5002_JacksonCountyMSWLF_GWMR_20170630

June 2017
Jackson County Closed Municipal Solid Waste Landfill
Spring 2017 Semiannual Water Quality
Monitoring Report
Prepared for Jackson County Solid Waste Department

Project Number: C61480-01.01 A:\Projects\Jackson County\Dillsboro GW\Reports\2017\Spring\FINAL5002March2017 Semiannual Water Quality Report mb.docx
June 2017
Jackson County Closed Municipal Solid Waste Landfill
Spring 2017 Semiannual Water Quality
Monitoring Report

Prepared for
Jackson County Solid Waste Department
401 Grindstaff Cove Rd.
Sylva, NC 28779
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, NC 28801

_____________________________________ Alec Macbeth, P.G.
Project Geologist

Spring 2017 Semiannual
Water Quality Monitoring Report i June 2017
TABLE OF CONTENTS
1 Introduction .................................................................................................................... 1
2 Semiannual Monitoring ................................................................................................ 3
2.1 Groundwater, Surface Water, and Leachate Sampling ..................................................................... 3
2.1.1 Monitoring Well Purging and Sampling Methods.............................................................. 3
2.1.2 Surface Water Sampling Methods ........................................................................................... 4
2.1.3 Leachate Sampling Methods ..................................................................................................... 4
2.2 Sample Handling, Documentation, and Analysis ............................................................................... 5
3 Findings .......................................................................................................................... 6
3.1 Analytical Results ......................................................................................................................................... 6
3.1.1 Groundwater .................................................................................................................................. 7
3.1.2 Surface Water............................................................................................................................... 10
3.1.3 Leachate......................................................................................................................................... 10
3.2 Groundwater Flow Direction................................................................................................................... 11
4 Summary ....................................................................................................................... 12
4.1 Groundwater Quality ................................................................................................................................ 12
4.1.1 Metals............................................................................................................................................. 12
4.1.2 VOCs ............................................................................................................................................... 12
4.1.3 Field Parameters and Other Constituents............................................................................ 12
4.2 Surface Water Quality............................................................................................................................... 13
4.3 Leachate Quality......................................................................................................................................... 13
5 Future Activities ............................................................................................................14
6 References ..................................................................................................................... 15

TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Summary of Analytical Results
Table 3 Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in
the Leachate Sample (LT-01)
Table 4 Well Construction Details and Corresponding Elevations

Spring 2017 Semiannual
Water Quality Monitoring Report ii June 2017
FIGURES
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Generalized Groundwater Flow Direction
Figure 4 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
Figure 5 Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-01)
Figure 6 Hydrograph and Tetrachloroethene Concentration vs. Time
(Monitoring Well MW-01)
Figure 7 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-03)
Figure 8 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-05R)
Figure 9 Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-05R)
Figure 10 Hydrograph and Vinyl Chloride Concentration vs. Time (Monitoring Well MW-05R)
Figure 11 Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-07)
APPENDICES
Appendix A Well Sampling Logs and Equipment Documentation & Instrument Calibration
Data Sheets
Appendix B Reports of Laboratory Analysis, Chain-of-Custody Documentation, and
Certificates of Analysis

Spring 2017 Semiannual
Water Quality Monitoring Report iii June 2017
ABBREVIATIONS
µg/L micrograms per liter
µS/cm microsiemens per centimeter
ACM Assessment of Corrective Measures
Altamont Altamont Environmental, Inc., which became Anchor QEA on December 29,
2016
AM Analytical Method
Anchor QEA Anchor QEA of North Carolina, PLLC
BOD biochemical oxygen demand
CAER Five-Year Corrective Action Evaluation Report
CAP Corrective Action Plan
CFR Code of Federal Regulations
cis-1,2-DCE cis-1,2-dichloroethene
COC constituents of concern
COD chemical oxygen demand
DENR North Carolina Department of Environment and Natural Resources, which is
now the DEQ
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
EDD Electronic Data Deliverable
EPA U.S. Environmental Protection Agency
GWPS Groundwater Protection Standards
IMAC interim maximum allowable concentrations
MDL method detection limit
mg/L milligrams per liter
MNA monitored natural attenuation
MRL method reporting limit
MSWLF Municipal Solid Waste Landfill
mV millivolt
NCAC North Carolina Administrative Code
NTU nephelometric turbidity units
ORP oxidation reduction potential
PWR partially weathered rock
SESD Science and Ecosystem Support Division
SM Standard Method
SU Standard Units

Spring 2017 Semiannual
Water Quality Monitoring Report iv June 2017
SWS Solid Waste Section
SWSL Solid Waste Section Limit
TOC total organic carbon
TWSA Tuckaseigee Water & Sewer Authority
VOC volatile organic compound

Spring 2017 Semiannual
Water Quality Monitoring Report 1 June 2017
1 Introduction
Anchor QEA of North Carolina, PLLC (Anchor QEA) is pleased to present this Semiannual Water
Quality Monitoring Report for Spring 2017.
The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill
(MSWLF) located approximately 0.75 miles west of Dillsboro, North Carolina, on the northeast side of
Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the landfill is
governed by the North Carolina Department of Environmental Quality (DEQ), Division of Waste
Management (DWM), Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson County.
The landfill permit requires semiannual monitoring of groundwater and surface water quality.
Since October 2007, when Altamont Environmental, Inc. [Altamont]1 began performing water quality
monitoring events, groundwater quality monitoring has indicated persistent low-level concentrations
of constituents that exceed groundwater standards. In response to the continued exceedances of
analyzed constituents, an Assessment of Corrective Measures (ACM) was submitted to the North
Carolina Department of Environment and Natural Resources (DENR), which is now the DEQ, on
September 7, 2010 and a Corrective Action Plan (CAP) was implemented upon approval by the DEQ
as recorded in the September 1, 2011 letter Approval of the County’s Corrective Action Plan. The
implemented remedy includes the extraction of leachate through dedicated submersible pumps
installed within the landfill gas extraction wells and disposal of the leachate into the Tuckaseigee
Water & Sewer Authority (TWSA) collection system. In addition to the leachate extraction,
groundwater natural attenuation parameters are monitored and natural attenuation processes are
evaluated. As discussed in the CAP, a corrective action evaluation report is prepared every 5 years.
The evaluation report analyzes the progress of the approved corrective action remedy based on
semiannual water quality monitoring data. The remedy was implemented in a phased approach with
full implementation occurring on September 6, 2013. The first Five-Year Corrective Action Evaluation
Report (CAER) was submitted by Altamont on October 31, 2016 and concluded that current
conditions of the monitored natural attenuation (MNA) parameters and Site geochemical parameters
allow for the slow degradation of the constituents of concern (COCs).
This report serves as the first semiannual water quality monitoring report for 2017 and as the 12th
report following approval of the CAP. This report provides an evaluation of groundwater and surface
water quality. The water quality monitoring network is presented on Figure 2. The generalized
groundwater flow direction in the upper parts of the underlying aquifer system (Figure 3) is also
provided in this report.

1 Altamont became Anchor QEA on December 29, 2016.

Spring 2017 Semiannual
Water Quality Monitoring Report 2 June 2017
In addition to groundwater and surface water monitoring, this report includes volatile organic
compound (VOC) analysis of the extracted leachate.
The water samples are collected from selected monitoring points during the spring and fall of each
year and are analyzed for the following (Table 1):
• Appendix I VOCs
• Appendix I Metals
• MNA parameters: alkalinity, biochemical oxygen demand (BOD), chemical oxygen demand
(COD), chloride, carbon dioxide, cyanide, ethane, ethene, hydrogen, ferrous iron, methane,
nitrate, sulfate, sulfide, total organic carbon (TOC), and volatile fatty acids.
The spring 2017 sampling event was performed on March 21 and 22, 2017, and is being reported in
accordance with requirements stipulated in the DEQ Solid Waste Management Rules codified under
Title 15A Subchapter 13B of the North Carolina Administrative Code (15A North Carolina
Administrative Code [NCAC] 13B).

Spring 2017 Semiannual
Water Quality Monitoring Report 3 June 2017
2 Semiannual Monitoring
2.1 Groundwater, Surface Water, and Leachate Sampling
The closed MSWLF monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06,
and MW-07), surface water sample locations (SW-01 and SW-02), and leachate sample
location (LT-01) were sampled on March 21 and 22, 2017 by Anchor QEA. Static groundwater level
measurements and all field parameter data are included on the well sampling logs presented in
Appendix A. Field equipment calibration logs for the YSI 556 Multi-parameter Water Quality Meter
and the Hach 2100Q Turbidimeter are also provided in Appendix A. The full suite of groundwater
and surface water laboratory analytical results is presented in the laboratory analysis reports in
Appendix B.
Monitoring well MW-02 serves as the Site’s background monitoring well, due to its location outside
of the contamination plume. Monitoring wells MW-01 and MW-06 are the Site’s upgradient
monitoring wells, MW-03 and MW-05R are located in the midgradient portion of the Site,
and MW-04 and MW-07 monitor downgradient portions of the Site.
The monitoring wells, surface water sample locations, and leachate sample location are depicted on
Figure 2.
2.1.1 Monitoring Well Purging and Sampling Methods
Prior to sampling the monitoring wells, the static water level was gauged in each well and an initial
round of field parameters consisting of pH, specific conductivity, dissolved oxygen (DO), turbidity,
temperature, and oxidation reduction potential (ORP) were measured.
Anchor QEA personnel used either low-flow techniques or disposable bailers (purge methods are
discussed further in Section 2.1.1.1) to purge the monitoring wells and collect groundwater samples.
Total depth, condition of the casing, and the groundwater recharge rate determined the purging and
sample collection method employed at each monitoring well.
2.1.1.1 Monitoring Wells
Four of the monitoring wells, MW-03, MW-04, MW-06, and MW-07 were purged using low-flow
techniques in accordance with the procedures described in the U.S. Environmental Protection
Agency’s (EPA’s) Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures (EPA 1996).
During purging, the pH, specific conductivity, DO, ORP, turbidity, and temperature (field parameters)
were measured and recorded approximately every 3 minutes. Well purging continued until these
parameters generally stabilized for three consecutive readings. The required stabilization criteria

Spring 2017 Semiannual
Water Quality Monitoring Report 4 June 2017
were determined by the EPA Region 4 Science and Ecosystem Support Division (SESD) Operating
Procedure: Groundwater Sampling (EPA 2013) and are summarized as follows:
• pH values within +/- 0.1 Standard Unit (SU)
• Specific conductivity values within +/- 5 percent
• Temperature, DO, and turbidity values within +/- 10 percent
• ORP values within +/- 10 millivolts
Once the parameters had stabilized, a groundwater sample was collected by a technician wearing a
new pair of nitrile gloves using laboratory-supplied sample containers.
Monitoring well MW-01 was purged and sampled using a new, disposable Teflon bailer on March 21,
2017. A bailer was used to purge and sample this monitoring well due to its slow recharge rate. The
well was purged of three successive well volumes prior to sample collection. During purging, a round
of field parameters was measured and recorded at the start of purging and after each consecutive
well volume was purged. After the third consecutive well volume was purged, a groundwater sample
was collected. Monitoring wells MW-02 and MW-05R were purged dry with a disposable,
polyethylene bailer on March 21, 2017 and the groundwater sample was collected on the following
day after the well had recharged. All field parameter data are shown on the well sampling logs,
included in Appendix A.
2.1.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02 were collected on March 22, 2017, at designated locations
from the Tuckasegee River, which is adjacent to and southwest of the landfill (Figure 2). Surface
water sampling location SW-01 is representative of surface water quality upstream of the landfill and
surface water sampling location SW-02 is representative of surface water quality downstream from
the landfill. One round of field parameters was measured and recorded at each surface water
sampling location immediately prior to collecting the sample (Appendix A). The surface water
samples were collected in laboratory-provided sample containers by a technician wearing a new pair
of nitrile gloves.
2.1.3 Leachate Sampling Methods
Dedicated bottom-loading, air-powered pumps, air-pressure lines, and a leachate force main
collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells
EW-1R, EW-2R, EW-3R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well
locations are presented on Figure 2. The leachate is pumped from the wells into a flow equalization
tank, which is connected to the TWSA wastewater collection system.
The flow equalization tank is situated to the northeast of the landfill adjacent to the existing landfill
gas flare. A grab sample of leachate (LT-01) was collected by taking a sample as the leachate entered

Spring 2017 Semiannual
Water Quality Monitoring Report 5 June 2017
the flow equalization tank. One round of field parameters was measured and recorded after
collecting the sample (Appendix A).
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to the closed MSWLF sampling locations are
provided on sampling logs (Appendix A). Following sample collection, each groundwater, surface
water, and leachate sample was immediately placed on ice in a sample cooler for transport to Prism
Laboratory, a North Carolina-certified laboratory located in Charlotte, NC. The groundwater samples
collected from the monitoring wells were analyzed for the following parameters:
• Appendix I Metals using EPA Approved Methods (EPA Method) 6020B and 7470A
• Appendix I VOCs using EPA Method 8260B
‒ Appendix I parameters are identified in Appendix I of the Code of Federal Regulations,
Title 40, Part 258 (40 CFR 258).
• MNA Parameters:
‒ Alkalinity using Standard Method (SM) 2320B
‒ BOD (5-Day) using SM 5210B
‒ Carbon dioxide, hydrogen, ethane, ethene, and methane using Analytical Method (AM)
20GAX
‒ COD using SM 5220D
‒ Chloride, nitrate, and sulfate using EPA Approved Method 9056A
‒ Cyanide using SM 4500-CN E
‒ Ferrous iron using SM 3500-Fe D
‒ Sulfide using SM 4500-S F
‒ TOC using SM 9060A
‒ Volatile fatty acids using AM23G
The surface water samples were analyzed for Appendix I parameters (as listed above). The leachate
sample was analyzed for Appendix I VOC parameters only.
Proper chain-of-custody documentation procedures were followed during collection and
transportation of each sample (Appendix B). Three trip blank samples for quality control/quality
assurance purposes were included in the sample coolers and analyzed for Appendix I VOCs. The
reports of laboratory analysis are provided in Appendix B. Laboratory analyses performed on the
samples are summarized in Table 1.

Spring 2017 Semiannual
Water Quality Monitoring Report 6 June 2017
3 Findings
3.1 Analytical Results
The laboratory analytical results and field parameter data for the groundwater samples (from
monitoring wells MW-01 through MW-07), surface water samples (SW-01 and SW-02), and leachate
sample (LT-01) collected at the landfill are included in Appendices A and B in hard copy and also
submitted separately to the DEQ DWM SWS in the Electronic Data Deliverable (EDD) format per DEQ
guidelines (most recently updated on May 5, 2010).
As stipulated in the SWS documents referenced in the paragraph above, all laboratory analytical
results were reported and appropriately qualified as follows:
• Non-detections: Non-detections (non-detects) are values reported by the laboratory as
below method detection limits (MDLs). They are tabulated on Table 2 and are qualified with
the “U” qualifier. The MDL is the minimum concentration of a substance that can be measured
and reported by a laboratory with 99 percent confidence that the constituent concentration is
greater than zero.
• Solid Waste Section Limits: All detections (values above the MDL) were compared to
constituent-specific Solid Waste Section Limits (SWSLs) established by DEQ. The SWSL is
defined as the lowest concentration of a constituent in a sample that can be quantitatively
determined with suitable precision and accuracy. A non-italicized “J” qualifier is used by the
laboratory for parameters that are detected at estimated concentrations greater than the MDL
but less than the laboratory’s method reporting limit (MRL). The MRL is the minimum
concentration of a target analyte that can be accurately determined by the referenced
method.
• Estimated or “J” Qualified: If the reported concentration is greater than the laboratory MDL
and MRL but less than the SWSL, the analytical result is qualified as estimated, and is flagged
with a “J” qualifier (italicized J-flag) by Anchor QEA, per SWS reporting requirements. In
addition to non-detects, detected concentrations of constituents below the applicable SWSLs
are included in Table 2.
• 2L Standard: Detected concentrations of constituents in groundwater samples were
compared to applicable North Carolina groundwater quality standards. For most constituents,
this standard is the 2L standard, defined in 15A NCAC 2L.0202. Detected concentrations of
analytes in groundwater with no established 2L standard were compared either to the interim
maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]) or Groundwater Protection Standards (GWPS),
pursuant to 15A NCAC 13B.1634.
• 2B Standard: Detections of analytes in surface-water samples were compared to the
surface-water quality standards described in 15A NCAC 2B (2B standards).

Spring 2017 Semiannual
Water Quality Monitoring Report 7 June 2017
Table 2 presents the summary of detected constituents and outlines concentrations of analytes that
were above applicable SWSLs, as well as detected analytes that exceeded their respective 2L
standard, IMAC, GWPS, or 2B standard.
3.1.1 Groundwater
Measured field parameters and analytical results of groundwater samples collected from the
monitoring wells are discussed in the following sections.
3.1.1.1 Field Parameters
During groundwater sampling on March 21 and 22, 2017, pH readings were obtained. The pH
readings obtained from samples collected from wells MW-01, MW-03, MW-04, MW-05R, MW-06,
and MW-07 were below 6.5 SU, thus outside the acceptable pH range of 6.5 to 8.5 SU specified in
15A NCAC 02L .0202[c] (Table 2). The recorded pH readings are consistent with historical data.
The highest turbidity (136 NTU) was measured in the groundwater sample collected from well
MW-05R. Elevated turbidity levels are generally observed in monitoring wells that are purged via the
bailer method. Bailers were lowered gently to minimize water column disturbance when samples
were collected. The lowest turbidity was measured (0.32 nephelometric turbidity units [NTU]) in the
groundwater sample collected from well MW-03.
Dissolved oxygen concentrations at the Site ranged from 1.12 milligrams per liter (mg/L) in
monitoring well MW-07 to 6.24 mg/L in monitoring well MW-02. Specific conductivity concentrations
at the Site ranged from 108 microsiemens per centimeter (µS/cm) in monitoring well MW-06 to
591 µS/cm in monitoring well MW-05R. Oxidation reduction potential concentrations at the Site
ranged from -5.3 millivolts (mV) in monitoring well MW-05R to 259.5 mV in monitoring well MW-03.
Groundwater standards are not established for dissolved oxygen, specific conductivity, or oxidation
reduction potential.
3.1.1.2 Appendix I Metals
Five metals (cadmium, chromium, cobalt, thallium, and vanadium) were detected at concentrations
above their respective 2L, IMAC, or GWPS water quality standards in the groundwater samples
collected from one or more of the monitoring wells during the spring 2017 water quality monitoring
event. Cadmium and chromium exceeded their respective 2L standard, the other three metals
exceeded their IMACs.
Cadmium was detected in one monitoring well, MW-01, at a concentration of 2.3 micrograms per
liter (µg/L) that exceeded its 2L standard of 2 µg/L. Cadmium concentrations in the samples collected
from MW-01 have exceeded the 2L standard during several prior sampling events, according to

Spring 2017 Semiannual
Water Quality Monitoring Report 8 June 2017
historical data. Cadmium was detected in all of the remaining monitoring wells on-Site, but below
the 2L standard; this condition is consistent with historical data.
Chromium was detected in one monitoring well, MW-02, at a concentration of 12 µg/L that
exceeded its 2L standard of 10 µg/L. According to historical data, this is the second monitoring event
where chromium exceeded its 2L standard in this monitoring well since the April 2007 sampling
event. As with cadmium, chromium was detected in all of the remaining monitoring wells on-Site,
but below the 2L standard.
Cobalt was detected above its IMAC in all collected groundwater samples, with the exception of
MW-07. Exceedances of cobalt in these samples showed concentrations ranging from 2.8 J µg/L
(MW-04) to 150 µg/L (MW-01). Historically, cobalt has been present above its applicable water
quality standard in groundwater samples from all seven monitoring wells.
Thallium was detected in all of the groundwater samples collected from the landfill. Three of the
groundwater samples (collected from wells MW-01, MW-02, and MW-06) contained concentrations
that were above the IMAC water quality standard of 0.2 µg/L. Concentrations of thallium in these
samples ranged from 0.31 J µg/L (MW-02) to 1.2 J µg/L (MW-01). Historically, thallium has been
detected at concentrations above its water quality standard in the samples collected from
groundwater monitoring wells MW-01, MW-05R, and MW-06.
Vanadium was detected in the groundwater samples collected from monitoring wells MW-02 and
MW-05R at concentrations of 20 J µg/L and 2.7 J µg/L, respectively. Historically, vanadium has been
present above its water quality standard in the samples collected from multiple groundwater
monitoring wells.
3.1.1.3 Appendix I VOCs
Four VOCs (1,4-dichlorobenzene, benzene, tetrachloroethene, and vinyl chloride) were detected at
concentrations above their respective 2L standards in the groundwater samples collected from one
or more monitoring wells during the spring 2017 water quality monitoring event. Concentration-
versus-time graphs were created for samples from those monitoring wells that had VOC
concentrations over their 2L standards during the spring 2017 sampling event. The graphs are
provided as Figure 4 through Figure 11.
1,4-dichlorobenzene was detected at concentrations above its 2L standard (6 µg/L) in monitoring
wells MW-01 (12 µg/L), MW-03 (12 µg/L), and MW-05R (10 µg/L). This VOC was also detected in
monitoring wells MW-04, MW-06, and MW-07 at concentrations above the SWSL but below the
2L standard (Table 2). Historical 1,4-dichlorobenze concentration trends in these wells have been
stable and slightly above or slightly below the 2L standard (Figures 4, 7, and 8).

