17047_REEP_Import Fill_20160912

Table 1Summary of Import Soil Analytical DataContinental Tire - Building Improvements (BF Project #17047-13-60)1900 Continental BoulevardCharlotte, North CarolinaH&H Job No. LRC-003LocationSample ID Quarry-1 Quarry-2 Quarry-3 Quarry-4 Quarry-5 911 BlendedSample Date 8/31/2016 8/31/2016 8/31/2016 8/31/2016 8/31/2016 1/21/2016Source911 StockpileUnitsVOCs (8260B)Acetone0.0646<0.0522 <0.0550 <0.0546 <0.0473 <0.044100,000 NA NASVOCs (8270)ALL BRL ALL BRL ALL BRL ALL BRL ALL BRL ALL BRLNA NA NARCRA Metals (6010/7196A)Arsenic<2.74 <2.62 <2.48 <2.58 <2.232.8 3.0 1.0 - 18 4.8Beryllium<1.37 <1.31 <1.24 <1.29 <1.120.68 460 BRL - 2.0 0.11Chromium15.8 6.48 10.9 44.4 5.02 16NE 7 - 300 65Chromium (VI)<6.72 <6.32 <6.13 <6.60 <5.48 <0.1456.30 NS NSChromium (III)15.8 6.48 10.9 44.4 5.02 16100,000 NS NSCopper5.83 5.17 22.9 23.9 11.7 269,400 3 - 100 34Lead20.4 14.8 22.3 17.2 8.58 2.6800 BRL - 50 16Manganese152 219 798 719 407 2805,200 8 - 3,394 594Nickel10.5 4.09 15.8 22.9 6.23 9.94,400 BRL - 150 23Silver<1.37 <1.31 <1.24 <1.29 <1.120.361,160 BRL - 5.0 NSZinc14.8 15.5 34.0 21.1 33.5 4670,000 25 -124 56Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (April 2016).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) Range and mean values for manganese from Southeastern USA soils from Elements in North American Soils4) Range and mean values for silver from conterminous United States soils from Elements in North American SoilsSoil concentrations are reported in milligrams per kilogram (mg/kg).Laboratory analytical methods are shown in parentheses.Only compounds detected in at least one sample shown above; see chain of custody form for complete list analyzed.NA = Not Applicable; NS = Not Specified; NE = Not Established; BRL = below laboratory reporting limitsScreening CriteriaOverburden Vulcan Materials CompanyIndustrial/CommercialPSRGs(1)Range Mean(mg/kg)Regional Background Metals in Soil(2,3,4)S:\AAA-Master Projects\LRC Patriot (LRC)\LRC-003 Continental EMP - bldg improvements\Vulcan Borrow Site\Tables\rwm data.xlsm9/12/2016Table 1Hart & Hickman, PC
QUARRY-1
QUARRY-2
QUARRY-3
QUARRY-4
QUARRY-5
JOB NO. LRC-003
REVISION NO. 0DATE: 9-12-16
FIGURE NO. 1
LEGEND
SITE PROPERTY BOUNDARY
SOIL SAMPLE LOCATION
CONTINENTAL TIRE (BF PROJECT# 17047-13-60)
1900 CONTINENTAL BOULEVARD
CHARLOTTE, NORTH CAROLINA
IMPORT SOIL SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
UPTOWN
CHARLOTTE
NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS DEPARTMENT (2014).
2.SOIL SAMPLES COLLECTED BY H&H FROM VULCAN
MATERIAL COMPANY QUARRY ON 8/31/16.
NATIO
N
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F
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R
D
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D
OLD NATIONS FORD ROADS:\AAA-Master Projects\LRC Patriot (LRC)\LRC-003 Continental EMP - bldg improvements\Vulcan Borrow Site\Figures\Import Soil Sample Location Map.dwg, FIG 1, 9/12/2016 11:02:21 AM, zbarlow
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-110980-1
TestAmerica Sample Delivery Group: LRC-003
Client Project/Site: Continental Tire
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Ralph McGee
Authorized for release by:
9/9/2016 1:54:06 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Continental Tire
TestAmerica Job ID: 490-110980-1
SDG: LRC-003
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
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Sample Summary
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-110980-1 Vulcan Quarry-1 Solid 08/31/16 14:20 09/01/16 09:20
490-110980-2 Vulcan Quarry-2 Solid 08/31/16 14:25 09/01/16 09:20
490-110980-3 Vulcan Quarry-3 Solid 08/31/16 14:30 09/01/16 09:20
490-110980-4 Vulcan Quarry-4 Solid 08/31/16 14:35 09/01/16 09:20
490-110980-5 Vulcan Quarry-5 Solid 08/31/16 14:40 09/01/16 09:20
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-110980-1
Project/Site: Continental Tire SDG: LRC-003
Job ID: 490-110980-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-110980-1
Comments
No additional comments.
Receipt
The samples were received on 9/1/2016 9:20 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 3.2º C.
GC/MS VOA
Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-368523.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Qualifiers
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
F2 MS/MSD RPD exceeds control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-1Client Sample ID: Vulcan Quarry-1
Matrix: SolidDate Collected: 08/31/16 14:20
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0646 0.0566 mg/Kg ☼08/31/16 13:20 09/08/16 20:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Benzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Bromobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Bromochloromethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Bromodichloromethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Bromoform ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Bromomethane ND
0.0566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼2-Butanone (MEK)ND
0.00566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Carbon disulfide ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Carbon tetrachloride ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Chlorobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Chlorodibromomethane ND
0.00566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Chloroethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Chloroform ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Chloromethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼2-Chlorotoluene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼4-Chlorotoluene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼cis-1,2-Dichloroethene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼cis-1,3-Dichloropropene ND
0.00566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2-Dibromo-3-Chloropropane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2-Dibromoethane (EDB)ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Dibromomethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2-Dichlorobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,3-Dichlorobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,4-Dichlorobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Dichlorodifluoromethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,1-Dichloroethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2-Dichloroethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,1-Dichloroethene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2-Dichloroethene, Total ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2-Dichloropropane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,3-Dichloropropane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼2,2-Dichloropropane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,1-Dichloropropene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Diisopropyl ether ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Ethylbenzene ND
0.00566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Hexachlorobutadiene ND
0.0566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼2-Hexanone ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Isopropylbenzene ND
0.0113 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Methylene Chloride ND
0.0566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼4-Methyl-2-pentanone (MIBK)ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Methyl tert-butyl ether ND
0.00566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Naphthalene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼n-Butylbenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼N-Propylbenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼p-Isopropyltoluene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼sec-Butylbenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Styrene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-1Client Sample ID: Vulcan Quarry-1
Matrix: SolidDate Collected: 08/31/16 14:20
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00226 mg/Kg ☼08/31/16 13:20 09/08/16 20:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,1,2,2-Tetrachloroethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Tetrachloroethene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Toluene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼trans-1,2-Dichloroethene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼trans-1,3-Dichloropropene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2,3-Trichlorobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2,4-Trichlorobenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,1,1-Trichloroethane ND
0.00566 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,1,2-Trichloroethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Trichloroethene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Trichlorofluoromethane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2,3-Trichloropropane ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,2,4-Trimethylbenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼1,3,5-Trimethylbenzene ND
0.00226 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Vinyl chloride ND
0.00679 mg/Kg 08/31/16 13:20 09/08/16 20:40 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)103 70-130 08/31/16 13:20 09/08/16 20:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)113 08/31/16 13:20 09/08/16 20:40 170-130
1,2-Dichloroethane-d4 (Surr)119 08/31/16 13:20 09/08/16 20:40 170-130
Toluene-d8 (Surr)101 08/31/16 13:20 09/08/16 20:40 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0923 mg/Kg ☼09/02/16 10:42 09/02/16 18:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Acenaphthylene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Anthracene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Benzo[a]anthracene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Benzo[a]pyrene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Benzo[b]fluoranthene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Benzo[g,h,i]perylene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Benzo[k]fluoranthene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Bis(2-chloroethoxy)methane ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Bis(2-chloroethyl)ether ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼bis (2-chloroisopropyl) ether ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Bis(2-ethylhexyl) phthalate ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4-Bromophenyl phenyl ether ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Butyl benzyl phthalate ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Carbazole ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4-Chloroaniline ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4-Chloro-3-methylphenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2-Chloronaphthalene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2-Chlorophenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4-Chlorophenyl phenyl ether ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Chrysene ND
0.917 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Cresols ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Dibenz(a,h)anthracene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-1Client Sample ID: Vulcan Quarry-1
Matrix: SolidDate Collected: 08/31/16 14:20
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.459 mg/Kg ☼09/02/16 10:42 09/02/16 18:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼1,3-Dichlorobenzene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼1,4-Dichlorobenzene ND
0.923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼3,3'-Dichlorobenzidine ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,4-Dichlorophenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Diethyl phthalate ND
0.923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,4-Dimethylphenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Dimethyl phthalate ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Di-n-butyl phthalate ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4,6-Dinitro-2-methylphenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,4-Dinitrophenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,4-Dinitrotoluene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,6-Dinitrotoluene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Di-n-octyl phthalate ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Fluoranthene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Fluorene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Hexachlorobenzene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Hexachlorobutadiene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Hexachlorocyclopentadiene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Hexachloroethane ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Indeno[1,2,3-cd]pyrene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Isophorone ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼1-Methylnaphthalene ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2-Methylnaphthalene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2-Methylphenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼3 & 4 Methylphenol ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Naphthalene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2-Nitroaniline ND
0.923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼3-Nitroaniline ND
0.923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4-Nitroaniline ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Nitrobenzene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2-Nitrophenol ND
