4903_IredellMSWLF_2nd2015WQMR_DIN25901_20150721 (2)

Iredell County Subtitle D Lined MSWLF, Phases 3 & 4
Statesville, North Carolina
July 2015
Permit Number: 49-03
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G15014.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 1
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 2
Surface Water Samples Page 2
Leachate Samples Page 2
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 3
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, or 2B (Appendix 1) Table 5
Detections in Leachate Samples above SWSL, GWP or 2L Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
APPENDICIES
Laboratory Analysis Reports and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
March 23, 2015
Mr. Ervin Lane
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (DEQ)
217 West Jones Street
Raleigh, NC 27603
Re: Semi-Annual Water Quality Monitoring Report
Iredell County Subtitle D Lined MSWLF, Phases 3 & 4
Permit No. 49-03
MESCO Project No. G15014.0
Event Date(s): July 21-23, 2015
Introduction
On behalf of Iredell County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the summer 2015 event performed at the Iredell County Subtitle D Lined
Municipal Solid Waste Landfill (MSWLF), Phases 3 & 4. NCDEQ Solid Waste Rules 15A NCAC 13B.1632
requires that Iredell County provide this report to the SWS on a semi-annual basis. This report documents the
quality of the ground and surface waters during this monitoring event performed on July 21-23, 2015. Laboratory
analytical results indicate that vinyl chloride was detected in excess of the NC groundwater 2L Standard and the
Solids Waste Section Limit (SWSL) in sample MW-21S for the first time. No contaminants were detected in any of
the surface water samples. No parameters were detected in any water sample above federal “Primary Drinking
Water Standards”.
Background
The Iredell County Subtitle D lined MSWLF, permit #49-03, is located at 354 Twin Oaks Road, Statesville, North
Carolina. The site location topographic map is depicted in the attached Figure 1. The lined MSWLF is comprised
of contiguous Phase 3 (inactive) & Phase 4 (active) which are treated as a single unit in this report.
Water quality at this facility has been monitored at least semi-annually since prior to operation in 2002 with all
historical data available and reviewed in support of this report. This event was performed in accordance with the
NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the permit to operate.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS issued
memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Detections compared to Standards tables, a groundwater flow directions/rates table, a field
observations table, a field data results table, potentiometric map, quality assurance/quality control data, and
laboratory analytical data results are also enclosed.
Sampling Procedure
MESCO performed the sampling in general accordance with the SWS approved Ground and Surface Water
Sampling and Analysis Plan contained in the Hydrogeologic Design Study revised on May 8, 2007. Groundwater
sample collection for this event included ten downgradient groundwater monitoring wells (MW-18, MW-19SR,
MW-19D, MW-21S, MW-21D, MW-27S, MW-27D, MW-28, MW-29 and MW-30), one background well (MW-
17), and one leachate sample (FORCEMAIN). The unnamed tributary of Fourth Creek, which serves as the local
discharge feature between both distinct units (Phases 3&4 and Phases 1 &2) was monitored at two locations (SW-1
and SW-5). Quality control measures were implemented during this event, including submittal and subsequent
blank quantification, equipment blank (EB), field blank (FB) and travel blank (TB). Monitoring locations are shown
on the potentiometric map (Figure 2).

A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated with no deficiencies observed as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was utilized to purge the wells to a minimum of three times
the volume of standing water in the well or until dry. Surface water samples were collected from previously
designated locations. The leachate sample was taken directly from the Phase 3 forcemain (FORCEMAIN) which
contains leachate originating from both Phases 3 & 4. During well purging and surface water sample collection the
required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved
containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-
certified laboratory under proper chain of custody (C-O-C) protocols within the specified hold times for each
analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included static water depth, pH, specific
conductance, temperature, total dissolved solids (TDS) and visual turbidity. A summary of the field parameter data
is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis on the
groundwater and surface water samples for the constituents listed in 40 CFR 258 Appendix I. A raw leachate
sample was analyzed for the required leachate specific list, which includes Appendix I, nitrate, phosphorus,
chemical oxygen demand (COD), biological oxygen demand (BOD), and sulfate. A sampling and analysis table
summarizing the locations, targeted constituents, and methods is presented on Table 4. Laboratory results and C-O-
Cs are presented in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L), the North Carolina Surface Water Standards (2B) for a Class C water-body or
the Federal “Drinking Water Standard” Maximum Contaminant Level (MCL).
Quality Control Samples
Methylene chloride was detected in the quality control field blank (FB); however, neither methylene chloride nor
any other chlorinated VOCs were detected in any other samples therefore the laboratory induced artifact
contamination is non-consequential.
Groundwater Samples
Total vanadium was detected in non-quantifiable “j-qualified” levels in samples MW-19SR (8.7 µg/L) and MW-30
(6.9 µg/L) in excess of the GWP Standard (3.5 µg/L).
Vinyl chloride was detected in sample MW-21S (1.2 µg/L) in excess of it's respective 2L Standard (0.03 µg/L).
Surfacewater Samples
No constituents were detected above the applicable 2B Standard in the surface water samples.
Leachate Samples
The leachate sample (FORCEMAIN) contained quantifiable concentrations of eight total metals and eight VOCs as
listed in Table 6. The concentrations of analytes detected in the leachate samples are much lower (by an order of
magnitude) then averages of leachate from similar landfills as published by the EPA 1 which is generally consistent
with results historically reported.
1 1988 EPA document-Summary of Data on MSWLFLeachate Characteristics – EPA/530-SW-88-038
2
Figures
Closed C&D
Lined MSWLF
34 21
C&D
Closed Unlined MSWLF
STATESVILLE
Topographic Map with Site Location
Iredell County Landfill
Figure 102.5 2.5 MILES
STATESVILLE EAST QUADRANGLE
N
354 Twin Oaks Rd
Statesville, NC 28625
Lat:35-46-17.8012
Long:-80-49-22.2973
Northing:740719.35
Easting:1459306.76
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LINED MSWLFPHASE 4ACTIVEPTO 7/30/08July 23, 2015WELL ID15A NCAC 2L Groundwater Quality Standard 0.03MW-17854.3538.29816.06MW-18800.726.63794.09MW-19SR797.2610.59786.67MW-19D*795.819.36786.45MW-21S823.9735.39788.581.2MW-21D*822.7633.09789.67MW-27S808.0013.10794.90MW-27D*806.9512.05794.90MW-28810.179.29800.88MW-29809.0611.32797.74MW-30797.918.11789.80P-4839.2522.75816.50NSP4-7S818.4712.88805.59NSP4-7D*819.0013.34805.66NS* = Wells not used for groundwater contouringNS = Not Sampled since not requiredM ³M´4XDOLILHGFRQFHQWUDWLRQ6:6/FRQVLGHUHGDQHVWLPDWH Groundwater Levels & VOCs Detected Above 2L StandardsTOP OF CASING ELEVATION (FT AMSL)DEPTH TO WATER (FT BTOC)GROUNDWATER POTENTIOMETRIC ELEVATION (FT AMSL)Vinyl Chloride (UG/L)
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Tables
Iredell County Subtitle D Lined MSWLF, Phases 3 & 4 Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
July 21-23, 2015
Latitude Longitude
(inches)(ft)
MW-17 5/9/02 2 45.00 30.00 15 Soil 854.35 850.94 816.06 38.29 35.7717 -80.8367
MW-18 6/2/00 2 20.00 5.00 15 Soil 800.72 796.09 794.09 6.63 35.7685 -80.8345
MW-19SR 6/30/06 2 22.02 7.02 15 Sandy Silt 797.26 794.54 786.67 10.59 35.7698 -80.8327
MW-19D 5/9/02 2 59.00 49.00 10 Rock 795.81 793.26 786.45 9.36 35.7685 -80.8345
MW-21S 6/2/00 2 41.00 26.00 15 Silt 823.97 821.03 788.58 35.39 35.7714 -80.8327
MW-21D 6/17/00 2 138.25 128.25 10 Rock 822.76 819.25 789.67 33.09 35.7714 -80.8327
MW-27S 1/3/05 2 20.09 5.09 15 Sandy Silt 808.00 803.90 794.90 13.10 35.7684 -80.8357
MW-27D 1/3/05 2 44.42 39.42 5 Silty Sand 806.95 804.69 794.90 12.05 35.7684 -80.8357
MW-28 12/27/04 2 12.42 7.42 5 Sandy Silt 810.17 807.49 800.88 9.29 35.7691 -80.8380
MW-29 12/27/04 2 17.68 7.68 10 Silty Sand 809.06 806.49 797.74 11.32 35.7687 -80.8372
MW-30 12/14/10 2 17.40 6.40 11 Silt 797.91 794.91 789.80 8.11 35.7689 -80.8333
NOTE:
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length Geology of
Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Iredell County Subtitle D MSWLF, Phase 3 & 4 Page 1 of 1
Table 2
Field Observations of Monitoring Locations
July 21-23, 2015
Locked Comments
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19SR Yes Yes Yes Yes Yes Yes
MW-19D Yes Yes Yes Yes Yes Yes
MW-21S Yes Yes Yes Yes Yes Yes
MW-21D Yes Yes Yes Yes Yes Yes
MW-27S Yes Yes Yes Yes Yes Yes Repaired by MESCO in June 2014
MW-27D Yes Yes Yes Yes Yes Yes
MW-28 Yes Yes Yes Yes Yes Yes
MW-29 Yes Yes Yes Yes Yes Yes
MW-30 Yes Yes Yes Yes Yes Yes
SW-1 Yes
SW-2 Yes
SW-5 Yes
P4-7S Yes Yes Yes Yes Yes Yes
P4-7D Yes Yes Yes Yes Yes Yes
P-4 Yes Yes Yes Yes Yes Yes
FORCEMAIN Yes Sample from valve as typical
Any unusual field conditions, observations, or events:
MW-27S repaired by MESCO in June 2014 after being bumped by mower.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete Surface
Pad Effective
na na na na na
na na na na na
na na na na na
na na na na na
na = not available or applicable
MW-27S top of PVC elevation changed to 808.00 amsl was 807.25 amsl. Elevation determined in field by string level pulled from MW-27D.
