50.0 11/27/17 09:53
2-Nitrophenol ug/L ND 10.0 11/27/17 09:53
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/27/17 09:53
3,3'-Dichlorobenzidine ug/L ND 20.0 11/27/17 09:53
3-Nitroaniline ug/L ND 50.0 11/27/17 09:53
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/27/17 09:53
4-Bromophenylphenyl ether ug/L ND 10.0 11/27/17 09:53
4-Chloro-3-methylphenol ug/L ND 20.0 11/27/17 09:53
4-Chloroaniline ug/L ND 20.0 11/27/17 09:53
4-Chlorophenylphenyl ether ug/L ND 10.0 11/27/17 09:53
4-Nitroaniline ug/L ND 20.0 11/27/17 09:53
4-Nitrophenol ug/L ND 50.0 11/27/17 09:53
Acenaphthene ug/L ND 10.0 11/27/17 09:53
Acenaphthylene ug/L ND 10.0 11/27/17 09:53
Acetophenone ug/L ND 10.0 11/27/17 09:53
Anthracene ug/L ND 10.0 11/27/17 09:53
Benzo(a)anthracene ug/L ND 10.0 11/27/17 09:53
Benzo(a)pyrene ug/L ND 10.0 11/27/17 09:53
Benzo(b)fluoranthene ug/L ND 10.0 11/27/17 09:53
Benzo(g,h,i)perylene ug/L ND 10.0 11/27/17 09:53
Benzo(k)fluoranthene ug/L ND 10.0 11/27/17 09:53
Benzyl alcohol ug/L ND 20.0 11/27/17 09:53
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/27/17 09:53
bis(2-Chloroethyl) ether ug/L ND 10.0 11/27/17 09:53
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/27/17 09:53
Butylbenzylphthalate ug/L ND 10.0 11/27/17 09:53
Chrysene ug/L ND 10.0 11/27/17 09:53
Di-n-butylphthalate ug/L ND 10.0 11/27/17 09:53
Di-n-octylphthalate ug/L ND 10.0 11/27/17 09:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153602
Associated Lab Samples:92364018001, 92364018010
Matrix: Water
Analyzed
Dibenz(a,h)anthracene ug/L ND 10.0 11/27/17 09:53
Dibenzofuran ug/L ND 10.0 11/27/17 09:53
Diethylphthalate ug/L ND 10.0 11/27/17 09:53
Dimethylphthalate ug/L ND 10.0 11/27/17 09:53
Diphenylamine ug/L ND 10.0 11/27/17 09:53
Fluoranthene ug/L ND 10.0 11/27/17 09:53
Fluorene ug/L ND 10.0 11/27/17 09:53
Hexachlorobenzene ug/L ND 10.0 11/27/17 09:53
Hexachlorocyclopentadiene ug/L ND 10.0 11/27/17 09:53
Hexachloroethane ug/L ND 10.0 11/27/17 09:53
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/27/17 09:53
Isophorone ug/L ND 10.0 11/27/17 09:53
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/27/17 09:53
N-Nitrosodimethylamine ug/L ND 10.0 11/27/17 09:53
N-Nitrosodiphenylamine ug/L ND 10.0 11/27/17 09:53
Nitrobenzene ug/L ND 10.0 11/27/17 09:53
Phenanthrene ug/L ND 10.0 11/27/17 09:53
Phenol ug/L ND 10.0 11/27/17 09:53
Pyrene ug/L ND 10.0 11/27/17 09:53
2,4,6-Tribromophenol (S)%49 31-170 11/27/17 09:53
2-Fluorobiphenyl (S)%52 45-139 11/27/17 09:53
2-Fluorophenol (S)%42 13-118 11/27/17 09:53
Nitrobenzene-d5 (S)%56 40-121 11/27/17 09:53
Phenol-d6 (S)%35 18-105 11/27/17 09:53
Terphenyl-d14 (S)%72 48-146 11/27/17 09:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153603LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/L 28.250 56 18-120
2,4,5-Trichlorophenol ug/L 17.0 L25034 43-113
2,4,6-Trichlorophenol ug/L 17.3 L25035 42-120
2,4-Dichlorophenol ug/L 18.550 37 30-120
2,4-Dimethylphenol ug/L 37.950 76 29-111
2,4-Dinitrophenol ug/L 19.8J L22508 19-132
2,4-Dinitrotoluene ug/L 37.850 76 58-128
2,6-Dinitrotoluene ug/L 38.750 77 54-129
2-Chloronaphthalene ug/L 32.450 65 43-117
2-Chlorophenol ug/L 18.950 38 37-120
2-Methylnaphthalene ug/L 30.450 61 33-120
2-Methylphenol(o-Cresol)ug/L 27.250 54 31-120
2-Nitroaniline ug/L 73.2100 73 48-121
2-Nitrophenol ug/L 16.950 34 25-116
3&4-Methylphenol(m&p Cresol)ug/L 24.950 50 23-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153603LABORATORY CONTROL SAMPLE:
LCSSpike
3,3'-Dichlorobenzidine ug/L 76.5100 77 10-154