0.923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼4-Nitrophenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼N-Nitrosodi-n-propylamine ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Pentachlorophenol ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Phenanthrene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Phenol ND
0.0923 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼Pyrene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼1,2,4-Trichlorobenzene ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,4,5-Trichlorophenol ND
0.459 mg/Kg 09/02/16 10:42 09/02/16 18:02 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)37 29-120 09/02/16 10:42 09/02/16 18:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)39 09/02/16 10:42 09/02/16 18:02 110-120
Nitrobenzene-d5 (Surr)37 09/02/16 10:42 09/02/16 18:02 127-120
Phenol-d5 (Surr)42 09/02/16 10:42 09/02/16 18:02 110-120
Terphenyl-d14 (Surr)65 09/02/16 10:42 09/02/16 18:02 113-120
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-1Client Sample ID: Vulcan Quarry-1
Matrix: SolidDate Collected: 08/31/16 14:20
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)60 10-120 09/02/16 10:42 09/02/16 18:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony ND 13.7 mg/Kg ☼09/06/16 14:16 09/07/16 02:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.74 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Arsenic ND
1.37 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Beryllium ND
1.37 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Cadmium ND
1.37 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Chromium 15.8
2.74 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Copper 5.83
1.37 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Lead 20.4 F1
4.11 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Manganese 152 F2 F1
2.74 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Nickel 10.5
2.74 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Selenium ND
1.37 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Silver ND F1
2.74 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Thallium ND
13.7 mg/Kg 09/06/16 14:16 09/07/16 02:21 1☼Zinc 14.8
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.137 mg/Kg ☼09/06/16 10:01 09/06/16 17:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.72 mg/Kg ☼09/07/16 09:06 09/07/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 71.9 0.1 %09/03/16 08:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-2Client Sample ID: Vulcan Quarry-2
Matrix: SolidDate Collected: 08/31/16 14:25
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0522 mg/Kg ☼08/31/16 13:25 09/08/16 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Benzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Bromobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Bromochloromethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Bromodichloromethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Bromoform ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Bromomethane ND
0.0522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼2-Butanone (MEK)ND
0.00522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Carbon disulfide ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Carbon tetrachloride ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Chlorobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Chlorodibromomethane ND
0.00522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Chloroethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Chloroform ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Chloromethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼2-Chlorotoluene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼4-Chlorotoluene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼cis-1,2-Dichloroethene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼cis-1,3-Dichloropropene ND
0.00522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2-Dibromo-3-Chloropropane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2-Dibromoethane (EDB)ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Dibromomethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2-Dichlorobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,3-Dichlorobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,4-Dichlorobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Dichlorodifluoromethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,1-Dichloroethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2-Dichloroethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,1-Dichloroethene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2-Dichloroethene, Total ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2-Dichloropropane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,3-Dichloropropane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼2,2-Dichloropropane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,1-Dichloropropene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Diisopropyl ether ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Ethylbenzene ND
0.00522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Hexachlorobutadiene ND
0.0522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼2-Hexanone ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Isopropylbenzene ND
0.0104 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Methylene Chloride ND
0.0522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼4-Methyl-2-pentanone (MIBK)ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Methyl tert-butyl ether ND
0.00522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Naphthalene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼n-Butylbenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼N-Propylbenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼p-Isopropyltoluene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼sec-Butylbenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Styrene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-2Client Sample ID: Vulcan Quarry-2
Matrix: SolidDate Collected: 08/31/16 14:25
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00209 mg/Kg ☼08/31/16 13:25 09/08/16 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,1,2,2-Tetrachloroethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Tetrachloroethene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Toluene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼trans-1,2-Dichloroethene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼trans-1,3-Dichloropropene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2,3-Trichlorobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2,4-Trichlorobenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,1,1-Trichloroethane ND
0.00522 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,1,2-Trichloroethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Trichloroethene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Trichlorofluoromethane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2,3-Trichloropropane ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,2,4-Trimethylbenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼1,3,5-Trimethylbenzene ND
0.00209 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Vinyl chloride ND
0.00626 mg/Kg 08/31/16 13:25 09/08/16 21:07 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)98 70-130 08/31/16 13:25 09/08/16 21:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 08/31/16 13:25 09/08/16 21:07 170-130
1,2-Dichloroethane-d4 (Surr)113 08/31/16 13:25 09/08/16 21:07 170-130
Toluene-d8 (Surr)102 08/31/16 13:25 09/08/16 21:07 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0860 mg/Kg ☼09/02/16 10:42 09/02/16 18:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Acenaphthylene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Anthracene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Benzo[a]anthracene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Benzo[a]pyrene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Benzo[b]fluoranthene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Benzo[g,h,i]perylene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Benzo[k]fluoranthene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Bis(2-chloroethoxy)methane ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Bis(2-chloroethyl)ether ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼bis (2-chloroisopropyl) ether ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Bis(2-ethylhexyl) phthalate ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4-Bromophenyl phenyl ether ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Butyl benzyl phthalate ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Carbazole ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4-Chloroaniline ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4-Chloro-3-methylphenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2-Chloronaphthalene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2-Chlorophenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4-Chlorophenyl phenyl ether ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Chrysene ND
0.855 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Cresols ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Dibenz(a,h)anthracene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-2Client Sample ID: Vulcan Quarry-2
Matrix: SolidDate Collected: 08/31/16 14:25
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.427 mg/Kg ☼09/02/16 10:42 09/02/16 18:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼1,3-Dichlorobenzene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼1,4-Dichlorobenzene ND
0.860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼3,3'-Dichlorobenzidine ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,4-Dichlorophenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Diethyl phthalate ND
0.860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,4-Dimethylphenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Dimethyl phthalate ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Di-n-butyl phthalate ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4,6-Dinitro-2-methylphenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,4-Dinitrophenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,4-Dinitrotoluene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,6-Dinitrotoluene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Di-n-octyl phthalate ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Fluoranthene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Fluorene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Hexachlorobenzene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Hexachlorobutadiene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Hexachlorocyclopentadiene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Hexachloroethane ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Indeno[1,2,3-cd]pyrene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Isophorone ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼1-Methylnaphthalene ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2-Methylnaphthalene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2-Methylphenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼3 & 4 Methylphenol ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Naphthalene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2-Nitroaniline ND
0.860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼3-Nitroaniline ND
0.860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4-Nitroaniline ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Nitrobenzene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2-Nitrophenol ND
0.860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼4-Nitrophenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼N-Nitrosodi-n-propylamine ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Pentachlorophenol ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Phenanthrene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Phenol ND
0.0860 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼Pyrene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼1,2,4-Trichlorobenzene ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,4,5-Trichlorophenol ND
0.427 mg/Kg 09/02/16 10:42 09/02/16 18:22 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)59 29-120 09/02/16 10:42 09/02/16 18:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)65 09/02/16 10:42 09/02/16 18:22 110-120
Nitrobenzene-d5 (Surr)64 09/02/16 10:42 09/02/16 18:22 127-120
Phenol-d5 (Surr)66 09/02/16 10:42 09/02/16 18:22 110-120
Terphenyl-d14 (Surr)78 09/02/16 10:42 09/02/16 18:22 113-120
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-2Client Sample ID: Vulcan Quarry-2
Matrix: SolidDate Collected: 08/31/16 14:25
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)76 10-120 09/02/16 10:42 09/02/16 18:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony ND 13.1 mg/Kg ☼09/06/16 14:16 09/07/16 02:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.62 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Arsenic ND
1.31 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Beryllium ND
1.31 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Cadmium ND
1.31 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Chromium 6.48
2.62 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Copper 5.17
1.31 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Lead 14.8
3.93 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Manganese 219
2.62 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Nickel 4.09
2.62 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Selenium ND
1.31 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Silver ND
2.62 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Thallium ND
13.1 mg/Kg 09/06/16 14:16 09/07/16 02:45 1☼Zinc 15.5
