6001_MecklenburgCoHarrisburgMSWLF_GWMR_20180105

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#PENCE HARRISBURGV
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60-01 Harrisburg Rd Landfill Methane Wells
P-3
µ2017 Aerial Photo
#=CL#
December 22, 2017
LIMS USE: FR - AMBER GRZYMSKI
LIMS OBJECT ID: 92365695
92365695
Project:
Pace Project No.:
RE:
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
Harrisburg Rd. Landfill
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 05, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Minnesota Certification IDs
1700 Elm Street SE, Suite 200, Minneapolis, MN 55414-
2485
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #:MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Mississippi Certification #: MN00064
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon NwTPH Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DW Certification #: 9952 C
West Virginia DEP Certification #: 382
Wisconsin Certification #: 999407970
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92365695001 6001-HBW28 EPA 6010 14 PASI-ASER
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365695002 6001-HBW20 EPA 6010 14 PASI-ASER
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365695003 6001-HBW14 EPA 6010 14 PASI-ASER
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365695004 Blank EPA 8260 52 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:6001-HBW28 Lab ID:92365695001 Collected:12/05/17 09:45 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/18/17 07:46 7440-36-012/06/17 22:455.0 1
Arsenic ND ug/L 12/18/17 07:46 7440-38-212/06/17 22:4510.0 1
Barium 26.8 ug/L 12/18/17 07:46 7440-39-312/06/17 22:455.0 1
Beryllium ND ug/L 12/18/17 07:46 7440-41-712/06/17 22:451.0 1
Cadmium ND ug/L 12/18/17 07:46 7440-43-912/06/17 22:451.0 1
Chromium ND ug/L 12/18/17 07:46 7440-47-312/06/17 22:455.0 1
Cobalt 18.3 ug/L 12/18/17 07:46 7440-48-412/06/17 22:455.0 1
Copper 49.7 ug/L 12/18/17 07:46 7440-50-812/06/17 22:455.0 1
Lead ND ug/L 12/18/17 07:46 7439-92-112/06/17 22:455.0 1
Nickel ND ug/L 12/18/17 07:46 7440-02-012/06/17 22:455.0 1
Selenium ND ug/L 12/18/17 07:46 7782-49-212/06/17 22:4510.0 1
Silver ND ug/L 12/18/17 07:46 7440-22-412/06/17 22:455.0 1
Vanadium 6.8 ug/L 12/18/17 07:46 7440-62-212/06/17 22:455.0 1
Zinc ND ug/L 12/18/17 07:46 7440-66-612/06/17 22:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:06 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 02:02 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 02:02 107-13-110.0 1
Benzene ND ug/L 12/07/17 02:02 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 02:02 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 02:02 75-27-41.0 1
Bromoform ND ug/L 12/07/17 02:02 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 02:02 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 02:02 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 02:02 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 02:02 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 02:02 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 02:02 75-00-31.0 1
Chloroform ND ug/L 12/07/17 02:02 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 02:02 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 02:02 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 02:02 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 02:02 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 02:02 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 02:02 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 02:02 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 02:02 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 02:02 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 02:02 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 02:02 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 02:02 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 02:02 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 02:02 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:6001-HBW28 Lab ID:92365695001 Collected:12/05/17 09:45 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 02:02 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 02:02 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 02:02 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 02:02 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 02:02 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 02:02 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 02:02 108-10-15.0 1
Styrene ND ug/L 12/07/17 02:02 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 02:02 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 02:02 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 02:02 127-18-41.0 1
Toluene ND ug/L 12/07/17 02:02 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 02:02 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 02:02 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 02:02 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 02:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 02:02 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 02:02 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 02:02 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 02:02 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 02:02 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 02:02 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %12/07/17 02:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %12/07/17 02:02 17060-07-070-130 1
Toluene-d8 (S)100 %12/07/17 02:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:6001-HBW20 Lab ID:92365695002 Collected:12/05/17 10:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/18/17 07:50 7440-36-012/06/17 22:455.0 1
Arsenic ND ug/L 12/18/17 07:50 7440-38-212/06/17 22:4510.0 1
Barium 13.2 ug/L 12/18/17 07:50 7440-39-312/06/17 22:455.0 1
Beryllium ND ug/L 12/18/17 07:50 7440-41-712/06/17 22:451.0 1
Cadmium ND ug/L 12/18/17 07:50 7440-43-912/06/17 22:451.0 1
Chromium ND ug/L 12/18/17 07:50 7440-47-312/06/17 22:455.0 1
Cobalt ND ug/L 12/18/17 07:50 7440-48-412/06/17 22:455.0 1
Copper 8.1 ug/L 12/18/17 07:50 7440-50-812/06/17 22:455.0 1
Lead ND ug/L 12/18/17 07:50 7439-92-112/06/17 22:455.0 1
Nickel ND ug/L 12/18/17 07:50 7440-02-012/06/17 22:455.0 1
Selenium ND ug/L 12/18/17 07:50 7782-49-212/06/17 22:4510.0 1
Silver ND ug/L 12/18/17 07:50 7440-22-412/06/17 22:455.0 1
Vanadium 16.9 ug/L 12/18/17 07:50 7440-62-212/06/17 22:455.0 1
Zinc ND ug/L 12/18/17 07:50 7440-66-612/06/17 22:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:09 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 02:20 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 02:20 107-13-110.0 1
Benzene ND ug/L 12/07/17 02:20 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 02:20 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 02:20 75-27-41.0 1
Bromoform ND ug/L 12/07/17 02:20 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 02:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 02:20 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 02:20 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 02:20 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 02:20 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 02:20 75-00-31.0 1
Chloroform ND ug/L 12/07/17 02:20 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 02:20 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 02:20 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 02:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 02:20 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 02:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 02:20 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 02:20 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 02:20 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 02:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 02:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 02:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 02:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 02:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 02:20 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:6001-HBW20 Lab ID:92365695002 Collected:12/05/17 10:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 02:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 02:20 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 02:20 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 02:20 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 02:20 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 02:20 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 02:20 108-10-15.0 1
Styrene ND ug/L 12/07/17 02:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 02:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 02:20 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 02:20 127-18-41.0 1
Toluene ND ug/L 12/07/17 02:20 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 02:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 02:20 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 02:20 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 02:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 02:20 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 02:20 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 02:20 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 02:20 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 02:20 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 02:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %12/07/17 02:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %12/07/17 02:20 17060-07-070-130 1
Toluene-d8 (S)108 %12/07/17 02:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:6001-HBW14 Lab ID:92365695003 Collected:12/05/17 10:45 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/18/17 07:54 7440-36-012/06/17 22:455.0 1
Arsenic ND ug/L 12/18/17 07:54 7440-38-212/06/17 22:4510.0 1
Barium 93.4 ug/L 12/18/17 07:54 7440-39-312/06/17 22:455.0 1
Beryllium ND ug/L 12/18/17 07:54 7440-41-712/06/17 22:451.0 1
Cadmium ND ug/L 12/18/17 07:54 7440-43-912/06/17 22:451.0 1
Chromium ND ug/L 12/18/17 07:54 7440-47-312/06/17 22:455.0 1
Cobalt ND ug/L 12/18/17 07:54 7440-48-412/06/17 22:455.0 1
Copper 22.0 ug/L 12/18/17 07:54 7440-50-812/06/17 22:455.0 1
Lead ND ug/L 12/18/17 07:54 7439-92-112/06/17 22:455.0 1
Nickel ND ug/L 12/18/17 07:54 7440-02-012/06/17 22:455.0 1
Selenium ND ug/L 12/18/17 07:54 7782-49-212/06/17 22:4510.0 1
Silver ND ug/L 12/18/17 07:54 7440-22-412/06/17 22:455.0 1
Vanadium 10.7 ug/L 12/18/17 07:54 7440-62-212/06/17 22:455.0 1
Zinc ND ug/L 12/18/17 07:54 7440-66-612/06/17 22:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:32 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 02:38 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 02:38 107-13-110.0 1
