5601_McDowellMSWLF_GWMR_FID1088017

#=CL#
March 28, 2018
LIMS USE: FR - RANDELL THOMAS
LIMS OBJECT ID: 92374792
92374792
Project:
Pace Project No.:
RE:
Mr. Randell Thomas
McDowell County Landfill
60 East Court St
Marion, NC 28752
Land Fill MW's 2/26
Dear Mr. Thomas:
Enclosed are the analytical results for sample(s) received by the laboratory on February 26, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Lab ID Sample ID Matrix Date Collected Date Received
92374792001 MW-1 Water 02/26/18 13:25 02/26/18 14:55
92374792002 MW-2 Water 02/26/18 13:40 02/26/18 14:55
92374792003 MW-3 Water 02/26/18 12:35 02/26/18 14:55
92374792004 MW-4 Water 02/26/18 12:10 02/26/18 14:55
92374792005 TVL BLK Water 02/26/18 09:00 02/26/18 14:55
92374792006 Equip Blk Water 02/26/18 09:00 02/26/18 14:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92374792001 MW-1 EPA 6010 15 PASI-ASER, SH1
EPA 7470 1 PASI-ASER
EPA 8260 63 PASI-CSWB
92374792002 MW-2 EPA 6010 15 PASI-ASER, SH1
EPA 7470 1 PASI-ASER
EPA 8260 63 PASI-CSWB
92374792003 MW-3 EPA 6010 15 PASI-ASER, SH1
EPA 7470 1 PASI-ASER
EPA 8260 63 PASI-CSWB
92374792004 MW-4 EPA 6010 15 PASI-ASER, SH1
EPA 7470 1 PASI-ASER
EPA 8260 63 PASI-CSWB
92374792005 TVL BLK EPA 8260 63 PASI-CSWB
92374792006 Equip Blk EPA 6010 15 PASI-ASER, SH1
EPA 7470 1 PASI-ASER
EPA 8260 63 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-1 Lab ID:92374792001 Collected:02/26/18 13:25 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Thomas O
Shea 02/26/18 13:251
Collected Date 2/26/18 02/26/18 13:251
Collected Time 13:25 02/26/18 13:251
pH 5.1 Std. Units 02/26/18 13:250.10 1
Temperature 20.1 deg C 02/26/18 13:250.50 1
Static Water Level 18.74 feet 02/26/18 13:251
Specific Conductance 404 umhos/cm 02/26/18 13:251.0 1
Turbidity 26.74 NTU 02/26/18 13:251.0 1
Odor No Odor 02/26/18 13:251
Appearance Cloudy 02/26/18 13:251
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 03/08/18 06:14 7440-36-002/28/18 01:305.0 3.9 1
Arsenic 5.0U ug/L 03/08/18 06:14 7440-38-202/28/18 01:3010.0 5.0 1
Barium 267 ug/L 03/08/18 06:14 7440-39-302/28/18 01:305.0 2.5 1
Beryllium 0.50U ug/L 03/08/18 06:14 7440-41-702/28/18 01:301.0 0.50 1
Cadmium 0.50U ug/L 03/08/18 06:14 7440-43-902/28/18 01:301.0 0.50 1
Chromium 2.5U ug/L 03/08/18 06:14 7440-47-302/28/18 01:305.0 2.5 1
Cobalt 2.5U ug/L 03/05/18 17:09 7440-48-402/28/18 01:305.0 2.5 1
Copper 2.5U ug/L 03/08/18 06:14 7440-50-802/28/18 01:305.0 2.5 1
Lead 2.5U ug/L 03/08/18 06:14 7439-92-102/28/18 01:305.0 2.5 1
Nickel 2.5U ug/L 03/08/18 06:14 7440-02-002/28/18 01:305.0 2.5 1
Selenium 5.0U ug/L 03/08/18 06:14 7782-49-202/28/18 01:3010.0 5.0 1
Silver 2.5U ug/L 03/08/18 06:14 7440-22-402/28/18 01:305.0 2.5 1
Thallium 5.0U ug/L 03/08/18 06:14 7440-28-002/28/18 01:3010.0 5.0 1
Vanadium 2.5U ug/L 03/08/18 06:14 7440-62-202/28/18 01:305.0 2.5 1
Zinc 14.0 ug/L 03/08/18 06:14 7440-66-602/28/18 01:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/28/18 16:31 7439-97-602/27/18 09:550.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 03/02/18 16:49 67-64-125.0 10.0 1
Benzene 0.25U ug/L 03/02/18 16:49 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 03/02/18 16:49 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 03/02/18 16:49 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 03/02/18 16:49 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 03/02/18 16:49 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 03/02/18 16:49 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 03/02/18 16:49 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 03/02/18 16:49 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 03/02/18 16:49 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 03/02/18 16:49 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 03/02/18 16:49 67-66-31.0 0.14 1
Chloromethane 0.28J ug/L 03/02/18 16:49 74-87-31.0 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-1 Lab ID:92374792001 Collected:02/26/18 13:25 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Chlorotoluene 0.35U ug/L 03/02/18 16:49 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 03/02/18 16:49 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 03/02/18 16:49 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 03/02/18 16:49 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 03/02/18 16:49 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 03/02/18 16:49 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 03/02/18 16:49 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 03/02/18 16:49 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 03/02/18 16:49 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 03/02/18 16:49 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 03/02/18 16:49 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 03/02/18 16:49 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 03/02/18 16:49 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 03/02/18 16:49 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 03/02/18 16:49 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 03/02/18 16:49 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 03/02/18 16:49 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 03/02/18 16:49 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 03/02/18 16:49 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 03/02/18 16:49 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 03/02/18 16:49 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 03/02/18 16:49 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 03/02/18 16:49 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 03/02/18 16:49 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 03/02/18 16:49 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 03/02/18 16:49 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 03/02/18 16:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 03/02/18 16:49 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 03/02/18 16:49 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 03/02/18 16:49 91-20-31.0 0.24 1
Styrene 0.26U ug/L 03/02/18 16:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 03/02/18 16:49 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 03/02/18 16:49 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 03/02/18 16:49 127-18-41.0 0.46 1
