14006 Classic Cofefe Stream Sampling AMEC 20120531

June 12, 2012
LIMS USE: FR - ROB FOSTER
LIMS OBJECT ID: 92119682
92119682
Project:
Pace Project No.:
RE:
Mr. Rob Foster
AMEC-Charlotte
2801 Yorkmont Road Suite 100
Charlotte, NC 28208
FORMER PLIANA FACILITY
Dear Mr. Foster:
Enclosed are the analytical results for sample(s) received by the laboratory on May 31, 2012. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia Certification #: 00072West Virginia Certification #: 356Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92119682001 DS EPA 6010 13 PASI-AJDA
EPA 7471 1 PASI-ASHB
EPA 8270 by SIM 21 PASI-CPPM
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
EPA 7196 1 PASI-ASDH
92119682002 SS EPA 6010 13 PASI-AJDA
EPA 7471 1 PASI-ASHB
EPA 8270 by SIM 21 PASI-CPPM
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
EPA 7196 1 PASI-ASDH
92119682003 US EPA 6010 13 PASI-AJDA
EPA 7471 1 PASI-ASHB
EPA 8270 by SIM 21 PASI-CPPM
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
EPA 7196 1 PASI-ASDH
92119682004 DS EPA 1664A 1 PASI-CAM1
EPA 6010 14 PASI-AJMW
SM 9222D 1 PASI-CKDF
SM 9223 2 PASI-CTNM
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 63 PASI-CMCK
EPA 180.1 1 PASI-ALMD
SM 2540D 1 PASI-ALMD
SM 5210B 1 PASI-ADMN
EPA 350.1 1 PASI-ASDH
EPA 351.2 1 PASI-AJDA
EPA 353.2 3 PASI-ADMN
EPA 365.1 1 PASI-AJDA
SM 5220D 1 PASI-ADMN
EPA 7196 1 PASI-ADMN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92119682005 SS EPA 1664A 1 PASI-CAM1
EPA 6010 14 PASI-AJMW
SM 9222D 1 PASI-CKDF
SM 9223 2 PASI-CTNM
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 63 PASI-CMCK
EPA 180.1 1 PASI-ALMD
SM 2540D 1 PASI-ALMD
SM 5210B 1 PASI-ADMN
EPA 350.1 1 PASI-ASDH
EPA 351.2 1 PASI-AJDA
EPA 353.2 3 PASI-ADMN
EPA 365.1 1 PASI-AJDA
SM 5220D 1 PASI-ADMN
EPA 7196 1 PASI-ADMN
92119682006 US EPA 1664A 1 PASI-CAM1
EPA 6010 14 PASI-AJMW
SM 9222D 1 PASI-CKDF
SM 9223 2 PASI-CTNM
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 63 PASI-CMCK
EPA 180.1 1 PASI-ALMD
SM 2540D 1 PASI-ALMD
SM 5210B 1 PASI-ADMN
EPA 350.1 1 PASI-ASDH
EPA 351.2 1 PASI-AJDA
EPA 353.2 3 PASI-ADMN
EPA 365.1 1 PASI-AJDA
SM 5220D 1 PASI-ADMN
EPA 7196 1 PASI-ADMN
92119682007 FIELD BLANK EPA 6010 14 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 63 PASI-CMCK
EPA 7196 1 PASI-ADMN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92119682008 DS-USGS SSC SM 2540D 1 PASI-ALMD
92119682009 SS-USGS SSC SM 2540D 1 PASI-ALMD
92119682010 US-USGS SSC SM 2540D 1 PASI-ALMD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682001 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 06/02/12 15:24 7440-36-006/01/12 13:450.49
Arsenic ND mg/kg 1 06/02/12 15:24 7440-38-206/01/12 13:450.49
Beryllium ND mg/kg 1 06/02/12 15:24 7440-41-706/01/12 13:450.098
Cadmium ND mg/kg 1 06/02/12 15:24 7440-43-906/01/12 13:450.098
Chromium 15.8 mg/kg 1 06/02/12 15:24 7440-47-306/01/12 13:450.49
Copper 4.2 mg/kg 1 06/02/12 15:24 7440-50-806/01/12 13:450.49
Lead 2.0 mg/kg 1 06/02/12 15:24 7439-92-106/01/12 13:450.49
Manganese 112 mg/kg 1 06/02/12 15:24 7439-96-506/01/12 13:450.49
Nickel 1.3 mg/kg 1 06/02/12 15:24 7440-02-006/01/12 13:450.49
Selenium ND mg/kg 1 06/02/12 15:24 7782-49-206/01/12 13:450.98
Silver ND mg/kg 1 06/02/12 15:24 7440-22-406/01/12 13:450.49
Thallium ND mg/kg 1 06/02/12 15:24 7440-28-006/01/12 13:450.98
Zinc 19.8 mg/kg 1 06/02/12 15:24 7440-66-606/01/12 13:450.98
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.031 mg/kg 1 06/05/12 14:39 7439-97-606/04/12 10:300.0026
8270 MSSV MW PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 06/01/12 15:49 83-32-906/01/12 08:2612.0
Acenaphthylene ND ug/kg 1 06/01/12 15:49 208-96-806/01/12 08:2612.0
Anthracene ND ug/kg 1 06/01/12 15:49 120-12-706/01/12 08:2612.0
Benzo(a)anthracene ND ug/kg 1 06/01/12 15:49 56-55-306/01/12 08:2612.0
Benzo(a)pyrene 15.5 ug/kg 1 06/01/12 15:49 50-32-806/01/12 08:2612.0
Benzo(b)fluoranthene 15.8 ug/kg 1 06/01/12 15:49 205-99-206/01/12 08:2612.0
Benzo(g,h,i)perylene ND ug/kg 1 06/01/12 15:49 191-24-206/01/12 08:2612.0
Benzo(k)fluoranthene 13.4 ug/kg 1 06/01/12 15:49 207-08-906/01/12 08:2612.0
Chrysene 19.0 ug/kg 1 06/01/12 15:49 218-01-906/01/12 08:2612.0
Dibenz(a,h)anthracene ND ug/kg 1 06/01/12 15:49 53-70-306/01/12 08:2612.0
Fluoranthene 27.3 ug/kg 1 06/01/12 15:49 206-44-006/01/12 08:2612.0
Fluorene ND ug/kg 1 06/01/12 15:49 86-73-706/01/12 08:2612.0
Indeno(1,2,3-cd)pyrene ND ug/kg 1 06/01/12 15:49 193-39-506/01/12 08:2612.0
1-Methylnaphthalene ND ug/kg 1 06/01/12 15:49 90-12-006/01/12 08:2612.0
2-Methylnaphthalene ND ug/kg 1 06/01/12 15:49 91-57-606/01/12 08:2612.0
Naphthalene ND ug/kg 1 06/01/12 15:49 91-20-306/01/12 08:2612.0
Phenanthrene ND ug/kg 1 06/01/12 15:49 85-01-806/01/12 08:2612.0
Pyrene 21.6 ug/kg 1 06/01/12 15:49 129-00-006/01/12 08:2612.0
Surrogates
Nitrobenzene-d5 (S)74 %1 06/01/12 15:49 4165-60-006/01/12 08:2610-128
2-Fluorobiphenyl (S)65 %1 06/01/12 15:49 321-60-806/01/12 08:2610-110
Terphenyl-d14 (S)100 %1 06/01/12 15:49 1718-51-006/01/12 08:2639-119
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 06/05/12 18:39 83-32-906/04/12 08:40394
Acenaphthylene ND ug/kg 1 06/05/12 18:39 208-96-806/04/12 08:40394
Aniline ND ug/kg 1 06/05/12 18:39 62-53-306/04/12 08:40394
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 6 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682001 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Anthracene ND ug/kg 1 06/05/12 18:39 120-12-706/04/12 08:40394
Benzo(a)anthracene ND ug/kg 1 06/05/12 18:39 56-55-306/04/12 08:40394
Benzo(a)pyrene ND ug/kg 1 06/05/12 18:39 50-32-806/04/12 08:40394
Benzo(b)fluoranthene ND ug/kg 1 06/05/12 18:39 205-99-206/04/12 08:40394
Benzo(g,h,i)perylene ND ug/kg 1 06/05/12 18:39 191-24-206/04/12 08:40394
Benzo(k)fluoranthene ND ug/kg 1 06/05/12 18:39 207-08-906/04/12 08:40394
Benzoic Acid ND ug/kg 1 06/05/12 18:39 65-85-006/04/12 08:401970
Benzyl alcohol ND ug/kg 1 06/05/12 18:39 100-51-606/04/12 08:40787
4-Bromophenylphenyl ether ND ug/kg 1 06/05/12 18:39 101-55-306/04/12 08:40394
Butylbenzylphthalate ND ug/kg 1 06/05/12 18:39 85-68-706/04/12 08:40394
4-Chloro-3-methylphenol ND ug/kg 1 06/05/12 18:39 59-50-706/04/12 08:40787
4-Chloroaniline ND ug/kg 1 06/05/12 18:39 106-47-806/04/12 08:401970
bis(2-Chloroethoxy)methane ND ug/kg 1 06/05/12 18:39 111-91-106/04/12 08:40394
bis(2-Chloroethyl) ether ND ug/kg 1 06/05/12 18:39 111-44-406/04/12 08:40394
bis(2-Chloroisopropyl) ether ND ug/kg 1 06/05/12 18:39 108-60-106/04/12 08:40394
2-Chloronaphthalene ND ug/kg 1 06/05/12 18:39 91-58-706/04/12 08:40394
2-Chlorophenol ND ug/kg 1 06/05/12 18:39 95-57-806/04/12 08:40394
4-Chlorophenylphenyl ether ND ug/kg 1 06/05/12 18:39 7005-72-306/04/12 08:40394
Chrysene ND ug/kg 1 06/05/12 18:39 218-01-906/04/12 08:40394
Dibenz(a,h)anthracene ND ug/kg 1 06/05/12 18:39 53-70-306/04/12 08:40394
Dibenzofuran ND ug/kg 1 06/05/12 18:39 132-64-906/04/12 08:40394
1,2-Dichlorobenzene ND ug/kg 1 06/05/12 18:39 95-50-106/04/12 08:40394
1,3-Dichlorobenzene ND ug/kg 1 06/05/12 18:39 541-73-106/04/12 08:40394
1,4-Dichlorobenzene ND ug/kg 1 06/05/12 18:39 106-46-706/04/12 08:40394
3,3'-Dichlorobenzidine ND ug/kg 1 06/05/12 18:39 91-94-106/04/12 08:401970
2,4-Dichlorophenol ND ug/kg 1 06/05/12 18:39 120-83-206/04/12 08:40394
Diethylphthalate ND ug/kg 1 06/05/12 18:39 84-66-206/04/12 08:40394
2,4-Dimethylphenol ND ug/kg 1 06/05/12 18:39 105-67-906/04/12 08:40394
Dimethylphthalate ND ug/kg 1 06/05/12 18:39 131-11-306/04/12 08:40394
Di-n-butylphthalate ND ug/kg 1 06/05/12 18:39 84-74-206/04/12 08:40394
4,6-Dinitro-2-methylphenol ND ug/kg 1 06/05/12 18:39 534-52-106/04/12 08:40787
2,4-Dinitrophenol ND ug/kg 1 06/05/12 18:39 51-28-506/04/12 08:401970
2,4-Dinitrotoluene ND ug/kg 1 06/05/12 18:39 121-14-206/04/12 08:40394
2,6-Dinitrotoluene ND ug/kg 1 06/05/12 18:39 606-20-206/04/12 08:40394
Di-n-octylphthalate ND ug/kg 1 06/05/12 18:39 117-84-006/04/12 08:40394
bis(2-Ethylhexyl)phthalate ND ug/kg 1 06/05/12 18:39 117-81-706/04/12 08:40394
Fluoranthene ND ug/kg 1 06/05/12 18:39 206-44-006/04/12 08:40394
Fluorene ND ug/kg 1 06/05/12 18:39 86-73-706/04/12 08:40394
Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 18:39 87-68-306/04/12 08:40394
Hexachlorobenzene ND ug/kg 1 06/05/12 18:39 118-74-106/04/12 08:40394
Hexachlorocyclopentadiene ND ug/kg 1 06/05/12 18:39 77-47-406/04/12 08:40394
Hexachloroethane ND ug/kg 1 06/05/12 18:39 67-72-106/04/12 08:40394
Indeno(1,2,3-cd)pyrene ND ug/kg 1 06/05/12 18:39 193-39-506/04/12 08:40394
Isophorone ND ug/kg 1 06/05/12 18:39 78-59-106/04/12 08:40394
1-Methylnaphthalene ND ug/kg 1 06/05/12 18:39 90-12-006/04/12 08:40394
2-Methylnaphthalene ND ug/kg 1 06/05/12 18:39 91-57-606/04/12 08:40394
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 7 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682001 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Methylphenol(o-Cresol)ND ug/kg 1 06/05/12 18:39 95-48-706/04/12 08:40394
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 06/05/12 18:3906/04/12 08:40394
Naphthalene ND ug/kg 1 06/05/12 18:39 91-20-306/04/12 08:40394
2-Nitroaniline ND ug/kg 1 06/05/12 18:39 88-74-406/04/12 08:401970
3-Nitroaniline ND ug/kg 1 06/05/12 18:39 99-09-206/04/12 08:401970
4-Nitroaniline ND ug/kg 1 06/05/12 18:39 100-01-606/04/12 08:40787
Nitrobenzene ND ug/kg 1 06/05/12 18:39 98-95-306/04/12 08:40394
2-Nitrophenol ND ug/kg 1 06/05/12 18:39 88-75-506/04/12 08:40394
4-Nitrophenol ND ug/kg 1 06/05/12 18:39 100-02-706/04/12 08:401970
N-Nitrosodimethylamine ND ug/kg 1 06/05/12 18:39 62-75-906/04/12 08:40394
N-Nitroso-di-n-propylamine ND ug/kg 1 06/05/12 18:39 621-64-706/04/12 08:40394
N-Nitrosodiphenylamine ND ug/kg 1 06/05/12 18:39 86-30-606/04/12 08:40394
Pentachlorophenol ND ug/kg 1 06/05/12 18:39 87-86-506/04/12 08:401970
Phenanthrene ND ug/kg 1 06/05/12 18:39 85-01-806/04/12 08:40394
Phenol ND ug/kg 1 06/05/12 18:39 108-95-206/04/12 08:40394
Pyrene ND ug/kg 1 06/05/12 18:39 129-00-006/04/12 08:40394
1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 18:39 120-82-106/04/12 08:40394
2,4,5-Trichlorophenol ND ug/kg 1 06/05/12 18:39 95-95-406/04/12 08:40394
2,4,6-Trichlorophenol ND ug/kg 1 06/05/12 18:39 88-06-206/04/12 08:40394
Surrogates
Nitrobenzene-d5 (S)61 %1 06/05/12 18:39 4165-60-006/04/12 08:4023-110
2-Fluorobiphenyl (S)48 %1 06/05/12 18:39 321-60-806/04/12 08:4030-110
Terphenyl-d14 (S)65 %1 06/05/12 18:39 1718-51-006/04/12 08:4028-110
Phenol-d6 (S)51 %1 06/05/12 18:39 13127-88-306/04/12 08:4022-110
2-Fluorophenol (S)54 %1 06/05/12 18:39 367-12-406/04/12 08:4013-110
2,4,6-Tribromophenol (S)68 %1 06/05/12 18:39 118-79-606/04/12 08:4027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 06/04/12 16:41 67-64-197.9
Benzene ND ug/kg 1 06/04/12 16:41 71-43-24.9
Bromobenzene ND ug/kg 1 06/04/12 16:41 108-86-14.9
Bromochloromethane ND ug/kg 1 06/04/12 16:41 74-97-54.9
Bromodichloromethane ND ug/kg 1 06/04/12 16:41 75-27-44.9
Bromoform ND ug/kg 1 06/04/12 16:41 75-25-24.9
Bromomethane ND ug/kg 1 06/04/12 16:41 74-83-99.8
2-Butanone (MEK)ND ug/kg 1 06/04/12 16:41 78-93-397.9
n-Butylbenzene ND ug/kg 1 06/04/12 16:41 104-51-84.9
sec-Butylbenzene ND ug/kg 1 06/04/12 16:41 135-98-84.9
tert-Butylbenzene ND ug/kg 1 06/04/12 16:41 98-06-64.9
Carbon tetrachloride ND ug/kg 1 06/04/12 16:41 56-23-54.9
Chlorobenzene ND ug/kg 1 06/04/12 16:41 108-90-74.9
Chloroethane ND ug/kg 1 06/04/12 16:41 75-00-39.8
Chloroform ND ug/kg 1 06/04/12 16:41 67-66-34.9
Chloromethane ND ug/kg 1 06/04/12 16:41 74-87-39.8
2-Chlorotoluene ND ug/kg 1 06/04/12 16:41 95-49-84.9
4-Chlorotoluene ND ug/kg 1 06/04/12 16:41 106-43-44.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 8 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682001 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane ND ug/kg 1 06/04/12 16:41 96-12-84.9
Dibromochloromethane ND ug/kg 1 06/04/12 16:41 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 06/04/12 16:41 106-93-44.9
Dibromomethane ND ug/kg 1 06/04/12 16:41 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 06/04/12 16:41 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 06/04/12 16:41 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 06/04/12 16:41 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 06/04/12 16:41 75-71-89.8
1,1-Dichloroethane ND ug/kg 1 06/04/12 16:41 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 06/04/12 16:41 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 06/04/12 16:41 75-35-44.9
cis-1,2-Dichloroethene ND ug/kg 1 06/04/12 16:41 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 06/04/12 16:41 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 06/04/12 16:41 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 06/04/12 16:41 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 06/04/12 16:41 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 06/04/12 16:41 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 06/04/12 16:41 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 06/04/12 16:41 10061-02-64.9
Diisopropyl ether ND ug/kg 1 06/04/12 16:41 108-20-34.9
Ethylbenzene ND ug/kg 1 06/04/12 16:41 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 06/04/12 16:41 87-68-34.9
2-Hexanone ND ug/kg 1 06/04/12 16:41 591-78-649.0
Isopropylbenzene (Cumene)ND ug/kg 1 06/04/12 16:41 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 06/04/12 16:41 99-87-64.9
Methylene Chloride ND ug/kg 1 06/04/12 16:41 75-09-219.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/04/12 16:41 108-10-149.0
Methyl-tert-butyl ether ND ug/kg 1 06/04/12 16:41 1634-04-44.9
Naphthalene ND ug/kg 1 06/04/12 16:41 91-20-34.9
n-Propylbenzene ND ug/kg 1 06/04/12 16:41 103-65-14.9
Styrene ND ug/kg 1 06/04/12 16:41 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 06/04/12 16:41 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 06/04/12 16:41 79-34-54.9
Tetrachloroethene ND ug/kg 1 06/04/12 16:41 127-18-44.9
Toluene ND ug/kg 1 06/04/12 16:41 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 06/04/12 16:41 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 06/04/12 16:41 120-82-14.9
1,1,1-Trichloroethane ND ug/kg 1 06/04/12 16:41 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 06/04/12 16:41 79-00-54.9
Trichloroethene ND ug/kg 1 06/04/12 16:41 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 06/04/12 16:41 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 06/04/12 16:41 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 06/04/12 16:41 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 06/04/12 16:41 108-67-84.9
Vinyl acetate ND ug/kg 1 06/04/12 16:41 108-05-449.0
Vinyl chloride ND ug/kg 1 06/04/12 16:41 75-01-49.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 9 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682001 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Xylene (Total)ND ug/kg 1 06/04/12 16:41 1330-20-79.8
m&p-Xylene ND ug/kg 1 06/04/12 16:41 179601-23-19.8
o-Xylene ND ug/kg 1 06/04/12 16:41 95-47-64.9
Surrogates
Dibromofluoromethane (S)118 %1 06/04/12 16:41 1868-53-770-130
Toluene-d8 (S)106 %1 06/04/12 16:41 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 06/04/12 16:41 460-00-470-130
1,2-Dichloroethane-d4 (S)122 %1 06/04/12 16:41 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.4 %1 06/01/12 13:020.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 06/06/12 14:42 18540-29-9 N206/06/12 12:370.57
Sample:SS Lab ID:92119682002 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 06/02/12 15:28 7440-36-006/01/12 13:450.66
Arsenic ND mg/kg 1 06/02/12 15:28 7440-38-206/01/12 13:450.66
Beryllium 0.18 mg/kg 1 06/02/12 15:28 7440-41-706/01/12 13:450.13
Cadmium 1.9 mg/kg 1 06/02/12 15:28 7440-43-906/01/12 13:450.13
Chromium 176 mg/kg 1 06/02/12 15:28 7440-47-306/01/12 13:450.66
Copper 27.5 mg/kg 1 06/02/12 15:28 7440-50-806/01/12 13:450.66
Lead 2.8 mg/kg 1 06/02/12 15:28 7439-92-106/01/12 13:450.66
Manganese 232 mg/kg 1 06/02/12 15:28 7439-96-506/01/12 13:450.66
Nickel 56.9 mg/kg 1 06/02/12 15:28 7440-02-006/01/12 13:450.66
Selenium ND mg/kg 1 06/02/12 15:28 7782-49-206/01/12 13:451.3
Silver ND mg/kg 1 06/02/12 15:28 7440-22-406/01/12 13:450.66
Thallium ND mg/kg 1 06/02/12 15:28 7440-28-006/01/12 13:451.3
Zinc 36.4 mg/kg 1 06/02/12 15:28 7440-66-606/01/12 13:451.3
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury ND mg/kg 1 06/05/12 12:17 7439-97-606/04/12 10:300.0064
8270 MSSV MW PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 06/01/12 16:09 83-32-906/01/12 08:2614.0
Acenaphthylene ND ug/kg 1 06/01/12 16:09 208-96-806/01/12 08:2614.0
Anthracene ND ug/kg 1 06/01/12 16:09 120-12-706/01/12 08:2614.0
Benzo(a)anthracene ND ug/kg 1 06/01/12 16:09 56-55-306/01/12 08:2614.0
Benzo(a)pyrene ND ug/kg 1 06/01/12 16:09 50-32-806/01/12 08:2614.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 10 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682002 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV MW PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3546
Benzo(b)fluoranthene ND ug/kg 1 06/01/12 16:09 205-99-206/01/12 08:2614.0
Benzo(g,h,i)perylene ND ug/kg 1 06/01/12 16:09 191-24-206/01/12 08:2614.0
Benzo(k)fluoranthene ND ug/kg 1 06/01/12 16:09 207-08-906/01/12 08:2614.0
Chrysene ND ug/kg 1 06/01/12 16:09 218-01-906/01/12 08:2614.0
Dibenz(a,h)anthracene ND ug/kg 1 06/01/12 16:09 53-70-306/01/12 08:2614.0
Fluoranthene ND ug/kg 1 06/01/12 16:09 206-44-006/01/12 08:2614.0
Fluorene ND ug/kg 1 06/01/12 16:09 86-73-706/01/12 08:2614.0
Indeno(1,2,3-cd)pyrene ND ug/kg 1 06/01/12 16:09 193-39-506/01/12 08:2614.0
1-Methylnaphthalene ND ug/kg 1 06/01/12 16:09 90-12-006/01/12 08:2614.0
2-Methylnaphthalene ND ug/kg 1 06/01/12 16:09 91-57-606/01/12 08:2614.0
Naphthalene ND ug/kg 1 06/01/12 16:09 91-20-306/01/12 08:2614.0
Phenanthrene ND ug/kg 1 06/01/12 16:09 85-01-806/01/12 08:2614.0
Pyrene ND ug/kg 1 06/01/12 16:09 129-00-006/01/12 08:2614.0
Surrogates
Nitrobenzene-d5 (S)36 %1 06/01/12 16:09 4165-60-006/01/12 08:2610-128
2-Fluorobiphenyl (S)55 %1 06/01/12 16:09 321-60-806/01/12 08:2610-110
Terphenyl-d14 (S)70 %1 06/01/12 16:09 1718-51-006/01/12 08:2639-119
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 06/05/12 19:07 83-32-906/04/12 08:40460
Acenaphthylene ND ug/kg 1 06/05/12 19:07 208-96-806/04/12 08:40460
Aniline ND ug/kg 1 06/05/12 19:07 62-53-306/04/12 08:40460
Anthracene ND ug/kg 1 06/05/12 19:07 120-12-706/04/12 08:40460
Benzo(a)anthracene ND ug/kg 1 06/05/12 19:07 56-55-306/04/12 08:40460
Benzo(a)pyrene ND ug/kg 1 06/05/12 19:07 50-32-806/04/12 08:40460
Benzo(b)fluoranthene ND ug/kg 1 06/05/12 19:07 205-99-206/04/12 08:40460
Benzo(g,h,i)perylene ND ug/kg 1 06/05/12 19:07 191-24-206/04/12 08:40460
Benzo(k)fluoranthene ND ug/kg 1 06/05/12 19:07 207-08-906/04/12 08:40460
Benzoic Acid ND ug/kg 1 06/05/12 19:07 65-85-006/04/12 08:402300
Benzyl alcohol ND ug/kg 1 06/05/12 19:07 100-51-606/04/12 08:40920
4-Bromophenylphenyl ether ND ug/kg 1 06/05/12 19:07 101-55-306/04/12 08:40460
Butylbenzylphthalate ND ug/kg 1 06/05/12 19:07 85-68-706/04/12 08:40460
4-Chloro-3-methylphenol ND ug/kg 1 06/05/12 19:07 59-50-706/04/12 08:40920
4-Chloroaniline ND ug/kg 1 06/05/12 19:07 106-47-806/04/12 08:402300
bis(2-Chloroethoxy)methane ND ug/kg 1 06/05/12 19:07 111-91-106/04/12 08:40460
bis(2-Chloroethyl) ether ND ug/kg 1 06/05/12 19:07 111-44-406/04/12 08:40460