Benzene ND ug/L 12/07/17 02:38 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 02:38 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 02:38 75-27-41.0 1
Bromoform ND ug/L 12/07/17 02:38 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 02:38 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 02:38 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 02:38 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 02:38 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 02:38 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 02:38 75-00-31.0 1
Chloroform ND ug/L 12/07/17 02:38 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 02:38 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 02:38 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 02:38 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 02:38 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 02:38 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 02:38 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 02:38 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 02:38 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 02:38 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 02:38 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 02:38 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 02:38 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 02:38 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 02:38 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:6001-HBW14 Lab ID:92365695003 Collected:12/05/17 10:45 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 02:38 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 02:38 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 02:38 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 02:38 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 02:38 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 02:38 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 02:38 108-10-15.0 1
Styrene ND ug/L 12/07/17 02:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 02:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 02:38 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 02:38 127-18-41.0 1
Toluene ND ug/L 12/07/17 02:38 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 02:38 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 02:38 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 02:38 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 02:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 02:38 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 02:38 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 02:38 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 02:38 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 02:38 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 02:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %12/07/17 02:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %12/07/17 02:38 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/17 02:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:Blank Lab ID:92365695004 Collected:12/05/17 09:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 02:56 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 02:56 107-13-110.0 1
Benzene ND ug/L 12/07/17 02:56 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 02:56 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 02:56 75-27-41.0 1
Bromoform ND ug/L 12/07/17 02:56 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 02:56 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 02:56 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 02:56 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 02:56 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 02:56 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 02:56 75-00-31.0 1
Chloroform ND ug/L 12/07/17 02:56 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 02:56 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 02:56 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 02:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 02:56 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 02:56 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 02:56 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 02:56 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 02:56 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 02:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 02:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 02:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 02:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 02:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 02:56 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 12/07/17 02:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 02:56 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 02:56 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 02:56 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 02:56 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 02:56 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 02:56 108-10-15.0 1
Styrene ND ug/L 12/07/17 02:56 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 02:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 02:56 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 02:56 127-18-41.0 1
Toluene ND ug/L 12/07/17 02:56 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 02:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 02:56 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 02:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 02:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 02:56 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 02:56 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 02:56 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 02:56 1330-20-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Sample:Blank Lab ID:92365695004 Collected:12/05/17 09:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
m&p-Xylene ND ug/L 12/07/17 02:56 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 02:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %12/07/17 02:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %12/07/17 02:56 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/17 02:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389726
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92365695001, 92365695002, 92365695003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2162165
Associated Lab Samples:92365695001, 92365695002, 92365695003
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 12/18/17 06:00
Arsenic ug/L ND 10.0 12/21/17 22:06
Barium ug/L ND 5.0 12/18/17 06:00
Beryllium ug/L ND 1.0 12/18/17 06:00
Cadmium ug/L ND 1.0 12/18/17 06:00
Chromium ug/L ND 5.0 12/18/17 06:00
Cobalt ug/L ND 5.0 12/18/17 06:00
Copper ug/L ND 5.0 12/18/17 06:00
Lead ug/L ND 5.0 12/18/17 06:00
Nickel ug/L ND 5.0 12/18/17 06:00
Selenium ug/L ND 10.0 12/18/17 06:00
Silver ug/L ND 5.0 12/18/17 06:00
Vanadium ug/L ND 5.0 12/18/17 06:00
Zinc ug/L ND 10.0 12/18/17 06:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2162166LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 421500 84 80-120
Arsenic ug/L 469500 94 80-120
Barium ug/L 460500 92 80-120
Beryllium ug/L 442500 88 80-120
Cadmium ug/L 449500 90 80-120
Chromium ug/L 451500 90 80-120
Cobalt ug/L 440500 88 80-120
Copper ug/L 459500 92 80-120
Lead ug/L 437500 87 80-120
Nickel ug/L 440500 88 80-120
Selenium ug/L 440500 88 80-120
Silver ug/L 218250 87 80-120
Vanadium ug/L 458500 92 80-120
Zinc ug/L 431500 86 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2162167MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92365630001
2162168
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 85 75-12584 250011.8 438 431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2162167MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92365630001
2162168
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 91 75-12590 1500ND459454
Barium ug/L 500 83 75-12582 2500ND415408
Beryllium ug/L 500 86 75-12585 1500ND432427
Cadmium ug/L 500 92 75-12591 1500ND460456
Chromium ug/L 500 88 75-12587 250013.4 456 448
Cobalt ug/L 500 79 75-12579 0500227622620
Copper ug/L 500 95 75-12593 2500ND479470
Lead ug/L 500 78 75-12578 1500ND391389
Nickel ug/L 500 79 75-12578 1500179572569
Selenium ug/L 500 89 75-12589 1500ND447444
Silver ug/L 250 95 75-12593 1250ND237234
Vanadium ug/L 500 92 75-12591 1500ND458454
Zinc ug/L 500 83 75-12583 0500193609608
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
514093
EPA 3020
EPA 6020
6020 MET
Associated Lab Samples:92365695001, 92365695002, 92365695003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2796082
Associated Lab Samples:92365695001, 92365695002, 92365695003
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 12/18/17 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2796083LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 105100 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2796084MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363096001
2796085
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 101 75-125103 31000.19 101 104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389662
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92365695001, 92365695002, 92365695003, 92365695004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2161466
Associated Lab Samples:92365695001, 92365695002, 92365695003, 92365695004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/07/17 00:34
1,1,1-Trichloroethane ug/L ND 1.0 12/07/17 00:34
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/07/17 00:34
1,1,2-Trichloroethane ug/L ND 1.0 12/07/17 00:34
1,1-Dichloroethane ug/L ND 1.0 12/07/17 00:34
1,1-Dichloroethene ug/L ND 1.0 12/07/17 00:34
1,2,3-Trichloropropane ug/L ND 1.0 12/07/17 00:34
1,2-Dibromo-3-chloropropane ug/L ND 2.0 12/07/17 00:34
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/17 00:34
1,2-Dichlorobenzene ug/L ND 1.0 12/07/17 00:34
1,2-Dichloroethane ug/L ND 1.0 12/07/17 00:34
1,2-Dichloropropane ug/L ND 1.0 12/07/17 00:34
1,4-Dichlorobenzene ug/L ND 1.0 12/07/17 00:34
2-Butanone (MEK)ug/L ND 5.0 12/07/17 00:34
2-Hexanone ug/L ND 5.0 12/07/17 00:34
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 12/07/17 00:34
Acetone ug/L ND 25.0 12/07/17 00:34
Acrylonitrile ug/L ND 10.0 12/07/17 00:34
Benzene ug/L ND 1.0 12/07/17 00:34
Bromochloromethane ug/L ND 1.0 12/07/17 00:34
Bromodichloromethane ug/L ND 1.0 12/07/17 00:34
Bromoform ug/L ND 1.0 12/07/17 00:34
Bromomethane ug/L ND 2.0 12/07/17 00:34
Carbon disulfide ug/L ND 2.0 12/07/17 00:34
Carbon tetrachloride ug/L ND 1.0 12/07/17 00:34