Toluene 0.26U ug/L 03/02/18 16:49 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 03/02/18 16:49 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 03/02/18 16:49 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 03/02/18 16:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 03/02/18 16:49 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 03/02/18 16:49 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 03/02/18 16:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 03/02/18 16:49 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 03/02/18 16:49 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 03/02/18 16:49 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 03/02/18 16:49 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 03/02/18 16:49 179601-23-12.0 0.66 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-1 Lab ID:92374792001 Collected:02/26/18 13:25 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
o-Xylene 0.23U ug/L 03/02/18 16:49 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/02/18 16:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %03/02/18 16:49 17060-07-070-130 1
Toluene-d8 (S)99 %03/02/18 16:49 2037-26-570-130 1
Sample:MW-2 Lab ID:92374792002 Collected:02/26/18 13:40 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Thomas O
Shea 02/26/18 13:401
Collected Date 2/26/18 02/26/18 13:401
Collected Time 13:40 02/26/18 13:401
pH 6.0 Std. Units 02/26/18 13:400.10 1
Temperature 16.3 deg C 02/26/18 13:400.50 1
Static Water Level 39.03 feet 02/26/18 13:401
Specific Conductance 845 umhos/cm 02/26/18 13:401.0 1
Turbidity 26.64 NTU 02/26/18 13:401.0 1
Odor Organic
Odor 02/26/18 13:401
Appearance Cloudy 02/26/18 13:401
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 03/08/18 06:17 7440-36-002/28/18 01:305.0 3.9 1
Arsenic 5.0U ug/L 03/08/18 06:17 7440-38-202/28/18 01:3010.0 5.0 1
Barium 165 ug/L 03/08/18 06:17 7440-39-302/28/18 01:305.0 2.5 1
Beryllium 0.50U ug/L 03/08/18 06:17 7440-41-702/28/18 01:301.0 0.50 1
Cadmium 0.50U ug/L 03/08/18 06:17 7440-43-902/28/18 01:301.0 0.50 1
Chromium 2.5U ug/L 03/08/18 06:17 7440-47-302/28/18 01:305.0 2.5 1
Cobalt 26.3 ug/L 03/05/18 17:12 7440-48-402/28/18 01:305.0 2.5 1
Copper 2.5U ug/L 03/08/18 06:17 7440-50-802/28/18 01:305.0 2.5 1
Lead 2.5U ug/L 03/08/18 06:17 7439-92-102/28/18 01:305.0 2.5 1
Nickel 8.7 ug/L 03/08/18 06:17 7440-02-002/28/18 01:305.0 2.5 1
Selenium 5.0U ug/L 03/08/18 06:17 7782-49-202/28/18 01:3010.0 5.0 1
Silver 2.5U ug/L 03/08/18 06:17 7440-22-402/28/18 01:305.0 2.5 1
Thallium 15.6 ug/L 03/08/18 06:17 7440-28-002/28/18 01:3010.0 5.0 1
Vanadium 5.5 ug/L 03/08/18 06:17 7440-62-202/28/18 01:305.0 2.5 1
Zinc 10.4 ug/L 03/08/18 06:17 7440-66-602/28/18 01:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/28/18 16:38 7439-97-602/27/18 09:550.20 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-2 Lab ID:92374792002 Collected:02/26/18 13:40 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 03/02/18 17:06 67-64-125.0 10.0 1
Benzene 2.9 ug/L 03/02/18 17:06 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 03/02/18 17:06 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 03/02/18 17:06 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 03/02/18 17:06 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 03/02/18 17:06 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 03/02/18 17:06 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 03/02/18 17:06 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 03/02/18 17:06 56-23-51.0 0.25 1
Chlorobenzene 12.1 ug/L 03/02/18 17:06 108-90-71.0 0.23 1
Chloroethane 0.61J ug/L 03/02/18 17:06 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 03/02/18 17:06 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 03/02/18 17:06 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 03/02/18 17:06 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 03/02/18 17:06 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 03/02/18 17:06 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 03/02/18 17:06 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 03/02/18 17:06 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 03/02/18 17:06 74-95-31.0 0.21 1
1,2-Dichlorobenzene 2.2 ug/L 03/02/18 17:06 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.28J ug/L 03/02/18 17:06 541-73-11.0 0.24 1
1,4-Dichlorobenzene 8.8 ug/L 03/02/18 17:06 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 03/02/18 17:06 75-71-81.0 0.21 1
1,1-Dichloroethane 0.92J ug/L 03/02/18 17:06 75-34-31.0 0.32 1
1,2-Dichloroethane 0.40J ug/L 03/02/18 17:06 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 03/02/18 17:06 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 20.8 ug/L 03/02/18 17:06 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 03/02/18 17:06 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 03/02/18 17:06 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 03/02/18 17:06 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 03/02/18 17:06 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 03/02/18 17:06 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 03/02/18 17:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 03/02/18 17:06 10061-02-61.0 0.26 1
Diisopropyl ether 1.3 ug/L 03/02/18 17:06 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 03/02/18 17:06 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 03/02/18 17:06 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 03/02/18 17:06 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 03/02/18 17:06 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 03/02/18 17:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 03/02/18 17:06 108-10-15.0 0.33 1
Methyl-tert-butyl ether 1.1 ug/L 03/02/18 17:06 1634-04-41.0 0.21 1
Naphthalene 0.40J ug/L 03/02/18 17:06 91-20-31.0 0.24 1
Styrene 0.26U ug/L 03/02/18 17:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 03/02/18 17:06 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 03/02/18 17:06 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-2 Lab ID:92374792002 Collected:02/26/18 13:40 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 03/02/18 17:06 127-18-41.0 0.46 1
