9801_WilsonCounty_MSWLF_GWMR_20171004

November 8, 2017

Mr. Ervin Lane, Hydrogeologist
NC Division of Waste Management
Solid Waste Section
Mail Service Center 1646
Raleigh, NC 27699-1646

Re: 2017 Second Semi-Annual Water Quality Monitoring Results
Closed Wilson County Landfill
Wilson, North Carolina
Permit #98-01

Dear Ervin:

Babb & Associates, P.A. has completed the 2017 second semi-annual sampling event at the closed Wilson
County Landfill. On October 4, 2017, nine groundwater monitoring wells and five surface water
monitoring stations were sampled and analyzed for volatile organic compounds (VOCs) by EPA Method
8260 and Appendix I inorganic compounds.

A site map is provided with this report which shows the groundwater and surface water sample locations
and shallow potentiometric surface. Additional attachments to this report include tables summarizing the
groundwater and surface water analytical results (Tables 1 & 2), field parameters collected during the
monitoring event (Table 3), well construction information (Table 4), and groundwater flow rates (Table 5).
The laboratory analytical report, in pdf and EDD formats, is included as Appendix A.

If there are any questions regarding the attached information, please contact me at [phone].

Respectfully,

Babb & Associates, P.A.

Gary D. Babb, P.G.
President

Enclosures

cc: Mr. Andy Davis, Director
Wilson County Solid Waste

Water Quality Monitoring Report

Wilson County Municipal Solid Waste Landfill
2400 Highway 42 East
Wilson, North Carolina
Permit No. 98-01

Prepared for:

Wilson County Solid Waste
P.O. Box 1728
Wilson, North Carolina 27894

Prepared by:

Babb & Associates, P.A.
P.O. Box 37697
Raleigh, North Carolina 27627

October 2017

___________________________________
Gary D. Babb, Licensed Geologist

Table of Contents

1.0 Introduction 1
1.1 Site Information
1.2 Site Geology
1.3 Site Hydrogeology

2.0 Water Quality Monitoring Program 5
2.1 Groundwater Monitoring Network
2.2 Surface Water Monitoring Network

3.0 Water Quality Sample Collection 7
3.1 Field Sample Procedures
3.2 Field Quality Assurance
3.3 Sample Delivery/Chain-of-Custody

4.0 Laboratory Analysis 9

5.0 Hydrogeological Conditions 10

6.0 Laboratory Analytical Results 11
6.1 Groundwater Analytical Results
6.2 Surface Water Analytical Results
6.3 Quality Control Sample

7.0 Conclusions 13

Figure 1 Water Quality Monitoring Sample Locations/Potentiometric Map

Table 1 Groundwater Analytical Results
Table 2 Surface Water Analytical Results
Table 3 Field Parameter Measurements
Table 4 Well Construction Information/Elevations
Table 5 Groundwater Flow Rates

Appendix A ENCO Laboratory Analytical Report

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 1

1.0 Introduction

1.1 Site Information

The closed Wilson County Landfill is located approximately 3.5 miles east of downtown
Wilson, NC at the intersection of NC 42 and Tucker Court. Originally, the site of the
closed Wilson County Landfill facility was dominated by a hill (approximately 108 feet
above msl) located in the central portion of the present site. Several residential/farm
houses were located in the northeast portion of the site. An intermittent stream
originating in the northern portion of the site flowed southeastward eventually flowing
into an unnamed stream southeast of the site. This unnamed stream flowed westward
becoming part of the southern site boundary and traversed the southwestern most portion
of the site and emptied into the Toisnot Swamp Canal. The remainder of the site
contained drainage features that radiated outward from the dominant hill and discharged
into these streams or with other drainage features located to the northwest of the site.
Wetland areas were associated with streams and the Toisnot Swamp. Prior to
construction of the landfill facility, agriculture was the primary land use in this area of
Wilson County.

Surrounding properties within 1,500 feet of the site are currently being used for farming,
residential, or solid waste management purposes. Land south of the site is mostly
farmland with a mobile home park located approximately 1,200 feet to the south. Land
immediately west of the site is owned by Wilson County and used for construction and
demolition debris disposal, recycling/reclaimation, and other solid waste management
activities. Land north of the site is mostly used for farmland with wooded areas. Land
east of the site is mostly farmland with wooded areas and light residential use.

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October 2017 Page 2

1.2 Site Geology

The closed Wilson County Landfill is located in the western portion of the Carolina
Coastal Plain near the Fall Line. The Fall Line is the province boundary between the
Piedmont and the Coastal Plain provinces. It represents a significant change in lithology,
which in turn reflects a change in stream gradients. Lithology of the Piedmont province
is primarily igneous and metamorphic while the Coastal Plain province is primarily
sedimentary. In general, rivers and streams in the Piedmont province have higher flow
rates with well-defined channels while Coastal Plain rivers and streams are meandering
with lesser defined channels resulting in swamps and bays. These streams, swamps, and
bays are the major discharge point of the uppermost aquifer.

The Carolina Coastal Plain is underlain by flat-lying to very gently eastward dipping
sedimentary strata which overlay a foundation of crystalline rocks. These sediments
were deposited during repeated marine transgressive and regressive cycles due to
fluctuations in sea level caused by expansion and recession of glacial ice caps during the
Pliocene and early Pleistocene epochs (approximately 2 to 5 million years ago).

Sediments in the area of the closed Wilson County Landfill facility are classified as being
in the Yorktown Formation. Information gathered from the Geologic Map of North
Carolina, 1985 and The Geology of the Carolina, 1991, cites that sediments of the
Yorktown Formation are fossiliferous clay with varying amounts of fine-grained sand,
silty sand, sandy silt, silty clay, and bluish gray shell material. These types of deposits
are found mainly north of the Neuse River and are commonly concentrated in lenses and
vary in vertical and horizontal dimensions. The topography of the Coastal Plain is
characterized by flat to gently undulating relief.

The local geology is characterized by relatively thin layers (0.5 - 7.0 feet) of clays, silts,
and sands in varying textures and colors that overlie a gray/black silty clay/sand that is
found throughout the area. The drainage canals located on the northwest and southeast
Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 3

property boundaries expose these silty clay and sand layers. The original soils at the site
were excavated to create capacity for waste disposal.

1.3 Site Hydrogeology

The major groundwater discharge features influencing groundwater flow direction at the
site are the Toisnot Swamp and drainage ditches located to the southeast and northwest of
the site. Groundwater level measurements collected on October 4, 2017 indicate that the
general groundwater flow direction on the facility is to the south-southeast towards the
Toisnot Swamp Canal. However, the presence of drainage ditches have an impact on
localized groundwater flow. Groundwater flow near the southeastern drainage ditch
tends to be in a more southerly direction towards the drainage ditch. A Potentiometric
Map indicating groundwater flow directions is provided as Figure 1.

Aquifer hydraulic conductivity testing was performed in June 1997 on five of the site
monitoring wells and consisted of rising and falling head tests (slug tests). The results of
the slug test data was analyzed using the Bouwer and Rice method and are summarized
on the table below:

WELL ID HYDRAULIC
CONDUCTIVITY
(centimeters/second)
TYPE OF TEST FORMATION
MW-3A 3.80 x 10-5 Falling Yorktown
P-3 1.27 x 10-4 Rising Alluvium/Yorktown
MW-4 1.01 x 10-4 Rising Alluvium
MW-4 5.89 x 10-4 Falling Alluvium
MW-5 8.50 x 10-5 Rising Alluvium
MW-5 2.06 x 10-4 Falling Alluvium
MW-6 1.85 x 10-4 Rising Yorktown
MW-6 6.53 x 10-4 Falling Yorktown
MW-7 1.66 x 10-4 Rising Alluvium
MW-7 1.95 x 10-4 Falling Alluvium

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 4

The geometric average of the shallow water table aquifer hydraulic conductivity is 2.56 x
10-4 cm/sec (0.73 feet per day). This value may be considered a reasonable estimate of
the hydraulic conductivity of the shallow water table aquifer at the closed Wilson County
Landfill site.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 5

2.0 Water Quality Monitoring Program

The water quality monitoring network at the closed Wilson County Landfill is evaluated on a
semi-annual basis. The location of the groundwater and surface water samples collected during
the semi-annual monitoring events is shown on the attached Figure 1.

