3420_ForsythCoOmniSourceLandfillWQMR_DIN28678_20170412

2211 W. Meadowview Rd., #101
Greensboro, NC 27409
tel: [phone]
fax: [phone]
www.JoyceEngineering.com

August 4, 2017

Ms. Jaclynne Drummond
Compliance Hydrogeologist
NC Department of Environmental Quality
Division of Waste Management – Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

RE: First Semiannual Water Quality Monitoring Report of 2017
OmniSource Kernersville Landfill, Permit No. 34-20
Kernersville, North Carolina
JOYCE Project No. 00799.1702.12 Task No. 02

Dear Ms. Drummond:

On behalf of OmniSource Southeast, Joyce Engineering is submitting the First Semiannual
Water Quality Monitoring Report of 2017 for the OmniSource Kernersville Landfill, Permit No.
34-20. The attached report contains electronic versions of the complete report and all appendices
for the April 2016 sampling event. Also attached is the North Carolina Environmental Monitoring
Reporting Form and the associated laboratory EDDs.

If you wish to have a hard copy of the report, drawings, or appendices, we will be happy to
provide it upon your request. Please feel free to contact me or Amy Davis at [phone] if you
have any questions regarding this report.

Sincerely,
JOYCE ENGINEERING

Van Burbach, Ph.D., P.G.
Senior Technical Consultant

Attachment

C: James Winegar, OmniSource Southeast, LLC
Gary Cosentino, OmniSource Kernersville

PREPARED FOR:

OMNISOURCE SOUTHEAST, LLC
2233 WAL-PAT ROAD
SMITHFIELD, NC 27577

OMNISOURCE SOUTHEAST
KERNERSVILLE LANDFILL
PERMIT NO. 34-20

FIRST SEMIANNUAL WATER QUALITY
MONITORING REPORT OF 2017

AUGUST 2017

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE PROJECT NO. 799.1702.12

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First Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering
OmniSource Kernersville Landfill, Permit No. 34-20 August 2017

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First Semiannual Water Quality Monitoring Report of 2017
OmniSource Southeast Landfill, Permit No. 34-20
Kernersville, North Carolina

TABLE OF CONTENTS

1.0 INTRODUCTION ..................................................................................................................1
1.1 Site Information .............................................................................................................. 1
1.2 Site Geology and Hydrogeology ..................................................................................... 1
1.3 Regulatory Status ............................................................................................................ 2

2.0 FACILITY MONITORING PROGRAM ...............................................................................2
2.1 Groundwater Monitoring Program ................................................................................. 2
2.2 Surface Water Monitoring Program ................................................................................ 2

3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2017........................................................3
3.1 Field Work and Visual Inspection .................................................................................. 3
3.2 Laboratory Analysis and Quality Control ....................................................................... 4

4.0 DATA ANALYSIS .................................................................................................................4
4.1 Groundwater Data Analysis and Comparisons to Standards .......................................... 4
4.2 Surface Water Data Analysis and Comparisons to Standards ........................................ 5

5.0 CONCLUSIONS.....................................................................................................................6

6.0 REFERENCES .......................................................................................................................6

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First Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering
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TABLE OF CONTENCTS (Continued)

Tables
Table 1 Historical Groundwater Elevation Data
Table 2 Groundwater Gradients and Calculated Flow Rates
Table 3 Quantified Detections by Location
Table 4 Exceedances by Location
Table 5 Field Parameter Data by Location
Table 6 Historical Detected Groundwater Constituents
Table 7 Historical Detected Surface Water Constituents

Figure
Figure 1 Site Location Map

Drawing
Drawing 1 Groundwater Potentiometric Surface Map

Appendices
Appendix A Field Data Logs
Appendix B Laboratory Analytical Reports and Chains of Custody

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1.0 INTRODUCTION
1.1 Site Information
The OmniSource Landfill is owned and operated by OmniSource Southeast, LLC and is located
in Kernersville, Forsyth County, North Carolina. The existing landfill was initially permitted in
the early 1970’s by the state of North Carolina as a private industrial landfill used to dispose of
residue from the automobile shredder under Permit Number 34-17, and was owned and operated
by Atlantic Scrap and Processing, LLC. The landfill received automotive shredder residue
(ASR, or “fluff”) consisting of plastic, glass, rubber, foam, fabric, etc., that was generated by the
on-site operations. The landfill stopped receiving waste and was closed in the mid-1990s. In
2005, the facility received a permit for a mining operation to recover additional metal from the
ASR waste. Currently the facility is operating a landfill mining operation under Permit Number
34-20.

The OmniSource Landfill includes approximately 14 acres located within OmniSource-Southeast
property located at 1426 West Mountain Street in Kernersville, North Carolina. Access to the
landfill area is limited from the southern end by means of the fenced scrap processing area and
from other directions by berms, topography, and the side-slopes of the landfill. The site location
is shown in Figure 1 on an excerpt from the 7.5-minute USGS topographic map for the area.

1.2 Site Geology and Hydrogeology
The OmniSource Landfill is located in the Piedmont physiographic providence of North Carolina
and is underlain by intrusive granitic rocks of Pennsylvanian to Permian age which are part of
the Carolina Slate Belt Geologic Unit.

The groundwater level measurements taken on April 12, 2017 were used to construct the
groundwater surface contours shown in Drawing 1. Historical static water levels are provided in
Table 1. Groundwater flow at the site is toward the northeast.

Using the hydraulic gradients along the flow paths shown on Drawing 1, the linear flow velocity
(V) was estimated using the modified Darcy equation: V=Ki/n. The average hydraulic gradient
(i) based on the flow paths shown on Drawing 1 is 0.0646 ft/ft. An effective porosity (n) of 30%
was estimated based on typical values for piedmont aquifers. Hydraulic conductivity (K) of 1.73
ft/day was estimated from slug testing done by JOYCE at nearby site is Kernersville, NC in
November of 2013. The calculated groundwater flow rate averages approximately 136 ft/yr. A
summary of the hydraulic gradients and linear flow velocities is provided in Table 2.

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1.3 Regulatory Status
The OmniSource Landfill is currently monitoring groundwater in accordance with criteria set
forth in Title 15A Subchapter 13B .0500 of the North Carolina Solid Waste Management Rules
(NCSWMR) as well as the approved sampling and analysis plan dated October 2011.

2.0 FACILITY MONITORING PROGRAM
2.1 Groundwater Monitoring Program
The original groundwater monitoring network consisted of 4 monitoring wells installed in 1989;
MW-1, MW-2, MW-3 and MW-4. In 2001, MW-4R was installed to replace MW-4 and
MW-1R replaced MW-1 to further expand scrap metal processing activities. Monitoring wells
MW-2, MW-3, MW-4, and MW-4R were destroyed during mining operations. Replacement
wells MW-12, MW-13, and MW-14 were installed in 2012.

The current groundwater compliance monitoring network consists of four monitoring wells,
including one upgradient well (MW-1R) and three downgradient wells (MW-12, MW-13, and
MW-14). These wells are summarized below, along with their current monitoring program
status. The locations of the monitoring wells are shown on Drawing 1.

Monitoring Well Classification Monitoring Program Total Depth from TOC (ft)
MW-1R Upgradient Detection 104.73
MW-12 Downgradient Detection 28.82
MW-13 Downgradient Detection 26.15
MW-14 Downgradient Detection 33.68
TOC = Top of casing.
Groundwater samples are collected semiannually during the second and fourth quarters. Samples
are analyzed for all constituents listed in the NCSWMR Appendix I during the first and second
semiannual events.

2.2 Surface Water Monitoring Program
Surface water at the OmniSource Kernersville Landfill is monitored semiannually in conjunction
with the groundwater sampling events. Samples are collected from four surface water
monitoring points (SW-1, SW-2, SW-3 and SW-4). The locations of the surface water
monitoring points are shown on Drawing 1.

Surface water samples are collected and analyzed for the NCSWMR Appendix I list of
constituents during both semiannual monitoring events. The results are compared to the 15A
NCAC 2B (NC2B) Surface Water Standards in a value-to-value comparison. These surface
water monitoring points are summarized below, along with their current monitoring program
status.

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Surface Point Classification Monitoring Program
SW-1 Upstream/Compliance Surface Water
SW-2 Downstream/Compliance Surface Water
SW-3 Downstream/Compliance Surface Water
SW-4 Downstream/Compliance Surface Water

3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2017
3.1 Field Work and Visual Inspection
In order to detect potential releases of leachate in a timely manner, a visual inspection program
has been implemented at the OmniSource Kernersville Landfill. This inspection program
involves field personnel making the following observations:

 Observation of stress induced on the biological community (e.g., dead or dying vegetation);
 Indications of leachate impact (e.g., seeps, impacted surface water);
 Observations of erosion; and
 Negative changes around the waste facility.

On April 12, 2017, Joyce Engineering (JOYCE) personnel visited the facility to purge and
sample the facility’s monitoring wells MW-1R, MW-12, MW-13, and MW-14. Prior to purging,
the depth to static water level was measured for all monitoring wells with an electronic water
level indicator, accurate to 0.01 foot.

Monitoring wells were purged and sampled, in accordance with the October 2011 Sampling &
Analysis Plan, using either a 12-volt submersible pump or disposable bailer. Measurements of
temperature, pH, specific conductivity, and turbidity were recorded in the site log book prior to
purging, after each purge volume, and during sampling. Prior to sampling, laboratory-supplied
containers were prepared with the following information:

 Monitoring well number (completed by field personnel);
 Date and time of sample collection (completed by field personnel);
 Initials of sampling personnel (completed by field personnel);
 Project name and number (completed by the laboratory);
 Chemical preservative (completed by the laboratory); and
 Requested chemical analysis (completed by the laboratory).

Groundwater samples from each monitoring well were collected directly from the 12-volt pump
or disposable bailers in the provided laboratory containers either immediately after purging or
within 24 hours of the final purge volume. Immediately after collection, the samples were

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placed in a laboratory-provided cooler and chilled on ice. Field data logs are provided in
Appendix A.

Surface water samples from SW-1, SW-2, SW-3 and SW-4 were collected directly from stream
flow, by lowering the prepared sample containers into the stream flow. Care was taken not to
overflow the sample containers (which could lead to preservative loss) and to avoid sampling-
induced turbidity. At the time of sampling, surface water was also measured for temperature,
pH, specific conductivity, and turbidity. After sample collection, the samples were placed in a
laboratory-provided cooler and chilled on ice. Field data logs are provided in Appendix A.

3.2 Laboratory Analysis and Quality Control
The April 12, 2017, groundwater and surface water samples were submitted to Pace Analytical
Services of Huntersville, North Carolina. The samples were analyzed for the NCSWMR
Appendix I constituents. JOYCE requested a Level II data report for the final laboratory report.
The samples were received by the laboratory on April 13, 2017, in good condition, properly
preserved, and within analysis hold times.

In addition to samples collected for compliance monitoring at the OmniSource Kernersville
Landfill, a Field Blank was collected by JOYCE personnel as part of the April 2017 sampling
event. Also, a Trip Blank was prepared by the laboratory to accompany the volatile sampling
containers during shipment to and from the laboratory. The April 2017 Field Blank was
analyzed for the NCSWMR Appendix I constituents while the April 2017 Trip Blank was
analyzed for the NCSWMR Appendix I volatile organics only.

Upon receipt of the laboratory data package, the data was reviewed by JOYCE personnel for the
following:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate;
and Laboratory Control Samples;
 Blank qualified data (B-flags);
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.