Toluene 0.26U ug/L 03/02/18 17:06 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 03/02/18 17:06 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.88J ug/L 03/02/18 17:06 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 03/02/18 17:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 03/02/18 17:06 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 03/02/18 17:06 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 03/02/18 17:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 03/02/18 17:06 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 03/02/18 17:06 108-05-42.0 0.35 1
Vinyl chloride 1.2 ug/L 03/02/18 17:06 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 03/02/18 17:06 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 03/02/18 17:06 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 03/02/18 17:06 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)103 %03/02/18 17:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %03/02/18 17:06 17060-07-070-130 1
Toluene-d8 (S)99 %03/02/18 17:06 2037-26-570-130 1
Sample:MW-3 Lab ID:92374792003 Collected:02/26/18 12:35 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Thomas O
Shea
02/26/18 12:351
Collected Date 2/26/18 02/26/18 12:351
Collected Time 12:35 02/26/18 12:351
pH 6.4 Std. Units 02/26/18 12:350.10 1
Temperature 17.4 deg C 02/26/18 12:350.50 1
Static Water Level 42.25 feet 02/26/18 12:351
Specific Conductance 749 umhos/cm 02/26/18 12:351.0 1
Turbidity 124 NTU 02/26/18 12:351.0 1
Odor Slight
Odor
02/26/18 12:351
Appearance Cloudy 02/26/18 12:351
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 03/08/18 06:20 7440-36-002/28/18 01:305.0 3.9 1
Arsenic 5.0U ug/L 03/08/18 06:20 7440-38-202/28/18 01:3010.0 5.0 1
Barium 958 ug/L 03/08/18 06:20 7440-39-302/28/18 01:305.0 2.5 1
Beryllium 1.7 ug/L 03/08/18 06:20 7440-41-702/28/18 01:301.0 0.50 1
Cadmium 0.59J ug/L 03/08/18 06:20 7440-43-902/28/18 01:301.0 0.50 1
Chromium 3.4J ug/L 03/08/18 06:20 7440-47-302/28/18 01:305.0 2.5 1
Cobalt 9.1 ug/L 03/05/18 17:15 7440-48-402/28/18 01:305.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-3 Lab ID:92374792003 Collected:02/26/18 12:35 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Copper 3.0J ug/L 03/08/18 06:20 7440-50-802/28/18 01:305.0 2.5 1
Lead 2.7J ug/L 03/08/18 06:20 7439-92-102/28/18 01:305.0 2.5 1
Nickel 4.0J ug/L 03/08/18 06:20 7440-02-002/28/18 01:305.0 2.5 1
Selenium 5.0U ug/L 03/08/18 06:20 7782-49-202/28/18 01:3010.0 5.0 1
Silver 2.5U ug/L 03/08/18 06:20 7440-22-402/28/18 01:305.0 2.5 1
Thallium 5.0U ug/L 03/08/18 06:20 7440-28-002/28/18 01:3010.0 5.0 1
Vanadium 10.7 ug/L 03/08/18 06:20 7440-62-202/28/18 01:305.0 2.5 1
Zinc 27.3 ug/L 03/08/18 06:20 7440-66-602/28/18 01:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/28/18 16:40 7439-97-602/27/18 09:550.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 03/02/18 17:22 67-64-125.0 10.0 1
Benzene 0.25U ug/L 03/02/18 17:22 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 03/02/18 17:22 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 03/02/18 17:22 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 03/02/18 17:22 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 03/02/18 17:22 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 03/02/18 17:22 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 03/02/18 17:22 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 03/02/18 17:22 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 03/02/18 17:22 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 03/02/18 17:22 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 03/02/18 17:22 67-66-31.0 0.14 1
Chloromethane 0.64J ug/L 03/02/18 17:22 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 03/02/18 17:22 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 03/02/18 17:22 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 03/02/18 17:22 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 03/02/18 17:22 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 03/02/18 17:22 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 03/02/18 17:22 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 03/02/18 17:22 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 03/02/18 17:22 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 03/02/18 17:22 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 03/02/18 17:22 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 03/02/18 17:22 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 03/02/18 17:22 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 03/02/18 17:22 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 03/02/18 17:22 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 03/02/18 17:22 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 03/02/18 17:22 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 03/02/18 17:22 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 03/02/18 17:22 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 03/02/18 17:22 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 03/02/18 17:22 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-3 Lab ID:92374792003 Collected:02/26/18 12:35 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene 0.26U ug/L 03/02/18 17:22 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 03/02/18 17:22 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 03/02/18 17:22 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 03/02/18 17:22 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 03/02/18 17:22 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 03/02/18 17:22 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 03/02/18 17:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 03/02/18 17:22 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 03/02/18 17:22 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 03/02/18 17:22 91-20-31.0 0.24 1
Styrene 0.26U ug/L 03/02/18 17:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 03/02/18 17:22 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 03/02/18 17:22 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 03/02/18 17:22 127-18-41.0 0.46 1
Toluene 0.26U ug/L 03/02/18 17:22 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 03/02/18 17:22 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 03/02/18 17:22 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 03/02/18 17:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 03/02/18 17:22 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 03/02/18 17:22 79-01-61.0 0.47 1