3-Nitroaniline ug/L 72.0100 72 43-115
4,6-Dinitro-2-methylphenol ug/L 28.6 L210029 44-124
4-Bromophenylphenyl ether ug/L 34.450 69 34-113
4-Chloro-3-methylphenol ug/L 60.9100 61 31-110
4-Chloroaniline ug/L 69.2100 69 20-120
4-Chlorophenylphenyl ether ug/L 32.650 65 34-116
4-Nitroaniline ug/L 74.0100 74 46-128
4-Nitrophenol ug/L 42.5J250 17 11-120
Acenaphthene ug/L 32.350 65 48-114
Acenaphthylene ug/L 32.650 65 48-112
Acetophenone ug/L 32.4100 32 24-120
Anthracene ug/L 35.750 71 57-118
Benzo(a)anthracene ug/L 39.450 79 56-121
Benzo(a)pyrene ug/L 37.950 76 55-127
Benzo(b)fluoranthene ug/L 38.050 76 53-128
Benzo(g,h,i)perylene ug/L 38.850 78 54-125
Benzo(k)fluoranthene ug/L 37.350 75 51-123
Benzyl alcohol ug/L 63.3100 63 27-120
bis(2-Chloroethoxy)methane ug/L 35.650 71 32-120
bis(2-Chloroethyl) ether ug/L 33.650 67 33-111
bis(2-Ethylhexyl)phthalate ug/L 39.350 79 50-145
Butylbenzylphthalate ug/L 39.750 79 54-138
Chrysene ug/L 40.250 80 58-127
Di-n-butylphthalate ug/L 37.750 75 56-125
Di-n-octylphthalate ug/L 39.550 79 50-134
Dibenz(a,h)anthracene ug/L 38.550 77 53-129
Dibenzofuran ug/L 32.950 66 45-120
Diethylphthalate ug/L 34.850 70 53-120
Dimethylphthalate ug/L 34.550 69 55-116
Diphenylamine ug/L 38.150 76 42-120
Fluoranthene ug/L 36.850 74 57-125
Fluorene ug/L 33.950 68 53-118
Hexachlorobenzene ug/L 36.750 73 49-116
Hexachlorocyclopentadiene ug/L 33.850 68 26-158
Hexachloroethane ug/L 27.250 54 30-114
Indeno(1,2,3-cd)pyrene ug/L 39.550 79 55-128
Isophorone ug/L 35.650 71 31-118
N-Nitroso-di-n-propylamine ug/L 33.650 67 32-119
N-Nitrosodimethylamine ug/L 36.950 74 13-120
N-Nitrosodiphenylamine ug/L 38.150 76 43-120
Nitrobenzene ug/L 37.350 75 33-110
Phenanthrene ug/L 35.250 70 57-117
Phenol ug/L 17.250 34 10-120
Pyrene ug/L 38.450 77 55-122
2,4,6-Tribromophenol (S)%38 31-170
2-Fluorobiphenyl (S)%70 45-139
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153603LABORATORY CONTROL SAMPLE:
LCSSpike
2-Fluorophenol (S)%24 13-118
Nitrobenzene-d5 (S)%67 40-121
Phenol-d6 (S)%29 18-105
Terphenyl-d14 (S)%74 48-146
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153604MATRIX SPIKE SAMPLE:
MSSpike
Result
92364222001
2,2'-Oxybis(1-chloropropane)ug/L 19.7 M15039 50-150ND
2,4,5-Trichlorophenol ug/L 9.2J M05018 19-105ND
2,4,6-Trichlorophenol ug/L 9.6J50 19 13-108ND
2,4-Dichlorophenol ug/L 33.950 68 19-111ND
2,4-Dimethylphenol ug/L 29.450 59 21-103ND
2,4-Dinitrophenol ug/L 61.9250 25 10-109ND
2,4-Dinitrotoluene ug/L 9.4J M15019 27-104ND
2,6-Dinitrotoluene ug/L 8.8J M15018 28-101ND
2-Chloronaphthalene ug/L 7.5J50 15 14-102ND
2-Chlorophenol ug/L 23.050 46 16-110ND
2-Methylnaphthalene ug/L 23.250 46 13-110ND
2-Methylphenol(o-Cresol)ug/L 22.650 45 19-110ND
2-Nitroaniline ug/L 21.5J M110021 26-103ND
2-Nitrophenol ug/L 23.550 47 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 24.250 41 20-1103.47J
3,3'-Dichlorobenzidine ug/L ND M11000 25-112ND
3-Nitroaniline ug/L 6.5J M11007 29-110ND
4,6-Dinitro-2-methylphenol ug/L 56.0100 56 10-117ND
4-Bromophenylphenyl ether ug/L 22.750 45 20-105ND
4-Chloro-3-methylphenol ug/L 32.0100 32 22-110ND
4-Chloroaniline ug/L ND M11006 20-100ND
4-Chlorophenylphenyl ether ug/L 7.3J M15015 19-102ND
4-Nitroaniline ug/L 6.7J M11007 29-110ND
4-Nitrophenol ug/L 33.8J250 14 10-110ND
Acenaphthene ug/L 7.4J M15015 17-100ND
Acenaphthylene ug/L 7.4J M15015 21-100ND
Anthracene ug/L 23.950 48 24-109ND
Benzo(a)anthracene ug/L 22.050 44 22-117ND
Benzo(a)pyrene ug/L 23.650 47 23-104ND
Benzo(b)fluoranthene ug/L 23.750 47 23-103ND