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.129 mg/Kg ☼09/06/16 10:01 09/06/16 17:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.32 mg/Kg ☼09/07/16 09:06 09/07/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 76.5 0.1 %09/03/16 08:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-3Client Sample ID: Vulcan Quarry-3
Matrix: SolidDate Collected: 08/31/16 14:30
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0550 mg/Kg ☼08/31/16 13:30 09/08/16 21:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Benzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Bromobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Bromochloromethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Bromodichloromethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Bromoform ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Bromomethane ND
0.0550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼2-Butanone (MEK)ND
0.00550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Carbon disulfide ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Carbon tetrachloride ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Chlorobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Chlorodibromomethane ND
0.00550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Chloroethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Chloroform ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Chloromethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼2-Chlorotoluene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼4-Chlorotoluene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼cis-1,2-Dichloroethene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼cis-1,3-Dichloropropene ND
0.00550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2-Dibromo-3-Chloropropane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2-Dibromoethane (EDB)ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Dibromomethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2-Dichlorobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,3-Dichlorobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,4-Dichlorobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Dichlorodifluoromethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,1-Dichloroethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2-Dichloroethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,1-Dichloroethene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2-Dichloroethene, Total ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2-Dichloropropane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,3-Dichloropropane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼2,2-Dichloropropane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,1-Dichloropropene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Diisopropyl ether ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Ethylbenzene ND
0.00550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Hexachlorobutadiene ND
0.0550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼2-Hexanone ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Isopropylbenzene ND
0.0110 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Methylene Chloride ND
0.0550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼4-Methyl-2-pentanone (MIBK)ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Methyl tert-butyl ether ND
0.00550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Naphthalene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼n-Butylbenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼N-Propylbenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼p-Isopropyltoluene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼sec-Butylbenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Styrene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-3Client Sample ID: Vulcan Quarry-3
Matrix: SolidDate Collected: 08/31/16 14:30
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00220 mg/Kg ☼08/31/16 13:30 09/08/16 21:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,1,2,2-Tetrachloroethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Tetrachloroethene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Toluene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼trans-1,2-Dichloroethene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼trans-1,3-Dichloropropene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2,3-Trichlorobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2,4-Trichlorobenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,1,1-Trichloroethane ND
0.00550 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,1,2-Trichloroethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Trichloroethene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Trichlorofluoromethane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2,3-Trichloropropane ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,2,4-Trimethylbenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼1,3,5-Trimethylbenzene ND
0.00220 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Vinyl chloride ND
0.00660 mg/Kg 08/31/16 13:30 09/08/16 21:35 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)95 70-130 08/31/16 13:30 09/08/16 21:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)111 08/31/16 13:30 09/08/16 21:35 170-130
1,2-Dichloroethane-d4 (Surr)113 08/31/16 13:30 09/08/16 21:35 170-130
Toluene-d8 (Surr)103 08/31/16 13:30 09/08/16 21:35 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0836 mg/Kg ☼09/02/16 10:42 09/02/16 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Acenaphthylene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Anthracene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Benzo[a]anthracene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Benzo[a]pyrene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Benzo[b]fluoranthene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Benzo[g,h,i]perylene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Benzo[k]fluoranthene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Bis(2-chloroethoxy)methane ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Bis(2-chloroethyl)ether ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼bis (2-chloroisopropyl) ether ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Bis(2-ethylhexyl) phthalate ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4-Bromophenyl phenyl ether ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Butyl benzyl phthalate ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Carbazole ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4-Chloroaniline ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4-Chloro-3-methylphenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2-Chloronaphthalene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2-Chlorophenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4-Chlorophenyl phenyl ether ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Chrysene ND
0.831 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Cresols ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Dibenz(a,h)anthracene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-3Client Sample ID: Vulcan Quarry-3
Matrix: SolidDate Collected: 08/31/16 14:30
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.416 mg/Kg ☼09/02/16 10:42 09/02/16 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼1,3-Dichlorobenzene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼1,4-Dichlorobenzene ND
0.836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼3,3'-Dichlorobenzidine ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,4-Dichlorophenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Diethyl phthalate ND
0.836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,4-Dimethylphenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Dimethyl phthalate ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Di-n-butyl phthalate ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4,6-Dinitro-2-methylphenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,4-Dinitrophenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,4-Dinitrotoluene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,6-Dinitrotoluene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Di-n-octyl phthalate ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Fluoranthene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Fluorene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Hexachlorobenzene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Hexachlorobutadiene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Hexachlorocyclopentadiene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Hexachloroethane ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Indeno[1,2,3-cd]pyrene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Isophorone ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼1-Methylnaphthalene ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2-Methylnaphthalene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2-Methylphenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼3 & 4 Methylphenol ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Naphthalene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2-Nitroaniline ND
0.836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼3-Nitroaniline ND
0.836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4-Nitroaniline ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Nitrobenzene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2-Nitrophenol ND
0.836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼4-Nitrophenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼N-Nitrosodi-n-propylamine ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Pentachlorophenol ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Phenanthrene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Phenol ND
0.0836 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼Pyrene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼1,2,4-Trichlorobenzene ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,4,5-Trichlorophenol ND
0.416 mg/Kg 09/02/16 10:42 09/02/16 18:41 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)64 29-120 09/02/16 10:42 09/02/16 18:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)70 09/02/16 10:42 09/02/16 18:41 110-120
Nitrobenzene-d5 (Surr)70 09/02/16 10:42 09/02/16 18:41 127-120
Phenol-d5 (Surr)76 09/02/16 10:42 09/02/16 18:41 110-120
Terphenyl-d14 (Surr)84 09/02/16 10:42 09/02/16 18:41 113-120
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-3Client Sample ID: Vulcan Quarry-3
Matrix: SolidDate Collected: 08/31/16 14:30
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)81 10-120 09/02/16 10:42 09/02/16 18:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony ND 12.4 mg/Kg ☼09/06/16 14:16 09/07/16 02:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.48 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Arsenic ND
1.24 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Beryllium ND
1.24 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Cadmium ND
1.24 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Chromium 10.9
2.48 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Copper 22.9
1.24 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Lead 22.3
3.72 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Manganese 798
2.48 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Nickel 15.8
2.48 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Selenium ND
1.24 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Silver ND
2.48 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Thallium ND
12.4 mg/Kg 09/06/16 14:16 09/07/16 02:50 1☼Zinc 34.0
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.125 mg/Kg ☼09/06/16 10:01 09/06/16 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.13 mg/Kg ☼09/07/16 09:06 09/07/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 80.0 0.1 %09/03/16 08:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-4Client Sample ID: Vulcan Quarry-4
Matrix: SolidDate Collected: 08/31/16 14:35
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0546 mg/Kg ☼08/31/16 13:35 09/08/16 22:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Benzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Bromobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Bromochloromethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Bromodichloromethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Bromoform ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Bromomethane ND
0.0546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼2-Butanone (MEK)ND
0.00546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Carbon disulfide ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Carbon tetrachloride ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Chlorobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Chlorodibromomethane ND
0.00546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Chloroethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Chloroform ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Chloromethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼2-Chlorotoluene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼4-Chlorotoluene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼cis-1,2-Dichloroethene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼cis-1,3-Dichloropropene ND
