3412_ForsythCoOldSalisburyRdCDLF_GWMR_DIN28674_20170717

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ASSESSMENT
MONITORING
REPORT
Including the May 2017 Groundwater
Sampling Event
Old Salisbury Road Landfill
NCDEQ Permit NO. 34-12
HDR Project No. 10043322
Forsyth County, North Carolina
July 2017

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Table of Contents
Table of Contents
List of Tables ........................................................................................................................ i
List of Figures ....................................................................................................................... i
Appendices .......................................................................................................................... ii
List of Acronyms .................................................................................................................. ii
1.0 Introduction ..................................................................................................................... 1
1.1. Facility Background ...................................................................................................... 1
1.2. Regulatory Authority .................................................................................................... 1
1.3. Geologic Characteristics .............................................................................................. 3
1.3.1. Regional Geologic and Hydrogeologic Setting ...................................................... 3
1.3.2. Site Specific Topography and Drainage ................................................................ 3
1.3.3. Site Specific Hydrogeology ................................................................................... 4
2.0 Monitoring Network ......................................................................................................... 5
3.0 Data Collection ................................................................................................................ 7
4.0 Results ............................................................................................................................ 9
4.1. Detected Groundwater Constituents ............................................................................ 9
4.2. Landfill Gas .................................................................................................................10
5.0 Summary & Recommendations ......................................................................................11

List of Tables
Table 1 - Existing Groundwater Monitoring Well Details ............................................................. 5
Table 2 - Sampling Schedule ..................................................................................................... 6
Table 3 - Recent Water Level Readings ..................................................................................... 7
Table 4 - Hydraulic Gradient & Flow Velocity ............................................................................. 8
Table 5 - Methane Gas Readings..............................................................................................10
Table 6 - Event Lab Summary – May 2017 ...............................................................................12
Table 7 - Event Field Summary – May 2017 .............................................................................13

List of Figures
Figure 1 - Groundwater Contours and Sample Locations – Spring 2017 .................................... 2
Figure 2 - Historic Groundwater Elevations ................................................................................ 7
Figure 3 - Selected Groundwater Detections in MW-2R ............................................................. 9

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Table of Contents
Appendices
Appendix A – Summary of Groundwater Monitoring Results
Appendix B – Laboratory Groundwater Report
Appendix C – Field Data
Appendix D – Electronic Files

List of Acronyms
2L 15A NCAC Subchapter 02L - Groundwater Classification and Standards
µg/L micrograms per liter
EPA United States Environmental Protection Agency
MCL Maximum Contaminant Level
MDL method detction limit
NC DENR North Carolina Department of Environment and Natural Resources
NCDEQ North Carolina Department of Environmental Quality1
ND not detected in sample
NS not sampled
NTU Nephelometric turbidity units
PCB polychlorinated biphenyl
PCE tetrachloroethene
PRL practical reporting limit
PVC polyvinyl chloride
SWSL solid waste section limits
SVOC semi-volatile organic compound
VOC volatile organic compound
USGS U.S. Geological Survey
1Prior to September 18, 2015, the NCDEQ was referred to as the NC DENR. Both naming conventions are used in this report, as appropriate.