2.1 Groundwater Monitoring Network

There are nine groundwater monitoring wells located at the facility that comprise the
existing groundwater monitoring system (Figure 1). Monitoring well MW-1A is located
to the northwest of the landfill area and serves as the sidegradient groundwater
monitoring well. This well is situated on the northwest edge of the drainage ditch that
separates former fill and borrow areas. Monitoring well MW-2 is located at the entrance
to the landfill at Landfill Road (SR 1503) and serves as the upgradient groundwater
monitoring well providing background water quality. Monitoring well MW-3 is located
on the landfill side of the drainage ditch on the southeast property boundary of the
landfill. Monitoring well MW-3A, added in 2004, is also located on the southeastern side
of the landfill but on the opposite side of the drainage ditch. Monitoring wells MW-4 and
MW-5 are both located to the southwest and downgradient of the landfill but
hydraulically upgradient of the Toisnot Swamp Canal. Monitoring wells MW-6 and
MW-7 are located on the southeast border of the landfill. Monitoring well MW-8 is
considered a side-gradient monitoring well to the west of the former landfill area.

Table 4 provides monitoring well construction information including installation date,
well depth/screened interval, survey elevations, and lat/long for each well location. Table
5 provides the estimated hydraulic conductivity values for select monitoring wells based
on falling/rising head slug tests.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 6

2.2 Surface Water Monitoring Network

There are presently five surface water monitoring stations associated with the closed
Wilson County Landfill. Surface water monitoring stations SW-1 and SW-2 are both
located on the Toisnot Swamp Canal. The upstream sampling location (SW-1) is located
approximately 400 feet northwest of the landfill property boundary. The downstream
sampling location (SW-2) is located approximately 1,100 feet southeast of the landfill
property boundary. The drainage canal located along the southeastern boundary of the
landfill is monitored with surface water stations SW-3 and SW-4. The drainage canal
located on the northwestern boundary of the landfill is monitoring with surface water
station SW-5. Please note that surface water station SW-5 was dry at the time of sample
collection. These surface water monitoring locations are shown on Figure 1.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 7

3.0 Water Quality Sample Collection

Samples of groundwater and surface water were collected in accordance with the approved
Wilson County 1996 Water Quality Monitoring Plan and the 2008 NC Solid Waste Section
Guidelines for Groundwater, Soil, and Surface Water Sampling Guidance Document. A brief
description of the sample collection procedure is provided below.

3.1 Field Sample Procedures

Prior to groundwater sampling, water levels were obtained from each well using an
electric water level meter capable of measuring the depth to water to the nearest 0.01 feet.
This information was later used to determine the elevation of the water table in each
monitoring well relative to surveyed datum (Table 3). The depth to water in each well
was also used to determine the volume of standing water in the well casing. This
information allowed for the purging of a minimum of three casing volumes from each
well prior to sample collection to assure a fresh groundwater sample was collected. New
disposable laboratory gloves were worn by sampling personnel and each well was purged
and sampled with a new disposable bailer which was discarded after use.

After the monitoring wells had been allowed to recover from purging, samples were
collected in the following order:

 Volatile organic compounds
 Inorganic compounds
 Field Parameters (pH, Conductivity, Temperature)

The samples are collected directly in the laboratory-supplied containers which are pre-
filled with the appropriate preservative. No filtering of the samples is performed prior to
collection. After collection, the samples are placed in a cooler on ice for overnight
shipment to the analytical laboratory.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 8

Surface water samples are collected directly into the laboratory-supplied containers as
grab samples. Sampling personnel wear new disposable laboratory gloves for each
surface water sample collected. As with the groundwater samples, these samples are
stored in a cooler on ice prior to overnight delivery to the analytical laboratory.

3.2 Field Quality Assurance

One trip blank sample was prepared by the analytical laboratory and accompanied the
sample shipment until receipt back at the laboratory. The trip blank sample was analyzed
for volatile organic compounds. Temperature blanks are also provided with the sample
shipments to assure the proper temperature is maintained until delivery to the analytical
laboratory.

3.3 Sample Delivery/Chain of Custody

All groundwater and surface water samples are stored in coolers on ice immediately after
collection. Individual sample containers for each well or surface water sample are placed
in zip lock plastic bags to reduce the potential for cross contamination. Chain-of-Custody
control documents are prepared and shipped with each cooler. Custody seals are also
used for each cooler to maintain sample integrity until delivery to the analytical
laboratory. The sample coolers are shipped via Federal Express for next morning
delivery to the analytical laboratory.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 9

4.0 Laboratory Analysis

The samples were analyzed for parameters specified by the Solid Waste Section for Detection
Monitoring at permitted solid waste facilities. The standard Detection Monitoring Program for
groundwater and surface water samples consists of the Appendix I parameters. The Appendix I
analysis consists of volatile organic compounds by EPA Method 8260B and inorganic
compounds by EPA Methods 6010C/6020A.

The laboratory performing the water quality analysis is Environmental Conservation
Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory.
Internal quality control samples, including matrix spikes/matrix spike duplicates, are performed
by ENCO for each set of samples. The ENCO laboratory report, including internal quality
control samples, is provided with this report in Appendix A.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 10

5.0 Hydrogeological Conditions

The depth to groundwater was measured in the nine compliance monitoring wells during the
October 4, 2017 monitoring event. The groundwater elevations were calculated relative to the
surveyed measuring point (top of casing) for each monitoring well. The groundwater elevations
are summarized on Table 3 and the potentiometric surface of the shallow water table is shown on
Figure 1.

The general direction of groundwater flow, based on the water level information collected during
this monitoring event, is also shown on Figure 1. Groundwater flow direction is generally to the
south-southwest, toward the Toisnot Swamp Canal.

Based on the results of prior hydrologic tests conducted at the site, groundwater flow rate in the
shallow saprolite ranges from 0.108 ft/day to 1.85 ft/day. The average hydraulic conductivity
and transmissivity values for the site are provided on Table 5.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 11

6.0 Laboratory Analytical Results

Final laboratory analytical results for the samples collected on October 4, 2017 were received
from the analytical laboratory on October 17, 2017. A summary of the analytical results are
provided on Table 1 (groundwater), Table 2 (surface water), and Table 3 (field parameters).

6.1 Groundwater Analytical Results

During this monitoring event, four volatile organic compounds (VOCs) were reported
above the laboratory reporting limits. Monitoring well MW-7 reported the compounds
cis-1,2-dichloroethene, tetrachloroethene, trichloroethene, and vinyl chloride at
concentrations above the laboratory method reporting limits. Of these four reported
VOCs, only two compounds (tetrachloroethene – 1.5 ug/l and vinyl chloride – 1.7 ug/l)
exceeded the NC 2L Groundwater Standard of 0.7 ug/l and 0.03 ug/l, respectively. No
other VOCs were detected at concentrations exceeding the laboratory reporting limits,
Solid Waste Section Limits (SWSLs), or the NC 2L Groundwater Standards in any of the
remaining eight groundwater monitoring wells.

No inorganic compounds were detected at a concentration that exceeded the NC 2L
Groundwater Standards in any of the nine groundwater monitoring wells sampled during
this monitoring event. The inorganic compound barium was reported above the
laboratory detection limit and SWSL in monitoring wells MW-3A, MW-4, MW-5, and
MW-7; however, the reported concentrations did not exceed the established NC 2L
Groundwater Standard. The inorganic compound beryllium was reported above the
laboratory detection limit and SWSL in monitoring wells MW-1A, MW-3 and MW-6;
however, there is no established NC 2L Groundwater Standard for beryllium. Monitoring
wells MW-1A and MW-6 also reported a detectable concentrations of cobalt, which does
not have an established NC 2L Groundwater Standard. Monitoring wells MW-1A, MW-
3, MW-6, and MW-8 reported detectable concentrations of zinc, although the
concentrations were well below the established NC 2L Groundwater Standard. A
Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 12

summary of the groundwater laboratory analytical results and the corresponding NC 2L
Groundwater Standards are provided on Table 1.

6.2 Surface Water Analytical Results

The laboratory analytical report indicated no VOCs were present in any of the surface
water samples above the SWSLs, laboratory detection limits, or 2B Surface Water
Standards.