0.00546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2-Dibromo-3-Chloropropane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2-Dibromoethane (EDB)ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Dibromomethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2-Dichlorobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,3-Dichlorobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,4-Dichlorobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Dichlorodifluoromethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,1-Dichloroethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2-Dichloroethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,1-Dichloroethene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2-Dichloroethene, Total ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2-Dichloropropane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,3-Dichloropropane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼2,2-Dichloropropane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,1-Dichloropropene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Diisopropyl ether ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Ethylbenzene ND
0.00546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Hexachlorobutadiene ND
0.0546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼2-Hexanone ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Isopropylbenzene ND
0.0109 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Methylene Chloride ND
0.0546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼4-Methyl-2-pentanone (MIBK)ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Methyl tert-butyl ether ND
0.00546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Naphthalene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼n-Butylbenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼N-Propylbenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼p-Isopropyltoluene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼sec-Butylbenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Styrene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-4Client Sample ID: Vulcan Quarry-4
Matrix: SolidDate Collected: 08/31/16 14:35
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00218 mg/Kg ☼08/31/16 13:35 09/08/16 22:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,1,2,2-Tetrachloroethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Tetrachloroethene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Toluene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼trans-1,2-Dichloroethene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼trans-1,3-Dichloropropene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2,3-Trichlorobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2,4-Trichlorobenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,1,1-Trichloroethane ND
0.00546 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,1,2-Trichloroethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Trichloroethene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Trichlorofluoromethane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2,3-Trichloropropane ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,2,4-Trimethylbenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼1,3,5-Trimethylbenzene ND
0.00218 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Vinyl chloride ND
0.00655 mg/Kg 08/31/16 13:35 09/08/16 22:02 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)98 70-130 08/31/16 13:35 09/08/16 22:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)118 08/31/16 13:35 09/08/16 22:02 170-130
1,2-Dichloroethane-d4 (Surr)113 08/31/16 13:35 09/08/16 22:02 170-130
Toluene-d8 (Surr)104 08/31/16 13:35 09/08/16 22:02 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0897 mg/Kg ☼09/02/16 10:42 09/02/16 19:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Acenaphthylene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Anthracene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Benzo[a]anthracene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Benzo[a]pyrene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Benzo[b]fluoranthene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Benzo[g,h,i]perylene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Benzo[k]fluoranthene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Bis(2-chloroethoxy)methane ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Bis(2-chloroethyl)ether ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼bis (2-chloroisopropyl) ether ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Bis(2-ethylhexyl) phthalate ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4-Bromophenyl phenyl ether ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Butyl benzyl phthalate ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Carbazole ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4-Chloroaniline ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4-Chloro-3-methylphenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2-Chloronaphthalene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2-Chlorophenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4-Chlorophenyl phenyl ether ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Chrysene ND
0.892 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Cresols ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Dibenz(a,h)anthracene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-4Client Sample ID: Vulcan Quarry-4
Matrix: SolidDate Collected: 08/31/16 14:35
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.446 mg/Kg ☼09/02/16 10:42 09/02/16 19:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼1,3-Dichlorobenzene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼1,4-Dichlorobenzene ND
0.897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼3,3'-Dichlorobenzidine ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,4-Dichlorophenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Diethyl phthalate ND
0.897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,4-Dimethylphenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Dimethyl phthalate ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Di-n-butyl phthalate ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4,6-Dinitro-2-methylphenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,4-Dinitrophenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,4-Dinitrotoluene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,6-Dinitrotoluene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Di-n-octyl phthalate ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Fluoranthene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Fluorene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Hexachlorobenzene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Hexachlorobutadiene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Hexachlorocyclopentadiene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Hexachloroethane ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Indeno[1,2,3-cd]pyrene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Isophorone ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼1-Methylnaphthalene ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2-Methylnaphthalene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2-Methylphenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼3 & 4 Methylphenol ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Naphthalene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2-Nitroaniline ND
0.897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼3-Nitroaniline ND
0.897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4-Nitroaniline ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Nitrobenzene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2-Nitrophenol ND
0.897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼4-Nitrophenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼N-Nitrosodi-n-propylamine ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Pentachlorophenol ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Phenanthrene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Phenol ND
0.0897 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼Pyrene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼1,2,4-Trichlorobenzene ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,4,5-Trichlorophenol ND
0.446 mg/Kg 09/02/16 10:42 09/02/16 19:01 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)52 29-120 09/02/16 10:42 09/02/16 19:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)52 09/02/16 10:42 09/02/16 19:01 110-120
Nitrobenzene-d5 (Surr)53 09/02/16 10:42 09/02/16 19:01 127-120
Phenol-d5 (Surr)57 09/02/16 10:42 09/02/16 19:01 110-120
Terphenyl-d14 (Surr)74 09/02/16 10:42 09/02/16 19:01 113-120
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-4Client Sample ID: Vulcan Quarry-4
Matrix: SolidDate Collected: 08/31/16 14:35
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)68 10-120 09/02/16 10:42 09/02/16 19:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony ND 12.9 mg/Kg ☼09/06/16 14:16 09/07/16 02:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.58 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Arsenic ND
1.29 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Beryllium ND
1.29 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Cadmium ND
1.29 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Chromium 44.4
2.58 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Copper 23.9
1.29 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Lead 17.2
3.87 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Manganese 719
2.58 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Nickel 22.9
2.58 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Selenium ND
1.29 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Silver ND
2.58 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Thallium ND
12.9 mg/Kg 09/06/16 14:16 09/07/16 02:55 1☼Zinc 21.1
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.132 mg/Kg ☼09/06/16 10:01 09/06/16 17:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.60 mg/Kg ☼09/07/16 09:06 09/07/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 73.8 0.1 %09/03/16 08:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-5Client Sample ID: Vulcan Quarry-5
Matrix: SolidDate Collected: 08/31/16 14:40
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0473 mg/Kg ☼08/31/16 13:40 09/08/16 22:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Benzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Bromobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Bromochloromethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Bromodichloromethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Bromoform ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Bromomethane ND
0.0473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼2-Butanone (MEK)ND
0.00473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Carbon disulfide ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Carbon tetrachloride ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Chlorobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Chlorodibromomethane ND
0.00473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Chloroethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Chloroform ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Chloromethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼2-Chlorotoluene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼4-Chlorotoluene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼cis-1,2-Dichloroethene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼cis-1,3-Dichloropropene ND
0.00473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2-Dibromo-3-Chloropropane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2-Dibromoethane (EDB)ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Dibromomethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2-Dichlorobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,3-Dichlorobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,4-Dichlorobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Dichlorodifluoromethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,1-Dichloroethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2-Dichloroethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,1-Dichloroethene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2-Dichloroethene, Total ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2-Dichloropropane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,3-Dichloropropane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼2,2-Dichloropropane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,1-Dichloropropene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Diisopropyl ether ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Ethylbenzene ND
0.00473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Hexachlorobutadiene ND
0.0473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼2-Hexanone ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Isopropylbenzene ND
0.00947 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Methylene Chloride ND
0.0473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼4-Methyl-2-pentanone (MIBK)ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Methyl tert-butyl ether ND
0.00473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Naphthalene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼n-Butylbenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼N-Propylbenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼p-Isopropyltoluene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼sec-Butylbenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Styrene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-5Client Sample ID: Vulcan Quarry-5
Matrix: SolidDate Collected: 08/31/16 14:40