Chlorobenzene ug/L ND 1.0 12/07/17 00:34
Chloroethane ug/L ND 1.0 12/07/17 00:34
Chloroform ug/L ND 1.0 12/07/17 00:34
Chloromethane ug/L ND 1.0 12/07/17 00:34
cis-1,2-Dichloroethene ug/L ND 1.0 12/07/17 00:34
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/17 00:34
Dibromochloromethane ug/L ND 1.0 12/07/17 00:34
Dibromomethane ug/L ND 1.0 12/07/17 00:34
Ethylbenzene ug/L ND 1.0 12/07/17 00:34
Iodomethane ug/L ND 5.0 12/07/17 00:34
m&p-Xylene ug/L ND 2.0 12/07/17 00:34
Methylene Chloride ug/L ND 1.0 12/07/17 00:34
o-Xylene ug/L ND 1.0 12/07/17 00:34
Styrene ug/L ND 1.0 12/07/17 00:34
Tetrachloroethene ug/L ND 1.0 12/07/17 00:34
Toluene ug/L ND 1.0 12/07/17 00:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2161466
Associated Lab Samples:92365695001, 92365695002, 92365695003, 92365695004
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 12/07/17 00:34
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/17 00:34
trans-1,4-Dichloro-2-butene ug/L ND 1.0 12/07/17 00:34
Trichloroethene ug/L ND 1.0 12/07/17 00:34
Trichlorofluoromethane ug/L ND 1.0 12/07/17 00:34
Vinyl acetate ug/L ND 2.0 12/07/17 00:34
Vinyl chloride ug/L ND 1.0 12/07/17 00:34
Xylene (Total)ug/L ND 1.0 12/07/17 00:34
1,2-Dichloroethane-d4 (S)%94 70-130 12/07/17 00:34
4-Bromofluorobenzene (S)%95 70-130 12/07/17 00:34
Toluene-d8 (S)%107 70-130 12/07/17 00:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2161467LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.850 94 80-125
1,1,1-Trichloroethane ug/L 43.650 87 71-129
1,1,2,2-Tetrachloroethane ug/L 45.450 91 79-124
1,1,2-Trichloroethane ug/L 51.750 103 85-125
1,1-Dichloroethane ug/L 46.050 92 73-126
1,1-Dichloroethene ug/L 47.050 94 66-135
1,2,3-Trichloropropane ug/L 46.850 94 75-130
1,2-Dibromo-3-chloropropane ug/L 48.350 97 71-133
1,2-Dibromoethane (EDB)ug/L 46.750 93 83-124
1,2-Dichlorobenzene ug/L 49.050 98 80-133
1,2-Dichloroethane ug/L 44.450 89 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
1,4-Dichlorobenzene ug/L 47.350 95 78-130
2-Butanone (MEK)ug/L 95.0100 95 61-144
2-Hexanone ug/L 92.6100 93 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 89.7100 90 48-146
Acrylonitrile ug/L 233250 93 40-160
Benzene ug/L 50.450 101 80-125
Bromochloromethane ug/L 47.050 94 71-125
Bromodichloromethane ug/L 48.350 97 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 44.450 89 40-160
Carbon disulfide ug/L 46.050 92 50-160
Carbon tetrachloride ug/L 48.850 98 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 55.350 111 39-148
Chloroform ug/L 44.850 90 73-127
Chloromethane ug/L 39.450 79 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2161467LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 47.550 95 74-124
cis-1,3-Dichloropropene ug/L 51.250 102 72-132
Dibromochloromethane ug/L 47.450 95 78-125
Dibromomethane ug/L 49.850 100 82-120
Ethylbenzene ug/L 45.850 92 79-121
Iodomethane ug/L 84.2100 84 39-154
m&p-Xylene ug/L 94.7100 95 81-124
Methylene Chloride ug/L 46.350 93 64-133
o-Xylene ug/L 46.250 92 79-131
Styrene ug/L 46.150 92 84-126
Tetrachloroethene ug/L 45.550 91 78-122
Toluene ug/L 49.950 100 80-121
trans-1,2-Dichloroethene ug/L 46.350 93 71-127
trans-1,3-Dichloropropene ug/L 52.050 104 69-141
trans-1,4-Dichloro-2-butene ug/L 44.050 88 40-160
Trichloroethene ug/L 45.750 91 78-122
Trichlorofluoromethane ug/L 45.850 92 53-137
Vinyl acetate ug/L 94.5100 95 40-160
Vinyl chloride ug/L 46.650 93 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%107 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2165992MATRIX SPIKE SAMPLE:
MSSpike
Result
92365694002
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 20.220 101 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethane ug/L 19.220 95 70-130ND
1,1-Dichloroethene ug/L 20.020 100 70-166ND
1,2,3-Trichloropropane ug/L 18.220 91 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.520 103 70-130ND
1,2-Dichlorobenzene ug/L 20.420 102 70-130ND
1,2-Dichloroethane ug/L 19.320 97 70-130ND
1,2-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 37.440 93 70-130ND
2-Hexanone ug/L 38.240 95 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.540 94 70-130ND
Acetone ug/L 37.740 94 70-130ND
Acrylonitrile ug/L 90.7100 91 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2165992MATRIX SPIKE SAMPLE:
MSSpike
Result
92365694002
Benzene ug/L 20.520 103 70-148ND
Bromochloromethane ug/L 20.820 104 70-130ND
Bromodichloromethane ug/L 20.220 101 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 11.6 M1205870-130ND
Carbon disulfide ug/L 19.120 95 70-130ND
Carbon tetrachloride ug/L 21.520 108 70-130ND
Chlorobenzene ug/L 20.720 103 70-146ND
Chloroethane ug/L 23.120 115 70-130ND
Chloroform ug/L 18.820 94 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
cis-1,2-Dichloroethene ug/L 19.420 97 70-130ND
cis-1,3-Dichloropropene ug/L 20.720 104 70-130ND
Dibromochloromethane ug/L 21.120 106 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Ethylbenzene ug/L 20.720 104 70-130ND
Iodomethane ug/L 13.940 35 70-130ND
m&p-Xylene ug/L 41.940 105 70-130ND
Methylene Chloride ug/L 16.420 82 70-130ND
o-Xylene ug/L 22.620 113 70-130ND
Styrene ug/L 21.520 108 70-130ND
Tetrachloroethene ug/L 22.820 114 70-130ND
Toluene ug/L 20.020 100 70-155ND
trans-1,2-Dichloroethene ug/L 19.820 99 70-130ND
trans-1,3-Dichloropropene ug/L 19.720 99 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.620 78 70-130ND
Trichloroethene ug/L 21.620 108 69-151ND
Trichlorofluoromethane ug/L 20.220 101 70-130ND
Vinyl acetate ug/L 37.940 95 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92365694003
2165993SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92365694003
2165993SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%90 796
4-Bromofluorobenzene (S)%91 394
Toluene-d8 (S)%105 699
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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Page 19 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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Page 20 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92365695
Harrisburg Rd. Landfill
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92365695001 389726 3897706001-HBW28 EPA 3010A EPA 6010
92365695002 389726 3897706001-HBW20 EPA 3010A EPA 6010
92365695003 389726 3897706001-HBW14 EPA 3010A EPA 6010
92365695001 514093 5142576001-HBW28 EPA 3020 EPA 6020
92365695002 514093 5142576001-HBW20 EPA 3020 EPA 6020
92365695003 514093 5142576001-HBW14 EPA 3020 EPA 6020
92365695001 3896626001-HBW28 EPA 8260
92365695002 3896626001-HBW20 EPA 8260
92365695003 3896626001-HBW14 EPA 8260
92365695004 389662BlankEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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Page 21 of 24
Page 22 of 24
Page 23 of 24
Page 24 of 24
#=CL#
December 19, 2017
LIMS USE: FR - AMBER GRZYMSKI
LIMS OBJECT ID: 92365696
92365696
Project:
Pace Project No.:
RE:
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
Harrisburg Rd Landfill
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 05, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 26
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Minnesota Certification IDs
1700 Elm Street SE, Suite 200, Minneapolis, MN 55414-
2485
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #:MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Mississippi Certification #: MN00064
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon NwTPH Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DW Certification #: 9952 C
West Virginia DEP Certification #: 382
Wisconsin Certification #: 999407970
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 26
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92365696001 6001-HBW21 EPA 6010 14 PASI-AJMW1
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365696002 6001-HBW22 EPA 6010 14 PASI-AJMW1
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365696003 6001-HBW12B EPA 6010 14 PASI-AJMW1
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365696004 6001-HBW17B EPA 6010 14 PASI-AJMW1
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365696005 6001-MAINTE EPA 6010 14 PASI-AJMW1
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 3 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW21 Lab ID:92365696001 Collected:12/05/17 13:15 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/16/17 19:22 7440-36-012/07/17 09:455.0 1
Arsenic ND ug/L 12/16/17 19:22 7440-38-212/07/17 09:4510.0 1
Barium 10.5 ug/L 12/16/17 19:22 7440-39-312/07/17 09:455.0 1
Beryllium ND ug/L 12/16/17 19:22 7440-41-712/07/17 09:451.0 1
Cadmium ND ug/L 12/16/17 19:22 7440-43-912/07/17 09:451.0 1
Chromium ND ug/L 12/16/17 19:22 7440-47-312/07/17 09:455.0 1
Cobalt ND ug/L 12/16/17 19:22 7440-48-412/07/17 09:455.0 1
Copper ND ug/L 12/16/17 19:22 7440-50-812/07/17 09:455.0 1
Lead ND ug/L 12/16/17 19:22 7439-92-112/07/17 09:455.0 1
Nickel ND ug/L 12/16/17 19:22 7440-02-012/07/17 09:455.0 1
Selenium ND ug/L 12/16/17 19:22 7782-49-212/07/17 09:4510.0 1
Silver ND ug/L 12/16/17 19:22 7440-22-412/07/17 09:455.0 1
Vanadium 7.6 ug/L 12/16/17 19:22 7440-62-212/07/17 09:455.0 1
Zinc ND ug/L 12/16/17 19:22 7440-66-612/07/17 09:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:37 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 03:13 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 03:13 107-13-110.0 1
Benzene ND ug/L 12/07/17 03:13 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 03:13 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 03:13 75-27-41.0 1
Bromoform ND ug/L 12/07/17 03:13 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 03:13 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 03:13 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 03:13 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 03:13 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 03:13 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 03:13 75-00-31.0 1
Chloroform ND ug/L 12/07/17 03:13 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 03:13 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 03:13 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 03:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 03:13 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 03:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 03:13 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 03:13 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 03:13 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 03:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 03:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 03:13 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 03:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 03:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 03:13 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