Benzo(g,h,i)perylene ug/L 22.350 45 18-111ND
Benzo(k)fluoranthene ug/L 24.350 49 22-113ND
Benzyl alcohol ug/L 33.2100 33 19-101ND
bis(2-Chloroethoxy)methane ug/L 21.250 42 22-110ND
bis(2-Chloroethyl) ether ug/L 21.850 44 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 27750 75 23-102240
Butylbenzylphthalate ug/L 23.650 47 25-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2153604MATRIX SPIKE SAMPLE:
MSSpike
Result
92364222001
Chrysene ug/L 23.650 47 23-115ND
Di-n-butylphthalate ug/L 26.150 49 26-1101.42J
Di-n-octylphthalate ug/L 22.350 45 23-110ND
Dibenz(a,h)anthracene ug/L 22.650 45 21-112ND
Dibenzofuran ug/L 7.6J M15015 19-102ND
Diethylphthalate ug/L 10.7 M15018 29-110ND
Dimethylphthalate ug/L 7.9J M15016 27-110ND
Fluoranthene ug/L 24.450 49 23-112ND
Fluorene ug/L 7.7J M15015 22-104ND
Hexachlorobenzene ug/L 21.950 44 21-116ND
Hexachlorocyclopentadiene ug/L 7.8J50 16 10-110ND
Hexachloroethane ug/L 18.950 38 10-110ND
Indeno(1,2,3-cd)pyrene ug/L 23.250 46 20-113ND
Isophorone ug/L 27.950 56 50-150ND
N-Nitroso-di-n-propylamine ug/L 25.850 52 21-105ND
N-Nitrosodimethylamine ug/L 20.650 41 10-110ND
N-Nitrosodiphenylamine ug/L 25.350 51 23-107ND
Nitrobenzene ug/L 30.150 60 20-110ND
Phenanthrene ug/L 23.750 47 24-106ND
Phenol ug/L 31.250 30 12-11016.0
Pyrene ug/L 22.450 45 24-114ND
2,4,6-Tribromophenol (S)%52 31-170
2-Fluorobiphenyl (S)%S014 45-139
2-Fluorophenol (S)%37 13-118
Nitrobenzene-d5 (S)%53 40-121
Phenol-d6 (S)%33 18-105
Terphenyl-d14 (S)%S037 48-146
Parameter Units
Dup
Result QualifiersRPDResult
92363879001
2153605SAMPLE DUPLICATE:
2,2'-Oxybis(1-chloropropane)ug/L NDND
2,4,5-Trichlorophenol ug/L NDND
2,4,6-Trichlorophenol ug/L NDND
2,4-Dichlorophenol ug/L NDND
2,4-Dimethylphenol ug/L NDND
2,4-Dinitrophenol ug/L NDND
2,4-Dinitrotoluene ug/L NDND
2,6-Dinitrotoluene ug/L NDND
2-Chloronaphthalene ug/L NDND
2-Chlorophenol ug/L NDND
2-Methylnaphthalene ug/L NDND
2-Methylphenol(o-Cresol)ug/L NDND
2-Nitroaniline ug/L NDND
2-Nitrophenol ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363879001
2153605SAMPLE DUPLICATE:
3&4-Methylphenol(m&p Cresol)ug/L NDND
3,3'-Dichlorobenzidine ug/L NDND
3-Nitroaniline ug/L NDND
4,6-Dinitro-2-methylphenol ug/L NDND
4-Bromophenylphenyl ether ug/L NDND
4-Chloro-3-methylphenol ug/L NDND
4-Chloroaniline ug/L NDND
4-Chlorophenylphenyl ether ug/L NDND
4-Nitroaniline ug/L NDND
4-Nitrophenol ug/L NDND
Acenaphthene ug/L NDND
Acenaphthylene ug/L NDND
Acetophenone ug/L NDND
Anthracene ug/L NDND
Benzo(a)anthracene ug/L NDND
Benzo(a)pyrene ug/L NDND
Benzo(b)fluoranthene ug/L NDND
Benzo(g,h,i)perylene ug/L NDND
Benzo(k)fluoranthene ug/L NDND
Benzyl alcohol ug/L NDND
bis(2-Chloroethoxy)methane ug/L NDND
bis(2-Chloroethyl) ether ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Butylbenzylphthalate ug/L NDND
Chrysene ug/L NDND
Di-n-butylphthalate ug/L NDND
Di-n-octylphthalate ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Dibenzofuran ug/L NDND
Diethylphthalate ug/L NDND
Dimethylphthalate ug/L NDND
Diphenylamine ug/L NDND
Fluoranthene ug/L NDND
Fluorene ug/L NDND
Hexachlorobenzene ug/L NDND
Hexachlorocyclopentadiene ug/L NDND
Hexachloroethane ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
Isophorone ug/L NDND
N-Nitroso-di-n-propylamine ug/L NDND
N-Nitrosodimethylamine ug/L NDND
N-Nitrosodiphenylamine ug/L NDND
Nitrobenzene ug/L NDND
Phenanthrene ug/L NDND
Phenol ug/L NDND
Pyrene ug/L NDND
2,4,6-Tribromophenol (S)%64 266
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92363879001
2153605SAMPLE DUPLICATE:
2-Fluorobiphenyl (S)%73 3054