bis(2-Chloroisopropyl) ether ND ug/kg 1 06/05/12 19:07 108-60-106/04/12 08:40460
2-Chloronaphthalene ND ug/kg 1 06/05/12 19:07 91-58-706/04/12 08:40460
2-Chlorophenol ND ug/kg 1 06/05/12 19:07 95-57-806/04/12 08:40460
4-Chlorophenylphenyl ether ND ug/kg 1 06/05/12 19:07 7005-72-306/04/12 08:40460
Chrysene ND ug/kg 1 06/05/12 19:07 218-01-906/04/12 08:40460
Dibenz(a,h)anthracene ND ug/kg 1 06/05/12 19:07 53-70-306/04/12 08:40460
Dibenzofuran ND ug/kg 1 06/05/12 19:07 132-64-906/04/12 08:40460
1,2-Dichlorobenzene ND ug/kg 1 06/05/12 19:07 95-50-106/04/12 08:40460
1,3-Dichlorobenzene ND ug/kg 1 06/05/12 19:07 541-73-106/04/12 08:40460
1,4-Dichlorobenzene ND ug/kg 1 06/05/12 19:07 106-46-706/04/12 08:40460
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 11 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682002 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 06/05/12 19:07 91-94-106/04/12 08:402300
2,4-Dichlorophenol ND ug/kg 1 06/05/12 19:07 120-83-206/04/12 08:40460
Diethylphthalate ND ug/kg 1 06/05/12 19:07 84-66-206/04/12 08:40460
2,4-Dimethylphenol ND ug/kg 1 06/05/12 19:07 105-67-906/04/12 08:40460
Dimethylphthalate ND ug/kg 1 06/05/12 19:07 131-11-306/04/12 08:40460
Di-n-butylphthalate ND ug/kg 1 06/05/12 19:07 84-74-206/04/12 08:40460
4,6-Dinitro-2-methylphenol ND ug/kg 1 06/05/12 19:07 534-52-106/04/12 08:40920
2,4-Dinitrophenol ND ug/kg 1 06/05/12 19:07 51-28-506/04/12 08:402300
2,4-Dinitrotoluene ND ug/kg 1 06/05/12 19:07 121-14-206/04/12 08:40460
2,6-Dinitrotoluene ND ug/kg 1 06/05/12 19:07 606-20-206/04/12 08:40460
Di-n-octylphthalate ND ug/kg 1 06/05/12 19:07 117-84-006/04/12 08:40460
bis(2-Ethylhexyl)phthalate ND ug/kg 1 06/05/12 19:07 117-81-706/04/12 08:40460
Fluoranthene ND ug/kg 1 06/05/12 19:07 206-44-006/04/12 08:40460
Fluorene ND ug/kg 1 06/05/12 19:07 86-73-706/04/12 08:40460
Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 19:07 87-68-306/04/12 08:40460
Hexachlorobenzene ND ug/kg 1 06/05/12 19:07 118-74-106/04/12 08:40460
Hexachlorocyclopentadiene ND ug/kg 1 06/05/12 19:07 77-47-406/04/12 08:40460
Hexachloroethane ND ug/kg 1 06/05/12 19:07 67-72-106/04/12 08:40460
Indeno(1,2,3-cd)pyrene ND ug/kg 1 06/05/12 19:07 193-39-506/04/12 08:40460
Isophorone ND ug/kg 1 06/05/12 19:07 78-59-106/04/12 08:40460
1-Methylnaphthalene ND ug/kg 1 06/05/12 19:07 90-12-006/04/12 08:40460
2-Methylnaphthalene ND ug/kg 1 06/05/12 19:07 91-57-606/04/12 08:40460
2-Methylphenol(o-Cresol)ND ug/kg 1 06/05/12 19:07 95-48-706/04/12 08:40460
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 06/05/12 19:0706/04/12 08:40460
Naphthalene ND ug/kg 1 06/05/12 19:07 91-20-306/04/12 08:40460
2-Nitroaniline ND ug/kg 1 06/05/12 19:07 88-74-406/04/12 08:402300
3-Nitroaniline ND ug/kg 1 06/05/12 19:07 99-09-206/04/12 08:402300
4-Nitroaniline ND ug/kg 1 06/05/12 19:07 100-01-606/04/12 08:40920
Nitrobenzene ND ug/kg 1 06/05/12 19:07 98-95-306/04/12 08:40460
2-Nitrophenol ND ug/kg 1 06/05/12 19:07 88-75-506/04/12 08:40460
4-Nitrophenol ND ug/kg 1 06/05/12 19:07 100-02-706/04/12 08:402300
N-Nitrosodimethylamine ND ug/kg 1 06/05/12 19:07 62-75-906/04/12 08:40460
N-Nitroso-di-n-propylamine ND ug/kg 1 06/05/12 19:07 621-64-706/04/12 08:40460
N-Nitrosodiphenylamine ND ug/kg 1 06/05/12 19:07 86-30-606/04/12 08:40460
Pentachlorophenol ND ug/kg 1 06/05/12 19:07 87-86-506/04/12 08:402300
Phenanthrene ND ug/kg 1 06/05/12 19:07 85-01-806/04/12 08:40460
Phenol ND ug/kg 1 06/05/12 19:07 108-95-206/04/12 08:40460
Pyrene ND ug/kg 1 06/05/12 19:07 129-00-006/04/12 08:40460
1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 19:07 120-82-106/04/12 08:40460
2,4,5-Trichlorophenol ND ug/kg 1 06/05/12 19:07 95-95-406/04/12 08:40460
2,4,6-Trichlorophenol ND ug/kg 1 06/05/12 19:07 88-06-206/04/12 08:40460
Surrogates
Nitrobenzene-d5 (S)65 %1 06/05/12 19:07 4165-60-006/04/12 08:4023-110
2-Fluorobiphenyl (S)68 %1 06/05/12 19:07 321-60-806/04/12 08:4030-110
Terphenyl-d14 (S)73 %1 06/05/12 19:07 1718-51-006/04/12 08:4028-110
Phenol-d6 (S)67 %1 06/05/12 19:07 13127-88-306/04/12 08:4022-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 12 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682002 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)73 %1 06/05/12 19:07 367-12-406/04/12 08:4013-110
2,4,6-Tribromophenol (S)68 %1 06/05/12 19:07 118-79-606/04/12 08:4027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 06/04/12 17:00 67-64-1112
Benzene ND ug/kg 1 06/04/12 17:00 71-43-25.6
Bromobenzene ND ug/kg 1 06/04/12 17:00 108-86-15.6
Bromochloromethane ND ug/kg 1 06/04/12 17:00 74-97-55.6
Bromodichloromethane ND ug/kg 1 06/04/12 17:00 75-27-45.6
Bromoform ND ug/kg 1 06/04/12 17:00 75-25-25.6
Bromomethane ND ug/kg 1 06/04/12 17:00 74-83-911.2
2-Butanone (MEK)ND ug/kg 1 06/04/12 17:00 78-93-3112
n-Butylbenzene ND ug/kg 1 06/04/12 17:00 104-51-85.6
sec-Butylbenzene ND ug/kg 1 06/04/12 17:00 135-98-85.6
tert-Butylbenzene ND ug/kg 1 06/04/12 17:00 98-06-65.6
Carbon tetrachloride ND ug/kg 1 06/04/12 17:00 56-23-55.6
Chlorobenzene ND ug/kg 1 06/04/12 17:00 108-90-75.6
Chloroethane ND ug/kg 1 06/04/12 17:00 75-00-311.2
Chloroform ND ug/kg 1 06/04/12 17:00 67-66-35.6
Chloromethane ND ug/kg 1 06/04/12 17:00 74-87-311.2
2-Chlorotoluene ND ug/kg 1 06/04/12 17:00 95-49-85.6
4-Chlorotoluene ND ug/kg 1 06/04/12 17:00 106-43-45.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 06/04/12 17:00 96-12-85.6
Dibromochloromethane ND ug/kg 1 06/04/12 17:00 124-48-15.6
1,2-Dibromoethane (EDB)ND ug/kg 1 06/04/12 17:00 106-93-45.6
Dibromomethane ND ug/kg 1 06/04/12 17:00 74-95-35.6
1,2-Dichlorobenzene ND ug/kg 1 06/04/12 17:00 95-50-15.6
1,3-Dichlorobenzene ND ug/kg 1 06/04/12 17:00 541-73-15.6
1,4-Dichlorobenzene ND ug/kg 1 06/04/12 17:00 106-46-75.6
Dichlorodifluoromethane ND ug/kg 1 06/04/12 17:00 75-71-811.2
1,1-Dichloroethane ND ug/kg 1 06/04/12 17:00 75-34-35.6
1,2-Dichloroethane ND ug/kg 1 06/04/12 17:00 107-06-25.6
1,1-Dichloroethene ND ug/kg 1 06/04/12 17:00 75-35-45.6
cis-1,2-Dichloroethene ND ug/kg 1 06/04/12 17:00 156-59-25.6
trans-1,2-Dichloroethene ND ug/kg 1 06/04/12 17:00 156-60-55.6
1,2-Dichloropropane ND ug/kg 1 06/04/12 17:00 78-87-55.6
1,3-Dichloropropane ND ug/kg 1 06/04/12 17:00 142-28-95.6
2,2-Dichloropropane ND ug/kg 1 06/04/12 17:00 594-20-75.6
1,1-Dichloropropene ND ug/kg 1 06/04/12 17:00 563-58-65.6
cis-1,3-Dichloropropene ND ug/kg 1 06/04/12 17:00 10061-01-55.6
trans-1,3-Dichloropropene ND ug/kg 1 06/04/12 17:00 10061-02-65.6
Diisopropyl ether ND ug/kg 1 06/04/12 17:00 108-20-35.6
Ethylbenzene ND ug/kg 1 06/04/12 17:00 100-41-45.6
Hexachloro-1,3-butadiene ND ug/kg 1 06/04/12 17:00 87-68-35.6
2-Hexanone ND ug/kg 1 06/04/12 17:00 591-78-656.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 13 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682002 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 1 06/04/12 17:00 98-82-85.6
p-Isopropyltoluene ND ug/kg 1 06/04/12 17:00 99-87-65.6
Methylene Chloride ND ug/kg 1 06/04/12 17:00 75-09-222.4
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/04/12 17:00 108-10-156.1
Methyl-tert-butyl ether ND ug/kg 1 06/04/12 17:00 1634-04-45.6
Naphthalene ND ug/kg 1 06/04/12 17:00 91-20-35.6
n-Propylbenzene ND ug/kg 1 06/04/12 17:00 103-65-15.6
Styrene ND ug/kg 1 06/04/12 17:00 100-42-55.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 06/04/12 17:00 630-20-65.6
1,1,2,2-Tetrachloroethane ND ug/kg 1 06/04/12 17:00 79-34-55.6
Tetrachloroethene ND ug/kg 1 06/04/12 17:00 127-18-45.6
Toluene ND ug/kg 1 06/04/12 17:00 108-88-35.6
1,2,3-Trichlorobenzene ND ug/kg 1 06/04/12 17:00 87-61-65.6
1,2,4-Trichlorobenzene ND ug/kg 1 06/04/12 17:00 120-82-15.6
1,1,1-Trichloroethane ND ug/kg 1 06/04/12 17:00 71-55-65.6
1,1,2-Trichloroethane ND ug/kg 1 06/04/12 17:00 79-00-55.6
Trichloroethene ND ug/kg 1 06/04/12 17:00 79-01-65.6
Trichlorofluoromethane ND ug/kg 1 06/04/12 17:00 75-69-45.6
1,2,3-Trichloropropane ND ug/kg 1 06/04/12 17:00 96-18-45.6
1,2,4-Trimethylbenzene ND ug/kg 1 06/04/12 17:00 95-63-65.6
1,3,5-Trimethylbenzene ND ug/kg 1 06/04/12 17:00 108-67-85.6
Vinyl acetate ND ug/kg 1 06/04/12 17:00 108-05-456.1
Vinyl chloride ND ug/kg 1 06/04/12 17:00 75-01-411.2
Xylene (Total)ND ug/kg 1 06/04/12 17:00 1330-20-711.2
m&p-Xylene ND ug/kg 1 06/04/12 17:00 179601-23-111.2
o-Xylene ND ug/kg 1 06/04/12 17:00 95-47-65.6
Surrogates
Dibromofluoromethane (S)120 %1 06/04/12 17:00 1868-53-770-130
Toluene-d8 (S)108 %1 06/04/12 17:00 2037-26-570-130
4-Bromofluorobenzene (S)97 %1 06/04/12 17:00 460-00-470-130
1,2-Dichloroethane-d4 (S)127 %1 06/04/12 17:00 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 28.7 %1 06/01/12 13:020.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 06/06/12 14:42 18540-29-9 N206/06/12 12:370.66
Sample:US Lab ID:92119682003 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 06/02/12 15:33 7440-36-006/01/12 13:450.55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 14 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682003 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 1 06/02/12 15:33 7440-38-206/01/12 13:450.55
Beryllium ND mg/kg 1 06/02/12 15:33 7440-41-706/01/12 13:450.11
Cadmium ND mg/kg 1 06/02/12 15:33 7440-43-906/01/12 13:450.11
Chromium 6.2 mg/kg 1 06/02/12 15:33 7440-47-306/01/12 13:450.55
Copper 9.0 mg/kg 1 06/02/12 15:33 7440-50-806/01/12 13:450.55
Lead 1.8 mg/kg 1 06/02/12 15:33 7439-92-106/01/12 13:450.55
Manganese 159 mg/kg 1 06/02/12 15:33 7439-96-506/01/12 13:450.55
Nickel 4.6 mg/kg 1 06/02/12 15:33 7440-02-006/01/12 13:450.55
Selenium ND mg/kg 1 06/02/12 15:33 7782-49-206/01/12 13:451.1
Silver ND mg/kg 1 06/02/12 15:33 7440-22-406/01/12 13:450.55
Thallium ND mg/kg 1 06/02/12 15:33 7440-28-006/01/12 13:451.1
Zinc 25.7 mg/kg 1 06/02/12 15:33 7440-66-606/01/12 13:451.1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.010 mg/kg 1 06/05/12 12:22 7439-97-606/04/12 10:300.0025
8270 MSSV MW PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 06/01/12 16:29 83-32-906/01/12 08:2611.1
Acenaphthylene ND ug/kg 1 06/01/12 16:29 208-96-806/01/12 08:2611.1
Anthracene ND ug/kg 1 06/01/12 16:29 120-12-706/01/12 08:2611.1
Benzo(a)anthracene ND ug/kg 1 06/01/12 16:29 56-55-306/01/12 08:2611.1
Benzo(a)pyrene 15.7 ug/kg 1 06/01/12 16:29 50-32-806/01/12 08:2611.1
Benzo(b)fluoranthene 16.4 ug/kg 1 06/01/12 16:29 205-99-206/01/12 08:2611.1
Benzo(g,h,i)perylene ND ug/kg 1 06/01/12 16:29 191-24-206/01/12 08:2611.1
Benzo(k)fluoranthene 11.5 ug/kg 1 06/01/12 16:29 207-08-906/01/12 08:2611.1
Chrysene ND ug/kg 1 06/01/12 16:29 218-01-906/01/12 08:2611.1
Dibenz(a,h)anthracene ND ug/kg 1 06/01/12 16:29 53-70-306/01/12 08:2611.1
Fluoranthene 37.6 ug/kg 1 06/01/12 16:29 206-44-006/01/12 08:2611.1
Fluorene ND ug/kg 1 06/01/12 16:29 86-73-706/01/12 08:2611.1
Indeno(1,2,3-cd)pyrene ND ug/kg 1 06/01/12 16:29 193-39-506/01/12 08:2611.1
1-Methylnaphthalene ND ug/kg 1 06/01/12 16:29 90-12-006/01/12 08:2611.1
2-Methylnaphthalene ND ug/kg 1 06/01/12 16:29 91-57-606/01/12 08:2611.1
Naphthalene ND ug/kg 1 06/01/12 16:29 91-20-306/01/12 08:2611.1
Phenanthrene 16.6 ug/kg 1 06/01/12 16:29 85-01-806/01/12 08:2611.1
Pyrene 28.6 ug/kg 1 06/01/12 16:29 129-00-006/01/12 08:2611.1
Surrogates
Nitrobenzene-d5 (S)64 %1 06/01/12 16:29 4165-60-006/01/12 08:2610-128
2-Fluorobiphenyl (S)61 %1 06/01/12 16:29 321-60-806/01/12 08:2610-110
Terphenyl-d14 (S)103 %1 06/01/12 16:29 1718-51-006/01/12 08:2639-119
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 06/05/12 19:35 83-32-906/04/12 08:40364
Acenaphthylene ND ug/kg 1 06/05/12 19:35 208-96-806/04/12 08:40364
Aniline ND ug/kg 1 06/05/12 19:35 62-53-306/04/12 08:40364
Anthracene ND ug/kg 1 06/05/12 19:35 120-12-706/04/12 08:40364
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 15 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682003 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Benzo(a)anthracene ND ug/kg 1 06/05/12 19:35 56-55-306/04/12 08:40364
Benzo(a)pyrene ND ug/kg 1 06/05/12 19:35 50-32-806/04/12 08:40364
Benzo(b)fluoranthene ND ug/kg 1 06/05/12 19:35 205-99-206/04/12 08:40364
Benzo(g,h,i)perylene ND ug/kg 1 06/05/12 19:35 191-24-206/04/12 08:40364
Benzo(k)fluoranthene ND ug/kg 1 06/05/12 19:35 207-08-906/04/12 08:40364
Benzoic Acid ND ug/kg 1 06/05/12 19:35 65-85-006/04/12 08:401820
Benzyl alcohol ND ug/kg 1 06/05/12 19:35 100-51-606/04/12 08:40728
4-Bromophenylphenyl ether ND ug/kg 1 06/05/12 19:35 101-55-306/04/12 08:40364
Butylbenzylphthalate ND ug/kg 1 06/05/12 19:35 85-68-706/04/12 08:40364
4-Chloro-3-methylphenol ND ug/kg 1 06/05/12 19:35 59-50-706/04/12 08:40728
4-Chloroaniline ND ug/kg 1 06/05/12 19:35 106-47-806/04/12 08:401820
bis(2-Chloroethoxy)methane ND ug/kg 1 06/05/12 19:35 111-91-106/04/12 08:40364
bis(2-Chloroethyl) ether ND ug/kg 1 06/05/12 19:35 111-44-406/04/12 08:40364
bis(2-Chloroisopropyl) ether ND ug/kg 1 06/05/12 19:35 108-60-106/04/12 08:40364
2-Chloronaphthalene ND ug/kg 1 06/05/12 19:35 91-58-706/04/12 08:40364
2-Chlorophenol ND ug/kg 1 06/05/12 19:35 95-57-806/04/12 08:40364
4-Chlorophenylphenyl ether ND ug/kg 1 06/05/12 19:35 7005-72-306/04/12 08:40364
Chrysene ND ug/kg 1 06/05/12 19:35 218-01-906/04/12 08:40364
Dibenz(a,h)anthracene ND ug/kg 1 06/05/12 19:35 53-70-306/04/12 08:40364
Dibenzofuran ND ug/kg 1 06/05/12 19:35 132-64-906/04/12 08:40364
1,2-Dichlorobenzene ND ug/kg 1 06/05/12 19:35 95-50-106/04/12 08:40364
1,3-Dichlorobenzene ND ug/kg 1 06/05/12 19:35 541-73-106/04/12 08:40364
1,4-Dichlorobenzene ND ug/kg 1 06/05/12 19:35 106-46-706/04/12 08:40364
3,3'-Dichlorobenzidine ND ug/kg 1 06/05/12 19:35 91-94-106/04/12 08:401820
2,4-Dichlorophenol ND ug/kg 1 06/05/12 19:35 120-83-206/04/12 08:40364
Diethylphthalate ND ug/kg 1 06/05/12 19:35 84-66-206/04/12 08:40364
2,4-Dimethylphenol ND ug/kg 1 06/05/12 19:35 105-67-906/04/12 08:40364
Dimethylphthalate ND ug/kg 1 06/05/12 19:35 131-11-306/04/12 08:40364
Di-n-butylphthalate ND ug/kg 1 06/05/12 19:35 84-74-206/04/12 08:40364
4,6-Dinitro-2-methylphenol ND ug/kg 1 06/05/12 19:35 534-52-106/04/12 08:40728
2,4-Dinitrophenol ND ug/kg 1 06/05/12 19:35 51-28-506/04/12 08:401820
2,4-Dinitrotoluene ND ug/kg 1 06/05/12 19:35 121-14-206/04/12 08:40364
2,6-Dinitrotoluene ND ug/kg 1 06/05/12 19:35 606-20-206/04/12 08:40364
Di-n-octylphthalate ND ug/kg 1 06/05/12 19:35 117-84-006/04/12 08:40364
bis(2-Ethylhexyl)phthalate ND ug/kg 1 06/05/12 19:35 117-81-706/04/12 08:40364
Fluoranthene ND ug/kg 1 06/05/12 19:35 206-44-006/04/12 08:40364
Fluorene ND ug/kg 1 06/05/12 19:35 86-73-706/04/12 08:40364
Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 19:35 87-68-306/04/12 08:40364
Hexachlorobenzene ND ug/kg 1 06/05/12 19:35 118-74-106/04/12 08:40364
Hexachlorocyclopentadiene ND ug/kg 1 06/05/12 19:35 77-47-406/04/12 08:40364
Hexachloroethane ND ug/kg 1 06/05/12 19:35 67-72-106/04/12 08:40364
Indeno(1,2,3-cd)pyrene ND ug/kg 1 06/05/12 19:35 193-39-506/04/12 08:40364
Isophorone ND ug/kg 1 06/05/12 19:35 78-59-106/04/12 08:40364
1-Methylnaphthalene ND ug/kg 1 06/05/12 19:35 90-12-006/04/12 08:40364
2-Methylnaphthalene ND ug/kg 1 06/05/12 19:35 91-57-606/04/12 08:40364
2-Methylphenol(o-Cresol)ND ug/kg 1 06/05/12 19:35 95-48-706/04/12 08:40364
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 16 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682003 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 06/05/12 19:3506/04/12 08:40364
Naphthalene ND ug/kg 1 06/05/12 19:35 91-20-306/04/12 08:40364
2-Nitroaniline ND ug/kg 1 06/05/12 19:35 88-74-406/04/12 08:401820
3-Nitroaniline ND ug/kg 1 06/05/12 19:35 99-09-206/04/12 08:401820
4-Nitroaniline ND ug/kg 1 06/05/12 19:35 100-01-606/04/12 08:40728
Nitrobenzene ND ug/kg 1 06/05/12 19:35 98-95-306/04/12 08:40364
2-Nitrophenol ND ug/kg 1 06/05/12 19:35 88-75-506/04/12 08:40364
4-Nitrophenol ND ug/kg 1 06/05/12 19:35 100-02-706/04/12 08:401820
N-Nitrosodimethylamine ND ug/kg 1 06/05/12 19:35 62-75-906/04/12 08:40364
N-Nitroso-di-n-propylamine ND ug/kg 1 06/05/12 19:35 621-64-706/04/12 08:40364
N-Nitrosodiphenylamine ND ug/kg 1 06/05/12 19:35 86-30-606/04/12 08:40364
Pentachlorophenol ND ug/kg 1 06/05/12 19:35 87-86-506/04/12 08:401820
Phenanthrene ND ug/kg 1 06/05/12 19:35 85-01-806/04/12 08:40364
Phenol ND ug/kg 1 06/05/12 19:35 108-95-206/04/12 08:40364
Pyrene ND ug/kg 1 06/05/12 19:35 129-00-006/04/12 08:40364
1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 19:35 120-82-106/04/12 08:40364
2,4,5-Trichlorophenol ND ug/kg 1 06/05/12 19:35 95-95-406/04/12 08:40364
2,4,6-Trichlorophenol ND ug/kg 1 06/05/12 19:35 88-06-206/04/12 08:40364
Surrogates
Nitrobenzene-d5 (S)54 %1 06/05/12 19:35 4165-60-006/04/12 08:4023-110
2-Fluorobiphenyl (S)54 %1 06/05/12 19:35 321-60-806/04/12 08:4030-110
Terphenyl-d14 (S)86 %1 06/05/12 19:35 1718-51-006/04/12 08:4028-110
Phenol-d6 (S)57 %1 06/05/12 19:35 13127-88-306/04/12 08:4022-110
2-Fluorophenol (S)51 %1 06/05/12 19:35 367-12-406/04/12 08:4013-110
2,4,6-Tribromophenol (S)64 %1 06/05/12 19:35 118-79-606/04/12 08:4027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 06/04/12 17:18 67-64-193.8
Benzene ND ug/kg 1 06/04/12 17:18 71-43-24.7
Bromobenzene ND ug/kg 1 06/04/12 17:18 108-86-14.7
Bromochloromethane ND ug/kg 1 06/04/12 17:18 74-97-54.7
Bromodichloromethane ND ug/kg 1 06/04/12 17:18 75-27-44.7
Bromoform ND ug/kg 1 06/04/12 17:18 75-25-24.7
Bromomethane ND ug/kg 1 06/04/12 17:18 74-83-99.4
2-Butanone (MEK)ND ug/kg 1 06/04/12 17:18 78-93-393.8
n-Butylbenzene ND ug/kg 1 06/04/12 17:18 104-51-84.7
sec-Butylbenzene ND ug/kg 1 06/04/12 17:18 135-98-84.7
tert-Butylbenzene ND ug/kg 1 06/04/12 17:18 98-06-64.7
Carbon tetrachloride ND ug/kg 1 06/04/12 17:18 56-23-54.7
Chlorobenzene ND ug/kg 1 06/04/12 17:18 108-90-74.7
Chloroethane ND ug/kg 1 06/04/12 17:18 75-00-39.4
Chloroform ND ug/kg 1 06/04/12 17:18 67-66-34.7
Chloromethane ND ug/kg 1 06/04/12 17:18 74-87-39.4
2-Chlorotoluene ND ug/kg 1 06/04/12 17:18 95-49-84.7
4-Chlorotoluene ND ug/kg 1 06/04/12 17:18 106-43-44.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 06/04/12 17:18 96-12-84.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 17 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682003 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Dibromochloromethane ND ug/kg 1 06/04/12 17:18 124-48-14.7
1,2-Dibromoethane (EDB)ND ug/kg 1 06/04/12 17:18 106-93-44.7
Dibromomethane ND ug/kg 1 06/04/12 17:18 74-95-34.7
1,2-Dichlorobenzene ND ug/kg 1 06/04/12 17:18 95-50-14.7
1,3-Dichlorobenzene ND ug/kg 1 06/04/12 17:18 541-73-14.7
1,4-Dichlorobenzene ND ug/kg 1 06/04/12 17:18 106-46-74.7
Dichlorodifluoromethane ND ug/kg 1 06/04/12 17:18 75-71-89.4
1,1-Dichloroethane ND ug/kg 1 06/04/12 17:18 75-34-34.7
1,2-Dichloroethane ND ug/kg 1 06/04/12 17:18 107-06-24.7
1,1-Dichloroethene ND ug/kg 1 06/04/12 17:18 75-35-44.7
cis-1,2-Dichloroethene ND ug/kg 1 06/04/12 17:18 156-59-24.7
trans-1,2-Dichloroethene ND ug/kg 1 06/04/12 17:18 156-60-54.7
1,2-Dichloropropane ND ug/kg 1 06/04/12 17:18 78-87-54.7
1,3-Dichloropropane ND ug/kg 1 06/04/12 17:18 142-28-94.7
2,2-Dichloropropane ND ug/kg 1 06/04/12 17:18 594-20-74.7
1,1-Dichloropropene ND ug/kg 1 06/04/12 17:18 563-58-64.7
cis-1,3-Dichloropropene ND ug/kg 1 06/04/12 17:18 10061-01-54.7
trans-1,3-Dichloropropene ND ug/kg 1 06/04/12 17:18 10061-02-64.7
Diisopropyl ether ND ug/kg 1 06/04/12 17:18 108-20-34.7