4.0 DATA ANALYSIS
4.1 Groundwater Data Analysis and Comparisons to Standards
The Laboratory Analytical Report from the April 2017 sampling event was received April 24,
2017, from Pace Analytical and is included in Appendix B with the chains-of-custody.
Constituents that were detected at quantified concentrations above the North Carolina

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OmniSource Kernersville Landfill, Permit No. 34-20 August 2017

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Department of Environmental Quality (NCDEQ) Solid Waste Section Limits (SWSL) in
groundwater during the April 2017 sampling event are summarized in Table 3.

Analytical results from monitoring wells were compared directly to the North Carolina
Groundwater Standards found in 15A NCAC 02L.0202 (NC2L Standards) or the NCDEQ Solid
Waste Section Groundwater Protection Standards (GWPS) for constituents with no listed NC2L
standard. Constituents in exceedance of the appropriate standards are summarized in Table 4.
Field parameter data for the April 2017 sampling event are summarized in Table 5. Inorganic
constituents barium beryllium copper and zinc were detected at quantified concentrations above
the SWSL in one or more monitoring wells. No organic constituents were detected at quantified
concentrations above the SWSL. No inorganic or organic constituents were detected above the
NC2L or GWPS.

4.2 Surface Water Data Analysis and Comparisons to Standards
Analytical results for surface water samples were compared directly to either the Freshwater
Aquatic Surface Water Standards or Human Health Surface Water Standards (whichever is
lower) found in 15A NCAC 02B (NC2B Standards). Constituents in exceedance of the
appropriate standards are summarized in Table 4. Field parameter data for the April 2017
sampling event are summarized in Table 5. The results for the upstream surface water sample,
SW-1, indicated one inorganic constituent with a quantified concentration above the SWSL
during the April 2017 sampling event. Zinc was quantified at a concentration of 54.8 µg/L in
SW-1, which is above the respective NC2B standard for freshwater aquatic life (FAL), which is
36 µg/L. In addition, three organic constituents, tetrachloroethene, Carbon Tetrachloride and
Chloroform were detected above the SWSL in SW-1. Tetrachloroethene was found at a
concentration of 5.2 µg/L, which exceeds the NC2B human health standard, for (3.3 µg/L).

Since surface water sampling point SW-1 is upstream of the OmniSource landfill, it is highly
unlikely that the constituents detected in SW-1 are due to a release from the landfill. Zinc was
also detected at qualified concentrations exceeding the NC2B standard at 36.8 µg/L. SW-3 is the
surface point located just downstream from SW-1 on the property. The most likely source of
detected constituents in SW-1 and SW-3 is the former Destructo-Chemway/CaroLawn property,
which is directly upstream of the SW-1 location. This property is a NC Inactive Hazardous Site,
which was the source of a major spill of hazardous material, including chlorinated solvents, in
1977. The spill flowed down the creek where SW-1 is located and eventually contaminated the
Kernersville Reservoir. We believe the organic constituents and some of the inorganic
constituents detected in SW-1 are residuals from this incident.

Zinc was the only constituent detected in surface water samples SW-2 and SW-4 at quantified
concentrations above its respective SWSL during the April 2017 sampling event. No constituent
detected was higher than the NC2B standard for freshwater aquatic life. The April 2017 result is
not higher than historical values for zinc in SW-2 and it is lower than the concentration of zinc
detected in the upstream sample, SW-1, which had a zinc concentration of 54.8 µg/L. The fact

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that zinc concentrations consistently decrease moving progressively downstream from SW-1
supports the contention that the origin of the zinc is the CaroLawn site. Historical surface water
data can be found in Table 7.

5.0 CONCLUSIONS
There were no exceedances of groundwater protection standards in any of the monitoring wells
during the April 2017 sampling event. The facility should remain in detection monitoring. The
next semiannual sampling event is tentatively scheduled for October 2017.

6.0 REFERENCES
Brown, Philip M., Chief Geologist, 1985, Geologic Map of North Carolina, The North Carolina
Geologic Survey, scale 1:500,000.

Fetter, C.W., 2001, Applied Hydrogeology, Fourth Edition: Prentice-Hall, Inc..

Johnson, A.I., 1967, Specific Yield - Compilation of Specific Yields For Various Materials: U.S.
Geological Survey Water Supply Paper 1662-D.

Joyce Engineering, Inc. 2014. 2014 Operations Plan, OmniSource – Kernersville Landfill
Reclamation Project. May 2014.

North Carolina Department of Environment and Natural Resources, 1990-2012, Solid Waste
Management Regulations.

USEPA, 1981. Neely, N., D. Gillespie, F. Schauf, and J. Walsh. Remedial Actions at
Hazardous Sites, Survey and Case Studies: Section 5, Site D – Destructo/CaroLawn,
Kernersville, NC. EPA-430-9-81-005. January 1981.

USEPA, 1986. RCRA Ground Water Monitoring Technical Enforcement Guidance Document
(TEGD).

USEPA, 1992. Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance, Chapter 2, July.

W.Z Baumgartner & Associates, Inc. 2011. Sampling & Analysis Plan For Groundwater
Monitoring, OmniSource Southeast Industriall Landfill. October 2011.

W.Z Baumgartner & Associates, Inc. 2013. Groundwater Monitoirng Report, April 10, 2013
Sampling Event, OmniSource Southeast Landfill, Permit: 3417-TP. May 2014.

Tables

Table 1 Historical Groundwater Elevation Data
Table 2 Groundwater Gradients and Calculated Flow Rates
Table 3 Quantified Detections by Location
Table 4 Exceedances by Location
Table 5 Field Parameter Data by Location
Table 6 Historical Detected Groundwater Constituents
Table 7 Historical Detected Surface Water Constituents

TABLE 1:
HISTORICAL GROUNDWATER ELEVATION DATA
Background
MW-1R MW-12 MW-13 MW-14
Well TOC Elev.:988.67 855.85 838.45 847.45
Well Total Depth:104.73 28.82 26.15 33.68
10-Apr-13 952.17 847.73 832.84 835.05
11-Sep-13 949.72 847.69 832.55 834.20
24-Apr-14 953.02 847.60 833.12 834.96
02-Oct-14 949.11 847.80 832.76 834.22
29-Apr-15 950.99 847.82 833.13 835.29
14-Oct-15 946.27 847.85 832.90 834.73
12-Apr-16 950.12 847.95 832.90 823.80
12-Oct-16 948.62 847.00 833.00 834.90
12-Apr-17 948.64 847.90 832.53 835.35
Notes:
TOC = top of casing.
Water levels are measured from TOC.
All elevations are in feet above mean sea level.
Downgradient
OmniSource Kernersville Landfill
Permit No. 34-20
Joyce Engineering
TABLE 2:
GROUNDWATER GRADIENTS AND CALCULATED FLOW RATES
GROUND-HORIZ.HYDRAULIC EFFECTIVE LINEAR
FLOW WATER GRADIENT,CONDUCTIVITY,POROSITY VELOCITY,
DIRECTION ELEVATION i K n e V
(feet)(ft/ft)(ft/day)(ft/year)
940
860
940
860
Average:0.0646 Average:136.1
Notes:
Linear flow velocity is caculated by: V = Ki/ne
Hydraulic conductivity (K ) value based on slug tests at another site locaed approxiamtely 10 miles from the facility in a simialr geologic seting.
Effective porosity (n e ) is estimated at 30% (0.30), which is typical for saprolite aquifiers in the North Carolina Piedmont.
Refer to Drawling 1 for gradient calculation segments.

143.00.0679 1.73E+00 0.30
0.0613
April 12, 2017
GRADIENT
CALCULATION
SEGMENT
FLOW LINE
LENGTH
(feet)
i 2 1178 NE
i 1 1305 NE 1.73E+00 0.30 129.1
OmniSource - Kernersville Landfill
Permit No. 34-20 Joyce Engineering
TABLE 3:
Quantified Detections
WELL ID PARAMETER RESULT UNITS SWSL DATE
3420-MW12 Barium 161 µg/L 100 4/12/2017
3420-MW13 Copper 13.6 µg/L 10 4/12/2017
3420-MW13 Zinc 19.6 µg/L 10 4/12/2017
3420-MW14 Barium 137 µg/L 100 4/12/2017
3420-MW14 Beryllium 1.9 µg/L 1 4/12/2017
3420-SW1 Zinc 54.8 µg/L 10 4/12/2017
3420-SW1 Carbon Tetrachloride 1.0 µg/L 1 4/12/2017
3420-SW1 Chloroform 6.3 µg/L 5 4/12/2017
3420-SW1 Tetrachloroethene 5.2 µg/L 1 4/12/2017
3420-SW2 Zinc 29.9 µg/L 10 4/12/2017
3420-SW3 Zinc 36.8 µg/L 10 4/12/2017
3420-SW4 Zinc 31.6 µg/L 10 4/12/2017
NOTES:All results in micrograms per liter (µg/L).
SWSL = NC Soild Waste Section Reporting Limit.
Methylene Chloride was Blank-qualified due to concentrations
detected in both field and trip blanks.
OmniSource Kernersville
Permit No. 34-20
Joyce Engineering
TABLE 4:
Exceedances
WELL ID PARAMETER RESULT UNITS SWSL NC 2L / GWPS / NC 2B GPS DATE
3420-SW1 Zinc 54.8 µg/L 10.0 36 FAL NA 4/12/2017
3420-SW1 Tetrachloroethene 5.2 µg/L 1.0 3.3 FAL NA 4/12/2017
3420-SW3 Zinc 36.8 µg/L 10.0 36 FAL NA 4/12/2017
NOTES:All results in micrograms per liter (µg/L).
SWSL = NC Soild Waste Section Reporting Limit.
NC 2L = NC Groundwater Standard from 15A NCAC 2L.0202.
GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L).
NC 2B = NC Surface Water Standard from 15A NCAC 2B.
FAL = Freshwater Aquatic Life Standard.
HH = Human Health Standard.
GPS = Groundwater Protection Standard as defined by 15A NCAC 13B.1634(g).
Bold results are in exceednace of the pertinent standard.
An ASD for Iron and Manganese approved by DENR-SWS on June 9, 2011.
OmniSource Kernersville
Permit No. 34-20
Joyce Engineering
TABLE 5:
Summary of Field Parameter Data
WELL ID PARAMETER RESULT UNITS COLLECT DATE
3420-MW1R pH 8.28 S.U.4/12/2017
3420-MW1R Temperature 16.5 °C 4/12/2017
3420-MW1R Conductivity 188.4 µS/cm 4/12/2017
3420-MW1R Turbididty 9.31 NTU 4/12/2017
3420-MW1R Static Water Level 40.03 ft 4/12/2017
3420-MW1R Well Depth 104.73 ft 4/12/2017
3420-MW12 pH 5.71 S.U.4/12/2017
3420-MW12 Temperature 14.5 °C 4/12/2017
3420-MW12 Conductivity 258 µS/cm 4/12/2017
3420-MW12 Turbididty 20.43 NTU 4/12/2017
3420-MW12 Static Water Level 7.95 ft 4/12/2017
3420-MW12 Well Depth 28.82 ft 4/12/2017
3420-MW13 pH 5.78 S.U.4/12/2017
3420-MW13 Temperature 15.3 °C 4/12/2017
3420-MW13 Conductivity 563 µS/cm 4/12/2017
3420-MW13 Turbididty 17 NTU 4/12/2017
3420-MW13 Static Water Level 5.92 ft 4/12/2017
3420-MW13 Well Depth 26.15 ft 4/12/2017
3420-MW14 pH 5.43 S.U.4/12/2017
3420-MW14 Temperature 15.2 °C 4/12/2017
3420-MW14 Conductivity 190.6 µS/cm 4/12/2017
3420-MW14 Turbididty 8.32 NTU 4/12/2017
3420-MW14 Static Water Level 12.1 ft 4/12/2017
3420-MW14 Well Depth 33.68 ft 4/12/2017
OmniSource Kernersville
Permit No. 34-20 1 of 2 Joyce Engineering
TABLE 5:
Summary of Field Parameter Data
WELL ID PARAMETER RESULT UNITS COLLECT DATE
3420-SW1 pH 6.48 S.U.4/12/2017
3420-SW1 Temperature 16.9 °C 4/12/2017
3420-SW1 Conductivity 110.5 µS/cm 4/12/2017
3420-SW1 Turbididty 10.78 NTU 4/12/2017
3420-SW2 pH 6.71 S.U.4/12/2017
3420-SW2 Temperature 16.2 °C 4/12/2017
3420-SW2 Conductivity 360 µS/cm 4/12/2017
3420-SW2 Turbididty 12.6 NTU 4/12/2017
3420-SW3 pH 6 S.U.4/12/2017
3420-SW3 Temperature 15.1 °C 4/12/2017
3420-SW3 Conductivity 132.6 µS/cm 4/12/2017
3420-SW3 Turbididty 15.39 NTU 4/12/2017
3420-SW4 pH 6.09 S.U.4/12/2017
3420-SW4 Temperature 16.0 °C 4/12/2017
3420-SW4 Conductivity 307 µS/cm 4/12/2017
3420-SW4 Turbididty 15.39 NTU 4/12/2017
NOTES:ºC = degrees Centigrade
S.U.= Standard Units
µS/cm = microsemens per centimeter
NTU = Nephelometric Turbidity Units