Spring 2017 Semiannual
Water Quality Monitoring Report 9 June 2017
Benzene was detected at a concentration above its 2L standard of 1 µg/L in monitoring wells MW-01
(1.8 µg/L), MW-05R (1.8 µg/L), and MW-07 (1.6 µg/L) during the spring 2017 sampling event.
Benzene was also detected in monitoring wells MW-03, MW-04, and MW-06 at concentrations below
both the SWSL and 2L standard (Table 2). Overall, historical benzene concentration trends in
monitoring wells MW-05R and MW-07 have been stable and slightly over the 2L standard, while
monitoring well MW-01 exhibits a downward trend in benzene concentrations (Figures 5, 9, and 11).
Tetrachloroethene was only detected in the sample collected from monitoring well MW-01, at a
concentration of 0.99 J µg/L (Table 2), which exceeded the 2L standard of 0.7 µg/L. Historical
concentration trends for tetrachloroethene in this monitoring well show consistent and stable
detections with occasional 2L exceedances (Figure 6).
The concentration of vinyl chloride in the sample collected from monitoring well MW-05R (1.3 µg/L)
was above the SWSL and the 2L standard (0.3 µg/L) during this sampling event. A concentration
trend graph for vinyl chloride concentrations in MW-05R is presented in Figure 10. Vinyl chloride was
not detected in any of the other monitoring wells during this sampling event (Table 2). Historically,
vinyl chloride has regularly exceeded its 2L standard in monitoring wells MW-04, MW-05R, and
MW-07, located in the southwestern part of the landfill.
A review of historical groundwater data indicates that three VOCs (1,4-dichlorobenzene, benzene,
and vinyl chloride) have been detected at relatively consistent concentrations for the past several
years. As described in Section 3.1.2, historical surface water samples from the Tuckasegee River,
which likely receives discharge from the saprolite groundwater-bearing zone, have consistently
shown no detections of these compounds, or any other VOCs.
3.1.1.4 Natural Attenuation Parameters
Groundwater samples collected from all monitoring wells were analyzed for additional parameters as
follows: alkalinity, BOD, COD, carbon dioxide, chloride, cyanide, ethane, ethene, hydrogen (for wells
MW-03, MW-04, MW-06, and MW-07 only), methane, iron (ferrous), nitrate, sulfate, sulfide, TOC, and
volatile fatty acids (Table 2). These parameters were detected in one or more groundwater samples
collected from the monitoring wells. Many of these parameters do not have established groundwater
standards. Of the parameters that do have established groundwater standards, none of the
parameters exceeded their respective standard. An in-depth analysis of the MNA parameters that
apply to the Site’s COCs was performed in the first Five-Year CAER (Altamont 2016). The first
Five-Year CAER concluded that MNA data provides evidence that both reductive degradation and
aerobic degradation is occurring in different portions of the Site.

Spring 2017 Semiannual
Water Quality Monitoring Report 10 June 2017
3.1.2 Surface Water
The following sections summarize measured field parameters and analytical results associated with
the two surface water samples collected during the spring 2017 sampling event.
3.1.2.1 Field Parameters
The pH readings for the upstream and downstream surface water samples collected during the
spring 2017 sampling event were recorded at 7.09 SU and 7.20 SU, respectively. The measured pH
reading for both surface water samples was within the 2B standard range of 6.0 to 9.0 SU.
Turbidity measured in SW-01 and SW-02 was below the 2B standard, which is established at 25 NTU
for the receiving water in streams not designated as trout waters.
DO was measured at a concentration of 10.86 mg/L in SW-01 and 8.28 mg/L in SW-02. The 2B
standard indicates “greater than or equal to 5.0 mg/L”; thus, each sample is within the acceptable DO
range.
Specific conductivity concentrations in surface water samples SW-01 and SW-02 were recorded at
32 µS/cm and 31 µS/cm, respectively. Oxidation reduction potential values for SW-01 and SW-02
were recorded at 224.5 mV and 203.2 mV. Concentrations of specific conductivity and oxidation
reduction potential are consistent with historical data in both surface water samples. 2B standards do
not exist for these parameters.
3.1.2.2 Appendix I Metals
Zinc was detected above the SWSL in SW-02, but below the 2B standard. Copper (2.9 J µg/L) and
lead (0.65 J µg/L) were detected at a concentration above their respective 2B surface water
standards, but below their SWSLs, in surface water sample SW-02. This is the first sampling event
that these metals have exceeded their 2B standards in the downstream surface water sample;
however, these metals have been detected consistently at various concentrations, upstream and
downstream of the landfill, according to historical data.
3.1.2.3 Appendix I VOCs
No VOCs were detected at concentrations above their respective MDLs in either the upstream or
downstream surface water samples (Table 2).
3.1.3 Leachate
Nine VOCs were detected in the leachate sample (Tables 2 and 3). Four of the detected VOCs
(1,4-dichlorobenzene, benzene, chlorobenzene, and ethylbenzene) were reported at concentrations
above their respective SWSLs.

Spring 2017 Semiannual
Water Quality Monitoring Report 11 June 2017
On September 1, 2012, leachate extraction was initiated following installation of the leachate
extraction pumps in the 10 landfill gas extraction wells. Between October 11, 2016 and March 21,
2017 approximately 3,202 gallons of leachate were discharged through a permanent connection to
the TWSA (Table 3). From September 1, 2012 to March 21, 2017 a total of approximately 334,212
gallons of leachate have been extracted and/or discharged from the landfill (Table 3).
In fall 2013 the active portion of the approved corrective action remedy was initiated. Based on the
leachate sample analytical results collected on March 21, 2017, Anchor QEA estimates that 0.00241
pounds of VOCs were removed with the extracted leachate between the October 2016 and the
March 2017 sampling events. Mass removal calculations are included in Table 3.
3.2 Groundwater Flow Direction
Groundwater levels in the saprolite2, partially weathered rock3 (PWR), and bedrock4 are monitored at
the closed MSWLF. Three bedrock monitoring wells, MW-01, MW-02, and MW-06, are located in the
northern and northwestern portions of the Site (Figure 3 and Table 4). Bedrock monitoring well
(MW-07) is located southwest of the landfill (Figure 3). The spring 2017 water level data collected
from these four bedrock wells (Table 4) were used to determine generalized bedrock groundwater
flow direction, which is to the southwest (Figure 3).
PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are
located in the central, southwest, and southern parts of the landfill, respectively. The spring 2017
water level data collected from monitoring wells MW-03, MW-04, and MW-05R (Table 4) indicate
that groundwater flow direction in the saprolite and PWR is also generally to the southwest, toward
the Tuckasegee River (Figure 3).

2 Saprolite is the result of in-place weathering to produce soil-like material that retains relict features of the parent rock.
3 PWR is rock generally found above the bedrock and is softer than the bedrock but not as soft as saprolite.
4 Bedrock is solid rock that underlies loose soil and saprolite.

Spring 2017 Semiannual
Water Quality Monitoring Report 12 June 2017
4 Summary
The first semiannual water quality monitoring event of 2017 was performed on March 21 and 22,
2017 at the Jackson County closed MSWLF. Table 2 of this report and the Reports of Laboratory
Analysis (Appendix B) provide detailed analytical results and field data summarizing the groundwater
and surface water quality at the landfill.
4.1 Groundwater Quality
4.1.1 Metals
Fourteen metals were detected in the groundwater samples collected from one or more of the
monitoring wells. Seven of the detected metals (barium, cadmium, chromium, cobalt, copper,
selenium, and zinc) were detected at concentrations above the associated SWSLs in one or more
monitoring wells (Table 2).
Five metals (cadmium, chromium, cobalt, thallium, and vanadium) were detected at concentrations
above their associated groundwater quality standards in one or more of the monitoring wells
(Table 2). Cobalt exceeded its 2L standard in all of the collected groundwater samples, with the
exception of MW-07. These results are consistent with historical data.
4.1.2 VOCs
Nine VOCs were detected in the groundwater samples collected from one or more of the monitoring
wells (Table 2). Seven VOCs (1,1-dichloroethane, 1,4-dichlorobenzene, benzene, chlorobenzene,
cis-1,2-dichloroethene, trichloroethylene, and vinyl chloride) were detected at concentrations above
their respective SWSLs (Table 2).
Four VOCs (1,4-dichlorobenzene, benzene, tetrachloroethene, and vinyl chloride) were detected at
concentrations above their respective 2L standards (Table 2). Concentration-versus-time graphs were
created for samples from those monitoring wells that had VOC concentrations over their 2L
standards. The graphs are provided as Figures 4 through 11 and summarized in Section 3.1.1.3.
4.1.3 Field Parameters and Other Constituents
Six of the samples collected from the monitoring wells had pH readings that were recorded outside
of the 2L standard range for pH (6.5 SU to 8.5 SU). These results are consistent with historical data
and are characteristic of the natural groundwater quality of the region.
Measured turbidity readings ranged from 0.32 NTUs in monitoring well MW-03 to 136 NTUs in
monitoring well MW-05R.

Spring 2017 Semiannual
Water Quality Monitoring Report 13 June 2017
Natural attenuation parameters (alkalinity, BOD, COD, chloride, carbon dioxide, hydrogen, ferrous
iron, methane, nitrate, sulfate, and TOC) were detected in groundwater samples collected from one
or more of the monitoring wells at various concentrations. Natural attenuation parameters are being
obtained as part of the CAP and further evaluation of these parameters will be performed in future
monitoring events. The next Five-Year CAER will be submitted in the Fall of 2021.
4.2 Surface Water Quality
Nine metals were detected in both surface water samples SW-01 (upstream of the landfill) and
SW-02 (downstream of the landfill) during the spring 2017 water quality monitoring event.
Concentrations of copper and lead in surface water sample SW-02 exceeded their respective 2B
surface water standards, but were reported at concentrations below their respective SWSLs. Zinc was
reported at a concentration above its SWSL, but below its 2B standard, in surface water sample
SW-02. The remaining detected metals were reported at concentrations below their respective
SWSLs and 2B surface water standards.
No VOCs were detected in either surface water sample location.
On the basis of these data, the groundwater migrating from the landfill toward the Tuckasegee River
is not impacting surface water quality with regard to metals and VOCs.
Field parameters including pH, turbidity, and dissolved oxygen measured in both surface water
samples were within the 2B standards established for these parameters.
4.3 Leachate Quality
The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for
Appendix I VOCs only. Nine VOCs were detected in the leachate sample (Tables 2 and 3). Water
quality standards do not exist for leachate. Since leachate extraction began, a total of approximately
334,212 gallons of leachate have been extracted from the landfill (Table 3). Anchor QEA estimates
that 0.00241 pounds of VOCs were removed with the extracted leachate between the October 2016
and the March 2017 sampling events.

Spring 2017 Semiannual
Water Quality Monitoring Report 14 June 2017
5 Future Activities
Anchor QEA will continue to monitor the water quality on a semiannual basis at the Jackson County
Closed Municipal Solid Waste landfill. During the fall of 2017, domestic well owners will be contacted
and groundwater samples will be collected from domestic wells if permitted to do so by the well
owner and if possible to do so based upon well pump operability. Domestic well samples will be
analyzed for VOCs only. Samples will be collected from monitoring wells, surface water monitoring
points, and the leachate flow equalization tank during the spring and fall of each year. In addition to
the natural attenuation parameters that were added as part of the approved corrective action, the
analytical suites associated with the current and future sampling events are outlined in the 2011 CAP
and recently submitted Five-Year CAER. The upcoming sampling event parameters are as follows:
Sampling Event Analytical Suite (not inclusive of natural attenuation parameters)
Fall 2017
Appendix II VOCs
Appendix II metals
Appendix II SVOCs
Cyanide and sulfide
Spring 2018
Appendix I VOCs
Appendix I Metals
Cyanide and sulfide

The next sampling event is scheduled for October 2017.

Spring 2017 Semiannual
Water Quality Monitoring Report 15 June 2017
6 References
Altamont (Altamont Environmental, Inc.), 2010. Assessment of Corrective Measures. September 7,
2010.
Altamont, 2011. Corrective Action Plan. June 30, 2011.
Altamont, 2016. Five-Year Corrective Action Evaluation Report. October 31, 2016.
DENR DWM SWS (North Carolina Department of Environment and Natural Resources Division of
Waste Management Solid Waste Section, 2006. Memorandum to SW Director/County
Manager/ Consultant/Laboratory, Re: New Guidelines for Electronic Submittal of Environmental
Monitoring Data. October 27, 2006.
DENR DWM SWS, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding New
Guidelines for Electronic Submittal of Environmental Data. February 23, 2007.
DENR DWM SWS. Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling,
Rev 4-08.
DENR DWM SWS, 2011. Approval of the County’s Corrective Action Plan. September 1, 2011.
EPA (U.S. Environmental Protection Agency), 1996. Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures. OSWER, EPA/540/S-95/504.
EPA, revised 2013. SESD Operating Procedure: Groundwater Sampling. March 6, 2013.