2-Fluorophenol (S)%51 250
Nitrobenzene-d5 (S)%78 2560
Phenol-d6 (S)%52 1744
Terphenyl-d14 (S)%76 473
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388426
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154775
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 11/28/17 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154776LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4910050000 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154777MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364134011
2154778
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500006280-12073 250000203mg/L 234000 240000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154779MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018001
2154780
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M15000010680-12069 350000670000723000 704000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387719
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151058
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Total Dissolved Solids ug/L ND 25000 11/21/17 01:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151059LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 250000250000 100 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92363887002
2151060SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 210000 2215 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92364018008
2151061SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 321000 1317000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387927
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2152239
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Sulfide ug/L ND 100 11/24/17 20:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2152240LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 457500 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2152241MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018001
2152242
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L M1,R15006880-12078 13500ND360 410
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2152243MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364032001
2152244
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 95 80-12098 3500ND476 489
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388266
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2154090
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005, 92364018006, 92364018007,92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Sulfate ug/L ND 1000 11/27/17 20:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2154091LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5050050000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154092MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879006
2154093
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 102 90-110103 150000783058900 59500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2154094MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018003
2154095
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 103 90-110106 350000ND51600 53000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388094
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004, 92364018005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153405
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004, 92364018005
Matrix: Water
Analyzed