Date Received: 09/01/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00189 mg/Kg ☼08/31/16 13:40 09/08/16 22:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,1,2,2-Tetrachloroethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Tetrachloroethene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Toluene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼trans-1,2-Dichloroethene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼trans-1,3-Dichloropropene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2,3-Trichlorobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2,4-Trichlorobenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,1,1-Trichloroethane ND
0.00473 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,1,2-Trichloroethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Trichloroethene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Trichlorofluoromethane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2,3-Trichloropropane ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,2,4-Trimethylbenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼1,3,5-Trimethylbenzene ND
0.00189 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Vinyl chloride ND
0.00568 mg/Kg 08/31/16 13:40 09/08/16 22:30 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)102 70-130 08/31/16 13:40 09/08/16 22:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)113 08/31/16 13:40 09/08/16 22:30 170-130
1,2-Dichloroethane-d4 (Surr)121 08/31/16 13:40 09/08/16 22:30 170-130
Toluene-d8 (Surr)103 08/31/16 13:40 09/08/16 22:30 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0747 mg/Kg ☼09/02/16 10:42 09/02/16 19:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Acenaphthylene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Anthracene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Benzo[a]anthracene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Benzo[a]pyrene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Benzo[b]fluoranthene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Benzo[g,h,i]perylene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Benzo[k]fluoranthene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Bis(2-chloroethoxy)methane ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Bis(2-chloroethyl)ether ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼bis (2-chloroisopropyl) ether ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Bis(2-ethylhexyl) phthalate ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4-Bromophenyl phenyl ether ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Butyl benzyl phthalate ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Carbazole ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4-Chloroaniline ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4-Chloro-3-methylphenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2-Chloronaphthalene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2-Chlorophenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4-Chlorophenyl phenyl ether ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Chrysene ND
0.742 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Cresols ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Dibenz(a,h)anthracene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-5Client Sample ID: Vulcan Quarry-5
Matrix: SolidDate Collected: 08/31/16 14:40
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.371 mg/Kg ☼09/02/16 10:42 09/02/16 19:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼1,3-Dichlorobenzene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼1,4-Dichlorobenzene ND
0.747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼3,3'-Dichlorobenzidine ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,4-Dichlorophenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Diethyl phthalate ND
0.747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,4-Dimethylphenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Dimethyl phthalate ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Di-n-butyl phthalate ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4,6-Dinitro-2-methylphenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,4-Dinitrophenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,4-Dinitrotoluene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,6-Dinitrotoluene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Di-n-octyl phthalate ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Fluoranthene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Fluorene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Hexachlorobenzene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Hexachlorobutadiene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Hexachlorocyclopentadiene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Hexachloroethane ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Indeno[1,2,3-cd]pyrene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Isophorone ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼1-Methylnaphthalene ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2-Methylnaphthalene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2-Methylphenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼3 & 4 Methylphenol ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Naphthalene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2-Nitroaniline ND
0.747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼3-Nitroaniline ND
0.747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4-Nitroaniline ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Nitrobenzene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2-Nitrophenol ND
0.747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼4-Nitrophenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼N-Nitrosodi-n-propylamine ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Pentachlorophenol ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Phenanthrene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Phenol ND
0.0747 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼Pyrene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼1,2,4-Trichlorobenzene ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,4,5-Trichlorophenol ND
0.371 mg/Kg 09/02/16 10:42 09/02/16 19:20 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)60 29-120 09/02/16 10:42 09/02/16 19:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)63 09/02/16 10:42 09/02/16 19:20 110-120
Nitrobenzene-d5 (Surr)64 09/02/16 10:42 09/02/16 19:20 127-120
Phenol-d5 (Surr)63 09/02/16 10:42 09/02/16 19:20 110-120
Terphenyl-d14 (Surr)77 09/02/16 10:42 09/02/16 19:20 113-120
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Client Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Lab Sample ID: 490-110980-5Client Sample ID: Vulcan Quarry-5
Matrix: SolidDate Collected: 08/31/16 14:40
Date Received: 09/01/16 09:20
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)76 10-120 09/02/16 10:42 09/02/16 19:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony ND 11.2 mg/Kg ☼09/06/16 14:16 09/07/16 03:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.23 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Arsenic ND
1.12 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Beryllium ND
1.12 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Cadmium ND
1.12 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Chromium 5.02
2.23 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Copper 11.7
1.12 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Lead 8.58
3.35 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Manganese 407
2.23 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Nickel 6.23
2.23 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Selenium ND
1.12 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Silver ND
2.23 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Thallium ND
11.2 mg/Kg 09/06/16 14:16 09/07/16 03:10 1☼Zinc 33.5
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.113 mg/Kg ☼09/06/16 10:01 09/06/16 18:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 5.48 mg/Kg ☼09/07/16 09:06 09/07/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 88.1 0.1 %09/03/16 08:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-368523/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
RL MDL
Acetone ND 0.0500 mg/Kg 09/08/16 15:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 09/08/16 15:38 1Benzene
ND 0.00200 mg/Kg 09/08/16 15:38 1Bromobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1Bromochloromethane
ND 0.00200 mg/Kg 09/08/16 15:38 1Bromodichloromethane
ND 0.00200 mg/Kg 09/08/16 15:38 1Bromoform
ND 0.00200 mg/Kg 09/08/16 15:38 1Bromomethane
ND 0.0500 mg/Kg 09/08/16 15:38 12-Butanone (MEK)
ND 0.00500 mg/Kg 09/08/16 15:38 1Carbon disulfide
ND 0.00200 mg/Kg 09/08/16 15:38 1Carbon tetrachloride
ND 0.00200 mg/Kg 09/08/16 15:38 1Chlorobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1Chlorodibromomethane
ND 0.00500 mg/Kg 09/08/16 15:38 1Chloroethane
ND 0.00200 mg/Kg 09/08/16 15:38 1Chloroform
ND 0.00200 mg/Kg 09/08/16 15:38 1Chloromethane
ND 0.00200 mg/Kg 09/08/16 15:38 12-Chlorotoluene
ND 0.00200 mg/Kg 09/08/16 15:38 14-Chlorotoluene
ND 0.00200 mg/Kg 09/08/16 15:38 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 09/08/16 15:38 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 09/08/16 15:38 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 09/08/16 15:38 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 09/08/16 15:38 1Dibromomethane
ND 0.00200 mg/Kg 09/08/16 15:38 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 09/08/16 15:38 11,1-Dichloroethane
ND 0.00200 mg/Kg 09/08/16 15:38 11,2-Dichloroethane
ND 0.00200 mg/Kg 09/08/16 15:38 11,1-Dichloroethene
ND 0.00200 mg/Kg 09/08/16 15:38 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 09/08/16 15:38 11,2-Dichloropropane
ND 0.00200 mg/Kg 09/08/16 15:38 11,3-Dichloropropane
ND 0.00200 mg/Kg 09/08/16 15:38 12,2-Dichloropropane
ND 0.00200 mg/Kg 09/08/16 15:38 11,1-Dichloropropene
ND 0.00200 mg/Kg 09/08/16 15:38 1Diisopropyl ether
ND 0.00200 mg/Kg 09/08/16 15:38 1Ethylbenzene
ND 0.00500 mg/Kg 09/08/16 15:38 1Hexachlorobutadiene
ND 0.0500 mg/Kg 09/08/16 15:38 12-Hexanone
ND 0.00200 mg/Kg 09/08/16 15:38 1Isopropylbenzene
ND 0.0100 mg/Kg 09/08/16 15:38 1Methylene Chloride
ND 0.0500 mg/Kg 09/08/16 15:38 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 09/08/16 15:38 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 09/08/16 15:38 1Naphthalene
ND 0.00200 mg/Kg 09/08/16 15:38 1n-Butylbenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1N-Propylbenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1p-Isopropyltoluene
ND 0.00200 mg/Kg 09/08/16 15:38 1sec-Butylbenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1Styrene
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-368523/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
RL MDL
tert-Butylbenzene ND 0.00200 mg/Kg 09/08/16 15:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 09/08/16 15:38 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 09/08/16 15:38 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 09/08/16 15:38 1Tetrachloroethene
ND 0.00200 mg/Kg 09/08/16 15:38 1Toluene
ND 0.00200 mg/Kg 09/08/16 15:38 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 09/08/16 15:38 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 09/08/16 15:38 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 09/08/16 15:38 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 09/08/16 15:38 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 09/08/16 15:38 1Trichloroethene
ND 0.00200 mg/Kg 09/08/16 15:38 1Trichlorofluoromethane
ND 0.00200 mg/Kg 09/08/16 15:38 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 09/08/16 15:38 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 09/08/16 15:38 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 09/08/16 15:38 1Vinyl chloride
ND 0.00600 mg/Kg 09/08/16 15:38 1Xylenes, Total
4-Bromofluorobenzene (Surr)102 70-130 09/08/16 15:38 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
110 09/08/16 15:38 1Dibromofluoromethane (Surr)70-130
110 09/08/16 15:38 11,2-Dichloroethane-d4 (Surr)70-130
103 09/08/16 15:38 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-368523/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
Acetone 0.250 0.2013 mg/Kg 81 45 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05173 mg/Kg 103 70 -130
Bromobenzene 0.0500 0.04961 mg/Kg 99 67 -130
Bromochloromethane 0.0500 0.05887 mg/Kg 118 70 -133
Bromodichloromethane 0.0500 0.04993 mg/Kg 100 70 -130
Bromoform 0.0500 0.05664 mg/Kg 113 59 -137
Bromomethane 0.0500 0.04113 mg/Kg 82 32 -150
2-Butanone (MEK)0.250 0.2230 mg/Kg 89 50 -149
Carbon disulfide 0.0500 0.05054 mg/Kg 101 66 -138
Carbon tetrachloride 0.0500 0.06224 mg/Kg 124 70 -131
Chlorobenzene 0.0500 0.05546 mg/Kg 111 70 -130
Chlorodibromomethane 0.0500 0.05702 mg/Kg 114 70 -130
Chloroethane 0.0500 0.04826 mg/Kg 97 37 -150
Chloroform 0.0500 0.05649 mg/Kg 113 70 -130
Chloromethane 0.0500 0.03172 mg/Kg 63 53 -150
2-Chlorotoluene 0.0500 0.05484 mg/Kg 110 70 -132
4-Chlorotoluene 0.0500 0.05595 mg/Kg 112 67 -135
cis-1,2-Dichloroethene 0.0500 0.05544 mg/Kg 111 70 -132
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-368523/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
cis-1,3-Dichloropropene 0.0500 0.05056 mg/Kg 101 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.04727 mg/Kg 95 47 -144
1,2-Dibromoethane (EDB)0.0500 0.05158 mg/Kg 103 69 -130
Dibromomethane 0.0500 0.05108 mg/Kg 102 70 -130
1,2-Dichlorobenzene 0.0500 0.05812 mg/Kg 116 70 -134
1,3-Dichlorobenzene 0.0500 0.05749 mg/Kg 115 69 -137
1,4-Dichlorobenzene 0.0500 0.05913 mg/Kg 118 66 -134
Dichlorodifluoromethane 0.0500 0.04592 mg/Kg 92 32 -150
1,1-Dichloroethane 0.0500 0.04958 mg/Kg 99 70 -130
1,2-Dichloroethane 0.0500 0.05799 mg/Kg 116 65 -134
1,1-Dichloroethene 0.0500 0.05232 mg/Kg 105 70 -131
1,2-Dichloroethene, Total 0.100 0.1080 mg/Kg 108 70 -130
1,2-Dichloropropane 0.0500 0.04809 mg/Kg 96 70 -130
