5601_McDowellCountyMSWLFPaceProject_SampleReport_20170227

#=CL#
February 27, 2017
LIMS USE: FR - RANDELL THOMAS
LIMS OBJECT ID: 92330164
92330164
Project:
Pace Project No.:
RE:
Mr. Randell Thomas
McDowell County Landfill
60 East Court St
Marion, NC 28752
Feb 2017 LF MW 2/15
Dear Mr. Thomas:
Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Lab ID Sample ID Matrix Date Collected Date Received
92330164001 MW-1 Water 02/15/17 14:30 02/15/17 16:45
92330164002 MW-2 Water 02/15/17 14:55 02/15/17 16:45
92330164003 MW-3 Water 02/15/17 15:10 02/15/17 16:45
92330164004 MW-4 Water 02/15/17 15:30 02/15/17 16:45
92330164005 TVL BLANK Water 02/15/17 09:00 02/15/17 16:45
92330164006 EQUIP BLANK Water 02/15/17 15:00 02/15/17 16:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92330164001 MW-1 EPA 6010 15 PASI-AJMW, SER
EPA 7470 1 PASI-AWAB
EPA 8260 63 PASI-CGAW
92330164002 MW-2 EPA 6010 15 PASI-AJMW, SER
EPA 7470 1 PASI-AWAB
EPA 8260 63 PASI-CGAW
92330164003 MW-3 EPA 6010 15 PASI-AJMW, SER
EPA 7470 1 PASI-AWAB
EPA 8260 63 PASI-CGAW
92330164004 MW-4 EPA 6010 15 PASI-AJMW, SER
EPA 7470 1 PASI-AWAB
EPA 8260 63 PASI-CGAW
92330164005 TVL BLANK EPA 8260 63 PASI-CGAW
92330164006 EQUIP BLANK EPA 6010 15 PASI-AJMW, SER
EPA 7470 1 PASI-AWAB
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-1 Lab ID:92330164001 Collected:02/15/17 14:30 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 02/15/17 14:301
Collected Date 2/15/17 02/15/17 14:301
Collected Time 14:30 02/15/17 14:301
Field pH 5.5 Std. Units 02/15/17 14:300.10 0.10 1
Field Temperature 19.0 deg C 02/15/17 14:300.50 0.50 1
Field Specific Conductance 385 umhos/cm 02/15/17 14:301.0 1.0 1
Turbidity 6.98 NTU 02/15/17 14:301.0 1.0 1
Odor No Oder 02/15/17 14:301
Appearance Clear 02/15/17 14:301
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 02/24/17 15:02 7440-36-002/18/17 01:005.0 3.9 1
Arsenic 5.0U ug/L 02/24/17 15:02 7440-38-202/18/17 01:0010.0 5.0 1
Barium 192 ug/L 02/24/17 15:02 7440-39-302/18/17 01:005.0 2.5 1
Beryllium 0.50U ug/L 02/24/17 15:02 7440-41-702/18/17 01:001.0 0.50 1
Cadmium 0.50U ug/L 02/24/17 15:02 7440-43-902/18/17 01:001.0 0.50 1
Chromium 2.5U ug/L 02/24/17 15:02 7440-47-302/18/17 01:005.0 2.5 1
Cobalt 2.7J ug/L 02/24/17 15:02 7440-48-402/18/17 01:005.0 2.5 1
Copper 2.5U ug/L 02/24/17 15:02 7440-50-802/18/17 01:005.0 2.5 1
Lead 2.5U ug/L 02/24/17 15:02 7439-92-102/18/17 01:005.0 2.5 1
Nickel 2.5U ug/L 02/24/17 15:02 7440-02-002/18/17 01:005.0 2.5 1
Selenium 5.0U ug/L 02/24/17 15:02 7782-49-202/18/17 01:0010.0 5.0 1
Silver 2.5U ug/L 02/24/17 15:02 7440-22-402/18/17 01:005.0 2.5 1
Thallium 5.0U ug/L 02/25/17 07:37 7440-28-002/18/17 01:0010.0 5.0 1
Vanadium 2.5U ug/L 02/24/17 15:02 7440-62-202/18/17 01:005.0 2.5 1
Zinc 13.0 ug/L 02/24/17 15:02 7440-66-602/18/17 01:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/23/17 17:19 7439-97-602/22/17 07:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 02/21/17 14:39 67-64-125.0 10.0 1
Benzene 0.25U ug/L 02/21/17 14:39 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 02/21/17 14:39 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 02/21/17 14:39 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 02/21/17 14:39 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 02/21/17 14:39 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 02/21/17 14:39 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 02/21/17 14:39 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 02/21/17 14:39 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 02/21/17 14:39 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 02/21/17 14:39 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 02/21/17 14:39 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 02/21/17 14:39 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 02/21/17 14:39 95-49-81.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-1 Lab ID:92330164001 Collected:02/15/17 14:30 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
4-Chlorotoluene 0.31U ug/L 02/21/17 14:39 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 02/21/17 14:39 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 02/21/17 14:39 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 02/21/17 14:39 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 02/21/17 14:39 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 02/21/17 14:39 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 02/21/17 14:39 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 02/21/17 14:39 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 02/21/17 14:39 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 02/21/17 14:39 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 02/21/17 14:39 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 02/21/17 14:39 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 02/21/17 14:39 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 02/21/17 14:39 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 02/21/17 14:39 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 02/21/17 14:39 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 02/21/17 14:39 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 02/21/17 14:39 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 02/21/17 14:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 02/21/17 14:39 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 02/21/17 14:39 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 02/21/17 14:39 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 02/21/17 14:39 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 02/21/17 14:39 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 02/21/17 14:39 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 02/21/17 14:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 02/21/17 14:39 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 02/21/17 14:39 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 02/21/17 14:39 91-20-31.0 0.24 1
Styrene 0.26U ug/L 02/21/17 14:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 02/21/17 14:39 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 02/21/17 14:39 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 02/21/17 14:39 127-18-41.0 0.46 1