The inorganic compound barium was reported above the laboratory reporting limit and
SWSL in surface water sample SW-1. The reported barium concentration in SW-1 of
160 ug/l is well below the established 2B Surface Water Standard of 1000 ug/l.
No other inorganic compounds were reported above the laboratory reporting limits,
SWSLs, or NC 2B Surface Water Standards in the samples collected from the four
surface water monitoring stations. Please note that surface water station SW-5 was dry at
the time of sample collection. A summary of the surface water analytical results and
corresponding NC 2B Surface Water Standard for the four surface water samples is
provided on Table 2.

6.3 Quality Control Sample

One trip blank was submitted and analyzed for quality assurance purposes. No VOCs
were detected at a concentration equaling or exceeding laboratory quantitation limits in
the trip blank.

Wilson County Closed Landfill Water Quality Monitoring Report
October 2017 Page 13

7.0 Conclusions

The results of this monitoring event report only minor variants from the established NC 2L
Groundwater Standards and NC 2B Surface Water Standards. Based on the results of this water
quality monitoring event, the closed Wilson County Landfill will remain in Detection
Monitoring in accordance with Title 15A NACA 13B .0601. The 2018 spring semi-annual water
quality monitoring event is tentatively scheduled for May 2018.

Attachments to this report include tables summarizing the groundwater and surface water
analytical results (Tables 1 & 2), field parameters collected during the monitoring event (Table
3), well construction information (Table 4), and hydrologic test results (Table 5). A copy of the
laboratory analytical report in pdf and EDD formats is included with this report in Appendix A.

SITE MAP

TABLES

TABLE 12017 Second Semi-Annual Groundwater Laboratory Analytical ResultsWilson County MSWLFWilson, North CarolinaPermit #98-01Parameter MW-1A MW-2 MW-3 MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 2L Std.Metals (ug/l) Barium 87.4 J 68.6 J 99.4 J 272 561 620 39.4 J 113 79.3 J 700Beryllium 1.65 BQL 1.85 BQL BQL BQL 2.07 0.174 J 0.289 J NECadmium BQL BQL BQL BQL BQL BQL 0.814 J BQL BQL 2Chromium BQL BQL BQL BQL BQL 1.87 J BQL BQL BQL 10Cobalt 23.2 BQL 2.46 J BQL BQL 2.66 J 19.9 BQL 3.84 J NECopper BQL BQL BQL BQL BQL BQL BQL BQL BQL 1000Nickel 32.2 J BQL 5.71 J BQL BQL 3.09 J 34.6 J BQL 4.42 J 100Selenium BQL BQL BQL BQL BQL BQL 2.31 J BQL BQL 20Silver BQL BQL BQL BQL BQL BQL BQL BQL BQL 20Thallium 0.787 J 0.558 J 0.336 J 0.362 J 0.527 J 0.574 J 0.596 J 0.816 J 0.758 J NEVanadium BQL BQL BQL BQL BQL 2.21 J 7.09 J BQL BQL NEZinc 67.7 6.59 J 19.0 BQL BQL BQL 50.8 9.18 J 10.6 1000Method 8260B (ug/l) 1,4-Dichlorobenzene BQL BQL BQL BQL BQL BQL BQL 0.84 J BQL 61,1-Dichloroethane BQL BQL BQL BQL BQL BQL BQL 3.5 J BQL 6cis-1,2-Dichloroethene BQL BQL BQL BQL BQL BQL BQL 47.0 BQL 701,2-Dichloropropane BQL BQL BQL BQL BQL BQL BQL 0.80 J BQL 0.6Tetrachloroethene BQL BQL BQL BQL BQL BQL BQL1.5BQL 0.7Trichloroethene BQL BQL BQL BQL BQL BQL BQL 1.7 BQL 3Vinyl Chloride BQL BQL BQL BQL BQL BQL BQL1.7BQL 0.03Notes:Samples collected on October 4, 2017BQL - Below laboratory quantitation limit.Bold concentrations equal or exceed established or interim standards.NE - Not established.J - Between MDL and RL
TABLE 22017 Second Semi-Annual Surface Water Laboratory Analytical ResultsWilson County MSWLFWilson, North CarolinaPermit #98-01Parameter SW-1 SW-2 SW-3 SW-4 SW-5 2B Std.Metals (ug/l) Dry Arsenic BQL BQL BQL BQL 10Barium 160 86.7 J 20.1 J 90.3 J 1000Beryllium BQL BQL BQL BQL 6.5Cadmium BQL BQL BQL BQL 2Chromium BQL BQL BQL BQL 50Cobalt 1.53 J 2.49 J 1.60 J 2.85 J 3Copper BQL BQL BQL BQL 7Lead BQL BQL BQL BQL 25Nickel BQL BQL 3.62 J BQL 88Silver BQL BQL BQL BQL 0.06Thallium 0.60 J 0.652 J 0.636 J 0.713 J 0.47Vanadium BQL BQL BQL BQL NEZinc BQL 6.62 J 7.82 J 4.60 J 50Method 8260B (ug/l)Dry4-Methyl-2-pentanone BQL BQL BQL BQL 26cis-1,2-Dichloroethene BQL 0.72 J BQL 1.2 J 330Toluene BQL BQL BQL BQL 11Notes:Samples collected on October 4, 2017BQL - Below laboratory quantitation limit.Bold concentrations equal or exceed established or interim standards.NE - Not established.J - Between MDL and RL
TABLE 32017 Second Semi-Annual Field ParametersWilson County MSWLFWilson, North CarolinaPermit #98-01Monitoring WellSample Date Sample Time Depth to GW GW Elevation Conductivity Temperature - C pHMW-1A 10/4/2017 915 16.92 92.47 340 21.3 6.0MW-2 10/4/2017 1240 10.80 109.24 56 23.9 4.8MW-3 10/4/2017 1150 18.97 89.17 111 19.2 5.7MW-3A 10/4/2017 1200 19.99 95.44 370 20.7 7.3MW-4 10/4/2017 1030 3.38 81.44 1128 20.2 6.5MW-5 10/4/2017 1010 5.57 81.57 1192 20.2 6.0MW-6 10/4/2017 1215 22.49 86.97 199 19.6 4.6MW-7 10/4/2017 1130 8.25 82.35 160 20.4 6.1MW-8 10/4/2017 920 10.58 81.68 227 19.1 5.2SW-1 10/4/2017 1100 NA NA 544 19.3 7.1SW-2 10/4/2017 1050 NA NA 154 17.9 7.0SW-3 10/4/2017 1225 NA NA 402 21.7 4.0SW-4 10/4/2017 1040 NA NA 164 17.4 7.3SW-5 10/4/2017 Dry NA NA Dry Dry Dry
TABLE 4Groundwater Monitoring Well ConstructionWilson County MSW LandfillWilson, North CaroliinaPermit #98-01Well IDDate DrilledWell DiameterTotal DepthTOS DepthScreened IntervalGround ElevationTOC ElevationGroundwater DepthGroundwater ElevationLat/Long GeologyMW-1A 6/3/04 2" 30.0' 15.0' 15' - 30' 107.10 109.39 16.92 92.47717305.1 N 2340146.21 Esilty sandy CLAYMW-2 4/26/89 2" 14.0' 4.0' 4' - 14' 118.02 120.04 10.80 109.24717575.76 N 2342716.01 Esilty sandy CLAYMW-3 6/3/04 2" 25.0' 10.0' 10' - 25' 105.86 108.14 18.97 89.17716665.86 N 2341686.99 Efine SANDMW-3A 5/15/97 2" 34.0' 24.0' 24' - 34' 113.74 115.43 19.99 95.44716681.30 N 2341690.92 Emed. grey SILTMW-4 4/26/89 2" 13.0' 3.0' 3' - 13' 82.88 84.82 3.38 81.44715502.17 N 2339430.85 Esilty sandy CLAYMW-5 4/26/89 2" 13.0' 3.0' 3' - 13' 85.48 87.14 5.57 81.57715895.82 N 2339078.98 Esilty sandy CLAYMW-6 5/15/97 2" 28.0' 18.0' 18' - 28' 106.06 109.46 22.49 86.97716169.90 N 2341285.55 Ef. to coarse SANDMW-7 5/15/97 2" 15.0' 10.0' 10' - 15' 86.08 90.60 8.25 82.35715883.59 N 2340278.91 Esilty sandy CLAYMW-8 6/3/04 2" 20.0' 5.0' 5' - 20' 89.86 92.26 10.58 81.68716707.97 N 2339545.89 Ecoarse SANDTOS - Top of ScreenTOC - Top of CasingGroundwater depths collected on 10/4/2017
TABLE 5Groundwater Flow Rates 1Wilson County MSW LandfillWilson, North CarolinaPermit #98-01Test Piezometer Test Type 2Hydraulic Conductivity (centimeters/second)Hydraulic Conductivity (feet/day)Geologic MaterialMW-3A Falling Head 3.80 x 10-50.108 med. grey SILTMW-4 Rising Head 1.01 x 10-40.227 silty sandy CLAYMW-4 Falling Head 5.89 x 10-41.67 silty sandy CLAYMW-5 Rising Head 8.50 x 10-50.24 silty sandy CLAYMW-5 Falling Head 2.06 x 10-40.585 silty sandy CLAYMW-6 Rising Head 1.85 x 10-40.524 f. to coarse SANDMW-6 Falling Head 6.53 x 10-41.85 f. to coarse SANDMW-7 Rising Head 1.66 x 10-40.471 silty sandy CLAYMW-7 Falling Head 1.95 x 10-40.553 silty sandy CLAY1 Data from June 2003 Groundwater and Surface Water Assessment Report2 Aquifer Testing by falling/rising head slug tests, analyzed using Bouwer and Rice method