Iredell County Subtitle D MSWLF, Phase 3 & 4 Page 1 of 1
Table 3
Summary of Field Parameter Data
July 21-23, 2015
Location Temperature ORP DO pH TDS
Units C mg/L SU visual
MW-17 38.29 816.06 854.35 16.7 NR NR 5.93 0 0 Clear
MW-18 6.63 794.09 800.72 16.1 NR NR 6.71 30 10 Clear
MW-19SR 10.59 786.67 797.26 17.4 NR NR 6.91 1860 920 Clear
MW-19D 9.36 786.45 795.81 16.9 NR NR 7.03 10 0 Clear
MW-21S 35.39 788.58 823.97 17.5 NR NR 6.41 10 0 Clear
MW-21D 33.09 789.67 822.76 18.1 NR NR 8.83 90 40 Clear
MW-27S 13.10 794.9 808.00 16.2 NR NR 6.51 90 40 Clear
MW-27D 12.05 794.9 806.95 15.9 NR NR 7.11 90 40 Clear
MW-28 9.29 800.88 810.17 18.4 NR NR 7.01 160 70 Very
MW-29 11.32 797.74 809.06 18.1 NR NR 6.93 70 30 Slight
MW-30 8.11 789.8 797.91 15.4 NR NR 7.11 90 40 Slight
Minimum 6.63 786.45 795.81 15.4 NR NR 5.93 0 0 Clear
Average 17.02 794.52 811.54 17.0 NR NR 6.95 227 108 Slight
Maximum 38.29 816.06 854.35 18.4 NR NR 8.83 1860 920 Very
SW-1 ---26.5 NR NR 6.98 130 60 Clear
SW-2 ---28.1 NR NR 7.03 210 100 Clear
SW-5 ---25.9 NR NR 7.03 110 50 Clear
Minimum ---25.9 NR NR 6.98 110 50 Clear
Average ---26.8 NR NR 7.01 150 70 Clear
Maximum ---28.1 NR NR 7.03 210 100 Clear
Water
Depth
Water
Elevation
TOC
Elevation
Specific
Conductance
Turbidity
of Metal
Sample
ft (btoc)ft (amsl)ft (amsl)mV цs/cm ppt
Iredell County Subtitle D Lined MSWLF, Phases 3 & 4 Page 1 of 1
Table 4
Sampling and Analysis Summary
July 23, 2015
Field Parameter Leachate
To
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MW-17 x x x x x x x
MW-18 x x x x x x x
MW-19SR x x x x x x x
MW-19D x x x x x x x
MW-21S x x x x x x x
MW-21D x x x x x x x
MW-27S x x x x x x x
MW-27D x x x x x x x
MW-28 x x x x x x x
MW-29 x x x x x x x
MW-30 x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
SW-5 x x x x x x x
FORCEMAIN x x x x x x x x
EB x x
FB x x
TB x
App. I
VO
C
s

App I = Appendix I List from current 40 CFR 258
Iredell County Subtitle D MSWLF, Phase 3 & 4 Page 1 of 1
Table 5
Detections in Water Samples above SWSL, GWP, 2L or 2B (Appendix I)
July 23, 2015
Sample ID Result Unit
MW-17 7/23/15 1.3 0.2 1 2100 NE
MW-17 Zinc, total 7/23/15 12.7 5 10 1000 5000
MW-19SR Barium, total 7/23/15 145 2.5 100 700 1300
MW-19SR Vanadium, total 7/23/15 8.7J 2.5 25 NE 3.5 NE
MW-21S Vinyl chloride 7/23/15 1.2 0.62 1 0.03 2 LFG
MW-21S 7/23/15 0.65J 0.46 1 0.7 5
MW-27D Copper, total 7/23/15 12.2 2.5 10 1000 1300
MW-30 Vanadium, total 7/23/15 6.9J 2.5 25 NE 3.5 NE
FB Methylene Chloride 7/23/15 0.99J 0.97 1 4.6 5
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B or MCL Standard
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
Trichlorofluoromethane ug/L
ug/L
ug/L
ug/L
ug/L
Tetrachloroethene ug/L
ug/L
ug/L
ug/L
1 Table contains Appendix I constituents detected above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Iredell County Subtitle D MSWLF, Phase 3 & 4 Page 1 of 1
Table 6
Detections in Leachate Sample Above SWSL, GWP, 2L or MCL
July 23, 2015
Sample ID Result Unit
FORCEMAIN 7/23/15 1.1 0.24 1 0.4 5 1841
FORCEMAIN 7/23/15 1.6 0.33 1 6 75 13.2
FORCEMAIN 7/23/15 726 3.8 400 4200 NE 4153
FORCEMAIN Acetone 7/23/15 1140 40 400 6000 NE 2163
FORCEMAIN Benzene 7/23/15 6.4 0.25 1 1 5 221
FORCEMAIN 7/23/15 15.9 0.3 1 550 700 274
FORCEMAIN Styrene 7/23/15 0.61J 0.26 1 100 100
FORCEMAIN Toluene 7/23/15 5.2 0.26 1 600 1000 1016
FORCEMAIN Xylene (Total)7/23/15 23.1 0.66 5 530 10000 141
FORCEMAIN Vinyl Chloride 7/23/15 ND<0.62 0.62 1 0.03 2 36.1
FORCEMAIN Antimony, total 7/23/15 16 3.8 6 NE 1.4 6 4520
FORCEMAIN Arsenic, total 7/23/15 16.4 2.5 10 10 10 41.8
FORCEMAIN Barium, total 7/23/15 823 2.5 100 700 1300 850
FORCEMAIN Chromium, total 7/23/15 38.8 2.5 10 10 100 175
FORCEMAIN Cobalt, total 7/23/15 16 2.5 10 NE 70 NE 90
FORCEMAIN Copper, total 7/23/15 29.9 2.5 10 1000 1300 168
FORCEMAIN Nickel, total 7/23/15 137 2.5 50 100 NE 325.5
FORCEMAIN Vanadium, total 7/23/15 19.9J 2.5 25 NE 3.5 NE 17.9
FORCEMAIN Zinc, total 7/23/15 21.8 5 10 1000 5000 8320
FORCEMAIN Sulfate 7/23/15 24400J 1000 250000 250000 NE 244000
FORCEMAIN BOD, 5 day 7/23/15 402000 2000 2000 NE NE 3837000
FORCEMAIN COD 7/23/15 1300000J 1250000 2500000 NE NE 4773000
FORCEMAIN Phosphorus 7/23/15 938 25 50 NE NE 7820
adjusted for actual sample preparation data and moisture content, where applicable.
NE = Not Established
BOLD = Concentration > 2L, GWP, MCL or “Average Leachate”
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 GWP 5 MCL 6 “Average
Leachate” 7
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
2-Butanone (MEK)ug/L
ug/L
ug/L
Ethylbenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains only constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit (Current as of Sampling Event)
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard (Current as of Sampling Event)
5 GWP = Groundwater Protection Standard (Current as of Sampling Event)
6 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
7 Average concentration of leachate from a comparable “Dry Tomb” Landfill published in 1988 by EPA document Summary of Data on MSWLF Leachate Characteristics
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
Iredell County Subtitle D MSWLF, Phase 3 & 4 Page 1 of 1
Table 7
July 21-22, 2015
(cm/sec)(%)(ft/ft)(ft/yr)
MW-17 3.73E-05 21.7 0.013 2 S71E 38.29 816.06 Silt
MW-18 7.43E-04 21.7 0.005 19 S39E 6.63 794.09 Silt
MW-19SR 4.54E-04 21.7 0.021 46 N47W 10.59 786.67 Sandy Silt
MW-19D 2.81E-03 21.7 n/a n/a N73W 9.36 786.45 Fractured Rock
MW-21S 1.67E-05 21.7 0.044 4 S40E 35.39 788.58
MW-21D 9.08E-07 21.7 n/a n/a S51E 33.09 789.67 Fractured Rock
MW-27S 5.62E-04 17.0 0.002 7 S16E 13.10 794.90 Silty Sand
MW-27D 4.67E-04 6.0 n/a n/a S20E 12.05 794.90 Clayey Sand
MW-28 1.52E-03 17.0 0.009 86 S34E 9.29 800.88 Silty Sand
MW-29 7.70E-04 17.0 0.016 73 S06E 11.32 797.74 Silty Sand
MW-30 2.66E-03 21.7 0.018 231 N12W 8.11 789.80 Silt
Minimum 9.08E-07 6.0 0.002 2 -6.63 786.45 -
Average 9.13E-04 19.0 0.016 58 -17.02 794.52 -
Maximum 2.81E-03 21.7 0.044 231 -38.29 816.06 -
NOTE:Values for hydraulic conductivity previously determined via slug test by MESCO.
Wells screened in rock or deeper cluster counterparts not utilized for flow directions/gradients.
Hydraulic Conductivity value for MW-19SR assumed identical to previously adjacent MW-19S.
K = hydraulic conductivity
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Average
Linear
Velocity
Rate
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation
Screened
Interval
Lithology
(ft btoc)(ft amsl)
Saprolite
Hydrologic Gradient calculated from groundwater elevations recorded on July 21-22, 2015.
Average linear velocity rate (Q) is defined by modified Darcy's equation:
ne = effective porosity
dh = head difference
dl = horizontal distance
Q=−K
ne
⋅dh
dl
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
August 05, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92260261
92260261
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
IREDELL LINED 3&4
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 45
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 45
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Lab ID Sample ID Matrix Date Collected Date Received
92260261001 FORCEMAIN Water 07/23/15 17:00 07/24/15 11:49
92260261002 MW-17 Water 07/23/15 08:35 07/24/15 11:49
92260261003 MW-18 Water 07/23/15 10:15 07/24/15 11:49
92260261004 MW-19SR Water 07/23/15 15:10 07/24/15 11:49
92260261005 MW-19D Water 07/23/15 14:30 07/24/15 11:49
92260261006 MW-21S Water 07/23/15 16:00 07/24/15 11:49
92260261007 MW-21D Water 07/23/15 16:40 07/24/15 11:49
92260261008 MW-27S Water 07/23/15 13:20 07/24/15 11:49
92260261009 MW-27D Water 07/23/15 11:40 07/24/15 11:49
92260261010 MW-28 Water 07/23/15 09:10 07/24/15 11:49
92260261011 MW-29 Water 07/23/15 09:35 07/24/15 11:49
92260261012 MW-30 Water 07/23/15 11:00 07/24/15 11:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 45
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92260261001 FORCEMAIN EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CGAW, SNP
SM 5210B 1 PASI-ABRJ
EPA 9040 1 PASI-AMLS
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
EPA 365.1 1 PASI-ASER
SM 5220D 1 PASI-AMJP
92260261002 MW-17 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261003 MW-18 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261004 MW-19SR EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261005 MW-19D EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261006 MW-21S EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261007 MW-21D EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261008 MW-27S EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261009 MW-27D EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261010 MW-28 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261011 MW-29 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
92260261012 MW-30 EPA 6010 15 PASI-AJMW
EPA 8260 51 PASI-CSNP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:FORCEMAIN Lab ID:92260261001 Collected:07/23/15 17:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony 16.0 ug/L 08/04/15 02:43 7440-36-007/27/15 19:006.0 3.8 1
Arsenic 16.4 ug/L 08/04/15 02:43 7440-38-207/27/15 19:0010.0 2.5 1
Barium 823 ug/L 08/04/15 02:43 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 02:43 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 02:43 7440-43-907/27/15 19:001.0 0.50 1
Chromium 38.8 ug/L 08/04/15 02:43 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt 16.0 ug/L 08/04/15 02:43 7440-48-407/27/15 19:0010.0 2.5 1
Copper 29.9 ug/L 08/04/15 02:43 7440-50-807/27/15 19:0010.0 2.5 1
Lead 3.5J ug/L 08/04/15 02:43 7439-92-107/27/15 19:0010.0 2.5 1
Nickel 137 ug/L 08/04/15 02:43 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 02:43 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 02:43 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 02:43 7440-28-007/27/15 19:005.5 5.0 1
Vanadium 19.9J ug/L 08/04/15 02:43 7440-62-207/27/15 19:0025.0 2.5 1
Zinc 21.8 ug/L 08/04/15 02:43 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 1140 ug/L 07/30/15 18:11 67-64-140040.0 4
Acrylonitrile ND ug/L 07/28/15 16:28 107-13-12001.9 1
Benzene 6.4 ug/L 07/28/15 16:28 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 16:28 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 16:28 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 16:28 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 16:28 74-83-910.0 0.29 1
2-Butanone (MEK)726 ug/L 07/30/15 18:11 78-93-34003.8 4
Carbon disulfide ND ug/L 07/28/15 16:28 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 16:28 56-23-51.0 0.25 1
Chlorobenzene 0.58J ug/L 07/28/15 16:28 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 16:28 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 16:28 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 16:28 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 16:28 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 16:28 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 16:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 16:28 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 16:28 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.6 ug/L 07/28/15 16:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 16:28 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 16:28 75-34-35.0 0.32 1
1,2-Dichloroethane 1.1 ug/L 07/28/15 16:28 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 16:28 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.30J ug/L 07/28/15 16:28 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 16:28 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 16:28 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 16:28 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 16:28 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:FORCEMAIN Lab ID:92260261001 Collected:07/23/15 17:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 16:28 10061-02-61.0 0.26 1
Ethylbenzene 15.9 ug/L 07/28/15 16:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 16:28 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 16:28 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 16:28 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)27.2J ug/L 07/28/15 16:28 108-10-11000.33 1
Styrene 0.61J ug/L 07/28/15 16:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 16:28 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 16:28 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 16:28 127-18-41.0 0.46 1
Toluene 5.2 ug/L 07/28/15 16:28 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 16:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 16:28 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 16:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 16:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 16:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 16:28 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 16:28 75-01-41.0 0.62 1
Xylene (Total)23.1 ug/L 07/28/15 16:28 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %07/28/15 16:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %07/28/15 16:28 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 16:28 2037-26-570-130 1
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 402000 ug/L 07/29/15 23:3907/25/15 04:41200020001
Analytical Method: EPA 90409040 pH
pH 7.1 Std. Units 07/27/15 14:40 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 24400J ug/L 07/29/15 19:41 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 07/25/15 00:141000010.0 1
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 938 ug/L 08/05/15 04:35 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 1300000J ug/L 07/27/15 15:4525000001250000100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-17 Lab ID:92260261002 Collected:07/23/15 08:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 02:53 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 02:53 7440-38-207/27/15 19:0010.0 2.5 1
Barium 60.2J ug/L 08/04/15 02:53 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 02:53 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 02:53 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 02:53 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 02:53 7440-48-407/27/15 19:0010.0 2.5 1
Copper 6.0J ug/L 08/04/15 02:53 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 02:53 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 02:53 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 02:53 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 02:53 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 02:53 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 02:53 7440-62-207/27/15 19:0025.0 2.5 1
Zinc 12.7 ug/L 08/04/15 02:53 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 17.3J ug/L 07/28/15 16:44 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 16:44 107-13-12001.9 1
Benzene ND ug/L 07/28/15 16:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 16:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 16:44 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 16:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 16:44 74-83-910.0 0.29 1
2-Butanone (MEK)9.3J ug/L 07/28/15 16:44 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 16:44 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 16:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 16:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 16:44 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 16:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 16:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 16:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 16:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 16:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 16:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 16:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 16:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 16:44 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 16:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 16:44 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 16:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 16:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 16:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 16:44 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 16:44 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 16:44 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-17 Lab ID:92260261002 Collected:07/23/15 08:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 16:44 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 16:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 16:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 16:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 16:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 16:44 108-10-11000.33 1
Styrene ND ug/L 07/28/15 16:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 16:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 16:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 16:44 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 16:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 16:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 16:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 16:44 79-01-61.0 0.47 1
Trichlorofluoromethane 1.3 ug/L 07/28/15 16:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 16:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 16:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 16:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 16:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %07/28/15 16:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/15 16:44 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 16:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-18 Lab ID:92260261003 Collected:07/23/15 10:15 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 02:56 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 02:56 7440-38-207/27/15 19:0010.0 2.5 1