Trichlorofluoromethane 0.30J ug/L 03/02/18 17:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 03/02/18 17:22 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 03/02/18 17:22 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 03/02/18 17:22 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 03/02/18 17:22 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 03/02/18 17:22 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 03/02/18 17:22 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %03/02/18 17:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %03/02/18 17:22 17060-07-070-130 1
Toluene-d8 (S)100 %03/02/18 17:22 2037-26-570-130 1
Sample:MW-4 Lab ID:92374792004 Collected:02/26/18 12:10 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Thomas O
Shea 02/26/18 12:101
Collected Date 2/26/18 02/26/18 12:101
Collected Time 12:10 02/26/18 12:101
pH 6.1 Std. Units 02/26/18 12:100.10 1
Temperature 16.4 deg C 02/26/18 12:100.50 1
Static Water Level 19.15 feet 02/26/18 12:101
Specific Conductance 75 umhos/cm 02/26/18 12:101.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-4 Lab ID:92374792004 Collected:02/26/18 12:10 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Turbidity 35.14 NTU 02/26/18 12:101.0 1
Odor No Odor 02/26/18 12:101
Appearance Cloudy 02/26/18 12:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 03/08/18 06:22 7440-36-002/28/18 01:305.0 3.9 1
Arsenic 5.0U ug/L 03/08/18 06:22 7440-38-202/28/18 01:3010.0 5.0 1
Barium 64.3 ug/L 03/08/18 06:22 7440-39-302/28/18 01:305.0 2.5 1
Beryllium 0.50U ug/L 03/08/18 06:22 7440-41-702/28/18 01:301.0 0.50 1
Cadmium 0.50U ug/L 03/08/18 06:22 7440-43-902/28/18 01:301.0 0.50 1
Chromium 2.5U ug/L 03/08/18 06:22 7440-47-302/28/18 01:305.0 2.5 1
Cobalt 2.5U ug/L 03/05/18 17:18 7440-48-402/28/18 01:305.0 2.5 1
Copper 2.5U ug/L 03/08/18 06:22 7440-50-802/28/18 01:305.0 2.5 1
Lead 2.5U ug/L 03/08/18 06:22 7439-92-102/28/18 01:305.0 2.5 1
Nickel 2.5U ug/L 03/08/18 06:22 7440-02-002/28/18 01:305.0 2.5 1
Selenium 5.0U ug/L 03/08/18 06:22 7782-49-202/28/18 01:3010.0 5.0 1
Silver 2.5U ug/L 03/08/18 06:22 7440-22-402/28/18 01:305.0 2.5 1
Thallium 5.0U ug/L 03/08/18 06:22 7440-28-002/28/18 01:3010.0 5.0 1
Vanadium 10.3 ug/L 03/08/18 06:22 7440-62-202/28/18 01:305.0 2.5 1
Zinc 12.0 ug/L 03/08/18 06:22 7440-66-602/28/18 01:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/28/18 16:43 7439-97-602/27/18 09:550.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 03/02/18 17:38 67-64-125.0 10.0 1
Benzene 0.25U ug/L 03/02/18 17:38 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 03/02/18 17:38 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 03/02/18 17:38 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 03/02/18 17:38 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 03/02/18 17:38 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 03/02/18 17:38 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 03/02/18 17:38 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 03/02/18 17:38 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 03/02/18 17:38 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 03/02/18 17:38 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 03/02/18 17:38 67-66-31.0 0.14 1
Chloromethane 0.33J ug/L 03/02/18 17:38 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 03/02/18 17:38 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 03/02/18 17:38 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 03/02/18 17:38 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 03/02/18 17:38 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 03/02/18 17:38 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 03/02/18 17:38 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 03/02/18 17:38 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 03/02/18 17:38 541-73-11.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:MW-4 Lab ID:92374792004 Collected:02/26/18 12:10 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene 0.33U ug/L 03/02/18 17:38 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 03/02/18 17:38 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 03/02/18 17:38 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 03/02/18 17:38 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 03/02/18 17:38 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 03/02/18 17:38 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 03/02/18 17:38 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 03/02/18 17:38 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 03/02/18 17:38 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 03/02/18 17:38 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 03/02/18 17:38 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 03/02/18 17:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 03/02/18 17:38 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 03/02/18 17:38 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 03/02/18 17:38 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 03/02/18 17:38 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 03/02/18 17:38 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 03/02/18 17:38 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 03/02/18 17:38 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 03/02/18 17:38 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 03/02/18 17:38 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 03/02/18 17:38 91-20-31.0 0.24 1
Styrene 0.26U ug/L 03/02/18 17:38 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 03/02/18 17:38 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 03/02/18 17:38 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 03/02/18 17:38 127-18-41.0 0.46 1