OmniSource Kernersville
Permit No. 34-20 2 of 2 Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Inorganic Compounds
Antimony 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------7.70 ND ND ND ---
GWPS = 1 µg/L (10/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 5.0 6.0 ND ND ND ND ND
2-Oct-14 5.0 6.0 6.5 ND ND ND ND
29-Apr-15 0.5 6.0 1.01 J ND ND ND ND
14-Oct-15 3.8 6.0 ND ND ND ND ND
12-Apr-16 3.8 6.0 ND ND ND ND ND
12-Oct-16 3.8 6.0 ND ND ND ND ND
12-Apr-17 3.9 6.0 ND ND ND ND ND
Arsenic 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------10.7 ND 3.40 ND ---
NC 2L = 100 µg/L (1/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 5.0 10.0 ND ND ND ND ND
2-Oct-14 5.0 10.0 ND ND ND ND ND
29-Apr-15 0.25 10.0 1.59 J ND ND ND ND
14-Oct-15 2.50 10.0 ND ND ND ND ND
12-Apr-16 2.50 10.0 3.0 B ND ND ND 3.2
12-Oct-16 2.50 10.0 ND ND ND ND ND
12-Apr-17 5.00 10.0 ND ND ND ND ND
Barium 12-Apr-12 ------41.5 166 41.0 118 ---
10-Oct-12 ------37.6 170 26.9 107 ---
NC 2L = 700 µg/L (1/01/10)10-Apr-13 ------26.9 166 27.5 98.2 ---
11-Sep-13 ------39.4 196 29.8 100 ---
24-Apr-14 5.0 100 21.2 J 184 39.3 J 88.8 J ND
2-Oct-14 5.0 100 15.5 J 195 43.5 J 106 ND
29-Apr-15 0.25 100 27.2 J 181 46.1 J 125 ND
14-Oct-15 2.50 100 17.2 J 179 43.1 J 121 ND
12-Apr-16 2.50 100 29.8 J 174 57.6 J 120 ---
12-Oct-16 2.50 100 9.6 J 148 47.2 J 169 ND
12-Apr-17 2.50 100 7.4 J 161 45.8 J 137 ND
Beryllium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND 1.10 ---
GWPS = 4 µg/L (10/23/07)10-Apr-13 ------ND ND ND 1.10 ---
11-Sep-13 ------ND ND ND 0.800 ---
24-Apr-14 1.0 1.0 ND ND ND 1.1 ND
2-Oct-14 1.0 1.0 ND ND 1.2 1.4 ND
29-Apr-15 0.25 1.0 ND 0.30 J 0.38 J 1.26 ND
14-Oct-15 0.50 1.0 ND ND ND 1.4 ND
12-Apr-16 0.50 1.0 ND ND 1.1 1.3 ND
12-Oct-16 0.50 1.0 ND ND 0.76 J 2.0 ND
12-Apr-17 0.50 1.0 ND ND 0.84 J 1.9 ND
Cadmium 12-Apr-16 0.50 1.0 1.7 ND ND ND ND
12-Oct-16 0.50 1.0 ND ND ND ND ND
12-Apr-17 0.50 1.0 ND ND ND ND ND
NC 2L = 2 µg/L (02/01/15)
OmniSource Kernersville Landfill
Permit No. 34-20 1 of 5
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Chromium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------2.50 ND ND ND ---
NC2B= 50 µg/L (05/01/07)10-Apr-13 ------2.30 ND ND ND ---
11-Sep-13 ------1.80 ND ND ND ---
24-Apr-14 5.0 10.0 ND ND ND ND ND
2-Oct-14 5.0 10.0 ND ND ND ND ND
29-Apr-15 0.25 10.0 ND 0.73 J 1.34 J ND ---
14-Oct-15 2.50 10.0 ND ND 2.8 J ND ND
12-Apr-16 2.50 10.0 ND ND 6.2 J ND ND
12-Oct-16 2.50 10.0 ND ND 3.8 J ND ND
12-Apr-17 2.50 10.0 ND ND 4.9 J ND ND
Cobalt 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------0.700 3.10 3.90 5.70 ---
GWPS = 1 µg/L (10/01/10)10-Apr-13 ------ND 1.90 2.80 3.80 ---
11-Sep-13 ------ND 2.60 4.10 ND ---
24-Apr-14 5.0 10.0 ND ND 5.5 J ND ND
2-Oct-14 5.0 10.0 ND ND 10.4 5.2 J ND
29-Apr-15 0.25 10.0 ND 3.02 J 7.91 J 5.08 J ND
14-Oct-15 2.50 10.0 ND ND 7.2 J 5.4 J ND
12-Apr-16 2.50 10.0 ND ND 7.3 J 4.8 J ND
12-Oct-16 2.50 10.0 ND ND 8.8 J 5.9 J ND
12-Apr-17 2.50 10.0 ND ND 6.7 J 5.5 J ND
Copper 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 1,000 µg/L (10/23/07)10-Apr-13 ------8.8 ND ND ND ---
11-Sep-13 ------10.0 ND ND ND ---
24-Apr-14 5.00 10.0 ND ND 7.5 J ND ND
2-Oct-14 5.00 10.0 ND ND 8.9 J ND ND
29-Apr-15 0.25 10.0 0.39 J 2.73 J 3.43 J 0.92 J ND
14-Oct-15 2.50 10.0 ND 3.5 J 4.3 J ND ND
12-Apr-16 2.50 10.0 ND 2.5 J 8.9 J ND ND
12-Oct-16 2.50 10.0 ND ND 7.8 J ND ND
12-Apr-17 2.50 10.0 ND ND 13.6 ND ND
Lead 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------4.9 ND ND ND ---
NC 2L = 15 µg/L (10/23/07)10-Apr-13 ------4.2 ND ND ND ---
11-Sep-13 ------6.2 ND ND ND ---
24-Apr-14 5.0 10.0 ND ND ND ND ND
2-Oct-14 5.0 10.0 ND ND ND ND ND
29-Apr-15 0.3 10.0 ND 1.60 J 1.26 J ND ND
14-Oct-15 2.5 10.0 ND 3.5 J ND ND ND
12-Apr-16 2.5 10.0 2.7 J ND 4.10 J ND ND
12-Oct-16 2.5 10.0 ND ND ND ND ND
12-Apr-17 2.5 10.0 ND ND 2.8 J ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 2 of 5
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Nickel 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND 2.30 ND 2.00 ---
NC 2L = 100 µg/L (10/23/07)10-Apr-13 ------ND 2.90 ND ND ---
11-Sep-13 ------ND ND ND 2.20 ---
24-Apr-14 5.0 50.0 ND ND ND ND ND
2-Oct-14 5.0 50.0 ND ND ND ND ND
29-Apr-15 0.5 50.0 ND 4.44 J 4.07 J 2.58 J ND
14-Oct-15 2.5 50.0 ND 5.8 J 4.9 J 2.6 J ND
12-Apr-16 2.5 50.0 ND 3.6 J 6.7 J 2.6 J ND
12-Oct-16 2.5 50.0 ND 3.2 J 6.4 J 3.7 J ND
12-Apr-17 2.5 50.0 ND 3.3 J 6.1 J 2.6 J ND
Selenium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 20 µg/L (1/01/10)10-Apr-13 ------ND ND ND 4.90 ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 10.0 10.0 ND ND ND ND ND
2-Oct-14 10.0 10.0 ND ND ND ND ND
29-Apr-15 0.25 10.0 ND ND ND ND ND
14-Oct-15 5.00 10.0 ND ND ND ND ND
12-Apr-16 5.00 10.0 ND ND ND ND ND
12-Oct-16 5.00 10.0 ND ND ND ND ND
12-Apr-17 5.00 10.0 ND ND ND ND ND
Thallium 12-Apr-17 0.02 5.5 ND 0.10 J ND 0.051 J ND
GWPS = 0.28 µg/L (2/1/15)
Vanadium 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
GWPS = 0.3 µg/L (10/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 5.00 25.0 ND ND 9.2 J ND ND
2-Oct-14 5.00 25.0 ND 5.0 J 20.1 J ND ND
29-Apr-15 0.25 25.0 4.12 J 2.54 J 5.42 J 0.31 J ND
14-Oct-15 2.50 25.0 ND 5.4 J 8.5 J ND ND
12-Apr-16 2.50 25.0 3.70 J ND 19.3 J ND ND
12-Oct-16 2.50 25.0 ND ND 14.9 J 3.80 J ND
12-Apr-17 2.50 25.0 ND ND 19.2 J ND ND
Zinc 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------27.3 ND ND ND ---
NC 2L = 1,000 µg/L (1/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------29.4 ND ND ND ---
24-Apr-14 10.0 10.0 ND 15.3 ND ND ND
2-Oct-14 10.0 10.0 ND ND ND ND ND
29-Apr-15 5.0 10.0 20.2 24.3 23.1 26.2 ND
14-Oct-15 5.0 10.0 7.1 J 8.9 J 7.6 J 5.1 J ND
12-Apr-16 5.0 10.0 15.4 16.2 12.4 ND ND
12-Oct-16 5.0 10.0 ND ND 7.9 J 7.3 J ND
12-Apr-17 5.0 10.0 ND ND 19.6 6.0 J ND
OmniSource Kernersville Landfill
Permit No. 34-20 3 of 5
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Organic Compounds
Acetone 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------12 20.9 ND ND ---
NC 2L = 6,000 µg/L (1/01/10)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 10.0 100 ND ND ND ND ND
2-Oct-14 10.0 100 ND ND ND ND ND
29-Apr-15 10.0 100 ND ND ND ND ND
14-Oct-15 10.0 100 ND ND ND ND ND
12-Apr-16 10.0 100 ND ND ND ND ND
12-Oct-16 10.0 100 ND ND ND ND ND
12-Apr-17 10.0 100 ND ND ND ND ND
Benzene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND 0.406 0.280 ND ---
NC 2L = 1 µg/L (10/23/07)10-Apr-13 ------ND 0.365 ND ND ---
11-Sep-13 ------ND 0.411 0.203 ND ---
24-Apr-14 0.25 1.0 ND 0.350 J ND ND ND
2-Oct-14 0.25 1.0 ND ND ND ND ND
29-Apr-15 0.20 1.0 1.43 ND ND ND ND
GCAL resample 27-May-15 0.20 1.0 1.45 ------------
Pace resample 24-Jun-15 0.25 1.0 0.88 J ------------
GCAL resample 24-Jun-15 0.20 1.0 0.96 J ------------
14-Oct-15 0.25 1.0 1.8 ND ND ND ND
Pace resample 11-Nov-15 0.30 1.0 1.0 ---------ND
12-Apr-16 0.25 1.0 0.29 J ND ND ND ND
12-Oct-16 0.25 1.0 ND ND ND ND ND
12-Apr-17 0.25 1.0 ND ND ND ND ND
Carbon disulfide 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND 1.9 ---
NC 2L = 700 µg/L (10/23/07)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 1.2 100 ND ND ND ND ND
2-Oct-14 1.2 100 ND ND ND ND ND
29-Apr-15 1.2 100 ND ND ND ND ND
14-Oct-15 1.2 100 ND ND ND ND ND
12-Apr-16 1.2 100 ND ND ND ND ND
12-Oct-16 1.2 100 ND ND ND ND ND
12-Apr-17 1.2 100 ND ND ND ND ND
Chloromethane 12-Apr-16 0.1 1 0.39 J ND 0.14 J ND ND
NC 2L = 3 µg/L (02/01/15)12-Oct-16 0.1 1 ND ND ND ND ND
12-Apr-17 0.1 1 ND ND ND ND ND
Cis-1,2-Dichloroethene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 70 µg/L (10/23/07)10-Apr-13 ------ND ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 0.19 5.0 ND 0.200 J ND ND ND
2-Oct-14 0.19 5.0 ND ND ND ND ND
29-Apr-15 0.19 5.0 ND ND ND ND ND
14-Oct-15 0.19 5.0 ND 0.20 J ND ND ND
12-Apr-16 0.19 5.0 ND ND ND ND ND
12-Oct-16 0.19 5.0 ND ND ND ND ND
12-Apr-17 0.19 5.0 ND ND ND ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 4 of 5
Joyce Engineering
TABLE 6:
HISTORICAL DETECTED GROUND WATER CONSTITUENTS
Sample
Analyte Collection Date DL QL MW-1R MW-12 MW-13 MW-14 Blanks
Methylene Chloride 14-Oct-15 0.97 1 ND ND ND ND 3.6
NC 2L = 5 µg/L (10/23/07)12-Apr-16 0.97 1 2.0 B 2.0 B 1.8 B 1.9 B 4.0 B
12-Oct-16 0.97 1 ND ND ND ND ND
12-Apr-17 0.97 1 ND ND ND ND ND
Styrene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND ND ND ND ---
NC 2L = 70 µg/L (10/23/07)10-Apr-13 ------0.515 ND ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 0.26 1.0 ND ND ND ND ND
2-Oct-14 0.26 1.0 ND ND ND ND ND
29-Apr-15 0.26 1.0 ND ND ND ND ND
14-Oct-15 0.26 1.0 ND ND ND ND ND
12-Apr-16 0.26 1.0 ND ND ND ND ND
12-Oct-16 0.26 1.0 ND ND ND ND ND
12-Apr-17 0.26 1.0 ND ND ND ND ND
Tetrachloroethene 12-Apr-12 ------ND ND ND ND ---
10-Oct-12 ------ND 0.319 ND ND ---