Toluene 0.26U ug/L 02/21/17 14:39 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 02/21/17 14:39 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 02/21/17 14:39 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 02/21/17 14:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 02/21/17 14:39 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 02/21/17 14:39 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 02/21/17 14:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 02/21/17 14:39 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 02/21/17 14:39 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 02/21/17 14:39 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 02/21/17 14:39 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 02/21/17 14:39 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 02/21/17 14:39 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-1 Lab ID:92330164001 Collected:02/15/17 14:30 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
4-Bromofluorobenzene (S)97 %02/21/17 14:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %02/21/17 14:39 17060-07-070-130 1
Toluene-d8 (S)99 %02/21/17 14:39 2037-26-570-130 1
Sample:MW-2 Lab ID:92330164002 Collected:02/15/17 14:55 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 02/15/17 14:551
Collected Date 2/15/17 02/15/17 14:551
Collected Time 14:55 02/15/17 14:551
Field pH 6.1 Std. Units 02/15/17 14:550.10 0.10 1
Field Temperature 15.6 deg C 02/15/17 14:550.50 0.50 1
Field Specific Conductance 802 umhos/cm 02/15/17 14:551.0 1.0 1
Turbidity 4.20 NTU 02/15/17 14:551.0 1.0 1
Odor Organic
Oder
02/15/17 14:551
Appearance Clear 02/15/17 14:551
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 02/24/17 15:05 7440-36-002/18/17 01:005.0 3.9 1
Arsenic 5.0U ug/L 02/24/17 15:05 7440-38-202/18/17 01:0010.0 5.0 1
Barium 171 ug/L 02/24/17 15:05 7440-39-302/18/17 01:005.0 2.5 1
Beryllium 0.50U ug/L 02/24/17 15:05 7440-41-702/18/17 01:001.0 0.50 1
Cadmium 0.50U ug/L 02/24/17 15:05 7440-43-902/18/17 01:001.0 0.50 1
Chromium 4.6J ug/L 02/24/17 15:05 7440-47-302/18/17 01:005.0 2.5 1
Cobalt 28.4 ug/L 02/24/17 15:05 7440-48-402/18/17 01:005.0 2.5 1
Copper 2.5U ug/L 02/24/17 15:05 7440-50-802/18/17 01:005.0 2.5 1
Lead 4.6J ug/L 02/24/17 15:05 7439-92-102/18/17 01:005.0 2.5 1
Nickel 8.7 ug/L 02/24/17 15:05 7440-02-002/18/17 01:005.0 2.5 1
Selenium 5.0U ug/L 02/24/17 15:05 7782-49-202/18/17 01:0010.0 5.0 1
Silver 2.5U ug/L 02/24/17 15:05 7440-22-402/18/17 01:005.0 2.5 1
Thallium 5.0U ug/L 02/25/17 07:49 7440-28-002/18/17 01:0010.0 5.0 1
Vanadium 3.4J ug/L 02/24/17 15:05 7440-62-202/18/17 01:005.0 2.5 1
Zinc 17.6 ug/L 02/24/17 15:05 7440-66-602/18/17 01:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/23/17 17:22 7439-97-602/22/17 07:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 02/21/17 14:56 67-64-125.0 10.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-2 Lab ID:92330164002 Collected:02/15/17 14:55 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene 2.6 ug/L 02/21/17 14:56 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 02/21/17 14:56 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 02/21/17 14:56 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 02/21/17 14:56 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 02/21/17 14:56 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 02/21/17 14:56 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 02/21/17 14:56 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 02/21/17 14:56 56-23-51.0 0.25 1
Chlorobenzene 4.4 ug/L 02/21/17 14:56 108-90-71.0 0.23 1
Chloroethane 0.86J ug/L 02/21/17 14:56 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 02/21/17 14:56 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 02/21/17 14:56 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 02/21/17 14:56 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 02/21/17 14:56 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 02/21/17 14:56 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 02/21/17 14:56 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 02/21/17 14:56 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 02/21/17 14:56 74-95-31.0 0.21 1
1,2-Dichlorobenzene 2.8 ug/L 02/21/17 14:56 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 02/21/17 14:56 541-73-11.0 0.24 1
1,4-Dichlorobenzene 8.3 ug/L 02/21/17 14:56 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 02/21/17 14:56 75-71-81.0 0.21 1
1,1-Dichloroethane 1.3 ug/L 02/21/17 14:56 75-34-31.0 0.32 1
1,2-Dichloroethane 0.34J ug/L 02/21/17 14:56 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 02/21/17 14:56 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 28.2 ug/L 02/21/17 14:56 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 02/21/17 14:56 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 02/21/17 14:56 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 02/21/17 14:56 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 02/21/17 14:56 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 02/21/17 14:56 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 02/21/17 14:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 02/21/17 14:56 10061-02-61.0 0.26 1
Diisopropyl ether 1.4 ug/L 02/21/17 14:56 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 02/21/17 14:56 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 02/21/17 14:56 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 02/21/17 14:56 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 02/21/17 14:56 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 02/21/17 14:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 02/21/17 14:56 108-10-15.0 0.33 1
Methyl-tert-butyl ether 1.2 ug/L 02/21/17 14:56 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 02/21/17 14:56 91-20-31.0 0.24 1
Styrene 0.26U ug/L 02/21/17 14:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 02/21/17 14:56 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 02/21/17 14:56 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 02/21/17 14:56 127-18-41.0 0.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-2 Lab ID:92330164002 Collected:02/15/17 14:55 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Toluene 0.26U ug/L 02/21/17 14:56 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 02/21/17 14:56 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.71J ug/L 02/21/17 14:56 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 02/21/17 14:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 02/21/17 14:56 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 02/21/17 14:56 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 02/21/17 14:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 02/21/17 14:56 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 02/21/17 14:56 108-05-42.0 0.35 1