Ethylbenzene ND ug/kg 1 06/04/12 17:18 100-41-44.7
Hexachloro-1,3-butadiene ND ug/kg 1 06/04/12 17:18 87-68-34.7
2-Hexanone ND ug/kg 1 06/04/12 17:18 591-78-646.9
Isopropylbenzene (Cumene)ND ug/kg 1 06/04/12 17:18 98-82-84.7
p-Isopropyltoluene ND ug/kg 1 06/04/12 17:18 99-87-64.7
Methylene Chloride ND ug/kg 1 06/04/12 17:18 75-09-218.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/04/12 17:18 108-10-146.9
Methyl-tert-butyl ether ND ug/kg 1 06/04/12 17:18 1634-04-44.7
Naphthalene ND ug/kg 1 06/04/12 17:18 91-20-34.7
n-Propylbenzene ND ug/kg 1 06/04/12 17:18 103-65-14.7
Styrene ND ug/kg 1 06/04/12 17:18 100-42-54.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 06/04/12 17:18 630-20-64.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 06/04/12 17:18 79-34-54.7
Tetrachloroethene ND ug/kg 1 06/04/12 17:18 127-18-44.7
Toluene ND ug/kg 1 06/04/12 17:18 108-88-34.7
1,2,3-Trichlorobenzene ND ug/kg 1 06/04/12 17:18 87-61-64.7
1,2,4-Trichlorobenzene ND ug/kg 1 06/04/12 17:18 120-82-14.7
1,1,1-Trichloroethane ND ug/kg 1 06/04/12 17:18 71-55-64.7
1,1,2-Trichloroethane ND ug/kg 1 06/04/12 17:18 79-00-54.7
Trichloroethene ND ug/kg 1 06/04/12 17:18 79-01-64.7
Trichlorofluoromethane ND ug/kg 1 06/04/12 17:18 75-69-44.7
1,2,3-Trichloropropane ND ug/kg 1 06/04/12 17:18 96-18-44.7
1,2,4-Trimethylbenzene ND ug/kg 1 06/04/12 17:18 95-63-64.7
1,3,5-Trimethylbenzene ND ug/kg 1 06/04/12 17:18 108-67-84.7
Vinyl acetate ND ug/kg 1 06/04/12 17:18 108-05-446.9
Vinyl chloride ND ug/kg 1 06/04/12 17:18 75-01-49.4
Xylene (Total)ND ug/kg 1 06/04/12 17:18 1330-20-79.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 18 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682003 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
m&p-Xylene ND ug/kg 1 06/04/12 17:18 179601-23-19.4
o-Xylene ND ug/kg 1 06/04/12 17:18 95-47-64.7
Surrogates
Dibromofluoromethane (S)119 %1 06/04/12 17:18 1868-53-770-130
Toluene-d8 (S)105 %1 06/04/12 17:18 2037-26-570-130
4-Bromofluorobenzene (S)92 %1 06/04/12 17:18 460-00-470-130
1,2-Dichloroethane-d4 (S)124 %1 06/04/12 17:18 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.3 %1 06/01/12 13:020.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 06/06/12 14:42 18540-29-9 N206/06/12 12:370.53
Sample:DS Lab ID:92119682004 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
HEM, Oil and Grease Analytical Method: EPA 1664A
Oil and Grease ND mg/L 1 06/04/12 14:575.0
6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C
Antimony 5.5 ug/L 1 06/04/12 19:56 7440-36-006/01/12 11:305.0
Arsenic ND ug/L 1 06/04/12 19:56 7440-38-206/01/12 11:305.0
Beryllium ND ug/L 1 06/04/12 19:56 7440-41-706/01/12 11:301.0
Cadmium ND ug/L 1 06/04/12 19:56 7440-43-906/01/12 11:301.0
Chromium ND ug/L 1 06/04/12 19:56 7440-47-306/01/12 11:305.0
Copper ND ug/L 1 06/04/12 19:56 7440-50-806/01/12 11:305.0
Lead ND ug/L 1 06/04/12 19:56 7439-92-106/01/12 11:305.0
Manganese 37.2 ug/L 1 06/04/12 19:56 7439-96-506/01/12 11:305.0
Nickel ND ug/L 1 06/04/12 19:56 7440-02-006/01/12 11:305.0
Selenium ND ug/L 1 06/04/12 19:56 7782-49-206/01/12 11:3010.0
Silver ND ug/L 1 06/04/12 19:56 7440-22-406/01/12 11:305.0
Thallium ND ug/L 1 06/04/12 19:56 7440-28-006/01/12 11:3010.0
Total Hardness 114000 ug/L 1 06/04/12 19:5606/01/12 11:30
Zinc ND ug/L 1 06/04/12 19:56 7440-66-606/01/12 11:3010.0
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D
Fecal Coliforms 5000 CFU/100 mL 1 05/31/12 14:39 N21.0
MBIO Total Coliform CHT Analytical Method: SM 9223 Preparation Method: SM 9223
Fecal/E. coli PRESENT 1 06/01/12 15:46 N205/31/12 15:32
Total Coliforms PRESENT 1 06/01/12 15:46 N205/31/12 15:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 19 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682004 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 06/07/12 12:27 7439-97-606/06/12 17:500.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 06/04/12 15:12 83-32-906/01/12 16:0010.0
Acenaphthylene ND ug/L 1 06/04/12 15:12 208-96-806/01/12 16:0010.0
Aniline ND ug/L 1 06/04/12 15:12 62-53-306/01/12 16:0010.0
Anthracene ND ug/L 1 06/04/12 15:12 120-12-706/01/12 16:0010.0
Benzo(a)anthracene ND ug/L 1 06/04/12 15:12 56-55-306/01/12 16:0010.0
Benzo(a)pyrene ND ug/L 1 06/04/12 15:12 50-32-806/01/12 16:0010.0
Benzo(b)fluoranthene ND ug/L 1 06/04/12 15:12 205-99-206/01/12 16:0010.0
Benzo(g,h,i)perylene ND ug/L 1 06/04/12 15:12 191-24-206/01/12 16:0010.0
Benzo(k)fluoranthene ND ug/L 1 06/04/12 15:12 207-08-906/01/12 16:0010.0
Benzoic Acid ND ug/L 1 06/04/12 15:12 65-85-006/01/12 16:0050.0
Benzyl alcohol ND ug/L 1 06/04/12 15:12 100-51-606/01/12 16:0020.0
4-Bromophenylphenyl ether ND ug/L 1 06/04/12 15:12 101-55-306/01/12 16:0010.0
Butylbenzylphthalate ND ug/L 1 06/04/12 15:12 85-68-706/01/12 16:0010.0
4-Chloro-3-methylphenol ND ug/L 1 06/04/12 15:12 59-50-706/01/12 16:0020.0
4-Chloroaniline ND ug/L 1 06/04/12 15:12 106-47-806/01/12 16:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 06/04/12 15:12 111-91-106/01/12 16:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 06/04/12 15:12 111-44-406/01/12 16:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/04/12 15:12 108-60-106/01/12 16:0010.0
2-Chloronaphthalene ND ug/L 1 06/04/12 15:12 91-58-706/01/12 16:0010.0
2-Chlorophenol ND ug/L 1 06/04/12 15:12 95-57-806/01/12 16:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 06/04/12 15:12 7005-72-306/01/12 16:0010.0
Chrysene ND ug/L 1 06/04/12 15:12 218-01-906/01/12 16:0010.0
Dibenz(a,h)anthracene ND ug/L 1 06/04/12 15:12 53-70-306/01/12 16:0010.0
Dibenzofuran ND ug/L 1 06/04/12 15:12 132-64-906/01/12 16:0010.0
1,2-Dichlorobenzene ND ug/L 1 06/04/12 15:12 95-50-106/01/12 16:0010.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 15:12 541-73-106/01/12 16:0010.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 15:12 106-46-706/01/12 16:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 06/04/12 15:12 91-94-106/01/12 16:0020.0
2,4-Dichlorophenol ND ug/L 1 06/04/12 15:12 120-83-206/01/12 16:0010.0
Diethylphthalate ND ug/L 1 06/04/12 15:12 84-66-206/01/12 16:0010.0
2,4-Dimethylphenol ND ug/L 1 06/04/12 15:12 105-67-906/01/12 16:0010.0
Dimethylphthalate ND ug/L 1 06/04/12 15:12 131-11-306/01/12 16:0010.0
Di-n-butylphthalate ND ug/L 1 06/04/12 15:12 84-74-206/01/12 16:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 06/04/12 15:12 534-52-106/01/12 16:0020.0
2,4-Dinitrophenol ND ug/L 1 06/04/12 15:12 51-28-506/01/12 16:0050.0
2,4-Dinitrotoluene ND ug/L 1 06/04/12 15:12 121-14-206/01/12 16:0010.0
2,6-Dinitrotoluene ND ug/L 1 06/04/12 15:12 606-20-206/01/12 16:0010.0
Di-n-octylphthalate ND ug/L 1 06/04/12 15:12 117-84-006/01/12 16:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/04/12 15:12 117-81-706/01/12 16:006.0
Fluoranthene ND ug/L 1 06/04/12 15:12 206-44-006/01/12 16:0010.0
Fluorene ND ug/L 1 06/04/12 15:12 86-73-706/01/12 16:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 15:12 87-68-306/01/12 16:0010.0
Hexachlorobenzene ND ug/L 1 06/04/12 15:12 118-74-106/01/12 16:0010.0
Hexachlorocyclopentadiene ND ug/L 1 06/04/12 15:12 77-47-406/01/12 16:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 20 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682004 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Hexachloroethane ND ug/L 1 06/04/12 15:12 67-72-106/01/12 16:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/04/12 15:12 193-39-506/01/12 16:0010.0
Isophorone ND ug/L 1 06/04/12 15:12 78-59-106/01/12 16:0010.0
1-Methylnaphthalene ND ug/L 1 06/04/12 15:12 90-12-006/01/12 16:0010.0
2-Methylnaphthalene ND ug/L 1 06/04/12 15:12 91-57-606/01/12 16:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 06/04/12 15:12 95-48-706/01/12 16:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 06/04/12 15:1206/01/12 16:0010.0
Naphthalene ND ug/L 1 06/04/12 15:12 91-20-306/01/12 16:0010.0
2-Nitroaniline ND ug/L 1 06/04/12 15:12 88-74-406/01/12 16:0050.0
3-Nitroaniline ND ug/L 1 06/04/12 15:12 99-09-206/01/12 16:0050.0
4-Nitroaniline ND ug/L 1 06/04/12 15:12 100-01-606/01/12 16:0020.0
Nitrobenzene ND ug/L 1 06/04/12 15:12 98-95-306/01/12 16:0010.0
2-Nitrophenol ND ug/L 1 06/04/12 15:12 88-75-506/01/12 16:0010.0
4-Nitrophenol ND ug/L 1 06/04/12 15:12 100-02-706/01/12 16:0050.0
N-Nitrosodimethylamine ND ug/L 1 06/04/12 15:12 62-75-906/01/12 16:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 06/04/12 15:12 621-64-706/01/12 16:0010.0
N-Nitrosodiphenylamine ND ug/L 1 06/04/12 15:12 86-30-606/01/12 16:0010.0
Pentachlorophenol ND ug/L 1 06/04/12 15:12 87-86-506/01/12 16:0025.0
Phenanthrene ND ug/L 1 06/04/12 15:12 85-01-806/01/12 16:0010.0
Phenol ND ug/L 1 06/04/12 15:12 108-95-206/01/12 16:0010.0
Pyrene ND ug/L 1 06/04/12 15:12 129-00-006/01/12 16:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 15:12 120-82-106/01/12 16:0010.0
2,4,5-Trichlorophenol ND ug/L 1 06/04/12 15:12 95-95-406/01/12 16:0010.0
2,4,6-Trichlorophenol ND ug/L 1 06/04/12 15:12 88-06-206/01/12 16:0010.0
Surrogates
Nitrobenzene-d5 (S)77 %1 06/04/12 15:12 4165-60-006/01/12 16:0021-110
2-Fluorobiphenyl (S)75 %1 06/04/12 15:12 321-60-806/01/12 16:0027-110
Terphenyl-d14 (S)109 %1 06/04/12 15:12 1718-51-0 S006/01/12 16:0031-107
Phenol-d6 (S)25 %1 06/04/12 15:12 13127-88-306/01/12 16:0010-110
2-Fluorophenol (S)42 %1 06/04/12 15:12 367-12-406/01/12 16:0012-110
2,4,6-Tribromophenol (S)83 %1 06/04/12 15:12 118-79-606/01/12 16:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 06/04/12 16:11 67-64-125.0
Benzene ND ug/L 1 06/04/12 16:11 71-43-21.0
Bromobenzene ND ug/L 1 06/04/12 16:11 108-86-11.0
Bromochloromethane ND ug/L 1 06/04/12 16:11 74-97-51.0
Bromodichloromethane ND ug/L 1 06/04/12 16:11 75-27-41.0
Bromoform ND ug/L 1 06/04/12 16:11 75-25-21.0
Bromomethane ND ug/L 1 06/04/12 16:11 74-83-92.0
2-Butanone (MEK)ND ug/L 1 06/04/12 16:11 78-93-35.0
Carbon tetrachloride ND ug/L 1 06/04/12 16:11 56-23-51.0
Chlorobenzene ND ug/L 1 06/04/12 16:11 108-90-71.0
Chloroethane ND ug/L 1 06/04/12 16:11 75-00-31.0
Chloroform ND ug/L 1 06/04/12 16:11 67-66-31.0
Chloromethane ND ug/L 1 06/04/12 16:11 74-87-31.0
2-Chlorotoluene ND ug/L 1 06/04/12 16:11 95-49-81.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 21 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682004 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
4-Chlorotoluene ND ug/L 1 06/04/12 16:11 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 06/04/12 16:11 96-12-85.0
Dibromochloromethane ND ug/L 1 06/04/12 16:11 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 06/04/12 16:11 106-93-41.0
Dibromomethane ND ug/L 1 06/04/12 16:11 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 06/04/12 16:11 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 16:11 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 16:11 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 06/04/12 16:11 75-71-81.0
1,1-Dichloroethane ND ug/L 1 06/04/12 16:11 75-34-31.0
1,2-Dichloroethane ND ug/L 1 06/04/12 16:11 107-06-21.0
1,1-Dichloroethene ND ug/L 1 06/04/12 16:11 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 06/04/12 16:11 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 06/04/12 16:11 156-60-51.0
1,2-Dichloropropane ND ug/L 1 06/04/12 16:11 78-87-51.0
1,3-Dichloropropane ND ug/L 1 06/04/12 16:11 142-28-91.0
2,2-Dichloropropane ND ug/L 1 06/04/12 16:11 594-20-71.0
1,1-Dichloropropene ND ug/L 1 06/04/12 16:11 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 06/04/12 16:11 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 06/04/12 16:11 10061-02-61.0
Diisopropyl ether ND ug/L 1 06/04/12 16:11 108-20-31.0
Ethylbenzene ND ug/L 1 06/04/12 16:11 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 16:11 87-68-31.0
2-Hexanone ND ug/L 1 06/04/12 16:11 591-78-65.0
p-Isopropyltoluene ND ug/L 1 06/04/12 16:11 99-87-61.0
Methylene Chloride ND ug/L 1 06/04/12 16:11 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/04/12 16:11 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 06/04/12 16:11 1634-04-41.0
Naphthalene ND ug/L 1 06/04/12 16:11 91-20-31.0
Styrene ND ug/L 1 06/04/12 16:11 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 06/04/12 16:11 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 06/04/12 16:11 79-34-51.0
Tetrachloroethene ND ug/L 1 06/04/12 16:11 127-18-41.0
Toluene ND ug/L 1 06/04/12 16:11 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 06/04/12 16:11 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 16:11 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 06/04/12 16:11 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 06/04/12 16:11 79-00-51.0
Trichloroethene ND ug/L 1 06/04/12 16:11 79-01-61.0
Trichlorofluoromethane ND ug/L 1 06/04/12 16:11 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 06/04/12 16:11 96-18-41.0
Vinyl acetate ND ug/L 1 06/04/12 16:11 108-05-42.0
Vinyl chloride ND ug/L 1 06/04/12 16:11 75-01-41.0
m&p-Xylene ND ug/L 1 06/04/12 16:11 179601-23-12.0
o-Xylene ND ug/L 1 06/04/12 16:11 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)102 %1 06/04/12 16:11 460-00-470-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 22 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:DS Lab ID:92119682004 Collected:05/31/12 10:30 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Surrogates
Dibromofluoromethane (S)102 %1 06/04/12 16:11 1868-53-770-130
1,2-Dichloroethane-d4 (S)104 %1 06/04/12 16:11 17060-07-070-130
Toluene-d8 (S)98 %1 06/04/12 16:11 2037-26-570-130
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 3.5 NTU 1 06/01/12 00:501.0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 1 06/01/12 22:512.6
5210B BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day ND mg/L 1 06/06/12 17:5006/01/12 20:552.0
350.1 Ammonia Analytical Method: EPA 350.1
Nitrogen, Ammonia ND mg/L 1 06/05/12 13:44 7664-41-70.10
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total ND mg/L 1 06/02/12 09:38 7727-37-90.50
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2
Nitrogen, Nitrate 0.59 mg/L 1 06/01/12 00:560.020
Nitrogen, Nitrite ND mg/L 1 06/01/12 00:560.020
Nitrogen, NO2 plus NO3 0.59 mg/L 1 06/01/12 00:560.020
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus ND mg/L 1 06/03/12 08:49 7723-14-00.050
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 1 06/06/12 21:0525.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196
Chromium, Hexavalent ND mg/L 1 05/31/12 22:21 18540-29-9 N20.050
Sample:SS Lab ID:92119682005 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
HEM, Oil and Grease Analytical Method: EPA 1664A
Oil and Grease ND mg/L 1 06/04/12 14:585.0
6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C
Antimony 6.9 ug/L 1 06/04/12 19:59 7440-36-006/01/12 11:305.0
Arsenic ND ug/L 1 06/04/12 19:59 7440-38-206/01/12 11:305.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 23 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682005 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C
Beryllium ND ug/L 1 06/04/12 19:59 7440-41-706/01/12 11:301.0
Cadmium ND ug/L 1 06/04/12 19:59 7440-43-906/01/12 11:301.0
Chromium ND ug/L 1 06/04/12 19:59 7440-47-306/01/12 11:305.0
Copper ND ug/L 1 06/04/12 19:59 7440-50-806/01/12 11:305.0
Lead ND ug/L 1 06/04/12 19:59 7439-92-106/01/12 11:305.0
Manganese 41.0 ug/L 1 06/04/12 19:59 7439-96-506/01/12 11:305.0
Nickel ND ug/L 1 06/04/12 19:59 7440-02-006/01/12 11:305.0
Selenium ND ug/L 1 06/04/12 19:59 7782-49-206/01/12 11:3010.0
Silver ND ug/L 1 06/04/12 19:59 7440-22-406/01/12 11:305.0
Thallium ND ug/L 1 06/04/12 19:59 7440-28-006/01/12 11:3010.0
Total Hardness 118000 ug/L 1 06/04/12 19:5906/01/12 11:30
Zinc ND ug/L 1 06/04/12 19:59 7440-66-606/01/12 11:3010.0
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D
Fecal Coliforms 890 CFU/100 mL 1 05/31/12 14:39 N2,u11.0
MBIO Total Coliform CHT Analytical Method: SM 9223 Preparation Method: SM 9223
Fecal/E. coli PRESENT 1 06/01/12 15:46 N205/31/12 15:32
Total Coliforms PRESENT 1 06/01/12 15:46 N205/31/12 15:32
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 06/07/12 12:34 7439-97-606/06/12 17:500.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 06/04/12 15:39 83-32-906/01/12 16:0010.0
Acenaphthylene ND ug/L 1 06/04/12 15:39 208-96-806/01/12 16:0010.0
Aniline ND ug/L 1 06/04/12 15:39 62-53-306/01/12 16:0010.0
Anthracene ND ug/L 1 06/04/12 15:39 120-12-706/01/12 16:0010.0
Benzo(a)anthracene ND ug/L 1 06/04/12 15:39 56-55-306/01/12 16:0010.0
Benzo(a)pyrene ND ug/L 1 06/04/12 15:39 50-32-806/01/12 16:0010.0
Benzo(b)fluoranthene ND ug/L 1 06/04/12 15:39 205-99-206/01/12 16:0010.0
Benzo(g,h,i)perylene ND ug/L 1 06/04/12 15:39 191-24-206/01/12 16:0010.0
Benzo(k)fluoranthene ND ug/L 1 06/04/12 15:39 207-08-906/01/12 16:0010.0
Benzoic Acid ND ug/L 1 06/04/12 15:39 65-85-006/01/12 16:0050.0
Benzyl alcohol ND ug/L 1 06/04/12 15:39 100-51-606/01/12 16:0020.0
4-Bromophenylphenyl ether ND ug/L 1 06/04/12 15:39 101-55-306/01/12 16:0010.0
Butylbenzylphthalate ND ug/L 1 06/04/12 15:39 85-68-706/01/12 16:0010.0
4-Chloro-3-methylphenol ND ug/L 1 06/04/12 15:39 59-50-706/01/12 16:0020.0
4-Chloroaniline ND ug/L 1 06/04/12 15:39 106-47-806/01/12 16:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 06/04/12 15:39 111-91-106/01/12 16:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 06/04/12 15:39 111-44-406/01/12 16:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/04/12 15:39 108-60-106/01/12 16:0010.0
2-Chloronaphthalene ND ug/L 1 06/04/12 15:39 91-58-706/01/12 16:0010.0
2-Chlorophenol ND ug/L 1 06/04/12 15:39 95-57-806/01/12 16:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 06/04/12 15:39 7005-72-306/01/12 16:0010.0
Chrysene ND ug/L 1 06/04/12 15:39 218-01-906/01/12 16:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 24 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682005 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Dibenz(a,h)anthracene ND ug/L 1 06/04/12 15:39 53-70-306/01/12 16:0010.0
Dibenzofuran ND ug/L 1 06/04/12 15:39 132-64-906/01/12 16:0010.0
1,2-Dichlorobenzene ND ug/L 1 06/04/12 15:39 95-50-106/01/12 16:0010.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 15:39 541-73-106/01/12 16:0010.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 15:39 106-46-706/01/12 16:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 06/04/12 15:39 91-94-106/01/12 16:0020.0
2,4-Dichlorophenol ND ug/L 1 06/04/12 15:39 120-83-206/01/12 16:0010.0
Diethylphthalate ND ug/L 1 06/04/12 15:39 84-66-206/01/12 16:0010.0
2,4-Dimethylphenol ND ug/L 1 06/04/12 15:39 105-67-906/01/12 16:0010.0
Dimethylphthalate ND ug/L 1 06/04/12 15:39 131-11-306/01/12 16:0010.0
Di-n-butylphthalate ND ug/L 1 06/04/12 15:39 84-74-206/01/12 16:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 06/04/12 15:39 534-52-106/01/12 16:0020.0
2,4-Dinitrophenol ND ug/L 1 06/04/12 15:39 51-28-506/01/12 16:0050.0
2,4-Dinitrotoluene ND ug/L 1 06/04/12 15:39 121-14-206/01/12 16:0010.0
2,6-Dinitrotoluene ND ug/L 1 06/04/12 15:39 606-20-206/01/12 16:0010.0
Di-n-octylphthalate ND ug/L 1 06/04/12 15:39 117-84-006/01/12 16:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/04/12 15:39 117-81-706/01/12 16:006.0
Fluoranthene ND ug/L 1 06/04/12 15:39 206-44-006/01/12 16:0010.0
Fluorene ND ug/L 1 06/04/12 15:39 86-73-706/01/12 16:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 15:39 87-68-306/01/12 16:0010.0