Toluene 0.26U ug/L 03/02/18 17:38 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 03/02/18 17:38 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 03/02/18 17:38 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 03/02/18 17:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 03/02/18 17:38 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 03/02/18 17:38 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 03/02/18 17:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 03/02/18 17:38 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 03/02/18 17:38 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 03/02/18 17:38 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 03/02/18 17:38 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 03/02/18 17:38 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 03/02/18 17:38 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/02/18 17:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %03/02/18 17:38 17060-07-070-130 1
Toluene-d8 (S)97 %03/02/18 17:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:TVL BLK Lab ID:92374792005 Collected:02/26/18 09:00 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 03/02/18 13:18 67-64-125.0 10.0 1
Benzene 0.25U ug/L 03/02/18 13:18 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 03/02/18 13:18 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 03/02/18 13:18 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 03/02/18 13:18 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 03/02/18 13:18 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 03/02/18 13:18 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 03/02/18 13:18 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 03/02/18 13:18 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 03/02/18 13:18 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 03/02/18 13:18 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 03/02/18 13:18 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 03/02/18 13:18 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 03/02/18 13:18 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 03/02/18 13:18 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 03/02/18 13:18 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 03/02/18 13:18 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 03/02/18 13:18 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 03/02/18 13:18 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 03/02/18 13:18 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 03/02/18 13:18 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 03/02/18 13:18 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 03/02/18 13:18 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 03/02/18 13:18 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 03/02/18 13:18 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 03/02/18 13:18 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 03/02/18 13:18 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 03/02/18 13:18 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 03/02/18 13:18 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 03/02/18 13:18 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 03/02/18 13:18 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 03/02/18 13:18 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 03/02/18 13:18 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 03/02/18 13:18 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 03/02/18 13:18 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 03/02/18 13:18 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 03/02/18 13:18 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 03/02/18 13:18 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 03/02/18 13:18 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 03/02/18 13:18 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 03/02/18 13:18 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 03/02/18 13:18 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 03/02/18 13:18 91-20-31.0 0.24 1
Styrene 0.26U ug/L 03/02/18 13:18 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 03/02/18 13:18 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 03/02/18 13:18 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
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Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:TVL BLK Lab ID:92374792005 Collected:02/26/18 09:00 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 03/02/18 13:18 127-18-41.0 0.46 1
Toluene 0.26U ug/L 03/02/18 13:18 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 03/02/18 13:18 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 03/02/18 13:18 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 03/02/18 13:18 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 03/02/18 13:18 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 03/02/18 13:18 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 03/02/18 13:18 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 03/02/18 13:18 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 03/02/18 13:18 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 03/02/18 13:18 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 03/02/18 13:18 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 03/02/18 13:18 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 03/02/18 13:18 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %03/02/18 13:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %03/02/18 13:18 17060-07-070-130 1
Toluene-d8 (S)98 %03/02/18 13:18 2037-26-570-130 1
Sample:Equip Blk Lab ID:92374792006 Collected:02/26/18 09:00 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 03/08/18 06:25 7440-36-002/28/18 01:305.0 3.9 1
Arsenic 5.0U ug/L 03/08/18 06:25 7440-38-202/28/18 01:3010.0 5.0 1
Barium 2.5U ug/L 03/08/18 06:25 7440-39-302/28/18 01:305.0 2.5 1
Beryllium 0.50U ug/L 03/08/18 06:25 7440-41-702/28/18 01:301.0 0.50 1
Cadmium 0.50U ug/L 03/08/18 06:25 7440-43-902/28/18 01:301.0 0.50 1
Chromium 2.5U ug/L 03/08/18 06:25 7440-47-302/28/18 01:305.0 2.5 1
Cobalt 2.5U ug/L 03/05/18 17:21 7440-48-402/28/18 01:305.0 2.5 1
Copper 2.5U ug/L 03/08/18 06:25 7440-50-802/28/18 01:305.0 2.5 1
Lead 2.5U ug/L 03/08/18 06:25 7439-92-102/28/18 01:305.0 2.5 1
Nickel 2.5U ug/L 03/08/18 06:25 7440-02-002/28/18 01:305.0 2.5 1
Selenium 5.0U ug/L 03/08/18 06:25 7782-49-202/28/18 01:3010.0 5.0 1
Silver 2.5U ug/L 03/08/18 06:25 7440-22-402/28/18 01:305.0 2.5 1
Thallium 5.0U ug/L 03/08/18 06:25 7440-28-002/28/18 01:3010.0 5.0 1
Vanadium 2.5U ug/L 03/08/18 06:25 7440-62-202/28/18 01:305.0 2.5 1