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Page 4 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW21 Lab ID:92365696001 Collected:12/05/17 13:15 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 03:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 03:13 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 03:13 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 03:13 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 03:13 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 03:13 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 03:13 108-10-15.0 1
Styrene ND ug/L 12/07/17 03:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 03:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 03:13 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 03:13 127-18-41.0 1
Toluene ND ug/L 12/07/17 03:13 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 03:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 03:13 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 03:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 03:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 03:13 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 03:13 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 03:13 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 03:13 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 03:13 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 03:13 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %12/07/17 03:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %12/07/17 03:13 17060-07-070-130 1
Toluene-d8 (S)108 %12/07/17 03:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW22 Lab ID:92365696002 Collected:12/05/17 13:00 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/16/17 19:26 7440-36-012/07/17 09:455.0 1
Arsenic ND ug/L 12/16/17 19:26 7440-38-212/07/17 09:4510.0 1
Barium 31.1 ug/L 12/16/17 19:26 7440-39-312/07/17 09:455.0 1
Beryllium ND ug/L 12/16/17 19:26 7440-41-712/07/17 09:451.0 1
Cadmium ND ug/L 12/16/17 19:26 7440-43-912/07/17 09:451.0 1
Chromium 11.7 ug/L 12/16/17 19:26 7440-47-312/07/17 09:455.0 1
Cobalt ND ug/L 12/16/17 19:26 7440-48-412/07/17 09:455.0 1
Copper ND ug/L 12/16/17 19:26 7440-50-812/07/17 09:455.0 1
Lead ND ug/L 12/16/17 19:26 7439-92-112/07/17 09:455.0 1
Nickel ND ug/L 12/16/17 19:26 7440-02-012/07/17 09:455.0 1
Selenium ND ug/L 12/16/17 19:26 7782-49-212/07/17 09:4510.0 1
Silver ND ug/L 12/16/17 19:26 7440-22-412/07/17 09:455.0 1
Vanadium ND ug/L 12/16/17 19:26 7440-62-212/07/17 09:455.0 1
Zinc ND ug/L 12/16/17 19:26 7440-66-612/07/17 09:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:40 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 03:31 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 03:31 107-13-110.0 1
Benzene ND ug/L 12/07/17 03:31 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 03:31 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 03:31 75-27-41.0 1
Bromoform ND ug/L 12/07/17 03:31 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 03:31 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 03:31 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 03:31 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 03:31 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 03:31 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 03:31 75-00-31.0 1
Chloroform ND ug/L 12/07/17 03:31 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 03:31 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 03:31 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 03:31 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 03:31 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 03:31 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 03:31 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 03:31 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 03:31 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 03:31 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 03:31 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 03:31 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 03:31 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 03:31 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 03:31 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW22 Lab ID:92365696002 Collected:12/05/17 13:00 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 03:31 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 03:31 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 03:31 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 03:31 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 03:31 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 03:31 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 03:31 108-10-15.0 1
Styrene ND ug/L 12/07/17 03:31 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 03:31 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 03:31 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 03:31 127-18-41.0 1
Toluene ND ug/L 12/07/17 03:31 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 03:31 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 03:31 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 03:31 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 03:31 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 03:31 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 03:31 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 03:31 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 03:31 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 03:31 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 03:31 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %12/07/17 03:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/17 03:31 17060-07-070-130 1
Toluene-d8 (S)108 %12/07/17 03:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW12B Lab ID:92365696003 Collected:12/05/17 13:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/16/17 19:30 7440-36-012/07/17 09:455.0 1
Arsenic ND ug/L 12/16/17 19:30 7440-38-212/07/17 09:4510.0 1
Barium 28.5 ug/L 12/16/17 19:30 7440-39-312/07/17 09:455.0 1
Beryllium ND ug/L 12/16/17 19:30 7440-41-712/07/17 09:451.0 1
Cadmium ND ug/L 12/16/17 19:30 7440-43-912/07/17 09:451.0 1
Chromium ND ug/L 12/16/17 19:30 7440-47-312/07/17 09:455.0 1
Cobalt ND ug/L 12/16/17 19:30 7440-48-412/07/17 09:455.0 1
Copper 9.7 ug/L 12/16/17 19:30 7440-50-812/07/17 09:455.0 1
Lead ND ug/L 12/16/17 19:30 7439-92-112/07/17 09:455.0 1
Nickel ND ug/L 12/16/17 19:30 7440-02-012/07/17 09:455.0 1
Selenium ND ug/L 12/16/17 19:30 7782-49-212/07/17 09:4510.0 1
Silver ND ug/L 12/16/17 19:30 7440-22-412/07/17 09:455.0 1
Vanadium 18.7 ug/L 12/16/17 19:30 7440-62-212/07/17 09:455.0 1
Zinc ND ug/L 12/16/17 19:30 7440-66-612/07/17 09:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:43 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 03:49 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 03:49 107-13-110.0 1
Benzene ND ug/L 12/07/17 03:49 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 03:49 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 03:49 75-27-41.0 1
Bromoform ND ug/L 12/07/17 03:49 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 03:49 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 03:49 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 03:49 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 03:49 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 03:49 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 03:49 75-00-31.0 1
Chloroform ND ug/L 12/07/17 03:49 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 03:49 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 03:49 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 03:49 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 03:49 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 03:49 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 03:49 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 03:49 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 03:49 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 03:49 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 03:49 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 03:49 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 03:49 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 03:49 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 03:49 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW12B Lab ID:92365696003 Collected:12/05/17 13:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 03:49 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 03:49 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 03:49 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 03:49 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 03:49 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 03:49 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 03:49 108-10-15.0 1
Styrene ND ug/L 12/07/17 03:49 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 03:49 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 03:49 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 03:49 127-18-41.0 1
Toluene ND ug/L 12/07/17 03:49 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 03:49 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 03:49 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 03:49 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 03:49 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 03:49 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 03:49 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 03:49 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 03:49 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 03:49 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 03:49 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %12/07/17 03:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/17 03:49 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/17 03:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW17B Lab ID:92365696004 Collected:12/05/17 11:45 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/16/17 19:35 7440-36-012/07/17 09:455.0 1
Arsenic ND ug/L 12/16/17 19:35 7440-38-212/07/17 09:4510.0 1
Barium 58.8 ug/L 12/16/17 19:35 7440-39-312/07/17 09:455.0 1
Beryllium ND ug/L 12/16/17 19:35 7440-41-712/07/17 09:451.0 1
Cadmium ND ug/L 12/16/17 19:35 7440-43-912/07/17 09:451.0 1
Chromium ND ug/L 12/16/17 19:35 7440-47-312/07/17 09:455.0 1
Cobalt 17.5 ug/L 12/16/17 19:35 7440-48-412/07/17 09:455.0 1
Copper 20.0 ug/L 12/16/17 19:35 7440-50-812/07/17 09:455.0 1
Lead ND ug/L 12/16/17 19:35 7439-92-112/07/17 09:455.0 1
Nickel ND ug/L 12/16/17 19:35 7440-02-012/07/17 09:455.0 1
Selenium ND ug/L 12/16/17 19:35 7782-49-212/07/17 09:4510.0 1
Silver ND ug/L 12/16/17 19:35 7440-22-412/07/17 09:455.0 1
