7502_PolkCountyCDLF_GWMReport_DIN25869_20150924.pdf

Prepared for
Polk County, North Carolina
Project Number 2036.13

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Fall 2015 Semiannual
Water Quality Monitoring Report
Polk County
Construction and Demolition Debris Landfill
and Municipal Solid Waste Landfill
Permit 75-02
Route 9, Polk County, North Carolina

January 15, 2016

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Table of Contents
1.0 Introduction .................................................................................................................... 1
2.0 C&D Landfill.................................................................................................................... 2
2.1 Sampling and Analysis Methods....................................................................................2
2.2 Analytical Results ..........................................................................................................3
2.2.1 Groundwater Samples ......................................................................................4
2.2.2 Surface Water Samples ....................................................................................4
3.0 MSW Landfill .................................................................................................................. 5
3.1 Sampling and Analysis Methods....................................................................................5
3.2 Analytical Results ..........................................................................................................5
3.2.1 Groundwater Samples ......................................................................................5
4.0 Background Monitoring Well .......................................................................................... 7
4.1 Statistical Analysis Methodology ...................................................................................7
4.2 Results of Statistical Analysis ........................................................................................7
5.0 Summary ........................................................................................................................ 8
5.1 Future Activities .............................................................................................................8

Figures
1. Site Location Map
2. Site Layout Map
3. Groundwater Elevation Map
Tables
1. Summary of Groundwater Elevation Data—September 2015
2. Summary of Laboratory Analyses Performed on Samples
3. Summary of Detected Constituents
4. Solid Waste Section Limits Exceedances Notification
5. Water Quality Standards Exceedances Notification
6. VOCs Background Well Comparison
7. Metals Background Well Comparison

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Appendices
A. Sampling Logs and Equipment Documentation and Instrument Calibration Data Sheets
B. Report of Laboratory Analysis and Chain-of-Custody Documentation
C. Environmental Monitoring Reporting Form and Electronic Submittal of Environmental Monitoring
Data 7502Sept2015 (Electronic Format Only)
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1.0 Introduction
The Polk County Solid Waste Department (County) maintains two landfills at the Polk County Route 9 Landfill
Facility (site), located on the west side of North Carolina Route 9, approximately 1.5 miles northwest of the
community of Mill Spring (Figure 1).
The northernmost landfill area is an inactive permitted Construction and Demolition Debris (C&D) Landfill
(Figure 2). The 3.5-acre C&D Landfill (formerly known as the “Operating Landfill”) was capped during the
summer of 2006, and a Closure Plan was submitted to Mr. James Coffey at the North Carolina Department
of Environmental Quality (DEQ), formerly known as the Department of Environment and Natural Resources
(DENR), on August 21, 2006.
The second landfill is a Municipal Solid Waste (MSW) Landfill composed of two discrete areas in the west-
central and southern parts of the site (Figure 2). The MSW Landfill (formerly known as the “Closed Landfill”)
is inactive, closed, and maintained by the County. It was officially closed on April 9, 1994.
Both landfills are regulated by the DEQ, Division of Waste Management (DWM), under Permit No.75-02 (Polk
County C&D Landfill and MSW Landfill) as well as DEQ Solid Waste Management Rules Title 15A, North
Carolina Administrative Code (NCAC) Subchapter 13B, Section .0500 Rule (C&D Landfill) and Title 15A NCAC
13B.1600 Rule (MSW Landfill). The permit requires semiannual monitoring of groundwater and surface
water quality. This report is being submitted in accordance with the monitoring and reporting requirements
stated in the permit as well as the rules, and it provides an evaluation of surface water and groundwater
quality for the C&D Landfill and an evaluation of the groundwater quality for the closed MSW Landfill.
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2.0 C&D Landfill
2.1 Sampling and Analysis Methods
Three monitoring wells (MW-01CD, MW-02CD, and MW-03CD) and three surface water locations (SS-1, SS-2,
and SP-1) are monitored in association with the C&D Landfill. All monitoring points were sampled by
Altamont Environmental, Inc. (Altamont) on September 22 and 24, 2015. The approximate locations of the
groundwater monitoring wells and surface water sampling points are shown on Figure 2. Field sampling logs
are included as Appendix A.
Monitoring wells MW-01CD, MW-02CD, and MW-03CD sampled during the fall 2015 sampling event are
constructed of 2-inch-diameter Schedule 40 polyvinyl chloride (PVC) well material. Well construction logs for
these wells are not available. Prior to sampling, water level measurements were obtained. Table 1 and
Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation.
Monitoring wells MW-01CD and MW-02CD were purged and sampled with a disposable bailer on September
22 and 24, 2015. Prior to collecting samples, Altamont technicians purged three well volumes and recorded
parameters after each well volume was purged. During purging the pH, specific conductivity, dissolved
oxygen (DO), oxidation-reduction potential (ORP), turbidity, and temperature were measured and recorded.
Well purging continued until three well volumes were purged and these parameters stabilized as determined
by three successive readings in which each parameter was generally within a range of values, as follows:
 pH +/- 0.1 unit
 Specific conductivity +/- 3 percent
 Temperature +/- 10 percent
 DO +/- 10 percent
 Turbidity +/- 10 percent
 ORP +/- 10 millivolts
Once all these parameters stabilized, a groundwater sample was collected in laboratory-supplied sample
containers by a technician wearing a new pair of nitrile gloves.
MW-03CD was purged dry after removing approximately 1.25 gallons of water and allowed to recharge. The
Altamont technician allowed the well to recharge and then returned to collect a sample in laboratory
supplied containers. During prior events, technicians sampled MW-03CD using low-flow techniques. Due to
complications with pumping groundwater at the depth of water in this well during previous sampling events,
a disposable bailer was used to purge MW-03CD during this event.
Monitoring well MW-3R was pumped dry using a Grundfos Redi Flow 2 pump on September 23, 2015 and
the groundwater sample was collected following recharge the next day, September 24, 2015. A duplicate
sample was taken at MW-2R to ensure consistency with laboratory practices, and is listed as MW-2RDUP.
The surface water sample collected at the SS-1 location is representative of surface water quality upstream
of the landfill. The surface water sample collected at the SS-2 location is representative of surface water
quality downstream of the landfill. The surface water sample collected from the SP-1 location is
representative of surface water quality at a nearby spring that is situated at an elevation lower than the
landfill in an apparent downgradient direction (Figure 2).
At each monitoring well and surface water sampling location, pH, specific conductivity, DO, ORP, turbidity,
and temperature were measured and a grab sample was collected by a technician wearing a new pair of
nitrile gloves.
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Groundwater and surface water samples were immediately placed on ice in sample coolers for transport to
the laboratory. Proper chain-of-custody documentation was maintained during the collection and transport of
each sample. A trip blank was also transported in the sample cooler.
The groundwater and surface water samples were analyzed by TestAmerica Laboratories, Inc. (TestAmerica),
a laboratory certified in North Carolina, for Appendix I VOCs by EPA Method 8260 and for Appendix I metals
by EPA Methods 6010, 6020, and 7470 (Table 2). The trip blank was also analyzed for VOCs by EPA Method
8260. Report of laboratory analysis and chain-of-custody forms are included as Appendix B. Additional
observations and descriptions pertaining to individual wells are provided on the sampling logs that are
included as Appendix A. Additionally, water level measurements and field parameters are summarized in the
Electronic Data Deliverable (EDD) format included in Appendix C.
2.2 Analytical Results
The laboratory analytical results for groundwater, surface water, and trip blank samples collected at the C&D
Landfill are provided in the Analytical Report analysis issued by TestAmerica on October 19, 2015 and
included as Appendix B. In addition, all the laboratory analytical results are summarized in the EDD
(Appendix C) format specified by the Solid Waste Section (SWS) on May 5, 2010.
As stipulated in the DWM document referenced above, all laboratory analytical results were reported and
appropriately qualified. Non-detections (non-detects), which are values reported by the laboratory as below
method detection limits (MDLs), are tabulated in Table 3 and the EDD at MDL levels, and are qualified with
the “U” qualifier. The MDL is the minimum concentration of a substance that can be measured and reported
by a laboratory with 99 percent confidence that the analyte concentration is greater than zero. All detections
(values above the MDL) were compared to analyte-specific Solid Waste Section Limits (SWSLs) established
by the SWS. The SWSL is the lowest concentration of an analyte in a sample that can be quantitatively
determined with suitable precision and accuracy. If the reported concentration is above the laboratory MDL
and below the method reporting limit (MRL), the analytical result is qualified by the laboratory as estimated,
and is flagged with a “J” qualifier (J-flag). The MRL is the minimum concentration of a target analyte that can
be accurately determined by the referenced method. If the reported concentration is above the laboratory
MRL and below the SWSL, the analytical result is qualified as estimated, and is flagged with an italicized “J”
qualifier (italicized J-flag) by Altamont per DEQ requirements. The MRL is listed in the “Report Limit” (RL)
column in the report of laboratory analysis (Appendix B). Concentrations below the respective SWSLs are not
discussed in the text of this report unless they exceed their contaminant-specific water quality standards.
Detected concentrations of analytes in groundwater samples were compared to current groundwater quality
standards specified in 15A NCAC 2L.0202, which are referred to as “2L standards”. Detected concentrations
of analytes in groundwater with no established 2L standards were compared either to the interim maximum
allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with 15A NCAC 02L
.0202 [c]) or Groundwater Protection (GWP) Standards, pursuant to 15A NCAC 13B.1634. Detections of
analytes in surface-water samples were compared to 15A NCAC 2B surface-water quality standards (2B
standards).
Table 3 presents the summary of laboratory analytical results for detected constituents only. Table 4
presents all analytical results that were above the applicable SWSLs. Table 5 presents only the
concentrations of analytes detected in groundwater and/or surface-water samples that exceeded their
respective 2L standards (including IMACs, if applicable), GWP Standards, or 2B standards.
In the EDD (Appendix C), the identification of a well (“WELL ID” on the table) consists of the name of the well
prefaced by the un-hyphenated permit number for the facility. For example, the groundwater sample from
monitoring well MW-01CD is identified on the tables as 7502-MW01CD. However, in the tables and figures
of this report, the identification of a well consists of the name of the well without the permit number
associated with the facility.
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2.2.1 Groundwater Samples
Eleven metals (barium, beryllium, cadmium, chromium, cobalt, copper, lead, nickel, thallium, vanadium, and
zinc) were detected in one or more of the groundwater samples collected from the monitoring wells at the
C&D landfill. Six of the detected metals (barium, beryllium, cadmium, lead, vanadium, and zinc) were
detected at concentrations above their respective SWSLs in one or more groundwater samples collected
from the monitoring wells (Table 4). In addition, four metals (cobalt, lead, thallium, and vanadium) exceeded
their respective 2L or IMAC groundwater standards in one or more groundwater samples collected at the
C&D landfill (Table 5). However, vanadium was detected in the laboratory method blank, which may have
artificially increased the vanadium concentrations reported during this monitoring event.
Four VOCs were detected in one or more of the groundwater samples collected at the C&D landfill (1,4-
dichlorobenzene, acetone, tetrahydrofuran, and trichlorofluoromethane). No VOCs were detected at
concentrations above their respective SWSLs (Table 3) or water quality standards. Acetone was also
detected in the trip blank, indicating that acetone detected during this monitoring event is likely due to
laboratory contamination.
Groundwater pH readings were obtained from all monitoring wells sampled. The measured groundwater pH
values in monitoring wells MW-01CD, MW-02CD, and MW-03CD were outside the 2L standard pH range of
6.5 to 8.5 Standard Units (SU) (Tables 3 and 5).
Turbidity values at the time of sampling monitoring wells MW-01CD, MW-02CD, and MW-03CD ranged from
73.75 nephelometric turbidity units (NTUs) to 562.1 NTUs (Table 3). Monitoring wells MW-02CD and MW-
03CD were purged with a bailer during this monitoring event instead of using low-flow techniques. This is
due to low-flow techniques being difficult when depth to water exceeds 100 feet. Additionally, these wells
have historically have not recharged well and have often gone dry during purging, as was the case with these
wells during this monitoring event. Both of these wells exhibited high turbidity levels (562.1 and 194.3 NTUs,
respectively) when the samples were collected. This likely contributed to the concentrations of detected
metals in these wells since metals adhere to suspended sediment.
2.2.2 Surface Water Samples
Four metals (barium, cobalt, lead, and vanadium) were detected in one or more surface water samples
collected at designated sampling locations (Table 3). Barium was detected at sample location SP-1 above its
respective SWSL, but below the 2B surface water standard.
Acetone was detected in all three surface water samples at concentrations below the SWSL. Acetone was
also detected in the trip blank. Acetone was also detected in the trip blank, indicating that acetone detected
during this monitoring event is likely due to laboratory contamination. No other VOCs were detected in the
surface water samples.
The pH readings obtained from all sampled locations were within the 2B standard range of 6.00 to 9.00 SU
(Table 3).
Turbidity values measured in the surface water samples ranged from 9.07 NTUs (SS-1) to 157.1 NTUs (SP-1)
(Table 3). Turbidity measured at SP-1 exceeded the 2B turbidity standard of 25 NTUs.

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3.0 MSW Landfill
3.1 Sampling and Analysis Methods
Three monitoring wells, MW-1R, MW-2R, and MW-3R, are monitored in association with the MSW Landfill.
During the fall 2015 sampling event, the monitoring wells were sampled by Altamont on September 22 and
24, 2015. The approximate locations of the groundwater monitoring wells are shown on Figure 2. Field
sampling logs are included as Appendix A.
Monitoring wells MW-1R and MW-2R are constructed of 2-inch-diameter Schedule 40 PVC well material. Well
construction logs for these wells are not available. The well construction record for the newly installed
monitoring well MW-3R is available and was included in Appendix D of the Fall 2012 Semiannual Water
Quality Monitoring Report dated February 7, 2013.
Prior to sampling the wells, field parameters and water level measurements were obtained. Table 1 and
Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation. Field
parameters are presented in the sampling logs (Appendix A) and in the EDD (Appendix C).
Monitoring wells MW-1R and MW-2R were purged and sampled using low-flow techniques in accordance
with the procedures described in “Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures”, U.S.
Environmental Protection Agency (EPA), Groundwater Issues (April 1996). Prior to collecting samples, these
wells were purged until field parameters stabilized as mentioned in Section 2.1. Once these parameters
stabilized, a groundwater sample was collected in laboratory-supplied sample containers by a technician
wearing a new pair of nitrile gloves.
Monitoring well MW-3R was pumped dry using a Grundfos Redi Flow 2 pump on September 23, 2015 and
the groundwater sample was collected following recharge the next day, September 24, 2015. A duplicate
sample was taken at MW-2R to evaluate consistency with laboratory practices, and is listed as MW-2RDUP.
Proper chain-of-custody documentation procedures were followed during collection and transport of the
samples. Analysis of the groundwater samples was performed by TestAmerica using the same methods
described in Section 2.1 (Table 2). Additional observations and descriptions pertaining to individual wells are
provided on the sampling logs included as Appendix A.
3.2 Analytical Results
3.2.1 Groundwater Samples
The laboratory analytical results for groundwater, surface water, and trip blank samples collected at the
MSW Landfill are provided in the Analytical Report analysis issued by TestAmerica on October 19, 2015 and
included as Appendix B. In addition, all the laboratory analytical results are summarized in the EDD
(Appendix C) format specified by the Solid Waste Section (SWS) on May 5, 2010.
Four metals (barium, lead, nickel, and vanadium) were detected in one or more of the groundwater samples
collected from the monitoring wells. Of the detected metals, barium was present at concentrations above its
respective SWSL in one or more groundwater samples collected from the monitoring wells (Table 4). In
addition, vanadium exceeded its respective IMAC concentration in all of the samples associated with the
MSW landfill. However, vanadium was detected in the laboratory method blank, which may have artificially
increased the vanadium concentrations reported during this monitoring event.
Four VOCs were detected in one or more groundwater samples collected from the monitoring wells (1,1-
dichloroethane, cis-1,2-dichloroethene, tetrahydrofuran, and trichloroethene). Cis-1,2-dichloroethene was
detected above its SWSL, but below its 2L groundwater standard (Table 4) in samples MW-2R and MW-
2RDUP. No VOCs were present at concentrations above established water quality standards.
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The measured pH was below the acceptable range established as the 2L standard in MW-1R, MW-2R, and
MW-2RDUP (Tables 3 and 5).
Turbidity values at the time of sampling monitoring wells MW-1R, MW-2R, MW-2RDUP, and MW-3R ranged
from 0.00 NTUs to 8.62 NTUs (Table 3).