Hexachlorobenzene ND ug/L 1 06/04/12 15:39 118-74-106/01/12 16:0010.0
Hexachlorocyclopentadiene ND ug/L 1 06/04/12 15:39 77-47-406/01/12 16:0010.0
Hexachloroethane ND ug/L 1 06/04/12 15:39 67-72-106/01/12 16:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/04/12 15:39 193-39-506/01/12 16:0010.0
Isophorone ND ug/L 1 06/04/12 15:39 78-59-106/01/12 16:0010.0
1-Methylnaphthalene ND ug/L 1 06/04/12 15:39 90-12-006/01/12 16:0010.0
2-Methylnaphthalene ND ug/L 1 06/04/12 15:39 91-57-606/01/12 16:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 06/04/12 15:39 95-48-706/01/12 16:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 06/04/12 15:3906/01/12 16:0010.0
Naphthalene ND ug/L 1 06/04/12 15:39 91-20-306/01/12 16:0010.0
2-Nitroaniline ND ug/L 1 06/04/12 15:39 88-74-406/01/12 16:0050.0
3-Nitroaniline ND ug/L 1 06/04/12 15:39 99-09-206/01/12 16:0050.0
4-Nitroaniline ND ug/L 1 06/04/12 15:39 100-01-606/01/12 16:0020.0
Nitrobenzene ND ug/L 1 06/04/12 15:39 98-95-306/01/12 16:0010.0
2-Nitrophenol ND ug/L 1 06/04/12 15:39 88-75-506/01/12 16:0010.0
4-Nitrophenol ND ug/L 1 06/04/12 15:39 100-02-706/01/12 16:0050.0
N-Nitrosodimethylamine ND ug/L 1 06/04/12 15:39 62-75-906/01/12 16:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 06/04/12 15:39 621-64-706/01/12 16:0010.0
N-Nitrosodiphenylamine ND ug/L 1 06/04/12 15:39 86-30-606/01/12 16:0010.0
Pentachlorophenol ND ug/L 1 06/04/12 15:39 87-86-506/01/12 16:0025.0
Phenanthrene ND ug/L 1 06/04/12 15:39 85-01-806/01/12 16:0010.0
Phenol ND ug/L 1 06/04/12 15:39 108-95-206/01/12 16:0010.0
Pyrene ND ug/L 1 06/04/12 15:39 129-00-006/01/12 16:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 15:39 120-82-106/01/12 16:0010.0
2,4,5-Trichlorophenol ND ug/L 1 06/04/12 15:39 95-95-406/01/12 16:0010.0
2,4,6-Trichlorophenol ND ug/L 1 06/04/12 15:39 88-06-206/01/12 16:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 25 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682005 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Surrogates
Nitrobenzene-d5 (S)65 %1 06/04/12 15:39 4165-60-006/01/12 16:0021-110
2-Fluorobiphenyl (S)71 %1 06/04/12 15:39 321-60-806/01/12 16:0027-110
Terphenyl-d14 (S)99 %1 06/04/12 15:39 1718-51-006/01/12 16:0031-107
Phenol-d6 (S)19 %1 06/04/12 15:39 13127-88-306/01/12 16:0010-110
2-Fluorophenol (S)36 %1 06/04/12 15:39 367-12-406/01/12 16:0012-110
2,4,6-Tribromophenol (S)75 %1 06/04/12 15:39 118-79-606/01/12 16:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 06/04/12 16:27 67-64-125.0
Benzene ND ug/L 1 06/04/12 16:27 71-43-21.0
Bromobenzene ND ug/L 1 06/04/12 16:27 108-86-11.0
Bromochloromethane ND ug/L 1 06/04/12 16:27 74-97-51.0
Bromodichloromethane ND ug/L 1 06/04/12 16:27 75-27-41.0
Bromoform ND ug/L 1 06/04/12 16:27 75-25-21.0
Bromomethane ND ug/L 1 06/04/12 16:27 74-83-92.0
2-Butanone (MEK)ND ug/L 1 06/04/12 16:27 78-93-35.0
Carbon tetrachloride ND ug/L 1 06/04/12 16:27 56-23-51.0
Chlorobenzene ND ug/L 1 06/04/12 16:27 108-90-71.0
Chloroethane ND ug/L 1 06/04/12 16:27 75-00-31.0
Chloroform ND ug/L 1 06/04/12 16:27 67-66-31.0
Chloromethane ND ug/L 1 06/04/12 16:27 74-87-31.0
2-Chlorotoluene ND ug/L 1 06/04/12 16:27 95-49-81.0
4-Chlorotoluene ND ug/L 1 06/04/12 16:27 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 06/04/12 16:27 96-12-85.0
Dibromochloromethane ND ug/L 1 06/04/12 16:27 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 06/04/12 16:27 106-93-41.0
Dibromomethane ND ug/L 1 06/04/12 16:27 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 06/04/12 16:27 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 16:27 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 16:27 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 06/04/12 16:27 75-71-81.0
1,1-Dichloroethane ND ug/L 1 06/04/12 16:27 75-34-31.0
1,2-Dichloroethane ND ug/L 1 06/04/12 16:27 107-06-21.0
1,1-Dichloroethene ND ug/L 1 06/04/12 16:27 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 06/04/12 16:27 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 06/04/12 16:27 156-60-51.0
1,2-Dichloropropane ND ug/L 1 06/04/12 16:27 78-87-51.0
1,3-Dichloropropane ND ug/L 1 06/04/12 16:27 142-28-91.0
2,2-Dichloropropane ND ug/L 1 06/04/12 16:27 594-20-71.0
1,1-Dichloropropene ND ug/L 1 06/04/12 16:27 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 06/04/12 16:27 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 06/04/12 16:27 10061-02-61.0
Diisopropyl ether ND ug/L 1 06/04/12 16:27 108-20-31.0
Ethylbenzene ND ug/L 1 06/04/12 16:27 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 16:27 87-68-31.0
2-Hexanone ND ug/L 1 06/04/12 16:27 591-78-65.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 26 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682005 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
p-Isopropyltoluene ND ug/L 1 06/04/12 16:27 99-87-61.0
Methylene Chloride ND ug/L 1 06/04/12 16:27 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/04/12 16:27 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 06/04/12 16:27 1634-04-41.0
Naphthalene ND ug/L 1 06/04/12 16:27 91-20-31.0
Styrene ND ug/L 1 06/04/12 16:27 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 06/04/12 16:27 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 06/04/12 16:27 79-34-51.0
Tetrachloroethene ND ug/L 1 06/04/12 16:27 127-18-41.0
Toluene ND ug/L 1 06/04/12 16:27 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 06/04/12 16:27 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 16:27 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 06/04/12 16:27 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 06/04/12 16:27 79-00-51.0
Trichloroethene ND ug/L 1 06/04/12 16:27 79-01-61.0
Trichlorofluoromethane ND ug/L 1 06/04/12 16:27 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 06/04/12 16:27 96-18-41.0
Vinyl acetate ND ug/L 1 06/04/12 16:27 108-05-42.0
Vinyl chloride ND ug/L 1 06/04/12 16:27 75-01-41.0
m&p-Xylene ND ug/L 1 06/04/12 16:27 179601-23-12.0
o-Xylene ND ug/L 1 06/04/12 16:27 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)102 %1 06/04/12 16:27 460-00-470-130
Dibromofluoromethane (S)102 %1 06/04/12 16:27 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 06/04/12 16:27 17060-07-070-130
Toluene-d8 (S)100 %1 06/04/12 16:27 2037-26-570-130
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 3.6 NTU 1 06/01/12 00:501.0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 1 06/01/12 22:512.5
5210B BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day ND mg/L 1 06/06/12 17:5006/01/12 20:552.0
350.1 Ammonia Analytical Method: EPA 350.1
Nitrogen, Ammonia ND mg/L 1 06/05/12 13:44 7664-41-70.10
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total ND mg/L 1 06/02/12 09:39 7727-37-90.50
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2
Nitrogen, Nitrate 0.61 mg/L 1 06/01/12 00:570.020
Nitrogen, Nitrite ND mg/L 1 06/01/12 00:570.020
Nitrogen, NO2 plus NO3 0.61 mg/L 1 06/01/12 00:570.020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 27 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:SS Lab ID:92119682005 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus ND mg/L 1 06/03/12 08:50 7723-14-00.050
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 1 06/06/12 21:0525.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196
Chromium, Hexavalent ND mg/L 1 05/31/12 22:21 18540-29-9 N20.050
Sample:US Lab ID:92119682006 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
HEM, Oil and Grease Analytical Method: EPA 1664A
Oil and Grease ND mg/L 1 06/04/12 14:585.0
6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C
Antimony ND ug/L 1 06/04/12 20:03 7440-36-006/01/12 11:305.0
Arsenic ND ug/L 1 06/04/12 20:03 7440-38-206/01/12 11:305.0
Beryllium ND ug/L 1 06/04/12 20:03 7440-41-706/01/12 11:301.0
Cadmium ND ug/L 1 06/04/12 20:03 7440-43-906/01/12 11:301.0
Chromium ND ug/L 1 06/04/12 20:03 7440-47-306/01/12 11:305.0
Copper ND ug/L 1 06/04/12 20:03 7440-50-806/01/12 11:305.0
Lead ND ug/L 1 06/04/12 20:03 7439-92-106/01/12 11:305.0
Manganese 31.1 ug/L 1 06/04/12 20:03 7439-96-506/01/12 11:305.0
Nickel ND ug/L 1 06/04/12 20:03 7440-02-006/01/12 11:305.0
Selenium ND ug/L 1 06/04/12 20:03 7782-49-206/01/12 11:3010.0
Silver ND ug/L 1 06/04/12 20:03 7440-22-406/01/12 11:305.0
Thallium ND ug/L 1 06/04/12 20:03 7440-28-006/01/12 11:3010.0
Total Hardness 115000 ug/L 1 06/04/12 20:0306/01/12 11:30
Zinc ND ug/L 1 06/04/12 20:03 7440-66-606/01/12 11:3010.0
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D
Fecal Coliforms 590 CFU/100 mL 1 05/31/12 14:39 N21.0
MBIO Total Coliform CHT Analytical Method: SM 9223 Preparation Method: SM 9223
Fecal/E. coli PRESENT 1 06/01/12 15:46 N205/31/12 15:32
Total Coliforms PRESENT 1 06/01/12 15:46 N205/31/12 15:32
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 06/07/12 12:37 7439-97-606/06/12 17:500.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 06/04/12 16:07 83-32-906/01/12 16:0010.0
Acenaphthylene ND ug/L 1 06/04/12 16:07 208-96-806/01/12 16:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 28 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682006 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Aniline ND ug/L 1 06/04/12 16:07 62-53-306/01/12 16:0010.0
Anthracene ND ug/L 1 06/04/12 16:07 120-12-706/01/12 16:0010.0
Benzo(a)anthracene ND ug/L 1 06/04/12 16:07 56-55-306/01/12 16:0010.0
Benzo(a)pyrene ND ug/L 1 06/04/12 16:07 50-32-806/01/12 16:0010.0
Benzo(b)fluoranthene ND ug/L 1 06/04/12 16:07 205-99-206/01/12 16:0010.0
Benzo(g,h,i)perylene ND ug/L 1 06/04/12 16:07 191-24-206/01/12 16:0010.0
Benzo(k)fluoranthene ND ug/L 1 06/04/12 16:07 207-08-906/01/12 16:0010.0
Benzoic Acid ND ug/L 1 06/04/12 16:07 65-85-006/01/12 16:0050.0
Benzyl alcohol ND ug/L 1 06/04/12 16:07 100-51-606/01/12 16:0020.0
4-Bromophenylphenyl ether ND ug/L 1 06/04/12 16:07 101-55-306/01/12 16:0010.0
Butylbenzylphthalate ND ug/L 1 06/04/12 16:07 85-68-706/01/12 16:0010.0
4-Chloro-3-methylphenol ND ug/L 1 06/04/12 16:07 59-50-706/01/12 16:0020.0
4-Chloroaniline ND ug/L 1 06/04/12 16:07 106-47-806/01/12 16:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 06/04/12 16:07 111-91-106/01/12 16:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 06/04/12 16:07 111-44-406/01/12 16:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/04/12 16:07 108-60-106/01/12 16:0010.0
2-Chloronaphthalene ND ug/L 1 06/04/12 16:07 91-58-706/01/12 16:0010.0
2-Chlorophenol ND ug/L 1 06/04/12 16:07 95-57-806/01/12 16:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 06/04/12 16:07 7005-72-306/01/12 16:0010.0
Chrysene ND ug/L 1 06/04/12 16:07 218-01-906/01/12 16:0010.0
Dibenz(a,h)anthracene ND ug/L 1 06/04/12 16:07 53-70-306/01/12 16:0010.0
Dibenzofuran ND ug/L 1 06/04/12 16:07 132-64-906/01/12 16:0010.0
1,2-Dichlorobenzene ND ug/L 1 06/04/12 16:07 95-50-106/01/12 16:0010.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 16:07 541-73-106/01/12 16:0010.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 16:07 106-46-706/01/12 16:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 06/04/12 16:07 91-94-106/01/12 16:0020.0
2,4-Dichlorophenol ND ug/L 1 06/04/12 16:07 120-83-206/01/12 16:0010.0
Diethylphthalate ND ug/L 1 06/04/12 16:07 84-66-206/01/12 16:0010.0
2,4-Dimethylphenol ND ug/L 1 06/04/12 16:07 105-67-906/01/12 16:0010.0
Dimethylphthalate ND ug/L 1 06/04/12 16:07 131-11-306/01/12 16:0010.0
Di-n-butylphthalate ND ug/L 1 06/04/12 16:07 84-74-206/01/12 16:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 06/04/12 16:07 534-52-106/01/12 16:0020.0
2,4-Dinitrophenol ND ug/L 1 06/04/12 16:07 51-28-506/01/12 16:0050.0
2,4-Dinitrotoluene ND ug/L 1 06/04/12 16:07 121-14-206/01/12 16:0010.0
2,6-Dinitrotoluene ND ug/L 1 06/04/12 16:07 606-20-206/01/12 16:0010.0
Di-n-octylphthalate ND ug/L 1 06/04/12 16:07 117-84-006/01/12 16:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/04/12 16:07 117-81-706/01/12 16:006.0
Fluoranthene ND ug/L 1 06/04/12 16:07 206-44-006/01/12 16:0010.0
Fluorene ND ug/L 1 06/04/12 16:07 86-73-706/01/12 16:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 16:07 87-68-306/01/12 16:0010.0
Hexachlorobenzene ND ug/L 1 06/04/12 16:07 118-74-106/01/12 16:0010.0
Hexachlorocyclopentadiene ND ug/L 1 06/04/12 16:07 77-47-406/01/12 16:0010.0
Hexachloroethane ND ug/L 1 06/04/12 16:07 67-72-106/01/12 16:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/04/12 16:07 193-39-506/01/12 16:0010.0
Isophorone ND ug/L 1 06/04/12 16:07 78-59-106/01/12 16:0010.0
1-Methylnaphthalene ND ug/L 1 06/04/12 16:07 90-12-006/01/12 16:0010.0
2-Methylnaphthalene ND ug/L 1 06/04/12 16:07 91-57-606/01/12 16:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 29 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682006 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Methylphenol(o-Cresol)ND ug/L 1 06/04/12 16:07 95-48-706/01/12 16:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 06/04/12 16:0706/01/12 16:0010.0
Naphthalene ND ug/L 1 06/04/12 16:07 91-20-306/01/12 16:0010.0
2-Nitroaniline ND ug/L 1 06/04/12 16:07 88-74-406/01/12 16:0050.0
3-Nitroaniline ND ug/L 1 06/04/12 16:07 99-09-206/01/12 16:0050.0
4-Nitroaniline ND ug/L 1 06/04/12 16:07 100-01-606/01/12 16:0020.0
Nitrobenzene ND ug/L 1 06/04/12 16:07 98-95-306/01/12 16:0010.0
2-Nitrophenol ND ug/L 1 06/04/12 16:07 88-75-506/01/12 16:0010.0
4-Nitrophenol ND ug/L 1 06/04/12 16:07 100-02-706/01/12 16:0050.0
N-Nitrosodimethylamine ND ug/L 1 06/04/12 16:07 62-75-906/01/12 16:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 06/04/12 16:07 621-64-706/01/12 16:0010.0
N-Nitrosodiphenylamine ND ug/L 1 06/04/12 16:07 86-30-606/01/12 16:0010.0
Pentachlorophenol ND ug/L 1 06/04/12 16:07 87-86-506/01/12 16:0025.0
Phenanthrene ND ug/L 1 06/04/12 16:07 85-01-806/01/12 16:0010.0
Phenol ND ug/L 1 06/04/12 16:07 108-95-206/01/12 16:0010.0
Pyrene ND ug/L 1 06/04/12 16:07 129-00-006/01/12 16:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 16:07 120-82-106/01/12 16:0010.0
2,4,5-Trichlorophenol ND ug/L 1 06/04/12 16:07 95-95-406/01/12 16:0010.0
2,4,6-Trichlorophenol ND ug/L 1 06/04/12 16:07 88-06-206/01/12 16:0010.0
Surrogates
Nitrobenzene-d5 (S)69 %1 06/04/12 16:07 4165-60-006/01/12 16:0021-110
2-Fluorobiphenyl (S)70 %1 06/04/12 16:07 321-60-806/01/12 16:0027-110
Terphenyl-d14 (S)104 %1 06/04/12 16:07 1718-51-006/01/12 16:0031-107
Phenol-d6 (S)24 %1 06/04/12 16:07 13127-88-306/01/12 16:0010-110
2-Fluorophenol (S)37 %1 06/04/12 16:07 367-12-406/01/12 16:0012-110
2,4,6-Tribromophenol (S)78 %1 06/04/12 16:07 118-79-606/01/12 16:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 06/04/12 16:42 67-64-125.0
Benzene ND ug/L 1 06/04/12 16:42 71-43-21.0
Bromobenzene ND ug/L 1 06/04/12 16:42 108-86-11.0
Bromochloromethane ND ug/L 1 06/04/12 16:42 74-97-51.0
Bromodichloromethane ND ug/L 1 06/04/12 16:42 75-27-41.0
Bromoform ND ug/L 1 06/04/12 16:42 75-25-21.0
Bromomethane ND ug/L 1 06/04/12 16:42 74-83-92.0
2-Butanone (MEK)ND ug/L 1 06/04/12 16:42 78-93-35.0
Carbon tetrachloride ND ug/L 1 06/04/12 16:42 56-23-51.0
Chlorobenzene ND ug/L 1 06/04/12 16:42 108-90-71.0
Chloroethane ND ug/L 1 06/04/12 16:42 75-00-31.0
Chloroform ND ug/L 1 06/04/12 16:42 67-66-31.0
Chloromethane ND ug/L 1 06/04/12 16:42 74-87-31.0
2-Chlorotoluene ND ug/L 1 06/04/12 16:42 95-49-81.0
4-Chlorotoluene ND ug/L 1 06/04/12 16:42 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 06/04/12 16:42 96-12-85.0
Dibromochloromethane ND ug/L 1 06/04/12 16:42 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 06/04/12 16:42 106-93-41.0
Dibromomethane ND ug/L 1 06/04/12 16:42 74-95-31.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 30 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682006 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene ND ug/L 1 06/04/12 16:42 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 16:42 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 16:42 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 06/04/12 16:42 75-71-81.0
1,1-Dichloroethane ND ug/L 1 06/04/12 16:42 75-34-31.0
1,2-Dichloroethane ND ug/L 1 06/04/12 16:42 107-06-21.0
1,1-Dichloroethene ND ug/L 1 06/04/12 16:42 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 06/04/12 16:42 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 06/04/12 16:42 156-60-51.0
1,2-Dichloropropane ND ug/L 1 06/04/12 16:42 78-87-51.0
1,3-Dichloropropane ND ug/L 1 06/04/12 16:42 142-28-91.0
2,2-Dichloropropane ND ug/L 1 06/04/12 16:42 594-20-71.0
1,1-Dichloropropene ND ug/L 1 06/04/12 16:42 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 06/04/12 16:42 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 06/04/12 16:42 10061-02-61.0
Diisopropyl ether ND ug/L 1 06/04/12 16:42 108-20-31.0
Ethylbenzene ND ug/L 1 06/04/12 16:42 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 16:42 87-68-31.0
2-Hexanone ND ug/L 1 06/04/12 16:42 591-78-65.0
p-Isopropyltoluene ND ug/L 1 06/04/12 16:42 99-87-61.0
Methylene Chloride ND ug/L 1 06/04/12 16:42 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/04/12 16:42 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 06/04/12 16:42 1634-04-41.0
Naphthalene ND ug/L 1 06/04/12 16:42 91-20-31.0
Styrene ND ug/L 1 06/04/12 16:42 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 06/04/12 16:42 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 06/04/12 16:42 79-34-51.0
Tetrachloroethene ND ug/L 1 06/04/12 16:42 127-18-41.0
Toluene ND ug/L 1 06/04/12 16:42 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 06/04/12 16:42 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 16:42 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 06/04/12 16:42 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 06/04/12 16:42 79-00-51.0
Trichloroethene ND ug/L 1 06/04/12 16:42 79-01-61.0
Trichlorofluoromethane ND ug/L 1 06/04/12 16:42 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 06/04/12 16:42 96-18-41.0
Vinyl acetate ND ug/L 1 06/04/12 16:42 108-05-42.0
Vinyl chloride ND ug/L 1 06/04/12 16:42 75-01-41.0
m&p-Xylene ND ug/L 1 06/04/12 16:42 179601-23-12.0
o-Xylene ND ug/L 1 06/04/12 16:42 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)100 %1 06/04/12 16:42 460-00-470-130
Dibromofluoromethane (S)110 %1 06/04/12 16:42 1868-53-770-130
1,2-Dichloroethane-d4 (S)108 %1 06/04/12 16:42 17060-07-070-130
Toluene-d8 (S)100 %1 06/04/12 16:42 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 31 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:US Lab ID:92119682006 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 4.0 NTU 1 06/01/12 00:501.0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 1 06/01/12 22:522.9
5210B BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day ND mg/L 1 06/06/12 17:5006/01/12 20:552.0
350.1 Ammonia Analytical Method: EPA 350.1
Nitrogen, Ammonia ND mg/L 1 06/05/12 13:46 7664-41-70.10
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total ND mg/L 1 06/02/12 10:16 7727-37-90.50
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2
Nitrogen, Nitrate 0.63 mg/L 1 06/01/12 00:580.020
Nitrogen, Nitrite ND mg/L 1 06/01/12 00:580.020
Nitrogen, NO2 plus NO3 0.63 mg/L 1 06/01/12 00:580.020
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus ND mg/L 1 06/03/12 08:51 7723-14-00.050