Vanadium ND ug/L 12/16/17 19:35 7440-62-212/07/17 09:455.0 1
Zinc 16.0 ug/L 12/16/17 19:35 7440-66-612/07/17 09:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium 0.16 ug/L 12/18/17 14:45 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 04:06 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 04:06 107-13-110.0 1
Benzene 7.9 ug/L 12/07/17 04:06 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 04:06 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 04:06 75-27-41.0 1
Bromoform ND ug/L 12/07/17 04:06 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 04:06 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 04:06 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 04:06 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 04:06 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 04:06 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 04:06 75-00-31.0 1
Chloroform ND ug/L 12/07/17 04:06 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 04:06 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 04:06 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 04:06 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 04:06 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 04:06 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 04:06 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 04:06 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 04:06 110-57-61.0 1
1,1-Dichloroethane 8.0 ug/L 12/07/17 04:06 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 04:06 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 04:06 75-35-41.0 1
cis-1,2-Dichloroethene 116 ug/L 12/07/17 04:06 156-59-21.0 1
trans-1,2-Dichloroethene 1.5 ug/L 12/07/17 04:06 156-60-51.0 1
1,2-Dichloropropane 10.7 ug/L 12/07/17 04:06 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-HBW17B Lab ID:92365696004 Collected:12/05/17 11:45 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 04:06 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 04:06 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 04:06 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 04:06 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 04:06 74-88-45.0 1
Methylene Chloride 2.5 ug/L 12/07/17 04:06 75-09-2 C91.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 04:06 108-10-15.0 1
Styrene ND ug/L 12/07/17 04:06 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 04:06 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 04:06 79-34-51.0 1
Tetrachloroethene 24.6 ug/L 12/07/17 04:06 127-18-41.0 1
Toluene ND ug/L 12/07/17 04:06 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 04:06 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 04:06 79-00-51.0 1
Trichloroethene 20.4 ug/L 12/07/17 04:06 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 04:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 04:06 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 04:06 108-05-42.0 1
Vinyl chloride 1.7 ug/L 12/07/17 04:06 75-01-41.0 1
Xylene (Total)11.4 ug/L 12/07/17 04:06 1330-20-71.0 1
m&p-Xylene 2.4 ug/L 12/07/17 04:06 179601-23-12.0 1
o-Xylene 9.0 ug/L 12/07/17 04:06 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)88 %12/07/17 04:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/07/17 04:06 17060-07-070-130 1
Toluene-d8 (S)106 %12/07/17 04:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-MAINTE Lab ID:92365696005 Collected:12/05/17 11:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/16/17 19:39 7440-36-012/07/17 09:455.0 1
Arsenic ND ug/L 12/16/17 19:39 7440-38-212/07/17 09:4510.0 1
Barium 8.4 ug/L 12/16/17 19:39 7440-39-312/07/17 09:455.0 1
Beryllium ND ug/L 12/16/17 19:39 7440-41-712/07/17 09:451.0 1
Cadmium ND ug/L 12/16/17 19:39 7440-43-912/07/17 09:451.0 1
Chromium ND ug/L 12/16/17 19:39 7440-47-312/07/17 09:455.0 1
Cobalt ND ug/L 12/16/17 19:39 7440-48-412/07/17 09:455.0 1
Copper 54.3 ug/L 12/16/17 19:39 7440-50-812/07/17 09:455.0 1
Lead ND ug/L 12/16/17 19:39 7439-92-112/07/17 09:455.0 1
Nickel ND ug/L 12/16/17 19:39 7440-02-012/07/17 09:455.0 1
Selenium ND ug/L 12/16/17 19:39 7782-49-212/07/17 09:4510.0 1
Silver ND ug/L 12/16/17 19:39 7440-22-412/07/17 09:455.0 1
Vanadium 6.0 ug/L 12/16/17 19:39 7440-62-212/07/17 09:455.0 1
Zinc 50.8 ug/L 12/16/17 19:39 7440-66-612/07/17 09:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:48 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 04:24 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 04:24 107-13-110.0 1
Benzene ND ug/L 12/07/17 04:24 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 04:24 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 04:24 75-27-41.0 1
Bromoform ND ug/L 12/07/17 04:24 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 04:24 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 04:24 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 04:24 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 04:24 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 04:24 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 04:24 75-00-31.0 1
Chloroform ND ug/L 12/07/17 04:24 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 04:24 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 04:24 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 04:24 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 04:24 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 04:24 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 04:24 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 04:24 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 04:24 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 04:24 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 04:24 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 04:24 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 04:24 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 04:24 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 04:24 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
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Huntersville, NC 28078
[phone]
Page 12 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Sample:6001-MAINTE Lab ID:92365696005 Collected:12/05/17 11:25 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 04:24 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 04:24 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 04:24 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 04:24 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 04:24 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 04:24 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 04:24 108-10-15.0 1
Styrene ND ug/L 12/07/17 04:24 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 04:24 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 04:24 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 04:24 127-18-41.0 1
Toluene ND ug/L 12/07/17 04:24 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 04:24 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 04:24 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 04:24 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 04:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 04:24 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 04:24 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 04:24 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 04:24 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 04:24 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 04:24 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)89 %12/07/17 04:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %12/07/17 04:24 17060-07-070-130 1
Toluene-d8 (S)109 %12/07/17 04:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389779
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2162352
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 12/16/17 18:54
Arsenic ug/L ND 10.0 12/16/17 18:54
Barium ug/L ND 5.0 12/16/17 18:54
Beryllium ug/L ND 1.0 12/16/17 18:54
Cadmium ug/L ND 1.0 12/16/17 18:54
Chromium ug/L ND 5.0 12/16/17 18:54
Cobalt ug/L ND 5.0 12/16/17 18:54
Copper ug/L ND 5.0 12/16/17 18:54
Lead ug/L ND 5.0 12/16/17 18:54
Nickel ug/L ND 5.0 12/16/17 18:54
Selenium ug/L ND 10.0 12/16/17 18:54
Silver ug/L ND 5.0 12/16/17 18:54
Vanadium ug/L ND 5.0 12/16/17 18:54
Zinc ug/L ND 10.0 12/16/17 18:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2162353LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 466500 93 80-120
Arsenic ug/L 486500 97 80-120
Barium ug/L 468500 94 80-120
Beryllium ug/L 475500 95 80-120
Cadmium ug/L 493500 99 80-120
Chromium ug/L 475500 95 80-120
Cobalt ug/L 480500 96 80-120
Copper ug/L 489500 98 80-120
Lead ug/L 477500 95 80-120
Nickel ug/L 478500 96 80-120
Selenium ug/L 510500 102 80-120
Silver ug/L 234250 93 80-120
Vanadium ug/L 478500 96 80-120
Zinc ug/L 484500 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2162354MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92365838001
2162355
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12592 3500ND471460
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 14 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2162354MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92365838001
2162355
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 99 75-12597 3500ND496484
Barium ug/L 500 95 75-12595 050054.9 531 531
Beryllium ug/L 500 97 75-12596 1500ND484481
Cadmium ug/L 500 100 75-12598 2500ND501491
Chromium ug/L 500 97 75-12597 050016.4 500 501
Cobalt ug/L 500 96 75-12594 2500ND482471
Copper ug/L 500 99 75-125100 05004.6J 501 503
Lead ug/L 500 95 75-12594 2500ND477469
Nickel ug/L 500 95 75-12593 250010.1 487 477
Selenium ug/L 500 102 75-125100 3500ND512499
Silver ug/L 250 97 75-12596 1250ND244241
Vanadium ug/L 500 99 75-12598 150013.2 508 505
Zinc ug/L 500 98 75-12596 25005.4J 496 484
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
514093
EPA 3020
EPA 6020
6020 MET
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2796082
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 12/18/17 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2796083LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 105100 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2796084MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363096001
2796085
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 101 75-125103 31000.19 101 104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389662
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2161466
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/07/17 00:34
1,1,1-Trichloroethane ug/L ND 1.0 12/07/17 00:34
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/07/17 00:34
1,1,2-Trichloroethane ug/L ND 1.0 12/07/17 00:34
1,1-Dichloroethane ug/L ND 1.0 12/07/17 00:34