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4.0 Background Monitoring Well
4.1 Statistical Analysis Methodology
In 2012, background monitoring well, MW-3R, was installed upgradient of the other two MSW monitoring
wells and three C&D monitoring wells. MW-3R was installed to establish background concentrations of
Appendix I VOCs and metals upgradient of the MSW Landfill and C&D Landfill. MW-3R, consistent with the
other five monitoring wells, is sampled on a semiannual basis. MW-3R has been sampled seven times from
October 2012 to September 2015.
A brief statistical analysis presented herein compares background concentrations in MW-3R to downgradient
monitoring wells, and applicable water quality standards. Historical data was summarized for MW-01CD,
MW-02CD, MW03CD, MW-1R, and MW-2R from the seven sampling events occurring from September 2012
to September 2015. Data from MW-3R was summarized from the seven sampling events occurring from
October 2012 to September 2015. Tables 6 and 7 list the constituents detected in each well for the subject
monitoring period, minimum concentration, maximum concentration, and average concentration of each
detected constituent, as well as the frequency of detection in each well. Results below the MDL were
assumed to equal half of the MDL.
4.2 Results of Statistical Analysis
A comparison of VOCs is presented in Table 6. No VOCs were detected in the background well (MW-3R)
during the subject statistical analysis period. Seven VOCs (1,1-dichloroethane, 1,4-dichlorobenzene,
acetone, cis-1,2-dichloroethene, tetrahydrofuran, trichloroethene, and trichlorofluoromethane) were
detected in one or more of the downgradient monitoring wells. However, all detections were at
concentrations below the respective 2L standards. A comparison of the average concentrations of VOCs in
downgradient wells with the average concentrations of VOCs in the background well shows that the majority
of average concentrations in downgradient wells exceed those of the background well.
A comparison of metals concentrations is presented in Table 7. Barium, lead, and vanadium were detected
in MW-3R. In all monitoring wells, vanadium was the only metal to exceed its appropriate groundwater
standard. Eleven metals (barium, beryllium, cadmium, chromium, cobalt, copper, lead, nickel, thallium,
vanadium, and zinc) were detected in one or more of the downgradient monitoring wells. Four of the average
concentrations of these metals (cobalt, lead, thallium, and vanadium) exceeded groundwater quality
standards in one or more downgradient monitoring wells. However, the maximum results for cobalt and
thallium include estimated (“J” flagged) values. Average concentrations for the majority of metals in
downgradient monitoring wells exceeded the average concentrations of those metals in the background well.

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5.0 Summary
Altamont completed the second semiannual water quality monitoring event of 2015 at the Polk County
Landfills on September 22, 23, and 24, 2015.
Tables 3, 4, and 5 of this report, the TestAmerica report of laboratory analysis included as Appendix B, and
the EDD in Appendix C provide detailed analytical results and field data demonstrating the groundwater and
surface water quality at the Polk County Landfills.
5.1 Future Activities
Altamont recommends that Polk County continue to monitor VOCs and metals concentrations in groundwater
and surface water at the closed C&D and MSW landfills.
Based on the data trends and evaluation presented in this report, Altamont has discussed with Polk County
options for addressing the water quality impacts identified at the site. Based on these discussions, Altamont
understands that Polk County is planning to replace monitoring wells MW-1R and MW-03CD early in 2016 in
an effort to obtain groundwater samples of a higher quality.
Altamont will continue to monitor the groundwater and surface water on a semiannual basis at the Polk
County C&D and MSW Landfills. The next sampling event is scheduled for March 2016.

FIGURES

Copyright:© 2013 National Geographic Society, i-cubed
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Landfill Site Boundary
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
















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
Landfill Site Boundary
!U 




P:\POLK COUNTY\ROUTE 9 LF\FIGURES\2015\SPRING\7502MARCH2015 FIGURE 2-SITE LAYOUT MAP.MXD0400800200Feet
Transfer Station
Scale Station
Inactive C & D Landfill
Inactive ClosedMSW Landfill cell
Inactive ClosedMSW Landfill cell
!U
!U!U
!U
!U
!U
!U
!U
!U
SS-2
SS-1
SP-01
MW-3R2,884.03
MW-2R2,802.56
MW-1R2,837.39
MW-03CD2,848.22
MW-02CD2,830.71 MW-01CD2,843.80 NC 9 HWYGARRETT R D
LANDFILL RD
B
U
R
T

B
L
A
C
K
W
E
L
L

R
D
W I L L I A M L N
MARTIN WALKER RD
G
R
E
E
N
H
IL
L
S R
D
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
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
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