Vinyl chloride 1.3 ug/L 02/21/17 14:56 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 02/21/17 14:56 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 02/21/17 14:56 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 02/21/17 14:56 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/21/17 14:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/21/17 14:56 17060-07-070-130 1
Toluene-d8 (S)100 %02/21/17 14:56 2037-26-570-130 1
Sample:MW-3 Lab ID:92330164003 Collected:02/15/17 15:10 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 02/15/17 15:101
Collected Date 2/15/17 02/15/17 15:101
Collected Time 15:10 02/15/17 15:101
Field pH 6.5 Std. Units 02/15/17 15:100.10 0.10 1
Field Temperature 15.6 deg C 02/15/17 15:100.50 0.50 1
Field Specific Conductance 850 umhos/cm 02/15/17 15:101.0 1.0 1
Turbidity 27.11 NTU 02/15/17 15:101.0 1.0 1
Odor Organic
Oder 02/15/17 15:101
Appearance Opaque 02/15/17 15:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 02/24/17 15:08 7440-36-002/18/17 01:005.0 3.9 1
Arsenic 5.0U ug/L 02/24/17 15:08 7440-38-202/18/17 01:0010.0 5.0 1
Barium 1060 ug/L 02/24/17 15:08 7440-39-302/18/17 01:005.0 2.5 1
Beryllium 1.3 ug/L 02/24/17 15:08 7440-41-702/18/17 01:001.0 0.50 1
Cadmium 0.50U ug/L 02/24/17 15:08 7440-43-902/18/17 01:001.0 0.50 1
Chromium 2.5U ug/L 02/24/17 15:08 7440-47-302/18/17 01:005.0 2.5 1
Cobalt 11.1 ug/L 02/24/17 15:08 7440-48-402/18/17 01:005.0 2.5 1
Copper 2.5U ug/L 02/24/17 15:08 7440-50-802/18/17 01:005.0 2.5 1
Lead 5.0J ug/L 02/24/17 15:08 7439-92-102/18/17 01:005.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-3 Lab ID:92330164003 Collected:02/15/17 15:10 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Nickel 4.1J ug/L 02/24/17 15:08 7440-02-002/18/17 01:005.0 2.5 1
Selenium 5.0U ug/L 02/24/17 15:08 7782-49-202/18/17 01:0010.0 5.0 1
Silver 2.5U ug/L 02/24/17 15:08 7440-22-402/18/17 01:005.0 2.5 1
Thallium 5.0U ug/L 02/25/17 07:52 7440-28-002/18/17 01:0010.0 5.0 1
Vanadium 3.3J ug/L 02/24/17 15:08 7440-62-202/18/17 01:005.0 2.5 1
Zinc 20.3 ug/L 02/24/17 15:08 7440-66-602/18/17 01:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/23/17 17:24 7439-97-602/22/17 07:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 02/21/17 15:13 67-64-125.0 10.0 1
Benzene 0.25U ug/L 02/21/17 15:13 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 02/21/17 15:13 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 02/21/17 15:13 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 02/21/17 15:13 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 02/21/17 15:13 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 02/21/17 15:13 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 02/21/17 15:13 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 02/21/17 15:13 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 02/21/17 15:13 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 02/21/17 15:13 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 02/21/17 15:13 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 02/21/17 15:13 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 02/21/17 15:13 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 02/21/17 15:13 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 02/21/17 15:13 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 02/21/17 15:13 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 02/21/17 15:13 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 02/21/17 15:13 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 02/21/17 15:13 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 02/21/17 15:13 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 02/21/17 15:13 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 02/21/17 15:13 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 02/21/17 15:13 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 02/21/17 15:13 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 02/21/17 15:13 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 02/21/17 15:13 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 02/21/17 15:13 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 02/21/17 15:13 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 02/21/17 15:13 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 02/21/17 15:13 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 02/21/17 15:13 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 02/21/17 15:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 02/21/17 15:13 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 02/21/17 15:13 108-20-31.0 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-3 Lab ID:92330164003 Collected:02/15/17 15:10 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene 0.30U ug/L 02/21/17 15:13 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 02/21/17 15:13 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 02/21/17 15:13 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 02/21/17 15:13 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 02/21/17 15:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 02/21/17 15:13 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 02/21/17 15:13 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 02/21/17 15:13 91-20-31.0 0.24 1
Styrene 0.26U ug/L 02/21/17 15:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 02/21/17 15:13 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 02/21/17 15:13 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 02/21/17 15:13 127-18-41.0 0.46 1
Toluene 0.26U ug/L 02/21/17 15:13 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 02/21/17 15:13 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 02/21/17 15:13 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 02/21/17 15:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 02/21/17 15:13 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 02/21/17 15:13 79-01-61.0 0.47 1
Trichlorofluoromethane 0.43J ug/L 02/21/17 15:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 02/21/17 15:13 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 02/21/17 15:13 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 02/21/17 15:13 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 02/21/17 15:13 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 02/21/17 15:13 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 02/21/17 15:13 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)99 %02/21/17 15:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %02/21/17 15:13 17060-07-070-130 1