NC 2L = 0.7 µg/L (10/23/07)10-Apr-13 ------ND 0.525 ND ND ---
11-Sep-13 ------ND ND ND ND ---
24-Apr-14 0.46 1.0 ND ND ND ND ND
2-Oct-14 0.46 1.0 ND ND ND ND ND
29-Apr-15 0.20 1.0 ND ND ND ND ND
14-Oct-15 0.46 1.0 ND ND ND ND ND
12-Apr-16 0.46 1.0 ND ND ND ND ND
12-Oct-16 0.46 1.0 ND ND ND ND ND
12-Apr-17 0.46 1.0 ND ND ND ND ND
Notes:
All concentrations are in micrograms per liter (µg/L).
NC 2L = North Carolina Groundwater Standards established under 15A NCAC 2L.0202.
GWPS = Groundwater Protection Standards established by the DENR-SWS for constituents with ne NC 2L standard.
RL = Laboratory reporting limit (NC SWSL or lower).
DL = Laboratory detection limit.
J = Estimated value between the DL and the SWSL.
B = Blank-qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above the DL.
--- = Data not available.
Data prior to May 2014 provided by W.Z. Baumgartner & Associates, Inc.
Bold values are above the NC 2L Standards or GWPS.
OmniSource Kernersville Landfill
Permit No. 34-20 5 of 5
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Inorganic Compounds
Antimony 29-Apr-15 0.5 6 1.69 J ND ------ND
14-Oct-15 3.8 6 ND ND ------ND
NC 2B = 640 µg/L (HH)12-Apr-16 3.8 6 ND ND ------ND
12-Oct-16 3.8 6 ND ND ND ND ND
12-Apr-17 3.9 6 ND ND ND ND ND
Arsenic 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND 69.0 ---------
NC 2B = 10 µg/L (HH)10-Apr-13 ------44.3 ND ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 5.0 10.0 Dry ND ------ND
2-Oct-14 5.0 10.0 Dry ND ------ND
29-Apr-15 0.3 10.0 0.39 J 0.27 J ------ND
14-Oct-15 2.5 10.0 ND ND ------ND
12-Apr-16 2.5 10.0 2.80 B ND ------3.2 J
12-Oct-16 2.5 10.0 ND ND ND ND ND
12-Apr-17 5.0 10.0 ND ND ND ND ND
Barium 12-Apr-12 ------52.4 79.1 ---------
10-Oct-12 ------52.6 87.4 ---------
NC 2B = 200,000 µg/L (HH)10-Apr-13 ------44.3 84.2 ---------
11-Sep-13 ------52.7 99.3 ---------
24-Apr-14 5.0 100 Dry 79.6 J ------ND
2-Oct-14 5.0 100 Dry 79.9 J ------ND
29-Apr-15 0.3 100 174 98.2 J ------ND
14-Oct-15 2.5 100 59.6 J 101 ------ND
12-Apr-16 2.5 100 69.0 J 89.1 J ------ND
12-Oct-16 2.5 100 67.5 J 96.3 J 58.2 J 96.2 J ND
12-Apr-17 2.5 100 59.1 J 80.6 J 49.1 J 82.1 J ND
Beryllium 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND ND ---------
NC 2B = 6.5 µg/L (FAL)10-Apr-13 ------ND ND ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 1.0 1.0 Dry ND ------ND
2-Oct-14 1.0 1.0 Dry ND ------ND
29-Apr-15 0.3 1.0 0.43 J ND ------ND
14-Oct-15 0.5 1.0 ND ND ------ND
12-Apr-16 0.5 1.0 ND ND ------ND
12-Oct-16 0.5 1.0 ND ND ND ND ND
12-Apr-17 0.5 1.0 ND ND ND ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 1 of 5
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Cadmium 29-Apr-15 0.3 1.0 1.40 ND ------ND
14-Oct-15 0.5 1.0 ND ND ------ND
NC 2B = .15 µg/L (05/01/07) (FAL)12-Apr-16 0.5 1.0 ND ND ------ND
12-Oct-16 0.5 1.0 ND ND ND ND ND
12-Apr-17 0.5 1.0 ND ND ND ND ND
Chromium 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND ND ---------
NC 2B = 24 µg/L (FAL)10-Apr-13 ------1.6 2.1 ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 5.0 10.0 Dry ND ------ND
2-Oct-14 5.0 10.0 Dry ND ------ND
29-Apr-15 0.3 10.0 5.40 J 0.39 J ------ND
14-Oct-15 2.5 10.0 ND ND ------ND
12-Apr-16 2.5 10.0 ND ND ------ND
12-Oct-16 2.5 10.0 ND ND ND ND ND
12-Apr-17 2.5 10.0 ND ND ND ND ND
Cobalt 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND 1.0 ---------
NC 2B = 4 µg/L (HH)10-Apr-13 ------ND ND ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 5.0 10.0 Dry ND ------ND
2-Oct-14 5.0 10.0 Dry ND ------ND
29-Apr-15 0.3 10.0 1.83 J 1.39 J ------ND
14-Oct-15 2.5 10.0 ND ND ------ND
12-Apr-16 2.5 10.0 ND ND ------ND
12-Oct-16 2.5 10.0 ND ND ND ND ND
12-Apr-17 2.5 10.0 ND ND ND ND ND
Copper 12-Apr-12 ------ ND ND ---------
10-Oct-12 ------11.8 13.5 ---------
NC 2B = 2.7 µg/L (FAL)10-Apr-13 ------ND ND ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 5.00 10.0 Dry 6.8 J ------ND
2-Oct-14 5.00 10.0 Dry ND ------ND
29-Apr-15 0.25 10.0 43.8 4.72 J ------ND
14-Oct-15 2.50 10.0 2.8 J 3.2 J ------ND
12-Apr-16 2.50 10.0 ND 3.4 J ------ND
12-Oct-16 2.50 10.0 ND 3.3 J ND 3.5 J ND
12-Apr-17 2.50 10.0 ND 4.7 J 3.2 J 4.1 J ND
OmniSource Kernersville Landfill
Permit No. 34-20 2 of 5
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Lead 29-Apr-15 0.25 10.0 69.2 0.92 J ------ND
14-Oct-15 2.50 10.0 ND ND ------ND
NC 2B = 14 µg/L (05/01/07) (FAL)12-Apr-16 2.50 10.0 ND ND ------ND
12-Oct-16 2.50 10.0 ND ND ND ND ND
12-Apr-17 2.50 10.0 ND 2.9 J 2.9 J 4.1 J ND
Nickel 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND 7.6 ---------
NC 2B = 16 µg/L (FAL) 10-Apr-13 ------ND 5.1 ---------
11-Sep-13 ------ND 4.5 ---------
24-Apr-14 5.0 50.0 Dry 6.7 J ------ND
2-Oct-14 5.0 50.0 Dry ND ------ND
29-Apr-15 0.5 50.0 9.67 J 5.43 J ------ND
14-Oct-15 2.5 50.0 ND 4.4 J ------ND
12-Apr-16 2.5 50.0 ND 5.4 J ------ND
12-Oct-16 2.5 50.0 ND 4.4 J ND 4.1 J ND
12-Apr-17 2.5 50.0 ND 4.0 J ND 3.6 J ND
Vanadium 29-Apr-15 0.25 25 3.01 J 0.40 J ------ND
14-Oct-15 2.5 25 ND ND ------ND
NC 2B = NE (05/01/07) 12-Apr-16 2.5 25 ND ND ------ND
12-Oct-16 2.5 25 ND ND ND ND ND
12-Apr-17 2.5 25 ND ND ND ND ND
Zinc 12-Apr-12 ------ND ND ---------
10-Oct-12 ------0.051 24.2 ---------
NC 2B = 36 µg/L (FAL)10-Apr-13 ------ND 29.4 ---------
11-Sep-13 ------0.169 23.2 ---------
24-Apr-14 10.0 10.0 Dry 27.7 ------ND
2-Oct-14 10.0 10.0 Dry 10.6 ------ND
29-Apr-15 5.0 10.0 438 62.0 ------ND
14-Oct-15 5.0 10.0 52.0 29.7 ------ND
12-Apr-16 5.0 10.0 62.8 31.9 ------ND
12-Oct-16 5.0 10.0 46.4 29.0 35.0 31.5 ND
12-Apr-17 5.0 10.0 54.8 29.9 36.8 31.6 ND
OmniSource Kernersville Landfill
Permit No. 34-20 3 of 5
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Organic Compounds
Acetone 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND 2.88 ---------
NC 2B = 2,000 µg/L (FAL)10-Apr-13 ------ND 8.34 ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 10.0 100.0 Dry ND ------ND
2-Oct-14 10.0 100.0 Dry ND ------ND
29-Apr-15 0.5 100.0 ND ND ------ND
14-Oct-15 10.0 100.0 ND ND ------ND
12-Apr-16 10.0 100.0 ND ND ------ND
12-Oct-16 10.0 100.0 ND ND ND ND ND
12-Apr-17 10.0 100.0 ND ND ND ND ND
Benzene 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND 0.509 ---------
NC 2B = 51 µg/L (HH)10-Apr-13 ------ND 0.369 ---------
11-Sep-13 ------ND 0.481 ---------
24-Apr-14 1.2 1.0 Dry 0.31 J ------ND
2-Oct-14 0.3 1.0 Dry ND ------ND
29-Apr-15 0.2 1.0 ND ND ------ND
14-Oct-15 0.3 1.0 ND 0.45 J ------ND
12-Apr-16 0.3 1.0 ND 0.29 J ------ND
12-Oct-16 0.3 1.0 ND 0.29 J ND ND ND
12-Apr-17 0.3 1.0 ND 0.26 J ND ND ND
Carbon tetrachloride 14-Oct-15 0.25 1.0 4.5 ND ------ND
NC 2B = 1.6 µg/L (HH)12-Apr-16 0.25 1.0 3.1 ND ------ND
12-Oct-16 0.25 1.0 1.6 ND ND ND ND
12-Apr-17 0.25 1.0 1.0 ND ND ND ND
cis-1,2-Dichloroethene 14-Oct-15 0.19 5 0.7 J ND ------ND
12-Apr-16 0.19 5 0.4 J ND ------ND
12-Oct-16 0.19 5 0.9 J ND ND ND ND
12-Apr-17 0.19 5 1.0 J ND ND ND ND
NC 2B = NE
Chloroform 14-Oct-15 0.14 5 13.9 ND ------ND
12-Apr-16 0.14 5 16.4 ND ------ND
12-Oct-16 0.14 5 7.8 ND ND ND ND
12-Apr-17 0.14 5 6.3 ND ND ND ND
NC 2B = NE
Methylene Chloride 12-Apr-16 0.97 1 2.2 B 1.7 B ------4.0 J
NC 2B = 590 µg/L (HH)12-Oct-16 0.97 1 ND ND ND ND ND
12-Apr-17 0.97 1 ND ND ND ND ND
Tetrachloroethene ------
NC 2B = 3.3 µg/L (10/23/07) (HH)29-Apr-15 0.2 1.0 8.1 ND ------ND
Resample >27-May-15 0.2 1.0 3.5 ---------ND
14-Oct-15 0.46 1.0 4.4 ND ------ND
12-Apr-16 0.46 1.0 3.3 ND ------ND
12-Oct-16 0.46 1.0 3.1 J ND 0.59 J ND ND
12-Apr-17 0.46 1.0 5.2 ND 0.98 J ND ND
OmniSource Kernersville Landfill
Permit No. 34-20 4 of 5
Joyce Engineering
TABLE 7:
HISTORICAL DETECTED SURFACE WATER CONSTITUENTS
Sample
Analyte Collection Date DL RL SW-1 SW-2 SW-3 SW-4 Blanks
Toluene 12-Apr-12 ------ND ND ---------
10-Oct-12 ------ND 0.257 ---------
NC 2B = 11 µg/L (HH)10-Apr-13 ------ND ND ---------
11-Sep-13 ------ND ND ---------
24-Apr-14 0.26 1.0 Dry ND ------ND
2-Oct-14 0.26 1.0 Dry ND ------ND
29-Apr-15 0.20 1.0 ND ND ------ND
14-Oct-15 0.26 1.0 ND ND ------ND
12-Apr-16 0.26 1.0 ND ND ------ND
12-Oct-16 0.26 1.0 ND ND ND ND ND
12-Apr-17 0.26 1.0 ND ND ND ND ND
Notes:
All concentrations are in micrograms per liter (µg/L).
NC 2B = North Carolina Surface Water Standards established under 15A NCAC 2B.
(NC 2B shown is the lowest of "Freshwater Aquatic Life" (FAL) or "Human Health" (HH) standard.)
RL = Laboratory reporting limit (NC SWSL or lower).
DL = Laboratory detection limit.
J = Estimated value between the DL and the SWSL.
B = Blank-qualified data; result is suspected to be biased high based on concentrations in the blanks.
ND = Not detected above the DL.
--- = Data not available.
Data prior to May 2014 provided by W.Z. Baumgartner & Associates, Inc.
Bold values exceed the NC 2B standard.
OmniSource Kernersville Landfill
Permit No. 34-20 5 of 5
Joyce Engineering