Chloride ug/L ND 1000 11/22/17 23:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153406LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2100020000 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2153407MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364320001
2153408
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 102 90-110102 0100002.3mg/L 12500 12500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2153409MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879006
2153410
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 102 90-110101 0100001620026500 26400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
388095
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples: 92364018006, 92364018007, 92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2153412
Associated Lab Samples:92364018006, 92364018007, 92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Chloride ug/L ND 1000 11/23/17 00:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2153413LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2150020000 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2153414MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364018006
2153415
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L M11000010790-110129 5100003570046400 48600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2153416MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92364159003
2153417
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L M11000015790-110124 61000039.7mg/L 55300 52100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387704
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples: 92364018005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151022
Associated Lab Samples:92364018005
Matrix: Water
Analyzed
Cyanide ug/L ND 8.0 11/21/17 12:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151023LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 107100 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151024MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363874001
2151025
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 106 80-12099 7100ND107 99.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151026MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363874006
2151027
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 88 80-12094 6100ND90.6 96.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387705
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples: 92364018001, 92364018002, 92364018003, 92364018004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151028
Associated Lab Samples:92364018001, 92364018002, 92364018003, 92364018004
Matrix: Water
Analyzed
Cyanide ug/L ND 8.0 11/21/17 12:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151029LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 105100 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151030MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363835001
2151031
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11008780-12078 11100ND88.0 79.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151032MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363879005
2151033
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 105 80-12098 7100ND107 99.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 90
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92364018
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
387749
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples: 92364018006, 92364018007, 92364018008, 92364018009, 92364018010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2151163