Toluene-d8 (S)101 %02/21/17 15:13 2037-26-570-130 1
Sample:MW-4 Lab ID:92330164004 Collected:02/15/17 15:30 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 02/15/17 15:301
Collected Date 2/15/17 02/15/17 15:301
Collected Time 15:30 02/15/17 15:301
Field pH 6.6 Std. Units 02/15/17 15:300.10 0.10 1
Field Temperature 14.8 deg C 02/15/17 15:300.50 0.50 1
Field Specific Conductance 103 umhos/cm 02/15/17 15:301.0 1.0 1
Turbidity 5.20 NTU 02/15/17 15:301.0 1.0 1
Odor No Oder 02/15/17 15:301
Appearance Clear 02/15/17 15:301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-4 Lab ID:92330164004 Collected:02/15/17 15:30 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 02/24/17 15:11 7440-36-002/18/17 01:005.0 3.9 1
Arsenic 5.0U ug/L 02/24/17 15:11 7440-38-202/18/17 01:0010.0 5.0 1
Barium 52.0 ug/L 02/24/17 15:11 7440-39-302/18/17 01:005.0 2.5 1
Beryllium 0.50U ug/L 02/24/17 15:11 7440-41-702/18/17 01:001.0 0.50 1
Cadmium 0.50U ug/L 02/24/17 15:11 7440-43-902/18/17 01:001.0 0.50 1
Chromium 2.5U ug/L 02/24/17 15:11 7440-47-302/18/17 01:005.0 2.5 1
Cobalt 2.5U ug/L 02/24/17 15:11 7440-48-402/18/17 01:005.0 2.5 1
Copper 2.5U ug/L 02/24/17 15:11 7440-50-802/18/17 01:005.0 2.5 1
Lead 2.5U ug/L 02/24/17 15:11 7439-92-102/18/17 01:005.0 2.5 1
Nickel 2.5U ug/L 02/24/17 15:11 7440-02-002/18/17 01:005.0 2.5 1
Selenium 5.0U ug/L 02/24/17 15:11 7782-49-202/18/17 01:0010.0 5.0 1
Silver 2.5U ug/L 02/24/17 15:11 7440-22-402/18/17 01:005.0 2.5 1
Thallium 5.0U ug/L 02/25/17 07:55 7440-28-002/18/17 01:0010.0 5.0 1
Vanadium 4.1J ug/L 02/24/17 15:11 7440-62-202/18/17 01:005.0 2.5 1
Zinc 5.0U ug/L 02/24/17 15:11 7440-66-602/18/17 01:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/23/17 17:31 7439-97-602/22/17 07:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 02/21/17 15:30 67-64-125.0 10.0 1
Benzene 0.25U ug/L 02/21/17 15:30 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 02/21/17 15:30 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 02/21/17 15:30 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 02/21/17 15:30 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 02/21/17 15:30 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 02/21/17 15:30 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 02/21/17 15:30 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 02/21/17 15:30 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 02/21/17 15:30 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 02/21/17 15:30 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 02/21/17 15:30 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 02/21/17 15:30 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 02/21/17 15:30 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 02/21/17 15:30 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 02/21/17 15:30 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 02/21/17 15:30 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 02/21/17 15:30 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 02/21/17 15:30 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 02/21/17 15:30 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 02/21/17 15:30 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 02/21/17 15:30 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 02/21/17 15:30 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 02/21/17 15:30 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 02/21/17 15:30 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 02/21/17 15:30 75-35-41.0 0.56 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:MW-4 Lab ID:92330164004 Collected:02/15/17 15:30 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,2-Dichloroethene 0.19U ug/L 02/21/17 15:30 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 02/21/17 15:30 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 02/21/17 15:30 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 02/21/17 15:30 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 02/21/17 15:30 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 02/21/17 15:30 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 02/21/17 15:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 02/21/17 15:30 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 02/21/17 15:30 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 02/21/17 15:30 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 02/21/17 15:30 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 02/21/17 15:30 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 02/21/17 15:30 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 02/21/17 15:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 02/21/17 15:30 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 02/21/17 15:30 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 02/21/17 15:30 91-20-31.0 0.24 1
Styrene 0.26U ug/L 02/21/17 15:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 02/21/17 15:30 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 02/21/17 15:30 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 02/21/17 15:30 127-18-41.0 0.46 1
Toluene 0.26U ug/L 02/21/17 15:30 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 02/21/17 15:30 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 02/21/17 15:30 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 02/21/17 15:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 02/21/17 15:30 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 02/21/17 15:30 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 02/21/17 15:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 02/21/17 15:30 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 02/21/17 15:30 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 02/21/17 15:30 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 02/21/17 15:30 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 02/21/17 15:30 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 02/21/17 15:30 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %02/21/17 15:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %02/21/17 15:30 17060-07-070-130 1
Toluene-d8 (S)94 %02/21/17 15:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:TVL BLANK Lab ID:92330164005 Collected:02/15/17 09:00 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 02/21/17 10:40 67-64-125.0 10.0 1