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



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



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
Landfill Site Boundary
!U 






0 300 600Feet


TABLES

Table 1
Summary of Groundwater Elevation Data---September 2015
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Top Of Casing (TOC)
Elevation (From
Assumed Datum)
Depth To Water Groundwater
Elevation
(feet) (feet TOC)(feet)
C&D Landfill
MW-01CD 2,955.50 111.70 2,843.80
MW-02CD 2,951.90 121.19 2,830.71
MW-03CD 2,969.60 121.38 2,848.22
MSW Landfill
MW-1R 2,867.70 30.31 2,837.39
MW-2R 2,837.20 34.64 2,802.56
MW-3R 2,962.00 77.97 2,884.03
Notes:
1. All elevations were based on an assumed datum of 3,000 feet.
2. Monitoring well MW-3R was surveyed on November 8, 2012 by Wes Cole Land Surveying, PA.
3. Monitoring wells MW-1R and MW-2R were surveyed on November 13, 2010 by Wes Cole
Land Surveying, PA.
4. Remaining wells were surveyed on December 9, 2006 by Wes Cole Land Surveying, PA.
5. Depth to water for all monitoring wells was measured on September 22, 23, and 24, 2015.
Well ID
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\7502Sept2015 T1 GW Elevation Data Page 1 of 1
Table 2
Summary of Laboratory Analyses Performed on Samples
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
GROUNDWATER SAMPLES
VOCs
EPA 8260 EPA 6010 EPA 6020 EPA 7470
C&D Landfill
75-02 MW-01CD 9/24/2015 X X X X
75-02 MW-02CD 9/22/2015 X X X X
75-02 MW-03CD 9/24/2015 X X X X
MSW Landfill
75-02 MW-1R 9/22/2015 X X X X
75-02 MW-2R 9/22/2015 X X X X
75-02 MW-2RDUP 9/22/2015 X X X X
75-02 MW-3R 9/24/2015 X X X X
SURFACE WATER SAMPLES
VOCs
EPA 8260 EPA 6010 EPA 6020 EPA 7470
C&D Landfill
75-02 SP-1 9/22/2015 X X X X
75-02 SS-1 9/22/2015 X X X X
75-02 SS-2 9/22/2015 X X X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260
75-02 TRIP BLANK 9/22/2015 X
Notes:
1. VOCs = volatile organic compounds
2. VOCs and metals analyses include Appendix I constituents per 40 CFR Part 258.
Metals
Metals
Facility
Permit Well ID Collect Date
Facility
Permit Sample ID Collect Date
Facility
Permit Sample ID Collect Date
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\7502Sept2015 T2,T3,T4,T5 Page 1 of 1
Table 3
Summary of Detected Constituents
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Metals (Appendix I)VOCs (Appendix I)Field Parameters
Laboratory Certification 387 387
Laboratory Methods EPA 6010, EPA 6020, EPA 7470 EPA 8260 5445 (pH only)
Parameter Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Thallium Vanadium Zinc
1,1-
Dichloro-
ethane
1,4-
Dichloro-
benzene
Acetone
cis-1,2-
Dichloro-
ethene
Methylene
Chloride
Tetrahydro-
furan
Trichloro-
ethene
Trichloro-
fluoro-
methane
pH Turbidity
CAS Number 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7440-28-0 7440-62-2 7440-66-6 75-34-3 106-46-7 67-64-1 156-59-2 75-09-2 109-99-9 79-01-6 75-69-4 SW320 SW330
SWS ID 15 23 34 51 53 54 131 152 194 209 213 75 71 100 78 140 458 201 203 320 330
Units µg/L ug/L ug/L ug/L ug/L ug/L ug/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
MW-01CD 9/24/2015 47.5 J 0.500 U 0.500 U 3.00 U 1.57 J 5.00 U 6.70 J 3.00 U 0.200 U 6.09 J, B 10.0 U 0.240 U 0.170 U 2.73 J 0.210 U 0.220 U 0.820 U 0.200 U 0.480 J 5.83 73.75
MW-02CD 9/22/2015 627 1.58 J 1.50 3.40 J 6.10 J 5.00 J 30.7 3.90 J 0.603 J 43.6 B 38.8 0.240 U 0.170 U 2.66 U 0.210 U 0.220 U 0.820 U 0.200 U 0.281 J 5.53 562.1
MW-03CD 9/24/2015 319 0.500 U 0.500 J 3.00 U 1.43 J 5.00 U 10.5 3.00 U 0.384 J 6.83 J, B 13.1 J 0.240 U 0.288 J 2.90 J 0.210 U 0.220 U 7.04 J 0.200 U 0.301 J 5.81 194.3
MW-1R 9/22/2015 60.7 J 0.500 U 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 4.90 J 0.200 U 1.74 J, B 10.0 U 0.240 U 0.170 U 2.66 U 2.00 J 0.220 U 1.70 J 0.200 U 0.210 U 4.57 3.32
MW-2R 9/22/2015 217 0.500 U 0.500 U 3.00 U 0.500 U 5.00 U 4.50 J 3.00 U 0.200 U 2.35 J, B 10.0 U 0.640 J 0.170 U 2.66 U 13.4 0.220 U 0.820 U 0.928 J 0.210 U 5.77 0.00
MW-2RDUP 9/22/2015 212 0.500 U 0.500 U 3.00 U 0.500 U 5.00 U 5.00 J 3.00 U 0.200 U 2.33 J, B 10.0 U 0.718 J 0.170 U 2.66 U 13.5 0.220 U 0.820 U 0.986 J 0.210 U 5.77 0.00
MW-3R 9/24/2015 9.10 J 0.500 U 0.500 U 3.00 U 0.500 U 5.00 U 3.70 J 3.00 U 0.200 U 2.00 J, B 10.0 U 0.240 U 0.170 U 2.66 U 0.210 U 0.220 U 0.820 U 0.200 U 0.210 U 6.68 8.62
SP-1 9/22/2015 174 0.500 U 0.500 U 3.00 U 1.48 J 5.00 U 6.70 J 3.00 U 0.200 U 5.20 J, B 10.0 U 0.240 U 0.170 U 3.99 J 0.210 U 0.220 U 0.820 U 0.200 U 0.210 U 6.79 157.1
SS-1 9/22/2015 42.5 J 0.500 U 0.500 U 3.00 U 0.500 U 5.00 U 3.70 J 3.00 U 0.200 U 2.64 J, B 10.0 U 0.240 U 0.170 U 3.92 J 0.210 U 0.220 U 0.820 U 0.200 U 0.210 U 6.74 9.07
SS-2 9/22/2015 38.2 J 0.500 U 0.500 U 3.00 U 0.500 U 5.00 U 3.70 J 3.00 U 0.200 U 2.55 J, B 10.0 U 0.240 U 0.170 U 3.98 J 0.210 U 0.220 U 0.820 U 0.200 U 0.210 U 7.21 9.08
TripBlank 9/22/2015 NA NA NA NA NA NA NA NA NA NA NA 0.240 U 0.170 U 12.3 J 0.210 U 1.33 J 0.820 U 0.200 U 0.210 U NA NA
MDL 5.00 0.500 0.500 3.00 0.500 5.00 2.00 3.00 0.200 0.100 10.0 0.240 0.170 2.66 0.210 0.220 0.820 0.200 0.210 NA NA
MRL 10 2.0 1.0 5.0 2.0 10.0 5.0 10 2.0 2.0 25 1.0 1.0 25 1.0 5.0 10 1.0 1.0 NA NA
SWSL 100 1 1 10 10 10 10 50 5.5 25 10 5 1 100 5 1 NE 1 1 NE NE
2L 700 NE 2 10 NE 1,000 15 100 NE NE 1,000 6 6 6,000 70 5 NE 3 2,000 6.5-8.5 NE
IMAC NE 4 NE NE 1 NE NE NE 0.2 0.3 NE NE NE NE NE NE NE NE NE NE NE
GWP NE 4 NE NE 1 NE NE NE 0.28 0.3 NE NE NE NE NE NE NE NE NE NE NE
2B 200,000 6.5 2 50 4 7 25 88 0.47 NE 50 100 100 2,000 720 590 NE 30 67,000 6.0-9.0 25
Notes:
1.Only detected constituents are listed on this table. Please refer to TestAmerica Report of Laboratory Analysis (Appendix B) for further details.
2."Lab Method" is the analytical method used to analyze the constituents.
3."CAS Number" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
4."SWS ID" is the Solid Waste Section Identification Number.
5."Units" are micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
6."Collect Date" is the date on which the sample was collected in the field.
7."Result" is analytical data reported by the laboratory or field data collected by Altamont.
8."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
9."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
10."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
11."U" is a laboratory data qualifier used for parameters not detected at concentrations above MDL.
12."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
An italicized "J" qualifier is assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
13."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources,
Subchapter 2L - Groundwater Classifications and Standards," DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
14."GWP" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DENR. Current standards were obtained from http://portal.ncdenr.org/web/sw/envmonitoringlist (last updated June 13, 2011).
GWP standard is used only if 2L or IMAC standards are not established for specific constituent.
15."2B" indicates surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water and Wetland Standards,"
(last amended on May 1, 2007) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
16."NE" means Not Established. "NA" means Not Applicable.
17.Bold numbers indicate a detection. Grayed cells indicate result in exceedance of the 2L, IMAC, GWP, or 2B standard.
18."B" is a laboratory data qualifier used for parameters detected in both the laboratory method blank and in the sample.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\7502Sept2015 T2,T3,T4,T5 Page 1 of 1
Table 4
Solid Waste Section Limits Exceedances Notification
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
FACILITY
PERMIT SAMPLE ID CAS
NUMBER SWS ID PARAMETER RESULT UNITS METHOD MDL MRL SWSL COLLECT DATE
GROUNDWATER SAMPLES
75-02 MW-02CD 7440-39-3 15 Barium 627 µg/L EPA 6010 5.00 10 100 9/22/2015
75-03 MW-02CD 7440-41-7 23 Beryllium 1.58 J µg/L EPA 6020 0.500 2.0 1 9/22/2015
75-02 MW-02CD 7440-43-9 34 Cadmium 1.50 µg/L EPA 6010 0.500 1.0 1 9/22/2015
75-02 MW-02CD 7439-92-1 131 Lead 30.7 µg/L EPA 6010 2.00 5.0 10 9/22/2015
75-02 MW-02CD 7440-62-2 209 Vanadium 43.6 B µg/L EPA 6020 0.100 2.0 25 9/22/2015
75-02 MW-02CD 7440-66-6 213 Zinc 38.8 µg/L EPA 6020 10.0 25 10 9/22/2015
75-02 MW-03CD 7440-39-3 15 Barium 319 µg/L EPA 6010 5.00 10 100 9/24/2015
75-02 MW-03CD 7439-92-1 131 Lead 10.5 µg/L EPA 6010 2.00 5.0 10 9/24/2015
75-02 MW-03CD 7440-66-6 213 Zinc 13.1 J µg/L EPA 6020 10.0 25.0 10 9/24/2015
75-02 MW-2R 7440-39-3 15 Barium 217 µg/L EPA 6010 5.00 10.0 100 9/22/2015
75-02 MW-2R 156-59-2 78 cis-1,2-Dichloroethene 13.4 µg/L EPA 8260 0.210 1.00 5 9/22/2015
75-02 MW-2RDUP 7440-39-3 15 Barium 212 µg/L EPA 6010 5.00 10.0 100 9/22/2015
75-02 MW-2RDUP 156-59-2 78 cis-1,2-Dichloroethene 13.5 µg/L EPA 8260 0.210 1.00 5 9/22/2015
75-02 SP-1 7440-39-3 15 Barium 174 µg/L EPA 6010 5.00 10.0 100 9/22/2015
Notes:
1."CAS NUMBER" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
2."SWS ID" is the Solid Waste Section Identification Number.
3."RESULT" is the analytical data reported by the laboratory.
4."µg/L" indicates unit of micrograms per liter for analytical results.
5."METHOD" is the analytical method used to analyze the constituents.
6."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence
that the analyte concentration is greater than zero.
7."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
8."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively
determined with suitable precision and accuracy.
9."COLLECT DATE" is the date on which the sample was collected in the field.
10.Grayed cells indicate result in exceedance of the applicable water quality standards ("2L", "IMAC", or "GWP").
11."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards," DENR
(Amended April 1, 2013). The IMAC concentrations are listed in Appendix #1 of the 2L rule.
12."GWP" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DENR. Current standards were obtained from
http://portal.ncdenr.org/web/sw/envmonitoringlist (last updated June 13, 2011). GWP standard is used only if 2L or IMAC standards are not
established for specific constituent.
13."B" is a laboratory data qualifier used for parameters detected in both the laboratory method blank and in the sample.
14."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
An italicized "J" qualifier is assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\7502Sept2015 T2,T3,T4,T5 Page 1 of 1
Table 5
Water Quality Standards Exceedances Notification
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
FACILITY
PERMIT WELL ID CAS
NUMBER
SWS
ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL
WATER
QUALITY
STANDARD
COLLECT
DATE CAUSE AND SIGNIFICANCE
GROUNDWATER SAMPLES - 2L STANDARD, IMAC OR GROUNDWATER PROTECTION STANDARD (GWP; ug/L or SU)
75-02 MW-01CD 7440-48-4 53 Cobalt 1.57 µg/L J EPA 6020 0.500 2.0 10 1 9/24/2015
75-02 MW-01CD 7440-62-2 209 Vanadium 6.09 µg/L J, B EPA 6020 0.100 2.0 25 0.3 9/24/2015
75-02 MW-01CD SW320 320 pH 5.83 SU 5445 NA NA NE 6.5 - 8.5 9/24/2015 Consistent with historic readings.
75-02 MW-02CD 7440-48-4 53 Cobalt 6.10 µg/L J EPA 6020 0.500 2.0 10 1 9/22/2015
75-02 MW-02CD 7439-92-1 131 Lead 30.7 µg/L EPA 6010 2.00 5.0 10 15 9/22/2015
75-02 MW-02CD 7440-28-0 194 Thallium 0.603 µg/L J EPA 6020 0.200 2.0 5.5 0.2 9/22/2015
