IH6692_20170131_Site Emails 1-31-17 to 5-24-17

1
Beverly, Trudy
From:Schroer, Katherine <[e-mail]>
Sent:Wednesday, May 24, 2017 11:05 AM
To:Callihan, Carolyn; Bussey, Donald; Zinn, Harry; Ahsanuzzaman, Noman; Beverly, Trudy
Cc:Powell, Greg; Adams, Glenn
Subject:RE: Table Harwell Road - UPDATE
Attachments:Harwell Road Well Survey.xlsx
Hi all,

Monitoring well logs for the Aquaterra wells MW-1s through MW-7s, and for MW-1i, MW-3i and -4i, and MW-6i are in
the Site Characterization Report (Aquaterra 10-18-1991). We had already found the logs for MW-8s through MW-11s and
MW-7i in the Response Action Report (Aquaterra 10-12-93).

The spreadsheet, attached, is updated.

For some reason, construction logs for MW-2i and MW-5i were not in either report, but I will keep looking.

Unlike the DEM (original MW-1 through MW-5) construction logs, location coordinates for the MW-1s and MW-1i
(Aquaterra) series were not written directly on the logs. However, the 1991 Site Characterization Report describes how
the wells were surveyed in using three permanent bench marks that were installed in the area (1st screenshot, below). The
second screen shot is a map figure from the 1991 Report showing the locations of the benchmarks (sorry for the poor scan
quality – that’s how it shows up in SEMS).

Please let me know if you have questions or need more information. I’ll update the spreadsheet after I find well
construction logs for MW-2i and MW-5i.

Regards,
Kathy

2

3
4

From: Callihan, Carolyn
Sent: Monday, May 22, 2017 1:41 PM
To: Bussey, Donald <[e-mail]>
Cc: Callihan, Carolyn <[e-mail]>; Schroer, Katherine <[e-mail]>
Subject: FW: Table Harwell Road

Sorry we missed including you on the list, Don.

See below and attached. More from Kathy… Harry and Kathy will be contacting each other soon.

Carolyn Callihan
Remedial Project Manager
Superfund Restoration and Site Evaluation Section
EPA Region 4
404-562-8913
[e-mail]

From: Schroer, Katherine
Sent: Monday, May 22, 2017 8:01 AM
To: Callihan, Carolyn <[e-mail]>; Zinn, Harry <[e-mail]>; Ahsanuzzaman, Noman
<[e-mail]>; Trudy Beverly ([e-mail]) <[e-mail]>
Cc: Powell, Greg <[e-mail]>
Subject: RE: Table Harwell Road

Good morning all,

Here are the well location/construction data that I have so far. I added to the excel spreadsheet that Don had already
started.

The lat/long data for the five DEM wells are from the Well Construction Records, which are in the appendix of the 1993
Response Action Report. For some reason, the Report includes Well Construction Records for only 4 (MW-8s through
MW-11s) of the 16 the Aquaterra Wells. Furthermore, the lat/long data are not written on the Well Construction Records
for those four Aquaterra Well records that are in the Report.

Perhaps not all of the appendix pages were scanned when the Response Action Report was being uploaded into SEMS; I
will request the hard copy report from Records. Meanwhile, I’ll look through the list of Harwell Road SEMS documents
again for that time period, to see what I can find.

Thanks,
Kathy

Katherine Schroer, Ph.D.
Hydrogeologist
U.S. EPA Region 4, Superfund Division
[e-mail]
[phone]

From: Callihan, Carolyn
Sent: Thursday, May 18, 2017 1:02 PM
5
To: Zinn, Harry <[e-mail]>; Schroer, Katherine <[e-mail]>; Ahsanuzzaman, Noman
<[e-mail]>; Trudy Beverly ([e-mail]) <[e-mail]>
Cc: Callihan, Carolyn <[e-mail]>; Powell, Greg <[e-mail]>
Subject: FW: Table Harwell Road

Harry,

Here are some notes Don Bussey jotted down during our site recon. He’s interested in the following parameters for the
wells out there.

Let me know when you plan to go back out there to look at the wells. Can you also plan on checking the private wells
that were discovered contaminated in the late 80’s/early 90’s? Don looked at the one on the Poole property (~300 ft deep
or so) near the motorcycle shop and said it was still open (not properly abandoned); it just didn’t have a pump in
it. Would be interested to find out which bedrock wells would be available for logging and packer testing if we decide to
go that route next year.

 Total Depth
 Casing depth
 Diameter of surface casing
 Is there a pump in well or is well open?
 Is there a building around the well, which would limit accessibility for logging/packer testing?
 GPS coordinates of each well

Kathy has been working on a spreadsheet as well and I will be talking to her tomorrow. Perhaps we can get everyone’s
notes together and create one spreadsheet.

Thanks so much!

Carolyn Callihan
Remedial Project Manager
Superfund Restoration and Site Evaluation Section
U.S. EPA, Region 4
[e-mail]
404-562-8913

From: Bussey, Donald
Sent: Thursday, May 18, 2017 12:35 PM
To: Callihan, Carolyn <[e-mail]>
Subject: Table Harwell Road

Don Bussey, CPG
Environmental Scientist
Hydrogeology
Borehole & Surficial Geophysics
Desktop Catchment Water Modeling
USEPA/OLEM/OSRTI/TIFSD/ERT-Las Vegas, Nevada
Office: [phone]
Cell: [phone]

6

Harwell Estates - Residential/Trailer Park Wells
Well #Total Depth Casing Depth Screen Depth Casing Diameter Latitude
Well #1 not known not known 6-inch 35.14035
Well #2 480 feet 34 feet 6-inch 35.19201
Abandoned 180-190 feet not known 4-inch 35.19098
Millsap 150 feet not known 6-inch 35.19163
#143 not known not known 6-inch 35.19067
L. Poole 300 feet not known 6-inch 35.18793
(others)
DEM Wells (5)19-40 feet N/A 2-inch
(constructed 1988)
MW-1 19 feet 9 feet 9 - 19 feet 2-inch 35.18694
MW-2 24 feet 14 feet 14 - 24 feet 2-inch 35.18806
MW-3 24 feet 14 feet 14 - 24 feet 2-inch 35.18750
MW-4 39 feet 29 feet 29 - 39 feet 2-inch 35.19028
MW-5 34 feet 20 feet 20 - 30 feet 2-inch 35.18778
Aquaterra Wells (16)not known N/A Look up
(constructed 1991-1992)
MW-1s 35 feet 24 feet 24 - 34 feet 2-inch
MW-2s 50 feet 40 feet 40 - 50 feet 2-inch
MW-3s 24 feet 14 feet 14 - 24 feet 2-inch
MW-4s 34 feet (misprint?)12 feet 12 - 22 feet 2-inch
MW-5s 24 feet 14 feet 14 - 24 feet 2-inch
MW-6s 25 feet 15 feet 15 - 25 feet 2-inch
MW-7s 23 feet 13 feet 13 to 23 feet 2-inch
MW-8s 35 feet 25 feet 25 - 35 feet 2-inch
MW-9s 35 feet 25 feet 25 - 35 feet 2-inch
MW-10s 35 feet 25 feet 25 - 35 feet 2-inch
MW-11s 35 feet 25 feet 25 - 35 feet 2-inch
MW-1i 60 feet 50 feet 60 - 50 feet 4-inch
MW-2i not yet available
MW-3i 52 feet 52 feet 51 - 41 feet 4-inch
MW-4i 56 feet 56 feet 56 - 46 feet 4-inch
MW-5i not yet available
MW-6i 60 feet 60 feet 60 - 50 feet 4-inch
MW-7i 55 feet 45 feet 45 to 55 feet 4-inch
Water line installed in Sept/Oct 2016
Park Manager: William Lewis [phone]
Longitude Notes
-81.13631 need to pull pump, no plate, solid well house (McCall Bros.), treatment system
-81.13816 shed, no roof, TD and Casing Depth on plate
-81.13692 abandoned well near Well #1, across street from Bowman #143, reported TD
-81.13683 #150 Harwell Road (Linda Millsap) - not contaminated?, reported TD, active (irrigation?)
-81.13702 #143 Harwell Road, active, fairly recent (say 2007)
-81.13723 L. Poole residential well, reported TD, 27 ppb TCE, no pump (open)
Cycle Shop, July 1988, five wells 1-5
-81.13639 reported as 35°11'13", 81°08'11" DEM - Groundwater Section Boring Logs (7-27-1988) SEMS #10001810
-81.13722 reportes as 35°11'17", 81°08'14" " "
-81.13750 reported as 35°11'15", 81°08'15" " "
-81.13833 reported as 35°11'25", 81°08'18" " "
-81.13861 reported as 35°11'16", 81°08'19" Well Construction Record (7-25-1988) SEMS #10001862
Cycle Shop/Pits, 1S-11S (11), with (7) intermediate. Response Action Report (Aquaterra 10/12/93)
Site Characterization Report (Aquaterra 10-18-1991) SEMS # 10001518
" "
" "
" "
" "
" "
" "
Response Action Report (Aquaterra 10-12-1993) SEMS #10445875
" "
" "
" "
Site Characterization Report (Aquaterra 10-18-1991) SEMS # 10001518
Site Characterization Report (Aquaterra 10-18-1991) SEMS # 10001518
" "
Site Characterization Report (Aquaterra 10-18-1991) SEMS # 10001518
Response Action Report (Aquaterra 10-12-1993) SEMS #10445875
1
Beverly, Trudy
From:Schroer, Katherine <[e-mail]>
Sent:Monday, May 22, 2017 8:01 AM
To:Callihan, Carolyn; Zinn, Harry; Ahsanuzzaman, Noman; Beverly, Trudy
Cc:Powell, Greg
Subject:RE: Table Harwell Road
Attachments:Harwell Road Well Survey.xlsx
Good morning all,

Here are the well location/construction data that I have so far. I added to the excel spreadsheet that Don had already
started.

The lat/long data for the five DEM wells are from the Well Construction Records, which are in the appendix of the 1993
Response Action Report. For some reason, the Report includes Well Construction Records for only 4 (MW-8s through
MW-11s) of the 16 the Aquaterra Wells. Furthermore, the lat/long data are not written on the Well Construction Records
for those four Aquaterra Well records that are in the Report.

Perhaps not all of the appendix pages were scanned when the Response Action Report was being uploaded into SEMS; I
will request the hard copy report from Records. Meanwhile, I’ll look through the list of Harwell Road SEMS documents
again for that time period, to see what I can find.

Thanks,
Kathy

Katherine Schroer, Ph.D.
Hydrogeologist
U.S. EPA Region 4, Superfund Division
[e-mail]
[phone]

From: Callihan, Carolyn
Sent: Thursday, May 18, 2017 1:02 PM
To: Zinn, Harry <[e-mail]>; Schroer, Katherine <[e-mail]>; Ahsanuzzaman, Noman
<[e-mail]>; Trudy Beverly ([e-mail]) <[e-mail]>
Cc: Callihan, Carolyn <[e-mail]>; Powell, Greg <[e-mail]>
Subject: FW: Table Harwell Road

Harry,

Here are some notes Don Bussey jotted down during our site recon. He’s interested in the following parameters for the
wells out there.

Let me know when you plan to go back out there to look at the wells. Can you also plan on checking the private wells
that were discovered contaminated in the late 80’s/early 90’s? Don looked at the one on the Poole property (~300 ft deep
or so) near the motorcycle shop and said it was still open (not properly abandoned); it just didn’t have a pump in
it. Would be interested to find out which bedrock wells would be available for logging and packer testing if we decide to
go that route next year.
2

 Total Depth
 Casing depth
 Diameter of surface casing
 Is there a pump in well or is well open?
 Is there a building around the well, which would limit accessibility for logging/packer testing?
 GPS coordinates of each well

Kathy has been working on a spreadsheet as well and I will be talking to her tomorrow. Perhaps we can get everyone’s
notes together and create one spreadsheet.

Thanks so much!

Carolyn Callihan
Remedial Project Manager
Superfund Restoration and Site Evaluation Section
U.S. EPA, Region 4
[e-mail]
404-562-8913

From: Bussey, Donald
Sent: Thursday, May 18, 2017 12:35 PM
To: Callihan, Carolyn <[e-mail]>
Subject: Table Harwell Road

Don Bussey, CPG
Environmental Scientist
Hydrogeology
Borehole & Surficial Geophysics
Desktop Catchment Water Modeling
USEPA/OLEM/OSRTI/TIFSD/ERT-Las Vegas, Nevada
Office: [phone]
Cell: [phone]

Harwell Estates - Residential/Trailer Park Wells
Well #Total Depth Casing Depth Screen Depth Casing Diameter Latitude
Well #1 not known not known 6-inch 35.14035
Well #2 480 feet 34 feet 6-inch 35.19201
Abandoned 180-190 feet not known 4-inch 35.19098
Millsap 150 feet not known 6-inch 35.19163
#143 not known not known 6-inch 35.19067
L. Poole 300 feet not known 6-inch 35.18793
(others)
DEM Wells (5)19-40 feet N/A 2-inch
MW-1 19 feet 9 feet 9 - 19 feet 2-inch 35.18694
MW-2 24 feet 14 feet 14 - 24 feet 2-inch 35.18806
MW-3 24 feet 14 feet 14 - 24 feet 2-inch 35.18750
MW-4 39 feet 29 feet 29 - 39 feet 2-inch 35.19028
MW-5 34 feet 20 feet 20 - 30 feet 2-inch 35.18778
Aquaterra Wells (16)not known N/A Look up
MW-1s
MW-2s
MW-3s
MW-4s
MW-5s
MW-6s
MW-7s
MW-8s 35 feet 25 feet 25 - 35 feet 2-inch
MW-9s 35 feet 25 feet 25 - 35 feet 2-inch
MW-10s 35 feet 25 feet 25 - 35 feet 2-inch
MW-11s 35 feet 25 feet 25 - 35 feet 2-inch
MW-1i
MW-2i
MW-3i
MW-4i
MW-5i
Water line installed in Sept/Oct 2016
Park Manager: William Lewis [phone]
Longitude Notes
-81.13631 need to pull pump, no plate, solid well house (McCall Bros.), treatment system
-81.13816 shed, no roof, TD and Casing Depth on plate
-81.13692 abandoned well near Well #1, across street from Bowman #143, reported TD
-81.13683 #150 Harwell Road (Linda Millsap) - not contaminated?, reported TD, active (irrigation?)
-81.13702 #143 Harwell Road, active, fairly recent (say 2007)
-81.13723 L. Poole residential well, reported TD, 27 ppb TCE, no pump (open)
Cycle Shop, July 1988, five wells 1-5
-81.13639 reported as 35°11'13", 81°08'11"
-81.13722 reportes as 35°11'17", 81°08'14"
-81.13750 reported as 35°11'15", 81°08'15"
-81.13833 reported as 35°11'25", 81°08'18"
-81.13861 reported as 35°11'16", 81°08'19"
Cycle Shop/Pits, 1S-11S (11), with (5) intermediate (Aquaterra report 10/12/93
constructed 1-28-92
constructed 1-28-92
constructed 1-28-92
constructed 1-28-92
1
Beverly, Trudy
From:Callihan, Carolyn <[e-mail]>
Sent:Thursday, May 18, 2017 1:02 PM
To:Zinn, Harry; Schroer, Katherine; Ahsanuzzaman, Noman; Beverly, Trudy
Cc:Callihan, Carolyn; Powell, Greg
Subject:FW: Table Harwell Road
Attachments:Harwell Road Well Survey.xlsx
Harry,

Here are some notes Don Bussey jotted down during our site recon. He’s interested in the following parameters for the
wells out there.

Let me know when you plan to go back out there to look at the wells. Can you also plan on checking the private wells
that were discovered contaminated in the late 80’s/early 90’s? Don looked at the one on the Poole property (~300 ft deep
or so) near the motorcycle shop and said it was still open (not properly abandoned); it just didn’t have a pump in
it. Would be interested to find out which bedrock wells would be available for logging and packer testing if we decide to
go that route next year.

 Total Depth
 Casing depth
 Diameter of surface casing
 Is there a pump in well or is well open?
 Is there a building around the well, which would limit accessibility for logging/packer testing?
 GPS coordinates of each well

Kathy has been working on a spreadsheet as well and I will be talking to her tomorrow. Perhaps we can get everyone’s
notes together and create one spreadsheet.

Thanks so much!

Carolyn Callihan
Remedial Project Manager
Superfund Restoration and Site Evaluation Section
U.S. EPA, Region 4
[e-mail]
404-562-8913

From: Bussey, Donald
Sent: Thursday, May 18, 2017 12:35 PM
To: Callihan, Carolyn <[e-mail]>
Subject: Table Harwell Road

Don Bussey, CPG
Environmental Scientist
Hydrogeology
Borehole & Surficial Geophysics
Desktop Catchment Water Modeling
2
USEPA/OLEM/OSRTI/TIFSD/ERT-Las Vegas, Nevada
Office: [phone]
Cell: [phone]

Harwell Estates - Residential/Trailer Park Wells
Well #Total Depth Casing Depth Casing Diameter Latitude Longitude
Well #1 not known not known 6-inch 35.14035 -81.13631
Well #2 480 feet 34 feet 6-inch 35.19201 -81.13816
Abandoned 180-190 feet not known 4-inch 35.19098 -81.13692
Millsap 150 feet not known 6-inch 35.19163 -81.13683
#143 not known not known 6-inch 35.19067 -81.13702
L. Poole 300 feet not known 6-inch 35.18793 -81.13723
(others)
DEM Wells (5)19-40 feet N/A 2-inch
Aquaterra Wells (16)not known N/A Look up
Water line installed in Sept/Oct 2016
Park Manager: William Lewis [phone]
Notes
need to pull pump, no plate, solid well house (McCall Bros.), treatment system
shed, no roof, TD and Casing Depth on plate
abandoned well near Well #1, across street from Bowman #143, reported TD
#150 Harwell Road (Linda Millsap) - not contaminated?, reported TD, active (irrigation?)
#143 Harwell Road, active, fairly recent (say 2007)
L. Poole residential well, reported TD, 27 ppb TCE, no pump (open)
Cycle Shop, July 1988, five wells 1-5
Cycle Shop/Pits, 1S-11S (11), with (5) intermediate (Aquaterra report 10/12/93
1
Beverly, Trudy
From:Beverly, Trudy
Sent:Friday, May 12, 2017 3:09 PM
To:'Callihan, Carolyn'
Subject:RE: SI approach for Harwell Road
Thanks for the update Carolyn.

From: Callihan, Carolyn [mailto:[e-mail]]
Sent: Friday, May 12, 2017 3:04 PM
To: Beverly, Trudy <[e-mail]>; Zinn, Harry <[e-mail]>
Cc: Callihan, Carolyn <[e-mail]>
Subject: FW: SI approach for Harwell Road

FYI

Carolyn Callihan
Remedial Project Manager
Superfund Restoration and Site Evaluation Section
U.S. EPA, Region 4
[e-mail]
404-562-8913

From: Callihan, Carolyn
Sent: Thursday, May 11, 2017 12:48 PM
To: Schroer, Katherine <[e-mail]>; Ahsanuzzaman, Noman <[e-mail]>;
Powell, Greg <[e-mail]>; Bussey, Donald <[e-mail]>; Zinn, Harry <[e-mail]>
Cc: Callihan, Carolyn <[e-mail]>; Lown, David <[e-mail]>
Subject: SI approach for Harwell Road

I discussed with Harry today about what we could do for the SI this FY. I also discussed it with Kathy Schroer and Greg
Powell today.

1. Surface water/sediment sampling of the creek
2. A full groundwater sampling event including all of the installed monitoring wells, available private wells and
Country Acres Wells 1-3.
3. Passive soil gas sampling in the area around the motorcycle shop, pattern shop and the two homes closest to that.
OH Materials did a soil gas survey here and it would help us to confirm hot spot areas and guide where to
concentrate future subsurface soil sampling. It would also give us some current data to focus a traditional VI
assessment as one of the next steps, perhaps in early FY18.

During a follow-up ESI in FY18, we could have SESD or ERT conduct surficial groundwater sampling and soil gas
sampling (with summas) for the VI assessment at areas outlined by the passive soil gas results. The ESI would also
concentrate on additional source sampling (subsurface soil sampling at the motorcycle shop and pattern shop) in these
areas as well. We are still discussing what to do at the septic pit area to obtain current source data there (or if we even
need to do that).

Thoughts?

Carolyn Callihan
Remedial Project Manager
2
Superfund Restoration and Site Evaluation Section
U.S. EPA, Region 4
[e-mail]
404-562-8913

From: Zinn, Harry [mailto:[e-mail]]
Sent: Thursday, May 11, 2017 11:12 AM
To: Callihan, Carolyn <[e-mail]>; Lown, David <[e-mail]>
Subject: VI concerns at Harwell Road

Attached is a map of the area where VI may be a concern for the Harwell Road TCE site and a list of the addresses for
those residences inside the blue line. Based on the contaminants found in the in the groundwater area of the septic pits
and the contaminants found in Country Acres Well #2 and the Well #4 (or #3) locations and the shallowness of the
groundwater in the entire area, the residences inside the blue line would be the first to investigate for VI issues.

Harry Zinn
Environmental Engineer
Federal Remediation Branch
Superfund Section
Division of Waste Management
North Carolina Department of Environmental Quality

919-707-8374 office
[e-mail] e-mail

Mailing Address 1646 Mail Service Center, Raleigh, NC 27699-1646
Physical Address 217 W. Jones Street, Raleigh, NC 27603

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

1
Beverly, Trudy
From:Beverly, Trudy
Sent:Thursday, May 04, 2017 10:29 AM
To:'Schroer, Katherine'
Subject:RE: Harwell Estates Mobile Home Park
Wonderful! I appreciate you sending the photos!
Trudy
From: Schroer, Katherine [mailto:[e-mail]]
Sent: Thursday, May 04, 2017 10:27 AM
To: Beverly, Trudy <[e-mail]>
Cc: Callihan, Carolyn <[e-mail]>
Subject: RE: Harwell Estates Mobile Home Park

Hi Trudy,

The tag photos are attached.
Well #2_a shows the casing depth (34 feet), depth (480 feet) and diameter (6 inches).
Well #2_b shows the words “casing depth” more clearly.

Let me know if you have any questions.

Regards,
Kathy

From: Beverly, Trudy [mailto:[e-mail]]
Sent: Thursday, May 4, 2017 9:02 AM
To: Schroer, Katherine <[e-mail]>
Subject: Harwell Estates Mobile Home Park

Hi Katherine,
I enjoyed meeting you last Tuesday during the Harwell Road Septic Pit/Harwell Estates Mobile Home Park site visit in
Gastonia, NC. You had taken some pictures of the tag on well #2 at the mobile home park. When you have time, please
email me copies of the photos.
Thanks for your time,
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-section/inactive-hazardous-
sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
2
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
*******************************************************************************

1
Beverly, Trudy
From:Beverly, Trudy
Sent:Tuesday, April 18, 2017 1:26 PM
To:Samantha Dye
Subject:RE: Harwell Estates Mobile Home Park Map
Thanks!

From: Samantha Dye [mailto:[e-mail]]
Sent: Tuesday, April 18, 2017 1:25 PM
To: Beverly, Trudy <[e-mail]>
Subject: RE: Harwell Estates Mobile Home Park Map

Hi Trudy,

I am so sorry that I have let this slip through the cracks. I will find out today what is happening.

Samantha Dye, MSEH, REHS
Assistant Administrator Environmental Health
Gaston County Department of Health & Human Services
991 W. Hudson Blvd., Gastonia, NC 28052
Office 704-853-5230 |Cell 980-522-0340| Fax [phone]

Please tell us how we are doing by taking this very quick survey. We appreciate your comments.
https://www.surveymonkey.com/s/gastonehsfeedback

From: Beverly, Trudy [mailto:[e-mail]]
Sent: Tuesday, April 18, 2017 8:35 AM
To: Samantha Dye
Subject: Harwell Estates Mobile Home Park Map

Hi Sam,
Do you have an update on the map for Harwell Estates Mobile Home Park?
Thanks,
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-section/inactive-hazardous-
sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
2
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
*******************************************************************************

This message may contain confidential information and is intended only for the individual named. If you are not
the named addressee you should not disseminate, distribute or copy this email. Please notify the sender
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1
Beverly, Trudy
From:Tripp, Christopher <[e-mail]>
Sent:Monday, April 17, 2017 3:34 PM
To:Beverly, Trudy
Subject:Harwell well sampling results
Attachments:Harwell Results and MCL_033117.xlsx
Trudy,

Please find attached the table with sampling results from Harwell that we spoke about over the phone today.

Thanks,

Christopher Tripp - On-Scene Coordinator
U.S. Environmental Protection Agency, Region 4 | 61 Forsyth St SW | Atlanta, Georgia | 30303
Emergency Response, Removal and Prevention Branch (ERRPB)
office: 404-562-8745 | cell: 470-426-3336
epaosc.org

TABLE 1
HARWELL ROAD PRIVATE WELL
ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES
TDD No. TT-01-067
Harwell Road Private Well
Volatile Organic Compounds (μg/L)
Acetone NE 250 U 100 U 25 U 25 U 250 U 250 U 25 U 10.8 37.1 18.6
2-Butanone (MEK)NE 50 U 20 U 5.0 U 5.0 U 50 U 35.3 J 5.0 U 4.0 U 5.0 U 4.7
1,1-Dichloroethane NE 10 U 98.3 4.8 1.9 10 U 10 U 1.0 U 0.50 U 1.0 U 0.50
1,1-Dichloroethene 7 22.3 141 7.9 2.6 18.7 21.1 1.0 U 0.50 U 1.0 U 0.50
cis-1,2-Dichloroethene 70 15.5 194 9.1 3.6 12.7 13.5 1.0 U 0.50 U 1.0 U 0.50
trans-1,2-Dichloroethene 100 10 U 2.4 J 1.0 U 1.0 U 10 U 10 U 1.0 U 0.50 U 1.0 U 0.50
Tetrachloroethene 5 29.4 10.9 1.0 U 1.0 U 25.9 27 1.0 U 0.50 U 1.0 U 0.50
1,1,1-Trichloroethane 200 10 U 5.6 1.0 U 1.0 U 10 U 10 U 1.0 U 0.50 U 1.0 U 0.50
Trichloroethene 5 944 409 14.1 3.5 817 872 2.8 5.3 1.0 U 3.0
Semivolatile Organic Compounds (μg/L)ND ND ND ND ND ND ND ND NA NA
Metals (μg/L)
Aluminum NE 100 U 100 U 68.6 J 57.5 J 11.9 181 256 223 14.6 6.6
Antimony 6 5.0 U 5.0 U 5.0 U 5.0 U 0.22 J 0.10 J 0.28 J 1.0 U 0.10 J 1.0
Arsenic 10 10 U 10 U 10 U 10 U 1.1 0.96 1.9 1.4 0.53 1.0
Barium 2,000 13.3 5.0 U 24.7 25.7 17 98.8 176 183 57.2 14.7
Beryllium 4 1.0 U 1.0 U 1.0 U 1.0 U 0.046 J 0.067 J 0.026 J 1.0 U 0.031 J 1.0
Cadmium 5 1.0 U 1.0 U 1.0 U 1.0 U 0.16 0.12 0.080 U 1.0 U 0.080 U 1.0
Calcium NE 16,400 92,200 17,200 16,400 19,000 57,000 33,000 32,300 37,100 7,700
Chromium 100 5.0 U 5.0 U 5.0 U 5.0 U 0.42 J 3.6 0.12 J 1.2 0.50 U 0.79
Cobalt NE 5.0 U 5.0 U 5.0 U 5.0 U 0.20 1.1 0.082 J 1.0 U 0.059 J 1.0
Copper 1,300 2.9 J 5.0 U 5.0 U 5.0 U 37.4 32.6 3.3 7.9 2.7 4.6
Iron NE 368 1,730 302 333 1,370 2,270 224 124 16.3 J 40
Lead 15 5.0 U 5.0 U 5.0 U 5.0 U 172 16.4 4.6 6.0 2.3 0.72
Magnesium NE 3,840 5,200 3,110 3,000 4,390 4,930 4,400 4,250 4,580 2,260
Manganese NE 196 763 18.6 25.2 240 5780 194 119 10.2 2.7
Nickel NE 5.0 U 5.0 U 5.0 U 5.0 U 1.2 3.8 0.50 U 0.83 J 0.58 0.68
Potassium NE 2,770 J 2,940 J 5,000 U 5,000 U 3,210 3,760 6,870 4,740 2,840 1,810
Selenium 50 10 U 10 U 10 U 10 U 0.32 J 0.50 U 0.41 J 1.0 U 0.50 U 0.56
Silver NE 5.0 U 5.0 U 5.0 U 5.0 U 0.50 U 0.50 U 0.50 U 0.10 U 0.10 J 0.10
Sodium NE 12,000 12,900 8,670 8,630 13,100 12,500 12,700 12,300 12,000 9,750
Thallium 2 10 U 10 U 10 U 10 U 0.053 J 0.089 J 0.044 J 1.0 U 0.040 J 1.0
Vanadium NE 5.0 U 5.0 U 5.0 U 5.0 U 0.26 J 1.2 3.1 2.6 1.3 1.2
Zinc NE 8.1 J 25.2 10 U 10 U 101 26.8 4.9 J 7.5 5.2 12.5
Notes:
DS Downstream I Influent NA Not analyzed for W Well
E Effluent INT Intermediate ND Not detected
EPA U.S. Environmental Protection Agency MCL 2012 Maximum Contaminant Level NE Not established
H Harwell Road µg/L Micrograms per liter US Upstream
J The analyte was positively identified; the associated value is the approximate concentration of the analyte in the sample.
U The analyte was analyzed for, but was not detected at or above the associated value (reporting limit).
BOLD Bolded and shaded values exceed the 2012 EPA MCL.
Well 1
Date: 3/9/17
Well 2
Date: 3/9/17 Date: 3/9/17 Date: 3/24/17 Date: 3/24/17
0309171344US
Downstream Upstream
Analyte
0309171049W1 0309171139W2 0309171320DS 0328171430E
Well 1-Effluent
Date: 3/28/17
0324171245E
Well 1- Effluent
Date: 3/24/17
0324171230I 0324171355INT
EPA MCL
Well 1- Influent Well 1-Intermediate
Date: 3/9/17
0328171500-1
143 Harwell
Private We
Date: 3/28/
0324171245E
Well 1- Effluent
Drinking Water
Date: 3/24/17
TABLE 1
HARWELL ROAD PRIVATE WELL
ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES
TDD No. TT-01-067
Harwell Road Private Well
Volatile Organic Compounds (μg/L)
Acetone NE
2-Butanone (MEK)NE
1,1-Dichloroethane NE
1,1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 100
Tetrachloroethene 5
1,1,1-Trichloroethane 200
Trichloroethene 5
Semivolatile Organic Compounds (μg/L)
Metals (μg/L)
Aluminum NE
Antimony 6
Arsenic 10
Barium 2,000
Beryllium 4
Cadmium 5
Calcium NE
Chromium 100
Cobalt NE
Copper 1,300
Iron NE
Lead 15
Magnesium NE
Manganese NE
Nickel NE
Potassium NE
Selenium 50
Silver NE
Sodium NE
Thallium 2
Vanadium NE
Zinc NE
Notes:
DS Downstream
E Effluent
EPA U.S. Environmental Protection Agenc
H Harwell Road
J The analyte was positively identified;
U The analyte was analyzed for, but wa
BOLD Bolded and shaded values exceed
Analyte EPA MCL
U
U
U
U
U
U
J
U
U
U
U
J
U
U
J
J
J
U
U
143H
Rd-
ell
17
1
Beverly, Trudy
From:Callihan, Carolyn <[e-mail]>
Sent:Wednesday, April 12, 2017 2:20 PM
To:Zinn, Harry; Beverly, Trudy; Ahsanuzzaman, Noman; Schroer, Katherine; Bussey, Donald; Tripp,
Christopher; Powell, Greg
Cc:Parker, Stuart; Henderson, Melanie; Callihan, Carolyn
Subject:RE: Harwell Road Site visit
All,

Thanks for your help with scheduling this site visit. I think Tuesday afternoon, April 25, at 1:30 pm will be the best time
to meet. That will give the folks that are traveling in time to get lunch.