Tables
Table 1
Summary of Laboratory Analyses Performed on Samples
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 1 of 1
June 2017
GROUNDWATER SAMPLES SURFACE WATER, LEACHATE, DOMESTIC WELL, AND QUALITY CONTROL SAMPLES
Metals Mercury VOCs Metals VOCs Mercury
Sample
Name
Date
Collected Sample Name Date
Collected
MW-01 03/21/2017 X X X SW-01 03/22/2017 X X X
MW-02 03/22/2017 X X X SW-02 03/22/2017 X X X
MW-03 03/21/2017 X X X LT-01 03/21/2017 X
MW-04 03/22/2017 X X X TripBlank (1)03/21/2017 X
MW-05R 03/22/2017 X X X TripBlank (2)03/22/2017 X
MW-06 03/21/2017 X X X TripBlank (LT01)03/21/2017 X
MW-07 03/22/2017 X X X
GROUNDWATER SAMPLES
Total
Alkalinity to
pH 4.5
BOD COD Cyanide Volatile Fatty
Acids Ferrous Iron Nitrate as N Chloride Sulfate TOC Sulfide
Ethane,
Ethene,
Methane
Hydrogen Carbon
Dioxide
Sample
Name
Date
Collected
MW-01 03/21/2017 X X X X X X X X X X X X X
MW-02 03/22/2017 X X X X X X X X X X X X X
MW-03 03/21/2017 X X X X X X X X X X X X X X
MW-04 03/22/2017 X X X X X X X X X X X X X X
MW-05R 03/22/2017 X X X X X X X X X X X X X
MW-06 03/21/2017 X X X X X X X X X X X X X X
MW-07 03/22/2017 X X X X X X X X X X X X X X
Notes:
VOCs volatile organic compounds
BOD biochemical oxygen demand
COD chemical oxygen demand
TOC total organic carbon
Analyses Appendix I constituents were analyzed per Title 40 Code of Federal Regulations (CFR) Part 258.Blank cell Analysis was not performed on that sample.
AM20GAXEPA 9056A
EPA 6020B
SM 4500-S FSM 3500-Fe D
EPA 8260B EPA 7470A
AM23G SM 9060A
Analysis
Analysis
Analysis
EPA 7470AEPA 6020B EPA 8260B
Natural Attenuation Parameters
SM 2320B SM 5210B SM 5220D SM 4500-CN-
E
Table 2
Summary of Analytical Results
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 1 of 3
June 2017
Metals
402
EPA 6020B, 7470A
Parameter
ArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadNickelSeleniumSilver ThalliumVanadiumZincCAS Number 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7782-49-2 7440-22-4 7440-28-0 7440-62-2 7440-66-6
SWS ID 14 15 23 34 51 53 54 131 152 183 184 194 209 213
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Sample Name Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Groundwater Samples
MW-01 03/21/2017 0.45 U 120 0.092 J 2.3 0.67 J 150 8.1 J 0.66 J 15 J 0.45 U 0.067 U 1.2 J 0.79 U 95 B
MW-02 03/22/2017 2.9 J 120 0.33 J 0.11 J 12 31 16 4.3 J 9.6 J 12 0.067 U 0.31 J 20 J 41 B
MW-03 03/21/2017 0.45 U 170 0.096 J 0.32 J 0.73 J 59 1.7 J 0.27 J 8.2 J 0.45 U 0.067 U 0.19 J 0.79 U 11 B
MW-04 03/22/2017 0.45 U 84 J 0.073 J 0.26 J 1.3 J 2.8 J 1.0 J 0.29 J 2.2 J 0.76 J 0.81 J 0.19 J 0.79 U 7.3 J, B
MW-05R 03/22/2017 0.53 J 180 0.12 J 1.4 2.4 J 18 4.2 J 0.90 J 6.7 J 0.98 J 0.067 U 0.10 J 2.7 J 16 B
MW-06 03/21/2017 0.45 U 81 J 0.12 J 0.22 J 1.4 J 91 2.7 J 0.37 J 26 J 0.71 J 0.067 U 0.84 J 0.79 U 31 B
MW-07 03/22/2017 0.45 U 490 0.068 U 0.14 J 0.63 J 0.93 J 1.4 J 0.50 J 7.6 J 0.45 U 0.067 U 0.072 J 0.79 U 13 B
Leachate Sample
LT-01 03/21/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA NA
Surface Water Samples
SW-01 03/22/2017 0.45 U 21 J 0.068 U 0.053 U 0.85 J 0.32 J 1.9 J 0.46 J 0.86 J 0.45 U 0.067 U 0.062 J 1.1 J 7.4 J, B
SW-02 03/22/2017 0.45 U 17 J 0.068 U 0.053 U 0.64 J 0.24 J 2.9 J 0.65 J 1.0 J 0.45 U 0.067 U 0.050 J 0.79 U 11 B
Quality Control Samples
TripBlank (1)03/21/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA NA
TripBlank (2)03/22/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA NA
TripBlank (LT01)03/21/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA NA
MDL 0.45 0.12 0.068 0.053 0.32 0.056 0.41 0.061 0.082 0.45 0.067 0.018 0.79 1.30
MRL 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 2.0 5.0 5.0 1.0 1.0 10
SWSL 10 100 1 1 10 10 10 10 50 10 10 5.5 25 10
2L 10 700 NE 2 10 NE 1,000 15 100 20 20 NE NE 1,000
IMAC NE NE 4 NE NE 1 NE NE NE NE NE 0.2 0.3 NE
GWPS NE NE 4 NE NE 1 NE NE NE NE NE 0.28 0.3 NE
2B 10 200,000 6.5 0.15 35 4 2.7 0.54 16 5 0.06 0.47 NE 36
Notes:
Lab Method The analytical method used to analyze the constituents.
Cas Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID Solid Waste Section Identification Number.
Units
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Anchor QEA.
MDL Method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL Method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in the associated laboratory blank at a concentration greater than one-half of the report limit.
2L
IMAC Interim Maximum Allowable Concentration, analytes that do not have an established 2L standard were compared to the IMAC in accordance with 15A NCAC 02L .0202 [c].
GWPS
2B
100 Indicates a detection with a result at or exceeding the SWSL.
180 Shaded cell indicates result in exceedance of the 2L or IMAC standard or greater than or equal to the GWPS (if no 2L or IMAC exist), and 2B standard if applicable.
NA Not analyzed.
NE Not established.
Lab Certification
Lab Method
Laboratory and
Regulatory Thresholds
Surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards," (last amended
June 2016). Where no 2B standard exists, the National Criteria per Environmental Protection Agency (EPA) from standards Table (Current as of May 15, 2013) for the most stringent of
fresh water and human health was used.
Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-list (last updated June, 2011).
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ
(Amended April 1, 2013).
Micrograms per liter (µg/L) and milligrams per liter (mg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, microsiemens per
centimeter (µS/cm) for specific conductivity, degrees celcius (°C) for temperature, and millivolts (mV) for oxidation reduction potential.
Table 2
Summary of Analytical Results
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 2 of 3
June 2017
Parameter
CAS Number
SWS ID
Units
Sample Name Collect Date
Groundwater Samples
MW-01 03/21/2017
MW-02 03/22/2017
MW-03 03/21/2017
MW-04 03/22/2017
MW-05R 03/22/2017
MW-06 03/21/2017
MW-07 03/22/2017
Leachate Sample
LT-01 03/21/2017
Surface Water Samples
SW-01 03/22/2017
SW-02 03/22/2017
Quality Control Samples
TripBlank (1)03/21/2017
TripBlank (2)03/22/2017
TripBlank (LT01)03/21/2017
MDL
MRL
SWSL
2L
IMAC
GWPS
2B
Lab Certification
Lab Method
Laboratory and
Regulatory Thresholds
Field Parameters Volatile Organic Compounds (VOCs)
5445 (pH only)402
EPA 8260B
TemperatureDissolved OxygenpHTurbiditySpecific ConductivityOxidation Reduction Potential1,1-Dichloroethane1,4-DichlorobenzeneAcetoneBenzeneChlorobenzenecis-1,2-DichloroetheneEthylbenzenem & p Xyleneo-XyleneTetrachloroetheneTetrahydrofuranTrichloroethyleneVinyl ChlorideXylene (Total)SW325 7782-44-7 SW320 SW330 SW323 SW336 75-34-3 106-46-7 67-64-1 71-43-2 108-90-7 156-59-2 100-41-4 108-38-3/106-42-3 95-47-6 127-18-4 109-99-9 79-01-6 75-01-4 1330-20-7
325 356 320 330 323 336 75 71 3 16 39 78 110 359 408 192 458 201 211 346
°C mg/L SU NTU µS/cm mV µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
25.61 1.70 5.77 8.78 220 39.7 5.1 12 8.8 J 1.8 3.1 8.8 0.061 U 0.12 U 0.044 U 0.99 J 0.16 U 1.1 0.097 U 0.15 U
17.62 6.24 6.62 37.9 198 203.3 0.80 J 0.050 U 0.31 U 0.048 U 0.062 U 1.4 J 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
17.43 1.59 5.58 0.32 289 259.5 2.2 J 12 0.31 U 0.57 J 7.4 3.8 J 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
14.12 2.86 5.75 0.36 562 210.5 0.083 U 5.7 0.31 U 0.90 J 4.3 6.2 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
14.52 4.51 6.37 136 591 -5.3 0.083 U 10 0.31 U 1.8 8.4 10 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 1.3 0.15 U
14.74 3.44 5.63 3.46 108 121.0 4.4 J 4.9 11 J 0.69 J 0.79 J 4.5 J 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
15.04 1.12 6.03 6.47 588 134.2 0.083 U 5.5 0.31 U 1.6 6.3 4.5 J 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
24.83 5.12 7.00 28.0 4120 -62.0 0.083 U 4.6 9.4 J 1.5 4.3 0.056 U 1.4 0.58 J 0.92 0.098 U 66 0.078 U 0.097 U 1.5 J
11.53 10.86 7.09 11.2 32 224.5 0.083 U 0.050 U 0.31 U 0.048 U 0.062 U 0.056 U 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
13.15 8.28 7.20 14.8 31 203.2 0.083 U 0.050 U 0.31 U 0.048 U 0.062 U 0.056 U 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
NA NA NA NA NA NA 0.083 U 0.050 U 0.31 U 0.048 U 0.062 U 0.056 U 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
NA NA NA NA NA NA 0.083 U 0.050 U 0.31 U 0.048 U 0.062 U 0.056 U 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
NA NA NA NA NA NA 0.083 U 0.050 U 0.31 U 0.048 U 0.062 U 0.056 U 0.061 U 0.12 U 0.044 U 0.098 U 0.16 U 0.078 U 0.097 U 0.15 U
NA NA NA NA NA NA 0.083 0.050 0.31 0.048 0.062 0.056 0.061 0.12 0.044 0.098 0.16 0.078 0.097 0.15
NA NA NA NA NA NA 0.50 0.50 5.0 0.50 0.50 0.50 0.50 1.0 0.50 0.50 10 0.50 0.50 3.0
NE NE NE NE NE NE 5 1 100 1 3 5 1 NE NE 1 NE 1 1 5
NE NE 6.5-8.5 NE NE NE 6 6 6,000 1 50 70 600 NE NE 0.7 NE 3 0.03 500
NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE > 5.0 6.0-9.0 25 NE NE 100 100 2,000 51 140 720 97 NE 600 3.3 NE 3 2.4 670
Notes:
Lab Method The analytical method used to analyze the constituents.
Cas Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID Solid Waste Section Identification Number.
Units
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Anchor QEA.
MDL Method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL Method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in the associated laboratory blank at a concentration greater than one-half of the report limit.
2L
IMAC Interim Maximum Allowable Concentration, analytes that do not have an established 2L standard were compared to the IMAC in accordance with 15A NCAC 02L .0202 [c].
GWPS
2B
100 Indicates a detection with a result at or exceeding the SWSL.
180 Shaded cell indicates result in exceedance of the 2L or IMAC standard or greater than or equal to the GWPS (if no 2L or IMAC exist), and 2B standard if applicable.
NA Not analyzed.
NE Not established.
Micrograms per liter (µg/L) and milligrams per liter (mg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, microsiemens per centimeter (µS/cm) for specific conductivity,
degrees celcius (°C) for temperature, and millivolts (mV) for oxidation reduction potential.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ (Amended April 1, 2013).
Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-
section/environmental-monitoring/environmental-monitoring-list (last updated June, 2011).
Surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards," (last amended June 2016). Where no 2B standard
exists, the National Criteria per Environmental Protection Agency (EPA) from standards Table (Current as of May 15, 2013) for the most stringent of fresh water and human health was used.
Table 2
Summary of Analytical Results
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 3 of 3
June 2017
Parameter
CAS Number
SWS ID
Units
Sample Name Collect Date
Groundwater Samples
MW-01 03/21/2017
MW-02 03/22/2017
MW-03 03/21/2017
MW-04 03/22/2017
MW-05R 03/22/2017
MW-06 03/21/2017
MW-07 03/22/2017
Leachate Sample
LT-01 03/21/2017
Surface Water Samples
SW-01 03/22/2017
SW-02 03/22/2017
Quality Control Samples
TripBlank (1)03/21/2017
TripBlank (2)03/22/2017
TripBlank (LT01)03/21/2017
MDL
MRL
SWSL
2L
IMAC
GWPS
2B
Lab Certification
Lab Method
Laboratory and
Regulatory Thresholds
Natural Attenuation Parameters
402, 618
SM2320B SM 5210B EPA 9056A SM 5220D SM 4500-CN-E SM 3500-Fe-D EPA 9056A EPA 9056A EPA 9060A AM23G
Total Alkalinity, to pH 4.5BODChlorideCODCyanideIron, FerrousNitrate as NSulfateTOCAcetic AcidMethaneEthaneEtheneCarbon DioxideHydrogen SW337 SW316 16887-00-6 SW317 57-12-5 NA SW303 14808-79-8 C-012 64-19-7 74-82-8 74-84-0 74-85-1 124-38-9 1333-74-0
337 316 301 317 58 334 303 315 357 NE 456 331 332 459 420
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L µg/L µg/L µg/L mg/L nM
Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
110,000 1,800 J 880 J 29,000 J 9.5 J 24,000 17 U 820 J 11,800 0.1 U 1,700 0.1 U 0.1 U 280 NA
51,000 2,000 U 29,000 300,000 4.4 J 71 U 390 J 13,000 J 8,500 J 0.13 0.5 U 0.1 U 0.1 U 59 NA
89,000 120 J 40,000 14,000 U 3.9 J 140 J 1,900 J, B 2,000 J 10,500 0.1 U 3.3 0.018 0.042 380 51
160,000 860 J 89,000 110,000 1.8 J 71 U 440 J 67,000 J 17,500 0.1 U 180 0.031 0.031 300 50
230,000 1,200 J 76,000 33,000 J 1.1 J 17,000 310 J 2,000 J 12,700 0.1 U 3,300 0.21 0.28 140 NA
52,000 920 J 1,100 1,400 U 3.1 J 4,500 77 J, B 950 J 9,600 0.1 U 11 0.1 U 0.13 270 29
260,000 120 J 71,000 1,400 U 1.0 U 290 91 J 23,000 J 9,000 0.1 U 340 0.15 0.22 350 9.6
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
770 NE 44 14,000 1.0 71/710 17 320 300/1,500 0.007 0.006/0.027 0.001/0.002 0.006/0.027 0.24/0.42 0.075/0.75
5,000 2,000 1,000 50,000 5.0 200/2,000 100 1,000 2,000/10,000 0.10 0.05/0.5 0.01/0.1 0.01/0.1 2.0/5.0 0.6/6.0
NE NE NE NE 10 NE 10,000 250,000 NE NE NE NE NE NE NE
NE NE 250,000 NE 70 300 10,000 250,000 NE NE NE NE NE NE NE
NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 230,000 NE 5 NE NE NE NE NE NE NE NE NE NE
Notes:
Lab Method The analytical method used to analyze the constituents.
Cas Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID Solid Waste Section Identification Number.
Units
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Anchor QEA.
MDL Method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL Method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in the associated laboratory blank at a concentration greater than one-half of the report limit.
2L
IMAC Interim Maximum Allowable Concentration, analytes that do not have an established 2L standard were compared to the IMAC in accordance with 15A NCAC 02L .0202 [c].
GWPS
2B
100 Indicates a detection with a result at or exceeding the SWSL.
180 Shaded cell indicates result in exceedance of the 2L or IMAC standard or greater than or equal to the GWPS (if no 2L or IMAC exist), and 2B standard if applicable.
NA Not analyzed.
NE Not established.
AM20GAX
Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-
guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-list (last updated June, 2011).
Surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards," (last amended June 2016). Where
no 2B standard exists, the National Criteria per Environmental Protection Agency (EPA) from standards Table (Current as of May 15, 2013) for the most stringent of fresh water and human health was used.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ
(Amended April 1, 2013).
Micrograms per liter (µg/L) and milligrams per liter (mg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, microsiemens per centimeter (µS/cm) for specific
conductivity, degrees celcius (°C) for temperature, and millivolts (mV) for oxidation reduction potential.
Table 3
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
1 of 4
June 2017
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
09/01/2012 10/25/2012 1,4-Dichlorobenzene 0.0034 11,500 11,500 0.00033
4-Methyl-2-
pentanone (MIBK)0.0021 J 0.00020
Acetone 0.0292 0.00280
Benzene 0.0021 0.00020
Chlorobenzene 0.0029 0.00028
cis-1,2-
Dichloroethene 0.00063 J 0.00006
Dichlorodifluoro-
methane 0.00093 J 0.00009
Ethylbenzene 0.0102 0.00098
Naphthalene 0.0069 0.00066
Styrene 0.00033 J 0.00003
Toluene 0.003 0.00029
Xylene (Total)0.0094 0.00090
Total 0.00682 0.00682
10/26/2012 04/11/2013 1,4-Dichlorobenzene 0.006 65,500 54,000 0.00270
Acetone 0.012 J 0.00540
Benzene 0.0011 0.00049
Carbon disulfide 0.0067 J 0.00301
Chlorobenzene 0.0024 J 0.00108
cis-1,2-
Dichloroethene 0.00058 J 0.00026
Ethylbenzene 0.0083 0.00373
Toluene 0.00059 J 0.00027
Xylene (Total)0.0078 0.00351
Total 0.02045 0.02727
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
Table 3
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
2 of 4
June 2017
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
04/12/2013 10/08/2013 1,4-Dichlorobenzene 0.0055 114,737 49,237 0.00226
4-Methyl-2-
pentanone (MIBK)0.0012 J 0.00049
Benzene 0.0020 0.00082
Chlorobenzene 0.0039 0.00160
cis-1,2-
Dichloroethene 0.00080 J 0.00033
Ethylbenzene 0.0151 0.00619
Naphthalene 0.0184 0.00754
Toluene 0.0012 0.00049
Xylene (Total)0.0090 0.00369
Total 0.02341 0.05068
10/09/2013 04/08/2014 1,4-Dichlorobenzene 0.0056 168,821 54,084 0.00252
Benzene 0.0018 0.00081
Chlorobenzene 0.0051 0.00230
cis-1,2-
Dichloroethene 0.00049 J 0.00022
Ethylbenzene 0.0047 0.00212
Toluene 0.00041 J 0.00018
Xylene (Total)0.0021 J 0.00095
Total 0.00910 0.05978
04/08/2014 10/23/2014 1,4-Dichlorobenzene 0.0053 179,652 10,831 0.00048
Benzene 0.0014 0.00013
Chlorobenzene 0.003 0.00027
cis-1,2-
Dichloroethene 0.00049 J 0.00004
Ethylbenzene 0.0027 0.00024
Toluene 0.00051 J 0.00005
Xylene (Total)0.0014 J 0.00013
Total 0.00133 0.06111
Table 3
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
3 of 4
June 2017
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
10/23/2014 04/21/2015
1,2,3-
Trimethylbenzene 0.00062 219,965 40,313 0.00021
1,2,4-
Trimethylbenzene 0.00076 0.00026
2-Chlorotoluene 0.00067 0.00022
1,4-Dichlorobenzene 0.0059 0.00198
Acetone 0.00790 0.00265
Benzene 0.0022 0.00074
Chlorobenzene 0.003 0.00101
Ethylbenzene 0.0056 0.00188
Isopropylbenzene 0.0013 0.00044
Methy Tert-butyl-
Ether 0.0013 0.00044
Napthalene 0.024 0.00806
n-Propylbenzene 0.00088 0.00030
Tetrahydrofuran 0.089 0.02988
Toluene 0.00054 J 0.00018
Vinyl Chloride 0.00038 J 0.00013
Xylene (Total)0.0030 J 0.00101
Total 0.04937 0.11048
04/21/2015 10/13/2015 1,4-Dichlorobenzene 0.00600 256,685 36,720 0.00183
2-Butanone 0.00960 J 0.00294
Benzene 0.00210 0.00064
Chlorobenzene 0.0040 0.00122
Ethylbenzene 0.00710 0.00217
m,p-Xylenes 0.0014 0.00043
Naphthalene 0.021 0.00642
o-Xylene 0.0017 0.00052
Tetrahydrofuran 0.062 0.01896
Toluene 0.00058 J 0.00018
Total Xylenes 0.0031 J 0.00095
Total 0.03626 0.14674
10/13/2015 04/05/2016 1,4-Dichlorobenzene 0.00590 315,663 58,978 0.00290
Benzene 0.00170 0.00083
Chlorobenzene 0.0038 0.00187
Ethylbenzene 0.00500 0.00246m,p-Xylenes 0.0010 0.00049
o-Xylene 0.0015 0.00074
Toluene 0.00063 J 0.00031
Total Xylenes 0.0025 J 0.00123
Total 0.01082 0.15756
Table 3
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
4 of 4
June 2017
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
04/05/2016 10/11/2016 331,010 15,347 0.00000
Total 0.00000 0.15756
10/11/2016 03/21/2017 1,4-Dichlorobenzene 0.0046 334,212 3,202 0.00012
Acetone 0.0094 J 0.00025
Benzene 0.0015 0.00004
Chlorobenzene 0.0043 0.00011
Ethylbenzene 0.0014 0.00004
m,p-Xylenes 0.0006 J 0.00002
o-Xylene 0.00092 0.00002
Tetrahydrofuran 0.066 0.00176
Total Xylenes 0.0015 J 0.00004
Total 0.00241 0.15997
Notes:
Detections Only detected VOCs in leachate sample LT-01 are included in the mass removal calculation.
Extraction Leachate extraction at the landfill initiated on September 1, 2012.
Volume Extraction volume measurements were recorded and provided by Jackson County staff.
Calculations
Cumulative Flow Interpolated between LT-01 Sample Dates.
Differential Flow Represents the total flow between the LT-01 Sample Dates.
Mass Removed
mg/L milligrams per liter.
J Indicates laboratory estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
October 2016 No VOCs were detected in the leachate sample collected during the October 2016 sampling event.
Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of
leachate quality until the next sampling event occurs, and that the leachate removal system has a 100% removal and treatment efficiency.
Mass Removed and Treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the
Concentration by the Differential Flow for the specified period.
Formula: ((concentration[mg/L])*(2.2e-6 lb)/(0.264 gal))*(Differential flow)
No detected compounds.
Table 4
Well Construction Details and Corresponding Elevations
Spring 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 1 of 1
June 2017
Date Drilled
Ground
Surface
Elevation
TOC
Elevation Stick Up Total Well
Depth
Depth To
Water
Groundwater
Elevation
Approx.
Depth to
Bedrock
Approx. Top
of Bedrock
Elevation
Depth to
Top of
Screened
Interval
Depth to
Bottom of
Screened
Interval
Top Elevation
of Screened
Interval
Elevation of
Bottom of
Screened
Interval
(mm/dd/yyyy)(feet)(feet)(feet
above gs) (feet bgs)(feet below
TOC) (feet)(feet bgs)(feet)(feet bgs)(feet bgs)(feet)(feet)
50-02 MW-01 04/23/1992 2,169.40 2,171.42 2.0 110.5 102.55 2,068.87 83.0 2,086.40 95.0 110.0 2,074.40 2,059.40 bedrock S&ME, Inc.
50-02 MW-02 04/22/1992 2,013.15 2,015.38 2.3 60.7 41.23 1,974.15 13.0 2,000.15 45.0 60.0 1,968.15 1,953.15 bedrock S&ME, Inc.
50-02 MW-03 04/21/1992 2,044.16 2,045.53 1.3 65.5 54.25 1,991.28 57.0 1,987.16 48.5 63.5 1,995.66 1,980.66
partially
weathered
bedrock
S&ME, Inc.
50-02 MW-04 04/21/1992 1,978.68 1,980.77 2.0 43.0 28.10 1,952.67 NA NA 25.0 40.0 1,953.68 1,938.68 saprolite S&ME, Inc.
50-02 MW-05R 01/26/2012 2,027.98 2,030.95 2.8 54.0 52.86 1,978.09 NA NA 44.0 54.0 1,983.98 1,973.98 saprolite
Altamont
Environmental,
Inc.
50-02 MW-06 03/23/2004 2,136.58 2,139.57 3.0 94.0 90.85 2,048.72 47.6 2,088.98 84.6 94.6 2,051.98 2,041.98 bedrock
50-02 MW-07 07/30/2010 1,978.71 1,981.29 2.6 95.0 32.68 1,948.61 44.0 1,935.00 70.0 95.0 1,908.71 1,883.71 bedrock
Notes:
Elevations
TOC top of casing
gs ground surface
bgs below ground surface
NA Not Applicable
Depth to Bedrock and
Screened Interval
Depth to Water Measured on March 21 and 22, 2017.
MW-05R
MW-01 through MW-04 Depth to Bedrock and Screened Interval taken from S&ME boring logs completed April 21, 22, and 23, 1992. MW-06 Depth to Bedrock and Screened Interval taken from Altamont boring log completed March 23, 2004. MW-07 Depth to
Bedrock and Screened Interval taken from Altamont boring log completed July 30, 2010. MW-05R Screened Interval taken from Altamont boring log completed January 26, 2012.
Monitoring well MW-05 was abandoned on January 26, 2012 by NYEG Drilling, LLC. Monitoring well MW-05R was installed on January 26, 2012 as a replacement to the well MW-05 by NYEG Drilling, LLC. The well MW-05R was surveyed by Wes Cole Land
Surveying, P.A. on September 28, 2012.
Facility Permit Well ID
Source of Well
Construction
Information
Geology of
Screened
Interval
Altamont
Environmental,
Inc.
Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level (msl) and are based on surveying completed by Davenport & Associates, Inc. Elevations associated with wells MW-05R and MW-07 are
measured relative to horizontal North American Datum (NAD) 83 and are based on surveying completed by Wes Cole Land Surveying, P.A.