Barium 26.6J ug/L 08/04/15 02:56 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 02:56 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 02:56 7440-43-907/27/15 19:001.0 0.50 1
Chromium 2.7J ug/L 08/04/15 02:56 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 02:56 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 02:56 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 02:56 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 02:56 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 02:56 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 02:56 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 02:56 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 02:56 7440-62-207/27/15 19:0025.0 2.5 1
Zinc 8.4J ug/L 08/04/15 02:56 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 17:01 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 17:01 107-13-12001.9 1
Benzene ND ug/L 07/28/15 17:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 17:01 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 17:01 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 17:01 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 17:01 74-83-910.0 0.29 1
2-Butanone (MEK)2.7J ug/L 07/28/15 17:01 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 17:01 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 17:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 17:01 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 17:01 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 17:01 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 17:01 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 17:01 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 17:01 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 17:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 17:01 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 17:01 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 17:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 17:01 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 17:01 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 17:01 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 17:01 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 17:01 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 17:01 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 17:01 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 17:01 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 17:01 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-18 Lab ID:92260261003 Collected:07/23/15 10:15 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 17:01 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 17:01 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 17:01 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 17:01 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 17:01 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 17:01 108-10-11000.33 1
Styrene ND ug/L 07/28/15 17:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 17:01 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 17:01 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 17:01 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 17:01 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 17:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 17:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 17:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 17:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 17:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 17:01 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 17:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 17:01 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %07/28/15 17:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 17:01 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 17:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-19SR Lab ID:92260261004 Collected:07/23/15 15:10 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 02:59 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 02:59 7440-38-207/27/15 19:0010.0 2.5 1
Barium 145 ug/L 08/04/15 02:59 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 02:59 7440-41-707/27/15 19:001.0 0.50 1
Cadmium 0.87J ug/L 08/04/15 02:59 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 02:59 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 02:59 7440-48-407/27/15 19:0010.0 2.5 1
Copper 5.2J ug/L 08/04/15 02:59 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 02:59 7439-92-107/27/15 19:0010.0 2.5 1
Nickel 3.4J ug/L 08/04/15 02:59 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 02:59 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 02:59 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 02:59 7440-28-007/27/15 19:005.5 5.0 1
Vanadium 8.7J ug/L 08/04/15 02:59 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 02:59 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 17:18 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 17:18 107-13-12001.9 1
Benzene ND ug/L 07/28/15 17:18 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 17:18 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 17:18 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 17:18 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 17:18 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 17:18 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 17:18 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 17:18 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 17:18 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 17:18 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 17:18 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 17:18 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 17:18 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 17:18 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 17:18 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 17:18 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 17:18 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 17:18 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 17:18 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 17:18 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 17:18 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 17:18 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 17:18 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 17:18 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 17:18 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 17:18 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 17:18 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-19SR Lab ID:92260261004 Collected:07/23/15 15:10 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 17:18 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 17:18 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 17:18 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 17:18 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 17:18 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 17:18 108-10-11000.33 1
Styrene ND ug/L 07/28/15 17:18 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 17:18 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 17:18 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 17:18 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 17:18 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 17:18 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 17:18 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 17:18 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 17:18 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 17:18 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 17:18 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 17:18 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 17:18 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %07/28/15 17:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 17:18 17060-07-070-130 1
Toluene-d8 (S)102 %07/28/15 17:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-19D Lab ID:92260261005 Collected:07/23/15 14:30 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:02 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:02 7440-38-207/27/15 19:0010.0 2.5 1
Barium ND ug/L 08/04/15 03:02 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:02 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:02 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:02 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:02 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:02 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:02 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:02 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:02 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:02 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:02 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:02 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:02 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 17:35 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 17:35 107-13-12001.9 1
Benzene ND ug/L 07/28/15 17:35 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 17:35 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 17:35 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 17:35 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 17:35 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 17:35 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 17:35 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 17:35 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 17:35 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 17:35 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 17:35 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 17:35 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 17:35 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 17:35 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 17:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 17:35 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 17:35 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 17:35 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 17:35 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 17:35 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 17:35 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 17:35 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 17:35 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 17:35 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 17:35 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 17:35 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 17:35 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-19D Lab ID:92260261005 Collected:07/23/15 14:30 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 17:35 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 17:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 17:35 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 17:35 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 17:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 17:35 108-10-11000.33 1
Styrene ND ug/L 07/28/15 17:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 17:35 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 17:35 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 17:35 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 17:35 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 17:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 17:35 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 17:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 17:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 17:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 17:35 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 17:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 17:35 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 17:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %07/28/15 17:35 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 17:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-21S Lab ID:92260261006 Collected:07/23/15 16:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:05 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:05 7440-38-207/27/15 19:0010.0 2.5 1
Barium 81.6J ug/L 08/04/15 03:05 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:05 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:05 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:05 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:05 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:05 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:05 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:05 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:05 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:05 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:05 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:05 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:05 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 17:51 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 17:51 107-13-12001.9 1
Benzene ND ug/L 07/28/15 17:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 17:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 17:51 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 17:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 17:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 17:51 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 17:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 17:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 17:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 17:51 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 17:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 17:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 17:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 17:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 17:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 17:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 17:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 17:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 17:51 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 17:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 17:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 17:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 17:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 17:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 17:51 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 17:51 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 17:51 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-21S Lab ID:92260261006 Collected:07/23/15 16:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 17:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 17:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 17:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 17:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 17:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 17:51 108-10-11000.33 1
Styrene ND ug/L 07/28/15 17:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 17:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 17:51 79-34-53.0 0.40 1
Tetrachloroethene 0.65J ug/L 07/28/15 17:51 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 17:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 17:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 17:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 17:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 17:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 17:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 17:51 108-05-450.0 0.35 1
Vinyl chloride 1.2 ug/L 07/28/15 17:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 17:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 17:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 17:51 17060-07-070-130 1
Toluene-d8 (S)98 %07/28/15 17:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-21D Lab ID:92260261007 Collected:07/23/15 16:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:08 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:08 7440-38-207/27/15 19:0010.0 2.5 1
Barium 18.7J ug/L 08/04/15 03:08 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:08 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:08 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:08 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:08 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:08 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:08 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:08 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:08 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:08 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:08 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:08 7440-62-207/27/15 19:0025.0 2.5 1
Zinc 5.8J ug/L 08/04/15 03:08 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 18:08 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 18:08 107-13-12001.9 1