Trudy, where would be a convenient place for us to meet?

Thanks!

Carolyn Callihan
Remedial Project Manager
Superfund Restoration and Site Evaluation Section
U.S. EPA, Region 4
[e-mail]
404-562-8913
1
Beverly, Trudy
From:Samantha Dye <[e-mail]>
Sent:Wednesday, March 29, 2017 8:13 AM
To:Beverly, Trudy
Subject:RE: Harwell Estates Mobile Home Park/Harwell Road Septic Pit #NCD986166692
Okay

Samantha Dye, MSEH, REHS
Assistant Administrator Environmental Health
Gaston County Department of Health & Human Services
991 W. Hudson Blvd., Gastonia, NC 28052
Office 704-853-5230 |Cell 980-522-0340| Fax [phone]

Please tell us how we are doing by taking this very quick survey. We appreciate your comments.
https://www.surveymonkey.com/s/gastonehsfeedback

From: Beverly, Trudy [mailto:[e-mail]]
Sent: Wednesday, March 29, 2017 8:13 AM
To: Samantha Dye
Subject: RE: Harwell Estates Mobile Home Park/Harwell Road Septic Pit #NCD986166692

I’ll give you a call.

From: Samantha Dye [mailto:[e-mail]]
Sent: Wednesday, March 29, 2017 8:09 AM
To: Beverly, Trudy <[e-mail]>
Subject: RE: Harwell Estates Mobile Home Park/Harwell Road Septic Pit #NCD986166692

Hi Trudy,

Thank you for keeping me in the loop. I am sorry that I haven’t sent the map. I am going to the administration office today
for training and I will check on the map.

If the Milsaps’ want to connect to the water line, would they be able to do so if they pay for it?

Thanks,
Sam

Samantha Dye, MSEH, REHS
Assistant Administrator Environmental Health
Gaston County Department of Health & Human Services
991 W. Hudson Blvd., Gastonia, NC 28052
Office 704-853-5230 |Cell 980-522-0340| Fax [phone]

Please tell us how we are doing by taking this very quick survey. We appreciate your comments.
https://www.surveymonkey.com/s/gastonehsfeedback

2
From: Beverly, Trudy [mailto:[e-mail]]
Sent: Wednesday, March 29, 2017 7:57 AM
To: Jesneck, Charlotte; Day, Collin; Bateson, James
Cc: Ramey, David E; Samantha Dye
Subject: FW: Harwell Estates Mobile Home Park/Harwell Road Septic Pit #NCD986166692

fyi

From: Beverly, Trudy
Sent: Wednesday, March 29, 2017 7:48 AM
To: 'Eichinger, Kevin' <[e-mail]>
Cc: Tripp, Christopher <[e-mail]>; Zinn, Harry <[e-mail]>
Subject: RE: Harwell Estates Mobile Home Park/Harwell Road Septic Pit #NCD986166692

Kevin, I appreciate all that you have done.

Chris,
Mr. Bowman’s phone number is [phone]. He’s told me in the past that he can be reached between the hours of
6:00am and 8:00pm.
Hope that helps,
Trudy
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Tuesday, March 28, 2017 5:53 PM
To: Beverly, Trudy <[e-mail]>
Cc: Tripp, Christopher <[e-mail]>
Subject: Re: Harwell Estates Mobile Home Park/Harwell Road Septic Pit #NCD986166692

Thanks Trudy for all your help. Good summary of our current plans. Do you have Mr. Bowman's phone number for
Chris? I forgot to get it from him this morning and they were not at home this afternoon.

On Mar 28, 2017, at 17:23, Beverly, Trudy <[e-mail]> wrote:
Hi Chris,

It was nice speaking with you by phone this afternoon about the Harwell Estates Mobile Home
Park/Harwell Road Septic Pit area in Gastonia, NC. I will be copying you on further communications
related to this area since you are taking over as the US EPA site manager from Kevin Eichinger and
coordinating running the waterline to the mobile home park. You stated that you and Kevin met with
Two Rivers Utilities today to discuss plans for running a waterline for Harwell Estates and that you plan
to find a local engineer to draw plans for the project.

Kevin Eichinger relayed by phone this afternoon that US EPA will be sampling well #1 for Harwell
Estates weekly for volatile organic compounds (including 1,4-Dioxane) and metals for the next six
months. After six months, the EPA plans to sample well #1 monthly to ensure that the temporary
treatment system is effectively filtering out contaminants to below standards or until the waterline
connection is completed with Two Rivers Utilities. Kevin also stated that you and he spoke with Jobill
Bowman (143 L L Harwell Road) about options for his water supply source due to TCE detections in his
water supply well. It is my understanding that US EPA plans to sample Mr. Bowman’s water supply well
again in two weeks and then monthly afterward to monitor for contaminant changes. Mr. Eichinger also
said that EPA will be unable to provide Lynda Millsaps’ residence (150 L L Harwell Road) with a
municipal connection since her water supply well has had no volatile organic compound detections. He
relayed that EPA plans to sample Ms. Millsaps’ water supply well after the waterline completion of Two
Rivers Utilities with the mobile home park and plans to continue sampling her well at some frequency
afterward to monitor for possible contaminant changes.

3
You can reach me directly by phone at [phone] or by email at [e-mail]. I look
forward to working with you.

Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-
section/inactive-hazardous-sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-
gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

<image001.png>
North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties unless the content is exempt by statute or other regulation.
*******************************************************************************

This message may contain confidential information and is intended only for the individual named. If you are not
the named addressee you should not disseminate, distribute or copy this email. Please notify the sender
immediately by email if you have received this email by mistake and delete it from your system. Emails that do
not contain confidential medical information are subject to North Carolina General Statute, Chapter 132 and
may be considered a matter of public record.
This message may contain confidential information and is intended only for the individual named. If you are not the
named addressee you should not disseminate, distribute or copy this email. Please notify the sender immediately by email
if you have received this email by mistake and delete it from your system. Emails that do not contain confidential medical
information are subject to North Carolina General Statute, Chapter 132 and may be considered a matter of public record.
1
Beverly, Trudy
From:Adams, George
Sent:Friday, March 24, 2017 11:32 AM
To:Day, Collin; Ramey, David E; Beverly, Trudy
Subject:FW: Harwell Road NCD986166692
Attachments:harwell.pdf
This is septic I think. I think this is all.

From: Zinn, Harry
Sent: Thursday, August 02, 2012 1:09 PM
To: Adams, George <[e-mail]>
Subject: RE: Harwell Road NCD986166692

Here is a file that I just scanned for you. Hope it helps.

Harry Zinn 
Site Evaluation and Removal Branch 
Superfund Section 
Division of Waste Management 
North Carolina Department of Environment and Natural Resources 
phone and fax  919‐707‐8374 
Mailing Address           1646 Mail Service Center 
Raleigh, NC 27699‐1646 

Physical Address         217 W. Jones Street 
Raleigh, NC 27603 

****************************************************** 
E‐mail correspondence to and from this address may be subject to the  
North Carolina Public Records Law and may be disclosed to third parties. 
******************************************************* 

From: Adams, George
Sent: Thursday, August 02, 2012 11:41 AM
To: Zinn, Harry
Subject: Harwell Road NCD986166692

Harry, do you remember approximately where this Site was located? I may have asked you before, but I can’t find my
notes. I believe it was located at the end of Harwell Road in Gastonia, across from an elementary school. I don’t think
our IHSB database info plots it correctly.

George Adams - [e-mail]
North Carolina Department of Environment & Natural Resources
Division of Waste Management - Superfund Section - Inactive Hazardous Sites Branch
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Phone: [phone] Fax: [phone]

2
Email correspondence to and from this address is subject to the North Carolina Public Records Law
and may be disclosed to third parties unless the content is exempt by statute or other
regulation. Please note: my e-mail address has changed to [e-mail]

Submissions of all work plans, reports, and cover letters must now include companion electronic copies on compact
disc. Specific requirements including electronic file formats may be found under "Electronic Document
Submittal" at the Inactive Hazardous Sites Program’s website.

1
Beverly, Trudy
From:Adams, George
Sent:Friday, March 24, 2017 11:28 AM
To:Ramey, David E; Day, Collin; Beverly, Trudy
Subject:FW: Harwell Road NCD986166692
Attachments:Harwell NCD986166692 8-2-12.pdf; Country Acres NCD0136182 8-2-12.pdf
Info that I found for Harwell Road area.

From: Adams, George
Sent: Thursday, August 02, 2012 3:37 PM
To: Parris, Bruce <[e-mail]>
Subject: FW: Harwell Road NCD986166692

The PWS explained that this is not a SDWA violation bc it is not four times > MCL from any grab sample or the average
(yet) is > MCL for four consecutive quarterly samples.

I don’t understand the Harwell Road area very well and I didn’t screen these Sites. Based on what I can tell, it looks
related so I updated the AB spreadsheet to indicate so. I also changed the RP to N. If you choose to assign the Site to
someone, they may disagree with me.

From: Adams, George
Sent: Thursday, August 02, 2012 2:35 PM
To: Zinn, Harry; Bateson, James
Cc: Antrilli, Vincent; Parker, Stuart
Subject: RE: Harwell Road NCD986166692

--Harry, thanks I think this was the piece that I needed.

SERB/BA folks, I know y’all are looking at multiple sites in Gaston County lately, and I would like to apprise you of a
recent development from Public Water. Jeff Westmoreland came by this morning and let me know about some recent
detections of CVOCs in a PWS community well, Country Acres/ Southgate, Water System # NC0136182, Well #2.
2-1-2006 = NDET
2-5-2009 = NDET
2-21-2012 = 10 ppb TCE, 8 ppb cis-1,2-DCE, 7.5 ppb 1,1-DCE
5-29-2012 = 10 ppb TCE, 8.9 ppb cis-1,2-DCE, 7.3 ppb 1,1-DCE

I estimated the well location to be approximately 35.19439 -81.13461, although I don’t have exact coordinates. This well
is one of two wells that provide source water to the PWS noted above. You can actually see the reservoir water tank near
well # 2, if you go to Gaston County GIS and enter PID# 151010. The population served by the system is 668. The water
system that owns this well (Country Acres) has discussed trying to drill a new one to serve the community. Apparently
there is a NPDES permit to discharge back flush (elevated Mn and Fe) from a sand filter to a creek nearby. I couldn’t the
permit, but I can probably track it down.
There is/was a nearby school that had a community well, W A Bess Elementary NC0136715. I believe the EPA
lore is that it was tested in 1995 and was okay. Subsequently, a heating oil release (LUST # 20234) was
discovered. The PWS registration of the well (NTNC) is now inactive. That doesn’t mean that it isn’t used, but
I spoke with PWS, and they believe the school was connected to another community system (they are going to
look into it).
2
Based on my best preliminary guestimation, I believe this is not a new Site, but rather part of the Harwell Road
complex of Sites. I also trying to gather some information from UST state lead for a LUST in the vicinity (the
Country Store # 16547). Could this warrant a second looks by SERB? With the information recently generated
by Vince for Union Road (NONCD0002647) along with this new data, the Site or Sites would hopefully rank
high enough for EPA involvement. Again, we greatly appreciate your efforts. I can tell you folks are busy
with yet another fire – George

From: Zinn, Harry
Sent: Thursday, August 02, 2012 1:09 PM
To: Adams, George
Subject: RE: Harwell Road NCD986166692

Here is a file that I just scanned for you. Hope it helps.

Harry Zinn 
Site Evaluation and Removal Branch 
Superfund Section 
Division of Waste Management 
North Carolina Department of Environment and Natural Resources 
phone and fax  919‐707‐8374 
Mailing Address           1646 Mail Service Center 
Raleigh, NC 27699‐1646 

Physical Address         217 W. Jones Street 
Raleigh, NC 27603 

****************************************************** 
E‐mail correspondence to and from this address may be subject to the  
North Carolina Public Records Law and may be disclosed to third parties. 
******************************************************* 

From: Adams, George
Sent: Thursday, August 02, 2012 11:41 AM
To: Zinn, Harry
Subject: Harwell Road NCD986166692

Harry, do you remember approximately where this Site was located? I may have asked you before, but I can’t find my
notes. I believe it was located at the end of Harwell Road in Gastonia, across from an elementary school. I don’t think
our IHSB database info plots it correctly.

George Adams - [e-mail]
North Carolina Department of Environment & Natural Resources
Division of Waste Management - Superfund Section - Inactive Hazardous Sites Branch
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Phone: [phone] Fax: [phone]

Email correspondence to and from this address is subject to the North Carolina Public Records Law
and may be disclosed to third parties unless the content is exempt by statute or other
regulation. Please note: my e-mail address has changed to [e-mail]

3
Submissions of all work plans, reports, and cover letters must now include companion electronic copies on compact
disc. Specific requirements including electronic file formats may be found under "Electronic Document
Submittal" at the Inactive Hazardous Sites Program’s website.

Gaston County, NC
Office of the Director of Revenue, GIS Division
Disclaimer:The information provided is not to be considered as a Legal
Document or Description. The Map and Parcel Data is believed to be accurate, but Gaston County does not guarantee its accuracy. Values based on last general reappraisal - 2007
Print Date: 8/2/2012
Print Scale 1:2091 or 1" = 174'
PARCEL INFORMATION
PID #: 151010
PIN #: 3563224408
NEIGH.HOOD #: 5B064
NEIGH.HOOD NAME: WOODBRIDGE
OWNER ID #: 1540222
CURRENT OWNER 1: AQUA OF NORTH CAROLINA
INC
CURRENT OWNER 2:
MAILING ADDRESS 1: 762 W LANCASTER AVE
MAILING ADDRESS 2:
CITY: BRYN MAWR
STATE: PA
ZIP CODE: 19010-3489
JAN1 OWNER 1: AQUA OF NORTH CAROLINA INC
JAN1 OWNER 2:
PROPERTY ADDRESS: WOODBRIDGE DR
DEED BOOK: 4465
DEED PAGE: 0582
DEED TYPE: CB
SALES AMOUNT: 0
DEED RECORDING DATE: 05/26/2009
PLAT BOOK:
PLAT PAGE:
LEGAL DESC 1: *
LEGAL DESC 2:
STRUCTURE CODE #:
STRUCTURE TYPE:
YEAR BUILT: 0
SQ FT: 0
BASEMENT: NO
# BEDROOMS: 0
# BATHS: 0
MULTI-STRUCTURES: NO
ACREAGE: 0.53
TAX DISTRICT: UNION ROAD FD
TOWNSHIP CODE: 10
TOWNSHIP DESC: GASTONIA TOWNSHIP
VOLUNTARY AG DIST: No
LAND VALUE: $2,000
IMPV. VALUE: $625
TOTAL VALUE: $2,625
PRESENT USE VALUE ASSESSMENT: NO
Page 1 of 1
8/2/2012http://egov1.co.gaston.nc.us/servlet/com.esri.esrimap.Esrimap?ServiceName=MSOVERVI...
feet
km
3000
1
1
Beverly, Trudy
From:Beverly, Trudy
Sent:Thursday, March 23, 2017 7:48 PM
To:Eichinger, Kevin
Cc:Day, Collin; Jesneck, Charlotte
Subject:RE: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17
Sample Result Letters & HREs
Kevin,
I’ve been working on a site history for this area, but do not have it ready for today.
Trudy
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Thursday, March 23, 2017 10:30 AM
To: Beverly, Trudy <[e-mail]>
Subject: Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17 Sample Result
Letters & HREs

Today if possible.

On Mar 23, 2017, at 07:42, Beverly, Trudy <[e-mail]> wrote:
Kevin,
Do you have a deadline for comments on the draft?
Trudy
From: Zinn, Harry
Sent: Wednesday, March 22, 2017 1:51 PM
To: Eichinger, Kevin <[e-mail]>; Beverly, Trudy <[e-mail]>
Cc: Samantha Dye <[e-mail]>; Earnest, Emily <[e-mail]>;
Day, Collin <[e-mail]>; Jesneck, Charlotte <[e-mail]>; Bateson,
James <[e-mail]>
Subject: RE: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

Kevin,
Wanted to add my two cents worth on the Facts Sheet. Carolyn Callihan is currently filling a FOIA
request for a report from Roy F. Weston , the Technical Assistance Team for EPA. Weston sampled ten
well in the area on July 5, 1989, Five of these wells were impacted, however two wells owned by K.
Harwell and located on LL Harwell as well as J. Harwell, J.D. Harwell, and Jennings Harwell and had no
detections. Weston performed a second visit on July 25, 1989 to document contaminants in the septic pit,
survey the well elevations and establish direction of groundwater flow and extent of contamination. A
third Weston visit in November 1989 to conduct geophysical surveys and create geologic cross sections. I
believe that a report covering these three visits is in the EPA archives.

Harry Zinn
Environmental Engineer
Federal Remediation Branch
Superfund Section
Division of Waste Management
North Carolina Department of Environmental Quality

919-707-8374 office
[e-mail] e-mail
2

Mailing Address 1646 Mail Service Center, Raleigh, NC 27699-1646
Physical Address 217 W. Jones Street, Raleigh, NC 27603

<image001.png>

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Wednesday, March 22, 2017 8:09 AM
To: Beverly, Trudy <[e-mail]>
Cc: Samantha Dye <[e-mail]>; Earnest, Emily <[e-mail]>;
Zinn, Harry <[e-mail]>; Day, Collin <[e-mail]>; Jesneck, Charlotte
<[e-mail]>; Bateson, James <[e-mail]>
Subject: Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

See the attached. It is just draft, so feel free to comment. You all can still comment even if you
do not want your contact info listed. I am not 100% happy with the background, but felt it was
necessary to include something.

Kevin

From: Beverly, Trudy <[e-mail]>
Sent: Wednesday, March 22, 2017 8:04 AM
To: Eichinger, Kevin
Cc: Samantha Dye; Earnest, Emily; Zinn, Harry; Day, Collin; Jesneck, Charlotte;
[e-mail]
Subject: RE: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

Hi Kevin,
What information is going on the fact sheet? Will those listed on the fact sheet have the opportunity to
review it before it is given to residents?
Thanks,
Trudy
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Tuesday, March 21, 2017 5:22 PM
To: Beverly, Trudy <[e-mail]>
Subject: Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

Trudy,

We are creating a short information notice that we will give the residents. Do you want your
contact info listed on the fact sheet? How about Gaston County Public Health?

Thanks,
Kevin

3
From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, March 21, 2017 3:28 PM
To: Eichinger, Kevin; Earnest, Emily; Samantha Dye; Zinn, Harry
Cc: Day, Collin; Ramey, David E; Jesneck, Charlotte; [e-mail]; Antrilli, Vincent
Subject: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17
Sample Result Letters & HREs

Kevin, Emily, Sam, & Harry,
Please see the attached Report of Analysis from my 3/9/17 water supply well sampling trip and the
sample result letters for the area around L L Harwell Road, Gastonia, NC. Sample results from 3/16/17
should be available soon and I will forward them to you when I have received and processed them. I will
be back out at the site area on Thursday, March 23, 2017 for more community outreach, information
gathering, and sampling. Matt Costner from Aqua NC is meeting me at the Country Acres/South Gate
communities to sample well #1 (still in operation in conjunction with a Two Rivers/City of Gastonia
municipal connection) and well #2 (offline since 2013 and soon to be abandoned).
Let me know if you have questions,
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-
section/inactive-hazardous-sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-
gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

<image002.png>
North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties unless the content is exempt by statute or other regulation.
*******************************************************************************

1
Beverly, Trudy
From:Jesneck, Charlotte
Sent:Thursday, March 23, 2017 1:26 PM
To:Beverly, Trudy; Bateson, James; Day, Collin
Subject:Re: HR EPA Fact Sheet
If JIm is ok, I think that would be good.
From: Beverly, Trudy
Sent: Thursday, March 23, 2017 1:20:35 PM
To: Jesneck, Charlotte; Bateson, James; Day, Collin
Subject: RE: HR EPA Fact Sheet

Kevin had asked if I wanted my contact information added on the bottom with his (EPA On-Scene Coordinator) &
Stephanie Brown’s (EPA Community Involvement Coordinator). Do you want it to be included?

From: Jesneck, Charlotte
Sent: Thursday, March 23, 2017 1:12 PM
To: Bateson, James <[e-mail]>; Beverly, Trudy <[e-mail]>; Day, Collin
<[e-mail]>
Subject: HR EPA Fact Sheet

I don't have any comments on the fact sheet.
1
Beverly, Trudy
From:Eichinger, Kevin <[e-mail]>
Sent:Thursday, March 23, 2017 10:30 AM
To:Beverly, Trudy
Subject:Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17
Sample Result Letters & HREs
Today if possible.

On Mar 23, 2017, at 07:42, Beverly, Trudy <[e-mail]> wrote:
Kevin,
Do you have a deadline for comments on the draft?
Trudy
From: Zinn, Harry
Sent: Wednesday, March 22, 2017 1:51 PM
To: Eichinger, Kevin <[e-mail]>; Beverly, Trudy <[e-mail]>
Cc: Samantha Dye <[e-mail]>; Earnest, Emily <[e-mail]>;
Day, Collin <[e-mail]>; Jesneck, Charlotte <[e-mail]>; Bateson,
James <[e-mail]>
Subject: RE: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

Kevin,
Wanted to add my two cents worth on the Facts Sheet. Carolyn Callihan is currently filling a FOIA
request for a report from Roy F. Weston , the Technical Assistance Team for EPA. Weston sampled ten
well in the area on July 5, 1989, Five of these wells were impacted, however two wells owned by K.
Harwell and located on LL Harwell as well as J. Harwell, J.D. Harwell, and Jennings Harwell and had no
detections. Weston performed a second visit on July 25, 1989 to document contaminants in the septic pit,
survey the well elevations and establish direction of groundwater flow and extent of contamination. A
third Weston visit in November 1989 to conduct geophysical surveys and create geologic cross sections. I
believe that a report covering these three visits is in the EPA archives.

Harry Zinn
Environmental Engineer
Federal Remediation Branch
Superfund Section
Division of Waste Management
North Carolina Department of Environmental Quality

919-707-8374 office
[e-mail] e-mail

Mailing Address 1646 Mail Service Center, Raleigh, NC 27699-1646
Physical Address 217 W. Jones Street, Raleigh, NC 27603

<image001.png>

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

2
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Wednesday, March 22, 2017 8:09 AM
To: Beverly, Trudy <[e-mail]>
Cc: Samantha Dye <[e-mail]>; Earnest, Emily <[e-mail]>;
Zinn, Harry <[e-mail]>; Day, Collin <[e-mail]>; Jesneck, Charlotte
<[e-mail]>; Bateson, James <[e-mail]>
Subject: Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

See the attached. It is just draft, so feel free to comment. You all can still comment even if you
do not want your contact info listed. I am not 100% happy with the background, but felt it was
necessary to include something.

Kevin

From: Beverly, Trudy <[e-mail]>
Sent: Wednesday, March 22, 2017 8:04 AM
To: Eichinger, Kevin
Cc: Samantha Dye; Earnest, Emily; Zinn, Harry; Day, Collin; Jesneck, Charlotte;
[e-mail]
Subject: RE: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

Hi Kevin,
What information is going on the fact sheet? Will those listed on the fact sheet have the opportunity to
review it before it is given to residents?
Thanks,
Trudy
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Tuesday, March 21, 2017 5:22 PM
To: Beverly, Trudy <[e-mail]>
Subject: Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip &
3/21/17 Sample Result Letters & HREs

Trudy,

We are creating a short information notice that we will give the residents. Do you want your
contact info listed on the fact sheet? How about Gaston County Public Health?

Thanks,
Kevin

From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, March 21, 2017 3:28 PM
To: Eichinger, Kevin; Earnest, Emily; Samantha Dye; Zinn, Harry
Cc: Day, Collin; Ramey, David E; Jesneck, Charlotte; [e-mail]; Antrilli, Vincent
Subject: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17
Sample Result Letters & HREs

Kevin, Emily, Sam, & Harry,
3
Please see the attached Report of Analysis from my 3/9/17 water supply well sampling trip and the
sample result letters for the area around L L Harwell Road, Gastonia, NC. Sample results from 3/16/17
should be available soon and I will forward them to you when I have received and processed them. I will
be back out at the site area on Thursday, March 23, 2017 for more community outreach, information
gathering, and sampling. Matt Costner from Aqua NC is meeting me at the Country Acres/South Gate
communities to sample well #1 (still in operation in conjunction with a Two Rivers/City of Gastonia
municipal connection) and well #2 (offline since 2013 and soon to be abandoned).
Let me know if you have questions,
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-
section/inactive-hazardous-sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-
gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

<image002.png>
North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties unless the content is exempt by statute or other regulation.
*******************************************************************************

1
Beverly, Trudy
From:Eichinger, Kevin <[e-mail]>
Sent:Wednesday, March 22, 2017 8:09 AM
To:Beverly, Trudy
Cc:Samantha Dye; Earnest, Emily; Zinn, Harry; Day, Collin; Jesneck, Charlotte; Bateson, James
Subject:Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17
Sample Result Letters & HREs
Attachments:Harwell_Factsheet__1_3.21.17_KME.docx
See the attached. It is just draft, so feel free to comment. You all can still comment even if you do not want your
contact info listed. I am not 100% happy with the background, but felt it was necessary to include something.