LAB REPORT

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CA14379
Raleigh, NC 27606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Wilson County MSWLF
Attn: Gary Babb
Babb & Associates (BA024)
3605 Country Cove Lane
Bill Scott
Project Manager
Monday, October 16, 2017
RE: Laboratory Results for
Dear Gary Babb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, October 5, 2017.
The total number of pages in this report, including this page is 55.
Page 1 of 58
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
9801-MW1A CA14379-01 Sampled:10/04/17 09:15 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:27
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 13:27
EPA 8260B 10/18/17 10/12/17 12:37 10/12/2017 22:00
9801-MW2 CA14379-02 Sampled:10/04/17 12:40 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:29
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 13:30
EPA 8260B 10/18/17 10/12/17 12:37 10/12/2017 22:30
9801-MW3 CA14379-03 Sampled:10/04/17 11:50 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:40
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 13:50
EPA 8260B 10/18/17 10/12/17 12:37 10/12/2017 23:00
9801-MW3A CA14379-04 Sampled:10/04/17 12:00 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:42
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 13:53
EPA 8260B 10/18/17 10/12/17 12:37 10/12/2017 23:30
9801-MW4 CA14379-05 Sampled:10/04/17 10:30 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:45
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 13:57
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 00:00
9801-MW5 CA14379-06 Sampled:10/04/17 10:10 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:48
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:01
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 00:30
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9801-MW6 CA14379-07 Sampled:10/04/17 12:15 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:50
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:04
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 01:00
9801-MW6 CA14379-07RE1 Sampled:10/04/17 12:15 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:49
9801-MW7 CA14379-08 Sampled:10/04/17 11:30 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:53
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:12
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 01:30
9801-MW8 CA14379-09 Sampled:10/04/17 09:20 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:55
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:16
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 02:00
9801-SW1 CA14379-10 Sampled:10/04/17 11:00 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 14:58
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:19
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 02:30
9801-SW2 CA14379-11 Sampled:10/04/17 10:50 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 15:00
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:23
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 03:00
9801-SW3 CA14379-12 Sampled:10/04/17 12:25 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 15:03
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:27
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 03:31
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9801-SW4 CA14379-13 Sampled:10/04/17 10:40 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 04/02/18 10/11/17 10:43 10/13/2017 15:13
EPA 6020B 04/02/18 10/09/17 10:49 10/11/2017 14:53
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 04:01
9801-Tripblank CA14379-14 Sampled:10/04/17 09:15 Received:10/05/17 09:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 10/18/17 10/12/17 12:37 10/13/2017 04:31
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW1A CA14379-01
Flag NotesMDLNC SWSLMRLDF
87.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.65 ug/L EPA 6010D 11.000.1301Beryllium - Total
23.2 ug/L EPA 6010D 1010.01.101Cobalt - Total
32.2 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.787 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
67.7 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW2 CA14379-02
Flag NotesMDLNC SWSLMRLDF
68.6 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.558 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
6.59 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW3 CA14379-03
Flag NotesMDLNC SWSLMRLDF
99.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.85 ug/L EPA 6010D 11.000.1301Beryllium - Total
2.46 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
5.71 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.336 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
19.0 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW3A CA14379-04
Flag NotesMDLNC SWSLMRLDF
272 ug/L EPA 6010D 10010.01.001Barium - Total
0.362 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW4 CA14379-05
Flag NotesMDLNC SWSLMRLDF
561 ug/L EPA 6010D 10010.01.001Barium - Total
0.527 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW5 CA14379-06
Flag NotesMDLNC SWSLMRLDF
620 ug/L EPA 6010D 10010.01.001Barium - Total
1.87 ug/L EPA 6010DJ 1010.01.401Chromium - Total
2.66 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.09 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.574 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
2.21 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW6 CA14379-07
Flag NotesMDLNC SWSLMRLDF
39.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.07 ug/L EPA 6010D 11.000.1301Beryllium - Total
0.814 ug/L EPA 6010DJ 11.000.3601Cadmium - Total
19.9 ug/L EPA 6010D 1010.01.101Cobalt - Total
34.6 ug/L EPA 6010DJ 5010.02.201Nickel - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW6 CA14379-07
Flag NotesMDLNC SWSLMRLDF
2.31 ug/L EPA 6020BJ 103.000.9101Selenium - Total
7.09 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
50.8 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW6 CA14379-07RE1
Flag NotesMDLNC SWSLMRLDF
0.596 ug/L EPA 6020BJD QI-035.55.000.5505Thallium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW7 CA14379-08
Flag NotesMDLNC SWSLMRLDF
3.5 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
0.80 ug/L EPA 8260BJ 11.00.1011,2-Dichloropropane
0.84 ug/L EPA 8260BJ 11.00.1911,4-Dichlorobenzene
113 ug/L EPA 6010D 10010.01.001Barium - Total
47 ug/L EPA 8260B 51.00.151cis-1,2-Dichloroethene
1.5 ug/L EPA 8260B 11.00.171Tetrachloroethene
0.816 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
1.7 ug/L EPA 8260B 11.00.151Trichloroethene
1.7 ug/L EPA 8260B 11.00.321Vinyl chloride
9.18 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW8 CA14379-09
Flag NotesMDLNC SWSLMRLDF
79.3 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.289 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
3.84 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
4.42 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.758 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
10.6 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW1 CA14379-10
Flag NotesMDLNC SWSLMRLDF
160 ug/L EPA 6010D 10010.01.001Barium - Total
1.53 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
0.600 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW2 CA14379-11
Flag NotesMDLNC SWSLMRLDF
86.7 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.72 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
2.49 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
0.652 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
6.62 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW3 CA14379-12
Flag NotesMDLNC SWSLMRLDF
20.1 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.60 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.62 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.636 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
7.82 ug/L EPA 6010DJ 1010.04.401Zinc - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW4 CA14379-13
Flag NotesMDLNC SWSLMRLDF
90.3 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.2 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
2.85 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
0.713 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
4.60 ug/L EPA 6010DJ 1010.04.401Zinc - Total
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ANALYTICAL RESULTS
9801-MW1ADescription:Lab Sample ID:CA14379-01 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/12/17 22:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/12/17 22:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/12/17 22:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/12/17 22:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 22:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/12/17 22:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 22:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 22:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/12/17 22:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/12/17 22:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/12/17 22:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/12/17 22:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/12/17 22:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/12/17 22:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/12/17 22:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/12/17 22:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/12/17 22:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/12/17 22:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/12/17 22:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 22:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/12/17 22:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 22:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/12/17 22:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/12/17 22:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/12/17 22:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 22:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 22:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/12/17 22:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/12/17 22:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 22:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/12/17 22:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/12/17 22:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 22:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/12/17 22:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 22:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/12/17 22:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/12/17 22:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 22:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/12/17 22:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/12/17 22:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 22:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 22:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 22:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 22:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/12/17 22:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 22:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/12/17 22:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/12/17 22:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
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9801-MW1ADescription:Lab Sample ID:CA14379-01 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/12/17 22:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136110 %MRKEPA 8260B 10/12/17 22:007J120315550.0 1
Dibromofluoromethane 67-129120 %MRKEPA 8260B 10/12/17 22:007J120316050.0 1
Toluene-d8 59-134126 %MRKEPA 8260B 10/12/17 22:007J120316350.0 1
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9801-MW1ADescription:Lab Sample ID:CA14379-01 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 13:27Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:27Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:27Barium [7440-39-3] ^1.00 JMV10.087.4 J 1001
ug/L EPA 6010D 10/13/17 14:27Beryllium [7440-41-7] ^0.130 JMV1.001.65 11
ug/L EPA 6010D 10/13/17 14:27Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:27Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:27Cobalt [7440-48-4] ^1.10 JMV10.023.2 101
ug/L EPA 6010D 10/13/17 14:27Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:27Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:27Nickel [7440-02-0] ^2.20 JMV10.032.2 J 501
ug/L EPA 6020B 10/11/17 13:27Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:27Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 13:27Thallium [7440-28-0] ^0.110 JDH1.000.787 J 5.51
ug/L EPA 6010D 10/13/17 14:27Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:27Zinc [7440-66-6] ^4.40 JMV10.067.7 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW2Description:Lab Sample ID:CA14379-02 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:40 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/12/17 22:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/12/17 22:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/12/17 22:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/12/17 22:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 22:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/12/17 22:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 22:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 22:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/12/17 22:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/12/17 22:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/12/17 22:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/12/17 22:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/12/17 22:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/12/17 22:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/12/17 22:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/12/17 22:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/12/17 22:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/12/17 22:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/12/17 22:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 22:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/12/17 22:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 22:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/12/17 22:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/12/17 22:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/12/17 22:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 22:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 22:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/12/17 22:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/12/17 22:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 22:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/12/17 22:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/12/17 22:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 22:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/12/17 22:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 22:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/12/17 22:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/12/17 22:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 22:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/12/17 22:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/12/17 22:30Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 22:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 22:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 22:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 22:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/12/17 22:30Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 22:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/12/17 22:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/12/17 22:30Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/12/17 22:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW2Description:Lab Sample ID:CA14379-02 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:40 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136108 %MRKEPA 8260B 10/12/17 22:307J120315450.0 1
