4502_HendersonCountyMSWLF_SampleResults_20171002

#=CL#
October 02, 2017
LIMS USE: FR - MICHAEL BALDWIN
LIMS OBJECT ID: 92356385
92356385
Project:
Pace Project No.:
RE:
Mr. Michael Baldwin
Kimberly Clark
32 Smyth Avenue
Hendersonville, NC 28793
South LF MW 9/21
Dear Mr. Baldwin:
Enclosed are the analytical results for sample(s) received by the laboratory on September 21, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92356385
South LF MW 9/21
Lab ID Sample ID Matrix Date Collected Date Received
92356385001 MW-1S Water 09/21/17 10:15 09/21/17 14:30
92356385002 MW-2S Water 09/21/17 11:35 09/21/17 14:30
92356385003 MW-3S Water 09/21/17 11:40 09/21/17 14:30
92356385004 MW-4S Water 09/21/17 11:00 09/21/17 14:30
92356385005 MW-5S Water 09/21/17 11:15 09/21/17 14:30
92356385006 MW-6S Water 09/21/17 10:45 09/21/17 14:30
92356385007 MW-7S Water 09/21/17 10:30 09/21/17 14:30
92356385008 EQUIP BLK Water 09/21/17 09:55 09/21/17 14:30
92356385009 TVL BLK Water 09/21/17 09:00 09/21/17 14:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92356385
South LF MW 9/21
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92356385001 MW-1S EPA 8260 63 PASI-CZDO
92356385004 MW-4S EPA 8260 63 PASI-CZDO
92356385005 MW-5S EPA 8260 63 PASI-CZDO
92356385006 MW-6S EPA 8260 63 PASI-CZDO
92356385007 MW-7S EPA 8260 63 PASI-CZDO
92356385008 EQUIP BLK EPA 8260 63 PASI-CZDO
92356385009 TVL BLK EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-1S Lab ID:92356385001 Collected:09/21/17 10:15 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 10:151
Collected Date 9/21/17 09/21/17 10:151
Collected Time 10:15 09/21/17 10:151
Field pH 5.6 Std. Units 09/21/17 10:150.10 0.10 1
Field Temperature 14.8 deg C 09/21/17 10:150.50 0.50 1
Static Water Level 15.91 feet 09/21/17 10:151
Field Specific Conductance 218 umhos/cm 09/21/17 10:151.0 1.0 1
Turbidity 5.39 NTU 09/21/17 10:151.0 1.0 1
Odor No Odor 09/21/17 10:151
Appearance Clear 09/21/17 10:151
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 07:06 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 07:06 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 07:06 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 07:06 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 07:06 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 07:06 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 07:06 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 07:06 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 07:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 07:06 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 07:06 75-00-31.0 0.54 1
Chloroform ND ug/L 09/29/17 07:06 67-66-31.0 0.14 1
Chloromethane 0.14J ug/L 09/29/17 07:06 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 07:06 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 07:06 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 07:06 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 07:06 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 07:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 07:06 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 07:06 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 07:06 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 07:06 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 07:06 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 07:06 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 07:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 07:06 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/29/17 07:06 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 07:06 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 07:06 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 07:06 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 07:06 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 07:06 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/29/17 07:06 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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2225 Riverside Dr.
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Page 5 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-1S Lab ID:92356385001 Collected:09/21/17 10:15 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 09/29/17 07:06 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 07:06 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 07:06 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 07:06 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 07:06 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 07:06 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 07:06 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 07:06 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 07:06 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 07:06 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 07:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 07:06 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 07:06 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/29/17 07:06 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 07:06 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 07:06 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 07:06 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 07:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 07:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 07:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 07:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 07:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 07:06 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 07:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 07:06 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 07:06 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 07:06 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)103 %09/29/17 07:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/29/17 07:06 17060-07-070-130 1
Toluene-d8 (S)107 %09/29/17 07:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-2S Lab ID:92356385002 Collected:09/21/17 11:35 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 11:351
Collected Date 9/21/17 09/21/17 11:351
Collected Time 11:35 09/21/17 11:351
Field pH 5.9 Std. Units 09/21/17 11:350.10 0.10 1
Field Temperature 20.5 deg C 09/21/17 11:350.50 0.50 1
Static Water Level 5.12 feet 09/21/17 11:351
Field Specific Conductance 90 umhos/cm 09/21/17 11:351.0 1.0 1
Turbidity 28.28 NTU 09/21/17 11:351.0 1.0 1
Odor No Odor 09/21/17 11:351
Appearance Clear to
Cloudy 09/21/17 11:351