Zinc 5.0U ug/L 03/08/18 06:25 7440-66-602/28/18 01:3010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 02/28/18 16:45 7439-97-602/27/18 09:550.20 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
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Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:Equip Blk Lab ID:92374792006 Collected:02/26/18 09:00 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 03/02/18 13:35 67-64-125.0 10.0 1
Benzene 0.25U ug/L 03/02/18 13:35 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 03/02/18 13:35 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 03/02/18 13:35 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 03/02/18 13:35 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 03/02/18 13:35 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 03/02/18 13:35 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 03/02/18 13:35 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 03/02/18 13:35 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 03/02/18 13:35 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 03/02/18 13:35 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 03/02/18 13:35 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 03/02/18 13:35 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 03/02/18 13:35 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 03/02/18 13:35 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 03/02/18 13:35 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 03/02/18 13:35 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 03/02/18 13:35 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 03/02/18 13:35 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 03/02/18 13:35 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 03/02/18 13:35 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 03/02/18 13:35 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 03/02/18 13:35 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 03/02/18 13:35 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 03/02/18 13:35 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 03/02/18 13:35 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 03/02/18 13:35 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 03/02/18 13:35 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 03/02/18 13:35 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 03/02/18 13:35 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 03/02/18 13:35 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 03/02/18 13:35 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 03/02/18 13:35 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 03/02/18 13:35 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 03/02/18 13:35 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 03/02/18 13:35 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 03/02/18 13:35 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 03/02/18 13:35 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 03/02/18 13:35 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 03/02/18 13:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 03/02/18 13:35 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 03/02/18 13:35 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 03/02/18 13:35 91-20-31.0 0.24 1
Styrene 0.26U ug/L 03/02/18 13:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 03/02/18 13:35 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 03/02/18 13:35 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Sample:Equip Blk Lab ID:92374792006 Collected:02/26/18 09:00 Received:02/26/18 14:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 03/02/18 13:35 127-18-41.0 0.46 1
Toluene 0.26U ug/L 03/02/18 13:35 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 03/02/18 13:35 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 03/02/18 13:35 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 03/02/18 13:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 03/02/18 13:35 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 03/02/18 13:35 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 03/02/18 13:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 03/02/18 13:35 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 03/02/18 13:35 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 03/02/18 13:35 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 03/02/18 13:35 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 03/02/18 13:35 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 03/02/18 13:35 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/02/18 13:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/02/18 13:35 17060-07-070-130 1
Toluene-d8 (S)98 %03/02/18 13:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
399807
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2217347
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792006
Matrix:Water
AnalyzedMDL
Mercury ug/L 0.10U 0.20 02/28/18 15:470.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2217348LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2217349MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92374788001
2217350
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 107 75-125115 7 252.5ND 2.7 2.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
399961
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2218187
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792006
Matrix:Water
AnalyzedMDL
Antimony ug/L 3.9U 5.0 03/08/18 05:363.9
Arsenic ug/L 5.0U 10.0 03/08/18 05:365.0
Barium ug/L 2.5U 5.0 03/08/18 05:362.5
Beryllium ug/L 0.50U 1.0 03/08/18 05:360.50
Cadmium ug/L 0.50U 1.0 03/08/18 05:360.50
Chromium ug/L 2.5U 5.0 03/08/18 05:362.5
Cobalt ug/L 2.5U 5.0 03/05/18 16:222.5
Copper ug/L 2.5U 5.0 03/08/18 05:362.5
Lead ug/L 2.5U 5.0 03/08/18 05:362.5
Nickel ug/L 2.5U 5.0 03/08/18 05:362.5
Selenium ug/L 5.0U 10.0 03/08/18 05:365.0
Silver ug/L 2.5U 5.0 03/08/18 05:362.5
Thallium ug/L 5.0U 10.0 03/08/18 05:365.0
Vanadium ug/L 2.5U 5.0 03/08/18 05:362.5
Zinc ug/L 5.0U 10.0 03/08/18 05:365.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2218188LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 465500 93 80-120
Barium ug/L 479500 96 80-120
Beryllium ug/L 468500 94 80-120
Cadmium ug/L 460500 92 80-120
Chromium ug/L 503500 101 80-120
Cobalt ug/L 477500 95 80-120