Dibromofluoromethane 67-129122 %MRKEPA 8260B 10/12/17 22:307J120316150.0 1
Toluene-d8 59-134125 %MRKEPA 8260B 10/12/17 22:307J120316350.0 1
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9801-MW2Description:Lab Sample ID:CA14379-02 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:40 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 13:30Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:29Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:29Barium [7440-39-3] ^1.00 JMV10.068.6 J 1001
ug/L EPA 6010D 10/13/17 14:29Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 14:29Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:29Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:29Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 10/13/17 14:29Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:29Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:29Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 13:30Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:29Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 13:30Thallium [7440-28-0] ^0.110 JDH1.000.558 J 5.51
ug/L EPA 6010D 10/13/17 14:29Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:29Zinc [7440-66-6] ^4.40 JMV10.06.59 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW3Description:Lab Sample ID:CA14379-03 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:50 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/12/17 23:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/12/17 23:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/12/17 23:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/12/17 23:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 23:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/12/17 23:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 23:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 23:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/12/17 23:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/12/17 23:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/12/17 23:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/12/17 23:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/12/17 23:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/12/17 23:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/12/17 23:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/12/17 23:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/12/17 23:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/12/17 23:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/12/17 23:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 23:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/12/17 23:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 23:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/12/17 23:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/12/17 23:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/12/17 23:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 23:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 23:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/12/17 23:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/12/17 23:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 23:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/12/17 23:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/12/17 23:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 23:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/12/17 23:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 23:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/12/17 23:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/12/17 23:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 23:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/12/17 23:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/12/17 23:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 23:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 23:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 23:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 23:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/12/17 23:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 23:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/12/17 23:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/12/17 23:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/12/17 23:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW3Description:Lab Sample ID:CA14379-03 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:50 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136106 %MRKEPA 8260B 10/12/17 23:007J120315350.0 1
Dibromofluoromethane 67-129119 %MRKEPA 8260B 10/12/17 23:007J120316050.0 1
Toluene-d8 59-134126 %MRKEPA 8260B 10/12/17 23:007J120316350.0 1
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9801-MW3Description:Lab Sample ID:CA14379-03 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:50 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 13:50Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:40Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:40Barium [7440-39-3] ^1.00 JMV10.099.4 J 1001
ug/L EPA 6010D 10/13/17 14:40Beryllium [7440-41-7] ^0.130 JMV1.001.85 11
ug/L EPA 6010D 10/13/17 14:40Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:40Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:40Cobalt [7440-48-4] ^1.10 JMV10.02.46 J 101
ug/L EPA 6010D 10/13/17 14:40Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:40Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:40Nickel [7440-02-0] ^2.20 JMV10.05.71 J 501
ug/L EPA 6020B 10/11/17 13:50Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:40Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 13:50Thallium [7440-28-0] ^0.110 JDH1.000.336 J 5.51
ug/L EPA 6010D 10/13/17 14:40Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:40Zinc [7440-66-6] ^4.40 JMV10.019.0 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW3ADescription:Lab Sample ID:CA14379-04 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:00 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/12/17 23:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/12/17 23:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/12/17 23:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/12/17 23:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 23:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/12/17 23:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 23:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 23:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/12/17 23:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/12/17 23:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/12/17 23:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/12/17 23:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/12/17 23:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/12/17 23:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/12/17 23:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/12/17 23:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/12/17 23:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/12/17 23:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/12/17 23:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 23:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/12/17 23:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 23:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/12/17 23:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/12/17 23:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/12/17 23:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 23:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 23:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/12/17 23:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/12/17 23:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 23:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/12/17 23:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/12/17 23:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/12/17 23:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/12/17 23:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/12/17 23:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/12/17 23:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/12/17 23:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/12/17 23:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/12/17 23:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/12/17 23:30Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/12/17 23:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/12/17 23:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/12/17 23:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 23:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/12/17 23:30Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/12/17 23:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/12/17 23:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/12/17 23:30Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/12/17 23:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW3ADescription:Lab Sample ID:CA14379-04 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:00 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136120 %MRKEPA 8260B 10/12/17 23:307J120316050.0 1
Dibromofluoromethane 67-129134 %MRKEPA 8260B 10/12/17 23:307J120316750.0 QS-031
Toluene-d8 59-134135 %MRKEPA 8260B 10/12/17 23:307J120316850.0 QS-031
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9801-MW3ADescription:Lab Sample ID:CA14379-04 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:00 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 13:53Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:42Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:42Barium [7440-39-3] ^1.00 JMV10.0272 1001
ug/L EPA 6010D 10/13/17 14:42Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 14:42Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:42Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:42Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 10/13/17 14:42Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:42Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:42Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 13:53Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:42Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 13:53Thallium [7440-28-0] ^0.110 JDH1.000.362 J 5.51
ug/L EPA 6010D 10/13/17 14:42Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:42Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW4Description:Lab Sample ID:CA14379-05 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:30 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 00:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 00:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 00:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 00:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 00:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 00:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 00:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 00:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 00:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 00:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 00:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 00:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 00:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 00:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 00:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 00:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 00:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 00:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 00:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 00:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 00:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 00:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 00:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 00:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 00:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 00:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 00:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 00:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 00:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 00:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 00:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 00:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 00:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 00:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 00:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 00:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 00:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 00:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 00:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 00:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 00:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 00:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 00:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 00:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 00:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 00:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 00:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 00:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 00:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW4Description:Lab Sample ID:CA14379-05 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:30 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136105 %MRKEPA 8260B 10/13/17 00:007J120315250.0 1
Dibromofluoromethane 67-129122 %MRKEPA 8260B 10/13/17 00:007J120316150.0 1
Toluene-d8 59-134126 %MRKEPA 8260B 10/13/17 00:007J120316350.0 1
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9801-MW4Description:Lab Sample ID:CA14379-05 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:30 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 13:57Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:45Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:45Barium [7440-39-3] ^1.00 JMV10.0561 1001
ug/L EPA 6010D 10/13/17 14:45Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 14:45Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:45Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:45Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 10/13/17 14:45Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:45Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:45Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 13:57Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:45Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 13:57Thallium [7440-28-0] ^0.110 JDH1.000.527 J 5.51