Benzene 0.25U ug/L 02/21/17 10:40 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 02/21/17 10:40 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 02/21/17 10:40 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 02/21/17 10:40 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 02/21/17 10:40 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 02/21/17 10:40 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 02/21/17 10:40 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 02/21/17 10:40 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 02/21/17 10:40 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 02/21/17 10:40 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 02/21/17 10:40 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 02/21/17 10:40 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 02/21/17 10:40 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 02/21/17 10:40 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 02/21/17 10:40 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 02/21/17 10:40 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 02/21/17 10:40 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 02/21/17 10:40 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 02/21/17 10:40 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 02/21/17 10:40 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 02/21/17 10:40 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 02/21/17 10:40 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 02/21/17 10:40 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 02/21/17 10:40 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 02/21/17 10:40 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 02/21/17 10:40 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 02/21/17 10:40 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 02/21/17 10:40 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 02/21/17 10:40 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 02/21/17 10:40 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 02/21/17 10:40 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 02/21/17 10:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 02/21/17 10:40 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 02/21/17 10:40 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 02/21/17 10:40 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 02/21/17 10:40 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 02/21/17 10:40 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 02/21/17 10:40 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 02/21/17 10:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 02/21/17 10:40 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 02/21/17 10:40 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 02/21/17 10:40 91-20-31.0 0.24 1
Styrene 0.26U ug/L 02/21/17 10:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 02/21/17 10:40 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 02/21/17 10:40 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:TVL BLANK Lab ID:92330164005 Collected:02/15/17 09:00 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 02/21/17 10:40 127-18-41.0 0.46 1
Toluene 0.26U ug/L 02/21/17 10:40 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 02/21/17 10:40 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 02/21/17 10:40 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 02/21/17 10:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 02/21/17 10:40 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 02/21/17 10:40 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 02/21/17 10:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 02/21/17 10:40 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 02/21/17 10:40 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 02/21/17 10:40 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 02/21/17 10:40 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 02/21/17 10:40 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 02/21/17 10:40 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)96 %02/21/17 10:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %02/21/17 10:40 17060-07-070-130 1
Toluene-d8 (S)104 %02/21/17 10:40 2037-26-570-130 1
Sample:EQUIP BLANK Lab ID:92330164006 Collected:02/15/17 15:00 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 02/24/17 15:14 7440-36-002/18/17 01:005.0 3.9 1
Arsenic 5.0U ug/L 02/24/17 15:14 7440-38-202/18/17 01:0010.0 5.0 1
Barium 2.5U ug/L 02/24/17 15:14 7440-39-302/18/17 01:005.0 2.5 1
Beryllium 0.50U ug/L 02/24/17 15:14 7440-41-702/18/17 01:001.0 0.50 1
Cadmium 0.50U ug/L 02/24/17 15:14 7440-43-902/18/17 01:001.0 0.50 1
Chromium 2.5U ug/L 02/24/17 15:14 7440-47-302/18/17 01:005.0 2.5 1
Cobalt 2.5U ug/L 02/24/17 15:14 7440-48-402/18/17 01:005.0 2.5 1
Copper 2.5U ug/L 02/24/17 15:14 7440-50-802/18/17 01:005.0 2.5 1
Lead 2.5U ug/L 02/24/17 15:14 7439-92-102/18/17 01:005.0 2.5 1
Nickel 2.5U ug/L 02/24/17 15:14 7440-02-002/18/17 01:005.0 2.5 1
Selenium 5.0U ug/L 02/24/17 15:14 7782-49-202/18/17 01:0010.0 5.0 1
Silver 2.5U ug/L 02/24/17 15:14 7440-22-402/18/17 01:005.0 2.5 1
Thallium 5.0U ug/L 02/25/17 07:59 7440-28-002/18/17 01:0010.0 5.0 1
Vanadium 2.5U ug/L 02/24/17 15:14 7440-62-202/18/17 01:005.0 2.5 1
Zinc 5.0U ug/L 02/24/17 15:14 7440-66-602/18/17 01:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/23/17 17:33 7439-97-602/22/17 07:000.20 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:EQUIP BLANK Lab ID:92330164006 Collected:02/15/17 15:00 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 02/21/17 10:57 67-64-125.0 10.0 1