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-3S Lab ID:92356385003 Collected:09/21/17 11:40 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 11:401
Collected Date 9/21/17 09/21/17 11:401
Collected Time 11:40 09/21/17 11:401
Field pH 5.2 Std. Units 09/21/17 11:400.10 0.10 1
Field Temperature 19.5 deg C 09/21/17 11:400.50 0.50 1
Static Water Level 6.58 feet 09/21/17 11:401
Field Specific Conductance 166 umhos/cm 09/21/17 11:401.0 1.0 1
Turbidity 6.37 NTU 09/21/17 11:401.0 1.0 1
Odor No Odor 09/21/17 11:401
Appearance Clear 09/21/17 11:401
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-4S Lab ID:92356385004 Collected:09/21/17 11:00 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 11:001
Collected Date 9/21/17 09/21/17 11:001
Collected Time 11:00 09/21/17 11:001
Field pH 5.8 Std. Units 09/21/17 11:000.10 0.10 1
Field Temperature 17.9 deg C 09/21/17 11:000.50 0.50 1
Static Water Level 5.59 feet 09/21/17 11:001
Field Specific Conductance 395 umhos/cm 09/21/17 11:001.0 1.0 1
Turbidity 13.28 NTU 09/21/17 11:001.0 1.0 1
Odor Organic
Odor 09/21/17 11:001
Appearance Clear 09/21/17 11:001
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 07:23 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 07:23 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 07:23 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 07:23 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 07:23 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 07:23 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 07:23 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 07:23 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 07:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 07:23 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 07:23 75-00-31.0 0.54 1
Chloroform ND ug/L 09/29/17 07:23 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/29/17 07:23 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 07:23 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 07:23 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 07:23 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 07:23 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 07:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 07:23 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 07:23 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 07:23 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 07:23 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 07:23 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 07:23 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 07:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 07:23 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/29/17 07:23 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 07:23 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 07:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 07:23 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 07:23 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 07:23 563-58-61.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-4S Lab ID:92356385004 Collected:09/21/17 11:00 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
cis-1,3-Dichloropropene ND ug/L 09/29/17 07:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/29/17 07:23 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 07:23 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 07:23 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 07:23 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 07:23 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 07:23 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 07:23 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 07:23 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 07:23 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 07:23 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 07:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 07:23 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 07:23 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/29/17 07:23 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 07:23 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 07:23 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 07:23 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 07:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 07:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 07:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 07:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 07:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 07:23 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 07:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 07:23 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 07:23 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 07:23 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %09/29/17 07:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %09/29/17 07:23 17060-07-070-130 1
Toluene-d8 (S)107 %09/29/17 07:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-5S Lab ID:92356385005 Collected:09/21/17 11:15 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 11:151
Collected Date 9/21/17 09/21/17 11:151
Collected Time 11:15 09/21/17 11:151
Field pH 5.6 Std. Units 09/21/17 11:150.10 0.10 1
Field Temperature 17.3 deg C 09/21/17 11:150.50 0.50 1
Static Water Level 5.25 feet 09/21/17 11:151
Field Specific Conductance 121 umhos/cm 09/21/17 11:151.0 1.0 1
Turbidity 1.72 NTU 09/21/17 11:151.0 1.0 1
Odor Organic
Odor 09/21/17 11:151
Appearance Clear 09/21/17 11:151
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 07:40 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 07:40 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 07:40 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 07:40 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 07:40 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 07:40 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 07:40 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 07:40 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 07:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 07:40 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 07:40 75-00-31.0 0.54 1
