5002_JacksonCounty_MSWLF_GW_DIN28754_20171010

2/7/18

February 2018
Jackson County Closed Municipal Solid Waste Landfill
Fall 2017 Semiannual Water Quality Monitoring
Report
Prepared for Jackson County Solid Waste Department

Project Number: 761480-01.01
\\asheville1\asheville\Projects\Jackson County\Dillsboro GW\Reports\2017\Fall\5002October2017 Semiannual Water Quality Report.docx
February 2018
Jackson County Closed Municipal Solid Waste Landfill
Fall 2017 Semiannual Water Quality Monitoring
Report

Prepared for
Jackson County Solid Waste Department
401 Grindstaff Cove Road
Sylva, North Carolina 28779
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801

_____________________________________
Alec Macbeth, PG
Project Geologist

Fall 2017 Semiannual Water Quality Monitoring Report i February 2018
TABLE OF CONTENTS
1 Introduction ................................................................................................................................ 1
2 Semiannual Monitoring ........................................................................................................... 3
2.1 Groundwater, Surface Water, Domestic Well and Leachate Sampling ........................................... 3
Monitoring Well Purging and Sampling Methods ................................................................. 3
Surface Water Sampling Methods ................................................................................................ 4
Leachate Sampling Methods .......................................................................................................... 4
Domestic Well Sampling Methods ............................................................................................... 5
2.2 Sample Handling, Documentation, and Analysis .................................................................................... 5
3 Findings ........................................................................................................................................ 7
3.1 Analytical Results ................................................................................................................................................. 7
Groundwater ......................................................................................................................................... 8
Surface Water ..................................................................................................................................... 10
Leachate ............................................................................................................................................... 11
Domestic Well .................................................................................................................................... 11
3.2 Groundwater Flow Direction ........................................................................................................................ 12
4 Summary .................................................................................................................................... 13
4.1 Groundwater Quality....................................................................................................................................... 13
Metals.................................................................................................................................................... 13
VOCs and SVOCs .............................................................................................................................. 13
Field Parameters and Other Constituents ............................................................................... 14
4.2 Surface Water Quality ..................................................................................................................................... 14
4.3 Domestic Well Water Quality ...................................................................................................................... 14
4.4 Leachate Quality ............................................................................................................................................... 14
5 Future Activities ....................................................................................................................... 16
6 References ................................................................................................................................. 17

Fall 2017 Semiannual Water Quality Monitoring Report ii February 2018
TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Summary of Analytical Results
Table 3 Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in
the Leachate Sample (LT-01)
Table 4 Well Construction Details and Corresponding Elevations
FIGURES
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Generalized Groundwater Flow Direction
Figure 4 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time (Monitoring Well MW-01)
Figure 5 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time (Monitoring Well MW-05R)
APPENDICES
Appendix A Well Sampling Logs and Equipment Documentation & Instrument Calibration
Data Sheets
Appendix B Reports of Laboratory Analysis, Chain-of-Custody Documentation, and
Certificates of Analysis

Fall 2017 Semiannual Water Quality Monitoring Report iii February 2018
ABBREVIATIONS
µg/L micrograms per liter
µS/cm microsiemens per centimeter
Altamont Altamont Environmental, Inc.
Anchor QEA Anchor QEA of North Carolina, PLLC
BOD biochemical oxygen demand
CAER Five-Year Corrective Action Evaluation Report
CAP Corrective Action Plan
CFR Code of Federal Regulations
COD chemical oxygen demand
DENR North Carolina Department of Environment and Natural Resources (now the
DEQ)
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
EPA U.S. Environmental Protection Agency
GWPS Groundwater Protection Standards
IMAC interim maximum allowable concentration
MDL method detection limit
mg/L milligrams per liter
MNA monitored natural attenuation
MRL method reporting limit
MSWLF Municipal Solid Waste Landfill
mV millivolts
NCAC North Carolina Administrative Code
NTU nephelometric turbidity units
ORP oxidation reduction potential
PWR partially weathered rock
SM Standard Method
SU Standard Units
SWS Solid Waste Section
SWSL Solid Waste Section Limit
TOC total organic carbon
TWSA Tuckaseigee Water & Sewer Authority
VOC volatile organic compound

Fall 2017 Semiannual Water Quality Monitoring Report 1 February 2018
1 Introduction
The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill
(MSWLF [the Site]), located approximately 0.75 miles west of Dillsboro, North Carolina, on the
northeast side of Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the
landfill is governed by the North Carolina Department of Environmental Quality (DEQ), Division of
Waste Management (DWM), Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson
County. The landfill permit requires semiannual monitoring of groundwater and surface water
quality.
Since October 2007, when Altamont Environmental, Inc. [Altamont]1 began performing water quality
monitoring events, groundwater quality monitoring has indicated persistent low-level concentrations
of constituents that exceed groundwater standards. In response to the continued exceedances of
analyzed constituents, an Assessment of Corrective Measures was submitted to the North Carolina
Department of Environment and Natural Resources (DENR), which is now the DEQ, on September 7,
2010 (Altamont 2010). A Corrective Action Plan (CAP; Altamont 2011) was implemented upon
approval of the Assessment of Corrective Measures by the DEQ, as recorded in the September 1,
2011 letter Approval of the County’s Corrective Action Plan (DENR 2011). The implemented remedy
includes the extraction of leachate through dedicated submersible pumps installed within landfill gas
extraction wells, and disposal of the leachate into the Tuckaseigee Water & Sewer Authority (TWSA)
collection system. In addition to leachate extraction, groundwater natural attenuation parameters are
monitored and natural attenuation processes are evaluated. As discussed in the CAP, a corrective
action evaluation report is prepared every 5 years. The evaluation report analyzes the progress of the
approved corrective action remedy based on semiannual water quality monitoring data. The remedy
was implemented in a phased approach, reaching full implementation on September 6, 2013. The
first Five-Year Corrective Action Evaluation Report (CAER) was submitted by Altamont on October 31,
2016 (Altamont 2016), and concluded that the current conditions of the monitored natural
attenuation (MNA) parameters and Site geochemical parameters allow for slow degradation of the
constituents of concern. The next CAER will be submitted in the fall of 2021.
This report serves as the second semiannual water quality monitoring report for 2017 and the
thirteenth report following approval of the CAP. This report provides an evaluation of groundwater
and surface water quality based on the water quality monitoring network presented in Figure 2. The
generalized groundwater flow direction in the upper parts of the underlying aquifer system (within
the saprolite and partially weathered rock [PWR]; Figure 3) is also provided in this report.

1 Altamont became Anchor QEA of North Carolina, PLLC, on December 29, 2016.

Fall 2017 Semiannual Water Quality Monitoring Report 2 February 2018
In addition to groundwater and surface water monitoring results, this report includes volatile organic
compound (VOC) analysis of the extracted leachate and one domestic water well.
The water samples collected from the monitoring points during the fall sampling event were
analyzed for a range of parameters, as presented in Section 2.2 and Table 1 of this report.
The fall 2017 sampling event was performed on October 10 and 11, 2017, and is being reported in
accordance with the requirements stipulated in the DEQ Solid Waste Management Rules codified
under Title 15A, Subchapter 13B of the North Carolina Administrative Code (15A NCAC 13B).

Fall 2017 Semiannual Water Quality Monitoring Report 3 February 2018
2 Semiannual Monitoring
2.1 Groundwater, Surface Water, Domestic Well and Leachate Sampling
The closed MSWLF monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06,
and MW-07), surface water sample locations (SW-01 and SW-02), leachate sample location (LT-01),
and domestic well (DW-01) were sampled on October 10 and 11, 2017, by Anchor QEA of North
Carolina, PLLC (Anchor QEA). Static groundwater level measurements and all field parameter data are
included on the well sampling logs presented in Appendix A. Field equipment calibration logs for the
YSI 556 Multi-Parameter Water Quality Meter and the Hach 2100Q Turbidimeter are also provided in
Appendix A. The full suite of groundwater and surface water laboratory analytical results is presented
in the laboratory analysis reports in Appendix B.
MW-02 serves as the Site’s background monitoring well, due to its location outside of the
contamination plume. MW-01 and MW-06 are the Site’s upgradient monitoring wells, MW-03 and
MW-05R are located in the midgradient portion of the Site, and MW-04 and MW-07 monitor
downgradient portions of the Site. Monitoring wells MW-4 and MW-5 are screened in saprolite,
monitoring well MW-3 is screened in PWR, and monitoring wells MW-1, MW-2, MW-6, and MW-7
are screened in bedrock. Table 2 provides well construction details.
The monitoring wells and surface water, leachate, and domestic well sample locations are depicted in
Figure 2.
Monitoring Well Purging and Sampling Methods
Prior to monitoring well sampling, the static water level was gauged in each well, and an initial round
of field parameters consisting of pH, specific conductivity, dissolved oxygen (DO), turbidity,
temperature, and oxidation reduction potential (ORP) was measured.
Anchor QEA personnel used either low-flow techniques or disposable bailers to purge the
monitoring wells and collect groundwater samples, as discussed in Section 2.1.1.1. Total monitoring
well depth, depth to groundwater, and groundwater recharge rate determined the purging and
sample collection method employed at each monitoring well.
2.1.1.1 Monitoring Wells
Four of the seven monitoring wells (MW-03, MW-04, MW-06, and MW-07) were purged using low-
flow techniques in accordance with the procedures described in the U.S. Environmental Protection
Agency’s (EPA’s) Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures (EPA 1996).
During purging, field parameters (pH, specific conductivity, DO, ORP, turbidity, and temperature)
were measured and recorded approximately every 3 minutes. Well purging continued until these
parameters generally stabilized for three consecutive readings. The required stabilization criteria

Fall 2017 Semiannual Water Quality Monitoring Report 4 February 2018
were determined by the EPA Region 4 Science and Ecosystem Support Division’s Operating
Procedure: Groundwater Sampling (EPA 2017), and are summarized as follows:
• pH values within +/- 0.1 Standard Unit (SU)
• Specific conductivity values within +/- 5 percent
• Temperature, DO, and turbidity values within +/- 10 percent
• ORP values within +/- 10 millivolts (mV)
Once the parameters had stabilized, a groundwater sample was collected by a technician wearing a
new pair of nitrile gloves, using laboratory-supplied sample containers.
The remaining three monitoring wells were purged and sampled using bailing methods. MW-01 was
purged and sampled using a disposable Teflon bailer on October 11, 2017. A bailer was used to
purge and sample this monitoring well due to a bend in the casing that accommodates a flexible
Teflon bailer, but not a bladder pump. The well was purged of three successive well volumes prior to
sample collection. A round of field parameters was measured and recorded at the start of purging
and after each consecutive well volume was purged. After the third consecutive well volume was
purged, a groundwater sample was collected. MW-02 and MW-05R were purged dry with a
disposable polyethylene bailer on October 10, 2017, and the groundwater sample was collected on
the following day after the well had recharged. All field parameter data are shown in the well
sampling logs included in Appendix A.
Surface Water Sampling Methods
Surface water samples SW-01 and SW-02 were collected on October 10 and 11, 2017, respectively, at
designated locations from the Tuckasegee River, which is adjacent to and southwest of the landfill
(Figure 2). Sampling location SW-01 is representative of surface water quality upstream of the
landfill, and sampling location SW-02 is representative of surface water quality downstream of the
landfill. One round of field parameters was measured and recorded at each surface water sampling
location immediately prior to collecting the sample (Appendix A). The surface water samples were
collected in laboratory-provided sample containers by a technician wearing a new pair of nitrile
gloves.
Leachate Sampling Methods
Dedicated bottom-loading, air-powered pumps, air pressure lines, and a leachate force main
collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells
EW-1R, EW-2R, EW-3R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well
locations are presented in Figure 2. Leachate is pumped from the wells into a flow equalization tank,
which is connected to the TWSA wastewater collection system.

Fall 2017 Semiannual Water Quality Monitoring Report 5 February 2018
The flow equalization tank is situated to the northeast of the landfill, adjacent to the existing landfill
gas flare. A grab sample of leachate (LT-01) was collected on October 11, 2017, by taking a sample as
the leachate entered the flow equalization tank. One round of field parameters was measured and
recorded after collecting the sample (Appendix A).
Domestic Well Sampling Methods
The domestic well water sample (DW-01) was collected on October 10, 2017, from an outside spigot
at the private residence located at 318 Joe Wilkey Road, bordering the northern boundary of the
landfill (Figure 2). The well was purged of three successive volumes of 10 gallons each prior to
sample collection. During purging, a round of field parameters was measured and recorded at the
start of purging and after each consecutive 10-gallon volume was purged. After the third consecutive
volume was purged, a groundwater sample was collected. The domestic well water sample was
collected in laboratory-provided sample containers by a technician wearing a new pair of nitrile
gloves.
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to the closed MSWLF sampling locations are
provided in the sampling logs (Appendix A). Following sample collection, each groundwater, surface
water, leachate, and domestic well water sample was immediately placed on ice in a sample cooler
for transport to Prism Laboratory, a North Carolina-certified laboratory located in Charlotte, North
Carolina.
The groundwater samples collected from the monitoring wells were analyzed for the following
parameters (Table 1):
• Appendix II Metals, using EPA Methods 6020B and 7470A
• Appendix II VOCs, using EPA Method 8260B
• Appendix II SVOCs, using EPA Method 8270D
• MNA Parameters:
‒ Alkalinity, using Standard Method (SM) 2320B
‒ BOD (5-Day), using SM 5210B
‒ Carbon dioxide, hydrogen, ethane, ethene, and methane, using Analytical Method 20GAX
‒ COD, using SM 5220D
‒ Chloride, nitrate, and sulfate, using EPA Method 9056A
‒ Cyanide, using SM 4500-CN E
‒ Ferrous iron, using SM 3500-Fe D
‒ Sulfide, using SM 4500-S F
‒ TOC using SM 9060A
‒ Volatile fatty acids using AM23G

Fall 2017 Semiannual Water Quality Monitoring Report 6 February 2018
The surface water samples were analyzed for the following parameters:
• Appendix II Metals, using EPA Methods 6020B and 7470A
• Appendix II VOCs, using EPA Method 8260B
• Appendix II SVOCs, using EPA Method 8270D
The leachate sample was analyzed for the following parameters:
• Appendix I VOCs, using EPA Method 8260B
The domestic well sample was analyzed for the following parameters:
• Appendix I VOCs, using EPA Method 524.2
Note: Appendix I and II parameters are identified in Appendix I and II of the Code of Federal
Regulations (CFR), Title 40, Part 258.
Proper chain-of-custody documentation procedures were followed during collection and
transportation of each sample (Appendix B). Four trip blank samples for quality control/quality
assurance purposes were included in the sample coolers and analyzed for VOCs. The reports of
laboratory analysis are provided in Appendix B.

Fall 2017 Semiannual Water Quality Monitoring Report 7 February 2018
3 Findings
3.1 Analytical Results
The laboratory analytical results and field parameter data for the groundwater samples (MW-01
through MW-07), surface water samples (SW-01 and SW-02), leachate sample (LT-01), and domestic
well sample (DW-01) collected at or adjacent to the landfill are included in Appendices A and B in
hard copy, and have been submitted separately to the DEQ DWM SWS in the Electronic Data
Deliverable format, per DEQ guidelines (last updated on May 5, 2010).
As stipulated in the SWS documents referenced in the preceding paragraph, all laboratory analytical
results were reported and appropriately qualified as follows:
• Non-detections: Non-detections (non-detects) are values reported by the laboratory as
below method detection limits (MDLs). They are tabulated in Table 2, flagged with a “U”
qualifier. The MDL is the minimum concentration of a substance that can be measured and
reported by a laboratory with 99 percent confidence that the constituent concentration is
greater than zero.
• Solid Waste Section Limits: All detections (values above the MDL) were compared to the
constituent-specific Solid Waste Section Limits (SWSLs) established by the DEQ. The SWSL is
defined as the lowest concentration of a constituent in a sample that can be quantitatively
determined with suitable precision and accuracy. A non-italicized “J” qualifier is used by the
laboratory to mark parameters that are detected at estimated concentrations greater than the
MDL but less than the laboratory’s method reporting limit (MRL). The MRL is the minimum
concentration of a target analyte that can be accurately determined by the referenced
method.
• Estimated or “J”-Qualified: If the reported concentration is greater than the laboratory MDL
and MRL, but less than the SWSL, the analytical result is qualified as estimated and is flagged
with an italicized “J” qualifier by Anchor QEA, per SWS reporting requirements. In addition to
non-detects, detected concentrations of constituents below the applicable SWSLs are
included in Table 2.
• 2L Standard: Detected concentrations of constituents in groundwater samples were
compared to applicable North Carolina groundwater quality standards. For most constituents,
this standard is the 2L standard, defined in 15A NCAC 2L .0202. Detected concentrations of
analytes in groundwater with no established 2L standard were compared either to the interim
maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]) or Groundwater Protection Standards (GWPS),
pursuant to 15A NCAC 13B .1634.
• 2B Standard: Detections of analytes in surface water samples were compared to the surface
water quality standards described in 15A NCAC 2B (2B standards).

Fall 2017 Semiannual Water Quality Monitoring Report 8 February 2018
Table 2 presents a summary of detected constituents and outlines concentrations of analytes that
were above applicable SWSLs, as well as detected analytes that exceeded their respective 2L
standard, IMAC, GWPS, or 2B standard.
Groundwater
Measured field parameters and analytical results of groundwater samples collected from the
monitoring wells are discussed in the following sections.
3.1.1.1 Field Parameters
During groundwater sampling on October 10 and 11, 2017, pH readings were obtained. The pH
readings from samples collected from wells MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and
MW-07 ranged from 5.57 to 6.26, all below the pH range of 6.5 to 8.5 SU specified in 15A NCAC 02L
.0202[c] (Table 2). The recorded pH readings are consistent with historical data.
The turbidity in the wells sampled using low-flow techniques ranged from 2.06 nephelometric
turbidity units (NTUs) to 4.45 NTUs. The lowest turbidity (2.06 NTUs) was measured in the
groundwater sample collected from well MW-04. The turbidity values from the wells sampled using
bailing methods was 12.6 NTUs to 200 NTUs, with the highest value sampled from MW-5R. Elevated
turbidity levels are generally observed in monitoring wells that are purged via the bailer method.
Bailers were lowered gently to minimize water column disturbance when samples were collected.
DO concentrations at the Site ranged from 1.47 milligrams per liter (mg/L) in MW-07 to 8.92 mg/L in
MW-06. Specific conductivity concentrations at the Site ranged from 131 microsiemens per
centimeter (µS/cm) in MW-06 to 661 µS/cm in MW-07. ORP concentrations at the Site ranged from
48.0 mV in MW-01 to 284.8 mV in MW-03. Groundwater standards are not established for DO,
specific conductivity, or ORP.
3.1.1.2 Appendix II Metals
Fifteen metals were detected in the groundwater samples collected from one or more of the
monitoring wells. Seven of the metals (barium, cadmium, cobalt, copper, nickel, thallium, and zinc)
were detected at concentrations above the associated SWSLs in one or more of the monitoring wells
(Table 2).
Six of the metals (antimony, cadmium, cobalt, thallium, vanadium, and zinc) were detected at
concentrations above their respective 2L, IMAC, or GWPS water quality standards in one or more of
the monitoring wells.
Antimony was detected above the IMAC in the groundwater samples collected from MW-01 and
MW-05R, at concentrations of 4.3 J micrograms per liter (µg/L) and 4.1 J µg/L, respectively.

Fall 2017 Semiannual Water Quality Monitoring Report 9 February 2018
Cadmium was detected in MW-01 at a concentration of 38 µg/L, which exceeded the 2L standard of
2 µg/L. Cadmium concentrations in the samples collected from MW-01 have exceeded the 2L
standard during several prior sampling events. Cadmium was detected at “J”-flagged values in five
other monitoring wells (MW-03, MW-04, MW-05R, MW-06, and MW-07), below the 2L standard;
these results are consistent with historical data.
Cobalt was detected above the IMAC in all groundwater samples, with the exception of MW-07.
Exceedances of cobalt in these samples showed concentrations ranging from 1.5 J µg/L (MW-02) to
92 µg/L (MW-01). Historically, cobalt has been present above its applicable water quality standard in
groundwater samples from all monitoring wells, with the recent exception of MW-07.
Thallium was detected in MW-01, MW-03, MW-05R, and MW-06. Three of the groundwater samples,
collected from wells MW-01 (6.1 µg/L), MW-05R (0.27 J µg/L), and MW-06 (1.6 J µg/L), contained
concentrations that were above the IMAC water quality standard of 0.2 µg/L. Historically, thallium
has been detected above the water quality standard in samples collected from multiple groundwater
monitoring wells.
Vanadium was detected above the IMAC water quality standard of 0.3 µg/L in MW-01, MW-02,
MW-05R, MW-06, and MW-07, at concentrations ranging from 0.46 J µg/L (MW-07) to 12 J µg/L
(MW-05R). Historically, vanadium has been detected above the water quality standard in samples
collected from multiple groundwater monitoring wells.
Zinc was detected in MW-01 at a concentration of 1,200 µg/L, which exceeded the 2L standard of
1,000 µg/L. Historically, zinc has not been detected above its water quality standard in samples
collected from any of the groundwater monitoring wells.
3.1.1.3 Appendix II VOCs and SVOCs
No VOCs were detected at concentrations above their respective 2L standards in the groundwater
samples collected from the monitoring wells during the fall 2017 water quality monitoring event.
One SVOC, 1,4-dichlorobenzene, was detected in monitoring wells MW-01, MW-03, MW-04, MW-
05R, and MW-07 at concentrations above the SWSL. This compound was detected at concentrations
above the 2L standard in monitoring wells MW-01 (7.5 µg/L) and MW-05R (6.9 µg/L). Historical
concentration-versus-time graphs were created for those monitoring wells where VOC
concentrations above the 2L standards were detected during previous sampling events. 1,4-
dichlorobenzene is included in the analyses for VOCs using EPA Method 8260B and for SVOCs using
EPA Method 8270D laboratory tests. In these analyses, the most protective (higher) value has been
assessed. Because this analyte appears in both laboratory tests, the results are included in the
concentration-versus-time graphs (Figures 4 and 5).

Fall 2017 Semiannual Water Quality Monitoring Report 10 February 2018
A review of historical groundwater data indicates that 1,4-dichlorobenzene has been detected at
relatively consistent concentrations at the Site for the past several years. As described in Section
3.1.2, historical surface water samples from the Tuckasegee River, which likely receives discharge
from the saprolite groundwater-bearing zone, have consistently shown no detection of 1,4-
dichlorobenzene, or other VOCs or SVOCs included in the applicable laboratory methods.
3.1.1.4 Natural Attenuation Parameters
Groundwater samples collected from all monitoring wells were analyzed for additional parameters as
follows: alkalinity, BOD, COD, carbon dioxide, chloride, cyanide, ethane, ethene, hydrogen (for wells
MW-03, MW-04, MW-06, and MW-07 only), methane, iron (ferrous), nitrate, sulfate, sulfide, TOC, and
volatile fatty acids (Table 2). These parameters were detected in one or more groundwater samples
collected from the monitoring wells.
Many of these parameters do not have established groundwater standards. Of the parameters that
do have established groundwater standards, only those detected in groundwater samples from MW-
01 (13,000 µg/L), MW-05 (1,400 µg/L), and MW-06 (2,500 µg/L) exceeded the ferrous iron 2L
standard of 300 µg/L. An in-depth analysis of the MNA parameters that apply to the Site’s
constituents of concern was performed in the first CAER (Altamont 2016), which concluded that MNA
data provide evidence that both reductive degradation and aerobic degradation are occurring in
different portions of the Site.
Surface Water
The following sections summarize measured field parameters and analytical results associated with
the two surface water samples collected during the fall 2017 sampling event.
3.1.2.1 Field Parameters
The pH readings for the upstream (SW-01) and downstream (SW-02) surface water samples were
recorded at 7.55 SU and 6.86 SU, respectively. The measured pH reading for both surface water
samples was within the 2B standard range of 6.0 to 9.0 SU.
Turbidity measured in SW-01 (11.3 NTUs) and SW-02 (8.06 NTUs) was below the 2B standard, which
is established at 25 NTUs for the receiving water in streams not designated as trout waters.
DO was measured at a concentration of 9.21 mg/L in SW-01 and 8.09 mg/L in SW-02. The 2B
standard is “greater than or equal to 5.0 mg/L”, meaning each sample was within the acceptable DO
range.
Specific conductivity concentrations in surface water samples SW-01 and SW-02 were recorded at
22 µS/cm and 24 µS/cm, respectively. ORP values for SW-01 and SW-02 were recorded at 125.8 mV

Fall 2017 Semiannual Water Quality Monitoring Report 11 February 2018
and 165.5 mV. Concentrations of specific conductivity and ORP are consistent with historical data in
both surface water samples. 2B standards do not exist for these parameters.
3.1.2.2 Appendix II Metals
Ten metals were detected in one or both surface water samples collected during the fall 2017
sampling event. Only one metal, zinc, was detected at concentrations above the SWSL in SW-01 and
SW-02, but below the 2B standard. The remaining nine metals were detected at concentrations
below their respective SWSL and 2B standards.
3.1.2.3 Appendix II VOCs and SVOCs
No VOCs or SVOCs were detected at concentrations above their respective MDLs in either the
upstream or downstream surface water samples (Table 2).
Leachate
Eight VOCs were detected in the leachate sample (Tables 2 and 3). Only 1,4-dichlorobenzene was
reported at a concentration above the SWSL.
On September 1, 2012, leachate extraction was initiated following installation of leachate extraction
pumps in the 10 landfill gas extraction wells. Between March 21, 2017, and October 11, 2017,
approximately 30,548 gallons of leachate were discharged through a permanent connection to the
TWSA (Table 3). From September 1, 2012, to October 11, 2017, a total of approximately 364,760
gallons of leachate were extracted or discharged from the landfill (Table 3).
In the fall of 2013, the active portion of the approved corrective action remedy was initiated. Based
on the leachate sample analytical results collected on October 11, 2017, Anchor QEA estimates that
0.03630 pounds of VOCs were removed with the extracted leachate between the March 21, 2017 and
October 11, 2017 sampling events. Mass removal calculations are included in Table 3.
Domestic Well
The following sections summarize measured field parameters and analytical results associated with
the one domestic well water sample collected during the fall 2017 sampling event.
3.1.4.1 Field Parameters
The pH reading for the domestic well water sample (DW-01) was 7.10 SU, which was within the 2B
standard range of 6.0 to 9.0 SU.
Turbidity measured in DW-01 was 2.28 NTUs. DO was measured at a concentration of 6.46 mg/L in
DW-01. Specific conductivity and ORP values in DW-01 were recorded at 50 µS/cm and 166.3 mV,
respectively. These parameters do not have established water quality standards.

Fall 2017 Semiannual Water Quality Monitoring Report 12 February 2018
3.1.4.2 Appendix II VOCs
No VOCs were detected at concentrations above their respective MDLs in the DW-01 sample
(Table 2).
3.2 Groundwater Flow Direction
Groundwater levels in the saprolite2, PWR3, and bedrock4 are monitored at the closed MSWLF. Three
bedrock monitoring wells, MW-01, MW-02, and MW-06, are located in the northern and
northwestern portions of the Site (Figure 3 and Table 4). Bedrock monitoring well MW-07 is located
southwest of the landfill (Figure 3). The fall 2017 water level data collected from these four bedrock
wells (Table 4) were used to determine generalized bedrock groundwater flow direction, which is to
the southwest (Figure 3).
PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are
located in the central, southwest, and southern parts of the landfill, respectively. The fall 2017 water
level data collected from monitoring wells MW-03, MW-04, and MW-05R (Table 4) indicate that
groundwater flow direction in the saprolite and PWR is also generally to the southwest, toward the
Tuckasegee River (Figure 3).

2 Saprolite is the result of in-place weathering, producing soil-like material that retains relict features of the parent rock. 3 PWR is rock generally found above the bedrock that is softer than bedrock, but not as soft as saprolite.
4 Bedrock is solid rock that underlies loose soil and saprolite.

Fall 2017 Semiannual Water Quality Monitoring Report 13 February 2018
4 Summary
The second semiannual water quality monitoring event of 2017 was performed on October 10 and
11 at the Jackson County closed MSWLF. Table 2 of this report and the reports of laboratory analysis
(Appendix B) provide detailed analytical results and field data summarizing groundwater and surface
water quality at the landfill.
4.1 Groundwater Quality
Metals
Fifteen metals were detected in the groundwater samples collected from one or more of the
monitoring wells. Seven of the metals (barium, cadmium, cobalt, copper, nickel, thallium, and zinc)
were detected at concentrations above the associated SWSLs in one or more monitoring wells (Table
2).
Six of the metals (antimony, cadmium, cobalt, thallium, vanadium, and zinc) were detected at
concentrations above their associated groundwater quality standards in one or more of the
monitoring wells (Table 2).
Antimony was detected above the IMAC in the groundwater samples collected from MW-01 and
MW-05R. Cadmium was detected in MW-01 at a concentration that exceeded the 2L standard.
Cobalt was detected above the IMAC in all groundwater samples, with the exception of MW-07.
Thallium was detected above the IMAC in samples collected from monitoring wells MW-01,
MW-05R, and MW-06. Vanadium was detected above the IMAC in the groundwater samples
collected from MW-01, MW-02, MW-05R, MW-06, and MW-07. Zinc was detected in MW-01 in
exceedance of the 2L standard. These results are consistent with historical data, with the exception of
zinc, which has not historically exceeded the 2L standard
VOCs and SVOCs
1,4-dichlorobenzene was detected above the SWSL in all monitoring wells by the SVOC analysis
method (EPA Method 8270D), with the exception of MW-02 and MW-06 (Table 2). This SVOC was
detected above the 2L standard in monitoring wells MW-01 and MW-05R. 1,4-dichlorobenzene was
not detected by the VOC analysis method (EPA Method 8260B).
No other VOCs or SVOCs were detected in the groundwater samples collected from any of the
monitoring wells during the fall 2017 water quality monitoring event.

Fall 2017 Semiannual Water Quality Monitoring Report 14 February 2018
Field Parameters and Other Constituents
All seven of the samples collected from the monitoring wells had pH readings outside of the 2L
standard range (6.5 SU to 8.5 SU). These results are consistent with historical data and are
characteristic of the natural groundwater quality of the region.
Measured turbidity readings ranged from 2.04 NTUs to 200 NTUs in monitoring wells MW-04 and
MW-05R, respectively.
Natural attenuation parameters (alkalinity, BOD, COD, chloride, carbon dioxide, hydrogen, ferrous
iron, methane, nitrate, sulfate, and TOC) were detected in groundwater samples collected from one
or more of the monitoring wells at various concentrations. Groundwater samples from MW-01
(13,000 µg/L), MW-05 (1,400 µg/L), and MW-06 (2,500 µg/L) exceeded the ferrous iron 2L standard
of 300 µg/L.
Natural attenuation parameters are being obtained as part of the CAP, and further evaluation of
these parameters will be performed during future monitoring events. The next CAER will be
submitted in the fall of 2021.
4.2 Surface Water Quality
Ten metals were detected in one or both surface water samples, SW-01 (upstream of the landfill) and
SW-02 (downstream of the landfill), during the fall 2017 water quality monitoring event. Zinc was
detected above the SWSL in SW-01 and SW-02, but below the 2B standard. No VOCs or SVOCs were
detected at concentrations above their respective MDLs in either the upstream or downstream
surface water samples.
On the basis of these data, the groundwater migrating from the landfill toward the Tuckasegee River
is not impacting surface water quality with regard to metals, VOCs, or SVOCs.
Field parameters including pH, turbidity, and DO measured in both surface water samples were
within the 2B standards established for these parameters.
4.3 Domestic Well Water Quality
No VOCs were detected at concentrations above their respective MDLs in the domestic well water
samples.
4.4 Leachate Quality
The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for
Appendix I VOCs only. Eight VOCs were detected in the leachate sample (Tables 2 and 3). Water
quality standards do not exist for leachate. Since leachate extraction began, a total of approximately

Fall 2017 Semiannual Water Quality Monitoring Report 15 February 2018
364,760 gallons of leachate have been extracted from the landfill (Table 3). Anchor QEA estimates
that 0.03630 pounds of VOCs were removed with the extracted leachate between the March and
October 2017 sampling events.

Fall 2017 Semiannual Water Quality Monitoring Report 16 February 2018
5 Future Activities
Anchor QEA will continue to monitor water quality on a semiannual basis at the Jackson County
closed MSWLF. During the spring and fall of 2018, samples will be collected from monitoring wells,
surface water monitoring points, and the leachate flow equalization tank. During the fall of 2018,
domestic well owners will be contacted, and groundwater samples will be collected from the wells if
permitted by the well owner and if possible based on well pump operability. Domestic well samples
will be analyzed for VOCs only. In addition to the natural attenuation parameters that were added as
part of the approved corrective action, the analytical suites associated with the current and future
sampling events are outlined in the 2011 CAP and recently submitted CAER. The upcoming sampling
event parameters are as follows:
Sampling Event Analytical Suite (not inclusive of natural attenuation parameters)
Spring 2018
Appendix I VOCs
Appendix I Metals
Cyanide and sulfide
Fall 2018
Appendix II VOCs
Appendix II SVOCs
Appendix II Metals
Appendix II Herbicides
Appendix II Pesticides
Appendix II Polychlorinated Biphenyls
Cyanide and sulfide

The next sampling event is scheduled for spring 2018.

Fall 2017 Semiannual Water Quality Monitoring Report 17 February 2018
6 References
Altamont (Altamont Environmental, Inc.), 2010. Assessment of Corrective Measures. September 7,
2010.
Altamont, 2011. Corrective Action Plan. June 30, 2011.
Altamont, 2016. Five-Year Corrective Action Evaluation Report. October 31, 2016.
DENR, 2011. Approval of the County’s Corrective Action Plan. September 1, 2011.
EPA (U.S. Environmental Protection Agency), 1996. Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures. OSWER, EPA/540/S-95/504. April 1996.
EPA, 2017. Operating Procedure: Groundwater Sampling. Science and Ecosystem Support Division.
April 26, 2017.