Benzene 0.25U ug/L 02/21/17 10:57 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 02/21/17 10:57 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 02/21/17 10:57 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 02/21/17 10:57 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 02/21/17 10:57 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 02/21/17 10:57 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 02/21/17 10:57 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 02/21/17 10:57 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 02/21/17 10:57 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 02/21/17 10:57 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 02/21/17 10:57 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 02/21/17 10:57 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 02/21/17 10:57 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 02/21/17 10:57 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 02/21/17 10:57 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 02/21/17 10:57 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 02/21/17 10:57 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 02/21/17 10:57 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 02/21/17 10:57 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 02/21/17 10:57 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 02/21/17 10:57 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 02/21/17 10:57 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 02/21/17 10:57 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 02/21/17 10:57 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 02/21/17 10:57 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 02/21/17 10:57 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 02/21/17 10:57 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 02/21/17 10:57 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 02/21/17 10:57 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 02/21/17 10:57 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 02/21/17 10:57 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 02/21/17 10:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 02/21/17 10:57 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 02/21/17 10:57 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 02/21/17 10:57 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 02/21/17 10:57 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 02/21/17 10:57 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 02/21/17 10:57 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 02/21/17 10:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 02/21/17 10:57 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 02/21/17 10:57 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 02/21/17 10:57 91-20-31.0 0.24 1
Styrene 0.26U ug/L 02/21/17 10:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 02/21/17 10:57 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 02/21/17 10:57 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Asheville, NC 28804
[phone]
Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Sample:EQUIP BLANK Lab ID:92330164006 Collected:02/15/17 15:00 Received:02/15/17 16:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 02/21/17 10:57 127-18-41.0 0.46 1
Toluene 0.26U ug/L 02/21/17 10:57 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 02/21/17 10:57 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 02/21/17 10:57 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 02/21/17 10:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 02/21/17 10:57 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 02/21/17 10:57 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 02/21/17 10:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 02/21/17 10:57 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 02/21/17 10:57 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 02/21/17 10:57 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 02/21/17 10:57 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 02/21/17 10:57 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 02/21/17 10:57 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)96 %02/21/17 10:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %02/21/17 10:57 17060-07-070-130 1
Toluene-d8 (S)93 %02/21/17 10:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349177
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936998
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164006
Matrix:Water
AnalyzedMDL
Mercury ug/L 0.10U 0.20 02/23/17 17:030.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936999LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1937000MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330396004
1937001
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 93 75-12591 1 252.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
348742
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1934817
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164006
Matrix:Water
AnalyzedMDL
Antimony ug/L 3.9U 5.0 02/24/17 14:163.9
Arsenic ug/L 5.0U 10.0 02/24/17 14:165.0
Barium ug/L 2.5U 5.0 02/24/17 14:162.5
Beryllium ug/L 0.50U 1.0 02/24/17 14:160.50
Cadmium ug/L 0.50U 1.0 02/24/17 14:160.50
Chromium ug/L 2.5U 5.0 02/24/17 14:162.5
Cobalt ug/L 2.5U 5.0 02/24/17 14:162.5
Copper ug/L 2.5U 5.0 02/24/17 14:162.5
Lead ug/L 2.5U 5.0 02/24/17 14:162.5
Nickel ug/L 2.5U 5.0 02/24/17 14:162.5
Selenium ug/L 5.0U 10.0 02/24/17 14:165.0
Silver ug/L 2.5U 5.0 02/24/17 14:162.5
Thallium ug/L 5.0U 10.0 02/25/17 07:225.0
Vanadium ug/L 2.5U 5.0 02/24/17 14:162.5
Zinc ug/L 5.0U 10.0 02/24/17 14:165.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1934818LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 488500 98 80-120
Arsenic ug/L 499500 100 80-120
Barium ug/L 455500 91 80-120
Beryllium ug/L 441500 88 80-120
Cadmium ug/L 480500 96 80-120
Chromium ug/L 489500 98 80-120
Cobalt ug/L 481500 96 80-120
Copper ug/L 502500 100 80-120
Lead ug/L 477500 95 80-120
Nickel ug/L 473500 95 80-120
Selenium ug/L 488500 98 80-120
Silver ug/L 236250 94 80-120
Thallium ug/L 453500 91 80-120
Vanadium ug/L 433500 87 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1934819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92330340003
1934820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-125101 2 20500ND494506
Arsenic ug/L 500 101 75-125104 2 20500ND508521
Barium ug/L 500 90 75-12590 1 2050089.0J 541 537
Beryllium ug/L 500 89 75-12587 2 20500ND444437
Cadmium ug/L 500 96 75-12599 3 20500ND482495
Chromium ug/L 500 98 75-125102 3 20500ND492510
Cobalt ug/L 500 95 75-12597 3 20500ND474488
Copper ug/L 500 102 75-125103 1 205003.2J 511 518
Lead ug/L 500 94 75-12597 3 20500ND470486
Nickel ug/L 500 93 75-12596 3 20500ND465479
Selenium ug/L 500 97 75-12599 2 20500ND486494
Silver ug/L 250 96 75-12598 2 20250ND239245
Thallium ug/L 500 89 75-12593 5 20500ND443464
Vanadium ug/L 500 89 75-12591 3 205005.2J 449 461
Zinc ug/L 500 93 75-12596 4 205005.4J 471 487
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
349146