Chloroform ND ug/L 09/29/17 07:40 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/29/17 07:40 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 07:40 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 07:40 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 07:40 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 07:40 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 07:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 07:40 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 07:40 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 07:40 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 07:40 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 07:40 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 07:40 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 07:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 07:40 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/29/17 07:40 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 07:40 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 07:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 07:40 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 07:40 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 07:40 563-58-61.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-5S Lab ID:92356385005 Collected:09/21/17 11:15 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
cis-1,3-Dichloropropene ND ug/L 09/29/17 07:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/29/17 07:40 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 07:40 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 07:40 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 07:40 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 07:40 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 07:40 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 07:40 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 07:40 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 07:40 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 07:40 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 07:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 07:40 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 07:40 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/29/17 07:40 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 07:40 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 07:40 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 07:40 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 07:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 07:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 07:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 07:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 07:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 07:40 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 07:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 07:40 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 07:40 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 07:40 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)101 %09/29/17 07:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %09/29/17 07:40 17060-07-070-130 1
Toluene-d8 (S)106 %09/29/17 07:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-6S Lab ID:92356385006 Collected:09/21/17 10:45 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 10:451
Collected Date 9/21/17 09/21/17 10:451
Collected Time 10:45 09/21/17 10:451
Field pH 6.7 Std. Units 09/21/17 10:450.10 0.10 1
Field Temperature 17.6 deg C 09/21/17 10:450.50 0.50 1
Static Water Level 8.54 feet 09/21/17 10:451
Field Specific Conductance 69 umhos/cm 09/21/17 10:451.0 1.0 1
Turbidity 12.89 NTU 09/21/17 10:451.0 1.0 1
Odor No Odor 09/21/17 10:451
Appearance Clear 09/21/17 10:451
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 07:58 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 07:58 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 07:58 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 07:58 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 07:58 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 07:58 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 07:58 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 07:58 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 07:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 07:58 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 07:58 75-00-31.0 0.54 1
Chloroform ND ug/L 09/29/17 07:58 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/29/17 07:58 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 07:58 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 07:58 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 07:58 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 07:58 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 07:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 07:58 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 07:58 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 07:58 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 07:58 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 07:58 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 07:58 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 07:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 07:58 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/29/17 07:58 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 07:58 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 07:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 07:58 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 07:58 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 07:58 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/29/17 07:58 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-6S Lab ID:92356385006 Collected:09/21/17 10:45 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 09/29/17 07:58 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 07:58 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 07:58 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 07:58 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 07:58 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 07:58 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 07:58 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 07:58 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 07:58 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 07:58 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 07:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 07:58 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 07:58 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/29/17 07:58 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 07:58 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 07:58 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 07:58 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 07:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 07:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 07:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 07:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 07:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 07:58 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 07:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 07:58 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 07:58 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 07:58 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)103 %09/29/17 07:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %09/29/17 07:58 17060-07-070-130 1