Kevin

From: Beverly, Trudy <[e-mail]>
Sent: Wednesday, March 22, 2017 8:04 AM
To: Eichinger, Kevin
Cc: Samantha Dye; Earnest, Emily; Zinn, Harry; Day, Collin; Jesneck, Charlotte; [e-mail]
Subject: RE: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17 Sample Result
Letters & HREs

Hi Kevin,
What information is going on the fact sheet? Will those listed on the fact sheet have the opportunity to review it before it
is given to residents?
Thanks,
Trudy
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Tuesday, March 21, 2017 5:22 PM
To: Beverly, Trudy <[e-mail]>
Subject: Re: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17 Sample Result
Letters & HREs

Trudy,

We are creating a short information notice that we will give the residents. Do you want your contact info listed
on the fact sheet? How about Gaston County Public Health?

Thanks,
Kevin

From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, March 21, 2017 3:28 PM
To: Eichinger, Kevin; Earnest, Emily; Samantha Dye; Zinn, Harry
Cc: Day, Collin; Ramey, David E; Jesneck, Charlotte; [e-mail]; Antrilli, Vincent
Subject: L L Harwell Road Area, Gastonia - Report of Analysis from 3/9/17 Sampling Trip & 3/21/17 Sample Result
Letters & HREs

2
Kevin, Emily, Sam, & Harry,
Please see the attached Report of Analysis from my 3/9/17 water supply well sampling trip and the sample result letters
for the area around L L Harwell Road, Gastonia, NC. Sample results from 3/16/17 should be available soon and I will
forward them to you when I have received and processed them. I will be back out at the site area on Thursday, March 23,
2017 for more community outreach, information gathering, and sampling. Matt Costner from Aqua NC is meeting me at
the Country Acres/South Gate communities to sample well #1 (still in operation in conjunction with a Two Rivers/City of
Gastonia municipal connection) and well #2 (offline since 2013 and soon to be abandoned).
Let me know if you have questions,
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-section/inactive-hazardous-
sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
*******************************************************************************

U.S. Environmental Protection Agency
LL Harwell Road
Private Well Contamination
Gastonia, Gaston County, North Carolina

Introduction
This information sheet summarizes the history of the Site, present Site status, and future activities planned
for the Site.

Background
Between 1950 and 1978, chlorinated solvents were believed to be dumped on the property located on Harwell Road
at Beaty Road. The owner of property hauled septic tank sludge from local industries. Previous owners also
conducted septic sludge dumping activities and drum burial on the property. North Carolina Department of
Environmental Quality (NCDEQ), then called North Carolina Department of Environmental Management, became
aware of the site in May of 1987 and began site assessment activities. The United States Environmental Protection
Agency (the EPA) began supplying bottled water to impacted residents in July of 1989.
On December 26, 1989, the EPA issued a Unilateral Administrative Order (UAO) to Homelite Textron and R.A.
McKee to conduct removal activities at the Harwell Road Septic Pits Site and to provide permanent alternate water
supply to affected residents. On May 14, 1990, the EPA issued a revised UAO to Homelite Textron and R.A. McKee
to include additional removal activities at the Harwell Road Septic Pits Site. Scope of this work included the removal
and disposal of contaminated media. Multiple buried drums and contaminated soil was removed from the property.
On November 2, 1990, an additional action was taken by the EPA due to TCE contamination in the groundwater.
EPA connected residents of the Southgate Subdivision to a community water supply system.
NCDEQ, as part of a focused private well sampling project in the area, discovered contamination of the
groundwater at the Harwell Estates Community and advised impacted residents to not use their well-water for
cooking, drinking or bathing. Contaminants found in the well-water include 1,1 Dicloroethene (1,1-DCE), Cis-
1,2-Dichloroethene (cis-1,2-DCE), Tetrachloroethene (PCE), and Trichloroethene (TCE). NCDEQ began
supplying bottle water to impacted residents. NCDEQ also requested EPA assistance on March 8, 2017.

EPA arrived on March 9, 2017 and perform confirmatory sampling at the two private wells that service the
Harwell Estates Mobile Home Community. Sample results were received on March 10, 2017 and multiple
contaminants exceeded EPA’s safe drinking water criteria. EPA’s mobilized additional contractors on March 9th
to install a temporary, drinking water certified, filtration system and connect impacted residences public water.

EPA Planned Activities
Number 1 March 2017
Installation of a multi-stage temporary charcoal drinking water filtration system began on March 22, 2017, and is
anticipated to be completed by March 24, 2017. Once the installation is complete, the EPA will sample the water
to ensure it meets drinking water safety standards. Upon receipt of the sampling results, the EPA will notify the
community whether it is safe to resume using the water again; presumably by Friday, March 24, 2017. The EPA
will then test the water weekly to assure that the filtration system is removing the contaminants. The charcoal
filter media will be replaced if or when there is any indication contamination. The final plan is to connect the
mobile home park to the municipal water system (Two Rivers Utilities). This process can take several months. We
will maintain the filtration system until the water line is installed.
The EPA and NCDEQ are currently investigating the source and extent of the ground water contamination.
NCDEQ is testing private wells throughout the area. Additional residences will be address by the EPA if issues
are found with their well-water.

FOR MORE
INFORMATION
EPA On-Scene Coordinator
Kevin Eichinger [phone]
[e-mail]

EPA Community Involvement Coordinator
Stephanie Y. Brown [phone]
[e-mail]31T

1
Beverly, Trudy
From:Beverly, Trudy
Sent:Monday, March 13, 2017 8:31 AM
To:Zinn, Harry
Subject:FW: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results - Harwell Estates Mobile
Home Park
Attachments:92332882_fr_draft.pdf; ATT00001.htm
Sorry about that. I forgot to add you on to this email.

From: Beverly, Trudy
Sent: Monday, March 13, 2017 7:36 AM
To: Jesneck, Charlotte <[e-mail]>; Day, Collin <[e-mail]>; Ramey, David E
<[e-mail]>; 'Samantha Dye' <[e-mail]>; Earnest, Emily
<[e-mail]>; Assefa, Hanna <[e-mail]>
Subject: RE: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results - Harwell Estates Mobile Home
Park

fyi

From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Friday, March 10, 2017 9:22 PM
To: Beverly, Trudy <[e-mail]>
Cc: Bateson, James <[e-mail]>
Subject: Fwd: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results

Results of out sampling. Sending the summary table next.

Begin forwarded message:
From: "Taylor, Todd" <[e-mail]>
Date: March 10, 2017 at 17:21:05 EST
To: Kevin Eichinger <[e-mail]>
Cc: "Vasser, Bryan" <[e-mail]>
Subject: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results
Hello,

Attached are the preliminary results for VOC, SVOC the metals will follow when complete. When the
samples are QC’d I will forward as well.

Regards,
Todd

Todd Taylor|ENV.SCI.V
Direct: 615.992-5556 |
[e-mail]
Tetra Tech Inc. |
712 Melrose Avenue | Nashville, TN 37211 | www.tetratech.com
2
PLEASE NOTE: This message, including any attachments, may include privileged, confidential and/or
inside information. Any distribution or use of this communication by anyone other than the intended
recipient is strictly prohibited and may be unlawful. If you are not the intended recipient, please notify the
sender by replying to this message and then delete it from your system.

#=CL#
March 10, 2017
LIMS USE: FR Prelim - JESSICA
LIMS OBJECT ID: 92332882
92332882
Project:
Pace Project No.:
RE:
Jessica Vickers
Tetra Tech
950 South 4th Street
Baldwyn, MS 38824
HARWELL RD PRIVA 103X902701067
Dear Jessica Vickers:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 1 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 2 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID Matrix Date Collected Date Received
92332882001 0309171049W1 Water 03/09/17 10:49 03/09/17 15:07
92332882002 0309171139W2 Water 03/09/17 11:39 03/09/17 15:07
92332882003 0309171320DS Water 03/09/17 13:20 03/09/17 15:07
92332882004 0309171344US Water 03/09/17 13:44 03/09/17 15:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 3 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92332882001 0309171049W1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882002 0309171139W2 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882003 0309171320DS EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882004 0309171344US EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 4 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92332882001 0309171049W1
1,1-Dichloroethene 22.3 ug/L 03/10/17 11:2710.0EPA 8260
cis-1,2-Dichloroethene 15.5 ug/L 03/10/17 11:2710.0EPA 8260
Tetrachloroethene 29.4 ug/L 03/10/17 11:2710.0EPA 8260
Trichloroethene 944 ug/L 03/10/17 11:2710.0EPA 8260
92332882002 0309171139W2
1,1-Dichloroethane 98.3 ug/L 03/10/17 11:444.0EPA 8260
1,1-Dichloroethene 141 ug/L 03/10/17 11:444.0EPA 8260
cis-1,2-Dichloroethene 194 ug/L 03/10/17 11:444.0EPA 8260
trans-1,2-Dichloroethene 2.4J ug/L 03/10/17 11:444.0EPA 8260
Tetrachloroethene 10.9 ug/L 03/10/17 11:444.0EPA 8260
1,1,1-Trichloroethane 5.6 ug/L 03/10/17 11:444.0EPA 8260
Trichloroethene 409 ug/L 03/10/17 11:444.0EPA 8260
92332882003 0309171320DS
1,1-Dichloroethane 4.8 ug/L 03/10/17 10:531.0EPA 8260
1,1-Dichloroethene 7.9 ug/L 03/10/17 10:531.0EPA 8260
cis-1,2-Dichloroethene 9.1 ug/L 03/10/17 10:531.0EPA 8260
Trichloroethene 14.1 ug/L 03/10/17 10:531.0EPA 8260
92332882004 0309171344US
1,1-Dichloroethane 1.9 ug/L 03/10/17 11:101.0EPA 8260
1,1-Dichloroethene 2.6 ug/L 03/10/17 11:101.0EPA 8260
cis-1,2-Dichloroethene 3.6 ug/L 03/10/17 11:101.0EPA 8260
Trichloroethene 3.5 ug/L 03/10/17 11:101.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 5 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Method:
Client:Tetra Tech EMI
EPA 8270
Date:March 10, 2017
Description:8270 MSSV Semivolatile Organic
General Information:
4 samples were analyzed for EPA 8270. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 6 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Method:
Client:Tetra Tech EMI
EPA 8260
Date:March 10, 2017
Description:8260 MSV Low Level
General Information:
4 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 7 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:03 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:03 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:03 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:03 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:03 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:03 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:03 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:03 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:03 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:03 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:03 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:03 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:03 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:03 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:03 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:03 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:03 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:03 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:03 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:03 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:03 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:03 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:03 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:03 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:03 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:03 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:03 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:03 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:03 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:03 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:03 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:03 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:03 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:03 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:03 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:03 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:03 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:03 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:03 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:03 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:03 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:03 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:03 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:03 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:03 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:03 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 8 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:03 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:03 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:03 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:0303/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:03 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:03 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:03 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:03 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:03 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:03 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:03 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:03 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:03 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:03 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:03 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:03 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:03 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:0303/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:03 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:03 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:03 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:03 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)69 %03/10/17 12:03 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)69 %03/10/17 12:03 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)82 %03/10/17 12:03 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)23 %03/10/17 12:03 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)33 %03/10/17 12:03 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)77 %03/10/17 12:03 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:27 67-64-125010010
Benzene ND ug/L 03/10/17 11:27 71-43-210.0 2.5 10
Bromobenzene ND ug/L 03/10/17 11:27 108-86-110.0 3.0 10
Bromochloromethane ND ug/L 03/10/17 11:27 74-97-510.0 1.7 10
Bromodichloromethane ND ug/L 03/10/17 11:27 75-27-410.0 1.8 10
Bromoform ND ug/L 03/10/17 11:27 75-25-210.0 2.6 10
Bromomethane ND ug/L 03/10/17 11:27 74-83-920.0 2.9 10
2-Butanone (MEK)ND ug/L 03/10/17 11:27 78-93-350.0 9.6 10
Carbon tetrachloride ND ug/L 03/10/17 11:27 56-23-510.0 2.5 10
Chlorobenzene ND ug/L 03/10/17 11:27 108-90-710.0 2.3 10
Chloroethane ND ug/L 03/10/17 11:27 75-00-310.0 5.4 10
Chloroform ND ug/L 03/10/17 11:27 67-66-310.0 1.4 10
Chloromethane ND ug/L 03/10/17 11:27 74-87-310.0 1.1 10
2-Chlorotoluene ND ug/L 03/10/17 11:27 95-49-810.0 3.5 10
4-Chlorotoluene ND ug/L 03/10/17 11:27 106-43-410.0 3.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 9 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:27 96-12-820.0 20.0 10
Dibromochloromethane ND ug/L 03/10/17 11:27 124-48-110.0 2.1 10
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:27 106-93-410.0 2.7 10
Dibromomethane ND ug/L 03/10/17 11:27 74-95-310.0 2.1 10
1,2-Dichlorobenzene ND ug/L 03/10/17 11:27 95-50-110.0 3.0 10
1,3-Dichlorobenzene ND ug/L 03/10/17 11:27 541-73-110.0 2.4 10
1,4-Dichlorobenzene ND ug/L 03/10/17 11:27 106-46-710.0 3.3 10
Dichlorodifluoromethane ND ug/L 03/10/17 11:27 75-71-810.0 2.1 10
1,1-Dichloroethane ND ug/L 03/10/17 11:27 75-34-310.0 3.2 10
1,2-Dichloroethane ND ug/L 03/10/17 11:27 107-06-210.0 2.4 10
1,1-Dichloroethene 22.3 ug/L 03/10/17 11:27 75-35-410.0 5.6 10
cis-1,2-Dichloroethene 15.5 ug/L 03/10/17 11:27 156-59-210.0 1.9 10
trans-1,2-Dichloroethene ND ug/L 03/10/17 11:27 156-60-510.0 4.9 10
1,2-Dichloropropane ND ug/L 03/10/17 11:27 78-87-510.0 2.7 10
1,3-Dichloropropane ND ug/L 03/10/17 11:27 142-28-910.0 2.8 10
2,2-Dichloropropane ND ug/L 03/10/17 11:27 594-20-710.0 1.3 10
1,1-Dichloropropene ND ug/L 03/10/17 11:27 563-58-610.0 4.9 10
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:27 10061-01-510.0 1.3 10
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:27 10061-02-610.0 2.6 10
Diisopropyl ether ND ug/L 03/10/17 11:27 108-20-310.0 1.2 10
Ethylbenzene ND ug/L 03/10/17 11:27 100-41-410.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:27 87-68-310.0 7.1 10
2-Hexanone ND ug/L 03/10/17 11:27 591-78-650.0 4.6 10
p-Isopropyltoluene ND ug/L 03/10/17 11:27 99-87-610.0 3.1 10
Methylene Chloride ND ug/L 03/10/17 11:27 75-09-220.0 9.7 10
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:27 108-10-150.0 3.3 10
Methyl-tert-butyl ether ND ug/L 03/10/17 11:27 1634-04-410.0 2.1 10
Naphthalene ND ug/L 03/10/17 11:27 91-20-310.0 2.4 10
Styrene ND ug/L 03/10/17 11:27 100-42-510.0 2.6 10
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:27 630-20-610.0 3.3 10
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:27 79-34-510.0 4.0 10
Tetrachloroethene 29.4 ug/L 03/10/17 11:27 127-18-410.0 4.6 10
Toluene ND ug/L 03/10/17 11:27 108-88-310.0 2.6 10
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:27 87-61-610.0 3.3 10
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:27 120-82-110.0 3.5 10
1,1,1-Trichloroethane ND ug/L 03/10/17 11:27 71-55-610.0 4.8 10
1,1,2-Trichloroethane ND ug/L 03/10/17 11:27 79-00-510.0 2.9 10
Trichloroethene 944 ug/L 03/10/17 11:27 79-01-610.0 4.7 10
Trichlorofluoromethane ND ug/L 03/10/17 11:27 75-69-410.0 2.0 10
1,2,3-Trichloropropane ND ug/L 03/10/17 11:27 96-18-410.0 4.1 10
Vinyl acetate ND ug/L 03/10/17 11:27 108-05-420.0 3.5 10
Vinyl chloride ND ug/L 03/10/17 11:27 75-01-410.0 6.2 10
Xylene (Total)ND ug/L 03/10/17 11:27 1330-20-710.0 6.6 10
m&p-Xylene ND ug/L 03/10/17 11:27 179601-23-120.0 6.6 10
o-Xylene ND ug/L 03/10/17 11:27 95-47-610.0 2.3 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 10 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)97 %03/10/17 11:27 460-00-470-130 10
1,2-Dichloroethane-d4 (S)99 %03/10/17 11:27 17060-07-070-130 10
Toluene-d8 (S)100 %03/10/17 11:27 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 11 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:31 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:31 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:31 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:31 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:31 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:31 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:31 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:31 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:31 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:31 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:31 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:31 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:31 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:31 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:31 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:31 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:31 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:31 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:31 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:31 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:31 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:31 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:31 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:31 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:31 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:31 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:31 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:31 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:31 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:31 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:31 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:31 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:31 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:31 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:31 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:31 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:31 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:31 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:31 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:31 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:31 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:31 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:31 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:31 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:31 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:31 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 12 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:31 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:31 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:31 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:3103/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:31 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:31 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:31 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:31 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:31 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:31 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:31 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:31 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:31 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:31 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:31 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:31 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:31 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:3103/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:31 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:31 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:31 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:31 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)67 %03/10/17 12:31 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)66 %03/10/17 12:31 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)79 %03/10/17 12:31 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)20 %03/10/17 12:31 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)31 %03/10/17 12:31 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)73 %03/10/17 12:31 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:44 67-64-110040.0 4
Benzene ND ug/L 03/10/17 11:44 71-43-24.0 1.0 4
Bromobenzene ND ug/L 03/10/17 11:44 108-86-14.0 1.2 4
Bromochloromethane ND ug/L 03/10/17 11:44 74-97-54.0 0.68 4
Bromodichloromethane ND ug/L 03/10/17 11:44 75-27-44.0 0.72 4
Bromoform ND ug/L 03/10/17 11:44 75-25-24.0 1.0 4
Bromomethane ND ug/L 03/10/17 11:44 74-83-98.0 1.2 4
2-Butanone (MEK)ND ug/L 03/10/17 11:44 78-93-320.0 3.8 4
Carbon tetrachloride ND ug/L 03/10/17 11:44 56-23-54.0 1.0 4
Chlorobenzene ND ug/L 03/10/17 11:44 108-90-74.0 0.92 4
Chloroethane ND ug/L 03/10/17 11:44 75-00-34.0 2.2 4
Chloroform ND ug/L 03/10/17 11:44 67-66-34.0 0.56 4
Chloromethane ND ug/L 03/10/17 11:44 74-87-34.0 0.44 4
2-Chlorotoluene ND ug/L 03/10/17 11:44 95-49-84.0 1.4 4
4-Chlorotoluene ND ug/L 03/10/17 11:44 106-43-44.0 1.2 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 13 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:44 96-12-88.0 8.0 4
Dibromochloromethane ND ug/L 03/10/17 11:44 124-48-14.0 0.84 4
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:44 106-93-44.0 1.1 4
Dibromomethane ND ug/L 03/10/17 11:44 74-95-34.0 0.84 4
1,2-Dichlorobenzene ND ug/L 03/10/17 11:44 95-50-14.0 1.2 4
1,3-Dichlorobenzene ND ug/L 03/10/17 11:44 541-73-14.0 0.96 4
1,4-Dichlorobenzene ND ug/L 03/10/17 11:44 106-46-74.0 1.3 4
Dichlorodifluoromethane ND ug/L 03/10/17 11:44 75-71-84.0 0.84 4
1,1-Dichloroethane 98.3 ug/L 03/10/17 11:44 75-34-34.0 1.3 4
1,2-Dichloroethane ND ug/L 03/10/17 11:44 107-06-24.0 0.96 4
1,1-Dichloroethene 141 ug/L 03/10/17 11:44 75-35-44.0 2.2 4
cis-1,2-Dichloroethene 194 ug/L 03/10/17 11:44 156-59-24.0 0.76 4
trans-1,2-Dichloroethene 2.4J ug/L 03/10/17 11:44 156-60-54.0 2.0 4
1,2-Dichloropropane ND ug/L 03/10/17 11:44 78-87-54.0 1.1 4
1,3-Dichloropropane ND ug/L 03/10/17 11:44 142-28-94.0 1.1 4
2,2-Dichloropropane ND ug/L 03/10/17 11:44 594-20-74.0 0.52 4
1,1-Dichloropropene ND ug/L 03/10/17 11:44 563-58-64.0 2.0 4
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:44 10061-01-54.0 0.52 4
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:44 10061-02-64.0 1.0 4
Diisopropyl ether ND ug/L 03/10/17 11:44 108-20-34.0 0.48 4
Ethylbenzene ND ug/L 03/10/17 11:44 100-41-44.0 1.2 4
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:44 87-68-34.0 2.8 4
2-Hexanone ND ug/L 03/10/17 11:44 591-78-620.0 1.8 4
p-Isopropyltoluene ND ug/L 03/10/17 11:44 99-87-64.0 1.2 4
Methylene Chloride ND ug/L 03/10/17 11:44 75-09-28.0 3.9 4
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:44 108-10-120.0 1.3 4
Methyl-tert-butyl ether ND ug/L 03/10/17 11:44 1634-04-44.0 0.84 4
Naphthalene ND ug/L 03/10/17 11:44 91-20-34.0 0.96 4
Styrene ND ug/L 03/10/17 11:44 100-42-54.0 1.0 4
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:44 630-20-64.0 1.3 4
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:44 79-34-54.0 1.6 4
Tetrachloroethene 10.9 ug/L 03/10/17 11:44 127-18-44.0 1.8 4
Toluene ND ug/L 03/10/17 11:44 108-88-34.0 1.0 4
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:44 87-61-64.0 1.3 4
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:44 120-82-14.0 1.4 4
1,1,1-Trichloroethane 5.6 ug/L 03/10/17 11:44 71-55-64.0 1.9 4
1,1,2-Trichloroethane ND ug/L 03/10/17 11:44 79-00-54.0 1.2 4
Trichloroethene 409 ug/L 03/10/17 11:44 79-01-64.0 1.9 4
Trichlorofluoromethane ND ug/L 03/10/17 11:44 75-69-44.0 0.80 4
1,2,3-Trichloropropane ND ug/L 03/10/17 11:44 96-18-44.0 1.6 4
Vinyl acetate ND ug/L 03/10/17 11:44 108-05-48.0 1.4 4
Vinyl chloride ND ug/L 03/10/17 11:44 75-01-44.0 2.5 4
Xylene (Total)ND ug/L 03/10/17 11:44 1330-20-74.0 2.6 4
m&p-Xylene ND ug/L 03/10/17 11:44 179601-23-18.0 2.6 4
o-Xylene ND ug/L 03/10/17 11:44 95-47-64.0 0.92 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 14 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)97 %03/10/17 11:44 460-00-470-130 4
1,2-Dichloroethane-d4 (S)102 %03/10/17 11:44 17060-07-070-130 4
Toluene-d8 (S)100 %03/10/17 11:44 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 15 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:59 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:59 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:59 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:59 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:59 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:59 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:59 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:59 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:59 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:59 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:59 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:59 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:59 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:59 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:59 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:59 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:59 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:59 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:59 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:59 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:59 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:59 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:59 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:59 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:59 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:59 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:59 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:59 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:59 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:59 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:59 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:59 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:59 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:59 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:59 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:59 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:59 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:59 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:59 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:59 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:59 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:59 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:59 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:59 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:59 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:59 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 16 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:59 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:59 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:59 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:5903/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:59 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:59 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:59 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:59 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:59 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:59 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:59 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:59 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:59 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:59 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:59 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:59 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:59 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:5903/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:59 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:59 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:59 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:59 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)69 %03/10/17 12:59 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)70 %03/10/17 12:59 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)78 %03/10/17 12:59 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)22 %03/10/17 12:59 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)34 %03/10/17 12:59 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)74 %03/10/17 12:59 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 10:53 67-64-125.0 10.0 1
Benzene ND ug/L 03/10/17 10:53 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/10/17 10:53 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/10/17 10:53 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/10/17 10:53 75-27-41.0 0.18 1
Bromoform ND ug/L 03/10/17 10:53 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/10/17 10:53 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/10/17 10:53 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/10/17 10:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/10/17 10:53 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/10/17 10:53 75-00-31.0 0.54 1
Chloroform ND ug/L 03/10/17 10:53 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/10/17 10:53 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/10/17 10:53 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/10/17 10:53 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 17 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 10:53 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/10/17 10:53 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 10:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/10/17 10:53 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/10/17 10:53 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/10/17 10:53 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/10/17 10:53 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/10/17 10:53 75-71-81.0 0.21 1
1,1-Dichloroethane 4.8 ug/L 03/10/17 10:53 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/10/17 10:53 107-06-21.0 0.24 1
1,1-Dichloroethene 7.9 ug/L 03/10/17 10:53 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 9.1 ug/L 03/10/17 10:53 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/10/17 10:53 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/10/17 10:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/10/17 10:53 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/10/17 10:53 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/10/17 10:53 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/10/17 10:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/10/17 10:53 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/10/17 10:53 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/10/17 10:53 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 10:53 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/10/17 10:53 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/10/17 10:53 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/10/17 10:53 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 10:53 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/10/17 10:53 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/10/17 10:53 91-20-31.0 0.24 1
Styrene ND ug/L 03/10/17 10:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 10:53 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 10:53 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/10/17 10:53 127-18-41.0 0.46 1
Toluene ND ug/L 03/10/17 10:53 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/10/17 10:53 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 10:53 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/10/17 10:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/10/17 10:53 79-00-51.0 0.29 1
Trichloroethene 14.1 ug/L 03/10/17 10:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/10/17 10:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/10/17 10:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/10/17 10:53 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/10/17 10:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/10/17 10:53 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/10/17 10:53 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/10/17 10:53 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)98 %03/10/17 10:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %03/10/17 10:53 17060-07-070-130 1
Toluene-d8 (S)101 %03/10/17 10:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 19 of 32
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 14:29 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 14:29 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 14:29 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 14:29 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 14:29 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 14:29 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 14:29 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 14:29 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 14:29 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 14:29 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 14:29 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 14:29 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 14:29 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 14:29 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 14:29 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 14:29 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 14:29 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 14:29 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 14:29 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 14:29 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 14:29 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 14:29 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 14:29 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 14:29 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 14:29 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 14:29 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 14:29 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 14:29 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 14:29 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 14:29 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 14:29 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 14:29 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 14:29 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 14:29 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 14:29 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 14:29 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 14:29 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 14:29 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 14:29 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 14:29 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 14:29 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 14:29 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 14:29 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 14:29 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 14:29 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 14:29 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 20 of 32
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 14:29 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 14:29 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 14:29 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 14:2903/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 14:29 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 14:29 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 14:29 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 14:29 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 14:29 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 14:29 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 14:29 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 14:29 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 14:29 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 14:29 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 14:29 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 14:29 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 14:29 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 14:2903/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 14:29 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 14:29 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 14:29 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 14:29 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)70 %03/10/17 14:29 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)70 %03/10/17 14:29 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)81 %03/10/17 14:29 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)25 %03/10/17 14:29 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)36 %03/10/17 14:29 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)76 %03/10/17 14:29 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:10 67-64-125.0 10.0 1
Benzene ND ug/L 03/10/17 11:10 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/10/17 11:10 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/10/17 11:10 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/10/17 11:10 75-27-41.0 0.18 1
Bromoform ND ug/L 03/10/17 11:10 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/10/17 11:10 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/10/17 11:10 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/10/17 11:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/10/17 11:10 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/10/17 11:10 75-00-31.0 0.54 1
Chloroform ND ug/L 03/10/17 11:10 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/10/17 11:10 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/10/17 11:10 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/10/17 11:10 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 21 of 32
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:10 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/10/17 11:10 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/10/17 11:10 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/10/17 11:10 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/10/17 11:10 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/10/17 11:10 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/10/17 11:10 75-71-81.0 0.21 1
1,1-Dichloroethane 1.9 ug/L 03/10/17 11:10 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/10/17 11:10 107-06-21.0 0.24 1
1,1-Dichloroethene 2.6 ug/L 03/10/17 11:10 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 3.6 ug/L 03/10/17 11:10 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/10/17 11:10 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/10/17 11:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/10/17 11:10 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/10/17 11:10 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/10/17 11:10 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:10 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/10/17 11:10 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/10/17 11:10 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:10 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/10/17 11:10 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/10/17 11:10 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/10/17 11:10 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:10 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/10/17 11:10 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/10/17 11:10 91-20-31.0 0.24 1
Styrene ND ug/L 03/10/17 11:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:10 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:10 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/10/17 11:10 127-18-41.0 0.46 1
Toluene ND ug/L 03/10/17 11:10 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:10 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:10 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/10/17 11:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/10/17 11:10 79-00-51.0 0.29 1
Trichloroethene 3.5 ug/L 03/10/17 11:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/10/17 11:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/10/17 11:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/10/17 11:10 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/10/17 11:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/10/17 11:10 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/10/17 11:10 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/10/17 11:10 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 22 of 32
Pace Analytical Services, LLC
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[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)95 %03/10/17 11:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/10/17 11:10 17060-07-070-130 1
Toluene-d8 (S)100 %03/10/17 11:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 23 of 32
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351627
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950708
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/10/17 07:100.33
1,1,1-Trichloroethane ug/L ND 1.0 03/10/17 07:100.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/10/17 07:100.40
1,1,2-Trichloroethane ug/L ND 1.0 03/10/17 07:100.29
1,1-Dichloroethane ug/L ND 1.0 03/10/17 07:100.32
1,1-Dichloroethene ug/L ND 1.0 03/10/17 07:100.56
1,1-Dichloropropene ug/L ND 1.0 03/10/17 07:100.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/10/17 07:100.33
1,2,3-Trichloropropane ug/L ND 1.0 03/10/17 07:100.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/10/17 07:100.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/10/17 07:102.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/10/17 07:100.27
1,2-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.30
1,2-Dichloroethane ug/L ND 1.0 03/10/17 07:100.24
1,2-Dichloropropane ug/L ND 1.0 03/10/17 07:100.27
1,3-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.24
1,3-Dichloropropane ug/L ND 1.0 03/10/17 07:100.28
1,4-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.33
2,2-Dichloropropane ug/L ND 1.0 03/10/17 07:100.13
2-Butanone (MEK)ug/L ND 5.0 03/10/17 07:100.96
2-Chlorotoluene ug/L ND 1.0 03/10/17 07:100.35
2-Hexanone ug/L ND 5.0 03/10/17 07:100.46
4-Chlorotoluene ug/L ND 1.0 03/10/17 07:100.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/10/17 07:100.33
Acetone ug/L ND 25.0 03/10/17 07:1010.0
Benzene ug/L ND 1.0 03/10/17 07:100.25
Bromobenzene ug/L ND 1.0 03/10/17 07:100.30
Bromochloromethane ug/L ND 1.0 03/10/17 07:100.17
Bromodichloromethane ug/L ND 1.0 03/10/17 07:100.18
Bromoform ug/L ND 1.0 03/10/17 07:100.26
Bromomethane ug/L ND 2.0 03/10/17 07:100.29
Carbon tetrachloride ug/L ND 1.0 03/10/17 07:100.25
Chlorobenzene ug/L ND 1.0 03/10/17 07:100.23
Chloroethane ug/L ND 1.0 03/10/17 07:100.54
Chloroform ug/L ND 1.0 03/10/17 07:100.14
Chloromethane ug/L ND 1.0 03/10/17 07:100.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/10/17 07:100.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/10/17 07:100.13
Dibromochloromethane ug/L ND 1.0 03/10/17 07:100.21
Dibromomethane ug/L ND 1.0 03/10/17 07:100.21
Dichlorodifluoromethane ug/L ND 1.0 03/10/17 07:100.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 24 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950708
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/10/17 07:100.12
Ethylbenzene ug/L ND 1.0 03/10/17 07:100.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/10/17 07:100.71
m&p-Xylene ug/L ND 2.0 03/10/17 07:100.66
Methyl-tert-butyl ether ug/L ND 1.0 03/10/17 07:100.21
Methylene Chloride ug/L ND 2.0 03/10/17 07:100.97
Naphthalene ug/L ND 1.0 03/10/17 07:100.24
o-Xylene ug/L ND 1.0 03/10/17 07:100.23
p-Isopropyltoluene ug/L ND 1.0 03/10/17 07:100.31
Styrene ug/L ND 1.0 03/10/17 07:100.26
Tetrachloroethene ug/L ND 1.0 03/10/17 07:100.46
Toluene ug/L ND 1.0 03/10/17 07:100.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/10/17 07:100.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/10/17 07:100.26
Trichloroethene ug/L ND 1.0 03/10/17 07:100.47
Trichlorofluoromethane ug/L ND 1.0 03/10/17 07:100.20
Vinyl acetate ug/L ND 2.0 03/10/17 07:100.35
Vinyl chloride ug/L ND 1.0 03/10/17 07:100.62
Xylene (Total)ug/L ND 1.0 03/10/17 07:100.66
1,2-Dichloroethane-d4 (S)%100 70-130 03/10/17 07:10
4-Bromofluorobenzene (S)%97 70-130 03/10/17 07:10
Toluene-d8 (S)%102 70-130 03/10/17 07:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950709LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950710
1,1,1,2-Tetrachloroethane ug/L 51.750 103 70-13010050.1 3 30
1,1,1-Trichloroethane ug/L 51.950 104 70-13010150.7 2 30
1,1,2,2-Tetrachloroethane ug/L 51.750 103 70-13010150.7 2 30
1,1,2-Trichloroethane ug/L 50.750 101 70-13010251.0 1 30
1,1-Dichloroethane ug/L 50.350 101 70-13010049.8 1 30
1,1-Dichloroethene ug/L 54.650 109 70-13210552.7 4 30
1,1-Dichloropropene ug/L 54.250 108 70-13010753.4 1 30
1,2,3-Trichlorobenzene ug/L 51.750 103 70-13510251.2 1 30
1,2,3-Trichloropropane ug/L 51.150 102 70-13010250.8 1 30
1,2,4-Trichlorobenzene ug/L 52.550 105 70-13410351.3 2 30
1,2-Dibromo-3-chloropropane ug/L 52.350 105 70-13010653.2 2 30
1,2-Dibromoethane (EDB)ug/L 50.750 101 70-13010150.4 1 30
1,2-Dichlorobenzene ug/L 51.350 103 70-13010150.6 1 30
1,2-Dichloroethane ug/L 47.350 95 70-1309246.1 2 30
1,2-Dichloropropane ug/L 52.350 105 70-1309949.7 5 30
1,3-Dichlorobenzene ug/L 51.650 103 70-13010049.9 3 30
1,3-Dichloropropane ug/L 52.150 104 70-13010351.5 1 30
1,4-Dichlorobenzene ug/L 50.550 101 70-1309949.4 2 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 25 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950709LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950710
2,2-Dichloropropane ug/L 51.450 103 58-1459547.6 8 30
2-Butanone (MEK)ug/L 98.4100 98 70-145101101 3 30
2-Chlorotoluene ug/L 52.950 106 70-13010150.5 5 30
2-Hexanone ug/L 104100 104 70-144106106 1 30
4-Chlorotoluene ug/L 51.450 103 70-1309949.6 4 30
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-140101101 1 30
Acetone ug/L 104100 104 50-175109109 5 30
Benzene ug/L 53.350 107 70-13010351.6 3 30
Bromobenzene ug/L 52.050 104 70-13010150.3 3 30
Bromochloromethane ug/L 53.050 106 70-13010250.8 4 30
Bromodichloromethane ug/L 53.450 107 70-13010351.6 3 30
Bromoform ug/L 50.550 101 70-13010250.8 1 30
Bromomethane ug/L 34.450 69 54-1307135.4 3 30
Carbon tetrachloride ug/L 50.350 101 70-1329949.5 2 30
Chlorobenzene ug/L 51.550 103 70-13010150.4 2 30
Chloroethane ug/L 47.750 95 64-1349346.5 2 30
Chloroform ug/L 49.450 99 70-1309547.5 4 30
Chloromethane ug/L 41.550 83 64-1308341.6 0 30
cis-1,2-Dichloroethene ug/L 50.450 101 70-13110049.8 1 30
cis-1,3-Dichloropropene ug/L 52.650 105 70-13010251.1 3 30
Dibromochloromethane ug/L 52.150 104 70-13010251.2 2 30
Dibromomethane ug/L 49.850 100 70-1319648.2 3 30
Dichlorodifluoromethane ug/L 51.150 102 56-13010150.7 1 30
Diisopropyl ether ug/L 50.450 101 70-1309849.0 3 30
Ethylbenzene ug/L 53.050 106 70-13010351.5 3 30
Hexachloro-1,3-butadiene ug/L 52.650 105 70-13010250.9 3 30
m&p-Xylene ug/L 105100 105 70-130101101 4 30
Methyl-tert-butyl ether ug/L 52.150 104 70-13010451.8 1 30
Methylene Chloride ug/L 50.650 101 63-13010150.5 0 30
Naphthalene ug/L 53.950 108 70-13810753.4 1 30
o-Xylene ug/L 52.550 105 70-13010351.6 2 30
p-Isopropyltoluene ug/L 50.750 101 70-1309949.5 2 30
Styrene ug/L 53.950 108 70-13010452.1 3 30
Tetrachloroethene ug/L 50.950 102 70-1309949.4 3 30
Toluene ug/L 52.850 106 70-13010351.4 3 30
trans-1,2-Dichloroethene ug/L 53.250 106 70-13010652.8 1 30
trans-1,3-Dichloropropene ug/L 51.650 103 70-13210351.3 0 30
Trichloroethene ug/L 50.150 100 70-1309849.1 2 30
Trichlorofluoromethane ug/L 53.850 108 62-13310652.9 2 30
Vinyl acetate ug/L 105100 105 66-157106106 1 30
Vinyl chloride ug/L 45.850 92 50-1508944.7 2 30
Xylene (Total)ug/L 157150 105 70-130102153 3 30
1,2-Dichloroethane-d4 (S)%97 70-13094
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 26 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351633
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950722
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/10/17 12:001.9
1,2-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.2
1,3-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.1
1,4-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.2
1-Methylnaphthalene ug/L ND 10.0 03/10/17 12:000.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/10/17 12:001.6
2,4,5-Trichlorophenol ug/L ND 10.0 03/10/17 12:002.2
2,4,6-Trichlorophenol ug/L ND 10.0 03/10/17 12:001.9
2,4-Dichlorophenol ug/L ND 10.0 03/10/17 12:001.7
2,4-Dimethylphenol ug/L ND 10.0 03/10/17 12:002.2
2,4-Dinitrophenol ug/L ND 50.0 03/10/17 12:006.5
2,4-Dinitrotoluene ug/L ND 10.0 03/10/17 12:001.2
2,6-Dinitrotoluene ug/L ND 10.0 03/10/17 12:001.7
2-Chloronaphthalene ug/L ND 10.0 03/10/17 12:002.2
2-Chlorophenol ug/L ND 10.0 03/10/17 12:001.5
2-Methylnaphthalene ug/L ND 10.0 03/10/17 12:000.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/10/17 12:001.7
2-Nitroaniline ug/L ND 50.0 03/10/17 12:002.8
2-Nitrophenol ug/L ND 10.0 03/10/17 12:001.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/10/17 12:001.7
3,3'-Dichlorobenzidine ug/L ND 20.0 03/10/17 12:001.4
3-Nitroaniline ug/L ND 50.0 03/10/17 12:002.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/10/17 12:001.7
4-Bromophenylphenyl ether ug/L ND 10.0 03/10/17 12:001.3
4-Chloro-3-methylphenol ug/L ND 20.0 03/10/17 12:004.2
4-Chloroaniline ug/L ND 20.0 03/10/17 12:003.4
4-Chlorophenylphenyl ether ug/L ND 10.0 03/10/17 12:002.1
4-Nitroaniline ug/L ND 20.0 03/10/17 12:002.5
4-Nitrophenol ug/L ND 50.0 03/10/17 12:005.8
Acenaphthene ug/L ND 10.0 03/10/17 12:000.25
Acenaphthylene ug/L ND 10.0 03/10/17 12:000.21
Aniline ug/L ND 10.0 03/10/17 12:001.3
Anthracene ug/L ND 10.0 03/10/17 12:000.14
Benzo(a)anthracene ug/L ND 10.0 03/10/17 12:000.33
Benzo(a)pyrene ug/L ND 10.0 03/10/17 12:000.30
Benzo(b)fluoranthene ug/L ND 10.0 03/10/17 12:000.28
Benzo(g,h,i)perylene ug/L ND 10.0 03/10/17 12:000.38
Benzo(k)fluoranthene ug/L ND 10.0 03/10/17 12:000.43
Benzoic Acid ug/L ND 50.0 03/10/17 12:0011.1
Benzyl alcohol ug/L ND 20.0 03/10/17 12:003.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/10/17 12:001.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 27 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950722
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 03/10/17 12:001.5
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/10/17 12:000.85
Butylbenzylphthalate ug/L ND 10.0 03/10/17 12:000.75
Chrysene ug/L ND 10.0 03/10/17 12:000.21
Di-n-butylphthalate ug/L ND 10.0 03/10/17 12:001.1
Di-n-octylphthalate ug/L ND 10.0 03/10/17 12:000.86
Dibenz(a,h)anthracene ug/L ND 10.0 03/10/17 12:000.55
Dibenzofuran ug/L ND 10.0 03/10/17 12:001.8
Diethylphthalate ug/L ND 10.0 03/10/17 12:001.3
Dimethylphthalate ug/L ND 10.0 03/10/17 12:001.5
Fluoranthene ug/L ND 10.0 03/10/17 12:000.21
Fluorene ug/L ND 10.0 03/10/17 12:000.21
Hexachloro-1,3-butadiene ug/L ND 10.0 03/10/17 12:001.8
Hexachlorobenzene ug/L ND 10.0 03/10/17 12:001.1
Hexachlorocyclopentadiene ug/L ND 10.0 03/10/17 12:001.8
Hexachloroethane ug/L ND 10.0 03/10/17 12:001.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/10/17 12:000.29
Isophorone ug/L ND 10.0 03/10/17 12:001.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/10/17 12:002.1
N-Nitrosodimethylamine ug/L ND 10.0 03/10/17 12:001.3
N-Nitrosodiphenylamine ug/L ND 10.0 03/10/17 12:001.3
Naphthalene ug/L ND 10.0 03/10/17 12:000.34
Nitrobenzene ug/L ND 10.0 03/10/17 12:001.7
Pentachlorophenol ug/L ND 25.0 03/10/17 12:002.3
Phenanthrene ug/L ND 10.0 03/10/17 12:000.22
Phenol ug/L ND 10.0 03/10/17 12:001.7
Pyrene ug/L ND 10.0 03/10/17 12:000.19
2,4,6-Tribromophenol (S)%78 27-110 03/10/17 12:00
2-Fluorobiphenyl (S)%67 27-110 03/10/17 12:00
2-Fluorophenol (S)%37 12-110 03/10/17 12:00
Nitrobenzene-d5 (S)%70 21-110 03/10/17 12:00
Phenol-d6 (S)%21 10-110 03/10/17 12:00
Terphenyl-d14 (S)%88 31-107 03/10/17 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
1,2,4-Trichlorobenzene ug/L 15.025 60 31-1206015.1 1 30
1,2-Dichlorobenzene ug/L 14.725 59 38-1205714.3 2 30
1,3-Dichlorobenzene ug/L 13.325 53 30-1225714.1 6 30
1,4-Dichlorobenzene ug/L 13.625 54 37-1205413.5 0 30
1-Methylnaphthalene ug/L 17.325 69 34-1136917.2 0 30
2,2'-Oxybis(1-chloropropane)ug/L 16.825 67 18-1206115.4 9 30
2,4,5-Trichlorophenol ug/L 16.825 67 43-1136315.8 6 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 28 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
2,4,6-Trichlorophenol ug/L 18.625 75 42-1207418.5 1 30
2,4-Dichlorophenol ug/L 17.625 71 30-1206817.1 3 30
2,4-Dimethylphenol ug/L 19.625 78 29-1117518.8 4 30
2,4-Dinitrophenol ug/L 108125 86 19-13291114 6 30
2,4-Dinitrotoluene ug/L 23.725 95 58-1289122.7 5 30
2,6-Dinitrotoluene ug/L 25.125 100 54-1299924.6 2 30
2-Chloronaphthalene ug/L 20.725 83 43-1178020.1 3 30
2-Chlorophenol ug/L 15.325 61 37-1205914.7 4 30
2-Methylnaphthalene ug/L 17.425 70 33-1207318.2 4 30
2-Methylphenol(o-Cresol)ug/L 12.625 50 31-1204611.5 9 30
2-Nitroaniline ug/L 35.3J50 71 48-1217035.0J 30
2-Nitrophenol ug/L 19.025 76 25-1168020.1 6 30
3&4-Methylphenol(m&p Cresol)ug/L 27.825 111 23-1209724.3 13 30
3,3'-Dichlorobenzidine ug/L 39.950 80 10-1547436.8 8 30
3-Nitroaniline ug/L 40.6J50 81 43-1157939.3J 30
4,6-Dinitro-2-methylphenol ug/L 43.550 87 44-1248341.3 5 30
4-Bromophenylphenyl ether ug/L 18.925 76 34-1137418.6 2 30
4-Chloro-3-methylphenol ug/L 39.150 78 31-1107135.4 10 30
4-Chloroaniline ug/L 38.250 76 20-1207135.7 7 30
4-Chlorophenylphenyl ether ug/L 18.425 74 34-1167117.7 4 30
4-Nitroaniline ug/L 42.050 84 46-1288140.3 4 30
4-Nitrophenol ug/L 42.2J125 34 11-1203442.5J 30
Acenaphthene ug/L 19.325 77 48-1147518.6 4 30
Acenaphthylene ug/L 19.225 77 48-1127418.4 4 30
Aniline ug/L 12.125 48 26-1204411.1 9 30
Anthracene ug/L 20.125 80 57-1187418.6 8 30
Benzo(a)anthracene ug/L 20.125 81 56-1217418.5 9 30
Benzo(a)pyrene ug/L 19.425 77 55-1277418.4 5 30
Benzo(b)fluoranthene ug/L 21.225 85 53-1287819.6 8 30
Benzo(g,h,i)perylene ug/L 21.325 85 54-1258320.7 3 30
Benzo(k)fluoranthene ug/L 21.325 85 51-1237819.5 9 30
Benzoic Acid ug/L 32.0J125 26 10-1202531.9J 30
Benzyl alcohol ug/L 27.750 55 27-1204924.5 12 30
bis(2-Chloroethoxy)methane ug/L 18.525 74 32-1207117.9 3 30
bis(2-Chloroethyl) ether ug/L 16.925 68 33-1116015.0 12 30
bis(2-Ethylhexyl)phthalate ug/L 23.425 94 50-1458721.9 7 30
Butylbenzylphthalate ug/L 24.425 98 54-1389223.0 6 30
Chrysene ug/L 20.425 82 58-1277719.2 6 30
Di-n-butylphthalate ug/L 23.125 93 56-1258721.8 6 30
Di-n-octylphthalate ug/L 20.425 82 50-1347919.8 3 30
Dibenz(a,h)anthracene ug/L 22.125 89 53-1298521.3 4 30
Dibenzofuran ug/L 18.625 74 45-1207418.4 1 30
Diethylphthalate ug/L 22.225 89 53-1208521.3 4 30
Dimethylphthalate ug/L 21.225 85 55-1168320.8 2 30
Fluoranthene ug/L 21.425 86 57-1258020.0 7 30
Fluorene ug/L 20.025 80 53-1187619.1 5 30
Hexachloro-1,3-butadiene ug/L 13.725 55 23-1206014.9 8 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 29 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
Hexachlorobenzene ug/L 19.625 79 49-1167518.8 4 30
Hexachlorocyclopentadiene ug/L 14.325 57 26-1586015.0 5 30
Hexachloroethane ug/L 12.825 51 30-1145714.3 11 30
Indeno(1,2,3-cd)pyrene ug/L 22.925 91 55-1288521.3 7 30
Isophorone ug/L 21.825 87 31-1188220.5 6 30
N-Nitroso-di-n-propylamine ug/L 16.925 68 32-1196315.8 7 30
N-Nitrosodimethylamine ug/L 10.125 40 13-1204511.3 11 30
N-Nitrosodiphenylamine ug/L 19.625 78 43-1207318.4 6 30
Naphthalene ug/L 17.625 70 32-1207017.6 0 30
Nitrobenzene ug/L 20.225 81 33-1108020.1 1 30
Pentachlorophenol ug/L 44.050 88 10-1378040.1 9 30
Phenanthrene ug/L 20.425 82 57-1177618.9 8 30
Phenol ug/L 8.5J25 34 10-120307.5J 30
Pyrene ug/L 18.425 74 55-1226917.2 7 30
2,4,6-Tribromophenol (S)%89 27-11080
2-Fluorobiphenyl (S)%72 27-11068
2-Fluorophenol (S)%39 12-11036
Nitrobenzene-d5 (S)%72 21-11069
Phenol-d6 (S)%27 10-11023
Terphenyl-d14 (S)%76 31-10770
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 30 of 32
Pace Analytical Services, LLC
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[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 31 of 32
Pace Analytical Services, LLC
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[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92332882001 351633 3516770309171049W1EPA 3510 EPA 8270
92332882002 351633 3516770309171139W2EPA 3510 EPA 8270
92332882003 351633 3516770309171320DSEPA 3510 EPA 8270
92332882004 351633 3516770309171344USEPA 3510 EPA 8270
92332882001 3516270309171049W1EPA 8260
92332882002 3516270309171139W2EPA 8260
92332882003 3516270309171320DSEPA 8260
92332882004 3516270309171344USEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 32 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
file:///C/Users/tamechum/Desktop/Harwell%20Estates%20Mobile%20Home%20Pakr/Laserfiche/Harwell/ATT00001.htm[4/27/2018 1:53:58 PM]
1
Beverly, Trudy
From:Beverly, Trudy
Sent:Monday, March 13, 2017 7:39 AM
To:Earnest, Emily; Assefa, Hanna
Subject:FW: Harwell Response - Harwell Estates Mobile Home Park
Attachments:01-067 Harwell Estates Well Response Results 031017.xls; ATT00001.htm
EPA has taken some stream samples (see other email) and has preliminary results from well #1 & #2 confirming previous
detections.