ug/L EPA 6010D 10/13/17 14:45Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:45Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW5Description:Lab Sample ID:CA14379-06 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:10 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 00:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 00:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 00:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 00:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 00:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 00:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 00:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 00:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 00:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 00:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 00:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 00:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 00:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 00:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 00:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 00:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 00:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 00:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 00:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 00:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 00:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 00:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 00:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 00:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 00:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 00:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 00:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 00:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 00:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 00:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 00:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 00:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 00:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 00:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 00:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 00:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 00:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 00:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 00:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 00:30Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 00:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 00:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 00:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 00:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 00:30Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 00:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 00:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 00:30Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 00:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW5Description:Lab Sample ID:CA14379-06 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:10 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136114 %MRKEPA 8260B 10/13/17 00:307J120315750.0 1
Dibromofluoromethane 67-129123 %MRKEPA 8260B 10/13/17 00:307J120316150.0 1
Toluene-d8 59-134125 %MRKEPA 8260B 10/13/17 00:307J120316350.0 1
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9801-MW5Description:Lab Sample ID:CA14379-06 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:10 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:01Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:48Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:48Barium [7440-39-3] ^1.00 JMV10.0620 1001
ug/L EPA 6010D 10/13/17 14:48Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 14:48Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:48Chromium [7440-47-3] ^1.40 JMV10.01.87 J 101
ug/L EPA 6010D 10/13/17 14:48Cobalt [7440-48-4] ^1.10 JMV10.02.66 J 101
ug/L EPA 6010D 10/13/17 14:48Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:48Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:48Nickel [7440-02-0] ^2.20 JMV10.03.09 J 501
ug/L EPA 6020B 10/11/17 14:01Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:48Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:01Thallium [7440-28-0] ^0.110 JDH1.000.574 J 5.51
ug/L EPA 6010D 10/13/17 14:48Vanadium [7440-62-2] ^1.40 JMV10.02.21 J 251
ug/L EPA 6010D 10/13/17 14:48Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW6Description:Lab Sample ID:CA14379-07 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 01:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 01:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 01:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 01:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 01:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 01:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 01:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 01:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 01:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 01:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 01:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 01:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 01:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 01:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 01:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 01:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 01:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 01:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 01:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 01:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 01:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 01:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 01:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 01:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 01:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 01:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 01:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 01:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 01:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 01:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 01:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 01:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 01:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 01:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 01:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 01:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 01:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 01:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 01:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 01:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 01:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 01:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 01:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 01:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 01:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 01:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 01:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 01:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 01:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW6Description:Lab Sample ID:CA14379-07 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136108 %MRKEPA 8260B 10/13/17 01:007J120315450.0 1
Dibromofluoromethane 67-129123 %MRKEPA 8260B 10/13/17 01:007J120316250.0 1
Toluene-d8 59-134127 %MRKEPA 8260B 10/13/17 01:007J120316350.0 1
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9801-MW6Description:Lab Sample ID:CA14379-07 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:04Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:50Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:50Barium [7440-39-3] ^1.00 JMV10.039.4 J 1001
ug/L EPA 6010D 10/13/17 14:50Beryllium [7440-41-7] ^0.130 JMV1.002.07 11
ug/L EPA 6010D 10/13/17 14:50Cadmium [7440-43-9] ^0.360 JMV1.000.814 J 11
ug/L EPA 6010D 10/13/17 14:50Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:50Cobalt [7440-48-4] ^1.10 JMV10.019.9 101
ug/L EPA 6010D 10/13/17 14:50Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:50Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:50Nickel [7440-02-0] ^2.20 JMV10.034.6 J 501
ug/L EPA 6020B 10/11/17 14:04Selenium [7782-49-2] ^0.910 JDH3.002.31 J 101
ug/L EPA 6010D 10/13/17 14:50Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:49Thallium [7440-28-0] ^0.550 JDH5.000.596 JD QI-035.55
ug/L EPA 6010D 10/13/17 14:50Vanadium [7440-62-2] ^1.40 JMV10.07.09 J 251
ug/L EPA 6010D 10/13/17 14:50Zinc [7440-66-6] ^4.40 JMV10.050.8 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW7Description:Lab Sample ID:CA14379-08 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:30 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 01:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 01:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 01:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 01:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 01:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.03.5 J 51
ug/L EPA 8260B 10/13/17 01:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 01:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 01:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 01:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 01:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 01:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 01:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.80 J 11
ug/L EPA 8260B 10/13/17 01:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.84 J 11
ug/L EPA 8260B 10/13/17 01:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 01:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 01:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 01:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 01:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 01:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 01:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 01:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 01:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 01:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 01:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 01:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 01:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 01:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 01:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 01:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 01:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.047 51
ug/L EPA 8260B 10/13/17 01:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 01:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 01:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 01:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 01:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 01:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 01:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 01:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 01:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 01:30Tetrachloroethene [127-18-4] ^0.17 MRK1.01.5 11
ug/L EPA 8260B 10/13/17 01:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 01:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 01:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 01:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 01:30Trichloroethene [79-01-6] ^0.15 MRK1.01.7 11
ug/L EPA 8260B 10/13/17 01:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 01:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 01:30Vinyl chloride [75-01-4] ^0.32 MRK1.01.7 11
ug/L EPA 8260B 10/13/17 01:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW7Description:Lab Sample ID:CA14379-08 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:30 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136108 %MRKEPA 8260B 10/13/17 01:307J120315450.0 1
Dibromofluoromethane 67-129120 %MRKEPA 8260B 10/13/17 01:307J120316050.0 1
Toluene-d8 59-134127 %MRKEPA 8260B 10/13/17 01:307J120316350.0 1
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9801-MW7Description:Lab Sample ID:CA14379-08 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:30 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:12Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:53Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:53Barium [7440-39-3] ^1.00 JMV10.0113 1001
ug/L EPA 6010D 10/13/17 14:53Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 14:53Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:53Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:53Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 10/13/17 14:53Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:53Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:53Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 14:12Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:53Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:12Thallium [7440-28-0] ^0.110 JDH1.000.816 J 5.51
ug/L EPA 6010D 10/13/17 14:53Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:53Zinc [7440-66-6] ^4.40 JMV10.09.18 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW8Description:Lab Sample ID:CA14379-09 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:20 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 02:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 02:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 02:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 02:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 02:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 02:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 02:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 02:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 02:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 02:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 02:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 02:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 02:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 02:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 02:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 02:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 02:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 02:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 02:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 02:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 02:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 02:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 02:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 02:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 02:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 02:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 02:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 02:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 02:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 02:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 02:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 02:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 02:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 02:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 02:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 02:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 02:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 02:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 02:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 02:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 02:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 02:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 02:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 02:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 02:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 02:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 02:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 02:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 02:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW8Description:Lab Sample ID:CA14379-09 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:20 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136110 %MRKEPA 8260B 10/13/17 02:007J120315550.0 1