1,3-Dichloropropane 0.0500 0.04895 mg/Kg 98 70 -130
2,2-Dichloropropane 0.0500 0.05784 mg/Kg 116 57 -150
1,1-Dichloropropene 0.0500 0.05372 mg/Kg 107 70 -130
Diisopropyl ether 0.0500 0.04804 mg/Kg 96 68 -134
Ethylbenzene 0.0500 0.05389 mg/Kg 108 70 -130
Hexachlorobutadiene 0.0500 0.05428 mg/Kg 109 64 -137
2-Hexanone 0.250 0.2048 mg/Kg 82 47 -148
Isopropylbenzene 0.0500 0.05598 mg/Kg 112 70 -130
Methylene Chloride 0.0500 0.05220 mg/Kg 104 69 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2126 mg/Kg 85 48 -150
Methyl tert-butyl ether 0.0500 0.05220 mg/Kg 104 54 -145
Naphthalene 0.0500 0.04970 mg/Kg 99 55 -149
n-Butylbenzene 0.0500 0.05504 mg/Kg 110 57 -150
N-Propylbenzene 0.0500 0.05570 mg/Kg 111 62 -150
p-Isopropyltoluene 0.0500 0.05727 mg/Kg 115 66 -147
sec-Butylbenzene 0.0500 0.05607 mg/Kg 112 68 -147
Styrene 0.0500 0.05446 mg/Kg 109 70 -131
tert-Butylbenzene 0.0500 0.05515 mg/Kg 110 70 -138
1,1,1,2-Tetrachloroethane 0.0500 0.05560 mg/Kg 111 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04729 mg/Kg 95 61 -134
Tetrachloroethene 0.0500 0.05928 mg/Kg 119 70 -130
Toluene 0.0500 0.05313 mg/Kg 106 70 -130
trans-1,2-Dichloroethene 0.0500 0.05254 mg/Kg 105 70 -130
trans-1,3-Dichloropropene 0.0500 0.05206 mg/Kg 104 67 -130
1,2,3-Trichlorobenzene 0.0500 0.05384 mg/Kg 108 57 -146
1,2,4-Trichlorobenzene 0.0500 0.05556 mg/Kg 111 47 -150
1,1,1-Trichloroethane 0.0500 0.05895 mg/Kg 118 70 -130
1,1,2-Trichloroethane 0.0500 0.05076 mg/Kg 102 70 -130
Trichloroethene 0.0500 0.05659 mg/Kg 113 70 -130
Trichlorofluoromethane 0.0500 0.05445 mg/Kg 109 53 -150
1,2,3-Trichloropropane 0.0500 0.05244 mg/Kg 105 60 -139
1,2,4-Trimethylbenzene 0.0500 0.05654 mg/Kg 113 70 -140
1,3,5-Trimethylbenzene 0.0500 0.05663 mg/Kg 113 69 -141
Vinyl chloride 0.0500 0.03808 mg/Kg 76 63 -150
Xylenes, Total 0.100 0.1060 mg/Kg 106 70 -130
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-368523/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
4-Bromofluorobenzene (Surr)70 -130
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
108Dibromofluoromethane (Surr)70 -130
1111,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-368523/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
Acetone 0.250 0.2232 mg/Kg 89 45 -145 10 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05216 mg/Kg 104 70 -130 1 37
Bromobenzene 0.0500 0.04990 mg/Kg 100 67 -130 1 40
Bromochloromethane 0.0500 0.06026 mg/Kg 121 70 -133 2 15
Bromodichloromethane 0.0500 0.05435 mg/Kg 109 70 -130 8 20
Bromoform 0.0500 0.05529 mg/Kg 111 59 -137 2 17
Bromomethane 0.0500 0.04445 mg/Kg 89 32 -150 8 45
2-Butanone (MEK)0.250 0.2188 mg/Kg 88 50 -149 2 39
Carbon disulfide 0.0500 0.05094 mg/Kg 102 66 -138 1 41
Carbon tetrachloride 0.0500 0.06360 mg/Kg 127 70 -131 2 41
Chlorobenzene 0.0500 0.05591 mg/Kg 112 70 -130 1 40
Chlorodibromomethane 0.0500 0.05437 mg/Kg 109 70 -130 5 14
Chloroethane 0.0500 0.04777 mg/Kg 96 37 -150 1 50
Chloroform 0.0500 0.05704 mg/Kg 114 70 -130 1 15
Chloromethane 0.0500 0.03690 mg/Kg 74 53 -150 15 47
2-Chlorotoluene 0.0500 0.05471 mg/Kg 109 70 -132 0 41
4-Chlorotoluene 0.0500 0.05424 mg/Kg 108 67 -135 3 41
cis-1,2-Dichloroethene 0.0500 0.05438 mg/Kg 109 70 -132 2 18
cis-1,3-Dichloropropene 0.0500 0.05053 mg/Kg 101 70 -130 0 42
1,2-Dibromo-3-Chloropropane 0.0500 0.04970 mg/Kg 99 47 -144 5 38
1,2-Dibromoethane (EDB)0.0500 0.05227 mg/Kg 105 69 -130 1 17
Dibromomethane 0.0500 0.05580 mg/Kg 112 70 -130 9 19
1,2-Dichlorobenzene 0.0500 0.05795 mg/Kg 116 70 -134 0 40
1,3-Dichlorobenzene 0.0500 0.05868 mg/Kg 117 69 -137 2 41
1,4-Dichlorobenzene 0.0500 0.05858 mg/Kg 117 66 -134 1 41
Dichlorodifluoromethane 0.0500 0.05049 mg/Kg 101 32 -150 9 50
1,1-Dichloroethane 0.0500 0.05000 mg/Kg 100 70 -130 1 42
1,2-Dichloroethane 0.0500 0.05691 mg/Kg 114 65 -134 2 16
1,1-Dichloroethene 0.0500 0.05379 mg/Kg 108 70 -131 3 43
1,2-Dichloroethene, Total 0.100 0.1064 mg/Kg 106 70 -130 2 41
1,2-Dichloropropane 0.0500 0.04932 mg/Kg 99 70 -130 3 15
1,3-Dichloropropane 0.0500 0.04869 mg/Kg 97 70 -130 1 15
2,2-Dichloropropane 0.0500 0.05677 mg/Kg 114 57 -150 2 42
1,1-Dichloropropene 0.0500 0.05274 mg/Kg 105 70 -130 2 41
Diisopropyl ether 0.0500 0.04587 mg/Kg 92 68 -134 5 36
Ethylbenzene 0.0500 0.05407 mg/Kg 108 70 -130 0 38
Hexachlorobutadiene 0.0500 0.05427 mg/Kg 109 64 -137 0 44
2-Hexanone 0.250 0.2057 mg/Kg 82 47 -148 0 38
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-368523/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368523
Isopropylbenzene 0.0500 0.05586 mg/Kg 112 70 -130 0 39
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.05191 mg/Kg 104 69 -130 1 19
4-Methyl-2-pentanone (MIBK)0.250 0.2148 mg/Kg 86 48 -150 1 41
Methyl tert-butyl ether 0.0500 0.05172 mg/Kg 103 54 -145 1 36
Naphthalene 0.0500 0.04954 mg/Kg 99 55 -149 0 37
n-Butylbenzene 0.0500 0.05496 mg/Kg 110 57 -150 0 39
N-Propylbenzene 0.0500 0.05409 mg/Kg 108 62 -150 3 38
p-Isopropyltoluene 0.0500 0.05688 mg/Kg 114 66 -147 1 38
sec-Butylbenzene 0.0500 0.05632 mg/Kg 113 68 -147 0 38
Styrene 0.0500 0.05409 mg/Kg 108 70 -131 1 40
tert-Butylbenzene 0.0500 0.05605 mg/Kg 112 70 -138 2 38
1,1,1,2-Tetrachloroethane 0.0500 0.05731 mg/Kg 115 70 -130 3 41
1,1,2,2-Tetrachloroethane 0.0500 0.04727 mg/Kg 95 61 -134 0 16
Tetrachloroethene 0.0500 0.05771 mg/Kg 115 70 -130 3 41
Toluene 0.0500 0.05380 mg/Kg 108 70 -130 1 40
trans-1,2-Dichloroethene 0.0500 0.05198 mg/Kg 104 70 -130 1 41
trans-1,3-Dichloropropene 0.0500 0.05261 mg/Kg 105 67 -130 1 41
1,2,3-Trichlorobenzene 0.0500 0.05370 mg/Kg 107 57 -146 0 42
1,2,4-Trichlorobenzene 0.0500 0.05420 mg/Kg 108 47 -150 2 43
1,1,1-Trichloroethane 0.0500 0.06128 mg/Kg 123 70 -130 4 41
1,1,2-Trichloroethane 0.0500 0.05010 mg/Kg 100 70 -130 1 17
Trichloroethene 0.0500 0.05976 mg/Kg 120 70 -130 5 41
Trichlorofluoromethane 0.0500 0.05569 mg/Kg 111 53 -150 2 49
1,2,3-Trichloropropane 0.0500 0.05267 mg/Kg 105 60 -139 0 16
1,2,4-Trimethylbenzene 0.0500 0.05657 mg/Kg 113 70 -140 0 38
1,3,5-Trimethylbenzene 0.0500 0.05511 mg/Kg 110 69 -141 3 38
Vinyl chloride 0.0500 0.04171 mg/Kg 83 63 -150 9 46
Xylenes, Total 0.100 0.1081 mg/Kg 108 70 -130 2 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
94
LCSD LCSD
Qualifier Limits%Recovery
109Dibromofluoromethane (Surr)70 -130
1071,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-367460/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
RL MDL
Acenaphthene ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Acenaphthylene
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Anthracene
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Benzo[a]anthracene
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Benzo[a]pyrene
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Benzo[b]fluoranthene
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-367460/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
RL MDL
Benzo[g,h,i]perylene ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Benzo[k]fluoranthene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Bis(2-chloroethoxy)methane
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Bis(2-chloroethyl)ether
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1bis (2-chloroisopropyl) ether
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Bis(2-ethylhexyl) phthalate
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 14-Bromophenyl phenyl ether
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Butyl benzyl phthalate
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Carbazole
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 14-Chloroaniline
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 14-Chloro-3-methylphenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12-Chloronaphthalene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12-Chlorophenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 14-Chlorophenyl phenyl ether
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Chrysene
ND 0.666 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Cresols
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Dibenz(a,h)anthracene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Dibenzofuran
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 11,2-Dichlorobenzene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 11,3-Dichlorobenzene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 11,4-Dichlorobenzene
ND 0.670 mg/Kg 09/02/16 10:42 09/02/16 17:22 13,3'-Dichlorobenzidine
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,4-Dichlorophenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Diethyl phthalate
ND 0.670 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,4-Dimethylphenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Dimethyl phthalate
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Di-n-butyl phthalate
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 14,6-Dinitro-2-methylphenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,4-Dinitrophenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,4-Dinitrotoluene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,6-Dinitrotoluene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Di-n-octyl phthalate
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Fluoranthene
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Fluorene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Hexachlorobenzene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Hexachlorobutadiene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Hexachlorocyclopentadiene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Hexachloroethane
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Indeno[1,2,3-cd]pyrene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Isophorone
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 11-Methylnaphthalene
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 12-Methylnaphthalene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12-Methylphenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 13 & 4 Methylphenol
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Naphthalene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12-Nitroaniline
ND 0.670 mg/Kg 09/02/16 10:42 09/02/16 17:22 13-Nitroaniline
ND 0.670 mg/Kg 09/02/16 10:42 09/02/16 17:22 14-Nitroaniline
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-367460/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
RL MDL
Nitrobenzene ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12-Nitrophenol
ND 0.670 mg/Kg 09/02/16 10:42 09/02/16 17:22 14-Nitrophenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1N-Nitrosodi-n-propylamine
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Pentachlorophenol
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Phenanthrene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Phenol
ND 0.0670 mg/Kg 09/02/16 10:42 09/02/16 17:22 1Pyrene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 11,2,4-Trichlorobenzene
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,4,5-Trichlorophenol
ND 0.333 mg/Kg 09/02/16 10:42 09/02/16 17:22 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)44 29-120 09/02/16 17:22 1
MB MB
Surrogate
09/02/16 10:42
Dil FacPreparedAnalyzedQualifierLimits%Recovery
51 09/02/16 10:42 09/02/16 17:22 12-Fluorophenol (Surr)10-120
51 09/02/16 10:42 09/02/16 17:22 1Nitrobenzene-d5 (Surr)27-120
54 09/02/16 10:42 09/02/16 17:22 1Phenol-d5 (Surr)10-120
60 09/02/16 10:42 09/02/16 17:22 1Terphenyl-d14 (Surr)13-120
55 09/02/16 10:42 09/02/16 17:22 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-367460/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Acenaphthene 1.67 1.412 mg/Kg 85 36 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.448 mg/Kg 87 38 -120
Anthracene 1.67 1.499 mg/Kg 90 46 -124
Benzo[a]anthracene 1.67 1.559 mg/Kg 94 45 -120
Benzo[a]pyrene 1.67 1.537 mg/Kg 92 45 -120
Benzo[b]fluoranthene 1.67 1.608 mg/Kg 97 42 -120
Benzo[g,h,i]perylene 1.67 1.643 mg/Kg 99 38 -120
Benzo[k]fluoranthene 1.67 1.472 mg/Kg 88 42 -120
Bis(2-chloroethoxy)methane 1.67 1.330 mg/Kg 80 32 -120
Bis(2-chloroethyl)ether 1.67 1.233 mg/Kg 74 31 -120
bis (2-chloroisopropyl) ether 1.67 1.337 mg/Kg 80 32 -120
Bis(2-ethylhexyl) phthalate 1.67 1.590 mg/Kg 95 43 -120
4-Bromophenyl phenyl ether 1.67 1.501 mg/Kg 90 40 -120
Butyl benzyl phthalate 1.67 1.640 mg/Kg 98 43 -133
Carbazole 1.67 1.542 mg/Kg 93 44 -120
4-Chloroaniline 1.67 1.362 mg/Kg 82 35 -120
4-Chloro-3-methylphenol 1.67 1.606 mg/Kg 96 38 -120
2-Chloronaphthalene 1.67 1.330 mg/Kg 80 34 -120
2-Chlorophenol 1.67 1.290 mg/Kg 77 32 -120
4-Chlorophenyl phenyl ether 1.67 1.457 mg/Kg 87 42 -120
Chrysene 1.67 1.551 mg/Kg 93 43 -120
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-367460/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Cresols 3.33 2.837 mg/Kg 85 36 -129
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dibenz(a,h)anthracene 1.67 1.605 mg/Kg 96 32 -128
Dibenzofuran 1.67 1.388 mg/Kg 83 41 -120
1,2-Dichlorobenzene 1.67 1.199 mg/Kg 72 33 -120
1,3-Dichlorobenzene 1.67 1.154 mg/Kg 69 32 -120
1,4-Dichlorobenzene 1.67 1.152 mg/Kg 69 32 -120
3,3'-Dichlorobenzidine 1.67 1.372 mg/Kg 82 39 -120
2,4-Dichlorophenol 1.67 1.456 mg/Kg 87 32 -120
Diethyl phthalate 1.67 1.517 mg/Kg 91 41 -122
2,4-Dimethylphenol 1.67 1.377 mg/Kg 83 32 -120
Dimethyl phthalate 1.67 1.491 mg/Kg 89 55 -120
Di-n-butyl phthalate 1.67 1.517 mg/Kg 91 46 -127
4,6-Dinitro-2-methylphenol 3.33 1.698 mg/Kg 51 27 -134
2,4-Dinitrophenol 3.33 1.361 mg/Kg 41 10 -142
2,4-Dinitrotoluene 1.67 1.442 mg/Kg 87 43 -120
2,6-Dinitrotoluene 1.67 1.591 mg/Kg 95 43 -120
Di-n-octyl phthalate 1.67 1.651 mg/Kg 99 40 -130
Fluoranthene 1.67 1.532 mg/Kg 92 46 -120
Fluorene 1.67 1.438 mg/Kg 86 42 -120
Hexachlorobenzene 1.67 1.549 mg/Kg 93 44 -120
Hexachlorobutadiene 1.67 1.244 mg/Kg 75 31 -120
Hexachlorocyclopentadiene 1.67 0.9423 mg/Kg 57 24 -120
Hexachloroethane 1.67 1.235 mg/Kg 74 33 -120
Indeno[1,2,3-cd]pyrene 1.67 1.542 mg/Kg 93 41 -121