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 1 06/06/12 21:0525.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196
Chromium, Hexavalent ND mg/L 1 05/31/12 22:21 18540-29-9 N20.050
Sample:FIELD BLANK Lab ID:92119682007 Collected:05/31/12 12:45 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C
Antimony ND ug/L 1 06/04/12 20:06 7440-36-006/01/12 11:305.0
Arsenic ND ug/L 1 06/04/12 20:06 7440-38-206/01/12 11:305.0
Beryllium ND ug/L 1 06/04/12 20:06 7440-41-706/01/12 11:301.0
Cadmium ND ug/L 1 06/04/12 20:06 7440-43-906/01/12 11:301.0
Chromium ND ug/L 1 06/04/12 20:06 7440-47-306/01/12 11:305.0
Copper ND ug/L 1 06/04/12 20:06 7440-50-806/01/12 11:305.0
Lead ND ug/L 1 06/04/12 20:06 7439-92-106/01/12 11:305.0
Manganese ND ug/L 1 06/04/12 20:06 7439-96-506/01/12 11:305.0
Nickel ND ug/L 1 06/04/12 20:06 7440-02-006/01/12 11:305.0
Selenium ND ug/L 1 06/04/12 20:06 7782-49-206/01/12 11:3010.0
Silver ND ug/L 1 06/04/12 20:06 7440-22-406/01/12 11:305.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 32 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:FIELD BLANK Lab ID:92119682007 Collected:05/31/12 12:45 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C
Thallium ND ug/L 1 06/04/12 20:06 7440-28-006/01/12 11:3010.0
Total Hardness 150 ug/L 1 06/04/12 20:0606/01/12 11:30
Zinc ND ug/L 1 06/04/12 20:06 7440-66-606/01/12 11:3010.0
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 06/07/12 12:40 7439-97-606/06/12 17:500.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 06/06/12 18:34 83-32-906/05/12 14:0010.0
Acenaphthylene ND ug/L 1 06/06/12 18:34 208-96-806/05/12 14:0010.0
Aniline ND ug/L 1 06/06/12 18:34 62-53-306/05/12 14:0010.0
Anthracene ND ug/L 1 06/06/12 18:34 120-12-706/05/12 14:0010.0
Benzo(a)anthracene ND ug/L 1 06/06/12 18:34 56-55-306/05/12 14:0010.0
Benzo(a)pyrene ND ug/L 1 06/06/12 18:34 50-32-806/05/12 14:0010.0
Benzo(b)fluoranthene ND ug/L 1 06/06/12 18:34 205-99-206/05/12 14:0010.0
Benzo(g,h,i)perylene ND ug/L 1 06/06/12 18:34 191-24-206/05/12 14:0010.0
Benzo(k)fluoranthene ND ug/L 1 06/06/12 18:34 207-08-906/05/12 14:0010.0
Benzoic Acid ND ug/L 1 06/06/12 18:34 65-85-006/05/12 14:0050.0
Benzyl alcohol ND ug/L 1 06/06/12 18:34 100-51-606/05/12 14:0020.0
4-Bromophenylphenyl ether ND ug/L 1 06/06/12 18:34 101-55-306/05/12 14:0010.0
Butylbenzylphthalate ND ug/L 1 06/06/12 18:34 85-68-706/05/12 14:0010.0
4-Chloro-3-methylphenol ND ug/L 1 06/06/12 18:34 59-50-706/05/12 14:0020.0
4-Chloroaniline ND ug/L 1 06/06/12 18:34 106-47-806/05/12 14:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 06/06/12 18:34 111-91-106/05/12 14:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 06/06/12 18:34 111-44-406/05/12 14:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/06/12 18:34 108-60-106/05/12 14:0010.0
2-Chloronaphthalene ND ug/L 1 06/06/12 18:34 91-58-706/05/12 14:0010.0
2-Chlorophenol ND ug/L 1 06/06/12 18:34 95-57-806/05/12 14:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 06/06/12 18:34 7005-72-306/05/12 14:0010.0
Chrysene ND ug/L 1 06/06/12 18:34 218-01-906/05/12 14:0010.0
Dibenz(a,h)anthracene ND ug/L 1 06/06/12 18:34 53-70-306/05/12 14:0010.0
Dibenzofuran ND ug/L 1 06/06/12 18:34 132-64-906/05/12 14:0010.0
1,2-Dichlorobenzene ND ug/L 1 06/06/12 18:34 95-50-106/05/12 14:0010.0
1,3-Dichlorobenzene ND ug/L 1 06/06/12 18:34 541-73-106/05/12 14:0010.0
1,4-Dichlorobenzene ND ug/L 1 06/06/12 18:34 106-46-706/05/12 14:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 06/06/12 18:34 91-94-106/05/12 14:0020.0
2,4-Dichlorophenol ND ug/L 1 06/06/12 18:34 120-83-206/05/12 14:0010.0
Diethylphthalate ND ug/L 1 06/06/12 18:34 84-66-206/05/12 14:0010.0
2,4-Dimethylphenol ND ug/L 1 06/06/12 18:34 105-67-906/05/12 14:0010.0
Dimethylphthalate ND ug/L 1 06/06/12 18:34 131-11-306/05/12 14:0010.0
Di-n-butylphthalate ND ug/L 1 06/06/12 18:34 84-74-206/05/12 14:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 06/06/12 18:34 534-52-106/05/12 14:0020.0
2,4-Dinitrophenol ND ug/L 1 06/06/12 18:34 51-28-506/05/12 14:0050.0
2,4-Dinitrotoluene ND ug/L 1 06/06/12 18:34 121-14-206/05/12 14:0010.0
2,6-Dinitrotoluene ND ug/L 1 06/06/12 18:34 606-20-206/05/12 14:0010.0
Di-n-octylphthalate ND ug/L 1 06/06/12 18:34 117-84-006/05/12 14:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 33 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:FIELD BLANK Lab ID:92119682007 Collected:05/31/12 12:45 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/06/12 18:34 117-81-706/05/12 14:006.0
Fluoranthene ND ug/L 1 06/06/12 18:34 206-44-006/05/12 14:0010.0
Fluorene ND ug/L 1 06/06/12 18:34 86-73-706/05/12 14:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 06/06/12 18:34 87-68-306/05/12 14:0010.0
Hexachlorobenzene ND ug/L 1 06/06/12 18:34 118-74-106/05/12 14:0010.0
Hexachlorocyclopentadiene ND ug/L 1 06/06/12 18:34 77-47-406/05/12 14:0010.0
Hexachloroethane ND ug/L 1 06/06/12 18:34 67-72-106/05/12 14:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/06/12 18:34 193-39-506/05/12 14:0010.0
Isophorone ND ug/L 1 06/06/12 18:34 78-59-106/05/12 14:0010.0
1-Methylnaphthalene ND ug/L 1 06/06/12 18:34 90-12-006/05/12 14:0010.0
2-Methylnaphthalene ND ug/L 1 06/06/12 18:34 91-57-606/05/12 14:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 06/06/12 18:34 95-48-706/05/12 14:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 06/06/12 18:3406/05/12 14:0010.0
Naphthalene ND ug/L 1 06/06/12 18:34 91-20-306/05/12 14:0010.0
2-Nitroaniline ND ug/L 1 06/06/12 18:34 88-74-406/05/12 14:0050.0
3-Nitroaniline ND ug/L 1 06/06/12 18:34 99-09-206/05/12 14:0050.0
4-Nitroaniline ND ug/L 1 06/06/12 18:34 100-01-606/05/12 14:0020.0
Nitrobenzene ND ug/L 1 06/06/12 18:34 98-95-306/05/12 14:0010.0
2-Nitrophenol ND ug/L 1 06/06/12 18:34 88-75-506/05/12 14:0010.0
4-Nitrophenol ND ug/L 1 06/06/12 18:34 100-02-706/05/12 14:0050.0
N-Nitrosodimethylamine ND ug/L 1 06/06/12 18:34 62-75-906/05/12 14:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 06/06/12 18:34 621-64-706/05/12 14:0010.0
N-Nitrosodiphenylamine ND ug/L 1 06/06/12 18:34 86-30-606/05/12 14:0010.0
Pentachlorophenol ND ug/L 1 06/06/12 18:34 87-86-506/05/12 14:0025.0
Phenanthrene ND ug/L 1 06/06/12 18:34 85-01-806/05/12 14:0010.0
Phenol ND ug/L 1 06/06/12 18:34 108-95-206/05/12 14:0010.0
Pyrene ND ug/L 1 06/06/12 18:34 129-00-006/05/12 14:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 06/06/12 18:34 120-82-106/05/12 14:0010.0
2,4,5-Trichlorophenol ND ug/L 1 06/06/12 18:34 95-95-406/05/12 14:0010.0
2,4,6-Trichlorophenol ND ug/L 1 06/06/12 18:34 88-06-206/05/12 14:0010.0
Surrogates
Nitrobenzene-d5 (S)78 %1 06/06/12 18:34 4165-60-006/05/12 14:0021-110
2-Fluorobiphenyl (S)80 %1 06/06/12 18:34 321-60-806/05/12 14:0027-110
Terphenyl-d14 (S)91 %1 06/06/12 18:34 1718-51-006/05/12 14:0031-107
Phenol-d6 (S)25 %1 06/06/12 18:34 13127-88-306/05/12 14:0010-110
2-Fluorophenol (S)39 %1 06/06/12 18:34 367-12-406/05/12 14:0012-110
2,4,6-Tribromophenol (S)91 %1 06/06/12 18:34 118-79-606/05/12 14:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 06/04/12 15:56 67-64-125.0
Benzene ND ug/L 1 06/04/12 15:56 71-43-21.0
Bromobenzene ND ug/L 1 06/04/12 15:56 108-86-11.0
Bromochloromethane ND ug/L 1 06/04/12 15:56 74-97-51.0
Bromodichloromethane ND ug/L 1 06/04/12 15:56 75-27-41.0
Bromoform ND ug/L 1 06/04/12 15:56 75-25-21.0
Bromomethane ND ug/L 1 06/04/12 15:56 74-83-92.0
2-Butanone (MEK)ND ug/L 1 06/04/12 15:56 78-93-35.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 34 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:FIELD BLANK Lab ID:92119682007 Collected:05/31/12 12:45 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Carbon tetrachloride ND ug/L 1 06/04/12 15:56 56-23-51.0
Chlorobenzene ND ug/L 1 06/04/12 15:56 108-90-71.0
Chloroethane ND ug/L 1 06/04/12 15:56 75-00-31.0
Chloroform ND ug/L 1 06/04/12 15:56 67-66-31.0
Chloromethane ND ug/L 1 06/04/12 15:56 74-87-31.0
2-Chlorotoluene ND ug/L 1 06/04/12 15:56 95-49-81.0
4-Chlorotoluene ND ug/L 1 06/04/12 15:56 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 06/04/12 15:56 96-12-85.0
Dibromochloromethane ND ug/L 1 06/04/12 15:56 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 06/04/12 15:56 106-93-41.0
Dibromomethane ND ug/L 1 06/04/12 15:56 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 06/04/12 15:56 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 06/04/12 15:56 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 06/04/12 15:56 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 06/04/12 15:56 75-71-81.0
1,1-Dichloroethane ND ug/L 1 06/04/12 15:56 75-34-31.0
1,2-Dichloroethane ND ug/L 1 06/04/12 15:56 107-06-21.0
1,1-Dichloroethene ND ug/L 1 06/04/12 15:56 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 06/04/12 15:56 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 06/04/12 15:56 156-60-51.0
1,2-Dichloropropane ND ug/L 1 06/04/12 15:56 78-87-51.0
1,3-Dichloropropane ND ug/L 1 06/04/12 15:56 142-28-91.0
2,2-Dichloropropane ND ug/L 1 06/04/12 15:56 594-20-71.0
1,1-Dichloropropene ND ug/L 1 06/04/12 15:56 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 06/04/12 15:56 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 06/04/12 15:56 10061-02-61.0
Diisopropyl ether ND ug/L 1 06/04/12 15:56 108-20-31.0
Ethylbenzene ND ug/L 1 06/04/12 15:56 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 06/04/12 15:56 87-68-31.0
2-Hexanone ND ug/L 1 06/04/12 15:56 591-78-65.0
p-Isopropyltoluene ND ug/L 1 06/04/12 15:56 99-87-61.0
Methylene Chloride ND ug/L 1 06/04/12 15:56 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/04/12 15:56 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 06/04/12 15:56 1634-04-41.0
Naphthalene ND ug/L 1 06/04/12 15:56 91-20-31.0
Styrene ND ug/L 1 06/04/12 15:56 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 06/04/12 15:56 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 06/04/12 15:56 79-34-51.0
Tetrachloroethene ND ug/L 1 06/04/12 15:56 127-18-41.0
Toluene ND ug/L 1 06/04/12 15:56 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 06/04/12 15:56 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 06/04/12 15:56 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 06/04/12 15:56 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 06/04/12 15:56 79-00-51.0
Trichloroethene ND ug/L 1 06/04/12 15:56 79-01-61.0
Trichlorofluoromethane ND ug/L 1 06/04/12 15:56 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 06/04/12 15:56 96-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 35 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Sample:FIELD BLANK Lab ID:92119682007 Collected:05/31/12 12:45 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Vinyl acetate ND ug/L 1 06/04/12 15:56 108-05-42.0
Vinyl chloride ND ug/L 1 06/04/12 15:56 75-01-41.0
m&p-Xylene ND ug/L 1 06/04/12 15:56 179601-23-12.0
o-Xylene ND ug/L 1 06/04/12 15:56 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)102 %1 06/04/12 15:56 460-00-470-130
Dibromofluoromethane (S)102 %1 06/04/12 15:56 1868-53-770-130
1,2-Dichloroethane-d4 (S)108 %1 06/04/12 15:56 17060-07-070-130
Toluene-d8 (S)98 %1 06/04/12 15:56 2037-26-570-130
7196 Chromium, Hexavalent Analytical Method: EPA 7196
Chromium, Hexavalent ND mg/L 1 05/31/12 22:21 18540-29-9 N20.050
Sample:DS-USGS SSC Lab ID:92119682008 Collected:05/31/12 10:31 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 1 06/01/12 22:522.7
Sample:SS-USGS SSC Lab ID:92119682009 Collected:05/31/12 11:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 1 06/04/12 16:472.5
Sample:US-USGS SSC Lab ID:92119682010 Collected:05/31/12 12:15 Received:05/31/12 14:18 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 1 06/04/12 16:472.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 36 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/12129
EPA 1664A
EPA 1664A
1664 HEM, Oil and Grease
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772582
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Oil and Grease mg/L ND 5.0 06/04/12 14:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772583LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/L 35.140 88 78-114
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
772584MATRIX SPIKE SAMPLE:
MSSpike
Result
5063691001
Oil and Grease mg/L 71.040 85 78-11437.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 37 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MBCH/4171
SM 9222D
SM 9222D
9222D MBIO Fecal Coliform - CHT
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771863
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Fecal Coliforms CFU/100 mL ND 1.0 N205/31/12 14:39
Parameter Units
Dup
Result QualifiersRPDResult
92119682006
771864SAMPLE DUPLICATE:
Fecal Coliforms CFU/100 mL 600 N22590
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 38 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/4268
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772562
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 06/07/12 12:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772563LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
772741MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92119682004
772742
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 105 75-125108 32.5ND 2.6 2.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 39 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/4264
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771499
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 06/05/12 15:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771500LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.074.067 112 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771501MATRIX SPIKE SAMPLE:
MSSpike
Result
92119682001
Mercury mg/kg 0.070.043 90 75-1250.031
Parameter Units
Dup
Result QualifiersRPDResult
92119682002
771502SAMPLE DUPLICATE:
Mercury mg/kg .0039JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 40 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/10716
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771442
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 06/02/12 14:31
Arsenic mg/kg ND 0.50 06/02/12 14:31
Beryllium mg/kg ND 0.10 06/02/12 14:31
Cadmium mg/kg ND 0.10 06/02/12 14:31
Chromium mg/kg ND 0.50 06/02/12 14:31
Copper mg/kg ND 0.50 06/02/12 14:31
Lead mg/kg ND 0.50 06/02/12 14:31
Manganese mg/kg ND 0.50 06/02/12 14:31
Nickel mg/kg ND 0.50 06/02/12 14:31
Selenium mg/kg ND 1.0 06/02/12 14:31
Silver mg/kg ND 0.50 06/02/12 14:31
Thallium mg/kg ND 1.0 06/02/12 14:31
Zinc mg/kg ND 1.0 06/02/12 14:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771443LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 47.850 96 80-120
Arsenic mg/kg 48.350 97 80-120
Beryllium mg/kg 49.450 99 80-120
Cadmium mg/kg 49.150 98 80-120
Chromium mg/kg 48.050 96 80-120
Copper mg/kg 48.250 96 80-120
Lead mg/kg 49.250 98 80-120
Manganese mg/kg 48.850 98 80-120
Nickel mg/kg 48.950 98 80-120
Selenium mg/kg 48.250 96 80-120
Silver mg/kg 24.525 98 80-120
Thallium mg/kg 48.150 96 80-120
Zinc mg/kg 48.150 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771444MATRIX SPIKE SAMPLE:
MSSpike
Result
92119645001
Antimony mg/kg 36.938.5 96 75-125ND
Arsenic mg/kg 39.938.5 104 75-125ND
Beryllium mg/kg 38.438.5 100 75-125ND
Cadmium mg/kg 34.938.5 91 75-125ND
Chromium mg/kg 75.4 M138.5 163 75-12512.7 ug/g
Copper mg/kg 278 M138.5 597 75-12547.9 ug/g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 41 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771444MATRIX SPIKE SAMPLE:
MSSpike
Result
92119645001
Lead mg/kg 44.538.5 107 75-1253.32 ug/g
Manganese mg/kg 41.538.5 96 75-1254.43 ug/g
Nickel mg/kg 44.038.5 96 75-1257.06 ug/g
Selenium mg/kg 50.238.5 125 75-1252.20 ug/g
Silver mg/kg 18.519.2 95 75-125ND
Thallium mg/kg 30.138.5 78 75-125ND
Zinc mg/kg 93.8 M138.5 30 75-12582.1 ug/g
Parameter Units
Dup
Result QualifiersRPDResult
92119645002
771445SAMPLE DUPLICATE:
Antimony mg/kg NDND
Arsenic mg/kg NDND
Beryllium mg/kg 0.43 190.519 ug/g
Cadmium mg/kg .063J0.250 ug/g
Chromium mg/kg 12.8 313.2 ug/g
Copper mg/kg 1.4 11.42 ug/g
Lead mg/kg 5.3 85.72 ug/g
Manganese mg/kg 64.8 1854.2 ug/g
Nickel mg/kg 5.3 D6478.61 ug/g
Selenium mg/kg 2.8 D6272.17 ug/g
Silver mg/kg .071JND
Thallium mg/kg NDND
Zinc mg/kg 17.9 D64528.3 ug/g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 42 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/10715
SM 3030C
EPA 6010
6010 MET 3030C
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771438
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 06/05/12 14:31
Arsenic ug/L ND 5.0 06/04/12 19:16
Beryllium ug/L ND 1.0 06/04/12 19:16
Cadmium ug/L ND 1.0 06/04/12 19:16
Chromium ug/L ND 5.0 06/04/12 19:16
Copper ug/L ND 5.0 06/04/12 19:16
Lead ug/L ND 5.0 06/04/12 19:16
Manganese ug/L ND 5.0 06/04/12 19:16
Nickel ug/L ND 5.0 06/04/12 19:16
Selenium ug/L ND 10.0 06/04/12 19:16
Silver ug/L ND 5.0 06/04/12 19:16
Thallium ug/L ND 10.0 06/04/12 19:16
Total Hardness ug/L 63.1 06/04/12 19:16
Zinc ug/L ND 10.0 06/04/12 19:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771439LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 494500 99 80-120
Arsenic ug/L 503500 101 80-120
Beryllium ug/L 523500 105 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 482500 96 80-120
Copper ug/L 478500 96 80-120
Lead ug/L 503500 101 80-120
Manganese ug/L 484500 97 80-120
Nickel ug/L 488500 98 80-120
Selenium ug/L 574500 115 80-120
Silver ug/L 249250 100 80-120
Thallium ug/L 406500 81 80-120
Total Hardness ug/L 33700
Zinc ug/L 537500 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771440MATRIX SPIKE SAMPLE:
MSSpike
Result
92119749020
Antimony ug/L 500500 99 75-1255.7
Arsenic ug/L 515500 103 75-125ND
Beryllium ug/L 510500 102 75-125ND
Cadmium ug/L 498500 100 75-125ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 43 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771440MATRIX SPIKE SAMPLE:
MSSpike
Result
92119749020
Chromium ug/L 596500 95 75-125120
Copper ug/L 488500 97 75-1252.1J
Lead ug/L 487500 97 75-125ND
Manganese ug/L 490500 95 75-12516.7
Nickel ug/L 480500 96 75-125ND
Selenium ug/L 545500 109 75-125ND
Silver ug/L 248250 99 75-125ND
Thallium ug/L 417500 83 75-1254.2J
Total Hardness ug/L 133000103000
Zinc ug/L 516500 103 75-1252.5J
Parameter Units
Dup
Result QualifiersRPDResult
92119749021
771441SAMPLE DUPLICATE:
Antimony ug/L 5.7 85.3
Arsenic ug/L NDND
Beryllium ug/L NDND
Cadmium ug/L NDND
Chromium ug/L 120 1119
Copper ug/L 2.1J2.1J
Lead ug/L NDND
Manganese ug/L 17.9 117.7
Nickel ug/L NDND
Selenium ug/L NDND
Silver ug/L NDND
Thallium ug/L ND3.3J
Total Hardness ug/L 103000 0103000
Zinc ug/L 4J2.2J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 44 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/19322
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772640
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/04/12 15:24
1,1,1-Trichloroethane ug/L ND 1.0 06/04/12 15:24
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/04/12 15:24
1,1,2-Trichloroethane ug/L ND 1.0 06/04/12 15:24
1,1-Dichloroethane ug/L ND 1.0 06/04/12 15:24
1,1-Dichloroethene ug/L ND 1.0 06/04/12 15:24
1,1-Dichloropropene ug/L ND 1.0 06/04/12 15:24
1,2,3-Trichlorobenzene ug/L ND 1.0 06/04/12 15:24
1,2,3-Trichloropropane ug/L ND 1.0 06/04/12 15:24
1,2,4-Trichlorobenzene ug/L ND 1.0 06/04/12 15:24