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Introduction
1.0 Introduction
HDR Engineering, Inc. of the Carolinas (HDR), on behalf of the Winston-Salem City/County
Utility Commission (the City), is hereby submitting assessment monitoring results for
groundwater at the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North
Carolina. The assessment monitoring is being conducted to address the detection of benzene
and tetrachloroethene (PCE) above the groundwater monitoring standards in samples collected
from groundwater monitoring well MW-2R during the May 2011 and June 2011 events.
1.1. Facility Background
The OSR landfill covers approximately 56 acres and is situated within a 140-acre tract north of
Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The
site is accessed via Old Salisbury Road (State Road 3011). The Forsyth/Davidson County line
borders the site to the south. Figure 1 illustrates the location of the OSR landfill. The facility was
originally issued a permit to operate on July 3, 1996 and opened in August of the same year.
1.2. Regulatory Authority
The site is currently operated under NC DENR facility permit number 34-12 dated April 6, 2015
(DIN 23258). The groundwater monitoring and reporting requirements are addressed in Items
36 to 45 of the permit. A Groundwater Monitoring Plan was last approved as noted by NC
DENR on March 5, 2015 (DIN 23910). Groundwater and surface water monitoring plans for the
site are addressed by NC Solid Waste Management Rules 15A NCAC 13B .0544(b) and
.0544(c) respectively. The site is currently in assessment monitoring due to detections in MW-
2R.
An Assessment Monitoring Plan for MW-2R was submitted in accordance with 15A NCAC 13B
.0545 by HDR on December 9, 2011. The plan was approved with two exceptions on January
17, 2012. The first exception required the location of MW-15 to be in the same flow path as
MW-2R; the second required all wells to be sampled for Appendix II constituents.
In February of 2014 the City requested, and NC DENR approved, the following modifications to
the facility’s assessment monitoring program.
• Groundwater monitoring wells MW-1R, MW-2R, MW-4R and MW-15 will be sampled
semiannually for Appendix I constituents and those additional constituents in Appendix II
that have been detected in the last two years;
• Groundwater monitoring wells MW-1R, MW-2R, MW-4R and MW-15 will be sampled
during every other Fall event for the entire Appendix II constituent list. The next event for
this occurred in the Fall of 2015. Additional Appendix II constituents detected will be
added to the sampling program for subsequent semiannual events; and
• All of the other remaining groundwater monitoring wells and surface water locations will
continue to be sampled semiannually for the full Appendix I constituent list.
In May 2014, the monitoring plan for the facility was updated to incorporate the recent changes
and submitted as part of the renewal package for the facility’s NC DENR Permit to Operate. In
1
FORSYTH COUNTY
DAVIDSON COUNTY FORSYTH COUNTY
DAVIDSON COUNTY
V
IV
VI
II
I
SHEET TITLE
PROJECT TITLE
PROJECT MANAGER
DATE
PROJECT NUMBER
REFERENCE DOCUMENT
EXHIBIT NUMBER
REFERENCE SHEET
SHEET TITLE
PROJECT TITLE
GROUNDWATER CONTOURS
AND SAMPLE LOCATIONS
SPRING 2017
Winston-Salem City/County Utilities | Assessment Monitoring Report
Introduction
the Fall 2015 (Annual) Report HDR recommended a change to the semi-annual sampling
schedule. NCDEQ approved the additional parameters and wells. No parameters were
approved to be removed.
1.3. Geologic Characteristics
This section paraphrases the descriptions in the original July 2003 Ground Water Monitoring
Plan and the 2003 Design Hydrogeologic Investigation Report.
1.3.1. Regional Geologic and Hydrogeologic Setting
According to the 1985 Geologic Map of North Carolina, OSR is located in the Charlotte belt of
the Piedmont Physiographic Province. This Province contains metamorphic and igneous
plutonic rocks, which in some areas have been extensively weathered and eroded forming an
undulating and well-dissected topography.
Subsurface conditions generally consist of a veneer of topsoil underlain by residual soils,
saprolite, partially weathered rock, and fractured rock. There is generally a gradual transition
from one material type to the next with varying thickness of each.
The area is underlain by granite rock. The bedrock is typically fractured and is overlain by highly
weathered bedrock called saprolite. The saprolite varies in thickness from a few feet near
bedrock outcrops to over 100 feet. The saprolite material retains some of the original (relict)
structural features of the parent rock. The nearer surface residual soils are formed by the in-
place physical and chemical weathering of the saprolite and usually do not retain the relict
structural features.
In the Piedmont Physiographic Province, groundwater is present within the openings created by
fractures and joints within the bedrock and within the pore spaces of the overlying-saprolite. The
saprolite/bedrock aquifers are primarily recharged by precipitation in the interstream areas,
which infiltrates through the unsaturated zone to the water table. The depth to groundwater is
generally deeper beneath uplands than beneath valleys. The water table is commonly close to
the top of bedrock and is more often than not, located within the saprolite. Groundwater
generally moves laterally and downward through the saprolite and bedrock toward streams, and
surface water bodies. The water table surface is generally a subdued reflection of the surface
topography.
1.3.2. Site Specific Topography and Drainage
Surface drainage at the subject site is primarily controlled by a north-northwesterly trending
ridge within the property. Surface runoff is directed by a ridge within the site. Construction of the
landfill generally mimics and replaced the natural ridge that existed prior to the landfill. This
ridge directs runoff northeast, west and southwest into tributaries of South Fork Muddy Creek.
The majority of surface runoff within this site is directed to South Fork Muddy Creek on the
north. A small area in the extreme southeasterly section of the site appears to drain south into
Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow to the west where they
converge with Muddy Creek. Muddy Creek flows to the south and converges with the Yadkin
River.
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Winston-Salem City/County Utilities | Assessment Monitoring Report
Introduction
1.3.3. Site Specific Hydrogeology
As documented in the Design Hydrogeological Investigation Report submitted by HDR on
December 2, 2003, the uppermost aquifer underlying the facility is comprised of three
stratigraphic units. The stratigraphic downward progression of the three units is saprolite
transitioning into partially weather bedrock, then competent bedrock. Groundwater flow through
the saprolite and partially weathered bedrock is through the soil matrix, while groundwater flow
through the bedrock is primarily fracture flow.
The average effective porosity of the saprolite stratum is 17 (unitless), while the saprolite
transition zone has an effective porosity of 25. The effective porosity of the bedrock is
significantly less at 2.
The historical hydraulic conductivity (K) calculated for the saprolite is 0.259 feet per day (ft./day)
(9.1 x 10-5 cm/sec). The historical average hydraulic conductivity for the transition zone is 0.466
ft./day (1.65 x 10-4 cm/sec). The historic hydraulic conductivity of the bedrock aquifer was
considerably less than either the saprolite or transition zone units with a K value of 0.043 ft./day
(1.5 x 10-5 cm/sec). Detailed calculations of the hydraulic conductivity, flow rates, and porosity
were provided in the 2003 Design Hydrogeologic Investigation Report.
Based on historical field observations (i.e., soil boring records) and laboratory test results from
the 2003 Design Hydrogeologic Investigation Report, the uppermost aquifer beneath the facility
predominantly exists within the unconsolidated saprolite soil and transition zone units that have
been classified as micaceous silty sands and sandy silts produced by the in-situ weathering of
the granodiorite parent rock. Groundwater flow within the uppermost aquifer is predominantly
porous flow through the unconsolidated units. There is no evidence of discrete flow patterns
within the saprolite and transition zones of the uppermost aquifer resulting from relict quartz
veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In
general, the flow of groundwater occurs for the facility is from higher elevations onsite to lower
elevations onsite under unconfined (water table) conditions regardless of the stratigraphic unit in
which it resides. As such, the static water table generally mimics the topography.