Tables
Table 1
Summary of Laboratory Analyses Performed on Samples
GROUNDWATER SAMPLES SURFACE WATER, LEACHATE, DOMESTIC WELL, AND QUALITY CONTROL SAMPLES
Metals Mercury VOCs SVOCs Metals Mercury VOCs VOCs SVOCs
Sample
Name
Date
Collected Sample Name Date
Collected
MW-01 10/11/2017 X X X X DW-01 10/10/2017 X
MW-02 10/11/2017 X X X X SW-01 10/10/2017 X X X X
MW-03 10/10/2017 X X X X SW-02 10/11/2017 X X X X
MW-04 10/10/2017 X X X X LT-01 10/11/2017 X
MW-05R 10/11/2017 X X X X TripBlank (1)10/10/2017 X
MW-06 10/11/2017 X X X X TripBlank (2)10/11/2017 X
MW-07 10/10/2017 X X X X TripBlank (DW)10/10/2017 X
TripBlank (LT)10/10/2017 X
GROUNDWATER SAMPLES
Total
Alkalinity to
pH 4.5
BOD COD Cyanide Volatile Fatty
Acids Ferrous Iron Nitrate as N Chloride Sulfate TOC Sulfide
Ethane,
Ethene,
Methane
Hydrogen Carbon
Dioxide
Sample
Name
Date
Collected
MW-01 10/11/2017 X X X X X X X X X X X X X
MW-02 10/11/2017 X X X X X X X X X X X X X
MW-03 10/10/2017 X X X X X X X X X X X X X X
MW-04 10/10/2017 X X X X X X X X X X X X X X
MW-05R 10/11/2017 X X X X X X X X X X X X X
MW-06 10/11/2017 X X X X X X X X X X X X X X
MW-07 10/10/2017 X X X X X X X X X X X X X X
Notes:
VOCs volatile organic compoundsBODbiochemical oxygen demand
COD chemical oxygen demand
TOC total organic carbonAnalysesAppendix I constituents were analyzed per Title 40 Code of Federal Regulations (CFR) Part 258.Blank cell Analysis was not performed on that sample.
AM20GAXEPA 9056A
EPA 6020B
SM 4500-S F
EPA 8270DEPA 8260B
SM 3500-Fe D
EPA 7470A EPA 524.2
AM23G SM 9060A
Analysis
Analysis
Analysis
EPA 7470AEPA 6020B EPA 8260B
Natural Attenuation Parameters
SM 2320B SM 5210B SM 5220D SM 4500-CN-
E
EPA 8270D
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 1 of 1
January 2018
Table 2
Well Construction Details and Corresponding Elevations
Date Drilled
Ground
Surface
Elevation
TOC
Elevation Stick Up Total Well
Depth
Depth To
Water
Groundwater
Elevation
Approx.
Depth to
Bedrock
Approx. Top
of Bedrock
Elevation
Depth to
Top of
Screened
Interval
Depth to
Bottom of
Screened
Interval
Top Elevation
of Screened
Interval
Elevation of
Bottom of
Screened
Interval
(mm/dd/yyyy)(feet)(feet)(feet
above gs) (feet bgs)(feet below
TOC) (feet)(feet bgs)(feet)(feet bgs)(feet bgs)(feet)(feet)
50-02 MW-01 04/23/1992 2,169.40 2,171.42 2.0 110.5 105.15 2,066.27 83.0 2,086.40 95.0 110.0 2,074.40 2,059.40 bedrock S&ME, Inc.
50-02 MW-02 04/22/1992 2,013.15 2,015.38 2.3 60.7 41.83 1,973.55 13.0 2,000.15 45.0 60.0 1,968.15 1,953.15 bedrock S&ME, Inc.
50-02 MW-03 04/21/1992 2,044.16 2,045.53 1.3 65.5 53.24 1,992.29 57.0 1,987.16 48.5 63.5 1,995.66 1,980.66
partially
weathered
rock
S&ME, Inc.
50-02 MW-04 04/21/1992 1,978.68 1,980.77 2.0 43.0 28.10 1,952.67 NA NA 25.0 40.0 1,953.68 1,938.68 saprolite S&ME, Inc.
50-02 MW-05R 01/26/2012 2,027.98 2,030.95 2.8 54.0 53.13 1,977.82 NA NA 44.0 54.0 1,983.98 1,973.98 saprolite
Altamont
Environmental,
Inc.
50-02 MW-06 03/23/2004 2,136.58 2,139.57 3.0 94.0 92.23 2,047.34 47.6 2,088.98 84.6 94.6 2,051.98 2,041.98 bedrock
50-02 MW-07 07/30/2010 1,978.71 1,981.29 2.6 95.0 31.55 1,949.74 44.0 1,935.00 70.0 95.0 1,908.71 1,883.71 bedrock
Notes:
Elevations
TOC top of casing
gs ground surface
bgs below ground surface
NA Not Applicable
Depth to Bedrock and
Screened Interval
Depth to Water Measured on October 10 and 11, 2017.
MW-05R Monitoring well MW-05 was abandoned on January 26, 2012 by NYEG Drilling, LLC. Monitoring well MW-05R was installed on January 26, 2012 as a replacement to the well MW-05 by NYEG Drilling, LLC. The well MW-05R was surveyed by Wes Cole Land
Surveying, P.A. on September 28, 2012.
Facility Permit Well ID
Source of Well
Construction
Information
Geology of
Screened
Interval
Altamont
Environmental,
Inc.
Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level (msl) and are based on surveying completed by Davenport & Associates, Inc. Elevations associated with wells MW-05R and MW-07 are measured relative to
horizontal North American Datum (NAD) 83 and are based on surveying completed by Wes Cole Land Surveying, P.A.
MW-01 through MW-04 Depth to Bedrock and Screened Interval taken from S&ME boring logs completed April 21, 22, and 23, 1992. MW-06 Depth to Bedrock and Screened Interval taken from Altamont boring log completed March 23, 2004. MW-07 Depth to Bedrock and
Screened Interval taken from Altamont boring log completed July 30, 2010. MW-05R Screened Interval taken from Altamont boring log completed January 26, 2012.
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 1 of 1
January 2018
Table 3
Summary of Analytical Results
Parameter
CAS Number
SWS ID
Units
Sample Name Collect Date
MW-01 10/11/2017
MW-02 10/11/2017
MW-03 10/10/2017
MW-04 10/10/2017
MW-05R 10/11/2017
MW-06 10/11/2017
MW-07 10/10/2017
LT-01 10/11/2017
SW-01 10/10/2017
SW-02 10/11/2017
DW-01 10/10/2017
TRIPBLANK1 10/10/2017
TRIPBLANK2 10/11/2017
TRIPBLANK (LT)10/10/2017
TRIPBLANK(DW)10/10/2017
MDL
MRL
SWSL
2L
IMAC
GWPS
2B
Lab Method
Lab Certification
Laboratory and
Regulatory Thresholds
Groundwater Samples
Leachate Sample
Surface Water Samples
Domestic Well Sample
Quality Control Samples BerylliumCadmiumChromiumCobaltCopperLeadNickelSeleniumSilver ThalliumTinVanadiumZinc7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7782-49-2 7440-22-4 7440-28-0 7440-31-5 7440-62-2 7440-66-6
23 34 51 53 54 131 152 183 184 194 195 209 213
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Result Result Result Result Result Result Result Result Result Result Result Result Result
0.088 J 38 0.053 J 92 58 3.0 J 9.9 J 0.63 U 0.32 J 6.1 0.21 U 0.72 J 1,200
0.070 J 0.078 U 0.95 J 1.5 J 0.22 U 0.34 J 0.85 U 0.63 U 0.063 U 0.099 U 0.21 U 1.1 J 8.9 J
0.057 U 0.37 J 0.47 J 49 0.61 J 0.11 J 17 0.63 U 0.063 U 0.10 J 0.21 U 0.10 U 23
0.057 U 0.27 J 0.54 J 2.7 J 0.88 J 0.24 J 1.5 J 0.68 J 0.063 U 0.099 U 0.21 U 0.13 J 31
0.44 J 0.41 J 8.7 J 27 16 3.7 J 12 J 1.0 J 0.063 U 0.27 J 0.21 U 12 J 51
0.057 U 0.41 J 0.66 J 89 1.9 J 0.20 J 74 0.63 U 0.063 U 1.6 J 0.21 U 0.60 J 52
0.057 U 0.11 J 0.62 J 0.98 J 0.42 J 0.28 J 8.2 J 0.63 U 0.063 U 0.099 U 0.21 U 0.46 J 30
NA NA NA NA NA NA NA NA NA NA NA NA NA
0.057 U 0.078 U 1.3 J 0.51 J 1.6 J 0.55 J 1.1 J 0.63 U 0.063 U 0.099 U 0.43 J 1.4 J 20
0.057 U 0.078 U 0.89 J 0.39 J 1.1 J 0.44 J 0.85 U 0.63 U 0.063 U 0.099 U 0.21 U 0.76 J 17
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
0.057 0.078 0.19 0.0071 0.22 0.093 0.85 0.63 0.063 0.099 0.21 0.10 2.80
1.0 1.0 1.0 1.0 5.0 1.0 2.0 1.0 1.0 1.0 5.0 1.0 10
1 1 10 10 10 10 50 10 10 5.5 100 25 10
NE 2 10 NE 1,000 15 100 20 20 NE NE NE 1,000
4 NE NE 1 NE NE NE NE NE 0.2 2,000 0.3 NE
4 NE NE 1 NE NE NE NE NE 0.28 2,000 0.3 NE
6.5 0.15 35 4 2.7 0.54 16 5 0.06 0.47 800 NE 36
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 1 of 4
January 2018
Table 3
Summary of Analytical Results
Parameter
CAS Number
SWS ID
Units
Sample Name Collect Date
MW-01 10/11/2017
MW-02 10/11/2017
MW-03 10/10/2017
MW-04 10/10/2017
MW-05R 10/11/2017
MW-06 10/11/2017
MW-07 10/10/2017
LT-01 10/11/2017
SW-01 10/10/2017
SW-02 10/11/2017
DW-01 10/10/2017
TRIPBLANK1 10/10/2017
TRIPBLANK2 10/11/2017
TRIPBLANK (LT)10/10/2017
TRIPBLANK(DW)10/10/2017
MDL
MRL
SWSL
2L
IMAC
GWPS
2B
Lab Method
Lab Certification
Laboratory and
Regulatory Thresholds
Groundwater Samples
Leachate Sample
Surface Water Samples
Domestic Well Sample
Quality Control Samples
Volatile Organic Compounds (VOCs) and Semivolatile Organic Compounds (SVOCs)Natural Attenuation Parameters
402, 618 402, 618
VOCs - EPA 8260B, 524.2 (DW-01 only), SVOCs - EPA 8270D SM 2320B SM 5210B EPA 9056A SM 5220D SM 4500-CN-E SM 3500-Fe-D EPA 9056A EPA 9056A EPA 9060A
1,4-Dichlorobenzene AcetoneAcetonitrileBenzeneChlorobenzeneEthylbenzeneNaphthaleneTetrahydrofuranTotal Alkalinity,to pH 4.5BODChlorideCODCyanideIron, FerrousNitrate as NSulfateTOC106-46-7 67-64-1 75-05-8 71-43-2 108-90-7 100-41-4 91-20-3 109-99-9 SW337 SW316 16887-00-6 SW317 57-12-5 NA SW303 14808-79-8 C-012
71 3 4 16 39 110 148 458 337 316 301 317 58 334 303 315 357
µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
7.5 Jb
0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 77,000 1,800 J 810 J 17,000 U 1.1 J 13,000 110 J 200 U 10,600
1.8 Ua 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 46,000 1,400 J 820 J 17,000 U 1.2 J 37 J 150 J 670 J 2,600
3.7 Jb
0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 79,000 600 J 32,000 73,000 2.0 J 17 J 6,900 850 J 6,100
3.0 Jb 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 160,000 1,300 J 80,000 46,000 J 1.0 U 14 U 1,600 67,000 J 10,700
6.9 Jb
0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 240,000 1,700 J 74,000 41,000 J 1.0 U 1,400 81 J 2,100 J 9,300
2.5 Ua 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 49,000 2,000 U 24,000 25,000 J 2.7 J 2,500 290 J 12,000 J 1,700 J
3.4 Jb
0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U 260,000 80 J 73,000 33,000 J 1.0 J 51 J 130 21,000 10,100
4.1 6.7 J 8.0 J 0.61 J 1.2 J 0.87 J 1.2 J 120 NA NA NA NA NA NA NA NA NA
1.7 Ua 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U NA NA NA NA NA NA NA NA NA
2.0 Ua 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U NA NA NA NA NA NA NA NA NA
0.057 U NA NA 0.028 Ua 0.048 Ua 0.053 Ua 0.16 Ua NA NA NA NA NA NA NA NA NA NA
0.050 Uc 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U NA NA NA NA NA NA NA NA NA
0.050 Uc 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U NA NA NA NA NA NA NA NA NA
0.050 Uc 0.31 U 3.0 U 0.048 U 0.062 U 0.061 U 0.19 U 0.16 U NA NA NA NA NA NA NA NA NA
0.057 Ua NA NA 0.028 Ua 0.048 Ua 0.053 Ua 0.16 Ua NA NA NA NA NA NA NA NA NA NA
0.050/0.057/1.8 0.31 3.00 0.048/0.078 0.062/0.076 0.061 0.059/0.19 0.160 770 NE 200 17,000 1.0 14/1,800 7.7 260 600
0.50/10 5.0 10.0 0.50 0.50 0.50 0.50/1.0 10.00 5,000 2,000 1,000 50,000 5.0 200/5,000 100 1,000 4,000
1 100 55 1 3 1 10 NE NE NE NE NE 10 NE 10,000 250,000 NE
6 6,000 NE 1 50 600 6 NE NE NE 250,000 NE 70 300 10,000 250,000 NE
NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 42 NE NE NE NE NE NE NE NE NE NE NE NE NE NE
100 2,000 NE 51 140 97 12 NE NE NE 230,000 NE 5 NE NE NE NE
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 2 of 4
January 2018
Table 3
Summary of Analytical Results
Parameter
CAS Number
SWS ID
Units
Sample Name Collect Date
MW-01 10/11/2017
MW-02 10/11/2017
MW-03 10/10/2017
MW-04 10/10/2017
MW-05R 10/11/2017
MW-06 10/11/2017
MW-07 10/10/2017
LT-01 10/11/2017
SW-01 10/10/2017
SW-02 10/11/2017
DW-01 10/10/2017
TRIPBLANK1 10/10/2017
TRIPBLANK2 10/11/2017
TRIPBLANK (LT)10/10/2017
TRIPBLANK(DW)10/10/2017
MDL
MRL
SWSL
2L
IMAC
GWPS
2B
Lab Method
Lab Certification
Laboratory and
Regulatory Thresholds
Groundwater Samples
Leachate Sample
Surface Water Samples
Domestic Well Sample
Quality Control Samples
Natural Attenuation Parameters Field Parameters
402 5445 (pH only)Acetic AcidFormic AcidMethaneEthaneEtheneCarbon DioxideHydrogen Dissolved OxygenTemperatureSpecific ConductivityOxidation Reduction PotentialpHTurbidity64-19-7 64-18-6 74-82-8 74-84-0 74-85-1 124-38-9 1333-74-0 7782-44-7 SW325 SW323 SW336 SW320 SW330
NE NE 456 331 332 459 420 356 325 323 336 320 330
mg/L mg/L µg/L µg/L µg/L mg/L nM mg/L °C µS/cm mV SU NTU
Result Result Result Result Result Result Result Result Result Result Result Result Result
0.13 0.2 U 1,200 0.1 U 0.1 U 240 NA 5.47 16.6 168 48.0 5.78 35.5
0.44 0.2 U 8.7 0.1 U 0.1 U 67 NA 7.47 19.87 219 189.2 6.26 12.6
0.10 0.52 4.6 0.01 U 0.026 340 21 2.82 18.86 283 284.8 5.57 2.85
0.16 0.73 110 0.031 0.017 440 79 1.53 16.74 611 227.4 5.73 2.06
0.35 0.2 U 9.8 0.1 U 0.16 130 NA 6.21 16.58 600 104.0 5.98 200
0.57 0.2 U 9.3 0.1 U 0.11 160 40 8.92 18.36 131 88.0 5.74 3.68
0.17 0.56 270 0.12 0.18 400 45 1.47 18.76 661 133.2 5.98 4.45
NA NA NA NA NA NA NA 4.13 29.72 6162 36.0 6.83 9.39
NA NA NA NA NA NA NA 9.21 17.91 22 125.8 7.55 11.3
NA NA NA NA NA NA NA 8.09 18.84 24 165.5 6.86 8.06
NA NA NA NA NA NA NA 6.46 15.58 50 166.3 7.10 2.28
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA
0.012 0.004 0.02 0.001/0.002 0.006 0.510 0.075 NA NA NA NA NA NA
0.10 0.10 0.5 0.01/0.1 0.01 5.0 0.6 NA NA NA NA NA NA
NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE NE NE NE NE NE NE NE NE NE 6.5-8.5 NE
NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE NE NE NE NE NE >5.0 NE NE NE 6.0-9.0 25
AM23G AM20GAX
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 3 of 4
January 2018
Table 3
Summary of Analytical Results
Notes:
*
°C
µg/L
µS/cm
2B
2L
B
BOD
Bold entry
CAS Number
COD
Collect Date
EPA
GWPS
IMAC
J
J
Jb
Lab Method
MDL
mg/L
MRL
mV
NA
NE
nM
NTU
Result
Shaded cell
SM
SU
SWS ID
SWSL
TOC
U
Ua
Uc
Only results, MDLs, MRLs, certification numbers, and methods for detected constituents are listed in this table. Please refer to the Prism Report of Laboratory Analysis for further details.
Solid Waste Section Limit (identified by the North Carolina Department of Environmental Quality); the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy
total organic carbon
a laboratory data qualifier used for parameters not detected at concentrations above the MDL
assigned by Anchor QEA to reflect a detected concentration that is greater than the MRL and MDL, but less than the SWSL
two results reported for EPA Method 6280B and 8270D - the most protective result used in analysis
the analytical method used to analyze the constituents
method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero
method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method
not analyzed
micrograms per liter
milligrams per liter
Standard Units
nephelometric turbidity units
not established
analytical data reported by the laboratory, or field data collected by Anchor QEA
indicates the parameter had multiple MDLs and MRLs listed by the laboratory in the analytical report. The lowest MDL or MRL was reported in this table. Refer to the Prism Laboratory Report of Analysis for further details.
surface water standard per North Carolina Administrative Code (NCAC), Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards (last amended June 2016). Where no 2B standard exists, the most stringent
standards for fresh water and human health were used from the EPA National Criteria standards table (current as of May 15, 2013).
groundwater standards from North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards (amended April 1, 2013)
a laboratory data qualifier used for parameters that were detected in the associated laboratory blank at a concentration greater than one half of the report limit
biochemical oxygen demand
indicates a detection with a result at or exceeding the SWSL
a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters
chemical oxygen demand
the date on which the sample was collected in the field
U.S. Environmental Protection Agency (Method)
Groundwater Protection Standard, pursuant to 15A NCAC 13B .1634," Department of Environmental Quality
Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-list (last updated June, 2011).
Interim Maximum Allowable Concentration. Analytes that do not have an established 2L standard were compared to the IMAC in accordance with 15A NCAC 02L .0202 [c].
a laboratory data qualifier used for parameters detected at estimated concentrations above the MDL, but below the MRL and SWSL
initial calibration verification not met for analyte - analyte is not detected in sample
degrees Celsius
microsiemens per centimeter
millivolt
nanomoles
Solid Waste Section Identification Number
two results reported for EPA Method 6280B and 8270D - the most protective result used in analysis
indicates a result in exceedance of the 2L or IMAC standard, or greater than or equal to the GWPS (if no 2L or IMAC exist) and 2B standard, if applicable
Standard Method
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Page 4 of 4
January 2018
Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
09/01/2012 10/25/2012 1,4-Dichlorobenzene 0.0034 11,500 11,500 0.000334-Methyl-2-
pentanone (MIBK)0.0021 J 0.00020
Acetone 0.0292 0.00280
Benzene 0.0021 0.00020
Chlorobenzene 0.0029 0.00028
cis-1,2-
Dichloroethene 0.00063 J 0.00006
Dichlorodifluoro-
methane 0.00093 J 0.00009
Ethylbenzene 0.0102 0.00098
Naphthalene 0.0069 0.00066
Styrene 0.00033 J 0.00003
Toluene 0.003 0.00029
Xylene (Total)0.0094 0.00090
Total 0.00682 0.00682
10/26/2012 04/11/2013 1,4-Dichlorobenzene 0.006 65,500 54,000 0.00270
Acetone 0.012 J 0.00540
Benzene 0.0011 0.00049
Carbon disulfide 0.0067 J 0.00301
Chlorobenzene 0.0024 J 0.00108
cis-1,2-
Dichloroethene 0.00058 J 0.00026
Ethylbenzene 0.0083 0.00373
Toluene 0.00059 J 0.00027
Xylene (Total)0.0078 0.00351
Total 0.02045 0.02727
04/12/2013 10/08/2013 1,4-Dichlorobenzene 0.0055 114,737 49,237 0.00226
4-Methyl-2-
pentanone (MIBK)0.0012 J 0.00049
Benzene 0.0020 0.00082
Chlorobenzene 0.0039 0.00160
cis-1,2-
Dichloroethene 0.00080 J 0.00033
Ethylbenzene 0.0151 0.00619
Naphthalene 0.0184 0.00754
Toluene 0.0012 0.00049
Xylene (Total)0.0090 0.00369
Total 0.02341 0.05068
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
1 of 4
January 2018
Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
10/09/2013 04/08/2014 1,4-Dichlorobenzene 0.0056 168,821 54,084 0.00252
Benzene 0.0018 0.00081
Chlorobenzene 0.0051 0.00230
cis-1,2-
Dichloroethene 0.00049 J 0.00022
Ethylbenzene 0.0047 0.00212
Toluene 0.00041 J 0.00018
Xylene (Total)0.0021 J 0.00095
Total 0.00910 0.05978
04/08/2014 10/23/2014 1,4-Dichlorobenzene 0.0053 179,652 10,831 0.00048
Benzene 0.0014 0.00013
Chlorobenzene 0.003 0.00027
cis-1,2-
Dichloroethene 0.00049 J 0.00004
Ethylbenzene 0.0027 0.00024
Toluene 0.00051 J 0.00005
Xylene (Total)0.0014 J 0.00013
Total 0.00133 0.06111
10/23/2014 04/21/2015
1,2,3-
Trimethylbenzene 0.00062 219,965 40,313 0.00021
1,2,4-
Trimethylbenzene 0.00076 0.00026
2-Chlorotoluene 0.00067 0.00022
1,4-Dichlorobenzene 0.0059 0.00198
Acetone 0.00790 0.00265
Benzene 0.0022 0.00074
Chlorobenzene 0.003 0.00101
Ethylbenzene 0.0056 0.00188
Isopropylbenzene 0.0013 0.00044
Methy Tert-butyl-
Ether 0.0013 0.00044
Napthalene 0.024 0.00806
n-Propylbenzene 0.00088 0.00030
Tetrahydrofuran 0.089 0.02988
Toluene 0.00054 J 0.00018
Vinyl Chloride 0.00038 J 0.00013
Xylene (Total)0.0030 J 0.00101
Total 0.04937 0.11048
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
2 of 4
January 2018
Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
04/21/2015 10/13/2015 1,4-Dichlorobenzene 0.00600 256,685 36,720 0.00183
2-Butanone 0.00960 J 0.00294
Benzene 0.00210 0.00064
Chlorobenzene 0.0040 0.00122
Ethylbenzene 0.00710 0.00217
m,p-Xylenes 0.0014 0.00043
Naphthalene 0.021 0.00642
o-Xylene 0.0017 0.00052
Tetrahydrofuran 0.062 0.01896
Toluene 0.00058 J 0.00018
Total Xylenes 0.0031 J 0.00095
Total 0.03626 0.14674
10/13/2015 04/05/2016 1,4-Dichlorobenzene 0.00590 315,663 58,978 0.00290
Benzene 0.00170 0.00083
Chlorobenzene 0.0038 0.00187
Ethylbenzene 0.00500 0.00246
m,p-Xylenes 0.0010 0.00049
o-Xylene 0.0015 0.00074
Toluene 0.00063 J 0.00031
Total Xylenes 0.0025 J 0.00123
Total 0.01082 0.15756
04/05/2016 10/11/2016 331,010 15,347 0.00000
Total 0.00000 0.15756
10/11/2016 03/21/2017 1,4-Dichlorobenzene 0.0046 334,212 3,202 0.00012
Acetone 0.0094 J 0.00025
Benzene 0.0015 0.00004
Chlorobenzene 0.0043 0.00011
Ethylbenzene 0.0014 0.00004
m,p-Xylenes 0.0006 J 0.00002
o-Xylene 0.00092 0.00002
Tetrahydrofuran 0.066 0.00176
Total Xylenes 0.0015 J 0.00004
Total 0.00241 0.15997
No detected compounds.
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
3 of 4
January 2018
Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the
Leachate Sample (LT-01)
Cumulative
Flow
Differential
Flow
Mass
Removed
Cumulative
Mass Removed
Beginning Ending (gallons)(gallons)(pounds)(pounds)
Sample Dates Detected Volatile
Organic Compounds
Concentration
in LT-01
(mg/L)
03/21/2017 10/11/2017 1,4-Dichlorobenzene 0.0041 364,760 30,548 0.00104
Acetone 0.0067 J 0.00170
Acetonitrile 0.008 J 0.00204
Benzene 0.00061 0.00016
Chlorobenzene 0.0012 0.00031
Ethylbenzene 0.00087 0.00022
Naphthalene 0.0012 0.00031
Tetrahydrofuran 0.12 0.03053
Total 0.03630 0.19627
Notes:
Detections Only detected VOCs in leachate sample LT-01 are included in the mass removal calculation.
Extraction Leachate extraction at the landfill initiated on September 1, 2012.
Volume Extraction volume measurements were recorded and provided by Jackson County staff.
Calculations
Cumulative Flow Interpolated between LT-01 Sample Dates.
Differential Flow Represents the total flow between the LT-01 Sample Dates.
Mass Removed
mg/L milligrams per liter.
J Indicates laboratory estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
October 2016 No VOCs were detected in the leachate sample collected during the October 2016 sampling event.
Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of
leachate quality until the next sampling event occurs, and that the leachate removal system has a 100% removal and treatment efficiency.
Mass Removed and Treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the
Concentration by the Differential Flow for the specified period.
Formula: ((concentration[mg/L])*(2.2e-6 lb)/(0.264 gal))*(Differential flow)
Fall 2017 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
4 of 4
January 2018

Figures
[0 2,000 4,0001,000
Feet
LEGEND:
Site Parcel Boundary
Publish Date: 2018/02/07, 8:30 AM | User: alesueurFilepath: \\Asheville1\Asheville\Projects\Jackson County\Dillsboro GIS\Maps\2017\Fall Water Quality\Figure 1 Site Location Map AQ.mxd
Figure 1Site Location Map
Semiannual Water Quality ReportJackson County Closed MSW Landfill, Permit No. 50-02, Jackson County, North Carolina
SOURCES:Basemap: USGS Topographic Maps - GreensCreek and Whittier 7.5 Minute QuadranglesParcels: Jackson County GIS
Anchor QEA of North Carolina, PLLC
#I#I"
!U
!A !A !A
!A
!A
!A
!A !A
!A!A
@A@A
@A
@A
@A
@A @A
Flow Direction
256021
2
0
2060
20
2
0 222020802180
20802180
212
0
2540208020
2
0
25202180
20802060
21802
0
4
0
2020212022402120
2140216
0
222
0
2480246020402440
206024202080
23
8
02360 21
6
02340
19
6
0
19
6
0
21
4
0
20
6
0
2
1
2
0
2
0
4
020802
3
2
0
19
8
020
2
0
19
8
0
2
160
218022
8
0
2
2
6022402
2
2
0 214021802160
SW-01
SW-02
LT-01
DW-01 US 441S/US74 WH
A
YW
O
O
D

R
D
C
OW
E
E

T
U
N
N
E
L

R
D
DELLWOOD DR
TU
N
N
E
L

M
O
U
N
T
A
I
N

R
D
GREEN ENERGY PARK RDHUNDREDACRE LNWHITE
FA
LCON
DRS US 441HARMONY HLMOODY RDS US 441WESTERN LNFUGITIVE RUN
JOE
W
I
L
K
E
Y

R
D
MW-04
MW-07
MW-05R
MW-02
MW-03
MW-06 MW-01
TT
UUCC
KK
AA
SS
EE
GG
EE
EE
RRIIVV
EE
RRLAURELLAURELBRANCHBRANCH
[
0 500
Feet
NOTES:1. Sample locations are approximate.LEGEND:
@A Monitoring Well
!A Extraction Well
#ISurface Water Sample Location
!U Domestic Well Sample Location
"Leachate Sample Location and
Flow Equilization Tank
Road
Elevation Contour (20-Foot Interval)
Property Boundary
Publish Date: 2018/02/07, 8:25 AM | User: alesueurFilepath: \\Asheville1\Asheville\Projects\Jackson County\Dillsboro GIS\Maps\2017\Fall Water Quality\Figure 2 Sample Location Map AQ.mxd
Figure 2Site Layout Map
Semiannual Water Quality Report
Jackson County Closed MSW Landfill, Permit No. 50-02, Jackson County, North Carolina
SOURCES:Basemap: NC OneMap 2010Contours, Roads, and Parcels: Jackson County GIS
Anchor QEA of North Carolina, PLLC
!U
!U
!U !U
!U
!U
!U
Flo
w Direction
24202020 22202
06
0
2
3
8
0
20802
3
6
02340 2180
23202
28
0
2
2
6
0
2
2
4
022202180 216021401960 19
8
0 218020202120
2040
21202140
2060
2080
21
60 2160HAYWOOD RD
FUGITIVE RUNJ O E W I L K E Y R D
GREEN ENERGY PARK RDHAY
W
O
O
D RD
TUNNEL MOUNTAIN RD
MW-07
(1,949.74)
MW-02
(1,973.55)
MW-06(2,047.34)MW-01
(2,066.27)
MW-04
(1,952.67)
MW-05R(1,977.82)
MW-03(1,992.29)GENERALIZEDGROUNDWATERFLOW DIRECTIONTUCKASEGEE RIVER
TUCKASEGEE RIVER
Wilkey
Wilkey
Wilkey
Connor
2
2
0
0
24002100
230022002000
21
00
[
0 200
Feet
NOTES:1. Monitoring well locations are approximate.2. Groundwater elevations and flow direction are updated on a semiannual basis following sample collection events inApril and October.3. Groundwater flow direction is based on groundwater elevations in monitoring wells MW-03, MW-04, and MW-05R.Direction is calculated based on depth to water measured on October 10 and 11, 2017.4. Last names of property owners are shown in parcels that border the landfill property.5. PWR: partially weathered rock6. (1,992.29): groundwater elevation in feet (North American Vertical Datum 1988)
LEGEND:
!U Saprolite Monitoring Well
!U PWR Monitoring Well
!U Bedrock Monitoring Well
Groundwater Flow Direction
Stream
Property Boundary
Road
Elevation Contour (20-Foot Interval)
Publish Date: 2018/02/07, 8:33 AM | User: alesueurFilepath: \\Asheville1\Asheville\Projects\Jackson County\Dillsboro GIS\Maps\2017\Fall Water Quality\Figure 3 Groundwater Elevation Map AQ.mxd
Figure 3Generalized Groundwater Flow Direction
Semiannual Water Quality ReportJackson County Closed MSW Landfill, Permit No. 50-02, Dillsboro, North Carolina
SOURCES:1. Elevation contours, roads, and parcels: Jackson County GIS2. Groundwater elevations: calculated from surveysperformed by Davenport & Associates, Inc. (MW-01, MW-02,MW-03, MW-04, and MW-06) and Wes Cole Land Surveying,P.A. (MW-05R and MW-07)
Anchor QEA of North Carolina, PLLC
Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
Monitoring Well MW-01
Fall 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill January 2018
15
17.8
<0.33
7.6
5.6 5.3
11.0
8.5
< 0.33
9.8
10.9
10
8.0
9.5 10
12.8
11
14
13
6.9
12
7.5 J
2060
2062
2064
2066
2068
2070
2072
2074
2076
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007 Oct, 2007 Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010 Oct, 2010 Apr, 2011 Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Oct, 2017Groundwater Elevation (feet)1,4-Dichlorobenzene Concentration (μg/L) Sampling Date
1,4-Dichlorobenzene Groundwater Elevation
Notes:1. 2L Standard = 6 μg/L 2. "J" indicates result is estimated by laboratory3. "<" indicates result is less than method detection limit4. Oct, 2017 result reported in semi-volatile organic compound list.
Figure 5
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
Monitoring Well MW-05R
Fall 2017 Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill January 2018
17
18.8
<0.33
16.2 15.9
13.1
12.1
13.9
<0.33 U
Not
Sampled
2.5
1.3 1.5
7.3 6.9
4.3
5.6
6.5 6.5
4.4
10
6.9 J
1970
1972
1974
1976
1978
1980
1982
1984
1986
1988
1990
0
2
4
6
8
10
12
14
16
18
20
Apr, 2007Oct, 2007Apr, 2008Oct, 2008Apr, 2009Oct, 2009Apr, 2010Oct, 2010Apr, 2011Oct, 2011Apr, 2012Oct, 2012 Apr, 2013 Oct, 2013 Apr, 2014Oct, 2014Apr, 2015Oct, 2015Apr, 2016Oct, 2016Mar, 2017Oct, 2017Groundwater Elevation (feet)1,4-Dichlorobenzene Concentration (μg/L) Sampling Date
1,4-Dichlorobenzene Groundwater Elevation
Notes:Constituent concentration after January 2012 was found in MW-05R. Constituent concentration before January 2012 was found in MW-05.
Groundwater elevation in October 2011 was interpolated.2L Standard = 6 μg/L "J" indicates result is estimated by laboratory"<" indicates result is less than method detection limit
Oct, 2017 result reported in semi-volatile organic compound list

Appendix A
Well Sampling Logs and Equipment
Documentation & Instrument Calibration
Data Sheets