75-02 MW-02CD 7440-62-2 209 Vanadium 43.6 µg/L B EPA 6020 0.100 2.0 25 0.3 9/22/2015
75-02 MW-02CD 320 320 pH 5.53 SU 5445 NA NA NE 6.5 - 8.5 9/22/2015 Consistent with historic readings.
75-02 MW-03CD 7440-48-4 53 Cobalt 1.43 µg/L J EPA 6020 0.500 2.0 10 1 9/24/2015
75-02 MW-03CD 7440-28-0 194 Thallium 0.384 µg/L J EPA 6020 0.200 2.0 5.5 0.2 9/24/2015
75-02 MW-03CD 7440-62-2 209 Vanadium 6.83 µg/L J, B EPA 6020 0.100 2.0 25 0.3 9/24/2015
75-02 MW-03CD SW320 320 pH 5.81 SU 5445 NA NA NE 6.5 - 8.5 9/24/2015 Consistent with historic readings.
75-02 MW-1R 7440-62-2 209 Vanadium 1.74 µg/L J, B EPA 6020 0.100 2.0 25 0.3 9/22/2015
75-02 MW-1R SW320 320 pH 4.57 SU 5445 NA NA NE 6.5 - 8.5 9/22/2015 Consistent with historic readings.
75-02 MW-2R 7440-62-2 209 Vanadium 2.35 µg/L J, B EPA 6020 0.100 2.0 25 0.3 9/22/2015
75-02 MW-2R SW320 320 pH 5.77 SU 5445 NA NA NE 6.5 - 8.5 9/22/2015 Consistent with historic readings.
75-02 MW-2RDUP 7440-62-2 209 Vanadium 2.33 µg/L J, B EPA 6020 0.100 2.0 25 0.3 9/22/2015
75-02 MW-2RDUP SW320 320 pH 5.77 SU 5445 NA NA NE 6.5 - 8.5 9/22/2015 Consistent with historic readings.
75-02 MW-3R 7440-62-2 209 Vanadium 2.00 µg/L J, B EPA 6010 0.100 2.0 25 0.3 9/24/2015
75-02 SP-1 SW330 330 Turbidity 157.1 NTU NA NA NA NE 25 9/22/2015
Notes:
1."CAS NUMBER" is a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
2."SWS ID" is the Solid Waste Section Identification Number.
3."RESULT" is analytical data reported by the laboratory or field data collected by Altamont.
4."UNITS" are micrograms per liter (µg/L) for analytical results and Standard Units (SU) for pH.
5."QUALIFIER" is a data qualifier or "flag". A blank cell indicates that there is no qualifier associated with the reported result.
6."METHOD" is the analytical method used to analyze the constituents.
7."MDL" is the method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
8."MRL" is the method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
9."SWSL" is the Solid Waste Section Limit. This limit (identified by DENR) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
10."WATER QUALITY STANDARD" refers to the 2L Standard, Interim Maximum Allowable Concentration (IMAC), or Groundwater Protection Standard (GWP) for groundwater, 2B Standard for surface water.
11."COLLECT DATE" is the date on which the sample was collected in the field.
12.2L standard and IMAC are from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2L -
Groundwater Classifications and Standards," DENR (Amended April 1, 2013). The IMAC concentrations are listed in Appendix #1 of the 2L rule.
13."NE" means not established.
14.Blank cell indicates that there is no relevant information associated with this cell.
15.2B standard is from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water
and Wetland Standards," (last amended on May 1, 2007) or National Criteria per EPA obtained from table current as of May 15, 2013.
16."B" is a laboratory data qualifier used for parameters detected in both the laboratory method blank and in the sample.
17."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
An italicized "J" qualifier is assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\7502Sept2015 T2,T3,T4,T5 Page 1 of 1
Table 6
VOCs Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
1/7 Acetone 1.41 U 10 U 3.538 6,000
7/7 Trichlorofluoromethane 0.28 J 0.65 J 0.427 2,000
1/3 Acetone 2.53 J 2.66 U 1.730 6,000
2/3 Trichlorofluoromethane 0.210 U 0.42 J 0.269 2,000
1/3 Xylene (Total)0.38 U 0.47 J 0.317 500
1/7 1,2-Dichlorobenzene 0.12 U 0.30 U 0.135 20
2/7 1,4-Dichlorobenzene 0.33 U 0.463 U 0.219 6
2/7 Acetone 0.598 U 4.59 J 4.117 6,000
2/6 Tetrahydrafuran 2.53 J 7.04 J 2.628 NE
7/7 Trichlorofluoromethane 0.301 J 0.52 J 0.387 2,000
1/7 Xylene (Total)0.38 U 0.55 J 0.336 500
1/7 1,4-Dichlorobenzene 0.17 J 0.33 U 0.167 6
2/7 cis-1,2-Dichloroethene 0.19 U 2.0 J 0.619 70
9/13 1,1-Dichloroethane 0.24 U 1.06 J 0.586 6
12/13 cis-1,2-Dichloroethene 5.2 13.9 10.673 70
3/13 Tetrachloroethene 0.14 U 0.46 U 0.190 0.7
12/13 Trichloroethene 0.200 U 1.56 1.020 3
1/13 Vinyl chloride 0.18 U 0.62 U 0.210 0.03
0/7 1,1-Dichloroethane 0.215 U 0.32 U 0.141 6
0/7 1,2-Dichlorobenzene 0.19 U 0.3 U 0.291 20
0/7 1,4-Dichlorobenzene 0.33 U 0.463 U 0.152 6
0/7 cis-1,2-Dichloroethene 0.19 U 0.19 U 0.106 70
0/7 Acetone 0.598 U 10 U 3.338 6,000
0/7 Tetrachloroethene 0.264 U 0.46 U 0.170 0.7
0/7 Trichloroethene 0.227 U 0.47 U 0.179 3
0/7 Trichlorofluoromethane 0.137 U 0.21 U 0.116 2,000
0/7 Vinyl chloride 0.189 U 0.62 U 0.216 0.03
0/7 Xylene (Total)0.20 U 0.66 U 0.278 500
Notes:
1."µg/L" = micrograms per liter
2."Min." = minimum concentration (µg/L)
3."Max." = maximum concentration (µg/L)
4."Avg." = average concentration (µg/L)
5."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards,"
DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
6."U" is a laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
7."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
8."NA" = not applicable
9."# Detections" = number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples collected
during 6 of the 7 sampling events, thus there are 13 total samples representing MW-2R.
10.Grayed cells indicate results above 2L Standard or IMAC.
11.Average concentrations were calculated by summing the contiuent detections and dividing by the number of samples. When the sample was
below the MDL, half of the MDL value was used as the result. Some results are estimated (J flagged) and the average concentration is thus estimated.
12.MW-02CD was only sampled in September 2012, March 2015, and September 2015 due to a lack of well recharge during other sampling events.
13.The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-2R
(and MW-
2RDUP)
MW-3R
MW-1R
MW-03CD
MW-02CD
September 2012 - September 2015
Well # Detections Detected Constituents Concentration (µg/L)2L Standard or
IMAC
MW-01CD
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\Statistics_Background Sept 2015 Page 1 of 1
Table 7
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
7/7 Barium 2.5/3.69/5.0 12.5 J 104 41.71 700
1/7 Beryllium 0.0594/0.65/0.50/1.0 0.5 U 1.0 U 0.42 4
1/7 Cadmium 0.0278/0.155/0.50/1.0 0.3 J 1.0 U 0.36 2
1/7 Chromium 1.47/2.5/5.0 2.5 U 5.0 U 2.15 10
1/7 Cobalt 2.5/3.39/5.0 1.57 5.0 U 2.07 1
2/7 Copper 0.672/2.5/5.0 2.5 U 8.30 J 3.83 1,000
3/7 Lead 2.5/5.0/5.41 2.5 U 7.72 J 4.40 15
1/7 Silver 1.05/2.5/5.0 2.5 U 5.02 J 2.36 20
2/7 Thallium 0.019/0.025/0.641 0.019 U 0.641 U 0.14 0.2
2/7 Vanadium 0.0661/2.5/5.0 1.8 J 10 U 3.09 0.3
4/7 Zinc 2.26/5.0/10.0 10.0 U 105 22.54 1,000
3/3 Barium 2.5/3.69/5.0 41.0 J 627 249.20 700
1/3 Beryllium 0.5/0.65 0.5 U 1.58 J 0.72 4
2/3 Cadmium 0.0278/0.155/0.50/1.0 0.3 J 1.5 0.68 2
2/3 Chromium 1.47/5.0 3.0 U 3.66 J 2.85 10
1/3 Cobalt 2.5/3.39/5.0 3.39 U 6.1 J 3.43 1
2/3 Copper 0.672/5.0 5.0 U 5.52 J 4.34 1,000
2/3 Lead 5.0/5.41 2.0 U 30.7 14.20 15
1/3 Nickel 1.05/2.5/5.0 3.0 U 3.9 J 2.31 100
1/3 Silver 1.05/5.0 2.5 U 4.99 J 2.58 20
1/3 Thallium 0.2/0.641 0.2 U 0.641 U 0.34 0.2
1/3 Vanadium 0.0661/2.5/5.0 1.6 J 43.6 16.73 0.3
2/3 Zinc 2.26/5.0/10.0 10 U 38.8 19.80 1,000
7/7 Barium 2.5/3.69/5.0 184 768 362.71 700
2/7 Beryllium 0.65/1.0 0.570 J 1.7 0.62 4
4/7 Chromium 1.47/2.5/5.0 4.30 J 20.3 6.89 10
3/7 Cobalt 2.5/3.39/5.0 3.39 U 10.1 3.79 1
4/7 Copper 0.672/2.5/5.0 5.0 U 21.8 8.80 1,000
4/7 Lead 1.05/2.5/5.0 5.0 U 8.15 J 7.42 15
4/7 Nickel 1.05/2.5/5.0 3.0 U 10.9 J 5.85 100
1/7 Silver 1.05/2.5/5.0 2.5 U 5.97 J 2.50 20
6/7 Thallium 0.019/0.025/0.641 0.026 J 0.644 J 0.23 0.2
7/7 Vanadium 0.0661/2.5/5.0 4.0 J 54 16.35 0.3
7/7 Zinc 2.26/5.0/10.0 13.1 J 223 46.13 1,000
1/7 Arsenic 2.5/3.69/5.0/ 10.0 2.5 U 25.6 4.11 10
7/7 Barium 2.5/3.69/5.0 41.4 J 2,270 350.71 700
3/7 Beryllium 0.0594/0.65/0.50/1.0 0.50 U 13.3 1.27 4
3/7 Cadmium 0.0278/0.155/0.50/1.0 0.3 J 5.8 0.79 2
3/7 Chromium 1.47/2.5/5.0 3.60 J 51.5 5.34 10
3/7 Copper 0.672/2.5/5.0 2.5 U 122 11.30 1,000
3/7 Lead 2.0/2.5/5 2.0 U 64.7 6.52 15
3/7 Nickel 2.5/3.06/5.0 2.5 U 29.1 J 3.96 100
1/7 Silver 1.05/2.5/5.0 2.5 U 5.0 U 2.00 20
3/7 Thallium 0.019/0.025/0.641 0.025 U 1.2 J 0.17 0.2
4/7 Vanadium 0.0661/2.5/5.0 2.5 U 407 32.67 0.3
6/7 Zinc 2.26/5.0/10.0 10 U 428 12.24 1,000
MW-03CD
MW-1R
MW-02CD
Well
MW-01CD
September 2012 - September 2015
# Detections MDL (ug/L)
Concentration (µg/L)
Constituents Detected 2L Standard
or IMAC
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\Statistics_Background Sept 2015 Page 1 of 2
Table 7
Metals Background Well Comparison
Polk County C&D and MSW Landfills, Route 9, Polk County, North Carolina
Min.Max.Avg.
Well
MW-01CD
September 2012 - September 2015
# Detections MDL (ug/L)
Concentration (µg/L)
Constituents Detected 2L Standard
or IMAC
13/13 Barium 2.5/3.69/5.0 63.3 J 217 159.33 700
1/13 Cadmium 0.0278/0.155/0.50/1.0 0.155 U 1.0 U 0.34 2
2/13 Chromium 1.47/2.5/5.0 2.5 U 5.0 U 2.16 10
2/13 Copper 0.672/2.5/5.0 2.5 U 7.01 J 2.99 1,000
2/13 Lead 2.0/2.5/5.0/5.41 2.0 U 5.41 U 2.45 15
1/13 Nickel 2.5/3.06/5.0 2.5 U 5.0 U 2.03 100
2/13 Silver 1.05/2.5/5.0 2.5 U 5.88 J 2.40 20
1/13 Thallium 0.019/0.025/0.641 0.019 U 0.641 U 0.09 0.2
2/13 Vanadium 0.0661/0.1/2.5/5.0 0.2 U 0.5 U 1.60 0.3
6/13 Zinc 2.26/5.0/10.0 10.0 U 19.5 10.20 1,000
0/7 Arsenic 3.69/5.0/ 10.0 3.69 U 10.0 U 3.00 10
6/7 Barium 2.5/3.69/5.0 3.25 J 12.3 J 6.54 700
0/7 Beryllium 0.13/0.5/1.0 0.13 U 1.0 U 0.33 4
1/7 Cadmium 0.0278/0.155/0.50/1.0 0.04 J 1.0 U 0.33 2
1/7 Chromium 1.47/2.5/5.0 2.02 J 5.0 U 1.97 10
0/7 Cobalt 2.5/3.39/5.0 3.39 U 5.0 U 2.21 1
0/7 Copper 0.672/5.0 0.672 U 5.0 U 2.01 1,000
1/7 Lead 2.0/2.5/5.0/5.41 2.0 U 5.41 U 2.31 15
0/7 Nickel 2.5/3.06/5.0 2.5 U 5.0 U 1.90 100
0/7 Silver 1.05/2.5/5.0 1.05 U 5.0 U 1.68 20
0/7 Thallium 0.019/0.025/0.641 0.019U 0.641 U 0.08 0.2
1/7 Vanadium 0.903/5.0 0.903 U 5.0 U 1.61 0.3
0/7 Zinc 2.26/5.0/10.0 2.26 U 10.0 U 4.09 1,000
Notes:
1."µg/L" = micrograms per liter
2."Min." = minimum concentration (µg/L)
3."Max." = maximum concentration (ug/L)
4."Avg." = average concentration (µg/L)
5."2L" and "IMAC" (Interim Maximum Allowable Concentration) are groundwater standards from "North Carolina Administrative Code,
Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater Classifications and Standards,"
DENR (Amended April 1, 2013). The IMAC concentrations listed in Appendix #1 of the 2L.
6."U" is a laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
7."J" is a laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
8."NA" = not applicable
9."# Detections" = number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples collected
during 6 of the 7 sampling events, thus there are 13 total samples representing MW-2R.
10.Grayed cells indicate results above 2L Standard or IMAC.
11.Average concentrations were calculated by summing the constituent detections and dividing by the number of samples. When the sample was
below the MDL, half of the MDL value was used as the result. Some results are estimated (J flagged) and the average concentration is thus estimated.
12.MW-02CD was only sampled in September 2012, March 2015, and September 2015 due to a lack of well recharge during subsequent sampling events.
13.The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-2R (and
MW-2RDUP)
MW-3R
P:\Polk County\Route 9 LF\Analytical & Data\Water\2015\Fall\Tables\Statistics_Background Sept 2015 Page 2 of 2