Isophorone 1.67 1.374 mg/Kg 82 33 -120
1-Methylnaphthalene 1.67 1.299 mg/Kg 78 32 -120
2-Methylnaphthalene 1.67 1.288 mg/Kg 77 28 -120
2-Methylphenol 1.67 1.416 mg/Kg 85 36 -120
3 & 4 Methylphenol 1.67 1.421 mg/Kg 85 37 -120
Naphthalene 1.67 1.251 mg/Kg 75 32 -120
2-Nitroaniline 1.67 1.561 mg/Kg 94 40 -120
3-Nitroaniline 1.67 1.471 mg/Kg 88 42 -120
4-Nitroaniline 1.67 1.460 mg/Kg 88 43 -120
Nitrobenzene 1.67 1.318 mg/Kg 79 26 -120
2-Nitrophenol 1.67 1.342 mg/Kg 81 29 -120
4-Nitrophenol 3.33 3.034 mg/Kg 91 32 -136
N-Nitrosodi-n-propylamine 1.67 1.421 mg/Kg 85 35 -120
Pentachlorophenol 3.33 2.834 mg/Kg 85 44 -134
Phenanthrene 1.67 1.481 mg/Kg 89 45 -120
Phenol 1.67 1.369 mg/Kg 82 30 -120
Pyrene 1.67 1.645 mg/Kg 99 43 -120
1,2,4-Trichlorobenzene 1.67 1.224 mg/Kg 73 29 -120
2,4,5-Trichlorophenol 1.67 1.580 mg/Kg 95 39 -120
2,4,6-Trichlorophenol 1.67 1.616 mg/Kg 97 39 -120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
75
LCS LCS
Qualifier Limits%Recovery
732-Fluorophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-367460/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Nitrobenzene-d5 (Surr)27 -120
Surrogate
80
LCS LCS
Qualifier Limits%Recovery
81Phenol-d5 (Surr)10 -120
97Terphenyl-d14 (Surr)13 -120
922,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Vulcan Quarry-5Lab Sample ID: 490-110980-5 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Acenaphthene ND 1.84 1.232 mg/Kg 67 19 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene ND 1.84 1.251 mg/Kg 68 25 -120☼
Anthracene ND 1.84 1.298 mg/Kg 71 28 -125☼
Benzo[a]anthracene ND 1.84 1.371 mg/Kg 75 23 -120☼
Benzo[a]pyrene ND 1.84 1.335 mg/Kg 73 15 -128☼
Benzo[b]fluoranthene ND 1.84 1.486 mg/Kg 81 12 -133☼
Benzo[g,h,i]perylene ND 1.84 1.485 mg/Kg 81 22 -120☼
Benzo[k]fluoranthene ND 1.84 1.314 mg/Kg 71 28 -120☼
Bis(2-chloroethoxy)methane ND 1.84 1.172 mg/Kg 64 24 -120☼
Bis(2-chloroethyl)ether ND 1.84 1.132 mg/Kg 62 22 -120☼
bis (2-chloroisopropyl) ether ND 1.84 1.213 mg/Kg 66 20 -120☼
Bis(2-ethylhexyl) phthalate ND 1.84 1.355 mg/Kg 74 26 -120☼
4-Bromophenyl phenyl ether ND 1.84 1.317 mg/Kg 72 31 -120☼
Butyl benzyl phthalate ND 1.84 1.457 mg/Kg 79 24 -133☼
Carbazole ND 1.84 1.312 mg/Kg 71 25 -123☼
4-Chloroaniline ND 1.84 1.203 mg/Kg 65 26 -120☼
4-Chloro-3-methylphenol ND 1.84 1.371 mg/Kg 75 21 -120☼
2-Chloronaphthalene ND 1.84 1.204 mg/Kg 66 24 -120☼
2-Chlorophenol ND 1.84 1.179 mg/Kg 64 25 -120☼
4-Chlorophenyl phenyl ether ND 1.84 1.275 mg/Kg 69 26 -120☼
Chrysene ND 1.84 1.345 mg/Kg 73 20 -120☼
Cresols ND 3.67 2.458 mg/Kg 67 10 -200☼
Dibenz(a,h)anthracene ND 1.84 1.387 mg/Kg 75 12 -128☼
Dibenzofuran ND 1.84 1.214 mg/Kg 66 21 -120☼
1,2-Dichlorobenzene ND 1.84 1.109 mg/Kg 60 10 -120☼
1,3-Dichlorobenzene ND 1.84 1.097 mg/Kg 60 10 -120☼
1,4-Dichlorobenzene ND 1.84 1.067 mg/Kg 58 10 -120☼
3,3'-Dichlorobenzidine ND 1.84 1.171 mg/Kg 64 10 -120☼
2,4-Dichlorophenol ND 1.84 1.280 mg/Kg 70 17 -120☼
Diethyl phthalate ND 1.84 1.303 mg/Kg 71 29 -122☼
2,4-Dimethylphenol ND 1.84 1.251 mg/Kg 68 17 -120☼
Dimethyl phthalate ND 1.84 1.323 mg/Kg 72 30 -120☼
Di-n-butyl phthalate ND 1.84 1.342 mg/Kg 73 29 -126☼
4,6-Dinitro-2-methylphenol ND 3.67 1.585 mg/Kg 43 10 -134☼
2,4-Dinitrophenol ND 3.67 1.460 mg/Kg 40 10 -150☼
2,4-Dinitrotoluene ND 1.84 1.273 mg/Kg 69 24 -121☼
2,6-Dinitrotoluene ND 1.84 1.374 mg/Kg 75 24 -120☼
Di-n-octyl phthalate ND 1.84 1.419 mg/Kg 77 27 -130☼
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Vulcan Quarry-5Lab Sample ID: 490-110980-5 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Fluoranthene ND 1.84 1.347 mg/Kg 73 10 -143☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Fluorene ND 1.84 1.293 mg/Kg 70 20 -120☼
Hexachlorobenzene ND 1.84 1.327 mg/Kg 72 25 -120☼
Hexachlorobutadiene ND 1.84 1.144 mg/Kg 62 10 -120☼
Hexachlorocyclopentadiene ND 1.84 0.8182 mg/Kg 45 10 -120☼
Hexachloroethane ND 1.84 1.151 mg/Kg 63 10 -120☼
Indeno[1,2,3-cd]pyrene ND 1.84 1.374 mg/Kg 75 22 -121☼
Isophorone ND 1.84 1.222 mg/Kg 66 24 -120☼
1-Methylnaphthalene ND 1.84 1.162 mg/Kg 63 10 -120☼
2-Methylnaphthalene ND 1.84 1.157 mg/Kg 63 13 -120☼
2-Methylphenol ND 1.84 1.230 mg/Kg 67 23 -120☼
3 & 4 Methylphenol ND 1.84 1.228 mg/Kg 67 19 -120☼
Naphthalene ND 1.84 1.141 mg/Kg 62 10 -120☼
2-Nitroaniline ND 1.84 1.330 mg/Kg 72 31 -120☼
3-Nitroaniline ND 1.84 1.287 mg/Kg 70 31 -120☼
4-Nitroaniline ND 1.84 1.178 mg/Kg 64 28 -120☼
Nitrobenzene ND 1.84 1.257 mg/Kg 68 19 -120☼
2-Nitrophenol ND 1.84 1.236 mg/Kg 67 23 -120☼
4-Nitrophenol ND 3.67 2.727 mg/Kg 74 16 -139☼
N-Nitrosodi-n-propylamine ND 1.84 1.296 mg/Kg 55 24 -120☼
Pentachlorophenol ND 3.67 2.762 mg/Kg 75 19 -145☼
Phenanthrene ND 1.84 1.284 mg/Kg 70 21 -122☼
Phenol ND 1.84 1.215 mg/Kg 66 15 -120☼
Pyrene ND 1.84 1.415 mg/Kg 77 20 -123☼
1,2,4-Trichlorobenzene ND 1.84 1.133 mg/Kg 62 14 -120☼
2,4,5-Trichlorophenol ND 1.84 1.367 mg/Kg 74 27 -120☼
2,4,6-Trichlorophenol ND 1.84 1.423 mg/Kg 77 24 -122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
62
MS MS
Qualifier Limits%Recovery
632-Fluorophenol (Surr)10 -120
67Nitrobenzene-d5 (Surr)27 -120
65Phenol-d5 (Surr)10 -120
79Terphenyl-d14 (Surr)13 -120
772,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Vulcan Quarry-5Lab Sample ID: 490-110980-5 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Acenaphthene ND 1.85 1.206 mg/Kg 65 19 -120 2 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene ND 1.85 1.255 mg/Kg 68 25 -120 0 50☼
Anthracene ND 1.85 1.296 mg/Kg 70 28 -125 0 49☼
Benzo[a]anthracene ND 1.85 1.298 mg/Kg 70 23 -120 5 50☼
Benzo[a]pyrene ND 1.85 1.306 mg/Kg 70 15 -128 2 50☼
Benzo[b]fluoranthene ND 1.85 1.408 mg/Kg 76 12 -133 5 50☼
Benzo[g,h,i]perylene ND 1.85 1.379 mg/Kg 74 22 -120 7 50☼
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Vulcan Quarry-5Lab Sample ID: 490-110980-5 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
Benzo[k]fluoranthene ND 1.85 1.256 mg/Kg 68 28 -120 4 45☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bis(2-chloroethoxy)methane ND 1.85 1.209 mg/Kg 65 24 -120 3 50☼
Bis(2-chloroethyl)ether ND 1.85 1.169 mg/Kg 63 22 -120 3 50☼
bis (2-chloroisopropyl) ether ND 1.85 1.240 mg/Kg 67 20 -120 2 50☼
Bis(2-ethylhexyl) phthalate ND 1.85 1.306 mg/Kg 70 26 -120 4 50☼
4-Bromophenyl phenyl ether ND 1.85 1.301 mg/Kg 70 31 -120 1 37☼
Butyl benzyl phthalate ND 1.85 1.412 mg/Kg 76 24 -133 3 50☼
Carbazole ND 1.85 1.326 mg/Kg 72 25 -123 1 46☼
4-Chloroaniline ND 1.85 1.255 mg/Kg 68 26 -120 4 50☼
4-Chloro-3-methylphenol ND 1.85 1.352 mg/Kg 73 21 -120 1 49☼
2-Chloronaphthalene ND 1.85 1.214 mg/Kg 66 24 -120 1 50☼
2-Chlorophenol ND 1.85 1.246 mg/Kg 67 25 -120 5 50☼
4-Chlorophenyl phenyl ether ND 1.85 1.266 mg/Kg 68 26 -120 1 50☼
Chrysene ND 1.85 1.280 mg/Kg 69 20 -120 5 49☼
Cresols ND 3.71 2.488 mg/Kg 67 10 -200 1 50☼
Dibenz(a,h)anthracene ND 1.85 1.347 mg/Kg 73 12 -128 3 50☼
Dibenzofuran ND 1.85 1.228 mg/Kg 66 21 -120 1 50☼
1,2-Dichlorobenzene ND 1.85 1.140 mg/Kg 61 10 -120 3 50☼
1,3-Dichlorobenzene ND 1.85 1.066 mg/Kg 58 10 -120 3 50☼
1,4-Dichlorobenzene ND 1.85 1.091 mg/Kg 59 10 -120 2 50☼
3,3'-Dichlorobenzidine ND 1.85 1.175 mg/Kg 63 10 -120 0 50☼
2,4-Dichlorophenol ND 1.85 1.296 mg/Kg 70 17 -120 1 50☼
Diethyl phthalate ND 1.85 1.337 mg/Kg 72 29 -122 3 45☼
2,4-Dimethylphenol ND 1.85 1.234 mg/Kg 67 17 -120 1 50☼
Dimethyl phthalate ND 1.85 1.310 mg/Kg 71 30 -120 1 46☼
Di-n-butyl phthalate ND 1.85 1.327 mg/Kg 72 29 -126 1 49☼
4,6-Dinitro-2-methylphenol ND 3.71 1.639 mg/Kg 44 10 -134 3 50☼
2,4-Dinitrophenol ND 3.71 1.515 mg/Kg 41 10 -150 4 50☼
2,4-Dinitrotoluene ND 1.85 1.301 mg/Kg 70 24 -121 2 50☼
2,6-Dinitrotoluene ND 1.85 1.448 mg/Kg 78 24 -120 5 50☼
Di-n-octyl phthalate ND 1.85 1.313 mg/Kg 71 27 -130 8 50☼
Fluoranthene ND 1.85 1.328 mg/Kg 72 10 -143 1 50☼
Fluorene ND 1.85 1.249 mg/Kg 67 20 -120 3 50☼
Hexachlorobenzene ND 1.85 1.311 mg/Kg 71 25 -120 1 50☼
Hexachlorobutadiene ND 1.85 1.165 mg/Kg 63 10 -120 2 50☼
Hexachlorocyclopentadiene ND 1.85 0.8705 mg/Kg 47 10 -120 6 50☼
Hexachloroethane ND 1.85 1.174 mg/Kg 63 10 -120 2 50☼
Indeno[1,2,3-cd]pyrene ND 1.85 1.313 mg/Kg 71 22 -121 5 50☼
Isophorone ND 1.85 1.223 mg/Kg 66 24 -120 0 50☼
1-Methylnaphthalene ND 1.85 1.162 mg/Kg 63 10 -120 0 50☼
2-Methylnaphthalene ND 1.85 1.166 mg/Kg 63 13 -120 1 50☼
2-Methylphenol ND 1.85 1.258 mg/Kg 68 23 -120 2 50☼
3 & 4 Methylphenol ND 1.85 1.230 mg/Kg 66 19 -120 0 50☼
Naphthalene ND 1.85 1.151 mg/Kg 62 10 -120 1 50☼
2-Nitroaniline ND 1.85 1.422 mg/Kg 77 31 -120 7 50☼
3-Nitroaniline ND 1.85 1.259 mg/Kg 68 31 -120 2 49☼
4-Nitroaniline ND 1.85 1.210 mg/Kg 65 28 -120 3 49☼
Nitrobenzene ND 1.85 1.237 mg/Kg 67 19 -120 2 50☼
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Vulcan Quarry-5Lab Sample ID: 490-110980-5 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367446 Prep Batch: 367460
2-Nitrophenol ND 1.85 1.256 mg/Kg 68 23 -120 2 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Nitrophenol ND 3.71 2.779 mg/Kg 75 16 -139 2 45☼
N-Nitrosodi-n-propylamine ND 1.85 1.243 mg/Kg 51 24 -120 4 50☼
Pentachlorophenol ND 3.71 2.734 mg/Kg 74 19 -145 1 50☼
Phenanthrene ND 1.85 1.288 mg/Kg 70 21 -122 0 50☼
Phenol ND 1.85 1.234 mg/Kg 67 15 -120 2 50☼
Pyrene ND 1.85 1.351 mg/Kg 73 20 -123 5 50☼
1,2,4-Trichlorobenzene ND 1.85 1.130 mg/Kg 61 14 -120 0 50☼
2,4,5-Trichlorophenol ND 1.85 1.464 mg/Kg 79 27 -120 7 50☼
2,4,6-Trichlorophenol ND 1.85 1.452 mg/Kg 78 24 -122 2 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
61
MSD MSD
Qualifier Limits%Recovery
592-Fluorophenol (Surr)10 -120
65Nitrobenzene-d5 (Surr)27 -120
65Phenol-d5 (Surr)10 -120
73Terphenyl-d14 (Surr)13 -120
762,4,6-Tribromophenol (Surr)10 -120
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-368059/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368191 Prep Batch: 368059
RL MDL
Antimony ND 9.84 mg/Kg 09/06/16 14:16 09/07/16 01:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.97 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Arsenic
ND 0.984 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Beryllium
ND 0.984 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Cadmium
ND 0.984 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Chromium
ND 1.97 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Copper
ND 0.984 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Lead
ND 2.95 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Manganese
ND 1.97 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Nickel
ND 1.97 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Selenium
ND 0.984 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Silver
ND 1.97 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Thallium
ND 9.84 mg/Kg 09/06/16 14:16 09/07/16 01:54 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-368059/16-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368191 Prep Batch: 368059
Silver 19.6 16.39 mg/Kg 84 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-368059/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368191 Prep Batch: 368059
Antimony 39.8 36.66 mg/Kg 92 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 19.9 17.32 mg/Kg 87 80 -120
Beryllium 19.9 18.59 mg/Kg 93 80 -120
Cadmium 19.9 18.27 mg/Kg 92 80 -120
Chromium 79.5 73.56 mg/Kg 92 80 -120
Copper 99.4 88.09 mg/Kg 89 80 -120
Lead 19.9 19.22 mg/Kg 97 80 -120
Manganese 199 192.4 mg/Kg 97 80 -120
Nickel 199 185.0 mg/Kg 93 80 -120
Selenium 19.9 17.34 mg/Kg 87 80 -120
Thallium 119 110.3 mg/Kg 92 80 -120
Zinc 199 177.7 mg/Kg 89 80 -120
Client Sample ID: Vulcan Quarry-1Lab Sample ID: 490-110980-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368191 Prep Batch: 368059
Antimony ND 54.0 45.43 mg/Kg 84 75 -125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic ND 27.0 22.60 mg/Kg 84 75 -125☼
Beryllium ND 27.0 24.23 mg/Kg 90 75 -125☼
Cadmium ND 27.0 23.41 mg/Kg 87 75 -125☼
Chromium 15.8 108 107.8 mg/Kg 85 75 -125☼
Copper 5.83 135 119.2 mg/Kg 84 75 -125☼
Lead 20.4 F1 27.0 39.40 F1 mg/Kg 70 75 -125☼
Manganese 152 F2 F1 270 349.7 F1 mg/Kg 73 75 -125☼
Nickel 10.5 270 242.1 mg/Kg 86 75 -125☼
Selenium ND 27.0 22.63 mg/Kg 84 75 -125☼
Silver ND F1 27.0 13.94 F1 mg/Kg 52 75 -125☼
Thallium ND 162 136.5 mg/Kg 84 75 -125☼
Zinc 14.8 270 240.5 mg/Kg 84 75 -125☼
Client Sample ID: Vulcan Quarry-1Lab Sample ID: 490-110980-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368191 Prep Batch: 368059
Antimony ND 54.8 46.60 mg/Kg 85 75 -125 3 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic ND 27.4 22.97 mg/Kg 84 75 -125 2 20☼
Beryllium ND 27.4 25.02 mg/Kg 91 75 -125 3 20☼
Cadmium ND 27.4 23.98 mg/Kg 88 75 -125 2 20☼
Chromium 15.8 110 121.2 mg/Kg 96 75 -125 12 20☼
Copper 5.83 137 123.3 mg/Kg 86 75 -125 3 20☼
Lead 20.4 F1 27.4 47.69 mg/Kg 100 75 -125 19 20☼
Manganese 152 F2 F1 274 450.4 F2 mg/Kg 109 75 -125 25 20☼
Nickel 10.5 274 251.5 mg/Kg 88 75 -125 4 20☼
Selenium ND 27.4 23.68 mg/Kg 86 75 -125 5 20☼
Silver ND F1 27.4 14.15 F1 mg/Kg 52 75 -125 2 20☼
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Vulcan Quarry-1Lab Sample ID: 490-110980-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368191 Prep Batch: 368059
Thallium ND 164 139.1 mg/Kg 85 75 -125 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Zinc 14.8 274 253.4 mg/Kg 87 75 -125 5 20☼
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-367943/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368369 Prep Batch: 367943
RL MDL
Mercury ND 0.100 mg/Kg 09/06/16 10:01 09/06/16 17:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-367943/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368369 Prep Batch: 367943
Mercury 0.163 0.1552 mg/Kg 95 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-110375-G-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368369 Prep Batch: 367943
Mercury ND 0.170 0.1409 mg/Kg 83 80 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-110375-G-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368369 Prep Batch: 367943