Toluene-d8 (S)108 %09/29/17 07:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-7S Lab ID:92356385007 Collected:09/21/17 10:30 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 09/21/17 10:301
Collected Date 9/21/17 09/21/17 10:301
Collected Time 10:30 09/21/17 10:301
Field pH 6.1 Std. Units 09/21/17 10:300.10 0.10 1
Field Temperature 17.5 deg C 09/21/17 10:300.50 0.50 1
Static Water Level 5.95 feet 09/21/17 10:301
Field Oxidation Potential 129 mV 09/21/17 10:301
Turbidity 4.44 NTU 09/21/17 10:301.0 1.0 1
Odor No Odor 09/21/17 10:301
Appearance Clear 09/21/17 10:301
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 08:15 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 08:15 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 08:15 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 08:15 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 08:15 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 08:15 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 08:15 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 08:15 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 08:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 08:15 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 08:15 75-00-31.0 0.54 1
Chloroform ND ug/L 09/29/17 08:15 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/29/17 08:15 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 08:15 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 08:15 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 08:15 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 08:15 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 08:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 08:15 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 08:15 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 08:15 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 08:15 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 08:15 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 08:15 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 08:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 08:15 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.20J ug/L 09/29/17 08:15 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 08:15 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 08:15 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 08:15 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 08:15 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 08:15 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/29/17 08:15 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:MW-7S Lab ID:92356385007 Collected:09/21/17 10:30 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 09/29/17 08:15 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 08:15 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 08:15 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 08:15 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 08:15 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 08:15 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 08:15 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 08:15 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 08:15 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 08:15 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 08:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 08:15 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 08:15 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 09/29/17 08:15 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 08:15 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 08:15 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 08:15 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 08:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 08:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 08:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 08:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 08:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 08:15 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 08:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 08:15 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 08:15 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 08:15 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %09/29/17 08:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/29/17 08:15 17060-07-070-130 1
Toluene-d8 (S)107 %09/29/17 08:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:EQUIP BLK Lab ID:92356385008 Collected:09/21/17 09:55 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 01:36 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 01:36 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 01:36 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 01:36 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 01:36 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 01:36 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 01:36 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 01:36 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 01:36 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 01:36 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 01:36 75-00-31.0 0.54 1