1,1-Dichloroethene ug/L ND 1.0 12/07/17 00:34
1,2,3-Trichloropropane ug/L ND 1.0 12/07/17 00:34
1,2-Dibromo-3-chloropropane ug/L ND 2.0 12/07/17 00:34
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/17 00:34
1,2-Dichlorobenzene ug/L ND 1.0 12/07/17 00:34
1,2-Dichloroethane ug/L ND 1.0 12/07/17 00:34
1,2-Dichloropropane ug/L ND 1.0 12/07/17 00:34
1,4-Dichlorobenzene ug/L ND 1.0 12/07/17 00:34
2-Butanone (MEK)ug/L ND 5.0 12/07/17 00:34
2-Hexanone ug/L ND 5.0 12/07/17 00:34
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 12/07/17 00:34
Acetone ug/L ND 25.0 12/07/17 00:34
Acrylonitrile ug/L ND 10.0 12/07/17 00:34
Benzene ug/L ND 1.0 12/07/17 00:34
Bromochloromethane ug/L ND 1.0 12/07/17 00:34
Bromodichloromethane ug/L ND 1.0 12/07/17 00:34
Bromoform ug/L ND 1.0 12/07/17 00:34
Bromomethane ug/L ND 2.0 12/07/17 00:34
Carbon disulfide ug/L ND 2.0 12/07/17 00:34
Carbon tetrachloride ug/L ND 1.0 12/07/17 00:34
Chlorobenzene ug/L ND 1.0 12/07/17 00:34
Chloroethane ug/L ND 1.0 12/07/17 00:34
Chloroform ug/L ND 1.0 12/07/17 00:34
Chloromethane ug/L ND 1.0 12/07/17 00:34
cis-1,2-Dichloroethene ug/L ND 1.0 12/07/17 00:34
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/17 00:34
Dibromochloromethane ug/L ND 1.0 12/07/17 00:34
Dibromomethane ug/L ND 1.0 12/07/17 00:34
Ethylbenzene ug/L ND 1.0 12/07/17 00:34
Iodomethane ug/L ND 5.0 12/07/17 00:34
m&p-Xylene ug/L ND 2.0 12/07/17 00:34
Methylene Chloride ug/L ND 1.0 12/07/17 00:34
o-Xylene ug/L ND 1.0 12/07/17 00:34
Styrene ug/L ND 1.0 12/07/17 00:34
Tetrachloroethene ug/L ND 1.0 12/07/17 00:34
Toluene ug/L ND 1.0 12/07/17 00:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2161466
Associated Lab Samples:92365696001, 92365696002, 92365696003, 92365696004, 92365696005
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 12/07/17 00:34
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/17 00:34
trans-1,4-Dichloro-2-butene ug/L ND 1.0 12/07/17 00:34
Trichloroethene ug/L ND 1.0 12/07/17 00:34
Trichlorofluoromethane ug/L ND 1.0 12/07/17 00:34
Vinyl acetate ug/L ND 2.0 12/07/17 00:34
Vinyl chloride ug/L ND 1.0 12/07/17 00:34
Xylene (Total)ug/L ND 1.0 12/07/17 00:34
1,2-Dichloroethane-d4 (S)%94 70-130 12/07/17 00:34
4-Bromofluorobenzene (S)%95 70-130 12/07/17 00:34
Toluene-d8 (S)%107 70-130 12/07/17 00:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2161467LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.850 94 80-125
1,1,1-Trichloroethane ug/L 43.650 87 71-129
1,1,2,2-Tetrachloroethane ug/L 45.450 91 79-124
1,1,2-Trichloroethane ug/L 51.750 103 85-125
1,1-Dichloroethane ug/L 46.050 92 73-126
1,1-Dichloroethene ug/L 47.050 94 66-135
1,2,3-Trichloropropane ug/L 46.850 94 75-130
1,2-Dibromo-3-chloropropane ug/L 48.350 97 71-133
1,2-Dibromoethane (EDB)ug/L 46.750 93 83-124
1,2-Dichlorobenzene ug/L 49.050 98 80-133
1,2-Dichloroethane ug/L 44.450 89 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
1,4-Dichlorobenzene ug/L 47.350 95 78-130
2-Butanone (MEK)ug/L 95.0100 95 61-144
2-Hexanone ug/L 92.6100 93 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 89.7100 90 48-146
Acrylonitrile ug/L 233250 93 40-160
Benzene ug/L 50.450 101 80-125
Bromochloromethane ug/L 47.050 94 71-125
Bromodichloromethane ug/L 48.350 97 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 44.450 89 40-160
Carbon disulfide ug/L 46.050 92 50-160
Carbon tetrachloride ug/L 48.850 98 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 55.350 111 39-148
Chloroform ug/L 44.850 90 73-127
Chloromethane ug/L 39.450 79 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2161467LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 47.550 95 74-124
cis-1,3-Dichloropropene ug/L 51.250 102 72-132
Dibromochloromethane ug/L 47.450 95 78-125
Dibromomethane ug/L 49.850 100 82-120
Ethylbenzene ug/L 45.850 92 79-121
Iodomethane ug/L 84.2100 84 39-154
m&p-Xylene ug/L 94.7100 95 81-124
Methylene Chloride ug/L 46.350 93 64-133
o-Xylene ug/L 46.250 92 79-131
Styrene ug/L 46.150 92 84-126
Tetrachloroethene ug/L 45.550 91 78-122
Toluene ug/L 49.950 100 80-121
trans-1,2-Dichloroethene ug/L 46.350 93 71-127
trans-1,3-Dichloropropene ug/L 52.050 104 69-141
trans-1,4-Dichloro-2-butene ug/L 44.050 88 40-160
Trichloroethene ug/L 45.750 91 78-122
Trichlorofluoromethane ug/L 45.850 92 53-137
Vinyl acetate ug/L 94.5100 95 40-160
Vinyl chloride ug/L 46.650 93 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%107 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2165992MATRIX SPIKE SAMPLE:
MSSpike
Result
92365694002
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 20.220 101 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethane ug/L 19.220 95 70-130ND
1,1-Dichloroethene ug/L 20.020 100 70-166ND
1,2,3-Trichloropropane ug/L 18.220 91 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.520 103 70-130ND
1,2-Dichlorobenzene ug/L 20.420 102 70-130ND
1,2-Dichloroethane ug/L 19.320 97 70-130ND
1,2-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 37.440 93 70-130ND
2-Hexanone ug/L 38.240 95 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.540 94 70-130ND
Acetone ug/L 37.740 94 70-130ND
Acrylonitrile ug/L 90.7100 91 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2165992MATRIX SPIKE SAMPLE:
MSSpike
Result
92365694002
Benzene ug/L 20.520 103 70-148ND
Bromochloromethane ug/L 20.820 104 70-130ND
Bromodichloromethane ug/L 20.220 101 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 11.6 M1205870-130ND
Carbon disulfide ug/L 19.120 95 70-130ND
Carbon tetrachloride ug/L 21.520 108 70-130ND
Chlorobenzene ug/L 20.720 103 70-146ND
Chloroethane ug/L 23.120 115 70-130ND
Chloroform ug/L 18.820 94 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
cis-1,2-Dichloroethene ug/L 19.420 97 70-130ND
cis-1,3-Dichloropropene ug/L 20.720 104 70-130ND
Dibromochloromethane ug/L 21.120 106 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Ethylbenzene ug/L 20.720 104 70-130ND
Iodomethane ug/L 13.940 35 70-130ND
m&p-Xylene ug/L 41.940 105 70-130ND
Methylene Chloride ug/L 16.420 82 70-130ND
o-Xylene ug/L 22.620 113 70-130ND
Styrene ug/L 21.520 108 70-130ND
Tetrachloroethene ug/L 22.820 114 70-130ND
Toluene ug/L 20.020 100 70-155ND
trans-1,2-Dichloroethene ug/L 19.820 99 70-130ND
trans-1,3-Dichloropropene ug/L 19.720 99 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.620 78 70-130ND
Trichloroethene ug/L 21.620 108 69-151ND
Trichlorofluoromethane ug/L 20.220 101 70-130ND
Vinyl acetate ug/L 37.940 95 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92365694003
2165993SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92365694003
2165993SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%90 796
4-Bromofluorobenzene (S)%91 394
Toluene-d8 (S)%105 699
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 26
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 26
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92365696
Harrisburg Rd Landfill
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92365696001 389779 3899726001-HBW21 EPA 3010A EPA 6010
92365696002 389779 3899726001-HBW22 EPA 3010A EPA 6010
92365696003 389779 3899726001-HBW12B EPA 3010A EPA 6010
92365696004 389779 3899726001-HBW17B EPA 3010A EPA 6010
92365696005 389779 3899726001-MAINTE EPA 3010A EPA 6010
92365696001 514093 5142576001-HBW21 EPA 3020 EPA 6020
92365696002 514093 5142576001-HBW22 EPA 3020 EPA 6020
92365696003 514093 5142576001-HBW12B EPA 3020 EPA 6020
92365696004 514093 5142576001-HBW17B EPA 3020 EPA 6020
92365696005 514093 5142576001-MAINTE EPA 3020 EPA 6020
92365696001 3896626001-HBW21 EPA 8260
92365696002 3896626001-HBW22 EPA 8260
92365696003 3896626001-HBW12B EPA 8260
92365696004 3896626001-HBW17B EPA 8260
92365696005 3896626001-MAINTE EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 26
Page 24 of 26
Page 25 of 26
Page 26 of 26
#=CL#
December 22, 2017
LIMS USE: FR - AMBER GRZYMSKI
LIMS OBJECT ID: 92365694
92365694
Project:
Pace Project No.:
RE:
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
Harris Rd Landfill (Permit #60
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 05, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Minnesota Certification IDs
1700 Elm Street SE, Suite 200, Minneapolis, MN 55414-
2485
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #:MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Mississippi Certification #: MN00064
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon NwTPH Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DW Certification #: 9952 C
West Virginia DEP Certification #: 382
Wisconsin Certification #: 999407970
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92365694001 6001-HB2006 EPA 6010 14 PASI-ASER
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365694002 6001-HB2008 EPA 6010 14 PASI-ASER
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
92365694003 6001-HB2010 EPA 6010 14 PASI-ASER
EPA 6020 1 PASI-MTT3
EPA 8260 52 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Sample:6001-HB2006 Lab ID:92365694001 Collected:12/05/17 14:00 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/18/17 07:26 7440-36-012/06/17 22:455.0 1
Arsenic ND ug/L 12/18/17 07:26 7440-38-212/06/17 22:4510.0 1
Barium 18.0 ug/L 12/18/17 07:26 7440-39-312/06/17 22:455.0 1
Beryllium ND ug/L 12/18/17 07:26 7440-41-712/06/17 22:451.0 1
Cadmium ND ug/L 12/18/17 07:26 7440-43-912/06/17 22:451.0 1
Chromium ND ug/L 12/18/17 07:26 7440-47-312/06/17 22:455.0 1
Cobalt ND ug/L 12/18/17 07:26 7440-48-412/06/17 22:455.0 1
Copper ND ug/L 12/18/17 07:26 7440-50-812/06/17 22:455.0 1
Lead ND ug/L 12/18/17 07:26 7439-92-112/06/17 22:455.0 1
Nickel ND ug/L 12/18/17 07:26 7440-02-012/06/17 22:455.0 1
Selenium ND ug/L 12/18/17 07:26 7782-49-212/06/17 22:4510.0 1
Silver ND ug/L 12/18/17 07:26 7440-22-412/06/17 22:455.0 1
Vanadium ND ug/L 12/18/17 07:26 7440-62-212/06/17 22:455.0 1
Zinc ND ug/L 12/18/17 07:26 7440-66-612/06/17 22:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:34 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 01:09 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 01:09 107-13-110.0 1
Benzene ND ug/L 12/07/17 01:09 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 01:09 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 01:09 75-27-41.0 1
Bromoform ND ug/L 12/07/17 01:09 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 01:09 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 01:09 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 01:09 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 01:09 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 01:09 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 01:09 75-00-31.0 1