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Monitoring Network
2.0 Monitoring Network
Sampling occurs semiannually for the site monitoring wells and four surface water monitoring
locations. The groundwater monitoring locations are depicted on the Figure 1. Table 1 provides
location and construction details for the existing monitoring wells.
Groundwater monitoring well MW-1R is located hydraulically upgradient of the landfill and is
considered as the background well for the site. Upstream surface water (SW-1) and
downstream surface water (SW-2) samples are obtained from the adjacent stream to the east.
Surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity
of MW-2R. SW-3 is located south of the entrance road near MW-2R; SW-4 is located on the
north side of the entrance road, downstream of SW-3.
Table 1 - Existing Groundwater Monitoring Well Details

The sampled locations were evaluated by the methods and for the analytical parameters listed
in Table 2. Samples were collected from each of the landfill groundwater wells using the
dedicated QEDTM MicroPurge ® pumps that were installed in August 2004, except MW-15,
which is sampled with a bailer. Field measurements of pH, conductivity, redox, temperature,
turbidity, dissolved oxygen, and depth to groundwater are collected for each well in addition to
the parameters listed in Table 2.

OSR LF
WELL Installed
NC Sate
Plane
Northing
NC Sate
Plane
Easting
Well
Diameter
(inches)
Well
Depth
(below
ground)
Depth:
Ground to
Top of
Screen
Screened
Interval
(ft)
Screened Interval
Geology
Top Of
Casing
Elevation
(ft MSL)
Ground
Elevation
(ft MSL)
MW-1R 12/27/1995 820,411 1,622,983 2 60.0 45 15 Granitic saprolite 836.42 833.40
MW-2R 12/29/1995 820,974 1,622,722 2 23.0 8 15 Granitic saprolite 785.22 781.81MW-3R 7/7/1999 821,237 1,621,463 2 27.0 12 15 Granitic saprolite 776.60 772.90MW-4R 12/28/1995 820,435 1,621,428 2 20.0 5 15 Granitic saprolite 767.96 765.70
MW-5R 12/29/1995 820,137 1,622,130 2 32.0 17 15 Granitic saprolite 784.36 782.30MW-7 12/28/1995 820,886 1,621,424 2 48.0 33 15 Granitic saprolite 803.66 802.10MW-8 7/7/1999 821,930 1,621,485 2 27.0 12 15 Granitic saprolite 762.50 759.80
MW-9 8/11/2004 822,311 1,621,986 2 60.0 45 15 Sand 790.28 788.04MW-10 8/10/2004 822,626 1,622,699 2 21.0 6 15 Sand 738.21 735.70MW-11 8/10/2004 822,307 1,622,838 2 20.0 5 15 Sand 732.59 730.35
MW-12 8/9/2004 821,844 1,622,955 2 16.0 6 10 Silt 739.07 736.41MW-13 8/9/2004 821,500 1,622,915 2 20.0 5 15 Sand 751.23 749.19
MW-14 8/11/2004 822,420 1,622,260 2 60.0 45 15 Sand 783.88 781.44MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58
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Winston-Salem City/County Utilities | Assessment Monitoring Report
Monitoring Network
Table 2 - Sampling Schedule
Method Parameter(s) Frequency Monitoring Wells Surface Water
EPA 300.0 Sulfate 2x/year All All
EPA 6010 Trace Metals 2x/year All All
EPA 7470 Mercury 2x/year All All
EPA 8081
Pesticides Fall of odd years (2017) All None
4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, delta-BHC, Endosulfan I,
Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Heptachlor epoxide & Methoxychlor
(Pesticides recently detected)
2x/year
MW-1R, MW-2R,
MW-4, MW-7, MW-10 & MW-15 None
EPA 8082 PCB’s Fall of odd years (2017) All None
EPA 8151
Herbicides Fall of odd years (2017) All None
2,4,5-TP (Silvex), 2,4-D
(Herbicides previously detected) 2x/year MW-1R, MW-2R,
MW-4R & MW-15 None
EPA 8260
App I VOCs + Tetrahydrofuran 2x/year All All
Appendix II VOCs Fall of odd years (2017) All None
Dichlorodifluoromethane
(Appendix II VOC
recently detected)
2x/year All None
EPA 8270
SVOCs Fall of odd years (2017) All None
Benzo(a)anthracene, Bis(2-
ethylhexyl)phthalate, Chrysene Dibenz(a,h)anthracene &
Indeno(1,2,3-cd)pyrene
(SVOCs recently detected)
2x/year MW-1R, MW-2R, MW-4R , MW-3R & MW-15 SW-2
SM 2320B Alkalinity 2x/year All All
SM 2540C Total Dissolved Solids 2x/year All All
SM 4500 Chloride, Cyanide, Sulfide 2x/year All All
Field Temperature, Specific
conductance, Dissolved Oxygen, Redox, Turbidity, pH 2x/year All All
Field Total well depth and static water level 2x/year All NA