Benzene ND ug/L 07/28/15 18:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 18:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 18:08 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 18:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 18:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 18:08 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 18:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 18:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 18:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 18:08 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 18:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 18:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 18:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 18:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 18:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 18:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 18:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 18:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 18:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 18:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 18:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 18:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 18:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 18:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 18:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 18:08 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 18:08 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-21D Lab ID:92260261007 Collected:07/23/15 16:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 18:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 18:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 18:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 18:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 18:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 18:08 108-10-11000.33 1
Styrene ND ug/L 07/28/15 18:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 18:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 18:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 18:08 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 18:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 18:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 18:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 18:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 18:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 18:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 18:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 18:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 18:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 18:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %07/28/15 18:08 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 18:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-27S Lab ID:92260261008 Collected:07/23/15 13:20 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:11 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:11 7440-38-207/27/15 19:0010.0 2.5 1
Barium 20.9J ug/L 08/04/15 03:11 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:11 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:11 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:11 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:11 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:11 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:11 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:11 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:11 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:11 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:11 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:11 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:11 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 18:24 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 18:24 107-13-12001.9 1
Benzene ND ug/L 07/28/15 18:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 18:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 18:24 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 18:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 18:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 18:24 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 18:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 18:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 18:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 18:24 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 18:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 18:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 18:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 18:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 18:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 18:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 18:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 18:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 18:24 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 18:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 18:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 18:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 18:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 18:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 18:24 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 18:24 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 18:24 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-27S Lab ID:92260261008 Collected:07/23/15 13:20 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 18:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 18:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 18:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 18:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 18:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 18:24 108-10-11000.33 1
Styrene ND ug/L 07/28/15 18:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 18:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 18:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 18:24 127-18-41.0 0.46 1
Toluene 0.60J ug/L 07/28/15 18:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 18:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 18:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 18:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 18:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 18:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 18:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 18:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 18:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %07/28/15 18:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 18:24 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 18:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-27D Lab ID:92260261009 Collected:07/23/15 11:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:24 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:24 7440-38-207/27/15 19:0010.0 2.5 1
Barium 7.7J ug/L 08/04/15 03:24 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:24 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:24 7440-43-907/27/15 19:001.0 0.50 1
Chromium 3.0J ug/L 08/04/15 03:24 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:24 7440-48-407/27/15 19:0010.0 2.5 1
Copper 12.2 ug/L 08/04/15 03:24 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:24 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:24 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:24 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:24 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:24 7440-28-007/27/15 19:005.5 5.0 1
Vanadium 3.0J ug/L 08/04/15 03:24 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:24 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 18:41 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 18:41 107-13-12001.9 1
Benzene ND ug/L 07/28/15 18:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 18:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 18:41 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 18:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 18:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 18:41 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 18:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 18:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 18:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 18:41 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 18:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 18:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 18:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 18:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 18:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 18:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 18:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 18:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 18:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 18:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 18:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 18:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 18:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 18:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 18:41 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 18:41 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 18:41 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-27D Lab ID:92260261009 Collected:07/23/15 11:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 18:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 18:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 18:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 18:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 18:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 18:41 108-10-11000.33 1
Styrene ND ug/L 07/28/15 18:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 18:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 18:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 18:41 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 18:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 18:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 18:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 18:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 18:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 18:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 18:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 18:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 18:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %07/28/15 18:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/15 18:41 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 18:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-28 Lab ID:92260261010 Collected:07/23/15 09:10 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:27 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:27 7440-38-207/27/15 19:0010.0 2.5 1
Barium 11.7J ug/L 08/04/15 03:27 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:27 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:27 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:27 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:27 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:27 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:27 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:27 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:27 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:27 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:27 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:27 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:27 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 18:58 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 18:58 107-13-12001.9 1
Benzene ND ug/L 07/28/15 18:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 18:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 18:58 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 18:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 18:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 18:58 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 18:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 18:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 18:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 18:58 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 18:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 18:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 18:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 18:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 18:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 18:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 18:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 18:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 18:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 18:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 18:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 18:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 18:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 18:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 18:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 18:58 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 18:58 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-28 Lab ID:92260261010 Collected:07/23/15 09:10 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 18:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 18:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 18:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 18:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 18:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 18:58 108-10-11000.33 1
Styrene ND ug/L 07/28/15 18:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 18:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 18:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 18:58 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 18:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 18:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 18:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 18:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 18:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 18:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 18:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 18:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 18:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %07/28/15 18:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 18:58 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 18:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-29 Lab ID:92260261011 Collected:07/23/15 09:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:30 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:30 7440-38-207/27/15 19:0010.0 2.5 1
Barium 24.3J ug/L 08/04/15 03:30 7440-39-307/27/15 19:001002.5 1
Beryllium 0.57J ug/L 08/04/15 03:30 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:30 7440-43-907/27/15 19:001.0 0.50 1
Chromium 2.7J ug/L 08/04/15 03:30 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:30 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:30 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:30 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:30 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:30 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:30 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:30 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:30 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:30 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 19:14 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 19:14 107-13-12001.9 1
Benzene ND ug/L 07/28/15 19:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 19:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 19:14 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 19:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 19:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 19:14 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 19:14 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 19:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 19:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 19:14 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 19:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 19:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 19:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 19:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 19:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 19:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 19:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 19:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 19:14 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 19:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 19:14 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 19:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 19:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 19:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 19:14 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 19:14 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 19:14 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Page 25 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-29 Lab ID:92260261011 Collected:07/23/15 09:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 19:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 19:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 19:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 19:14 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 19:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 19:14 108-10-11000.33 1
Styrene ND ug/L 07/28/15 19:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 19:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 19:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 19:14 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 19:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 19:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 19:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 19:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 19:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 19:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 19:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 19:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 19:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %07/28/15 19:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %07/28/15 19:14 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 19:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Page 26 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-30 Lab ID:92260261012 Collected:07/23/15 11:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:33 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:33 7440-38-207/27/15 19:0010.0 2.5 1