From: Beverly, Trudy
Sent: Monday, March 13, 2017 7:35 AM
To: 'Eichinger, Kevin' <[e-mail]>
Cc: Bateson, James <[e-mail]>; Day, Collin <[e-mail]>; Jesneck, Charlotte
<[e-mail]>; Ramey, David E <[e-mail]>; 'Samantha Dye'
<[e-mail]>
Subject: RE: Harwell Response

Thank you for the information.
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-section/inactive-
hazardous-sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-
maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
*******************************************************************************
From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Friday, March 10, 2017 9:24 PM
To: Beverly, Trudy <[e-mail]>
2
Cc: Bateson, James <[e-mail]>
Subject: Fwd: Harwell Response

Here is the summary table. Confirms the well sample data. Also take a look at the creek samples. Found TCE is
the creek.

Begin forwarded message:
From: "Taylor, Todd" <[e-mail]>
Date: March 10, 2017 at 21:13:18 EST
To: Kevin Eichinger <[e-mail]>
Subject: Harwell Response
Hello Kevin,

The table is attached.
<01-067 Harwell Estates Well Response Results 2-7-17.xls>
TABLE 1
SUMMARY OF DETECTED ANALYTES
1 of 1 Harwell Estates Well Response
Sample ID
Date
Sampled
1,4-
Dichlorobenzene
(µg/L)
1,1-
Dichloroethane
(µg/L)
1,2-
Dichloroethane
(µg/L)
1,1-DCE
(µg/L)
Cis-1,2-DCE
(µg/L)
trans-1,2-
DCE
(µg/L)
PCE
(µg/L)
1,1,1-
Trichloroethane
(µg/L)
TCE
(µg/L)
Vinyl
Chloride
(µg/L)
75 5 7 70 100 5 200 5 2
48 280 17 280 36 360 41 8,000 2.8 1.9
WELLHEAD #1 2/7/2017 ND NA ND 32 16 ND 42 ND 930 ND
WELLHEAD #1
AFTER FILTER
2/7/2017 ND NA ND 34 21 ND 33 ND 1100 ND
WELL #2 2/7/2017 0.98 NA 0.79 170 160 2.5 12 8.2 370 1.9
0309171049W1 -
EPA Well 1 Sample
3/9/2017 ND ND ND 22.3 15.5 ND 29.4 ND 944 ND
0309171139W2 -
EPA Well 2 Sample
3/9/2017 ND 98.3 ND 141 194 2.4J 10.9 5.6 409 ND
0309171320DS -
Downstream Sample
3/9/2017 ND 4.8 ND 7.9 9.1 ND ND ND 14.1 ND
0309171344US -
Upstream Sample
3/9/2017 ND 1.9 ND 2.6 3.6 ND ND ND 3.5 ND
Notes
Bold Exceeds the respective MCL
Bold Exceeds the respective MCL and RML
MCL EPA Maximum Contaminant Level
PCE Tetrachloroethylene
RML EPA Removal Management Level - Hazard Quotient = 1
TCE Trichloroethylene
U Analyte was not detected at concentrations above the laboratory reporting limit shown.
µg/L Micrograms per liter
EPA MCL
EPA RML
file:///C/Users/tamechum/Desktop/Harwell%20Estates%20Mobile%20Home%20Pakr/Laserfiche/Harwell/ATT00001.htm[4/27/2018 1:56:00 PM]
1
Beverly, Trudy
From:Beverly, Trudy
Sent:Monday, March 13, 2017 7:36 AM
To:Jesneck, Charlotte; Day, Collin; Ramey, David E; Samantha Dye; Earnest, Emily; Assefa, Hanna
Subject:RE: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results - Harwell Estates Mobile
Home Park
Attachments:92332882_fr_draft.pdf; ATT00001.htm
fyi

From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Friday, March 10, 2017 9:22 PM
To: Beverly, Trudy <[e-mail]>
Cc: Bateson, James <[e-mail]>
Subject: Fwd: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results

Results of out sampling. Sending the summary table next.

Begin forwarded message:
From: "Taylor, Todd" <[e-mail]>
Date: March 10, 2017 at 17:21:05 EST
To: Kevin Eichinger <[e-mail]>
Cc: "Vasser, Bryan" <[e-mail]>
Subject: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results
Hello,

Attached are the preliminary results for VOC, SVOC the metals will follow when complete. When the
samples are QC’d I will forward as well.

Regards,
Todd

Todd Taylor|ENV.SCI.V
Direct: 615.992-5556 |
[e-mail]
Tetra Tech Inc. |
712 Melrose Avenue | Nashville, TN 37211 | www.tetratech.com
PLEASE NOTE: This message, including any attachments, may include privileged, confidential and/or
inside information. Any distribution or use of this communication by anyone other than the intended
recipient is strictly prohibited and may be unlawful. If you are not the intended recipient, please notify the
sender by replying to this message and then delete it from your system.