Associated Lab Samples:92364018006, 92364018007, 92364018008, 92364018009, 92364018010
Matrix: Water
Analyzed
Cyanide ug/L ND 8.0 11/21/17 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2151164LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 98.2100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2151165MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363417001
2151166
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 101 80-120104 31000.0084mg/L 110 113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 90
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92364018
OSR
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
BATCH QUALIFIERS
Batch: 408387
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[M5]
ANALYTE QUALIFIERS
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.1g
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 90
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92364018
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92364018001 3412-MW2R
92364018002 3412-MW8
92364018003 3412-MW9
92364018004 3412-MW11
92364018005 3412-MW12
92364018006 3412-SW1
92364018007 3412-SW3
92364018008 3412-SW4
92364018009 3412-MW10
92364018010 3412-SW2
92364018001 388080 3886433412-MW2R EPA 3510 EPA 8081
92364018009 388080 3886433412-MW10 EPA 3510 EPA 8081
92364018001 388331 3884663412-MW2R EPA 3510 EPA 8082
92364018001 406966 4083873412-MW2R EPA 8151 EPA 8151
92364018001 387775 3879213412-MW2R EPA 3010A EPA 6010
92364018002 387775 3879213412-MW8 EPA 3010A EPA 6010
92364018003 387775 3879213412-MW9 EPA 3010A EPA 6010
92364018004 387775 3879213412-MW11 EPA 3010A EPA 6010
92364018005 387775 3879213412-MW12 EPA 3010A EPA 6010
92364018006 387775 3879213412-SW1 EPA 3010A EPA 6010
92364018007 387775 3879213412-SW3 EPA 3010A EPA 6010
92364018008 387775 3879213412-SW4 EPA 3010A EPA 6010
92364018009 387775 3879213412-MW10 EPA 3010A EPA 6010
92364018010 387775 3879213412-SW2 EPA 3010A EPA 6010
92364018001 387486 3875503412-MW2R EPA 3010A EPA 6020B
92364018002 387486 3875503412-MW8 EPA 3010A EPA 6020B
92364018003 387486 3875503412-MW9 EPA 3010A EPA 6020B
92364018004 387486 3875503412-MW11 EPA 3010A EPA 6020B
92364018005 387486 3875503412-MW12 EPA 3010A EPA 6020B
92364018006 387486 3875503412-SW1 EPA 3010A EPA 6020B
92364018007 387486 3875503412-SW3 EPA 3010A EPA 6020B
92364018008 387486 3875503412-SW4 EPA 3010A EPA 6020B
92364018009 387486 3875503412-MW10 EPA 3010A EPA 6020B
92364018010 387486 3875503412-SW2 EPA 3010A EPA 6020B
92364018001 388398 3884203412-MW2R EPA 7470 EPA 7470
92364018002 388398 3884203412-MW8 EPA 7470 EPA 7470
92364018003 388398 3884203412-MW9 EPA 7470 EPA 7470
92364018004 388398 3884203412-MW11 EPA 7470 EPA 7470
92364018005 388398 3884203412-MW12 EPA 7470 EPA 7470
92364018006 388398 3884203412-SW1 EPA 7470 EPA 7470
92364018007 388398 3884203412-SW3 EPA 7470 EPA 7470
92364018008 388398 3884203412-SW4 EPA 7470 EPA 7470
92364018009 388398 3884203412-MW10 EPA 7470 EPA 7470
92364018010 388398 3884203412-SW2 EPA 7470 EPA 7470
92364018001 388120 3882953412-MW2R EPA 3510 EPA 8270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 90
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92364018
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92364018010 388120 3882953412-SW2 EPA 3510 EPA 8270
92364018001 3881683412-MW2R EPA 8260
92364018002 3881683412-MW8 EPA 8260
92364018003 3881683412-MW9 EPA 8260
92364018004 3881683412-MW11 EPA 8260
92364018005 3881683412-MW12 EPA 8260
92364018006 3881683412-SW1 EPA 8260