Mercury ND 0.175 0.1448 mg/Kg 83 80 -120 3 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 490-368183/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
RL MDL
Chromium, hex ND 4.98 mg/Kg 09/07/16 09:06 09/07/16 16:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 490-368183/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
Chromium, hex 64.7 60.91 mg/Kg 94 80 -120
Analyte
LCSI LCSI
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method: 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 490-368183/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
Chromium, hex 39.2 40.95 mg/Kg 105 80 -120
Analyte
LCSS LCSS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSSD 490-368183/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
Chromium, hex 39.1 40.87 mg/Kg 105 80 -120 0 20
Analyte
LCSSD LCSSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 280-87113-G-1-D MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
Chromium, hex ND 44.9 40.45 mg/Kg 90 75 -125☼
Analyte
MSS MSS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 280-87113-G-1-E MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
Chromium, hex ND 73.3 62.70 mg/Kg 85 75 -125☼
Analyte
MSI MSI
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: DuplicateLab Sample ID: 280-87113-G-1-C DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 368433 Prep Batch: 368183
Chromium, hex ND ND mg/Kg NC 20☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: Moisture - Percent Moisture
Client Sample ID: Vulcan Quarry-1Lab Sample ID: 490-110980-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 367666
Percent Solids 71.9 71.6 %0.5 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
GC/MS VOA
Prep Batch: 367546
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-110980-1 Vulcan Quarry-1 Total/NA
Solid 5035490-110980-2 Vulcan Quarry-2 Total/NA
Solid 5035490-110980-3 Vulcan Quarry-3 Total/NA
Solid 5035490-110980-4 Vulcan Quarry-4 Total/NA
Solid 5035490-110980-5 Vulcan Quarry-5 Total/NA
Analysis Batch: 368523
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 367546490-110980-1 Vulcan Quarry-1 Total/NA
Solid 8260B 367546490-110980-2 Vulcan Quarry-2 Total/NA
Solid 8260B 367546490-110980-3 Vulcan Quarry-3 Total/NA
Solid 8260B 367546490-110980-4 Vulcan Quarry-4 Total/NA
Solid 8260B 367546490-110980-5 Vulcan Quarry-5 Total/NA
Solid 8260BMB 490-368523/9 Method Blank Total/NA
Solid 8260BLCS 490-368523/3 Lab Control Sample Total/NA
Solid 8260BLCSD 490-368523/4 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Analysis Batch: 367446
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 367460490-110980-1 Vulcan Quarry-1 Total/NA
Solid 8270D 367460490-110980-2 Vulcan Quarry-2 Total/NA
Solid 8270D 367460490-110980-3 Vulcan Quarry-3 Total/NA
Solid 8270D 367460490-110980-4 Vulcan Quarry-4 Total/NA
Solid 8270D 367460490-110980-5 Vulcan Quarry-5 Total/NA
Solid 8270D 367460MB 490-367460/1-A Method Blank Total/NA
Solid 8270D 367460LCS 490-367460/2-A Lab Control Sample Total/NA
Solid 8270D 367460490-110980-5 MS Vulcan Quarry-5 Total/NA
Solid 8270D 367460490-110980-5 MSD Vulcan Quarry-5 Total/NA
Prep Batch: 367460
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-110980-1 Vulcan Quarry-1 Total/NA
Solid 3550C490-110980-2 Vulcan Quarry-2 Total/NA
Solid 3550C490-110980-3 Vulcan Quarry-3 Total/NA
Solid 3550C490-110980-4 Vulcan Quarry-4 Total/NA
Solid 3550C490-110980-5 Vulcan Quarry-5 Total/NA
Solid 3550CMB 490-367460/1-A Method Blank Total/NA
Solid 3550CLCS 490-367460/2-A Lab Control Sample Total/NA
Solid 3550C490-110980-5 MS Vulcan Quarry-5 Total/NA
Solid 3550C490-110980-5 MSD Vulcan Quarry-5 Total/NA
Metals
Prep Batch: 367943
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-110980-1 Vulcan Quarry-1 Total/NA
Solid 7471B490-110980-2 Vulcan Quarry-2 Total/NA
Solid 7471B490-110980-3 Vulcan Quarry-3 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Metals (Continued)
Prep Batch: 367943 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-110980-4 Vulcan Quarry-4 Total/NA
Solid 7471B490-110980-5 Vulcan Quarry-5 Total/NA
Solid 7471BMB 490-367943/1-A Method Blank Total/NA
Solid 7471BLCS 490-367943/2-A Lab Control Sample Total/NA
Solid 7471B490-110375-G-1-B MS Matrix Spike Total/NA
Solid 7471B490-110375-G-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 368059
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-110980-1 Vulcan Quarry-1 Total/NA
Solid 3051A490-110980-2 Vulcan Quarry-2 Total/NA
Solid 3051A490-110980-3 Vulcan Quarry-3 Total/NA
Solid 3051A490-110980-4 Vulcan Quarry-4 Total/NA
Solid 3051A490-110980-5 Vulcan Quarry-5 Total/NA
Solid 3051AMB 490-368059/1-A Method Blank Total/NA
Solid 3051ALCS 490-368059/16-A Lab Control Sample Total/NA
Solid 3051ALCS 490-368059/2-A Lab Control Sample Total/NA
Solid 3051A490-110980-1 MS Vulcan Quarry-1 Total/NA
Solid 3051A490-110980-1 MSD Vulcan Quarry-1 Total/NA
Analysis Batch: 368191
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 368059490-110980-1 Vulcan Quarry-1 Total/NA
Solid 6010D 368059490-110980-2 Vulcan Quarry-2 Total/NA
Solid 6010D 368059490-110980-3 Vulcan Quarry-3 Total/NA
Solid 6010D 368059490-110980-4 Vulcan Quarry-4 Total/NA
Solid 6010D 368059490-110980-5 Vulcan Quarry-5 Total/NA
Solid 6010D 368059MB 490-368059/1-A Method Blank Total/NA
Solid 6010D 368059LCS 490-368059/16-A Lab Control Sample Total/NA
Solid 6010D 368059LCS 490-368059/2-A Lab Control Sample Total/NA
Solid 6010D 368059490-110980-1 MS Vulcan Quarry-1 Total/NA
Solid 6010D 368059490-110980-1 MSD Vulcan Quarry-1 Total/NA
Analysis Batch: 368369
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 367943490-110980-1 Vulcan Quarry-1 Total/NA
Solid 7471B 367943490-110980-2 Vulcan Quarry-2 Total/NA
Solid 7471B 367943490-110980-3 Vulcan Quarry-3 Total/NA
Solid 7471B 367943490-110980-4 Vulcan Quarry-4 Total/NA
Solid 7471B 367943490-110980-5 Vulcan Quarry-5 Total/NA
Solid 7471B 367943MB 490-367943/1-A Method Blank Total/NA
Solid 7471B 367943LCS 490-367943/2-A Lab Control Sample Total/NA
Solid 7471B 367943490-110375-G-1-B MS Matrix Spike Total/NA
Solid 7471B 367943490-110375-G-1-C MSD Matrix Spike Duplicate Total/NA
General Chemistry
Analysis Batch: 367666
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-110980-1 Vulcan Quarry-1 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
General Chemistry (Continued)
Analysis Batch: 367666 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-110980-2 Vulcan Quarry-2 Total/NA
Solid Moisture490-110980-3 Vulcan Quarry-3 Total/NA
Solid Moisture490-110980-4 Vulcan Quarry-4 Total/NA
Solid Moisture490-110980-5 Vulcan Quarry-5 Total/NA
Solid Moisture490-110956-B-8 MS Matrix Spike Total/NA
Solid Moisture490-110956-B-8 MSD Matrix Spike Duplicate Total/NA
Solid Moisture490-110980-1 DU Vulcan Quarry-1 Total/NA
Prep Batch: 368183
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A490-110980-1 Vulcan Quarry-1 Total/NA
Solid 3060A490-110980-2 Vulcan Quarry-2 Total/NA
Solid 3060A490-110980-3 Vulcan Quarry-3 Total/NA
Solid 3060A490-110980-4 Vulcan Quarry-4 Total/NA
Solid 3060A490-110980-5 Vulcan Quarry-5 Total/NA
Solid 3060AMB 490-368183/1-A Method Blank Total/NA
Solid 3060ALCSI 490-368183/4-A Lab Control Sample Total/NA
Solid 3060ALCSS 490-368183/2-A Lab Control Sample Total/NA
Solid 3060ALCSSD 490-368183/3-A Lab Control Sample Dup Total/NA
Solid 3060A280-87113-G-1-D MSS Matrix Spike Total/NA
Solid 3060A280-87113-G-1-E MSI Matrix Spike Total/NA
Solid 3060A280-87113-G-1-C DU Duplicate Total/NA
Analysis Batch: 368433
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 368183490-110980-1 Vulcan Quarry-1 Total/NA
Solid 7196A 368183490-110980-2 Vulcan Quarry-2 Total/NA
Solid 7196A 368183490-110980-3 Vulcan Quarry-3 Total/NA
Solid 7196A 368183490-110980-4 Vulcan Quarry-4 Total/NA
Solid 7196A 368183490-110980-5 Vulcan Quarry-5 Total/NA
Solid 7196A 368183MB 490-368183/1-A Method Blank Total/NA
Solid 7196A 368183LCSI 490-368183/4-A Lab Control Sample Total/NA
Solid 7196A 368183LCSS 490-368183/2-A Lab Control Sample Total/NA
Solid 7196A 368183LCSSD 490-368183/3-A Lab Control Sample Dup Total/NA
Solid 7196A 368183280-87113-G-1-D MSS Matrix Spike Total/NA
Solid 7196A 368183280-87113-G-1-E MSI Matrix Spike Total/NA
Solid 7196A 368183280-87113-G-1-C DU Duplicate Total/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-110980-1
Project/Site: Continental Tire SDG: LRC-003
Client Sample ID: Vulcan Quarry-1 Lab Sample ID: 490-110980-1
Matrix: SolidDate Collected: 08/31/16 14:20
Date Received: 09/01/16 09:20
Prep 5035 JLP08/31/16 13:20 TAL NSH367546
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.147 g 5.0 mL
Analysis 8260B 1 368523 09/08/16 20:40 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 367460 09/02/16 10:42 LOJ TAL NSHTotal/NA 30.29 g 1.00 mL
Analysis 8270D 1 367446 09/02/16 18:02 T1C TAL NSHTotal/NA
Prep 3051A 368059 09/06/16 14:16 PG1 TAL NSHTotal/NA 0.508 g 100 mL
Analysis 6010D 1 368191 09/07/16 02:21 RDF TAL NSHTotal/NA
Prep 7471B 367943 09/06/16 10:01 LCS TAL NSHTotal/NA 0.610 g 100 mL
Analysis 7471B 1 368369 09/06/16 17:44 BLG TAL NSHTotal/NA
Prep 3060A 368183 09/07/16 09:06 BLM TAL NSHTotal/NA 2.5854 g 500 mL
Analysis 7196A 1 368433 09/07/16 16:27 BLM TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 367666 09/03/16 08:43 AAB TAL NSHTotal/NA
Client Sample ID: Vulcan Quarry-2 Lab Sample ID: 490-110980-2
Matrix: SolidDate Collected: 08/31/16 14:25
Date Received: 09/01/16 09:20
Prep 5035 JLP08/31/16 13:25 TAL NSH367546
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.261 g 5.0 mL
Analysis 8260B 1 368523 09/08/16 21:07 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 367460 09/02/16 10:42 LOJ TAL NSHTotal/NA 30.53 g 1.00 mL
Analysis 8270D 1 367446 09/02/16 18:22 T1C TAL NSHTotal/NA
Prep 3051A 368059 09/06/16 14:16 PG1 TAL NSHTotal/NA 0.498 g 100 mL
Analysis 6010D 1 368191 09/07/16 02:45 RDF TAL NSHTotal/NA
Prep 7471B 367943 09/06/16 10:01 LCS TAL NSHTotal/NA 0.609 g 100 mL
Analysis 7471B 1 368369 09/06/16 17:52 BLG TAL NSHTotal/NA
Prep 3060A 368183 09/07/16 09:06 BLM TAL NSHTotal/NA 2.5856 g 500 mL
Analysis 7196A 1 368433 09/07/16 16:27 BLM TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 367666 09/03/16 08:43 AAB TAL NSHTotal/NA
Client Sample ID: Vulcan Quarry-3 Lab Sample ID: 490-110980-3
Matrix: SolidDate Collected: 08/31/16 14:30
Date Received: 09/01/16 09:20
Prep 5035 JLP08/31/16 13:30 TAL NSH367546
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.684 g 5.0 mL
Analysis 8260B 1 368523 09/08/16 21:35 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 367460 09/02/16 10:42 LOJ TAL NSHTotal/NA 30.06 g 1.00 mL
Analysis 8270D 1 367446 09/02/16 18:41 T1C TAL NSHTotal/NA
Prep 3051A 368059 09/06/16 14:16 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 1 368191 09/07/16 02:50 RDF TAL NSHTotal/NA
Prep 7471B 367943 09/06/16 10:01 LCS TAL NSHTotal/NA 0.600 g 100 mL
Analysis 7471B 1 368369 09/06/16 17:55 BLG TAL NSHTotal/NA
Prep 3060A 368183 09/07/16 09:06 BLM TAL NSHTotal/NA 2.5486 g 500 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-110980-1
Project/Site: Continental Tire SDG: LRC-003
Client Sample ID: Vulcan Quarry-3 Lab Sample ID: 490-110980-3
Matrix: SolidDate Collected: 08/31/16 14:30
Date Received: 09/01/16 09:20
Analysis 7196A BLM09/07/16 16:271 TAL NSH368433
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis Moisture 1 367666 09/03/16 08:43 AAB TAL NSHTotal/NA
Client Sample ID: Vulcan Quarry-4 Lab Sample ID: 490-110980-4
Matrix: SolidDate Collected: 08/31/16 14:35
Date Received: 09/01/16 09:20
Prep 5035 JLP08/31/16 13:35 TAL NSH367546
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.203 g 5.0 mL
Analysis 8260B 1 368523 09/08/16 22:02 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 367460 09/02/16 10:42 LOJ TAL NSHTotal/NA 30.35 g 1.00 mL
Analysis 8270D 1 367446 09/02/16 19:01 T1C TAL NSHTotal/NA
Prep 3051A 368059 09/06/16 14:16 PG1 TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6010D 1 368191 09/07/16 02:55 RDF TAL NSHTotal/NA
Prep 7471B 367943 09/06/16 10:01 LCS TAL NSHTotal/NA 0.614 g 100 mL
Analysis 7471B 1 368369 09/06/16 17:58 BLG TAL NSHTotal/NA
Prep 3060A 368183 09/07/16 09:06 BLM TAL NSHTotal/NA 2.5657 g 500 mL
Analysis 7196A 1 368433 09/07/16 16:27 BLM TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 367666 09/03/16 08:43 AAB TAL NSHTotal/NA
Client Sample ID: Vulcan Quarry-5 Lab Sample ID: 490-110980-5
Matrix: SolidDate Collected: 08/31/16 14:40
Date Received: 09/01/16 09:20
Prep 5035 JLP08/31/16 13:40 TAL NSH367546
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.991 g 5.0 mL
Analysis 8260B 1 368523 09/08/16 22:30 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 367460 09/02/16 10:42 LOJ TAL NSHTotal/NA 30.54 g 1.00 mL
Analysis 8270D 1 367446 09/02/16 19:20 T1C TAL NSHTotal/NA
Prep 3051A 368059 09/06/16 14:16 PG1 TAL NSHTotal/NA 0.508 g 100 mL
Analysis 6010D 1 368191 09/07/16 03:10 RDF TAL NSHTotal/NA
Prep 7471B 367943 09/06/16 10:01 LCS TAL NSHTotal/NA 0.602 g 100 mL
Analysis 7471B 1 368369 09/06/16 18:00 BLG TAL NSHTotal/NA
Prep 3060A 368183 09/07/16 09:06 BLM TAL NSHTotal/NA 2.5895 g 500 mL
Analysis 7196A 1 368433 09/07/16 16:27 BLM TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 367666 09/03/16 08:43 AAB TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-110980-1Client: Hart & Hickman, PC
SDG: LRC-003Project/Site: Continental Tire
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
SW8467196AChromium, Hexavalent TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-110980-1
Project/Site: Continental Tire SDG: LRC-003
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Moisture Solid Percent Solids
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-110980-1
SDG Number: LRC-003
Login Number: 110980
Question Answer Comment
Creator: Ngo, Phiet
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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