Copper ug/L 498500 100 80-120
Lead ug/L 478500 96 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 443500 89 80-120
Silver ug/L 241250 97 80-120
Thallium ug/L 472500 94 80-120
Vanadium ug/L 469500 94 80-120
Zinc ug/L 504500 101 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2218189MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92374940001
2218190
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-125103 1 20500ND509515
Arsenic ug/L 500 98 75-125100 2 20500ND490499
Barium ug/L 500 99 75-125100 1 2050055.9 551 557
Beryllium ug/L 500 99 75-125100 2 20500ND493502
Cadmium ug/L 500 96 75-12597 1 20500ND480487
Chromium ug/L 500 102 75-125104 1 20500107619628
Cobalt ug/L 500 97 75-12598 1 20500ND485491
Copper ug/L 500 104 75-125105 1 20500ND520524
Lead ug/L 500 98 75-12599 2 20500ND488497
Nickel ug/L 500 97 75-12599 2 2050015.6 503 512
Selenium ug/L 500 97 75-12598 2 20500ND486494
Silver ug/L 250 103 75-125104 1 20250ND259261
Thallium ug/L 500 97 75-12599 2 2050014.3 499 507
Vanadium ug/L 500 98 75-12599 2 20500ND489497
Zinc ug/L 500 103 75-125105 2 2050024.0 541 550
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
400341
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792005, 92374792006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2220333
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792005, 92374792006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L 0.33U 1.0 03/02/18 12:130.33
1,1,1-Trichloroethane ug/L 0.48U 1.0 03/02/18 12:130.48
1,1,2,2-Tetrachloroethane ug/L 0.40U 1.0 03/02/18 12:130.40
1,1,2-Trichloroethane ug/L 0.29U 1.0 03/02/18 12:130.29
1,1-Dichloroethane ug/L 0.32U 1.0 03/02/18 12:130.32
1,1-Dichloroethene ug/L 0.56U 1.0 03/02/18 12:130.56
1,1-Dichloropropene ug/L 0.49U 1.0 03/02/18 12:130.49
1,2,3-Trichlorobenzene ug/L 0.33U 1.0 03/02/18 12:130.33
1,2,3-Trichloropropane ug/L 0.41U 1.0 03/02/18 12:130.41
1,2,4-Trichlorobenzene ug/L 0.35U 1.0 03/02/18 12:130.35
1,2-Dibromo-3-chloropropane ug/L 2.0U 2.0 03/02/18 12:132.0
1,2-Dibromoethane (EDB)ug/L 0.27U 1.0 03/02/18 12:130.27
1,2-Dichlorobenzene ug/L 0.30U 1.0 03/02/18 12:130.30
1,2-Dichloroethane ug/L 0.24U 1.0 03/02/18 12:130.24
1,2-Dichloropropane ug/L 0.27U 1.0 03/02/18 12:130.27
1,3-Dichlorobenzene ug/L 0.24U 1.0 03/02/18 12:130.24
1,3-Dichloropropane ug/L 0.28U 1.0 03/02/18 12:130.28
1,4-Dichlorobenzene ug/L 0.33U 1.0 03/02/18 12:130.33
2,2-Dichloropropane ug/L 0.13U 1.0 03/02/18 12:130.13
2-Butanone (MEK)ug/L 0.96U 5.0 03/02/18 12:130.96
2-Chlorotoluene ug/L 0.35U 1.0 03/02/18 12:130.35
2-Hexanone ug/L 0.46U 5.0 03/02/18 12:130.46
4-Chlorotoluene ug/L 0.31U 1.0 03/02/18 12:130.31
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 5.0 03/02/18 12:130.33
Acetone ug/L 10.0U 25.0 03/02/18 12:1310.0
Benzene ug/L 0.25U 1.0 03/02/18 12:130.25
Bromobenzene ug/L 0.30U 1.0 03/02/18 12:130.30
Bromochloromethane ug/L 0.17U 1.0 03/02/18 12:130.17
Bromodichloromethane ug/L 0.18U 1.0 03/02/18 12:130.18
Bromoform ug/L 0.26U 1.0 03/02/18 12:130.26
Bromomethane ug/L 0.29U 2.0 03/02/18 12:130.29
Carbon tetrachloride ug/L 0.25U 1.0 03/02/18 12:130.25
Chlorobenzene ug/L 0.23U 1.0 03/02/18 12:130.23
Chloroethane ug/L 0.54U 1.0 03/02/18 12:130.54
Chloroform ug/L 0.31J 1.0 03/02/18 12:130.14
Chloromethane ug/L 0.11U 1.0 03/02/18 12:130.11
cis-1,2-Dichloroethene ug/L 0.19U 1.0 03/02/18 12:130.19
cis-1,3-Dichloropropene ug/L 0.13U 1.0 03/02/18 12:130.13
Dibromochloromethane ug/L 0.21U 1.0 03/02/18 12:130.21
Dibromomethane ug/L 0.21U 1.0 03/02/18 12:130.21
Dichlorodifluoromethane ug/L 0.21U 1.0 03/02/18 12:130.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
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Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2220333
Associated Lab Samples:92374792001, 92374792002, 92374792003, 92374792004, 92374792005, 92374792006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L 0.12U 1.0 03/02/18 12:130.12
Ethylbenzene ug/L 0.30U 1.0 03/02/18 12:130.30
Hexachloro-1,3-butadiene ug/L 0.71U 1.0 03/02/18 12:130.71
m&p-Xylene ug/L 0.66U 2.0 03/02/18 12:130.66
Methyl-tert-butyl ether ug/L 0.21U 1.0 03/02/18 12:130.21
Methylene Chloride ug/L 0.97U 1.0 03/02/18 12:130.97
Naphthalene ug/L 0.24U 1.0 03/02/18 12:130.24
o-Xylene ug/L 0.23U 1.0 03/02/18 12:130.23
p-Isopropyltoluene ug/L 0.31U 1.0 03/02/18 12:130.31
Styrene ug/L 0.26U 1.0 03/02/18 12:130.26
Tetrachloroethene ug/L 0.46U 1.0 03/02/18 12:130.46
Toluene ug/L 0.26U 1.0 03/02/18 12:130.26
trans-1,2-Dichloroethene ug/L 0.49U 1.0 03/02/18 12:130.49
trans-1,3-Dichloropropene ug/L 0.26U 1.0 03/02/18 12:130.26
Trichloroethene ug/L 0.47U 1.0 03/02/18 12:130.47
Trichlorofluoromethane ug/L 0.20U 1.0 03/02/18 12:130.20
Vinyl acetate ug/L 0.35U 2.0 03/02/18 12:130.35
Vinyl chloride ug/L 0.62U 1.0 03/02/18 12:130.62
Xylene (Total)ug/L 0.66U 1.0 03/02/18 12:130.66
1,2-Dichloroethane-d4 (S)%102 70-130 03/02/18 12:13
4-Bromofluorobenzene (S)%99 70-130 03/02/18 12:13
Toluene-d8 (S)%100 70-130 03/02/18 12:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2220334LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.450 109 80-125
1,1,1-Trichloroethane ug/L 53.050 106 71-129
1,1,2,2-Tetrachloroethane ug/L 52.550 105 79-124
1,1,2-Trichloroethane ug/L 54.050 108 85-125
1,1-Dichloroethane ug/L 48.150 96 73-126
1,1-Dichloroethene ug/L 54.750 109 66-135
1,1-Dichloropropene ug/L 52.150 104 74-135
1,2,3-Trichlorobenzene ug/L 56.250 112 73-135
1,2,3-Trichloropropane ug/L 54.450 109 75-130
1,2,4-Trichlorobenzene ug/L 56.750 113 75-134
1,2-Dibromo-3-chloropropane ug/L 49.750 99 71-133
1,2-Dibromoethane (EDB)ug/L 53.150 106 83-124
1,2-Dichlorobenzene ug/L 55.750 111 80-133
1,2-Dichloroethane ug/L 49.050 98 67-128
1,2-Dichloropropane ug/L 52.650 105 75-132
1,3-Dichlorobenzene ug/L 53.550 107 77-130
1,3-Dichloropropane ug/L 53.450 107 76-131
1,4-Dichlorobenzene ug/L 53.050 106 78-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
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Asheville, NC 28804
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2220334LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 55.150 110 40-160
2-Butanone (MEK)ug/L 92.7100 93 61-144
2-Chlorotoluene ug/L 51.350 103 74-132
2-Hexanone ug/L 107100 107 68-143
4-Chlorotoluene ug/L 52.450 105 76-133
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 72-135