Figures
[0 2,000 4,0001,000
Feet
LEGEND:
Site Parcel Boundary
Publish Date: 2017/06/05, 11:57 AM | User: alesueurFilepath: P:\Jackson County\Dillsboro GIS\MXD\2017\Spring Water Quality\Figure 1 Site Location Map AQ.mxd
Figure 1Site Location Map
Jackson County Closed MSW Landfill Water Quality ReportJackson County Closed MSW Landfill, Permit #50-02, Jackson County, NC
SOURCE(S):Basemap: USGS Topographic Maps - GreensCreek and Whittier 7.5 Minute QuadranglesParcels: Jackson County GIS
Anchor QEA of North Carolina, PLLC
#I#I"
!A !A !A
!A
!A
!A
!A !A
!A!A
@A@A
@A
@A
@A
@A @A
Flow Direction
25602
1
2
0
2060
20
20 222020802180
20802180
2120
25402080202
0
25202180
2080206 0
21802
0
4
0
20202120224021 2 0
21402160
2220
2480246020402 4 4 0
206024202080
2
38
02360 21602340
1960
1
9
6
0
2
1
4
0
2
0
6
0
2
1
2
0
2
0
4
020802320 1980
202
0
1
9
8
0216021802
2
8
0226022402220 214021 8 0
2160
SW-01
SW-02
LT-01 US 441S/US74 WH
AY
WO
O
D R
D
C
O
WEE T
U
N
N
EL R
D
DELLWOOD DRTUNNEL MOUNTAIN RD
GREEN ENERGY PARK RDHUNDREDACRE LNWHI
TE FAL
CON DRS US 441HARMONY HLMOODY RDS US 441WESTERN LNF U G IT IV E R U N
JOE WILKEY RD
MW-04
MW-07
MW-05R
MW-02
MW-03
MW-06 MW-01
[
0 500 1,000250
Feet
NOTE(S):1. Sample locations are approximate.2. Adjacent property owner name shownwithin their respective property boundary.
LEGEND:
@A Monitoring Well
!A Extraction Well
#ISurface Water Sample Location
"Leachate Sample Location
Road
Elevation Contour (20 ft Interval)
Property Boundary
Publish Date: 2017/06/05, 12:04 PM | User: alesueurFilepath: P:\Jackson County\Dillsboro GIS\MXD\2017\Spring Water Quality\Figure 2 Sample Location Map AQ.mxd
Figure 2Site Layout Map
Jackson County Closed MSW Landfill Water Quality Report
Jackson County Closed MSW Landfill, Permit #50-02, Jackson County, NC
SOURCE(S):Basemap: NC OneMap 2010Contours, Roads, and Parcels: Jackson County GIS
Anchor QEA of North Carolina, PLLC
!U
!U
!U !U
!U
!U
!U
Fl
o
w

D
i
r
e
c
t
i
o
n
20
0
0
21002300 22002
4
0
0
21002200Wilkey
Wilkey
Wilkey
Connor
TU
C
K
A
S
E
G
E
E

R
I
V
E
R
TU
C
K
A
S
E
G
E
E

R
I
V
E
R
TU
C
K
A
S
E
G
E
E

R
I
V
E
R
TU
C
K
A
S
E
G
E
E

R
I
V
E
R
GENERALIZED GROUNDWATER FLOW DIRECTIONMW-03
(1,991.28)
MW-04
(1,952.67)
MW-05R
(1,978.09)
MW-01
(2,068.87)
MW-06(2,048.72)
MW-02
(1,974.15)
MW-07
(1,948.61)
TU
N
N
E
L

M
O
U
N
T
A
I
N

R
D
JOE WILKEY RD
GREEN ENERGY PARK RDHA
Y
W
O
O
D

R
D
FUGITIVE RUN
HA
Y
W
O
O
D

R
D
2
0
4
0
20
6
0
1
9
8
0 20
8
0196021
2
0
2
1
4
0
224022
6
0
2
2
8
02320 2160
23402
3
6
0
2
3
8
0
2180
24202220
2020222020
2
0
216021
4
0
208021
6
0
21
8
0
206021202180[
0 200 400100
Feet
NOTES:1.Monitoring well locations are approximate.2.Groundwater elevations and flow direction are updated on a semiannual basis following sample collection events in April and October.3.Groundwater flow direction is based on groundwater elevations in monitoring wells MW-03, MW-04, and MW-05R. Direction is calculated based on depth to water measured on March 21 and 22, 2017.4.Last names of property owners are shown in parcels that border the landfill property.5.PWR = Partially weathered rock6.(1,991.28) = Groundwater elevation in feet
LEGEND:
!U PWR Monitoring Well
!U Saprolite Monitoring Well
!U Bedrock Monitoring Well
Groundwater Flow Direction
Stream
Property Boundary
Road
Elevation Contour (20 ft Interval)
Publish Date: 2017/03/24, 2:29 PM | User: alesueurFilepath: P:\Jackson County\Dillsboro GIS\MXD\2017\Spring Water Quality\Figure 3 Groundwater Elevation Map AQ.mxd
Figure 3Generalized Groundwater Flow Direction
Jackson County MSW Landfill Water Quality ReportJackson County Closed MSW Landfill, Permit #50-02, Dillsboro, North Carolina
SOURCES:Elevation contours, roads, and parcels: Jackson County GIS
Anchor QEA of North Carolina, PLLC
Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
Monitoring Well MW-01
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
15
17.8
<0.33
7.6
5.6 5.3
11.0
8.5
< 0.33
9.8
10.9
10
8.0
9.5 10
12.8
11
14
13
6.9
12
2060
2062
2064
2066
2068
2070
2072
2074
2076
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007 Oct, 2007 Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010 Oct, 2010 Apr, 2011 Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)1,4-Dichlorobenzene Concentration (μg/L) Sampling Date
1,4-Dichlorobenzene Groundwater Elevation
Notes:1. 2L Standard = 6 μg/L 2. "J" indicates result is estimated by laboratory3. "<" indicates result is less than method detection limit
Figure 5
Hydrograph and Benzene Concentration vs. Time
Monitoring Well MW-01
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
6.2 6.8
5.9 5.5 5.8
5.0 5.2
3.5
2.7 2.1 2.8
1.7 1.7
3.4 3.0 2.4
1.5 1.5
2.4
1.3 1.8
2060
2062
2064
2066
2068
2070
2072
2074
2076
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007 Oct, 2007 Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010 Oct, 2010 Apr, 2011 Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)Benzene Concentration (μg/L) Sampling Date
Benzene Groundwater Elevation
Notes:1. 2L Standard = 1 μg/L
2. "J" indicates result is estimated by laboratory3. "<" indicates result is less than method detection limit
Figure 6
Hydrograph and Tetrachloroethene Concentration vs. Time
Monitoring Well MW-01
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
1.6 1.6
<0.46 0.70 J 0.49 J 0.48 J 0.69 J <0.46 <0.460.78 J J0.78 J 0.68 J 0.77 J 0.60 J 0.67 J 0.67 J 0.44 J 0.85 J 0.79 J 1.2 1.1
2060
2062
2064
2066
2068
2070
2072
2074
2076
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007 Oct, 2007 Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010 Oct, 2010 Apr, 2011 Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)Tetrachloroethene Concentration (μg/L) Sampling Date
Tetrachloroethene Groundwater Elevation
Notes:1. 2L Standard = 0.7 μg/L 2. "J" indicates result is estimated by laboratory3. "<" indicates result is less than method detection limit
Figure 7
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
Monitoring Well MW-03
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
11
18.4
< 0.33
12.6
4.9
8.3
3.5
9.5
< 0.33
11.2
2.5
8.6
1.8
6.4
4.2
10.2
2
9.2
2.2
4.7
12
1984
1986
1988
1990
1992
1994
1996
1998
2000
2002
2004
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007Oct, 2007Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010Oct, 2010Apr, 2011Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet-relative)1,4-Dichlorobenzene Concentration (μg/L) Sampling Date
1,4-Dichlorobenzene Groundwater Elevation
Notes:
1. 2L Standard = 6 μg/L 2. "J" indicates result is estimated by laboratory3. "<" indicates result is less than method detection limit
Figure 8
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
Monitoring Well MW-05R
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
17
18.8
<0.33
16.2 15.9
13.1
12.1
13.9
<0.33 U
Not
Sampled
2.5
1.3 1.5
7.3 6.9
4.3
5.6
6.5 6.5
4.4
10
1970
1972
1974
1976
1978
1980
1982
1984
1986
1988
1990
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007Oct, 2007Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010Oct, 2010Apr, 2011Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)1,4-Dichlorobenzene Concentration (μg/L) Sampling Date
1,4-Dichlorobenzene Groundwater Elevation
Notes:
Constituent concentration after January 2012 was found in MW-05R. Constituent concentration before January 2012 was found in MW-05.Groundwater elevation in October 2011 was interpolated.
2L Standard = 6 μg/L "J" indicates result is estimated by laboratory"<" indicates result is less than method detection limit
Figure 9
Hydrograph and Benzene Concentration vs. Time
Monitoring Well MW-05R
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
1.9 1.6
0.56 J 1.2 1.0 1.2
2.0 1.8 1.5 Not
Sampled
1.3 1.3 1.5 2.0 2.2 1.5 1.4 1.9 1.9
0.82 J
1.8
1970
1972
1974
1976
1978
1980
1982
1984
1986
1988
1990
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007Oct, 2007Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010Oct, 2010Apr, 2011Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)Benzene Concentration (μg/L) Sampling Date
Benzene Groundwater Elevation
Notes:Constituent concentration after January 2012 was found in MW-05R.
Constituent concentration before January 2012 was found in MW-05.Groundwater elevation in October 2011 was interpolated.2L Standard = 1 μg/L
"J" indicates result is estimated by laboratory"<" indicates result is less than method detection limit
Figure 10
Hydrograph and Vinyl Chloride Concentration vs. Time
Monitoring Well MW-05R
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
< 0.58
1.4 0.93 J 0.78 J 0.99 J 0.93 J 1.5 1.6 1.1 Not
Sampled
0.82 J 0.62 J < 0.32
1.0
2.5 2.9
1.8 1.8 2.0
0.62 J 1.3
1970
1972
1974
1976
1978
1980
1982
1984
1986
1988
1990
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007Oct, 2007Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010Oct, 2010Apr, 2011Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)Vinyl Chloride Concentration (μg/L) Sampling Date
Vinyl Chloride Groundwater Elevation
Notes:Constituent concentration after January 2012 was found in MW-05R. Constituent concentration before January 2012 was found in MW-05.Groundwater elevation in October 2011 was interpolated.2L Standard = 0.03 μg/L
"J" indicates result is estimated by laboratory"<" indicates result is less than method detection limit
Figure 11
Hydrograph and Benzene Concentration vs. Time
Monitoring Well MW-07
Spring 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill June 2017
1.1 1.1 1.4 1.4 1.7 1.4 1.3 1.1 1.2 1.7 1.6 0.87 J 1.6
1940
1942
1944
1946
1948
1950
1952
0
2
4
6
8
10
12
14
16
18
20
Apr, 2011Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Groundwater Elevation (feet)Benzene Concentration (μg/L) Sampling Date Benzene Groundwater Elevation
Notes:1. 2L Standard = 1 μg/L
2. "J" indicates result is estimated by laboratory3. "<" indicates result is less than method detection limit

Appendix A
Well Sampling Logs and Equipment
Documentation & Instrument Calibration
Data Sheets