APPENDICES

APPENDIX A

Sampling Logs and
Equipment Documentation and
Instrument Calibration Data Sheets

APPENDIX B

Report of Laboratory Analysis
and
Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-88227-1
TestAmerica Sample Delivery Group: 75-02
Client Project/Site: Polk County Route 9 Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
10/19/2015 1:50:37 PM
Roxanne Connor, Senior Project Manager
[phone]
[e-mail]
Designee for
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Polk County Route 9 Landfill
TestAmerica Job ID: 490-88227-1
SDG: 75-02
Page 2 of 55 TestAmerica Nashville10/19/2015
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
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Sample Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-88227-1 MW-01CD Water 09/24/15 10:30 09/25/15 10:15
490-88227-2 MW-03CD Water 09/24/15 12:52 09/25/15 10:15
490-88227-3 MW-1R Water 09/22/15 10:21 09/25/15 10:15
490-88227-4 MW-2R Water 09/22/15 14:37 09/25/15 10:15
490-88227-5 MW-2RDUP Water 09/22/15 14:37 09/25/15 10:15
490-88227-6 MW-3R Water 09/24/15 12:03 09/25/15 10:15
490-88227-7 SP-1 Water 09/22/15 13:16 09/25/15 10:15
490-88227-8 SS-1 Water 09/22/15 14:58 09/25/15 10:15
490-88227-9 SS-2 Water 09/22/15 15:14 09/25/15 10:15
490-88227-10 Trip Blank Water 09/22/15 01:00 09/25/15 10:15
490-88227-11 MW-02CD Water 09/22/15 12:03 09/25/15 10:15
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Job ID: 490-88227-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-88227-1
Comments
No additional comments.
Receipt
The samples were received on 9/25/2015 10:15 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 5.3º C.
GC/MS VOA
Method(s) 8260B: The method blank for analytical batch 490-286856 contained Iodomethane above the method detection limit. This
target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not
performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 6020A: The method blank for 490-287860 contained Vanadium above the method detection limit. This target analyte
concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.
Method(s) 6020A: The method blank for 490-289223 contained Vanadium above the method detection limit. This target analyte
concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
B Compound was found in the blank and sample.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 09/24/15 10:30
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 2.73 J 25.0 2.66 ug/L 10/04/15 22:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/04/15 22:07 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/04/15 22:07 1Benzene<0.200
1.00 0.150 ug/L 10/04/15 22:07 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/04/15 22:07 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/04/15 22:07 1Bromoform<0.290
1.00 0.350 ug/L 10/04/15 22:07 1Bromomethane<0.350
50.0 2.64 ug/L 10/04/15 22:07 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/04/15 22:07 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/04/15 22:07 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/04/15 22:07 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/04/15 22:07 1Chloroethane<0.360
1.00 0.230 ug/L 10/04/15 22:07 1Chloroform<0.230
1.00 0.360 ug/L 10/04/15 22:07 1Chloromethane<0.360
1.00 0.210 ug/L 10/04/15 22:07 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/04/15 22:07 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/04/15 22:07 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/04/15 22:07 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/04/15 22:07 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/04/15 22:07 1Dibromomethane<0.450
1.00 0.190 ug/L 10/04/15 22:07 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/04/15 22:07 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/04/15 22:07 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/04/15 22:07 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/04/15 22:07 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/04/15 22:07 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/04/15 22:07 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/04/15 22:07 12-Hexanone <1.28
10.0 1.50 ug/L 10/04/15 22:07 1Iodomethane<1.50
5.00 0.220 ug/L 10/04/15 22:07 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/04/15 22:07 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/04/15 22:07 1Styrene<0.280
1.00 0.150 ug/L 10/04/15 22:07 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/04/15 22:07 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/04/15 22:07 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/04/15 22:07 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/04/15 22:07 1Toluene<0.170
5.00 0.460 ug/L 10/04/15 22:07 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/04/15 22:07 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/04/15 22:07 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/04/15 22:07 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/04/15 22:07 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/04/15 22:07 1Trichloroethene<0.200
1.00 0.210 ug/L 10/04/15 22:07 1Trichlorofluoromethane0.480 J
1.00 0.230 ug/L 10/04/15 22:07 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/04/15 22:07 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/04/15 22:07 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/04/15 22:07 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 09/24/15 10:30
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)96 70-130 10/04/15 22:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 10/04/15 22:07 170-130
1,2-Dichloroethane-d4 (Surr)108 10/04/15 22:07 170-130
Toluene-d8 (Surr)99 10/04/15 22:07 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:00 1Barium0.0475
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:00 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 21:45 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:00 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:00 1Lead0.00670
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:00 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:00 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 21:45 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 10/13/15 10:08 10/13/15 21:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 21:59 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 21:59 1Cobalt1.57 J
2.00 0.200 ug/L 10/13/15 10:08 10/13/15 21:00 1Thallium<0.200
2.00 0.100 ug/L 10/13/15 10:08 10/14/15 13:16 1Vanadium6.09 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 21:59 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-2Client Sample ID: MW-03CD
Matrix: WaterDate Collected: 09/24/15 12:52
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 2.90 J 25.0 2.66 ug/L 10/04/15 22:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/04/15 22:35 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/04/15 22:35 1Benzene<0.200
1.00 0.150 ug/L 10/04/15 22:35 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/04/15 22:35 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/04/15 22:35 1Bromoform<0.290
1.00 0.350 ug/L 10/04/15 22:35 1Bromomethane<0.350
50.0 2.64 ug/L 10/04/15 22:35 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/04/15 22:35 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/04/15 22:35 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/04/15 22:35 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/04/15 22:35 1Chloroethane<0.360
1.00 0.230 ug/L 10/04/15 22:35 1Chloroform<0.230
1.00 0.360 ug/L 10/04/15 22:35 1Chloromethane<0.360
1.00 0.210 ug/L 10/04/15 22:35 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/04/15 22:35 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/04/15 22:35 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/04/15 22:35 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/04/15 22:35 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/04/15 22:35 1Dibromomethane<0.450
1.00 0.190 ug/L 10/04/15 22:35 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/04/15 22:35 11,4-Dichlorobenzene 0.288 J
1.00 0.240 ug/L 10/04/15 22:35 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/04/15 22:35 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/04/15 22:35 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/04/15 22:35 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/04/15 22:35 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/04/15 22:35 12-Hexanone <1.28
10.0 1.50 ug/L 10/04/15 22:35 1Iodomethane<1.50
5.00 0.220 ug/L 10/04/15 22:35 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/04/15 22:35 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/04/15 22:35 1Styrene<0.280
1.00 0.150 ug/L 10/04/15 22:35 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/04/15 22:35 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/04/15 22:35 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/04/15 22:35 1Tetrahydrofuran7.04 J
1.00 0.170 ug/L 10/04/15 22:35 1Toluene<0.170
5.00 0.460 ug/L 10/04/15 22:35 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/04/15 22:35 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/04/15 22:35 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/04/15 22:35 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/04/15 22:35 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/04/15 22:35 1Trichloroethene<0.200
1.00 0.210 ug/L 10/04/15 22:35 1Trichlorofluoromethane0.301 J
1.00 0.230 ug/L 10/04/15 22:35 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/04/15 22:35 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/04/15 22:35 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/04/15 22:35 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-2Client Sample ID: MW-03CD
Matrix: WaterDate Collected: 09/24/15 12:52
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)97 70-130 10/04/15 22:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 10/04/15 22:35 170-130
1,2-Dichloroethane-d4 (Surr)106 10/04/15 22:35 170-130
Toluene-d8 (Surr)100 10/04/15 22:35 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:21 1Barium0.319
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:21 1Cadmium0.000500 J
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:07 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:21 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:21 1Lead0.0105
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:21 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:21 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:07 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 17:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:02 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:02 1Cobalt1.43 J
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 17:20 1Thallium0.384 J
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 16:43 1Vanadium6.83 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:02 1Zinc13.1 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-3Client Sample ID: MW-1R
Matrix: WaterDate Collected: 09/22/15 10:21
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/04/15 23:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/04/15 23:03 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/04/15 23:03 1Benzene<0.200
1.00 0.150 ug/L 10/04/15 23:03 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/04/15 23:03 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/04/15 23:03 1Bromoform<0.290
1.00 0.350 ug/L 10/04/15 23:03 1Bromomethane<0.350
50.0 2.64 ug/L 10/04/15 23:03 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/04/15 23:03 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/04/15 23:03 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/04/15 23:03 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/04/15 23:03 1Chloroethane<0.360
1.00 0.230 ug/L 10/04/15 23:03 1Chloroform<0.230
1.00 0.360 ug/L 10/04/15 23:03 1Chloromethane<0.360
1.00 0.210 ug/L 10/04/15 23:03 1cis-1,2-Dichloroethene 2.00
1.00 0.170 ug/L 10/04/15 23:03 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/04/15 23:03 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/04/15 23:03 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/04/15 23:03 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/04/15 23:03 1Dibromomethane<0.450
1.00 0.190 ug/L 10/04/15 23:03 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/04/15 23:03 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/04/15 23:03 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/04/15 23:03 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/04/15 23:03 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/04/15 23:03 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/04/15 23:03 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/04/15 23:03 12-Hexanone <1.28
10.0 1.50 ug/L 10/04/15 23:03 1Iodomethane<1.50
5.00 0.220 ug/L 10/04/15 23:03 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/04/15 23:03 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/04/15 23:03 1Styrene<0.280
1.00 0.150 ug/L 10/04/15 23:03 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/04/15 23:03 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/04/15 23:03 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/04/15 23:03 1Tetrahydrofuran1.70 J
1.00 0.170 ug/L 10/04/15 23:03 1Toluene<0.170
5.00 0.460 ug/L 10/04/15 23:03 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/04/15 23:03 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/04/15 23:03 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/04/15 23:03 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/04/15 23:03 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/04/15 23:03 1Trichloroethene<0.200
1.00 0.210 ug/L 10/04/15 23:03 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/04/15 23:03 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/04/15 23:03 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/04/15 23:03 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/04/15 23:03 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-3Client Sample ID: MW-1R
Matrix: WaterDate Collected: 09/22/15 10:21
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)98 70-130 10/04/15 23:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 10/04/15 23:03 170-130
1,2-Dichloroethane-d4 (Surr)108 10/04/15 23:03 170-130
Toluene-d8 (Surr)102 10/04/15 23:03 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:26 1Barium0.0607
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:26 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:20 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:26 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:26 1Lead<0.00200
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:26 1Nickel0.00490 J
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:26 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:20 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 17:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:08 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:08 1Cobalt<0.500
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 17:25 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 16:48 1Vanadium1.74 J B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:08 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/04/15 23:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/04/15 23:31 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/04/15 23:31 1Benzene<0.200
1.00 0.150 ug/L 10/04/15 23:31 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/04/15 23:31 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/04/15 23:31 1Bromoform<0.290
1.00 0.350 ug/L 10/04/15 23:31 1Bromomethane<0.350
50.0 2.64 ug/L 10/04/15 23:31 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/04/15 23:31 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/04/15 23:31 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/04/15 23:31 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/04/15 23:31 1Chloroethane<0.360
1.00 0.230 ug/L 10/04/15 23:31 1Chloroform<0.230
1.00 0.360 ug/L 10/04/15 23:31 1Chloromethane<0.360
1.00 0.210 ug/L 10/04/15 23:31 1cis-1,2-Dichloroethene 13.4
1.00 0.170 ug/L 10/04/15 23:31 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/04/15 23:31 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/04/15 23:31 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/04/15 23:31 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/04/15 23:31 1Dibromomethane<0.450
1.00 0.190 ug/L 10/04/15 23:31 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/04/15 23:31 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/04/15 23:31 11,1-Dichloroethane 0.640 J
1.00 0.200 ug/L 10/04/15 23:31 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/04/15 23:31 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/04/15 23:31 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/04/15 23:31 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/04/15 23:31 12-Hexanone <1.28
10.0 1.50 ug/L 10/04/15 23:31 1Iodomethane<1.50
5.00 0.220 ug/L 10/04/15 23:31 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/04/15 23:31 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/04/15 23:31 1Styrene<0.280
1.00 0.150 ug/L 10/04/15 23:31 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/04/15 23:31 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/04/15 23:31 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/04/15 23:31 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/04/15 23:31 1Toluene<0.170
5.00 0.460 ug/L 10/04/15 23:31 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/04/15 23:31 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/04/15 23:31 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/04/15 23:31 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/04/15 23:31 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/04/15 23:31 1Trichloroethene0.928 J
1.00 0.210 ug/L 10/04/15 23:31 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/04/15 23:31 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/04/15 23:31 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/04/15 23:31 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/04/15 23:31 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)96 70-130 10/04/15 23:31 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 10/04/15 23:31 170-130
1,2-Dichloroethane-d4 (Surr)108 10/04/15 23:31 170-130
Toluene-d8 (Surr)100 10/04/15 23:31 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:30 1Barium0.217
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:30 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:25 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:30 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:30 1Lead0.00450 J
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:30 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:30 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:25 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 17:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:13 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:13 1Cobalt<0.500
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 17:42 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:05 1Vanadium2.35 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:13 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/04/15 23:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/04/15 23:58 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/04/15 23:58 1Benzene<0.200
1.00 0.150 ug/L 10/04/15 23:58 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/04/15 23:58 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/04/15 23:58 1Bromoform<0.290
1.00 0.350 ug/L 10/04/15 23:58 1Bromomethane<0.350
50.0 2.64 ug/L 10/04/15 23:58 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/04/15 23:58 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/04/15 23:58 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/04/15 23:58 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/04/15 23:58 1Chloroethane<0.360
1.00 0.230 ug/L 10/04/15 23:58 1Chloroform<0.230
1.00 0.360 ug/L 10/04/15 23:58 1Chloromethane<0.360
1.00 0.210 ug/L 10/04/15 23:58 1cis-1,2-Dichloroethene 13.5
1.00 0.170 ug/L 10/04/15 23:58 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/04/15 23:58 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/04/15 23:58 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/04/15 23:58 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/04/15 23:58 1Dibromomethane<0.450
1.00 0.190 ug/L 10/04/15 23:58 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/04/15 23:58 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/04/15 23:58 11,1-Dichloroethane 0.718 J
1.00 0.200 ug/L 10/04/15 23:58 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/04/15 23:58 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/04/15 23:58 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/04/15 23:58 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/04/15 23:58 12-Hexanone <1.28
10.0 1.50 ug/L 10/04/15 23:58 1Iodomethane<1.50
5.00 0.220 ug/L 10/04/15 23:58 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/04/15 23:58 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/04/15 23:58 1Styrene<0.280
1.00 0.150 ug/L 10/04/15 23:58 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/04/15 23:58 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/04/15 23:58 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/04/15 23:58 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/04/15 23:58 1Toluene<0.170
5.00 0.460 ug/L 10/04/15 23:58 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/04/15 23:58 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/04/15 23:58 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/04/15 23:58 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/04/15 23:58 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/04/15 23:58 1Trichloroethene0.986 J
1.00 0.210 ug/L 10/04/15 23:58 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/04/15 23:58 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/04/15 23:58 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/04/15 23:58 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/04/15 23:58 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)97 70-130 10/04/15 23:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 10/04/15 23:58 170-130
1,2-Dichloroethane-d4 (Surr)105 10/04/15 23:58 170-130
Toluene-d8 (Surr)100 10/04/15 23:58 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:34 1Barium0.212
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:34 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:29 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:34 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:34 1Lead0.00500