Chloroform 0.14J ug/L 09/29/17 01:36 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/29/17 01:36 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 01:36 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 01:36 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 01:36 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 01:36 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 01:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 01:36 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 01:36 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 01:36 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 01:36 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 01:36 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 01:36 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 01:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 01:36 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/29/17 01:36 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 01:36 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 01:36 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 01:36 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 01:36 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 01:36 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/29/17 01:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/29/17 01:36 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 01:36 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 01:36 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 01:36 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 01:36 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 01:36 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 01:36 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 01:36 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 01:36 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 01:36 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 01:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 01:36 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 01:36 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:EQUIP BLK Lab ID:92356385008 Collected:09/21/17 09:55 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 09/29/17 01:36 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 01:36 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 01:36 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 01:36 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 01:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 01:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 01:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 01:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 01:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 01:36 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 01:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 01:36 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 01:36 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 01:36 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %09/29/17 01:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/29/17 01:36 17060-07-070-130 1
Toluene-d8 (S)107 %09/29/17 01:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:TVL BLK Lab ID:92356385009 Collected:09/21/17 09:00 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 09/29/17 01:54 67-64-125.0 10.0 1
Benzene ND ug/L 09/29/17 01:54 71-43-21.0 0.25 1
Bromobenzene ND ug/L 09/29/17 01:54 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 09/29/17 01:54 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 09/29/17 01:54 75-27-41.0 0.18 1
Bromoform ND ug/L 09/29/17 01:54 75-25-21.0 0.26 1
Bromomethane ND ug/L 09/29/17 01:54 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 09/29/17 01:54 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 09/29/17 01:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/29/17 01:54 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/29/17 01:54 75-00-31.0 0.54 1
Chloroform ND ug/L 09/29/17 01:54 67-66-31.0 0.14 1
Chloromethane ND ug/L 09/29/17 01:54 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 09/29/17 01:54 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 09/29/17 01:54 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/17 01:54 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 09/29/17 01:54 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/17 01:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/29/17 01:54 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/29/17 01:54 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/29/17 01:54 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/29/17 01:54 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 09/29/17 01:54 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 09/29/17 01:54 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 09/29/17 01:54 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/29/17 01:54 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/29/17 01:54 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/29/17 01:54 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 09/29/17 01:54 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/29/17 01:54 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/29/17 01:54 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 09/29/17 01:54 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/29/17 01:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/29/17 01:54 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 09/29/17 01:54 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 09/29/17 01:54 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 09/29/17 01:54 87-68-31.0 0.71 1
2-Hexanone ND ug/L 09/29/17 01:54 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 09/29/17 01:54 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 09/29/17 01:54 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/29/17 01:54 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 09/29/17 01:54 1634-04-41.0 0.21 1
Naphthalene ND ug/L 09/29/17 01:54 91-20-31.0 0.24 1
Styrene ND ug/L 09/29/17 01:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/17 01:54 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/17 01:54 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356385
South LF MW 9/21
Sample:TVL BLK Lab ID:92356385009 Collected:09/21/17 09:00 Received:09/21/17 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 09/29/17 01:54 127-18-41.0 0.46 1
Toluene ND ug/L 09/29/17 01:54 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 09/29/17 01:54 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 09/29/17 01:54 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/29/17 01:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/29/17 01:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/29/17 01:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/29/17 01:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/29/17 01:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/29/17 01:54 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 09/29/17 01:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/29/17 01:54 1330-20-71.0 1.0 1
m&p-Xylene ND ug/L 09/29/17 01:54 179601-23-12.0 0.66 1