Chloroform ND ug/L 12/07/17 01:09 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 01:09 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 01:09 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 01:09 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 01:09 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 01:09 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 01:09 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 01:09 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 01:09 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 01:09 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 01:09 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 01:09 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 01:09 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 01:09 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 01:09 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Sample:6001-HB2006 Lab ID:92365694001 Collected:12/05/17 14:00 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 01:09 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 01:09 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 01:09 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 01:09 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 01:09 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 01:09 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 01:09 108-10-15.0 1
Styrene ND ug/L 12/07/17 01:09 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 01:09 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 01:09 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 01:09 127-18-41.0 1
Toluene ND ug/L 12/07/17 01:09 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 01:09 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 01:09 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 01:09 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 01:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 01:09 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 01:09 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 01:09 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 01:09 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 01:09 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 01:09 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %12/07/17 01:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/17 01:09 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/17 01:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Sample:6001-HB2008 Lab ID:92365694002 Collected:12/05/17 14:10 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/18/17 07:30 7440-36-012/06/17 22:455.0 1
Arsenic ND ug/L 12/18/17 07:30 7440-38-212/06/17 22:4510.0 1
Barium 21.7 ug/L 12/18/17 07:30 7440-39-312/06/17 22:455.0 1
Beryllium ND ug/L 12/18/17 07:30 7440-41-712/06/17 22:451.0 1
Cadmium ND ug/L 12/18/17 07:30 7440-43-912/06/17 22:451.0 1
Chromium ND ug/L 12/18/17 07:30 7440-47-312/06/17 22:455.0 1
Cobalt ND ug/L 12/18/17 07:30 7440-48-412/06/17 22:455.0 1
Copper ND ug/L 12/18/17 07:30 7440-50-812/06/17 22:455.0 1
Lead ND ug/L 12/18/17 07:30 7439-92-112/06/17 22:455.0 1
Nickel ND ug/L 12/18/17 07:30 7440-02-012/06/17 22:455.0 1
Selenium ND ug/L 12/18/17 07:30 7782-49-212/06/17 22:4510.0 1
Silver ND ug/L 12/18/17 07:30 7440-22-412/06/17 22:455.0 1
Vanadium ND ug/L 12/18/17 07:30 7440-62-212/06/17 22:455.0 1
Zinc ND ug/L 12/18/17 07:30 7440-66-612/06/17 22:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:51 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 01:27 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 01:27 107-13-110.0 1
Benzene ND ug/L 12/07/17 01:27 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 01:27 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 01:27 75-27-41.0 1
Bromoform ND ug/L 12/07/17 01:27 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 01:27 74-83-9 M12.0 1
2-Butanone (MEK)ND ug/L 12/07/17 01:27 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 01:27 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 01:27 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 01:27 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 01:27 75-00-31.0 1
Chloroform ND ug/L 12/07/17 01:27 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 01:27 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 01:27 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 01:27 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 01:27 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 01:27 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 01:27 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 01:27 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 01:27 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 01:27 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 01:27 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 01:27 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 01:27 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 01:27 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 01:27 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Sample:6001-HB2008 Lab ID:92365694002 Collected:12/05/17 14:10 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 01:27 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 01:27 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 01:27 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 01:27 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 01:27 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 01:27 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 01:27 108-10-15.0 1
Styrene ND ug/L 12/07/17 01:27 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 01:27 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 01:27 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 01:27 127-18-41.0 1
Toluene ND ug/L 12/07/17 01:27 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 01:27 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 01:27 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 01:27 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 01:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 01:27 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 01:27 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 01:27 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 01:27 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 01:27 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 01:27 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)92 %12/07/17 01:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/07/17 01:27 17060-07-070-130 1
Toluene-d8 (S)98 %12/07/17 01:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Sample:6001-HB2010 Lab ID:92365694003 Collected:12/05/17 10:50 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 12/18/17 07:42 7440-36-012/06/17 22:455.0 1
Arsenic ND ug/L 12/18/17 07:42 7440-38-212/06/17 22:4510.0 1
Barium 37.2 ug/L 12/18/17 07:42 7440-39-312/06/17 22:455.0 1
Beryllium ND ug/L 12/18/17 07:42 7440-41-712/06/17 22:451.0 1
Cadmium ND ug/L 12/18/17 07:42 7440-43-912/06/17 22:451.0 1
Chromium ND ug/L 12/18/17 07:42 7440-47-312/06/17 22:455.0 1
Cobalt ND ug/L 12/18/17 07:42 7440-48-412/06/17 22:455.0 1
Copper ND ug/L 12/18/17 07:42 7440-50-812/06/17 22:455.0 1
Lead ND ug/L 12/18/17 07:42 7439-92-112/06/17 22:455.0 1
Nickel ND ug/L 12/18/17 07:42 7440-02-012/06/17 22:455.0 1
Selenium ND ug/L 12/18/17 07:42 7782-49-212/06/17 22:4510.0 1
Silver ND ug/L 12/18/17 07:42 7440-22-412/06/17 22:455.0 1
Vanadium ND ug/L 12/18/17 07:42 7440-62-212/06/17 22:455.0 1
Zinc ND ug/L 12/18/17 07:42 7440-66-612/06/17 22:4510.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 30206020 MET ICPMS
Thallium ND ug/L 12/18/17 14:54 7440-28-012/18/17 07:090.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/17 01:45 67-64-125.0 1
Acrylonitrile ND ug/L 12/07/17 01:45 107-13-110.0 1
Benzene ND ug/L 12/07/17 01:45 71-43-21.0 1
Bromochloromethane ND ug/L 12/07/17 01:45 74-97-51.0 1
Bromodichloromethane ND ug/L 12/07/17 01:45 75-27-41.0 1
Bromoform ND ug/L 12/07/17 01:45 75-25-21.0 1
Bromomethane ND ug/L 12/07/17 01:45 74-83-92.0 1
2-Butanone (MEK)ND ug/L 12/07/17 01:45 78-93-35.0 1
Carbon disulfide ND ug/L 12/07/17 01:45 75-15-02.0 1
Carbon tetrachloride ND ug/L 12/07/17 01:45 56-23-51.0 1
Chlorobenzene ND ug/L 12/07/17 01:45 108-90-71.0 1
Chloroethane ND ug/L 12/07/17 01:45 75-00-31.0 1
Chloroform ND ug/L 12/07/17 01:45 67-66-31.0 1
Chloromethane ND ug/L 12/07/17 01:45 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/17 01:45 96-12-82.0 1
Dibromochloromethane ND ug/L 12/07/17 01:45 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/17 01:45 106-93-41.0 1
Dibromomethane ND ug/L 12/07/17 01:45 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 12/07/17 01:45 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 12/07/17 01:45 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/17 01:45 110-57-61.0 1
1,1-Dichloroethane ND ug/L 12/07/17 01:45 75-34-31.0 1
1,2-Dichloroethane ND ug/L 12/07/17 01:45 107-06-21.0 1
1,1-Dichloroethene ND ug/L 12/07/17 01:45 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 12/07/17 01:45 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 12/07/17 01:45 156-60-51.0 1
1,2-Dichloropropane ND ug/L 12/07/17 01:45 78-87-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 8 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Sample:6001-HB2010 Lab ID:92365694003 Collected:12/05/17 10:50 Received:12/05/17 15:22 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 12/07/17 01:45 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 12/07/17 01:45 10061-02-61.0 1
Ethylbenzene ND ug/L 12/07/17 01:45 100-41-41.0 1
2-Hexanone ND ug/L 12/07/17 01:45 591-78-65.0 1
Iodomethane ND ug/L 12/07/17 01:45 74-88-45.0 1
Methylene Chloride ND ug/L 12/07/17 01:45 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/17 01:45 108-10-15.0 1
Styrene ND ug/L 12/07/17 01:45 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/17 01:45 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/17 01:45 79-34-51.0 1
Tetrachloroethene ND ug/L 12/07/17 01:45 127-18-41.0 1
Toluene ND ug/L 12/07/17 01:45 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 12/07/17 01:45 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 12/07/17 01:45 79-00-51.0 1
Trichloroethene ND ug/L 12/07/17 01:45 79-01-61.0 1
Trichlorofluoromethane ND ug/L 12/07/17 01:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/07/17 01:45 96-18-41.0 1
Vinyl acetate ND ug/L 12/07/17 01:45 108-05-42.0 1
Vinyl chloride ND ug/L 12/07/17 01:45 75-01-41.0 1
Xylene (Total)ND ug/L 12/07/17 01:45 1330-20-71.0 1
m&p-Xylene ND ug/L 12/07/17 01:45 179601-23-12.0 1
o-Xylene ND ug/L 12/07/17 01:45 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %12/07/17 01:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/17 01:45 17060-07-070-130 1
Toluene-d8 (S)99 %12/07/17 01:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389726