Figure

Figure 1 Site Location Map

Drawing

Drawing 1 Groundwater Potentiometric Surface Map

9609509409309209109008908808708609709509709809901000101010201030970960950940930920910900890880870860850850860870101098
0
97
0
96
0
95
0
94
0
93
0
92
0
910
920
93
0
930
92
0
910
900
890
88
0870
8608508509901000101010201030104010501060 1040102010009909809609509509
5
0950
970
970
96
0
9
5
0960950970960980
970
970
MW-1R
948.64
MW-12
847.90
PROPERTY LINESHREDDER IN-FEED
STORAGE
TRUCK LOADOUT
OFFICE
EXISTING SEDIMENT /
DETENTION POND
EXISTING SEDIMENT /
DETENTION POND
FINES PROCESSING AND
STOCKPILE AREA
FINES POLISHING
MW-14
835.35
MW-13
832.53
920
900
880
860
840
860
880900
920 940i
i
SW-2
SW-4
SW-3
SW-1 GWGWGW
GW GWGWGW
GW GW
GW
GW
GW GWGWGWGWGW
GWGWGWGWGWGWGWGWGWGW
GW GWGW
GW
GW GWGWGWGW GWGWGW
GWGWGWGWGWGWGWGWGW
GWGWGWGW940840
MW-12
SW-2
PROPERTY LINE
EXISTING 10' TOPOGRAPHIC CONTOUR
EXISTING 2' TOPOGRAPHIC CONTOUR
EXISTING ROAD
GROUNDWATER SURFACE CONTOUR
[FEET ABOVE MEAN SEA LEVEL (AMSL)]
GROUNDWATER FLOW DIRECTION
TREE LINE
GROUNDWATER MONITORING WELL LOCATION AND IDENTIFICATION
WITH STATIC WATER LEVEL ELEVATION (FEET AMSL)
SURFACE MONITORING POINT LOCATION AND IDENTIFICATION
SEGMENT USED FOR GRADIENT CALCULATION
1.TOPOGRAPHIC CONTOUR INTERVAL = 2 FEET
2.GROUNDWATER CONTOUR INTERVAL = 20 FEET
3.STATIC WATER LEVELS WERE MEASURED ON 04/12/17.
4.GROUNDWATER CONTOURS BASED ON LINEAR
INTERPOLATION BETWEEN AND EXTRAPOLATION FROM
KNOWN DATA, TOPOGRAPHIC CONTOURS, AND KNOWN
FIELD CONDITIONS. THEREFORE, GROUNDWATER
CONTOURS MAY NOT REFLECT ACTUAL GROUNDWATER
CONDITIONS.
i
LEGEND
1280
NOTES
847.90
FLOW PATH LENGTH
i = 1,305F
i = 1,178 LF
0
(FEET)
GRAPHIC SCALE
20010050
PROJECT NO.APPROVEDCHECKEDDRAWNDESIGNEDDATEDATEREVISIONS AND RECORD OF ISSUEBYNOAPPCKSCALE All rights reserved.Ó Joyce Engineering, Inc.DRAWING NO.L:\OMNI SOURCE\KERNERSVILLE\GW EVENT MAP\GW EVENT APRIL 2017.dwg Layout=Layout12211 W. MEADOWVIEW ROADGREENSBORO, NC 27407PHONE: [phone]NC CORP LIC: C-0782799OMNISOURCE SOUTHEAST - KERNERSVILLE SITEKERNERSVILLE, NORTH CAROLINA20171
AS SHOWNGROUNDWATER CONTOUR MAPAPRIL 12, 2017GERWHVBAE06/23/170
(FEET)
GRAPHIC SCALE
600300150