Appendix B
Reports of Laboratory Analysis, Chain-of-
Custody Documentation, and Certificates
of Analysis
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/18/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill (Permit 50-02)
Project No.: 50-02
Lab Submittal Date: 03/22/2017
Prism Work Order: 7030361
This is a Revised Report and supercedes the original laboratory report data 4/11/17. Mercury has been
added.
TOC analysis was subcontracted to GCAL. Dissolved Hydrogen, Methane, Ethane, Ethene and Volitle
Fatty Acid analyses subcontracted to Microseeps/Pace. Laboratory reports are attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
MI Matrix spike outside of the control limits. Matrix interference suspected.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 58
Sample Receipt Summary
04/18/2017
Prism Work Order: 7030361
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030361-01 03/21/17MW-01 03/22/17Water
7030361-02 03/21/17MW-03 03/22/17Water
7030361-03 03/21/17MW-06 03/22/17Water
7030361-04 03/21/17Trip Blank 03/22/17Water
Samples were received in good condition at 1.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 58
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030361
04/18/2017
Summary of Detections
880 J ug/L7030361-01 MW-01 Chloride 9056A
820 J ug/L7030361-01 MW-01 Sulfate 9056A
1800 J ug/L7030361-01 MW-01 Biochemical Oxygen Demand SM5210 B
29000 J ug/L7030361-01 MW-01 Chemical Oxygen Demand SM5220 D
9.5 ug/L7030361-01 MW-01 Cyanide SM4500-CN E
24000 ug/L7030361-01 MW-01 Ferrous Iron SM3500-Fe D
110000 ug/L7030361-01 MW-01 Total Alkalinity to pH 4.5 SM2320 B
120 ug/L7030361-01 MW-01 Barium 6020B
0.092 J ug/L7030361-01 MW-01 Beryllium 6020B
2.3 ug/L7030361-01 MW-01 Cadmium 6020B
0.67 J ug/L7030361-01 MW-01 Chromium 6020B
150 ug/L7030361-01 MW-01 Cobalt 6020B
8.1 ug/L7030361-01 MW-01 Copper 6020B
0.66 J ug/L7030361-01 MW-01 Lead 6020B
15 ug/L7030361-01 MW-01 Nickel 6020B
1.2 ug/L7030361-01 MW-01 Thallium 6020B
95 BH, B ug/L7030361-01 MW-01 Zinc 6020B
5.1 ug/L7030361-01 MW-01 1,1-Dichloroethane 8260B
12 ug/L7030361-01 MW-01 1,4-Dichlorobenzene 8260B
8.8 ug/L7030361-01 MW-01 Acetone 8260B
1.8 ug/L7030361-01 MW-01 Benzene 8260B
3.1 ug/L7030361-01 MW-01 Chlorobenzene 8260B
8.8 ug/L7030361-01 MW-01 cis-1,2-Dichloroethylene 8260B
0.99 ug/L7030361-01 MW-01 Tetrachloroethylene 8260B
1.1 ug/L7030361-01 MW-01 Trichloroethylene 8260B
40000 ug/L7030361-02 MW-03 Chloride 9056A
1900 B ug/L7030361-02 MW-03 Nitrate as N 9056A
2000 ug/L7030361-02 MW-03 Sulfate 9056A
120 J ug/L7030361-02 MW-03 Biochemical Oxygen Demand SM5210 B
3.9 J ug/L7030361-02 MW-03 Cyanide SM4500-CN E
140 J ug/L7030361-02 MW-03 Ferrous Iron SM3500-Fe D
89000 ug/L7030361-02 MW-03 Total Alkalinity to pH 4.5 SM2320 B
170 ug/L7030361-02 MW-03 Barium 6020B
0.096 J ug/L7030361-02 MW-03 Beryllium 6020B
0.32 J ug/L7030361-02 MW-03 Cadmium 6020B
0.73 J ug/L7030361-02 MW-03 Chromium 6020B
59 ug/L7030361-02 MW-03 Cobalt 6020B
1.7 J ug/L7030361-02 MW-03 Copper 6020B
0.27 J ug/L7030361-02 MW-03 Lead 6020B
8.2 ug/L7030361-02 MW-03 Nickel 6020B
0.19 J ug/L7030361-02 MW-03 Thallium 6020B
11 B ug/L7030361-02 MW-03 Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 58
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030361
04/18/2017
Summary of Detections
2.2 ug/L7030361-02 MW-03 1,1-Dichloroethane 8260B
12 ug/L7030361-02 MW-03 1,4-Dichlorobenzene 8260B
0.57 ug/L7030361-02 MW-03 Benzene 8260B
7.4 ug/L7030361-02 MW-03 Chlorobenzene 8260B
3.8 ug/L7030361-02 MW-03 cis-1,2-Dichloroethylene 8260B
1100 ug/L7030361-03 MW-06 Chloride 9056A
77 J, B ug/L7030361-03 MW-06 Nitrate as N 9056A
950 J ug/L7030361-03 MW-06 Sulfate 9056A
920 J ug/L7030361-03 MW-06 Biochemical Oxygen Demand SM5210 B
3.1 J ug/L7030361-03 MW-06 Cyanide SM4500-CN E
4500 ug/L7030361-03 MW-06 Ferrous Iron SM3500-Fe D
52000 ug/L7030361-03 MW-06 Total Alkalinity to pH 4.5 SM2320 B
81 ug/L7030361-03 MW-06 Barium 6020B
0.12 J ug/L7030361-03 MW-06 Beryllium 6020B
0.22 J ug/L7030361-03 MW-06 Cadmium 6020B
1.4 ug/L7030361-03 MW-06 Chromium 6020B
91 ug/L7030361-03 MW-06 Cobalt 6020B
2.7 J ug/L7030361-03 MW-06 Copper 6020B
0.37 J ug/L7030361-03 MW-06 Lead 6020B
26 ug/L7030361-03 MW-06 Nickel 6020B
0.71 J ug/L7030361-03 MW-06 Selenium 6020B
0.84 J ug/L7030361-03 MW-06 Thallium 6020B
31 B ug/L7030361-03 MW-06 Zinc 6020B
4.4 ug/L7030361-03 MW-06 1,1-Dichloroethane 8260B
4.9 ug/L7030361-03 MW-06 1,4-Dichlorobenzene 8260B
11 ug/L7030361-03 MW-06 Acetone 8260B
0.69 ug/L7030361-03 MW-06 Benzene 8260B
0.79 ug/L7030361-03 MW-06 Chlorobenzene 8260B
4.5 ug/L7030361-03 MW-06 cis-1,2-Dichloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-01
Prism Work Order: 7030361
Time Collected: 03/21/17 12:03
Time Submitted: 03/22/17 09:30
MW-01
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0386110003/22/17 16:05 EGCJug/L 44ChlorideNE880
9056A P7C038611003/22/17 16:05 EGCug/L 17Nitrate as N 10000<17
9056A P7C0386110003/22/17 16:05 EGCJug/L 320Sulfate250000820
General Chemistry Parameters
SM5210 B P7C0368120003/22/17 12:39 SLSJug/LBiochemical Oxygen Demand NE1800
SM5220 D P7C03761500003/23/17 9:25 BMSJug/L 14000Chemical Oxygen Demand NE29000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCug/L 1.0Cyanide109.5
SM3500-Fe D P7C03661020003/22/17 10:00 BMSug/L 710Ferrous Iron NE24000
SM4500-S F P7C0397120003/23/17 15:30 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 12:20 EGCug/L 770Total Alkalinity to pH 4.5 NE110000
Total Metals
7470A P7D025510.20 4/18/17 12:00 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:13 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:13 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:13 bgmug/L 0.12Barium100120
6020B P7D002611.0 4/5/17 14:13 bgmJug/L 0.068Beryllium10.092
6020B P7D002611.0 4/5/17 14:13 bgmug/L 0.053Cadmium12.3
6020B P7D002611.0 4/5/17 14:13 bgmJug/L 0.32Chromium100.67
6020B P7D002611.0 4/5/17 14:13 bgmug/L 0.056Cobalt10150
6020B P7D002615.0 4/5/17 14:13 bgmug/L 0.41Copper108.1
6020B P7D002611.0 4/5/17 14:13 bgmJug/L 0.061Lead100.66
6020B P7D002612.0 4/5/17 14:13 bgmug/L 0.082Nickel5015
6020B P7D002615.0 4/5/17 14:13 bgmug/L 0.45Selenium10<0.45
6020B P7D002615.0 4/5/17 14:13 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:13 bgmug/L 0.018Thallium5.51.2
6020B P7D002611.0 4/5/17 14:13 bgmug/L 0.79Vanadium25<0.79
6020B P7D00261104/5/17 14:13 bgmBH,
B
ug/L 1.3Zinc1095
Volatile Organic Compounds by GC/MS
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0831,1-Dichloroethane 55.1
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C050211.0 3/30/17 16:58 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C050212.0 3/30/17 16:58 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-01
Prism Work Order: 7030361
Time Collected: 03/21/17 12:03
Time Submitted: 03/22/17 09:30
MW-01
50-02
SWSL
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.0501,4-Dichlorobenzene 112
8260B P7C050215.0 3/30/17 16:58 KDMug/L 0.31Acetone1008.8
8260B P7C05021203/30/17 16:58 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.048Benzene11.8
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C050211.0 3/30/17 16:58 KDMug/L 0.040Bromoform3<0.040
8260B P7C050211.0 3/30/17 16:58 KDMug/L 0.18Bromomethane10<0.18
8260B P7C050215.0 3/30/17 16:58 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.062Chlorobenzene33.1
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.22Chloroethane10<0.22
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.076Chloroform5<0.076
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.079Chloromethane1<0.079
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.056cis-1,2-Dichloroethylene 58.8
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C050211.0 3/30/17 16:58 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C050215.0 3/30/17 16:58 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C050215.0 3/30/17 16:58 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C050215.0 3/30/17 16:58 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C050215.0 3/30/17 16:58 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C050211.0 3/30/17 16:58 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.047Styrene1<0.047
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.098Tetrachloroethylene10.99
8260B P7C05021103/30/17 16:58 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.044Toluene1<0.044
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05021103/30/17 16:58 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-01
Prism Work Order: 7030361
Time Collected: 03/21/17 12:03
Time Submitted: 03/22/17 09:30
MW-01
50-02
SWSL
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.078Trichloroethylene11.1
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C050212.0 3/30/17 16:58 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C050210.50 3/30/17 16:58 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C050213.0 3/30/17 16:58 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-129108 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-02
Prism Work Order: 7030361
Time Collected: 03/21/17 13:48
Time Submitted: 03/22/17 09:30
MW-03
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0386110003/22/17 15:49 EGCug/L 44ChlorideNE40000
9056A P7C038611003/22/17 15:49 EGCBug/L 17Nitrate as N 100001900
9056A P7C0386110003/22/17 15:49 EGCug/L 320Sulfate2500002000
General Chemistry Parameters
SM5210 B P7C0368120003/22/17 12:39 SLSJug/LBiochemical Oxygen Demand NE120
SM5220 D P7C03761500003/23/17 9:25 BMSug/L 14000Chemical Oxygen Demand NE<14000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCJug/L 1.0Cyanide103.9
SM3500-Fe D P7C036612003/22/17 10:00 BMSJug/L 71Ferrous Iron NE140
SM4500-S F P7C0397120003/23/17 15:30 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 12:20 EGCug/L 770Total Alkalinity to pH 4.5 NE89000
Total Metals
7470A P7D025510.20 4/18/17 12:12 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:17 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:17 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:17 bgmug/L 0.12Barium100170
6020B P7D002611.0 4/5/17 14:17 bgmJug/L 0.068Beryllium10.096
6020B P7D002611.0 4/5/17 14:17 bgmJug/L 0.053Cadmium10.32
6020B P7D002611.0 4/5/17 14:17 bgmJug/L 0.32Chromium100.73
6020B P7D002611.0 4/5/17 14:17 bgmug/L 0.056Cobalt1059
6020B P7D002615.0 4/5/17 14:17 bgmJug/L 0.41Copper101.7
6020B P7D002611.0 4/5/17 14:17 bgmJug/L 0.061Lead100.27
6020B P7D002612.0 4/5/17 14:17 bgmug/L 0.082Nickel508.2
6020B P7D002615.0 4/5/17 14:17 bgmug/L 0.45Selenium10<0.45
6020B P7D002615.0 4/5/17 14:17 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:17 bgmJug/L 0.018Thallium5.50.19
6020B P7D002611.0 4/5/17 14:17 bgmug/L 0.79Vanadium25<0.79
6020B P7D00261104/5/17 14:17 bgmBug/L 1.3Zinc1011
Volatile Organic Compounds by GC/MS
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0831,1-Dichloroethane 52.2
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C050211.0 3/30/17 17:32 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C050212.0 3/30/17 17:32 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0511,2-Dibromoethane 1<0.051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-02
Prism Work Order: 7030361
Time Collected: 03/21/17 13:48
Time Submitted: 03/22/17 09:30
MW-03
50-02
SWSL
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.0501,4-Dichlorobenzene 112
8260B P7C050215.0 3/30/17 17:32 KDMug/L 0.31Acetone100<0.31
8260B P7C05021203/30/17 17:32 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.048Benzene10.57
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C050211.0 3/30/17 17:32 KDMug/L 0.040Bromoform3<0.040
8260B P7C050211.0 3/30/17 17:32 KDMug/L 0.18Bromomethane10<0.18
8260B P7C050215.0 3/30/17 17:32 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.062Chlorobenzene37.4
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.22Chloroethane10<0.22
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.076Chloroform5<0.076
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.079Chloromethane1<0.079
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.056cis-1,2-Dichloroethylene 53.8
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C050211.0 3/30/17 17:32 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C050215.0 3/30/17 17:32 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C050215.0 3/30/17 17:32 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C050215.0 3/30/17 17:32 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C050215.0 3/30/17 17:32 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C050211.0 3/30/17 17:32 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.047Styrene1<0.047
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05021103/30/17 17:32 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.044Toluene1<0.044
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05021103/30/17 17:32 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.078Trichloroethylene1<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-02
Prism Work Order: 7030361
Time Collected: 03/21/17 13:48
Time Submitted: 03/22/17 09:30
MW-03
50-02
SWSL
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C050212.0 3/30/17 17:32 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C050210.50 3/30/17 17:32 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C050213.0 3/30/17 17:32 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12494 %4-Bromofluorobenzene
75-129109 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-03
Prism Work Order: 7030361
Time Collected: 03/21/17 10:26
Time Submitted: 03/22/17 09:30
MW-06
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0386110003/22/17 15:33 EGCug/L 44ChlorideNE1100
9056A P7C038611003/22/17 15:33 EGCJ, B ug/L 17Nitrate as N 1000077
9056A P7C0386110003/22/17 15:33 EGCJug/L 320Sulfate250000950
General Chemistry Parameters
SM5210 B P7C0368120003/22/17 12:39 SLSJug/LBiochemical Oxygen Demand NE920
SM5220 D P7C03761500003/23/17 9:25 BMSug/L 14000Chemical Oxygen Demand NE<14000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCJug/L 1.0Cyanide103.1
SM3500-Fe D P7C0366510003/22/17 10:00 BMSug/L 360Ferrous Iron NE4500
SM4500-S F P7C0397120003/23/17 15:30 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 12:20 EGCug/L 770Total Alkalinity to pH 4.5 NE52000
Total Metals
7470A P7D025510.20 4/18/17 12:16 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:21 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:21 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:21 bgmug/L 0.12Barium10081
6020B P7D002611.0 4/5/17 14:21 bgmJug/L 0.068Beryllium10.12
6020B P7D002611.0 4/5/17 14:21 bgmJug/L 0.053Cadmium10.22
6020B P7D002611.0 4/5/17 14:21 bgmug/L 0.32Chromium101.4
6020B P7D002611.0 4/5/17 14:21 bgmug/L 0.056Cobalt1091
6020B P7D002615.0 4/5/17 14:21 bgmJug/L 0.41Copper102.7
6020B P7D002611.0 4/5/17 14:21 bgmJug/L 0.061Lead100.37
6020B P7D002612.0 4/5/17 14:21 bgmug/L 0.082Nickel5026
6020B P7D002615.0 4/5/17 14:21 bgmJug/L 0.45Selenium100.71
6020B P7D002615.0 4/5/17 14:21 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:21 bgmJug/L 0.018Thallium5.50.84
6020B P7D002611.0 4/5/17 14:21 bgmug/L 0.79Vanadium25<0.79
6020B P7D00261104/5/17 14:21 bgmBug/L 1.3Zinc1031
Volatile Organic Compounds by GC/MS
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0831,1-Dichloroethane 54.4
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C050211.0 3/30/17 18:06 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C050212.0 3/30/17 18:06 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0511,2-Dibromoethane 1<0.051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-03
Prism Work Order: 7030361
Time Collected: 03/21/17 10:26
Time Submitted: 03/22/17 09:30
MW-06
50-02
SWSL
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.0501,4-Dichlorobenzene 14.9
8260B P7C050215.0 3/30/17 18:06 KDMug/L 0.31Acetone10011
8260B P7C05021203/30/17 18:06 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.048Benzene10.69
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C050211.0 3/30/17 18:06 KDMug/L 0.040Bromoform3<0.040
8260B P7C050211.0 3/30/17 18:06 KDMug/L 0.18Bromomethane10<0.18
8260B P7C050215.0 3/30/17 18:06 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.062Chlorobenzene30.79
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.22Chloroethane10<0.22
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.076Chloroform5<0.076
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.079Chloromethane1<0.079
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.056cis-1,2-Dichloroethylene 54.5
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C050211.0 3/30/17 18:06 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C050215.0 3/30/17 18:06 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C050215.0 3/30/17 18:06 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C050215.0 3/30/17 18:06 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C050215.0 3/30/17 18:06 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C050211.0 3/30/17 18:06 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.047Styrene1<0.047
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05021103/30/17 18:06 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.044Toluene1<0.044
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05021103/30/17 18:06 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.078Trichloroethylene1<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-03
Prism Work Order: 7030361
Time Collected: 03/21/17 10:26
Time Submitted: 03/22/17 09:30
MW-06
50-02
SWSL
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C050212.0 3/30/17 18:06 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C050210.50 3/30/17 18:06 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C050213.0 3/30/17 18:06 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129108 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-04
Prism Work Order: 7030361
Time Collected: 03/21/17 00:00
Time Submitted: 03/22/17 09:30
Trip Blank
50-02
SWSL
Volatile Organic Compounds by GC/MS
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C050211.0 3/30/17 15:17 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C050212.0 3/30/17 15:17 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C050215.0 3/30/17 15:17 KDMug/L 0.31Acetone100<0.31
8260B P7C05021203/30/17 15:17 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.048Benzene1<0.048
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C050211.0 3/30/17 15:17 KDMug/L 0.040Bromoform3<0.040
8260B P7C050211.0 3/30/17 15:17 KDMug/L 0.18Bromomethane10<0.18
8260B P7C050215.0 3/30/17 15:17 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.22Chloroethane10<0.22
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.076Chloroform5<0.076
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.079Chloromethane1<0.079
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C050211.0 3/30/17 15:17 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C050215.0 3/30/17 15:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C050215.0 3/30/17 15:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C050215.0 3/30/17 15:17 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C050215.0 3/30/17 15:17 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 58
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030361-04
Prism Work Order: 7030361
Time Collected: 03/21/17 00:00
Time Submitted: 03/22/17 09:30
Trip Blank
50-02
SWSL
8260B P7C050211.0 3/30/17 15:17 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.047Styrene1<0.047
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05021103/30/17 15:17 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.044Toluene1<0.044
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05021103/30/17 15:17 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C050212.0 3/30/17 15:17 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C050210.50 3/30/17 15:17 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C050213.0 3/30/17 15:17 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129107 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0502 - 5030B
Blank (P7C0502-BLK1)Prepared & Analyzed: 03/30/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0502 - 5030B
Blank (P7C0502-BLK1)Prepared & Analyzed: 03/30/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9648.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10652.8