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/04/12 15:24
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/12 15:24
1,2-Dichlorobenzene ug/L ND 1.0 06/04/12 15:24
1,2-Dichloroethane ug/L ND 1.0 06/04/12 15:24
1,2-Dichloropropane ug/L ND 1.0 06/04/12 15:24
1,3-Dichlorobenzene ug/L ND 1.0 06/04/12 15:24
1,3-Dichloropropane ug/L ND 1.0 06/04/12 15:24
1,4-Dichlorobenzene ug/L ND 1.0 06/04/12 15:24
2,2-Dichloropropane ug/L ND 1.0 06/04/12 15:24
2-Butanone (MEK)ug/L ND 5.0 06/04/12 15:24
2-Chlorotoluene ug/L ND 1.0 06/04/12 15:24
2-Hexanone ug/L ND 5.0 06/04/12 15:24
4-Chlorotoluene ug/L ND 1.0 06/04/12 15:24
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/04/12 15:24
Acetone ug/L ND 25.0 06/04/12 15:24
Benzene ug/L ND 1.0 06/04/12 15:24
Bromobenzene ug/L ND 1.0 06/04/12 15:24
Bromochloromethane ug/L ND 1.0 06/04/12 15:24
Bromodichloromethane ug/L ND 1.0 06/04/12 15:24
Bromoform ug/L ND 1.0 06/04/12 15:24
Bromomethane ug/L ND 2.0 06/04/12 15:24
Carbon tetrachloride ug/L ND 1.0 06/04/12 15:24
Chlorobenzene ug/L ND 1.0 06/04/12 15:24
Chloroethane ug/L ND 1.0 06/04/12 15:24
Chloroform ug/L ND 1.0 06/04/12 15:24
Chloromethane ug/L ND 1.0 06/04/12 15:24
cis-1,2-Dichloroethene ug/L ND 1.0 06/04/12 15:24
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/12 15:24
Dibromochloromethane ug/L ND 1.0 06/04/12 15:24
Dibromomethane ug/L ND 1.0 06/04/12 15:24
Dichlorodifluoromethane ug/L ND 1.0 06/04/12 15:24
Diisopropyl ether ug/L ND 1.0 06/04/12 15:24
Ethylbenzene ug/L ND 1.0 06/04/12 15:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 45 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772640
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 06/04/12 15:24
m&p-Xylene ug/L ND 2.0 06/04/12 15:24
Methyl-tert-butyl ether ug/L ND 1.0 06/04/12 15:24
Methylene Chloride ug/L ND 2.0 06/04/12 15:24
Naphthalene ug/L ND 1.0 06/04/12 15:24
o-Xylene ug/L ND 1.0 06/04/12 15:24
p-Isopropyltoluene ug/L ND 1.0 06/04/12 15:24
Styrene ug/L ND 1.0 06/04/12 15:24
Tetrachloroethene ug/L ND 1.0 06/04/12 15:24
Toluene ug/L ND 1.0 06/04/12 15:24
trans-1,2-Dichloroethene ug/L ND 1.0 06/04/12 15:24
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/12 15:24
Trichloroethene ug/L ND 1.0 06/04/12 15:24
Trichlorofluoromethane ug/L ND 1.0 06/04/12 15:24
Vinyl acetate ug/L ND 2.0 06/04/12 15:24
Vinyl chloride ug/L ND 1.0 06/04/12 15:24
1,2-Dichloroethane-d4 (S)%106 70-130 06/04/12 15:24
4-Bromofluorobenzene (S)%100 70-130 06/04/12 15:24
Dibromofluoromethane (S)%99 70-130 06/04/12 15:24
Toluene-d8 (S)%100 70-130 06/04/12 15:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772641LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 70-130
1,1,1-Trichloroethane ug/L 47.150 94 70-130
1,1,2,2-Tetrachloroethane ug/L 49.950 100 70-130
1,1,2-Trichloroethane ug/L 52.550 105 70-130
1,1-Dichloroethane ug/L 43.550 87 70-130
1,1-Dichloroethene ug/L 48.550 97 70-132
1,1-Dichloropropene ug/L 48.250 96 70-130
1,2,3-Trichlorobenzene ug/L 49.150 98 70-135
1,2,3-Trichloropropane ug/L 53.050 106 70-130
1,2,4-Trichlorobenzene ug/L 49.550 99 70-134
1,2-Dibromo-3-chloropropane ug/L 51.650 103 70-130
1,2-Dibromoethane (EDB)ug/L 50.050 100 70-130
1,2-Dichlorobenzene ug/L 47.050 94 70-130
1,2-Dichloroethane ug/L 47.950 96 70-130
1,2-Dichloropropane ug/L 49.450 99 70-130
1,3-Dichlorobenzene ug/L 47.350 95 70-130
1,3-Dichloropropane ug/L 49.550 99 70-130
1,4-Dichlorobenzene ug/L 47.950 96 70-130
2,2-Dichloropropane ug/L 44.150 88 58-145
2-Butanone (MEK)ug/L 108100 108 70-145
2-Chlorotoluene ug/L 46.650 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 46 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772641LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 111100 111 70-144
4-Chlorotoluene ug/L 48.750 97 70-130
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 70-140
Acetone ug/L 124100 124 50-175
Benzene ug/L 49.450 99 70-130
Bromobenzene ug/L 47.250 94 70-130
Bromochloromethane ug/L 49.350 99 70-130
Bromodichloromethane ug/L 48.150 96 70-130
Bromoform ug/L 52.350 105 70-130
Bromomethane ug/L 38.250 76 54-130
Carbon tetrachloride ug/L 52.750 105 70-132
Chlorobenzene ug/L 49.150 98 70-130
Chloroethane ug/L 52.550 105 64-134
Chloroform ug/L 46.950 94 70-130
Chloromethane ug/L 43.850 88 64-130
cis-1,2-Dichloroethene ug/L 48.150 96 70-131
cis-1,3-Dichloropropene ug/L 50.650 101 70-130
Dibromochloromethane ug/L 52.050 104 70-130
Dibromomethane ug/L 50.250 100 70-131
Dichlorodifluoromethane ug/L 35.450 71 56-130
Diisopropyl ether ug/L 50.350 101 70-130
Ethylbenzene ug/L 48.950 98 70-130
Hexachloro-1,3-butadiene ug/L 53.850 108 70-130
m&p-Xylene ug/L 94.9100 95 70-130
Methyl-tert-butyl ether ug/L 50.450 101 70-130
Methylene Chloride ug/L 54.750 109 63-130
Naphthalene ug/L 49.250 98 70-138
o-Xylene ug/L 46.050 92 70-130
p-Isopropyltoluene ug/L 51.750 103 70-130
Styrene ug/L 50.050 100 70-130
Tetrachloroethene ug/L 49.050 98 70-130
Toluene ug/L 47.450 95 70-130
trans-1,2-Dichloroethene ug/L 47.650 95 70-130
trans-1,3-Dichloropropene ug/L 51.750 103 70-132
Trichloroethene ug/L 50.550 101 70-130
Trichlorofluoromethane ug/L 49.450 99 62-133
Vinyl acetate ug/L 94.4100 94 66-157
Vinyl chloride ug/L 46.750 93 69-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%104 70-130
Dibromofluoromethane (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 47 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
772642MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92119860001
772643
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 660.2 56.4
Benzene ug/L 50 95 70-14894 250ND47.7 46.9
Chlorobenzene ug/L 50 115 70-146115 050ND57.7 57.5
Toluene ug/L 50 112 70-155112 050ND56.1 56.2
Trichloroethene ug/L 161.4 61.8
1,2-Dichloroethane-d4 (S)%112 70-130105
4-Bromofluorobenzene (S)%104 70-130102
Dibromofluoromethane (S)%105 70-130100
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 48 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/19317
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772575
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.5 06/04/12 12:41
1,1,1-Trichloroethane ug/kg ND 5.5 06/04/12 12:41
1,1,2,2-Tetrachloroethane ug/kg ND 5.5 06/04/12 12:41
1,1,2-Trichloroethane ug/kg ND 5.5 06/04/12 12:41
1,1-Dichloroethane ug/kg ND 5.5 06/04/12 12:41
1,1-Dichloroethene ug/kg ND 5.5 06/04/12 12:41
1,1-Dichloropropene ug/kg ND 5.5 06/04/12 12:41
1,2,3-Trichlorobenzene ug/kg ND 5.5 06/04/12 12:41
1,2,3-Trichloropropane ug/kg ND 5.5 06/04/12 12:41
1,2,4-Trichlorobenzene ug/kg ND 5.5 06/04/12 12:41
1,2,4-Trimethylbenzene ug/kg ND 5.5 06/04/12 12:41
1,2-Dibromo-3-chloropropane ug/kg ND 5.5 06/04/12 12:41
1,2-Dibromoethane (EDB)ug/kg ND 5.5 06/04/12 12:41
1,2-Dichlorobenzene ug/kg ND 5.5 06/04/12 12:41
1,2-Dichloroethane ug/kg ND 5.5 06/04/12 12:41
1,2-Dichloropropane ug/kg ND 5.5 06/04/12 12:41
1,3,5-Trimethylbenzene ug/kg ND 5.5 06/04/12 12:41
1,3-Dichlorobenzene ug/kg ND 5.5 06/04/12 12:41
1,3-Dichloropropane ug/kg ND 5.5 06/04/12 12:41
1,4-Dichlorobenzene ug/kg ND 5.5 06/04/12 12:41
2,2-Dichloropropane ug/kg ND 5.5 06/04/12 12:41
2-Butanone (MEK)ug/kg ND 110 06/04/12 12:41
2-Chlorotoluene ug/kg ND 5.5 06/04/12 12:41
2-Hexanone ug/kg ND 54.8 06/04/12 12:41
4-Chlorotoluene ug/kg ND 5.5 06/04/12 12:41
4-Methyl-2-pentanone (MIBK)ug/kg ND 54.8 06/04/12 12:41
Acetone ug/kg ND 110 06/04/12 12:41
Benzene ug/kg ND 5.5 06/04/12 12:41
Bromobenzene ug/kg ND 5.5 06/04/12 12:41
Bromochloromethane ug/kg ND 5.5 06/04/12 12:41
Bromodichloromethane ug/kg ND 5.5 06/04/12 12:41
Bromoform ug/kg ND 5.5 06/04/12 12:41
Bromomethane ug/kg ND 11.0 06/04/12 12:41
Carbon tetrachloride ug/kg ND 5.5 06/04/12 12:41
Chlorobenzene ug/kg ND 5.5 06/04/12 12:41
Chloroethane ug/kg ND 11.0 06/04/12 12:41
Chloroform ug/kg ND 5.5 06/04/12 12:41
Chloromethane ug/kg ND 11.0 06/04/12 12:41
cis-1,2-Dichloroethene ug/kg ND 5.5 06/04/12 12:41
cis-1,3-Dichloropropene ug/kg ND 5.5 06/04/12 12:41
Dibromochloromethane ug/kg ND 5.5 06/04/12 12:41
Dibromomethane ug/kg ND 5.5 06/04/12 12:41
Dichlorodifluoromethane ug/kg ND 11.0 06/04/12 12:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 49 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772575
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.5 06/04/12 12:41
Ethylbenzene ug/kg ND 5.5 06/04/12 12:41
Hexachloro-1,3-butadiene ug/kg ND 5.5 06/04/12 12:41
Isopropylbenzene (Cumene)ug/kg ND 5.5 06/04/12 12:41
m&p-Xylene ug/kg ND 11.0 06/04/12 12:41
Methyl-tert-butyl ether ug/kg ND 5.5 06/04/12 12:41
Methylene Chloride ug/kg ND 21.9 06/04/12 12:41
n-Butylbenzene ug/kg ND 5.5 06/04/12 12:41
n-Propylbenzene ug/kg ND 5.5 06/04/12 12:41
Naphthalene ug/kg ND 5.5 06/04/12 12:41
o-Xylene ug/kg ND 5.5 06/04/12 12:41
p-Isopropyltoluene ug/kg ND 5.5 06/04/12 12:41
sec-Butylbenzene ug/kg ND 5.5 06/04/12 12:41
Styrene ug/kg ND 5.5 06/04/12 12:41
tert-Butylbenzene ug/kg ND 5.5 06/04/12 12:41
Tetrachloroethene ug/kg ND 5.5 06/04/12 12:41
Toluene ug/kg ND 5.5 06/04/12 12:41
trans-1,2-Dichloroethene ug/kg ND 5.5 06/04/12 12:41
trans-1,3-Dichloropropene ug/kg ND 5.5 06/04/12 12:41
Trichloroethene ug/kg ND 5.5 06/04/12 12:41
Trichlorofluoromethane ug/kg ND 5.5 06/04/12 12:41
Vinyl acetate ug/kg ND 54.8 06/04/12 12:41
Vinyl chloride ug/kg ND 11.0 06/04/12 12:41
Xylene (Total)ug/kg ND 11.0 06/04/12 12:41
1,2-Dichloroethane-d4 (S)%117 70-132 06/04/12 12:41
4-Bromofluorobenzene (S)%96 70-130 06/04/12 12:41
Dibromofluoromethane (S)%113 70-130 06/04/12 12:41
Toluene-d8 (S)%105 70-130 06/04/12 12:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772576LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 47.248.7 97 70-131
1,1,1-Trichloroethane ug/kg 48.648.7 100 70-141
1,1,2,2-Tetrachloroethane ug/kg 46.748.7 96 70-130
1,1,2-Trichloroethane ug/kg 51.348.7 105 70-132
1,1-Dichloroethane ug/kg 49.348.7 101 70-143
1,1-Dichloroethene ug/kg 55.548.7 114 70-137
1,1-Dichloropropene ug/kg 52.048.7 107 70-135
1,2,3-Trichlorobenzene ug/kg 45.448.7 93 69-153
1,2,3-Trichloropropane ug/kg 46.748.7 96 70-130
1,2,4-Trichlorobenzene ug/kg 47.248.7 97 55-171
1,2,4-Trimethylbenzene ug/kg 51.148.7 105 70-149
1,2-Dibromo-3-chloropropane ug/kg 48.248.7 99 68-141
1,2-Dibromoethane (EDB)ug/kg 48.448.7 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 50 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772576LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 47.348.7 97 70-140
1,2-Dichloroethane ug/kg 53.848.7 110 70-137
1,2-Dichloropropane ug/kg 51.648.7 106 70-133
1,3,5-Trimethylbenzene ug/kg 50.548.7 104 70-143
1,3-Dichlorobenzene ug/kg 46.948.7 96 70-144
1,3-Dichloropropane ug/kg 50.348.7 103 70-132
1,4-Dichlorobenzene ug/kg 47.348.7 97 70-142
2,2-Dichloropropane ug/kg 52.048.7 107 68-152
2-Butanone (MEK)ug/kg 11297.5 115 70-149
2-Chlorotoluene ug/kg 49.648.7 102 70-141
2-Hexanone ug/kg 10697.5 109 70-149
4-Chlorotoluene ug/kg 52.348.7 107 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 10597.5 107 70-153
Acetone ug/kg 11097.5 113 70-157
Benzene ug/kg 51.048.7 105 70-130
Bromobenzene ug/kg 52.248.7 107 70-141
Bromochloromethane ug/kg 47.548.7 97 70-149
Bromodichloromethane ug/kg 49.948.7 102 70-130
Bromoform ug/kg 47.748.7 98 70-131
Bromomethane ug/kg 43.148.7 88 64-136
Carbon tetrachloride ug/kg 50.748.7 104 70-154
Chlorobenzene ug/kg 46.948.7 96 70-135
Chloroethane ug/kg 50.348.7 103 68-151
Chloroform ug/kg 56.548.7 116 70-130
Chloromethane ug/kg 47.448.7 97 70-132
cis-1,2-Dichloroethene ug/kg 57.448.7 118 70-140
cis-1,3-Dichloropropene ug/kg 50.548.7 104 70-137
Dibromochloromethane ug/kg 47.648.7 98 70-130
Dibromomethane ug/kg 51.648.7 106 70-136
Dichlorodifluoromethane ug/kg 35.548.7 73 36-148
Diisopropyl ether ug/kg 57.248.7 117 70-139
Ethylbenzene ug/kg 48.948.7 100 70-137
Hexachloro-1,3-butadiene ug/kg 45.748.7 94 70-145
Isopropylbenzene (Cumene)ug/kg 42.648.7 87 70-141
m&p-Xylene ug/kg 98.597.5 101 70-140
Methyl-tert-butyl ether ug/kg 58.848.7 121 45-150
Methylene Chloride ug/kg 51.148.7 105 70-133
n-Butylbenzene ug/kg 51.348.7 105 65-155
n-Propylbenzene ug/kg 50.048.7 103 70-148
Naphthalene ug/kg 42.148.7 86 70-148
o-Xylene ug/kg 47.148.7 97 70-141
p-Isopropyltoluene ug/kg 50.248.7 103 70-148
sec-Butylbenzene ug/kg 50.048.7 103 70-145
Styrene ug/kg 48.348.7 99 70-138
tert-Butylbenzene ug/kg 47.548.7 97 70-143
Tetrachloroethene ug/kg 44.148.7 91 70-140
Toluene ug/kg 49.248.7 101 70-130
trans-1,2-Dichloroethene ug/kg 53.648.7 110 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 51 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772576LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 50.648.7 104 70-138
Trichloroethene ug/kg 47.748.7 98 70-132
Trichlorofluoromethane ug/kg 48.948.7 100 69-134
Vinyl acetate ug/kg 12497.5 128 24-161
Vinyl chloride ug/kg 46.148.7 95 55-140
Xylene (Total)ug/kg 146146 100 70-141
1,2-Dichloroethane-d4 (S)%109 70-132
4-Bromofluorobenzene (S)%96 70-130
Dibromofluoromethane (S)%107 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
772907MATRIX SPIKE SAMPLE:
MSSpike
Result
92119897005
1,1-Dichloroethene ug/kg 48.153.8 89 49-180ND
Benzene ug/kg 45.053.8 84 50-166ND
Chlorobenzene ug/kg 50.553.8 94 43-169ND
Toluene ug/kg 51.953.8 97 52-163ND
Trichloroethene ug/kg 48.353.8 90 49-167ND
1,2-Dichloroethane-d4 (S)%117 70-132
4-Bromofluorobenzene (S)%90 70-130
Dibromofluoromethane (S)%105 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92119682002
772906SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 52 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Dup
Result QualifiersRPDResult
92119682002
772906SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 26.9JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 53 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Dup
Result QualifiersRPDResult
92119682002
772906SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%119 5127
4-Bromofluorobenzene (S)%93 397
Dibromofluoromethane (S)%111 6120
Toluene-d8 (S)%104 1108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 54 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/17699
EPA 3546
EPA 8270 by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771416
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
1-Methylnaphthalene ug/kg ND 10.0 06/01/12 15:28
2-Methylnaphthalene ug/kg ND 10.0 06/01/12 15:28
Acenaphthene ug/kg ND 10.0 06/01/12 15:28
Acenaphthylene ug/kg ND 10.0 06/01/12 15:28
Anthracene ug/kg ND 10.0 06/01/12 15:28
Benzo(a)anthracene ug/kg ND 10.0 06/01/12 15:28
Benzo(a)pyrene ug/kg ND 10.0 06/01/12 15:28
Benzo(b)fluoranthene ug/kg ND 10.0 06/01/12 15:28
Benzo(g,h,i)perylene ug/kg ND 10.0 06/01/12 15:28
Benzo(k)fluoranthene ug/kg ND 10.0 06/01/12 15:28
Chrysene ug/kg ND 10.0 06/01/12 15:28
Dibenz(a,h)anthracene ug/kg ND 10.0 06/01/12 15:28
Fluoranthene ug/kg ND 10.0 06/01/12 15:28
Fluorene ug/kg ND 10.0 06/01/12 15:28
Indeno(1,2,3-cd)pyrene ug/kg ND 10.0 06/01/12 15:28
Naphthalene ug/kg ND 10.0 06/01/12 15:28
Phenanthrene ug/kg ND 10.0 06/01/12 15:28
Pyrene ug/kg ND 10.0 06/01/12 15:28
2-Fluorobiphenyl (S)%77 10-110 06/01/12 15:28
Nitrobenzene-d5 (S)%87 10-128 06/01/12 15:28
Terphenyl-d14 (S)%119 39-119 06/01/12 15:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771417LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 30.933.3 93 29-108
2-Methylnaphthalene ug/kg 29.333.3 88 30-104
Acenaphthene ug/kg 31.633.3 95 38-109
Acenaphthylene ug/kg 31.233.3 94 41-109
Anthracene ug/kg 34.533.3 104 45-114
Benzo(a)anthracene ug/kg 32.333.3 97 45-109
Benzo(a)pyrene ug/kg 33.833.3 101 47-117
Benzo(b)fluoranthene ug/kg 28.933.3 87 32-113
Benzo(g,h,i)perylene ug/kg 26.533.3 79 10-149
Benzo(k)fluoranthene ug/kg 30.833.3 92 41-104
Chrysene ug/kg 36.233.3 109 35-116
Dibenz(a,h)anthracene ug/kg 29.233.3 87 13-139
Fluoranthene ug/kg 30.033.3 90 43-110
Fluorene ug/kg 32.533.3 98 45-111
Indeno(1,2,3-cd)pyrene ug/kg 28.233.3 85 17-135
Naphthalene ug/kg 30.633.3 92 26-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 55 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771417LABORATORY CONTROL SAMPLE:
LCSSpike
Phenanthrene ug/kg 30.833.3 92 45-110
Pyrene ug/kg 28.733.3 86 38-114
2-Fluorobiphenyl (S)%84 10-110
Nitrobenzene-d5 (S)%93 10-128
Terphenyl-d14 (S)%S012439-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
771418MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92119589004
771419
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1-Methylnaphthalene ug/kg 40.6 84 50-15073 1640.1ND 34.5 29.5
2-Methylnaphthalene ug/kg 40.6 80 50-15068 1740.1ND 32.8 27.5
Acenaphthene ug/kg 40.6 88 50-15076 1640.1ND 35.8 30.6
Acenaphthylene ug/kg 40.6 87 50-15075 1640.1ND 35.4 30.1
Anthracene ug/kg 40.6 99 50-15081 2040.1ND 40.9 33.4
Benzo(a)anthracene ug/kg 40.6 91 50-15085 840.1ND 37.0 34.1
Benzo(a)pyrene ug/kg 40.6 96 50-15090 840.1ND 38.9 36.0
Benzo(b)fluoranthene ug/kg 40.6 83 50-15081 440.1ND 33.7 32.4
Benzo(g,h,i)perylene ug/kg 40.6 74 50-15070 740.1ND 29.8 27.9
Benzo(k)fluoranthene ug/kg 40.6 77 50-15067 1540.1ND 31.3 26.9
Chrysene ug/kg 40.6 100 50-15093 840.1ND 40.7 37.5
Dibenz(a,h)anthracene ug/kg 40.6 81 50-15076 740.1ND 33.0 30.7
Fluoranthene ug/kg 40.6 85 50-15075 1340.1ND 35.1 30.9
Fluorene ug/kg 40.6 90 50-15077 1740.1ND 37.2 31.4
Indeno(1,2,3-cd)pyrene ug/kg 40.6 77 50-15073 640.1ND 31.2 29.2
Naphthalene ug/kg 40.6 84 50-15073 1640.1ND 34.1 29.1
Phenanthrene ug/kg 40.6 84 50-15075 1240.1ND 34.6 30.7
Pyrene ug/kg 40.6 82 50-15072 1340.1ND 33.8 29.5
2-Fluorobiphenyl (S)%78 10-11066
Nitrobenzene-d5 (S)%84 10-12873
Terphenyl-d14 (S)%S012539-119114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 56 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/17720
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772491
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 06/05/12 17:16
1,2-Dichlorobenzene ug/kg ND 330 06/05/12 17:16
1,3-Dichlorobenzene ug/kg ND 330 06/05/12 17:16
1,4-Dichlorobenzene ug/kg ND 330 06/05/12 17:16
1-Methylnaphthalene ug/kg ND 330 06/05/12 17:16
2,4,5-Trichlorophenol ug/kg ND 330 06/05/12 17:16
2,4,6-Trichlorophenol ug/kg ND 330 06/05/12 17:16
2,4-Dichlorophenol ug/kg ND 330 06/05/12 17:16
2,4-Dimethylphenol ug/kg ND 330 06/05/12 17:16
2,4-Dinitrophenol ug/kg ND 1650 06/05/12 17:16
2,4-Dinitrotoluene ug/kg ND 330 06/05/12 17:16
2,6-Dinitrotoluene ug/kg ND 330 06/05/12 17:16
2-Chloronaphthalene ug/kg ND 330 06/05/12 17:16
2-Chlorophenol ug/kg ND 330 06/05/12 17:16
2-Methylnaphthalene ug/kg ND 330 06/05/12 17:16
2-Methylphenol(o-Cresol)ug/kg ND 330 06/05/12 17:16
2-Nitroaniline ug/kg ND 1650 06/05/12 17:16
2-Nitrophenol ug/kg ND 330 06/05/12 17:16
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 06/05/12 17:16
3,3'-Dichlorobenzidine ug/kg ND 1650 06/05/12 17:16
3-Nitroaniline ug/kg ND 1650 06/05/12 17:16
4,6-Dinitro-2-methylphenol ug/kg ND 660 06/05/12 17:16
4-Bromophenylphenyl ether ug/kg ND 330 06/05/12 17:16
4-Chloro-3-methylphenol ug/kg ND 660 06/05/12 17:16
4-Chloroaniline ug/kg ND 1650 06/05/12 17:16
4-Chlorophenylphenyl ether ug/kg ND 330 06/05/12 17:16
4-Nitroaniline ug/kg ND 660 06/05/12 17:16
4-Nitrophenol ug/kg ND 1650 06/05/12 17:16
Acenaphthene ug/kg ND 330 06/05/12 17:16
Acenaphthylene ug/kg ND 330 06/05/12 17:16
Aniline ug/kg ND 330 06/05/12 17:16
Anthracene ug/kg ND 330 06/05/12 17:16
Benzo(a)anthracene ug/kg ND 330 06/05/12 17:16
Benzo(a)pyrene ug/kg ND 330 06/05/12 17:16