Appendix B
Reports of Laboratory Analysis, Chain-of-
Custody Documentation, and Certificates
of Analysis
Page 1 of 13
Page 2 of 13
Page 3 of 13
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Page 13 of 13
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
10/30/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill (Permit 50-02)
Project No.: 50-02
Lab Submittal Date: 10/11/2017
Prism Work Order: 7100184
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 13
Sample Receipt Summary
10/30/2017
Prism Work Order: 7100184
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7100184-01 10/10/17DW-01 10/11/17Drinking Water
7100184-02 10/10/17Trip Blank (DW)10/11/17Drinking Water
Samples were received at 12.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order:
Summary of Detections
There were no detections reported.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Drinking Water
Client Sample ID:
Prism Sample ID: 7100184-01
Prism Work Order: 7100184
Time Collected: 10/10/17 13:15
Time Submitted: 10/11/17 09:15
DW-01
50-02
SWSL
Volatile Organic Compounds by GC/MS
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0181,1,1,2-Tetrachloroethane <0.018
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0721,1,1-Trichloroethane <0.072
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0811,1,2,2-Tetrachloroethane <0.081
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0921,1,2-Trichloroethane <0.092
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0511,1-Dichloroethane <0.051
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0541,1-Dichloroethylene <0.054
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0311,1-Dichloropropylene <0.031
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.421,2,3-Trichlorobenzene <0.42
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.121,2,3-Trichloropropane <0.12
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.161,2,4-Trichlorobenzene <0.16
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0401,2,4-Trimethylbenzene <0.040
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.171,2-Dichlorobenzene <0.17
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0501,2-Dichloroethane <0.050
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0841,2-Dichloropropane <0.084
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0541,3,5-Trimethylbenzene <0.054
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0961,3-Dichlorobenzene <0.096
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0851,3-Dichloropropane <0.085
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0571,4-Dichlorobenzene <0.057
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0542,2-Dichloropropane <0.054
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0462-Chlorotoluene <0.046
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0614-Chlorotoluene <0.061
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.0424-Isopropyltoluene <0.042
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.028Benzene<0.028
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.11Bromobenzene<0.11
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.051Bromochloromethane<0.051
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.054Bromodichloromethane<0.054
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.031Bromoform<0.031
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.046Bromomethane<0.046
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.048Carbon Tetrachloride <0.048
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.048Chlorobenzene<0.048
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.12Chloroethane<0.12
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.025Chloroform<0.025
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.056Chloromethane<0.056
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.038cis-1,2-Dichloroethylene <0.038
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.070cis-1,3-Dichloropropylene <0.070
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.062Dibromochloromethane<0.062
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 13
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Drinking Water
Client Sample ID:
Prism Sample ID: 7100184-01
Prism Work Order: 7100184
Time Collected: 10/10/17 13:15
Time Submitted: 10/11/17 09:15
DW-01
50-02
SWSL
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.051Dibromomethane<0.051
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.076Dichlorodifluoromethane<0.076
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.053Ethylbenzene<0.053
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.14Hexachlorobutadiene<0.14
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.053Isopropylbenzene (Cumene)<0.053
524.2 P7J048811.0 10/24/17 15:20KDMug/L 0.057m,p-Xylenes <0.057
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.062Methylene Chloride <0.062
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.042Methyl-tert-Butyl Ether <0.042
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.16Naphthalene<0.16
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.065n-Butylbenzene <0.065
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.051n-Propylbenzene <0.051
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.034o-Xylene <0.034
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.042sec-Butylbenzene <0.042
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.038Styrene<0.038
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.060tert-Butylbenzene <0.060
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.068Tetrachloroethylene<0.068
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.024Toluene<0.024
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.036trans-1,2-Dichloroethylene <0.036
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.074trans-1,3-Dichloropropylene <0.074
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.056Trichloroethylene<0.056
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.044Trichlorofluoromethane<0.044
524.2 P7J048810.50 10/24/17 15:20KDMug/L 0.059Vinyl chloride <0.059
524.2 P7J048811.0 10/24/17 15:20KDMug/L 0.37Total Trihalomethanes <0.37
524.2 P7J048811.5 10/24/17 15:20KDMug/L 0.25Xylenes, total <0.25
Surrogate Recovery Control Limits
70-130105 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Drinking Water
Client Sample ID:
Prism Sample ID: 7100184-02
Prism Work Order: 7100184
Time Collected: 10/10/17 13:15
Time Submitted: 10/11/17 09:15
Trip Blank (DW)
50-02
SWSL
Volatile Organic Compounds by GC/MS
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0181,1,1,2-Tetrachloroethane <0.018
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0721,1,1-Trichloroethane <0.072
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0811,1,2,2-Tetrachloroethane <0.081
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0921,1,2-Trichloroethane <0.092
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0511,1-Dichloroethane <0.051
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0541,1-Dichloroethylene <0.054
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0311,1-Dichloropropylene <0.031
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.421,2,3-Trichlorobenzene <0.42
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.121,2,3-Trichloropropane <0.12
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.161,2,4-Trichlorobenzene <0.16
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0401,2,4-Trimethylbenzene <0.040
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.171,2-Dichlorobenzene <0.17
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0501,2-Dichloroethane <0.050
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0841,2-Dichloropropane <0.084
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0541,3,5-Trimethylbenzene <0.054
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0961,3-Dichlorobenzene <0.096
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0851,3-Dichloropropane <0.085
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0571,4-Dichlorobenzene <0.057
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0542,2-Dichloropropane <0.054
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0462-Chlorotoluene <0.046
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0614-Chlorotoluene <0.061
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.0424-Isopropyltoluene <0.042
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.028Benzene<0.028
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.11Bromobenzene<0.11
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.051Bromochloromethane<0.051
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.054Bromodichloromethane<0.054
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.031Bromoform<0.031
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.046Bromomethane<0.046
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.048Carbon Tetrachloride <0.048
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.048Chlorobenzene<0.048
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.12Chloroethane<0.12
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.025Chloroform<0.025
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.056Chloromethane<0.056
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.038cis-1,2-Dichloroethylene <0.038
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.070cis-1,3-Dichloropropylene <0.070
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.062Dibromochloromethane<0.062
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 13
Laboratory Report
10/30/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Drinking Water
Client Sample ID:
Prism Sample ID: 7100184-02
Prism Work Order: 7100184
Time Collected: 10/10/17 13:15
Time Submitted: 10/11/17 09:15
Trip Blank (DW)
50-02
SWSL
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.051Dibromomethane<0.051
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.076Dichlorodifluoromethane<0.076
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.053Ethylbenzene<0.053
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.14Hexachlorobutadiene<0.14
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.053Isopropylbenzene (Cumene)<0.053
524.2 P7J048811.0 10/24/17 14:45KDMug/L 0.057m,p-Xylenes <0.057
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.062Methylene Chloride <0.062
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.042Methyl-tert-Butyl Ether <0.042
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.16Naphthalene<0.16
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.065n-Butylbenzene <0.065
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.051n-Propylbenzene <0.051
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.034o-Xylene <0.034
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.042sec-Butylbenzene <0.042
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.038Styrene<0.038
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.060tert-Butylbenzene <0.060
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.068Tetrachloroethylene<0.068
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.024Toluene<0.024
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.036trans-1,2-Dichloroethylene <0.036
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.074trans-1,3-Dichloropropylene <0.074
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.056Trichloroethylene<0.056
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.044Trichlorofluoromethane<0.044
524.2 P7J048810.50 10/24/17 14:45KDMug/L 0.059Vinyl chloride <0.059
524.2 P7J048811.0 10/24/17 14:45KDMug/L 0.37Total Trihalomethanes <0.37
524.2 P7J048811.5 10/24/17 14:45KDMug/L 0.25Xylenes, total <0.25
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-130101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 13
10/30/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100184
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0488 - 524.2
Blank (P7J0488-BLK1)Prepared & Analyzed: 10/24/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL0.50
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL0.50
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methylene Chloride ug/LBRL0.50
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL0.50
n-Butylbenzene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 13
10/30/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100184
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0488 - 524.2
Blank (P7J0488-BLK1)Prepared & Analyzed: 10/24/17
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl chloride ug/LBRL0.50
Total Trihalomethanes ug/LBRL1.0
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10050.1
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.0
LCS (P7J0488-BS1)Prepared & Analyzed: 10/24/17
1,1,1,2-Tetrachloroethane ug/L22.8 0.50 20.00 70-130114
1,1,1-Trichloroethane ug/L20.8 0.50 20.00 70-130104
1,1,2,2-Tetrachloroethane ug/L20.8 0.50 20.00 70-130104
1,1,2-Trichloroethane ug/L20.2 0.50 20.00 70-130101
1,1-Dichloroethane ug/L21.8 0.50 20.00 70-130109
1,1-Dichloroethylene ug/L22.7 0.50 20.00 70-130114
1,1-Dichloropropylene ug/L23.5 0.50 20.00 70-130118
1,2,3-Trichlorobenzene ug/L21.1 0.50 20.00 70-130105
1,2,3-Trichloropropane ug/L21.3 0.50 20.00 70-130107
1,2,4-Trichlorobenzene ug/L23.6 0.50 20.00 70-130118
1,2,4-Trimethylbenzene ug/L22.0 0.50 20.00 70-130110
1,2-Dichlorobenzene ug/L23.6 0.50 20.00 70-130118
1,2-Dichloroethane ug/L21.6 0.50 20.00 70-130108
1,2-Dichloropropane ug/L21.2 0.50 20.00 70-130106
1,3,5-Trimethylbenzene ug/L22.6 0.50 20.00 70-130113
1,3-Dichlorobenzene ug/L23.0 0.50 20.00 70-130115
1,3-Dichloropropane ug/L21.6 0.50 20.00 70-130108
1,4-Dichlorobenzene ug/L22.8 0.50 20.00 70-130114
2,2-Dichloropropane ug/L23.4 0.50 20.00 70-130117
2-Chlorotoluene ug/L24.0 0.50 20.00 70-130120
4-Chlorotoluene ug/L23.6 0.50 20.00 70-130118
4-Isopropyltoluene ug/L23.4 0.50 20.00 70-130117
Benzene ug/L21.6 0.50 20.00 70-130108
Bromobenzene ug/L22.3 0.50 20.00 70-130111
Bromochloromethane ug/L21.7 0.50 20.00 70-130108
Bromodichloromethane ug/L21.7 0.50 20.00 70-130108
Bromoform ug/L20.3 0.50 20.00 70-130101
Bromomethane ug/L17.8 0.50 20.00 70-13089
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 13
10/30/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100184
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0488 - 524.2
LCS (P7J0488-BS1)Prepared & Analyzed: 10/24/17
Carbon Tetrachloride ug/L22.7 0.50 20.00 70-130114
Chlorobenzene ug/L22.6 0.50 20.00 70-130113
Chloroethane ug/L21.4 0.50 20.00 70-130107
Chloroform ug/L22.8 0.50 20.00 70-130114
Chloromethane ug/L20.1 0.50 20.00 70-130100
cis-1,2-Dichloroethylene ug/L21.8 0.50 20.00 70-130109
cis-1,3-Dichloropropylene ug/L22.9 0.50 20.00 70-130114
Dibromochloromethane ug/L21.6 0.50 20.00 70-130108
Dibromomethane ug/L22.0 0.50 20.00 70-130110
Dichlorodifluoromethane ug/L24.4 0.50 20.00 70-130122
Ethylbenzene ug/L23.6 0.50 20.00 70-130118
Hexachlorobutadiene ug/L23.4 0.50 20.00 70-130117
Isopropylbenzene (Cumene)ug/L24.1 0.50 20.00 70-130120
Methylene Chloride ug/L19.7 0.50 20.00 70-13099
Methyl-tert-Butyl Ether ug/L20.3 0.50 20.00 70-130102
Naphthalene ug/L21.5 0.50 20.00 70-130108
n-Butylbenzene ug/L22.3 0.50 20.00 70-130111
n-Propylbenzene ug/L24.2 0.50 20.00 70-130121
o-Xylene ug/L21.2 0.50 20.00 70-130106
sec-Butylbenzene ug/L22.0 0.50 20.00 70-130110
Styrene ug/L20.7 0.50 20.00 70-130104
tert-Butylbenzene ug/L21.9 0.50 20.00 70-130110
Tetrachloroethylene ug/L22.8 0.50 20.00 70-130114
Toluene ug/L22.8 0.50 20.00 70-130114
trans-1,2-Dichloroethylene ug/L22.5 0.50 20.00 70-130113
trans-1,3-Dichloropropylene ug/L21.5 0.50 20.00 70-130108
Trichloroethylene ug/L22.2 0.50 20.00 70-130111
Trichlorofluoromethane ug/L24.6 0.50 20.00 70-130123
Vinyl chloride ug/L24.1 0.50 20.00 70-130121
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10451.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9547.3
ug/L 50.00 70-130Surrogate: Toluene-d8 10050.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 13
10/30/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100184
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0488 - 524.2
LCS Dup (P7J0488-BSD1)Prepared & Analyzed: 10/24/17
1,1,1,2-Tetrachloroethane ug/L21.9 0.50 20.00 2070-130110 4
1,1,1-Trichloroethane ug/L20.0 0.50 20.00 2070-130100 4
1,1,2,2-Tetrachloroethane ug/L20.4 0.50 20.00 2070-130102 2
1,1,2-Trichloroethane ug/L21.9 0.50 20.00 2070-130110 8
1,1-Dichloroethane ug/L20.9 0.50 20.00 2070-130105 4
1,1-Dichloroethylene ug/L22.6 0.50 20.00 2070-130113 0.4
1,1-Dichloropropylene ug/L23.1 0.50 20.00 2070-130116 2
1,2,3-Trichlorobenzene ug/L20.6 0.50 20.00 2070-130103 2
1,2,3-Trichloropropane ug/L22.3 0.50 20.00 2070-130112 5
1,2,4-Trichlorobenzene ug/L22.1 0.50 20.00 2070-130111 7
1,2,4-Trimethylbenzene ug/L21.8 0.50 20.00 2070-130109 0.9
1,2-Dichlorobenzene ug/L21.7 0.50 20.00 2070-130108 9
1,2-Dichloroethane ug/L20.9 0.50 20.00 2070-130105 3
1,2-Dichloropropane ug/L21.2 0.50 20.00 2070-130106 0.3
1,3,5-Trimethylbenzene ug/L21.8 0.50 20.00 2070-130109 4
1,3-Dichlorobenzene ug/L22.2 0.50 20.00 2070-130111 4
1,3-Dichloropropane ug/L20.8 0.50 20.00 2070-130104 4
1,4-Dichlorobenzene ug/L22.0 0.50 20.00 2070-130110 3
2,2-Dichloropropane ug/L20.3 0.50 20.00 2070-130102 14
2-Chlorotoluene ug/L23.0 0.50 20.00 2070-130115 4
4-Chlorotoluene ug/L23.4 0.50 20.00 2070-130117 1
4-Isopropyltoluene ug/L22.3 0.50 20.00 2070-130112 5
Benzene ug/L21.5 0.50 20.00 2070-130108 0.4
Bromobenzene ug/L20.9 0.50 20.00 2070-130104 6
Bromochloromethane ug/L19.2 0.50 20.00 2070-13096 12
Bromodichloromethane ug/L21.7 0.50 20.00 2070-130109 0.2
Bromoform ug/L19.4 0.50 20.00 2070-13097 4
Bromomethane ug/L18.8 0.50 20.00 2070-13094 6
Carbon Tetrachloride ug/L20.1 0.50 20.00 2070-130100 12
Chlorobenzene ug/L22.2 0.50 20.00 2070-130111 2
Chloroethane ug/L21.2 0.50 20.00 2070-130106 0.7
Chloroform ug/L19.3 0.50 20.00 2070-13096 17
Chloromethane ug/L20.5 0.50 20.00 2070-130102 2
cis-1,2-Dichloroethylene ug/L21.8 0.50 20.00 2070-130109 0.2
cis-1,3-Dichloropropylene ug/L22.5 0.50 20.00 2070-130112 2
Dibromochloromethane ug/L21.1 0.50 20.00 2070-130106 2
Dibromomethane ug/L22.0 0.50 20.00 2070-130110 0.09
Dichlorodifluoromethane ug/L23.4 0.50 20.00 2070-130117 4
Ethylbenzene ug/L22.4 0.50 20.00 2070-130112 5
Hexachlorobutadiene ug/L22.7 0.50 20.00 2070-130114 3
Isopropylbenzene (Cumene)ug/L23.5 0.50 20.00 2070-130118 2
Methylene Chloride ug/L19.7 0.50 20.00 2070-13099 0
Methyl-tert-Butyl Ether ug/L20.1 0.50 20.00 2070-130100 1
Naphthalene ug/L21.3 0.50 20.00 2070-130106 1
n-Butylbenzene ug/L21.9 0.50 20.00 2070-130109 2
n-Propylbenzene ug/L23.4 0.50 20.00 2070-130117 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 13
10/30/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100184
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0488 - 524.2
LCS Dup (P7J0488-BSD1)Prepared & Analyzed: 10/24/17
o-Xylene ug/L20.9 0.50 20.00 2070-130104 1
sec-Butylbenzene ug/L22.2 0.50 20.00 2070-130111 0.9
Styrene ug/L19.9 0.50 20.00 2070-13099 4
tert-Butylbenzene ug/L21.6 0.50 20.00 2070-130108 1
Tetrachloroethylene ug/L21.6 0.50 20.00 2070-130108 6
Toluene ug/L22.2 0.50 20.00 2070-130111 2
trans-1,2-Dichloroethylene ug/L22.8 0.50 20.00 2070-130114 1
trans-1,3-Dichloropropylene ug/L22.2 0.50 20.00 2070-130111 3
Trichloroethylene ug/L21.6 0.50 20.00 2070-130108 3
Trichlorofluoromethane ug/L24.2 0.50 20.00 2070-130121 2
Vinyl chloride ug/L23.3 0.50 20.00 2070-130117 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9547.3
ug/L 50.00 70-130Surrogate: Toluene-d8 10049.8
Sample Extraction Data
Prep Method: 524.2
Lab Number Batch Date/TimeInitialFinal
P7J04887100184-01 10/24/17 9:5625 25mL mL
P7J04887100184-02 10/24/17 9:5625 25mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 13
Page 13 of 13
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
11/09/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill (Permit 50-02)
Project No.: 50-02
Lab Submittal Date: 10/11/2017
Prism Work Order: 7100185
TOC analysis was subcontracted to GCAL. Methane, Ethane, Ethene, Carbon Dioxide, Dissolved Oxygen
and Volatile Fatty Acids analyses subcontracted to Pace. Laboratory reports are attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A Initial calibration verification criteria not met for analyte. Analyte is not detected in sample.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 77
Sample Receipt Summary
11/09/2017
Prism Work Order: 7100185
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7100185-01 10/10/17MW-03 10/11/17Water
7100185-02 10/10/17MW-04 10/11/17Water
7100185-03 10/10/17MW-07 10/11/17Water
7100185-04 10/10/17Trip Blank 10/11/17Water
Samples were received at 12.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 77
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7100185
11/09/2017
Summary of Detections
32000 ug/L7100185-01 MW-03 Chloride 9056A
6900 ug/L7100185-01 MW-03 Nitrate as N 9056A
850 J ug/L7100185-01 MW-03 Sulfate 9056A
600 J ug/L7100185-01 MW-03 Biochemical Oxygen Demand SM5210 B
73000 ug/L7100185-01 MW-03 Chemical Oxygen Demand SM5220 D
2.0 J ug/L7100185-01 MW-03 Cyanide SM4500-CN E
17 J ug/L7100185-01 MW-03 Ferrous Iron SM3500-Fe D
79000 ug/L7100185-01 MW-03 Total Alkalinity to pH 4.5 SM2320 B
3.7 J ug/L7100185-01 MW-03 1,4-Dichlorobenzene 8270D
0.095 J ug/L7100185-01 MW-03 Arsenic 6020B
160 ug/L7100185-01 MW-03 Barium 6020B
0.37 J ug/L7100185-01 MW-03 Cadmium 6020B
0.47 J ug/L7100185-01 MW-03 Chromium 6020B
49 ug/L7100185-01 MW-03 Cobalt 6020B
0.61 J ug/L7100185-01 MW-03 Copper 6020B
0.11 J ug/L7100185-01 MW-03 Lead 6020B
17 ug/L7100185-01 MW-03 Nickel 6020B
0.10 J ug/L7100185-01 MW-03 Thallium 6020B
23 ug/L7100185-01 MW-03 Zinc 6020B
80000 ug/L7100185-02 MW-04 Chloride 9056A
1600 ug/L7100185-02 MW-04 Nitrate as N 9056A
67000 ug/L7100185-02 MW-04 Sulfate 9056A
1300 J ug/L7100185-02 MW-04 Biochemical Oxygen Demand SM5210 B
46000 J ug/L7100185-02 MW-04 Chemical Oxygen Demand SM5220 D
160000 ug/L7100185-02 MW-04 Total Alkalinity to pH 4.5 SM2320 B
3.0 J ug/L7100185-02 MW-04 1,4-Dichlorobenzene 8270D
0.12 J ug/L7100185-02 MW-04 Arsenic 6020B
77 ug/L7100185-02 MW-04 Barium 6020B
0.27 J ug/L7100185-02 MW-04 Cadmium 6020B
0.54 J ug/L7100185-02 MW-04 Chromium 6020B
2.7 ug/L7100185-02 MW-04 Cobalt 6020B
0.88 J ug/L7100185-02 MW-04 Copper 6020B
0.24 J ug/L7100185-02 MW-04 Lead 6020B
1.5 J ug/L7100185-02 MW-04 Nickel 6020B
0.68 J ug/L7100185-02 MW-04 Selenium 6020B
0.13 J ug/L7100185-02 MW-04 Vanadium 6020B
31 ug/L7100185-02 MW-04 Zinc 6020B
73000 ug/L7100185-03 MW-07 Chloride 9056A
130 ug/L7100185-03 MW-07 Nitrate as N 9056A
21000 ug/L7100185-03 MW-07 Sulfate 9056A
80 J ug/L7100185-03 MW-07 Biochemical Oxygen Demand SM5210 B
33000 J ug/L7100185-03 MW-07 Chemical Oxygen Demand SM5220 D
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 77
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7100185
11/09/2017
Summary of Detections
1.0 J ug/L7100185-03 MW-07 Cyanide SM4500-CN E
51 J ug/L7100185-03 MW-07 Ferrous Iron SM3500-Fe D
260000 ug/L7100185-03 MW-07 Total Alkalinity to pH 4.5 SM2320 B
3.4 J ug/L7100185-03 MW-07 1,4-Dichlorobenzene 8270D
0.14 J ug/L7100185-03 MW-07 Arsenic 6020B
520 ug/L7100185-03 MW-07 Barium 6020B
0.11 J ug/L7100185-03 MW-07 Cadmium 6020B
0.62 J ug/L7100185-03 MW-07 Chromium 6020B
0.98 J ug/L7100185-03 MW-07 Cobalt 6020B
0.42 J ug/L7100185-03 MW-07 Copper 6020B
0.28 J ug/L7100185-03 MW-07 Lead 6020B
8.2 ug/L7100185-03 MW-07 Nickel 6020B
0.46 J ug/L7100185-03 MW-07 Vanadium 6020B
30 ug/L7100185-03 MW-07 Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-01
Prism Work Order: 7100185
Time Collected: 10/10/17 14:05
Time Submitted: 10/11/17 09:15
MW-03
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02101100010/12/17 9:16 EGCug/L 40ChlorideNE32000
9056A P7J0210110010/12/17 9:16 EGCug/L 7.7Nitrate as N 100006900
9056A P7J02101100010/12/17 9:16 EGCJug/L 200Sulfate250000850
General Chemistry Parameters
SM5210 B P7J01971200010/11/17 15:36 SLSJug/LBiochemical Oxygen Demand NE600
SM5220 D P7J020815000010/12/17 9:55 BMSug/L 17000Chemical Oxygen Demand NE73000
SM4500-CN E P7J022115.0 10/13/17 13:15EGCJug/L 1.0Cyanide102.0
SM3500-Fe D P7J0195120010/11/17 12:10 EGCJug/L 14Ferrous Iron NE17
SM4500-S F P7J01871200010/11/17 12:40EGCug/L 830Sulfide1000<830
SM2320 B P7J02131500010/13/17 9:00 CLBug/L 770Total Alkalinity to pH 4.5 NE79000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311111/6/17 14:53 JMVug/L 2.71,2,4,5-Tetrachlorobenzene 10<2.7
8270D P7J028311111/6/17 14:53 JMVug/L 2.01,2,4-Trichlorobenzene 10<2.0
8270D P7J028311111/6/17 14:53 JMVug/L 1.81,2-Dichlorobenzene 5<1.8
8270D P7J028312211/6/17 14:53 JMVug/L 3.11,3,5-Trinitrobenzene 10<3.1
8270D P7J028311111/6/17 14:53 JMVug/L 2.11,3-Dichlorobenzene 5<2.1
8270D P7J028311111/6/17 14:53 JMVJug/L 1.81,4-Dichlorobenzene 13.7
8270D P7J028311111/6/17 14:53 JMVug/L 3.11,4-Naphthoquinone 10<3.1
8270D P7J028311111/6/17 14:53 JMVug/L 3.21,4-Phenylenediamine 10<3.2
8270D P7J028311111/6/17 14:53 JMVAug/L 1.91-Naphthylamine 10<1.9
8270D P7J028311111/6/17 14:53 JMVug/L 3.12,3,4,6-Tetrachlorophenol 10<3.1
8270D P7J028311111/6/17 14:53 JMVug/L 1.82,4,5-Trichlorophenol 10<1.8
8270D P7J028311111/6/17 14:53 JMVug/L 2.12,4,6-Trichlorophenol 10<2.1
8270D P7J028311111/6/17 14:53 JMVug/L 2.92,4-Dichlorophenol 10<2.9
8270D P7J028311111/6/17 14:53 JMVug/L 3.92,4-Dimethylphenol 10<3.9
8270D P7J028311111/6/17 14:53 JMVug/L 3.02,4-Dinitrophenol 50<3.0
8270D P7J028311111/6/17 14:53 JMVug/L 1.62,4-Dinitrotoluene 10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 2.32,6-Dichlorophenol 10<2.3
8270D P7J028311111/6/17 14:53 JMVug/L 1.32,6-Dinitrotoluene 10<1.3
8270D P7J028311111/6/17 14:53 JMVug/L 3.02-Acetylaminofluorene 20<3.0
8270D P7J028311111/6/17 14:53 JMVug/L 3.02-Chloronaphthalene 10<3.0
8270D P7J028311111/6/17 14:53 JMVug/L 2.12-Chlorophenol 10<2.1
8270D P7J028311111/6/17 14:53 JMVug/L 2.72-Methylnaphthalene 10<2.7
8270D P7J028311111/6/17 14:53 JMVug/L 2.02-Methylphenol 10<2.0
8270D P7J028311111/6/17 14:53 JMVAug/L 2.32-Naphthylamine 10<2.3
8270D P7J028311111/6/17 14:53 JMVug/L 1.62-Nitroaniline 50<1.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-01
Prism Work Order: 7100185
Time Collected: 10/10/17 14:05
Time Submitted: 10/11/17 09:15
MW-03
50-02
SWSL
8270D P7J028311111/6/17 14:53 JMVug/L 2.72-Nitrophenol 10<2.7
8270D P7J028311111/6/17 14:53 JMVug/L 1.63,3’-Dichlorobenzidine 20<1.6
8270D P7J028312211/6/17 14:53 JMVAug/L 3.53,3·-Dimethylbenzidine 10<3.5
8270D P7J028311111/6/17 14:53 JMVug/L 1.73/4-Methylphenol 10<1.7
8270D P7J028311111/6/17 14:53 JMVug/L 2.73-Methylcholanthrene 10<2.7
8270D P7J028311111/6/17 14:53 JMVug/L 1.63-Nitroaniline 50<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.54,6-Dinitro-2-methylphenol 50<1.5
8270D P7J028311111/6/17 14:53 JMVAug/L 2.84-Aminobiphenyl 20<2.8
8270D P7J028311111/6/17 14:53 JMVug/L 1.44-Bromophenyl phenyl ether 10<1.4
8270D P7J028311111/6/17 14:53 JMVug/L 2.74-Chloro-3-methylphenol 20<2.7
8270D P7J028311111/6/17 14:53 JMVug/L 2.84-Chloroaniline 20<2.8
8270D P7J028311111/6/17 14:53 JMVug/L 1.54-Chlorophenyl phenyl ether 10<1.5
8270D P7J028311111/6/17 14:53 JMVug/L 1.04-Nitroaniline 20<1.0
8270D P7J028311111/6/17 14:53 JMVug/L 0.674-Nitrophenol 50<0.67
8270D P7J028311111/6/17 14:53 JMVug/L 3.05-Nitro-o-toluidine 10<3.0
8270D P7J028311111/6/17 14:53 JMVug/L 2.97,12-Dimethylbenz(a)anthracene 10<2.9
8270D P7J028311111/6/17 14:53 JMVug/L 2.0Acenaphthene10<2.0
8270D P7J028311111/6/17 14:53 JMVug/L 2.3Acenaphthylene10<2.3
8270D P7J028311111/6/17 14:53 JMVug/L 2.6Acetophenone10<2.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Anthracene10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Benzo(a)anthracene 10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Benzo(a)pyrene 10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.3Benzo(b)fluoranthene 10<1.3
8270D P7J028312211/6/17 14:53 JMVug/L 1.6Benzo(b&k)fluoranthene NE<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.5Benzo(g,h,i)perylene 10<1.5
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Benzo(k)fluoranthene 10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 2.4Benzyl alcohol 20<2.4
8270D P7J028311111/6/17 14:53 JMVug/L 2.9bis(2-Chloroethoxy)methane 10<2.9
8270D P7J028311111/6/17 14:53 JMVug/L 2.6Bis(2-Chloroethyl)ether 10<2.6
8270D P7J028311111/6/17 14:53 JMVug/L 2.2Bis(2-chloroisopropyl)ether NE<2.2
8270D P7J028311111/6/17 14:53 JMVug/L 1.5Bis(2-Ethylhexyl)phthalate 15<1.5
8270D P7J028311111/6/17 14:53 JMVug/L 1.5Butyl benzyl phthalate 10<1.5
8270D P7J028311111/6/17 14:53 JMVug/L 2.8Chlorobenzilate10<2.8
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Chrysene10<1.6
8270D P7J028312211/6/17 14:53 JMVug/L 3.2Diallate10<3.2
8270D P7J028311111/6/17 14:53 JMVug/L 1.3Dibenzo(a,h)anthracene 10<1.3
8270D P7J028311111/6/17 14:53 JMVug/L 2.0Dibenzofuran10<2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-01
Prism Work Order: 7100185
Time Collected: 10/10/17 14:05
Time Submitted: 10/11/17 09:15
MW-03
50-02
SWSL
8270D P7J028311111/6/17 14:53 JMVug/L 3.7Diethyl phthalate 6000<3.7
8270D P7J028311111/6/17 14:53 JMVug/L 3.5Dimethoate20<3.5
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Dimethyl phthalate 10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.9Di-n-butyl phthalate 10<1.9
8270D P7J028311111/6/17 14:53 JMVug/L 1.5Di-n-octyl phthalate 10<1.5
8270D P7J028311111/6/17 14:53 JMVug/L 3.1Diphenylamine10<3.1
8270D P7J028312211/6/17 14:53 JMVug/L 3.2Disulfoton10<3.2
8270D P7J028311111/6/17 14:53 JMVug/L 3.1Ethyl Methanesulfonate 20<3.1
8270D P7J028312211/7/17 16:21 JMVug/L 4.8Famphur20<4.8
8270D P7J028311111/6/17 14:53 JMVug/L 1.9Fluoranthene10<1.9
8270D P7J028311111/6/17 14:53 JMVug/L 1.9Fluorene10<1.9
8270D P7J028311111/6/17 14:53 JMVug/L 1.4Hexachlorobenzene10<1.4
8270D P7J028311111/6/17 14:53 JMVug/L 2.4Hexachlorobutadiene10<2.4
8270D P7J028311111/6/17 14:53 JMVug/L 1.9Hexachlorocyclopentadiene10<1.9
8270D P7J028311111/6/17 14:53 JMVug/L 2.0Hexachloroethane10<2.0
8270D P7J028311111/6/17 14:53 JMVug/L 2.2Hexachloropropene10<2.2
8270D P7J028311111/6/17 14:53 JMVug/L 4.4Indeno(1,2,3-cd)pyrene 10<4.4
8270D P7J028311111/6/17 14:53 JMVug/L 3.0Isodrin20<3.0
8270D P7J028311111/6/17 14:53 JMVug/L 2.8Isophorone10<2.8
8270D P7J028311111/6/17 14:53 JMVug/L 4.3Isosafrole10<4.3
8270D P7J028312211/7/17 16:21 JMVug/L 3.2Kepone20<3.2
8270D P7J0283111011/6/17 14:53 JMVAug/L 13Methapyrilene100<13
8270D P7J028312211/6/17 14:53 JMVug/L 2.7Methyl Methanesulfonate 10<2.7
8270D P7J028312211/6/17 14:53 JMVug/L 3.8Methyl parathion 10<3.8
8270D P7J028311111/6/17 14:53 JMVug/L 2.9Nitrobenzene10<2.9
8270D P7J028311111/6/17 14:53 JMVug/L 2.8N-Nitrosodibutylamine 10<2.8
8270D P7J028311111/6/17 14:53 JMVug/L 2.0N-Nitrosodiethylamine 20<2.0
8270D P7J028311111/6/17 14:53 JMVug/L 1.3N-Nitrosodimethylamine 10<1.3
8270D P7J028311111/6/17 14:53 JMVug/L 2.4N-Nitroso-di-n-propylamine 10<2.4
8270D P7J028311111/6/17 14:53 JMVug/L 1.5N-Nitrosodiphenylamine 10<1.5
8270D P7J028311111/6/17 14:53 JMVug/L 1.7N-Nitrosomethylethylamine 10<1.7
8270D P7J028311111/6/17 14:53 JMVug/L 2.7N-Nitrosopiperidine 20<2.7
8270D P7J028311111/6/17 14:53 JMVug/L 2.2N-Nitrosopyrrolidine 10<2.2
8270D P7J028311111/6/17 14:53 JMVug/L 3.1O,O,O-Triethyl phosphorothioate 10<3.1
8270D P7J028311111/6/17 14:53 JMVAug/L 2.0o-Toluidine 10<2.0
8270D P7J028311111/6/17 14:53 JMVug/L 3.4Parathion10<3.4
8270D P7J028312211/6/17 14:53 JMVug/L 2.5p-Dimethylaminoazobenzene 10<2.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-01
Prism Work Order: 7100185
Time Collected: 10/10/17 14:05
Time Submitted: 10/11/17 09:15
MW-03
50-02
SWSL
8270D P7J028311111/6/17 14:53 JMVug/L 2.9Pentachlorobenzene10<2.9
8270D P7J028311111/6/17 14:53 JMVug/L 2.6Pentachloronitrobenzene20<2.6
8270D P7J028311111/6/17 14:53 JMVug/L 1.4Pentachlorophenol25<1.4
8270D P7J028312211/6/17 14:53 JMVug/L 3.3Phenacetin20<3.3
8270D P7J028311111/6/17 14:53 JMVug/L 1.7Phenanthrene10<1.7
8270D P7J028311111/6/17 14:53 JMVug/L 1.1Phenol10<1.1
8270D P7J028311111/6/17 14:53 JMVug/L 3.1Phorate10<3.1
8270D P7J028311111/6/17 14:53 JMVug/L 3.2Pronamide10<3.2
8270D P7J028311111/6/17 14:53 JMVug/L 1.6Pyrene10<1.6
8270D P7J028311111/6/17 14:53 JMVug/L 2.5Safrole10<2.5
8270D P7J028311111/6/17 14:53 JMVug/L 2.2Thionazin20<2.2
Surrogate Recovery Control Limits
44-11983 %2-Fluorobiphenyl
19-11928 %2-Fluorophenol
44-12076 %Nitrobenzene-d5
11-5219 %Phenol-d5
50-13487 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 15:04JABug/L 0.036Mercury0.2<0.036
6020B P7J034011.0 10/19/17 17:59EGCug/L 0.19Antimony6<0.19
6020B P7J020011.0 10/16/17 16:19EGCJug/L 0.031Arsenic100.095
6020B P7J034015.0 10/19/17 17:59EGCug/L 0.97Barium100160
6020B P7J020011.0 10/16/17 16:19EGCug/L 0.057Beryllium1<0.057
6020B P7J020011.0 10/16/17 16:19EGCJug/L 0.078Cadmium10.37
6020B P7J020011.0 10/16/17 16:19EGCJug/L 0.19Chromium100.47
6020B P7J020011.0 10/16/17 16:19EGCug/L 0.0071Cobalt1049
6020B P7J020015.0 10/16/17 16:19EGCJug/L 0.22Copper100.61
6020B P7J020011.0 10/16/17 16:19EGCJug/L 0.093Lead100.11
6020B P7J020012.0 10/16/17 16:19EGCug/L 0.85Nickel5017
6020B P7J020015.0 10/16/17 16:19EGCug/L 0.63Selenium10<0.63
6020B P7J020015.0 10/16/17 16:19EGCug/L 0.063Silver10<0.063
6020B P7J020011.0 10/16/17 16:19EGCJug/L 0.099Thallium5.50.10
6020B P7J020011010/16/17 16:19EGCug/L 0.21Tin100<0.21
6020B P7J020011.0 10/16/17 16:19EGCug/L 0.10Vanadium25<0.10
6020B P7J034011010/19/17 17:59EGCug/L 2.8Zinc1023
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-01
Prism Work Order: 7100185
Time Collected: 10/10/17 14:05
Time Submitted: 10/11/17 09:15
MW-03
50-02
SWSL
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 8:33 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 8:33 KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 8:33 KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 8:33 KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 8:33 KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 8:33 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 8:33 KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 8:33 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 8:33 KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.065Dibromomethane10<0.065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-01