ug/L 50.00 77-123Surrogate: Toluene-d8 9446.9
LCS (P7C0502-BS1)Prepared & Analyzed: 03/30/17
1,1,1,2-Tetrachloroethane ug/L20.3 0.50 20.00 79-134101
1,1,1-Trichloroethane ug/L21.2 0.50 20.00 75-136106
1,1,2,2-Tetrachloroethane ug/L19.5 0.50 20.00 62-12797
1,1,2-Trichloroethane ug/L21.8 0.50 20.00 70-140109
1,1-Dichloroethane ug/L20.2 0.50 20.00 78-130101
1,1-Dichloroethylene ug/L21.1 0.50 20.00 70-154106
1,2,3-Trichloropropane ug/L20.2 1.0 20.00 71-127101
1,2-Dibromo-3-chloropropane ug/L18.4 2.0 20.00 63-13492
1,2-Dibromoethane ug/L20.8 0.50 20.00 77-135104
1,2-Dichlorobenzene ug/L20.2 0.50 20.00 78-128101
1,2-Dichloroethane ug/L21.6 0.50 20.00 68-131108
1,2-Dichloropropane ug/L20.2 0.50 20.00 77-130101
1,4-Dichlorobenzene ug/L19.5 0.50 20.00 75-12698
Acetone ug/L36.0 5.0 40.00 40-16690
Acrylonitrile ug/L40.9 20 40.00 81-127102
Benzene ug/L20.8 0.50 20.00 77-128104
Bromochloromethane ug/L21.1 0.50 20.00 78-135106
Bromodichloromethane ug/L21.5 0.50 20.00 76-138107
Bromoform ug/L19.2 1.0 20.00 71-13596
Bromomethane ug/L20.2 1.0 20.00 41-168101
Carbon disulfide ug/L21.8 5.0 20.00 59-135109
Carbon Tetrachloride ug/L20.4 0.50 20.00 72-142102
Chlorobenzene ug/L20.3 0.50 20.00 78-119101
Chloroethane ug/L20.6 0.50 20.00 57-142103
Chloroform ug/L19.6 0.50 20.00 77-13098
Chloromethane ug/L19.7 0.50 20.00 47-14598
cis-1,2-Dichloroethylene ug/L20.6 0.50 20.00 76-141103
cis-1,3-Dichloropropylene ug/L22.3 0.50 20.00 65-140112
Dibromochloromethane ug/L21.0 0.50 20.00 75-134105
Dibromomethane ug/L20.3 0.50 20.00 76-138102
Ethylbenzene ug/L20.6 0.50 20.00 80-127103
m,p-Xylenes ug/L42.4 1.0 40.00 77-133106
Methyl Butyl Ketone (2-Hexanone)ug/L17.5 5.0 20.00 64-13788
Methyl Ethyl Ketone (2-Butanone)ug/L19.7 5.0 20.00 71-13498
Methyl Iodide ug/L20.1 5.0 20.00 70-130101
Methyl Isobutyl Ketone ug/L20.6 5.0 20.00 69-134103
Methylene Chloride ug/L19.4 1.0 20.00 73-13197
o-Xylene ug/L20.3 0.50 20.00 78-128102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0502 - 5030B
LCS (P7C0502-BS1)Prepared & Analyzed: 03/30/17
Styrene ug/L19.3 0.50 20.00 78-12997
Tetrachloroethylene ug/L20.6 0.50 20.00 80-129103
Tetrahydrofuran ug/L19.9 10 20.00 70-13099
Toluene ug/L21.1 0.50 20.00 76-131105
trans-1,2-Dichloroethylene ug/L20.8 0.50 20.00 76-135104
trans-1,3-Dichloropropylene ug/L21.6 0.50 20.00 67-140108
trans-1,4-Dichloro-2-butene ug/L20.4 10 20.00 70-130102
Trichloroethylene ug/L21.8 0.50 20.00 77-133109
Trichlorofluoromethane ug/L22.1 0.50 20.00 62-148111
Vinyl acetate ug/L21.0 2.0 20.00 34-167105
Vinyl chloride ug/L21.2 0.50 20.00 57-141106
Xylenes, total ug/L62.7 3.0 60.00 77-133104
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 77-123Surrogate: Toluene-d8 9547.3
LCS Dup (P7C0502-BSD1)Prepared & Analyzed: 03/30/17
1,1,1,2-Tetrachloroethane ug/L19.4 0.50 20.00 2079-13497 5
1,1,1-Trichloroethane ug/L19.8 0.50 20.00 2075-13699 7
1,1,2,2-Tetrachloroethane ug/L18.8 0.50 20.00 2062-12794 4
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 2070-140104 5
1,1-Dichloroethane ug/L18.8 0.50 20.00 2078-13094 7
1,1-Dichloroethylene ug/L20.0 0.50 20.00 2070-154100 5
1,2,3-Trichloropropane ug/L19.5 1.0 20.00 2071-12797 4
1,2-Dibromo-3-chloropropane ug/L18.6 2.0 20.00 2063-13493 1
1,2-Dibromoethane ug/L20.3 0.50 20.00 2077-135101 3
1,2-Dichlorobenzene ug/L19.6 0.50 20.00 2078-12898 3
1,2-Dichloroethane ug/L20.9 0.50 20.00 2068-131104 3
1,2-Dichloropropane ug/L19.4 0.50 20.00 2077-13097 4
1,4-Dichlorobenzene ug/L18.8 0.50 20.00 2075-12694 4
Acetone ug/L35.6 5.0 40.00 2040-16689 1
Acrylonitrile ug/L41.4 20 40.00 2081-127103 1
Benzene ug/L19.8 0.50 20.00 2077-12899 5
Bromochloromethane ug/L20.3 0.50 20.00 2078-135102 4
Bromodichloromethane ug/L21.2 0.50 20.00 2076-138106 2
Bromoform ug/L19.7 1.0 20.00 2071-13599 3
Bromomethane ug/L19.8 1.0 20.00 2041-16899 2
Carbon disulfide ug/L21.2 5.0 20.00 2059-135106 3
Carbon Tetrachloride ug/L19.2 0.50 20.00 2072-14296 6
Chlorobenzene ug/L19.4 0.50 20.00 2078-11997 4
Chloroethane ug/L19.8 0.50 20.00 2057-14299 4
Chloroform ug/L18.9 0.50 20.00 2077-13094 4
Chloromethane ug/L18.7 0.50 20.00 2047-14593 5
cis-1,2-Dichloroethylene ug/L20.0 0.50 20.00 2076-141100 3
cis-1,3-Dichloropropylene ug/L21.3 0.50 20.00 2065-140106 5
Dibromochloromethane ug/L20.2 0.50 20.00 2075-134101 4
Dibromomethane ug/L21.5 0.50 20.00 2076-138107 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0502 - 5030B
LCS Dup (P7C0502-BSD1)Prepared & Analyzed: 03/30/17
Ethylbenzene ug/L19.4 0.50 20.00 2080-12797 6
m,p-Xylenes ug/L40.4 1.0 40.00 2077-133101 5
Methyl Butyl Ketone (2-Hexanone)ug/L18.1 5.0 20.00 2064-13791 3
Methyl Ethyl Ketone (2-Butanone)ug/L20.0 5.0 20.00 2071-134100 2
Methyl Iodide ug/L18.9 5.0 20.00 2070-13095 6
Methyl Isobutyl Ketone ug/L20.0 5.0 20.00 2069-134100 3
Methylene Chloride ug/L18.6 1.0 20.00 2073-13193 4
o-Xylene ug/L19.3 0.50 20.00 2078-12896 5
Styrene ug/L18.6 0.50 20.00 2078-12993 4
Tetrachloroethylene ug/L19.7 0.50 20.00 2080-12999 4
Tetrahydrofuran ug/L20.1 10 20.00 2070-130100 1
Toluene ug/L20.0 0.50 20.00 2076-131100 5
trans-1,2-Dichloroethylene ug/L20.0 0.50 20.00 2076-135100 4
trans-1,3-Dichloropropylene ug/L21.1 0.50 20.00 2067-140105 3
trans-1,4-Dichloro-2-butene ug/L19.6 10 20.00 2070-13098 4
Trichloroethylene ug/L20.4 0.50 20.00 2077-133102 7
Trichlorofluoromethane ug/L20.6 0.50 20.00 2062-148103 7
Vinyl acetate ug/L21.0 2.0 20.00 2034-167105 0.1
Vinyl chloride ug/L20.4 0.50 20.00 2057-141102 4
Xylenes, total ug/L59.7 3.0 60.00 2077-13399 5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 77-123Surrogate: Toluene-d8 9447.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0026 - 3005A
Blank (P7D0026-BLK1)Prepared: 04/04/17 Analyzed: 04/05/17
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L0.486 5.0 J
Beryllium ug/LBRL1.0
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Cobalt ug/LBRL1.0
Copper ug/L0.911 5.0 J
Lead ug/L0.308 1.0 J
Nickel ug/L0.326 2.0 J
Selenium ug/LBRL5.0
Silver ug/L0.143 5.0 J
Thallium ug/L0.0330 1.0 J
Vanadium ug/LBRL1.0
Zinc ug/L5.30 10 B, J
LCS (P7D0026-BS1)Prepared: 04/04/17 Analyzed: 04/05/17
Antimony ug/L98.0 1.0 100.0 80-12098
Arsenic ug/L1021.0 100.0 80-120102
Barium ug/L1025.0 100.0 80-120102
Beryllium ug/L1081.0 100.0 80-120108
Cadmium ug/L1021.0 100.0 80-120102
Chromium ug/L1001.0 100.0 80-120100
Cobalt ug/L1151.0 100.0 80-120115
Copper ug/L1165.0 100.0 80-120116
Lead ug/L1081.0 100.0 80-120108
Nickel ug/L1102.0 100.0 80-120110
Selenium ug/L99.1 5.0 100.0 80-12099
Silver ug/L1145.0 100.0 80-120114
Thallium ug/L1051.0 100.0 80-120105
Vanadium ug/L97.7 1.0 100.0 80-12098
Zinc ug/L110 10 100.0 B80-120110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0255 - 7470A
Blank (P7D0255-BLK1)Prepared & Analyzed: 04/18/17
Mercury ug/LBRL0.20
LCS (P7D0255-BS1)Prepared & Analyzed: 04/18/17
Mercury ug/L9.14 0.20 9.375 80-12097
Matrix Spike (P7D0255-MS1)Prepared & Analyzed: 04/18/17 Source: 7030361-01
Mercury ug/L7.43 0.20 9.375 BRL MI80-12079
Matrix Spike Dup (P7D0255-MSD1)Prepared & Analyzed: 04/18/17 Source: 7030361-01
Mercury ug/L7.53 0.20 9.375 BRL 2080-12080 1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7C0386 - NO PREP
Blank (P7C0386-BLK1)Prepared & Analyzed: 03/21/17
Chloride ug/L2531000 J
Nitrate as N ug/L60.0 100 B, J
Sulfate ug/LBRL1000
LCS (P7C0386-BS1)Prepared & Analyzed: 03/21/17
Chloride ug/L399001000 40000 80-120100
Nitrate as N ug/L3910100 4000 B80-12098
Sulfate ug/L396001000 40000 80-12099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0366 - NO PREP
Blank (P7C0366-BLK1)Prepared & Analyzed: 03/22/17
Ferrous Iron ug/LBRL200
LCS (P7C0366-BS1)Prepared & Analyzed: 03/22/17
Ferrous Iron ug/L1920200 90-110
Matrix Spike (P7C0366-MS1)Prepared & Analyzed: 03/22/17 Source: 7030361-02
Ferrous Iron ug/L2060200 143 80-120
Matrix Spike Dup (P7C0366-MSD1)Prepared & Analyzed: 03/22/17 Source: 7030361-02
Ferrous Iron ug/L2040200 143 2080-120 0.9
Batch P7C0368 - NO PREP
Blank (P7C0368-BLK1)Prepared & Analyzed: 03/22/17
Biochemical Oxygen Demand ug/L1602000 J
LCS (P7C0368-BS1)Prepared & Analyzed: 03/22/17
Biochemical Oxygen Demand ug/L1940002000 198000 84.6-115.498
Batch P7C0376 - NO PREP
Blank (P7C0376-BLK1)Prepared & Analyzed: 03/23/17
Chemical Oxygen Demand ug/LBRL50000
LCS (P7C0376-BS1)Prepared & Analyzed: 03/23/17
Chemical Oxygen Demand ug/L50700051000 505100 90-110100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 58
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0376 - NO PREP
Matrix Spike (P7C0376-MS1)Prepared & Analyzed: 03/23/17 Source: 7030361-02
Chemical Oxygen Demand ug/L49600051000 505100 BRL 80-12098
Matrix Spike Dup (P7C0376-MSD1)Prepared & Analyzed: 03/23/17 Source: 7030361-02
Chemical Oxygen Demand ug/L49400051000 505100 BRL 2080-12098 0.5
Batch P7C0397 - SM4500-S C
Blank (P7C0397-BLK1)Prepared & Analyzed: 03/23/17
Sulfide ug/LBRL2000
LCS (P7C0397-BS1)Prepared & Analyzed: 03/23/17
Sulfide ug/L8500 2000 10000 70-13085
Batch P7C0412 - NO PREP
Blank (P7C0412-BLK1)Prepared & Analyzed: 03/24/17
Total Alkalinity to pH 4.5 ug/LBRL5000
LCS (P7C0412-BS1)Prepared & Analyzed: 03/24/17
Total Alkalinity to pH 4.5 ug/L2500005000 250000 90-110100
Duplicate (P7C0412-DUP1)Prepared & Analyzed: 03/24/17 Source: 7030361-03
Total Alkalinity to pH 4.5 ug/L569005000 51800 209
Batch P7C0426 - SM4500-CN C
Blank (P7C0426-BLK1)Prepared & Analyzed: 03/27/17
Cyanide ug/L1.00 5.0 J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030361
Time Submitted: 3/22/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0426 - SM4500-CN C
LCS (P7C0426-BS1)Prepared & Analyzed: 03/27/17
Cyanide ug/L90.1 5.0 100.0 85-11590
Sample Extraction Data
Prep Method: SM4500-CN C
Lab Number Batch Date/TimeInitialFinal
P7C04267030361-01 03/27/17 6:2050 50mL mL
P7C04267030361-02 03/27/17 6:2050 50mL mL
P7C04267030361-03 03/27/17 6:2050 50mL mL
Prep Method: SM4500-S C
Lab Number Batch Date/TimeInitialFinal
P7C03977030361-01 03/23/17 15:30200 200mL mL
P7C03977030361-02 03/23/17 15:30200 200mL mL
P7C03977030361-03 03/23/17 15:30200 200mL mL
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D00267030361-01 04/04/17 7:3050 50mL mL
P7D00267030361-02 04/04/17 7:3050 50mL mL
P7D00267030361-03 04/04/17 7:3050 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D02557030361-01 04/18/17 8:4020 30mL mL
P7D02557030361-02 04/18/17 8:4020 30mL mL
P7D02557030361-03 04/18/17 8:4020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7C05027030361-01 03/30/17 10:2110 10mL mL
P7C05027030361-02 03/30/17 10:2110 10mL mL
P7C05027030361-03 03/30/17 10:2110 10mL mL
P7C05027030361-04 03/30/17 10:2110 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 58
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Analysis
7030361-01 TOC (Sub)
7030361-02 TOC (Sub)
7030361-03 TOC (Sub)
Lab Number
The following analyses were subcontracted to Microseeps/Pace
Analysis
7030361-01 Methane, Ethane, Ethene (AM20GAX)
7030361-01 Volatile Fatty Acids (Sub)
7030361-02 Dissolved Hydrogen (Sub)
7030361-02 Methane, Ethane, Ethene (AM20GAX)
7030361-02 Volatile Fatty Acids (Sub)
7030361-03 Dissolved Hydrogen (Sub)
7030361-03 Methane, Ethane, Ethene (AM20GAX)
7030361-03 Volatile Fatty Acids (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/20/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill (Permit 50-02)
Project No.: 50-02
Lab Submittal Date: 03/23/2017
Prism Work Order: 7030375
This is a Revised Report and supercedes the original laboratory report data 4/11/17. Mercury has been
added.
Dissolved Hydrogen, Methane, Ethane, Ethene and Volatile Fatty Acid subcontracted to
Microseeps/Pace. TOC subcontracted to GCAL. Laboratory reports are attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Angela D. Overcash For Robbi A. Jones
VP Laboratory Services
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 64
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BHL MB greater than one half of the RL, but sample concentrations are either less than the RL or greater than 10x the
MB.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
MI Matrix spike outside of the control limits. Matrix interference suspected.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 64
Sample Receipt Summary
04/20/2017
Prism Work Order: 7030375
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030375-01 03/22/17MW-02 03/23/17Water
7030375-02 03/22/17MW-04 03/23/17Water
7030375-03 03/22/17MW-05R 03/23/17Water
7030375-04 03/22/17MW-07 03/23/17Water
7030375-05 03/22/17Trip Blank (2)03/23/17Water
Samples were received in good condition at 0.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 64
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030375
04/20/2017
Summary of Detections
29000 ug/L7030375-01 MW-02 Chloride 9056A
390 ug/L7030375-01 MW-02 Nitrate as N 9056A
13000 ug/L7030375-01 MW-02 Sulfate 9056A
300000 ug/L7030375-01 MW-02 Chemical Oxygen Demand SM5220 D
4.4 J ug/L7030375-01 MW-02 Cyanide SM4500-CN E
51000 ug/L7030375-01 MW-02 Total Alkalinity to pH 4.5 SM2320 B
2.9 ug/L7030375-01 MW-02 Arsenic 6020B
120 ug/L7030375-01 MW-02 Barium 6020B
0.33 J ug/L7030375-01 MW-02 Beryllium 6020B
0.11 J ug/L7030375-01 MW-02 Cadmium 6020B
12 ug/L7030375-01 MW-02 Chromium 6020B
31 ug/L7030375-01 MW-02 Cobalt 6020B
16 ug/L7030375-01 MW-02 Copper 6020B
4.3 ug/L7030375-01 MW-02 Lead 6020B
9.6 ug/L7030375-01 MW-02 Nickel 6020B
12 ug/L7030375-01 MW-02 Selenium 6020B
0.31 J ug/L7030375-01 MW-02 Thallium 6020B
20 ug/L7030375-01 MW-02 Vanadium 6020B
41 B ug/L7030375-01 MW-02 Zinc 6020B
0.80 ug/L7030375-01 MW-02 1,1-Dichloroethane 8260B
1.4 ug/L7030375-01 MW-02 cis-1,2-Dichloroethylene 8260B
89000 ug/L7030375-02 MW-04 Chloride 9056A
440 ug/L7030375-02 MW-04 Nitrate as N 9056A
67000 ug/L7030375-02 MW-04 Sulfate 9056A
860 J ug/L7030375-02 MW-04 Biochemical Oxygen Demand SM5210 B
110000 ug/L7030375-02 MW-04 Chemical Oxygen Demand SM5220 D
1.8 J ug/L7030375-02 MW-04 Cyanide SM4500-CN E
160000 ug/L7030375-02 MW-04 Total Alkalinity to pH 4.5 SM2320 B
84 ug/L7030375-02 MW-04 Barium 6020B
0.073 J ug/L7030375-02 MW-04 Beryllium 6020B
0.26 J ug/L7030375-02 MW-04 Cadmium 6020B
1.3 ug/L7030375-02 MW-04 Chromium 6020B
2.8 ug/L7030375-02 MW-04 Cobalt 6020B
1.0 J ug/L7030375-02 MW-04 Copper 6020B
0.29 J ug/L7030375-02 MW-04 Lead 6020B
2.2 ug/L7030375-02 MW-04 Nickel 6020B
0.76 J ug/L7030375-02 MW-04 Selenium 6020B
0.81 J ug/L7030375-02 MW-04 Silver 6020B
0.19 J ug/L7030375-02 MW-04 Thallium 6020B
7.3 BHL, J,
B
ug/L7030375-02 MW-04 Zinc 6020B
5.7 ug/L7030375-02 MW-04 1,4-Dichlorobenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 64
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030375
04/20/2017
Summary of Detections
0.90 ug/L7030375-02 MW-04 Benzene 8260B
4.3 ug/L7030375-02 MW-04 Chlorobenzene 8260B
6.2 ug/L7030375-02 MW-04 cis-1,2-Dichloroethylene 8260B
76000 ug/L7030375-03 MW-05R Chloride 9056A
310 ug/L7030375-03 MW-05R Nitrate as N 9056A
2000 ug/L7030375-03 MW-05R Sulfate 9056A
1200 J ug/L7030375-03 MW-05R Biochemical Oxygen Demand SM5210 B
33000 J ug/L7030375-03 MW-05R Chemical Oxygen Demand SM5220 D
1.1 J ug/L7030375-03 MW-05R Cyanide SM4500-CN E
17000 ug/L7030375-03 MW-05R Ferrous Iron SM3500-Fe D
230000 ug/L7030375-03 MW-05R Total Alkalinity to pH 4.5 SM2320 B
0.53 J ug/L7030375-03 MW-05R Arsenic 6020B
180 ug/L7030375-03 MW-05R Barium 6020B
0.12 J ug/L7030375-03 MW-05R Beryllium 6020B
1.4 ug/L7030375-03 MW-05R Cadmium 6020B
2.4 ug/L7030375-03 MW-05R Chromium 6020B
18 ug/L7030375-03 MW-05R Cobalt 6020B
4.2 J ug/L7030375-03 MW-05R Copper 6020B
0.90 J ug/L7030375-03 MW-05R Lead 6020B
6.7 ug/L7030375-03 MW-05R Nickel 6020B
0.98 J ug/L7030375-03 MW-05R Selenium 6020B
0.10 J ug/L7030375-03 MW-05R Thallium 6020B
2.7 ug/L7030375-03 MW-05R Vanadium 6020B
16 B ug/L7030375-03 MW-05R Zinc 6020B
10 ug/L7030375-03 MW-05R 1,4-Dichlorobenzene 8260B
1.8 ug/L7030375-03 MW-05R Benzene 8260B
8.4 ug/L7030375-03 MW-05R Chlorobenzene 8260B
10 ug/L7030375-03 MW-05R cis-1,2-Dichloroethylene 8260B
1.3 ug/L7030375-03 MW-05R Vinyl chloride 8260B
71000 ug/L7030375-04 MW-07 Chloride 9056A
91 J ug/L7030375-04 MW-07 Nitrate as N 9056A
23000 ug/L7030375-04 MW-07 Sulfate 9056A
120 J ug/L7030375-04 MW-07 Biochemical Oxygen Demand SM5210 B
290 ug/L7030375-04 MW-07 Ferrous Iron SM3500-Fe D
260000 ug/L7030375-04 MW-07 Total Alkalinity to pH 4.5 SM2320 B
490 ug/L7030375-04 MW-07 Barium 6020B
0.14 J ug/L7030375-04 MW-07 Cadmium 6020B
0.63 J ug/L7030375-04 MW-07 Chromium 6020B
0.93 J ug/L7030375-04 MW-07 Cobalt 6020B
1.4 J ug/L7030375-04 MW-07 Copper 6020B
0.50 J ug/L7030375-04 MW-07 Lead 6020B
7.6 ug/L7030375-04 MW-07 Nickel 6020B
0.072 J ug/L7030375-04 MW-07 Thallium 6020B
13 B ug/L7030375-04 MW-07 Zinc 6020B
5.5 ug/L7030375-04 MW-07 1,4-Dichlorobenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 64
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030375
04/20/2017
Summary of Detections
1.6 ug/L7030375-04 MW-07 Benzene 8260B
6.3 ug/L7030375-04 MW-07 Chlorobenzene 8260B
4.5 ug/L7030375-04 MW-07 cis-1,2-Dichloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-01
Prism Work Order: 7030375
Time Collected: 03/22/17 13:30
Time Submitted: 03/23/17 09:30
MW-02
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0434110003/23/17 11:50 EGCug/L 44ChlorideNE29000
9056A P7C043411003/23/17 11:50 EGCug/L 17Nitrate as N 10000390
9056A P7C0434110003/23/17 11:50 EGCug/L 320Sulfate25000013000
General Chemistry Parameters
SM5210 B P7C0392120003/23/17 12:48 SLSug/LBiochemical Oxygen Demand NE<
SM5220 D P7C04721500003/29/17 9:34 BMSug/L 14000Chemical Oxygen Demand NE300000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCJug/L 1.0Cyanide104.4
SM3500-Fe D P7C038012003/23/17 10:00 BMSug/L 71Ferrous Iron NE<71
SM4500-S F P7C0397120003/23/17 16:00 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 12:40 EGCug/L 770Total Alkalinity to pH 4.5 NE51000
Total Metals
7470A P7D025510.20 4/18/17 12:19 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:25 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:25 bgmug/L 0.45Arsenic102.9
6020B P7D002615.0 4/5/17 14:25 bgmug/L 0.12Barium100120
6020B P7D002611.0 4/5/17 14:25 bgmJug/L 0.068Beryllium10.33
6020B P7D002611.0 4/5/17 14:25 bgmJug/L 0.053Cadmium10.11
6020B P7D002611.0 4/5/17 14:25 bgmug/L 0.32Chromium1012
6020B P7D002611.0 4/5/17 14:25 bgmug/L 0.056Cobalt1031
6020B P7D002615.0 4/5/17 14:25 bgmug/L 0.41Copper1016
6020B P7D002611.0 4/5/17 14:25 bgmug/L 0.061Lead104.3
6020B P7D002612.0 4/5/17 14:25 bgmug/L 0.082Nickel509.6
6020B P7D002615.0 4/5/17 14:25 bgmug/L 0.45Selenium1012
6020B P7D002615.0 4/5/17 14:25 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:25 bgmJug/L 0.018Thallium5.50.31
6020B P7D002611.0 4/5/17 14:25 bgmug/L 0.79Vanadium2520
6020B P7D00261104/5/17 14:25 bgmBug/L 1.3Zinc1041
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0831,1-Dichloroethane 50.80
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 17:00 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 17:00 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0511,2-Dibromoethane 1<0.051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-01
Prism Work Order: 7030375
Time Collected: 03/22/17 13:30
Time Submitted: 03/23/17 09:30
MW-02
50-02
SWSL
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D001715.0 4/3/17 17:00 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 17:00 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.048Benzene1<0.048
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D001711.0 4/3/17 17:00 KDMug/L 0.040Bromoform3<0.040
8260B P7D001711.0 4/3/17 17:00 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 17:00 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.056cis-1,2-Dichloroethylene 51.4
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 17:00 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 17:00 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 17:00 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 17:00 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 17:00 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D001711.0 4/3/17 17:00 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 17:00 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 17:00 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.078Trichloroethylene1<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-01
Prism Work Order: 7030375
Time Collected: 03/22/17 13:30
Time Submitted: 03/23/17 09:30
MW-02
50-02