o-Xylene ND ug/L 09/29/17 01:54 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)103 %09/29/17 01:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %09/29/17 01:54 17060-07-070-130 1
Toluene-d8 (S)107 %09/29/17 01:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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[phone]
Page 20 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379878
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92356385008, 92356385009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2105341
Associated Lab Samples:92356385008, 92356385009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/29/17 00:270.33
1,1,1-Trichloroethane ug/L ND 1.0 09/29/17 00:270.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/29/17 00:270.40
1,1,2-Trichloroethane ug/L ND 1.0 09/29/17 00:270.29
1,1-Dichloroethane ug/L ND 1.0 09/29/17 00:270.32
1,1-Dichloroethene ug/L ND 1.0 09/29/17 00:270.56
1,1-Dichloropropene ug/L ND 1.0 09/29/17 00:270.49
1,2,3-Trichlorobenzene ug/L ND 1.0 09/29/17 00:270.33
1,2,3-Trichloropropane ug/L ND 1.0 09/29/17 00:270.41
1,2,4-Trichlorobenzene ug/L ND 1.0 09/29/17 00:270.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/29/17 00:272.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/29/17 00:270.27
1,2-Dichlorobenzene ug/L ND 1.0 09/29/17 00:270.30
1,2-Dichloroethane ug/L ND 1.0 09/29/17 00:270.24
1,2-Dichloropropane ug/L ND 1.0 09/29/17 00:270.27
1,3-Dichlorobenzene ug/L ND 1.0 09/29/17 00:270.24
1,3-Dichloropropane ug/L ND 1.0 09/29/17 00:270.28
1,4-Dichlorobenzene ug/L ND 1.0 09/29/17 00:270.33
2,2-Dichloropropane ug/L ND 1.0 09/29/17 00:270.13
2-Butanone (MEK)ug/L ND 5.0 09/29/17 00:270.96
2-Chlorotoluene ug/L ND 1.0 09/29/17 00:270.35
2-Hexanone ug/L ND 5.0 09/29/17 00:270.46
4-Chlorotoluene ug/L ND 1.0 09/29/17 00:270.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/29/17 00:270.33
Acetone ug/L ND 25.0 09/29/17 00:2710.0
Benzene ug/L ND 1.0 09/29/17 00:270.25
Bromobenzene ug/L ND 1.0 09/29/17 00:270.30
Bromochloromethane ug/L ND 1.0 09/29/17 00:270.17
Bromodichloromethane ug/L ND 1.0 09/29/17 00:270.18
Bromoform ug/L ND 1.0 09/29/17 00:270.26
Bromomethane ug/L ND 2.0 09/29/17 00:270.29
Carbon tetrachloride ug/L ND 1.0 09/29/17 00:270.25
Chlorobenzene ug/L ND 1.0 09/29/17 00:270.23
Chloroethane ug/L ND 1.0 09/29/17 00:270.54
Chloroform ug/L ND 1.0 09/29/17 00:270.14
Chloromethane ug/L ND 1.0 09/29/17 00:270.11
cis-1,2-Dichloroethene ug/L ND 1.0 09/29/17 00:270.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/29/17 00:270.13
Dibromochloromethane ug/L ND 1.0 09/29/17 00:270.21
Dibromomethane ug/L ND 1.0 09/29/17 00:270.21
Dichlorodifluoromethane ug/L ND 1.0 09/29/17 00:270.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2105341
Associated Lab Samples:92356385008, 92356385009
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 09/29/17 00:270.12
Ethylbenzene ug/L ND 1.0 09/29/17 00:270.30
Hexachloro-1,3-butadiene ug/L ND 1.0 09/29/17 00:270.71
m&p-Xylene ug/L ND 2.0 09/29/17 00:270.66
Methyl-tert-butyl ether ug/L ND 1.0 09/29/17 00:270.21
Methylene Chloride ug/L ND 2.0 09/29/17 00:270.97
Naphthalene ug/L ND 1.0 09/29/17 00:270.24
o-Xylene ug/L ND 1.0 09/29/17 00:270.23
p-Isopropyltoluene ug/L ND 1.0 09/29/17 00:270.31
Styrene ug/L ND 1.0 09/29/17 00:270.26
Tetrachloroethene ug/L ND 1.0 09/29/17 00:270.46
Toluene ug/L ND 1.0 09/29/17 00:270.26
trans-1,2-Dichloroethene ug/L ND 1.0 09/29/17 00:270.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/29/17 00:270.26
Trichloroethene ug/L ND 1.0 09/29/17 00:270.47
Trichlorofluoromethane ug/L ND 1.0 09/29/17 00:270.20
Vinyl acetate ug/L ND 2.0 09/29/17 00:270.35
Vinyl chloride ug/L ND 1.0 09/29/17 00:270.62
Xylene (Total)ug/L ND 1.0 09/29/17 00:271.0
1,2-Dichloroethane-d4 (S)%99 70-130 09/29/17 00:27
4-Bromofluorobenzene (S)%103 70-130 09/29/17 00:27
Toluene-d8 (S)%109 70-130 09/29/17 00:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2105342LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 70-130
1,1,1-Trichloroethane ug/L 48.950 98 70-130
1,1,2,2-Tetrachloroethane ug/L 48.450 97 70-130
1,1,2-Trichloroethane ug/L 46.850 94 70-130
1,1-Dichloroethane ug/L 45.050 90 70-130
1,1-Dichloroethene ug/L 49.150 98 70-132
1,1-Dichloropropene ug/L 51.750 103 70-130
1,2,3-Trichlorobenzene ug/L 50.550 101 70-135
1,2,3-Trichloropropane ug/L 48.750 97 70-130
1,2,4-Trichlorobenzene ug/L 49.850 100 70-134
1,2-Dibromo-3-chloropropane ug/L 46.850 94 70-130
1,2-Dibromoethane (EDB)ug/L 52.250 104 70-130
1,2-Dichlorobenzene ug/L 48.350 97 70-130
1,2-Dichloroethane ug/L 46.150 92 70-130
1,2-Dichloropropane ug/L 45.850 92 70-130
1,3-Dichlorobenzene ug/L 48.150 96 70-130
1,3-Dichloropropane ug/L 54.650 109 70-130
1,4-Dichlorobenzene ug/L 47.250 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2105342LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.450 99 58-145
2-Butanone (MEK)ug/L 91.4100 91 70-145
2-Chlorotoluene ug/L 47.950 96 70-130
2-Hexanone ug/L 93.5100 93 70-144
4-Chlorotoluene ug/L 47.750 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 85.2100 85 70-140
Acetone ug/L 103100 103 50-175
Benzene ug/L 47.750 95 70-130
Bromobenzene ug/L 49.250 98 70-130
Bromochloromethane ug/L 48.950 98 70-130
Bromodichloromethane ug/L 47.150 94 70-130
Bromoform ug/L 47.550 95 70-130
Bromomethane ug/L 45.950 92 54-130
Carbon tetrachloride ug/L 49.750 99 70-132
Chlorobenzene ug/L 50.050 100 70-130
Chloroethane ug/L 46.950 94 64-134
Chloroform ug/L 51.650 103 70-130
Chloromethane ug/L 39.850 80 64-130
cis-1,2-Dichloroethene ug/L 46.150 92 70-131
cis-1,3-Dichloropropene ug/L 51.050 102 70-130
Dibromochloromethane ug/L 52.650 105 70-130
Dibromomethane ug/L 44.650 89 70-131
Dichlorodifluoromethane ug/L 42.950 86 56-130
Diisopropyl ether ug/L 46.250 92 70-130
Ethylbenzene ug/L 48.850 98 70-130
Hexachloro-1,3-butadiene ug/L 49.450 99 70-130
m&p-Xylene ug/L 97.9100 98 70-130
Methyl-tert-butyl ether ug/L 48.250 96 70-130
Methylene Chloride ug/L 43.450 87 63-130
Naphthalene ug/L 50.950 102 70-138
o-Xylene ug/L 50.550 101 70-130
p-Isopropyltoluene ug/L 49.150 98 70-130
Styrene ug/L 49.750 99 70-130
Tetrachloroethene ug/L 46.950 94 70-130
Toluene ug/L 45.750 91 70-130
trans-1,2-Dichloroethene ug/L 45.350 91 70-130
trans-1,3-Dichloropropene ug/L 50.150 100 70-132
Trichloroethene ug/L 50.950 102 70-130
Trichlorofluoromethane ug/L 43.150 86 62-133
Vinyl acetate ug/L 88.1100 88 66-157
Vinyl chloride ug/L 44.850 90 50-150
Xylene (Total)ug/L 148150 99 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2106662MATRIX SPIKE SAMPLE:
MSSpike
Result
92356448004
1,1,1,2-Tetrachloroethane ug/L 21.320 107 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,2-Trichloroethane ug/L 21.520 108 70-130ND