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164005, 92330164006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936802
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164005, 92330164006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L 0.33U 1.0 02/21/17 10:060.33
1,1,1-Trichloroethane ug/L 0.48U 1.0 02/21/17 10:060.48
1,1,2,2-Tetrachloroethane ug/L 0.40U 1.0 02/21/17 10:060.40
1,1,2-Trichloroethane ug/L 0.29U 1.0 02/21/17 10:060.29
1,1-Dichloroethane ug/L 0.32U 1.0 02/21/17 10:060.32
1,1-Dichloroethene ug/L 0.56U 1.0 02/21/17 10:060.56
1,1-Dichloropropene ug/L 0.49U 1.0 02/21/17 10:060.49
1,2,3-Trichlorobenzene ug/L 0.33U 1.0 02/21/17 10:060.33
1,2,3-Trichloropropane ug/L 0.41U 1.0 02/21/17 10:060.41
1,2,4-Trichlorobenzene ug/L 0.35U 1.0 02/21/17 10:060.35
1,2-Dibromo-3-chloropropane ug/L 2.0U 2.0 02/21/17 10:062.0
1,2-Dibromoethane (EDB)ug/L 0.27U 1.0 02/21/17 10:060.27
1,2-Dichlorobenzene ug/L 0.30U 1.0 02/21/17 10:060.30
1,2-Dichloroethane ug/L 0.24U 1.0 02/21/17 10:060.24
1,2-Dichloropropane ug/L 0.27U 1.0 02/21/17 10:060.27
1,3-Dichlorobenzene ug/L 0.24U 1.0 02/21/17 10:060.24
1,3-Dichloropropane ug/L 0.28U 1.0 02/21/17 10:060.28
1,4-Dichlorobenzene ug/L 0.33U 1.0 02/21/17 10:060.33
2,2-Dichloropropane ug/L 0.13U 1.0 02/21/17 10:060.13
2-Butanone (MEK)ug/L 0.96U 5.0 02/21/17 10:060.96
2-Chlorotoluene ug/L 0.35U 1.0 02/21/17 10:060.35
2-Hexanone ug/L 0.46U 5.0 02/21/17 10:060.46
4-Chlorotoluene ug/L 0.31U 1.0 02/21/17 10:060.31
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 5.0 02/21/17 10:060.33
Acetone ug/L 10.0U 25.0 02/21/17 10:0610.0
Benzene ug/L 0.25U 1.0 02/21/17 10:060.25
Bromobenzene ug/L 0.30U 1.0 02/21/17 10:060.30
Bromochloromethane ug/L 0.17U 1.0 02/21/17 10:060.17
Bromodichloromethane ug/L 0.18U 1.0 02/21/17 10:060.18
Bromoform ug/L 0.26U 1.0 02/21/17 10:060.26
Bromomethane ug/L 0.29U 2.0 02/21/17 10:060.29
Carbon tetrachloride ug/L 0.25U 1.0 02/21/17 10:060.25
Chlorobenzene ug/L 0.23U 1.0 02/21/17 10:060.23
Chloroethane ug/L 0.54U 1.0 02/21/17 10:060.54
Chloroform ug/L 0.14U 1.0 02/21/17 10:060.14
Chloromethane ug/L 0.11U 1.0 02/21/17 10:060.11
cis-1,2-Dichloroethene ug/L 0.19U 1.0 02/21/17 10:060.19
cis-1,3-Dichloropropene ug/L 0.13U 1.0 02/21/17 10:060.13
Dibromochloromethane ug/L 0.21U 1.0 02/21/17 10:060.21
Dibromomethane ug/L 0.21U 1.0 02/21/17 10:060.21
Dichlorodifluoromethane ug/L 0.21U 1.0 02/21/17 10:060.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1936802
Associated Lab Samples:92330164001, 92330164002, 92330164003, 92330164004, 92330164005, 92330164006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L 0.12U 1.0 02/21/17 10:060.12
Ethylbenzene ug/L 0.30U 1.0 02/21/17 10:060.30
Hexachloro-1,3-butadiene ug/L 0.71U 1.0 02/21/17 10:060.71
m&p-Xylene ug/L 0.66U 2.0 02/21/17 10:060.66
Methyl-tert-butyl ether ug/L 0.21U 1.0 02/21/17 10:060.21
Methylene Chloride ug/L 0.97U 1.0 02/21/17 10:060.97
Naphthalene ug/L 0.24U 1.0 02/21/17 10:060.24
o-Xylene ug/L 0.23U 1.0 02/21/17 10:060.23
p-Isopropyltoluene ug/L 0.31U 1.0 02/21/17 10:060.31
Styrene ug/L 0.26U 1.0 02/21/17 10:060.26
Tetrachloroethene ug/L 0.46U 1.0 02/21/17 10:060.46
Toluene ug/L 0.26U 1.0 02/21/17 10:060.26
trans-1,2-Dichloroethene ug/L 0.49U 1.0 02/21/17 10:060.49
trans-1,3-Dichloropropene ug/L 0.26U 1.0 02/21/17 10:060.26
Trichloroethene ug/L 0.47U 1.0 02/21/17 10:060.47
Trichlorofluoromethane ug/L 0.20U 1.0 02/21/17 10:060.20
Vinyl acetate ug/L 0.35U 2.0 02/21/17 10:060.35
Vinyl chloride ug/L 0.62U 1.0 02/21/17 10:060.62
Xylene (Total)ug/L 0.66U 1.0 02/21/17 10:060.66
1,2-Dichloroethane-d4 (S)%111 70-130 02/21/17 10:06
4-Bromofluorobenzene (S)%97 70-130 02/21/17 10:06
Toluene-d8 (S)%94 70-130 02/21/17 10:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936803LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.850 98 80-125
1,1,1-Trichloroethane ug/L 49.050 98 71-129
1,1,2,2-Tetrachloroethane ug/L 46.550 93 79-124
1,1,2-Trichloroethane ug/L 49.750 99 85-125
1,1-Dichloroethane ug/L 48.550 97 73-126
1,1-Dichloroethene ug/L 48.350 97 66-135
1,1-Dichloropropene ug/L 52.650 105 74-135
1,2,3-Trichlorobenzene ug/L 50.750 101 73-135
1,2,3-Trichloropropane ug/L 47.750 95 75-130
1,2,4-Trichlorobenzene ug/L 52.450 105 75-134
1,2-Dibromo-3-chloropropane ug/L 48.950 98 71-133
1,2-Dibromoethane (EDB)ug/L 47.750 95 83-124
1,2-Dichlorobenzene ug/L 49.250 98 80-133
1,2-Dichloroethane ug/L 47.950 96 67-128
1,2-Dichloropropane ug/L 49.750 99 75-132
1,3-Dichlorobenzene ug/L 48.650 97 77-130
1,3-Dichloropropane ug/L 48.950 98 76-131
1,4-Dichlorobenzene ug/L 48.050 96 78-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1936803LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 52.650 105 40-160
2-Butanone (MEK)ug/L 101100 101 61-144
2-Chlorotoluene ug/L 49.350 99 74-132
2-Hexanone ug/L 97.8100 98 68-143
4-Chlorotoluene ug/L 49.450 99 76-133
4-Methyl-2-pentanone (MIBK)ug/L 98.4100 98 72-135
Acetone ug/L 90.9100 91 48-146
Benzene ug/L 53.850 108 80-125
Bromobenzene ug/L 49.950 100 75-125
Bromochloromethane ug/L 49.850 100 71-125
Bromodichloromethane ug/L 50.750 101 78-124
Bromoform ug/L 47.450 95 71-128
Bromomethane ug/L 43.650 87 40-160
Carbon tetrachloride ug/L 50.550 101 69-131
Chlorobenzene ug/L 48.650 97 81-122
Chloroethane ug/L 47.750 95 39-148
Chloroform ug/L 49.350 99 73-127
Chloromethane ug/L 43.150 86 44-146
cis-1,2-Dichloroethene ug/L 49.350 99 74-124
cis-1,3-Dichloropropene ug/L 51.550 103 72-132
Dibromochloromethane ug/L 49.450 99 78-125
Dibromomethane ug/L 48.450 97 82-120
Dichlorodifluoromethane ug/L 31.150 62 34-157
Diisopropyl ether ug/L 50.950 102 69-135
Ethylbenzene ug/L 48.550 97 79-121
Hexachloro-1,3-butadiene ug/L 52.850 106 72-131
m&p-Xylene ug/L 97.8100 98 81-124
Methyl-tert-butyl ether ug/L 49.750 99 74-131
Methylene Chloride ug/L 45.850 92 64-133
Naphthalene ug/L 51.050 102 73-133
o-Xylene ug/L 49.350 99 79-131
p-Isopropyltoluene ug/L 48.550 97 80-131
Styrene ug/L 49.650 99 84-126
Tetrachloroethene ug/L 47.850 96 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 47.950 96 71-127
trans-1,3-Dichloropropene ug/L 51.550 103 69-141
Trichloroethene ug/L 48.150 96 78-122
Trichlorofluoromethane ug/L 50.550 101 53-137
Vinyl acetate ug/L 99.4100 99 40-160
Vinyl chloride ug/L 37.850 76 58-137
Xylene (Total)ug/L 147150 98 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1936805MATRIX SPIKE SAMPLE:
MSSpike
Result
92330376009
1,1,1,2-Tetrachloroethane ug/L 20.620 103 70-130ND