SWSL
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 17:00 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 17:00 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D001713.0 4/3/17 17:00 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129123 %Dibromofluoromethane
77-12391 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-02
Prism Work Order: 7030375
Time Collected: 03/22/17 10:29
Time Submitted: 03/23/17 09:30
MW-04
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0434110003/23/17 11:19 EGCug/L 44ChlorideNE89000
9056A P7C043411003/23/17 11:19 EGCug/L 17Nitrate as N 10000440
9056A P7C0434110003/23/17 11:19 EGCug/L 320Sulfate25000067000
General Chemistry Parameters
SM5210 B P7C0392120003/23/17 12:48 SLSJug/LBiochemical Oxygen Demand NE860
SM5220 D P7C04721500003/29/17 9:34 BMSug/L 14000Chemical Oxygen Demand NE110000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCJug/L 1.0Cyanide101.8
SM3500-Fe D P7C038012003/23/17 10:00 BMSug/L 71Ferrous Iron NE<71
SM4500-S F P7C0397120003/23/17 16:00 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 12:40 EGCug/L 770Total Alkalinity to pH 4.5 NE160000
Total Metals
7470A P7D025510.20 4/18/17 12:23 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:38 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:38 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:38 bgmug/L 0.12Barium10084
6020B P7D002611.0 4/5/17 14:38 bgmJug/L 0.068Beryllium10.073
6020B P7D002611.0 4/5/17 14:38 bgmJug/L 0.053Cadmium10.26
6020B P7D002611.0 4/5/17 14:38 bgmug/L 0.32Chromium101.3
6020B P7D002611.0 4/5/17 14:38 bgmug/L 0.056Cobalt102.8
6020B P7D002615.0 4/5/17 14:38 bgmJug/L 0.41Copper101.0
6020B P7D002611.0 4/5/17 14:38 bgmJug/L 0.061Lead100.29
6020B P7D002612.0 4/5/17 14:38 bgmug/L 0.082Nickel502.2
6020B P7D002615.0 4/5/17 14:38 bgmJug/L 0.45Selenium100.76
6020B P7D002615.0 4/5/17 14:38 bgmJug/L 0.067Silver100.81
6020B P7D002611.0 4/5/17 14:38 bgmJug/L 0.018Thallium5.50.19
6020B P7D002611.0 4/5/17 14:38 bgmug/L 0.79Vanadium25<0.79
6020B P7D00261104/5/17 14:38 bgmBH
L, J,
B
ug/L 1.3Zinc107.3
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 17:34 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 17:34 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-02
Prism Work Order: 7030375
Time Collected: 03/22/17 10:29
Time Submitted: 03/23/17 09:30
MW-04
50-02
SWSL
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.0501,4-Dichlorobenzene 15.7
8260B P7D001715.0 4/3/17 17:34 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 17:34 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.048Benzene10.90
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D001711.0 4/3/17 17:34 KDMug/L 0.040Bromoform3<0.040
8260B P7D001711.0 4/3/17 17:34 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 17:34 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.062Chlorobenzene34.3
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.056cis-1,2-Dichloroethylene 56.2
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 17:34 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 17:34 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 17:34 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 17:34 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 17:34 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D001711.0 4/3/17 17:34 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 17:34 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 17:34 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-02
Prism Work Order: 7030375
Time Collected: 03/22/17 10:29
Time Submitted: 03/23/17 09:30
MW-04
50-02
SWSL
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 17:34 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 17:34 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D001713.0 4/3/17 17:34 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129121 %Dibromofluoromethane
77-12391 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-03
Prism Work Order: 7030375
Time Collected: 03/22/17 09:15
Time Submitted: 03/23/17 09:30
MW-05R
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0434110003/23/17 11:03 EGCug/L 44ChlorideNE76000
9056A P7C043411003/23/17 11:03 EGCug/L 17Nitrate as N 10000310
9056A P7C0434110003/23/17 11:03 EGCug/L 320Sulfate2500002000
General Chemistry Parameters
SM5210 B P7C0392120003/23/17 12:48 SLSJug/LBiochemical Oxygen Demand NE1200
SM5220 D P7C04721500003/29/17 9:34 BMSJug/L 14000Chemical Oxygen Demand NE33000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCJug/L 1.0Cyanide101.1
SM3500-Fe D P7C03802550003/23/17 10:00 BMSug/L 1800Ferrous Iron NE17000
SM4500-S F P7C0397120003/23/17 16:00 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 13:00 EGCug/L 770Total Alkalinity to pH 4.5 NE230000
Total Metals
7470A P7D025510.20 4/18/17 12:27 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:42 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:42 bgmJug/L 0.45Arsenic100.53
6020B P7D002615.0 4/5/17 14:42 bgmug/L 0.12Barium100180
6020B P7D002611.0 4/5/17 14:42 bgmJug/L 0.068Beryllium10.12
6020B P7D002611.0 4/5/17 14:42 bgmug/L 0.053Cadmium11.4
6020B P7D002611.0 4/5/17 14:42 bgmug/L 0.32Chromium102.4
6020B P7D002611.0 4/5/17 14:42 bgmug/L 0.056Cobalt1018
6020B P7D002615.0 4/5/17 14:42 bgmJug/L 0.41Copper104.2
6020B P7D002611.0 4/5/17 14:42 bgmJug/L 0.061Lead100.90
6020B P7D002612.0 4/5/17 14:42 bgmug/L 0.082Nickel506.7
6020B P7D002615.0 4/5/17 14:42 bgmJug/L 0.45Selenium100.98
6020B P7D002615.0 4/5/17 14:42 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:42 bgmJug/L 0.018Thallium5.50.10
6020B P7D002611.0 4/5/17 14:42 bgmug/L 0.79Vanadium252.7
6020B P7D00261104/5/17 14:42 bgmBug/L 1.3Zinc1016
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 18:08 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 18:08 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0511,2-Dibromoethane 1<0.051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-03
Prism Work Order: 7030375
Time Collected: 03/22/17 09:15
Time Submitted: 03/23/17 09:30
MW-05R
50-02
SWSL
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.0501,4-Dichlorobenzene 110
8260B P7D001715.0 4/3/17 18:08 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 18:08 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.048Benzene11.8
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D001711.0 4/3/17 18:08 KDMug/L 0.040Bromoform3<0.040
8260B P7D001711.0 4/3/17 18:08 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 18:08 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.062Chlorobenzene38.4
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.056cis-1,2-Dichloroethylene 510
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 18:08 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 18:08 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 18:08 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 18:08 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 18:08 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D001711.0 4/3/17 18:08 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 18:08 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 18:08 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.078Trichloroethylene1<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-03
Prism Work Order: 7030375
Time Collected: 03/22/17 09:15
Time Submitted: 03/23/17 09:30
MW-05R
50-02
SWSL
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 18:08 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 18:08 KDMug/L 0.097Vinyl chloride 11.3
8260B P7D001713.0 4/3/17 18:08 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124109 %4-Bromofluorobenzene
75-129110 %Dibromofluoromethane
77-12388 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-04
Prism Work Order: 7030375
Time Collected: 03/22/17 12:17
Time Submitted: 03/23/17 09:30
MW-07
50-02
SWSL
Anions by Ion Chromatography
9056A P7C0434110003/23/17 11:35 EGCug/L 44ChlorideNE71000
9056A P7C043411003/23/17 11:35 EGCJug/L 17Nitrate as N 1000091
9056A P7C0434110003/23/17 11:35 EGCug/L 320Sulfate25000023000
General Chemistry Parameters
SM5210 B P7C0392120003/23/17 12:48 SLSJug/LBiochemical Oxygen Demand NE120
SM5220 D P7C04721500003/29/17 9:34 BMSug/L 14000Chemical Oxygen Demand NE<14000
SM4500-CN E P7C042615.0 3/27/17 15:00 EGCug/L 1.0Cyanide10<1.0
SM3500-Fe D P7C038012003/23/17 10:00 BMSug/L 71Ferrous Iron NE290
SM4500-S F P7C0397120003/23/17 16:00 EGCug/L 830Sulfide1000<830
SM2320 B P7C0412150003/24/17 13:00 EGCug/L 770Total Alkalinity to pH 4.5 NE260000
Total Metals
7470A P7D028910.20 4/19/17 13:59 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:46 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:46 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:46 bgmug/L 0.12Barium100490
6020B P7D002611.0 4/5/17 14:46 bgmug/L 0.068Beryllium1<0.068
6020B P7D002611.0 4/5/17 14:46 bgmJug/L 0.053Cadmium10.14
6020B P7D002611.0 4/5/17 14:46 bgmJug/L 0.32Chromium100.63
6020B P7D002611.0 4/5/17 14:46 bgmJug/L 0.056Cobalt100.93
6020B P7D002615.0 4/5/17 14:46 bgmJug/L 0.41Copper101.4
6020B P7D002611.0 4/5/17 14:46 bgmJug/L 0.061Lead100.50
6020B P7D002612.0 4/5/17 14:46 bgmug/L 0.082Nickel507.6
6020B P7D002615.0 4/5/17 14:46 bgmug/L 0.45Selenium10<0.45
6020B P7D002615.0 4/5/17 14:46 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:46 bgmJug/L 0.018Thallium5.50.072
6020B P7D002611.0 4/5/17 14:46 bgmug/L 0.79Vanadium25<0.79
6020B P7D00261104/5/17 14:46 bgmBug/L 1.3Zinc1013
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 18:42 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 18:42 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0511,2-Dibromoethane 1<0.051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-04
Prism Work Order: 7030375
Time Collected: 03/22/17 12:17
Time Submitted: 03/23/17 09:30
MW-07
50-02
SWSL
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.0501,4-Dichlorobenzene 15.5
8260B P7D001715.0 4/3/17 18:42 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 18:42 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.048Benzene11.6
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D001711.0 4/3/17 18:42 KDMug/L 0.040Bromoform3<0.040
8260B P7D001711.0 4/3/17 18:42 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 18:42 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.062Chlorobenzene36.3
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.056cis-1,2-Dichloroethylene 54.5
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 18:42 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 18:42 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 18:42 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 18:42 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 18:42 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D001711.0 4/3/17 18:42 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 18:42 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 18:42 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.078Trichloroethylene1<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-04
Prism Work Order: 7030375
Time Collected: 03/22/17 12:17
Time Submitted: 03/23/17 09:30
MW-07
50-02
SWSL
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 18:42 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 18:42 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D001713.0 4/3/17 18:42 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124109 %4-Bromofluorobenzene
75-129106 %Dibromofluoromethane
77-12391 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-05
Prism Work Order: 7030375
Time Collected: 03/22/17 00:00
Time Submitted: 03/23/17 09:30
Trip Blank (2)
50-02
SWSL
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 14:11 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 14:11 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D001715.0 4/3/17 14:11 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 14:11 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.048Benzene1<0.048
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D001711.0 4/3/17 14:11 KDMug/L 0.040Bromoform3<0.040
8260B P7D001711.0 4/3/17 14:11 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 14:11 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 14:11 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 14:11 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 14:11 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 14:11 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 14:11 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 64
Laboratory Report
04/20/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030375-05
Prism Work Order: 7030375
Time Collected: 03/22/17 00:00
Time Submitted: 03/23/17 09:30
Trip Blank (2)
50-02
SWSL
8260B P7D001711.0 4/3/17 14:11 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 14:11 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 14:11 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 14:11 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 14:11 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D001713.0 4/3/17 14:11 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-12389 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
Blank (P7D0017-BLK1)Prepared & Analyzed: 04/03/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
Blank (P7D0017-BLK1)Prepared & Analyzed: 04/03/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10854.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9045.0
LCS (P7D0017-BS1)Prepared & Analyzed: 04/03/17
1,1,1,2-Tetrachloroethane ug/L20.5 0.50 20.00 79-134102
1,1,1-Trichloroethane ug/L24.5 0.50 20.00 75-136122
1,1,2,2-Tetrachloroethane ug/L18.2 0.50 20.00 62-12791
1,1,2-Trichloroethane ug/L22.2 0.50 20.00 70-140111
1,1-Dichloroethane ug/L22.8 0.50 20.00 78-130114
1,1-Dichloroethylene ug/L25.2 0.50 20.00 70-154126
1,2,3-Trichloropropane ug/L19.6 1.0 20.00 71-12798
1,2-Dibromo-3-chloropropane ug/L18.5 2.0 20.00 63-13492
1,2-Dibromoethane ug/L20.2 0.50 20.00 77-135101
1,2-Dichlorobenzene ug/L19.6 0.50 20.00 78-12898
1,2-Dichloroethane ug/L24.0 0.50 20.00 68-131120
1,2-Dichloropropane ug/L22.3 0.50 20.00 77-130111
1,4-Dichlorobenzene ug/L18.9 0.50 20.00 75-12695
Acetone ug/L44.5 5.0 40.00 40-166111
Acrylonitrile ug/L47.3 20 40.00 81-127118
Benzene ug/L23.4 0.50 20.00 77-128117
Bromochloromethane ug/L23.1 0.50 20.00 78-135116
Bromodichloromethane ug/L22.6 0.50 20.00 76-138113
Bromoform ug/L20.0 1.0 20.00 71-135100
Bromomethane ug/L24.6 1.0 20.00 41-168123
Carbon disulfide ug/L24.9 5.0 20.00 59-135125
Carbon Tetrachloride ug/L23.4 0.50 20.00 72-142117
Chlorobenzene ug/L20.1 0.50 20.00 78-119101
Chloroethane ug/L24.8 0.50 20.00 57-142124
Chloroform ug/L22.6 0.50 20.00 77-130113
Chloromethane ug/L22.8 0.50 20.00 47-145114
cis-1,2-Dichloroethylene ug/L24.1 0.50 20.00 76-141120
cis-1,3-Dichloropropylene ug/L23.3 0.50 20.00 65-140116
Dibromochloromethane ug/L20.4 0.50 20.00 75-134102
Dibromomethane ug/L22.2 0.50 20.00 76-138111
Ethylbenzene ug/L20.5 0.50 20.00 80-127103
m,p-Xylenes ug/L42.8 1.0 40.00 77-133107
Methyl Butyl Ketone (2-Hexanone)ug/L19.3 5.0 20.00 64-13797
Methyl Ethyl Ketone (2-Butanone)ug/L22.3 5.0 20.00 71-134111
Methyl Iodide ug/L23.8 5.0 20.00 70-130119
Methyl Isobutyl Ketone ug/L20.2 5.0 20.00 69-134101
Methylene Chloride ug/L22.0 1.0 20.00 73-131110
o-Xylene ug/L20.4 0.50 20.00 78-128102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
LCS (P7D0017-BS1)Prepared & Analyzed: 04/03/17
Styrene ug/L19.2 0.50 20.00 78-12996
Tetrachloroethylene ug/L21.0 0.50 20.00 80-129105
Tetrahydrofuran ug/L22.8 10 20.00 70-130114
Toluene ug/L21.7 0.50 20.00 76-131108
trans-1,2-Dichloroethylene ug/L23.2 0.50 20.00 76-135116
trans-1,3-Dichloropropylene ug/L23.0 0.50 20.00 67-140115
trans-1,4-Dichloro-2-butene ug/L20.1 10 20.00 70-130101
Trichloroethylene ug/L22.5 0.50 20.00 77-133113
Trichlorofluoromethane ug/L26.2 0.50 20.00 62-148131
Vinyl acetate ug/L24.1 2.0 20.00 34-167120
Vinyl chloride ug/L25.2 0.50 20.00 57-141126
Xylenes, total ug/L63.2 3.0 60.00 77-133105
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10954.7
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.7
LCS Dup (P7D0017-BSD1)Prepared & Analyzed: 04/03/17
1,1,1,2-Tetrachloroethane ug/L19.7 0.50 20.00 2079-13499 4
1,1,1-Trichloroethane ug/L21.6 0.50 20.00 2075-136108 12
1,1,2,2-Tetrachloroethane ug/L18.9 0.50 20.00 2062-12794 3
1,1,2-Trichloroethane ug/L21.2 0.50 20.00 2070-140106 5
1,1-Dichloroethane ug/L20.8 0.50 20.00 2078-130104 9
1,1-Dichloroethylene ug/L22.8 0.50 20.00 2070-154114 10
1,2,3-Trichloropropane ug/L19.6 1.0 20.00 2071-12798 0.1
1,2-Dibromo-3-chloropropane ug/L18.3 2.0 20.00 2063-13492 0.7
1,2-Dibromoethane ug/L20.2 0.50 20.00 2077-135101 0.2
1,2-Dichlorobenzene ug/L19.4 0.50 20.00 2078-12897 1
1,2-Dichloroethane ug/L22.4 0.50 20.00 2068-131112 7
1,2-Dichloropropane ug/L21.0 0.50 20.00 2077-130105 6
1,4-Dichlorobenzene ug/L18.9 0.50 20.00 2075-12694 0.2
Acetone ug/L39.1 5.0 40.00 2040-16698 13
Acrylonitrile ug/L44.9 20 40.00 2081-127112 5
Benzene ug/L21.1 0.50 20.00 2077-128105 11
Bromochloromethane ug/L21.3 0.50 20.00 2078-135106 8
Bromodichloromethane ug/L21.6 0.50 20.00 2076-138108 5
Bromoform ug/L19.2 1.0 20.00 2071-13596 4
Bromomethane ug/L23.6 1.0 20.00 2041-168118 4
Carbon disulfide ug/L23.1 5.0 20.00 2059-135116 7
Carbon Tetrachloride ug/L20.4 0.50 20.00 2072-142102 14
Chlorobenzene ug/L19.6 0.50 20.00 2078-11998 3
Chloroethane ug/L22.8 0.50 20.00 2057-142114 8
Chloroform ug/L20.1 0.50 20.00 2077-130101 12
Chloromethane ug/L21.6 0.50 20.00 2047-145108 6
cis-1,2-Dichloroethylene ug/L21.3 0.50 20.00 2076-141107 12
cis-1,3-Dichloropropylene ug/L22.0 0.50 20.00 2065-140110 5
Dibromochloromethane ug/L20.8 0.50 20.00 2075-134104 2
Dibromomethane ug/L21.6 0.50 20.00 2076-138108 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
LCS Dup (P7D0017-BSD1)Prepared & Analyzed: 04/03/17
Ethylbenzene ug/L19.7 0.50 20.00 2080-12798 4
m,p-Xylenes ug/L41.3 1.0 40.00 2077-133103 4
Methyl Butyl Ketone (2-Hexanone)ug/L18.6 5.0 20.00 2064-13793 4
Methyl Ethyl Ketone (2-Butanone)ug/L20.9 5.0 20.00 2071-134105 6
Methyl Iodide ug/L22.0 5.0 20.00 2070-130110 8
Methyl Isobutyl Ketone ug/L22.4 5.0 20.00 2069-134112 10
Methylene Chloride ug/L20.7 1.0 20.00 2073-131103 6
o-Xylene ug/L19.9 0.50 20.00 2078-128100 2
Styrene ug/L18.6 0.50 20.00 2078-12993 3
Tetrachloroethylene ug/L20.1 0.50 20.00 2080-129100 4
Tetrahydrofuran ug/L20.9 10 20.00 2070-130104 9
Toluene ug/L21.0 0.50 20.00 2076-131105 3
trans-1,2-Dichloroethylene ug/L23.1 0.50 20.00 2076-135115 0.6
trans-1,3-Dichloropropylene ug/L22.6 0.50 20.00 2067-140113 2
trans-1,4-Dichloro-2-butene ug/L20.2 10 20.00 2070-130101 0.6
Trichloroethylene ug/L21.6 0.50 20.00 2077-133108 4
Trichlorofluoromethane ug/L23.8 0.50 20.00 2062-148119 9
Vinyl acetate ug/L22.5 2.0 20.00 2034-167112 7
Vinyl chloride ug/L22.5 0.50 20.00 2057-141112 11
Xylenes, total ug/L61.2 3.0 60.00 2077-133102 3
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9648.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9246.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0026 - 3005A
Blank (P7D0026-BLK1)Prepared: 04/04/17 Analyzed: 04/05/17
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L0.486 5.0 J
Beryllium ug/LBRL1.0
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Cobalt ug/LBRL1.0
Copper ug/L0.911 5.0 J
Lead ug/L0.308 1.0 J
Nickel ug/L0.326 2.0 J
Selenium ug/LBRL5.0
Silver ug/L0.143 5.0 J
Thallium ug/L0.0330 1.0 J
Vanadium ug/LBRL1.0
Zinc ug/L5.30 10 B, J
LCS (P7D0026-BS1)Prepared: 04/04/17 Analyzed: 04/05/17
Antimony ug/L98.0 1.0 100.0 80-12098
Arsenic ug/L1021.0 100.0 80-120102
Barium ug/L1025.0 100.0 80-120102
Beryllium ug/L1081.0 100.0 80-120108
Cadmium ug/L1021.0 100.0 80-120102
Chromium ug/L1001.0 100.0 80-120100
Cobalt ug/L1151.0 100.0 80-120115
Copper ug/L1165.0 100.0 80-120116
Lead ug/L1081.0 100.0 80-120108
Nickel ug/L1102.0 100.0 80-120110
Selenium ug/L99.1 5.0 100.0 80-12099
Silver ug/L1145.0 100.0 80-120114
Thallium ug/L1051.0 100.0 80-120105
Vanadium ug/L97.7 1.0 100.0 80-12098
Zinc ug/L11010 100.0 B80-120110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0255 - 7470A
Blank (P7D0255-BLK1)Prepared & Analyzed: 04/18/17
Mercury ug/LBRL0.20
LCS (P7D0255-BS1)Prepared & Analyzed: 04/18/17
Mercury ug/L9.14 0.20 9.375 80-12097
Batch P7D0289 - 7470A
Blank (P7D0289-BLK1)Prepared & Analyzed: 04/19/17