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Data Collection
3.0 Data Collection
The monitoring program consists of collection and analysis of groundwater samples from 14
wells. The sampling event occurred over three days (May 30 to June 1, 2017). Pace Analytical
Laboratories, Inc. (Pace) of Huntersville, North Carolina (NC Cert. # 5342), on behalf of HDR,
sampled the groundwater monitoring wells for this report. Synoptic groundwater elevations were
measured at all wells on May 30, 2017.
The depth from the top of the PVC casing to groundwater is measured to the nearest 0.01 foot
prior to purging each well. This depth to water, when subtracted from the reference datum,
provides a groundwater surface elevation. Table 3 provides the recent water level readings as
well as depicted in Figure 1. Figure 2 depicts the relative groundwater elevations in the on-site
monitoring wells over time.
Table 3 - Recent Water Level Readings

Figure 2 - Historic Groundwater Elevations

720
730
740
750
760
770
780
790
800
810
Groundwater Surface Elevation (feet above msl)Sample Date
MW-1R
MW-2R
MW-5R
MW-6R
MW-7
MW-15
MW-4R
MW-3R
MW-8
MW-13
MW-9
MW-12
MW-14
MW-11
MW-10
MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8
5/30/2017 801.28 777.39 758.13 759.75 773.56 766.84 747.33
MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
5/30/2017 737.46 726.66 728.65 734.49 742.53 732.02 763.98
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Winston-Salem City/County Utilities | Assessment Monitoring Report
Data Collection
A variable speed micro-purge pump (or bailer in the case of MW-15) was used to purge
groundwater from each well until stabilization of measured field parameters (pH, conductivity,
redox, temperature, turbidity, and dissolved oxygen) occurred. Following completion of purging
activities, the wells were sampled using the same pump and field parameters (pH, specific
conductance, redox, turbidity, dissolved oxygen, and temperature) were recorded on field
sampling logs. Copies of these logs are provided in Appendix B.
Table 3 illustrates the hydraulic gradients calculated between representative well pairs and the
corresponding flow velocities. The flow velocities have been calculated based on the values for
hydraulic conductivity (0.466 ft./day) and effective porosity (25%), as presented in Table 2-9 of
the December 2003 OSR Design Hydrogeologic Investigation Report for the landfill.
The minimum and maximum values are based on the historic data collected from the site
beginning in May 2003. HDR estimates a travel time of about four years between MW-2R and
MW-15, based on the estimated flow rate of 47 ft./yr and a distance of 195 feet.
Table 4 - Hydraulic Gradient & Flow Velocity
Hydraulic Gradient (ft/ft)
Flow
Velocity (ft/yr)
Based on Historic Record
Minimum Maximum Nov 2014 May 2015 Nov 2015 May 2016 Nov 2016 May 2017
MW-1R to
MW-4R
0.024
17
0.028
19
0.028
19
0.027
18
0.027
19
0.026
18
0.028
19
0.027
18
MW-1R to
MW-2R
0.032
22
0.040
27
0.040
27
0.038
26
0.037
25
0.037
25
0.040
27
0.038
26
MW-2R to
MW-13
0.060
41
0.064
44
0.062
42
0.062
42
0.062
42
0.064
43
0.062
42
0.062
42
MW-13 to
MW-10
0.013
9
0.014
10
0.014
10
0.014
9
0.014
10
0.013
9
0.014
9
0.014
9
MW-2R to
MW-15
0.068
46
0.072
49
0.068
46
0.069
47
0.070
48
0.072
49
0.068
47
0.069
47

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Results
4.0 Results
4.1. Detected Groundwater Constituents
Detections of benzene and PCE above the groundwater standards triggered assessment
monitoring for well MW-2R. The trends of selected containments detected in MW-2R above the
SWSL are shown on Figure 3.

Figure 3 - Selected Groundwater Detections in MW-2R
A summary of the constituents detected during this period, along with the NCDEQ solid waste
section limits (SWSL) and applicable North Carolina state maximum concentration levels, are
provided in Table 6. There were twenty-eight detections above the 2L standard; these
detections comprised five parameters in thirteen locations during this event. Methylene chloride
was only detected above the SWSL MW-7 during this event. Barium, cobalt, zinc,
trichloroethene, and trichloroflouromethane were also detected between the two standards.
Finally, the QAQC Equipment Blank sample reported Lead in excess of the MCL.