APPENDICES

Appendix A

Field Data Logs

Appendix B

Laboratory Analytical Reports
and Chains of Custody

#=CL#
April 20, 2017
LIMS USE: FR - ALEX EVERHART
LIMS OBJECT ID: 92337093
92337093
Project:
Pace Project No.:
RE:
Mr. Alex Everhart
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
OMNISOURCE/KERNERSVILLE LF
Dear Mr. Everhart:
Enclosed are the analytical results for sample(s) received by the laboratory on April 13, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc:Mr. Van Burbach, Joyce Engineering-NC
Alex Everhart, Joyce Engineering-NC
REPORT OF LABORATORY ANALYSIS
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Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID Matrix Date Collected Date Received
92337093001 3420-MW1R Water 04/12/17 13:30 04/13/17 09:45
92337093002 3420-MW12 Water 04/12/17 09:55 04/13/17 09:45
92337093003 3420-MW13 Water 04/12/17 11:55 04/13/17 09:45
92337093004 3420-MW14 Water 04/12/17 11:48 04/13/17 09:45
92337093005 3420-SW1 Water 04/12/17 13:10 04/13/17 09:45
92337093006 3420-SW2 Water 04/12/17 11:20 04/13/17 09:45
92337093007 3420-SW3 Water 04/12/17 10:05 04/13/17 09:45
92337093008 3420-SW4 Water 04/12/17 11:30 04/13/17 09:45
92337093009 3420-FIELD BLANK Water 04/12/17 13:45 04/13/17 09:45
92337093010 3420-TRIP BLANK Water 04/12/17 07:00 04/13/17 09:45
REPORT OF LABORATORY ANALYSIS
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Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92337093001 3420-MW1R EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093002 3420-MW12 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093003 3420-MW13 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093004 3420-MW14 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093005 3420-SW1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093006 3420-SW2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093007 3420-SW3 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093008 3420-SW4 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093009 3420-FIELD BLANK EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92337093010 3420-TRIP BLANK EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 39
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92337093001 3420-MW1R
Barium 7.4J ug/L 04/19/17 02:00100EPA 6010
92337093002 3420-MW12
Barium 161 ug/L 04/19/17 02:12100EPA 6010
Nickel 3.3J ug/L 04/19/17 02:1250.0EPA 6010
Thallium 0.10J ug/L 04/18/17 13:235.5EPA 6020B
92337093003 3420-MW13
Barium 45.8J ug/L 04/19/17 02:15100EPA 6010
Beryllium 0.84J ug/L 04/19/17 02:151.0EPA 6010
Chromium 4.9J ug/L 04/19/17 02:1510.0EPA 6010
Cobalt 6.7J ug/L 04/19/17 02:1510.0EPA 6010
Copper 13.6 ug/L 04/19/17 02:1510.0EPA 6010
Lead 2.8J ug/L 04/19/17 02:1510.0EPA 6010
Nickel 6.1J ug/L 04/19/17 02:1550.0EPA 6010
Vanadium 19.2J ug/L 04/19/17 02:1525.0EPA 6010
Zinc 19.6 ug/L 04/19/17 02:1510.0EPA 6010
92337093004 3420-MW14
Barium 137 ug/L 04/19/17 02:19100EPA 6010
Beryllium 1.9 ug/L 04/19/17 02:191.0EPA 6010
Cobalt 5.5J ug/L 04/19/17 02:1910.0EPA 6010
Nickel 2.6J ug/L 04/19/17 02:1950.0EPA 6010
Zinc 6.0J ug/L 04/19/17 02:1910.0EPA 6010
Thallium 0.051J ug/L 04/18/17 13:365.5EPA 6020B
92337093005 3420-SW1
Barium 59.1J ug/L 04/19/17 02:22100EPA 6010
Zinc 54.8 ug/L 04/19/17 02:2210.0EPA 6010
Carbon tetrachloride 1.0 ug/L 04/14/17 03:161.0EPA 8260
Chloroform 6.3 ug/L 04/14/17 03:165.0EPA 8260
cis-1,2-Dichloroethene 1.0J ug/L 04/14/17 03:165.0EPA 8260
Tetrachloroethene 5.2 ug/L 04/14/17 03:161.0EPA 8260
92337093006 3420-SW2
Barium 80.6J ug/L 04/19/17 02:25100EPA 6010
Copper 4.7J ug/L 04/19/17 02:2510.0EPA 6010
Lead 2.9J ug/L 04/19/17 02:2510.0EPA 6010
Nickel 4.0J ug/L 04/19/17 02:2550.0EPA 6010
Zinc 29.9 ug/L 04/19/17 02:2510.0EPA 6010
Benzene 0.26J ug/L 04/14/17 03:341.0EPA 8260
92337093007 3420-SW3
Barium 49.1J ug/L 04/19/17 02:28100EPA 6010
Copper 3.2J ug/L 04/19/17 02:2810.0EPA 6010
Lead 2.9J ug/L 04/19/17 02:2810.0EPA 6010
Zinc 36.8 ug/L 04/19/17 02:2810.0EPA 6010
Tetrachloroethene 0.98J ug/L 04/14/17 03:511.0EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 5 of 39
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92337093008 3420-SW4
Barium 82.1J ug/L 04/19/17 02:31100EPA 6010
Copper 4.1J ug/L 04/19/17 02:3110.0EPA 6010
Lead 4.1J ug/L 04/19/17 02:3110.0EPA 6010
Nickel 3.6J ug/L 04/19/17 02:3150.0EPA 6010
Zinc 31.6 ug/L 04/19/17 02:3110.0EPA 6010
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW1R Lab ID:92337093001 Collected:04/12/17 13:30 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:00 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:00 7440-38-204/18/17 00:3010.0 5.0 1
Barium 7.4J ug/L 04/19/17 02:00 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:00 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:00 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:00 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:00 7440-48-404/18/17 00:3010.0 2.5 1
Copper ND ug/L 04/19/17 02:00 7440-50-804/18/17 00:3010.0 2.5 1
Lead ND ug/L 04/19/17 02:00 7439-92-104/18/17 00:3010.0 2.5 1
Nickel ND ug/L 04/19/17 02:00 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:00 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:00 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:00 7440-62-204/18/17 00:3025.0 2.5 1
Zinc ND ug/L 04/19/17 02:00 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:21 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 02:05 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 02:05 107-13-12001.9 1
Benzene ND ug/L 04/14/17 02:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 02:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 02:05 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 02:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 02:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 02:05 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 02:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 02:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 02:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 02:05 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 02:05 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 02:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 02:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 02:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 02:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 02:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 02:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 02:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 02:05 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 02:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 02:05 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 02:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 02:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 02:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 02:05 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
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Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW1R Lab ID:92337093001 Collected:04/12/17 13:30 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 02:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 02:05 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 02:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 02:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 02:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 02:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 02:05 108-10-11000.33 1
Styrene ND ug/L 04/14/17 02:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 02:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 02:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 02:05 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 02:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 02:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 02:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 02:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 02:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 02:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 02:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 02:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 02:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)87 %04/14/17 02:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %04/14/17 02:05 17060-07-070-130 1
Toluene-d8 (S)106 %04/14/17 02:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
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Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW12 Lab ID:92337093002 Collected:04/12/17 09:55 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:12 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:12 7440-38-204/18/17 00:3010.0 5.0 1
Barium 161 ug/L 04/19/17 02:12 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:12 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:12 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:12 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:12 7440-48-404/18/17 00:3010.0 2.5 1
Copper ND ug/L 04/19/17 02:12 7440-50-804/18/17 00:3010.0 2.5 1
Lead ND ug/L 04/19/17 02:12 7439-92-104/18/17 00:3010.0 2.5 1
Nickel 3.3J ug/L 04/19/17 02:12 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:12 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:12 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:12 7440-62-204/18/17 00:3025.0 2.5 1
Zinc ND ug/L 04/19/17 02:12 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.10J ug/L 04/18/17 13:23 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 02:23 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 02:23 107-13-12001.9 1
Benzene ND ug/L 04/14/17 02:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 02:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 02:23 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 02:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 02:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 02:23 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 02:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 02:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 02:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 02:23 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 02:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 02:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 02:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 02:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 02:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 02:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 02:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 02:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 02:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 02:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 02:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 02:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 02:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 02:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 02:23 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
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Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW12 Lab ID:92337093002 Collected:04/12/17 09:55 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 02:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 02:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 02:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 02:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 02:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 02:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 02:23 108-10-11000.33 1
Styrene ND ug/L 04/14/17 02:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 02:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 02:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 02:23 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 02:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 02:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 02:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 02:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 02:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 02:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 02:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 02:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 02:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)92 %04/14/17 02:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %04/14/17 02:23 17060-07-070-130 1
Toluene-d8 (S)106 %04/14/17 02:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW13 Lab ID:92337093003 Collected:04/12/17 11:55 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:15 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:15 7440-38-204/18/17 00:3010.0 5.0 1
Barium 45.8J ug/L 04/19/17 02:15 7440-39-304/18/17 00:301002.5 1
Beryllium 0.84J ug/L 04/19/17 02:15 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:15 7440-43-904/18/17 00:301.0 0.50 1
Chromium 4.9J ug/L 04/19/17 02:15 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt 6.7J ug/L 04/19/17 02:15 7440-48-404/18/17 00:3010.0 2.5 1
Copper 13.6 ug/L 04/19/17 02:15 7440-50-804/18/17 00:3010.0 2.5 1
Lead 2.8J ug/L 04/19/17 02:15 7439-92-104/18/17 00:3010.0 2.5 1
Nickel 6.1J ug/L 04/19/17 02:15 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:15 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:15 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium 19.2J ug/L 04/19/17 02:15 7440-62-204/18/17 00:3025.0 2.5 1
Zinc 19.6 ug/L 04/19/17 02:15 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:25 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 02:40 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 02:40 107-13-12001.9 1
Benzene ND ug/L 04/14/17 02:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 02:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 02:40 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 02:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 02:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 02:40 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 02:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 02:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 02:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 02:40 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 02:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 02:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 02:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 02:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 02:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 02:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 02:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 02:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 02:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 02:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 02:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 02:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 02:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 02:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 02:40 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW13 Lab ID:92337093003 Collected:04/12/17 11:55 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 02:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 02:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 02:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 02:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 02:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 02:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 02:40 108-10-11000.33 1
Styrene ND ug/L 04/14/17 02:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 02:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 02:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 02:40 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 02:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 02:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 02:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 02:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 02:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 02:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 02:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 02:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 02:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)92 %04/14/17 02:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %04/14/17 02:40 17060-07-070-130 1
Toluene-d8 (S)109 %04/14/17 02:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW14 Lab ID:92337093004 Collected:04/12/17 11:48 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:19 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:19 7440-38-204/18/17 00:3010.0 5.0 1
Barium 137 ug/L 04/19/17 02:19 7440-39-304/18/17 00:301002.5 1
Beryllium 1.9 ug/L 04/19/17 02:19 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:19 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:19 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt 5.5J ug/L 04/19/17 02:19 7440-48-404/18/17 00:3010.0 2.5 1
Copper ND ug/L 04/19/17 02:19 7440-50-804/18/17 00:3010.0 2.5 1
Lead ND ug/L 04/19/17 02:19 7439-92-104/18/17 00:3010.0 2.5 1
Nickel 2.6J ug/L 04/19/17 02:19 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:19 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:19 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:19 7440-62-204/18/17 00:3025.0 2.5 1
Zinc 6.0J ug/L 04/19/17 02:19 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.051J ug/L 04/18/17 13:36 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 02:58 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 02:58 107-13-12001.9 1