1,1,1-Trichloroethane ug/L 21.420 107 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.020 105 70-130ND
1,1,2-Trichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethane ug/L 21.320 106 70-130ND
1,1-Dichloroethene ug/L 22.520 113 70-166ND
1,1-Dichloropropene ug/L 23.120 116 70-130ND
1,2,3-Trichlorobenzene ug/L 20.120 100 70-130ND
1,2,3-Trichloropropane ug/L 20.420 102 70-130ND
1,2,4-Trichlorobenzene ug/L 19.520 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.920 105 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 20.320 101 70-130ND
1,2-Dichloroethane ug/L 22.420 112 70-130ND
1,2-Dichloropropane ug/L 22.320 111 70-130ND
1,3-Dichlorobenzene ug/L 20.020 100 70-130ND
1,3-Dichloropropane ug/L 21.520 107 70-130ND
1,4-Dichlorobenzene ug/L 20.120 100 70-130ND
2,2-Dichloropropane ug/L 19.920 99 70-130ND
2-Butanone (MEK)ug/L 45.340 113 70-130ND
2-Chlorotoluene ug/L 21.020 105 70-130ND
2-Hexanone ug/L 47.540 119 70-130ND
4-Chlorotoluene ug/L 20.920 105 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 47.040 118 70-130ND
Acetone ug/L 47.040 114 70-130ND
Benzene ug/L 22.220 111 70-148ND
Bromobenzene ug/L 21.420 107 70-130ND
Bromochloromethane ug/L 21.520 108 70-130ND
Bromodichloromethane ug/L 22.320 112 70-130ND
Bromoform ug/L 18.920 94 70-130ND
Bromomethane ug/L 20.720 103 70-130ND
Carbon tetrachloride ug/L 21.220 106 70-130ND
Chlorobenzene ug/L 21.420 107 70-146ND
Chloroethane ug/L 21.420 107 70-130ND
Chloroform ug/L 20.920 104 70-130ND
Chloromethane ug/L 19.920 100 70-130ND
cis-1,2-Dichloroethene ug/L 21.420 107 70-130ND
cis-1,3-Dichloropropene ug/L 21.020 105 70-130ND
Dibromochloromethane ug/L 20.220 101 70-130ND
Dibromomethane ug/L 20.420 102 70-130ND
Dichlorodifluoromethane ug/L 19.720 99 70-130ND
Diisopropyl ether ug/L 21.420 107 70-130ND
Ethylbenzene ug/L 21.320 107 70-130ND
Hexachloro-1,3-butadiene ug/L 19.520 98 70-130ND
m&p-Xylene ug/L 42.640 107 70-130ND
Methyl-tert-butyl ether ug/L 20.420 102 70-130ND
Methylene Chloride ug/L 19.620 98 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Asheville, NC 28804
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1936805MATRIX SPIKE SAMPLE:
MSSpike
Result
92330376009
Naphthalene ug/L 20.020 100 70-130ND
o-Xylene ug/L 21.420 107 70-130ND
p-Isopropyltoluene ug/L 19.820 99 70-130ND
Styrene ug/L 21.120 106 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Toluene ug/L 22.120 111 70-155ND
trans-1,2-Dichloroethene ug/L 22.720 114 70-130ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-130ND
Trichloroethene ug/L 21.320 106 69-151ND
Trichlorofluoromethane ug/L 23.320 116 70-130ND
Vinyl acetate ug/L 35.040 88 70-130ND
Vinyl chloride ug/L 17.920 90 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330376008
1936804SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L 0.33U 30ND
1,1,1-Trichloroethane ug/L 0.48U 30ND
1,1,2,2-Tetrachloroethane ug/L 0.40U 30ND
1,1,2-Trichloroethane ug/L 0.29U 30ND
1,1-Dichloroethane ug/L 0.32U 30ND
1,1-Dichloroethene ug/L 0.56U 30ND
1,1-Dichloropropene ug/L 0.49U 30ND
1,2,3-Trichlorobenzene ug/L 0.33U 30ND
1,2,3-Trichloropropane ug/L 0.41U 30ND
1,2,4-Trichlorobenzene ug/L 0.35U 30ND
1,2-Dibromo-3-chloropropane ug/L 2.0U 30ND
1,2-Dibromoethane (EDB)ug/L 0.27U 30ND
1,2-Dichlorobenzene ug/L 0.30U 30ND
1,2-Dichloroethane ug/L 0.24U 30ND
1,2-Dichloropropane ug/L 0.27U 30ND
1,3-Dichlorobenzene ug/L 0.24U 30ND
1,3-Dichloropropane ug/L 0.28U 30ND
1,4-Dichlorobenzene ug/L 0.33U 30ND
2,2-Dichloropropane ug/L 0.13U 30ND
2-Butanone (MEK)ug/L 0.96U 30ND
2-Chlorotoluene ug/L 0.35U 30ND
2-Hexanone ug/L 0.46U 30ND
4-Chlorotoluene ug/L 0.31U 30ND
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 30ND
Acetone ug/L 10.0U 30ND
Benzene ug/L 0.25U 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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2225 Riverside Dr.
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[phone]
Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92330376008
1936804SAMPLE DUPLICATE:
Bromobenzene ug/L 0.30U 30ND
Bromochloromethane ug/L 0.17U 30ND
Bromodichloromethane ug/L 0.18U 30ND
Bromoform ug/L 0.26U 30ND
Bromomethane ug/L 0.29U 30ND
Carbon tetrachloride ug/L 0.25U 30ND
Chlorobenzene ug/L 0.23U 30ND
Chloroethane ug/L 0.54U 30ND
Chloroform ug/L 0.14U 30ND
Chloromethane ug/L 0.11U 30ND
cis-1,2-Dichloroethene ug/L 0.19U 30ND
cis-1,3-Dichloropropene ug/L 0.13U 30ND
Dibromochloromethane ug/L 0.21U 30ND
Dibromomethane ug/L 0.21U 30ND
Dichlorodifluoromethane ug/L 0.21U 30ND
Diisopropyl ether ug/L 0.12U 30ND
Ethylbenzene ug/L 0.30U 30ND
Hexachloro-1,3-butadiene ug/L 0.71U 30ND
m&p-Xylene ug/L 0.66U 30ND
Methyl-tert-butyl ether ug/L 0.21U 30ND
Methylene Chloride ug/L 0.97U 30ND
Naphthalene ug/L 0.24U 30ND
o-Xylene ug/L 0.23U 30ND
p-Isopropyltoluene ug/L 0.31U 30ND
Styrene ug/L 0.26U 30ND
Tetrachloroethene ug/L 0.46U 30ND
Toluene ug/L 0.26U 30ND
trans-1,2-Dichloroethene ug/L 0.49U 30ND
trans-1,3-Dichloropropene ug/L 0.26U 30ND
Trichloroethene ug/L 0.47U 30ND
Trichlorofluoromethane ug/L 0.20U 30ND
Vinyl acetate ug/L 0.35U 30ND
Vinyl chloride ug/L 0.62U 30ND
Xylene (Total)ug/L 0.66U 30ND
1,2-Dichloroethane-d4 (S)%104 1103
4-Bromofluorobenzene (S)%98 199
Toluene-d8 (S)%100 2102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Asheville, NC 28804
[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
Pace Analytical Services, LLC
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[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92330164
Feb 2017 LF MW 2/15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92330164001 MW-1
92330164002 MW-2
92330164003 MW-3
92330164004 MW-4
92330164001 348742 348902MW-1 EPA 3010A EPA 6010
92330164002 348742 348902MW-2 EPA 3010A EPA 6010
92330164003 348742 348902MW-3 EPA 3010A EPA 6010
92330164004 348742 348902MW-4 EPA 3010A EPA 6010
92330164006 348742 348902EQUIP BLANK EPA 3010A EPA 6010
92330164001 349177 349284MW-1 EPA 7470 EPA 7470
92330164002 349177 349284MW-2 EPA 7470 EPA 7470
92330164003 349177 349284MW-3 EPA 7470 EPA 7470
92330164004 349177 349284MW-4 EPA 7470 EPA 7470
92330164006 349177 349284EQUIP BLANK EPA 7470 EPA 7470
92330164001 349146MW-1 EPA 8260
92330164002 349146MW-2 EPA 8260
92330164003 349146MW-3 EPA 8260
92330164004 349146MW-4 EPA 8260
92330164005 349146TVL BLANK EPA 8260
92330164006 349146EQUIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2017 03:40 PM
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Asheville, NC 28804
[phone]
Page 28 of 31
Page 29 of 31
Page 30 of 31
Page 31 of 31