Appendix A contains historical summaries of detections by well and by parameter. The complete
laboratory analyses are provided in Appendix B. The field data sheets are provided in Appendix
C. A Microsoft Excel file containing the analysis data in NCDEQ electronic data deliverable
format is include as part of Appendix D.
0.1
1
10
100
1000
10000
100000
1000000
1-Jan-09 1-Jan-10 1-Jan-11 1-Jan-12 1-Jan-13 1-Jan-14 1-Jan-15 1-Jan-16 1-Jan-17 1-Jan-18Detected Concentration (ug/L)Date Sample Collected
MW-2R Groundwater Detections
OSR Construction & Demolition Landfill Permit 34-12
Total Dissolved Solids
Sulfate
Chloride
Manganese
Iron
Barium
Selenium
Chromium
Methylene Chloride
Lead
Benzene
bis(2-Ethylhexyl)phthalate
Heptachlor
delta-BHC
Chloromethane
alpha-BHC
4,4'-DDT
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Winston-Salem City/County Utilities | Assessment Monitoring Report
Results

The constituents detected above 2L groundwater standards for this event, all from Appendix I
are as follows.
Appendix I constituents:
• Sulfate in MW-10
• Iron in MW-2R, MW-3R, MW-4R, MW-10, MW-11, MW-12, MW-15, and all four surface
water samples.
• Manganese in MW-2R, MW-3R, MW-4R, MW-7, MW-10, MW-11, MW-12, MW-15 and
all four surface water samples.
• Benzene in MW-2R.
• Total dissolved solids in MW-2R, MW-4, and MW-10.
4.2. Landfill Gas
Landfill gas is measured at MW-2R and wells in the vicinity of MM-1 during each groundwater
event. These results do not indicate the presence of methane gas in these wells. The results do
indicate the presence of carbon dioxide above ambient levels in MM-1. The City is responsible
for quarterly sampling of all methane monitoring wells and the related reporting, which is not
included in this document.
Table 5 - Methane Gas Readings
Date Time ID # CH4 (%) CO2 (%) O2 (%) Balance (%)
28-Nov-16 09:47 MM-1 0.0% 4.2% 20.1% 75.0%
28-Nov-16 09:30 MW-13 0.0% 0.6% 20.4% 79.3%
28-Nov-16 09:43 MW-15 0.0% 0.8% 20.1% 79.1%
28-Nov-16 10:01 MW-1R 0.0% 0.3% 20.6% 79.1%
28-Nov-16 09:51 MW-2R 0.0% 1.2% 20.2% 79.1%
30-May-17 10:29 MM-1 0.0% 4.3% 16.4% 79.3%
30-May-17 10:47 MW-13 0.0% 0.3% 21.0% 78.7%
30-May-17 10:38 MW-15 0.0% 0.4% 20.9% 78.7%
30-May-17 10:20 MW-1R 0.0% 0.2% 21.3% 78.5%
30-May-17 10:32 MW-2R 0.0% 0.5% 21.1% 78.3%
Highlighted cells are outside of normal atmospheric ranges