1,1-Dichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethene ug/L 22.920 115 70-166ND
1,1-Dichloropropene ug/L 24.120 120 70-130ND
1,2,3-Trichlorobenzene ug/L 21.920 110 70-130ND
1,2,3-Trichloropropane ug/L 22.220 111 70-130ND
1,2,4-Trichlorobenzene ug/L 22.420 112 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.520 98 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.520 108 70-130ND
1,2-Dichlorobenzene ug/L 20.820 104 70-130ND
1,2-Dichloroethane ug/L 20.320 102 70-130ND
1,2-Dichloropropane ug/L 20.120 101 70-130ND
1,3-Dichlorobenzene ug/L 20.920 104 70-130ND
1,3-Dichloropropane ug/L 23.620 118 70-130ND
1,4-Dichlorobenzene ug/L 20.520 103 70-130ND
2,2-Dichloropropane ug/L 25.920 129 70-130ND
2-Butanone (MEK)ug/L 37.740 94 70-130ND
2-Chlorotoluene ug/L 20.820 104 70-130ND
2-Hexanone ug/L 41.140 103 70-130ND
4-Chlorotoluene ug/L 21.520 107 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.840 90 70-130ND
Acetone ug/L 53.740 92 70-130ND
Benzene ug/L 22.320 111 70-148ND
Bromobenzene ug/L 21.820 109 70-130ND
Bromochloromethane ug/L 22.920 115 70-130ND
Bromodichloromethane ug/L 21.520 108 70-130ND
Bromoform ug/L 19.820 99 70-130ND
Bromomethane ug/L 24.020 120 70-130ND
Carbon tetrachloride ug/L 24.420 122 70-130ND
Chlorobenzene ug/L 23.220 116 70-146ND
Chloroethane ug/L 20.320 102 70-130ND
Chloroform ug/L 22.420 110 70-130ND
Chloromethane ug/L 18.920 95 70-130ND
cis-1,2-Dichloroethene ug/L 21.620 104 70-130ND
cis-1,3-Dichloropropene ug/L 21.920 109 70-130ND
Dibromochloromethane ug/L 21.320 106 70-130ND
Dibromomethane ug/L 20.820 104 70-130ND
Dichlorodifluoromethane ug/L 21.020 105 70-130ND
Diisopropyl ether ug/L 18.620 93 70-130ND
Ethylbenzene ug/L 22.320 112 70-130ND
Hexachloro-1,3-butadiene ug/L 23.620 118 70-130ND
m&p-Xylene ug/L 45.340 113 70-130ND
Methyl-tert-butyl ether ug/L 20.020 100 70-130ND
Methylene Chloride ug/L 18.220 91 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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Asheville, NC 28804
[phone]
Page 24 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2106662MATRIX SPIKE SAMPLE:
MSSpike
Result
92356448004
Naphthalene ug/L 21.920 109 70-130ND
o-Xylene ug/L 22.720 114 70-130ND
p-Isopropyltoluene ug/L 22.720 114 70-130ND
Styrene ug/L 22.220 111 70-130ND
Tetrachloroethene ug/L 51.620 125 70-13026.6
Toluene ug/L 21.720 108 70-155ND
trans-1,2-Dichloroethene ug/L 21.120 106 70-130ND
trans-1,3-Dichloropropene ug/L 21.620 108 70-130ND
Trichloroethene ug/L 22.820 111 69-151ND
Trichlorofluoromethane ug/L 20.720 103 70-130ND
Vinyl acetate ug/L 36.840 92 70-130ND
Vinyl chloride ug/L 21.920 109 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92356448005
2106663SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L 1.2 1 301.3
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92356448005
2106663SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 15.2 5 3014.4
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 297
4-Bromofluorobenzene (S)%101 0101
Toluene-d8 (S)%107 0107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379927
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92356385001, 92356385004, 92356385005, 92356385006, 92356385007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2105590
Associated Lab Samples:92356385001, 92356385004, 92356385005, 92356385006, 92356385007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/29/17 00:440.33
1,1,1-Trichloroethane ug/L ND 1.0 09/29/17 00:440.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/29/17 00:440.40
1,1,2-Trichloroethane ug/L ND 1.0 09/29/17 00:440.29
1,1-Dichloroethane ug/L ND 1.0 09/29/17 00:440.32
1,1-Dichloroethene ug/L ND 1.0 09/29/17 00:440.56
1,1-Dichloropropene ug/L ND 1.0 09/29/17 00:440.49
1,2,3-Trichlorobenzene ug/L ND 1.0 09/29/17 00:440.33
1,2,3-Trichloropropane ug/L ND 1.0 09/29/17 00:440.41
1,2,4-Trichlorobenzene ug/L ND 1.0 09/29/17 00:440.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/29/17 00:442.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/29/17 00:440.27
1,2-Dichlorobenzene ug/L ND 1.0 09/29/17 00:440.30
1,2-Dichloroethane ug/L ND 1.0 09/29/17 00:440.24
1,2-Dichloropropane ug/L ND 1.0 09/29/17 00:440.27
1,3-Dichlorobenzene ug/L ND 1.0 09/29/17 00:440.24
1,3-Dichloropropane ug/L ND 1.0 09/29/17 00:440.28
1,4-Dichlorobenzene ug/L ND 1.0 09/29/17 00:440.33
2,2-Dichloropropane ug/L ND 1.0 09/29/17 00:440.13
2-Butanone (MEK)ug/L ND 5.0 09/29/17 00:440.96
2-Chlorotoluene ug/L ND 1.0 09/29/17 00:440.35
2-Hexanone ug/L ND 5.0 09/29/17 00:440.46
4-Chlorotoluene ug/L ND 1.0 09/29/17 00:440.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/29/17 00:440.33
Acetone ug/L ND 25.0 09/29/17 00:4410.0
Benzene ug/L ND 1.0 09/29/17 00:440.25
Bromobenzene ug/L ND 1.0 09/29/17 00:440.30
Bromochloromethane ug/L ND 1.0 09/29/17 00:440.17
Bromodichloromethane ug/L ND 1.0 09/29/17 00:440.18
Bromoform ug/L ND 1.0 09/29/17 00:440.26
Bromomethane ug/L ND 2.0 09/29/17 00:440.29
Carbon tetrachloride ug/L ND 1.0 09/29/17 00:440.25
Chlorobenzene ug/L ND 1.0 09/29/17 00:440.23
Chloroethane ug/L ND 1.0 09/29/17 00:440.54
Chloroform ug/L ND 1.0 09/29/17 00:440.14
Chloromethane ug/L ND 1.0 09/29/17 00:440.11
cis-1,2-Dichloroethene ug/L ND 1.0 09/29/17 00:440.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/29/17 00:440.13
Dibromochloromethane ug/L ND 1.0 09/29/17 00:440.21
Dibromomethane ug/L ND 1.0 09/29/17 00:440.21
Dichlorodifluoromethane ug/L ND 1.0 09/29/17 00:440.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2105590
Associated Lab Samples:92356385001, 92356385004, 92356385005, 92356385006, 92356385007
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 09/29/17 00:440.12
Ethylbenzene ug/L ND 1.0 09/29/17 00:440.30
Hexachloro-1,3-butadiene ug/L ND 1.0 09/29/17 00:440.71
m&p-Xylene ug/L ND 2.0 09/29/17 00:440.66
Methyl-tert-butyl ether ug/L ND 1.0 09/29/17 00:440.21
Methylene Chloride ug/L ND 2.0 09/29/17 00:440.97
Naphthalene ug/L ND 1.0 09/29/17 00:440.24
o-Xylene ug/L ND 1.0 09/29/17 00:440.23
p-Isopropyltoluene ug/L ND 1.0 09/29/17 00:440.31
Styrene ug/L ND 1.0 09/29/17 00:440.26
Tetrachloroethene ug/L ND 1.0 09/29/17 00:440.46
Toluene ug/L ND 1.0 09/29/17 00:440.26
trans-1,2-Dichloroethene ug/L ND 1.0 09/29/17 00:440.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/29/17 00:440.26
Trichloroethene ug/L ND 1.0 09/29/17 00:440.47
Trichlorofluoromethane ug/L ND 1.0 09/29/17 00:440.20
Vinyl acetate ug/L ND 2.0 09/29/17 00:440.35
Vinyl chloride ug/L ND 1.0 09/29/17 00:440.62
Xylene (Total)ug/L ND 1.0 09/29/17 00:441.0
1,2-Dichloroethane-d4 (S)%97 70-130 09/29/17 00:44