Barium 10.6J ug/L 08/04/15 03:33 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:33 7440-41-707/27/15 19:001.0 0.50 1
Cadmium 0.50J ug/L 08/04/15 03:33 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:33 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:33 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:33 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:33 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:33 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:33 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:33 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:33 7440-28-007/27/15 19:005.5 5.0 1
Vanadium 6.9J ug/L 08/04/15 03:33 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:33 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 19:31 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 19:31 107-13-12001.9 1
Benzene ND ug/L 07/28/15 19:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 19:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 19:31 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 19:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 19:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 19:31 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 19:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 19:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 19:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 19:31 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 19:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 19:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 19:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 19:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 19:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 19:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 19:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 19:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 19:31 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 19:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 19:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 19:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 19:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 19:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 19:31 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 19:31 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 19:31 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Sample:MW-30 Lab ID:92260261012 Collected:07/23/15 11:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 19:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 19:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 19:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 19:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 19:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 19:31 108-10-11000.33 1
Styrene ND ug/L 07/28/15 19:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 19:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 19:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 19:31 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 19:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 19:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 19:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 19:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 19:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 19:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 19:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 19:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 19:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %07/28/15 19:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %07/28/15 19:31 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 19:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19105
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92260261001, 92260261002, 92260261003, 92260261004, 92260261005, 92260261006, 92260261007,
92260261008, 92260261009, 92260261010, 92260261011, 92260261012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519047
Associated Lab Samples:92260261001, 92260261002, 92260261003, 92260261004, 92260261005, 92260261006, 92260261007,
92260261008, 92260261009, 92260261010, 92260261011, 92260261012
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 08/04/15 02:28
Arsenic ug/L ND 10.0 08/04/15 02:28
Barium ug/L ND 100 08/04/15 02:28
Beryllium ug/L ND 1.0 08/04/15 02:28
Cadmium ug/L ND 1.0 08/04/15 02:28
Chromium ug/L ND 10.0 08/04/15 02:28
Cobalt ug/L ND 10.0 08/04/15 02:28
Copper ug/L ND 10.0 08/04/15 02:28
Lead ug/L ND 10.0 08/04/15 02:28
Nickel ug/L ND 50.0 08/04/15 02:28
Selenium ug/L ND 10.0 08/04/15 02:28
Silver ug/L ND 10.0 08/04/15 02:28
Thallium ug/L ND 5.5 08/04/15 02:28
Vanadium ug/L ND 25.0 08/04/15 02:28
Zinc ug/L ND 10.0 08/04/15 02:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519048LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 455500 91 80-120
Barium ug/L 469500 94 80-120
Beryllium ug/L 476500 95 80-120
Cadmium ug/L 464500 93 80-120
Chromium ug/L 479500 96 80-120
Cobalt ug/L 466500 93 80-120
Copper ug/L 470500 94 80-120
Lead ug/L 460500 92 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 447500 89 80-120
Silver ug/L 228250 91 80-120
Thallium ug/L 466500 93 80-120
Vanadium ug/L 473500 95 80-120
Zinc ug/L 464500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1519049MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260261001
1519050
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12595 1 2550016.0 486 492
Arsenic ug/L 500 95 75-12596 1 2550016.4 492 496
Barium ug/L 500 93 75-125101 3 2550082312901330
Beryllium ug/L 500 94 75-12595 0 25500ND472474
Cadmium ug/L 500 94 75-12595 1 25500ND471475
Chromium ug/L 500 94 75-12595 1 2550038.8 508 515
Cobalt ug/L 500 88 75-12589 1 2550016.0 457 460
Copper ug/L 500 96 75-12599 2 2550029.9 512 524
Lead ug/L 500 85 75-12586 1 255003.5J 430 434
Nickel ug/L 500 86 75-12587 1 25500137569573
Selenium ug/L 500 89 75-12591 2 25500ND447454
Silver ug/L 250 94 75-12595 1 25250ND236239
Thallium ug/L 500 83 75-12583 1 25500ND413417
Vanadium ug/L 500 95 75-12596 1 2550019.9J 495 501
Zinc ug/L 500 89 75-12591 2 2550021.8 469 476
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32734
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92260261001, 92260261002, 92260261003, 92260261004, 92260261005, 92260261006, 92260261007,
92260261008, 92260261009, 92260261010, 92260261011, 92260261012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519680
Associated Lab Samples:92260261001, 92260261002, 92260261003, 92260261004, 92260261005, 92260261006, 92260261007,
92260261008, 92260261009, 92260261010, 92260261011, 92260261012
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 13:41
1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 13:41
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 13:41
1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 13:41
1,1-Dichloroethane ug/L ND 5.0 07/28/15 13:41
1,1-Dichloroethene ug/L ND 5.0 07/28/15 13:41
1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 13:41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 13:41
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/15 13:41
1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 13:41
1,2-Dichloroethane ug/L ND 1.0 07/28/15 13:41
1,2-Dichloropropane ug/L ND 1.0 07/28/15 13:41
1,3-Dichloropropane ug/L ND 1.0 07/28/15 13:41
1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 13:41
2-Butanone (MEK)ug/L ND 100 07/28/15 13:41
2-Hexanone ug/L ND 50.0 07/28/15 13:41
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/28/15 13:41
Acetone ug/L ND 100 07/28/15 13:41
Acrylonitrile ug/L ND 200 07/28/15 13:41
Benzene ug/L ND 1.0 07/28/15 13:41
Bromochloromethane ug/L ND 3.0 07/28/15 13:41
Bromodichloromethane ug/L ND 1.0 07/28/15 13:41
Bromoform ug/L ND 3.0 07/28/15 13:41
Bromomethane ug/L ND 10.0 07/28/15 13:41
Carbon disulfide ug/L ND 100 07/28/15 13:41
Carbon tetrachloride ug/L ND 1.0 07/28/15 13:41
Chlorobenzene ug/L ND 3.0 07/28/15 13:41
Chloroethane ug/L ND 10.0 07/28/15 13:41
Chloroform ug/L ND 5.0 07/28/15 13:41
Chloromethane ug/L ND 1.0 07/28/15 13:41
cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 13:41
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 13:41
Dibromochloromethane ug/L ND 3.0 07/28/15 13:41
Dibromomethane ug/L ND 10.0 07/28/15 13:41
Ethylbenzene ug/L ND 1.0 07/28/15 13:41
Iodomethane ug/L ND 10.0 07/28/15 13:41
Methylene Chloride ug/L ND 1.0 07/28/15 13:41
Styrene ug/L ND 1.0 07/28/15 13:41
Tetrachloroethene ug/L ND 1.0 07/28/15 13:41
Toluene ug/L ND 1.0 07/28/15 13:41
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519680
Associated Lab Samples:92260261001, 92260261002, 92260261003, 92260261004, 92260261005, 92260261006, 92260261007,
92260261008, 92260261009, 92260261010, 92260261011, 92260261012
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 13:41
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/15 13:41
trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 13:41
Trichloroethene ug/L ND 1.0 07/28/15 13:41
Trichlorofluoromethane ug/L ND 1.0 07/28/15 13:41
Vinyl acetate ug/L ND 50.0 07/28/15 13:41
Vinyl chloride ug/L ND 1.0 07/28/15 13:41
Xylene (Total)ug/L ND 5.0 07/28/15 13:41
1,2-Dichloroethane-d4 (S)%106 70-130 07/28/15 13:41
4-Bromofluorobenzene (S)%103 70-130 07/28/15 13:41
Toluene-d8 (S)%99 70-130 07/28/15 13:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519681LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 80-125
1,1,1-Trichloroethane ug/L 52.150 104 71-129
1,1,2,2-Tetrachloroethane ug/L 55.750 111 79-124
1,1,2-Trichloroethane ug/L 52.650 105 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 51.250 102 66-135
1,2,3-Trichloropropane ug/L 55.250 110 75-130
1,2-Dibromo-3-chloropropane ug/L 51.550 103 71-133
1,2-Dibromoethane (EDB)ug/L 54.450 109 83-124
1,2-Dichlorobenzene ug/L 54.650 109 80-133
1,2-Dichloroethane ug/L 48.450 97 67-128
1,2-Dichloropropane ug/L 48.650 97 75-132
1,3-Dichloropropane ug/L 53.750 107 76-131
1,4-Dichlorobenzene ug/L 52.650 105 78-130
2-Butanone (MEK)ug/L 96.8J100 97 61-144
2-Hexanone ug/L 109100 109 68-143
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 72-135
Acetone ug/L 90.5J100 91 48-146
Acrylonitrile ug/L 224250 90 40-160
Benzene ug/L 51.950 104 80-125
Bromochloromethane ug/L 55.650 111 71-125
Bromodichloromethane ug/L 54.350 109 78-124
Bromoform ug/L 50.550 101 71-128
Bromomethane ug/L 41.650 83 40-160
Carbon disulfide ug/L 46.3J50 93 50-160
Carbon tetrachloride ug/L 54.450 109 69-131
Chlorobenzene ug/L 53.650 107 81-122
Chloroethane ug/L 45.650 91 39-148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Page 32 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519681LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 52.750 105 73-127
Chloromethane ug/L 42.450 85 44-146
cis-1,2-Dichloroethene ug/L 49.850 100 74-124
cis-1,3-Dichloropropene ug/L 52.550 105 72-132
Dibromochloromethane ug/L 54.950 110 78-125
Dibromomethane ug/L 54.450 109 82-120
Ethylbenzene ug/L 54.450 109 79-121
Iodomethane ug/L 90.6100 91 39-154
Methylene Chloride ug/L 49.050 98 64-133
Styrene ug/L 53.150 106 84-126
Tetrachloroethene ug/L 52.750 105 78-122
Toluene ug/L 52.450 105 80-121
trans-1,2-Dichloroethene ug/L 47.850 96 71-127
trans-1,3-Dichloropropene ug/L 53.650 107 69-141
trans-1,4-Dichloro-2-butene ug/L 55.0J50 110 40-160
Trichloroethene ug/L 48.550 97 78-122
Trichlorofluoromethane ug/L 51.650 103 53-137
Vinyl acetate ug/L 101100 101 40-160
Vinyl chloride ug/L 46.250 92 58-137
Xylene (Total)ug/L 159150 106 81-126
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1519682MATRIX SPIKE SAMPLE:
MSSpike
Result
92260223002
1,1,1,2-Tetrachloroethane ug/L 21.120 106 70-130ND
1,1,1-Trichloroethane ug/L 23.120 115 70-130ND
1,1,2,2-Tetrachloroethane ug/L 23.120 116 70-130ND
1,1,2-Trichloroethane ug/L 21.720 108 70-130ND
1,1-Dichloroethane ug/L 21.220 106 70-130ND
1,1-Dichloroethene ug/L 23.420 117 70-166ND
1,2,3-Trichloropropane ug/L 23.620 118 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.120 100 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.320 111 70-130ND
1,2-Dichlorobenzene ug/L 22.820 114 70-130ND
1,2-Dichloroethane ug/L 20.920 103 70-130ND
1,2-Dichloropropane ug/L 20.520 103 70-130ND
1,3-Dichloropropane ug/L 22.120 110 70-130ND
1,4-Dichlorobenzene ug/L 22.020 110 70-130ND
2-Butanone (MEK)ug/L 43.5J40 109 70-130ND
2-Hexanone ug/L 44.5J40 111 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.6J40 111 70-130ND
Acetone ug/L 53.4J40 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 33 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1519682MATRIX SPIKE SAMPLE:
MSSpike
Result
92260223002
Acrylonitrile ug/L 97.4J100 97 70-130ND
Benzene ug/L 22.620 113 70-148ND
Bromochloromethane ug/L 22.920 114 70-130ND
Bromodichloromethane ug/L 22.120 111 70-130ND
Bromoform ug/L 18.520 92 70-130ND
Bromomethane ug/L 10.4 M1205270-130ND
Carbon disulfide ug/L 20.9J20 102 70-130ND
Carbon tetrachloride ug/L 23.520 118 70-130ND
Chlorobenzene ug/L 23.020 115 70-146ND
Chloroethane ug/L 20.720 103 70-130ND
Chloroform ug/L 22.320 111 70-130ND
Chloromethane ug/L 18.920 94 70-130ND
cis-1,2-Dichloroethene ug/L 21.120 106 70-130ND
cis-1,3-Dichloropropene ug/L 20.120 101 70-130ND
Dibromochloromethane ug/L 21.220 106 70-130ND
Dibromomethane ug/L 22.620 113 70-130ND
Ethylbenzene ug/L 23.420 117 70-130ND
Iodomethane ug/L 16.2 M1404070-130ND
Methylene Chloride ug/L 21.320 106 70-130ND
Styrene ug/L 21.520 108 70-130ND
Tetrachloroethene ug/L 22.820 114 70-130ND
Toluene ug/L 22.620 113 70-155ND
trans-1,2-Dichloroethene ug/L 21.120 105 70-130ND
trans-1,3-Dichloropropene ug/L 20.820 104 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.8J20 104 70-130ND
Trichloroethene ug/L 21.120 105 69-151ND
Trichlorofluoromethane ug/L 24.220 121 70-130ND
Vinyl acetate ug/L 36.0J40 90 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92260223004
1519683SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 34 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92260223004
1519683SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 5.2 3 305.4
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%104 1106
4-Bromofluorobenzene (S)%102 0102
Toluene-d8 (S)%100 199
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 35 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/39092
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92260261001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1518626
Associated Lab Samples:92260261001
Matrix:Water
Analyzed
BOD, 5 day ug/L ND 2000 07/29/15 23:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1518627LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 175000198000 88 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92260323002
1518628SAMPLE DUPLICATE:
BOD, 5 day ug/L 19900 2 1020.4 mg/L
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 36 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/39105
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92260261001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92259778001
1518745SAMPLE DUPLICATE:
pH Std. Units 7.7 H6097.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Huntersville, NC 28078
[phone]
Page 37 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23918
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92260261001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1521083
Associated Lab Samples:92260261001
Matrix:Water
Analyzed
Sulfate ug/L ND 250000 07/29/15 14:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1521084LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19700J20000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1521085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260733001
1521086
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 93 90-11092 1 1020000ND20400J20200J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1521087MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260735001
1521088
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 94 90-11094 0 10200004.6 mg/L 23400J 23500J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Huntersville, NC 28078
[phone]
Page 38 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23868
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92260261001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1518622
Associated Lab Samples:92260261001
Matrix:Water
Analyzed
Nitrogen, Nitrate ug/L ND 20.0 07/25/15 00:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1518623LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 25002500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1518624MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260382003
1518625
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 96 90-11097 1 1025000.85 mg/L 3250 3280
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Huntersville, NC 28078
[phone]
Page 39 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23961
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92260261001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1524543
Associated Lab Samples:92260261001
Matrix:Water
Analyzed
Phosphorus ug/L ND 50.0 08/05/15 04:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1524544LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 24402500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1524545MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260787001
1524546
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 96 90-11095 0 1025002.5 mg/L 4860 4840