#=CL#
March 10, 2017
LIMS USE: FR Prelim - JESSICA
LIMS OBJECT ID: 92332882
92332882
Project:
Pace Project No.:
RE:
Jessica Vickers
Tetra Tech
950 South 4th Street
Baldwyn, MS 38824
HARWELL RD PRIVA 103X902701067
Dear Jessica Vickers:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Page 1 of 32
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#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID Matrix Date Collected Date Received
92332882001 0309171049W1 Water 03/09/17 10:49 03/09/17 15:07
92332882002 0309171139W2 Water 03/09/17 11:39 03/09/17 15:07
92332882003 0309171320DS Water 03/09/17 13:20 03/09/17 15:07
92332882004 0309171344US Water 03/09/17 13:44 03/09/17 15:07
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92332882001 0309171049W1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882002 0309171139W2 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882003 0309171320DS EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882004 0309171344US EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92332882001 0309171049W1
1,1-Dichloroethene 22.3 ug/L 03/10/17 11:2710.0EPA 8260
cis-1,2-Dichloroethene 15.5 ug/L 03/10/17 11:2710.0EPA 8260
Tetrachloroethene 29.4 ug/L 03/10/17 11:2710.0EPA 8260
Trichloroethene 944 ug/L 03/10/17 11:2710.0EPA 8260
92332882002 0309171139W2
1,1-Dichloroethane 98.3 ug/L 03/10/17 11:444.0EPA 8260
1,1-Dichloroethene 141 ug/L 03/10/17 11:444.0EPA 8260
cis-1,2-Dichloroethene 194 ug/L 03/10/17 11:444.0EPA 8260
trans-1,2-Dichloroethene 2.4J ug/L 03/10/17 11:444.0EPA 8260
Tetrachloroethene 10.9 ug/L 03/10/17 11:444.0EPA 8260
1,1,1-Trichloroethane 5.6 ug/L 03/10/17 11:444.0EPA 8260
Trichloroethene 409 ug/L 03/10/17 11:444.0EPA 8260
92332882003 0309171320DS
1,1-Dichloroethane 4.8 ug/L 03/10/17 10:531.0EPA 8260
1,1-Dichloroethene 7.9 ug/L 03/10/17 10:531.0EPA 8260
cis-1,2-Dichloroethene 9.1 ug/L 03/10/17 10:531.0EPA 8260
Trichloroethene 14.1 ug/L 03/10/17 10:531.0EPA 8260
92332882004 0309171344US
1,1-Dichloroethane 1.9 ug/L 03/10/17 11:101.0EPA 8260
1,1-Dichloroethene 2.6 ug/L 03/10/17 11:101.0EPA 8260
cis-1,2-Dichloroethene 3.6 ug/L 03/10/17 11:101.0EPA 8260
Trichloroethene 3.5 ug/L 03/10/17 11:101.0EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Page 5 of 32
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#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Method:
Client:Tetra Tech EMI
EPA 8270
Date:March 10, 2017
Description:8270 MSSV Semivolatile Organic
General Information:
4 samples were analyzed for EPA 8270. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Method:
Client:Tetra Tech EMI
EPA 8260
Date:March 10, 2017
Description:8260 MSV Low Level
General Information:
4 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:03 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:03 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:03 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:03 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:03 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:03 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:03 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:03 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:03 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:03 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:03 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:03 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:03 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:03 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:03 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:03 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:03 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:03 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:03 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:03 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:03 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:03 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:03 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:03 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:03 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:03 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:03 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:03 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:03 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:03 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:03 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:03 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:03 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:03 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:03 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:03 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:03 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:03 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:03 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:03 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:03 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:03 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:03 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:03 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:03 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:03 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:03 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:03 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:03 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:0303/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:03 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:03 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:03 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:03 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:03 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:03 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:03 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:03 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:03 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:03 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:03 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:03 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:03 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:0303/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:03 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:03 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:03 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:03 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)69 %03/10/17 12:03 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)69 %03/10/17 12:03 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)82 %03/10/17 12:03 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)23 %03/10/17 12:03 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)33 %03/10/17 12:03 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)77 %03/10/17 12:03 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:27 67-64-125010010
Benzene ND ug/L 03/10/17 11:27 71-43-210.0 2.5 10
Bromobenzene ND ug/L 03/10/17 11:27 108-86-110.0 3.0 10
Bromochloromethane ND ug/L 03/10/17 11:27 74-97-510.0 1.7 10
Bromodichloromethane ND ug/L 03/10/17 11:27 75-27-410.0 1.8 10
Bromoform ND ug/L 03/10/17 11:27 75-25-210.0 2.6 10
Bromomethane ND ug/L 03/10/17 11:27 74-83-920.0 2.9 10
2-Butanone (MEK)ND ug/L 03/10/17 11:27 78-93-350.0 9.6 10
Carbon tetrachloride ND ug/L 03/10/17 11:27 56-23-510.0 2.5 10
Chlorobenzene ND ug/L 03/10/17 11:27 108-90-710.0 2.3 10
Chloroethane ND ug/L 03/10/17 11:27 75-00-310.0 5.4 10
Chloroform ND ug/L 03/10/17 11:27 67-66-310.0 1.4 10
Chloromethane ND ug/L 03/10/17 11:27 74-87-310.0 1.1 10
2-Chlorotoluene ND ug/L 03/10/17 11:27 95-49-810.0 3.5 10
4-Chlorotoluene ND ug/L 03/10/17 11:27 106-43-410.0 3.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 9 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:27 96-12-820.0 20.0 10
Dibromochloromethane ND ug/L 03/10/17 11:27 124-48-110.0 2.1 10
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:27 106-93-410.0 2.7 10
Dibromomethane ND ug/L 03/10/17 11:27 74-95-310.0 2.1 10
1,2-Dichlorobenzene ND ug/L 03/10/17 11:27 95-50-110.0 3.0 10
1,3-Dichlorobenzene ND ug/L 03/10/17 11:27 541-73-110.0 2.4 10
1,4-Dichlorobenzene ND ug/L 03/10/17 11:27 106-46-710.0 3.3 10
Dichlorodifluoromethane ND ug/L 03/10/17 11:27 75-71-810.0 2.1 10
1,1-Dichloroethane ND ug/L 03/10/17 11:27 75-34-310.0 3.2 10
1,2-Dichloroethane ND ug/L 03/10/17 11:27 107-06-210.0 2.4 10
1,1-Dichloroethene 22.3 ug/L 03/10/17 11:27 75-35-410.0 5.6 10
cis-1,2-Dichloroethene 15.5 ug/L 03/10/17 11:27 156-59-210.0 1.9 10
trans-1,2-Dichloroethene ND ug/L 03/10/17 11:27 156-60-510.0 4.9 10
1,2-Dichloropropane ND ug/L 03/10/17 11:27 78-87-510.0 2.7 10
1,3-Dichloropropane ND ug/L 03/10/17 11:27 142-28-910.0 2.8 10
2,2-Dichloropropane ND ug/L 03/10/17 11:27 594-20-710.0 1.3 10
1,1-Dichloropropene ND ug/L 03/10/17 11:27 563-58-610.0 4.9 10
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:27 10061-01-510.0 1.3 10
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:27 10061-02-610.0 2.6 10
Diisopropyl ether ND ug/L 03/10/17 11:27 108-20-310.0 1.2 10
Ethylbenzene ND ug/L 03/10/17 11:27 100-41-410.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:27 87-68-310.0 7.1 10
2-Hexanone ND ug/L 03/10/17 11:27 591-78-650.0 4.6 10
p-Isopropyltoluene ND ug/L 03/10/17 11:27 99-87-610.0 3.1 10
Methylene Chloride ND ug/L 03/10/17 11:27 75-09-220.0 9.7 10
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:27 108-10-150.0 3.3 10
Methyl-tert-butyl ether ND ug/L 03/10/17 11:27 1634-04-410.0 2.1 10
Naphthalene ND ug/L 03/10/17 11:27 91-20-310.0 2.4 10
Styrene ND ug/L 03/10/17 11:27 100-42-510.0 2.6 10
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:27 630-20-610.0 3.3 10
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:27 79-34-510.0 4.0 10
Tetrachloroethene 29.4 ug/L 03/10/17 11:27 127-18-410.0 4.6 10
Toluene ND ug/L 03/10/17 11:27 108-88-310.0 2.6 10
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:27 87-61-610.0 3.3 10
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:27 120-82-110.0 3.5 10
1,1,1-Trichloroethane ND ug/L 03/10/17 11:27 71-55-610.0 4.8 10
1,1,2-Trichloroethane ND ug/L 03/10/17 11:27 79-00-510.0 2.9 10
Trichloroethene 944 ug/L 03/10/17 11:27 79-01-610.0 4.7 10
Trichlorofluoromethane ND ug/L 03/10/17 11:27 75-69-410.0 2.0 10
1,2,3-Trichloropropane ND ug/L 03/10/17 11:27 96-18-410.0 4.1 10
Vinyl acetate ND ug/L 03/10/17 11:27 108-05-420.0 3.5 10
Vinyl chloride ND ug/L 03/10/17 11:27 75-01-410.0 6.2 10
Xylene (Total)ND ug/L 03/10/17 11:27 1330-20-710.0 6.6 10
m&p-Xylene ND ug/L 03/10/17 11:27 179601-23-120.0 6.6 10
o-Xylene ND ug/L 03/10/17 11:27 95-47-610.0 2.3 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 10 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)97 %03/10/17 11:27 460-00-470-130 10
1,2-Dichloroethane-d4 (S)99 %03/10/17 11:27 17060-07-070-130 10
Toluene-d8 (S)100 %03/10/17 11:27 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 11 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:31 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:31 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:31 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:31 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:31 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:31 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:31 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:31 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:31 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:31 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:31 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:31 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:31 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:31 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:31 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:31 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:31 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:31 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:31 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:31 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:31 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:31 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:31 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:31 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:31 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:31 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:31 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:31 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:31 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:31 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:31 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:31 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:31 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:31 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:31 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:31 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:31 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:31 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:31 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:31 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:31 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:31 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:31 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:31 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:31 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:31 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 12 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:31 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:31 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:31 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:3103/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:31 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:31 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:31 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:31 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:31 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:31 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:31 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:31 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:31 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:31 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:31 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:31 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:31 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:3103/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:31 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:31 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:31 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:31 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)67 %03/10/17 12:31 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)66 %03/10/17 12:31 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)79 %03/10/17 12:31 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)20 %03/10/17 12:31 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)31 %03/10/17 12:31 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)73 %03/10/17 12:31 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:44 67-64-110040.0 4
Benzene ND ug/L 03/10/17 11:44 71-43-24.0 1.0 4
Bromobenzene ND ug/L 03/10/17 11:44 108-86-14.0 1.2 4
Bromochloromethane ND ug/L 03/10/17 11:44 74-97-54.0 0.68 4
Bromodichloromethane ND ug/L 03/10/17 11:44 75-27-44.0 0.72 4
Bromoform ND ug/L 03/10/17 11:44 75-25-24.0 1.0 4
Bromomethane ND ug/L 03/10/17 11:44 74-83-98.0 1.2 4
2-Butanone (MEK)ND ug/L 03/10/17 11:44 78-93-320.0 3.8 4
Carbon tetrachloride ND ug/L 03/10/17 11:44 56-23-54.0 1.0 4
Chlorobenzene ND ug/L 03/10/17 11:44 108-90-74.0 0.92 4
Chloroethane ND ug/L 03/10/17 11:44 75-00-34.0 2.2 4
Chloroform ND ug/L 03/10/17 11:44 67-66-34.0 0.56 4
Chloromethane ND ug/L 03/10/17 11:44 74-87-34.0 0.44 4
2-Chlorotoluene ND ug/L 03/10/17 11:44 95-49-84.0 1.4 4
4-Chlorotoluene ND ug/L 03/10/17 11:44 106-43-44.0 1.2 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 13 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:44 96-12-88.0 8.0 4
Dibromochloromethane ND ug/L 03/10/17 11:44 124-48-14.0 0.84 4
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:44 106-93-44.0 1.1 4
Dibromomethane ND ug/L 03/10/17 11:44 74-95-34.0 0.84 4
1,2-Dichlorobenzene ND ug/L 03/10/17 11:44 95-50-14.0 1.2 4
1,3-Dichlorobenzene ND ug/L 03/10/17 11:44 541-73-14.0 0.96 4
1,4-Dichlorobenzene ND ug/L 03/10/17 11:44 106-46-74.0 1.3 4
Dichlorodifluoromethane ND ug/L 03/10/17 11:44 75-71-84.0 0.84 4
1,1-Dichloroethane 98.3 ug/L 03/10/17 11:44 75-34-34.0 1.3 4
1,2-Dichloroethane ND ug/L 03/10/17 11:44 107-06-24.0 0.96 4
1,1-Dichloroethene 141 ug/L 03/10/17 11:44 75-35-44.0 2.2 4
cis-1,2-Dichloroethene 194 ug/L 03/10/17 11:44 156-59-24.0 0.76 4
trans-1,2-Dichloroethene 2.4J ug/L 03/10/17 11:44 156-60-54.0 2.0 4
1,2-Dichloropropane ND ug/L 03/10/17 11:44 78-87-54.0 1.1 4
1,3-Dichloropropane ND ug/L 03/10/17 11:44 142-28-94.0 1.1 4
2,2-Dichloropropane ND ug/L 03/10/17 11:44 594-20-74.0 0.52 4
1,1-Dichloropropene ND ug/L 03/10/17 11:44 563-58-64.0 2.0 4
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:44 10061-01-54.0 0.52 4
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:44 10061-02-64.0 1.0 4
Diisopropyl ether ND ug/L 03/10/17 11:44 108-20-34.0 0.48 4
Ethylbenzene ND ug/L 03/10/17 11:44 100-41-44.0 1.2 4
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:44 87-68-34.0 2.8 4
2-Hexanone ND ug/L 03/10/17 11:44 591-78-620.0 1.8 4
p-Isopropyltoluene ND ug/L 03/10/17 11:44 99-87-64.0 1.2 4
Methylene Chloride ND ug/L 03/10/17 11:44 75-09-28.0 3.9 4
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:44 108-10-120.0 1.3 4
Methyl-tert-butyl ether ND ug/L 03/10/17 11:44 1634-04-44.0 0.84 4
Naphthalene ND ug/L 03/10/17 11:44 91-20-34.0 0.96 4
Styrene ND ug/L 03/10/17 11:44 100-42-54.0 1.0 4
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:44 630-20-64.0 1.3 4
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:44 79-34-54.0 1.6 4
Tetrachloroethene 10.9 ug/L 03/10/17 11:44 127-18-44.0 1.8 4
Toluene ND ug/L 03/10/17 11:44 108-88-34.0 1.0 4
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:44 87-61-64.0 1.3 4
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:44 120-82-14.0 1.4 4
1,1,1-Trichloroethane 5.6 ug/L 03/10/17 11:44 71-55-64.0 1.9 4
1,1,2-Trichloroethane ND ug/L 03/10/17 11:44 79-00-54.0 1.2 4
Trichloroethene 409 ug/L 03/10/17 11:44 79-01-64.0 1.9 4
Trichlorofluoromethane ND ug/L 03/10/17 11:44 75-69-44.0 0.80 4
1,2,3-Trichloropropane ND ug/L 03/10/17 11:44 96-18-44.0 1.6 4
Vinyl acetate ND ug/L 03/10/17 11:44 108-05-48.0 1.4 4
Vinyl chloride ND ug/L 03/10/17 11:44 75-01-44.0 2.5 4
Xylene (Total)ND ug/L 03/10/17 11:44 1330-20-74.0 2.6 4
m&p-Xylene ND ug/L 03/10/17 11:44 179601-23-18.0 2.6 4
o-Xylene ND ug/L 03/10/17 11:44 95-47-64.0 0.92 4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 14 of 32
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)97 %03/10/17 11:44 460-00-470-130 4
1,2-Dichloroethane-d4 (S)102 %03/10/17 11:44 17060-07-070-130 4
Toluene-d8 (S)100 %03/10/17 11:44 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 15 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:59 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:59 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:59 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:59 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:59 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:59 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:59 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:59 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:59 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:59 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:59 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:59 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:59 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:59 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:59 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:59 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:59 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:59 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:59 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:59 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:59 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:59 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:59 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:59 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:59 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:59 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:59 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:59 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:59 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:59 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:59 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:59 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:59 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:59 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:59 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:59 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:59 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:59 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:59 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:59 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:59 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:59 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:59 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:59 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:59 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:59 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 16 of 32
Pace Analytical Services, LLC
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[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:59 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:59 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:59 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:5903/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:59 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:59 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:59 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:59 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:59 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:59 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:59 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:59 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:59 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:59 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:59 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:59 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:59 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:5903/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:59 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:59 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:59 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:59 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)69 %03/10/17 12:59 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)70 %03/10/17 12:59 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)78 %03/10/17 12:59 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)22 %03/10/17 12:59 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)34 %03/10/17 12:59 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)74 %03/10/17 12:59 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 10:53 67-64-125.0 10.0 1
Benzene ND ug/L 03/10/17 10:53 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/10/17 10:53 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/10/17 10:53 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/10/17 10:53 75-27-41.0 0.18 1
Bromoform ND ug/L 03/10/17 10:53 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/10/17 10:53 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/10/17 10:53 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/10/17 10:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/10/17 10:53 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/10/17 10:53 75-00-31.0 0.54 1
Chloroform ND ug/L 03/10/17 10:53 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/10/17 10:53 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/10/17 10:53 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/10/17 10:53 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 17 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 10:53 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/10/17 10:53 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 10:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/10/17 10:53 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/10/17 10:53 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/10/17 10:53 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/10/17 10:53 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/10/17 10:53 75-71-81.0 0.21 1
1,1-Dichloroethane 4.8 ug/L 03/10/17 10:53 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/10/17 10:53 107-06-21.0 0.24 1
1,1-Dichloroethene 7.9 ug/L 03/10/17 10:53 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 9.1 ug/L 03/10/17 10:53 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/10/17 10:53 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/10/17 10:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/10/17 10:53 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/10/17 10:53 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/10/17 10:53 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/10/17 10:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/10/17 10:53 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/10/17 10:53 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/10/17 10:53 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 10:53 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/10/17 10:53 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/10/17 10:53 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/10/17 10:53 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 10:53 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/10/17 10:53 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/10/17 10:53 91-20-31.0 0.24 1
Styrene ND ug/L 03/10/17 10:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 10:53 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 10:53 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/10/17 10:53 127-18-41.0 0.46 1
Toluene ND ug/L 03/10/17 10:53 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/10/17 10:53 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 10:53 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/10/17 10:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/10/17 10:53 79-00-51.0 0.29 1
Trichloroethene 14.1 ug/L 03/10/17 10:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/10/17 10:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/10/17 10:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/10/17 10:53 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/10/17 10:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/10/17 10:53 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/10/17 10:53 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/10/17 10:53 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 18 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)98 %03/10/17 10:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %03/10/17 10:53 17060-07-070-130 1
Toluene-d8 (S)101 %03/10/17 10:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 19 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 14:29 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 14:29 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 14:29 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 14:29 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 14:29 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 14:29 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 14:29 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 14:29 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 14:29 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 14:29 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 14:29 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 14:29 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 14:29 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 14:29 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 14:29 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 14:29 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 14:29 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 14:29 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 14:29 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 14:29 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 14:29 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 14:29 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 14:29 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 14:29 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 14:29 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 14:29 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 14:29 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 14:29 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 14:29 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 14:29 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 14:29 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 14:29 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 14:29 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 14:29 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 14:29 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 14:29 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 14:29 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 14:29 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 14:29 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 14:29 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 14:29 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 14:29 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 14:29 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 14:29 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 14:29 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 14:29 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 20 of 32
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[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 14:29 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 14:29 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 14:29 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 14:2903/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 14:29 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 14:29 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 14:29 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 14:29 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 14:29 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 14:29 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 14:29 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 14:29 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 14:29 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 14:29 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 14:29 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 14:29 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 14:29 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 14:2903/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 14:29 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 14:29 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 14:29 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 14:29 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)70 %03/10/17 14:29 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)70 %03/10/17 14:29 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)81 %03/10/17 14:29 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)25 %03/10/17 14:29 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)36 %03/10/17 14:29 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)76 %03/10/17 14:29 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:10 67-64-125.0 10.0 1
Benzene ND ug/L 03/10/17 11:10 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/10/17 11:10 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/10/17 11:10 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/10/17 11:10 75-27-41.0 0.18 1
Bromoform ND ug/L 03/10/17 11:10 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/10/17 11:10 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/10/17 11:10 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/10/17 11:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/10/17 11:10 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/10/17 11:10 75-00-31.0 0.54 1
Chloroform ND ug/L 03/10/17 11:10 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/10/17 11:10 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/10/17 11:10 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/10/17 11:10 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 21 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:10 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/10/17 11:10 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/10/17 11:10 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/10/17 11:10 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/10/17 11:10 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/10/17 11:10 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/10/17 11:10 75-71-81.0 0.21 1
1,1-Dichloroethane 1.9 ug/L 03/10/17 11:10 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/10/17 11:10 107-06-21.0 0.24 1
1,1-Dichloroethene 2.6 ug/L 03/10/17 11:10 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 3.6 ug/L 03/10/17 11:10 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/10/17 11:10 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/10/17 11:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/10/17 11:10 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/10/17 11:10 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/10/17 11:10 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:10 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/10/17 11:10 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/10/17 11:10 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:10 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/10/17 11:10 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/10/17 11:10 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/10/17 11:10 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:10 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/10/17 11:10 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/10/17 11:10 91-20-31.0 0.24 1
Styrene ND ug/L 03/10/17 11:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:10 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:10 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/10/17 11:10 127-18-41.0 0.46 1
Toluene ND ug/L 03/10/17 11:10 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:10 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:10 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/10/17 11:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/10/17 11:10 79-00-51.0 0.29 1
Trichloroethene 3.5 ug/L 03/10/17 11:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/10/17 11:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/10/17 11:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/10/17 11:10 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/10/17 11:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/10/17 11:10 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/10/17 11:10 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/10/17 11:10 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 22 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)95 %03/10/17 11:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/10/17 11:10 17060-07-070-130 1
Toluene-d8 (S)100 %03/10/17 11:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 23 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351627
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950708
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/10/17 07:100.33
1,1,1-Trichloroethane ug/L ND 1.0 03/10/17 07:100.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/10/17 07:100.40
1,1,2-Trichloroethane ug/L ND 1.0 03/10/17 07:100.29
1,1-Dichloroethane ug/L ND 1.0 03/10/17 07:100.32
1,1-Dichloroethene ug/L ND 1.0 03/10/17 07:100.56
1,1-Dichloropropene ug/L ND 1.0 03/10/17 07:100.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/10/17 07:100.33
1,2,3-Trichloropropane ug/L ND 1.0 03/10/17 07:100.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/10/17 07:100.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/10/17 07:102.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/10/17 07:100.27
1,2-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.30
1,2-Dichloroethane ug/L ND 1.0 03/10/17 07:100.24
1,2-Dichloropropane ug/L ND 1.0 03/10/17 07:100.27
1,3-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.24
1,3-Dichloropropane ug/L ND 1.0 03/10/17 07:100.28
1,4-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.33
2,2-Dichloropropane ug/L ND 1.0 03/10/17 07:100.13
2-Butanone (MEK)ug/L ND 5.0 03/10/17 07:100.96
2-Chlorotoluene ug/L ND 1.0 03/10/17 07:100.35
2-Hexanone ug/L ND 5.0 03/10/17 07:100.46
4-Chlorotoluene ug/L ND 1.0 03/10/17 07:100.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/10/17 07:100.33
Acetone ug/L ND 25.0 03/10/17 07:1010.0
Benzene ug/L ND 1.0 03/10/17 07:100.25
Bromobenzene ug/L ND 1.0 03/10/17 07:100.30
Bromochloromethane ug/L ND 1.0 03/10/17 07:100.17
Bromodichloromethane ug/L ND 1.0 03/10/17 07:100.18
Bromoform ug/L ND 1.0 03/10/17 07:100.26
Bromomethane ug/L ND 2.0 03/10/17 07:100.29
Carbon tetrachloride ug/L ND 1.0 03/10/17 07:100.25
Chlorobenzene ug/L ND 1.0 03/10/17 07:100.23
Chloroethane ug/L ND 1.0 03/10/17 07:100.54
Chloroform ug/L ND 1.0 03/10/17 07:100.14
Chloromethane ug/L ND 1.0 03/10/17 07:100.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/10/17 07:100.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/10/17 07:100.13
Dibromochloromethane ug/L ND 1.0 03/10/17 07:100.21
Dibromomethane ug/L ND 1.0 03/10/17 07:100.21
Dichlorodifluoromethane ug/L ND 1.0 03/10/17 07:100.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 24 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950708
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/10/17 07:100.12
Ethylbenzene ug/L ND 1.0 03/10/17 07:100.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/10/17 07:100.71
m&p-Xylene ug/L ND 2.0 03/10/17 07:100.66
Methyl-tert-butyl ether ug/L ND 1.0 03/10/17 07:100.21
Methylene Chloride ug/L ND 2.0 03/10/17 07:100.97
Naphthalene ug/L ND 1.0 03/10/17 07:100.24
o-Xylene ug/L ND 1.0 03/10/17 07:100.23
p-Isopropyltoluene ug/L ND 1.0 03/10/17 07:100.31
Styrene ug/L ND 1.0 03/10/17 07:100.26
Tetrachloroethene ug/L ND 1.0 03/10/17 07:100.46
Toluene ug/L ND 1.0 03/10/17 07:100.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/10/17 07:100.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/10/17 07:100.26
Trichloroethene ug/L ND 1.0 03/10/17 07:100.47
Trichlorofluoromethane ug/L ND 1.0 03/10/17 07:100.20
Vinyl acetate ug/L ND 2.0 03/10/17 07:100.35
Vinyl chloride ug/L ND 1.0 03/10/17 07:100.62
Xylene (Total)ug/L ND 1.0 03/10/17 07:100.66
1,2-Dichloroethane-d4 (S)%100 70-130 03/10/17 07:10
4-Bromofluorobenzene (S)%97 70-130 03/10/17 07:10
Toluene-d8 (S)%102 70-130 03/10/17 07:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950709LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950710
1,1,1,2-Tetrachloroethane ug/L 51.750 103 70-13010050.1 3 30
1,1,1-Trichloroethane ug/L 51.950 104 70-13010150.7 2 30
1,1,2,2-Tetrachloroethane ug/L 51.750 103 70-13010150.7 2 30
1,1,2-Trichloroethane ug/L 50.750 101 70-13010251.0 1 30
1,1-Dichloroethane ug/L 50.350 101 70-13010049.8 1 30
1,1-Dichloroethene ug/L 54.650 109 70-13210552.7 4 30
1,1-Dichloropropene ug/L 54.250 108 70-13010753.4 1 30
1,2,3-Trichlorobenzene ug/L 51.750 103 70-13510251.2 1 30
1,2,3-Trichloropropane ug/L 51.150 102 70-13010250.8 1 30
1,2,4-Trichlorobenzene ug/L 52.550 105 70-13410351.3 2 30
1,2-Dibromo-3-chloropropane ug/L 52.350 105 70-13010653.2 2 30
1,2-Dibromoethane (EDB)ug/L 50.750 101 70-13010150.4 1 30
1,2-Dichlorobenzene ug/L 51.350 103 70-13010150.6 1 30
1,2-Dichloroethane ug/L 47.350 95 70-1309246.1 2 30
1,2-Dichloropropane ug/L 52.350 105 70-1309949.7 5 30
1,3-Dichlorobenzene ug/L 51.650 103 70-13010049.9 3 30
1,3-Dichloropropane ug/L 52.150 104 70-13010351.5 1 30
1,4-Dichlorobenzene ug/L 50.550 101 70-1309949.4 2 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 25 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950709LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950710
2,2-Dichloropropane ug/L 51.450 103 58-1459547.6 8 30
2-Butanone (MEK)ug/L 98.4100 98 70-145101101 3 30
2-Chlorotoluene ug/L 52.950 106 70-13010150.5 5 30
2-Hexanone ug/L 104100 104 70-144106106 1 30
4-Chlorotoluene ug/L 51.450 103 70-1309949.6 4 30
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-140101101 1 30
Acetone ug/L 104100 104 50-175109109 5 30
Benzene ug/L 53.350 107 70-13010351.6 3 30
Bromobenzene ug/L 52.050 104 70-13010150.3 3 30
Bromochloromethane ug/L 53.050 106 70-13010250.8 4 30
Bromodichloromethane ug/L 53.450 107 70-13010351.6 3 30
Bromoform ug/L 50.550 101 70-13010250.8 1 30
Bromomethane ug/L 34.450 69 54-1307135.4 3 30
Carbon tetrachloride ug/L 50.350 101 70-1329949.5 2 30
Chlorobenzene ug/L 51.550 103 70-13010150.4 2 30
Chloroethane ug/L 47.750 95 64-1349346.5 2 30
Chloroform ug/L 49.450 99 70-1309547.5 4 30
Chloromethane ug/L 41.550 83 64-1308341.6 0 30
cis-1,2-Dichloroethene ug/L 50.450 101 70-13110049.8 1 30
cis-1,3-Dichloropropene ug/L 52.650 105 70-13010251.1 3 30
Dibromochloromethane ug/L 52.150 104 70-13010251.2 2 30
Dibromomethane ug/L 49.850 100 70-1319648.2 3 30
Dichlorodifluoromethane ug/L 51.150 102 56-13010150.7 1 30
Diisopropyl ether ug/L 50.450 101 70-1309849.0 3 30
Ethylbenzene ug/L 53.050 106 70-13010351.5 3 30
Hexachloro-1,3-butadiene ug/L 52.650 105 70-13010250.9 3 30
m&p-Xylene ug/L 105100 105 70-130101101 4 30
Methyl-tert-butyl ether ug/L 52.150 104 70-13010451.8 1 30
Methylene Chloride ug/L 50.650 101 63-13010150.5 0 30
Naphthalene ug/L 53.950 108 70-13810753.4 1 30
o-Xylene ug/L 52.550 105 70-13010351.6 2 30
p-Isopropyltoluene ug/L 50.750 101 70-1309949.5 2 30
Styrene ug/L 53.950 108 70-13010452.1 3 30
Tetrachloroethene ug/L 50.950 102 70-1309949.4 3 30
Toluene ug/L 52.850 106 70-13010351.4 3 30
trans-1,2-Dichloroethene ug/L 53.250 106 70-13010652.8 1 30
trans-1,3-Dichloropropene ug/L 51.650 103 70-13210351.3 0 30
Trichloroethene ug/L 50.150 100 70-1309849.1 2 30
Trichlorofluoromethane ug/L 53.850 108 62-13310652.9 2 30
Vinyl acetate ug/L 105100 105 66-157106106 1 30
Vinyl chloride ug/L 45.850 92 50-1508944.7 2 30
Xylene (Total)ug/L 157150 105 70-130102153 3 30
1,2-Dichloroethane-d4 (S)%97 70-13094
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351633
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950722
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/10/17 12:001.9
1,2-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.2
1,3-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.1
1,4-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.2
1-Methylnaphthalene ug/L ND 10.0 03/10/17 12:000.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/10/17 12:001.6
2,4,5-Trichlorophenol ug/L ND 10.0 03/10/17 12:002.2
2,4,6-Trichlorophenol ug/L ND 10.0 03/10/17 12:001.9
2,4-Dichlorophenol ug/L ND 10.0 03/10/17 12:001.7
2,4-Dimethylphenol ug/L ND 10.0 03/10/17 12:002.2
2,4-Dinitrophenol ug/L ND 50.0 03/10/17 12:006.5
2,4-Dinitrotoluene ug/L ND 10.0 03/10/17 12:001.2
2,6-Dinitrotoluene ug/L ND 10.0 03/10/17 12:001.7
2-Chloronaphthalene ug/L ND 10.0 03/10/17 12:002.2
2-Chlorophenol ug/L ND 10.0 03/10/17 12:001.5
2-Methylnaphthalene ug/L ND 10.0 03/10/17 12:000.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/10/17 12:001.7
2-Nitroaniline ug/L ND 50.0 03/10/17 12:002.8
2-Nitrophenol ug/L ND 10.0 03/10/17 12:001.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/10/17 12:001.7
3,3'-Dichlorobenzidine ug/L ND 20.0 03/10/17 12:001.4
3-Nitroaniline ug/L ND 50.0 03/10/17 12:002.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/10/17 12:001.7
4-Bromophenylphenyl ether ug/L ND 10.0 03/10/17 12:001.3
4-Chloro-3-methylphenol ug/L ND 20.0 03/10/17 12:004.2
4-Chloroaniline ug/L ND 20.0 03/10/17 12:003.4
4-Chlorophenylphenyl ether ug/L ND 10.0 03/10/17 12:002.1
4-Nitroaniline ug/L ND 20.0 03/10/17 12:002.5
4-Nitrophenol ug/L ND 50.0 03/10/17 12:005.8
Acenaphthene ug/L ND 10.0 03/10/17 12:000.25
Acenaphthylene ug/L ND 10.0 03/10/17 12:000.21
Aniline ug/L ND 10.0 03/10/17 12:001.3
Anthracene ug/L ND 10.0 03/10/17 12:000.14
Benzo(a)anthracene ug/L ND 10.0 03/10/17 12:000.33
Benzo(a)pyrene ug/L ND 10.0 03/10/17 12:000.30
Benzo(b)fluoranthene ug/L ND 10.0 03/10/17 12:000.28
Benzo(g,h,i)perylene ug/L ND 10.0 03/10/17 12:000.38
Benzo(k)fluoranthene ug/L ND 10.0 03/10/17 12:000.43
Benzoic Acid ug/L ND 50.0 03/10/17 12:0011.1
Benzyl alcohol ug/L ND 20.0 03/10/17 12:003.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/10/17 12:001.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 27 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950722
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 03/10/17 12:001.5
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/10/17 12:000.85
Butylbenzylphthalate ug/L ND 10.0 03/10/17 12:000.75
Chrysene ug/L ND 10.0 03/10/17 12:000.21
Di-n-butylphthalate ug/L ND 10.0 03/10/17 12:001.1
Di-n-octylphthalate ug/L ND 10.0 03/10/17 12:000.86
Dibenz(a,h)anthracene ug/L ND 10.0 03/10/17 12:000.55
Dibenzofuran ug/L ND 10.0 03/10/17 12:001.8
Diethylphthalate ug/L ND 10.0 03/10/17 12:001.3
Dimethylphthalate ug/L ND 10.0 03/10/17 12:001.5
Fluoranthene ug/L ND 10.0 03/10/17 12:000.21
Fluorene ug/L ND 10.0 03/10/17 12:000.21
Hexachloro-1,3-butadiene ug/L ND 10.0 03/10/17 12:001.8
Hexachlorobenzene ug/L ND 10.0 03/10/17 12:001.1
Hexachlorocyclopentadiene ug/L ND 10.0 03/10/17 12:001.8
Hexachloroethane ug/L ND 10.0 03/10/17 12:001.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/10/17 12:000.29
Isophorone ug/L ND 10.0 03/10/17 12:001.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/10/17 12:002.1
N-Nitrosodimethylamine ug/L ND 10.0 03/10/17 12:001.3
N-Nitrosodiphenylamine ug/L ND 10.0 03/10/17 12:001.3
Naphthalene ug/L ND 10.0 03/10/17 12:000.34
Nitrobenzene ug/L ND 10.0 03/10/17 12:001.7
Pentachlorophenol ug/L ND 25.0 03/10/17 12:002.3
Phenanthrene ug/L ND 10.0 03/10/17 12:000.22
Phenol ug/L ND 10.0 03/10/17 12:001.7
Pyrene ug/L ND 10.0 03/10/17 12:000.19
2,4,6-Tribromophenol (S)%78 27-110 03/10/17 12:00
2-Fluorobiphenyl (S)%67 27-110 03/10/17 12:00
2-Fluorophenol (S)%37 12-110 03/10/17 12:00
Nitrobenzene-d5 (S)%70 21-110 03/10/17 12:00
Phenol-d6 (S)%21 10-110 03/10/17 12:00
Terphenyl-d14 (S)%88 31-107 03/10/17 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
1,2,4-Trichlorobenzene ug/L 15.025 60 31-1206015.1 1 30
1,2-Dichlorobenzene ug/L 14.725 59 38-1205714.3 2 30
1,3-Dichlorobenzene ug/L 13.325 53 30-1225714.1 6 30
1,4-Dichlorobenzene ug/L 13.625 54 37-1205413.5 0 30
1-Methylnaphthalene ug/L 17.325 69 34-1136917.2 0 30
2,2'-Oxybis(1-chloropropane)ug/L 16.825 67 18-1206115.4 9 30
2,4,5-Trichlorophenol ug/L 16.825 67 43-1136315.8 6 30
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
2,4,6-Trichlorophenol ug/L 18.625 75 42-1207418.5 1 30
2,4-Dichlorophenol ug/L 17.625 71 30-1206817.1 3 30
2,4-Dimethylphenol ug/L 19.625 78 29-1117518.8 4 30
2,4-Dinitrophenol ug/L 108125 86 19-13291114 6 30
2,4-Dinitrotoluene ug/L 23.725 95 58-1289122.7 5 30
2,6-Dinitrotoluene ug/L 25.125 100 54-1299924.6 2 30
2-Chloronaphthalene ug/L 20.725 83 43-1178020.1 3 30
2-Chlorophenol ug/L 15.325 61 37-1205914.7 4 30
2-Methylnaphthalene ug/L 17.425 70 33-1207318.2 4 30
2-Methylphenol(o-Cresol)ug/L 12.625 50 31-1204611.5 9 30
2-Nitroaniline ug/L 35.3J50 71 48-1217035.0J 30
2-Nitrophenol ug/L 19.025 76 25-1168020.1 6 30
3&4-Methylphenol(m&p Cresol)ug/L 27.825 111 23-1209724.3 13 30
3,3'-Dichlorobenzidine ug/L 39.950 80 10-1547436.8 8 30
3-Nitroaniline ug/L 40.6J50 81 43-1157939.3J 30
4,6-Dinitro-2-methylphenol ug/L 43.550 87 44-1248341.3 5 30
4-Bromophenylphenyl ether ug/L 18.925 76 34-1137418.6 2 30
4-Chloro-3-methylphenol ug/L 39.150 78 31-1107135.4 10 30
4-Chloroaniline ug/L 38.250 76 20-1207135.7 7 30
4-Chlorophenylphenyl ether ug/L 18.425 74 34-1167117.7 4 30
4-Nitroaniline ug/L 42.050 84 46-1288140.3 4 30
4-Nitrophenol ug/L 42.2J125 34 11-1203442.5J 30
Acenaphthene ug/L 19.325 77 48-1147518.6 4 30
Acenaphthylene ug/L 19.225 77 48-1127418.4 4 30
Aniline ug/L 12.125 48 26-1204411.1 9 30
Anthracene ug/L 20.125 80 57-1187418.6 8 30
Benzo(a)anthracene ug/L 20.125 81 56-1217418.5 9 30
Benzo(a)pyrene ug/L 19.425 77 55-1277418.4 5 30
Benzo(b)fluoranthene ug/L 21.225 85 53-1287819.6 8 30
Benzo(g,h,i)perylene ug/L 21.325 85 54-1258320.7 3 30
Benzo(k)fluoranthene ug/L 21.325 85 51-1237819.5 9 30
Benzoic Acid ug/L 32.0J125 26 10-1202531.9J 30
Benzyl alcohol ug/L 27.750 55 27-1204924.5 12 30
bis(2-Chloroethoxy)methane ug/L 18.525 74 32-1207117.9 3 30
bis(2-Chloroethyl) ether ug/L 16.925 68 33-1116015.0 12 30
bis(2-Ethylhexyl)phthalate ug/L 23.425 94 50-1458721.9 7 30
Butylbenzylphthalate ug/L 24.425 98 54-1389223.0 6 30
Chrysene ug/L 20.425 82 58-1277719.2 6 30
Di-n-butylphthalate ug/L 23.125 93 56-1258721.8 6 30
Di-n-octylphthalate ug/L 20.425 82 50-1347919.8 3 30
Dibenz(a,h)anthracene ug/L 22.125 89 53-1298521.3 4 30
Dibenzofuran ug/L 18.625 74 45-1207418.4 1 30
Diethylphthalate ug/L 22.225 89 53-1208521.3 4 30
Dimethylphthalate ug/L 21.225 85 55-1168320.8 2 30
Fluoranthene ug/L 21.425 86 57-1258020.0 7 30
Fluorene ug/L 20.025 80 53-1187619.1 5 30
Hexachloro-1,3-butadiene ug/L 13.725 55 23-1206014.9 8 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 29 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
Hexachlorobenzene ug/L 19.625 79 49-1167518.8 4 30
Hexachlorocyclopentadiene ug/L 14.325 57 26-1586015.0 5 30
Hexachloroethane ug/L 12.825 51 30-1145714.3 11 30
Indeno(1,2,3-cd)pyrene ug/L 22.925 91 55-1288521.3 7 30
Isophorone ug/L 21.825 87 31-1188220.5 6 30
N-Nitroso-di-n-propylamine ug/L 16.925 68 32-1196315.8 7 30
N-Nitrosodimethylamine ug/L 10.125 40 13-1204511.3 11 30
N-Nitrosodiphenylamine ug/L 19.625 78 43-1207318.4 6 30
Naphthalene ug/L 17.625 70 32-1207017.6 0 30
Nitrobenzene ug/L 20.225 81 33-1108020.1 1 30
Pentachlorophenol ug/L 44.050 88 10-1378040.1 9 30
Phenanthrene ug/L 20.425 82 57-1177618.9 8 30
Phenol ug/L 8.5J25 34 10-120307.5J 30
Pyrene ug/L 18.425 74 55-1226917.2 7 30
2,4,6-Tribromophenol (S)%89 27-11080
2-Fluorobiphenyl (S)%72 27-11068
2-Fluorophenol (S)%39 12-11036
Nitrobenzene-d5 (S)%72 21-11069
Phenol-d6 (S)%27 10-11023
Terphenyl-d14 (S)%76 31-10770
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 30 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92332882001 351633 3516770309171049W1EPA 3510 EPA 8270
92332882002 351633 3516770309171139W2EPA 3510 EPA 8270
92332882003 351633 3516770309171320DSEPA 3510 EPA 8270
92332882004 351633 3516770309171344USEPA 3510 EPA 8270
92332882001 3516270309171049W1EPA 8260
92332882002 3516270309171139W2EPA 8260
92332882003 3516270309171320DSEPA 8260
92332882004 3516270309171344USEPA 8260
REPORT OF LABORATORY ANALYSIS
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[phone]
file:///C/Users/tamechum/Desktop/Harwell%20Estates%20Mobile%20Home%20Pakr/Laserfiche/Harwell/ATT00001.htm[4/27/2018 1:57:40 PM]
1
Beverly, Trudy
From:Beverly, Trudy
Sent:Monday, March 13, 2017 7:33 AM
To:Eichinger, Kevin
Cc:Bateson, James; Day, Collin; Jesneck, Charlotte; Zinn, Harry; Ramey, David E
Subject:RE: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results
Thank you, Kevin.