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:34 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:34 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:29 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 17:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:30 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:30 1Cobalt<0.500
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 17:59 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:11 1Vanadium2.33 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:30 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 09/24/15 12:03
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/05/15 00:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/05/15 00:26 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/05/15 00:26 1Benzene<0.200
1.00 0.150 ug/L 10/05/15 00:26 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/05/15 00:26 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/05/15 00:26 1Bromoform<0.290
1.00 0.350 ug/L 10/05/15 00:26 1Bromomethane<0.350
50.0 2.64 ug/L 10/05/15 00:26 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/05/15 00:26 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/05/15 00:26 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/05/15 00:26 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/05/15 00:26 1Chloroethane<0.360
1.00 0.230 ug/L 10/05/15 00:26 1Chloroform<0.230
1.00 0.360 ug/L 10/05/15 00:26 1Chloromethane<0.360
1.00 0.210 ug/L 10/05/15 00:26 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/05/15 00:26 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/05/15 00:26 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/05/15 00:26 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/05/15 00:26 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/05/15 00:26 1Dibromomethane<0.450
1.00 0.190 ug/L 10/05/15 00:26 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/05/15 00:26 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/05/15 00:26 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/05/15 00:26 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/05/15 00:26 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/05/15 00:26 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/05/15 00:26 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/05/15 00:26 12-Hexanone <1.28
10.0 1.50 ug/L 10/05/15 00:26 1Iodomethane<1.50
5.00 0.220 ug/L 10/05/15 00:26 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/05/15 00:26 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/05/15 00:26 1Styrene<0.280
1.00 0.150 ug/L 10/05/15 00:26 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/05/15 00:26 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/05/15 00:26 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/05/15 00:26 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/05/15 00:26 1Toluene<0.170
5.00 0.460 ug/L 10/05/15 00:26 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/05/15 00:26 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/05/15 00:26 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/05/15 00:26 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/05/15 00:26 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/05/15 00:26 1Trichloroethene<0.200
1.00 0.210 ug/L 10/05/15 00:26 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/05/15 00:26 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/05/15 00:26 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/05/15 00:26 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/05/15 00:26 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 09/24/15 12:03
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)97 70-130 10/05/15 00:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 10/05/15 00:26 170-130
1,2-Dichloroethane-d4 (Surr)106 10/05/15 00:26 170-130
Toluene-d8 (Surr)100 10/05/15 00:26 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:48 1Barium0.00910 J
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:48 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:33 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:48 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:48 1Lead0.00370 J
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:48 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:48 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:33 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 18:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:36 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:36 1Cobalt<0.500
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 18:04 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:16 1Vanadium2.00 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:36 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 09/22/15 13:16
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 3.99 J 25.0 2.66 ug/L 10/05/15 00:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/05/15 00:54 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/05/15 00:54 1Benzene<0.200
1.00 0.150 ug/L 10/05/15 00:54 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/05/15 00:54 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/05/15 00:54 1Bromoform<0.290
1.00 0.350 ug/L 10/05/15 00:54 1Bromomethane<0.350
50.0 2.64 ug/L 10/05/15 00:54 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/05/15 00:54 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/05/15 00:54 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/05/15 00:54 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/05/15 00:54 1Chloroethane<0.360
1.00 0.230 ug/L 10/05/15 00:54 1Chloroform<0.230
1.00 0.360 ug/L 10/05/15 00:54 1Chloromethane<0.360
1.00 0.210 ug/L 10/05/15 00:54 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/05/15 00:54 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/05/15 00:54 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/05/15 00:54 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/05/15 00:54 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/05/15 00:54 1Dibromomethane<0.450
1.00 0.190 ug/L 10/05/15 00:54 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/05/15 00:54 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/05/15 00:54 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/05/15 00:54 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/05/15 00:54 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/05/15 00:54 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/05/15 00:54 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/05/15 00:54 12-Hexanone <1.28
10.0 1.50 ug/L 10/05/15 00:54 1Iodomethane<1.50
5.00 0.220 ug/L 10/05/15 00:54 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/05/15 00:54 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/05/15 00:54 1Styrene<0.280
1.00 0.150 ug/L 10/05/15 00:54 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/05/15 00:54 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/05/15 00:54 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/05/15 00:54 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/05/15 00:54 1Toluene<0.170
5.00 0.460 ug/L 10/05/15 00:54 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/05/15 00:54 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/05/15 00:54 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/05/15 00:54 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/05/15 00:54 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/05/15 00:54 1Trichloroethene<0.200
1.00 0.210 ug/L 10/05/15 00:54 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/05/15 00:54 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/05/15 00:54 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/05/15 00:54 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/05/15 00:54 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 09/22/15 13:16
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)97 70-130 10/05/15 00:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 10/05/15 00:54 170-130
1,2-Dichloroethane-d4 (Surr)105 10/05/15 00:54 170-130
Toluene-d8 (Surr)101 10/05/15 00:54 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:53 1Barium0.174
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:53 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:38 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:53 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:53 1Lead0.00670
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:53 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:53 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:38 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 18:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:41 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:41 1Cobalt1.48 J
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 18:10 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:22 1Vanadium5.20 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:41 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/29/15 14:25 09/29/15 18:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 09/22/15 14:58
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 3.92 J 25.0 2.66 ug/L 10/05/15 01:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/05/15 01:22 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/05/15 01:22 1Benzene<0.200
1.00 0.150 ug/L 10/05/15 01:22 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/05/15 01:22 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/05/15 01:22 1Bromoform<0.290
1.00 0.350 ug/L 10/05/15 01:22 1Bromomethane<0.350
50.0 2.64 ug/L 10/05/15 01:22 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/05/15 01:22 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/05/15 01:22 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/05/15 01:22 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/05/15 01:22 1Chloroethane<0.360
1.00 0.230 ug/L 10/05/15 01:22 1Chloroform<0.230
1.00 0.360 ug/L 10/05/15 01:22 1Chloromethane<0.360
1.00 0.210 ug/L 10/05/15 01:22 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/05/15 01:22 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/05/15 01:22 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/05/15 01:22 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/05/15 01:22 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/05/15 01:22 1Dibromomethane<0.450
1.00 0.190 ug/L 10/05/15 01:22 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/05/15 01:22 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/05/15 01:22 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/05/15 01:22 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/05/15 01:22 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/05/15 01:22 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/05/15 01:22 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/05/15 01:22 12-Hexanone <1.28
10.0 1.50 ug/L 10/05/15 01:22 1Iodomethane<1.50
5.00 0.220 ug/L 10/05/15 01:22 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/05/15 01:22 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/05/15 01:22 1Styrene<0.280
1.00 0.150 ug/L 10/05/15 01:22 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/05/15 01:22 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/05/15 01:22 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/05/15 01:22 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/05/15 01:22 1Toluene<0.170
5.00 0.460 ug/L 10/05/15 01:22 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/05/15 01:22 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/05/15 01:22 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/05/15 01:22 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/05/15 01:22 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/05/15 01:22 1Trichloroethene<0.200
1.00 0.210 ug/L 10/05/15 01:22 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/05/15 01:22 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/05/15 01:22 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/05/15 01:22 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/05/15 01:22 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 09/22/15 14:58
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)98 70-130 10/05/15 01:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 10/05/15 01:22 170-130
1,2-Dichloroethane-d4 (Surr)110 10/05/15 01:22 170-130
Toluene-d8 (Surr)102 10/05/15 01:22 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 05:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:57 1Barium0.0425
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 05:57 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:42 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:57 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 05:57 1Lead0.00370 J
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 05:57 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 05:57 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:42 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 18:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:47 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:47 1Cobalt<0.500
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 18:16 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:28 1Vanadium2.64 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:47 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 09/22/15 15:14
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 3.98 J 25.0 2.66 ug/L 10/05/15 01:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/05/15 01:50 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/05/15 01:50 1Benzene<0.200
1.00 0.150 ug/L 10/05/15 01:50 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/05/15 01:50 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/05/15 01:50 1Bromoform<0.290
1.00 0.350 ug/L 10/05/15 01:50 1Bromomethane<0.350
50.0 2.64 ug/L 10/05/15 01:50 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/05/15 01:50 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/05/15 01:50 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/05/15 01:50 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/05/15 01:50 1Chloroethane<0.360
1.00 0.230 ug/L 10/05/15 01:50 1Chloroform<0.230
1.00 0.360 ug/L 10/05/15 01:50 1Chloromethane<0.360
1.00 0.210 ug/L 10/05/15 01:50 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/05/15 01:50 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/05/15 01:50 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/05/15 01:50 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/05/15 01:50 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/05/15 01:50 1Dibromomethane<0.450
1.00 0.190 ug/L 10/05/15 01:50 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/05/15 01:50 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/05/15 01:50 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/05/15 01:50 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/05/15 01:50 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/05/15 01:50 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/05/15 01:50 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/05/15 01:50 12-Hexanone <1.28
10.0 1.50 ug/L 10/05/15 01:50 1Iodomethane<1.50
5.00 0.220 ug/L 10/05/15 01:50 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/05/15 01:50 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/05/15 01:50 1Styrene<0.280
1.00 0.150 ug/L 10/05/15 01:50 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/05/15 01:50 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/05/15 01:50 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/05/15 01:50 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/05/15 01:50 1Toluene<0.170
5.00 0.460 ug/L 10/05/15 01:50 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/05/15 01:50 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/05/15 01:50 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/05/15 01:50 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/05/15 01:50 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/05/15 01:50 1Trichloroethene<0.200
1.00 0.210 ug/L 10/05/15 01:50 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/05/15 01:50 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/05/15 01:50 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/05/15 01:50 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/05/15 01:50 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 09/22/15 15:14
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)98 70-130 10/05/15 01:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 10/05/15 01:50 170-130
1,2-Dichloroethane-d4 (Surr)107 10/05/15 01:50 170-130
Toluene-d8 (Surr)101 10/05/15 01:50 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 06:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 06:01 1Barium0.0382
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 06:01 1Cadmium<0.000500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:46 1Chromium<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 06:01 1Copper<0.00500
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 06:01 1Lead0.00370 J
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 06:01 1Nickel<0.00300
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 06:01 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 22:46 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 18:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:52 1Beryllium<0.500
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 20:52 1Cobalt<0.500
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 18:21 1Thallium<0.200
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:33 1Vanadium2.55 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 20:52 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 09/22/15 01:00
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 12.3 J 25.0 2.66 ug/L 10/04/15 19:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/04/15 19:19 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/04/15 19:19 1Benzene<0.200
1.00 0.150 ug/L 10/04/15 19:19 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/04/15 19:19 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/04/15 19:19 1Bromoform<0.290
1.00 0.350 ug/L 10/04/15 19:19 1Bromomethane<0.350
50.0 2.64 ug/L 10/04/15 19:19 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/04/15 19:19 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/04/15 19:19 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/04/15 19:19 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/04/15 19:19 1Chloroethane<0.360
1.00 0.230 ug/L 10/04/15 19:19 1Chloroform<0.230
1.00 0.360 ug/L 10/04/15 19:19 1Chloromethane<0.360
1.00 0.210 ug/L 10/04/15 19:19 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/04/15 19:19 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/04/15 19:19 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/04/15 19:19 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/04/15 19:19 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/04/15 19:19 1Dibromomethane<0.450
1.00 0.190 ug/L 10/04/15 19:19 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/04/15 19:19 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/04/15 19:19 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/04/15 19:19 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/04/15 19:19 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/04/15 19:19 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/04/15 19:19 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/04/15 19:19 12-Hexanone <1.28
10.0 1.50 ug/L 10/04/15 19:19 1Iodomethane<1.50
5.00 0.220 ug/L 10/04/15 19:19 1Methylene Chloride 1.33 J
10.0 0.810 ug/L 10/04/15 19:19 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/04/15 19:19 1Styrene<0.280
1.00 0.150 ug/L 10/04/15 19:19 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/04/15 19:19 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/04/15 19:19 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/04/15 19:19 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/04/15 19:19 1Toluene<0.170
5.00 0.460 ug/L 10/04/15 19:19 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/04/15 19:19 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/04/15 19:19 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/04/15 19:19 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/04/15 19:19 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/04/15 19:19 1Trichloroethene<0.200
1.00 0.210 ug/L 10/04/15 19:19 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/04/15 19:19 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/04/15 19:19 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/04/15 19:19 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/04/15 19:19 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 09/22/15 01:00
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)95 70-130 10/04/15 19:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 10/04/15 19:19 170-130
1,2-Dichloroethane-d4 (Surr)110 10/04/15 19:19 170-130
Toluene-d8 (Surr)100 10/04/15 19:19 170-130
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-11Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 09/22/15 12:03
Date Received: 09/25/15 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/05/15 02:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 10/05/15 02:18 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/05/15 02:18 1Benzene<0.200
1.00 0.150 ug/L 10/05/15 02:18 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/05/15 02:18 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/05/15 02:18 1Bromoform<0.290
1.00 0.350 ug/L 10/05/15 02:18 1Bromomethane<0.350
50.0 2.64 ug/L 10/05/15 02:18 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/05/15 02:18 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/05/15 02:18 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/05/15 02:18 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/05/15 02:18 1Chloroethane<0.360
1.00 0.230 ug/L 10/05/15 02:18 1Chloroform<0.230
1.00 0.360 ug/L 10/05/15 02:18 1Chloromethane<0.360
1.00 0.210 ug/L 10/05/15 02:18 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/05/15 02:18 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/05/15 02:18 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/05/15 02:18 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/05/15 02:18 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/05/15 02:18 1Dibromomethane<0.450