Prism Work Order: 7100185
Time Collected: 10/10/17 14:05
Time Submitted: 10/11/17 09:15
MW-03
50-02
SWSL
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 8:33 KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 8:33 KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 8:33 KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 8:33 KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 8:33 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 8:33 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 8:33 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 8:33 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 8:33 KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 8:33 KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 8:33 KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 8:33 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 8:33 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 8:33 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 8:33 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 8:33 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12996 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-02
Prism Work Order: 7100185
Time Collected: 10/10/17 09:45
Time Submitted: 10/11/17 09:15
MW-04
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02101100010/11/17 15:58 BMSug/L 40ChlorideNE80000
9056A P7J0210110010/11/17 15:58 BMSug/L 7.7Nitrate as N 100001600
9056A P7J02101100010/11/17 15:58 BMSug/L 200Sulfate25000067000
General Chemistry Parameters
SM5210 B P7J01971200010/11/17 15:36 SLSJug/LBiochemical Oxygen Demand NE1300
SM5220 D P7J020815000010/12/17 9:55 BMSJug/L 17000Chemical Oxygen Demand NE46000
SM4500-CN E P7J022115.0 10/13/17 13:15EGCug/L 1.0Cyanide10<1.0
SM3500-Fe D P7J0195120010/11/17 12:10EGCug/L 14Ferrous Iron NE<14
SM4500-S F P7J01871200010/11/17 12:40EGCug/L 830Sulfide1000<830
SM2320 B P7J02131500010/13/17 9:00 CLBug/L 770Total Alkalinity to pH 4.5 NE160000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311011/6/17 15:15 JMVug/L 2.51,2,4,5-Tetrachlorobenzene 10<2.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.81,2,4-Trichlorobenzene 10<1.8
8270D P7J028311011/6/17 15:15 JMVug/L 1.71,2-Dichlorobenzene 5<1.7
8270D P7J028312111/6/17 15:15 JMVug/L 2.81,3,5-Trinitrobenzene 10<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 1.91,3-Dichlorobenzene 5<1.9
8270D P7J028311011/6/17 15:15 JMVJug/L 1.71,4-Dichlorobenzene 13.0
8270D P7J028311011/6/17 15:15 JMVug/L 2.81,4-Naphthoquinone 10<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 2.91,4-Phenylenediamine 10<2.9
8270D P7J028311011/6/17 15:15 JMVAug/L 1.81-Naphthylamine 10<1.8
8270D P7J028311011/6/17 15:15 JMVug/L 2.92,3,4,6-Tetrachlorophenol 10<2.9
8270D P7J028311011/6/17 15:15 JMVug/L 1.62,4,5-Trichlorophenol 10<1.6
8270D P7J028311011/6/17 15:15 JMVug/L 1.92,4,6-Trichlorophenol 10<1.9
8270D P7J028311011/6/17 15:15 JMVug/L 2.62,4-Dichlorophenol 10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 3.62,4-Dimethylphenol 10<3.6
8270D P7J028311011/6/17 15:15 JMVug/L 2.82,4-Dinitrophenol 50<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 1.52,4-Dinitrotoluene 10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 2.12,6-Dichlorophenol 10<2.1
8270D P7J028311011/6/17 15:15 JMVug/L 1.22,6-Dinitrotoluene 10<1.2
8270D P7J028311011/6/17 15:15 JMVug/L 2.82-Acetylaminofluorene 20<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 2.82-Chloronaphthalene 10<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 1.92-Chlorophenol 10<1.9
8270D P7J028311011/6/17 15:15 JMVug/L 2.52-Methylnaphthalene 10<2.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.92-Methylphenol 10<1.9
8270D P7J028311011/6/17 15:15 JMVAug/L 2.12-Naphthylamine 10<2.1
8270D P7J028311011/6/17 15:15 JMVug/L 1.52-Nitroaniline 50<1.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-02
Prism Work Order: 7100185
Time Collected: 10/10/17 09:45
Time Submitted: 10/11/17 09:15
MW-04
50-02
SWSL
8270D P7J028311011/6/17 15:15 JMVug/L 2.42-Nitrophenol 10<2.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.53,3’-Dichlorobenzidine 20<1.5
8270D P7J028312111/6/17 15:15 JMVAug/L 3.23,3·-Dimethylbenzidine 10<3.2
8270D P7J028311011/6/17 15:15 JMVug/L 1.63/4-Methylphenol 10<1.6
8270D P7J028311011/6/17 15:15 JMVug/L 2.53-Methylcholanthrene 10<2.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.43-Nitroaniline 50<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.44,6-Dinitro-2-methylphenol 50<1.4
8270D P7J028311011/6/17 15:15 JMVAug/L 2.54-Aminobiphenyl 20<2.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.34-Bromophenyl phenyl ether 10<1.3
8270D P7J028311011/6/17 15:15 JMVug/L 2.44-Chloro-3-methylphenol 20<2.4
8270D P7J028311011/6/17 15:15 JMVug/L 2.54-Chloroaniline 20<2.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.44-Chlorophenyl phenyl ether 10<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 0.964-Nitroaniline 20<0.96
8270D P7J028311011/6/17 15:15 JMVug/L 0.624-Nitrophenol 50<0.62
8270D P7J028311011/6/17 15:15 JMVug/L 2.75-Nitro-o-toluidine 10<2.7
8270D P7J028311011/6/17 15:15 JMVug/L 2.77,12-Dimethylbenz(a)anthracene 10<2.7
8270D P7J028311011/6/17 15:15 JMVug/L 1.9Acenaphthene10<1.9
8270D P7J028311011/6/17 15:15 JMVug/L 2.1Acenaphthylene10<2.1
8270D P7J028311011/6/17 15:15 JMVug/L 2.4Acetophenone10<2.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Anthracene10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Benzo(a)anthracene 10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Benzo(a)pyrene 10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.2Benzo(b)fluoranthene 10<1.2
8270D P7J028312111/6/17 15:15 JMVug/L 1.5Benzo(b&k)fluoranthene NE<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.4Benzo(g,h,i)perylene 10<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Benzo(k)fluoranthene 10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 2.2Benzyl alcohol 20<2.2
8270D P7J028311011/6/17 15:15 JMVug/L 2.6bis(2-Chloroethoxy)methane 10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 2.4Bis(2-Chloroethyl)ether 10<2.4
8270D P7J028311011/6/17 15:15 JMVug/L 2.0Bis(2-chloroisopropyl)ether NE<2.0
8270D P7J028311011/6/17 15:15 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate 15<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.4Butyl benzyl phthalate 10<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 2.6Chlorobenzilate10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Chrysene10<1.5
8270D P7J028312111/6/17 15:15 JMVug/L 2.9Diallate10<2.9
8270D P7J028311011/6/17 15:15 JMVug/L 1.2Dibenzo(a,h)anthracene 10<1.2
8270D P7J028311011/6/17 15:15 JMVug/L 1.8Dibenzofuran10<1.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-02
Prism Work Order: 7100185
Time Collected: 10/10/17 09:45
Time Submitted: 10/11/17 09:15
MW-04
50-02
SWSL
8270D P7J028311011/6/17 15:15 JMVug/L 3.4Diethyl phthalate 6000<3.4
8270D P7J028311011/6/17 15:15 JMVug/L 3.2Dimethoate20<3.2
8270D P7J028311011/6/17 15:15 JMVug/L 1.4Dimethyl phthalate 10<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.7Di-n-butyl phthalate 10<1.7
8270D P7J028311011/6/17 15:15 JMVug/L 1.3Di-n-octyl phthalate 10<1.3
8270D P7J028311011/6/17 15:15 JMVug/L 2.9Diphenylamine10<2.9
8270D P7J028312111/6/17 15:15 JMVug/L 2.9Disulfoton10<2.9
8270D P7J028311011/6/17 15:15 JMVug/L 2.9Ethyl Methanesulfonate 20<2.9
8270D P7J028312111/7/17 16:44 JMVug/L 4.4Famphur20<4.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.7Fluoranthene10<1.7
8270D P7J028311011/6/17 15:15 JMVug/L 1.7Fluorene10<1.7
8270D P7J028311011/6/17 15:15 JMVug/L 1.3Hexachlorobenzene10<1.3
8270D P7J028311011/6/17 15:15 JMVug/L 2.2Hexachlorobutadiene10<2.2
8270D P7J028311011/6/17 15:15 JMVug/L 1.8Hexachlorocyclopentadiene10<1.8
8270D P7J028311011/6/17 15:15 JMVug/L 1.8Hexachloroethane10<1.8
8270D P7J028311011/6/17 15:15 JMVug/L 2.1Hexachloropropene10<2.1
8270D P7J028311011/6/17 15:15 JMVug/L 4.0Indeno(1,2,3-cd)pyrene 10<4.0
8270D P7J028311011/6/17 15:15 JMVug/L 2.8Isodrin20<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 2.6Isophorone10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 3.9Isosafrole10<3.9
8270D P7J028312111/7/17 16:44 JMVug/L 2.9Kepone20<2.9
8270D P7J0283110011/6/17 15:15 JMVAug/L 12Methapyrilene100<12
8270D P7J028312111/6/17 15:15 JMVug/L 2.4Methyl Methanesulfonate 10<2.4
8270D P7J028312111/6/17 15:15 JMVug/L 3.5Methyl parathion 10<3.5
8270D P7J028311011/6/17 15:15 JMVug/L 2.6Nitrobenzene10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 2.6N-Nitrosodibutylamine 10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 1.9N-Nitrosodiethylamine 20<1.9
8270D P7J028311011/6/17 15:15 JMVug/L 1.2N-Nitrosodimethylamine 10<1.2
8270D P7J028311011/6/17 15:15 JMVug/L 2.2N-Nitroso-di-n-propylamine 10<2.2
8270D P7J028311011/6/17 15:15 JMVug/L 1.4N-Nitrosodiphenylamine 10<1.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.6N-Nitrosomethylethylamine 10<1.6
8270D P7J028311011/6/17 15:15 JMVug/L 2.5N-Nitrosopiperidine 20<2.5
8270D P7J028311011/6/17 15:15 JMVug/L 2.0N-Nitrosopyrrolidine 10<2.0
8270D P7J028311011/6/17 15:15 JMVug/L 2.8O,O,O-Triethyl phosphorothioate 10<2.8
8270D P7J028311011/6/17 15:15 JMVAug/L 1.8o-Toluidine 10<1.8
8270D P7J028311011/6/17 15:15 JMVug/L 3.1Parathion10<3.1
8270D P7J028312111/6/17 15:15 JMVug/L 2.3p-Dimethylaminoazobenzene 10<2.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-02
Prism Work Order: 7100185
Time Collected: 10/10/17 09:45
Time Submitted: 10/11/17 09:15
MW-04
50-02
SWSL
8270D P7J028311011/6/17 15:15 JMVug/L 2.6Pentachlorobenzene10<2.6
8270D P7J028311011/6/17 15:15 JMVug/L 2.4Pentachloronitrobenzene20<2.4
8270D P7J028311011/6/17 15:15 JMVug/L 1.3Pentachlorophenol25<1.3
8270D P7J028312111/6/17 15:15 JMVug/L 3.1Phenacetin20<3.1
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Phenanthrene10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 1.0Phenol10<1.0
8270D P7J028311011/6/17 15:15 JMVug/L 2.8Phorate10<2.8
8270D P7J028311011/6/17 15:15 JMVug/L 2.9Pronamide10<2.9
8270D P7J028311011/6/17 15:15 JMVug/L 1.5Pyrene10<1.5
8270D P7J028311011/6/17 15:15 JMVug/L 2.3Safrole10<2.3
8270D P7J028311011/6/17 15:15 JMVug/L 2.0Thionazin20<2.0
Surrogate Recovery Control Limits
44-11978 %2-Fluorobiphenyl
19-11922 %2-Fluorophenol
44-12070 %Nitrobenzene-d5
11-5217 %Phenol-d5
50-13479 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 15:08JABug/L 0.036Mercury0.2<0.036
6020B P7J034011.0 10/19/17 18:24EGCug/L 0.19Antimony6<0.19
6020B P7J020011.0 10/16/17 16:28EGCJug/L 0.031Arsenic100.12
6020B P7J034015.0 10/19/17 18:24EGCug/L 0.97Barium10077
6020B P7J020011.0 10/16/17 16:28EGCug/L 0.057Beryllium1<0.057
6020B P7J020011.0 10/16/17 16:28EGCJug/L 0.078Cadmium10.27
6020B P7J020011.0 10/16/17 16:28EGCJug/L 0.19Chromium100.54
6020B P7J020011.0 10/16/17 16:28EGCug/L 0.0071Cobalt102.7
6020B P7J020015.0 10/16/17 16:28EGCJug/L 0.22Copper100.88
6020B P7J020011.0 10/16/17 16:28EGCJug/L 0.093Lead100.24
6020B P7J020012.0 10/16/17 16:28EGCJug/L 0.85Nickel501.5
6020B P7J020015.0 10/16/17 16:28EGCJug/L 0.63Selenium100.68
6020B P7J020015.0 10/16/17 16:28EGCug/L 0.063Silver10<0.063
6020B P7J020011.0 10/16/17 16:28EGCug/L 0.099Thallium5.5<0.099
6020B P7J020011010/16/17 16:28EGCug/L 0.21Tin100<0.21
6020B P7J020011.0 10/16/17 16:28EGCJug/L 0.10Vanadium250.13
6020B P7J034011010/19/17 18:24EGCug/L 2.8Zinc1031
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-02
Prism Work Order: 7100185
Time Collected: 10/10/17 09:45
Time Submitted: 10/11/17 09:15
MW-04
50-02
SWSL
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 8:58 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 8:58 KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 8:58 KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 8:58 KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 8:58 KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 8:58 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 8:58 KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 8:58 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 8:58 KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.065Dibromomethane10<0.065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-02
Prism Work Order: 7100185
Time Collected: 10/10/17 09:45
Time Submitted: 10/11/17 09:15
MW-04
50-02
SWSL
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 8:58 KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 8:58 KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 8:58 KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 8:58 KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 8:58 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 8:58 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 8:58 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 8:58 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 8:58 KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 8:58 KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 8:58 KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 8:58 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 8:58 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 8:58 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 8:58 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 8:58 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12995 %Dibromofluoromethane
77-12399 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-03
Prism Work Order: 7100185
Time Collected: 10/10/17 11:21
Time Submitted: 10/11/17 09:15
MW-07
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02101100010/11/17 16:14 BMSug/L 40ChlorideNE73000
9056A P7J0210110010/11/17 16:14 BMSug/L 7.7Nitrate as N 10000130
9056A P7J02101100010/11/17 16:14 BMSug/L 200Sulfate25000021000
General Chemistry Parameters
SM5210 B P7J01971200010/11/17 15:36 SLSJug/LBiochemical Oxygen Demand NE80
SM5220 D P7J020815000010/12/17 9:55 BMSJug/L 17000Chemical Oxygen Demand NE33000
SM4500-CN E P7J022115.0 10/13/17 13:15EGCJug/L 1.0Cyanide101.0
SM3500-Fe D P7J0195120010/11/17 12:10 EGCJug/L 14Ferrous Iron NE51
SM4500-S F P7J01871200010/11/17 12:40EGCug/L 830Sulfide1000<830
SM2320 B P7J02131500010/13/17 9:00 CLBug/L 770Total Alkalinity to pH 4.5 NE260000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311011/6/17 15:37 JMVug/L 2.41,2,4,5-Tetrachlorobenzene 10<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.81,2,4-Trichlorobenzene 10<1.8
8270D P7J028311011/6/17 15:37 JMVug/L 1.61,2-Dichlorobenzene 5<1.6
8270D P7J028312011/6/17 15:37 JMVug/L 2.81,3,5-Trinitrobenzene 10<2.8
8270D P7J028311011/6/17 15:37 JMVug/L 1.91,3-Dichlorobenzene 5<1.9
8270D P7J028311011/6/17 15:37 JMVJug/L 1.61,4-Dichlorobenzene 13.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.71,4-Naphthoquinone 10<2.7
8270D P7J028311011/6/17 15:37 JMVug/L 2.81,4-Phenylenediamine 10<2.8
8270D P7J028311011/6/17 15:37 JMVAug/L 1.71-Naphthylamine 10<1.7
8270D P7J028311011/6/17 15:37 JMVug/L 2.82,3,4,6-Tetrachlorophenol 10<2.8
8270D P7J028311011/6/17 15:37 JMVug/L 1.62,4,5-Trichlorophenol 10<1.6
8270D P7J028311011/6/17 15:37 JMVug/L 1.82,4,6-Trichlorophenol 10<1.8
8270D P7J028311011/6/17 15:37 JMVug/L 2.62,4-Dichlorophenol 10<2.6
8270D P7J028311011/6/17 15:37 JMVug/L 3.42,4-Dimethylphenol 10<3.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.72,4-Dinitrophenol 50<2.7
8270D P7J028311011/6/17 15:37 JMVug/L 1.42,4-Dinitrotoluene 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.02,6-Dichlorophenol 10<2.0
8270D P7J028311011/6/17 15:37 JMVug/L 1.12,6-Dinitrotoluene 10<1.1
8270D P7J028311011/6/17 15:37 JMVug/L 2.72-Acetylaminofluorene 20<2.7
8270D P7J028311011/6/17 15:37 JMVug/L 2.72-Chloronaphthalene 10<2.7
8270D P7J028311011/6/17 15:37 JMVug/L 1.92-Chlorophenol 10<1.9
8270D P7J028311011/6/17 15:37 JMVug/L 2.42-Methylnaphthalene 10<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.82-Methylphenol 10<1.8
8270D P7J028311011/6/17 15:37 JMVAug/L 2.12-Naphthylamine 10<2.1
8270D P7J028311011/6/17 15:37 JMVug/L 1.42-Nitroaniline 50<1.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-03
Prism Work Order: 7100185
Time Collected: 10/10/17 11:21
Time Submitted: 10/11/17 09:15
MW-07
50-02
SWSL
8270D P7J028311011/6/17 15:37 JMVug/L 2.42-Nitrophenol 10<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.43,3’-Dichlorobenzidine 20<1.4
8270D P7J028312011/6/17 15:37 JMVAug/L 3.13,3·-Dimethylbenzidine 10<3.1
8270D P7J028311011/6/17 15:37 JMVug/L 1.53/4-Methylphenol 10<1.5
8270D P7J028311011/6/17 15:37 JMVug/L 2.43-Methylcholanthrene 10<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.43-Nitroaniline 50<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.44,6-Dinitro-2-methylphenol 50<1.4
8270D P7J028311011/6/17 15:37 JMVAug/L 2.44-Aminobiphenyl 20<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.34-Bromophenyl phenyl ether 10<1.3
8270D P7J028311011/6/17 15:37 JMVug/L 2.44-Chloro-3-methylphenol 20<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.44-Chloroaniline 20<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.34-Chlorophenyl phenyl ether 10<1.3
8270D P7J028311011/6/17 15:37 JMVug/L 0.934-Nitroaniline 20<0.93
8270D P7J028311011/6/17 15:37 JMVug/L 0.604-Nitrophenol 50<0.60
8270D P7J028311011/6/17 15:37 JMVug/L 2.65-Nitro-o-toluidine 10<2.6
8270D P7J028311011/6/17 15:37 JMVug/L 2.67,12-Dimethylbenz(a)anthracene 10<2.6
8270D P7J028311011/6/17 15:37 JMVug/L 1.8Acenaphthene10<1.8
8270D P7J028311011/6/17 15:37 JMVug/L 2.0Acenaphthylene10<2.0
8270D P7J028311011/6/17 15:37 JMVug/L 2.4Acetophenone10<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Anthracene10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Benzo(a)anthracene 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Benzo(a)pyrene 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.1Benzo(b)fluoranthene 10<1.1
8270D P7J028312011/6/17 15:37 JMVug/L 1.4Benzo(b&k)fluoranthene NE<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Benzo(g,h,i)perylene 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Benzo(k)fluoranthene 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.1Benzyl alcohol 20<2.1
8270D P7J028311011/6/17 15:37 JMVug/L 2.6bis(2-Chloroethoxy)methane 10<2.6
8270D P7J028311011/6/17 15:37 JMVug/L 2.3Bis(2-Chloroethyl)ether 10<2.3
8270D P7J028311011/6/17 15:37 JMVug/L 2.0Bis(2-chloroisopropyl)ether NE<2.0
8270D P7J028311011/6/17 15:37 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate 15<1.3
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Butyl benzyl phthalate 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.5Chlorobenzilate10<2.5
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Chrysene10<1.4
8270D P7J028312011/6/17 15:37 JMVug/L 2.8Diallate10<2.8
8270D P7J028311011/6/17 15:37 JMVug/L 1.2Dibenzo(a,h)anthracene 10<1.2
8270D P7J028311011/6/17 15:37 JMVug/L 1.8Dibenzofuran10<1.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-03
Prism Work Order: 7100185
Time Collected: 10/10/17 11:21
Time Submitted: 10/11/17 09:15
MW-07
50-02
SWSL
8270D P7J028311011/6/17 15:37 JMVug/L 3.3Diethyl phthalate 6000<3.3
8270D P7J028311011/6/17 15:37 JMVug/L 3.1Dimethoate20<3.1
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Dimethyl phthalate 10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.7Di-n-butyl phthalate 10<1.7
8270D P7J028311011/6/17 15:37 JMVug/L 1.3Di-n-octyl phthalate 10<1.3
8270D P7J028311011/6/17 15:37 JMVug/L 2.8Diphenylamine10<2.8
8270D P7J028312011/6/17 15:37 JMVug/L 2.8Disulfoton10<2.8
8270D P7J028311011/6/17 15:37 JMVug/L 2.8Ethyl Methanesulfonate 20<2.8
8270D P7J028312011/7/17 17:07 JMVug/L 4.3Famphur20<4.3
8270D P7J028311011/6/17 15:37 JMVug/L 1.7Fluoranthene10<1.7
8270D P7J028311011/6/17 15:37 JMVug/L 1.7Fluorene10<1.7
8270D P7J028311011/6/17 15:37 JMVug/L 1.3Hexachlorobenzene10<1.3
8270D P7J028311011/6/17 15:37 JMVug/L 2.1Hexachlorobutadiene10<2.1
8270D P7J028311011/6/17 15:37 JMVug/L 1.7Hexachlorocyclopentadiene10<1.7
8270D P7J028311011/6/17 15:37 JMVug/L 1.7Hexachloroethane10<1.7
8270D P7J028311011/6/17 15:37 JMVug/L 2.0Hexachloropropene10<2.0
8270D P7J028311011/6/17 15:37 JMVug/L 3.9Indeno(1,2,3-cd)pyrene 10<3.9
8270D P7J028311011/6/17 15:37 JMVug/L 2.7Isodrin20<2.7
8270D P7J028311011/6/17 15:37 JMVug/L 2.5Isophorone10<2.5
8270D P7J028311011/6/17 15:37 JMVug/L 3.8Isosafrole10<3.8
8270D P7J028312011/7/17 17:07 JMVug/L 2.8Kepone20<2.8
8270D P7J0283110011/6/17 15:37 JMVAug/L 12Methapyrilene100<12
8270D P7J028312011/6/17 15:37 JMVug/L 2.4Methyl Methanesulfonate 10<2.4
8270D P7J028312011/6/17 15:37 JMVug/L 3.4Methyl parathion 10<3.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.6Nitrobenzene10<2.6
8270D P7J028311011/6/17 15:37 JMVug/L 2.5N-Nitrosodibutylamine 10<2.5
8270D P7J028311011/6/17 15:37 JMVug/L 1.8N-Nitrosodiethylamine 20<1.8
8270D P7J028311011/6/17 15:37 JMVug/L 1.1N-Nitrosodimethylamine 10<1.1
8270D P7J028311011/6/17 15:37 JMVug/L 2.2N-Nitroso-di-n-propylamine 10<2.2
8270D P7J028311011/6/17 15:37 JMVug/L 1.3N-Nitrosodiphenylamine 10<1.3
8270D P7J028311011/6/17 15:37 JMVug/L 1.5N-Nitrosomethylethylamine 10<1.5
8270D P7J028311011/6/17 15:37 JMVug/L 2.4N-Nitrosopiperidine 20<2.4
8270D P7J028311011/6/17 15:37 JMVug/L 1.9N-Nitrosopyrrolidine 10<1.9
8270D P7J028311011/6/17 15:37 JMVug/L 2.8O,O,O-Triethyl phosphorothioate 10<2.8
8270D P7J028311011/6/17 15:37 JMVAug/L 1.8o-Toluidine 10<1.8
8270D P7J028311011/6/17 15:37 JMVug/L 3.0Parathion10<3.0
8270D P7J028312011/6/17 15:37 JMVug/L 2.3p-Dimethylaminoazobenzene 10<2.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-03
Prism Work Order: 7100185
Time Collected: 10/10/17 11:21
Time Submitted: 10/11/17 09:15
MW-07
50-02
SWSL
8270D P7J028311011/6/17 15:37 JMVug/L 2.6Pentachlorobenzene10<2.6
8270D P7J028311011/6/17 15:37 JMVug/L 2.3Pentachloronitrobenzene20<2.3
8270D P7J028311011/6/17 15:37 JMVug/L 1.2Pentachlorophenol25<1.2
8270D P7J028312011/6/17 15:37 JMVug/L 3.0Phenacetin20<3.0
8270D P7J028311011/6/17 15:37 JMVug/L 1.5Phenanthrene10<1.5
8270D P7J028311011/6/17 15:37 JMVug/L 0.98Phenol10<0.98
8270D P7J028311011/6/17 15:37 JMVug/L 2.8Phorate10<2.8
8270D P7J028311011/6/17 15:37 JMVug/L 2.8Pronamide10<2.8
8270D P7J028311011/6/17 15:37 JMVug/L 1.4Pyrene10<1.4
8270D P7J028311011/6/17 15:37 JMVug/L 2.2Safrole10<2.2
8270D P7J028311011/6/17 15:37 JMVug/L 1.9Thionazin20<1.9
Surrogate Recovery Control Limits
44-11986 %2-Fluorobiphenyl
19-11954 %2-Fluorophenol
44-12078 %Nitrobenzene-d5
11-5234 %Phenol-d5
50-13486 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 15:12JABug/L 0.036Mercury0.2<0.036
6020B P7J034011.0 10/19/17 18:32EGCug/L 0.19Antimony6<0.19
6020B P7J020011.0 10/16/17 16:36EGCJug/L 0.031Arsenic100.14
6020B P7J034015.0 10/19/17 18:32EGCug/L 0.97Barium100520
6020B P7J020011.0 10/16/17 16:36EGCug/L 0.057Beryllium1<0.057
6020B P7J020011.0 10/16/17 16:36EGCJug/L 0.078Cadmium10.11
6020B P7J020011.0 10/16/17 16:36EGCJug/L 0.19Chromium100.62
6020B P7J020011.0 10/16/17 16:36EGCJug/L 0.0071Cobalt100.98
6020B P7J020015.0 10/16/17 16:36EGCJug/L 0.22Copper100.42
6020B P7J020011.0 10/16/17 16:36EGCJug/L 0.093Lead100.28
6020B P7J020012.0 10/16/17 16:36EGCug/L 0.85Nickel508.2
6020B P7J020015.0 10/16/17 16:36EGCug/L 0.63Selenium10<0.63
6020B P7J020015.0 10/16/17 16:36EGCug/L 0.063Silver10<0.063
6020B P7J020011.0 10/16/17 16:36EGCug/L 0.099Thallium5.5<0.099
6020B P7J020011010/16/17 16:36EGCug/L 0.21Tin100<0.21
6020B P7J020011.0 10/16/17 16:36EGCJug/L 0.10Vanadium250.46
6020B P7J034011010/19/17 18:32EGCug/L 2.8Zinc1030
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-03
Prism Work Order: 7100185
Time Collected: 10/10/17 11:21
Time Submitted: 10/11/17 09:15
MW-07
50-02
SWSL
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 9:24 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 9:24 KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 9:24 KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 9:24 KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 9:24 KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 9:24 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 9:24 KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 9:24 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 9:24 KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.065Dibromomethane10<0.065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-03
Prism Work Order: 7100185
Time Collected: 10/10/17 11:21
Time Submitted: 10/11/17 09:15
MW-07
50-02
SWSL
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 9:24 KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 9:24 KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 9:24 KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 9:24 KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 9:24 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 9:24 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 9:24 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 9:24 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 9:24 KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 9:24 KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 9:24 KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 9:24 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 9:24 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 9:24 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 9:24 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 9:24 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12997 %Dibromofluoromethane
77-12399 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-04
Prism Work Order: 7100185
Time Collected: 10/10/17 00:00
Time Submitted: 10/11/17 09:15
Trip Blank
50-02
SWSL
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 6:25 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 6:25 KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 6:25 KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 6:25 KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 6:25 KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 6:25 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 6:25 KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 6:25 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 6:25 KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 77
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100185-04
Prism Work Order: 7100185
Time Collected: 10/10/17 00:00
Time Submitted: 10/11/17 09:15
Trip Blank
50-02
SWSL
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.065Dibromomethane10<0.065
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 6:25 KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 6:25 KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 6:25 KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 6:25 KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 6:25 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 6:25 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 6:25 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 6:25 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 6:25 KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 6:25 KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 6:25 KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 6:25 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 6:25 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 6:25 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 6:25 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 6:25 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12995 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
Blank (P7J0385-BLK1)Prepared: 10/21/17 Analyzed: 10/22/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
Acetone ug/LBRL5.0
Acetonitrile ug/LBRL10
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Allyl Chloride (3-Chloropropylene)ug/LBRL10
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
Chloroprene ug/LBRL10
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethyl Methacrylate ug/LBRL10
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isobutyl alcohol ug/LBRL20
m,p-Xylenes ug/LBRL1.0
Methacrylonitrile ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
Blank (P7J0385-BLK1)Prepared: 10/21/17 Analyzed: 10/22/17
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methyl Methacrylate ug/LBRL10
Methylene Chloride ug/LBRL1.0
Naphthalene ug/LBRL1.0
o-Xylene ug/LBRL0.50
Propionitrile (Ethyl Cyanide)ug/LBRL10
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9246.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9446.9
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.5
LCS (P7J0385-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 79-13498
1,1,1-Trichloroethane ug/L21.3 0.50 20.00 75-136107
1,1,2,2-Tetrachloroethane ug/L21.0 0.50 20.00 62-127105
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-140103
1,1-Dichloroethane ug/L20.2 0.50 20.00 78-130101
1,1-Dichloroethylene ug/L20.0 0.50 20.00 70-154100
1,1-Dichloropropylene ug/L20.9 0.50 20.00 71-136104
1,2,3-Trichloropropane ug/L20.9 1.0 20.00 71-127105
1,2,4-Trichlorobenzene ug/L19.8 1.0 20.00 66-13999
1,2-Dibromo-3-chloropropane ug/L18.8 2.0 20.00 63-13494
1,2-Dibromoethane ug/L21.3 0.50 20.00 77-135107
1,2-Dichlorobenzene ug/L20.3 0.50 20.00 78-128101
1,2-Dichloroethane ug/L20.5 0.50 20.00 68-131103
1,2-Dichloropropane ug/L20.4 0.50 20.00 77-130102
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 77-125101
1,3-Dichloropropane ug/L21.6 0.50 20.00 76-132108
1,4-Dichlorobenzene ug/L20.0 0.50 20.00 75-126100
2,2-Dichloropropane ug/L18.4 2.0 20.00 29-14992
Acetone ug/L41.1 5.0 40.00 40-166103
Acetonitrile ug/L19.0 10 20.00 70-13095
Acrolein ug/L37.8 20 40.00 70-13095
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
LCS (P7J0385-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
Acrylonitrile ug/L39.9 20 40.00 81-127100
Allyl Chloride (3-Chloropropylene)ug/L23.1 10 20.00 70-130116
Benzene ug/L20.4 0.50 20.00 77-128102
Bromochloromethane ug/L21.3 0.50 20.00 78-135107
Bromodichloromethane ug/L21.2 0.50 20.00 76-138106
Bromoform ug/L17.4 1.0 20.00 71-13587
Bromomethane ug/L14.0 1.0 20.00 41-16870
Carbon disulfide ug/L21.0 5.0 20.00 59-135105
Carbon Tetrachloride ug/L20.1 0.50 20.00 72-142100
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L18.7 0.50 20.00 57-14294
Chloroform ug/L19.8 0.50 20.00 77-13099
Chloromethane ug/L15.3 0.50 20.00 47-14577
Chloroprene ug/L19.4 10 20.00 70-13097
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 76-141104
cis-1,3-Dichloropropylene ug/L21.2 0.50 20.00 65-140106
Dibromochloromethane ug/L19.3 0.50 20.00 75-13496
Dibromomethane ug/L20.7 0.50 20.00 76-138104
Dichlorodifluoromethane ug/L19.3 1.0 20.00 28-16397
Ethyl Methacrylate ug/L19.3 10 20.00 70-13096
Ethylbenzene ug/L21.1 0.50 20.00 80-127105
Hexachlorobutadiene ug/L19.3 2.0 20.00 61-13496
Isobutyl alcohol ug/L20.9 20 20.00 70-130104
m,p-Xylenes ug/L44.3 1.0 40.00 77-133111
Methacrylonitrile ug/L19.1 10 20.00 70-13095
Methyl Butyl Ketone (2-Hexanone)ug/L21.8 5.0 20.00 64-137109
Methyl Ethyl Ketone (2-Butanone)ug/L19.9 5.0 20.00 71-13499
Methyl Iodide ug/L17.8 5.0 20.00 70-13089
Methyl Isobutyl Ketone ug/L21.3 5.0 20.00 69-134107
Methyl Methacrylate ug/L19.5 10 20.00 70-13097
Methylene Chloride ug/L18.4 1.0 20.00 73-13192
Naphthalene ug/L20.7 1.0 20.00 64-136103
o-Xylene ug/L21.3 0.50 20.00 78-128107
Propionitrile (Ethyl Cyanide)ug/L18.4 10 20.00 70-13092
Styrene ug/L20.0 0.50 20.00 78-129100
Tetrachloroethylene ug/L20.5 0.50 20.00 80-129102
Tetrahydrofuran ug/L19.9 10 20.00 70-13099
Toluene ug/L20.8 0.50 20.00 76-131104
trans-1,2-Dichloroethylene ug/L20.9 0.50 20.00 76-135104
trans-1,3-Dichloropropylene ug/L19.2 0.50 20.00 67-14096
trans-1,4-Dichloro-2-butene ug/L20.2 10 20.00 70-130101
Trichloroethylene ug/L20.8 0.50 20.00 77-133104
Trichlorofluoromethane ug/L20.2 0.50 20.00 62-148101
Vinyl acetate ug/L20.7 2.0 20.00 34-167104
Vinyl chloride ug/L20.4 0.50 20.00 57-141102
Xylenes, total ug/L65.6 1.5 60.00 77-133109
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
LCS (P7J0385-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 8843.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9346.6
ug/L 50.00 77-123Surrogate: Toluene-d8 9145.4
LCS Dup (P7J0385-BSD1)Prepared: 10/21/17 Analyzed: 10/22/17
1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 2079-13498 0.2
1,1,1-Trichloroethane ug/L21.0 0.50 20.00 2075-136105 2
1,1,2,2-Tetrachloroethane ug/L21.5 0.50 20.00 2062-127108 3
1,1,2-Trichloroethane ug/L21.1 0.50 20.00 2070-140106 2
1,1-Dichloroethane ug/L20.1 0.50 20.00 2078-130101 0.7
1,1-Dichloroethylene ug/L20.0 0.50 20.00 2070-154100 0.1
1,1-Dichloropropylene ug/L20.6 0.50 20.00 2071-136103 1
1,2,3-Trichloropropane ug/L21.2 1.0 20.00 2071-127106 1
1,2,4-Trichlorobenzene ug/L20.0 1.0 20.00 2066-139100 0.8
1,2-Dibromo-3-chloropropane ug/L19.3 2.0 20.00 2063-13496 3
1,2-Dibromoethane ug/L21.3 0.50 20.00 2077-135107 0.05
1,2-Dichlorobenzene ug/L20.8 0.50 20.00 2078-128104 3
1,2-Dichloroethane ug/L20.9 0.50 20.00 2068-131104 2
1,2-Dichloropropane ug/L20.4 0.50 20.00 2077-130102 0.1
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 2077-125102 0.3
1,3-Dichloropropane ug/L21.7 0.50 20.00 2076-132108 0.3
1,4-Dichlorobenzene ug/L20.3 0.50 20.00 2075-126101 2
2,2-Dichloropropane ug/L18.5 2.0 20.00 2029-14992 0.2
Acetone ug/L42.4 5.0 40.00 2040-166106 3
Acetonitrile ug/L18.6 10 20.00 2070-13093 2
Acrolein ug/L39.0 20 40.00 2070-13098 3
Acrylonitrile ug/L40.7 20 40.00 2081-127102 2
Allyl Chloride (3-Chloropropylene)ug/L21.1 10 20.00 2070-130105 9
Benzene ug/L20.4 0.50 20.00 2077-128102 0.3
Bromochloromethane ug/L21.3 0.50 20.00 2078-135107 0.09
Bromodichloromethane ug/L21.3 0.50 20.00 2076-138106 0.5
Bromoform ug/L17.6 1.0 20.00 2071-13588 1
Bromomethane ug/L13.9 1.0 20.00 2041-16869 0.6
Carbon disulfide ug/L20.9 5.0 20.00 2059-135105 0.3
Carbon Tetrachloride ug/L19.9 0.50 20.00 2072-142100 0.8
Chlorobenzene ug/L20.3 0.50 20.00 2078-119102 1
Chloroethane ug/L18.2 0.50 20.00 2057-14291 3
Chloroform ug/L19.7 0.50 20.00 2077-13099 0.3