From: Eichinger, Kevin [mailto:[e-mail]]
Sent: Friday, March 10, 2017 9:22 PM
To: Beverly, Trudy <[e-mail]>
Cc: Bateson, James <[e-mail]>
Subject: Fwd: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results

Results of out sampling. Sending the summary table next.

Begin forwarded message:
From: "Taylor, Todd" <[e-mail]>
Date: March 10, 2017 at 17:21:05 EST
To: Kevin Eichinger <[e-mail]>
Cc: "Vasser, Bryan" <[e-mail]>
Subject: PRELIMINARY results (Harwell Rd Private Well TDD 01-076 )results
Hello,

Attached are the preliminary results for VOC, SVOC the metals will follow when complete. When the
samples are QC’d I will forward as well.

Regards,
Todd

Todd Taylor|ENV.SCI.V
Direct: 615.992-5556 |
[e-mail]
Tetra Tech Inc. |
712 Melrose Avenue | Nashville, TN 37211 | www.tetratech.com
PLEASE NOTE: This message, including any attachments, may include privileged, confidential and/or
inside information. Any distribution or use of this communication by anyone other than the intended
recipient is strictly prohibited and may be unlawful. If you are not the intended recipient, please notify the
sender by replying to this message and then delete it from your system.

#=CL#
March 10, 2017
LIMS USE: FR Prelim - JESSICA
LIMS OBJECT ID: 92332882
92332882
Project:
Pace Project No.:
RE:
Jessica Vickers
Tetra Tech
950 South 4th Street
Baldwyn, MS 38824
HARWELL RD PRIVA 103X902701067
Dear Jessica Vickers:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Page 1 of 32
Pace Analytical Services, LLC
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#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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SAMPLE SUMMARY
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID Matrix Date Collected Date Received
92332882001 0309171049W1 Water 03/09/17 10:49 03/09/17 15:07
92332882002 0309171139W2 Water 03/09/17 11:39 03/09/17 15:07
92332882003 0309171320DS Water 03/09/17 13:20 03/09/17 15:07
92332882004 0309171344US Water 03/09/17 13:44 03/09/17 15:07
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92332882001 0309171049W1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882002 0309171139W2 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882003 0309171320DS EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92332882004 0309171344US EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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SUMMARY OF DETECTION
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92332882001 0309171049W1
1,1-Dichloroethene 22.3 ug/L 03/10/17 11:2710.0EPA 8260
cis-1,2-Dichloroethene 15.5 ug/L 03/10/17 11:2710.0EPA 8260
Tetrachloroethene 29.4 ug/L 03/10/17 11:2710.0EPA 8260
Trichloroethene 944 ug/L 03/10/17 11:2710.0EPA 8260
92332882002 0309171139W2
1,1-Dichloroethane 98.3 ug/L 03/10/17 11:444.0EPA 8260
1,1-Dichloroethene 141 ug/L 03/10/17 11:444.0EPA 8260
cis-1,2-Dichloroethene 194 ug/L 03/10/17 11:444.0EPA 8260
trans-1,2-Dichloroethene 2.4J ug/L 03/10/17 11:444.0EPA 8260
Tetrachloroethene 10.9 ug/L 03/10/17 11:444.0EPA 8260
1,1,1-Trichloroethane 5.6 ug/L 03/10/17 11:444.0EPA 8260
Trichloroethene 409 ug/L 03/10/17 11:444.0EPA 8260
92332882003 0309171320DS
1,1-Dichloroethane 4.8 ug/L 03/10/17 10:531.0EPA 8260
1,1-Dichloroethene 7.9 ug/L 03/10/17 10:531.0EPA 8260
cis-1,2-Dichloroethene 9.1 ug/L 03/10/17 10:531.0EPA 8260
Trichloroethene 14.1 ug/L 03/10/17 10:531.0EPA 8260
92332882004 0309171344US
1,1-Dichloroethane 1.9 ug/L 03/10/17 11:101.0EPA 8260
1,1-Dichloroethene 2.6 ug/L 03/10/17 11:101.0EPA 8260
cis-1,2-Dichloroethene 3.6 ug/L 03/10/17 11:101.0EPA 8260
Trichloroethene 3.5 ug/L 03/10/17 11:101.0EPA 8260
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Method:
Client:Tetra Tech EMI
EPA 8270
Date:March 10, 2017
Description:8270 MSSV Semivolatile Organic
General Information:
4 samples were analyzed for EPA 8270. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Method:
Client:Tetra Tech EMI
EPA 8260
Date:March 10, 2017
Description:8260 MSV Low Level
General Information:
4 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:03 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:03 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:03 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:03 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:03 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:03 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:03 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:03 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:03 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:03 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:03 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:03 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:03 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:03 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:03 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:03 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:03 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:03 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:03 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:03 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:03 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:03 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:03 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:03 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:03 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:03 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:03 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:03 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:03 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:03 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:03 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:03 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:03 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:03 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:03 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:03 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:03 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:03 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:03 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:03 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:03 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:03 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:03 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:03 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:03 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:03 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:03 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:03 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:03 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:0303/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:03 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:03 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:03 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:03 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:03 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:03 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:03 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:03 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:03 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:03 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:03 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:03 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:03 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:0303/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:03 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:03 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:03 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:03 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)69 %03/10/17 12:03 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)69 %03/10/17 12:03 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)82 %03/10/17 12:03 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)23 %03/10/17 12:03 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)33 %03/10/17 12:03 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)77 %03/10/17 12:03 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:27 67-64-125010010
Benzene ND ug/L 03/10/17 11:27 71-43-210.0 2.5 10
Bromobenzene ND ug/L 03/10/17 11:27 108-86-110.0 3.0 10
Bromochloromethane ND ug/L 03/10/17 11:27 74-97-510.0 1.7 10
Bromodichloromethane ND ug/L 03/10/17 11:27 75-27-410.0 1.8 10
Bromoform ND ug/L 03/10/17 11:27 75-25-210.0 2.6 10
Bromomethane ND ug/L 03/10/17 11:27 74-83-920.0 2.9 10
2-Butanone (MEK)ND ug/L 03/10/17 11:27 78-93-350.0 9.6 10
Carbon tetrachloride ND ug/L 03/10/17 11:27 56-23-510.0 2.5 10
Chlorobenzene ND ug/L 03/10/17 11:27 108-90-710.0 2.3 10
Chloroethane ND ug/L 03/10/17 11:27 75-00-310.0 5.4 10
Chloroform ND ug/L 03/10/17 11:27 67-66-310.0 1.4 10
Chloromethane ND ug/L 03/10/17 11:27 74-87-310.0 1.1 10
2-Chlorotoluene ND ug/L 03/10/17 11:27 95-49-810.0 3.5 10
4-Chlorotoluene ND ug/L 03/10/17 11:27 106-43-410.0 3.1 10
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:27 96-12-820.0 20.0 10
Dibromochloromethane ND ug/L 03/10/17 11:27 124-48-110.0 2.1 10
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:27 106-93-410.0 2.7 10
Dibromomethane ND ug/L 03/10/17 11:27 74-95-310.0 2.1 10
1,2-Dichlorobenzene ND ug/L 03/10/17 11:27 95-50-110.0 3.0 10
1,3-Dichlorobenzene ND ug/L 03/10/17 11:27 541-73-110.0 2.4 10
1,4-Dichlorobenzene ND ug/L 03/10/17 11:27 106-46-710.0 3.3 10
Dichlorodifluoromethane ND ug/L 03/10/17 11:27 75-71-810.0 2.1 10
1,1-Dichloroethane ND ug/L 03/10/17 11:27 75-34-310.0 3.2 10
1,2-Dichloroethane ND ug/L 03/10/17 11:27 107-06-210.0 2.4 10
1,1-Dichloroethene 22.3 ug/L 03/10/17 11:27 75-35-410.0 5.6 10
cis-1,2-Dichloroethene 15.5 ug/L 03/10/17 11:27 156-59-210.0 1.9 10
trans-1,2-Dichloroethene ND ug/L 03/10/17 11:27 156-60-510.0 4.9 10
1,2-Dichloropropane ND ug/L 03/10/17 11:27 78-87-510.0 2.7 10
1,3-Dichloropropane ND ug/L 03/10/17 11:27 142-28-910.0 2.8 10
2,2-Dichloropropane ND ug/L 03/10/17 11:27 594-20-710.0 1.3 10
1,1-Dichloropropene ND ug/L 03/10/17 11:27 563-58-610.0 4.9 10
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:27 10061-01-510.0 1.3 10
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:27 10061-02-610.0 2.6 10
Diisopropyl ether ND ug/L 03/10/17 11:27 108-20-310.0 1.2 10
Ethylbenzene ND ug/L 03/10/17 11:27 100-41-410.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:27 87-68-310.0 7.1 10
2-Hexanone ND ug/L 03/10/17 11:27 591-78-650.0 4.6 10
p-Isopropyltoluene ND ug/L 03/10/17 11:27 99-87-610.0 3.1 10
Methylene Chloride ND ug/L 03/10/17 11:27 75-09-220.0 9.7 10
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:27 108-10-150.0 3.3 10
Methyl-tert-butyl ether ND ug/L 03/10/17 11:27 1634-04-410.0 2.1 10
Naphthalene ND ug/L 03/10/17 11:27 91-20-310.0 2.4 10
Styrene ND ug/L 03/10/17 11:27 100-42-510.0 2.6 10
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:27 630-20-610.0 3.3 10
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:27 79-34-510.0 4.0 10
Tetrachloroethene 29.4 ug/L 03/10/17 11:27 127-18-410.0 4.6 10
Toluene ND ug/L 03/10/17 11:27 108-88-310.0 2.6 10
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:27 87-61-610.0 3.3 10
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:27 120-82-110.0 3.5 10
1,1,1-Trichloroethane ND ug/L 03/10/17 11:27 71-55-610.0 4.8 10
1,1,2-Trichloroethane ND ug/L 03/10/17 11:27 79-00-510.0 2.9 10
Trichloroethene 944 ug/L 03/10/17 11:27 79-01-610.0 4.7 10
Trichlorofluoromethane ND ug/L 03/10/17 11:27 75-69-410.0 2.0 10
1,2,3-Trichloropropane ND ug/L 03/10/17 11:27 96-18-410.0 4.1 10
Vinyl acetate ND ug/L 03/10/17 11:27 108-05-420.0 3.5 10
Vinyl chloride ND ug/L 03/10/17 11:27 75-01-410.0 6.2 10
Xylene (Total)ND ug/L 03/10/17 11:27 1330-20-710.0 6.6 10
m&p-Xylene ND ug/L 03/10/17 11:27 179601-23-120.0 6.6 10
o-Xylene ND ug/L 03/10/17 11:27 95-47-610.0 2.3 10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 10 of 32
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171049W1 Lab ID:92332882001 Collected:03/09/17 10:49 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)97 %03/10/17 11:27 460-00-470-130 10
1,2-Dichloroethane-d4 (S)99 %03/10/17 11:27 17060-07-070-130 10
Toluene-d8 (S)100 %03/10/17 11:27 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 11 of 32
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:31 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:31 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:31 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:31 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:31 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:31 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:31 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:31 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:31 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:31 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:31 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:31 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:31 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:31 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:31 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:31 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:31 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:31 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:31 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:31 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:31 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:31 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:31 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:31 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:31 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:31 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:31 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:31 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:31 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:31 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:31 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:31 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:31 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:31 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:31 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:31 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:31 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:31 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:31 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:31 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:31 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:31 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:31 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:31 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:31 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:31 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 12 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:31 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:31 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:31 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:3103/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:31 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:31 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:31 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:31 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:31 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:31 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:31 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:31 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:31 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:31 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:31 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:31 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:31 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:3103/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:31 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:31 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:31 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:31 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)67 %03/10/17 12:31 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)66 %03/10/17 12:31 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)79 %03/10/17 12:31 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)20 %03/10/17 12:31 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)31 %03/10/17 12:31 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)73 %03/10/17 12:31 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:44 67-64-110040.0 4
Benzene ND ug/L 03/10/17 11:44 71-43-24.0 1.0 4
Bromobenzene ND ug/L 03/10/17 11:44 108-86-14.0 1.2 4
Bromochloromethane ND ug/L 03/10/17 11:44 74-97-54.0 0.68 4
Bromodichloromethane ND ug/L 03/10/17 11:44 75-27-44.0 0.72 4
Bromoform ND ug/L 03/10/17 11:44 75-25-24.0 1.0 4
Bromomethane ND ug/L 03/10/17 11:44 74-83-98.0 1.2 4
2-Butanone (MEK)ND ug/L 03/10/17 11:44 78-93-320.0 3.8 4
Carbon tetrachloride ND ug/L 03/10/17 11:44 56-23-54.0 1.0 4
Chlorobenzene ND ug/L 03/10/17 11:44 108-90-74.0 0.92 4
Chloroethane ND ug/L 03/10/17 11:44 75-00-34.0 2.2 4
Chloroform ND ug/L 03/10/17 11:44 67-66-34.0 0.56 4
Chloromethane ND ug/L 03/10/17 11:44 74-87-34.0 0.44 4
2-Chlorotoluene ND ug/L 03/10/17 11:44 95-49-84.0 1.4 4
4-Chlorotoluene ND ug/L 03/10/17 11:44 106-43-44.0 1.2 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 13 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:44 96-12-88.0 8.0 4
Dibromochloromethane ND ug/L 03/10/17 11:44 124-48-14.0 0.84 4
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:44 106-93-44.0 1.1 4
Dibromomethane ND ug/L 03/10/17 11:44 74-95-34.0 0.84 4
1,2-Dichlorobenzene ND ug/L 03/10/17 11:44 95-50-14.0 1.2 4
1,3-Dichlorobenzene ND ug/L 03/10/17 11:44 541-73-14.0 0.96 4
1,4-Dichlorobenzene ND ug/L 03/10/17 11:44 106-46-74.0 1.3 4
Dichlorodifluoromethane ND ug/L 03/10/17 11:44 75-71-84.0 0.84 4
1,1-Dichloroethane 98.3 ug/L 03/10/17 11:44 75-34-34.0 1.3 4
1,2-Dichloroethane ND ug/L 03/10/17 11:44 107-06-24.0 0.96 4
1,1-Dichloroethene 141 ug/L 03/10/17 11:44 75-35-44.0 2.2 4
cis-1,2-Dichloroethene 194 ug/L 03/10/17 11:44 156-59-24.0 0.76 4
trans-1,2-Dichloroethene 2.4J ug/L 03/10/17 11:44 156-60-54.0 2.0 4
1,2-Dichloropropane ND ug/L 03/10/17 11:44 78-87-54.0 1.1 4
1,3-Dichloropropane ND ug/L 03/10/17 11:44 142-28-94.0 1.1 4
2,2-Dichloropropane ND ug/L 03/10/17 11:44 594-20-74.0 0.52 4
1,1-Dichloropropene ND ug/L 03/10/17 11:44 563-58-64.0 2.0 4
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:44 10061-01-54.0 0.52 4
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:44 10061-02-64.0 1.0 4
Diisopropyl ether ND ug/L 03/10/17 11:44 108-20-34.0 0.48 4
Ethylbenzene ND ug/L 03/10/17 11:44 100-41-44.0 1.2 4
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:44 87-68-34.0 2.8 4
2-Hexanone ND ug/L 03/10/17 11:44 591-78-620.0 1.8 4
p-Isopropyltoluene ND ug/L 03/10/17 11:44 99-87-64.0 1.2 4
Methylene Chloride ND ug/L 03/10/17 11:44 75-09-28.0 3.9 4
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:44 108-10-120.0 1.3 4
Methyl-tert-butyl ether ND ug/L 03/10/17 11:44 1634-04-44.0 0.84 4
Naphthalene ND ug/L 03/10/17 11:44 91-20-34.0 0.96 4
Styrene ND ug/L 03/10/17 11:44 100-42-54.0 1.0 4
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:44 630-20-64.0 1.3 4
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:44 79-34-54.0 1.6 4
Tetrachloroethene 10.9 ug/L 03/10/17 11:44 127-18-44.0 1.8 4
Toluene ND ug/L 03/10/17 11:44 108-88-34.0 1.0 4
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:44 87-61-64.0 1.3 4
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:44 120-82-14.0 1.4 4
1,1,1-Trichloroethane 5.6 ug/L 03/10/17 11:44 71-55-64.0 1.9 4
1,1,2-Trichloroethane ND ug/L 03/10/17 11:44 79-00-54.0 1.2 4
Trichloroethene 409 ug/L 03/10/17 11:44 79-01-64.0 1.9 4
Trichlorofluoromethane ND ug/L 03/10/17 11:44 75-69-44.0 0.80 4
1,2,3-Trichloropropane ND ug/L 03/10/17 11:44 96-18-44.0 1.6 4
Vinyl acetate ND ug/L 03/10/17 11:44 108-05-48.0 1.4 4
Vinyl chloride ND ug/L 03/10/17 11:44 75-01-44.0 2.5 4
Xylene (Total)ND ug/L 03/10/17 11:44 1330-20-74.0 2.6 4
m&p-Xylene ND ug/L 03/10/17 11:44 179601-23-18.0 2.6 4
o-Xylene ND ug/L 03/10/17 11:44 95-47-64.0 0.92 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 14 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171139W2 Lab ID:92332882002 Collected:03/09/17 11:39 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)97 %03/10/17 11:44 460-00-470-130 4
1,2-Dichloroethane-d4 (S)102 %03/10/17 11:44 17060-07-070-130 4
Toluene-d8 (S)100 %03/10/17 11:44 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 15 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 12:59 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 12:59 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 12:59 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 12:59 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 12:59 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 12:59 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 12:59 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 12:59 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 12:59 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 12:59 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 12:59 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 12:59 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 12:59 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 12:59 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 12:59 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 12:59 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 12:59 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 12:59 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 12:59 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 12:59 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 12:59 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 12:59 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 12:59 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 12:59 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 12:59 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 12:59 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 12:59 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 12:59 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 12:59 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 12:59 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 12:59 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 12:59 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 12:59 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 12:59 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 12:59 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 12:59 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 12:59 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 12:59 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 12:59 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 12:59 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 12:59 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 12:59 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 12:59 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 12:59 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 12:59 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 12:59 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 16 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 12:59 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 12:59 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 12:59 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 12:5903/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 12:59 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 12:59 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 12:59 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 12:59 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 12:59 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 12:59 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 12:59 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 12:59 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 12:59 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 12:59 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 12:59 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 12:59 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 12:59 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 12:5903/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 12:59 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 12:59 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 12:59 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 12:59 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)69 %03/10/17 12:59 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)70 %03/10/17 12:59 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)78 %03/10/17 12:59 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)22 %03/10/17 12:59 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)34 %03/10/17 12:59 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)74 %03/10/17 12:59 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 10:53 67-64-125.0 10.0 1
Benzene ND ug/L 03/10/17 10:53 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/10/17 10:53 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/10/17 10:53 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/10/17 10:53 75-27-41.0 0.18 1
Bromoform ND ug/L 03/10/17 10:53 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/10/17 10:53 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/10/17 10:53 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/10/17 10:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/10/17 10:53 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/10/17 10:53 75-00-31.0 0.54 1
Chloroform ND ug/L 03/10/17 10:53 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/10/17 10:53 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/10/17 10:53 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/10/17 10:53 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 17 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 10:53 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/10/17 10:53 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 10:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/10/17 10:53 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/10/17 10:53 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/10/17 10:53 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/10/17 10:53 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/10/17 10:53 75-71-81.0 0.21 1
1,1-Dichloroethane 4.8 ug/L 03/10/17 10:53 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/10/17 10:53 107-06-21.0 0.24 1
1,1-Dichloroethene 7.9 ug/L 03/10/17 10:53 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 9.1 ug/L 03/10/17 10:53 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/10/17 10:53 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/10/17 10:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/10/17 10:53 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/10/17 10:53 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/10/17 10:53 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/10/17 10:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/10/17 10:53 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/10/17 10:53 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/10/17 10:53 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 10:53 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/10/17 10:53 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/10/17 10:53 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/10/17 10:53 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 10:53 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/10/17 10:53 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/10/17 10:53 91-20-31.0 0.24 1