1.00 0.190 ug/L 10/05/15 02:18 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/05/15 02:18 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/05/15 02:18 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/05/15 02:18 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/05/15 02:18 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/05/15 02:18 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/05/15 02:18 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/05/15 02:18 12-Hexanone <1.28
10.0 1.50 ug/L 10/05/15 02:18 1Iodomethane<1.50
5.00 0.220 ug/L 10/05/15 02:18 1Methylene Chloride <0.220
10.0 0.810 ug/L 10/05/15 02:18 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/05/15 02:18 1Styrene<0.280
1.00 0.150 ug/L 10/05/15 02:18 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/05/15 02:18 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/05/15 02:18 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/05/15 02:18 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/05/15 02:18 1Toluene<0.170
5.00 0.460 ug/L 10/05/15 02:18 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/05/15 02:18 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/05/15 02:18 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/05/15 02:18 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/05/15 02:18 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/05/15 02:18 1Trichloroethene<0.200
1.00 0.210 ug/L 10/05/15 02:18 1Trichlorofluoromethane0.281 J
1.00 0.230 ug/L 10/05/15 02:18 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/05/15 02:18 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/05/15 02:18 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/05/15 02:18 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-88227-11Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 09/22/15 12:03
Date Received: 09/25/15 10:15
4-Bromofluorobenzene (Surr)97 70-130 10/05/15 02:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)103 10/05/15 02:18 170-130
1,2-Dichloroethane-d4 (Surr)106 10/05/15 02:18 170-130
Toluene-d8 (Surr)101 10/05/15 02:18 170-130
Method: 6010C - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 06:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 06:55 1Barium0.627
0.00100 0.000500 mg/L 09/28/15 16:55 10/03/15 06:55 1Cadmium0.00150
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 23:00 1Chromium0.00340 J
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 06:55 1Copper0.00500 J
0.00500 0.00200 mg/L 09/28/15 16:55 10/03/15 06:55 1Lead0.0307
0.0100 0.00300 mg/L 09/28/15 16:55 10/03/15 06:55 1Nickel0.00390 J
0.0100 0.00500 mg/L 09/28/15 16:55 10/03/15 06:55 1Selenium<0.00500
0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 23:00 1Silver<0.00300
Method: 6020A - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 16:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 19:34 1Beryllium1.58 J
2.00 0.500 ug/L 09/28/15 16:55 10/03/15 19:34 1Cobalt6.10
2.00 0.200 ug/L 09/28/15 16:55 10/07/15 16:52 1Thallium0.603 J
2.00 0.100 ug/L 10/07/15 18:58 10/08/15 17:39 1Vanadium43.6 B
25.0 10.0 ug/L 09/28/15 16:55 10/03/15 19:34 1Zinc38.8
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-286856/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/04/15 17:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 10/04/15 17:30 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/04/15 17:30 1Benzene
<0.150 0.1501.00 ug/L 10/04/15 17:30 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/04/15 17:30 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/04/15 17:30 1Bromoform
<0.350 0.3501.00 ug/L 10/04/15 17:30 1Bromomethane
<2.64 2.6450.0 ug/L 10/04/15 17:30 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/04/15 17:30 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/04/15 17:30 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/04/15 17:30 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/04/15 17:30 1Chloroethane
<0.230 0.2301.00 ug/L 10/04/15 17:30 1Chloroform
<0.360 0.3601.00 ug/L 10/04/15 17:30 1Chloromethane
<0.210 0.2101.00 ug/L 10/04/15 17:30 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/04/15 17:30 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/04/15 17:30 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/04/15 17:30 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/04/15 17:30 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/04/15 17:30 1Dibromomethane
<0.190 0.1901.00 ug/L 10/04/15 17:30 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/04/15 17:30 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/04/15 17:30 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/04/15 17:30 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/04/15 17:30 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/04/15 17:30 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/04/15 17:30 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/04/15 17:30 12-Hexanone
1.584 J 1.5010.0 ug/L 10/04/15 17:30 1Iodomethane
<0.220 0.2205.00 ug/L 10/04/15 17:30 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/04/15 17:30 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/04/15 17:30 1Styrene
<0.150 0.1501.00 ug/L 10/04/15 17:30 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/04/15 17:30 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/04/15 17:30 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/04/15 17:30 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/04/15 17:30 1Toluene
<0.460 0.4605.00 ug/L 10/04/15 17:30 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/04/15 17:30 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/04/15 17:30 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/04/15 17:30 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/04/15 17:30 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/04/15 17:30 1Trichloroethene
<0.210 0.2101.00 ug/L 10/04/15 17:30 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/04/15 17:30 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/04/15 17:30 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/04/15 17:30 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/04/15 17:30 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-286856/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
4-Bromofluorobenzene (Surr)94 70-130 10/04/15 17:30 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 10/04/15 17:30 1Dibromofluoromethane (Surr)70-130
106 10/04/15 17:30 11,2-Dichloroethane-d4 (Surr)70-130
99 10/04/15 17:30 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-286856/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
Acetone 250 265.7 ug/L 106 54-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 543.4 ug/L 109 61-140
Benzene 50.0 54.00 ug/L 108 80-121
Bromochloromethane 50.0 52.10 ug/L 104 78-129
Bromodichloromethane 50.0 54.69 ug/L 109 75-129
Bromoform 50.0 51.22 ug/L 102 46-145
Bromomethane 50.0 51.31 ug/L 103 41-150
2-Butanone (MEK)250 265.5 ug/L 106 62-133
Carbon disulfide 50.0 54.63 ug/L 109 77-126
Carbon tetrachloride 50.0 53.91 ug/L 108 64-147
Chlorobenzene 50.0 52.78 ug/L 106 80-120
Chloroethane 50.0 53.68 ug/L 107 72-120
Chloroform 50.0 53.99 ug/L 108 73-129
Chloromethane 50.0 49.93 ug/L 100 12-150
cis-1,2-Dichloroethene 50.0 54.86 ug/L 110 76-125
cis-1,3-Dichloropropene 50.0 54.33 ug/L 109 74-140
Dibromochloromethane 50.0 53.30 ug/L 107 69-133
1,2-Dibromo-3-Chloropropane 50.0 53.70 ug/L 107 54-125
1,2-Dibromoethane (EDB)50.0 53.24 ug/L 106 80-129
Dibromomethane 50.0 52.49 ug/L 105 71-125
1,2-Dichlorobenzene 50.0 52.21 ug/L 104 80-121
1,4-Dichlorobenzene 50.0 52.39 ug/L 105 80-120
1,1-Dichloroethane 50.0 54.10 ug/L 108 78-125
1,2-Dichloroethane 50.0 51.58 ug/L 103 77-121
1,1-Dichloroethene 50.0 55.52 ug/L 111 79-124
1,2-Dichloropropane 50.0 53.72 ug/L 107 75-120
Ethylbenzene 50.0 50.83 ug/L 102 80-130
2-Hexanone 250 277.4 ug/L 111 60-142
Iodomethane 50.0 60.95 ug/L 122 40-150
Methylene Chloride 50.0 53.26 ug/L 107 79-123
4-Methyl-2-pentanone (MIBK)250 273.5 ug/L 109 60-137
Styrene 50.0 51.61 ug/L 103 80-127
1,1,1,2-Tetrachloroethane 50.0 52.56 ug/L 105 74-135
1,1,2,2-Tetrachloroethane 50.0 51.30 ug/L 103 69-131
Tetrachloroethene 50.0 53.98 ug/L 108 80-126
Tetrahydrofuran 100 108.0 ug/L 108 51-124
Toluene 50.0 50.93 ug/L 102 80-126
trans-1,4-Dichloro-2-butene 50.0 52.28 ug/L 105 41-147
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-286856/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
trans-1,2-Dichloroethene 50.0 54.03 ug/L 108 79-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
trans-1,3-Dichloropropene 50.0 54.52 ug/L 109 63-134
1,1,1-Trichloroethane 50.0 52.80 ug/L 106 78-135
1,1,2-Trichloroethane 50.0 53.15 ug/L 106 80-124
Trichloroethene 50.0 53.30 ug/L 107 80-123
Trichlorofluoromethane 50.0 54.19 ug/L 108 65-124
1,2,3-Trichloropropane 50.0 50.58 ug/L 101 70-131
Vinyl acetate 100 117.6 ug/L 118 54-139
Vinyl chloride 50.0 55.47 ug/L 111 68-120
Xylenes, Total 100 101.8 ug/L 102 80-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-286856/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
Acetone 250 262.2 ug/L 105 54-145 1 21
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 537.1 ug/L 107 61-140 1 18
Benzene 50.0 53.20 ug/L 106 80-121 2 17
Bromochloromethane 50.0 51.35 ug/L 103 78-129 1 17
Bromodichloromethane 50.0 53.86 ug/L 108 75-129 2 18
Bromoform 50.0 50.57 ug/L 101 46-145 1 16
Bromomethane 50.0 55.06 ug/L 110 41-150 7 50
2-Butanone (MEK)250 271.8 ug/L 109 62-133 2 19
Carbon disulfide 50.0 55.59 ug/L 111 77-126 2 21
Carbon tetrachloride 50.0 53.21 ug/L 106 64-147 1 19
Chlorobenzene 50.0 52.35 ug/L 105 80-120 1 14
Chloroethane 50.0 53.35 ug/L 107 72-120 1 20
Chloroform 50.0 53.30 ug/L 107 73-129 1 18
Chloromethane 50.0 50.98 ug/L 102 12-150 2 31
cis-1,2-Dichloroethene 50.0 53.50 ug/L 107 76-125 3 17
cis-1,3-Dichloropropene 50.0 54.47 ug/L 109 74-140 0 15
Dibromochloromethane 50.0 53.31 ug/L 107 69-133 0 15
1,2-Dibromo-3-Chloropropane 50.0 54.25 ug/L 108 54-125 1 24
1,2-Dibromoethane (EDB)50.0 52.12 ug/L 104 80-129 2 15
Dibromomethane 50.0 52.53 ug/L 105 71-125 0 16
1,2-Dichlorobenzene 50.0 52.56 ug/L 105 80-121 1 15
1,4-Dichlorobenzene 50.0 53.12 ug/L 106 80-120 1 15
1,1-Dichloroethane 50.0 53.44 ug/L 107 78-125 1 17
1,2-Dichloroethane 50.0 52.12 ug/L 104 77-121 1 17
1,1-Dichloroethene 50.0 53.86 ug/L 108 79-124 3 17
1,2-Dichloropropane 50.0 52.04 ug/L 104 75-120 3 17
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-286856/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
Ethylbenzene 50.0 50.42 ug/L 101 80-130 1 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2-Hexanone 250 275.4 ug/L 110 60-142 1 15
Iodomethane 50.0 61.81 ug/L 124 40-150 1 23
Methylene Chloride 50.0 52.76 ug/L 106 79-123 1 17
4-Methyl-2-pentanone (MIBK)250 272.1 ug/L 109 60-137 1 17
Styrene 50.0 50.99 ug/L 102 80-127 1 24
1,1,1,2-Tetrachloroethane 50.0 51.63 ug/L 103 74-135 2 16
1,1,2,2-Tetrachloroethane 50.0 52.38 ug/L 105 69-131 2 20
Tetrachloroethene 50.0 53.67 ug/L 107 80-126 1 16
Tetrahydrofuran 100 112.7 ug/L 113 51-124 4 18
Toluene 50.0 50.41 ug/L 101 80-126 1 15
trans-1,4-Dichloro-2-butene 50.0 53.41 ug/L 107 41-147 2 26
trans-1,2-Dichloroethene 50.0 53.52 ug/L 107 79-126 1 16
trans-1,3-Dichloropropene 50.0 53.94 ug/L 108 63-134 1 14
1,1,1-Trichloroethane 50.0 51.81 ug/L 104 78-135 2 17
1,1,2-Trichloroethane 50.0 52.98 ug/L 106 80-124 0 15
Trichloroethene 50.0 53.39 ug/L 107 80-123 0 17
Trichlorofluoromethane 50.0 53.81 ug/L 108 65-124 1 18
1,2,3-Trichloropropane 50.0 51.36 ug/L 103 70-131 2 19
Vinyl acetate 100 114.1 ug/L 114 54-139 3 21
Vinyl chloride 50.0 55.19 ug/L 110 68-120 1 17
Xylenes, Total 100 100.9 ug/L 101 80-132 1 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
1011,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-87982-B-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
Acetone <2.66 250 217.4 ug/L 87 45-141
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 458.6 ug/L 92 50-148
Benzene <0.200 50.0 51.17 ug/L 102 75-133
Bromochloromethane <0.150 50.0 50.35 ug/L 101 67-139
Bromodichloromethane <0.170 50.0 50.29 ug/L 101 70-140
Bromoform <0.290 50.0 45.03 ug/L 90 42-147
Bromomethane <0.350 50.0 48.11 ug/L 96 16-163
2-Butanone (MEK)<2.64 250 207.3 ug/L 83 50-138
Carbon disulfide <0.220 50.0 52.76 ug/L 106 48-152
Carbon tetrachloride <0.180 50.0 54.85 ug/L 110 62-164
Chlorobenzene <0.180 50.0 50.05 ug/L 100 80-129
Chloroethane <0.360 50.0 52.56 ug/L 105 58-137
Chloroform <0.230 50.0 51.62 ug/L 103 66-138
Chloromethane <0.360 50.0 47.47 ug/L 95 10-169
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-87982-B-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
cis-1,2-Dichloroethene <0.210 50.0 50.30 ug/L 101 68-138
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
cis-1,3-Dichloropropene <0.170 50.0 51.59 ug/L 103 71-141
Dibromochloromethane <0.250 50.0 48.39 ug/L 97 66-140
1,2-Dibromo-3-Chloropropane <0.940 50.0 43.64 ug/L 87 52-126
1,2-Dibromoethane (EDB)<0.210 50.0 47.40 ug/L 95 75-137
Dibromomethane <0.450 50.0 49.33 ug/L 99 58-140
1,2-Dichlorobenzene <0.190 50.0 48.04 ug/L 96 79-128
1,4-Dichlorobenzene <0.170 50.0 49.41 ug/L 99 78-126
1,1-Dichloroethane <0.240 50.0 51.38 ug/L 103 71-139
1,2-Dichloroethane <0.200 50.0 48.64 ug/L 97 64-136
1,1-Dichloroethene <0.250 50.0 53.70 ug/L 107 70-142
1,2-Dichloropropane <0.250 50.0 48.98 ug/L 98 67-131
Ethylbenzene <0.190 50.0 49.09 ug/L 98 79-139
2-Hexanone <1.28 250 218.0 ug/L 87 50-150
Iodomethane <1.50 50.0 54.82 ug/L 110 34-191
Methylene Chloride <0.220 50.0 48.83 ug/L 98 64-139
4-Methyl-2-pentanone (MIBK)<0.810 250 221.0 ug/L 88 50-147
Styrene <0.280 50.0 48.91 ug/L 98 61-148
1,1,1,2-Tetrachloroethane <0.150 50.0 49.58 ug/L 99 73-141
1,1,2,2-Tetrachloroethane <0.190 50.0 43.75 ug/L 88 56-143
Tetrachloroethene <0.140 50.0 53.71 ug/L 107 72-145
Tetrahydrofuran 4.42 J F2 100 85.49 ug/L 81 34-133
Toluene <0.170 50.0 49.83 ug/L 100 75-136
trans-1,4-Dichloro-2-butene <0.460 50.0 43.76 ug/L 88 29-156
trans-1,2-Dichloroethene <0.230 50.0 52.24 ug/L 104 66-143
trans-1,3-Dichloropropene <0.170 50.0 49.87 ug/L 100 59-135
1,1,1-Trichloroethane <0.190 50.0 52.57 ug/L 105 76-149
1,1,2-Trichloroethane <0.190 50.0 48.68 ug/L 97 74-134
Trichloroethene <0.200 50.0 52.27 ug/L 105 73-144
Trichlorofluoromethane <0.210 50.0 55.02 ug/L 110 58-139
1,2,3-Trichloropropane <0.230 50.0 43.47 ug/L 87 53-144
Vinyl acetate <1.71 100 99.89 ug/L 100 37-154
Vinyl chloride <0.180 50.0 53.85 ug/L 108 56-129
Xylenes, Total <0.580 100 97.33 ug/L 97 74-141
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
MS MS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-87982-C-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
Acetone <2.66 250 241.9 ug/L 97 45-141 11 21
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 492.1 ug/L 98 50-148 7 18
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-87982-C-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
Benzene <0.200 50.0 51.59 ug/L 103 75-133 1 17
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromochloromethane <0.150 50.0 50.51 ug/L 101 67-139 0 17
Bromodichloromethane <0.170 50.0 52.73 ug/L 105 70-140 5 18
Bromoform <0.290 50.0 46.94 ug/L 94 42-147 4 16
Bromomethane <0.350 50.0 52.36 ug/L 105 16-163 8 50
2-Butanone (MEK)<2.64 250 234.3 ug/L 94 50-138 12 19
Carbon disulfide <0.220 50.0 53.41 ug/L 107 48-152 1 21
Carbon tetrachloride <0.180 50.0 55.03 ug/L 110 62-164 0 19
Chlorobenzene <0.180 50.0 50.58 ug/L 101 80-129 1 14
Chloroethane <0.360 50.0 53.81 ug/L 108 58-137 2 20
Chloroform <0.230 50.0 53.07 ug/L 106 66-138 3 18
Chloromethane <0.360 50.0 50.58 ug/L 101 10-169 6 31
cis-1,2-Dichloroethene <0.210 50.0 52.78 ug/L 106 68-138 5 17
cis-1,3-Dichloropropene <0.170 50.0 51.04 ug/L 102 71-141 1 15
Dibromochloromethane <0.250 50.0 49.33 ug/L 99 66-140 2 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 47.12 ug/L 94 52-126 8 24
1,2-Dibromoethane (EDB)<0.210 50.0 48.73 ug/L 97 75-137 3 15
Dibromomethane <0.450 50.0 50.57 ug/L 101 58-140 2 16
1,2-Dichlorobenzene <0.190 50.0 48.94 ug/L 98 79-128 2 15
1,4-Dichlorobenzene <0.170 50.0 49.66 ug/L 99 78-126 0 15
1,1-Dichloroethane <0.240 50.0 52.46 ug/L 105 71-139 2 17
1,2-Dichloroethane <0.200 50.0 50.87 ug/L 102 64-136 4 17
1,1-Dichloroethene <0.250 50.0 54.97 ug/L 110 70-142 2 17
1,2-Dichloropropane <0.250 50.0 51.22 ug/L 102 67-131 4 17
Ethylbenzene <0.190 50.0 49.48 ug/L 99 79-139 1 15
2-Hexanone <1.28 250 238.9 ug/L 96 50-150 9 15
Iodomethane <1.50 50.0 56.58 ug/L 113 34-191 3 23
Methylene Chloride <0.220 50.0 51.01 ug/L 102 64-139 4 17
4-Methyl-2-pentanone (MIBK)<0.810 250 239.7 ug/L 96 50-147 8 17
Styrene <0.280 50.0 49.35 ug/L 99 61-148 1 24
1,1,1,2-Tetrachloroethane <0.150 50.0 49.51 ug/L 99 73-141 0 16
1,1,2,2-Tetrachloroethane <0.190 50.0 46.93 ug/L 94 56-143 7 20
Tetrachloroethene <0.140 50.0 53.55 ug/L 107 72-145 0 16
Tetrahydrofuran 4.42 J F2 100 104.5 F2 ug/L 100 34-133 20 18
Toluene <0.170 50.0 49.39 ug/L 99 75-136 1 15
trans-1,4-Dichloro-2-butene <0.460 50.0 46.04 ug/L 92 29-156 5 26
trans-1,2-Dichloroethene <0.230 50.0 53.87 ug/L 108 66-143 3 16
trans-1,3-Dichloropropene <0.170 50.0 49.83 ug/L 100 59-135 0 14
1,1,1-Trichloroethane <0.190 50.0 52.79 ug/L 106 76-149 0 17
1,1,2-Trichloroethane <0.190 50.0 49.23 ug/L 98 74-134 1 15
Trichloroethene <0.200 50.0 52.41 ug/L 105 73-144 0 17
Trichlorofluoromethane <0.210 50.0 56.15 ug/L 112 58-139 2 18
1,2,3-Trichloropropane <0.230 50.0 45.80 ug/L 92 53-144 5 19
Vinyl acetate <1.71 100 107.6 ug/L 108 37-154 7 21
Vinyl chloride <0.180 50.0 54.57 ug/L 109 56-129 1 17
Xylenes, Total <0.580 100 98.20 ug/L 98 74-141 1 15
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-87982-C-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286856
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
MSD MSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
1021,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Method: 6010C - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-285108/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286661 Prep Batch: 285108
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 09/28/15 16:55 10/03/15 04:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00500 0.005000.0100 mg/L 09/28/15 16:55 10/03/15 04:38 1Barium
<0.000500 0.0005000.00100 mg/L 09/28/15 16:55 10/03/15 04:38 1Cadmium
<0.00500 0.005000.0100 mg/L 09/28/15 16:55 10/03/15 04:38 1Copper
<0.00200 0.002000.00500 mg/L 09/28/15 16:55 10/03/15 04:38 1Lead
<0.00300 0.003000.0100 mg/L 09/28/15 16:55 10/03/15 04:38 1Nickel
<0.00500 0.005000.0100 mg/L 09/28/15 16:55 10/03/15 04:38 1Selenium
Client Sample ID: Method BlankLab Sample ID: MB 490-285108/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287190 Prep Batch: 285108
RL MDL
Chromium <0.00300 0.00500 0.00300 mg/L 09/28/15 16:55 10/05/15 21:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00300 0.003000.00500 mg/L 09/28/15 16:55 10/05/15 21:32 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-285108/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286661 Prep Batch: 285108
Arsenic 0.0500 0.04510 mg/L 90 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.046 mg/L 102 80-120
Cadmium 0.0500 0.05050 mg/L 101 80-120
Copper 0.250 0.2415 mg/L 97 80-120
Lead 0.0500 0.05090 mg/L 102 80-120
Nickel 0.500 0.5185 mg/L 104 80-120
Selenium 0.0500 0.05230 mg/L 105 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-285108/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287190 Prep Batch: 285108
Chromium 0.200 0.1930 mg/L 97 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Silver 0.0500 0.04020 mg/L 80 80-120
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 6010C - Metals (ICP) (Continued)
Client Sample ID: MW-01CDLab Sample ID: 490-88227-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286661 Prep Batch: 285108
Arsenic <0.00860 0.0500 0.05000 mg/L 100 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0475 2.00 2.130 mg/L 104 75-125
Cadmium <0.000500 0.0500 0.05240 mg/L 105 75-125
Copper <0.00500 0.250 0.2481 mg/L 99 75-125
Lead 0.00670 0.0500 0.05890 mg/L 104 75-125
Nickel <0.00300 0.500 0.5226 mg/L 105 75-125
Selenium <0.00500 0.0500 0.05420 mg/L 108 75-125
Client Sample ID: MW-01CDLab Sample ID: 490-88227-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287190 Prep Batch: 285108
Chromium <0.00300 0.200 0.1972 mg/L 99 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Silver <0.00300 0.0500 0.04010 mg/L 80 75-125
Client Sample ID: MW-01CDLab Sample ID: 490-88227-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 286661 Prep Batch: 285108
Arsenic <0.00860 0.0500 0.04900 mg/L 98 75-125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0475 2.00 2.139 mg/L 105 75-125 0 20
Cadmium <0.000500 0.0500 0.05270 mg/L 105 75-125 1 20
Copper <0.00500 0.250 0.2486 mg/L 99 75-125 0 20
Lead 0.00670 0.0500 0.06040 mg/L 107 75-125 3 20
Nickel <0.00300 0.500 0.5245 mg/L 105 75-125 0 20
Selenium <0.00500 0.0500 0.05380 mg/L 108 75-125 1 20
Client Sample ID: MW-01CDLab Sample ID: 490-88227-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287190 Prep Batch: 285108
Chromium <0.00300 0.200 0.1966 mg/L 98 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Silver <0.00300 0.0500 0.04070 mg/L 81 75-125 1 20
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-285109/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287131 Prep Batch: 285109
RL MDL
Beryllium <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/03/15 19:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.5002.00 ug/L 09/28/15 16:55 10/03/15 19:23 1Cobalt
<10.0 10.025.0 ug/L 09/28/15 16:55 10/03/15 19:23 1Zinc
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-285109/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287893 Prep Batch: 285109
RL MDL
Antimony <0.500 2.00 0.500 ug/L 09/28/15 16:55 10/07/15 16:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.200 0.2002.00 ug/L 09/28/15 16:55 10/07/15 16:40 1Thallium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-285109/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287131 Prep Batch: 285109
Beryllium 100 117.0 ug/L 117 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Cobalt 100 111.3 ug/L 111 80-120
Zinc 100 106.4 ug/L 106 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-285109/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287893 Prep Batch: 285109
Antimony 100 102.8 ug/L 103 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Thallium 100 109.8 ug/L 110 80-120
Client Sample ID: MW-02CDLab Sample ID: 490-88227-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287131 Prep Batch: 285109
Beryllium 1.58 J 100 94.83 ug/L 93 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Cobalt 6.10 100 99.84 ug/L 94 75-125
Zinc 38.8 100 128.6 ug/L 90 75-125
Client Sample ID: MW-02CDLab Sample ID: 490-88227-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287893 Prep Batch: 285109
Antimony <0.500 100 96.81 ug/L 97 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Thallium 0.603 J 100 97.01 ug/L 96 75-125