Dibromofluoromethane 67-129128 %MRKEPA 8260B 10/13/17 02:007J120316450.0 1
Toluene-d8 59-134128 %MRKEPA 8260B 10/13/17 02:007J120316450.0 1
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9801-MW8Description:Lab Sample ID:CA14379-09 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:20 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:16Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:55Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:55Barium [7440-39-3] ^1.00 JMV10.079.3 J 1001
ug/L EPA 6010D 10/13/17 14:55Beryllium [7440-41-7] ^0.130 JMV1.000.289 J 11
ug/L EPA 6010D 10/13/17 14:55Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:55Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:55Cobalt [7440-48-4] ^1.10 JMV10.03.84 J 101
ug/L EPA 6010D 10/13/17 14:55Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:55Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:55Nickel [7440-02-0] ^2.20 JMV10.04.42 J 501
ug/L EPA 6020B 10/11/17 14:16Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:55Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:16Thallium [7440-28-0] ^0.110 JDH1.000.758 J 5.51
ug/L EPA 6010D 10/13/17 14:55Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:55Zinc [7440-66-6] ^4.40 JMV10.010.6 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW1Description:Lab Sample ID:CA14379-10 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:00 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 02:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 02:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 02:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 02:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 02:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 02:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 02:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 02:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 02:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 02:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 02:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 02:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 02:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 02:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 02:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 02:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 02:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 02:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 02:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 02:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 02:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 02:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 02:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 02:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 02:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 02:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 02:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 02:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 02:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 02:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 02:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 02:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 02:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 02:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 02:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 02:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 02:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 02:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 02:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 02:30Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 02:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 02:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 02:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 02:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 02:30Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 02:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 02:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 02:30Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 02:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW1Description:Lab Sample ID:CA14379-10 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:00 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136107 %MRKEPA 8260B 10/13/17 02:307J120315350.0 1
Dibromofluoromethane 67-129122 %MRKEPA 8260B 10/13/17 02:307J120316150.0 1
Toluene-d8 59-134127 %MRKEPA 8260B 10/13/17 02:307J120316350.0 1
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9801-SW1Description:Lab Sample ID:CA14379-10 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 11:00 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:19Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 14:58Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 14:58Barium [7440-39-3] ^1.00 JMV10.0160 1001
ug/L EPA 6010D 10/13/17 14:58Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 14:58Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 14:58Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 14:58Cobalt [7440-48-4] ^1.10 JMV10.01.53 J 101
ug/L EPA 6010D 10/13/17 14:58Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 14:58Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 14:58Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 14:19Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 14:58Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:19Thallium [7440-28-0] ^0.110 JDH1.000.600 J 5.51
ug/L EPA 6010D 10/13/17 14:58Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 14:58Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW2Description:Lab Sample ID:CA14379-11 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:50 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 03:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 03:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 03:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 03:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 03:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 03:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 03:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 03:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 03:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 03:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 03:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 03:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 03:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 03:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 03:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 03:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 03:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 03:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 03:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 03:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 03:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 03:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 03:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 03:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 03:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 03:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 03:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 03:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 03:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 03:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.72 J 51
ug/L EPA 8260B 10/13/17 03:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 03:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 03:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 03:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 03:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 03:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 03:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 03:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 03:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 03:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 03:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 03:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 03:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 03:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 03:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 03:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 03:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 03:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 03:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW2Description:Lab Sample ID:CA14379-11 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:50 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136109 %MRKEPA 8260B 10/13/17 03:007J120315450.0 1
Dibromofluoromethane 67-129125 %MRKEPA 8260B 10/13/17 03:007J120316250.0 1
Toluene-d8 59-134126 %MRKEPA 8260B 10/13/17 03:007J120316350.0 1
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9801-SW2Description:Lab Sample ID:CA14379-11 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:50 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:23Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 15:00Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 15:00Barium [7440-39-3] ^1.00 JMV10.086.7 J 1001
ug/L EPA 6010D 10/13/17 15:00Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 15:00Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 15:00Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 15:00Cobalt [7440-48-4] ^1.10 JMV10.02.49 J 101
ug/L EPA 6010D 10/13/17 15:00Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 15:00Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 15:00Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 14:23Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 15:00Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:23Thallium [7440-28-0] ^0.110 JDH1.000.652 J 5.51
ug/L EPA 6010D 10/13/17 15:00Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 15:00Zinc [7440-66-6] ^4.40 JMV10.06.62 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW3Description:Lab Sample ID:CA14379-12 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:25 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 03:311,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 03:311,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 03:311,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 03:311,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 03:311,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 03:311,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 03:311,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 03:311,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 03:311,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 03:311,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 03:311,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 03:311,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 03:311,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 03:312-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 03:312-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 03:314-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 03:31Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 03:31Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 03:31Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 03:31Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 03:31Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 03:31Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 03:31Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 03:31Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 03:31Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 03:31Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 03:31Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 03:31Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 03:31Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 03:31cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 03:31cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 03:31Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 03:31Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 03:31Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 03:31Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 03:31m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 03:31Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 03:31o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 03:31Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 03:31Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 03:31Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 03:31trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 03:31trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 03:31trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 03:31Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 03:31Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 03:31Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 03:31Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 03:31Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW3Description:Lab Sample ID:CA14379-12 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:25 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136115 %MRKEPA 8260B 10/13/17 03:317J120315750.0 1
Dibromofluoromethane 67-129127 %MRKEPA 8260B 10/13/17 03:317J120316450.0 1
Toluene-d8 59-134133 %MRKEPA 8260B 10/13/17 03:317J120316650.0 1
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9801-SW3Description:Lab Sample ID:CA14379-12 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 12:25 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:27Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 15:03Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 15:03Barium [7440-39-3] ^1.00 JMV10.020.1 J 1001
ug/L EPA 6010D 10/13/17 15:03Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 15:03Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 15:03Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 15:03Cobalt [7440-48-4] ^1.10 JMV10.01.60 J 101
ug/L EPA 6010D 10/13/17 15:03Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 15:03Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 15:03Nickel [7440-02-0] ^2.20 JMV10.03.62 J 501
ug/L EPA 6020B 10/11/17 14:27Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 15:03Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:27Thallium [7440-28-0] ^0.110 JDH1.000.636 J 5.51
