No preview available
HomeMy WebLinkAbout6406-COMPOST-2014_analysis-FY16-17This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 07/26/2017 Carolina Recycled Ag Materials LLC Kyle Bass PO Box 519 Nashville, NC 27856 Project: Compost Lab Submittal Date: 07/12/2017 Prism Work Order: 7070190 Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. President/Project Manager Reviewed ByRobbi A. Jones Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: BHL MB greater than one half of the RL, but sample concentrations are either less than the RL or greater than 10x the MB. MI Matrix spike outside of the control limits. Matrix interference suspected. Method Detection LimitMDL Below Reporting LimitBRL Relative Percent DifferenceRPD *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 7 Sample Receipt Summary 07/26/2017 Prism Work Order: 7070190 Client Sample ID MatrixLab Sample ID Date Sampled Date Received 7070190-01 07/11/17CRAM Compost 07/12/17Solid Samples were received at 30.9 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 7 Laboratory Report 07/26/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 519 Project: CompostCarolina Recycled Ag Materials LLC Nashville, NC 27856 Attn: Kyle Bass Sample Matrix: Solid Client Sample ID: Prism Sample ID: 7070190-01 Prism Work Order: 7070190 Time Collected: 07/11/17 13:00 Time Submitted: 07/12/17 12:45 CRAM Compost General Chemistry Parameters 62.7 *SM2540 G P7G027810.100 7/18/17 14:30 JLB% by Weight 0.100% Solids Microbiological Parameters BRL *SM9221 E P7G019010.3 7/12/17 12:59 BMSMPN/g dryFecal Coliforms Total Metals BRL *7471B P7G028710.032 7/20/17 11:05 JABmg/kg dry 0.0031Mercury 0.87 *6010D P7G024010.40 7/18/17 18:14 JABmg/kg dry 0.048Arsenic 1.4 *6010D P7G024010.40 7/18/17 18:14 JABmg/kg dry 0.011Cadmium 25 *6010D P7G024010.79 7/18/17 18:14 JABmg/kg dry 0.072Copper 7.8 *6010D P7G024010.40 7/18/17 18:14 JABmg/kg dry 0.074Lead 5.7 *6010D P7G024010.79 7/18/17 18:14 JABmg/kg dry 0.029Nickel 2.1 *6010D P7G024010.79 7/18/17 18:14 JABmg/kg dry 0.19Selenium 87 *6010D P7G024014.0 7/18/17 18:14 JABmg/kg dry 0.14Zinc This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 7 7/26/17 Level II QC Report PO Box 519 Project: CompostCarolina Recycled Ag Materials LLC Nashville, NC 27856 Attn: Kyle Bass Prism Work Order: 7070190 Time Submitted: 7/12/2017 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P7G0240 - 3050B Blank (P7G0240-BLK1)Prepared & Analyzed: 07/18/17 Arsenic mg/kg wetBRL0.25 Cadmium mg/kg wetBRL0.25 Copper mg/kg wetBRL0.50 BHL Lead mg/kg wetBRL0.25 BHL Nickel mg/kg wetBRL0.50 Selenium mg/kg wetBRL0.50 Zinc mg/kg wetBRL2.5 LCS (P7G0240-BS1)Prepared & Analyzed: 07/18/17 Arsenic mg/kg wet25.2 0.25 25.00 80-120101 Cadmium mg/kg wet24.4 0.25 25.00 80-12098 Copper mg/kg wet27.9 0.50 25.00 80-120112 Lead mg/kg wet25.0 0.25 25.00 80-120100 Nickel mg/kg wet25.4 0.50 25.00 80-120102 Selenium mg/kg wet24.4 0.50 25.00 80-12098 Zinc mg/kg wet24.7 2.5 25.00 80-12099 Matrix Spike (P7G0240-MS1)Prepared & Analyzed: 07/18/17 Source: 7070190-01 Arsenic mg/kg dry44.0 0.39 39.47 0.871 75-125109 Cadmium mg/kg dry33.1 0.39 39.47 1.43 75-12580 Copper mg/kg dry69.5 0.79 39.47 24.8 75-125113 Lead mg/kg dry41.3 0.39 39.47 7.76 75-12585 Nickel mg/kg dry40.8 0.79 39.47 5.66 75-12589 Selenium mg/kg dry47.7 0.79 39.46 2.11 75-125116 Zinc mg/kg dry1243.9 39.47 86.7 75-12594 Matrix Spike Dup (P7G0240-MSD1)Prepared & Analyzed: 07/18/17 Source: 7070190-01 Arsenic mg/kg dry42.9 0.39 39.47 0.871 2075-125106 3 Cadmium mg/kg dry32.5 0.39 39.47 1.43 2075-12579 2 Copper mg/kg dry65.6 0.79 39.47 24.8 2075-125103 6 Lead mg/kg dry39.1 0.39 39.47 7.76 2075-12579 6 Nickel mg/kg dry40.1 0.79 39.47 5.66 2075-12587 2 Selenium mg/kg dry45.6 0.79 39.46 2.11 2075-125110 4 Zinc mg/kg dry1183.9 39.47 86.7 2075-12579 5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 7 7/26/17 Level II QC Report PO Box 519 Project: CompostCarolina Recycled Ag Materials LLC Nashville, NC 27856 Attn: Kyle Bass Prism Work Order: 7070190 Time Submitted: 7/12/2017 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P7G0240 - 3050B Post Spike (P7G0240-PS1)Prepared & Analyzed: 07/18/17 Source: 7070190-01 Arsenic mg/L1.04 1.000 0.0219 80-120102 Cadmium mg/L0.799 1.000 0.0359 MI80-12076 Copper mg/L1.70 1.000 0.622 80-120108 Lead mg/L0.976 1.000 0.195 MI80-12078 Nickel mg/L0.947 1.000 0.142 80-12081 Selenium mg/L1.16 0.9998 0.0529 80-120111 Zinc mg/L3.08 1.000 2.18 80-12091 Batch P7G0287 - 7471B Blank (P7G0287-BLK1)Prepared & Analyzed: 07/20/17 Mercury mg/kg wetBRL0.020 LCS (P7G0287-BS1)Prepared & Analyzed: 07/20/17 Mercury mg/kg wet0.435 0.020 0.4167 80-120104 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 7 7/26/17 Level II QC Report PO Box 519 Project: CompostCarolina Recycled Ag Materials LLC Nashville, NC 27856 Attn: Kyle Bass Prism Work Order: 7070190 Time Submitted: 7/12/2017 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Microbiological Parameters - Quality Control Batch P7G0190 - NO PREP Blank (P7G0190-BLK1)Prepared & Analyzed: 07/12/17 Fecal Coliforms MPN/g wetBRL0.2 Sample Extraction Data Prep Method: Solids, Dry Weight Lab Number Batch Date/TimeInitialFinal P7G02787070190-01 07/18/17 14:3030 30g g Prep Method: 3050B Lab Number Batch Date/TimeInitialFinal P7G02407070190-01 07/18/17 8:002.01 50g mL Prep Method: 7471B Lab Number Batch Date/TimeInitialFinal P7G02877070190-01 07/20/17 8:000.59 50g mL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 7 Page 7 of 7