Acetone ug/L 91.6100 92 48-146
Benzene ug/L 50.650 101 80-125
Bromobenzene ug/L 53.050 106 75-125
Bromochloromethane ug/L 54.150 108 71-125
Bromodichloromethane ug/L 51.550 103 78-124
Bromoform ug/L 44.650 89 71-128
Bromomethane ug/L 31.050 62 40-160
Carbon tetrachloride ug/L 50.650 101 69-131
Chlorobenzene ug/L 51.050 102 81-122
Chloroethane ug/L 43.750 87 39-148
Chloroform ug/L 48.650 97 73-127
Chloromethane ug/L 42.050 84 44-146
cis-1,2-Dichloroethene ug/L 48.750 97 74-124
cis-1,3-Dichloropropene ug/L 53.550 107 72-132
Dibromochloromethane ug/L 52.650 105 78-125
Dibromomethane ug/L 53.150 106 82-120
Dichlorodifluoromethane ug/L 46.450 93 34-157
Diisopropyl ether ug/L 47.050 94 69-135
Ethylbenzene ug/L 52.350 105 79-121
Hexachloro-1,3-butadiene ug/L 57.850 116 72-131
m&p-Xylene ug/L 105100 105 81-124
Methyl-tert-butyl ether ug/L 48.950 98 74-131
Methylene Chloride ug/L 47.850 96 64-133
Naphthalene ug/L 57.850 116 73-133
o-Xylene ug/L 53.250 106 79-131
p-Isopropyltoluene ug/L 56.050 112 80-131
Styrene ug/L 51.650 103 84-126
Tetrachloroethene ug/L 47.550 95 78-122
Toluene ug/L 51.250 102 80-121
trans-1,2-Dichloroethene ug/L 50.550 101 71-127
trans-1,3-Dichloropropene ug/L 49.850 100 69-141
Trichloroethene ug/L 50.750 101 78-122
Trichlorofluoromethane ug/L 42.350 85 53-137
Vinyl acetate ug/L 105100 105 40-160
Vinyl chloride ug/L 46.550 93 58-137
Xylene (Total)ug/L 159150 106 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2220335MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92375276002
2220336
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 105 70-130109 4 3020ND21.1 21.9
1,1,1-Trichloroethane ug/L 20 104 70-130101 3 3020ND20.8 20.2
1,1,2,2-Tetrachloroethane ug/L 20 102 70-130102 0 3020ND20.4 20.4
1,1,2-Trichloroethane ug/L 20 99 70-13096 4 3020ND19.9 19.2
1,1-Dichloroethane ug/L 20 99 70-13097 2 3020ND19.8 19.3
1,1-Dichloroethene ug/L 20 106 70-166103 3 3020ND21.2 20.7
1,1-Dichloropropene ug/L 20 101 70-130100 0 3020ND20.1 20.0
1,2,3-Trichlorobenzene ug/L 20 113 70-130116 3 3020ND22.5 23.2
1,2,3-Trichloropropane ug/L 20 105 70-130103 2 3020ND20.9 20.6
1,2,4-Trichlorobenzene ug/L 20 114 70-130112 2 3020ND22.8 22.3
1,2-Dibromo-3-
chloropropane ug/L 20 115 70-130111 3 3020ND23.0 22.2
1,2-Dibromoethane (EDB)ug/L 20 104 70-130103 1 3020ND20.7 20.6
1,2-Dichlorobenzene ug/L 20 111 70-130110 1 3020ND22.2 22.0
1,2-Dichloroethane ug/L 20 94 70-13093 1 3020ND18.8 18.6
1,2-Dichloropropane ug/L 20 101 70-13097 4 3020ND20.2 19.4
1,3-Dichlorobenzene ug/L 20 114 70-130110 4 3020ND22.8 22.0
1,3-Dichloropropane ug/L 20 105 70-130108 3 3020ND21.0 21.7
1,4-Dichlorobenzene ug/L 20 112 70-130108 4 3020ND22.5 21.6
2,2-Dichloropropane ug/L 20 99 70-13098 1 3020ND19.8 19.6
2-Butanone (MEK)ug/L 40 94 70-13096 1 3040ND37.7 38.2
2-Chlorotoluene ug/L 20 116 70-130113 2 3020ND23.2 22.6
2-Hexanone ug/L 40 104 70-130103 1 3040ND41.6 41.1
4-Chlorotoluene ug/L 20 117 70-130113 3 3020ND23.4 22.7
4-Methyl-2-pentanone
(MIBK)ug/L 40 97 70-13095 2 3040ND38.8 37.9
Acetone ug/L 40 96 70-13096 1 3040ND38.6 38.3
Benzene ug/L 20 98 70-14895 3 3020ND19.6 18.9
Bromobenzene ug/L 20 114 70-130110 4 3020ND22.9 22.1
Bromochloromethane ug/L 20 99 70-13097 2 3020ND19.8 19.5
Bromodichloromethane ug/L 20 101 70-13099 2 3020ND20.3 19.8
Bromoform ug/L 20 113 70-130116 2 3020ND22.6 23.2
Bromomethane ug/L 20 78 70-13081 4 3020ND15.5 16.2
Carbon tetrachloride ug/L 20 109 70-130104 5 3020ND21.8 20.8
Chlorobenzene ug/L 20 106 70-146104 2 3020ND21.1 20.8
Chloroethane ug/L 20 105 70-130102 2 3020ND20.9 20.5
Chloroform ug/L 20 93 70-13092 1 3020ND18.6 18.4
Chloromethane ug/L 20 85 70-13083 2 3020ND17.0 16.6
cis-1,2-Dichloroethene ug/L 20 102 70-130100 1 3020ND20.3 20.1
cis-1,3-Dichloropropene ug/L 20 99 70-13096 4 3020ND19.9 19.1
Dibromochloromethane ug/L 20 113 70-130111 1 3020ND22.5 22.2
Dibromomethane ug/L 20 98 70-13094 4 3020ND19.6 18.9
Dichlorodifluoromethane ug/L 20 90 70-13091 1 3020ND18.0 18.2
Diisopropyl ether ug/L 20 101 70-13098 3 3020ND20.2 19.6
Ethylbenzene ug/L 20 110 70-130108 2 3020ND22.1 21.6
Hexachloro-1,3-butadiene ug/L 20 116 70-130110 5 3020ND23.2 22.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2220335MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92375276002
2220336
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 113 70-130111 2 3040ND45.1 44.2
Methyl-tert-butyl ether ug/L 20 88 70-13087 1 3020ND17.6 17.5
Methylene Chloride ug/L 20 91 70-13089 3 3020ND18.2 17.7
Naphthalene ug/L 20 112 70-130113 1 3020ND22.4 22.6
o-Xylene ug/L 20 108 70-130105 3 3020ND21.5 20.9
p-Isopropyltoluene ug/L 20 119 70-130115 3 3020ND23.8 23.1
Styrene ug/L 20 104 70-130104 1 3020ND20.7 20.9
Tetrachloroethene ug/L 20 104 70-130100 5 3020ND20.8 19.9
Toluene ug/L 20 100 70-15594 6 3020ND20.0 18.9
trans-1,2-Dichloroethene ug/L 20 104 70-130102 2 3020ND20.8 20.4
trans-1,3-Dichloropropene ug/L 20 101 70-13098 4 3020ND20.3 19.5
Trichloroethene ug/L 20 102 69-15199 2 3020ND20.3 19.8
Trichlorofluoromethane ug/L 20 101 70-13096 5 3020ND20.2 19.3
Vinyl acetate ug/L 40 95 70-13095 0 3040ND37.9 38.0
Vinyl chloride ug/L 20 106 70-130105 1 3020ND21.2 21.0
Xylene (Total)ug/L 60 111 70-130109 2 3060ND66.6 65.1
1,2-Dichloroethane-d4 (S)%109 70-130105
4-Bromofluorobenzene (S)%93 70-13096
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92374792
Land Fill MW's 2/26
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92374792001 MW-1
92374792002 MW-2
92374792003 MW-3
92374792004 MW-4
92374792001 399961 399978MW-1 EPA 3010A EPA 6010
92374792002 399961 399978MW-2 EPA 3010A EPA 6010
92374792003 399961 399978MW-3 EPA 3010A EPA 6010
92374792004 399961 399978MW-4 EPA 3010A EPA 6010
92374792006 399961 399978Equip Blk EPA 3010A EPA 6010
92374792001 399807 399888MW-1 EPA 7470 EPA 7470
92374792002 399807 399888MW-2 EPA 7470 EPA 7470
92374792003 399807 399888MW-3 EPA 7470 EPA 7470
92374792004 399807 399888MW-4 EPA 7470 EPA 7470
92374792006 399807 399888Equip Blk EPA 7470 EPA 7470
92374792001 400341MW-1 EPA 8260
92374792002 400341MW-2 EPA 8260
92374792003 400341MW-3 EPA 8260
92374792004 400341MW-4 EPA 8260
92374792005 400341TVL BLK EPA 8260
92374792006 400341Equip Blk EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2018 03:19 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 31
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