Styrene ND ug/L 03/10/17 10:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 10:53 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 10:53 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/10/17 10:53 127-18-41.0 0.46 1
Toluene ND ug/L 03/10/17 10:53 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/10/17 10:53 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 10:53 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/10/17 10:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/10/17 10:53 79-00-51.0 0.29 1
Trichloroethene 14.1 ug/L 03/10/17 10:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/10/17 10:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/10/17 10:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/10/17 10:53 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/10/17 10:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/10/17 10:53 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/10/17 10:53 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/10/17 10:53 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 18 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171320DS Lab ID:92332882003 Collected:03/09/17 13:20 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)98 %03/10/17 10:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %03/10/17 10:53 17060-07-070-130 1
Toluene-d8 (S)101 %03/10/17 10:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 19 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/10/17 14:29 83-32-903/10/17 08:3810.0 0.25 1
Acenaphthylene ND ug/L 03/10/17 14:29 208-96-803/10/17 08:3810.0 0.21 1
Aniline ND ug/L 03/10/17 14:29 62-53-303/10/17 08:3810.0 1.3 1
Anthracene ND ug/L 03/10/17 14:29 120-12-703/10/17 08:3810.0 0.14 1
Benzo(a)anthracene ND ug/L 03/10/17 14:29 56-55-303/10/17 08:3810.0 0.33 1
Benzo(a)pyrene ND ug/L 03/10/17 14:29 50-32-803/10/17 08:3810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 03/10/17 14:29 205-99-203/10/17 08:3810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 03/10/17 14:29 191-24-203/10/17 08:3810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 03/10/17 14:29 207-08-903/10/17 08:3810.0 0.43 1
Benzoic Acid ND ug/L 03/10/17 14:29 65-85-003/10/17 08:3850.0 11.1 1
Benzyl alcohol ND ug/L 03/10/17 14:29 100-51-603/10/17 08:3820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 03/10/17 14:29 101-55-303/10/17 08:3810.0 1.3 1
Butylbenzylphthalate ND ug/L 03/10/17 14:29 85-68-703/10/17 08:3810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 03/10/17 14:29 59-50-703/10/17 08:3820.0 4.2 1
4-Chloroaniline ND ug/L 03/10/17 14:29 106-47-803/10/17 08:3820.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/17 14:29 111-91-103/10/17 08:3810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 03/10/17 14:29 111-44-403/10/17 08:3810.0 1.5 1
2-Chloronaphthalene ND ug/L 03/10/17 14:29 91-58-703/10/17 08:3810.0 2.2 1
2-Chlorophenol ND ug/L 03/10/17 14:29 95-57-803/10/17 08:3810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 03/10/17 14:29 7005-72-303/10/17 08:3810.0 2.1 1
Chrysene ND ug/L 03/10/17 14:29 218-01-903/10/17 08:3810.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 03/10/17 14:29 53-70-303/10/17 08:3810.0 0.55 1
Dibenzofuran ND ug/L 03/10/17 14:29 132-64-903/10/17 08:3810.0 1.8 1
1,2-Dichlorobenzene ND ug/L 03/10/17 14:29 95-50-103/10/17 08:3810.0 1.2 1
1,3-Dichlorobenzene ND ug/L 03/10/17 14:29 541-73-103/10/17 08:3810.0 1.1 1
1,4-Dichlorobenzene ND ug/L 03/10/17 14:29 106-46-703/10/17 08:3810.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 03/10/17 14:29 91-94-103/10/17 08:3820.0 1.4 1
2,4-Dichlorophenol ND ug/L 03/10/17 14:29 120-83-203/10/17 08:3810.0 1.7 1
Diethylphthalate ND ug/L 03/10/17 14:29 84-66-203/10/17 08:3810.0 1.3 1
2,4-Dimethylphenol ND ug/L 03/10/17 14:29 105-67-903/10/17 08:3810.0 2.2 1
Dimethylphthalate ND ug/L 03/10/17 14:29 131-11-303/10/17 08:3810.0 1.5 1
Di-n-butylphthalate ND ug/L 03/10/17 14:29 84-74-203/10/17 08:3810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/17 14:29 534-52-103/10/17 08:3820.0 1.7 1
2,4-Dinitrophenol ND ug/L 03/10/17 14:29 51-28-503/10/17 08:3850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 03/10/17 14:29 121-14-203/10/17 08:3810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 03/10/17 14:29 606-20-203/10/17 08:3810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/17 14:29 117-84-003/10/17 08:3810.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/17 14:29 117-81-703/10/17 08:386.0 0.85 1
Fluoranthene ND ug/L 03/10/17 14:29 206-44-003/10/17 08:3810.0 0.21 1
Fluorene ND ug/L 03/10/17 14:29 86-73-703/10/17 08:3810.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 14:29 87-68-303/10/17 08:3810.0 1.8 1
Hexachlorobenzene ND ug/L 03/10/17 14:29 118-74-103/10/17 08:3810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 03/10/17 14:29 77-47-403/10/17 08:3810.0 1.8 1
Hexachloroethane ND ug/L 03/10/17 14:29 67-72-103/10/17 08:3810.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/17 14:29 193-39-503/10/17 08:3810.0 0.29 1
Isophorone ND ug/L 03/10/17 14:29 78-59-103/10/17 08:3810.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 20 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/10/17 14:29 90-12-003/10/17 08:3810.0 0.32 1
2-Methylnaphthalene ND ug/L 03/10/17 14:29 91-57-603/10/17 08:3810.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/17 14:29 95-48-703/10/17 08:3810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/17 14:2903/10/17 08:3810.0 1.7 1
Naphthalene ND ug/L 03/10/17 14:29 91-20-303/10/17 08:3810.0 0.34 1
2-Nitroaniline ND ug/L 03/10/17 14:29 88-74-403/10/17 08:3850.0 2.8 1
3-Nitroaniline ND ug/L 03/10/17 14:29 99-09-203/10/17 08:3850.0 2.4 1
4-Nitroaniline ND ug/L 03/10/17 14:29 100-01-603/10/17 08:3820.0 2.5 1
Nitrobenzene ND ug/L 03/10/17 14:29 98-95-303/10/17 08:3810.0 1.7 1
2-Nitrophenol ND ug/L 03/10/17 14:29 88-75-503/10/17 08:3810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/17 14:29 100-02-703/10/17 08:3850.0 5.8 1
N-Nitrosodimethylamine ND ug/L 03/10/17 14:29 62-75-903/10/17 08:3810.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/17 14:29 621-64-703/10/17 08:3810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 03/10/17 14:29 86-30-603/10/17 08:3810.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/17 14:29 108-60-103/10/17 08:3810.0 1.6 1
Pentachlorophenol ND ug/L 03/10/17 14:29 87-86-503/10/17 08:3825.0 2.3 1
Phenanthrene ND ug/L 03/10/17 14:29 85-01-803/10/17 08:3810.0 0.22 1
Phenol ND ug/L 03/10/17 14:2903/10/17 08:3810.0 1.7 1
Pyrene ND ug/L 03/10/17 14:29 129-00-003/10/17 08:3810.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 14:29 120-82-103/10/17 08:3810.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 03/10/17 14:29 95-95-403/10/17 08:3810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 03/10/17 14:29 88-06-203/10/17 08:3810.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)70 %03/10/17 14:29 4165-60-003/10/17 08:3821-110 1
2-Fluorobiphenyl (S)70 %03/10/17 14:29 321-60-803/10/17 08:3827-110 1
Terphenyl-d14 (S)81 %03/10/17 14:29 1718-51-003/10/17 08:3831-107 1
Phenol-d6 (S)25 %03/10/17 14:29 13127-88-303/10/17 08:3810-110 1
2-Fluorophenol (S)36 %03/10/17 14:29 367-12-403/10/17 08:3812-110 1
2,4,6-Tribromophenol (S)76 %03/10/17 14:29 118-79-603/10/17 08:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/10/17 11:10 67-64-125.0 10.0 1
Benzene ND ug/L 03/10/17 11:10 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/10/17 11:10 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/10/17 11:10 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/10/17 11:10 75-27-41.0 0.18 1
Bromoform ND ug/L 03/10/17 11:10 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/10/17 11:10 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/10/17 11:10 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/10/17 11:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/10/17 11:10 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/10/17 11:10 75-00-31.0 0.54 1
Chloroform ND ug/L 03/10/17 11:10 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/10/17 11:10 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/10/17 11:10 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/10/17 11:10 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 21 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/10/17 11:10 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/10/17 11:10 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/10/17 11:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/10/17 11:10 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/10/17 11:10 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/10/17 11:10 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/10/17 11:10 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/10/17 11:10 75-71-81.0 0.21 1
1,1-Dichloroethane 1.9 ug/L 03/10/17 11:10 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/10/17 11:10 107-06-21.0 0.24 1
1,1-Dichloroethene 2.6 ug/L 03/10/17 11:10 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 3.6 ug/L 03/10/17 11:10 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/10/17 11:10 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/10/17 11:10 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/10/17 11:10 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/10/17 11:10 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/10/17 11:10 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/10/17 11:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/10/17 11:10 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/10/17 11:10 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/10/17 11:10 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/10/17 11:10 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/10/17 11:10 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/10/17 11:10 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/10/17 11:10 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/10/17 11:10 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/10/17 11:10 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/10/17 11:10 91-20-31.0 0.24 1
Styrene ND ug/L 03/10/17 11:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/10/17 11:10 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/10/17 11:10 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/10/17 11:10 127-18-41.0 0.46 1
Toluene ND ug/L 03/10/17 11:10 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/10/17 11:10 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/10/17 11:10 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/10/17 11:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/10/17 11:10 79-00-51.0 0.29 1
Trichloroethene 3.5 ug/L 03/10/17 11:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/10/17 11:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/10/17 11:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/10/17 11:10 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/10/17 11:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/10/17 11:10 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/10/17 11:10 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/10/17 11:10 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Sample:0309171344US Lab ID:92332882004 Collected:03/09/17 13:44 Received:03/09/17 15:07 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)95 %03/10/17 11:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/10/17 11:10 17060-07-070-130 1
Toluene-d8 (S)100 %03/10/17 11:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 23 of 32
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Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351627
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950708
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/10/17 07:100.33
1,1,1-Trichloroethane ug/L ND 1.0 03/10/17 07:100.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/10/17 07:100.40
1,1,2-Trichloroethane ug/L ND 1.0 03/10/17 07:100.29
1,1-Dichloroethane ug/L ND 1.0 03/10/17 07:100.32
1,1-Dichloroethene ug/L ND 1.0 03/10/17 07:100.56
1,1-Dichloropropene ug/L ND 1.0 03/10/17 07:100.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/10/17 07:100.33
1,2,3-Trichloropropane ug/L ND 1.0 03/10/17 07:100.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/10/17 07:100.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/10/17 07:102.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/10/17 07:100.27
1,2-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.30
1,2-Dichloroethane ug/L ND 1.0 03/10/17 07:100.24
1,2-Dichloropropane ug/L ND 1.0 03/10/17 07:100.27
1,3-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.24
1,3-Dichloropropane ug/L ND 1.0 03/10/17 07:100.28
1,4-Dichlorobenzene ug/L ND 1.0 03/10/17 07:100.33
2,2-Dichloropropane ug/L ND 1.0 03/10/17 07:100.13
2-Butanone (MEK)ug/L ND 5.0 03/10/17 07:100.96
2-Chlorotoluene ug/L ND 1.0 03/10/17 07:100.35
2-Hexanone ug/L ND 5.0 03/10/17 07:100.46
4-Chlorotoluene ug/L ND 1.0 03/10/17 07:100.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/10/17 07:100.33
Acetone ug/L ND 25.0 03/10/17 07:1010.0
Benzene ug/L ND 1.0 03/10/17 07:100.25
Bromobenzene ug/L ND 1.0 03/10/17 07:100.30
Bromochloromethane ug/L ND 1.0 03/10/17 07:100.17
Bromodichloromethane ug/L ND 1.0 03/10/17 07:100.18
Bromoform ug/L ND 1.0 03/10/17 07:100.26
Bromomethane ug/L ND 2.0 03/10/17 07:100.29
Carbon tetrachloride ug/L ND 1.0 03/10/17 07:100.25
Chlorobenzene ug/L ND 1.0 03/10/17 07:100.23
Chloroethane ug/L ND 1.0 03/10/17 07:100.54
Chloroform ug/L ND 1.0 03/10/17 07:100.14
Chloromethane ug/L ND 1.0 03/10/17 07:100.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/10/17 07:100.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/10/17 07:100.13
Dibromochloromethane ug/L ND 1.0 03/10/17 07:100.21
Dibromomethane ug/L ND 1.0 03/10/17 07:100.21
Dichlorodifluoromethane ug/L ND 1.0 03/10/17 07:100.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 24 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950708
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/10/17 07:100.12
Ethylbenzene ug/L ND 1.0 03/10/17 07:100.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/10/17 07:100.71
m&p-Xylene ug/L ND 2.0 03/10/17 07:100.66
Methyl-tert-butyl ether ug/L ND 1.0 03/10/17 07:100.21
Methylene Chloride ug/L ND 2.0 03/10/17 07:100.97
Naphthalene ug/L ND 1.0 03/10/17 07:100.24
o-Xylene ug/L ND 1.0 03/10/17 07:100.23
p-Isopropyltoluene ug/L ND 1.0 03/10/17 07:100.31
Styrene ug/L ND 1.0 03/10/17 07:100.26
Tetrachloroethene ug/L ND 1.0 03/10/17 07:100.46
Toluene ug/L ND 1.0 03/10/17 07:100.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/10/17 07:100.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/10/17 07:100.26
Trichloroethene ug/L ND 1.0 03/10/17 07:100.47
Trichlorofluoromethane ug/L ND 1.0 03/10/17 07:100.20
Vinyl acetate ug/L ND 2.0 03/10/17 07:100.35
Vinyl chloride ug/L ND 1.0 03/10/17 07:100.62
Xylene (Total)ug/L ND 1.0 03/10/17 07:100.66
1,2-Dichloroethane-d4 (S)%100 70-130 03/10/17 07:10
4-Bromofluorobenzene (S)%97 70-130 03/10/17 07:10
Toluene-d8 (S)%102 70-130 03/10/17 07:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950709LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950710
1,1,1,2-Tetrachloroethane ug/L 51.750 103 70-13010050.1 3 30
1,1,1-Trichloroethane ug/L 51.950 104 70-13010150.7 2 30
1,1,2,2-Tetrachloroethane ug/L 51.750 103 70-13010150.7 2 30
1,1,2-Trichloroethane ug/L 50.750 101 70-13010251.0 1 30
1,1-Dichloroethane ug/L 50.350 101 70-13010049.8 1 30
1,1-Dichloroethene ug/L 54.650 109 70-13210552.7 4 30
1,1-Dichloropropene ug/L 54.250 108 70-13010753.4 1 30
1,2,3-Trichlorobenzene ug/L 51.750 103 70-13510251.2 1 30
1,2,3-Trichloropropane ug/L 51.150 102 70-13010250.8 1 30
1,2,4-Trichlorobenzene ug/L 52.550 105 70-13410351.3 2 30
1,2-Dibromo-3-chloropropane ug/L 52.350 105 70-13010653.2 2 30
1,2-Dibromoethane (EDB)ug/L 50.750 101 70-13010150.4 1 30
1,2-Dichlorobenzene ug/L 51.350 103 70-13010150.6 1 30
1,2-Dichloroethane ug/L 47.350 95 70-1309246.1 2 30
1,2-Dichloropropane ug/L 52.350 105 70-1309949.7 5 30
1,3-Dichlorobenzene ug/L 51.650 103 70-13010049.9 3 30
1,3-Dichloropropane ug/L 52.150 104 70-13010351.5 1 30
1,4-Dichlorobenzene ug/L 50.550 101 70-1309949.4 2 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 25 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950709LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950710
2,2-Dichloropropane ug/L 51.450 103 58-1459547.6 8 30
2-Butanone (MEK)ug/L 98.4100 98 70-145101101 3 30
2-Chlorotoluene ug/L 52.950 106 70-13010150.5 5 30
2-Hexanone ug/L 104100 104 70-144106106 1 30
4-Chlorotoluene ug/L 51.450 103 70-1309949.6 4 30
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-140101101 1 30
Acetone ug/L 104100 104 50-175109109 5 30
Benzene ug/L 53.350 107 70-13010351.6 3 30
Bromobenzene ug/L 52.050 104 70-13010150.3 3 30
Bromochloromethane ug/L 53.050 106 70-13010250.8 4 30
Bromodichloromethane ug/L 53.450 107 70-13010351.6 3 30
Bromoform ug/L 50.550 101 70-13010250.8 1 30
Bromomethane ug/L 34.450 69 54-1307135.4 3 30
Carbon tetrachloride ug/L 50.350 101 70-1329949.5 2 30
Chlorobenzene ug/L 51.550 103 70-13010150.4 2 30
Chloroethane ug/L 47.750 95 64-1349346.5 2 30
Chloroform ug/L 49.450 99 70-1309547.5 4 30
Chloromethane ug/L 41.550 83 64-1308341.6 0 30
cis-1,2-Dichloroethene ug/L 50.450 101 70-13110049.8 1 30
cis-1,3-Dichloropropene ug/L 52.650 105 70-13010251.1 3 30
Dibromochloromethane ug/L 52.150 104 70-13010251.2 2 30
Dibromomethane ug/L 49.850 100 70-1319648.2 3 30
Dichlorodifluoromethane ug/L 51.150 102 56-13010150.7 1 30
Diisopropyl ether ug/L 50.450 101 70-1309849.0 3 30
Ethylbenzene ug/L 53.050 106 70-13010351.5 3 30
Hexachloro-1,3-butadiene ug/L 52.650 105 70-13010250.9 3 30
m&p-Xylene ug/L 105100 105 70-130101101 4 30
Methyl-tert-butyl ether ug/L 52.150 104 70-13010451.8 1 30
Methylene Chloride ug/L 50.650 101 63-13010150.5 0 30
Naphthalene ug/L 53.950 108 70-13810753.4 1 30
o-Xylene ug/L 52.550 105 70-13010351.6 2 30
p-Isopropyltoluene ug/L 50.750 101 70-1309949.5 2 30
Styrene ug/L 53.950 108 70-13010452.1 3 30
Tetrachloroethene ug/L 50.950 102 70-1309949.4 3 30
Toluene ug/L 52.850 106 70-13010351.4 3 30
trans-1,2-Dichloroethene ug/L 53.250 106 70-13010652.8 1 30
trans-1,3-Dichloropropene ug/L 51.650 103 70-13210351.3 0 30
Trichloroethene ug/L 50.150 100 70-1309849.1 2 30
Trichlorofluoromethane ug/L 53.850 108 62-13310652.9 2 30
Vinyl acetate ug/L 105100 105 66-157106106 1 30
Vinyl chloride ug/L 45.850 92 50-1508944.7 2 30
Xylene (Total)ug/L 157150 105 70-130102153 3 30
1,2-Dichloroethane-d4 (S)%97 70-13094
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 26 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351633
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950722
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/10/17 12:001.9
1,2-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.2
1,3-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.1
1,4-Dichlorobenzene ug/L ND 10.0 03/10/17 12:001.2
1-Methylnaphthalene ug/L ND 10.0 03/10/17 12:000.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/10/17 12:001.6
2,4,5-Trichlorophenol ug/L ND 10.0 03/10/17 12:002.2
2,4,6-Trichlorophenol ug/L ND 10.0 03/10/17 12:001.9
2,4-Dichlorophenol ug/L ND 10.0 03/10/17 12:001.7
2,4-Dimethylphenol ug/L ND 10.0 03/10/17 12:002.2
2,4-Dinitrophenol ug/L ND 50.0 03/10/17 12:006.5
2,4-Dinitrotoluene ug/L ND 10.0 03/10/17 12:001.2
2,6-Dinitrotoluene ug/L ND 10.0 03/10/17 12:001.7
2-Chloronaphthalene ug/L ND 10.0 03/10/17 12:002.2
2-Chlorophenol ug/L ND 10.0 03/10/17 12:001.5
2-Methylnaphthalene ug/L ND 10.0 03/10/17 12:000.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/10/17 12:001.7
2-Nitroaniline ug/L ND 50.0 03/10/17 12:002.8
2-Nitrophenol ug/L ND 10.0 03/10/17 12:001.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/10/17 12:001.7
3,3'-Dichlorobenzidine ug/L ND 20.0 03/10/17 12:001.4
3-Nitroaniline ug/L ND 50.0 03/10/17 12:002.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/10/17 12:001.7
4-Bromophenylphenyl ether ug/L ND 10.0 03/10/17 12:001.3
4-Chloro-3-methylphenol ug/L ND 20.0 03/10/17 12:004.2
4-Chloroaniline ug/L ND 20.0 03/10/17 12:003.4
4-Chlorophenylphenyl ether ug/L ND 10.0 03/10/17 12:002.1
4-Nitroaniline ug/L ND 20.0 03/10/17 12:002.5
4-Nitrophenol ug/L ND 50.0 03/10/17 12:005.8
Acenaphthene ug/L ND 10.0 03/10/17 12:000.25
Acenaphthylene ug/L ND 10.0 03/10/17 12:000.21
Aniline ug/L ND 10.0 03/10/17 12:001.3
Anthracene ug/L ND 10.0 03/10/17 12:000.14
Benzo(a)anthracene ug/L ND 10.0 03/10/17 12:000.33
Benzo(a)pyrene ug/L ND 10.0 03/10/17 12:000.30
Benzo(b)fluoranthene ug/L ND 10.0 03/10/17 12:000.28
Benzo(g,h,i)perylene ug/L ND 10.0 03/10/17 12:000.38
Benzo(k)fluoranthene ug/L ND 10.0 03/10/17 12:000.43
Benzoic Acid ug/L ND 50.0 03/10/17 12:0011.1
Benzyl alcohol ug/L ND 20.0 03/10/17 12:003.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/10/17 12:001.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 27 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1950722
Associated Lab Samples:92332882001, 92332882002, 92332882003, 92332882004
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 03/10/17 12:001.5
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/10/17 12:000.85
Butylbenzylphthalate ug/L ND 10.0 03/10/17 12:000.75
Chrysene ug/L ND 10.0 03/10/17 12:000.21
Di-n-butylphthalate ug/L ND 10.0 03/10/17 12:001.1
Di-n-octylphthalate ug/L ND 10.0 03/10/17 12:000.86
Dibenz(a,h)anthracene ug/L ND 10.0 03/10/17 12:000.55
Dibenzofuran ug/L ND 10.0 03/10/17 12:001.8
Diethylphthalate ug/L ND 10.0 03/10/17 12:001.3
Dimethylphthalate ug/L ND 10.0 03/10/17 12:001.5
Fluoranthene ug/L ND 10.0 03/10/17 12:000.21
Fluorene ug/L ND 10.0 03/10/17 12:000.21
Hexachloro-1,3-butadiene ug/L ND 10.0 03/10/17 12:001.8
Hexachlorobenzene ug/L ND 10.0 03/10/17 12:001.1
Hexachlorocyclopentadiene ug/L ND 10.0 03/10/17 12:001.8
Hexachloroethane ug/L ND 10.0 03/10/17 12:001.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/10/17 12:000.29
Isophorone ug/L ND 10.0 03/10/17 12:001.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/10/17 12:002.1
N-Nitrosodimethylamine ug/L ND 10.0 03/10/17 12:001.3
N-Nitrosodiphenylamine ug/L ND 10.0 03/10/17 12:001.3
Naphthalene ug/L ND 10.0 03/10/17 12:000.34
Nitrobenzene ug/L ND 10.0 03/10/17 12:001.7
Pentachlorophenol ug/L ND 25.0 03/10/17 12:002.3
Phenanthrene ug/L ND 10.0 03/10/17 12:000.22
Phenol ug/L ND 10.0 03/10/17 12:001.7
Pyrene ug/L ND 10.0 03/10/17 12:000.19
2,4,6-Tribromophenol (S)%78 27-110 03/10/17 12:00
2-Fluorobiphenyl (S)%67 27-110 03/10/17 12:00
2-Fluorophenol (S)%37 12-110 03/10/17 12:00
Nitrobenzene-d5 (S)%70 21-110 03/10/17 12:00
Phenol-d6 (S)%21 10-110 03/10/17 12:00
Terphenyl-d14 (S)%88 31-107 03/10/17 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
1,2,4-Trichlorobenzene ug/L 15.025 60 31-1206015.1 1 30
1,2-Dichlorobenzene ug/L 14.725 59 38-1205714.3 2 30
1,3-Dichlorobenzene ug/L 13.325 53 30-1225714.1 6 30
1,4-Dichlorobenzene ug/L 13.625 54 37-1205413.5 0 30
1-Methylnaphthalene ug/L 17.325 69 34-1136917.2 0 30
2,2'-Oxybis(1-chloropropane)ug/L 16.825 67 18-1206115.4 9 30
2,4,5-Trichlorophenol ug/L 16.825 67 43-1136315.8 6 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 28 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
2,4,6-Trichlorophenol ug/L 18.625 75 42-1207418.5 1 30
2,4-Dichlorophenol ug/L 17.625 71 30-1206817.1 3 30
2,4-Dimethylphenol ug/L 19.625 78 29-1117518.8 4 30
2,4-Dinitrophenol ug/L 108125 86 19-13291114 6 30
2,4-Dinitrotoluene ug/L 23.725 95 58-1289122.7 5 30
2,6-Dinitrotoluene ug/L 25.125 100 54-1299924.6 2 30
2-Chloronaphthalene ug/L 20.725 83 43-1178020.1 3 30
2-Chlorophenol ug/L 15.325 61 37-1205914.7 4 30
2-Methylnaphthalene ug/L 17.425 70 33-1207318.2 4 30
2-Methylphenol(o-Cresol)ug/L 12.625 50 31-1204611.5 9 30
2-Nitroaniline ug/L 35.3J50 71 48-1217035.0J 30
2-Nitrophenol ug/L 19.025 76 25-1168020.1 6 30
3&4-Methylphenol(m&p Cresol)ug/L 27.825 111 23-1209724.3 13 30
3,3'-Dichlorobenzidine ug/L 39.950 80 10-1547436.8 8 30
3-Nitroaniline ug/L 40.6J50 81 43-1157939.3J 30
4,6-Dinitro-2-methylphenol ug/L 43.550 87 44-1248341.3 5 30
4-Bromophenylphenyl ether ug/L 18.925 76 34-1137418.6 2 30
4-Chloro-3-methylphenol ug/L 39.150 78 31-1107135.4 10 30
4-Chloroaniline ug/L 38.250 76 20-1207135.7 7 30
4-Chlorophenylphenyl ether ug/L 18.425 74 34-1167117.7 4 30
4-Nitroaniline ug/L 42.050 84 46-1288140.3 4 30
4-Nitrophenol ug/L 42.2J125 34 11-1203442.5J 30
Acenaphthene ug/L 19.325 77 48-1147518.6 4 30
Acenaphthylene ug/L 19.225 77 48-1127418.4 4 30
Aniline ug/L 12.125 48 26-1204411.1 9 30
Anthracene ug/L 20.125 80 57-1187418.6 8 30
Benzo(a)anthracene ug/L 20.125 81 56-1217418.5 9 30
Benzo(a)pyrene ug/L 19.425 77 55-1277418.4 5 30
Benzo(b)fluoranthene ug/L 21.225 85 53-1287819.6 8 30
Benzo(g,h,i)perylene ug/L 21.325 85 54-1258320.7 3 30
Benzo(k)fluoranthene ug/L 21.325 85 51-1237819.5 9 30
Benzoic Acid ug/L 32.0J125 26 10-1202531.9J 30
Benzyl alcohol ug/L 27.750 55 27-1204924.5 12 30
bis(2-Chloroethoxy)methane ug/L 18.525 74 32-1207117.9 3 30
bis(2-Chloroethyl) ether ug/L 16.925 68 33-1116015.0 12 30
bis(2-Ethylhexyl)phthalate ug/L 23.425 94 50-1458721.9 7 30
Butylbenzylphthalate ug/L 24.425 98 54-1389223.0 6 30
Chrysene ug/L 20.425 82 58-1277719.2 6 30
Di-n-butylphthalate ug/L 23.125 93 56-1258721.8 6 30
Di-n-octylphthalate ug/L 20.425 82 50-1347919.8 3 30
Dibenz(a,h)anthracene ug/L 22.125 89 53-1298521.3 4 30
Dibenzofuran ug/L 18.625 74 45-1207418.4 1 30
Diethylphthalate ug/L 22.225 89 53-1208521.3 4 30
Dimethylphthalate ug/L 21.225 85 55-1168320.8 2 30
Fluoranthene ug/L 21.425 86 57-1258020.0 7 30
Fluorene ug/L 20.025 80 53-1187619.1 5 30
Hexachloro-1,3-butadiene ug/L 13.725 55 23-1206014.9 8 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 29 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1950723LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1950724
Hexachlorobenzene ug/L 19.625 79 49-1167518.8 4 30
Hexachlorocyclopentadiene ug/L 14.325 57 26-1586015.0 5 30
Hexachloroethane ug/L 12.825 51 30-1145714.3 11 30
Indeno(1,2,3-cd)pyrene ug/L 22.925 91 55-1288521.3 7 30
Isophorone ug/L 21.825 87 31-1188220.5 6 30
N-Nitroso-di-n-propylamine ug/L 16.925 68 32-1196315.8 7 30
N-Nitrosodimethylamine ug/L 10.125 40 13-1204511.3 11 30
N-Nitrosodiphenylamine ug/L 19.625 78 43-1207318.4 6 30
Naphthalene ug/L 17.625 70 32-1207017.6 0 30
Nitrobenzene ug/L 20.225 81 33-1108020.1 1 30
Pentachlorophenol ug/L 44.050 88 10-1378040.1 9 30
Phenanthrene ug/L 20.425 82 57-1177618.9 8 30
Phenol ug/L 8.5J25 34 10-120307.5J 30
Pyrene ug/L 18.425 74 55-1226917.2 7 30
2,4,6-Tribromophenol (S)%89 27-11080
2-Fluorobiphenyl (S)%72 27-11068
2-Fluorophenol (S)%39 12-11036
Nitrobenzene-d5 (S)%72 21-11069
Phenol-d6 (S)%27 10-11023
Terphenyl-d14 (S)%76 31-10770
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 30 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 31 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92332882
HARWELL RD PRIVA 103X902701067
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92332882001 351633 3516770309171049W1EPA 3510 EPA 8270
92332882002 351633 3516770309171139W2EPA 3510 EPA 8270
92332882003 351633 3516770309171320DSEPA 3510 EPA 8270
92332882004 351633 3516770309171344USEPA 3510 EPA 8270
92332882001 3516270309171049W1EPA 8260
92332882002 3516270309171139W2EPA 8260
92332882003 3516270309171320DSEPA 8260
92332882004 3516270309171344USEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/10/2017 04:13 PM Page 32 of 32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
file:///C/Users/tamechum/Desktop/Harwell%20Estates%20Mobile%20Home%20Pakr/Laserfiche/Harwell/ATT00001.htm[4/27/2018 2:01:41 PM]
1
Beverly, Trudy
From:Eichinger, Kevin <[e-mail]>
Sent:Friday, March 10, 2017 9:24 PM
To:Beverly, Trudy
Cc:Bateson, James
Subject:Fwd: Harwell Response
Attachments:01-067 Harwell Estates Well Response Results 031017.xls; ATT00001.htm
Here is the summary table. Confirms the well sample data. Also take a look at the creek samples. Found TCE is the creek.