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1524547MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92261165002
1524548
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 93 90-11096 3 1025000.071
mg/L 2390 2460
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/05/2015 03:15 PM
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Huntersville, NC 28078
[phone]
Page 40 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/23877
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92260261001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519010
Associated Lab Samples:92260261001
Matrix:Water
Analyzed
Chemical Oxygen Demand ug/L ND 25000 07/27/15 15:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519011LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 741000750000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1519012MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260186003
1519013
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M17500001090-11010 0 375000028.0 mg/L 100000 100000
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 41 of 45
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analysis initiated outside of the 15 minute EPA recommended holding time.H6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 42 of 45
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92260261
IREDELL LINED 3&4
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92260261001 MPRP/19105 ICP/17174FORCEMAINEPA 3010 EPA 6010
92260261002 MPRP/19105 ICP/17174MW-17 EPA 3010 EPA 6010
92260261003 MPRP/19105 ICP/17174MW-18 EPA 3010 EPA 6010
92260261004 MPRP/19105 ICP/17174MW-19SR EPA 3010 EPA 6010
92260261005 MPRP/19105 ICP/17174MW-19D EPA 3010 EPA 6010
92260261006 MPRP/19105 ICP/17174MW-21S EPA 3010 EPA 6010
92260261007 MPRP/19105 ICP/17174MW-21D EPA 3010 EPA 6010
92260261008 MPRP/19105 ICP/17174MW-27S EPA 3010 EPA 6010
92260261009 MPRP/19105 ICP/17174MW-27D EPA 3010 EPA 6010
92260261010 MPRP/19105 ICP/17174MW-28 EPA 3010 EPA 6010
92260261011 MPRP/19105 ICP/17174MW-29 EPA 3010 EPA 6010
92260261012 MPRP/19105 ICP/17174MW-30 EPA 3010 EPA 6010
92260261001 MSV/32734FORCEMAINEPA 8260
92260261002 MSV/32734MW-17 EPA 8260
92260261003 MSV/32734MW-18 EPA 8260
92260261004 MSV/32734MW-19SR EPA 8260
92260261005 MSV/32734MW-19D EPA 8260
92260261006 MSV/32734MW-21S EPA 8260
92260261007 MSV/32734MW-21D EPA 8260
92260261008 MSV/32734MW-27S EPA 8260
92260261009 MSV/32734MW-27D EPA 8260
92260261010 MSV/32734MW-28 EPA 8260
92260261011 MSV/32734MW-29 EPA 8260
92260261012 MSV/32734MW-30 EPA 8260
92260261001 WET/39092 WET/39095FORCEMAINSM 5210B SM 5210B
92260261001 WET/39105FORCEMAINEPA 9040
92260261001 WETA/23918FORCEMAINEPA 300.0
92260261001 WETA/23868FORCEMAINEPA 353.2
92260261001 WETA/23961FORCEMAINEPA 365.1
92260261001 WETA/23877FORCEMAINSM 5220D
REPORT OF LABORATORY ANALYSIS
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Page 43 of 45
Page 44 of 45
Page 45 of 45
#=CL#
July 29, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92260081
92260081
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
IREDELL SW-1_5
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 23, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 17
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Lab ID Sample ID Matrix Date Collected Date Received
92260081001 SW-1 Water 07/21/15 11:35 07/23/15 13:05
92260081002 SW-5 Water 07/21/15 12:00 07/23/15 13:05
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92260081001 SW-1 EPA 6010 15 PASI-AJDA
EPA 8260 51 PASI-CSNP
92260081002 SW-5 EPA 6010 15 PASI-AJDA
EPA 8260 51 PASI-CSNP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Sample:SW-1 Lab ID:92260081001 Collected:07/21/15 11:35 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/29/15 05:36 7440-36-007/24/15 19:006.0 3.8 1
Arsenic ND ug/L 07/29/15 05:36 7440-38-207/24/15 19:0010.0 2.5 1
Barium 23.1J ug/L 07/29/15 05:36 7440-39-307/24/15 19:001002.5 1
Beryllium ND ug/L 07/29/15 05:36 7440-41-707/24/15 19:001.0 0.50 1
Cadmium ND ug/L 07/29/15 05:36 7440-43-907/24/15 19:001.0 0.50 1
Chromium ND ug/L 07/29/15 05:36 7440-47-307/24/15 19:0010.0 2.5 1
Cobalt ND ug/L 07/29/15 05:36 7440-48-407/24/15 19:0010.0 2.5 1
Copper ND ug/L 07/29/15 05:36 7440-50-807/24/15 19:0010.0 2.5 1
Lead ND ug/L 07/29/15 05:36 7439-92-107/24/15 19:0010.0 2.5 1
Nickel ND ug/L 07/29/15 05:36 7440-02-007/24/15 19:0050.0 2.5 1
Selenium ND ug/L 07/29/15 05:36 7782-49-207/24/15 19:0010.0 5.0 1
Silver ND ug/L 07/29/15 05:36 7440-22-407/24/15 19:0010.0 2.5 1
Thallium ND ug/L 07/29/15 05:36 7440-28-007/24/15 19:005.5 5.0 1
Vanadium ND ug/L 07/29/15 05:36 7440-62-207/24/15 19:0025.0 2.5 1
Zinc ND ug/L 07/29/15 05:36 7440-66-607/24/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 10:33 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 10:33 107-13-12001.9 1
Benzene ND ug/L 07/28/15 10:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 10:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 10:33 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 10:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 10:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 10:33 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 10:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 10:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 10:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 10:33 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 10:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 10:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 10:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 10:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 10:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 10:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 10:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 10:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 10:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 10:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 10:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 10:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 10:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 10:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 10:33 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 10:33 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 10:33 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/29/2015 02:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Sample:SW-1 Lab ID:92260081001 Collected:07/21/15 11:35 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 10:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 10:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 10:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 10:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 10:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 10:33 108-10-11000.33 1
Styrene ND ug/L 07/28/15 10:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 10:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 10:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 10:33 127-18-41.0 0.46 1
Toluene ND ug/L 07/28/15 10:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 10:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 10:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 10:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 10:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 10:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 10:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 10:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 10:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %07/28/15 10:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 10:33 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 10:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/29/2015 02:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Sample:SW-5 Lab ID:92260081002 Collected:07/21/15 12:00 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/29/15 05:39 7440-36-007/24/15 19:006.0 3.8 1
Arsenic ND ug/L 07/29/15 05:39 7440-38-207/24/15 19:0010.0 2.5 1
Barium 22.8J ug/L 07/29/15 05:39 7440-39-307/24/15 19:001002.5 1
Beryllium ND ug/L 07/29/15 05:39 7440-41-707/24/15 19:001.0 0.50 1
Cadmium ND ug/L 07/29/15 05:39 7440-43-907/24/15 19:001.0 0.50 1
Chromium ND ug/L 07/29/15 05:39 7440-47-307/24/15 19:0010.0 2.5 1
Cobalt ND ug/L 07/29/15 05:39 7440-48-407/24/15 19:0010.0 2.5 1
Copper ND ug/L 07/29/15 05:39 7440-50-807/24/15 19:0010.0 2.5 1
Lead ND ug/L 07/29/15 05:39 7439-92-107/24/15 19:0010.0 2.5 1
Nickel ND ug/L 07/29/15 05:39 7440-02-007/24/15 19:0050.0 2.5 1
Selenium ND ug/L 07/29/15 05:39 7782-49-207/24/15 19:0010.0 5.0 1
Silver ND ug/L 07/29/15 05:39 7440-22-407/24/15 19:0010.0 2.5 1
Thallium ND ug/L 07/29/15 05:39 7440-28-007/24/15 19:005.5 5.0 1
Vanadium ND ug/L 07/29/15 05:39 7440-62-207/24/15 19:0025.0 2.5 1
Zinc ND ug/L 07/29/15 05:39 7440-66-607/24/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 10:50 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 10:50 107-13-12001.9 1
Benzene ND ug/L 07/28/15 10:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 10:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 10:50 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 10:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 10:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 10:50 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 10:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 10:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 10:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 10:50 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 10:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 10:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 10:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 10:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 10:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 10:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 10:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 10:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 10:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 10:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 10:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 10:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 10:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 10:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 10:50 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 10:50 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 10:50 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/29/2015 02:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Sample:SW-5 Lab ID:92260081002 Collected:07/21/15 12:00 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 10:50 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 10:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 10:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 10:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 10:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 10:50 108-10-11000.33 1
Styrene ND ug/L 07/28/15 10:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 10:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 10:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 10:50 127-18-41.0 0.46 1
Toluene 0.27J ug/L 07/28/15 10:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 10:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 10:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 10:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 10:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 10:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 10:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 10:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 10:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %07/28/15 10:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %07/28/15 10:50 17060-07-070-130 1
Toluene-d8 (S)102 %07/28/15 10:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/29/2015 02:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19085
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92260081001, 92260081002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1517918
Associated Lab Samples:92260081001, 92260081002
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 07/29/15 04:12
Arsenic ug/L ND 10.0 07/29/15 04:12
Barium ug/L ND 100 07/29/15 04:12
Beryllium ug/L ND 1.0 07/29/15 04:12
Cadmium ug/L ND 1.0 07/29/15 04:12
Chromium ug/L ND 10.0 07/29/15 04:12
Cobalt ug/L ND 10.0 07/29/15 04:12
Copper ug/L ND 10.0 07/29/15 04:12
Lead ug/L ND 10.0 07/29/15 04:12
Nickel ug/L ND 50.0 07/29/15 04:12
Selenium ug/L ND 10.0 07/29/15 04:12
Silver ug/L ND 10.0 07/29/15 04:12
Thallium ug/L ND 5.5 07/29/15 04:12
Vanadium ug/L ND 25.0 07/29/15 04:12
Zinc ug/L ND 10.0 07/29/15 04:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1517919LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 439500 88 80-120
Arsenic ug/L 419500 84 80-120
Barium ug/L 431500 86 80-120
Beryllium ug/L 433500 87 80-120
Cadmium ug/L 429500 86 80-120
Chromium ug/L 426500 85 80-120
Cobalt ug/L 433500 87 80-120
Copper ug/L 431500 86 80-120
Lead ug/L 435500 87 80-120
Nickel ug/L 426500 85 80-120
Selenium ug/L 416500 83 80-120
Silver ug/L 213250 85 80-120
Thallium ug/L 434500 87 80-120
Vanadium ug/L 436500 87 80-120
Zinc ug/L 428500 86 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/29/2015 02:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1517920MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260066005
1517921
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 87 75-125101 14 25500ND438505
Arsenic ug/L 500 83 75-12597 15 25500ND417485
Barium ug/L 500 86 75-125100 13 2550087.4J 518 588
Beryllium ug/L 500 87 75-125100 14 25500ND435501
Cadmium ug/L 500 86 75-12599 14 25500ND430496
Chromium ug/L 500 86 75-12599 14 255004.1J 432 499
Cobalt ug/L 500 86 75-125100 14 25500ND432499
Copper ug/L 500 86 75-125100 15 25500ND432501
Lead ug/L 500 87 75-125100 14 25500ND433499
Nickel ug/L 500 85 75-12598 14 25500ND427494
Selenium ug/L 500 82 75-12596 15 25500ND414480
Silver ug/L 250 85 75-12599 14 25250ND214247
Thallium ug/L 500 87 75-125101 15 25500ND435504
Vanadium ug/L 500 87 75-125101 14 25500ND439507
Zinc ug/L 500 85 75-12599 15 255009.1J 436 504
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/29/2015 02:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32722
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92260081001, 92260081002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519232
Associated Lab Samples:92260081001, 92260081002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 04:10
1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 04:10
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 04:10
1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 04:10
1,1-Dichloroethane ug/L ND 5.0 07/28/15 04:10
1,1-Dichloroethene ug/L ND 5.0 07/28/15 04:10
1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 04:10
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 04:10
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/15 04:10
1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 04:10
1,2-Dichloroethane ug/L ND 1.0 07/28/15 04:10
1,2-Dichloropropane ug/L ND 1.0 07/28/15 04:10
1,3-Dichloropropane ug/L ND 1.0 07/28/15 04:10
1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 04:10
2-Butanone (MEK)ug/L ND 100 07/28/15 04:10
2-Hexanone ug/L ND 50.0 07/28/15 04:10
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/28/15 04:10
Acetone ug/L ND 100 07/28/15 04:10
Acrylonitrile ug/L ND 200 07/28/15 04:10
Benzene ug/L ND 1.0 07/28/15 04:10
Bromochloromethane ug/L ND 3.0 07/28/15 04:10
Bromodichloromethane ug/L ND 1.0 07/28/15 04:10
Bromoform ug/L ND 3.0 07/28/15 04:10
Bromomethane ug/L ND 10.0 07/28/15 04:10
Carbon disulfide ug/L ND 100 07/28/15 04:10
Carbon tetrachloride ug/L ND 1.0 07/28/15 04:10
Chlorobenzene ug/L ND 3.0 07/28/15 04:10
Chloroethane ug/L ND 10.0 07/28/15 04:10
Chloroform ug/L ND 5.0 07/28/15 04:10
Chloromethane ug/L ND 1.0 07/28/15 04:10
cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10
Dibromochloromethane ug/L ND 3.0 07/28/15 04:10
Dibromomethane ug/L ND 10.0 07/28/15 04:10
Ethylbenzene ug/L ND 1.0 07/28/15 04:10
Iodomethane ug/L ND 10.0 07/28/15 04:10
Methylene Chloride ug/L ND 1.0 07/28/15 04:10
Styrene ug/L ND 1.0 07/28/15 04:10
Tetrachloroethene ug/L ND 1.0 07/28/15 04:10
Toluene ug/L ND 1.0 07/28/15 04:10
trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10
REPORT OF LABORATORY ANALYSIS
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Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519232
Associated Lab Samples:92260081001, 92260081002
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10
trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 04:10
Trichloroethene ug/L ND 1.0 07/28/15 04:10
Trichlorofluoromethane ug/L ND 1.0 07/28/15 04:10
Vinyl acetate ug/L ND 50.0 07/28/15 04:10
Vinyl chloride ug/L ND 1.0 07/28/15 04:10
Xylene (Total)ug/L ND 5.0 07/28/15 04:10
1,2-Dichloroethane-d4 (S)%105 70-130 07/28/15 04:10
4-Bromofluorobenzene (S)%100 70-130 07/28/15 04:10
Toluene-d8 (S)%99 70-130 07/28/15 04:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519233LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.450 101 80-125
1,1,1-Trichloroethane ug/L 52.150 104 71-129
1,1,2,2-Tetrachloroethane ug/L 54.450 109 79-124
1,1,2-Trichloroethane ug/L 52.350 105 85-125
1,1-Dichloroethane ug/L 48.750 97 73-126
1,1-Dichloroethene ug/L 51.150 102 66-135
1,2,3-Trichloropropane ug/L 55.150 110 75-130
1,2-Dibromo-3-chloropropane ug/L 52.150 104 71-133
1,2-Dibromoethane (EDB)ug/L 53.250 106 83-124
1,2-Dichlorobenzene ug/L 54.050 108 80-133
1,2-Dichloroethane ug/L 48.750 97 67-128
1,2-Dichloropropane ug/L 50.150 100 75-132
1,3-Dichloropropane ug/L 52.150 104 76-131
1,4-Dichlorobenzene ug/L 52.550 105 78-130