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92365694001, 92365694002, 92365694003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2162165
Associated Lab Samples:92365694001, 92365694002, 92365694003
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 12/18/17 06:00
Arsenic ug/L ND 10.0 12/21/17 22:06
Barium ug/L ND 5.0 12/18/17 06:00
Beryllium ug/L ND 1.0 12/18/17 06:00
Cadmium ug/L ND 1.0 12/18/17 06:00
Chromium ug/L ND 5.0 12/18/17 06:00
Cobalt ug/L ND 5.0 12/18/17 06:00
Copper ug/L ND 5.0 12/18/17 06:00
Lead ug/L ND 5.0 12/18/17 06:00
Nickel ug/L ND 5.0 12/18/17 06:00
Selenium ug/L ND 10.0 12/18/17 06:00
Silver ug/L ND 5.0 12/18/17 06:00
Vanadium ug/L ND 5.0 12/18/17 06:00
Zinc ug/L ND 10.0 12/18/17 06:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2162166LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 421500 84 80-120
Arsenic ug/L 469500 94 80-120
Barium ug/L 460500 92 80-120
Beryllium ug/L 442500 88 80-120
Cadmium ug/L 449500 90 80-120
Chromium ug/L 451500 90 80-120
Cobalt ug/L 440500 88 80-120
Copper ug/L 459500 92 80-120
Lead ug/L 437500 87 80-120
Nickel ug/L 440500 88 80-120
Selenium ug/L 440500 88 80-120
Silver ug/L 218250 87 80-120
Vanadium ug/L 458500 92 80-120
Zinc ug/L 431500 86 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2162167MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92365630001
2162168
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 85 75-12584 250011.8 438 431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2162167MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92365630001
2162168
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 91 75-12590 1500ND459454
Barium ug/L 500 83 75-12582 2500ND415408
Beryllium ug/L 500 86 75-12585 1500ND432427
Cadmium ug/L 500 92 75-12591 1500ND460456
Chromium ug/L 500 88 75-12587 250013.4 456 448
Cobalt ug/L 500 79 75-12579 0500227622620
Copper ug/L 500 95 75-12593 2500ND479470
Lead ug/L 500 78 75-12578 1500ND391389
Nickel ug/L 500 79 75-12578 1500179572569
Selenium ug/L 500 89 75-12589 1500ND447444
Silver ug/L 250 95 75-12593 1250ND237234
Vanadium ug/L 500 92 75-12591 1500ND458454
Zinc ug/L 500 83 75-12583 0500193609608
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
514093
EPA 3020
EPA 6020
6020 MET
Associated Lab Samples:92365694001, 92365694002, 92365694003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2796082
Associated Lab Samples:92365694001, 92365694002, 92365694003
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 12/18/17 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2796083LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 105100 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2796084MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92363096001
2796085
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 101 75-125103 31000.19 101 104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
389662
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92365694001, 92365694002, 92365694003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2161466
Associated Lab Samples:92365694001, 92365694002, 92365694003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/07/17 00:34
1,1,1-Trichloroethane ug/L ND 1.0 12/07/17 00:34
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/07/17 00:34
1,1,2-Trichloroethane ug/L ND 1.0 12/07/17 00:34
1,1-Dichloroethane ug/L ND 1.0 12/07/17 00:34
1,1-Dichloroethene ug/L ND 1.0 12/07/17 00:34
1,2,3-Trichloropropane ug/L ND 1.0 12/07/17 00:34
1,2-Dibromo-3-chloropropane ug/L ND 2.0 12/07/17 00:34
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/17 00:34
1,2-Dichlorobenzene ug/L ND 1.0 12/07/17 00:34
1,2-Dichloroethane ug/L ND 1.0 12/07/17 00:34
1,2-Dichloropropane ug/L ND 1.0 12/07/17 00:34
1,4-Dichlorobenzene ug/L ND 1.0 12/07/17 00:34
2-Butanone (MEK)ug/L ND 5.0 12/07/17 00:34
2-Hexanone ug/L ND 5.0 12/07/17 00:34
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 12/07/17 00:34
Acetone ug/L ND 25.0 12/07/17 00:34
Acrylonitrile ug/L ND 10.0 12/07/17 00:34
Benzene ug/L ND 1.0 12/07/17 00:34
Bromochloromethane ug/L ND 1.0 12/07/17 00:34
Bromodichloromethane ug/L ND 1.0 12/07/17 00:34
Bromoform ug/L ND 1.0 12/07/17 00:34
Bromomethane ug/L ND 2.0 12/07/17 00:34
Carbon disulfide ug/L ND 2.0 12/07/17 00:34
Carbon tetrachloride ug/L ND 1.0 12/07/17 00:34
Chlorobenzene ug/L ND 1.0 12/07/17 00:34
Chloroethane ug/L ND 1.0 12/07/17 00:34
Chloroform ug/L ND 1.0 12/07/17 00:34
Chloromethane ug/L ND 1.0 12/07/17 00:34
cis-1,2-Dichloroethene ug/L ND 1.0 12/07/17 00:34
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/17 00:34
Dibromochloromethane ug/L ND 1.0 12/07/17 00:34
Dibromomethane ug/L ND 1.0 12/07/17 00:34
Ethylbenzene ug/L ND 1.0 12/07/17 00:34
Iodomethane ug/L ND 5.0 12/07/17 00:34
m&p-Xylene ug/L ND 2.0 12/07/17 00:34
Methylene Chloride ug/L ND 1.0 12/07/17 00:34
o-Xylene ug/L ND 1.0 12/07/17 00:34
Styrene ug/L ND 1.0 12/07/17 00:34
Tetrachloroethene ug/L ND 1.0 12/07/17 00:34
Toluene ug/L ND 1.0 12/07/17 00:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2161466
Associated Lab Samples:92365694001, 92365694002, 92365694003
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 12/07/17 00:34
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/17 00:34
trans-1,4-Dichloro-2-butene ug/L ND 1.0 12/07/17 00:34
Trichloroethene ug/L ND 1.0 12/07/17 00:34
Trichlorofluoromethane ug/L ND 1.0 12/07/17 00:34
Vinyl acetate ug/L ND 2.0 12/07/17 00:34
Vinyl chloride ug/L ND 1.0 12/07/17 00:34
Xylene (Total)ug/L ND 1.0 12/07/17 00:34
1,2-Dichloroethane-d4 (S)%94 70-130 12/07/17 00:34
4-Bromofluorobenzene (S)%95 70-130 12/07/17 00:34
Toluene-d8 (S)%107 70-130 12/07/17 00:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2161467LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.850 94 80-125
1,1,1-Trichloroethane ug/L 43.650 87 71-129
1,1,2,2-Tetrachloroethane ug/L 45.450 91 79-124
1,1,2-Trichloroethane ug/L 51.750 103 85-125
1,1-Dichloroethane ug/L 46.050 92 73-126
1,1-Dichloroethene ug/L 47.050 94 66-135
1,2,3-Trichloropropane ug/L 46.850 94 75-130
1,2-Dibromo-3-chloropropane ug/L 48.350 97 71-133
1,2-Dibromoethane (EDB)ug/L 46.750 93 83-124
1,2-Dichlorobenzene ug/L 49.050 98 80-133
1,2-Dichloroethane ug/L 44.450 89 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
1,4-Dichlorobenzene ug/L 47.350 95 78-130
2-Butanone (MEK)ug/L 95.0100 95 61-144
2-Hexanone ug/L 92.6100 93 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 89.7100 90 48-146
Acrylonitrile ug/L 233250 93 40-160
Benzene ug/L 50.450 101 80-125
Bromochloromethane ug/L 47.050 94 71-125
Bromodichloromethane ug/L 48.350 97 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 44.450 89 40-160
Carbon disulfide ug/L 46.050 92 50-160
Carbon tetrachloride ug/L 48.850 98 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 55.350 111 39-148
Chloroform ug/L 44.850 90 73-127
Chloromethane ug/L 39.450 79 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2161467LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 47.550 95 74-124
cis-1,3-Dichloropropene ug/L 51.250 102 72-132
Dibromochloromethane ug/L 47.450 95 78-125
Dibromomethane ug/L 49.850 100 82-120
Ethylbenzene ug/L 45.850 92 79-121
Iodomethane ug/L 84.2100 84 39-154
m&p-Xylene ug/L 94.7100 95 81-124
Methylene Chloride ug/L 46.350 93 64-133
o-Xylene ug/L 46.250 92 79-131
Styrene ug/L 46.150 92 84-126
Tetrachloroethene ug/L 45.550 91 78-122
Toluene ug/L 49.950 100 80-121
trans-1,2-Dichloroethene ug/L 46.350 93 71-127
trans-1,3-Dichloropropene ug/L 52.050 104 69-141
trans-1,4-Dichloro-2-butene ug/L 44.050 88 40-160
Trichloroethene ug/L 45.750 91 78-122
Trichlorofluoromethane ug/L 45.850 92 53-137
Vinyl acetate ug/L 94.5100 95 40-160
Vinyl chloride ug/L 46.650 93 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%107 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2165992MATRIX SPIKE SAMPLE:
MSSpike
Result
92365694002
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 20.220 101 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethane ug/L 19.220 95 70-130ND
1,1-Dichloroethene ug/L 20.020 100 70-166ND
1,2,3-Trichloropropane ug/L 18.220 91 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.920 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.520 103 70-130ND
1,2-Dichlorobenzene ug/L 20.420 102 70-130ND
1,2-Dichloroethane ug/L 19.320 97 70-130ND
1,2-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 37.440 93 70-130ND
2-Hexanone ug/L 38.240 95 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.540 94 70-130ND
Acetone ug/L 37.740 94 70-130ND
Acrylonitrile ug/L 90.7100 91 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2165992MATRIX SPIKE SAMPLE:
MSSpike
Result
92365694002
Benzene ug/L 20.520 103 70-148ND
Bromochloromethane ug/L 20.820 104 70-130ND
Bromodichloromethane ug/L 20.220 101 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 11.6 M1205870-130ND
Carbon disulfide ug/L 19.120 95 70-130ND
Carbon tetrachloride ug/L 21.520 108 70-130ND
Chlorobenzene ug/L 20.720 103 70-146ND
Chloroethane ug/L 23.120 115 70-130ND
Chloroform ug/L 18.820 94 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
cis-1,2-Dichloroethene ug/L 19.420 97 70-130ND
cis-1,3-Dichloropropene ug/L 20.720 104 70-130ND
Dibromochloromethane ug/L 21.120 106 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Ethylbenzene ug/L 20.720 104 70-130ND
Iodomethane ug/L 13.940 35 70-130ND
m&p-Xylene ug/L 41.940 105 70-130ND
Methylene Chloride ug/L 16.420 82 70-130ND
o-Xylene ug/L 22.620 113 70-130ND
Styrene ug/L 21.520 108 70-130ND
Tetrachloroethene ug/L 22.820 114 70-130ND
Toluene ug/L 20.020 100 70-155ND
trans-1,2-Dichloroethene ug/L 19.820 99 70-130ND
trans-1,3-Dichloropropene ug/L 19.720 99 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.620 78 70-130ND
Trichloroethene ug/L 21.620 108 69-151ND
Trichlorofluoromethane ug/L 20.220 101 70-130ND
Vinyl acetate ug/L 37.940 95 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92365694003
2165993SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92365694003
2165993SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%90 796
4-Bromofluorobenzene (S)%91 394
Toluene-d8 (S)%105 699
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92365694
Harris Rd Landfill (Permit #60
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92365694001 389726 3897706001-HB2006 EPA 3010A EPA 6010
92365694002 389726 3897706001-HB2008 EPA 3010A EPA 6010
92365694003 389726 3897706001-HB2010 EPA 3010A EPA 6010
92365694001 514093 5142576001-HB2006 EPA 3020 EPA 6020
92365694002 514093 5142576001-HB2008 EPA 3020 EPA 6020
92365694003 514093 5142576001-HB2010 EPA 3020 EPA 6020
92365694001 3896626001-HB2006 EPA 8260
92365694002 3896626001-HB2008 EPA 8260
92365694003 3896626001-HB2010 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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