Chloromethane ug/L14.8 0.50 20.00 2047-14574 4
Chloroprene ug/L17.6 10 20.00 2070-13088 10
cis-1,2-Dichloroethylene ug/L20.7 0.50 20.00 2076-141103 0.3
cis-1,3-Dichloropropylene ug/L21.3 0.50 20.00 2065-140107 0.8
Dibromochloromethane ug/L19.2 0.50 20.00 2075-13496 0.7
Dibromomethane ug/L20.8 0.50 20.00 2076-138104 0.1
Dichlorodifluoromethane ug/L19.0 1.0 20.00 2028-16395 2
Ethyl Methacrylate ug/L18.5 10 20.00 2070-13093 4
Ethylbenzene ug/L21.0 0.50 20.00 2080-127105 0.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
LCS Dup (P7J0385-BSD1)Prepared: 10/21/17 Analyzed: 10/22/17
Hexachlorobutadiene ug/L20.7 2.0 20.00 2061-134104 7
Isobutyl alcohol ug/L19.0 20 20.00 20 J70-13095 10
m,p-Xylenes ug/L43.8 1.0 40.00 2077-133109 1
Methacrylonitrile ug/L18.2 10 20.00 2070-13091 4
Methyl Butyl Ketone (2-Hexanone)ug/L21.8 5.0 20.00 2064-137109 0
Methyl Ethyl Ketone (2-Butanone)ug/L21.2 5.0 20.00 2071-134106 7
Methyl Iodide ug/L17.6 5.0 20.00 2070-13088 1
Methyl Isobutyl Ketone ug/L21.8 5.0 20.00 2069-134109 2
Methyl Methacrylate ug/L18.7 10 20.00 2070-13093 4
Methylene Chloride ug/L18.4 1.0 20.00 2073-13192 0.3
Naphthalene ug/L20.6 1.0 20.00 2064-136103 0.1
o-Xylene ug/L21.0 0.50 20.00 2078-128105 1
Propionitrile (Ethyl Cyanide)ug/L17.2 10 20.00 2070-13086 7
Styrene ug/L19.2 0.50 20.00 2078-12996 4
Tetrachloroethylene ug/L20.4 0.50 20.00 2080-129102 0.5
Tetrahydrofuran ug/L20.1 10 20.00 2070-130101 1
Toluene ug/L20.8 0.50 20.00 2076-131104 0.05
trans-1,2-Dichloroethylene ug/L21.0 0.50 20.00 2076-135105 0.5
trans-1,3-Dichloropropylene ug/L19.7 0.50 20.00 2067-14099 3
trans-1,4-Dichloro-2-butene ug/L17.1 10 20.00 2070-13086 17
Trichloroethylene ug/L20.4 0.50 20.00 2077-133102 2
Trichlorofluoromethane ug/L20.4 0.50 20.00 2062-148102 0.7
Vinyl acetate ug/L20.9 2.0 20.00 2034-167104 0.6
Vinyl chloride ug/L19.9 0.50 20.00 2057-14199 3
Xylenes, total ug/L64.8 1.5 60.00 2077-133108 1
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9045.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9447.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9145.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
Blank (P7J0283-BLK1)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4,5-Tetrachlorobenzene ug/LBRL10
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3,5-Trinitrobenzene ug/LBRL20
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1,4-Naphthoquinone ug/LBRL10
1,4-Phenylenediamine ug/LBRL10
1-Naphthylamine ug/LBRL10
2,3,4,6-Tetrachlorophenol ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dichlorophenol ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Acetylaminofluorene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Naphthylamine ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3’-Dichlorobenzidine ug/LBRL10
3,3·-Dimethylbenzidine ug/LBRL20
3/4-Methylphenol ug/LBRL10
3-Methylcholanthrene ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Aminobiphenyl ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
5-Nitro-o-toluidine ug/LBRL10
7,12-Dimethylbenz(a)anthracene ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Acetophenone ug/LBRL10
Anthracene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
Blank (P7J0283-BLK1)Prepared: 10/17/17 Analyzed: 11/06/17
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(b&k)fluoranthene ug/LBRL20
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chlorobenzilate ug/LBRL10
Chrysene ug/LBRL10
Diallate ug/LBRL20
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethoate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
Diphenylamine ug/LBRL10
Disulfoton ug/LBRL20
Ethyl Methanesulfonate ug/LBRL10
Famphur ug/LBRL20
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Hexachloropropene ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isodrin ug/LBRL10
Isophorone ug/LBRL10
Isosafrole ug/LBRL10
Kepone ug/LBRL20
Methapyrilene ug/LBRL100
Methyl Methanesulfonate ug/LBRL20
Methyl parathion ug/LBRL20
Nitrobenzene ug/LBRL10
N-Nitrosodibutylamine ug/LBRL10
N-Nitrosodiethylamine ug/LBRL10
N-Nitrosodimethylamine ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
Blank (P7J0283-BLK1)Prepared: 10/17/17 Analyzed: 11/06/17
N-Nitrosomethylethylamine ug/LBRL10
N-Nitrosopiperidine ug/LBRL10
N-Nitrosopyrrolidine ug/LBRL10
O,O,O-Triethyl phosphorothioate ug/LBRL10
o-Toluidine ug/LBRL10
Parathion ug/LBRL10
p-Dimethylaminoazobenzene ug/LBRL20
Pentachlorobenzene ug/LBRL10
Pentachloronitrobenzene ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenacetin ug/LBRL20
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Phorate ug/LBRL10
Pronamide ug/LBRL10
Pyrene ug/LBRL10
Safrole ug/LBRL10
Thionazin ug/LBRL10
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7336.3
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5050.0
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7135.6
ug/L 100.0 11-52Surrogate: Phenol-d5 3130.8
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8040.2
LCS (P7J0283-BS1)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4-Trichlorobenzene ug/L27.1 10 50.00 29-12654
1,2-Dichlorobenzene ug/L29.2 10 50.00 32-11158
1,3-Dichlorobenzene ug/L28.4 10 50.00 28-11057
1,4-Dichlorobenzene ug/L27.5 10 50.00 29-11255
2,4,5-Trichlorophenol ug/L43.5 10 50.00 53-12387
2,4,6-Trichlorophenol ug/L41.6 10 50.00 50-12583
2,4-Dichlorophenol ug/L37.5 10 50.00 47-12175
2,4-Dimethylphenol ug/L30.3 10 50.00 31-12461
2,4-Dinitrophenol ug/L28.5 10 50.00 23-14357
2,4-Dinitrotoluene ug/L43.2 10 50.00 57-12886
2,6-Dinitrotoluene ug/L44.3 10 50.00 57-12489
2-Chloronaphthalene ug/L35.8 10 50.00 40-11672
2-Chlorophenol ug/L40.3 10 50.00 38-11781
2-Methylnaphthalene ug/L31.1 10 50.00 40-12162
2-Methylphenol ug/L37.4 10 50.00 30-11775
2-Nitroaniline ug/L41.6 10 50.00 55-12783
2-Nitrophenol ug/L36.8 10 50.00 47-12374
3,3’-Dichlorobenzidine ug/L44.6 10 50.00 27-12989
3/4-Methylphenol ug/L30.6 10 50.00 29-11061
3-Nitroaniline ug/L43.3 10 50.00 41-12887
4,6-Dinitro-2-methylphenol ug/L37.0 10 50.00 44-13774
4-Bromophenyl phenyl ether ug/L42.0 10 50.00 55-12484
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS (P7J0283-BS1)Prepared: 10/17/17 Analyzed: 11/06/17
4-Chloro-3-methylphenol ug/L37.8 10 50.00 52-11976
4-Chloroaniline ug/L38.7 10 50.00 33-11777
4-Chlorophenyl phenyl ether ug/L40.3 10 50.00 53-12181
4-Nitroaniline ug/L45.9 10 50.00 45-13592
4-Nitrophenol ug/L17.8 10 50.00 10-7736
Acenaphthene ug/L39.3 10 50.00 47-12279
Acenaphthylene ug/L42.5 10 50.00 41-13085
Acetophenone ug/L42.9 10 50.00 46-11886
Anthracene ug/L47.6 10 50.00 57-12395
Benzo(a)anthracene ug/L45.6 10 50.00 58-12591
Benzo(a)pyrene ug/L43.0 10 50.00 54-12886
Benzo(b)fluoranthene ug/L41.3 10 50.00 53-13183
Benzo(g,h,i)perylene ug/L41.8 10 50.00 50-13484
Benzo(k)fluoranthene ug/L47.1 10 50.00 57-12994
Benzyl alcohol ug/L32.6 10 50.00 31-11265
bis(2-Chloroethoxy)methane ug/L39.1 10 50.00 48-12078
Bis(2-Chloroethyl)ether ug/L38.6 10 50.00 43-11877
Bis(2-chloroisopropyl)ether ug/L37.5 10 50.00 37-13075
Bis(2-Ethylhexyl)phthalate ug/L45.7 10 50.00 55-13591
Butyl benzyl phthalate ug/L44.3 10 50.00 53-13489
Chrysene ug/L45.4 10 50.00 59-12391
Dibenzo(a,h)anthracene ug/L15.3 10 50.00 L51-13431
Dibenzofuran ug/L40.0 10 50.00 53-11880
Diethyl phthalate ug/L43.3 10 50.00 56-12587
Dimethyl phthalate ug/L42.1 10 50.00 45-12784
Di-n-butyl phthalate ug/L45.6 10 50.00 59-12791
Di-n-octyl phthalate ug/L43.4 10 50.00 51-14087
Fluoranthene ug/L46.6 10 50.00 57-12893
Fluorene ug/L43.0 10 50.00 52-12486
Hexachlorobenzene ug/L43.5 10 50.00 53-12587
Hexachlorobutadiene ug/L26.4 10 50.00 22-12453
Hexachlorocyclopentadiene ug/L26.3 10 50.00 32-11753
Hexachloroethane ug/L27.6 10 50.00 21-11555
Indeno(1,2,3-cd)pyrene ug/L44.6 10 50.00 52-13489
Isophorone ug/L37.7 10 50.00 42-12475
Nitrobenzene ug/L34.2 10 50.00 45-12168
N-Nitrosodimethylamine ug/L28.2 10 50.00 10-11956
N-Nitroso-di-n-propylamine ug/L41.9 10 50.00 49-11984
N-Nitrosodiphenylamine ug/L53.1 10 50.00 51-123106
Pentachlorophenol ug/L38.0 10 50.00 35-13876
Phenanthrene ug/L47.0 10 50.00 59-12094
Phenol ug/L18.2 10 50.00 12-5836
Pyrene ug/L46.5 10 50.00 57-12693
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8341.4
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5554.8
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7236.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS (P7J0283-BS1)Prepared: 10/17/17 Analyzed: 11/06/17
ug/L 100.0 11-52Surrogate: Phenol-d5 3635.7
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8844.0
LCS (P7J0283-BS2)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4,5-Tetrachlorobenzene ug/L30.8 10 50.00 35-12162
1,3,5-Trinitrobenzene ug/L39.2 20 50.00 41-13778
1,4-Naphthoquinone ug/L41.6 10 50.00 45-13583
1,4-Phenylenediamine ug/L42.7 10 50.00 45-13585
1-Naphthylamine ug/L37.2 10 50.00 24-12474
2,3,4,6-Tetrachlorophenol ug/L41.5 10 50.00 50-12883
2,6-Dichlorophenol ug/L39.9 10 50.00 50-11880
2-Acetylaminofluorene ug/L43.7 10 50.00 60-13887
2-Naphthylamine ug/L35.2 10 50.00 45-13570
3,3·-Dimethylbenzidine ug/L24.3 20 50.00 45-13549
3-Methylcholanthrene ug/L38.9 10 50.00 56-13378
4-Aminobiphenyl ug/L38.3 10 50.00 45-13577
5-Nitro-o-toluidine ug/L43.6 10 50.00 38-12687
7,12-Dimethylbenz(a)anthracene ug/L42.6 10 50.00 61-13385
Acetophenone ug/L37.5 10 50.00 46-11875
Chlorobenzilate ug/L41.0 10 50.00 58-15082
Diallate ug/L39.6 20 50.00 45-13579
Dimethoate ug/L41.1 10 50.00 45-13582
Diphenylamine ug/L40.0 10 50.00 55-11180
Disulfoton ug/L38.2 20 50.00 55-13076
Ethyl Methanesulfonate ug/L36.7 10 50.00 62-11873
Famphur ug/L30.2 20 50.00 45-13560
Hexachloropropene ug/L21.0 10 50.00 L45-13542
Isodrin ug/L39.0 10 50.00 68-12878
Isosafrole ug/L35.1 10 50.00 56-12670
Kepone ug/L25.0 20 50.00 45-13550
Methapyrilene ug/LBRL100 50.00 L45-135
Methyl Methanesulfonate ug/L24.4 20 50.00 33-10749
Methyl parathion ug/L42.8 20 50.00 45-15986
N-Nitrosodibutylamine ug/L39.2 10 50.00 60-12178
N-Nitrosodiethylamine ug/L38.4 10 50.00 43-12177
N-Nitrosomethylethylamine ug/L38.6 10 50.00 41-11777
N-Nitrosopiperidine ug/L37.7 10 50.00 56-12175
N-Nitrosopyrrolidine ug/L37.6 10 50.00 48-11375
O,O,O-Triethyl phosphorothioate ug/L36.7 10 50.00 60-11973
o-Toluidine ug/L38.9 10 50.00 30-11078
Parathion ug/L41.3 10 50.00 66-14083
p-Dimethylaminoazobenzene ug/L40.2 20 50.00 45-13580
Pentachlorobenzene ug/L35.8 10 50.00 59-12372
Pentachloronitrobenzene ug/L41.6 10 50.00 54-13583
Phenacetin ug/L42.5 20 50.00 71-12485
Phorate ug/L40.0 10 50.00 38-13980
Pronamide ug/L41.0 10 50.00 65-12982
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS (P7J0283-BS2)Prepared: 10/17/17 Analyzed: 11/06/17
Safrole ug/L37.3 10 50.00 61-11975
Thionazin ug/L42.1 10 50.00 72-13284
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7336.6
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5050.1
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6833.8
ug/L 100.0 11-52Surrogate: Phenol-d5 3231.9
ug/L 50.00 50-134Surrogate: Terphenyl-d14 7437.2
LCS Dup (P7J0283-BSD1)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4-Trichlorobenzene ug/L23.7 10 50.00 2029-12647 13
1,2-Dichlorobenzene ug/L25.3 10 50.00 2032-11151 14
1,3-Dichlorobenzene ug/L24.2 10 50.00 2028-11048 16
1,4-Dichlorobenzene ug/L24.5 10 50.00 2029-11249 12
2,4,5-Trichlorophenol ug/L36.7 10 50.00 2053-12373 17
2,4,6-Trichlorophenol ug/L34.2 10 50.00 2050-12568 20
2,4-Dichlorophenol ug/L32.1 10 50.00 2047-12164 15
2,4-Dimethylphenol ug/L31.9 10 50.00 2031-12464 5
2,4-Dinitrophenol ug/L24.6 10 50.00 2023-14349 15
2,4-Dinitrotoluene ug/L36.2 10 50.00 2057-12872 18
2,6-Dinitrotoluene ug/L36.9 10 50.00 2057-12474 18
2-Chloronaphthalene ug/L30.0 10 50.00 2040-11660 18
2-Chlorophenol ug/L36.0 10 50.00 2038-11772 11
2-Methylnaphthalene ug/L26.4 10 50.00 2040-12153 16
2-Methylphenol ug/L34.1 10 50.00 2030-11768 9
2-Nitroaniline ug/L36.0 10 50.00 2055-12772 14
2-Nitrophenol ug/L31.2 10 50.00 2047-12362 16
3,3’-Dichlorobenzidine ug/L37.7 10 50.00 2027-12975 17
3/4-Methylphenol ug/L27.1 10 50.00 2029-11054 12
3-Nitroaniline ug/L39.0 10 50.00 2041-12878 10
4,6-Dinitro-2-methylphenol ug/L30.0 10 50.00 20 D44-13760 21
4-Bromophenyl phenyl ether ug/L34.9 10 50.00 2055-12470 19
4-Chloro-3-methylphenol ug/L32.6 10 50.00 2052-11965 15
4-Chloroaniline ug/L36.3 10 50.00 2033-11773 6
4-Chlorophenyl phenyl ether ug/L34.1 10 50.00 2053-12168 17
4-Nitroaniline ug/L39.9 10 50.00 2045-13580 14
4-Nitrophenol ug/L17.1 10 50.00 2010-7734 4
Acenaphthene ug/L32.6 10 50.00 2047-12265 19
Acenaphthylene ug/L35.0 10 50.00 2041-13070 19
Acetophenone ug/L36.3 10 50.00 2046-11873 17
Anthracene ug/L39.9 10 50.00 2057-12380 18
Benzo(a)anthracene ug/L38.0 10 50.00 2058-12576 18
Benzo(a)pyrene ug/L35.2 10 50.00 2054-12870 20
Benzo(b)fluoranthene ug/L34.5 10 50.00 2053-13169 18
Benzo(g,h,i)perylene ug/L34.4 10 50.00 2050-13469 19
Benzo(k)fluoranthene ug/L38.5 10 50.00 2057-12977 20
Benzyl alcohol ug/L29.5 10 50.00 2031-11259 10
bis(2-Chloroethoxy)methane ug/L33.2 10 50.00 2048-12066 16
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS Dup (P7J0283-BSD1)Prepared: 10/17/17 Analyzed: 11/06/17
Bis(2-Chloroethyl)ether ug/L33.7 10 50.00 2043-11867 13
Bis(2-chloroisopropyl)ether ug/L31.8 10 50.00 2037-13064 17
Bis(2-Ethylhexyl)phthalate ug/L37.9 10 50.00 2055-13576 19
Butyl benzyl phthalate ug/L37.1 10 50.00 2053-13474 18
Chrysene ug/L37.8 10 50.00 2059-12376 18
Dibenzo(a,h)anthracene ug/L15.8 10 50.00 20 L51-13432 3
Dibenzofuran ug/L33.3 10 50.00 2053-11867 18
Diethyl phthalate ug/L36.4 10 50.00 2056-12573 17
Dimethyl phthalate ug/L35.6 10 50.00 2045-12771 17
Di-n-butyl phthalate ug/L37.9 10 50.00 2059-12776 19
Di-n-octyl phthalate ug/L35.9 10 50.00 2051-14072 19
Fluoranthene ug/L38.6 10 50.00 2057-12877 19
Fluorene ug/L36.2 10 50.00 2052-12472 17
Hexachlorobenzene ug/L36.1 10 50.00 2053-12572 19
Hexachlorobutadiene ug/L23.2 10 50.00 2022-12446 13
Hexachlorocyclopentadiene ug/L22.3 10 50.00 2032-11745 17
Hexachloroethane ug/L23.5 10 50.00 2021-11547 16
Indeno(1,2,3-cd)pyrene ug/L36.8 10 50.00 2052-13474 19
Isophorone ug/L31.9 10 50.00 2042-12464 17
Nitrobenzene ug/L29.7 10 50.00 2045-12159 14
N-Nitrosodimethylamine ug/L26.3 10 50.00 2010-11953 7
N-Nitroso-di-n-propylamine ug/L34.6 10 50.00 2049-11969 19
N-Nitrosodiphenylamine ug/L44.8 10 50.00 2051-12390 17
Pentachlorophenol ug/L31.6 10 50.00 2035-13863 19
Phenanthrene ug/L39.6 10 50.00 2059-12079 17
Phenol ug/L16.5 10 50.00 2012-5833 10
Pyrene ug/L38.7 10 50.00 2057-12677 18
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 6934.3
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5151.3
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6331.3
ug/L 100.0 11-52Surrogate: Phenol-d5 3231.8
ug/L 50.00 50-134Surrogate: Terphenyl-d14 7537.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS Dup (P7J0283-BSD2)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4,5-Tetrachlorobenzene ug/L27.4 10 50.00 2035-12155 12
1,3,5-Trinitrobenzene ug/L45.7 20 50.00 2041-13791 15
1,4-Naphthoquinone ug/L51.9 10 50.00 20 D45-135104 22
1,4-Phenylenediamine ug/L45.5 10 50.00 2045-13591 6
1-Naphthylamine ug/L32.9 10 50.00 2024-12466 12
2,3,4,6-Tetrachlorophenol ug/L47.1 10 50.00 2050-12894 13
2,6-Dichlorophenol ug/L43.4 10 50.00 2050-11887 9
2-Acetylaminofluorene ug/L47.5 10 50.00 2060-13895 8
2-Naphthylamine ug/L37.5 10 50.00 2045-13575 6
3,3·-Dimethylbenzidine ug/L20.3 20 50.00 20 L245-13541 18
3-Methylcholanthrene ug/L41.9 10 50.00 2056-13384 7
4-Aminobiphenyl ug/L40.8 10 50.00 2045-13582 6
5-Nitro-o-toluidine ug/L47.5 10 50.00 2038-12695 9
7,12-Dimethylbenz(a)anthracene ug/L46.7 10 50.00 2061-13393 9
Acetophenone ug/L40.6 10 50.00 2046-11881 8
Chlorobenzilate ug/L45.2 10 50.00 2058-15090 10
Diallate ug/L44.3 20 50.00 2045-13589 11
Dimethoate ug/L45.7 10 50.00 2045-13591 11
Diphenylamine ug/L43.6 10 50.00 2055-11187 9
Disulfoton ug/L41.7 20 50.00 2055-13083 9
Ethyl Methanesulfonate ug/L41.3 10 50.00 2062-11883 12
Famphur ug/L34.4 20 50.00 20 L245-13569 13
Hexachloropropene ug/L18.1 10 50.00 20 L45-13536 15
Isodrin ug/L41.1 10 50.00 2068-12882 5
Isosafrole ug/L36.7 10 50.00 2056-12673 4
Kepone ug/L26.7 20 50.00 2045-13553 7
Methapyrilene ug/LBRL100 50.00 20 L45-135
Methyl Methanesulfonate ug/L26.6 20 50.00 2033-10753 9
Methyl parathion ug/L47.4 20 50.00 2045-15995 10
N-Nitrosodibutylamine ug/L42.2 10 50.00 2060-12184 7
N-Nitrosodiethylamine ug/L42.3 10 50.00 2043-12185 10
N-Nitrosomethylethylamine ug/L42.0 10 50.00 2041-11784 8
N-Nitrosopiperidine ug/L40.5 10 50.00 2056-12181 7
N-Nitrosopyrrolidine ug/L40.7 10 50.00 2048-11381 8
O,O,O-Triethyl phosphorothioate ug/L39.4 10 50.00 2060-11979 7
o-Toluidine ug/L38.1 10 50.00 2030-11076 2
Parathion ug/L46.6 10 50.00 2066-14093 12
p-Dimethylaminoazobenzene ug/L44.9 20 50.00 2045-13590 11
Pentachlorobenzene ug/L31.8 10 50.00 2059-12364 12
Pentachloronitrobenzene ug/L44.5 10 50.00 2054-13589 7
Phenacetin ug/L45.8 20 50.00 2071-12492 7
Phorate ug/L43.4 10 50.00 2038-13987 8
Pronamide ug/L44.7 10 50.00 2065-12989 9
Safrole ug/L39.1 10 50.00 2061-11978 5
Thionazin ug/L46.3 10 50.00 2072-13293 9
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7537.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS Dup (P7J0283-BSD2)Prepared: 10/17/17 Analyzed: 11/06/17
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5555.3
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7336.7
ug/L 100.0 11-52Surrogate: Phenol-d5 3635.5
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8542.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7J0200 - 3005A
Blank (P7J0200-BLK1)Prepared: 10/12/17 Analyzed: 10/16/17
Arsenic ug/L0.227 1.0 J
Beryllium ug/L0.381 1.0 J
Cadmium ug/LBRL1.0
Chromium ug/L0.282 1.0 J
Cobalt ug/L0.118 1.0 J
Copper ug/L1.85 5.0 J
Lead ug/L0.482 1.0 J
Nickel ug/LBRL2.0
Selenium ug/LBRL5.0
Silver ug/LBRL5.0
Thallium ug/L0.333 1.0 J
Tin ug/LBRL10
Vanadium ug/L0.115 1.0 J
LCS (P7J0200-BS1)Prepared: 10/12/17 Analyzed: 10/16/17
Arsenic ug/L1081.0 100.0 80-120108
Beryllium ug/L1071.0 100.0 80-120107
Cadmium ug/L1121.0 100.0 80-120112
Chromium ug/L1131.0 100.0 80-120113
Cobalt ug/L1171.0 100.0 80-120117
Copper ug/L1145.0 100.0 80-120114
Lead ug/L1121.0 100.0 80-120112
Nickel ug/L1182.0 100.0 80-120118
Selenium ug/L1095.0 100.0 80-120109
Silver ug/L1075.0 100.0 80-120107
Thallium ug/L1131.0 100.0 80-120113
Tin ug/L114 10 100.0 80-120114
Vanadium ug/L1091.0 100.0 80-120109
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7J0340 - 3005A
Blank (P7J0340-BLK1)Prepared & Analyzed: 10/19/17
Antimony ug/LBRL1.0
Barium ug/LBRL5.0
Zinc ug/LBRL10
LCS (P7J0340-BS1)Prepared & Analyzed: 10/19/17
Antimony ug/L99.8 1.0 100.0 80-120100
Barium ug/L1045.0 100.0 80-120104
Zinc ug/L10110 100.0 80-120101
Matrix Spike (P7J0340-MS1)Prepared & Analyzed: 10/19/17 Source: 7100185-01
Antimony ug/L1001.0 100.0 BRL 75-125100
Arsenic ug/L97.7 1.0 100.0 53.5 75-12544
Barium ug/L2555.0 100.0 155 75-12599
Cadmium ug/L1021.0 100.0 8.37 75-12594
Chromium ug/L1021.0 100.0 1430 75-125NR
Lead ug/L1021.0 100.0 5310 75-125NR
Selenium ug/L99.1 5.0 100.0 48.9 75-12550
Silver ug/L1015.0 100.0 1.18 75-125100
Zinc ug/L12510 100.0 22.6 75-125102
Matrix Spike Dup (P7J0340-MSD1)Prepared & Analyzed: 10/19/17 Source: 7100185-01
Antimony ug/L1031.0 100.0 BRL 2075-125103 3
Barium ug/L2635.0 100.0 155 2075-125108 3
Zinc ug/L12710 100.0 22.6 2075-125104 2
Post Spike (P7J0340-PS1)Prepared & Analyzed: 10/19/17 Source: 7100185-01
Antimony ug/L103 100.0 0.115 80-120103
Barium ug/L259 100.0 155 80-120104
Zinc ug/L128 100.0 22.6 80-120105
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7J0406 - 7470A
Blank (P7J0406-BLK1)Prepared & Analyzed: 10/23/17
Mercury ug/LBRL0.20
LCS (P7J0406-BS1)Prepared & Analyzed: 10/23/17
Mercury ug/L9.13 0.20 9.375 80-12097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7J0210 - NO PREP
Blank (P7J0210-BLK1)Prepared: 10/12/17 Analyzed: 10/26/17
Chloride ug/LBRL1000
Nitrate as N ug/LBRL100
Sulfate ug/LBRL1000
LCS (P7J0210-BS1)Prepared & Analyzed: 10/11/17
Chloride ug/L393001000 40000 80-12098
Nitrate as N ug/L3860100 4000 80-12097
Sulfate ug/L400001000 40000 80-120100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7J0187 - SM4500-S C
Blank (P7J0187-BLK1)Prepared & Analyzed: 10/11/17
Sulfide ug/L9702000 J
LCS (P7J0187-BS1)Prepared & Analyzed: 10/11/17
Sulfide ug/L9910 2000 10000 70-13099
Batch P7J0195 - NO PREP
Blank (P7J0195-BLK1)Prepared & Analyzed: 10/11/17
Ferrous Iron ug/LBRL200
LCS (P7J0195-BS1)Prepared & Analyzed: 10/11/17
Ferrous Iron ug/L2020200 90-110
Matrix Spike (P7J0195-MS1)Prepared & Analyzed: 10/11/17 Source: 7100185-03
Ferrous Iron ug/L2100200 51.0 80-120
Matrix Spike Dup (P7J0195-MSD1)Prepared & Analyzed: 10/11/17 Source: 7100185-03
Ferrous Iron ug/L2120200 51.0 2080-120 0.9
Batch P7J0197 - NO PREP
Blank (P7J0197-BLK1)Prepared & Analyzed: 10/11/17
Biochemical Oxygen Demand ug/L1002000 J
LCS (P7J0197-BS1)Prepared & Analyzed: 10/11/17
Biochemical Oxygen Demand ug/L2090002000 198000 84.6-115.4105
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 77
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100185
Time Submitted: 10/11/2017 9:15:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7J0208 - NO PREP
Blank (P7J0208-BLK1)Prepared & Analyzed: 10/12/17
Chemical Oxygen Demand ug/LBRL50000
LCS (P7J0208-BS1)Prepared & Analyzed: 10/12/17
Chemical Oxygen Demand ug/L48600051000 505100 90-11096
Batch P7J0213 - NO PREP
Blank (P7J0213-BLK1)Prepared: 10/12/17 Analyzed: 10/13/17
Total Alkalinity to pH 4.5 ug/LBRL5000
LCS (P7J0213-BS1)Prepared: 10/12/17 Analyzed: 10/13/17
Total Alkalinity to pH 4.5 ug/L2580005000 250000 90-110103
Batch P7J0221 - SM4500-CN C
Blank (P7J0221-BLK1)Prepared & Analyzed: 10/13/17
Cyanide ug/LBRL5.0
LCS (P7J0221-BS1)Prepared & Analyzed: 10/13/17
Cyanide ug/L1005.0 100.0 85-115100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 77
Sample Extraction Data
Prep Method: SM4500-CN C
Lab Number Batch Date/TimeInitialFinal
P7J02217100185-01 10/13/17 8:3050 50mL mL
P7J02217100185-02 10/13/17 8:3050 50mL mL
P7J02217100185-03 10/13/17 8:3050 50mL mL
Prep Method: SM4500-S C
Lab Number Batch Date/TimeInitialFinal
P7J01877100185-01 10/11/17 12:40200 200mL mL
P7J01877100185-02 10/11/17 12:40200 200mL mL
P7J01877100185-03 10/11/17 12:40200 200mL mL
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P7J02837100185-01 10/17/17 9:528901mL mL
P7J02837100185-01 10/17/17 9:528901mL mL
P7J02837100185-02 10/17/17 9:529701mL mL
P7J02837100185-02 10/17/17 9:529701mL mL
P7J02837100185-03 10/17/17 9:521000 1mL mL
P7J02837100185-03 10/17/17 9:521000 1mL mL
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7J03407100185-01 10/19/17 7:5550 50mL mL
P7J02007100185-01 10/12/17 7:5550 50mL mL
P7J02007100185-02 10/12/17 7:5550 50mL mL
P7J03407100185-02 10/19/17 7:5550 50mL mL
P7J02007100185-03 10/12/17 7:5550 50mL mL
P7J03407100185-03 10/19/17 7:5550 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7J04067100185-01 10/23/17 9:5020 30mL mL
P7J04067100185-02 10/23/17 9:5020 30mL mL
P7J04067100185-03 10/23/17 9:5020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7J03857100185-01 10/21/17 10:2410 10mL mL
P7J03857100185-02 10/21/17 10:2410 10mL mL
P7J03857100185-03 10/21/17 10:2410 10mL mL
P7J03857100185-04 10/21/17 10:2410 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 77
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Analysis
7100185-01 TOC (Sub)
7100185-02 TOC (Sub)
7100185-03 TOC (Sub)
Lab Number
The following analyses were subcontracted to Microseeps/Pace
Analysis
7100185-01 Dissolved Hydrogen (Sub)
7100185-01 Methane, Ethane, Ethene (AM20GAX)
7100185-01 Volatile Fatty Acids (Sub)
7100185-02 Dissolved Hydrogen (Sub)
7100185-02 Methane, Ethane, Ethene (AM20GAX)
7100185-02 Volatile Fatty Acids (Sub)
7100185-03 Dissolved Hydrogen (Sub)
7100185-03 Methane, Ethane, Ethene (AM20GAX)
7100185-03 Volatile Fatty Acids (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 77
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
11/09/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill (Permit 50-02)
Project No.: 50-02
Lab Submittal Date: 10/12/2017
Prism Work Order: 7100243
TOC analysis was subcontracted to GCAL. Methane, Ethane, Ethene, Carbon Dioxide, Dissolved Oxygen
and Volatile Fatty Acids analyses subcontracted to Pace. Laboratory reports are attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A Initial calibration verification criteria not met for analyte. Analyte is not detected in sample.
BM No dilution met the "Use 2, Leave 1" criteria. Result is an estimated value.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 98
Sample Receipt Summary
11/09/2017
Prism Work Order: 7100243
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7100243-01 10/11/17MW-01 10/12/17Water
7100243-02 10/11/17MW-02 10/12/17Water
7100243-03 10/11/17MW-05R 10/12/17Water
7100243-04 10/11/17MW-06 10/12/17Water
7100243-05 10/10/17SW-01 10/12/17Water
7100243-06 10/11/17SW-02 10/12/17Water
7100243-07 10/11/17Trip Blank 10/12/17Water
Samples were received in good condition at 4.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 98
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7100243
11/09/2017
Summary of Detections
810 J ug/L7100243-01 MW-01 Chloride 9056A
110 ug/L7100243-01 MW-01 Nitrate as N 9056A
1800 J ug/L7100243-01 MW-01 Biochemical Oxygen Demand SM5210 B
1.1 J ug/L7100243-01 MW-01 Cyanide SM4500-CN E
13000 ug/L7100243-01 MW-01 Ferrous Iron SM3500-Fe D
77000 ug/L7100243-01 MW-01 Total Alkalinity to pH 4.5 SM2320 B
7.5 J ug/L7100243-01 MW-01 1,4-Dichlorobenzene 8270D
4.3 ug/L7100243-01 MW-01 Antimony 6020B
1.3 ug/L7100243-01 MW-01 Arsenic 6020B
100 ug/L7100243-01 MW-01 Barium 6020B
0.088 J ug/L7100243-01 MW-01 Beryllium 6020B
38 ug/L7100243-01 MW-01 Cadmium 6020B
0.53 J ug/L7100243-01 MW-01 Chromium 6020B
92 ug/L7100243-01 MW-01 Cobalt 6020B
58 ug/L7100243-01 MW-01 Copper 6020B
3.0 ug/L7100243-01 MW-01 Lead 6020B
9.9 J ug/L7100243-01 MW-01 Nickel 6020B
0.32 J ug/L7100243-01 MW-01 Silver 6020B
6.1 ug/L7100243-01 MW-01 Thallium 6020B
0.72 J ug/L7100243-01 MW-01 Vanadium 6020B
1200 ug/L7100243-01 MW-01 Zinc 6020B
820 J ug/L7100243-02 MW-02 Chloride 9056A
150 ug/L7100243-02 MW-02 Nitrate as N 9056A
670 J ug/L7100243-02 MW-02 Sulfate 9056A
1400 J ug/L7100243-02 MW-02 Biochemical Oxygen Demand SM5210 B
1.2 J ug/L7100243-02 MW-02 Cyanide SM4500-CN E
37 J ug/L7100243-02 MW-02 Ferrous Iron SM3500-Fe D
46000 ug/L7100243-02 MW-02 Total Alkalinity to pH 4.5 SM2320 B
0.13 J ug/L7100243-02 MW-02 Arsenic 6020B
46 ug/L7100243-02 MW-02 Barium 6020B
0.070 J ug/L7100243-02 MW-02 Beryllium 6020B
0.95 J ug/L7100243-02 MW-02 Chromium 6020B
1.5 ug/L7100243-02 MW-02 Cobalt 6020B
1.3 J ug/L7100243-02 MW-02 Copper 6020B
0.34 J ug/L7100243-02 MW-02 Lead 6020B
1.1 ug/L7100243-02 MW-02 Vanadium 6020B
8.9 J ug/L7100243-02 MW-02 Zinc 6020B
74000 ug/L7100243-03 MW-05R Chloride 9056A
81 J ug/L7100243-03 MW-05R Nitrate as N 9056A
2100 ug/L7100243-03 MW-05R Sulfate 9056A
1700 BM, J ug/L7100243-03 MW-05R Biochemical Oxygen Demand SM5210 B
41000 J ug/L7100243-03 MW-05R Chemical Oxygen Demand SM5220 D
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 98
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7100243
11/09/2017
Summary of Detections
1400 ug/L7100243-03 MW-05R Ferrous Iron SM3500-Fe D
240000 ug/L7100243-03 MW-05R Total Alkalinity to pH 4.5 SM2320 B
6.9 J ug/L7100243-03 MW-05R 1,4-Dichlorobenzene 8270D
4.1 ug/L7100243-03 MW-05R Antimony 6020B
0.52 J ug/L7100243-03 MW-05R Arsenic 6020B
260 ug/L7100243-03 MW-05R Barium 6020B
0.44 J ug/L7100243-03 MW-05R Beryllium 6020B
0.41 J ug/L7100243-03 MW-05R Cadmium 6020B
8.7 ug/L7100243-03 MW-05R Chromium 6020B
27 ug/L7100243-03 MW-05R Cobalt 6020B
16 ug/L7100243-03 MW-05R Copper 6020B
3.7 ug/L7100243-03 MW-05R Lead 6020B
12 ug/L7100243-03 MW-05R Nickel 6020B
1.0 J ug/L7100243-03 MW-05R Selenium 6020B
0.27 J ug/L7100243-03 MW-05R Thallium 6020B
12 ug/L7100243-03 MW-05R Vanadium 6020B
51 ug/L7100243-03 MW-05R Zinc 6020B
24000 ug/L7100243-04 MW-06 Chloride 9056A
290 ug/L7100243-04 MW-06 Nitrate as N 9056A
12000 ug/L7100243-04 MW-06 Sulfate 9056A
25000 J ug/L7100243-04 MW-06 Chemical Oxygen Demand SM5220 D
2.7 J ug/L7100243-04 MW-06 Cyanide SM4500-CN E
2500 ug/L7100243-04 MW-06 Ferrous Iron SM3500-Fe D
49000 ug/L7100243-04 MW-06 Total Alkalinity to pH 4.5 SM2320 B
0.19 J ug/L7100243-04 MW-06 Arsenic 6020B
87 ug/L7100243-04 MW-06 Barium 6020B
0.41 J ug/L7100243-04 MW-06 Cadmium 6020B
0.66 J ug/L7100243-04 MW-06 Chromium 6020B
89 ug/L7100243-04 MW-06 Cobalt 6020B
1.9 J ug/L7100243-04 MW-06 Copper 6020B
0.20 J ug/L7100243-04 MW-06 Lead 6020B
74 ug/L7100243-04 MW-06 Nickel 6020B
1.6 ug/L7100243-04 MW-06 Thallium 6020B
0.60 J ug/L7100243-04 MW-06 Vanadium 6020B
52 ug/L7100243-04 MW-06 Zinc 6020B
0.15 J ug/L7100243-05 SW-01 Arsenic 6020B
21 ug/L7100243-05 SW-01 Barium 6020B
1.3 ug/L7100243-05 SW-01 Chromium 6020B
0.51 J ug/L7100243-05 SW-01 Cobalt 6020B
1.6 J ug/L7100243-05 SW-01 Copper 6020B
0.55 J ug/L7100243-05 SW-01 Lead 6020B
1.1 J ug/L7100243-05 SW-01 Nickel 6020B
0.43 J ug/L7100243-05 SW-01 Tin 6020B
1.4 ug/L7100243-05 SW-01 Vanadium 6020B
20 ug/L7100243-05 SW-01 Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 98
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7100243
11/09/2017
Summary of Detections
0.14 J ug/L7100243-06 SW-02 Arsenic 6020B
14 ug/L7100243-06 SW-02 Barium 6020B
0.89 J ug/L7100243-06 SW-02 Chromium 6020B
0.39 J ug/L7100243-06 SW-02 Cobalt 6020B
1.1 J ug/L7100243-06 SW-02 Copper 6020B
0.44 J ug/L7100243-06 SW-02 Lead 6020B
0.76 J ug/L7100243-06 SW-02 Vanadium 6020B
17 ug/L7100243-06 SW-02 Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-01
Prism Work Order: 7100243
Time Collected: 10/11/17 12:10
Time Submitted: 10/12/17 14:00
MW-01
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02391100010/12/17 18:50BMSJug/L 40ChlorideNE810
9056A P7J0239110010/12/17 18:50BMSug/L 7.7Nitrate as N 10000110
9056A P7J02391100010/12/17 18:50BMSug/L 200Sulfate250000<200
General Chemistry Parameters
SM5210 B P7J02201200010/12/17 16:54SLSJug/LBiochemical Oxygen Demand NE1800
SM5220 D P7J030015000010/18/17 10:00BMSug/L 17000Chemical Oxygen Demand NE<17000
SM4500-CN E P7J033315.0 10/19/17 13:00EGCJug/L 1.0Cyanide101.1
SM3500-Fe D P7J023810200010/12/17 16:30EGCug/L 140Ferrous Iron NE13000
SM4500-S F P7J03171200010/18/17 11:55EGCug/L 830Sulfide1000<830
SM2320 B P7J03691500010/20/17 9:15 CLBug/L 770Total Alkalinity to pH 4.5 NE77000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311211/6/17 14:08 JMVug/L 2.91,2,4,5-Tetrachlorobenzene 10<2.9
8270D P7J028311211/6/17 14:08 JMVug/L 2.11,2,4-Trichlorobenzene 10<2.1
8270D P7J028311211/6/17 14:08 JMVug/L 2.01,2-Dichlorobenzene 5<2.0
8270D P7J028312411/6/17 14:08 JMVug/L 3.31,3,5-Trinitrobenzene 10<3.3
8270D P7J028311211/6/17 14:08 JMVug/L 2.21,3-Dichlorobenzene 5<2.2
8270D P7J028311211/6/17 14:08 JMVJug/L 1.91,4-Dichlorobenzene 17.5
8270D P7J028311211/6/17 14:08 JMVug/L 3.21,4-Naphthoquinone 10<3.2
8270D P7J028311211/6/17 14:08 JMVug/L 3.41,4-Phenylenediamine 10<3.4
8270D P7J028311211/6/17 14:08 JMVAug/L 2.01-Naphthylamine 10<2.0
8270D P7J028311211/6/17 14:08 JMVug/L 3.32,3,4,6-Tetrachlorophenol 10<3.3
8270D P7J028311211/6/17 14:08 JMVug/L 1.92,4,5-Trichlorophenol 10<1.9
8270D P7J028311211/6/17 14:08 JMVug/L 2.22,4,6-Trichlorophenol 10<2.2
8270D P7J028311211/6/17 14:08 JMVug/L 3.02,4-Dichlorophenol 10<3.0
8270D P7J028311211/6/17 14:08 JMVug/L 4.12,4-Dimethylphenol 10<4.1
8270D P7J028311211/6/17 14:08 JMVug/L 3.22,4-Dinitrophenol 50<3.2
8270D P7J028311211/6/17 14:08 JMVug/L 1.72,4-Dinitrotoluene 10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 2.42,6-Dichlorophenol 10<2.4
8270D P7J028311211/6/17 14:08 JMVug/L 1.32,6-Dinitrotoluene 10<1.3
8270D P7J028311211/6/17 14:08 JMVug/L 3.22-Acetylaminofluorene 20<3.2
8270D P7J028311211/6/17 14:08 JMVug/L 3.22-Chloronaphthalene 10<3.2
8270D P7J028311211/6/17 14:08 JMVug/L 2.22-Chlorophenol 10<2.2
8270D P7J028311211/6/17 14:08 JMVug/L 2.92-Methylnaphthalene 10<2.9
8270D P7J028311211/6/17 14:08 JMVug/L 2.22-Methylphenol 10<2.2
8270D P7J028311211/6/17 14:08 JMVAug/L 2.52-Naphthylamine 10<2.5
8270D P7J028311211/6/17 14:08 JMVug/L 1.72-Nitroaniline 50<1.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-01
Prism Work Order: 7100243
Time Collected: 10/11/17 12:10
Time Submitted: 10/12/17 14:00
MW-01
50-02
SWSL
8270D P7J028311211/6/17 14:08 JMVug/L 2.82-Nitrophenol 10<2.8
8270D P7J028311211/6/17 14:08 JMVug/L 1.73,3’-Dichlorobenzidine 20<1.7
8270D P7J028312411/6/17 14:08 JMVAug/L 3.73,3·-Dimethylbenzidine 10<3.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.83/4-Methylphenol 10<1.8
8270D P7J028311211/6/17 14:08 JMVug/L 2.93-Methylcholanthrene 10<2.9
8270D P7J028311211/6/17 14:08 JMVug/L 1.73-Nitroaniline 50<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.64,6-Dinitro-2-methylphenol 50<1.6
8270D P7J028311211/6/17 14:08 JMVAug/L 2.94-Aminobiphenyl 20<2.9
8270D P7J028311211/6/17 14:08 JMVug/L 1.54-Bromophenyl phenyl ether 10<1.5
8270D P7J028311211/6/17 14:08 JMVug/L 2.84-Chloro-3-methylphenol 20<2.8
8270D P7J028311211/6/17 14:08 JMVug/L 2.94-Chloroaniline 20<2.9
8270D P7J028311211/6/17 14:08 JMVug/L 1.64-Chlorophenyl phenyl ether 10<1.6
8270D P7J028311211/6/17 14:08 JMVug/L 1.14-Nitroaniline 20<1.1
8270D P7J028311211/6/17 14:08 JMVug/L 0.714-Nitrophenol 50<0.71
8270D P7J028311211/6/17 14:08 JMVug/L 3.25-Nitro-o-toluidine 10<3.2
8270D P7J028311211/6/17 14:08 JMVug/L 3.17,12-Dimethylbenz(a)anthracene 10<3.1
8270D P7J028311211/6/17 14:08 JMVug/L 2.2Acenaphthene10<2.2
8270D P7J028311211/6/17 14:08 JMVug/L 2.4Acenaphthylene10<2.4
8270D P7J028311211/6/17 14:08 JMVug/L 2.8Acetophenone10<2.8
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Anthracene10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Benzo(a)anthracene 10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Benzo(a)pyrene 10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.4Benzo(b)fluoranthene 10<1.4
8270D P7J028312411/6/17 14:08 JMVug/L 1.7Benzo(b&k)fluoranthene NE<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.6Benzo(g,h,i)perylene 10<1.6