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Summary & Recommendations
5.0 Summary & Recommendations
The level of detections from this event are generally consistent with previous events. The
pesticides, heptachlor and heptachlor epoxide that were last detected during the November
2016 sampling event were not detected in this current May 2017 event. These Appendix II
pesticides will be monitored in the forthcoming Fall 2017 sampling event and further
recommendations made if deemed appropriate or necessary.
Table 6 and Table 7 depict a summary of exceedances and field parameters for the May 2017
Sampling Event.
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Winston-Salem City/County Utilities | Assessment Monitoring Report
Summary & Recommendations
Table 6 - Event Lab Summary – May 2017
SWSL 2L Units Row Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4 Equipment Blank Trip Blank
EPA 300.0 µg/L
250000 250000 µg/L Sulfate 110000 125000 7740 6720 2700 960 333000 14100 86100 5670 663 58300 2530 10900 15200 18200 EPA 6010
µg/L
10 10 µg/L Arsenic 5.5
100 700 µg/L Barium 272 323 309 343 57.1 163 42.9 207 221 102 113 120 221 22.7 86.8 77.5 173 121
1 4000 µg/L Beryllium 0.6
10 10 µg/L Chromium 4.6 4.2
10 1000 µg/L Cobalt 20.6 11.5 59.9 21.8 3
10 1000 µg/L Copper 2.6 761
300 300 µg/L Iron 54.8 3870 89300 302 68.4 25.2 2400 26700 714 58 134 1740 5040 1790 8240 1480 27.1
10 15 µg/L Lead 3.4 4.1 18.2
50 50 µg/L Manganese 12.5 9200 6460 801 51.9 3 4.6 8390 1720 134 9.7 18.1 359 804 304 4750 2900
50 100 µg/L Nickel 17 5.8 6.9 4.4 2.7 3.6
NE NE µg/L Sodium 15800 72400 2240 42100 13900 17800 9240 15400 123000 11700 16200 10000 16900 21600 23000 11600 24600 23400
5.5 200 µg/L Thallium 0.043 0.021 0.048 0.049
100 2000000 µg/L Tin 4
25 300 µg/L Vanadium 4.4 2.7 5
10 1000 µg/L Zinc 5.5 8.6 8.9 5.1 5.4 5.7 16.2 10.1 455
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.48 1.3
1 0.4 µg/L 1,2-Dichloroethane 0.24
100 NE µg/L 4-Methyl-2-pentanone (MIBK) 2.8
100 6000 µg/L Acetone 10.3 21.4 11 18.4 15.7 15.8 22.5 21.1 12.1 17.3 14.7 13.2 11.2 16.2 16 18.3 18.7
1 1 µg/L Benzene 2.1 0.43
100 700 µg/L Carbon disulfide 2
5 70 µg/L Chloroform 0.4
1 3 µg/L Chloromethane 0.23
5 70 µg/L cis-1,2-Dichloroethene 0.38 0.51 1.1 0.2
5 1000 µg/L Dichlorodifluoromethane 1.5 3.6
1 600 µg/L Ethylbenzene 0.53
5 500 µg/L m&p-Xylene 1.2 1.2
1 5 µg/L Methylene Chloride 3.1
NE NE µg/L o-Xylene 0.46 1
1 0.7 µg/L Tetrachloroethene 0.61
NS NS µg/L Tetrahydrofuran 36.3 9.3 32 182 4.5 11.4 12 3.5
1 600 µg/L Toluene 0.27
1 3 µg/L Trichloroethene 1
1 2000 µg/L Trichlorofluoromethane 0.91 1.4 1 0.75 2.1
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 68600 587000 114000 315000 32300 85000 20800 25400 446000 135000 64500 42400 55300 98100 33200 46200 251000 187000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 8860 50400 2520 35800 15100 5290 3060 4610 13500 19700 4310 3260 104000 49200 13800 18400 27400 SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 4.4 4.4 9.9 4.3 4.4 4.6
Note - To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks.
12
Winston-Salem City/County Utilities | Assessment Monitoring Report
Summary & Recommendations
Table 7 - Event Field Summary – May 2017
Field MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
mg/L
Oxygen, Dissolved 1.3 1.9 0.5 0.1 5.4 0.4 5.4 6.51 0.6 0.3 0.3 4.03 3.28 3.06 4.7 6.3 4.3 6
mV
REDOX 179.6 -62.6 -60 154.4 182.6 210.2 195 178.8 -58.5 -10.4 107.5 138.8 147 121 -7.1 -15.2 -49.6 -38.5
NTU
Turbidity 3.5 3.4 5.3 9.93 3.1 4.2 1.16 0.4 34.3 8.58 9.26 1.75 5.42 23.24 15.12 14.72 7.94 7.13
Std. Units
Field pH 5.5 6.1 6.3 6 5.9 5.5 5.6 5.5 6.1 5.9 5.9 5.6 5.5 6.3 6.5 6.8 6.6 7.3
feet
Static Water Level 35.05 7.88 18.43 8.1 10.6 36.56 15.16 52.82 11.39 3.92 4.64 8.7 51.86 38.85
Total Well Depth 60 21 27 20 50 48 27 60 21 20 15.7 20 60 50.85
umhos/cm
Field Specific Conductance 209.7 1246 392.9 756 175.5 220.7 68.1 159 1714 354.9 367.4 116.5 173.7 690 250.9 172 549 461
deg C
Field Temperature 20.3 24.3 20.4 14.8 21.2 19.7 17 19.8 23 16.6 17.4 16.9 18.4 17.6 21 21 21.2 20.4

13
Winston-Salem City/County Utilities | Assessment Monitoring Report
Appendix A – Summary of Groundwater Monitoring Results
A
Appendix A – Summary of
Groundwater Monitoring
Results
A-1 Appendix II Detections (8 pages)
A-2 Detections by Well Location (19 pages)
A-3 Detections by Date (43 pages)