92364018007 3881693412-SW3 EPA 8260
92364018008 3881693412-SW4 EPA 8260
92364018009 3881693412-MW10 EPA 8260
92364018010 3881693412-SW2 EPA 8260
92364018011 3881693412-TRIP BLANK EPA 8260
92364018001 3884263412-MW2R SM 2320B
92364018002 3884263412-MW8 SM 2320B
92364018003 3884263412-MW9 SM 2320B
92364018004 3884263412-MW11 SM 2320B
92364018005 3884263412-MW12 SM 2320B
92364018006 3884263412-SW1 SM 2320B
92364018007 3884263412-SW3 SM 2320B
92364018008 3884263412-SW4 SM 2320B
92364018009 3884263412-MW10 SM 2320B
92364018010 3884263412-SW2 SM 2320B
92364018001 3877193412-MW2R SM 2540C
92364018002 3877193412-MW8 SM 2540C
92364018003 3877193412-MW9 SM 2540C
92364018004 3877193412-MW11 SM 2540C
92364018005 3877193412-MW12 SM 2540C
92364018006 3877193412-SW1 SM 2540C
92364018007 3877193412-SW3 SM 2540C
92364018008 3877193412-SW4 SM 2540C
92364018009 3877193412-MW10 SM 2540C
92364018010 3877193412-SW2 SM 2540C
92364018001 3879273412-MW2R SM 4500-S2D
92364018002 3879273412-MW8 SM 4500-S2D
92364018003 3879273412-MW9 SM 4500-S2D
92364018004 3879273412-MW11 SM 4500-S2D
92364018005 3879273412-MW12 SM 4500-S2D
92364018006 3879273412-SW1 SM 4500-S2D
92364018007 3879273412-SW3 SM 4500-S2D
92364018008 3879273412-SW4 SM 4500-S2D
92364018009 3879273412-MW10 SM 4500-S2D
92364018010 3879273412-SW2 SM 4500-S2D
92364018001 3882663412-MW2R EPA 300.0
92364018002 3882663412-MW8 EPA 300.0
92364018003 3882663412-MW9 EPA 300.0
92364018004 3882663412-MW11 EPA 300.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 90
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92364018
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92364018005 3882663412-MW12 EPA 300.0
92364018006 3882663412-SW1 EPA 300.0
92364018007 3882663412-SW3 EPA 300.0
92364018008 3882663412-SW4 EPA 300.0
92364018009 3882663412-MW10 EPA 300.0
92364018010 3882663412-SW2 EPA 300.0
92364018001 3880943412-MW2R SM 4500-Cl-E
92364018002 3880943412-MW8 SM 4500-Cl-E
92364018003 3880943412-MW9 SM 4500-Cl-E
92364018004 3880943412-MW11 SM 4500-Cl-E
92364018005 3880943412-MW12 SM 4500-Cl-E
92364018006 3880953412-SW1 SM 4500-Cl-E
92364018007 3880953412-SW3 SM 4500-Cl-E
92364018008 3880953412-SW4 SM 4500-Cl-E
92364018009 3880953412-MW10 SM 4500-Cl-E
92364018010 3880953412-SW2 SM 4500-Cl-E
92364018001 3877053412-MW2R SM 4500-CN-E
92364018002 3877053412-MW8 SM 4500-CN-E
92364018003 3877053412-MW9 SM 4500-CN-E
92364018004 3877053412-MW11 SM 4500-CN-E
92364018005 3877043412-MW12 SM 4500-CN-E
92364018006 3877493412-SW1 SM 4500-CN-E
92364018007 3877493412-SW3 SM 4500-CN-E
92364018008 3877493412-SW4 SM 4500-CN-E
92364018009 3877493412-MW10 SM 4500-CN-E
92364018010 3877493412-SW2 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2017 02:04 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 90
Page 86 of 90
Page 87 of 90
Page 88 of 90
Page 89 of 90
Page 90 of 90
This page intentionally left blank.
Winston-Salem City/County Utilities | Assessment Monitoring Report Appendix C – Field Data

C
Appendix C – Field Data

This page intentionally left blank.

This page intentionally left blank.
Winston-Salem City/County Utilities | Assessment Monitoring Report Appendix D – Electronic Files

D
Appendix D – Electronic Files
Portable Document Format (PDF) of this Report
Electronic Data Deliverable (EDD) of Groundwater
Results

This page intentionally left blank.

HDR Engineering, Inc. of the Carolinas
440 S Church Street, Suite 1000
Charlotte, NC 28202-2075
704.338.6700
NC License F0116
hdrinc.com
© 2018 HDR, Inc., all rights reserved