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Benzo(k)fluoranthene 10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 2.5Benzyl alcohol 20<2.5
8270D P7J028311211/6/17 14:08 JMVug/L 3.1bis(2-Chloroethoxy)methane 10<3.1
8270D P7J028311211/6/17 14:08 JMVug/L 2.8Bis(2-Chloroethyl)ether 10<2.8
8270D P7J028311211/6/17 14:08 JMVug/L 2.3Bis(2-chloroisopropyl)ether NE<2.3
8270D P7J028311211/6/17 14:08 JMVug/L 1.6Bis(2-Ethylhexyl)phthalate 15<1.6
8270D P7J028311211/6/17 14:08 JMVug/L 1.6Butyl benzyl phthalate 10<1.6
8270D P7J028311211/6/17 14:08 JMVug/L 3.0Chlorobenzilate10<3.0
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Chrysene10<1.7
8270D P7J028312411/6/17 14:08 JMVug/L 3.4Diallate10<3.4
8270D P7J028311211/6/17 14:08 JMVug/L 1.4Dibenzo(a,h)anthracene 10<1.4
8270D P7J028311211/6/17 14:08 JMVug/L 2.1Dibenzofuran10<2.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-01
Prism Work Order: 7100243
Time Collected: 10/11/17 12:10
Time Submitted: 10/12/17 14:00
MW-01
50-02
SWSL
8270D P7J028311211/6/17 14:08 JMVug/L 4.0Diethyl phthalate 6000<4.0
8270D P7J028311211/6/17 14:08 JMVug/L 3.7Dimethoate20<3.7
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Dimethyl phthalate 10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 2.0Di-n-butyl phthalate 10<2.0
8270D P7J028311211/6/17 14:08 JMVug/L 1.5Di-n-octyl phthalate 10<1.5
8270D P7J028311211/6/17 14:08 JMVug/L 3.3Diphenylamine10<3.3
8270D P7J028312411/6/17 14:08 JMVug/L 3.4Disulfoton10<3.4
8270D P7J028311211/6/17 14:08 JMVug/L 3.3Ethyl Methanesulfonate 20<3.3
8270D P7J028312411/7/17 17:30 JMVug/L 5.1Famphur20<5.1
8270D P7J028311211/6/17 14:08 JMVug/L 2.0Fluoranthene10<2.0
8270D P7J028311211/6/17 14:08 JMVug/L 2.0Fluorene10<2.0
8270D P7J028311211/6/17 14:08 JMVug/L 1.5Hexachlorobenzene10<1.5
8270D P7J028311211/6/17 14:08 JMVug/L 2.5Hexachlorobutadiene10<2.5
8270D P7J028311211/6/17 14:08 JMVug/L 2.1Hexachlorocyclopentadiene10<2.1
8270D P7J028311211/6/17 14:08 JMVug/L 2.1Hexachloroethane10<2.1
8270D P7J028311211/6/17 14:08 JMVug/L 2.4Hexachloropropene10<2.4
8270D P7J028311211/6/17 14:08 JMVug/L 4.6Indeno(1,2,3-cd)pyrene 10<4.6
8270D P7J028311211/6/17 14:08 JMVug/L 3.2Isodrin20<3.2
8270D P7J028311211/6/17 14:08 JMVug/L 3.0Isophorone10<3.0
8270D P7J028311211/6/17 14:08 JMVug/L 4.6Isosafrole10<4.6
8270D P7J028312411/7/17 17:30 JMVug/L 3.4Kepone20<3.4
8270D P7J0283112011/6/17 14:08 JMVAug/L 14Methapyrilene100<14
8270D P7J028312411/6/17 14:08 JMVug/L 2.8Methyl Methanesulfonate 10<2.8
8270D P7J028312411/6/17 14:08 JMVug/L 4.0Methyl parathion 10<4.0
8270D P7J028311211/6/17 14:08 JMVug/L 3.0Nitrobenzene10<3.0
8270D P7J028311211/6/17 14:08 JMVug/L 3.0N-Nitrosodibutylamine 10<3.0
8270D P7J028311211/6/17 14:08 JMVug/L 2.2N-Nitrosodiethylamine 20<2.2
8270D P7J028311211/6/17 14:08 JMVug/L 1.3N-Nitrosodimethylamine 10<1.3
8270D P7J028311211/6/17 14:08 JMVug/L 2.6N-Nitroso-di-n-propylamine 10<2.6
8270D P7J028311211/6/17 14:08 JMVug/L 1.6N-Nitrosodiphenylamine 10<1.6
8270D P7J028311211/6/17 14:08 JMVug/L 1.8N-Nitrosomethylethylamine 10<1.8
8270D P7J028311211/6/17 14:08 JMVug/L 2.9N-Nitrosopiperidine 20<2.9
8270D P7J028311211/6/17 14:08 JMVug/L 2.3N-Nitrosopyrrolidine 10<2.3
8270D P7J028311211/6/17 14:08 JMVug/L 3.3O,O,O-Triethyl phosphorothioate 10<3.3
8270D P7J028311211/6/17 14:08 JMVAug/L 2.1o-Toluidine 10<2.1
8270D P7J028311211/6/17 14:08 JMVug/L 3.6Parathion10<3.6
8270D P7J028312411/6/17 14:08 JMVug/L 2.7p-Dimethylaminoazobenzene 10<2.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-01
Prism Work Order: 7100243
Time Collected: 10/11/17 12:10
Time Submitted: 10/12/17 14:00
MW-01
50-02
SWSL
8270D P7J028311211/6/17 14:08 JMVug/L 3.0Pentachlorobenzene10<3.0
8270D P7J028311211/6/17 14:08 JMVug/L 2.8Pentachloronitrobenzene20<2.8
8270D P7J028311211/6/17 14:08 JMVug/L 1.5Pentachlorophenol25<1.5
8270D P7J028312411/6/17 14:08 JMVug/L 3.5Phenacetin20<3.5
8270D P7J028311211/6/17 14:08 JMVug/L 1.8Phenanthrene10<1.8
8270D P7J028311211/6/17 14:08 JMVug/L 1.2Phenol10<1.2
8270D P7J028311211/6/17 14:08 JMVug/L 3.3Phorate10<3.3
8270D P7J028311211/6/17 14:08 JMVug/L 3.4Pronamide10<3.4
8270D P7J028311211/6/17 14:08 JMVug/L 1.7Pyrene10<1.7
8270D P7J028311211/6/17 14:08 JMVug/L 2.6Safrole10<2.6
8270D P7J028311211/6/17 14:08 JMVug/L 2.3Thionazin20<2.3
Surrogate Recovery Control Limits
44-11967 %2-Fluorobiphenyl
19-11928 %2-Fluorophenol
44-12066 %Nitrobenzene-d5
11-5223 %Phenol-d5
50-13469 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 14:34JABug/L 0.036Mercury0.2<0.036
6020B P7J025611.0 10/18/17 6:42 EGCug/L 0.19Antimony64.3
6020B P7J025611.0 10/18/17 6:42 EGCug/L 0.031Arsenic101.3
6020B P7J025615.0 10/18/17 6:42 EGCug/L 0.97Barium100100
6020B P7J025611.0 10/18/17 6:42 EGCJug/L 0.057Beryllium10.088
6020B P7J025611.0 10/18/17 6:42 EGCug/L 0.078Cadmium138
6020B P7J025611.0 10/18/17 6:42 EGCJug/L 0.19Chromium100.53
6020B P7J025611.0 10/18/17 6:42 EGCug/L 0.0071Cobalt1092
6020B P7J025615.0 10/18/17 6:42 EGCug/L 0.22Copper1058
6020B P7J025611.0 10/18/17 6:42 EGCug/L 0.093Lead103.0
6020B P7J025611010/18/17 6:42 EGCJug/L 0.85Nickel509.9
6020B P7J025615.0 10/18/17 6:42 EGCug/L 0.63Selenium10<0.63
6020B P7J025615.0 10/18/17 6:42 EGCJug/L 0.063Silver100.32
6020B P7J025611.0 10/18/17 6:42 EGCug/L 0.099Thallium5.56.1
6020B P7J025615.0 10/18/17 6:42 EGCug/L 0.21Tin100<0.21
6020B P7J025611.0 10/18/17 6:42 EGCJug/L 0.10Vanadium250.72
6020B P7J025611010/18/17 6:42 EGCug/L 2.8Zinc101200
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-01
Prism Work Order: 7100243
Time Collected: 10/11/17 12:10
Time Submitted: 10/12/17 14:00
MW-01
50-02
SWSL
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 9:50 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 9:50 KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 9:50 KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 9:50 KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 9:50 KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 9:50 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 9:50 KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 9:50 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 9:50 KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.065Dibromomethane10<0.065
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.11Dichlorodifluoromethane5<0.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-01
Prism Work Order: 7100243
Time Collected: 10/11/17 12:10
Time Submitted: 10/12/17 14:00
MW-01
50-02
SWSL
8260B P7J038511010/22/17 9:50 KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 9:50 KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 9:50 KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 9:50 KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 9:50 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 9:50 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 9:50 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 9:50 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 9:50 KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 9:50 KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 9:50 KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 9:50 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 9:50 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 9:50 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 9:50 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 9:50 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12494 %4-Bromofluorobenzene
75-12995 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-02
Prism Work Order: 7100243
Time Collected: 10/11/17 13:30
Time Submitted: 10/12/17 14:00
MW-02
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02391100010/12/17 19:06BMSJug/L 40ChlorideNE820
9056A P7J0239110010/12/17 19:06BMSug/L 7.7Nitrate as N 10000150
9056A P7J02391100010/12/17 19:06BMSJug/L 200Sulfate250000670
General Chemistry Parameters
SM5210 B P7J02201200010/12/17 16:54SLSJug/LBiochemical Oxygen Demand NE1400
SM5220 D P7J030015000010/18/17 10:00BMSug/L 17000Chemical Oxygen Demand NE<17000
SM4500-CN E P7J033315.0 10/19/17 13:00EGCJug/L 1.0Cyanide101.2
SM3500-Fe D P7J0238120010/12/17 16:30EGCJug/L 14Ferrous Iron NE37
SM4500-S F P7J03171200010/18/17 12:20EGCug/L 830Sulfide1000<830
SM2320 B P7J03691500010/20/17 9:15 CLBug/L 770Total Alkalinity to pH 4.5 NE46000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311111/6/17 14:31 JMVug/L 2.61,2,4,5-Tetrachlorobenzene 10<2.6
8270D P7J028311111/6/17 14:31 JMVug/L 1.91,2,4-Trichlorobenzene 10<1.9
8270D P7J028311111/6/17 14:31 JMVug/L 1.81,2-Dichlorobenzene 5<1.8
8270D P7J028312211/6/17 14:31 JMVug/L 3.01,3,5-Trinitrobenzene 10<3.0
8270D P7J028311111/6/17 14:31 JMVug/L 2.01,3-Dichlorobenzene 5<2.0
8270D P7J028311111/6/17 14:31 JMVug/L 1.81,4-Dichlorobenzene 1<1.8
8270D P7J028311111/6/17 14:31 JMVug/L 2.91,4-Naphthoquinone 10<2.9
8270D P7J028311111/6/17 14:31 JMVug/L 3.11,4-Phenylenediamine 10<3.1
8270D P7J028311111/6/17 14:31 JMVAug/L 1.81-Naphthylamine 10<1.8
8270D P7J028311111/6/17 14:31 JMVug/L 3.02,3,4,6-Tetrachlorophenol 10<3.0
8270D P7J028311111/6/17 14:31 JMVug/L 1.72,4,5-Trichlorophenol 10<1.7
8270D P7J028311111/6/17 14:31 JMVug/L 2.02,4,6-Trichlorophenol 10<2.0
8270D P7J028311111/6/17 14:31 JMVug/L 2.82,4-Dichlorophenol 10<2.8
8270D P7J028311111/6/17 14:31 JMVug/L 3.72,4-Dimethylphenol 10<3.7
8270D P7J028311111/6/17 14:31 JMVug/L 2.92,4-Dinitrophenol 50<2.9
8270D P7J028311111/6/17 14:31 JMVug/L 1.62,4-Dinitrotoluene 10<1.6
8270D P7J028311111/6/17 14:31 JMVug/L 2.22,6-Dichlorophenol 10<2.2
8270D P7J028311111/6/17 14:31 JMVug/L 1.22,6-Dinitrotoluene 10<1.2
8270D P7J028311111/6/17 14:31 JMVug/L 2.92-Acetylaminofluorene 20<2.9
8270D P7J028311111/6/17 14:31 JMVug/L 2.92-Chloronaphthalene 10<2.9
8270D P7J028311111/6/17 14:31 JMVug/L 2.02-Chlorophenol 10<2.0
8270D P7J028311111/6/17 14:31 JMVug/L 2.62-Methylnaphthalene 10<2.6
8270D P7J028311111/6/17 14:31 JMVug/L 2.02-Methylphenol 10<2.0
8270D P7J028311111/6/17 14:31 JMVAug/L 2.22-Naphthylamine 10<2.2
8270D P7J028311111/6/17 14:31 JMVug/L 1.52-Nitroaniline 50<1.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-02
Prism Work Order: 7100243
Time Collected: 10/11/17 13:30
Time Submitted: 10/12/17 14:00
MW-02
50-02
SWSL
8270D P7J028311111/6/17 14:31 JMVug/L 2.52-Nitrophenol 10<2.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.53,3’-Dichlorobenzidine 20<1.5
8270D P7J028312211/6/17 14:31 JMVAug/L 3.33,3·-Dimethylbenzidine 10<3.3
8270D P7J028311111/6/17 14:31 JMVug/L 1.73/4-Methylphenol 10<1.7
8270D P7J028311111/6/17 14:31 JMVug/L 2.63-Methylcholanthrene 10<2.6
8270D P7J028311111/6/17 14:31 JMVug/L 1.53-Nitroaniline 50<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.54,6-Dinitro-2-methylphenol 50<1.5
8270D P7J028311111/6/17 14:31 JMVAug/L 2.64-Aminobiphenyl 20<2.6
8270D P7J028311111/6/17 14:31 JMVug/L 1.44-Bromophenyl phenyl ether 10<1.4
8270D P7J028311111/6/17 14:31 JMVug/L 2.54-Chloro-3-methylphenol 20<2.5
8270D P7J028311111/6/17 14:31 JMVug/L 2.64-Chloroaniline 20<2.6
8270D P7J028311111/6/17 14:31 JMVug/L 1.44-Chlorophenyl phenyl ether 10<1.4
8270D P7J028311111/6/17 14:31 JMVug/L 1.04-Nitroaniline 20<1.0
8270D P7J028311111/6/17 14:31 JMVug/L 0.654-Nitrophenol 50<0.65
8270D P7J028311111/6/17 14:31 JMVug/L 2.85-Nitro-o-toluidine 10<2.8
8270D P7J028311111/6/17 14:31 JMVug/L 2.87,12-Dimethylbenz(a)anthracene 10<2.8
8270D P7J028311111/6/17 14:31 JMVug/L 1.9Acenaphthene10<1.9
8270D P7J028311111/6/17 14:31 JMVug/L 2.2Acenaphthylene10<2.2
8270D P7J028311111/6/17 14:31 JMVug/L 2.5Acetophenone10<2.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Anthracene10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Benzo(a)anthracene 10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Benzo(a)pyrene 10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.2Benzo(b)fluoranthene 10<1.2
8270D P7J028312211/6/17 14:31 JMVug/L 1.5Benzo(b&k)fluoranthene NE<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Benzo(g,h,i)perylene 10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Benzo(k)fluoranthene 10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 2.3Benzyl alcohol 20<2.3
8270D P7J028311111/6/17 14:31 JMVug/L 2.8bis(2-Chloroethoxy)methane 10<2.8
8270D P7J028311111/6/17 14:31 JMVug/L 2.5Bis(2-Chloroethyl)ether 10<2.5
8270D P7J028311111/6/17 14:31 JMVug/L 2.1Bis(2-chloroisopropyl)ether NE<2.1
8270D P7J028311111/6/17 14:31 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate 15<1.4
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Butyl benzyl phthalate 10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 2.7Chlorobenzilate10<2.7
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Chrysene10<1.5
8270D P7J028312211/6/17 14:31 JMVug/L 3.0Diallate10<3.0
8270D P7J028311111/6/17 14:31 JMVug/L 1.3Dibenzo(a,h)anthracene 10<1.3
8270D P7J028311111/6/17 14:31 JMVug/L 1.9Dibenzofuran10<1.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-02
Prism Work Order: 7100243
Time Collected: 10/11/17 13:30
Time Submitted: 10/12/17 14:00
MW-02
50-02
SWSL
8270D P7J028311111/6/17 14:31 JMVug/L 3.6Diethyl phthalate 6000<3.6
8270D P7J028311111/6/17 14:31 JMVug/L 3.3Dimethoate20<3.3
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Dimethyl phthalate 10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.8Di-n-butyl phthalate 10<1.8
8270D P7J028311111/6/17 14:31 JMVug/L 1.4Di-n-octyl phthalate 10<1.4
8270D P7J028311111/6/17 14:31 JMVug/L 3.0Diphenylamine10<3.0
8270D P7J028312211/6/17 14:31 JMVug/L 3.0Disulfoton10<3.0
8270D P7J028311111/6/17 14:31 JMVug/L 3.0Ethyl Methanesulfonate 20<3.0
8270D P7J028312211/7/17 17:52 JMVug/L 4.6Famphur20<4.6
8270D P7J028311111/6/17 14:31 JMVug/L 1.8Fluoranthene10<1.8
8270D P7J028311111/6/17 14:31 JMVug/L 1.8Fluorene10<1.8
8270D P7J028311111/6/17 14:31 JMVug/L 1.4Hexachlorobenzene10<1.4
8270D P7J028311111/6/17 14:31 JMVug/L 2.3Hexachlorobutadiene10<2.3
8270D P7J028311111/6/17 14:31 JMVug/L 1.9Hexachlorocyclopentadiene10<1.9
8270D P7J028311111/6/17 14:31 JMVug/L 1.9Hexachloroethane10<1.9
8270D P7J028311111/6/17 14:31 JMVug/L 2.1Hexachloropropene10<2.1
8270D P7J028311111/6/17 14:31 JMVug/L 4.2Indeno(1,2,3-cd)pyrene 10<4.2
8270D P7J028311111/6/17 14:31 JMVug/L 2.9Isodrin20<2.9
8270D P7J028311111/6/17 14:31 JMVug/L 2.7Isophorone10<2.7
8270D P7J028311111/6/17 14:31 JMVug/L 4.1Isosafrole10<4.1
8270D P7J028312211/7/17 17:52 JMVug/L 3.1Kepone20<3.1
8270D P7J0283111011/6/17 14:31 JMVAug/L 13Methapyrilene100<13
8270D P7J028312211/6/17 14:31 JMVug/L 2.5Methyl Methanesulfonate 10<2.5
8270D P7J028312211/6/17 14:31 JMVug/L 3.6Methyl parathion 10<3.6
8270D P7J028311111/6/17 14:31 JMVug/L 2.8Nitrobenzene10<2.8
8270D P7J028311111/6/17 14:31 JMVug/L 2.7N-Nitrosodibutylamine 10<2.7
8270D P7J028311111/6/17 14:31 JMVug/L 1.9N-Nitrosodiethylamine 20<1.9
8270D P7J028311111/6/17 14:31 JMVug/L 1.2N-Nitrosodimethylamine 10<1.2
8270D P7J028311111/6/17 14:31 JMVug/L 2.3N-Nitroso-di-n-propylamine 10<2.3
8270D P7J028311111/6/17 14:31 JMVug/L 1.4N-Nitrosodiphenylamine 10<1.4
8270D P7J028311111/6/17 14:31 JMVug/L 1.7N-Nitrosomethylethylamine 10<1.7
8270D P7J028311111/6/17 14:31 JMVug/L 2.6N-Nitrosopiperidine 20<2.6
8270D P7J028311111/6/17 14:31 JMVug/L 2.1N-Nitrosopyrrolidine 10<2.1
8270D P7J028311111/6/17 14:31 JMVug/L 3.0O,O,O-Triethyl phosphorothioate 10<3.0
8270D P7J028311111/6/17 14:31 JMVAug/L 1.9o-Toluidine 10<1.9
8270D P7J028311111/6/17 14:31 JMVug/L 3.3Parathion10<3.3
8270D P7J028312211/6/17 14:31 JMVug/L 2.4p-Dimethylaminoazobenzene 10<2.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-02
Prism Work Order: 7100243
Time Collected: 10/11/17 13:30
Time Submitted: 10/12/17 14:00
MW-02
50-02
SWSL
8270D P7J028311111/6/17 14:31 JMVug/L 2.7Pentachlorobenzene10<2.7
8270D P7J028311111/6/17 14:31 JMVug/L 2.5Pentachloronitrobenzene20<2.5
8270D P7J028311111/6/17 14:31 JMVug/L 1.3Pentachlorophenol25<1.3
8270D P7J028312211/6/17 14:31 JMVug/L 3.2Phenacetin20<3.2
8270D P7J028311111/6/17 14:31 JMVug/L 1.6Phenanthrene10<1.6
8270D P7J028311111/6/17 14:31 JMVug/L 1.1Phenol10<1.1
8270D P7J028311111/6/17 14:31 JMVug/L 3.0Phorate10<3.0
8270D P7J028311111/6/17 14:31 JMVug/L 3.0Pronamide10<3.0
8270D P7J028311111/6/17 14:31 JMVug/L 1.5Pyrene10<1.5
8270D P7J028311111/6/17 14:31 JMVug/L 2.4Safrole10<2.4
8270D P7J028311111/6/17 14:31 JMVug/L 2.1Thionazin20<2.1
Surrogate Recovery Control Limits
44-11980 %2-Fluorobiphenyl
19-11923 %2-Fluorophenol
44-12072 %Nitrobenzene-d5
11-5217 %Phenol-d5
50-13481 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 14:45JABug/L 0.036Mercury0.2<0.036
6020B P7J025611.0 10/18/17 6:50 EGCug/L 0.19Antimony6<0.19
6020B P7J025611.0 10/18/17 6:50 EGCJug/L 0.031Arsenic100.13
6020B P7J025615.0 10/18/17 6:50 EGCug/L 0.97Barium10046
6020B P7J025611.0 10/18/17 6:50 EGCJug/L 0.057Beryllium10.070
6020B P7J025611.0 10/18/17 6:50 EGCug/L 0.078Cadmium1<0.078
6020B P7J025611.0 10/18/17 6:50 EGCJug/L 0.19Chromium100.95
6020B P7J025611.0 10/18/17 6:50 EGCug/L 0.0071Cobalt101.5
6020B P7J025615.0 10/18/17 6:50 EGCJug/L 0.22Copper101.3
6020B P7J025611.0 10/18/17 6:50 EGCJug/L 0.093Lead100.34
6020B P7J025611010/18/17 6:50 EGCug/L 0.85Nickel50<0.85
6020B P7J025615.0 10/18/17 6:50 EGCug/L 0.63Selenium10<0.63
6020B P7J025615.0 10/18/17 6:50 EGCug/L 0.063Silver10<0.063
6020B P7J025611.0 10/18/17 6:50 EGCug/L 0.099Thallium5.5<0.099
6020B P7J025615.0 10/18/17 6:50 EGCug/L 0.21Tin100<0.21
6020B P7J025611.0 10/18/17 6:50 EGCug/L 0.10Vanadium251.1
6020B P7J025611010/18/17 6:50 EGCJug/L 2.8Zinc108.9
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-02
Prism Work Order: 7100243
Time Collected: 10/11/17 13:30
Time Submitted: 10/12/17 14:00
MW-02
50-02
SWSL
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 10:15KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 10:15KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 10:15KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 10:15KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 10:15KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 10:15KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 10:15KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 10:15KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 10:15KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.065Dibromomethane10<0.065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-02
Prism Work Order: 7100243
Time Collected: 10/11/17 13:30
Time Submitted: 10/12/17 14:00
MW-02
50-02
SWSL
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 10:15KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 10:15KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 10:15KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 10:15KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 10:15KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 10:15KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 10:15KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 10:15KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 10:15KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 10:15KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 10:15KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 10:15KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 10:15KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 10:15KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 10:15KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 10:15KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12995 %Dibromofluoromethane
77-12399 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-03
Prism Work Order: 7100243
Time Collected: 10/11/17 09:00
Time Submitted: 10/12/17 14:00
MW-05R
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02391100010/12/17 19:22BMSug/L 40ChlorideNE74000
9056A P7J0239110010/12/17 19:22BMSJug/L 7.7Nitrate as N 1000081
9056A P7J02391100010/12/17 19:22BMSug/L 200Sulfate2500002100
General Chemistry Parameters
SM5210 B P7J02201200010/12/17 16:54SLSBM,
J
ug/LBiochemical Oxygen Demand NE1700
SM5220 D P7J030015000010/18/17 10:00BMSJug/L 17000Chemical Oxygen Demand NE41000
SM4500-CN E P7J033315.0 10/19/17 13:00EGCug/L 1.0Cyanide10<1.0
SM3500-Fe D P7J0238120010/12/17 16:30EGCug/L 14Ferrous Iron NE1400
SM4500-S F P7J03171200010/18/17 12:20EGCug/L 830Sulfide1000<830
SM2320 B P7J03691500010/20/17 9:15 CLBug/L 770Total Alkalinity to pH 4.5 NE240000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311311/6/17 15:59 JMVug/L 3.21,2,4,5-Tetrachlorobenzene 10<3.2
8270D P7J028311311/6/17 15:59 JMVug/L 2.31,2,4-Trichlorobenzene 10<2.3
8270D P7J028311311/6/17 15:59 JMVug/L 2.21,2-Dichlorobenzene 5<2.2
8270D P7J028312611/6/17 15:59 JMVug/L 3.61,3,5-Trinitrobenzene 10<3.6
8270D P7J028311311/6/17 15:59 JMVug/L 2.51,3-Dichlorobenzene 5<2.5
8270D P7J028311311/6/17 15:59 JMVJug/L 2.11,4-Dichlorobenzene 16.9
8270D P7J028311311/6/17 15:59 JMVug/L 3.61,4-Naphthoquinone 10<3.6
8270D P7J028311311/6/17 15:59 JMVug/L 3.71,4-Phenylenediamine 10<3.7
8270D P7J028311311/6/17 15:59 JMVAug/L 2.21-Naphthylamine 10<2.2
8270D P7J028311311/6/17 15:59 JMVug/L 3.72,3,4,6-Tetrachlorophenol 10<3.7
8270D P7J028311311/6/17 15:59 JMVug/L 2.12,4,5-Trichlorophenol 10<2.1
8270D P7J028311311/6/17 15:59 JMVug/L 2.42,4,6-Trichlorophenol 10<2.4
8270D P7J028311311/6/17 15:59 JMVug/L 3.42,4-Dichlorophenol 10<3.4
8270D P7J028311311/6/17 15:59 JMVug/L 4.52,4-Dimethylphenol 10<4.5
8270D P7J028311311/6/17 15:59 JMVug/L 3.62,4-Dinitrophenol 50<3.6
8270D P7J028311311/6/17 15:59 JMVug/L 1.92,4-Dinitrotoluene 10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 2.72,6-Dichlorophenol 10<2.7
8270D P7J028311311/6/17 15:59 JMVug/L 1.52,6-Dinitrotoluene 10<1.5
8270D P7J028311311/6/17 15:59 JMVug/L 3.52-Acetylaminofluorene 20<3.5
8270D P7J028311311/6/17 15:59 JMVug/L 3.62-Chloronaphthalene 10<3.6
8270D P7J028311311/6/17 15:59 JMVug/L 2.52-Chlorophenol 10<2.5
8270D P7J028311311/6/17 15:59 JMVug/L 3.22-Methylnaphthalene 10<3.2
8270D P7J028311311/6/17 15:59 JMVug/L 2.42-Methylphenol 10<2.4
8270D P7J028311311/6/17 15:59 JMVAug/L 2.72-Naphthylamine 10<2.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-03
Prism Work Order: 7100243
Time Collected: 10/11/17 09:00
Time Submitted: 10/12/17 14:00
MW-05R
50-02
SWSL
8270D P7J028311311/6/17 15:59 JMVug/L 1.92-Nitroaniline 50<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 3.12-Nitrophenol 10<3.1
8270D P7J028311311/6/17 15:59 JMVug/L 1.93,3’-Dichlorobenzidine 20<1.9
8270D P7J028312611/6/17 15:59 JMVAug/L 4.13,3·-Dimethylbenzidine 10<4.1
8270D P7J028311311/6/17 15:59 JMVug/L 2.03/4-Methylphenol 10<2.0
8270D P7J028311311/6/17 15:59 JMVug/L 3.23-Methylcholanthrene 10<3.2
8270D P7J028311311/6/17 15:59 JMVug/L 1.83-Nitroaniline 50<1.8
8270D P7J028311311/6/17 15:59 JMVug/L 1.84,6-Dinitro-2-methylphenol 50<1.8
8270D P7J028311311/6/17 15:59 JMVAug/L 3.24-Aminobiphenyl 20<3.2
8270D P7J028311311/6/17 15:59 JMVug/L 1.74-Bromophenyl phenyl ether 10<1.7
8270D P7J028311311/6/17 15:59 JMVug/L 3.14-Chloro-3-methylphenol 20<3.1
8270D P7J028311311/6/17 15:59 JMVug/L 3.24-Chloroaniline 20<3.2
8270D P7J028311311/6/17 15:59 JMVug/L 1.74-Chlorophenyl phenyl ether 10<1.7
8270D P7J028311311/6/17 15:59 JMVug/L 1.24-Nitroaniline 20<1.2
8270D P7J028311311/6/17 15:59 JMVug/L 0.794-Nitrophenol 50<0.79
8270D P7J028311311/6/17 15:59 JMVug/L 3.55-Nitro-o-toluidine 10<3.5
8270D P7J028311311/6/17 15:59 JMVug/L 3.47,12-Dimethylbenz(a)anthracene 10<3.4
8270D P7J028311311/6/17 15:59 JMVug/L 2.4Acenaphthene10<2.4
8270D P7J028311311/6/17 15:59 JMVug/L 2.7Acenaphthylene10<2.7
8270D P7J028311311/6/17 15:59 JMVug/L 3.1Acetophenone10<3.1
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Anthracene10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Benzo(a)anthracene 10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Benzo(a)pyrene 10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.5Benzo(b)fluoranthene 10<1.5
8270D P7J028312611/6/17 15:59 JMVug/L 1.9Benzo(b&k)fluoranthene NE<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.8Benzo(g,h,i)perylene 10<1.8
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Benzo(k)fluoranthene 10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 2.8Benzyl alcohol 20<2.8
8270D P7J028311311/6/17 15:59 JMVug/L 3.4bis(2-Chloroethoxy)methane 10<3.4
8270D P7J028311311/6/17 15:59 JMVug/L 3.0Bis(2-Chloroethyl)ether 10<3.0
8270D P7J028311311/6/17 15:59 JMVug/L 2.6Bis(2-chloroisopropyl)ether NE<2.6
8270D P7J028311311/6/17 15:59 JMVug/L 1.7Bis(2-Ethylhexyl)phthalate 15<1.7
8270D P7J028311311/6/17 15:59 JMVug/L 1.8Butyl benzyl phthalate 10<1.8
8270D P7J028311311/6/17 15:59 JMVug/L 3.3Chlorobenzilate10<3.3
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Chrysene10<1.9
8270D P7J028312611/6/17 15:59 JMVug/L 3.7Diallate10<3.7
8270D P7J028311311/6/17 15:59 JMVug/L 1.6Dibenzo(a,h)anthracene 10<1.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-03
Prism Work Order: 7100243
Time Collected: 10/11/17 09:00
Time Submitted: 10/12/17 14:00
MW-05R
50-02
SWSL
8270D P7J028311311/6/17 15:59 JMVug/L 2.3Dibenzofuran10<2.3
8270D P7J028311311/6/17 15:59 JMVug/L 4.4Diethyl phthalate 6000<4.4
8270D P7J028311311/6/17 15:59 JMVug/L 4.1Dimethoate20<4.1
8270D P7J028311311/6/17 15:59 JMVug/L 1.8Dimethyl phthalate 10<1.8
8270D P7J028311311/6/17 15:59 JMVug/L 2.2Di-n-butyl phthalate 10<2.2
8270D P7J028311311/6/17 15:59 JMVug/L 1.7Di-n-octyl phthalate 10<1.7
8270D P7J028311311/6/17 15:59 JMVug/L 3.7Diphenylamine10<3.7
8270D P7J028312611/6/17 15:59 JMVug/L 3.7Disulfoton10<3.7
8270D P7J028311311/6/17 15:59 JMVug/L 3.7Ethyl Methanesulfonate 20<3.7
8270D P7J028312611/7/17 18:15 JMVug/L 5.7Famphur20<5.7
8270D P7J028311311/6/17 15:59 JMVug/L 2.2Fluoranthene10<2.2
8270D P7J028311311/6/17 15:59 JMVug/L 2.2Fluorene10<2.2
8270D P7J028311311/6/17 15:59 JMVug/L 1.7Hexachlorobenzene10<1.7
8270D P7J028311311/6/17 15:59 JMVug/L 2.8Hexachlorobutadiene10<2.8
8270D P7J028311311/6/17 15:59 JMVug/L 2.3Hexachlorocyclopentadiene10<2.3
8270D P7J028311311/6/17 15:59 JMVug/L 2.3Hexachloroethane10<2.3
8270D P7J028311311/6/17 15:59 JMVug/L 2.6Hexachloropropene10<2.6
8270D P7J028311311/6/17 15:59 JMVug/L 5.1Indeno(1,2,3-cd)pyrene 10<5.1
8270D P7J028311311/6/17 15:59 JMVug/L 3.6Isodrin20<3.6
8270D P7J028311311/6/17 15:59 JMVug/L 3.3Isophorone10<3.3
8270D P7J028311311/6/17 15:59 JMVug/L 5.0Isosafrole10<5.0
8270D P7J028312611/7/17 18:15 JMVug/L 3.8Kepone20<3.8
8270D P7J0283113011/6/17 15:59 JMVAug/L 16Methapyrilene100<16
8270D P7J028312611/6/17 15:59 JMVug/L 3.1Methyl Methanesulfonate 10<3.1
8270D P7J028312611/6/17 15:59 JMVug/L 4.4Methyl parathion 10<4.4
8270D P7J028311311/6/17 15:59 JMVug/L 3.4Nitrobenzene10<3.4
8270D P7J028311311/6/17 15:59 JMVug/L 3.3N-Nitrosodibutylamine 10<3.3
8270D P7J028311311/6/17 15:59 JMVug/L 2.4N-Nitrosodiethylamine 20<2.4
8270D P7J028311311/6/17 15:59 JMVug/L 1.5N-Nitrosodimethylamine 10<1.5
8270D P7J028311311/6/17 15:59 JMVug/L 2.9N-Nitroso-di-n-propylamine 10<2.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.7N-Nitrosodiphenylamine 10<1.7
8270D P7J028311311/6/17 15:59 JMVug/L 2.0N-Nitrosomethylethylamine 10<2.0
8270D P7J028311311/6/17 15:59 JMVug/L 3.2N-Nitrosopiperidine 20<3.2
8270D P7J028311311/6/17 15:59 JMVug/L 2.6N-Nitrosopyrrolidine 10<2.6
8270D P7J028311311/6/17 15:59 JMVug/L 3.6O,O,O-Triethyl phosphorothioate 10<3.6
8270D P7J028311311/6/17 15:59 JMVAug/L 2.3o-Toluidine 10<2.3
8270D P7J028311311/6/17 15:59 JMVug/L 4.0Parathion10<4.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-03
Prism Work Order: 7100243
Time Collected: 10/11/17 09:00
Time Submitted: 10/12/17 14:00
MW-05R
50-02
SWSL
8270D P7J028312611/6/17 15:59 JMVug/L 3.0p-Dimethylaminoazobenzene 10<3.0
8270D P7J028311311/6/17 15:59 JMVug/L 3.4Pentachlorobenzene10<3.4
8270D P7J028311311/6/17 15:59 JMVug/L 3.1Pentachloronitrobenzene20<3.1
8270D P7J028311311/6/17 15:59 JMVug/L 1.6Pentachlorophenol25<1.6
8270D P7J028312611/6/17 15:59 JMVug/L 3.9Phenacetin20<3.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Phenanthrene10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 1.3Phenol10<1.3
8270D P7J028311311/6/17 15:59 JMVug/L 3.6Phorate10<3.6
8270D P7J028311311/6/17 15:59 JMVug/L 3.7Pronamide10<3.7
8270D P7J028311311/6/17 15:59 JMVug/L 1.9Pyrene10<1.9
8270D P7J028311311/6/17 15:59 JMVug/L 2.9Safrole10<2.9
8270D P7J028311311/6/17 15:59 JMVug/L 2.5Thionazin20<2.5
Surrogate Recovery Control Limits
44-11990 %2-Fluorobiphenyl
19-11935 %2-Fluorophenol
44-12081 %Nitrobenzene-d5
11-5226 %Phenol-d5
50-13485 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 14:49JABug/L 0.036Mercury0.2<0.036
6020B P7J025611.0 10/18/17 6:59 EGCug/L 0.19Antimony64.1
6020B P7J025611.0 10/18/17 6:59 EGCJug/L 0.031Arsenic100.52
6020B P7J025615.0 10/18/17 6:59 EGCug/L 0.97Barium100260
6020B P7J025611.0 10/18/17 6:59 EGCJug/L 0.057Beryllium10.44
6020B P7J025611.0 10/18/17 6:59 EGCJug/L 0.078Cadmium10.41
6020B P7J025611.0 10/18/17 6:59 EGCug/L 0.19Chromium108.7
6020B P7J025611.0 10/18/17 6:59 EGCug/L 0.0071Cobalt1027
6020B P7J025615.0 10/18/17 6:59 EGCug/L 0.22Copper1016
6020B P7J025611.0 10/18/17 6:59 EGCug/L 0.093Lead103.7
6020B P7J025611010/18/17 6:59 EGCug/L 0.85Nickel5012
6020B P7J025615.0 10/18/17 6:59 EGCJug/L 0.63Selenium101.0
6020B P7J025615.0 10/18/17 6:59 EGCug/L 0.063Silver10<0.063
6020B P7J025611.0 10/18/17 6:59 EGCJug/L 0.099Thallium5.50.27
6020B P7J025615.0 10/18/17 6:59 EGCug/L 0.21Tin100<0.21
6020B P7J025611.0 10/18/17 6:59 EGCug/L 0.10Vanadium2512
6020B P7J025611010/18/17 6:59 EGCug/L 2.8Zinc1051
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-03
Prism Work Order: 7100243
Time Collected: 10/11/17 09:00
Time Submitted: 10/12/17 14:00
MW-05R
50-02
SWSL
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 10:41KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 10:41KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 10:41KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 10:41KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 10:41KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 10:41KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 10:41KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 10:41KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 10:41KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.065Dibromomethane10<0.065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-03
Prism Work Order: 7100243
Time Collected: 10/11/17 09:00
Time Submitted: 10/12/17 14:00
MW-05R
50-02
SWSL
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 10:41KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 10:41KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 10:41KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 10:41KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 10:41KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 10:41KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 10:41KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 10:41KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 10:41KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 10:41KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 10:41KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 10:41KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 10:41KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 10:41KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 10:41KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 10:41KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12494 %4-Bromofluorobenzene
75-12993 %Dibromofluoromethane
77-12398 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-04
Prism Work Order: 7100243
Time Collected: 10/11/17 10:17
Time Submitted: 10/12/17 14:00
MW-06
50-02
SWSL
Anions by Ion Chromatography
9056A P7J02391100010/12/17 19:38BMSug/L 40ChlorideNE24000
9056A P7J0239110010/12/17 19:38BMSug/L 7.7Nitrate as N 10000290
9056A P7J02391100010/12/17 19:38BMSug/L 200Sulfate25000012000
General Chemistry Parameters
SM5210 B P7J02201200010/12/17 16:54SLSug/L 2000Biochemical Oxygen Demand NE<2000
SM5220 D P7J030015000010/18/17 10:00BMSJug/L 17000Chemical Oxygen Demand NE25000
SM4500-CN E P7J033315.0 10/19/17 13:00EGCJug/L 1.0Cyanide102.7
SM3500-Fe D P7J0238120010/12/17 16:30EGCug/L 14Ferrous Iron NE2500
SM4500-S F P7J03171200010/18/17 12:20EGCug/L 830Sulfide1000<830
SM2320 B P7J03691500010/20/17 9:15 CLBug/L 770Total Alkalinity to pH 4.5 NE49000
Semivolatile Organic Compounds by GC/MS
8270D P7J028311511/6/17 16:22 JMVug/L 3.71,2,4,5-Tetrachlorobenzene 10<3.7
8270D P7J028311511/6/17 16:22 JMVug/L 2.71,2,4-Trichlorobenzene 10<2.7
8270D P7J028311511/6/17 16:22 JMVug/L 2.51,2-Dichlorobenzene 5<2.5
8270D P7J028313111/6/17 16:22 JMVug/L 4.21,3,5-Trinitrobenzene 10<4.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.91,3-Dichlorobenzene 5<2.9
8270D P7J028311511/6/17 16:22 JMVug/L 2.51,4-Dichlorobenzene 1<2.5
8270D P7J028311511/6/17 16:22 JMVug/L 4.21,4-Naphthoquinone 10<4.2
8270D P7J028311511/6/17 16:22 JMVug/L 4.41,4-Phenylenediamine 10<4.4
8270D P7J028311511/6/17 16:22 JMVAug/L 2.61-Naphthylamine 10<2.6
8270D P7J028311511/6/17 16:22 JMVug/L 4.32,3,4,6-Tetrachlorophenol 10<4.3
8270D P7J028311511/6/17 16:22 JMVug/L 2.52,4,5-Trichlorophenol 10<2.5
8270D P7J028311511/6/17 16:22 JMVug/L 2.82,4,6-Trichlorophenol 10<2.8
8270D P7J028311511/6/17 16:22 JMVug/L 3.92,4-Dichlorophenol 10<3.9
8270D P7J028311511/6/17 16:22 JMVug/L 5.32,4-Dimethylphenol 10<5.3
8270D P7J028311511/6/17 16:22 JMVug/L 4.22,4-Dinitrophenol 50<4.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.22,4-Dinitrotoluene 10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 3.12,6-Dichlorophenol 10<3.1
8270D P7J028311511/6/17 16:22 JMVug/L 1.72,6-Dinitrotoluene 10<1.7
8270D P7J028311511/6/17 16:22 JMVug/L 4.12-Acetylaminofluorene 20<4.1
8270D P7J028311511/6/17 16:22 JMVug/L 4.22-Chloronaphthalene 10<4.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.92-Chlorophenol 10<2.9
8270D P7J028311511/6/17 16:22 JMVug/L 3.72-Methylnaphthalene 10<3.7
8270D P7J028311511/6/17 16:22 JMVug/L 2.82-Methylphenol 10<2.8
8270D P7J028311511/6/17 16:22 JMVAug/L 3.22-Naphthylamine 10<3.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.22-Nitroaniline 50<2.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-04
Prism Work Order: 7100243
Time Collected: 10/11/17 10:17
Time Submitted: 10/12/17 14:00