Benzene ND ug/L 04/14/17 02:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 02:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 02:58 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 02:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 02:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 02:58 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 02:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 02:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 02:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 02:58 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 02:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 02:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 02:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 02:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 02:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 02:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 02:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 02:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 02:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 02:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 02:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 02:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 02:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 02:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 02:58 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-MW14 Lab ID:92337093004 Collected:04/12/17 11:48 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 02:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 02:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 02:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 02:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 02:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 02:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 02:58 108-10-11000.33 1
Styrene ND ug/L 04/14/17 02:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 02:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 02:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 02:58 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 02:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 02:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 02:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 02:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 02:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 02:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 02:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 02:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 02:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)90 %04/14/17 02:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %04/14/17 02:58 17060-07-070-130 1
Toluene-d8 (S)109 %04/14/17 02:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW1 Lab ID:92337093005 Collected:04/12/17 13:10 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:22 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:22 7440-38-204/18/17 00:3010.0 5.0 1
Barium 59.1J ug/L 04/19/17 02:22 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:22 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:22 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:22 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:22 7440-48-404/18/17 00:3010.0 2.5 1
Copper ND ug/L 04/19/17 02:22 7440-50-804/18/17 00:3010.0 2.5 1
Lead ND ug/L 04/19/17 02:22 7439-92-104/18/17 00:3010.0 2.5 1
Nickel ND ug/L 04/19/17 02:22 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:22 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:22 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:22 7440-62-204/18/17 00:3025.0 2.5 1
Zinc 54.8 ug/L 04/19/17 02:22 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:38 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 03:16 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 03:16 107-13-12001.9 1
Benzene ND ug/L 04/14/17 03:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 03:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 03:16 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 03:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 03:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 03:16 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 03:16 75-15-01001.2 1
Carbon tetrachloride 1.0 ug/L 04/14/17 03:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 03:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 03:16 75-00-310.0 0.54 1
Chloroform 6.3 ug/L 04/14/17 03:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 03:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 03:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 03:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 03:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 03:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 03:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 03:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 03:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 03:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 03:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 03:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.0J ug/L 04/14/17 03:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 03:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 03:16 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW1 Lab ID:92337093005 Collected:04/12/17 13:10 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 03:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 03:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 03:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 03:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 03:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 03:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 03:16 108-10-11000.33 1
Styrene ND ug/L 04/14/17 03:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 03:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 03:16 79-34-53.0 0.40 1
Tetrachloroethene 5.2 ug/L 04/14/17 03:16 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 03:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 03:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 03:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 03:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 03:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 03:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 03:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 03:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 03:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)91 %04/14/17 03:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %04/14/17 03:16 17060-07-070-130 1
Toluene-d8 (S)108 %04/14/17 03:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW2 Lab ID:92337093006 Collected:04/12/17 11:20 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:25 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:25 7440-38-204/18/17 00:3010.0 5.0 1
Barium 80.6J ug/L 04/19/17 02:25 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:25 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:25 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:25 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:25 7440-48-404/18/17 00:3010.0 2.5 1
Copper 4.7J ug/L 04/19/17 02:25 7440-50-804/18/17 00:3010.0 2.5 1
Lead 2.9J ug/L 04/19/17 02:25 7439-92-104/18/17 00:3010.0 2.5 1
Nickel 4.0J ug/L 04/19/17 02:25 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:25 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:25 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:25 7440-62-204/18/17 00:3025.0 2.5 1
Zinc 29.9 ug/L 04/19/17 02:25 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:40 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 03:34 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 03:34 107-13-12001.9 1
Benzene 0.26J ug/L 04/14/17 03:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 03:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 03:34 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 03:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 03:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 03:34 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 03:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 03:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 03:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 03:34 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 03:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 03:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 03:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 03:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 03:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 03:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 03:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 03:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 03:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 03:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 03:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 03:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 03:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 03:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 03:34 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW2 Lab ID:92337093006 Collected:04/12/17 11:20 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 03:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 03:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 03:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 03:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 03:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 03:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 03:34 108-10-11000.33 1
Styrene ND ug/L 04/14/17 03:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 03:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 03:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 03:34 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 03:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 03:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 03:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 03:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 03:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 03:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 03:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 03:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 03:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)93 %04/14/17 03:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %04/14/17 03:34 17060-07-070-130 1
Toluene-d8 (S)112 %04/14/17 03:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW3 Lab ID:92337093007 Collected:04/12/17 10:05 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:28 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:28 7440-38-204/18/17 00:3010.0 5.0 1
Barium 49.1J ug/L 04/19/17 02:28 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:28 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:28 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:28 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:28 7440-48-404/18/17 00:3010.0 2.5 1
Copper 3.2J ug/L 04/19/17 02:28 7440-50-804/18/17 00:3010.0 2.5 1
Lead 2.9J ug/L 04/19/17 02:28 7439-92-104/18/17 00:3010.0 2.5 1
Nickel ND ug/L 04/19/17 02:28 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:28 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:28 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:28 7440-62-204/18/17 00:3025.0 2.5 1
Zinc 36.8 ug/L 04/19/17 02:28 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:42 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 03:51 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 03:51 107-13-12001.9 1
Benzene ND ug/L 04/14/17 03:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 03:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 03:51 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 03:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 03:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 03:51 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 03:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 03:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 03:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 03:51 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 03:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 03:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 03:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 03:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 03:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 03:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 03:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 03:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 03:51 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 03:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 03:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 03:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 03:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 03:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 03:51 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW3 Lab ID:92337093007 Collected:04/12/17 10:05 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 03:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 03:51 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 03:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 03:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 03:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 03:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 03:51 108-10-11000.33 1
Styrene ND ug/L 04/14/17 03:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 03:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 03:51 79-34-53.0 0.40 1
Tetrachloroethene 0.98J ug/L 04/14/17 03:51 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 03:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 03:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 03:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 03:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 03:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 03:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 03:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 03:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 03:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)93 %04/14/17 03:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %04/14/17 03:51 17060-07-070-130 1
Toluene-d8 (S)106 %04/14/17 03:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW4 Lab ID:92337093008 Collected:04/12/17 11:30 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:31 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:31 7440-38-204/18/17 00:3010.0 5.0 1
Barium 82.1J ug/L 04/19/17 02:31 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:31 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:31 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:31 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:31 7440-48-404/18/17 00:3010.0 2.5 1
Copper 4.1J ug/L 04/19/17 02:31 7440-50-804/18/17 00:3010.0 2.5 1
Lead 4.1J ug/L 04/19/17 02:31 7439-92-104/18/17 00:3010.0 2.5 1
Nickel 3.6J ug/L 04/19/17 02:31 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:31 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:31 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:31 7440-62-204/18/17 00:3025.0 2.5 1
Zinc 31.6 ug/L 04/19/17 02:31 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:44 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 04:09 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 04:09 107-13-12001.9 1
Benzene ND ug/L 04/14/17 04:09 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 04:09 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 04:09 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 04:09 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 04:09 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 04:09 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 04:09 75-15-0 M11001.2 1
Carbon tetrachloride ND ug/L 04/14/17 04:09 56-23-5 M11.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 04:09 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 04:09 75-00-3 M110.0 0.54 1
Chloroform ND ug/L 04/14/17 04:09 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 04:09 74-87-3 M11.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 04:09 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 04:09 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 04:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 04:09 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 04:09 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 04:09 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 04:09 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 04:09 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 04:09 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 04:09 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 04:09 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 04:09 156-60-5 M15.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 04:09 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-SW4 Lab ID:92337093008 Collected:04/12/17 11:30 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 04:09 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 04:09 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 04:09 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 04:09 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 04:09 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 04:09 75-09-2 M11.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 04:09 108-10-11000.33 1
Styrene ND ug/L 04/14/17 04:09 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 04:09 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 04:09 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 04:09 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 04:09 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 04:09 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 04:09 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 04:09 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 04:09 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 04:09 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 04:09 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 04:09 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 04:09 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)93 %04/14/17 04:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %04/14/17 04:09 17060-07-070-130 1
Toluene-d8 (S)109 %04/14/17 04:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-FIELD BLANK Lab ID:92337093009 Collected:04/12/17 13:45 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 04/19/17 02:34 7440-36-004/18/17 00:306.0 3.9 1
Arsenic ND ug/L 04/19/17 02:34 7440-38-204/18/17 00:3010.0 5.0 1
Barium ND ug/L 04/19/17 02:34 7440-39-304/18/17 00:301002.5 1
Beryllium ND ug/L 04/19/17 02:34 7440-41-704/18/17 00:301.0 0.50 1
Cadmium ND ug/L 04/19/17 02:34 7440-43-904/18/17 00:301.0 0.50 1
Chromium ND ug/L 04/19/17 02:34 7440-47-304/18/17 00:3010.0 2.5 1
Cobalt ND ug/L 04/19/17 02:34 7440-48-404/18/17 00:3010.0 2.5 1
Copper ND ug/L 04/19/17 02:34 7440-50-804/18/17 00:3010.0 2.5 1
Lead ND ug/L 04/19/17 02:34 7439-92-104/18/17 00:3010.0 2.5 1
Nickel ND ug/L 04/19/17 02:34 7440-02-004/18/17 00:3050.0 2.5 1