Begin forwarded message:
From: "Taylor, Todd" <[e-mail]>
Date: March 10, 2017 at 21:13:18 EST
To: Kevin Eichinger <[e-mail]>
Subject: Harwell Response
Hello Kevin,

The table is attached.
<01-067 Harwell Estates Well Response Results 2-7-17.xls>
TABLE 1
SUMMARY OF DETECTED ANALYTES
1 of 1 Harwell Estates Well Response
Sample ID
Date
Sampled
1,4-
Dichlorobenzene
(µg/L)
1,1-
Dichloroethane
(µg/L)
1,2-
Dichloroethane
(µg/L)
1,1-DCE
(µg/L)
Cis-1,2-DCE
(µg/L)
trans-1,2-
DCE
(µg/L)
PCE
(µg/L)
1,1,1-
Trichloroethane
(µg/L)
TCE
(µg/L)
Vinyl
Chloride
(µg/L)
75 5 7 70 100 5 200 5 2
48 280 17 280 36 360 41 8,000 2.8 1.9
WELLHEAD #1 2/7/2017 ND NA ND 32 16 ND 42 ND 930 ND
WELLHEAD #1
AFTER FILTER
2/7/2017 ND NA ND 34 21 ND 33 ND 1100 ND
WELL #2 2/7/2017 0.98 NA 0.79 170 160 2.5 12 8.2 370 1.9
0309171049W1 -
EPA Well 1 Sample
3/9/2017 ND ND ND 22.3 15.5 ND 29.4 ND 944 ND
0309171139W2 -
EPA Well 2 Sample
3/9/2017 ND 98.3 ND 141 194 2.4J 10.9 5.6 409 ND
0309171320DS -
Downstream Sample
3/9/2017 ND 4.8 ND 7.9 9.1 ND ND ND 14.1 ND
0309171344US -
Upstream Sample
3/9/2017 ND 1.9 ND 2.6 3.6 ND ND ND 3.5 ND
Notes
Bold Exceeds the respective MCL
Bold Exceeds the respective MCL and RML
MCL EPA Maximum Contaminant Level
PCE Tetrachloroethylene
RML EPA Removal Management Level - Hazard Quotient = 1
TCE Trichloroethylene
U Analyte was not detected at concentrations above the laboratory reporting limit shown.
µg/L Micrograms per liter
EPA MCL
EPA RML
file:///C/Users/tamechum/Desktop/Harwell%20Estates%20Mobile%20Home%20Pakr/Laserfiche/Harwell/ATT00001.htm[4/27/2018 2:00:16 PM]
1
Beverly, Trudy
From:Samantha Dye <[e-mail]>
Sent:Friday, March 10, 2017 1:54 PM
To:Beverly, Trudy
Subject:RE: NRC#1172741 - Harwell Estates Mobile Home Park NRC Report
Thanks.

Samantha Dye, MSEH, REHS
Assistant Administrator Environmental Health
Gaston County Department of Health & Human Services
991 W. Hudson Blvd., Gastonia, NC 28052
Office 704-853-5230 |Cell 980-522-0340| Fax [phone]

Please tell us how we are doing by taking this very quick survey. We appreciate your comments.
https://www.surveymonkey.com/s/gastonehsfeedback

From: Beverly, Trudy [mailto:[e-mail]]
Sent: Friday, March 10, 2017 1:47 PM
To: Samantha Dye
Subject: FW: NRC#1172741 - Harwell Estates Mobile Home Park NRC Report

Fyi, see below.

From: Beverly, Trudy
Sent: Friday, March 10, 2017 1:33 PM
To: Day, Collin <[e-mail]>; Jesneck, Charlotte <[e-mail]>; Bateson, James
<[e-mail]>
Cc: Ramey, David E <[e-mail]>
Subject: FW: NRC#1172741 - Harwell Estates Mobile Home Park NRC Report

NRC Incident Report Below for Harwell Estates Mobile Home Park below
Reported on 3-8-17 by Terry Tanner, US EPA REGION 4
Email chain with Samantha Dye (Gaston County Health) below report

-----Original Message-----
From: NCEOC [mailto:[e-mail]]
Sent: Friday, March 10, 2017 1:07 PM
To: Beverly, Trudy <[e-mail]>
Subject: FW: NRC#1172741

fyi

-----Original Message-----
From: [e-mail] [mailto:[e-mail]]
Sent: Wednesday, March 08, 2017 1:40 PM
To: NCEOC <[e-mail]>
Subject: NRC#1172741

NATIONAL RESPONSE CENTER 1-800-424-8802
2
***GOVERNMENT USE ONLY***GOVERNMENT USE ONLY***
Information released to a third party shall comply with any
applicable federal and/or state Freedom of Information and Privacy Laws

Incident Report # 1172741

INCIDENT DESCRIPTION

*Report taken by: MST1 HECTOR FUENTES at 13:28 on 08-MAR-17
Incident Type: FIXED
Incident Cause: UNKNOWN
Affected Area: DRINKING WATER SYSTEM
Incident was discovered on 08-MAR-17 at 11:45 local incident time.
Affected Medium: WATER DRINKING WATER SYSTEM
_______________________________________________________________________
REPORTING PARTY
Name: TERRY TANNER
Organization: US EPA REGION 4
Address: 61 FORSYTH ST. SW
ATLANTA, GA 30303

PRIMARY Phone: [phone]
Type of Organization: FEDERAL GOVERNMENT
_______________________________________________________________________
SUSPECTED RESPONSIBLE PARTY
Name: UNKNOWN

Type of Organization: UNKNOWN
________________________________________________________________________
INCIDENT LOCATION
HARWELL RD County: GASTON
City: GASTONIA State: NC

_______________________________________________________________________
RELEASED MATERIAL(S)
CHRIS Code: NCC Official Material Name: NO CHRIS CODE
Also Known As: DICHLOROETHENE
Qty Released: 0 UNKNOWN AMOUNT Qty in Water: 0 UNKNOWN AMOUNT
CHRIS Code: TCE Official Material Name: 1,1,1-TRICHLOROETHANE
Also Known As:
Qty Released: 0 UNKNOWN AMOUNT Qty in Water: 0 UNKNOWN AMOUNT
________________________________________________________________________
DESCRIPTION OF INCIDENT
CALLER REPORTED DRINKING WATER SYSTEM CONTAMINATION DUE TO UNKNOWN
CAUSE. INVESTIGATION UNDERWAY.

________________________________________________________________________
SENSITIVE INFORMATION

________________________________________________________________________
INCIDENT DETAILS
Package: N/A
3
Building ID:
Type of Fixed Object: OTHER
Power Generating Facility: UNKNOWN
Generating Capacity:
Type of Fuel:
NPDES:
NPDES Compliance: UNKNOWN
---WATER INFORMATION---
Body of Water: DRINKING WATER SYSTEM
Tributary of:
Nearest River Mile Marker:
Water Supply Contaminated: YES

______________________________________________________________________
IMPACT
Fire Involved: NO Fire Extinguished: UNKNOWN

INJURIES: NO Hospitalized: Empl/Crew: Passenger:
FATALITIES: NO Empl/Crew: Passenger: Occupant:
EVACUATIONS:NO Who Evacuated: Radius/Area:

Damages: NO
Hours Direction of
Closure Type Description of Closure Closed Closure
N
Air:
N Major
Road: Artery:N
N
Waterway:
N
Track:

Environmental Impact: UNKNOWN
Media Interest: UNKNOWN Community Impact due to Material:
______________________________________________________________________
REMEDIAL ACTIONS
INVESTIGATION UNDERWAY
Release Secured: UNKNOWN
Release Rate:
Estimated Release Duration:

______________________________________________________________________
WEATHER
Weather: UNKNOWN, ºF
______________________________________________________________________
ADDITIONAL AGENCIES NOTIFIED
Federal: EPA
State/Local:
State/Local On Scene:
State Agency Number:
_______________________________________________________________________
NOTIFICATIONS BY NRC
CENTERS FOR DISEASE CONTROL (GRASP)
08-MAR-17 13:39 (770)4887100
DHS NOC (NOC)
4
08-MAR-17 13:39 (202)2828114
DHS DEFENSE THREAT REDUCTION AGENCY (CHEMICAL AND BIOLOGICAL TECHNOLOGI
08-MAR-17 13:39 (703)7673477
DHS I&A STATE AND LOCAL PRGM OFFICE (RALEIGH, NC FUSION CENTER)
08-MAR-17 13:39 (202)5575179
DHS SOUTH CAROLINA FUSION CENTER (LE SENSITIVE ADVISORS & LIASON PROGRA
08-MAR-17 13:39 (866)4728477
DOT CRISIS MANAGEMENT CENTER (MAIN OFFICE)
08-MAR-17 13:39 (202)3661863
U.S. EPA IV (MAIN OFFICE)
(404)6504955
U.S. EPA IV (NC/SC INCIDENTS)
08-MAR-17 13:39 (404)6504955
U.S. EPA IV (DUTY OSC)
08-MAR-17 13:39 (404)6504955
FEDERAL EMERGENCY MANAGEMENT AGENCY (MAIN OFFICE)
08-MAR-17 13:39 (800)6347084
INFO ANALYSIS AND INFRA PROTECTION (MAIN OFFICE)
08-MAR-17 13:39
NC DEPT OF EMERGENCY MGMT (MAIN OFFICE)
08-MAR-17 13:39 (800)8580368
NC OCCUPATIONAL ENVMTL EPIDEMIOLOGY (COMMAND CENTER)
08-MAR-17 13:39 (919)7075950
NC PUBLIC HEALTH PREPARE AND RESPNS (PHPR COMMAND CENTER)
08-MAR-17 13:39 (919)7150919
NATIONAL INFRASTRUCTURE COORD CTR (MAIN OFFICE)
08-MAR-17 13:39 (202)2829201
NOAA RPTS FOR NC (MAIN OFFICE)
08-MAR-17 13:39 (206)5264911
NATIONAL RESPONSE CENTER HQ (AUTOMATIC REPORTS)
08-MAR-17 13:39 (202)2671136
HOMELAND SEC COORDINATION CENTER (MAIN OFFICE)
08-MAR-17 13:39 (202)2828300
DOI FOR REGION 4 (MAIN OFFICE)
08-MAR-17 13:39 (404)3314524
SEAHAWK IOC (INTER-AGENCY OPERATIONS CENTER)
08-MAR-17 13:39 (803)2060971
STATE OF NORTH CAROLINA DENR (MAIN OFFICE)
08-MAR-17 13:39 (919)8076300
SC DEPT OF ENV CNTL ATTN: ERS (MAIN OFFICE)
08-MAR-17 13:39 (803)2536488
TSA OFFICE OF SECURITY OPERATIONS (SURFACE COMPLIANCE BRANCH SE REGION)
08-MAR-17 13:39 (904)9804075
USCG DISTRICT 5 (D5 DRAT)
08-MAR-17 13:39 (757)3986231
USCG DISTRICT 5 (INTEL CHIEF)
08-MAR-17 13:39 (757)3986655
_______________________________________________________________________
ADDITIONAL INFORMATION

______________________________________________________________________
*** END INCIDENT REPORT #1172741 ***
Report any problems by calling 1-800-424-8802
PLEASE VISIT OUR WEB SITE AT http://www.nrc.uscg.mil E-mail correspondence sent to and from this address
may be subject to the provisions of G.S. 132-1, the North Carolina Public Records Law, and may be subject to monitoring
and disclosed to third parties, including law enforcement personnel, by an authorized state official.
5

________________________________

Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties by an authorized state official.

From: Jesneck, Charlotte
Sent: Thursday, March 09, 2017 8:52 AM
To: Beverly, Trudy <[e-mail]>; Day, Collin <[e-mail]>
Cc: Bateson, James <[e-mail]>
Subject: RE: Harwell

I forwarded to Jim. Just a reminder to copy him on this type of email. Thanks.

Charlotte Jesneck, LG
Branch Head
Inactive Hazardous Sites Branch
NC Department of Environmental Quality

919-707-8327 office
[e-mail]

Office Location: 217 W Jones Street, Raleigh, NC
Mail: 1646 Mail Service Center
Raleigh, NC 27699

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Beverly, Trudy
Sent: Wednesday, March 08, 2017 4:02 PM
To: Jesneck, Charlotte <[e-mail]>; Day, Collin <[e-mail]>
Subject: FW: Harwell
Importance: High

Fyi. Apparently there is some mix up and Sam (Gaston County Health) was able to explain about Harwell Estates Mobile
Home Park. See email from Samantha Dye below.

From: Beverly, Trudy
Sent: Wednesday, March 08, 2017 4:00 PM
To: 'Samantha Dye' <[e-mail]>; Assefa, Hanna <[e-mail]>; Earnest, Emily
<[e-mail]>
Subject: RE: Harwell

Thanks for letting us know.
Trudy
6
From: Samantha Dye [mailto:[e-mail]]
Sent: Wednesday, March 08, 2017 3:58 PM
To: Beverly, Trudy <[e-mail]>; Assefa, Hanna <[e-mail]>; Earnest, Emily
<[e-mail]>
Subject: Harwell

Hi ladies,

NC Emergency Management has sent out an alert that there was a spill of TCE at the MHP. I just spoke with Kennedy
Holt from NC OEEB and explained the situation. I just wanted to give you a heads up.

Best,
Sam

Samantha Dye, MSEH, REHS
Assistant Administrator Environmental Health
Gaston County Department of Health & Human Services
991 W. Hudson Blvd., Gastonia, NC 28052
Office 704-853-5230 |Cell 980-522-0340| Fax [phone]

Please tell us how we are doing by taking this very quick survey. We appreciate your comments.
https://www.surveymonkey.com/s/gastonehsfeedback

This message may contain confidential information and is intended only for the individual named. If you are not
the named addressee you should not disseminate, distribute or copy this email. Please notify the sender
immediately by email if you have received this email by mistake and delete it from your system. Emails that do
not contain confidential medical information are subject to North Carolina General Statute, Chapter 132 and
may be considered a matter of public record.

This message may contain confidential information and is intended only for the individual named. If you are not the
named addressee you should not disseminate, distribute or copy this email. Please notify the sender immediately by email
if you have received this email by mistake and delete it from your system. Emails that do not contain confidential medical
information are subject to North Carolina General Statute, Chapter 132 and may be considered a matter of public record.
1
Beverly, Trudy
From:Cook, Clinton
Sent:Friday, March 10, 2017 1:55 PM
To:Beverly, Trudy
Subject:RE: Harwell Mobile Home Park
Thanks for the information.

Clint

From: Beverly, Trudy
Sent: Friday, March 10, 2017 12:12 PM
To: Pitner, Andrew <[e-mail]>; Cook, Clinton <[e-mail]>
Cc: Westmoreland, Jeff <[e-mail]>; Day, Collin <[e-mail]>; Ramey, David E
<[e-mail]>
Subject: RE: Harwell Mobile Home Park

This is an area that I have been addressing. Harwell Estates Mobile home Park was in the middle of a property transaction
when the potential purchaser started gathering information about environmental impacts in the area. He, at my
recommendation asked the owners for voc & svoc sampling from the 2 wells supplying Harwell Estates. I offered to do
the sampling & rush the data. The owners wanted their well company to do the sampling. I received a copy of the sample
results on Monday, February 27, 2017. The park has federal exceedances of TCE (370-1100, standard is 5), PCE (12-42,
standard is 5), 1,1 DCE (32-170, standard is 7) ( in both wells (well #1 main supplier & well #2) and federal exceedances
of Cis1,2DCE (160, standard is 70) & 1,4-Dioxane (8.9, standard is 3) in their well #2(back up). I made a sampling trip to
the park and 2 very close neighbors on March 2, 2017. One neighbor was non-detect for vocs, the other had TCE below
state standards (3.2, standard is 5). I met with the Harwell Estates Mobile Home park owners and Kevin Eichinger, the
EPA OSC, Region 4 Emergency Response & Removal Branch yesterday to discuss EPA assisting with a temporary
treatment system for the park and eventually, a connection with the City of Gastonia system. IHSB does have 3 listed
sites near the area. I also collected 12 residential water supply well samples yesterday (4 of these includes Harwell
Estates and their immediate 2 neighbors that were sampled on March 2, 2017) and 8 other wells along Beaty Road, Teby
Drive, Matthew Street to the north east of Harwell Estates and have plans to do more in the future.
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-section/inactive-hazardous-
sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

2
North Carolina Department of Environmental Quality
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Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
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From: Pitner, Andrew
Sent: Thursday, March 09, 2017 5:28 PM
To: Cook, Clinton <[e-mail]>
Cc: Westmoreland, Jeff <[e-mail]>; Beverly, Trudy <[e-mail]>
Subject: RE: Harwell Mobile Home Park

WQROS isn’t really involved with this issue. I believe that DWM-IHSB is and I’ve cc’d Trudy.
A

From: Cook, Clinton
Sent: Thursday, March 09, 2017 5:02 PM
To: Pitner, Andrew <[e-mail]>
Cc: Westmoreland, Jeff <[e-mail]>
Subject: FW: Harwell Mobile Home Park
Importance: High

Andrew,

FYI, please see below. Please let me know, if you need additional information. (I’m sorry for not sending this earlier, I
thought that Mr. Watson was actively involved with this site.) Please note that Jeff Westmoreland has investigated the
area and has determined that the mobile home park does not serve enough connections or persons to be a public water
system.

Thanks,
Clint

From: Tommy Almond [mailto:[e-mail]]
Sent: Thursday, March 09, 2017 9:09 AM
To: Cook, Clinton <[e-mail]>
Subject: FW: Harwell Mobile Home Park
Importance: High

From: Curtis Hopper
Sent: Wednesday, March 08, 2017 3:17 PM
To: Tommy Almond
Subject: FW: Harwell Mobile Home Park
Importance: High

From: Samantha Dye
Sent: Friday, February 24, 2017 12:16 PM
To: Curtis Hopper; Chris Dobbins; Stephen Eaton
3
Subject: Harwell Mobile Home Park
Importance: High

Hi all,

I received a call from Jim Bateson with NCDEQ Waste Management in Raleigh and have spoken with Trudy Beverly
with NCDEQ Mooresville office. The Harwell mobile home park owner had water samples taken and has verbally given
the sample results as 370 ppb TCE, 12 ppb PCE, 170 DCA in the well. These levels are extremely high. The state has
requested a hard copy of the lab results but the owner is waiting until he speaks with an attorney later this afternoon. The
state will forward the results to Dr. Langley and the state toxicologists to review. The state has advised the owner to
provide bottle water to all residents but he does not want to notify the residents until he speaks with the attorney. The state
will be emailing the property owner a letter to let him know the gravity of this situation.

If the results are accurate, residents will need bottle water immediately and possibly will not be able to use the water at all.
I have given my personal cell number to Jim and Trudy to contact me if there is anything we can do to help. I will forward
any information to you as I receive it.

The MHP owners are Kenneth & Mildred Harwell. The MHP is located off Beaty Road.

Happy Friday!!

Sam

Samantha Dye, MSEH, REHS
Assistant Administrator Environmental Health
Gaston County Department of Health & Human Services
991 W. Hudson Blvd., Gastonia, NC 28052
Office 704-853-5230 |Cell 980-522-0340| Fax [phone]

Please tell us how we are doing by taking this very quick survey. We appreciate your comments.
https://www.surveymonkey.com/s/gastonehsfeedback

This message may contain confidential information and is intended only for the individual named. If you are not
the named addressee you should not disseminate, distribute or copy this email. Please notify the sender
immediately by email if you have received this email by mistake and delete it from your system. Emails that do
not contain confidential medical information are subject to North Carolina General Statute, Chapter 132 and
may be considered a matter of public record.
1
Beverly, Trudy
From:Bateson, James
Sent:Friday, February 24, 2017 12:19 PM
To:Beverly, Trudy; Jesneck, Charlotte; Day, Collin
Subject:Country Acres Map
Attachments:Country_Acres-Harwell_Rd_ loc__Map.pdf

Jim Bateson
Section Chief
Division of Waste Management, Superfund Section
North Carolina Department of Environmental Quality

[phone] phone and fax
[e-mail]

1646 Mail Service Center
Raleigh, NC 27699-1646

******************************************************* 
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North Carolina Public Records Law and may be disclosed to third parties. 
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!(
HARWELL ROADSEPTIC PITS
LEE'S MOTORWORKS
ASHE PATTERNSHOP
COUNTRY ACRESWELL #2 700800700
80074076
0
720780720780780740
720
740
760780Source: Gaston County, Parcels; Well Sample Locations, NC Division of Waste Management; Contour, NC DOT (Derived from 2007 LIDAR)
COUNTRY ACRES/SOUTHGATE WELL #2
1
NC PWS ID: NC0136182
Gastonia, NC
Gaston
SMM
Fig:
Site:
City
County:
Date:
Drawn By:
1 inch = 500 feet
0.1 0 0.10.05
Miles
North American Datum 1983North Carolina State Plane (3200)
Contour Interval 4 Feet
²
!(
08/17/2012
1
Beverly, Trudy
From:Beverly, Trudy
Sent:Tuesday, January 31, 2017 10:38 AM
To:[e-mail]
Subject:Superfund Files
Hi Tony,
I enjoyed speaking with you this morning about the area around Harwell Road in Gastonia. In property purchasing, I
suggest that you have any water supply wells sampled on the property (volatile organic compounds and semi volatile
compounds have been found in the area). You should also look into getting a phase I environmental report.
The following sites are listed in the Inactive Hazardous Site Branch’s inventory near your potential purchase:
Harwell Road Septic Pits – NCD986166692
Ashe Pattern Shop (Former) – NCD986145636
Lee Motor Works – NCD986175628
Our Superfund Section files and instructions can be found online at the following
website: https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records.
NCDEQ’s Public Water Section will also have sampling records from the Country Acres/Southgate community slightly
north of the property you are considering purchasing. They have had some solvent detections in the past. You may
further wish to contact an environmental attorney and discuss and findings from the phase 1 and file reviews for the
area. DEQ’s Brownfields Program may also be helpful since you may be developing the property.
-Hope this helps and let me know if I can offer further assistance.
Trudy
Trudy Beverly, LG - [e-mail]
Hydrogeologist, Western Region
NCDEQ - Division of Waste Management
Superfund Section - Inactive Hazardous Sites Branch
Mooresville Regional Office
610 East Center Ave., Suite 301
Mooresville, NC 28115
Phone: [phone] Fax: [phone]
Branch Website Address: https://deq.nc.gov/about/divisions/waste-management/superfund-section/inactive-hazardous-
sites-program

INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps

ONLINE ACCESS TO SUPERFUND SECTION DOCUMENTS:
https://deq.nc.gov/about/divisions/waste-management/superfund-section/sf-file-records

North Carolina Department of Environmental Quality
*******************************************************************************
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
*******************************************************************************