MW-06
50-02
SWSL
8270D P7J028311511/6/17 16:22 JMVug/L 3.62-Nitrophenol 10<3.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.23,3’-Dichlorobenzidine 20<2.2
8270D P7J028313111/6/17 16:22 JMVAug/L 4.83,3·-Dimethylbenzidine 10<4.8
8270D P7J028311511/6/17 16:22 JMVug/L 2.43/4-Methylphenol 10<2.4
8270D P7J028311511/6/17 16:22 JMVug/L 3.73-Methylcholanthrene 10<3.7
8270D P7J028311511/6/17 16:22 JMVug/L 2.13-Nitroaniline 50<2.1
8270D P7J028311511/6/17 16:22 JMVug/L 2.14,6-Dinitro-2-methylphenol 50<2.1
8270D P7J028311511/6/17 16:22 JMVAug/L 3.84-Aminobiphenyl 20<3.8
8270D P7J028311511/6/17 16:22 JMVug/L 2.04-Bromophenyl phenyl ether 10<2.0
8270D P7J028311511/6/17 16:22 JMVug/L 3.64-Chloro-3-methylphenol 20<3.6
8270D P7J028311511/6/17 16:22 JMVug/L 3.84-Chloroaniline 20<3.8
8270D P7J028311511/6/17 16:22 JMVug/L 2.04-Chlorophenyl phenyl ether 10<2.0
8270D P7J028311511/6/17 16:22 JMVug/L 1.44-Nitroaniline 20<1.4
8270D P7J028311511/6/17 16:22 JMVug/L 0.924-Nitrophenol 50<0.92
8270D P7J028311511/6/17 16:22 JMVug/L 4.15-Nitro-o-toluidine 10<4.1
8270D P7J028311511/6/17 16:22 JMVug/L 4.07,12-Dimethylbenz(a)anthracene 10<4.0
8270D P7J028311511/6/17 16:22 JMVug/L 2.8Acenaphthene10<2.8
8270D P7J028311511/6/17 16:22 JMVug/L 3.1Acenaphthylene10<3.1
8270D P7J028311511/6/17 16:22 JMVug/L 3.6Acetophenone10<3.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Anthracene10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Benzo(a)anthracene 10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Benzo(a)pyrene 10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 1.8Benzo(b)fluoranthene 10<1.8
8270D P7J028313111/6/17 16:22 JMVug/L 2.2Benzo(b&k)fluoranthene NE<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.1Benzo(g,h,i)perylene 10<2.1
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Benzo(k)fluoranthene 10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 3.3Benzyl alcohol 20<3.3
8270D P7J028311511/6/17 16:22 JMVug/L 4.0bis(2-Chloroethoxy)methane 10<4.0
8270D P7J028311511/6/17 16:22 JMVug/L 3.6Bis(2-Chloroethyl)ether 10<3.6
8270D P7J028311511/6/17 16:22 JMVug/L 3.0Bis(2-chloroisopropyl)ether NE<3.0
8270D P7J028311511/6/17 16:22 JMVug/L 2.0Bis(2-Ethylhexyl)phthalate 15<2.0
8270D P7J028311511/6/17 16:22 JMVug/L 2.1Butyl benzyl phthalate 10<2.1
8270D P7J028311511/6/17 16:22 JMVug/L 3.9Chlorobenzilate10<3.9
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Chrysene10<2.2
8270D P7J028313111/6/17 16:22 JMVug/L 4.3Diallate10<4.3
8270D P7J028311511/6/17 16:22 JMVug/L 1.8Dibenzo(a,h)anthracene 10<1.8
8270D P7J028311511/6/17 16:22 JMVug/L 2.7Dibenzofuran10<2.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-04
Prism Work Order: 7100243
Time Collected: 10/11/17 10:17
Time Submitted: 10/12/17 14:00
MW-06
50-02
SWSL
8270D P7J028311511/6/17 16:22 JMVug/L 5.1Diethyl phthalate 6000<5.1
8270D P7J028311511/6/17 16:22 JMVug/L 4.8Dimethoate20<4.8
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Dimethyl phthalate 10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 2.6Di-n-butyl phthalate 10<2.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.0Di-n-octyl phthalate 10<2.0
8270D P7J028311511/6/17 16:22 JMVug/L 4.3Diphenylamine10<4.3
8270D P7J028313111/6/17 16:22 JMVug/L 4.4Disulfoton10<4.4
8270D P7J028311511/6/17 16:22 JMVug/L 4.3Ethyl Methanesulfonate 20<4.3
8270D P7J028313111/7/17 18:38 JMVug/L 6.6Famphur20<6.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.6Fluoranthene10<2.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.6Fluorene10<2.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.0Hexachlorobenzene10<2.0
8270D P7J028311511/6/17 16:22 JMVug/L 3.3Hexachlorobutadiene10<3.3
8270D P7J028311511/6/17 16:22 JMVug/L 2.7Hexachlorocyclopentadiene10<2.7
8270D P7J028311511/6/17 16:22 JMVug/L 2.7Hexachloroethane10<2.7
8270D P7J028311511/6/17 16:22 JMVug/L 3.1Hexachloropropene10<3.1
8270D P7J028311511/6/17 16:22 JMVug/L 6.0Indeno(1,2,3-cd)pyrene 10<6.0
8270D P7J028311511/6/17 16:22 JMVug/L 4.2Isodrin20<4.2
8270D P7J028311511/6/17 16:22 JMVug/L 3.9Isophorone10<3.9
8270D P7J028311511/6/17 16:22 JMVug/L 5.9Isosafrole10<5.9
8270D P7J028313111/7/17 18:38 JMVug/L 4.4Kepone20<4.4
8270D P7J0283115011/6/17 16:22 JMVAug/L 18Methapyrilene100<18
8270D P7J028313111/6/17 16:22 JMVug/L 3.6Methyl Methanesulfonate 10<3.6
8270D P7J028313111/6/17 16:22 JMVug/L 5.2Methyl parathion 10<5.2
8270D P7J028311511/6/17 16:22 JMVug/L 3.9Nitrobenzene10<3.9
8270D P7J028311511/6/17 16:22 JMVug/L 3.9N-Nitrosodibutylamine 10<3.9
8270D P7J028311511/6/17 16:22 JMVug/L 2.8N-Nitrosodiethylamine 20<2.8
8270D P7J028311511/6/17 16:22 JMVug/L 1.7N-Nitrosodimethylamine 10<1.7
8270D P7J028311511/6/17 16:22 JMVug/L 3.4N-Nitroso-di-n-propylamine 10<3.4
8270D P7J028311511/6/17 16:22 JMVug/L 2.0N-Nitrosodiphenylamine 10<2.0
8270D P7J028311511/6/17 16:22 JMVug/L 2.4N-Nitrosomethylethylamine 10<2.4
8270D P7J028311511/6/17 16:22 JMVug/L 3.7N-Nitrosopiperidine 20<3.7
8270D P7J028311511/6/17 16:22 JMVug/L 3.0N-Nitrosopyrrolidine 10<3.0
8270D P7J028311511/6/17 16:22 JMVug/L 4.2O,O,O-Triethyl phosphorothioate 10<4.2
8270D P7J028311511/6/17 16:22 JMVAug/L 2.7o-Toluidine 10<2.7
8270D P7J028311511/6/17 16:22 JMVug/L 4.7Parathion10<4.7
8270D P7J028313111/6/17 16:22 JMVug/L 3.5p-Dimethylaminoazobenzene 10<3.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-04
Prism Work Order: 7100243
Time Collected: 10/11/17 10:17
Time Submitted: 10/12/17 14:00
MW-06
50-02
SWSL
8270D P7J028311511/6/17 16:22 JMVug/L 3.9Pentachlorobenzene10<3.9
8270D P7J028311511/6/17 16:22 JMVug/L 3.6Pentachloronitrobenzene20<3.6
8270D P7J028311511/6/17 16:22 JMVug/L 1.9Pentachlorophenol25<1.9
8270D P7J028313111/6/17 16:22 JMVug/L 4.6Phenacetin20<4.6
8270D P7J028311511/6/17 16:22 JMVug/L 2.3Phenanthrene10<2.3
8270D P7J028311511/6/17 16:22 JMVug/L 1.5Phenol10<1.5
8270D P7J028311511/6/17 16:22 JMVug/L 4.2Phorate10<4.2
8270D P7J028311511/6/17 16:22 JMVug/L 4.3Pronamide10<4.3
8270D P7J028311511/6/17 16:22 JMVug/L 2.2Pyrene10<2.2
8270D P7J028311511/6/17 16:22 JMVug/L 3.4Safrole10<3.4
8270D P7J028311511/6/17 16:22 JMVug/L 3.0Thionazin20<3.0
Surrogate Recovery Control Limits
44-11983 %2-Fluorobiphenyl
19-11930 %2-Fluorophenol
44-12070 %Nitrobenzene-d5
11-5223 %Phenol-d5
50-13487 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 14:53JABug/L 0.036Mercury0.2<0.036
6020B P7J025611.0 10/18/17 7:07 EGCug/L 0.19Antimony6<0.19
6020B P7J025611.0 10/18/17 7:07 EGCJug/L 0.031Arsenic100.19
6020B P7J025615.0 10/18/17 7:07 EGCug/L 0.97Barium10087
6020B P7J025611.0 10/18/17 7:07 EGCug/L 0.057Beryllium1<0.057
6020B P7J025611.0 10/18/17 7:07 EGCJug/L 0.078Cadmium10.41
6020B P7J025611.0 10/18/17 7:07 EGCJug/L 0.19Chromium100.66
6020B P7J025611.0 10/18/17 7:07 EGCug/L 0.0071Cobalt1089
6020B P7J025615.0 10/18/17 7:07 EGCJug/L 0.22Copper101.9
6020B P7J025611.0 10/18/17 7:07 EGCJug/L 0.093Lead100.20
6020B P7J025611010/18/17 7:07 EGCug/L 0.85Nickel5074
6020B P7J025615.0 10/18/17 7:07 EGCug/L 0.63Selenium10<0.63
6020B P7J025615.0 10/18/17 7:07 EGCug/L 0.063Silver10<0.063
6020B P7J025611.0 10/18/17 7:07 EGCug/L 0.099Thallium5.51.6
6020B P7J025615.0 10/18/17 7:07 EGCug/L 0.21Tin100<0.21
6020B P7J025611.0 10/18/17 7:07 EGCJug/L 0.10Vanadium250.60
6020B P7J025611010/18/17 7:07 EGCug/L 2.8Zinc1052
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-04
Prism Work Order: 7100243
Time Collected: 10/11/17 10:17
Time Submitted: 10/12/17 14:00
MW-06
50-02
SWSL
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 11:06KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 11:06KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 11:06KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 11:06KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 11:06KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 11:06KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 11:06KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 11:06KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 11:06KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.065Dibromomethane10<0.065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-04
Prism Work Order: 7100243
Time Collected: 10/11/17 10:17
Time Submitted: 10/12/17 14:00
MW-06
50-02
SWSL
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 11:06KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 11:06KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 11:06KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 11:06KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 11:06KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 11:06KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 11:06KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 11:06KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 11:06KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 11:06KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 11:06KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 11:06KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 11:06KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 11:06KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 11:06KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 11:06KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12494 %4-Bromofluorobenzene
75-12996 %Dibromofluoromethane
77-12397 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-05
Prism Work Order: 7100243
Time Collected: 10/10/17 12:10
Time Submitted: 10/12/17 14:00
SW-01
50-02
SWSL
Semivolatile Organic Compounds by GC/MS
8270D P7J028311011/6/17 16:44 JMVug/L 2.51,2,4,5-Tetrachlorobenzene 10<2.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.81,2,4-Trichlorobenzene 10<1.8
8270D P7J028311011/6/17 16:44 JMVug/L 1.71,2-Dichlorobenzene 5<1.7
8270D P7J028312111/6/17 16:44 JMVug/L 2.81,3,5-Trinitrobenzene 10<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 1.91,3-Dichlorobenzene 5<1.9
8270D P7J028311011/6/17 16:44 JMVug/L 1.71,4-Dichlorobenzene 1<1.7
8270D P7J028311011/6/17 16:44 JMVug/L 2.81,4-Naphthoquinone 10<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 2.91,4-Phenylenediamine 10<2.9
8270D P7J028311011/6/17 16:44 JMVAug/L 1.81-Naphthylamine 10<1.8
8270D P7J028311011/6/17 16:44 JMVug/L 2.92,3,4,6-Tetrachlorophenol 10<2.9
8270D P7J028311011/6/17 16:44 JMVug/L 1.62,4,5-Trichlorophenol 10<1.6
8270D P7J028311011/6/17 16:44 JMVug/L 1.92,4,6-Trichlorophenol 10<1.9
8270D P7J028311011/6/17 16:44 JMVug/L 2.62,4-Dichlorophenol 10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 3.62,4-Dimethylphenol 10<3.6
8270D P7J028311011/6/17 16:44 JMVug/L 2.82,4-Dinitrophenol 50<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 1.52,4-Dinitrotoluene 10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 2.12,6-Dichlorophenol 10<2.1
8270D P7J028311011/6/17 16:44 JMVug/L 1.22,6-Dinitrotoluene 10<1.2
8270D P7J028311011/6/17 16:44 JMVug/L 2.82-Acetylaminofluorene 20<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 2.82-Chloronaphthalene 10<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 1.92-Chlorophenol 10<1.9
8270D P7J028311011/6/17 16:44 JMVug/L 2.52-Methylnaphthalene 10<2.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.92-Methylphenol 10<1.9
8270D P7J028311011/6/17 16:44 JMVAug/L 2.12-Naphthylamine 10<2.1
8270D P7J028311011/6/17 16:44 JMVug/L 1.52-Nitroaniline 50<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 2.42-Nitrophenol 10<2.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.53,3’-Dichlorobenzidine 20<1.5
8270D P7J028312111/6/17 16:44 JMVAug/L 3.23,3·-Dimethylbenzidine 10<3.2
8270D P7J028311011/6/17 16:44 JMVug/L 1.63/4-Methylphenol 10<1.6
8270D P7J028311011/6/17 16:44 JMVug/L 2.53-Methylcholanthrene 10<2.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.43-Nitroaniline 50<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.44,6-Dinitro-2-methylphenol 50<1.4
8270D P7J028311011/6/17 16:44 JMVAug/L 2.54-Aminobiphenyl 20<2.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.34-Bromophenyl phenyl ether 10<1.3
8270D P7J028311011/6/17 16:44 JMVug/L 2.44-Chloro-3-methylphenol 20<2.4
8270D P7J028311011/6/17 16:44 JMVug/L 2.54-Chloroaniline 20<2.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-05
Prism Work Order: 7100243
Time Collected: 10/10/17 12:10
Time Submitted: 10/12/17 14:00
SW-01
50-02
SWSL
8270D P7J028311011/6/17 16:44 JMVug/L 1.44-Chlorophenyl phenyl ether 10<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 0.964-Nitroaniline 20<0.96
8270D P7J028311011/6/17 16:44 JMVug/L 0.624-Nitrophenol 50<0.62
8270D P7J028311011/6/17 16:44 JMVug/L 2.75-Nitro-o-toluidine 10<2.7
8270D P7J028311011/6/17 16:44 JMVug/L 2.77,12-Dimethylbenz(a)anthracene 10<2.7
8270D P7J028311011/6/17 16:44 JMVug/L 1.9Acenaphthene10<1.9
8270D P7J028311011/6/17 16:44 JMVug/L 2.1Acenaphthylene10<2.1
8270D P7J028311011/6/17 16:44 JMVug/L 2.4Acetophenone10<2.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Anthracene10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Benzo(a)anthracene 10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Benzo(a)pyrene 10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.2Benzo(b)fluoranthene 10<1.2
8270D P7J028312111/6/17 16:44 JMVug/L 1.5Benzo(b&k)fluoranthene NE<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.4Benzo(g,h,i)perylene 10<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Benzo(k)fluoranthene 10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 2.2Benzyl alcohol 20<2.2
8270D P7J028311011/6/17 16:44 JMVug/L 2.6bis(2-Chloroethoxy)methane 10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 2.4Bis(2-Chloroethyl)ether 10<2.4
8270D P7J028311011/6/17 16:44 JMVug/L 2.0Bis(2-chloroisopropyl)ether NE<2.0
8270D P7J028311011/6/17 16:44 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate 15<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.4Butyl benzyl phthalate 10<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 2.6Chlorobenzilate10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Chrysene10<1.5
8270D P7J028312111/6/17 16:44 JMVug/L 2.9Diallate10<2.9
8270D P7J028311011/6/17 16:44 JMVug/L 1.2Dibenzo(a,h)anthracene 10<1.2
8270D P7J028311011/6/17 16:44 JMVug/L 1.8Dibenzofuran10<1.8
8270D P7J028311011/6/17 16:44 JMVug/L 3.4Diethyl phthalate 6000<3.4
8270D P7J028311011/6/17 16:44 JMVug/L 3.2Dimethoate20<3.2
8270D P7J028311011/6/17 16:44 JMVug/L 1.4Dimethyl phthalate 10<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.7Di-n-butyl phthalate 10<1.7
8270D P7J028311011/6/17 16:44 JMVug/L 1.3Di-n-octyl phthalate 10<1.3
8270D P7J028311011/6/17 16:44 JMVug/L 2.9Diphenylamine10<2.9
8270D P7J028312111/6/17 16:44 JMVug/L 2.9Disulfoton10<2.9
8270D P7J028311011/6/17 16:44 JMVug/L 2.9Ethyl Methanesulfonate 20<2.9
8270D P7J028312111/7/17 19:00 JMVug/L 4.4Famphur20<4.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.7Fluoranthene10<1.7
8270D P7J028311011/6/17 16:44 JMVug/L 1.7Fluorene10<1.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-05
Prism Work Order: 7100243
Time Collected: 10/10/17 12:10
Time Submitted: 10/12/17 14:00
SW-01
50-02
SWSL
8270D P7J028311011/6/17 16:44 JMVug/L 1.3Hexachlorobenzene10<1.3
8270D P7J028311011/6/17 16:44 JMVug/L 2.2Hexachlorobutadiene10<2.2
8270D P7J028311011/6/17 16:44 JMVug/L 1.8Hexachlorocyclopentadiene10<1.8
8270D P7J028311011/6/17 16:44 JMVug/L 1.8Hexachloroethane10<1.8
8270D P7J028311011/6/17 16:44 JMVug/L 2.1Hexachloropropene10<2.1
8270D P7J028311011/6/17 16:44 JMVug/L 4.0Indeno(1,2,3-cd)pyrene 10<4.0
8270D P7J028311011/6/17 16:44 JMVug/L 2.8Isodrin20<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 2.6Isophorone10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 3.9Isosafrole10<3.9
8270D P7J028312111/7/17 19:00 JMVug/L 2.9Kepone20<2.9
8270D P7J0283110011/6/17 16:44 JMVAug/L 12Methapyrilene100<12
8270D P7J028312111/6/17 16:44 JMVug/L 2.4Methyl Methanesulfonate 10<2.4
8270D P7J028312111/6/17 16:44 JMVug/L 3.5Methyl parathion 10<3.5
8270D P7J028311011/6/17 16:44 JMVug/L 2.6Nitrobenzene10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 2.6N-Nitrosodibutylamine 10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 1.9N-Nitrosodiethylamine 20<1.9
8270D P7J028311011/6/17 16:44 JMVug/L 1.2N-Nitrosodimethylamine 10<1.2
8270D P7J028311011/6/17 16:44 JMVug/L 2.2N-Nitroso-di-n-propylamine 10<2.2
8270D P7J028311011/6/17 16:44 JMVug/L 1.4N-Nitrosodiphenylamine 10<1.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.6N-Nitrosomethylethylamine 10<1.6
8270D P7J028311011/6/17 16:44 JMVug/L 2.5N-Nitrosopiperidine 20<2.5
8270D P7J028311011/6/17 16:44 JMVug/L 2.0N-Nitrosopyrrolidine 10<2.0
8270D P7J028311011/6/17 16:44 JMVug/L 2.8O,O,O-Triethyl phosphorothioate 10<2.8
8270D P7J028311011/6/17 16:44 JMVAug/L 1.8o-Toluidine 10<1.8
8270D P7J028311011/6/17 16:44 JMVug/L 3.1Parathion10<3.1
8270D P7J028312111/6/17 16:44 JMVug/L 2.3p-Dimethylaminoazobenzene 10<2.3
8270D P7J028311011/6/17 16:44 JMVug/L 2.6Pentachlorobenzene10<2.6
8270D P7J028311011/6/17 16:44 JMVug/L 2.4Pentachloronitrobenzene20<2.4
8270D P7J028311011/6/17 16:44 JMVug/L 1.3Pentachlorophenol25<1.3
8270D P7J028312111/6/17 16:44 JMVug/L 3.1Phenacetin20<3.1
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Phenanthrene10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 1.0Phenol10<1.0
8270D P7J028311011/6/17 16:44 JMVug/L 2.8Phorate10<2.8
8270D P7J028311011/6/17 16:44 JMVug/L 2.9Pronamide10<2.9
8270D P7J028311011/6/17 16:44 JMVug/L 1.5Pyrene10<1.5
8270D P7J028311011/6/17 16:44 JMVug/L 2.3Safrole10<2.3
8270D P7J028311011/6/17 16:44 JMVug/L 2.0Thionazin20<2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-05
Prism Work Order: 7100243
Time Collected: 10/10/17 12:10
Time Submitted: 10/12/17 14:00
SW-01
50-02
SWSL
Surrogate Recovery Control Limits
44-11976 %2-Fluorobiphenyl
19-11927 %2-Fluorophenol
44-12068 %Nitrobenzene-d5
11-5219 %Phenol-d5
50-13478 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 14:56JABug/L 0.036Mercury0.2<0.036
6020B P7J027911.0 10/19/17 0:24 EGCug/L 0.19Antimony6<0.19
6020B P7J027911.0 10/19/17 0:24 EGCJug/L 0.031Arsenic100.15
6020B P7J027915.0 10/19/17 0:24 EGCug/L 0.97Barium10021
6020B P7J027911.0 10/19/17 0:24 EGCug/L 0.057Beryllium1<0.057
6020B P7J027911.0 10/19/17 0:24 EGCug/L 0.078Cadmium1<0.078
6020B P7J027911.0 10/19/17 0:24 EGCug/L 0.19Chromium101.3
6020B P7J027911.0 10/19/17 0:24 EGCJug/L 0.0071Cobalt100.51
6020B P7J034315.0 10/20/17 0:12 EGCJug/L 0.22Copper101.6
6020B P7J027911.0 10/19/17 0:24 EGCJug/L 0.093Lead100.55
6020B P7J034312.0 10/20/17 0:12 EGCJug/L 0.85Nickel501.1
6020B P7J027915.0 10/19/17 0:24 EGCug/L 0.63Selenium10<0.63
6020B P7J027915.0 10/19/17 0:24 EGCug/L 0.063Silver10<0.063
6020B P7J027911.0 10/19/17 0:24 EGCug/L 0.099Thallium5.5<0.099
6020B P7J027911010/19/17 0:24 EGCJug/L 0.21Tin1000.43
6020B P7J027911.0 10/19/17 0:24 EGCug/L 0.10Vanadium251.4
6020B P7J027911010/19/17 0:24 EGCug/L 2.8Zinc1020
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 11:32KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0661,2-Dichloroethane 1<0.066
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-05
Prism Work Order: 7100243
Time Collected: 10/10/17 12:10
Time Submitted: 10/12/17 14:00
SW-01
50-02
SWSL
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 11:32KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 11:32KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 11:32KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 11:32KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 11:32KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 11:32KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 11:32KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 11:32KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.065Dibromomethane10<0.065
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 11:32KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 11:32KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 11:32KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 11:32KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 11:32KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 11:32KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 11:32KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 11:32KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-05
Prism Work Order: 7100243
Time Collected: 10/10/17 12:10
Time Submitted: 10/12/17 14:00
SW-01
50-02
SWSL
8260B P7J038511010/22/17 11:32KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 11:32KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 11:32KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 11:32KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 11:32KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 11:32KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 11:32KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 11:32KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12495 %4-Bromofluorobenzene
75-12996 %Dibromofluoromethane
77-12398 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-06
Prism Work Order: 7100243
Time Collected: 10/11/17 13:50
Time Submitted: 10/12/17 14:00
SW-02
50-02
SWSL
Semivolatile Organic Compounds by GC/MS
8270D P7J028311211/6/17 17:06 JMVug/L 2.91,2,4,5-Tetrachlorobenzene 10<2.9
8270D P7J028311211/6/17 17:06 JMVug/L 2.11,2,4-Trichlorobenzene 10<2.1
8270D P7J028311211/6/17 17:06 JMVug/L 2.01,2-Dichlorobenzene 5<2.0
8270D P7J028312411/6/17 17:06 JMVug/L 3.31,3,5-Trinitrobenzene 10<3.3
8270D P7J028311211/6/17 17:06 JMVug/L 2.31,3-Dichlorobenzene 5<2.3
8270D P7J028311211/6/17 17:06 JMVug/L 2.01,4-Dichlorobenzene 1<2.0
8270D P7J028311211/6/17 17:06 JMVug/L 3.31,4-Naphthoquinone 10<3.3
8270D P7J028311211/6/17 17:06 JMVug/L 3.41,4-Phenylenediamine 10<3.4
8270D P7J028311211/6/17 17:06 JMVAug/L 2.01-Naphthylamine 10<2.0
8270D P7J028311211/6/17 17:06 JMVug/L 3.42,3,4,6-Tetrachlorophenol 10<3.4
8270D P7J028311211/6/17 17:06 JMVug/L 1.92,4,5-Trichlorophenol 10<1.9
8270D P7J028311211/6/17 17:06 JMVug/L 2.22,4,6-Trichlorophenol 10<2.2
8270D P7J028311211/6/17 17:06 JMVug/L 3.12,4-Dichlorophenol 10<3.1
8270D P7J028311211/6/17 17:06 JMVug/L 4.22,4-Dimethylphenol 10<4.2
8270D P7J028311211/6/17 17:06 JMVug/L 3.32,4-Dinitrophenol 50<3.3
8270D P7J028311211/6/17 17:06 JMVug/L 1.72,4-Dinitrotoluene 10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 2.42,6-Dichlorophenol 10<2.4
8270D P7J028311211/6/17 17:06 JMVug/L 1.42,6-Dinitrotoluene 10<1.4
8270D P7J028311211/6/17 17:06 JMVug/L 3.22-Acetylaminofluorene 20<3.2
8270D P7J028311211/6/17 17:06 JMVug/L 3.32-Chloronaphthalene 10<3.3
8270D P7J028311211/6/17 17:06 JMVug/L 2.32-Chlorophenol 10<2.3
8270D P7J028311211/6/17 17:06 JMVug/L 2.92-Methylnaphthalene 10<2.9
8270D P7J028311211/6/17 17:06 JMVug/L 2.22-Methylphenol 10<2.2
8270D P7J028311211/6/17 17:06 JMVAug/L 2.52-Naphthylamine 10<2.5
8270D P7J028311211/6/17 17:06 JMVug/L 1.72-Nitroaniline 50<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 2.92-Nitrophenol 10<2.9
8270D P7J028311211/6/17 17:06 JMVug/L 1.73,3’-Dichlorobenzidine 20<1.7
8270D P7J028312411/6/17 17:06 JMVAug/L 3.73,3·-Dimethylbenzidine 10<3.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.93/4-Methylphenol 10<1.9
8270D P7J028311211/6/17 17:06 JMVug/L 2.93-Methylcholanthrene 10<2.9
8270D P7J028311211/6/17 17:06 JMVug/L 1.73-Nitroaniline 50<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.74,6-Dinitro-2-methylphenol 50<1.7
8270D P7J028311211/6/17 17:06 JMVAug/L 3.04-Aminobiphenyl 20<3.0
8270D P7J028311211/6/17 17:06 JMVug/L 1.54-Bromophenyl phenyl ether 10<1.5
8270D P7J028311211/6/17 17:06 JMVug/L 2.94-Chloro-3-methylphenol 20<2.9
8270D P7J028311211/6/17 17:06 JMVug/L 3.04-Chloroaniline 20<3.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-06
Prism Work Order: 7100243
Time Collected: 10/11/17 13:50
Time Submitted: 10/12/17 14:00
SW-02
50-02
SWSL
8270D P7J028311211/6/17 17:06 JMVug/L 1.64-Chlorophenyl phenyl ether 10<1.6
8270D P7J028311211/6/17 17:06 JMVug/L 1.14-Nitroaniline 20<1.1
8270D P7J028311211/6/17 17:06 JMVug/L 0.724-Nitrophenol 50<0.72
8270D P7J028311211/6/17 17:06 JMVug/L 3.25-Nitro-o-toluidine 10<3.2
8270D P7J028311211/6/17 17:06 JMVug/L 3.17,12-Dimethylbenz(a)anthracene 10<3.1
8270D P7J028311211/6/17 17:06 JMVug/L 2.2Acenaphthene10<2.2
8270D P7J028311211/6/17 17:06 JMVug/L 2.5Acenaphthylene10<2.5
8270D P7J028311211/6/17 17:06 JMVug/L 2.8Acetophenone10<2.8
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Anthracene10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Benzo(a)anthracene 10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Benzo(a)pyrene 10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.4Benzo(b)fluoranthene 10<1.4
8270D P7J028312411/6/17 17:06 JMVug/L 1.7Benzo(b&k)fluoranthene NE<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Benzo(g,h,i)perylene 10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Benzo(k)fluoranthene 10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 2.6Benzyl alcohol 20<2.6
8270D P7J028311211/6/17 17:06 JMVug/L 3.1bis(2-Chloroethoxy)methane 10<3.1
8270D P7J028311211/6/17 17:06 JMVug/L 2.8Bis(2-Chloroethyl)ether 10<2.8
8270D P7J028311211/6/17 17:06 JMVug/L 2.4Bis(2-chloroisopropyl)ether NE<2.4
8270D P7J028311211/6/17 17:06 JMVug/L 1.6Bis(2-Ethylhexyl)phthalate 15<1.6
8270D P7J028311211/6/17 17:06 JMVug/L 1.6Butyl benzyl phthalate 10<1.6
8270D P7J028311211/6/17 17:06 JMVug/L 3.0Chlorobenzilate10<3.0
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Chrysene10<1.7
8270D P7J028312411/6/17 17:06 JMVug/L 3.4Diallate10<3.4
8270D P7J028311211/6/17 17:06 JMVug/L 1.4Dibenzo(a,h)anthracene 10<1.4
8270D P7J028311211/6/17 17:06 JMVug/L 2.1Dibenzofuran10<2.1
8270D P7J028311211/6/17 17:06 JMVug/L 4.0Diethyl phthalate 6000<4.0
8270D P7J028311211/6/17 17:06 JMVug/L 3.7Dimethoate20<3.7
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Dimethyl phthalate 10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 2.0Di-n-butyl phthalate 10<2.0
8270D P7J028311211/6/17 17:06 JMVug/L 1.6Di-n-octyl phthalate 10<1.6
8270D P7J028311211/6/17 17:06 JMVug/L 3.4Diphenylamine10<3.4
8270D P7J028312411/6/17 17:06 JMVug/L 3.4Disulfoton10<3.4
8270D P7J028311211/6/17 17:06 JMVug/L 3.3Ethyl Methanesulfonate 20<3.3
8270D P7J028312411/7/17 19:23 JMVug/L 5.2Famphur20<5.2
8270D P7J028311211/6/17 17:06 JMVug/L 2.0Fluoranthene10<2.0
8270D P7J028311211/6/17 17:06 JMVug/L 2.0Fluorene10<2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-06
Prism Work Order: 7100243
Time Collected: 10/11/17 13:50
Time Submitted: 10/12/17 14:00
SW-02
50-02
SWSL
8270D P7J028311211/6/17 17:06 JMVug/L 1.6Hexachlorobenzene10<1.6
8270D P7J028311211/6/17 17:06 JMVug/L 2.6Hexachlorobutadiene10<2.6
8270D P7J028311211/6/17 17:06 JMVug/L 2.1Hexachlorocyclopentadiene10<2.1
8270D P7J028311211/6/17 17:06 JMVug/L 2.1Hexachloroethane10<2.1
8270D P7J028311211/6/17 17:06 JMVug/L 2.4Hexachloropropene10<2.4
8270D P7J028311211/6/17 17:06 JMVug/L 4.7Indeno(1,2,3-cd)pyrene 10<4.7
8270D P7J028311211/6/17 17:06 JMVug/L 3.3Isodrin20<3.3
8270D P7J028311211/6/17 17:06 JMVug/L 3.0Isophorone10<3.0
8270D P7J028311211/6/17 17:06 JMVug/L 4.6Isosafrole10<4.6
8270D P7J028312411/7/17 19:23 JMVug/L 3.4Kepone20<3.4
8270D P7J0283112011/6/17 17:06 JMVAug/L 14Methapyrilene100<14
8270D P7J028312411/6/17 17:06 JMVug/L 2.9Methyl Methanesulfonate 10<2.9
8270D P7J028312411/6/17 17:06 JMVug/L 4.1Methyl parathion 10<4.1
8270D P7J028311211/6/17 17:06 JMVug/L 3.1Nitrobenzene10<3.1
8270D P7J028311211/6/17 17:06 JMVug/L 3.0N-Nitrosodibutylamine 10<3.0
8270D P7J028311211/6/17 17:06 JMVug/L 2.2N-Nitrosodiethylamine 20<2.2
8270D P7J028311211/6/17 17:06 JMVug/L 1.4N-Nitrosodimethylamine 10<1.4
8270D P7J028311211/6/17 17:06 JMVug/L 2.6N-Nitroso-di-n-propylamine 10<2.6
8270D P7J028311211/6/17 17:06 JMVug/L 1.6N-Nitrosodiphenylamine 10<1.6
8270D P7J028311211/6/17 17:06 JMVug/L 1.9N-Nitrosomethylethylamine 10<1.9
8270D P7J028311211/6/17 17:06 JMVug/L 2.9N-Nitrosopiperidine 20<2.9
8270D P7J028311211/6/17 17:06 JMVug/L 2.3N-Nitrosopyrrolidine 10<2.3
8270D P7J028311211/6/17 17:06 JMVug/L 3.3O,O,O-Triethyl phosphorothioate 10<3.3
8270D P7J028311211/6/17 17:06 JMVAug/L 2.1o-Toluidine 10<2.1
8270D P7J028311211/6/17 17:06 JMVug/L 3.7Parathion10<3.7
8270D P7J028312411/6/17 17:06 JMVug/L 2.7p-Dimethylaminoazobenzene 10<2.7
8270D P7J028311211/6/17 17:06 JMVug/L 3.1Pentachlorobenzene10<3.1
8270D P7J028311211/6/17 17:06 JMVug/L 2.8Pentachloronitrobenzene20<2.8
8270D P7J028311211/6/17 17:06 JMVug/L 1.5Pentachlorophenol25<1.5
8270D P7J028312411/6/17 17:06 JMVug/L 3.6Phenacetin20<3.6
8270D P7J028311211/6/17 17:06 JMVug/L 1.8Phenanthrene10<1.8
8270D P7J028311211/6/17 17:06 JMVug/L 1.2Phenol10<1.2
8270D P7J028311211/6/17 17:06 JMVug/L 3.3Phorate10<3.3
8270D P7J028311211/6/17 17:06 JMVug/L 3.4Pronamide10<3.4
8270D P7J028311211/6/17 17:06 JMVug/L 1.7Pyrene10<1.7
8270D P7J028311211/6/17 17:06 JMVug/L 2.6Safrole10<2.6
8270D P7J028311211/6/17 17:06 JMVug/L 2.3Thionazin20<2.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-06
Prism Work Order: 7100243
Time Collected: 10/11/17 13:50
Time Submitted: 10/12/17 14:00
SW-02
50-02
SWSL
Surrogate Recovery Control Limits
44-11985 %2-Fluorobiphenyl
19-11929 %2-Fluorophenol
44-12077 %Nitrobenzene-d5
11-5221 %Phenol-d5
50-13481 %Terphenyl-d14
Total Metals
7470A P7J040610.20 10/23/17 15:00JABug/L 0.036Mercury0.2<0.036
6020B P7J027911.0 10/19/17 0:32 EGCug/L 0.19Antimony6<0.19
6020B P7J027911.0 10/19/17 0:32 EGCJug/L 0.031Arsenic100.14
6020B P7J027915.0 10/19/17 0:32 EGCug/L 0.97Barium10014
6020B P7J027911.0 10/19/17 0:32 EGCug/L 0.057Beryllium1<0.057
6020B P7J027911.0 10/19/17 0:32 EGCug/L 0.078Cadmium1<0.078
6020B P7J027911.0 10/19/17 0:32 EGCJug/L 0.19Chromium100.89
6020B P7J027911.0 10/19/17 0:32 EGCJug/L 0.0071Cobalt100.39
6020B P7J034315.0 10/20/17 0:20 EGCJug/L 0.22Copper101.1
6020B P7J027911.0 10/19/17 0:32 EGCJug/L 0.093Lead100.44
6020B P7J034312.0 10/20/17 0:20 EGCug/L 0.85Nickel50<0.85
6020B P7J027915.0 10/19/17 0:32 EGCug/L 0.63Selenium10<0.63
6020B P7J027915.0 10/19/17 0:32 EGCug/L 0.063Silver10<0.063
6020B P7J027911.0 10/19/17 0:32 EGCug/L 0.099Thallium5.5<0.099
6020B P7J027911010/19/17 0:32 EGCug/L 0.21Tin100<0.21
6020B P7J027911.0 10/19/17 0:32 EGCJug/L 0.10Vanadium250.76
6020B P7J027911010/19/17 0:32 EGCug/L 2.8Zinc1017
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 11:58KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0661,2-Dichloroethane 1<0.066
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-06
Prism Work Order: 7100243
Time Collected: 10/11/17 13:50
Time Submitted: 10/12/17 14:00
SW-02
50-02
SWSL
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 11:58KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 11:58KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 11:58KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 11:58KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 11:58KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 11:58KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 11:58KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 11:58KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.065Dibromomethane10<0.065
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 11:58KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 11:58KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 11:58KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 11:58KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 11:58KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 11:58KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 11:58KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 11:58KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-06
Prism Work Order: 7100243
Time Collected: 10/11/17 13:50
Time Submitted: 10/12/17 14:00
SW-02
50-02
SWSL
8260B P7J038511010/22/17 11:58KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 11:58KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 11:58KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 11:58KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 11:58KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 11:58KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 11:58KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 11:58KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12494 %4-Bromofluorobenzene
75-12995 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-07
Prism Work Order: 7100243
Time Collected: 10/11/17 00:00
Time Submitted: 10/12/17 14:00
Trip Blank
50-02
SWSL
Volatile Organic Compounds by GC/MS
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0511,1-Dichloropropylene 5<0.051
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.131,2,4-Trichlorobenzene 10<0.13
8260B P7J038512.0 10/22/17 6:50 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0541,3-Dichlorobenzene 5<0.054
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0431,3-Dichloropropane 1<0.043
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7J038512.0 10/22/17 6:50 KDMug/L 0.112,2-Dichloropropane 15<0.11
8260B P7J038515.0 10/22/17 6:50 KDMug/L 0.31Acetone100<0.31
8260B P7J038511010/22/17 6:50 KDMug/L 3.0Acetonitrile55<3.0
8260B P7J038512010/22/17 6:50 KDMug/L 0.20Acrolein53<0.20
8260B P7J038512010/22/17 6:50 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7J038511010/22/17 6:50 KDMug/L 0.75Allyl Chloride (3-Chloropropylene)10<0.75
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.048Benzene1<0.048
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.040Bromoform3<0.040
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.18Bromomethane10<0.18
8260B P7J038515.0 10/22/17 6:50 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.22Chloroethane10<0.22
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.076Chloroform5<0.076
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.079Chloromethane1<0.079
8260B P7J038511010/22/17 6:50 KDMug/L 0.86Chloroprene20<0.86
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 98
Laboratory Report
11/09/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street Project No.:
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7100243-07
Prism Work Order: 7100243
Time Collected: 10/11/17 00:00
Time Submitted: 10/12/17 14:00
Trip Blank