Benzo(b)fluoranthene ug/kg ND 330 06/05/12 17:16
Benzo(g,h,i)perylene ug/kg ND 330 06/05/12 17:16
Benzo(k)fluoranthene ug/kg ND 330 06/05/12 17:16
Benzoic Acid ug/kg ND 1650 06/05/12 17:16
Benzyl alcohol ug/kg ND 660 06/05/12 17:16
bis(2-Chloroethoxy)methane ug/kg ND 330 06/05/12 17:16
bis(2-Chloroethyl) ether ug/kg ND 330 06/05/12 17:16
bis(2-Chloroisopropyl) ether ug/kg ND 330 06/05/12 17:16
bis(2-Ethylhexyl)phthalate ug/kg ND 330 06/05/12 17:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 57 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772491
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 06/05/12 17:16
Chrysene ug/kg ND 330 06/05/12 17:16
Di-n-butylphthalate ug/kg ND 330 06/05/12 17:16
Di-n-octylphthalate ug/kg ND 330 06/05/12 17:16
Dibenz(a,h)anthracene ug/kg ND 330 06/05/12 17:16
Dibenzofuran ug/kg ND 330 06/05/12 17:16
Diethylphthalate ug/kg ND 330 06/05/12 17:16
Dimethylphthalate ug/kg ND 330 06/05/12 17:16
Fluoranthene ug/kg ND 330 06/05/12 17:16
Fluorene ug/kg ND 330 06/05/12 17:16
Hexachloro-1,3-butadiene ug/kg ND 330 06/05/12 17:16
Hexachlorobenzene ug/kg ND 330 06/05/12 17:16
Hexachlorocyclopentadiene ug/kg ND 330 06/05/12 17:16
Hexachloroethane ug/kg ND 330 06/05/12 17:16
Indeno(1,2,3-cd)pyrene ug/kg ND 330 06/05/12 17:16
Isophorone ug/kg ND 330 06/05/12 17:16
N-Nitroso-di-n-propylamine ug/kg ND 330 06/05/12 17:16
N-Nitrosodimethylamine ug/kg ND 330 06/05/12 17:16
N-Nitrosodiphenylamine ug/kg ND 330 06/05/12 17:16
Naphthalene ug/kg ND 330 06/05/12 17:16
Nitrobenzene ug/kg ND 330 06/05/12 17:16
Pentachlorophenol ug/kg ND 1650 06/05/12 17:16
Phenanthrene ug/kg ND 330 06/05/12 17:16
Phenol ug/kg ND 330 06/05/12 17:16
Pyrene ug/kg ND 330 06/05/12 17:16
2,4,6-Tribromophenol (S)%71 27-110 06/05/12 17:16
2-Fluorobiphenyl (S)%73 30-110 06/05/12 17:16
2-Fluorophenol (S)%71 13-110 06/05/12 17:16
Nitrobenzene-d5 (S)%80 23-110 06/05/12 17:16
Phenol-d6 (S)%61 22-110 06/05/12 17:16
Terphenyl-d14 (S)%94 28-110 06/05/12 17:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772492LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11201670 67 39-101
1,2-Dichlorobenzene ug/kg 12101670 73 36-110
1,3-Dichlorobenzene ug/kg 11501670 69 35-110
1,4-Dichlorobenzene ug/kg 11901670 71 35-110
1-Methylnaphthalene ug/kg 12801670 77 45-105
2,4,5-Trichlorophenol ug/kg 12201670 73 48-109
2,4,6-Trichlorophenol ug/kg 12201670 73 45-111
2,4-Dichlorophenol ug/kg 12501670 75 51-116
2,4-Dimethylphenol ug/kg 12401670 74 42-103
2,4-Dinitrophenol ug/kg 55408330 66 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 58 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772492LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 12601670 76 46-114
2,6-Dinitrotoluene ug/kg 11901670 71 48-112
2-Chloronaphthalene ug/kg 11601670 70 44-105
2-Chlorophenol ug/kg 12001670 72 36-110
2-Methylnaphthalene ug/kg 12401670 75 39-112
2-Methylphenol(o-Cresol)ug/kg 13101670 79 39-101
2-Nitroaniline ug/kg 31203330 94 44-111
2-Nitrophenol ug/kg 11601670 70 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 13401670 81 43-103
3,3'-Dichlorobenzidine ug/kg 29903330 90 10-150
3-Nitroaniline ug/kg 26403330 79 35-110
4,6-Dinitro-2-methylphenol ug/kg 26603330 80 38-118
4-Bromophenylphenyl ether ug/kg 12901670 77 47-115
4-Chloro-3-methylphenol ug/kg 29103330 87 43-127
4-Chloroaniline ug/kg 23803330 71 34-109
4-Chlorophenylphenyl ether ug/kg 12601670 75 44-115
4-Nitroaniline ug/kg 30003330 90 37-111
4-Nitrophenol ug/kg 93408330 112 21-152
Acenaphthene ug/kg 13001670 78 38-117
Acenaphthylene ug/kg 12901670 77 46-107
Aniline ug/kg 10801670 65 29-110
Anthracene ug/kg 14101670 84 50-110
Benzo(a)anthracene ug/kg 15101670 91 47-116
Benzo(a)pyrene ug/kg 13901670 83 47-106
Benzo(b)fluoranthene ug/kg 14901670 90 47-109
Benzo(g,h,i)perylene ug/kg 13901670 83 39-115
Benzo(k)fluoranthene ug/kg 14001670 84 45-117
Benzoic Acid ug/kg 73708330 88 16-110
Benzyl alcohol ug/kg 24303330 73 38-105
bis(2-Chloroethoxy)methane ug/kg 11301670 68 39-110
bis(2-Chloroethyl) ether ug/kg 13401670 80 19-119
bis(2-Chloroisopropyl) ether ug/kg 11501670 69 21-110
bis(2-Ethylhexyl)phthalate ug/kg 13801670 83 35-116
Butylbenzylphthalate ug/kg 13801670 83 38-110
Chrysene ug/kg 14301670 86 49-110
Di-n-butylphthalate ug/kg 13201670 79 43-109
Di-n-octylphthalate ug/kg 14001670 84 37-109
Dibenz(a,h)anthracene ug/kg 13901670 83 43-116
Dibenzofuran ug/kg 13001670 78 45-106
Diethylphthalate ug/kg 13201670 79 41-114
Dimethylphthalate ug/kg 12601670 75 43-110
Fluoranthene ug/kg 14301670 86 50-114
Fluorene ug/kg 13401670 81 46-114
Hexachloro-1,3-butadiene ug/kg 12301670 74 28-111
Hexachlorobenzene ug/kg 13001670 78 46-120
Hexachlorocyclopentadiene ug/kg 11401670 68 18-119
Hexachloroethane ug/kg 12401670 74 33-110
Indeno(1,2,3-cd)pyrene ug/kg 13901670 83 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 59 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772492LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 11201670 67 44-109
N-Nitroso-di-n-propylamine ug/kg 12801670 77 43-104
N-Nitrosodimethylamine ug/kg 11801670 71 29-110
N-Nitrosodiphenylamine ug/kg 14201670 85 48-113
Naphthalene ug/kg 11801670 71 41-110
Nitrobenzene ug/kg 10401670 62 38-110
Pentachlorophenol ug/kg 21203330 64 32-128
Phenanthrene ug/kg 13601670 82 50-110
Phenol ug/kg 12001670 72 28-106
Pyrene ug/kg 14301670 86 45-114
2,4,6-Tribromophenol (S)%80 27-110
2-Fluorobiphenyl (S)%68 30-110
2-Fluorophenol (S)%67 13-110
Nitrobenzene-d5 (S)%71 23-110
Phenol-d6 (S)%66 22-110
Terphenyl-d14 (S)%88 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
772493MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92119682003
772494
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg R118603518-11951 361830ND652941
1,2-Dichlorobenzene ug/kg M0,M118603850-11048 231830ND705888
1,3-Dichlorobenzene ug/kg R118603327-11046 341830ND607852
1,4-Dichlorobenzene ug/kg 1860 35 28-11048 281830ND659876
1-Methylnaphthalene ug/kg 1860 48 24-11662 231830ND8981130
2,4,5-Trichlorophenol ug/kg 1860 70 28-11079 121830ND12901460
2,4,6-Trichlorophenol ug/kg 1860 56 17-11770 201830ND10501280
2,4-Dichlorophenol ug/kg 1860 51 21-12865 231830ND9451190
2,4-Dimethylphenol ug/kg 1860 36 10-12045 201830ND673822
2,4-Dinitrophenol ug/kg 9290 40 10-10751 229160ND37304640
2,4-Dinitrotoluene ug/kg 1860 67 36-10972 61830ND12401310
2,6-Dinitrotoluene ug/kg 1860 58 32-11069 161830ND10801270
2-Chloronaphthalene ug/kg 1860 43 30-10759 301830ND7971070
2-Chlorophenol ug/kg 1860 39 14-10647 161830ND733863
2-Methylnaphthalene ug/kg 1860 44 10-13559 281830ND8101070
2-Methylphenol(o-Cresol)ug/kg 1860 42 10-12449 151830ND779904
2-Nitroaniline ug/kg 3710 75 26-11692 203670ND27703380
2-Nitrophenol ug/kg 1860 38 28-10349 261830ND700906
3&4-Methylphenol(m&p
Cresol)ug/kg 1860 47 10-10950 51830ND864911
3,3'-Dichlorobenzidine ug/kg 3710 65 10-15071 83670ND24002610
3-Nitroaniline ug/kg 3710 71 22-11079 93670ND26502890
4,6-Dinitro-2-methylphenol ug/kg 3710 65 13-12166 13670ND24002430
4-Bromophenylphenyl ether ug/kg 1860 67 31-10976 111830ND12501390
4-Chloro-3-methylphenol ug/kg 3710 77 13-12887 123670ND28403200
4-Chloroaniline ug/kg 3710 47 18-102623670ND1750J2260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 60 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
772493MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92119682003
772494
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1860 60 29-11272 181830ND11101330
4-Nitroaniline ug/kg 3710 83 16-11185 13670ND30803120
4-Nitrophenol ug/kg 9290 114 14-135113 29160ND1060010400
Acenaphthene ug/kg 1860 54 26-11470 241830ND10101280
Acenaphthylene ug/kg 1860 53 32-10867 231830ND9841240
Aniline ug/kg 1860 32 10-10736 101830ND596659
Anthracene ug/kg 1860 77 32-11181 31830ND14401480
Benzo(a)anthracene ug/kg 1860 81 25-11778 61830ND16101520
Benzo(a)pyrene ug/kg 1860 73 25-10671 41830ND14601410
Benzo(b)fluoranthene ug/kg 1860 76 24-11075 21830ND15301500
Benzo(g,h,i)perylene ug/kg 1860 75 19-11272 51830ND14601390
Benzo(k)fluoranthene ug/kg 1860 78 24-11470 121830ND15201350
Benzoic Acid ug/kg 9290 34 10-11047 309160ND31604270
Benzyl alcohol ug/kg 3710 44 24-10654 183670ND16401970
bis(2-Chloroethoxy)methane ug/kg 1860 37 13-11950 271830ND694912
bis(2-Chloroethyl) ether ug/kg 1860 39 10-13448 211830ND715887
bis(2-Chloroisopropyl) ether ug/kg 1860 41 10-11349 171830ND757895
bis(2-Ethylhexyl)phthalate ug/kg 1860 77 10-12580 21830ND14401470
Butylbenzylphthalate ug/kg 1860 78 18-11079 01830ND14501450
Chrysene ug/kg 1860 79 30-11073 81830ND15801460
Di-n-butylphthalate ug/kg 1860 74 19-11275 01830ND13701370
Di-n-octylphthalate ug/kg 1860 77 17-10579 11830ND14301440
Dibenz(a,h)anthracene ug/kg 1860 74 23-11175 01830ND13701370
Dibenzofuran ug/kg 1860 58 35-10372 201830ND10801330
Diethylphthalate ug/kg 1860 67 27-11374 91830ND12501360
Dimethylphthalate ug/kg 1860 55 26-11169 211830ND10301270
Fluoranthene ug/kg 1860 75 33-10966 131830ND16401450
Fluorene ug/kg 1860 63 32-11376 171830ND11801390
Hexachloro-1,3-butadiene ug/kg 1860 37 16-11649 271830ND686897
Hexachlorobenzene ug/kg 1860 71 27-12077 81830ND13101410
Hexachlorocyclopentadiene ug/kg 1860 25 10-10833 251830ND470602
Hexachloroethane ug/kg 1860 40 10-11751 241830ND741944
Indeno(1,2,3-cd)pyrene ug/kg 1860 73 10-12271 41830ND14101360
Isophorone ug/kg 1860 42 28-11454 221830ND785983
N-Nitroso-di-n-propylamine ug/kg 1860 50 27-11357 121830ND9331050
N-Nitrosodimethylamine ug/kg R118603210-10948 391830ND589871
N-Nitrosodiphenylamine ug/kg 1860 74 10-12880 71830ND13701470
Naphthalene ug/kg R118603925-11057 351830ND7331040
Nitrobenzene ug/kg 1860 34 18-11445 251830ND640819
Pentachlorophenol ug/kg 3710 74 10-12273 33670ND27502670
Phenanthrene ug/kg 1860 73 30-11471 41830ND14901430
Phenol ug/kg 1860 43 11-10247 81830ND801870
Pyrene ug/kg 1860 82 25-11673 121830ND17601570
2,4,6-Tribromophenol (S)%68 27-11066
2-Fluorobiphenyl (S)%37 30-11049
2-Fluorophenol (S)%30 13-11036
Nitrobenzene-d5 (S)%39 23-11051
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 61 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
772493MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92119682003
772494
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol-d6 (S)%38 22-11044
Terphenyl-d14 (S)%79 28-11079
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 62 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/17711
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771844
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/12 14:16
1,2-Dichlorobenzene ug/L ND 10.0 06/04/12 14:16
1,3-Dichlorobenzene ug/L ND 10.0 06/04/12 14:16
1,4-Dichlorobenzene ug/L ND 10.0 06/04/12 14:16
1-Methylnaphthalene ug/L ND 10.0 06/04/12 14:16
2,4,5-Trichlorophenol ug/L ND 10.0 06/04/12 14:16
2,4,6-Trichlorophenol ug/L ND 10.0 06/04/12 14:16
2,4-Dichlorophenol ug/L ND 10.0 06/04/12 14:16
2,4-Dimethylphenol ug/L ND 10.0 06/04/12 14:16
2,4-Dinitrophenol ug/L ND 50.0 06/04/12 14:16
2,4-Dinitrotoluene ug/L ND 10.0 06/04/12 14:16
2,6-Dinitrotoluene ug/L ND 10.0 06/04/12 14:16
2-Chloronaphthalene ug/L ND 10.0 06/04/12 14:16
2-Chlorophenol ug/L ND 10.0 06/04/12 14:16
2-Methylnaphthalene ug/L ND 10.0 06/04/12 14:16
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/04/12 14:16
2-Nitroaniline ug/L ND 50.0 06/04/12 14:16
2-Nitrophenol ug/L ND 10.0 06/04/12 14:16
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/04/12 14:16
3,3'-Dichlorobenzidine ug/L ND 20.0 06/04/12 14:16
3-Nitroaniline ug/L ND 50.0 06/04/12 14:16
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/04/12 14:16
4-Bromophenylphenyl ether ug/L ND 10.0 06/04/12 14:16
4-Chloro-3-methylphenol ug/L ND 20.0 06/04/12 14:16
4-Chloroaniline ug/L ND 20.0 06/04/12 14:16
4-Chlorophenylphenyl ether ug/L ND 10.0 06/04/12 14:16
4-Nitroaniline ug/L ND 20.0 06/04/12 14:16
4-Nitrophenol ug/L ND 50.0 06/04/12 14:16
Acenaphthene ug/L ND 10.0 06/04/12 14:16
Acenaphthylene ug/L ND 10.0 06/04/12 14:16
Aniline ug/L ND 10.0 06/04/12 14:16
Anthracene ug/L ND 10.0 06/04/12 14:16
Benzo(a)anthracene ug/L ND 10.0 06/04/12 14:16
Benzo(a)pyrene ug/L ND 10.0 06/04/12 14:16
Benzo(b)fluoranthene ug/L ND 10.0 06/04/12 14:16
Benzo(g,h,i)perylene ug/L ND 10.0 06/04/12 14:16
Benzo(k)fluoranthene ug/L ND 10.0 06/04/12 14:16
Benzoic Acid ug/L ND 50.0 06/04/12 14:16
Benzyl alcohol ug/L ND 20.0 06/04/12 14:16
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/04/12 14:16
bis(2-Chloroethyl) ether ug/L ND 10.0 06/04/12 14:16
bis(2-Chloroisopropyl) ether ug/L ND 10.0 06/04/12 14:16
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/04/12 14:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 63 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771844
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Butylbenzylphthalate ug/L ND 10.0 06/04/12 14:16
Chrysene ug/L ND 10.0 06/04/12 14:16
Di-n-butylphthalate ug/L ND 10.0 06/04/12 14:16
Di-n-octylphthalate ug/L ND 10.0 06/04/12 14:16
Dibenz(a,h)anthracene ug/L ND 10.0 06/04/12 14:16
Dibenzofuran ug/L ND 10.0 06/04/12 14:16
Diethylphthalate ug/L ND 10.0 06/04/12 14:16
Dimethylphthalate ug/L ND 10.0 06/04/12 14:16
Fluoranthene ug/L ND 10.0 06/04/12 14:16
Fluorene ug/L ND 10.0 06/04/12 14:16
Hexachloro-1,3-butadiene ug/L ND 10.0 06/04/12 14:16
Hexachlorobenzene ug/L ND 10.0 06/04/12 14:16
Hexachlorocyclopentadiene ug/L ND 10.0 06/04/12 14:16
Hexachloroethane ug/L ND 10.0 06/04/12 14:16
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/04/12 14:16
Isophorone ug/L ND 10.0 06/04/12 14:16
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/04/12 14:16
N-Nitrosodimethylamine ug/L ND 10.0 06/04/12 14:16
N-Nitrosodiphenylamine ug/L ND 10.0 06/04/12 14:16
Naphthalene ug/L ND 10.0 06/04/12 14:16
Nitrobenzene ug/L ND 10.0 06/04/12 14:16
Pentachlorophenol ug/L ND 25.0 06/04/12 14:16
Phenanthrene ug/L ND 10.0 06/04/12 14:16
Phenol ug/L ND 10.0 06/04/12 14:16
Pyrene ug/L ND 10.0 06/04/12 14:16
2,4,6-Tribromophenol (S)%86 27-110 06/04/12 14:16
2-Fluorobiphenyl (S)%75 27-110 06/04/12 14:16
2-Fluorophenol (S)%40 12-110 06/04/12 14:16
Nitrobenzene-d5 (S)%80 21-110 06/04/12 14:16
Phenol-d6 (S)%24 10-110 06/04/12 14:16
Terphenyl-d14 (S)%102 31-107 06/04/12 14:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771845LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 38.250 76 10-110
1,2-Dichlorobenzene ug/L 36.950 74 10-110
1,3-Dichlorobenzene ug/L 34.150 68 10-110
1,4-Dichlorobenzene ug/L 34.850 70 10-110
1-Methylnaphthalene ug/L 43.150 86 21-110
2,4,5-Trichlorophenol ug/L 44.350 89 23-116
2,4,6-Trichlorophenol ug/L 43.950 88 21-114
2,4-Dichlorophenol ug/L 43.750 87 22-120
2,4-Dimethylphenol ug/L 36.150 72 15-109
2,4-Dinitrophenol ug/L 256250 103 10-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 64 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771845LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/L 44.450 89 24-119
2,6-Dinitrotoluene ug/L 42.650 85 25-116
2-Chloronaphthalene ug/L 40.250 80 18-110
2-Chlorophenol ug/L 38.450 77 10-104
2-Methylnaphthalene ug/L 41.850 84 16-110
2-Methylphenol(o-Cresol)ug/L 33.850 68 13-110
2-Nitroaniline ug/L 97.8100 98 20-117
2-Nitrophenol ug/L 43.250 86 16-108
3&4-Methylphenol(m&p Cresol)ug/L 30.750 61 14-110
3,3'-Dichlorobenzidine ug/L 102100 102 13-131
3-Nitroaniline ug/L 84.8100 85 15-117
4,6-Dinitro-2-methylphenol ug/L 103100 103 13-119
4-Bromophenylphenyl ether ug/L 45.850 92 23-120
4-Chloro-3-methylphenol ug/L 91.7100 92 21-119
4-Chloroaniline ug/L 77.6100 78 10-122
4-Chlorophenylphenyl ether ug/L 44.550 89 22-112
4-Nitroaniline ug/L 91.3100 91 14-118
4-Nitrophenol ug/L 134250 53 10-110
Acenaphthene ug/L 43.950 88 20-105
Acenaphthylene ug/L 43.450 87 23-106
Aniline ug/L 30.650 61 10-110
Anthracene ug/L 47.650 95 25-120
Benzo(a)anthracene ug/L 51.250 102 21-128
Benzo(a)pyrene ug/L 48.150 96 25-116
Benzo(b)fluoranthene ug/L 51.950 104 23-117
Benzo(g,h,i)perylene ug/L 48.750 97 17-128
Benzo(k)fluoranthene ug/L 48.350 97 25-127
Benzoic Acid ug/L 151250 61 10-110
Benzyl alcohol ug/L 72.4100 72 10-101
bis(2-Chloroethoxy)methane ug/L 41.650 83 19-107
bis(2-Chloroethyl) ether ug/L 45.750 91 10-108
bis(2-Chloroisopropyl) ether ug/L 36.950 74 10-108
bis(2-Ethylhexyl)phthalate ug/L 46.750 93 16-123
Butylbenzylphthalate ug/L 45.950 92 20-118
Chrysene ug/L 47.950 96 24-125
Di-n-butylphthalate ug/L 45.950 92 23-115
Di-n-octylphthalate ug/L 47.350 95 20-115
Dibenz(a,h)anthracene ug/L 49.250 98 18-131
Dibenzofuran ug/L 44.350 89 23-106
Diethylphthalate ug/L 45.750 91 24-115
Dimethylphthalate ug/L 43.550 87 22-113
Fluoranthene ug/L 49.250 98 24-125
Fluorene ug/L 46.450 93 24-114
Hexachloro-1,3-butadiene ug/L 37.650 75 10-110
Hexachlorobenzene ug/L 46.450 93 22-127
Hexachlorocyclopentadiene ug/L 42.350 85 10-110
Hexachloroethane ug/L 35.150 70 10-110
Indeno(1,2,3-cd)pyrene ug/L 48.950 98 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 65 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771845LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 39.350 79 23-114
N-Nitroso-di-n-propylamine ug/L 50.650 101 21-114
N-Nitrosodimethylamine ug/L 27.450 55 10-110
N-Nitrosodiphenylamine ug/L 48.250 96 24-123
Naphthalene ug/L 39.350 79 14-110
Nitrobenzene ug/L 37.450 75 16-106
Pentachlorophenol ug/L 79.1100 79 10-123
Phenanthrene ug/L 46.450 93 25-119
Phenol ug/L 19.550 39 10-110
Pyrene ug/L 47.350 95 22-127
2,4,6-Tribromophenol (S)%97 27-110
2-Fluorobiphenyl (S)%81 27-110
2-Fluorophenol (S)%44 12-110
Nitrobenzene-d5 (S)%88 21-110
Phenol-d6 (S)%31 10-110
Terphenyl-d14 (S)%102 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 66 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/17739
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92119682007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:773118
Associated Lab Samples:92119682007
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 06/06/12 14:14
1,2-Dichlorobenzene ug/L ND 10.0 06/06/12 14:14
1,3-Dichlorobenzene ug/L ND 10.0 06/06/12 14:14
1,4-Dichlorobenzene ug/L ND 10.0 06/06/12 14:14
1-Methylnaphthalene ug/L ND 10.0 06/06/12 14:14
2,4,5-Trichlorophenol ug/L ND 10.0 06/06/12 14:14
2,4,6-Trichlorophenol ug/L ND 10.0 06/06/12 14:14
2,4-Dichlorophenol ug/L ND 10.0 06/06/12 14:14
2,4-Dimethylphenol ug/L ND 10.0 06/06/12 14:14
2,4-Dinitrophenol ug/L ND 50.0 06/06/12 14:14
2,4-Dinitrotoluene ug/L ND 10.0 06/06/12 14:14
2,6-Dinitrotoluene ug/L ND 10.0 06/06/12 14:14
2-Chloronaphthalene ug/L ND 10.0 06/06/12 14:14
2-Chlorophenol ug/L ND 10.0 06/06/12 14:14
2-Methylnaphthalene ug/L ND 10.0 06/06/12 14:14
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/06/12 14:14
2-Nitroaniline ug/L ND 50.0 06/06/12 14:14
2-Nitrophenol ug/L ND 10.0 06/06/12 14:14
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/06/12 14:14
3,3'-Dichlorobenzidine ug/L ND 20.0 06/06/12 14:14
3-Nitroaniline ug/L ND 50.0 06/06/12 14:14
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/06/12 14:14
4-Bromophenylphenyl ether ug/L ND 10.0 06/06/12 14:14
4-Chloro-3-methylphenol ug/L ND 20.0 06/06/12 14:14
4-Chloroaniline ug/L ND 20.0 06/06/12 14:14
4-Chlorophenylphenyl ether ug/L ND 10.0 06/06/12 14:14
4-Nitroaniline ug/L ND 20.0 06/06/12 14:14
4-Nitrophenol ug/L ND 50.0 06/06/12 14:14
Acenaphthene ug/L ND 10.0 06/06/12 14:14
Acenaphthylene ug/L ND 10.0 06/06/12 14:14
Aniline ug/L ND 10.0 06/06/12 14:14
Anthracene ug/L ND 10.0 06/06/12 14:14