2-Butanone (MEK)ug/L 100100 100 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 239250 96 40-160
Benzene ug/L 51.550 103 80-125
Bromochloromethane ug/L 54.350 109 71-125
Bromodichloromethane ug/L 54.550 109 78-124
Bromoform ug/L 49.450 99 71-128
Bromomethane ug/L 43.550 87 40-160
Carbon disulfide ug/L 45.8J50 92 50-160
Carbon tetrachloride ug/L 54.750 109 69-131
Chlorobenzene ug/L 51.050 102 81-122
Chloroethane ug/L 46.050 92 39-148
Chloroform ug/L 51.750 103 73-127
Chloromethane ug/L 43.750 87 44-146
REPORT OF LABORATORY ANALYSIS
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Page 12 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519233LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.150 100 74-124
cis-1,3-Dichloropropene ug/L 51.450 103 72-132
Dibromochloromethane ug/L 52.650 105 78-125
Dibromomethane ug/L 55.250 110 82-120
Ethylbenzene ug/L 51.450 103 79-121
Iodomethane ug/L 89.1100 89 39-154
Methylene Chloride ug/L 51.050 102 64-133
Styrene ug/L 50.850 102 84-126
Tetrachloroethene ug/L 50.350 101 78-122
Toluene ug/L 52.850 106 80-121
trans-1,2-Dichloroethene ug/L 47.950 96 71-127
trans-1,3-Dichloropropene ug/L 51.050 102 69-141
trans-1,4-Dichloro-2-butene ug/L 53.1J50 106 40-160
Trichloroethene ug/L 49.450 99 78-122
Trichlorofluoromethane ug/L 50.850 102 53-137
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 46.350 93 58-137
Xylene (Total)ug/L 152150 101 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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Page 13 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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Page 14 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92260081
IREDELL SW-1_5
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92260081001 MPRP/19085 ICP/17163SW-1 EPA 3010 EPA 6010
92260081002 MPRP/19085 ICP/17163SW-5 EPA 3010 EPA 6010
92260081001 MSV/32722SW-1 EPA 8260
92260081002 MSV/32722SW-5 EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 15 of 17
Page 16 of 17
Page 17 of 17
#=CL#
July 30, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92260075
92260075
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
IREDELL SW-2
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 23, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 15
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92260075
IREDELL SW-2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 15
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92260075
IREDELL SW-2
Lab ID Sample ID Matrix Date Collected Date Received
92260075001 SW-2 Water 07/21/15 17:30 07/23/15 13:05
REPORT OF LABORATORY ANALYSIS
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Page 3 of 15
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92260075
IREDELL SW-2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92260075001 SW-2 EPA 6010 15 PASI-AJDA
EPA 8260 52 PASI-CSNP
REPORT OF LABORATORY ANALYSIS
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Page 4 of 15
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260075
IREDELL SW-2
Sample:SW-2 Lab ID:92260075001 Collected:07/21/15 17:30 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 07/29/15 05:32 7440-36-007/24/15 19:006.0 3.8 1
Arsenic ND ug/L 07/29/15 05:32 7440-38-207/24/15 19:0010.0 2.5 1
Barium 31.0J ug/L 07/29/15 05:32 7440-39-307/24/15 19:001002.5 1
Beryllium ND ug/L 07/29/15 05:32 7440-41-707/24/15 19:001.0 0.50 1
Cadmium ND ug/L 07/29/15 05:32 7440-43-907/24/15 19:001.0 0.50 1
Chromium ND ug/L 07/29/15 05:32 7440-47-307/24/15 19:0010.0 2.5 1
Cobalt ND ug/L 07/29/15 05:32 7440-48-407/24/15 19:0010.0 2.5 1
Copper ND ug/L 07/29/15 05:32 7440-50-807/24/15 19:0010.0 2.5 1
Lead ND ug/L 07/29/15 05:32 7439-92-107/24/15 19:0010.0 2.5 1
Nickel ND ug/L 07/29/15 05:32 7440-02-007/24/15 19:0050.0 2.5 1
Selenium ND ug/L 07/29/15 05:32 7782-49-207/24/15 19:0010.0 5.0 1
Silver ND ug/L 07/29/15 05:32 7440-22-407/24/15 19:0010.0 2.5 1
Thallium ND ug/L 07/29/15 05:32 7440-28-007/24/15 19:005.5 5.0 1
Vanadium ND ug/L 07/29/15 05:32 7440-62-207/24/15 19:0025.0 2.5 1
Zinc ND ug/L 07/29/15 05:32 7440-66-607/24/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 10:17 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 10:17 107-13-12001.9 1
Benzene ND ug/L 07/28/15 10:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 10:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 10:17 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 10:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 10:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 10:17 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 10:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 10:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 10:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 10:17 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 10:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 10:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 10:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 10:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 10:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 10:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 10:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 10:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 10:17 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 10:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 10:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 10:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 10:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 10:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 10:17 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 10:17 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 10:17 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 15
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260075
IREDELL SW-2
Sample:SW-2 Lab ID:92260075001 Collected:07/21/15 17:30 Received:07/23/15 13:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 10:17 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 10:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 10:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 10:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 10:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 10:17 108-10-11000.33 1
Styrene ND ug/L 07/28/15 10:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 10:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 10:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 10:17 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 10:17 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 10:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 10:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 10:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 10:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 10:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 10:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 10:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 10:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 10:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 10:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %07/28/15 10:17 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 10:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260075
IREDELL SW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19085
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92260075001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1517918
Associated Lab Samples:92260075001
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 07/29/15 04:12
Arsenic ug/L ND 10.0 07/29/15 04:12
Barium ug/L ND 100 07/29/15 04:12
Beryllium ug/L ND 1.0 07/29/15 04:12
Cadmium ug/L ND 1.0 07/29/15 04:12
Chromium ug/L ND 10.0 07/29/15 04:12
Cobalt ug/L ND 10.0 07/29/15 04:12
Copper ug/L ND 10.0 07/29/15 04:12
Lead ug/L ND 10.0 07/29/15 04:12
Nickel ug/L ND 50.0 07/29/15 04:12
Selenium ug/L ND 10.0 07/29/15 04:12
Silver ug/L ND 10.0 07/29/15 04:12
Thallium ug/L ND 5.5 07/29/15 04:12
Vanadium ug/L ND 25.0 07/29/15 04:12
Zinc ug/L ND 10.0 07/29/15 04:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1517919LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 439500 88 80-120
Arsenic ug/L 419500 84 80-120
Barium ug/L 431500 86 80-120
Beryllium ug/L 433500 87 80-120
Cadmium ug/L 429500 86 80-120
Chromium ug/L 426500 85 80-120
Cobalt ug/L 433500 87 80-120
Copper ug/L 431500 86 80-120
Lead ug/L 435500 87 80-120
Nickel ug/L 426500 85 80-120
Selenium ug/L 416500 83 80-120
Silver ug/L 213250 85 80-120
Thallium ug/L 434500 87 80-120
Vanadium ug/L 436500 87 80-120
Zinc ug/L 428500 86 80-120
REPORT OF LABORATORY ANALYSIS
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Page 7 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260075
IREDELL SW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1517920MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260066005
1517921
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 87 75-125101 14 25500ND438505
Arsenic ug/L 500 83 75-12597 15 25500ND417485
Barium ug/L 500 86 75-125100 13 2550087.4J 518 588
Beryllium ug/L 500 87 75-125100 14 25500ND435501
Cadmium ug/L 500 86 75-12599 14 25500ND430496
Chromium ug/L 500 86 75-12599 14 255004.1J 432 499
Cobalt ug/L 500 86 75-125100 14 25500ND432499
Copper ug/L 500 86 75-125100 15 25500ND432501
Lead ug/L 500 87 75-125100 14 25500ND433499
Nickel ug/L 500 85 75-12598 14 25500ND427494
Selenium ug/L 500 82 75-12596 15 25500ND414480
Silver ug/L 250 85 75-12599 14 25250ND214247
Thallium ug/L 500 87 75-125101 15 25500ND435504
Vanadium ug/L 500 87 75-125101 14 25500ND439507
Zinc ug/L 500 85 75-12599 15 255009.1J 436 504
REPORT OF LABORATORY ANALYSIS
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Page 8 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260075
IREDELL SW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32722
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92260075001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519232
Associated Lab Samples:92260075001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 04:10
1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 04:10
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 04:10
1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 04:10
1,1-Dichloroethane ug/L ND 5.0 07/28/15 04:10
1,1-Dichloroethene ug/L ND 5.0 07/28/15 04:10
1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 04:10
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 04:10
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/15 04:10
1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 04:10
1,2-Dichloroethane ug/L ND 1.0 07/28/15 04:10
1,2-Dichloropropane ug/L ND 1.0 07/28/15 04:10
1,3-Dichloropropane ug/L ND 1.0 07/28/15 04:10
1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 04:10
2-Butanone (MEK)ug/L ND 100 07/28/15 04:10
2-Hexanone ug/L ND 50.0 07/28/15 04:10
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/28/15 04:10
Acetone ug/L ND 100 07/28/15 04:10
Acrylonitrile ug/L ND 200 07/28/15 04:10
Benzene ug/L ND 1.0 07/28/15 04:10
Bromochloromethane ug/L ND 3.0 07/28/15 04:10
Bromodichloromethane ug/L ND 1.0 07/28/15 04:10
Bromoform ug/L ND 3.0 07/28/15 04:10
Bromomethane ug/L ND 10.0 07/28/15 04:10
Carbon disulfide ug/L ND 100 07/28/15 04:10
Carbon tetrachloride ug/L ND 1.0 07/28/15 04:10
Chlorobenzene ug/L ND 3.0 07/28/15 04:10
Chloroethane ug/L ND 10.0 07/28/15 04:10
Chloroform ug/L ND 5.0 07/28/15 04:10
Chloromethane ug/L ND 1.0 07/28/15 04:10
cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10
Dibromochloromethane ug/L ND 3.0 07/28/15 04:10
Dibromomethane ug/L ND 10.0 07/28/15 04:10
Ethylbenzene ug/L ND 1.0 07/28/15 04:10
Iodomethane ug/L ND 10.0 07/28/15 04:10
Methylene Chloride ug/L ND 1.0 07/28/15 04:10
Styrene ug/L ND 1.0 07/28/15 04:10
Tetrachloroethene ug/L ND 1.0 07/28/15 04:10
Tetrahydrofuran ug/L ND 10.0 07/28/15 04:10
Toluene ug/L ND 1.0 07/28/15 04:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/30/2015 08:58 AM
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Page 9 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260075
IREDELL SW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519232
Associated Lab Samples:92260075001
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10
trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 04:10
Trichloroethene ug/L ND 1.0 07/28/15 04:10
Trichlorofluoromethane ug/L ND 1.0 07/28/15 04:10
Vinyl acetate ug/L ND 50.0 07/28/15 04:10
Vinyl chloride ug/L ND 1.0 07/28/15 04:10
Xylene (Total)ug/L ND 5.0 07/28/15 04:10
1,2-Dichloroethane-d4 (S)%105 70-130 07/28/15 04:10
4-Bromofluorobenzene (S)%100 70-130 07/28/15 04:10
Toluene-d8 (S)%99 70-130 07/28/15 04:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519233LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.450 101 80-125
1,1,1-Trichloroethane ug/L 52.150 104 71-129
1,1,2,2-Tetrachloroethane ug/L 54.450 109 79-124
1,1,2-Trichloroethane ug/L 52.350 105 85-125
1,1-Dichloroethane ug/L 48.750 97 73-126
1,1-Dichloroethene ug/L 51.150 102 66-135
1,2,3-Trichloropropane ug/L 55.150 110 75-130
1,2-Dibromo-3-chloropropane ug/L 52.150 104 71-133
1,2-Dibromoethane (EDB)ug/L 53.250 106 83-124
1,2-Dichlorobenzene ug/L 54.050 108 80-133
1,2-Dichloroethane ug/L 48.750 97 67-128
1,2-Dichloropropane ug/L 50.150 100 75-132
1,3-Dichloropropane ug/L 52.150 104 76-131
1,4-Dichlorobenzene ug/L 52.550 105 78-130
2-Butanone (MEK)ug/L 100100 100 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 239250 96 40-160
Benzene ug/L 51.550 103 80-125
Bromochloromethane ug/L 54.350 109 71-125
Bromodichloromethane ug/L 54.550 109 78-124
Bromoform ug/L 49.450 99 71-128
Bromomethane ug/L 43.550 87 40-160
Carbon disulfide ug/L 45.8J50 92 50-160
Carbon tetrachloride ug/L 54.750 109 69-131
Chlorobenzene ug/L 51.050 102 81-122
Chloroethane ug/L 46.050 92 39-148
Chloroform ug/L 51.750 103 73-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/30/2015 08:58 AM
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Page 10 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260075
IREDELL SW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519233LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 43.750 87 44-146
cis-1,2-Dichloroethene ug/L 50.150 100 74-124
cis-1,3-Dichloropropene ug/L 51.450 103 72-132
Dibromochloromethane ug/L 52.650 105 78-125
Dibromomethane ug/L 55.250 110 82-120
Ethylbenzene ug/L 51.450 103 79-121
Iodomethane ug/L 89.1100 89 39-154
Methylene Chloride ug/L 51.050 102 64-133
Styrene ug/L 50.850 102 84-126
Tetrachloroethene ug/L 50.350 101 78-122
Tetrahydrofuran ug/L 508500 102 69-148
Toluene ug/L 52.850 106 80-121
trans-1,2-Dichloroethene ug/L 47.950 96 71-127
trans-1,3-Dichloropropene ug/L 51.050 102 69-141
trans-1,4-Dichloro-2-butene ug/L 53.1J50 106 40-160
Trichloroethene ug/L 49.450 99 78-122
Trichlorofluoromethane ug/L 50.850 102 53-137
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 46.350 93 58-137
Xylene (Total)ug/L 152150 101 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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Page 11 of 15
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92260075
IREDELL SW-2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/30/2015 08:58 AM
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Page 12 of 15
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92260075
IREDELL SW-2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92260075001 MPRP/19085 ICP/17163SW-2 EPA 3010 EPA 6010
92260075001 MSV/32722SW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/30/2015 08:58 AM
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[phone]
Page 13 of 15
Page 14 of 15
Page 15 of 15
#=CL#
August 04, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92260267
92260267
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
IREDELL BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92260267001 EB Water 07/23/15 17:35 07/24/15 11:49
92260267002 FB Water 07/23/15 17:40 07/24/15 11:49
92260267003 TB Water 07/23/15 00:00 07/24/15 11:49
REPORT OF LABORATORY ANALYSIS
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Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92260267001 EB EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CSNP
92260267002 FB EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CSNP
92260267003 TB EPA 8260 52 PASI-CSNP
REPORT OF LABORATORY ANALYSIS
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Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:EB Lab ID:92260267001 Collected:07/23/15 17:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:36 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:36 7440-38-207/27/15 19:0010.0 2.5 1
Barium ND ug/L 08/04/15 03:36 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:36 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:36 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:36 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:36 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:36 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:36 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:36 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:36 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:36 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:36 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:36 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:36 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 19:48 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 19:48 107-13-12001.9 1