50-02
SWSL
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.065Dibromomethane10<0.065
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.11Dichlorodifluoromethane5<0.11
8260B P7J038511010/22/17 6:50 KDMug/L 0.26Ethyl Methacrylate 10<0.26
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7J038512.0 10/22/17 6:50 KDMug/L 0.16Hexachlorobutadiene10<0.16
8260B P7J038512010/22/17 6:50 KDMug/L 10Isobutyl alcohol 100<10
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7J038511010/22/17 6:50 KDMug/L 0.57Methacrylonitrile100<0.57
8260B P7J038515.0 10/22/17 6:50 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7J038515.0 10/22/17 6:50 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7J038515.0 10/22/17 6:50 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7J038515.0 10/22/17 6:50 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7J038511010/22/17 6:50 KDMug/L 0.27Methyl Methacrylate 30<0.27
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7J038511.0 10/22/17 6:50 KDMug/L 0.19Naphthalene10<0.19
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.044o-Xylene NE<0.044
8260B P7J038511010/22/17 6:50 KDMug/L 2.1Propionitrile (Ethyl Cyanide)150<2.1
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.047Styrene1<0.047
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7J038511010/22/17 6:50 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.044Toluene1<0.044
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7J038511010/22/17 6:50 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7J038512.0 10/22/17 6:50 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7J038510.50 10/22/17 6:50 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7J038511.5 10/22/17 6:50 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-12496 %4-Bromofluorobenzene
75-12995 %Dibromofluoromethane
77-12399 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
Blank (P7J0385-BLK1)Prepared: 10/21/17 Analyzed: 10/22/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
Acetone ug/LBRL5.0
Acetonitrile ug/LBRL10
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Allyl Chloride (3-Chloropropylene)ug/LBRL10
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
Chloroprene ug/LBRL10
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethyl Methacrylate ug/LBRL10
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isobutyl alcohol ug/LBRL20
m,p-Xylenes ug/LBRL1.0
Methacrylonitrile ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
Blank (P7J0385-BLK1)Prepared: 10/21/17 Analyzed: 10/22/17
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methyl Methacrylate ug/LBRL10
Methylene Chloride ug/LBRL1.0
Naphthalene ug/LBRL1.0
o-Xylene ug/LBRL0.50
Propionitrile (Ethyl Cyanide)ug/LBRL10
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9246.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9446.9
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.5
LCS (P7J0385-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 79-13498
1,1,1-Trichloroethane ug/L21.3 0.50 20.00 75-136107
1,1,2,2-Tetrachloroethane ug/L21.0 0.50 20.00 62-127105
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-140103
1,1-Dichloroethane ug/L20.2 0.50 20.00 78-130101
1,1-Dichloroethylene ug/L20.0 0.50 20.00 70-154100
1,1-Dichloropropylene ug/L20.9 0.50 20.00 71-136104
1,2,3-Trichloropropane ug/L20.9 1.0 20.00 71-127105
1,2,4-Trichlorobenzene ug/L19.8 1.0 20.00 66-13999
1,2-Dibromo-3-chloropropane ug/L18.8 2.0 20.00 63-13494
1,2-Dibromoethane ug/L21.3 0.50 20.00 77-135107
1,2-Dichlorobenzene ug/L20.3 0.50 20.00 78-128101
1,2-Dichloroethane ug/L20.5 0.50 20.00 68-131103
1,2-Dichloropropane ug/L20.4 0.50 20.00 77-130102
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 77-125101
1,3-Dichloropropane ug/L21.6 0.50 20.00 76-132108
1,4-Dichlorobenzene ug/L20.0 0.50 20.00 75-126100
2,2-Dichloropropane ug/L18.4 2.0 20.00 29-14992
Acetone ug/L41.1 5.0 40.00 40-166103
Acetonitrile ug/L19.0 10 20.00 70-13095
Acrolein ug/L37.8 20 40.00 70-13095
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
LCS (P7J0385-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
Acrylonitrile ug/L39.9 20 40.00 81-127100
Allyl Chloride (3-Chloropropylene)ug/L23.1 10 20.00 70-130116
Benzene ug/L20.4 0.50 20.00 77-128102
Bromochloromethane ug/L21.3 0.50 20.00 78-135107
Bromodichloromethane ug/L21.2 0.50 20.00 76-138106
Bromoform ug/L17.4 1.0 20.00 71-13587
Bromomethane ug/L14.0 1.0 20.00 41-16870
Carbon disulfide ug/L21.0 5.0 20.00 59-135105
Carbon Tetrachloride ug/L20.1 0.50 20.00 72-142100
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L18.7 0.50 20.00 57-14294
Chloroform ug/L19.8 0.50 20.00 77-13099
Chloromethane ug/L15.3 0.50 20.00 47-14577
Chloroprene ug/L19.4 10 20.00 70-13097
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 76-141104
cis-1,3-Dichloropropylene ug/L21.2 0.50 20.00 65-140106
Dibromochloromethane ug/L19.3 0.50 20.00 75-13496
Dibromomethane ug/L20.7 0.50 20.00 76-138104
Dichlorodifluoromethane ug/L19.3 1.0 20.00 28-16397
Ethyl Methacrylate ug/L19.3 10 20.00 70-13096
Ethylbenzene ug/L21.1 0.50 20.00 80-127105
Hexachlorobutadiene ug/L19.3 2.0 20.00 61-13496
Isobutyl alcohol ug/L20.9 20 20.00 70-130104
m,p-Xylenes ug/L44.3 1.0 40.00 77-133111
Methacrylonitrile ug/L19.1 10 20.00 70-13095
Methyl Butyl Ketone (2-Hexanone)ug/L21.8 5.0 20.00 64-137109
Methyl Ethyl Ketone (2-Butanone)ug/L19.9 5.0 20.00 71-13499
Methyl Iodide ug/L17.8 5.0 20.00 70-13089
Methyl Isobutyl Ketone ug/L21.3 5.0 20.00 69-134107
Methyl Methacrylate ug/L19.5 10 20.00 70-13097
Methylene Chloride ug/L18.4 1.0 20.00 73-13192
Naphthalene ug/L20.7 1.0 20.00 64-136103
o-Xylene ug/L21.3 0.50 20.00 78-128107
Propionitrile (Ethyl Cyanide)ug/L18.4 10 20.00 70-13092
Styrene ug/L20.0 0.50 20.00 78-129100
Tetrachloroethylene ug/L20.5 0.50 20.00 80-129102
Tetrahydrofuran ug/L19.9 10 20.00 70-13099
Toluene ug/L20.8 0.50 20.00 76-131104
trans-1,2-Dichloroethylene ug/L20.9 0.50 20.00 76-135104
trans-1,3-Dichloropropylene ug/L19.2 0.50 20.00 67-14096
trans-1,4-Dichloro-2-butene ug/L20.2 10 20.00 70-130101
Trichloroethylene ug/L20.8 0.50 20.00 77-133104
Trichlorofluoromethane ug/L20.2 0.50 20.00 62-148101
Vinyl acetate ug/L20.7 2.0 20.00 34-167104
Vinyl chloride ug/L20.4 0.50 20.00 57-141102
Xylenes, total ug/L65.6 1.5 60.00 77-133109
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
LCS (P7J0385-BS1)Prepared: 10/21/17 Analyzed: 10/22/17
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 8843.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9346.6
ug/L 50.00 77-123Surrogate: Toluene-d8 9145.4
LCS Dup (P7J0385-BSD1)Prepared: 10/21/17 Analyzed: 10/22/17
1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 2079-13498 0.2
1,1,1-Trichloroethane ug/L21.0 0.50 20.00 2075-136105 2
1,1,2,2-Tetrachloroethane ug/L21.5 0.50 20.00 2062-127108 3
1,1,2-Trichloroethane ug/L21.1 0.50 20.00 2070-140106 2
1,1-Dichloroethane ug/L20.1 0.50 20.00 2078-130101 0.7
1,1-Dichloroethylene ug/L20.0 0.50 20.00 2070-154100 0.1
1,1-Dichloropropylene ug/L20.6 0.50 20.00 2071-136103 1
1,2,3-Trichloropropane ug/L21.2 1.0 20.00 2071-127106 1
1,2,4-Trichlorobenzene ug/L20.0 1.0 20.00 2066-139100 0.8
1,2-Dibromo-3-chloropropane ug/L19.3 2.0 20.00 2063-13496 3
1,2-Dibromoethane ug/L21.3 0.50 20.00 2077-135107 0.05
1,2-Dichlorobenzene ug/L20.8 0.50 20.00 2078-128104 3
1,2-Dichloroethane ug/L20.9 0.50 20.00 2068-131104 2
1,2-Dichloropropane ug/L20.4 0.50 20.00 2077-130102 0.1
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 2077-125102 0.3
1,3-Dichloropropane ug/L21.7 0.50 20.00 2076-132108 0.3
1,4-Dichlorobenzene ug/L20.3 0.50 20.00 2075-126101 2
2,2-Dichloropropane ug/L18.5 2.0 20.00 2029-14992 0.2
Acetone ug/L42.4 5.0 40.00 2040-166106 3
Acetonitrile ug/L18.6 10 20.00 2070-13093 2
Acrolein ug/L39.0 20 40.00 2070-13098 3
Acrylonitrile ug/L40.7 20 40.00 2081-127102 2
Allyl Chloride (3-Chloropropylene)ug/L21.1 10 20.00 2070-130105 9
Benzene ug/L20.4 0.50 20.00 2077-128102 0.3
Bromochloromethane ug/L21.3 0.50 20.00 2078-135107 0.09
Bromodichloromethane ug/L21.3 0.50 20.00 2076-138106 0.5
Bromoform ug/L17.6 1.0 20.00 2071-13588 1
Bromomethane ug/L13.9 1.0 20.00 2041-16869 0.6
Carbon disulfide ug/L20.9 5.0 20.00 2059-135105 0.3
Carbon Tetrachloride ug/L19.9 0.50 20.00 2072-142100 0.8
Chlorobenzene ug/L20.3 0.50 20.00 2078-119102 1
Chloroethane ug/L18.2 0.50 20.00 2057-14291 3
Chloroform ug/L19.7 0.50 20.00 2077-13099 0.3
Chloromethane ug/L14.8 0.50 20.00 2047-14574 4
Chloroprene ug/L17.6 10 20.00 2070-13088 10
cis-1,2-Dichloroethylene ug/L20.7 0.50 20.00 2076-141103 0.3
cis-1,3-Dichloropropylene ug/L21.3 0.50 20.00 2065-140107 0.8
Dibromochloromethane ug/L19.2 0.50 20.00 2075-13496 0.7
Dibromomethane ug/L20.8 0.50 20.00 2076-138104 0.1
Dichlorodifluoromethane ug/L19.0 1.0 20.00 2028-16395 2
Ethyl Methacrylate ug/L18.5 10 20.00 2070-13093 4
Ethylbenzene ug/L21.0 0.50 20.00 2080-127105 0.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7J0385 - 5030B
LCS Dup (P7J0385-BSD1)Prepared: 10/21/17 Analyzed: 10/22/17
Hexachlorobutadiene ug/L20.7 2.0 20.00 2061-134104 7
Isobutyl alcohol ug/L19.0 20 20.00 20 J70-13095 10
m,p-Xylenes ug/L43.8 1.0 40.00 2077-133109 1
Methacrylonitrile ug/L18.2 10 20.00 2070-13091 4
Methyl Butyl Ketone (2-Hexanone)ug/L21.8 5.0 20.00 2064-137109 0
Methyl Ethyl Ketone (2-Butanone)ug/L21.2 5.0 20.00 2071-134106 7
Methyl Iodide ug/L17.6 5.0 20.00 2070-13088 1
Methyl Isobutyl Ketone ug/L21.8 5.0 20.00 2069-134109 2
Methyl Methacrylate ug/L18.7 10 20.00 2070-13093 4
Methylene Chloride ug/L18.4 1.0 20.00 2073-13192 0.3
Naphthalene ug/L20.6 1.0 20.00 2064-136103 0.1
o-Xylene ug/L21.0 0.50 20.00 2078-128105 1
Propionitrile (Ethyl Cyanide)ug/L17.2 10 20.00 2070-13086 7
Styrene ug/L19.2 0.50 20.00 2078-12996 4
Tetrachloroethylene ug/L20.4 0.50 20.00 2080-129102 0.5
Tetrahydrofuran ug/L20.1 10 20.00 2070-130101 1
Toluene ug/L20.8 0.50 20.00 2076-131104 0.05
trans-1,2-Dichloroethylene ug/L21.0 0.50 20.00 2076-135105 0.5
trans-1,3-Dichloropropylene ug/L19.7 0.50 20.00 2067-14099 3
trans-1,4-Dichloro-2-butene ug/L17.1 10 20.00 2070-13086 17
Trichloroethylene ug/L20.4 0.50 20.00 2077-133102 2
Trichlorofluoromethane ug/L20.4 0.50 20.00 2062-148102 0.7
Vinyl acetate ug/L20.9 2.0 20.00 2034-167104 0.6
Vinyl chloride ug/L19.9 0.50 20.00 2057-14199 3
Xylenes, total ug/L64.8 1.5 60.00 2077-133108 1
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9045.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9447.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9145.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
Blank (P7J0283-BLK1)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4,5-Tetrachlorobenzene ug/LBRL10
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3,5-Trinitrobenzene ug/LBRL20
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1,4-Naphthoquinone ug/LBRL10
1,4-Phenylenediamine ug/LBRL10
1-Naphthylamine ug/LBRL10
2,3,4,6-Tetrachlorophenol ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dichlorophenol ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Acetylaminofluorene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Naphthylamine ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3’-Dichlorobenzidine ug/LBRL10
3,3·-Dimethylbenzidine ug/LBRL20
3/4-Methylphenol ug/LBRL10
3-Methylcholanthrene ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Aminobiphenyl ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
5-Nitro-o-toluidine ug/LBRL10
7,12-Dimethylbenz(a)anthracene ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Acetophenone ug/LBRL10
Anthracene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
Blank (P7J0283-BLK1)Prepared: 10/17/17 Analyzed: 11/06/17
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(b&k)fluoranthene ug/LBRL20
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chlorobenzilate ug/LBRL10
Chrysene ug/LBRL10
Diallate ug/LBRL20
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethoate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
Diphenylamine ug/LBRL10
Disulfoton ug/LBRL20
Ethyl Methanesulfonate ug/LBRL10
Famphur ug/LBRL20
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Hexachloropropene ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isodrin ug/LBRL10
Isophorone ug/LBRL10
Isosafrole ug/LBRL10
Kepone ug/LBRL20
Methapyrilene ug/LBRL100
Methyl Methanesulfonate ug/LBRL20
Methyl parathion ug/LBRL20
Nitrobenzene ug/LBRL10
N-Nitrosodibutylamine ug/LBRL10
N-Nitrosodiethylamine ug/LBRL10
N-Nitrosodimethylamine ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
Blank (P7J0283-BLK1)Prepared: 10/17/17 Analyzed: 11/06/17
N-Nitrosomethylethylamine ug/LBRL10
N-Nitrosopiperidine ug/LBRL10
N-Nitrosopyrrolidine ug/LBRL10
O,O,O-Triethyl phosphorothioate ug/LBRL10
o-Toluidine ug/LBRL10
Parathion ug/LBRL10
p-Dimethylaminoazobenzene ug/LBRL20
Pentachlorobenzene ug/LBRL10
Pentachloronitrobenzene ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenacetin ug/LBRL20
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Phorate ug/LBRL10
Pronamide ug/LBRL10
Pyrene ug/LBRL10
Safrole ug/LBRL10
Thionazin ug/LBRL10
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7336.3
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5050.0
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7135.6
ug/L 100.0 11-52Surrogate: Phenol-d5 3130.8
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8040.2
LCS (P7J0283-BS1)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4-Trichlorobenzene ug/L27.1 10 50.00 29-12654
1,2-Dichlorobenzene ug/L29.2 10 50.00 32-11158
1,3-Dichlorobenzene ug/L28.4 10 50.00 28-11057
1,4-Dichlorobenzene ug/L27.5 10 50.00 29-11255
2,4,5-Trichlorophenol ug/L43.5 10 50.00 53-12387
2,4,6-Trichlorophenol ug/L41.6 10 50.00 50-12583
2,4-Dichlorophenol ug/L37.5 10 50.00 47-12175
2,4-Dimethylphenol ug/L30.3 10 50.00 31-12461
2,4-Dinitrophenol ug/L28.5 10 50.00 23-14357
2,4-Dinitrotoluene ug/L43.2 10 50.00 57-12886
2,6-Dinitrotoluene ug/L44.3 10 50.00 57-12489
2-Chloronaphthalene ug/L35.8 10 50.00 40-11672
2-Chlorophenol ug/L40.3 10 50.00 38-11781
2-Methylnaphthalene ug/L31.1 10 50.00 40-12162
2-Methylphenol ug/L37.4 10 50.00 30-11775
2-Nitroaniline ug/L41.6 10 50.00 55-12783
2-Nitrophenol ug/L36.8 10 50.00 47-12374
3,3’-Dichlorobenzidine ug/L44.6 10 50.00 27-12989
3/4-Methylphenol ug/L30.6 10 50.00 29-11061
3-Nitroaniline ug/L43.3 10 50.00 41-12887
4,6-Dinitro-2-methylphenol ug/L37.0 10 50.00 44-13774
4-Bromophenyl phenyl ether ug/L42.0 10 50.00 55-12484
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS (P7J0283-BS1)Prepared: 10/17/17 Analyzed: 11/06/17
4-Chloro-3-methylphenol ug/L37.8 10 50.00 52-11976
4-Chloroaniline ug/L38.7 10 50.00 33-11777
4-Chlorophenyl phenyl ether ug/L40.3 10 50.00 53-12181
4-Nitroaniline ug/L45.9 10 50.00 45-13592
4-Nitrophenol ug/L17.8 10 50.00 10-7736
Acenaphthene ug/L39.3 10 50.00 47-12279
Acenaphthylene ug/L42.5 10 50.00 41-13085
Acetophenone ug/L42.9 10 50.00 46-11886
Anthracene ug/L47.6 10 50.00 57-12395
Benzo(a)anthracene ug/L45.6 10 50.00 58-12591
Benzo(a)pyrene ug/L43.0 10 50.00 54-12886
Benzo(b)fluoranthene ug/L41.3 10 50.00 53-13183
Benzo(g,h,i)perylene ug/L41.8 10 50.00 50-13484
Benzo(k)fluoranthene ug/L47.1 10 50.00 57-12994
Benzyl alcohol ug/L32.6 10 50.00 31-11265
bis(2-Chloroethoxy)methane ug/L39.1 10 50.00 48-12078
Bis(2-Chloroethyl)ether ug/L38.6 10 50.00 43-11877
Bis(2-chloroisopropyl)ether ug/L37.5 10 50.00 37-13075
Bis(2-Ethylhexyl)phthalate ug/L45.7 10 50.00 55-13591
Butyl benzyl phthalate ug/L44.3 10 50.00 53-13489
Chrysene ug/L45.4 10 50.00 59-12391
Dibenzo(a,h)anthracene ug/L15.3 10 50.00 L51-13431
Dibenzofuran ug/L40.0 10 50.00 53-11880
Diethyl phthalate ug/L43.3 10 50.00 56-12587
Dimethyl phthalate ug/L42.1 10 50.00 45-12784
Di-n-butyl phthalate ug/L45.6 10 50.00 59-12791
Di-n-octyl phthalate ug/L43.4 10 50.00 51-14087
Fluoranthene ug/L46.6 10 50.00 57-12893
Fluorene ug/L43.0 10 50.00 52-12486
Hexachlorobenzene ug/L43.5 10 50.00 53-12587
Hexachlorobutadiene ug/L26.4 10 50.00 22-12453
Hexachlorocyclopentadiene ug/L26.3 10 50.00 32-11753
Hexachloroethane ug/L27.6 10 50.00 21-11555
Indeno(1,2,3-cd)pyrene ug/L44.6 10 50.00 52-13489
Isophorone ug/L37.7 10 50.00 42-12475
Nitrobenzene ug/L34.2 10 50.00 45-12168
N-Nitrosodimethylamine ug/L28.2 10 50.00 10-11956
N-Nitroso-di-n-propylamine ug/L41.9 10 50.00 49-11984
N-Nitrosodiphenylamine ug/L53.1 10 50.00 51-123106
Pentachlorophenol ug/L38.0 10 50.00 35-13876
Phenanthrene ug/L47.0 10 50.00 59-12094
Phenol ug/L18.2 10 50.00 12-5836
Pyrene ug/L46.5 10 50.00 57-12693
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8341.4
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5554.8
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7236.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS (P7J0283-BS1)Prepared: 10/17/17 Analyzed: 11/06/17
ug/L 100.0 11-52Surrogate: Phenol-d5 3635.7
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8844.0
LCS (P7J0283-BS2)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4,5-Tetrachlorobenzene ug/L30.8 10 50.00 35-12162
1,3,5-Trinitrobenzene ug/L39.2 20 50.00 41-13778
1,4-Naphthoquinone ug/L41.6 10 50.00 45-13583
1,4-Phenylenediamine ug/L42.7 10 50.00 45-13585
1-Naphthylamine ug/L37.2 10 50.00 24-12474
2,3,4,6-Tetrachlorophenol ug/L41.5 10 50.00 50-12883
2,6-Dichlorophenol ug/L39.9 10 50.00 50-11880
2-Acetylaminofluorene ug/L43.7 10 50.00 60-13887
2-Naphthylamine ug/L35.2 10 50.00 45-13570
3,3·-Dimethylbenzidine ug/L24.3 20 50.00 45-13549
3-Methylcholanthrene ug/L38.9 10 50.00 56-13378
4-Aminobiphenyl ug/L38.3 10 50.00 45-13577
5-Nitro-o-toluidine ug/L43.6 10 50.00 38-12687
7,12-Dimethylbenz(a)anthracene ug/L42.6 10 50.00 61-13385
Acetophenone ug/L37.5 10 50.00 46-11875
Chlorobenzilate ug/L41.0 10 50.00 58-15082
Diallate ug/L39.6 20 50.00 45-13579
Dimethoate ug/L41.1 10 50.00 45-13582
Diphenylamine ug/L40.0 10 50.00 55-11180
Disulfoton ug/L38.2 20 50.00 55-13076
Ethyl Methanesulfonate ug/L36.7 10 50.00 62-11873
Famphur ug/L30.2 20 50.00 45-13560
Hexachloropropene ug/L21.0 10 50.00 L45-13542
Isodrin ug/L39.0 10 50.00 68-12878
Isosafrole ug/L35.1 10 50.00 56-12670
Kepone ug/L25.0 20 50.00 45-13550
Methapyrilene ug/LBRL100 50.00 L45-135
Methyl Methanesulfonate ug/L24.4 20 50.00 33-10749
Methyl parathion ug/L42.8 20 50.00 45-15986
N-Nitrosodibutylamine ug/L39.2 10 50.00 60-12178
N-Nitrosodiethylamine ug/L38.4 10 50.00 43-12177
N-Nitrosomethylethylamine ug/L38.6 10 50.00 41-11777
N-Nitrosopiperidine ug/L37.7 10 50.00 56-12175
N-Nitrosopyrrolidine ug/L37.6 10 50.00 48-11375
O,O,O-Triethyl phosphorothioate ug/L36.7 10 50.00 60-11973
o-Toluidine ug/L38.9 10 50.00 30-11078
Parathion ug/L41.3 10 50.00 66-14083
p-Dimethylaminoazobenzene ug/L40.2 20 50.00 45-13580
Pentachlorobenzene ug/L35.8 10 50.00 59-12372
Pentachloronitrobenzene ug/L41.6 10 50.00 54-13583
Phenacetin ug/L42.5 20 50.00 71-12485
Phorate ug/L40.0 10 50.00 38-13980
Pronamide ug/L41.0 10 50.00 65-12982
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS (P7J0283-BS2)Prepared: 10/17/17 Analyzed: 11/06/17
Safrole ug/L37.3 10 50.00 61-11975
Thionazin ug/L42.1 10 50.00 72-13284
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7336.6
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5050.1
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6833.8
ug/L 100.0 11-52Surrogate: Phenol-d5 3231.9
ug/L 50.00 50-134Surrogate: Terphenyl-d14 7437.2
LCS Dup (P7J0283-BSD1)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4-Trichlorobenzene ug/L23.7 10 50.00 2029-12647 13
1,2-Dichlorobenzene ug/L25.3 10 50.00 2032-11151 14
1,3-Dichlorobenzene ug/L24.2 10 50.00 2028-11048 16
1,4-Dichlorobenzene ug/L24.5 10 50.00 2029-11249 12
2,4,5-Trichlorophenol ug/L36.7 10 50.00 2053-12373 17
2,4,6-Trichlorophenol ug/L34.2 10 50.00 2050-12568 20
2,4-Dichlorophenol ug/L32.1 10 50.00 2047-12164 15
2,4-Dimethylphenol ug/L31.9 10 50.00 2031-12464 5
2,4-Dinitrophenol ug/L24.6 10 50.00 2023-14349 15
2,4-Dinitrotoluene ug/L36.2 10 50.00 2057-12872 18
2,6-Dinitrotoluene ug/L36.9 10 50.00 2057-12474 18
2-Chloronaphthalene ug/L30.0 10 50.00 2040-11660 18
2-Chlorophenol ug/L36.0 10 50.00 2038-11772 11
2-Methylnaphthalene ug/L26.4 10 50.00 2040-12153 16
2-Methylphenol ug/L34.1 10 50.00 2030-11768 9
2-Nitroaniline ug/L36.0 10 50.00 2055-12772 14
2-Nitrophenol ug/L31.2 10 50.00 2047-12362 16
3,3’-Dichlorobenzidine ug/L37.7 10 50.00 2027-12975 17
3/4-Methylphenol ug/L27.1 10 50.00 2029-11054 12
3-Nitroaniline ug/L39.0 10 50.00 2041-12878 10
4,6-Dinitro-2-methylphenol ug/L30.0 10 50.00 20 D44-13760 21
4-Bromophenyl phenyl ether ug/L34.9 10 50.00 2055-12470 19
4-Chloro-3-methylphenol ug/L32.6 10 50.00 2052-11965 15
4-Chloroaniline ug/L36.3 10 50.00 2033-11773 6
4-Chlorophenyl phenyl ether ug/L34.1 10 50.00 2053-12168 17
4-Nitroaniline ug/L39.9 10 50.00 2045-13580 14
4-Nitrophenol ug/L17.1 10 50.00 2010-7734 4
Acenaphthene ug/L32.6 10 50.00 2047-12265 19
Acenaphthylene ug/L35.0 10 50.00 2041-13070 19
Acetophenone ug/L36.3 10 50.00 2046-11873 17
Anthracene ug/L39.9 10 50.00 2057-12380 18
Benzo(a)anthracene ug/L38.0 10 50.00 2058-12576 18
Benzo(a)pyrene ug/L35.2 10 50.00 2054-12870 20
Benzo(b)fluoranthene ug/L34.5 10 50.00 2053-13169 18
Benzo(g,h,i)perylene ug/L34.4 10 50.00 2050-13469 19
Benzo(k)fluoranthene ug/L38.5 10 50.00 2057-12977 20
Benzyl alcohol ug/L29.5 10 50.00 2031-11259 10
bis(2-Chloroethoxy)methane ug/L33.2 10 50.00 2048-12066 16
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS Dup (P7J0283-BSD1)Prepared: 10/17/17 Analyzed: 11/06/17
Bis(2-Chloroethyl)ether ug/L33.7 10 50.00 2043-11867 13
Bis(2-chloroisopropyl)ether ug/L31.8 10 50.00 2037-13064 17
Bis(2-Ethylhexyl)phthalate ug/L37.9 10 50.00 2055-13576 19
Butyl benzyl phthalate ug/L37.1 10 50.00 2053-13474 18
Chrysene ug/L37.8 10 50.00 2059-12376 18
Dibenzo(a,h)anthracene ug/L15.8 10 50.00 20 L51-13432 3
Dibenzofuran ug/L33.3 10 50.00 2053-11867 18
Diethyl phthalate ug/L36.4 10 50.00 2056-12573 17
Dimethyl phthalate ug/L35.6 10 50.00 2045-12771 17
Di-n-butyl phthalate ug/L37.9 10 50.00 2059-12776 19
Di-n-octyl phthalate ug/L35.9 10 50.00 2051-14072 19
Fluoranthene ug/L38.6 10 50.00 2057-12877 19
Fluorene ug/L36.2 10 50.00 2052-12472 17
Hexachlorobenzene ug/L36.1 10 50.00 2053-12572 19
Hexachlorobutadiene ug/L23.2 10 50.00 2022-12446 13
Hexachlorocyclopentadiene ug/L22.3 10 50.00 2032-11745 17
Hexachloroethane ug/L23.5 10 50.00 2021-11547 16
Indeno(1,2,3-cd)pyrene ug/L36.8 10 50.00 2052-13474 19
Isophorone ug/L31.9 10 50.00 2042-12464 17
Nitrobenzene ug/L29.7 10 50.00 2045-12159 14
N-Nitrosodimethylamine ug/L26.3 10 50.00 2010-11953 7
N-Nitroso-di-n-propylamine ug/L34.6 10 50.00 2049-11969 19
N-Nitrosodiphenylamine ug/L44.8 10 50.00 2051-12390 17
Pentachlorophenol ug/L31.6 10 50.00 2035-13863 19
Phenanthrene ug/L39.6 10 50.00 2059-12079 17
Phenol ug/L16.5 10 50.00 2012-5833 10
Pyrene ug/L38.7 10 50.00 2057-12677 18
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 6934.3
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5151.3
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6331.3
ug/L 100.0 11-52Surrogate: Phenol-d5 3231.8
ug/L 50.00 50-134Surrogate: Terphenyl-d14 7537.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS Dup (P7J0283-BSD2)Prepared: 10/17/17 Analyzed: 11/06/17
1,2,4,5-Tetrachlorobenzene ug/L27.4 10 50.00 2035-12155 12
1,3,5-Trinitrobenzene ug/L45.7 20 50.00 2041-13791 15
1,4-Naphthoquinone ug/L51.9 10 50.00 20 D45-135104 22
1,4-Phenylenediamine ug/L45.5 10 50.00 2045-13591 6
1-Naphthylamine ug/L32.9 10 50.00 2024-12466 12
2,3,4,6-Tetrachlorophenol ug/L47.1 10 50.00 2050-12894 13
2,6-Dichlorophenol ug/L43.4 10 50.00 2050-11887 9
2-Acetylaminofluorene ug/L47.5 10 50.00 2060-13895 8
2-Naphthylamine ug/L37.5 10 50.00 2045-13575 6
3,3·-Dimethylbenzidine ug/L20.3 20 50.00 20 L245-13541 18
3-Methylcholanthrene ug/L41.9 10 50.00 2056-13384 7
4-Aminobiphenyl ug/L40.8 10 50.00 2045-13582 6
5-Nitro-o-toluidine ug/L47.5 10 50.00 2038-12695 9
7,12-Dimethylbenz(a)anthracene ug/L46.7 10 50.00 2061-13393 9
Acetophenone ug/L40.6 10 50.00 2046-11881 8
Chlorobenzilate ug/L45.2 10 50.00 2058-15090 10
Diallate ug/L44.3 20 50.00 2045-13589 11
Dimethoate ug/L45.7 10 50.00 2045-13591 11
Diphenylamine ug/L43.6 10 50.00 2055-11187 9
Disulfoton ug/L41.7 20 50.00 2055-13083 9
Ethyl Methanesulfonate ug/L41.3 10 50.00 2062-11883 12
Famphur ug/L34.4 20 50.00 20 L245-13569 13
Hexachloropropene ug/L18.1 10 50.00 20 L45-13536 15
Isodrin ug/L41.1 10 50.00 2068-12882 5
Isosafrole ug/L36.7 10 50.00 2056-12673 4
Kepone ug/L26.7 20 50.00 2045-13553 7
Methapyrilene ug/LBRL100 50.00 20 L45-135
Methyl Methanesulfonate ug/L26.6 20 50.00 2033-10753 9
Methyl parathion ug/L47.4 20 50.00 2045-15995 10
N-Nitrosodibutylamine ug/L42.2 10 50.00 2060-12184 7
N-Nitrosodiethylamine ug/L42.3 10 50.00 2043-12185 10
N-Nitrosomethylethylamine ug/L42.0 10 50.00 2041-11784 8
N-Nitrosopiperidine ug/L40.5 10 50.00 2056-12181 7
N-Nitrosopyrrolidine ug/L40.7 10 50.00 2048-11381 8
O,O,O-Triethyl phosphorothioate ug/L39.4 10 50.00 2060-11979 7
o-Toluidine ug/L38.1 10 50.00 2030-11076 2
Parathion ug/L46.6 10 50.00 2066-14093 12
p-Dimethylaminoazobenzene ug/L44.9 20 50.00 2045-13590 11
Pentachlorobenzene ug/L31.8 10 50.00 2059-12364 12
Pentachloronitrobenzene ug/L44.5 10 50.00 2054-13589 7
Phenacetin ug/L45.8 20 50.00 2071-12492 7
Phorate ug/L43.4 10 50.00 2038-13987 8
Pronamide ug/L44.7 10 50.00 2065-12989 9
Safrole ug/L39.1 10 50.00 2061-11978 5
Thionazin ug/L46.3 10 50.00 2072-13293 9
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7537.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7J0283 - 3510C MS
LCS Dup (P7J0283-BSD2)Prepared: 10/17/17 Analyzed: 11/06/17
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5555.3
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7336.7
ug/L 100.0 11-52Surrogate: Phenol-d5 3635.5
ug/L 50.00 50-134Surrogate: Terphenyl-d14 8542.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7J0256 - 3005A
Blank (P7J0256-BLK1)Prepared: 10/16/17 Analyzed: 10/18/17
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L1.00 5.0 J
Beryllium ug/L0.133 1.0 J
Cadmium ug/LBRL1.0
Chromium ug/L0.200 1.0 J
Cobalt ug/LBRL1.0
Copper ug/L0.474 5.0 J
Lead ug/L0.139 1.0 J
Nickel ug/LBRL10
Selenium ug/LBRL5.0
Silver ug/LBRL5.0
Thallium ug/LBRL1.0
Tin ug/LBRL5.0
Vanadium ug/L0.141 1.0 J
Zinc ug/L4.34 10 J
LCS (P7J0256-BS1)Prepared: 10/16/17 Analyzed: 10/18/17
Antimony ug/L1041.0 100.0 80-120104
Arsenic ug/L99.6 1.0 100.0 80-120100
Barium ug/L1115.0 100.0 80-120111
Beryllium ug/L95.2 1.0 100.0 80-12095
Cadmium ug/L1031.0 100.0 80-120103
Chromium ug/L1001.0 100.0 80-120100
Cobalt ug/L1051.0 100.0 80-120105
Copper ug/L1055.0 100.0 80-120105
Lead ug/L1041.0 100.0 80-120104
Nickel ug/L10410 100.0 80-120104
Selenium ug/L1005.0 100.0 80-120100
Silver ug/L98.9 5.0 100.0 80-12099
Thallium ug/L1051.0 100.0 80-120105
Tin ug/L1065.0 100.0 80-120106
Vanadium ug/L98.7 1.0 100.0 80-12099
Zinc ug/L10410 100.0 80-120104
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7J0279 - 3005A
Blank (P7J0279-BLK1)Prepared: 10/17/17 Analyzed: 10/18/17
Antimony ug/LBRL1.0
Arsenic ug/L0.0490 1.0 J
Barium ug/LBRL5.0
Beryllium ug/L0.0600 1.0 J
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Cobalt ug/L0.0130 1.0 J
Lead ug/L0.0950 1.0 J
Selenium ug/LBRL5.0
Silver ug/LBRL5.0
Thallium ug/LBRL1.0
Tin ug/LBRL10
Vanadium ug/LBRL1.0
Zinc ug/L3.03 10 J
LCS (P7J0279-BS1)Prepared: 10/17/17 Analyzed: 10/18/17
Antimony ug/L1061.0 100.0 80-120106
Arsenic ug/L1021.0 100.0 80-120102
Barium ug/L1095.0 100.0 80-120109
Beryllium ug/L1041.0 100.0 80-120104
Cadmium ug/L1091.0 100.0 80-120109
Chromium ug/L1031.0 100.0 80-120103
Cobalt ug/L1081.0 100.0 80-120108
Lead ug/L1091.0 100.0 80-120109
Selenium ug/L1035.0 100.0 80-120103
Silver ug/L1095.0 100.0 80-120109
Thallium ug/L1081.0 100.0 80-120108
Tin ug/L10910 100.0 80-120109
Vanadium ug/L1021.0 100.0 80-120102
Zinc ug/L111 10 100.0 80-120111
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7J0343 - 3005A
Blank (P7J0343-BLK1)Prepared & Analyzed: 10/19/17
Copper ug/L0.749 5.0 J
Nickel ug/LBRL2.0
LCS (P7J0343-BS1)Prepared & Analyzed: 10/19/17
Copper ug/L1095.0 100.0 80-120109
Nickel ug/L1102.0 100.0 80-120110
Batch P7J0406 - 7470A
Blank (P7J0406-BLK1)Prepared & Analyzed: 10/23/17
Mercury ug/LBRL0.20
LCS (P7J0406-BS1)Prepared & Analyzed: 10/23/17
Mercury ug/L9.13 0.20 9.375 80-12097
Matrix Spike (P7J0406-MS1)Prepared & Analyzed: 10/23/17 Source: 7100243-01
Mercury ug/L8.41 0.20 9.375 BRL 80-12090
Matrix Spike Dup (P7J0406-MSD1)Prepared & Analyzed: 10/23/17 Source: 7100243-01
Mercury ug/L8.23 0.20 9.375 BRL 2080-12088 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7J0239 - NO PREP
LCS (P7J0239-BS1)Prepared & Analyzed: 10/12/17
Chloride ug/L396001000 40000 80-12099
Nitrate as N ug/L3900100 4000 80-12098
Sulfate ug/L403001000 40000 80-120101
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7J0220 - NO PREP
Blank (P7J0220-BLK1)Prepared & Analyzed: 10/12/17
Biochemical Oxygen Demand ug/L1002000 J
LCS (P7J0220-BS1)Prepared & Analyzed: 10/12/17
Biochemical Oxygen Demand ug/L1970002000 198000 84.6-115.4100
Batch P7J0238 - NO PREP
Blank (P7J0238-BLK1)Prepared & Analyzed: 10/12/17
Ferrous Iron ug/LBRL200
LCS (P7J0238-BS1)Prepared & Analyzed: 10/12/17
Ferrous Iron ug/L2000200 2000 90-110100
Matrix Spike (P7J0238-MS1)Prepared & Analyzed: 10/12/17 Source: 7100243-02
Ferrous Iron ug/L2030200 2000 37.0 80-120100
Matrix Spike Dup (P7J0238-MSD1)Prepared & Analyzed: 10/12/17 Source: 7100243-02
Ferrous Iron ug/L2020200 2000 37.0 2080-12099 0.3
Batch P7J0300 - NO PREP
Blank (P7J0300-BLK1)Prepared & Analyzed: 10/18/17
Chemical Oxygen Demand ug/LBRL50000
LCS (P7J0300-BS1)Prepared & Analyzed: 10/18/17
Chemical Oxygen Demand ug/L49000051000 505100 90-11097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7J0300 - NO PREP
Matrix Spike (P7J0300-MS2)Prepared & Analyzed: 10/18/17 Source: 7100243-01
Chemical Oxygen Demand ug/L50500051000 505100 BRL 80-120100
Matrix Spike Dup (P7J0300-MSD2)Prepared & Analyzed: 10/18/17 Source: 7100243-01
Chemical Oxygen Demand ug/L48900051000 505100 BRL 2080-12097 3
Batch P7J0317 - SM4500-S C
Blank (P7J0317-BLK1)Prepared & Analyzed: 10/18/17
Sulfide ug/LBRL2000
LCS (P7J0317-BS1)Prepared & Analyzed: 10/18/17
Sulfide ug/L9600 2000 10000 70-13096
Batch P7J0333 - SM4500-CN C
Blank (P7J0333-BLK1)Prepared & Analyzed: 10/19/17
Cyanide ug/L1.40 5.0 J
LCS (P7J0333-BS1)Prepared & Analyzed: 10/19/17
Cyanide ug/L96.4 5.0 100.0 85-11596
Matrix Spike (P7J0333-MS1)Prepared & Analyzed: 10/19/17 Source: 7100243-01
Cyanide ug/L82.1 5.0 100.0 1.10 80-12081
Matrix Spike Dup (P7J0333-MSD1)Prepared & Analyzed: 10/19/17 Source: 7100243-01
Cyanide ug/L79.2 5.0 100.0 1.10 20 M80-12078 4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 98
11/9/17
Level II QC Report
231 Haywood Street Project No: 50-02
Project: Jackson Cty Landfill (Permit
50-02)
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7100243
Time Submitted: 10/12/2017 2:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7J0369 - NO PREP
Blank (P7J0369-BLK1)Prepared & Analyzed: 10/20/17
Total Alkalinity to pH 4.5 ug/LBRL5000
LCS (P7J0369-BS1)Prepared & Analyzed: 10/20/17
Total Alkalinity to pH 4.5 ug/L2540005000 250000 90-110102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 98
Sample Extraction Data
Prep Method: SM4500-CN C
Lab Number Batch Date/TimeInitialFinal
P7J03337100243-01 10/19/17 6:3050 50mL mL
P7J03337100243-02 10/19/17 6:3050 50mL mL
P7J03337100243-03 10/19/17 6:3050 50mL mL
P7J03337100243-04 10/19/17 6:3050 50mL mL
Prep Method: SM4500-S C
Lab Number Batch Date/TimeInitialFinal
P7J03177100243-01 10/18/17 11:55200 200mL mL
P7J03177100243-02 10/18/17 12:20200 200mL mL
P7J03177100243-03 10/18/17 12:20200 200mL mL
P7J03177100243-04 10/18/17 12:20200 200mL mL
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P7J02837100243-01 10/17/17 9:528401mL mL
P7J02837100243-01 10/17/17 9:528401mL mL
P7J02837100243-02 10/17/17 9:529301mL mL
P7J02837100243-02 10/17/17 9:529301mL mL
P7J02837100243-03 10/17/17 13:157601mL mL
P7J02837100243-03 10/17/17 13:157601mL mL
P7J02837100243-04 10/17/17 13:156501mL mL
P7J02837100243-04 10/17/17 13:156501mL mL
P7J02837100243-05 10/17/17 13:159701mL mL
P7J02837100243-05 10/17/17 13:159701mL mL
P7J02837100243-06 10/17/17 13:158301mL mL
P7J02837100243-06 10/17/17 13:158301mL mL
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7J02567100243-01 10/16/17 8:1550 50mL mL
P7J02567100243-02 10/16/17 8:1550 50mL mL
P7J02567100243-03 10/16/17 8:1550 50mL mL
P7J02567100243-04 10/16/17 8:1550 50mL mL
P7J02797100243-05 10/17/17 9:4150 50mL mL
P7J03437100243-05 10/19/17 9:1050 50mL mL
P7J02797100243-06 10/17/17 9:4150 50mL mL
P7J03437100243-06 10/19/17 9:1050 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7J04067100243-01 10/23/17 9:5020 30mL mL
P7J04067100243-02 10/23/17 9:5020 30mL mL
P7J04067100243-03 10/23/17 9:5020 30mL mL
P7J04067100243-04 10/23/17 9:5020 30mL mL
P7J04067100243-05 10/23/17 9:5020 30mL mL
P7J04067100243-06 10/23/17 9:5020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7J03857100243-01 10/21/17 10:2410 10mL mL
P7J03857100243-02 10/21/17 10:2410 10mL mL
P7J03857100243-03 10/21/17 10:2410 10mL mL
P7J03857100243-04 10/21/17 10:2410 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 98
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7J03857100243-05 10/21/17 10:2410 10mL mL
P7J03857100243-06 10/21/17 10:2410 10mL mL
P7J03857100243-07 10/21/17 10:2410 10mL mL
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Analysis
7100243-01 TOC (Sub)
7100243-02 TOC (Sub)
7100243-03 TOC (Sub)
7100243-04 TOC (Sub)
Lab Number
The following analyses were subcontracted to Microseeps/Pace
Analysis
7100243-01 Methane, Ethane, Ethene (AM20GAX)
7100243-01 Volatile Fatty Acids (Sub)
7100243-02 Methane, Ethane, Ethene (AM20GAX)
7100243-02 Volatile Fatty Acids (Sub)
7100243-03 Methane, Ethane, Ethene (AM20GAX)
7100243-03 Volatile Fatty Acids (Sub)
7100243-04 Dissolved Hydrogen (Sub)
7100243-04 Methane, Ethane, Ethene (AM20GAX)
7100243-04 Volatile Fatty Acids (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 98
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