Selenium ND ug/L 04/19/17 02:34 7782-49-204/18/17 00:3010.0 5.0 1
Silver ND ug/L 04/19/17 02:34 7440-22-404/18/17 00:3010.0 2.5 1
Vanadium ND ug/L 04/19/17 02:34 7440-62-204/18/17 00:3025.0 2.5 1
Zinc ND ug/L 04/19/17 02:34 7440-66-604/18/17 00:3010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 04/18/17 13:46 7440-28-004/17/17 20:305.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 04:44 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 04:44 107-13-12001.9 1
Benzene ND ug/L 04/14/17 04:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 04:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 04:44 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 04:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 04:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 04:44 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 04:44 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 04:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 04:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 04:44 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 04:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 04:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 04:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 04:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 04:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 04:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 04:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 04:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 04:44 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 04:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 04:44 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 04:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 04:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 04:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 04:44 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-FIELD BLANK Lab ID:92337093009 Collected:04/12/17 13:45 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 04/14/17 04:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 04:44 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 04:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 04:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 04:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 04:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 04:44 108-10-11000.33 1
Styrene ND ug/L 04/14/17 04:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 04:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 04:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 04:44 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 04:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 04:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 04:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 04:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 04:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 04:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 04:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 04:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/17 04:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)92 %04/14/17 04:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %04/14/17 04:44 17060-07-070-130 1
Toluene-d8 (S)109 %04/14/17 04:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-TRIP BLANK Lab ID:92337093010 Collected:04/12/17 07:00 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/17 05:02 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/17 05:02 107-13-12001.9 1
Benzene ND ug/L 04/14/17 05:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/17 05:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/17 05:02 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/17 05:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/17 05:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/17 05:02 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/17 05:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/17 05:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/17 05:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/17 05:02 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/17 05:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/17 05:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/17 05:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/17 05:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/17 05:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/17 05:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/17 05:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/17 05:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/17 05:02 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/17 05:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/17 05:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/17 05:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/17 05:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/17 05:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/17 05:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/17 05:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/17 05:02 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/17 05:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/17 05:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/17 05:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/17 05:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/17 05:02 108-10-11000.33 1
Styrene ND ug/L 04/14/17 05:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/17 05:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/17 05:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/17 05:02 127-18-41.0 0.46 1
Toluene ND ug/L 04/14/17 05:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/17 05:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/17 05:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/17 05:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/17 05:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/17 05:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/17 05:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/17 05:02 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Sample:3420-TRIP BLANK Lab ID:92337093010 Collected:04/12/17 07:00 Received:04/13/17 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 04/14/17 05:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %04/14/17 05:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %04/14/17 05:02 17060-07-070-130 1
Toluene-d8 (S)109 %04/14/17 05:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
356838
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1979709
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 04/19/17 01:133.9
Arsenic ug/L ND 10.0 04/19/17 01:135.0
Barium ug/L ND 100 04/19/17 01:132.5
Beryllium ug/L ND 1.0 04/19/17 01:130.50
Cadmium ug/L ND 1.0 04/19/17 01:130.50
Chromium ug/L ND 10.0 04/19/17 01:132.5
Cobalt ug/L ND 10.0 04/19/17 01:132.5
Copper ug/L ND 10.0 04/19/17 01:132.5
Lead ug/L ND 10.0 04/19/17 01:132.5
Nickel ug/L ND 50.0 04/19/17 01:132.5
Selenium ug/L ND 10.0 04/19/17 01:135.0
Silver ug/L ND 10.0 04/19/17 01:132.5
Vanadium ug/L ND 25.0 04/19/17 01:132.5
Zinc ug/L ND 10.0 04/19/17 01:135.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1979710LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 500500 100 80-120
Arsenic ug/L 492500 98 80-120
Barium ug/L 490500 98 80-120
Beryllium ug/L 484500 97 80-120
Cadmium ug/L 499500 100 80-120
Chromium ug/L 511500 102 80-120
Cobalt ug/L 504500 101 80-120
Copper ug/L 515500 103 80-120
Lead ug/L 496500 99 80-120
Nickel ug/L 494500 99 80-120
Selenium ug/L 506500 101 80-120
Silver ug/L 253250 101 80-120
Vanadium ug/L 486500 97 80-120
Zinc ug/L 513500 103 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1979711MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92337193001
1979712
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 100 75-125101 1 20500ND500506
Arsenic ug/L 500 98 75-125100 1 20500ND493499
Barium ug/L 500 99 75-12599 0 2050023.4 520 520
Beryllium ug/L 500 99 75-12599 0 20500ND497497
Cadmium ug/L 500 99 75-125100 1 20500ND494499
Chromium ug/L 500 100 75-125102 1 20500ND504511
Cobalt ug/L 500 99 75-125100 1 20500ND495499
Copper ug/L 500 103 75-125104 1 20500ND516521
Lead ug/L 500 97 75-12598 1 20500ND484488
Nickel ug/L 500 96 75-12597 1 20500ND484488
Selenium ug/L 500 100 75-125101 1 20500ND500503
Silver ug/L 250 100 75-125101 1 20250ND250254
Vanadium ug/L 500 98 75-12598 0 20500ND490490
Zinc ug/L 500 101 75-125103 1 205008.3J 515 521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
356803
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1979591
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 5.5 04/18/17 12:520.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1979592LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 95.8100 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1979593MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92337193001
1979594
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 95 75-12595 1 201000.022J 94.7 95.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1979595MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92337093003
1979596
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 91 75-12590 1 20100ND90.5 89.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
356614
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009, 92337093010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1978417
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009, 92337093010
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/13/17 19:370.33
1,1,1-Trichloroethane ug/L ND 1.0 04/13/17 19:370.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 04/13/17 19:370.40
1,1,2-Trichloroethane ug/L ND 1.0 04/13/17 19:370.29
1,1-Dichloroethane ug/L ND 5.0 04/13/17 19:370.32
1,1-Dichloroethene ug/L ND 5.0 04/13/17 19:370.56
1,2,3-Trichloropropane ug/L ND 1.0 04/13/17 19:370.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 04/13/17 19:372.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/13/17 19:370.27
1,2-Dichlorobenzene ug/L ND 5.0 04/13/17 19:370.30
1,2-Dichloroethane ug/L ND 1.0 04/13/17 19:370.24
1,2-Dichloropropane ug/L ND 1.0 04/13/17 19:370.27
1,4-Dichlorobenzene ug/L ND 1.0 04/13/17 19:370.33
2-Butanone (MEK)ug/L ND 100 04/13/17 19:370.96
2-Hexanone ug/L ND 50.0 04/13/17 19:370.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 04/13/17 19:370.33
Acetone ug/L ND 100 04/13/17 19:3710.0
Acrylonitrile ug/L ND 200 04/13/17 19:371.9
Benzene ug/L ND 1.0 04/13/17 19:370.25
Bromochloromethane ug/L ND 3.0 04/13/17 19:370.17
Bromodichloromethane ug/L ND 1.0 04/13/17 19:370.18
Bromoform ug/L ND 3.0 04/13/17 19:370.26
Bromomethane ug/L ND 10.0 04/13/17 19:370.29
Carbon disulfide ug/L ND 100 04/13/17 19:371.2
Carbon tetrachloride ug/L ND 1.0 04/13/17 19:370.25
Chlorobenzene ug/L ND 3.0 04/13/17 19:370.23
Chloroethane ug/L ND 10.0 04/13/17 19:370.54
Chloroform ug/L ND 5.0 04/13/17 19:370.14
Chloromethane ug/L ND 1.0 04/13/17 19:370.11
cis-1,2-Dichloroethene ug/L ND 5.0 04/13/17 19:370.19
cis-1,3-Dichloropropene ug/L ND 1.0 04/13/17 19:370.13
Dibromochloromethane ug/L ND 3.0 04/13/17 19:370.21
Dibromomethane ug/L ND 10.0 04/13/17 19:370.21
Ethylbenzene ug/L ND 1.0 04/13/17 19:370.30
Iodomethane ug/L ND 10.0 04/13/17 19:370.32
Methylene Chloride ug/L ND 1.0 04/13/17 19:370.97
Styrene ug/L ND 1.0 04/13/17 19:370.26
Tetrachloroethene ug/L ND 1.0 04/13/17 19:370.46
Toluene ug/L ND 1.0 04/13/17 19:370.26
trans-1,2-Dichloroethene ug/L ND 5.0 04/13/17 19:370.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
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[phone]
Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1978417
Associated Lab Samples:92337093001, 92337093002, 92337093003, 92337093004, 92337093005, 92337093006, 92337093007,
92337093008, 92337093009, 92337093010
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 04/13/17 19:370.26
trans-1,4-Dichloro-2-butene ug/L ND 100 04/13/17 19:371.0
Trichloroethene ug/L ND 1.0 04/13/17 19:370.47
Trichlorofluoromethane ug/L ND 1.0 04/13/17 19:370.20
Vinyl acetate ug/L ND 50.0 04/13/17 19:370.35
Vinyl chloride ug/L ND 1.0 04/13/17 19:370.62
Xylene (Total)ug/L ND 5.0 04/13/17 19:370.66
1,2-Dichloroethane-d4 (S)%88 70-130 04/13/17 19:37
4-Bromofluorobenzene (S)%93 70-130 04/13/17 19:37
Toluene-d8 (S)%108 70-130 04/13/17 19:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1978418LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 80-125
1,1,1-Trichloroethane ug/L 54.850 110 71-129
1,1,2,2-Tetrachloroethane ug/L 49.050 98 79-124
1,1,2-Trichloroethane ug/L 53.950 108 85-125
1,1-Dichloroethane ug/L 49.950 100 73-126
1,1-Dichloroethene ug/L 58.750 117 66-135
1,2,3-Trichloropropane ug/L 47.150 94 75-130
1,2-Dibromo-3-chloropropane ug/L 45.050 90 71-133
1,2-Dibromoethane (EDB)ug/L 54.150 108 83-124
1,2-Dichlorobenzene ug/L 50.650 101 80-133
1,2-Dichloroethane ug/L 48.250 96 67-128
1,2-Dichloropropane ug/L 52.450 105 75-132
1,4-Dichlorobenzene ug/L 49.250 98 78-130
2-Butanone (MEK)ug/L 98.7J100 99 61-144
2-Hexanone ug/L 89.2100 89 68-143
4-Methyl-2-pentanone (MIBK)ug/L 89.0J100 89 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 251250 100 40-160
Benzene ug/L 52.750 105 80-125
Bromochloromethane ug/L 55.250 110 71-125
Bromodichloromethane ug/L 54.850 110 78-124
Bromoform ug/L 42.050 84 71-128
Bromomethane ug/L 54.550 109 40-160
Carbon disulfide ug/L 55.9J50 112 50-160
Carbon tetrachloride ug/L 58.150 116 69-131
Chlorobenzene ug/L 52.450 105 81-122
Chloroethane ug/L 66.150 132 39-148
Chloroform ug/L 50.650 101 73-127
Chloromethane ug/L 57.650 115 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1978418LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 47.750 95 74-124
cis-1,3-Dichloropropene ug/L 52.050 104 72-132
Dibromochloromethane ug/L 56.050 112 78-125
Dibromomethane ug/L 53.450 107 82-120
Ethylbenzene ug/L 50.550 101 79-121
Iodomethane ug/L 115100 115 39-154
Methylene Chloride ug/L 55.650 111 64-133
Styrene ug/L 47.750 95 84-126
Tetrachloroethene ug/L 55.350 111 78-122
Toluene ug/L 48.150 96 80-121
trans-1,2-Dichloroethene ug/L 58.450 117 71-127
trans-1,3-Dichloropropene ug/L 51.650 103 69-141
trans-1,4-Dichloro-2-butene ug/L 42.7J50 85 40-160
Trichloroethene ug/L 57.250 114 78-122
Trichlorofluoromethane ug/L 67.450 135 53-137
Vinyl acetate ug/L 95.8100 96 40-160
Vinyl chloride ug/L 49.450 99 58-137
Xylene (Total)ug/L 142150 95 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1978420MATRIX SPIKE SAMPLE:
MSSpike
Result
92337093008
1,1,1,2-Tetrachloroethane ug/L 21.220 106 70-130ND
1,1,1-Trichloroethane ug/L 26.020 130 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,2-Trichloroethane ug/L 21.920 110 70-130ND
1,1-Dichloroethane ug/L 23.420 117 70-130ND
1,1-Dichloroethene ug/L 30.720 154 70-166ND
1,2,3-Trichloropropane ug/L 20.220 101 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.020 95 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.820 109 70-130ND
1,2-Dichlorobenzene ug/L 21.520 108 70-130ND
1,2-Dichloroethane ug/L 21.820 108 70-130ND
1,2-Dichloropropane ug/L 22.520 113 70-130ND
1,4-Dichlorobenzene ug/L 21.320 106 70-130ND
2-Butanone (MEK)ug/L 36.7J40 92 70-130ND
2-Hexanone ug/L 37.5J40 94 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.6J40 99 70-130ND
Acetone ug/L 42.6J40 106 70-130ND
Acrylonitrile ug/L 112J100 112 70-130ND
Benzene ug/L 24.920 125 70-148ND
Bromochloromethane ug/L 24.320 122 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1978420MATRIX SPIKE SAMPLE:
MSSpike
Result
92337093008
Bromodichloromethane ug/L 23.420 117 70-130ND
Bromoform ug/L 19.220 96 70-130ND
Bromomethane ug/L 23.020 115 70-130ND
Carbon disulfide ug/L 27.3J M12013770-130ND
Carbon tetrachloride ug/L 28.0 M12014070-130ND
Chlorobenzene ug/L 23.120 115 70-146ND
Chloroethane ug/L 28.5 M12014270-130ND
Chloroform ug/L 24.320 121 70-130ND
Chloromethane ug/L 29.2 M12014670-130ND
cis-1,2-Dichloroethene ug/L 23.720 118 70-130ND
cis-1,3-Dichloropropene ug/L 21.720 108 70-130ND
Dibromochloromethane ug/L 21.920 109 70-130ND
Dibromomethane ug/L 23.920 120 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 52.140 130 70-130ND
Methylene Chloride ug/L 26.4 M12013270-130ND
Styrene ug/L 20.420 102 70-130ND
Tetrachloroethene ug/L 24.720 124 70-130ND
Toluene ug/L 22.920 115 70-155ND
trans-1,2-Dichloroethene ug/L 27.0 M12013570-130ND
trans-1,3-Dichloropropene ug/L 21.420 107 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.5J20 98 70-130ND
Trichloroethene ug/L 24.420 122 69-151ND
Trichlorofluoromethane ug/L 31.4 M12015770-130ND
Vinyl acetate ug/L 37.5J40 94 70-130ND
Vinyl chloride ug/L 22.920 114 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92337093007
1978419SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92337093007
1978419SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 1.1 300.98J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%86 591
4-Bromofluorobenzene (S)%93 193
Toluene-d8 (S)%110 4106
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92337093
OMNISOURCE/KERNERSVILLE LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92337093001 356838 3569643420-MW1R EPA 3010A EPA 6010
92337093002 356838 3569643420-MW12 EPA 3010A EPA 6010
92337093003 356838 3569643420-MW13 EPA 3010A EPA 6010
92337093004 356838 3569643420-MW14 EPA 3010A EPA 6010
92337093005 356838 3569643420-SW1 EPA 3010A EPA 6010
92337093006 356838 3569643420-SW2 EPA 3010A EPA 6010
92337093007 356838 3569643420-SW3 EPA 3010A EPA 6010
92337093008 356838 3569643420-SW4 EPA 3010A EPA 6010
92337093009 356838 3569643420-FIELD BLANK EPA 3010A EPA 6010
92337093001 356803 3569563420-MW1R EPA 3010A EPA 6020B
92337093002 356803 3569563420-MW12 EPA 3010A EPA 6020B
92337093003 356803 3569563420-MW13 EPA 3010A EPA 6020B
92337093004 356803 3569563420-MW14 EPA 3010A EPA 6020B
92337093005 356803 3569563420-SW1 EPA 3010A EPA 6020B
92337093006 356803 3569563420-SW2 EPA 3010A EPA 6020B
92337093007 356803 3569563420-SW3 EPA 3010A EPA 6020B
92337093008 356803 3569563420-SW4 EPA 3010A EPA 6020B
92337093009 356803 3569563420-FIELD BLANK EPA 3010A EPA 6020B
92337093001 3566143420-MW1R EPA 8260
92337093002 3566143420-MW12 EPA 8260
92337093003 3566143420-MW13 EPA 8260
92337093004 3566143420-MW14 EPA 8260
92337093005 3566143420-SW1 EPA 8260
92337093006 3566143420-SW2 EPA 8260
92337093007 3566143420-SW3 EPA 8260
92337093008 3566143420-SW4 EPA 8260
92337093009 3566143420-FIELD BLANK EPA 8260
92337093010 3566143420-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/20/2017 04:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 39
Page 37 of 39
Page 38 of 39
Page 39 of 39