Mercury ug/LBRL0.20
LCS (P7D0289-BS1)Prepared & Analyzed: 04/19/17
Mercury ug/L9.10 0.20 9.375 80-12097
Matrix Spike (P7D0289-MS1)Prepared & Analyzed: 04/19/17 Source: 7030375-04
Mercury ug/L4.89 0.20 9.375 BRL MI80-12052
Matrix Spike Dup (P7D0289-MSD1)Prepared & Analyzed: 04/19/17 Source: 7030375-04
Mercury ug/L4.60 0.20 9.375 BRL 20 MI80-12049 6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7C0434 - NO PREP
Blank (P7C0434-BLK1)Prepared & Analyzed: 03/23/17
Chloride ug/LBRL1000
Nitrate as N ug/LBRL100
Sulfate ug/LBRL1000
LCS (P7C0434-BS1)Prepared & Analyzed: 03/23/17
Chloride ug/L397001000 40000 80-12099
Nitrate as N ug/L3900100 4000 80-12098
Sulfate ug/L400001000 40000 80-120100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0380 - NO PREP
Blank (P7C0380-BLK1)Prepared & Analyzed: 03/23/17
Ferrous Iron ug/LBRL200
LCS (P7C0380-BS1)Prepared & Analyzed: 03/23/17
Ferrous Iron ug/L1970200 90-110
Matrix Spike (P7C0380-MS1)Prepared & Analyzed: 03/23/17 Source: 7030375-02
Ferrous Iron ug/L2020200 BRL 80-120
Matrix Spike Dup (P7C0380-MSD1)Prepared & Analyzed: 03/23/17 Source: 7030375-02
Ferrous Iron ug/L2050200 BRL 2080-120 1
Batch P7C0392 - NO PREP
Blank (P7C0392-BLK1)Prepared & Analyzed: 03/23/17
Biochemical Oxygen Demand ug/L70.0 2000 J
LCS (P7C0392-BS1)Prepared & Analyzed: 03/23/17
Biochemical Oxygen Demand ug/L2050002000 198000 84.6-115.4104
Batch P7C0397 - SM4500-S C
Blank (P7C0397-BLK1)Prepared & Analyzed: 03/23/17
Sulfide ug/LBRL2000
LCS (P7C0397-BS1)Prepared & Analyzed: 03/23/17
Sulfide ug/L8500 2000 10000 70-13085
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 64
4/20/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030375
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0412 - NO PREP
Blank (P7C0412-BLK1)Prepared & Analyzed: 03/24/17
Total Alkalinity to pH 4.5 ug/LBRL5000
LCS (P7C0412-BS1)Prepared & Analyzed: 03/24/17
Total Alkalinity to pH 4.5 ug/L2500005000 250000 90-110100
Batch P7C0426 - SM4500-CN C
Blank (P7C0426-BLK1)Prepared & Analyzed: 03/27/17
Cyanide ug/L1.00 5.0 J
LCS (P7C0426-BS1)Prepared & Analyzed: 03/27/17
Cyanide ug/L90.1 5.0 100.0 85-11590
Batch P7C0472 - NO PREP
Blank (P7C0472-BLK1)Prepared & Analyzed: 03/29/17
Chemical Oxygen Demand ug/LBRL50000
LCS (P7C0472-BS1)Prepared & Analyzed: 03/29/17
Chemical Oxygen Demand ug/L49800051000 505100 90-11099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 64
Sample Extraction Data
Prep Method: SM4500-CN C
Lab Number Batch Date/TimeInitialFinal
P7C04267030375-01 03/27/17 6:2050 50mL mL
P7C04267030375-02 03/27/17 6:2050 50mL mL
P7C04267030375-03 03/27/17 6:2050 50mL mL
P7C04267030375-04 03/27/17 6:2050 50mL mL
Prep Method: SM4500-S C
Lab Number Batch Date/TimeInitialFinal
P7C03977030375-01 03/23/17 16:00200 200mL mL
P7C03977030375-02 03/23/17 16:00200 200mL mL
P7C03977030375-03 03/23/17 16:00200 200mL mL
P7C03977030375-04 03/23/17 16:00200 200mL mL
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D00267030375-01 04/04/17 7:3050 50mL mL
P7D00267030375-02 04/04/17 7:3050 50mL mL
P7D00267030375-03 04/04/17 7:3050 50mL mL
P7D00267030375-04 04/04/17 7:3050 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D02557030375-01 04/18/17 8:4020 30mL mL
P7D02557030375-02 04/18/17 8:4020 30mL mL
P7D02557030375-03 04/18/17 8:4020 30mL mL
P7D02897030375-04 04/19/17 8:3020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7D00177030375-01 04/03/17 9:5810 10mL mL
P7D00177030375-02 04/03/17 9:5810 10mL mL
P7D00177030375-03 04/03/17 9:5810 10mL mL
P7D00177030375-04 04/03/17 9:5810 10mL mL
P7D00177030375-05 04/03/17 9:5810 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Analysis
7030375-01 TOC (Sub)
7030375-02 TOC (Sub)
7030375-03 TOC (Sub)
7030375-04 TOC (Sub)
Lab Number
The following analyses were subcontracted to Microseeps/Pace
Analysis
7030375-01 Methane, Ethane, Ethene (AM20GAX)
7030375-01 Volatile Fatty Acids (Sub)
7030375-02 Dissolved Hydrogen (Sub)
7030375-02 Methane, Ethane, Ethene (AM20GAX)
7030375-02 Volatile Fatty Acids (Sub)
7030375-03 Methane, Ethane, Ethene (AM20GAX)
7030375-03 Volatile Fatty Acids (Sub)
7030375-04 Dissolved Hydrogen (Sub)
7030375-04 Methane, Ethane, Ethene (AM20GAX)
7030375-04 Volatile Fatty Acids (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/18/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill (Permit 50-02)
Project No.: 50-02
Lab Submittal Date: 03/23/2017
Prism Work Order: 7030376
This is a Revised Report and supercedes the original laboratory report data 4/11/17. Mercury has been
added.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BHL MB greater than one half of the RL, but sample concentrations are either less than the RL or greater than 10x the
MB.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 14
Sample Receipt Summary
04/18/2017
Prism Work Order: 7030376
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030376-01 03/22/17SW-01 03/23/17Water
7030376-02 03/22/17SW-02 03/23/17Water
Samples were received in good condition at 2.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 14
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030376
04/18/2017
Summary of Detections
21 ug/L7030376-01 SW-01 Barium 6020B
0.85 J ug/L7030376-01 SW-01 Chromium 6020B
0.32 J ug/L7030376-01 SW-01 Cobalt 6020B
1.9 J ug/L7030376-01 SW-01 Copper 6020B
0.46 J ug/L7030376-01 SW-01 Lead 6020B
0.86 J ug/L7030376-01 SW-01 Nickel 6020B
0.062 J ug/L7030376-01 SW-01 Thallium 6020B
1.1 ug/L7030376-01 SW-01 Vanadium 6020B
7.4 BHL, J,
B
ug/L7030376-01 SW-01 Zinc 6020B
17 ug/L7030376-02 SW-02 Barium 6020B
0.64 J ug/L7030376-02 SW-02 Chromium 6020B
0.24 J ug/L7030376-02 SW-02 Cobalt 6020B
2.9 J ug/L7030376-02 SW-02 Copper 6020B
0.65 J ug/L7030376-02 SW-02 Lead 6020B
1.0 J ug/L7030376-02 SW-02 Nickel 6020B
0.050 J ug/L7030376-02 SW-02 Thallium 6020B
11 B ug/L7030376-02 SW-02 Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 14
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030376-01
Prism Work Order: 7030376
Time Collected: 03/22/17 11:06
Time Submitted: 03/23/17 09:30
SW-01
50-02
SWSL
Total Metals
7470A P7D025510.20 4/18/17 12:31 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:51 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:51 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:51 bgmug/L 0.12Barium10021
6020B P7D002611.0 4/5/17 14:51 bgmug/L 0.068Beryllium1<0.068
6020B P7D002611.0 4/5/17 14:51 bgmug/L 0.053Cadmium1<0.053
6020B P7D002611.0 4/5/17 14:51 bgmJug/L 0.32Chromium100.85
6020B P7D002611.0 4/5/17 14:51 bgmJug/L 0.056Cobalt100.32
6020B P7D002615.0 4/5/17 14:51 bgmJug/L 0.41Copper101.9
6020B P7D002611.0 4/5/17 14:51 bgmJug/L 0.061Lead100.46
6020B P7D002612.0 4/5/17 14:51 bgmJug/L 0.082Nickel500.86
6020B P7D002615.0 4/5/17 14:51 bgmug/L 0.45Selenium10<0.45
6020B P7D002615.0 4/5/17 14:51 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:51 bgmJug/L 0.018Thallium5.50.062
6020B P7D002611.0 4/5/17 14:51 bgmug/L 0.79Vanadium251.1
6020B P7D00261104/5/17 14:51 bgmBH
L, J,
B
ug/L 1.3Zinc107.4
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 19:16 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 19:16 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D001715.0 4/3/17 19:16 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 19:16 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.048Benzene1<0.048
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.062Bromodichloromethane1<0.062
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 14
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030376-01
Prism Work Order: 7030376
Time Collected: 03/22/17 11:06
Time Submitted: 03/23/17 09:30
SW-01
50-02
SWSL
8260B P7D001711.0 4/3/17 19:16 KDMug/L 0.040Bromoform3<0.040
8260B P7D001711.0 4/3/17 19:16 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 19:16 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 19:16 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 19:16 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 19:16 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 19:16 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 19:16 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D001711.0 4/3/17 19:16 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 19:16 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 19:16 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 19:16 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 19:16 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D001713.0 4/3/17 19:16 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129110 %Dibromofluoromethane
77-12389 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 14
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030376-02
Prism Work Order: 7030376
Time Collected: 03/22/17 14:00
Time Submitted: 03/23/17 09:30
SW-02
50-02
SWSL
Total Metals
7470A P7D025510.20 4/18/17 12:35 JABug/L 0.030Mercury0.2<0.030
6020B P7D002611.0 4/5/17 14:55 bgmug/L 0.41Antimony6<0.41
6020B P7D002611.0 4/5/17 14:55 bgmug/L 0.45Arsenic10<0.45
6020B P7D002615.0 4/5/17 14:55 bgmug/L 0.12Barium10017
6020B P7D002611.0 4/5/17 14:55 bgmug/L 0.068Beryllium1<0.068
6020B P7D002611.0 4/5/17 14:55 bgmug/L 0.053Cadmium1<0.053
6020B P7D002611.0 4/5/17 14:55 bgmJug/L 0.32Chromium100.64
6020B P7D002611.0 4/5/17 14:55 bgmJug/L 0.056Cobalt100.24
6020B P7D002615.0 4/5/17 14:55 bgmJug/L 0.41Copper102.9
6020B P7D002611.0 4/5/17 14:55 bgmJug/L 0.061Lead100.65
6020B P7D002612.0 4/5/17 14:55 bgmJug/L 0.082Nickel501.0
6020B P7D002615.0 4/5/17 14:55 bgmug/L 0.45Selenium10<0.45
6020B P7D002615.0 4/5/17 14:55 bgmug/L 0.067Silver10<0.067
6020B P7D002611.0 4/5/17 14:55 bgmJug/L 0.018Thallium5.50.050
6020B P7D002611.0 4/5/17 14:55 bgmug/L 0.79Vanadium25<0.79
6020B P7D00261104/5/17 14:55 bgmBug/L 1.3Zinc1011
Volatile Organic Compounds by GC/MS
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7D001711.0 4/3/17 19:50 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7D001712.0 4/3/17 19:50 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7D001715.0 4/3/17 19:50 KDMug/L 0.31Acetone100<0.31
8260B P7D00171204/3/17 19:50 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.048Benzene1<0.048
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7D001711.0 4/3/17 19:50 KDMug/L 0.040Bromoform3<0.040
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 14
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030376-02
Prism Work Order: 7030376
Time Collected: 03/22/17 14:00
Time Submitted: 03/23/17 09:30
SW-02
50-02
SWSL
8260B P7D001711.0 4/3/17 19:50 KDMug/L 0.18Bromomethane10<0.18
8260B P7D001715.0 4/3/17 19:50 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.22Chloroethane10<0.22
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.076Chloroform5<0.076
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.079Chloromethane1<0.079
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.065Dibromomethane10<0.065
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7D001711.0 4/3/17 19:50 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7D001715.0 4/3/17 19:50 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7D001715.0 4/3/17 19:50 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7D001715.0 4/3/17 19:50 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7D001715.0 4/3/17 19:50 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7D001711.0 4/3/17 19:50 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.044o-Xylene NE<0.044
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.047Styrene1<0.047
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7D00171104/3/17 19:50 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.044Toluene1<0.044
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7D00171104/3/17 19:50 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7D001712.0 4/3/17 19:50 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7D001710.50 4/3/17 19:50 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7D001713.0 4/3/17 19:50 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129124 %Dibromofluoromethane
77-12391 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 14
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030376
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
Blank (P7D0017-BLK1)Prepared & Analyzed: 04/03/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 14
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030376
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
Blank (P7D0017-BLK1)Prepared & Analyzed: 04/03/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10854.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9045.0
LCS (P7D0017-BS1)Prepared & Analyzed: 04/03/17
1,1,1,2-Tetrachloroethane ug/L20.5 0.50 20.00 79-134102
1,1,1-Trichloroethane ug/L24.5 0.50 20.00 75-136122
1,1,2,2-Tetrachloroethane ug/L18.2 0.50 20.00 62-12791
1,1,2-Trichloroethane ug/L22.2 0.50 20.00 70-140111
1,1-Dichloroethane ug/L22.8 0.50 20.00 78-130114
1,1-Dichloroethylene ug/L25.2 0.50 20.00 70-154126
1,2,3-Trichloropropane ug/L19.6 1.0 20.00 71-12798
1,2-Dibromo-3-chloropropane ug/L18.5 2.0 20.00 63-13492
1,2-Dibromoethane ug/L20.2 0.50 20.00 77-135101
1,2-Dichlorobenzene ug/L19.6 0.50 20.00 78-12898
1,2-Dichloroethane ug/L24.0 0.50 20.00 68-131120
1,2-Dichloropropane ug/L22.3 0.50 20.00 77-130111
1,4-Dichlorobenzene ug/L18.9 0.50 20.00 75-12695
Acetone ug/L44.5 5.0 40.00 40-166111
Acrylonitrile ug/L47.3 20 40.00 81-127118
Benzene ug/L23.4 0.50 20.00 77-128117
Bromochloromethane ug/L23.1 0.50 20.00 78-135116
Bromodichloromethane ug/L22.6 0.50 20.00 76-138113
Bromoform ug/L20.0 1.0 20.00 71-135100
Bromomethane ug/L24.6 1.0 20.00 41-168123
Carbon disulfide ug/L24.9 5.0 20.00 59-135125
Carbon Tetrachloride ug/L23.4 0.50 20.00 72-142117
Chlorobenzene ug/L20.1 0.50 20.00 78-119101
Chloroethane ug/L24.8 0.50 20.00 57-142124
Chloroform ug/L22.6 0.50 20.00 77-130113
Chloromethane ug/L22.8 0.50 20.00 47-145114
cis-1,2-Dichloroethylene ug/L24.1 0.50 20.00 76-141120
cis-1,3-Dichloropropylene ug/L23.3 0.50 20.00 65-140116
Dibromochloromethane ug/L20.4 0.50 20.00 75-134102
Dibromomethane ug/L22.2 0.50 20.00 76-138111
Ethylbenzene ug/L20.5 0.50 20.00 80-127103
m,p-Xylenes ug/L42.8 1.0 40.00 77-133107
Methyl Butyl Ketone (2-Hexanone)ug/L19.3 5.0 20.00 64-13797
Methyl Ethyl Ketone (2-Butanone)ug/L22.3 5.0 20.00 71-134111
Methyl Iodide ug/L23.8 5.0 20.00 70-130119
Methyl Isobutyl Ketone ug/L20.2 5.0 20.00 69-134101
Methylene Chloride ug/L22.0 1.0 20.00 73-131110
o-Xylene ug/L20.4 0.50 20.00 78-128102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 14
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030376
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
LCS (P7D0017-BS1)Prepared & Analyzed: 04/03/17
Styrene ug/L19.2 0.50 20.00 78-12996
Tetrachloroethylene ug/L21.0 0.50 20.00 80-129105
Tetrahydrofuran ug/L22.8 10 20.00 70-130114
Toluene ug/L21.7 0.50 20.00 76-131108
trans-1,2-Dichloroethylene ug/L23.2 0.50 20.00 76-135116
trans-1,3-Dichloropropylene ug/L23.0 0.50 20.00 67-140115
trans-1,4-Dichloro-2-butene ug/L20.1 10 20.00 70-130101
Trichloroethylene ug/L22.5 0.50 20.00 77-133113
Trichlorofluoromethane ug/L26.2 0.50 20.00 62-148131
Vinyl acetate ug/L24.1 2.0 20.00 34-167120
Vinyl chloride ug/L25.2 0.50 20.00 57-141126
Xylenes, total ug/L63.2 3.0 60.00 77-133105
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10954.7
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.7
LCS Dup (P7D0017-BSD1)Prepared & Analyzed: 04/03/17
1,1,1,2-Tetrachloroethane ug/L19.7 0.50 20.00 2079-13499 4
1,1,1-Trichloroethane ug/L21.6 0.50 20.00 2075-136108 12
1,1,2,2-Tetrachloroethane ug/L18.9 0.50 20.00 2062-12794 3
1,1,2-Trichloroethane ug/L21.2 0.50 20.00 2070-140106 5
1,1-Dichloroethane ug/L20.8 0.50 20.00 2078-130104 9
1,1-Dichloroethylene ug/L22.8 0.50 20.00 2070-154114 10
1,2,3-Trichloropropane ug/L19.6 1.0 20.00 2071-12798 0.1
1,2-Dibromo-3-chloropropane ug/L18.3 2.0 20.00 2063-13492 0.7
1,2-Dibromoethane ug/L20.2 0.50 20.00 2077-135101 0.2
1,2-Dichlorobenzene ug/L19.4 0.50 20.00 2078-12897 1
1,2-Dichloroethane ug/L22.4 0.50 20.00 2068-131112 7
1,2-Dichloropropane ug/L21.0 0.50 20.00 2077-130105 6
1,4-Dichlorobenzene ug/L18.9 0.50 20.00 2075-12694 0.2
Acetone ug/L39.1 5.0 40.00 2040-16698 13
Acrylonitrile ug/L44.9 20 40.00 2081-127112 5
Benzene ug/L21.1 0.50 20.00 2077-128105 11
Bromochloromethane ug/L21.3 0.50 20.00 2078-135106 8
Bromodichloromethane ug/L21.6 0.50 20.00 2076-138108 5
Bromoform ug/L19.2 1.0 20.00 2071-13596 4
Bromomethane ug/L23.6 1.0 20.00 2041-168118 4
Carbon disulfide ug/L23.1 5.0 20.00 2059-135116 7
Carbon Tetrachloride ug/L20.4 0.50 20.00 2072-142102 14
Chlorobenzene ug/L19.6 0.50 20.00 2078-11998 3
Chloroethane ug/L22.8 0.50 20.00 2057-142114 8
Chloroform ug/L20.1 0.50 20.00 2077-130101 12
Chloromethane ug/L21.6 0.50 20.00 2047-145108 6
cis-1,2-Dichloroethylene ug/L21.3 0.50 20.00 2076-141107 12
cis-1,3-Dichloropropylene ug/L22.0 0.50 20.00 2065-140110 5
Dibromochloromethane ug/L20.8 0.50 20.00 2075-134104 2
Dibromomethane ug/L21.6 0.50 20.00 2076-138108 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 14
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030376
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0017 - 5030B
LCS Dup (P7D0017-BSD1)Prepared & Analyzed: 04/03/17
Ethylbenzene ug/L19.7 0.50 20.00 2080-12798 4
m,p-Xylenes ug/L41.3 1.0 40.00 2077-133103 4
Methyl Butyl Ketone (2-Hexanone)ug/L18.6 5.0 20.00 2064-13793 4
Methyl Ethyl Ketone (2-Butanone)ug/L20.9 5.0 20.00 2071-134105 6
Methyl Iodide ug/L22.0 5.0 20.00 2070-130110 8
Methyl Isobutyl Ketone ug/L22.4 5.0 20.00 2069-134112 10
Methylene Chloride ug/L20.7 1.0 20.00 2073-131103 6
o-Xylene ug/L19.9 0.50 20.00 2078-128100 2
Styrene ug/L18.6 0.50 20.00 2078-12993 3
Tetrachloroethylene ug/L20.1 0.50 20.00 2080-129100 4
Tetrahydrofuran ug/L20.9 10 20.00 2070-130104 9
Toluene ug/L21.0 0.50 20.00 2076-131105 3
trans-1,2-Dichloroethylene ug/L23.1 0.50 20.00 2076-135115 0.6
trans-1,3-Dichloropropylene ug/L22.6 0.50 20.00 2067-140113 2
trans-1,4-Dichloro-2-butene ug/L20.2 10 20.00 2070-130101 0.6
Trichloroethylene ug/L21.6 0.50 20.00 2077-133108 4
Trichlorofluoromethane ug/L23.8 0.50 20.00 2062-148119 9
Vinyl acetate ug/L22.5 2.0 20.00 2034-167112 7
Vinyl chloride ug/L22.5 0.50 20.00 2057-141112 11
Xylenes, total ug/L61.2 3.0 60.00 2077-133102 3
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9648.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9246.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 14
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030376
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0026 - 3005A
Blank (P7D0026-BLK1)Prepared: 04/04/17 Analyzed: 04/05/17
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L0.486 5.0 J
Beryllium ug/LBRL1.0
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Cobalt ug/LBRL1.0
Copper ug/L0.911 5.0 J
Lead ug/L0.308 1.0 J
Nickel ug/L0.326 2.0 J
Selenium ug/LBRL5.0
Silver ug/L0.143 5.0 J
Thallium ug/L0.0330 1.0 J
Vanadium ug/LBRL1.0
Zinc ug/L5.30 10 B, J
LCS (P7D0026-BS1)Prepared: 04/04/17 Analyzed: 04/05/17
Antimony ug/L98.0 1.0 100.0 80-12098
Arsenic ug/L1021.0 100.0 80-120102
Barium ug/L1025.0 100.0 80-120102
Beryllium ug/L1081.0 100.0 80-120108
Cadmium ug/L1021.0 100.0 80-120102
Chromium ug/L1001.0 100.0 80-120100
Cobalt ug/L1151.0 100.0 80-120115
Copper ug/L1165.0 100.0 80-120116
Lead ug/L1081.0 100.0 80-120108
Nickel ug/L1102.0 100.0 80-120110
Selenium ug/L99.1 5.0 100.0 80-12099
Silver ug/L1145.0 100.0 80-120114
Thallium ug/L1051.0 100.0 80-120105
Vanadium ug/L97.7 1.0 100.0 80-12098
Zinc ug/L110 10 100.0 B80-120110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 14
4/18/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030376
Time Submitted: 3/23/2017 9:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0255 - 7470A
Blank (P7D0255-BLK1)Prepared & Analyzed: 04/18/17
Mercury ug/LBRL0.20
LCS (P7D0255-BS1)Prepared & Analyzed: 04/18/17
Mercury ug/L9.14 0.20 9.375 80-12097
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D00267030376-01 04/04/17 7:3050 50mL mL
P7D00267030376-02 04/04/17 7:3050 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D02557030376-01 04/18/17 8:4020 30mL mL
P7D02557030376-02 04/18/17 8:4020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7D00177030376-01 04/03/17 9:5810 10mL mL
P7D00177030376-02 04/03/17 9:5810 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 14
Page 14 of 14