Benzene ND ug/L 07/28/15 19:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 19:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 19:48 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 19:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 19:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 19:48 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 19:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 19:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 19:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 19:48 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 19:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 19:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 19:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 19:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 19:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 19:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 19:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 19:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 19:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 19:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 19:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 19:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 19:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 19:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 19:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 19:48 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 19:48 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:EB Lab ID:92260267001 Collected:07/23/15 17:35 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 19:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 19:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 19:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 19:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 19:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 19:48 108-10-11000.33 1
Styrene ND ug/L 07/28/15 19:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 19:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 19:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 19:48 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 19:48 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 19:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 19:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 19:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 19:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 19:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 19:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 19:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 19:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 19:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %07/28/15 19:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/15 19:48 17060-07-070-130 1
Toluene-d8 (S)100 %07/28/15 19:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:FB Lab ID:92260267002 Collected:07/23/15 17:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 08/04/15 03:39 7440-36-007/27/15 19:006.0 3.8 1
Arsenic ND ug/L 08/04/15 03:39 7440-38-207/27/15 19:0010.0 2.5 1
Barium ND ug/L 08/04/15 03:39 7440-39-307/27/15 19:001002.5 1
Beryllium ND ug/L 08/04/15 03:39 7440-41-707/27/15 19:001.0 0.50 1
Cadmium ND ug/L 08/04/15 03:39 7440-43-907/27/15 19:001.0 0.50 1
Chromium ND ug/L 08/04/15 03:39 7440-47-307/27/15 19:0010.0 2.5 1
Cobalt ND ug/L 08/04/15 03:39 7440-48-407/27/15 19:0010.0 2.5 1
Copper ND ug/L 08/04/15 03:39 7440-50-807/27/15 19:0010.0 2.5 1
Lead ND ug/L 08/04/15 03:39 7439-92-107/27/15 19:0010.0 2.5 1
Nickel ND ug/L 08/04/15 03:39 7440-02-007/27/15 19:0050.0 2.5 1
Selenium ND ug/L 08/04/15 03:39 7782-49-207/27/15 19:0010.0 5.0 1
Silver ND ug/L 08/04/15 03:39 7440-22-407/27/15 19:0010.0 2.5 1
Thallium ND ug/L 08/04/15 03:39 7440-28-007/27/15 19:005.5 5.0 1
Vanadium ND ug/L 08/04/15 03:39 7440-62-207/27/15 19:0025.0 2.5 1
Zinc ND ug/L 08/04/15 03:39 7440-66-607/27/15 19:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 20:04 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 20:04 107-13-12001.9 1
Benzene ND ug/L 07/28/15 20:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 20:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 20:04 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 20:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 20:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 20:04 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 20:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 20:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 20:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 20:04 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 20:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 20:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 20:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 20:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 20:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 20:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 20:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 20:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 20:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 20:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 20:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 20:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 20:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 20:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 20:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 20:04 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 20:04 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:FB Lab ID:92260267002 Collected:07/23/15 17:40 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 07/28/15 20:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 20:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 20:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 20:04 74-88-410.0 0.32 1
Methylene Chloride 0.99J ug/L 07/28/15 20:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 20:04 108-10-11000.33 1
Styrene ND ug/L 07/28/15 20:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 20:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 20:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 20:04 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 20:04 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 20:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 20:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 20:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 20:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 20:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 20:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/28/15 20:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 20:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 20:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %07/28/15 20:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %07/28/15 20:04 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 20:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:TB Lab ID:92260267003 Collected:07/23/15 00:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 07/28/15 20:21 67-64-110010.0 1
Acrylonitrile ND ug/L 07/28/15 20:21 107-13-12001.9 1
Benzene ND ug/L 07/28/15 20:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/28/15 20:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/28/15 20:21 75-27-41.0 0.18 1
Bromoform ND ug/L 07/28/15 20:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/28/15 20:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/28/15 20:21 78-93-31000.96 1
Carbon disulfide ND ug/L 07/28/15 20:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/28/15 20:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/28/15 20:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/28/15 20:21 75-00-310.0 0.54 1
Chloroform ND ug/L 07/28/15 20:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/28/15 20:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/15 20:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/28/15 20:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/15 20:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/28/15 20:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/28/15 20:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/28/15 20:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/28/15 20:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/28/15 20:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/28/15 20:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/28/15 20:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/28/15 20:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/28/15 20:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/28/15 20:21 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 07/28/15 20:21 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 07/28/15 20:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/28/15 20:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/28/15 20:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/28/15 20:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/28/15 20:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/28/15 20:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/28/15 20:21 108-10-11000.33 1
Styrene ND ug/L 07/28/15 20:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/15 20:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/15 20:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/28/15 20:21 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 07/28/15 20:21 109-99-910.0 3.1 1
Toluene ND ug/L 07/28/15 20:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/28/15 20:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/28/15 20:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/28/15 20:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/28/15 20:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/28/15 20:21 96-18-41.0 0.41 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Sample:TB Lab ID:92260267003 Collected:07/23/15 00:00 Received:07/24/15 11:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl acetate ND ug/L 07/28/15 20:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/28/15 20:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/28/15 20:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %07/28/15 20:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %07/28/15 20:21 17060-07-070-130 1
Toluene-d8 (S)101 %07/28/15 20:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19105
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92260267001, 92260267002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519047
Associated Lab Samples:92260267001, 92260267002
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 08/04/15 02:28
Arsenic ug/L ND 10.0 08/04/15 02:28
Barium ug/L ND 100 08/04/15 02:28
Beryllium ug/L ND 1.0 08/04/15 02:28
Cadmium ug/L ND 1.0 08/04/15 02:28
Chromium ug/L ND 10.0 08/04/15 02:28
Cobalt ug/L ND 10.0 08/04/15 02:28
Copper ug/L ND 10.0 08/04/15 02:28
Lead ug/L ND 10.0 08/04/15 02:28
Nickel ug/L ND 50.0 08/04/15 02:28
Selenium ug/L ND 10.0 08/04/15 02:28
Silver ug/L ND 10.0 08/04/15 02:28
Thallium ug/L ND 5.5 08/04/15 02:28
Vanadium ug/L ND 25.0 08/04/15 02:28
Zinc ug/L ND 10.0 08/04/15 02:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519048LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 455500 91 80-120
Barium ug/L 469500 94 80-120
Beryllium ug/L 476500 95 80-120
Cadmium ug/L 464500 93 80-120
Chromium ug/L 479500 96 80-120
Cobalt ug/L 466500 93 80-120
Copper ug/L 470500 94 80-120
Lead ug/L 460500 92 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 447500 89 80-120
Silver ug/L 228250 91 80-120
Thallium ug/L 466500 93 80-120
Vanadium ug/L 473500 95 80-120
Zinc ug/L 464500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1519049MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92260261001
1519050
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12595 1 2550016.0 486 492
Arsenic ug/L 500 95 75-12596 1 2550016.4 492 496
Barium ug/L 500 93 75-125101 3 2550082312901330
Beryllium ug/L 500 94 75-12595 0 25500ND472474
Cadmium ug/L 500 94 75-12595 1 25500ND471475
Chromium ug/L 500 94 75-12595 1 2550038.8 508 515
Cobalt ug/L 500 88 75-12589 1 2550016.0 457 460
Copper ug/L 500 96 75-12599 2 2550029.9 512 524
Lead ug/L 500 85 75-12586 1 255003.5J 430 434
Nickel ug/L 500 86 75-12587 1 25500137569573
Selenium ug/L 500 89 75-12591 2 25500ND447454
Silver ug/L 250 94 75-12595 1 25250ND236239
Thallium ug/L 500 83 75-12583 1 25500ND413417
Vanadium ug/L 500 95 75-12596 1 2550019.9J 495 501
Zinc ug/L 500 89 75-12591 2 2550021.8 469 476
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32735
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92260267001, 92260267002, 92260267003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519691
Associated Lab Samples:92260267001, 92260267002, 92260267003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 13:58
1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 13:58
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 13:58
1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 13:58
1,1-Dichloroethane ug/L ND 5.0 07/28/15 13:58
1,1-Dichloroethene ug/L ND 5.0 07/28/15 13:58
1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 13:58
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 13:58
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/28/15 13:58
1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 13:58
1,2-Dichloroethane ug/L ND 1.0 07/28/15 13:58
1,2-Dichloropropane ug/L ND 1.0 07/28/15 13:58
1,3-Dichloropropane ug/L ND 1.0 07/28/15 13:58
1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 13:58
2-Butanone (MEK)ug/L ND 100 07/28/15 13:58
2-Hexanone ug/L ND 50.0 07/28/15 13:58
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/28/15 13:58
Acetone ug/L ND 100 07/28/15 13:58
Acrylonitrile ug/L ND 200 07/28/15 13:58
Benzene ug/L ND 1.0 07/28/15 13:58
Bromochloromethane ug/L ND 3.0 07/28/15 13:58
Bromodichloromethane ug/L ND 1.0 07/28/15 13:58
Bromoform ug/L ND 3.0 07/28/15 13:58
Bromomethane ug/L ND 10.0 07/28/15 13:58
Carbon disulfide ug/L ND 100 07/28/15 13:58
Carbon tetrachloride ug/L ND 1.0 07/28/15 13:58
Chlorobenzene ug/L ND 3.0 07/28/15 13:58
Chloroethane ug/L ND 10.0 07/28/15 13:58
Chloroform ug/L ND 5.0 07/28/15 13:58
Chloromethane ug/L ND 1.0 07/28/15 13:58
cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 13:58
cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 13:58
Dibromochloromethane ug/L ND 3.0 07/28/15 13:58
Dibromomethane ug/L ND 10.0 07/28/15 13:58
Ethylbenzene ug/L ND 1.0 07/28/15 13:58
Iodomethane ug/L ND 10.0 07/28/15 13:58
Methylene Chloride ug/L ND 1.0 07/28/15 13:58
Styrene ug/L ND 1.0 07/28/15 13:58
Tetrachloroethene ug/L ND 1.0 07/28/15 13:58
Tetrahydrofuran ug/L ND 10.0 07/28/15 13:58
Toluene ug/L ND 1.0 07/28/15 13:58
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1519691
Associated Lab Samples:92260267001, 92260267002, 92260267003
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 13:58
trans-1,3-Dichloropropene ug/L ND 1.0 07/28/15 13:58
trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 13:58
Trichloroethene ug/L ND 1.0 07/28/15 13:58
Trichlorofluoromethane ug/L ND 1.0 07/28/15 13:58
Vinyl acetate ug/L ND 50.0 07/28/15 13:58
Vinyl chloride ug/L ND 1.0 07/28/15 13:58
Xylene (Total)ug/L ND 5.0 07/28/15 13:58
1,2-Dichloroethane-d4 (S)%104 70-130 07/28/15 13:58
4-Bromofluorobenzene (S)%102 70-130 07/28/15 13:58
Toluene-d8 (S)%100 70-130 07/28/15 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519692LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.550 101 80-125
1,1,1-Trichloroethane ug/L 50.150 100 71-129
1,1,2,2-Tetrachloroethane ug/L 52.550 105 79-124
1,1,2-Trichloroethane ug/L 50.850 102 85-125
1,1-Dichloroethane ug/L 46.350 93 73-126
1,1-Dichloroethene ug/L 49.050 98 66-135
1,2,3-Trichloropropane ug/L 53.150 106 75-130
1,2-Dibromo-3-chloropropane ug/L 46.950 94 71-133
1,2-Dibromoethane (EDB)ug/L 51.850 104 83-124
1,2-Dichlorobenzene ug/L 51.850 104 80-133
1,2-Dichloroethane ug/L 46.750 93 67-128
1,2-Dichloropropane ug/L 48.050 96 75-132
1,3-Dichloropropane ug/L 51.250 102 76-131
1,4-Dichlorobenzene ug/L 50.950 102 78-130
2-Butanone (MEK)ug/L 91.9J100 92 61-144
2-Hexanone ug/L 99.9100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 72-135
Acetone ug/L 87.3J100 87 48-146
Acrylonitrile ug/L 221250 89 40-160
Benzene ug/L 49.650 99 80-125
Bromochloromethane ug/L 53.250 106 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 48.850 98 71-128
Bromomethane ug/L 41.050 82 40-160
Carbon disulfide ug/L 44.4J50 89 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 50.850 102 81-122
Chloroethane ug/L 44.050 88 39-148
Chloroform ug/L 49.650 99 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1519692LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 41.050 82 44-146
cis-1,2-Dichloroethene ug/L 47.850 96 74-124
cis-1,3-Dichloropropene ug/L 51.050 102 72-132
Dibromochloromethane ug/L 51.950 104 78-125
Dibromomethane ug/L 52.050 104 82-120
Ethylbenzene ug/L 51.550 103 79-121
Iodomethane ug/L 86.0100 86 39-154
Methylene Chloride ug/L 48.150 96 64-133
Styrene ug/L 50.650 101 84-126
Tetrachloroethene ug/L 49.950 100 78-122
Tetrahydrofuran ug/L 457500 91 69-148
Toluene ug/L 50.950 102 80-121
trans-1,2-Dichloroethene ug/L 46.350 93 71-127
trans-1,3-Dichloropropene ug/L 51.550 103 69-141
trans-1,4-Dichloro-2-butene ug/L 52.2J50 104 40-160
Trichloroethene ug/L 47.050 94 78-122
Trichlorofluoromethane ug/L 49.850 100 53-137
Vinyl acetate ug/L 97.7100 98 40-160
Vinyl chloride ug/L 44.750 89 58-137
Xylene (Total)ug/L 150150 100 81-126
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92260267
IREDELL BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92260267
IREDELL BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92260267001 MPRP/19105 ICP/17174EBEPA 3010 EPA 6010
92260267002 MPRP/19105 ICP/17174FBEPA 3010 EPA 6010
92260267001 MSV/32735EBEPA 8260
92260267002 MSV/32735FBEPA 8260
92260267003 MSV/32735TBEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 08/04/2015 03:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 19
Page 18 of 19
Page 19 of 19
Appendix B
Field Sampling Parameter Data Sheet(s)