Client Sample ID: MW-02CDLab Sample ID: 490-88227-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287131 Prep Batch: 285109
Beryllium 1.58 J 100 97.85 ug/L 96 75-125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Cobalt 6.10 100 100.1 ug/L 94 75-125 0 20
Zinc 38.8 100 127.4 ug/L 89 75-125 1 20
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: MW-02CDLab Sample ID: 490-88227-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 287893 Prep Batch: 285109
Antimony <0.500 100 94.64 ug/L 95 75-125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Thallium 0.603 J 100 97.40 ug/L 97 75-125 0 20
Client Sample ID: Method BlankLab Sample ID: MB 490-287860/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 288266 Prep Batch: 287860
RL MDL
Vanadium 1.252 J 2.00 0.100 ug/L 10/07/15 18:58 10/08/15 15:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-287860/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 288266 Prep Batch: 287860
Vanadium 100 98.09 ug/L 98 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-287860/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 288266 Prep Batch: 287860
Vanadium 100 99.29 ug/L 99 80-120 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-88778-A-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 288266 Prep Batch: 287860
Vanadium 1.27 J B 100 96.51 ug/L 95 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-88778-A-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 288266 Prep Batch: 287860
Vanadium 1.27 J B 100 96.68 ug/L 95 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-289223/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 289652 Prep Batch: 289223
RL MDL
Antimony <0.500 2.00 0.500 ug/L 10/13/15 10:08 10/13/15 19:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.200 0.2002.00 ug/L 10/13/15 10:08 10/13/15 19:48 1Thallium
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-289223/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 290561 Prep Batch: 289223
RL MDL
Vanadium 1.610 J 2.00 0.100 ug/L 10/13/15 10:08 10/16/15 13:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-289223/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 289652 Prep Batch: 289223
Antimony 100 99.88 ug/L 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Thallium 100 96.72 ug/L 97 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-289223/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 290125 Prep Batch: 289223
Vanadium 100 104.2 ug/L 104 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-89389-E-9-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 289652 Prep Batch: 289223
Antimony 0.831 J 100 102.7 ug/L 102 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Thallium <0.200 100 95.79 ug/L 96 75-125
Client Sample ID: Matrix SpikeLab Sample ID: 490-89389-E-9-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 290125 Prep Batch: 289223
Vanadium 6.00 B 100 108.8 ug/L 103 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-89389-E-9-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 289652 Prep Batch: 289223
Antimony 0.831 J 100 106.2 ug/L 105 75-125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Thallium <0.200 100 97.83 ug/L 98 75-125 2 20
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-89389-E-9-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 290125 Prep Batch: 289223
Vanadium 6.00 B 100 110.2 ug/L 104 75-125 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-285096/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285154 Prep Batch: 285096
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/28/15 15:25 09/29/15 01:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-285096/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285154 Prep Batch: 285096
Mercury 1.00 0.9547 ug/L 95 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-01CDLab Sample ID: 490-88227-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285154 Prep Batch: 285096
Mercury <0.150 1.00 1.000 ug/L 100 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-01CDLab Sample ID: 490-88227-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285154 Prep Batch: 285096
Mercury <0.150 1.00 0.9209 ug/L 92 75-125 8 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-285311/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285628 Prep Batch: 285311
RL MDL
Mercury <0.150 0.200 0.150 ug/L 09/29/15 14:25 09/29/15 17:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-285311/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285628 Prep Batch: 285311
Mercury 1.00 0.9596 ug/L 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-88139-D-2-D MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285628 Prep Batch: 285311
Mercury <0.150 F1 1.00 1.144 ug/L 114 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-88139-D-2-E MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 285628 Prep Batch: 285311
Mercury <0.150 F1 1.00 1.342 F1 ug/L 134 75-125 16 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
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QC Association Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
GC/MS VOA
Analysis Batch: 286856
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-87982-B-5 MS Matrix Spike Total/NA
Water 8260B490-87982-C-5 MSD Matrix Spike Duplicate Total/NA
Water 8260B490-88227-1 MW-01CD Total/NA
Water 8260B490-88227-2 MW-03CD Total/NA
Water 8260B490-88227-3 MW-1R Total/NA
Water 8260B490-88227-4 MW-2R Total/NA
Water 8260B490-88227-5 MW-2RDUP Total/NA
Water 8260B490-88227-6 MW-3R Total/NA
Water 8260B490-88227-7 SP-1 Total/NA
Water 8260B490-88227-8 SS-1 Total/NA
Water 8260B490-88227-9 SS-2 Total/NA
Water 8260B490-88227-10 Trip Blank Total/NA
Water 8260B490-88227-11 MW-02CD Total/NA
Water 8260BLCS 490-286856/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-286856/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-286856/7 Method Blank Total/NA
Metals
Prep Batch: 285096
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-88227-1 MW-01CD Total/NA
Water 7470A490-88227-1 MS MW-01CD Total/NA
Water 7470A490-88227-1 MSD MW-01CD Total/NA
Water 7470A490-88227-2 MW-03CD Total/NA
Water 7470A490-88227-3 MW-1R Total/NA
Water 7470A490-88227-4 MW-2R Total/NA
Water 7470A490-88227-5 MW-2RDUP Total/NA
Water 7470A490-88227-6 MW-3R Total/NA
Water 7470A490-88227-8 SS-1 Total/NA
Water 7470A490-88227-9 SS-2 Total/NA
Water 7470A490-88227-11 MW-02CD Total/NA
Water 7470ALCS 490-285096/2-A Lab Control Sample Total/NA
Water 7470AMB 490-285096/1-A Method Blank Total/NA
Prep Batch: 285108
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-88227-1 MW-01CD Total/NA
Water 3010A490-88227-1 MS MW-01CD Total/NA
Water 3010A490-88227-1 MSD MW-01CD Total/NA
Water 3010A490-88227-2 MW-03CD Total/NA
Water 3010A490-88227-3 MW-1R Total/NA
Water 3010A490-88227-4 MW-2R Total/NA
Water 3010A490-88227-5 MW-2RDUP Total/NA
Water 3010A490-88227-6 MW-3R Total/NA
Water 3010A490-88227-7 SP-1 Total/NA
Water 3010A490-88227-8 SS-1 Total/NA
Water 3010A490-88227-9 SS-2 Total/NA
Water 3010A490-88227-11 MW-02CD Total/NA
Water 3010ALCS 490-285108/2-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 285108 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010AMB 490-285108/1-A Method Blank Total/NA
Prep Batch: 285109
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-88227-1 MW-01CD Total/NA
Water 3010A490-88227-2 MW-03CD Total/NA
Water 3010A490-88227-3 MW-1R Total/NA
Water 3010A490-88227-4 MW-2R Total/NA
Water 3010A490-88227-5 MW-2RDUP Total/NA
Water 3010A490-88227-6 MW-3R Total/NA
Water 3010A490-88227-7 SP-1 Total/NA
Water 3010A490-88227-8 SS-1 Total/NA
Water 3010A490-88227-9 SS-2 Total/NA
Water 3010A490-88227-11 MW-02CD Total/NA
Water 3010A490-88227-11 MS MW-02CD Total/NA
Water 3010A490-88227-11 MSD MW-02CD Total/NA
Water 3010ALCS 490-285109/2-A Lab Control Sample Total/NA
Water 3010AMB 490-285109/1-A Method Blank Total/NA
Analysis Batch: 285154
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 285096490-88227-1 MW-01CD Total/NA
Water 7470A 285096490-88227-1 MS MW-01CD Total/NA
Water 7470A 285096490-88227-1 MSD MW-01CD Total/NA
Water 7470A 285096490-88227-2 MW-03CD Total/NA
Water 7470A 285096490-88227-3 MW-1R Total/NA
Water 7470A 285096490-88227-4 MW-2R Total/NA
Water 7470A 285096490-88227-5 MW-2RDUP Total/NA
Water 7470A 285096490-88227-6 MW-3R Total/NA
Water 7470A 285096490-88227-8 SS-1 Total/NA
Water 7470A 285096490-88227-9 SS-2 Total/NA
Water 7470A 285096490-88227-11 MW-02CD Total/NA
Water 7470A 285096LCS 490-285096/2-A Lab Control Sample Total/NA
Water 7470A 285096MB 490-285096/1-A Method Blank Total/NA
Prep Batch: 285311
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-88139-D-2-D MS Matrix Spike Total/NA
Water 7470A490-88139-D-2-E MSD Matrix Spike Duplicate Total/NA
Water 7470A490-88227-7 SP-1 Total/NA
Water 7470ALCS 490-285311/2-A Lab Control Sample Total/NA
Water 7470AMB 490-285311/1-A Method Blank Total/NA
Analysis Batch: 285628
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 285311490-88139-D-2-D MS Matrix Spike Total/NA
Water 7470A 285311490-88139-D-2-E MSD Matrix Spike Duplicate Total/NA
Water 7470A 285311490-88227-7 SP-1 Total/NA
Water 7470A 285311LCS 490-285311/2-A Lab Control Sample Total/NA
Water 7470A 285311MB 490-285311/1-A Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Analysis Batch: 286661
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010C 285108490-88227-1 MW-01CD Total/NA
Water 6010C 285108490-88227-1 MS MW-01CD Total/NA
Water 6010C 285108490-88227-1 MSD MW-01CD Total/NA
Water 6010C 285108490-88227-2 MW-03CD Total/NA
Water 6010C 285108490-88227-3 MW-1R Total/NA
Water 6010C 285108490-88227-4 MW-2R Total/NA
Water 6010C 285108490-88227-5 MW-2RDUP Total/NA
Water 6010C 285108490-88227-6 MW-3R Total/NA
Water 6010C 285108490-88227-7 SP-1 Total/NA
Water 6010C 285108490-88227-8 SS-1 Total/NA
Water 6010C 285108490-88227-9 SS-2 Total/NA
Water 6010C 285108490-88227-11 MW-02CD Total/NA
Water 6010C 285108LCS 490-285108/2-A Lab Control Sample Total/NA
Water 6010C 285108MB 490-285108/1-A Method Blank Total/NA
Analysis Batch: 287131
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 285109490-88227-1 MW-01CD Total/NA
Water 6020A 285109490-88227-2 MW-03CD Total/NA
Water 6020A 285109490-88227-3 MW-1R Total/NA
Water 6020A 285109490-88227-4 MW-2R Total/NA
Water 6020A 285109490-88227-5 MW-2RDUP Total/NA
Water 6020A 285109490-88227-6 MW-3R Total/NA
Water 6020A 285109490-88227-7 SP-1 Total/NA
Water 6020A 285109490-88227-8 SS-1 Total/NA
Water 6020A 285109490-88227-9 SS-2 Total/NA
Water 6020A 285109490-88227-11 MW-02CD Total/NA
Water 6020A 285109490-88227-11 MS MW-02CD Total/NA
Water 6020A 285109490-88227-11 MSD MW-02CD Total/NA
Water 6020A 285109LCS 490-285109/2-A Lab Control Sample Total/NA
Water 6020A 285109MB 490-285109/1-A Method Blank Total/NA
Analysis Batch: 287190
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010C 285108490-88227-1 MW-01CD Total/NA
Water 6010C 285108490-88227-1 MS MW-01CD Total/NA
Water 6010C 285108490-88227-1 MSD MW-01CD Total/NA
Water 6010C 285108490-88227-2 MW-03CD Total/NA
Water 6010C 285108490-88227-3 MW-1R Total/NA
Water 6010C 285108490-88227-4 MW-2R Total/NA
Water 6010C 285108490-88227-5 MW-2RDUP Total/NA
Water 6010C 285108490-88227-6 MW-3R Total/NA
Water 6010C 285108490-88227-7 SP-1 Total/NA
Water 6010C 285108490-88227-8 SS-1 Total/NA
Water 6010C 285108490-88227-9 SS-2 Total/NA
Water 6010C 285108490-88227-11 MW-02CD Total/NA
Water 6010C 285108LCS 490-285108/2-A Lab Control Sample Total/NA
Water 6010C 285108MB 490-285108/1-A Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 287860
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-88227-2 MW-03CD Total/NA
Water 3010A490-88227-3 MW-1R Total/NA
Water 3010A490-88227-4 MW-2R Total/NA
Water 3010A490-88227-5 MW-2RDUP Total/NA
Water 3010A490-88227-6 MW-3R Total/NA
Water 3010A490-88227-7 SP-1 Total/NA
Water 3010A490-88227-8 SS-1 Total/NA
Water 3010A490-88227-9 SS-2 Total/NA
Water 3010A490-88227-11 MW-02CD Total/NA
Water 3010A490-88778-A-1-B MS Matrix Spike Total/NA
Water 3010A490-88778-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 3010ALCS 490-287860/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-287860/3-A Lab Control Sample Dup Total/NA
Water 3010AMB 490-287860/1-A Method Blank Total/NA
Analysis Batch: 287893
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 285109490-88227-2 MW-03CD Total/NA
Water 6020A 285109490-88227-3 MW-1R Total/NA
Water 6020A 285109490-88227-4 MW-2R Total/NA
Water 6020A 285109490-88227-5 MW-2RDUP Total/NA
Water 6020A 285109490-88227-6 MW-3R Total/NA
Water 6020A 285109490-88227-7 SP-1 Total/NA
Water 6020A 285109490-88227-8 SS-1 Total/NA
Water 6020A 285109490-88227-9 SS-2 Total/NA
Water 6020A 285109490-88227-11 MW-02CD Total/NA
Water 6020A 285109490-88227-11 MS MW-02CD Total/NA
Water 6020A 285109490-88227-11 MSD MW-02CD Total/NA
Water 6020A 285109LCS 490-285109/2-A Lab Control Sample Total/NA
Water 6020A 285109MB 490-285109/1-A Method Blank Total/NA
Analysis Batch: 288266
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 287860490-88227-2 MW-03CD Total/NA
Water 6020A 287860490-88227-3 MW-1R Total/NA
Water 6020A 287860490-88227-4 MW-2R Total/NA
Water 6020A 287860490-88227-5 MW-2RDUP Total/NA
Water 6020A 287860490-88227-6 MW-3R Total/NA
Water 6020A 287860490-88227-7 SP-1 Total/NA
Water 6020A 287860490-88227-8 SS-1 Total/NA
Water 6020A 287860490-88227-9 SS-2 Total/NA
Water 6020A 287860490-88227-11 MW-02CD Total/NA
Water 6020A 287860490-88778-A-1-B MS Matrix Spike Total/NA
Water 6020A 287860490-88778-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 6020A 287860LCS 490-287860/2-A Lab Control Sample Total/NA
Water 6020A 287860LCSD 490-287860/3-A Lab Control Sample Dup Total/NA
Water 6020A 287860MB 490-287860/1-A Method Blank Total/NA
Prep Batch: 289223
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-88227-1 MW-01CD Total/NA
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QC Association Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 289223 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-89389-E-9-B MS Matrix Spike Total/NA
Water 3010A490-89389-E-9-C MSD Matrix Spike Duplicate Total/NA
Water 3010ALCS 490-289223/2-A Lab Control Sample Total/NA
Water 3010AMB 490-289223/1-A Method Blank Total/NA
Analysis Batch: 289652
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 289223490-88227-1 MW-01CD Total/NA
Water 6020A 289223490-89389-E-9-B MS Matrix Spike Total/NA
Water 6020A 289223490-89389-E-9-C MSD Matrix Spike Duplicate Total/NA
Water 6020A 289223LCS 490-289223/2-A Lab Control Sample Total/NA
Water 6020A 289223MB 490-289223/1-A Method Blank Total/NA
Analysis Batch: 290125
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 289223490-88227-1 MW-01CD Total/NA
Water 6020A 289223490-89389-E-9-B MS Matrix Spike Total/NA
Water 6020A 289223490-89389-E-9-C MSD Matrix Spike Duplicate Total/NA
Water 6020A 289223LCS 490-289223/2-A Lab Control Sample Total/NA
Analysis Batch: 290561
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020A 289223MB 490-289223/1-A Method Blank Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Client Sample ID: MW-01CD Lab Sample ID: 490-88227-1
Matrix: WaterDate Collected: 09/24/15 10:30
Date Received: 09/25/15 10:15
Analysis 8260B AK110/04/15 22:071 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:00 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 21:45 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 21:59 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 289223 10/13/15 10:08 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 289652 10/13/15 21:00 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 289223 10/13/15 10:08 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 290125 10/14/15 13:16 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:14 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-03CD Lab Sample ID: 490-88227-2
Matrix: WaterDate Collected: 09/24/15 12:52
Date Received: 09/25/15 10:15
Analysis 8260B AK110/04/15 22:351 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:21 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:07 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:02 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 17:20 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 16:43 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:22 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-1R Lab Sample ID: 490-88227-3
Matrix: WaterDate Collected: 09/22/15 10:21
Date Received: 09/25/15 10:15
Analysis 8260B AK110/04/15 23:031 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:26 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:20 BLG TAL NSHTotal/NA 50 mL 50 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Client Sample ID: MW-1R Lab Sample ID: 490-88227-3
Matrix: WaterDate Collected: 09/22/15 10:21
Date Received: 09/25/15 10:15
Prep 3010A ZLN09/28/15 16:55 TAL NSH285109
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:08 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 17:25 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 16:48 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:24 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-2R Lab Sample ID: 490-88227-4
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
Analysis 8260B AK110/04/15 23:311 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:30 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:25 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:13 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 17:42 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 17:05 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:26 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-2RDUP Lab Sample ID: 490-88227-5
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
Analysis 8260B AK110/04/15 23:581 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:34 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:29 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:30 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 17:59 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Client Sample ID: MW-2RDUP Lab Sample ID: 490-88227-5
Matrix: WaterDate Collected: 09/22/15 14:37
Date Received: 09/25/15 10:15
Analysis 6020A CME10/08/15 17:111 TAL NSH288266
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:29 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: MW-3R Lab Sample ID: 490-88227-6
Matrix: WaterDate Collected: 09/24/15 12:03
Date Received: 09/25/15 10:15
Analysis 8260B AK110/05/15 00:261 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:48 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:33 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:36 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 18:04 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 17:16 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:36 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SP-1 Lab Sample ID: 490-88227-7
Matrix: WaterDate Collected: 09/22/15 13:16
Date Received: 09/25/15 10:15
Analysis 8260B AK110/05/15 00:541 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:53 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:38 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:41 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 18:10 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 17:22 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285311 09/29/15 14:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285628 09/29/15 18:02 NJB TAL NSHTotal/NA 30 mL 30 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Client Sample ID: SS-1 Lab Sample ID: 490-88227-8
Matrix: WaterDate Collected: 09/22/15 14:58
Date Received: 09/25/15 10:15
Analysis 8260B AK110/05/15 01:221 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 05:57 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:42 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:47 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 18:16 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 17:28 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:41 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: SS-2 Lab Sample ID: 490-88227-9
Matrix: WaterDate Collected: 09/22/15 15:14
Date Received: 09/25/15 10:15
Analysis 8260B AK110/05/15 01:501 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 06:01 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 22:46 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 20:52 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 18:21 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 17:33 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:43 NJB TAL NSHTotal/NA 30 mL 30 mL
Client Sample ID: Trip Blank Lab Sample ID: 490-88227-10
Matrix: WaterDate Collected: 09/22/15 01:00
Date Received: 09/25/15 10:15
Analysis 8260B AK110/04/15 19:191 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
TestAmerica Nashville
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Client Sample ID: MW-02CD Lab Sample ID: 490-88227-11
Matrix: WaterDate Collected: 09/22/15 12:03
Date Received: 09/25/15 10:15
Analysis 8260B AK110/05/15 02:181 TAL NSH286856
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 286661 10/03/15 06:55 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285108 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010C 1 287190 10/05/15 23:00 BLG TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287131 10/03/15 19:34 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 285109 09/28/15 16:55 ZLN TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 287893 10/07/15 16:52 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 287860 10/07/15 18:58 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020A 1 288266 10/08/15 17:39 CME TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 285096 09/28/15 15:25 NJB TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 285154 09/29/15 01:46 NJB TAL NSHTotal/NA 30 mL 30 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-88227-1Client: Altamont Environmental, Inc.
SDG: 75-02Project/Site: Polk County Route 9 Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010CMetals (ICP)TAL NSH
SW8466020AMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-88227-1
Project/Site: Polk County Route 9 Landfill SDG: 75-02
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-15
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-88227-1
SDG Number: 75-02
Login Number: 88227
Question Answer Comment
Creator: Gundi, Hozar K
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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APPENDIX C

Environmental Monitoring Reporting Form
and Electronic Submittal of
Environmental Monitoring Data
7502Sept2015
(Electronic Format Only)