ug/L EPA 6010D 10/13/17 15:03Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 15:03Zinc [7440-66-6] ^4.40 JMV10.07.82 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW4Description:Lab Sample ID:CA14379-13 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:40 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 04:011,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 04:011,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 04:011,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 04:011,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 04:011,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 04:011,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 04:011,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 04:011,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 04:011,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 04:011,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 04:011,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 04:011,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 04:011,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 04:012-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 04:012-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 04:014-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 04:01Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 04:01Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 04:01Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 04:01Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 04:01Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 04:01Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 04:01Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 04:01Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 04:01Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 04:01Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 04:01Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 04:01Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 04:01Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 04:01cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.01.2 J 51
ug/L EPA 8260B 10/13/17 04:01cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 04:01Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 04:01Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 04:01Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 04:01Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 04:01m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 04:01Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 04:01o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 04:01Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 04:01Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 04:01Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 04:01trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 04:01trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 04:01trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 04:01Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 04:01Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 04:01Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 04:01Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 04:01Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW4Description:Lab Sample ID:CA14379-13 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:40 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136107 %MRKEPA 8260B 10/13/17 04:017J120315350.0 1
Dibromofluoromethane 67-129124 %MRKEPA 8260B 10/13/17 04:017J120316250.0 1
Toluene-d8 59-134126 %MRKEPA 8260B 10/13/17 04:017J120316350.0 1
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9801-SW4Description:Lab Sample ID:CA14379-13 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 10:40 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 10/11/17 14:53Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 10/13/17 15:13Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 10/13/17 15:13Barium [7440-39-3] ^1.00 JMV10.090.3 J 1001
ug/L EPA 6010D 10/13/17 15:13Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 10/13/17 15:13Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 10/13/17 15:13Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 10/13/17 15:13Cobalt [7440-48-4] ^1.10 JMV10.02.85 J 101
ug/L EPA 6010D 10/13/17 15:13Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 10/13/17 15:13Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 10/13/17 15:13Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 10/11/17 14:53Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 10/13/17 15:13Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 10/11/17 14:53Thallium [7440-28-0] ^0.110 JDH1.000.713 J 5.51
ug/L EPA 6010D 10/13/17 15:13Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 10/13/17 15:13Zinc [7440-66-6] ^4.40 JMV10.04.60 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-TripblankDescription:Lab Sample ID:CA14379-14 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 10/13/17 04:311,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 10/13/17 04:311,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 10/13/17 04:311,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 10/13/17 04:311,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 04:311,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 10/13/17 04:311,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 04:311,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 04:311,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 10/13/17 04:311,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 10/13/17 04:311,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 10/13/17 04:311,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 10/13/17 04:311,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 10/13/17 04:311,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 10/13/17 04:312-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 10/13/17 04:312-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 10/13/17 04:314-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 10/13/17 04:31Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 10/13/17 04:31Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 10/13/17 04:31Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 04:31Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 10/13/17 04:31Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 04:31Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 10/13/17 04:31Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 10/13/17 04:31Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 10/13/17 04:31Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 04:31Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 04:31Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 10/13/17 04:31Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 10/13/17 04:31Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 04:31cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 10/13/17 04:31cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 10/13/17 04:31Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 10/13/17 04:31Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 10/13/17 04:31Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 10/13/17 04:31Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 10/13/17 04:31m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 10/13/17 04:31Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 10/13/17 04:31o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 10/13/17 04:31Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 10/13/17 04:31Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 10/13/17 04:31Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 10/13/17 04:31trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 10/13/17 04:31trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 04:31trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 10/13/17 04:31Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 10/13/17 04:31Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 10/13/17 04:31Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 10/13/17 04:31Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 10/13/17 04:31Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-TripblankDescription:Lab Sample ID:CA14379-14 10/05/17 09:45Received:
Matrix:Water Sampled:10/04/17 09:15 Work Order:CA14379
Wilson County MSWLFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136113 %MRKEPA 8260B 10/13/17 04:317J120315750.0 1
Dibromofluoromethane 67-129126 %MRKEPA 8260B 10/13/17 04:317J120316350.0 1
Toluene-d8 59-134131 %MRKEPA 8260B 10/13/17 04:317J120316550.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7J12031 - EPA 5030B_MS
Prepared: 10/12/2017 12:37 Analyzed: 10/12/2017 20:29Blank (7J12031-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7J12031 - EPA 5030B_MS
Prepared: 10/12/2017 12:37 Analyzed: 10/12/2017 20:29Blank (7J12031-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 11156
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11759
ug/L 50.0 59-134Surrogate: Toluene-d8 12764
Prepared: 10/12/2017 12:37 Analyzed: 10/12/2017 18:29LCS (7J12031-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1339118 1,1-Dichloroethene
ug/L1.0 20.0 81-1349218 Benzene
ug/L1.0 20.0 83-1178818 Chlorobenzene
ug/L1.0 20.0 71-1188918 Toluene
ug/L1.0 20.0 74-1199619 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 11558
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11457
ug/L 50.0 59-134Surrogate: Toluene-d8 12964
Prepared: 10/12/2017 12:37 Analyzed: 10/12/2017 18:59Matrix Spike (7J12031-MS1)
Source: CA15731-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331040.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-1341050.15 U21 Benzene
ug/L1.0 20.0 83-1171010.17 U20 Chlorobenzene
ug/L1.0 20.0 71-1181020.14 U20 Toluene
ug/L1.0 20.0 74-1191140.15 U23 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 12060
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11356
ug/L 50.0 59-134Surrogate: Toluene-d8 13065
Prepared: 10/12/2017 12:37 Analyzed: 10/12/2017 19:29Matrix Spike Dup (7J12031-MSD1)
Source: CA15731-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13397 80.21 U19 1,1-Dichloroethene
ug/L1.0 20.0 1781-13499 50.15 U20 Benzene
ug/L1.0 20.0 1683-11797 40.17 U19 Chlorobenzene
ug/L1.0 20.0 1771-11899 30.14 U20 Toluene
ug/L1.0 20.0 2274-119106 70.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 12160
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11256
ug/L 50.0 59-134Surrogate: Toluene-d8 12864
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7J09024 - EPA 3005A
Prepared: 10/09/2017 10:49 Analyzed: 10/11/2017 12:24Blank (7J09024-BLK1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7J09024 - EPA 3005A
Prepared: 10/09/2017 10:49 Analyzed: 10/11/2017 12:24Blank (7J09024-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 10/09/2017 10:49 Analyzed: 10/11/2017 12:32LCS (7J09024-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120107215 Antimony
ug/L3.00 200 80-120113226 Selenium
ug/L1.00 200 80-120100200 Thallium
Prepared: 10/09/2017 10:49 Analyzed: 10/11/2017 12:58Matrix Spike (7J09024-MS1)
Source: CA14378-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251070.370 U213 Antimony
ug/L3.00 200 75-1251180.910 U236 Selenium
ug/L1.00 200 75-1251010.511202 Thallium
Prepared: 10/09/2017 10:49 Analyzed: 10/11/2017 13:01Matrix Spike Dup (7J09024-MSD1)
Source: CA14378-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125109 20.370 U217 Antimony
ug/L3.00 200 2075-125117 10.910 U234 Selenium
ug/L1.00 200 2075-125102 0.80.511204 Thallium
Prepared: 10/09/2017 10:49 Analyzed: 10/11/2017 13:05Post Spike (7J09024-PS1)
Source: CA14378-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201040.00592209 Antimony
ug/L3.00 200 80-1201100.462220 Selenium
ug/L1.00 200 75-125950.511191 Thallium
Batch 7J11012 - EPA 3005A
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 13:51Blank (7J11012-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7J11012 - EPA 3005A
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 13:51Blank (7J11012-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 13:53LCS (7J11012-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12099199 Arsenic
ug/L10.0 200 80-12097193 Barium
ug/L1.00 20.0 80-1209719.5 Beryllium
ug/L1.00 20.0 80-12010019.9 Cadmium
ug/L10.0 200 80-12098196 Chromium
ug/L10.0 200 80-120100199 Cobalt
ug/L10.0 200 80-12097195 Copper
ug/L10.0 200 80-12097194 Lead
ug/L10.0 200 80-12098195 Nickel
ug/L10.0 200 80-120104208 Silver
ug/L10.0 200 80-120100201 Vanadium
ug/L10.0 200 80-12097195 Zinc
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 14:06Matrix Spike (7J11012-MS1)
Source: CA14378-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251026.80 U205 Arsenic
ug/L10.0 200 75-12510074.8275 Barium
ug/L1.00 20.0 75-1251000.35420.3 Beryllium
ug/L1.00 20.0 75-1251001.7921.8 Cadmium
ug/L10.0 200 75-125971.40 U194 Chromium
ug/L10.0 200 75-12510089.5289 Cobalt
ug/L10.0 200 75-125951.60 U191 Copper
ug/L10.0 200 75-125973.10 U195 Lead
ug/L10.0 200 75-1259918.0217 Nickel
ug/L10.0 200 75-125991.90 U199 Silver
ug/L10.0 200 75-1251021.40 U204 Vanadium
ug/L10.0 200 75-12510142.0244 Zinc
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 14:09Matrix Spike Dup (7J11012-MSD1)
Source: CA14378-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125109 66.80 U217 Arsenic
ug/L10.0 200 2075-125103 274.8281 Barium
ug/L1.00 20.0 2075-125103 30.35421.0 Beryllium
ug/L1.00 20.0 2075-125102 21.7922.2 Cadmium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7J11012 - EPA 3005A
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 14:09Matrix Spike Dup (7J11012-MSD1) Continued
Source: CA14378-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125104 71.40 U209 Chromium
ug/L10.0 200 2075-125104 389.5298 Cobalt
ug/L10.0 200 2075-125103 81.60 U206 Copper
ug/L10.0 200 2075-125102 43.10 U204 Lead
ug/L10.0 200 2075-125102 318.0222 Nickel
ug/L10.0 200 2075-125109 91.90 U217 Silver
ug/L10.0 200 2075-125110 71.40 U220 Vanadium
ug/L10.0 200 2075-125105 342.0251 Zinc
Prepared: 10/11/2017 10:43 Analyzed: 10/13/2017 14:11Post Spike (7J11012-PS1)
Source: CA14378-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120107-0.002400.214 Arsenic
mg/L0.0100 0.200 80-1201040.07480.282 Barium
mg/L0.00100 0.0200 80-1201000.0003540.0204 Beryllium
mg/L0.00100 0.0200 80-1201040.001790.0225 Cadmium
mg/L0.0100 0.200 80-120990.0005700.198 Chromium
mg/L0.0100 0.200 80-1201050.08950.299 Cobalt
mg/L0.0100 0.200 80-12097-0.0007660.194 Copper
mg/L0.0100 0.200 80-120990.001360.200 Lead
mg/L0.0100 0.200 80-1201030.01800.223 Nickel
mg/L0.0100 0.200 80-120600.0002000.120 QM-08Silver
mg/L0.0100 0.200 80-1201030.0004460.206 Vanadium
mg/L0.0100 0.200 80-1201060.04200.254 Zinc
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FLAGS/NOTES AND DEFINITIONS
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
PQL: Practical Quantitation Limit.PQL
The internal standard(s) for this sample were outside the acceptance limits due to sample
matrix interference. The sample was reanalyzed at a dilution.
QI-03
Post-digestion spike did not meet method requirements due to confirmed matrix effects
(dilution test).
QM-08
Surrogate recovery outside acceptance limitsQS-03
The associated continuing calibration verification standard exhibited high bias; since the result is
ND, there is no impact.
QV-01
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