Benzo(a)anthracene ug/L ND 10.0 06/06/12 14:14
Benzo(a)pyrene ug/L ND 10.0 06/06/12 14:14
Benzo(b)fluoranthene ug/L ND 10.0 06/06/12 14:14
Benzo(g,h,i)perylene ug/L ND 10.0 06/06/12 14:14
Benzo(k)fluoranthene ug/L ND 10.0 06/06/12 14:14
Benzoic Acid ug/L ND 50.0 06/06/12 14:14
Benzyl alcohol ug/L ND 20.0 06/06/12 14:14
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/06/12 14:14
bis(2-Chloroethyl) ether ug/L ND 10.0 06/06/12 14:14
bis(2-Chloroisopropyl) ether ug/L ND 10.0 06/06/12 14:14
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/06/12 14:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 67 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:773118
Associated Lab Samples:92119682007
Matrix:Water
Analyzed
Butylbenzylphthalate ug/L ND 10.0 06/06/12 14:14
Chrysene ug/L ND 10.0 06/06/12 14:14
Di-n-butylphthalate ug/L ND 10.0 06/06/12 14:14
Di-n-octylphthalate ug/L ND 10.0 06/06/12 14:14
Dibenz(a,h)anthracene ug/L ND 10.0 06/06/12 14:14
Dibenzofuran ug/L ND 10.0 06/06/12 14:14
Diethylphthalate ug/L ND 10.0 06/06/12 14:14
Dimethylphthalate ug/L ND 10.0 06/06/12 14:14
Fluoranthene ug/L ND 10.0 06/06/12 14:14
Fluorene ug/L ND 10.0 06/06/12 14:14
Hexachloro-1,3-butadiene ug/L ND 10.0 06/06/12 14:14
Hexachlorobenzene ug/L ND 10.0 06/06/12 14:14
Hexachlorocyclopentadiene ug/L ND 10.0 06/06/12 14:14
Hexachloroethane ug/L ND 10.0 06/06/12 14:14
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/06/12 14:14
Isophorone ug/L ND 10.0 06/06/12 14:14
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/06/12 14:14
N-Nitrosodimethylamine ug/L ND 10.0 06/06/12 14:14
N-Nitrosodiphenylamine ug/L ND 10.0 06/06/12 14:14
Naphthalene ug/L ND 10.0 06/06/12 14:14
Nitrobenzene ug/L ND 10.0 06/06/12 14:14
Pentachlorophenol ug/L ND 25.0 06/06/12 14:14
Phenanthrene ug/L ND 10.0 06/06/12 14:14
Phenol ug/L ND 10.0 06/06/12 14:14
Pyrene ug/L ND 10.0 06/06/12 14:14
2,4,6-Tribromophenol (S)%80 27-110 06/06/12 14:14
2-Fluorobiphenyl (S)%70 27-110 06/06/12 14:14
2-Fluorophenol (S)%35 12-110 06/06/12 14:14
Nitrobenzene-d5 (S)%64 21-110 06/06/12 14:14
Phenol-d6 (S)%22 10-110 06/06/12 14:14
Terphenyl-d14 (S)%94 31-107 06/06/12 14:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
773119LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 33.050 66 10-110
1,2-Dichlorobenzene ug/L 34.550 69 10-110
1,3-Dichlorobenzene ug/L 35.150 70 10-110
1,4-Dichlorobenzene ug/L 34.850 70 10-110
1-Methylnaphthalene ug/L 31.750 63 21-110
2,4,5-Trichlorophenol ug/L 33.650 67 23-116
2,4,6-Trichlorophenol ug/L 40.150 80 21-114
2,4-Dichlorophenol ug/L 31.950 64 22-120
2,4-Dimethylphenol ug/L 27.750 55 15-109
2,4-Dinitrophenol ug/L 223250 89 10-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 68 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
773119LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/L 44.750 89 24-119
2,6-Dinitrotoluene ug/L 43.250 86 25-116
2-Chloronaphthalene ug/L 41.950 84 18-110
2-Chlorophenol ug/L 32.350 65 10-104
2-Methylnaphthalene ug/L 30.450 61 16-110
2-Methylphenol(o-Cresol)ug/L 25.050 50 13-110
2-Nitroaniline ug/L 70.6100 71 20-117
2-Nitrophenol ug/L 33.250 66 16-108
3&4-Methylphenol(m&p Cresol)ug/L 53.250 106 14-110
3,3'-Dichlorobenzidine ug/L 79.6100 80 13-131
3-Nitroaniline ug/L 73.7100 74 15-117
4,6-Dinitro-2-methylphenol ug/L 103100 103 13-119
4-Bromophenylphenyl ether ug/L 39.450 79 23-120
4-Chloro-3-methylphenol ug/L 61.7100 62 21-119
4-Chloroaniline ug/L 55.0100 55 10-122
4-Chlorophenylphenyl ether ug/L 43.350 87 22-112
4-Nitroaniline ug/L 73.1100 73 14-118
4-Nitrophenol ug/L 86.4250 35 10-110
Acenaphthene ug/L 37.950 76 20-105
Acenaphthylene ug/L 33.450 67 23-106
Aniline ug/L 23.350 47 10-110
Anthracene ug/L 40.250 80 25-120
Benzo(a)anthracene ug/L 41.350 83 21-128
Benzo(a)pyrene ug/L 40.650 81 25-116
Benzo(b)fluoranthene ug/L 42.050 84 23-117
Benzo(g,h,i)perylene ug/L 45.050 90 17-128
Benzo(k)fluoranthene ug/L 43.150 86 25-127
Benzoic Acid ug/L 53.9250 22 10-110
Benzyl alcohol ug/L 58.5100 59 10-101
bis(2-Chloroethoxy)methane ug/L 39.450 79 19-107
bis(2-Chloroethyl) ether ug/L 36.150 72 10-108
bis(2-Chloroisopropyl) ether ug/L 39.450 79 10-108
bis(2-Ethylhexyl)phthalate ug/L 50.950 102 16-123
Butylbenzylphthalate ug/L 50.950 102 20-118
Chrysene ug/L 37.350 75 24-125
Di-n-butylphthalate ug/L 47.050 94 23-115
Di-n-octylphthalate ug/L 43.950 88 20-115
Dibenz(a,h)anthracene ug/L 40.750 81 18-131
Dibenzofuran ug/L 38.150 76 23-106
Diethylphthalate ug/L 44.550 89 24-115
Dimethylphthalate ug/L 42.050 84 22-113
Fluoranthene ug/L 44.850 90 24-125
Fluorene ug/L 39.050 78 24-114
Hexachloro-1,3-butadiene ug/L 34.650 69 10-110
Hexachlorobenzene ug/L 42.950 86 22-127
Hexachlorocyclopentadiene ug/L 42.550 85 10-110
Hexachloroethane ug/L 39.550 79 10-110
Indeno(1,2,3-cd)pyrene ug/L 38.950 78 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 69 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
773119LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 34.450 69 23-114
N-Nitroso-di-n-propylamine ug/L 39.050 78 21-114
N-Nitrosodimethylamine ug/L 25.450 51 10-110
N-Nitrosodiphenylamine ug/L 39.450 79 24-123
Naphthalene ug/L 29.250 58 14-110
Nitrobenzene ug/L 32.350 65 16-106
Pentachlorophenol ug/L 92.9100 93 10-123
Phenanthrene ug/L 38.650 77 25-119
Phenol ug/L 13.850 28 10-110
Pyrene ug/L 42.250 84 22-127
2,4,6-Tribromophenol (S)%88 27-110
2-Fluorobiphenyl (S)%74 27-110
2-Fluorophenol (S)%38 12-110
Nitrobenzene-d5 (S)%57 21-110
Phenol-d6 (S)%24 10-110
Terphenyl-d14 (S)%96 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 70 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4784
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Dup
Result QualifiersRPDResult
92119689001
771399SAMPLE DUPLICATE:
Percent Moisture %42.5 142.1
Parameter Units
Dup
Result QualifiersRPDResult
92119751001
771400SAMPLE DUPLICATE:
Percent Moisture %24.1 625.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 71 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/21051
EPA 180.1
EPA 180.1
180.1 Turbidity
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771384
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Turbidity NTU ND 1.0 06/01/12 00:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771385LABORATORY CONTROL SAMPLE:
LCSSpike
Turbidity NTU 9.910 99 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92119631001
771386SAMPLE DUPLICATE:
Turbidity NTU 2.4 12.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 72 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/21066
SM 2540D
SM 2540D
2540D Total Suspended Solids
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772125
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682008
Matrix:Water
Analyzed
Total Suspended Solids mg/L ND 2.5 06/01/12 22:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772126LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 260250 104 80-120
Parameter Units
Dup
Result QualifiersRPDResult
92119756001
772270SAMPLE DUPLICATE:
Total Suspended Solids mg/L 200 3195
Parameter Units
Dup
Result QualifiersRPDResult
92119638008
772271SAMPLE DUPLICATE:
Total Suspended Solids mg/L 10.3 310
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 73 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/21084
SM 2540D
SM 2540D
2540D Total Suspended Solids
Associated Lab Samples:92119682009, 92119682010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772784
Associated Lab Samples:92119682009, 92119682010
Matrix:Water
Analyzed
Total Suspended Solids mg/L ND 2.5 06/04/12 16:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772785LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 274250 110 80-120
Parameter Units
Dup
Result QualifiersRPDResult
92119843001
772788SAMPLE DUPLICATE:
Total Suspended Solids mg/L 5450 95000
Parameter Units
Dup
Result QualifiersRPDResult
92119705001
772793SAMPLE DUPLICATE:
Total Suspended Solids mg/L 4.3 D6114.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 74 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/21068
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772203
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
BOD, 5 day mg/L ND 2.0 06/06/12 17:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772204LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day mg/L 177198 89 84-115
Parameter Units
Dup
Result QualifiersRPDResult
92119678001
772205SAMPLE DUPLICATE:
BOD, 5 day mg/L 4.1 D6223.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 75 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12256
EPA 350.1
EPA 350.1
350.1 Ammonia
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772888
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 06/05/12 13:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772889LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.05 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
772891MATRIX SPIKE SAMPLE:
MSSpike
Result
92119678001
Nitrogen, Ammonia mg/L 4.7 M156990-1101.2
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
772893MATRIX SPIKE SAMPLE:
MSSpike
Result
92119291003
Nitrogen, Ammonia mg/L 21.05 95 90-11016.2
Parameter Units
Dup
Result QualifiersRPDResult
92119678001
772890SAMPLE DUPLICATE:
Nitrogen, Ammonia mg/L 1.2 01.2
Parameter Units
Dup
Result QualifiersRPDResult
92119291003
772892SAMPLE DUPLICATE:
Nitrogen, Ammonia mg/L 16.1 116.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 76 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12235
EPA 351.2
EPA 351.2
351.2 TKN
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771463
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Nitrogen, Kjeldahl, Total mg/L ND 0.50 06/02/12 09:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771464LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 10.210 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771465MATRIX SPIKE SAMPLE:
MSSpike
Result
92119366012
Nitrogen, Kjeldahl, Total mg/L 16.0 M11012590-1103.5
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771473MATRIX SPIKE SAMPLE:
MSSpike
Result
92119750001
Nitrogen, Kjeldahl, Total mg/L 141 M61018990-110122
Parameter Units
Dup
Result QualifiersRPDResult
92119366013
771466SAMPLE DUPLICATE:
Nitrogen, Kjeldahl, Total mg/L 3.7 64.0
Parameter Units
Dup
Result QualifiersRPDResult
92119291006
771474SAMPLE DUPLICATE:
Nitrogen, Kjeldahl, Total mg/L 5.1 35.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 77 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12228
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771374
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.020 06/01/12 00:22
Nitrogen, Nitrite mg/L ND 0.020 06/01/12 00:22
Nitrogen, NO2 plus NO3 mg/L ND 0.020 06/01/12 00:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771375LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 5.15 101 90-110
Nitrogen, Nitrite mg/L 1.11 105 90-110
Nitrogen, NO2 plus NO3 mg/L 5.15 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771376MATRIX SPIKE SAMPLE:
MSSpike
Result
92119710001
Nitrogen, Nitrate mg/L 5.7 H1,M1511190-1100.13
Nitrogen, Nitrite mg/L 0.98 H119890-110ND
Nitrogen, NO2 plus NO3 mg/L 5.7 H1,M1511190-1100.13
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771378MATRIX SPIKE SAMPLE:
MSSpike
Result
92119743001
Nitrogen, Nitrate mg/L 5.6 H1510790-1100.23
Nitrogen, Nitrite mg/L 1.0 H1110090-110ND
Nitrogen, NO2 plus NO3 mg/L 5.6 H1510790-1100.23
Parameter Units
Dup
Result QualifiersRPDResult
92119710001
771377SAMPLE DUPLICATE:
Nitrogen, Nitrate mg/L 0.13 H160.13
Nitrogen, Nitrite mg/L ND H1ND
Nitrogen, NO2 plus NO3 mg/L 0.13 H160.13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 78 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Parameter Units
Dup
Result QualifiersRPDResult
92119743001
771379SAMPLE DUPLICATE:
Nitrogen, Nitrate mg/L 0.24 H110.23
Nitrogen, Nitrite mg/L ND H1ND
Nitrogen, NO2 plus NO3 mg/L 0.24 H110.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 79 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12240
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:772275
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Phosphorus mg/L ND 0.050 06/03/12 08:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
772276LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/L 2.52.5 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
772279MATRIX SPIKE SAMPLE:
MSSpike
Result
92119759009
Phosphorus mg/L 2.92.5 101 90-1100.35
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
772309MATRIX SPIKE SAMPLE:
MSSpike
Result
92119678001
Phosphorus mg/L 10.92.5 108 90-1108.2
Parameter Units
Dup
Result QualifiersRPDResult
92119270001
772280SAMPLE DUPLICATE:
Phosphorus mg/L 0.21 30.22
Parameter Units
Dup
Result QualifiersRPDResult
92119682004
772310SAMPLE DUPLICATE:
Phosphorus mg/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 80 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12268
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92119682004, 92119682005, 92119682006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:774437
Associated Lab Samples:92119682004, 92119682005, 92119682006
Matrix:Water
Analyzed
Chemical Oxygen Demand mg/L ND 25.0 06/06/12 21:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
774438LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand mg/L 774750 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
774439MATRIX SPIKE SAMPLE:
MSSpike
Result
92119650001
Chemical Oxygen Demand mg/L 1190750 96 75-125469
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
774441MATRIX SPIKE SAMPLE:
MSSpike
Result
92119682004
Chemical Oxygen Demand mg/L 751750 100 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92119650001
774440SAMPLE DUPLICATE:
Chemical Oxygen Demand mg/L 474 1469
Parameter Units
Dup
Result QualifiersRPDResult
92119682004
774442SAMPLE DUPLICATE:
Chemical Oxygen Demand mg/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 81 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12263
EPA 7196
EPA 7196
7196 Chromium, Hexavalent
Associated Lab Samples:92119682001, 92119682002, 92119682003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:773803
Associated Lab Samples:92119682001, 92119682002, 92119682003
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg ND 5.0 N206/06/12 14:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
773804LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 51.5 N25010390-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
773806MATRIX SPIKE SAMPLE:
MSSpike
Result
92119682001
Chromium, Hexavalent mg/kg 5.7 N269575-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92119682001
773805SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND N2ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 82 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/12226
EPA 7196
EPA 7196
7196 Chromium, Hexavalent
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:771347
Associated Lab Samples:92119682004, 92119682005, 92119682006, 92119682007
Matrix:Water
Analyzed
Chromium, Hexavalent mg/L ND 0.050 N205/31/12 22:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
771348LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/L 0.51 N2.5 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
771349MATRIX SPIKE SAMPLE:
MSSpike
Result
92119682004
Chromium, Hexavalent mg/L 0.51 N2.5 102 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92119682004
771350SAMPLE DUPLICATE:
Chromium, Hexavalent mg/L ND N2ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 83 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Results based upon colony counts outside acceptable range.u1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 84 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92119682004 GCSV/12129DSEPA 1664A
92119682005 GCSV/12129SSEPA 1664A
92119682006 GCSV/12129USEPA 1664A
92119682001 MPRP/10716 ICP/9861DSEPA 3050 EPA 6010
92119682002 MPRP/10716 ICP/9861SSEPA 3050 EPA 6010
92119682003 MPRP/10716 ICP/9861USEPA 3050 EPA 6010
92119682004 MPRP/10715 ICP/9860DSSM 3030C EPA 6010
92119682005 MPRP/10715 ICP/9860SSSM 3030C EPA 6010
92119682006 MPRP/10715 ICP/9860USSM 3030C EPA 6010
92119682007 MPRP/10715 ICP/9860FIELD BLANK SM 3030C EPA 6010
92119682004 MBCH/4171DSSM 9222D
92119682005 MBCH/4171SSSM 9222D
92119682006 MBCH/4171USSM 9222D
92119682004 MBCH/4168 MBCH/4173DSSM 9223 SM 9223
92119682005 MBCH/4168 MBCH/4173SSSM 9223 SM 9223
92119682006 MBCH/4168 MBCH/4173USSM 9223 SM 9223
92119682004 MERP/4268 MERC/4192DSEPA 7470 EPA 7470
92119682005 MERP/4268 MERC/4192SSEPA 7470 EPA 7470
92119682006 MERP/4268 MERC/4192USEPA 7470 EPA 7470
92119682007 MERP/4268 MERC/4192FIELD BLANK EPA 7470 EPA 7470
92119682001 MERP/4264 MERC/4185DSEPA 7471 EPA 7471
92119682002 MERP/4264 MERC/4185SSEPA 7471 EPA 7471
92119682003 MERP/4264 MERC/4185USEPA 7471 EPA 7471
92119682001 OEXT/17699 MSSV/6341DSEPA 3546 EPA 8270 by SIM
92119682002 OEXT/17699 MSSV/6341SSEPA 3546 EPA 8270 by SIM
92119682003 OEXT/17699 MSSV/6341USEPA 3546 EPA 8270 by SIM
92119682001 OEXT/17720 MSSV/6357DSEPA 3546 EPA 8270
92119682002 OEXT/17720 MSSV/6357SSEPA 3546 EPA 8270
92119682003 OEXT/17720 MSSV/6357USEPA 3546 EPA 8270
92119682004 OEXT/17711 MSSV/6348DSEPA 3510 EPA 8270
92119682005 OEXT/17711 MSSV/6348SSEPA 3510 EPA 8270
92119682006 OEXT/17711 MSSV/6348USEPA 3510 EPA 8270
92119682007 OEXT/17739 MSSV/6360FIELD BLANK EPA 3510 EPA 8270
92119682004 MSV/19322DSEPA 8260
92119682005 MSV/19322SSEPA 8260
92119682006 MSV/19322USEPA 8260
92119682007 MSV/19322FIELD BLANK EPA 8260
92119682001 MSV/19317DSEPA 8260
92119682002 MSV/19317SSEPA 8260
92119682003 MSV/19317USEPA 8260
92119682001 PMST/4784DSASTM D2974-87
92119682002 PMST/4784SSASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 85 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92119682
FORMER PLIANA FACILITY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92119682003 PMST/4784USASTM D2974-87
92119682004 WET/21051DSEPA 180.1
92119682005 WET/21051SSEPA 180.1
92119682006 WET/21051USEPA 180.1
92119682004 WET/21066DSSM 2540D
92119682005 WET/21066SSSM 2540D
92119682006 WET/21066USSM 2540D
92119682008 WET/21066DS-USGS SSC SM 2540D
92119682009 WET/21084SS-USGS SSC SM 2540D
92119682010 WET/21084US-USGS SSC SM 2540D
92119682004 WET/21068 WET/21069DSSM 5210B SM 5210B
92119682005 WET/21068 WET/21069SSSM 5210B SM 5210B
92119682006 WET/21068 WET/21069USSM 5210B SM 5210B
92119682004 WETA/12256DSEPA 350.1
92119682005 WETA/12256SSEPA 350.1
92119682006 WETA/12256USEPA 350.1
92119682004 WETA/12235DSEPA 351.2
92119682005 WETA/12235SSEPA 351.2
92119682006 WETA/12235USEPA 351.2
92119682004 WETA/12228DSEPA 353.2
92119682005 WETA/12228SSEPA 353.2
92119682006 WETA/12228USEPA 353.2
92119682004 WETA/12240DSEPA 365.1
92119682005 WETA/12240SSEPA 365.1
92119682006 WETA/12240USEPA 365.1
92119682004 WETA/12268DSSM 5220D
92119682005 WETA/12268SSSM 5220D
92119682006 WETA/12268USSM 5220D
92119682001 WETA/12263 WETA/12264DSEPA 7196 EPA 7196
92119682002 WETA/12263 WETA/12264SSEPA 7196 EPA 7196
92119682003 WETA/12263 WETA/12264USEPA 7196 EPA 7196
92119682004 WETA/12226DSEPA 7196
92119682005 WETA/12226SSEPA 7196
92119682006 WETA/12226USEPA 7196
92119682007 WETA/12226FIELD BLANK EPA 7196
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/12/2012 05:26 PM Page 86 of 86
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]