4-Bromofluorobenzene (S)%102 70-130 09/29/17 00:44
Toluene-d8 (S)%109 70-130 09/29/17 00:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2105591LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.550 105 70-130
1,1,1-Trichloroethane ug/L 47.050 94 70-130
1,1,2,2-Tetrachloroethane ug/L 51.050 102 70-130
1,1,2-Trichloroethane ug/L 49.650 99 70-130
1,1-Dichloroethane ug/L 43.050 86 70-130
1,1-Dichloroethene ug/L 48.950 98 70-132
1,1-Dichloropropene ug/L 51.250 102 70-130
1,2,3-Trichlorobenzene ug/L 52.950 106 70-135
1,2,3-Trichloropropane ug/L 53.450 107 70-130
1,2,4-Trichlorobenzene ug/L 51.850 104 70-134
1,2-Dibromo-3-chloropropane ug/L 47.650 95 70-130
1,2-Dibromoethane (EDB)ug/L 54.250 108 70-130
1,2-Dichlorobenzene ug/L 51.250 102 70-130
1,2-Dichloroethane ug/L 45.650 91 70-130
1,2-Dichloropropane ug/L 46.350 93 70-130
1,3-Dichlorobenzene ug/L 50.050 100 70-130
1,3-Dichloropropane ug/L 58.050 116 70-130
1,4-Dichlorobenzene ug/L 49.450 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2105591LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 48.250 96 58-145
2-Butanone (MEK)ug/L 94.6100 95 70-145
2-Chlorotoluene ug/L 49.150 98 70-130
2-Hexanone ug/L 99.4100 99 70-144
4-Chlorotoluene ug/L 50.550 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 89.4100 89 70-140
Acetone ug/L 102100 102 50-175
Benzene ug/L 48.350 97 70-130
Bromobenzene ug/L 51.250 102 70-130
Bromochloromethane ug/L 47.750 95 70-130
Bromodichloromethane ug/L 47.450 95 70-130
Bromoform ug/L 50.450 101 70-130
Bromomethane ug/L 46.550 93 54-130
Carbon tetrachloride ug/L 49.050 98 70-132
Chlorobenzene ug/L 51.050 102 70-130
Chloroethane ug/L 46.250 92 64-134
Chloroform ug/L 48.150 96 70-130
Chloromethane ug/L 38.950 78 64-130
cis-1,2-Dichloroethene ug/L 45.350 91 70-131
cis-1,3-Dichloropropene ug/L 51.250 102 70-130
Dibromochloromethane ug/L 53.350 107 70-130
Dibromomethane ug/L 46.150 92 70-131
Dichlorodifluoromethane ug/L 42.150 84 56-130
Diisopropyl ether ug/L 46.350 93 70-130
Ethylbenzene ug/L 50.350 101 70-130
Hexachloro-1,3-butadiene ug/L 51.050 102 70-130
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 48.850 98 70-130
Methylene Chloride ug/L 44.250 88 63-130
Naphthalene ug/L 54.150 108 70-138
o-Xylene ug/L 51.950 104 70-130
p-Isopropyltoluene ug/L 52.750 105 70-130
Styrene ug/L 52.150 104 70-130
Tetrachloroethene ug/L 49.950 100 70-130
Toluene ug/L 46.050 92 70-130
trans-1,2-Dichloroethene ug/L 44.850 90 70-130
trans-1,3-Dichloropropene ug/L 51.950 104 70-132
Trichloroethene ug/L 49.950 100 70-130
Trichlorofluoromethane ug/L 43.850 88 62-133
Vinyl acetate ug/L 90.7100 91 66-157
Vinyl chloride ug/L 43.550 87 50-150
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2106660MATRIX SPIKE SAMPLE:
MSSpike
Result
92356774003
1,1,1,2-Tetrachloroethane ug/L 21.220 106 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.120 105 70-130ND
1,1,2-Trichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethane ug/L 20.120 100 70-130ND
1,1-Dichloroethene ug/L 24.020 120 70-166ND
1,1-Dichloropropene ug/L 24.120 120 70-130ND
1,2,3-Trichlorobenzene ug/L 24.720 123 70-130ND
1,2,3-Trichloropropane ug/L 21.720 108 70-130ND
1,2,4-Trichlorobenzene ug/L 23.620 118 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.720 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.820 109 70-130ND
1,2-Dichlorobenzene ug/L 21.520 108 70-130ND
1,2-Dichloroethane ug/L 19.620 98 70-130ND
1,2-Dichloropropane ug/L 20.720 103 70-130ND
1,3-Dichlorobenzene ug/L 22.220 111 70-130ND
1,3-Dichloropropane ug/L 23.320 116 70-130ND
1,4-Dichlorobenzene ug/L 21.720 109 70-130ND
2,2-Dichloropropane ug/L 24.820 124 70-130ND
2-Butanone (MEK)ug/L 36.640 92 70-130ND
2-Chlorotoluene ug/L 22.520 112 70-130ND
2-Hexanone ug/L 42.140 105 70-130ND
4-Chlorotoluene ug/L 22.420 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 36.940 92 70-130ND
Acetone ug/L 42.740 107 70-130ND
Benzene ug/L 21.920 110 70-148ND
Bromobenzene ug/L 23.720 119 70-130ND
Bromochloromethane ug/L 21.420 107 70-130ND
Bromodichloromethane ug/L 21.420 107 70-130ND
Bromoform ug/L 20.020 100 70-130ND
Bromomethane ug/L 23.720 118 70-130ND
Carbon tetrachloride ug/L 24.920 125 70-130ND
Chlorobenzene ug/L 22.820 114 70-146ND
Chloroethane ug/L 20.820 104 70-130ND
Chloroform ug/L 22.620 113 70-130ND
Chloromethane ug/L 18.520 91 70-1300.17J
cis-1,2-Dichloroethene ug/L 20.520 102 70-130ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-130ND
Dibromochloromethane ug/L 21.820 109 70-130ND
Dibromomethane ug/L 21.020 105 70-130ND
Dichlorodifluoromethane ug/L 21.220 106 70-130ND
Diisopropyl ether ug/L 18.920 94 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Hexachloro-1,3-butadiene ug/L 26.3 M12013170-130ND
m&p-Xylene ug/L 45.640 114 70-130ND
Methyl-tert-butyl ether ug/L 20.820 104 70-130ND
Methylene Chloride ug/L 18.820 94 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2106660MATRIX SPIKE SAMPLE:
MSSpike
Result
92356774003
Naphthalene ug/L 23.720 119 70-130ND
o-Xylene ug/L 23.020 115 70-130ND
p-Isopropyltoluene ug/L 24.420 122 70-130ND
Styrene ug/L 22.120 110 70-130ND
Tetrachloroethene ug/L 22.720 114 70-130ND
Toluene ug/L 21.920 109 70-155ND
trans-1,2-Dichloroethene ug/L 21.520 108 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
Trichloroethene ug/L 22.820 114 69-151ND
Trichlorofluoromethane ug/L 20.420 102 70-130ND
Vinyl acetate ug/L 37.640 94 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92356774004
2106661SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356385
South LF MW 9/21
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92356774004
2106661SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.24J 300.25J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 3.4 10 303.1
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L 0.72J 300.70J
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 198
4-Bromofluorobenzene (S)%104 698
Toluene-d8 (S)%107 0107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92356385
South LF MW 9/21
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92356385
South LF MW 9/21
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92356385001 MW-1S
92356385002 MW-2S
92356385003 MW-3S
92356385004 MW-4S
92356385005 MW-5S
92356385006 MW-6S
92356385007 MW-7S
92356385001 379927MW-1S EPA 8260
92356385004 379927MW-4S EPA 8260
92356385005 379927MW-5S EPA 8260
92356385006 379927MW-6S EPA 8260
92356385007 379927MW-7S EPA 8260
92356385008 379878EQUIP BLK EPA 8260
92356385009 379878TVL BLK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2017 04:00 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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