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Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11Herbicides2 50 µg/L 2,4,5-TP (Silvex)2 50 µg/L MW-2R 0.14 0.23270µg/L2,4-D2 70 µg/L MW-2R 0.43 1.1Pesticides0.1 0.1 µg/L 4,4'-DDD0.1 0.1 µg/L MW-70.130.1 0.1 µg/L MW-150.0620.1 0.1 µg/L SW-30.0790.1 0.1 µg/L SW-40.110.060.1 0.1 µg/L 4,4'-DDT0.1 0.1 µg/L MW-2R0.540.1 0.1 µg/L MW-4R0.140.1 0.1 µg/L MW-110.050.1 0.1 µg/L SW-30.090.1 0.1 µg/L SW-40.050.05 2 µg/L Aldrin0.05 2 µg/L MW-2R0.120.05 0.006 µg/L alpha-BHC0.05 0.006 µg/L MW-2R0.120.05 0.019 µg/L beta-BHC0.05 0.019 µg/L MW-70.10.05 0.019 µg/L delta-BHC0.05 0.019 µg/L MW-2R0.180.05 0.019 µg/L MW-4R0.070.002 0.002 µg/L Dieldrin0.002 0.002 µg/L MW-70.11 0.080.1 40 µg/L Endosulfan I0.1 40 µg/L MW-7 0.150.1 40 µg/L MW-10 0.17MCLc:\pwworking\tpa\d0269489\W-S GW Revised1 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL0.1 42 µg/L Endosulfan II0.1 42 µg/L MW-4R0.120.1 42 µg/L SW-30.071 0.090.1 42 µg/L SW-40.070.1 2 µg/L Endrin0.1 2 µg/L MW-2R0.270.1 2 µg/L SW-10.080.1 2 µg/L Endrin aldehyde0.1 2 µg/L MW-2R0.23 0.280.1 2 µg/L SW-40.060.05 0.008 µg/L Heptachlor0.05 0.008 µg/L MW-2R0.480.05 0.008 µg/L MW-100.21 0.120.075 0.004 µg/L Heptachlor epoxide0.075 0.004 µg/L MW-70.12 0.070.075 0.004 µg/L MW-100.17 0.0931 40 µg/L Methoxychlor140µg/LMW-2R0.83SemiVOCs10 NE µg/L 2,4-Dinitrotoluene10 NE µg/L MW-2R 5.910 NE µg/L 2,6-Dinitrotoluene10 NE µg/L MW-2R 8.110 40 µg/L 3&4-Methylphenol(m&p Cresol)10 40 µg/L SW-33.620 NE µg/L 3,3'-Dichlorobenzidine20 NE µg/L SW-23.610 NE µg/L 3-Methylcholanthrene10 NE µg/L SW-22.910 0.05 µg/L Benzo(a)anthracene10 0.05 µg/L MW-1R1.410 0.05 µg/L SW-21.1c:\pwworking\tpa\d0269489\W-S GW Revised2 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL10 0.005 µg/L Benzo(a)pyrene10 0.005 µg/L MW-131.110 0.005 µg/L SW-22.510 0.05 µg/L Benzo(b)fluoranthene10 0.05 µg/L MW-13110 0.05 µg/L SW-22.810 200 µg/L Benzo(g,h,i)perylene10 200 µg/L MW-3R 110 200 µg/L MW-111.310 200 µg/L MW-121.210 200 µg/L MW-131.510 200 µg/L SW-21.810 0.5 µg/L Benzo(k)fluoranthene10 0.5 µg/L SW-22.515 3 µg/L bis(2-Ethylhexyl)phthalate15 3 µg/L MW-1R2.415 3 µg/L MW-2R1.115 3 µg/L MW-3R5.515 3 µg/L MW-5R115 3 µg/L MW-91315 3 µg/L MW-149.815 3 µg/L SW-21.110 5 µg/L Chrysene10 5 µg/L MW-1R1.510 5 µg/L SW-21.110 0.005 µg/L Dibenz(a,h)anthracene10 0.005 µg/L MW-3R110 0.005 µg/L MW-131.210 0.005 µg/L SW-22.110 100 µg/L Di-n-octylphthalate10 100 µg/L MW-8 5.610 100 µg/L MW-12 5.6c:\pwworking\tpa\d0269489\W-S GW Revised3 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL10 0.05 µg/L Indeno(1,2,3-cd)pyrene10 0.05 µg/L MW-3R1.110 0.05 µg/L MW-121.210 0.05 µg/L MW-131.510 0.05 µg/L SW-22.2VOCs1 200 µg/L 1,1,1-Trichloroethane1 200 µg/L MW-70.825 6 µg/L 1,1-Dichloroethane5 6 µg/L MW-2R 0.48 0.53 0.49 1.1 0.83 1.3 1.2 1.2 1.1 1.2 1.15 6 µg/L MW-7 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.84 1.2 1.2 1.9 3.85 350 µg/L 1,1-Dichloroethene5 350 µg/L MW-2R36.6 38.75 350 µg/L MW-153.15 350 µg/L SW-40.581 0.4 µg/L 1,2-Dichloroethane1 0.4 µg/L MW-2R 0.241 6 µg/L 1,4-Dichlorobenzene1 6 µg/L MW-2R 0.39 0.38 0.450 NE µg/L 2-Hexanone50 NE µg/L MW-2R0.4850 NE µg/L MW-10 0.69 0.9650 NE µg/L SW-2 1.850 NE µg/L SW-4 3.1100 NE µg/L 4-Methyl-2-pentanone (MIBK)100 NE µg/L MW-10 2.8 2.5 2.6 5.6 2.2100 6000 µg/L Acetone100 6000 µg/L Equipment Blank 18.35.5100 6000 µg/L GP-B-1 (12-16)3.6100 6000 µg/L MW-2R 10.320.3 3.7100 6000 µg/L MW-3R 21.4100 6000 µg/L MW-4R 11100 6000 µg/L MW-5R 18.4100 6000 µg/L MW-7 15.7100 6000 µg/L MW-8 15.83.8100 6000 µg/L MW-10 22.5 14.1 11.8100 6000 µg/L MW-11 21.1100 6000 µg/L MW-12 12.1c:\pwworking\tpa\d0269489\W-S GW Revised4 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL100 6000 µg/L MW-1317.3100 6000 µg/L MW-1414.7100 6000 µg/L MW-1513.2100 6000 µg/L SW-111.22.2100 6000 µg/L SW-24100 6000 µg/L SW-316.2100 6000 µg/L SW-41611µg/LBenzene11µg/LMW-2R2.12.21.7 1.5 1.7 2.5 1.8 1.9 1.4 1.3 1.52 1.6 1.31 1 µg/L MW-4R0.380.42 0.28 0.271 1 µg/L MW-70.43 0.420.260.291 1 µg/L MW-100.830.46 0.441 1 µg/L SW-30.420.54 0.32 0.880.34 0.25100 700 µg/L Carbon disulfide100 700 µg/L MW-1025.210 3000 µg/L Chloroethane10 3000 µg/L MW-2R2.110 3000 µg/L MW-71.35 70 µg/L Chloroform5 70 µg/L GP-B-1 (12-16)0.98570µg/LMW-2R0.160.26 0.365 70 µg/L MW-150.4 0.440.7 0.44 0.26 0.49 0.77 0.63 0.49 1.4570µg/LSW-40.971 3 µg/L Chloromethane13µg/LMW-2R0.2513µg/LMW-4R0.151 3 µg/L MW-70.1313µg/LMW-11 0.23c:\pwworking\tpa\d0269489\W-S GW Revised5 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL13µg/LMW-120.2113µg/LMW-140.245 70 µg/L cis-1,2-Dichloroethene5 70 µg/L MW-1R 0.38 0.25 70 µg/L MW-2R 0.51 0.47 0.26 0.5 0.38 0.41 0.26 0.25 0.33 0.46 0.265 70 µg/L MW-7 1.1 1.1 0.77 0.8 0.73 0.73 0.37 0.54 0.72 0.62 0.5 0.67 0.715 70 µg/L MW-10 0.2 0.33 0.35570µg/LSW-3 0.265 1000 µg/L Dichlorodifluoromethane5 1000 µg/L MW-2R 0.265 1000 µg/L MW-7 0.62 15 1000 µg/L MW-9 1.5 0.88 0.76 0.28 0.285 1000 µg/L MW-12 0.235 1000 µg/L MW-14 3.6 2.3 3.6 2.11 600 µg/L Ethylbenzene1 600 µg/L MW-1R 0.381 600 µg/L MW-10 0.53 0.55 0.4 1 0.735 500 µg/L m&p-Xylene5 500 µg/L MW-2R0.66 0.745 500 µg/L MW-7 1.2 2.2 1.8 0.84 1.5 1.1 0.96 1.45 500 µg/L MW-10 1.2 2.1 0.68 1.2 1.11 5 µg/L Methylene Chloride1 5 µg/L Equipment Blank61.1 1.8 3.215µg/LMW-1R 2.31 5 µg/L MW-2R 4.4 1.3 2.3 3.7 3.7 3 4.2 4.5 3.2 3.5 4.115µg/LMW-3R 3.42.315µg/LMW-4R 2.915µg/LMW-5R 3.21 5 µg/L MW-7 3.1 4.2 3.79.53.9 2.1 2.915µg/LMW-8 1.115µg/LMW-10 2.81.2c:\pwworking\tpa\d0269489\W-S GW Revised6 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL15µg/LMW-111.415µg/LMW-122215µg/LMW-141.615µg/LMW-152.415µg/LSW-1215µg/LSW-23.115µg/LSW-3115µg/LSW-41.210 6 µg/L Naphthalene10 6 µg/L MW-2R0.86 1.3 1.6 1.9NE NE µg/L o-XyleneNE NE µg/L MW-2R0.33 0.31 0.54 0.54 0.63 11.2 0.84NE NE µg/L MW-70.46 0.630.47 0.27 0.4 0.360.270.39NE NE µg/L MW-1012.10.43 0.85 0.651 0.7 µg/L Tetrachloroethene10.7µg/LMW-2R1.81.3 0.95 1.2 2 1.8 2.2 1.5 1.8 1.71.8 1.6 1.41 0.7 µg/L MW-70.481 0.7 µg/L MW-140.61NS NS µg/L TetrahydrofuranNS NS µg/L Equipment Blank3.2NS NS µg/L MW-2R 36.339.149.6 35.8 34.6 79.2 72.6 99.6 111 93.2 152197 274 226NS NS µg/L MW-4R 9.313.63.5 7 5.8 15.9 11.8 11.7 8.5 13.5 8.8NS NS µg/L MW-732 21.713.5 17.7 14.1 8.8 5.2 13.7 24.2 26 18.9NS NS µg/L MW-10 1822376.1 120 145 106 18.6 5NS NS µg/L MW-11 4.54.412.1NS NS µg/L MW-1211.4 26.812.4NS NS µg/L MW-1318.6NS NS µg/L MW-1512 16.827.3 19.8 16.9 15.5 21.4 14.7 7.4 6.3NS NS µg/L SW-218.4NS NS µg/L SW-36.33.310.2 9.7 18.9 5.1 4.8 4.5NS NS µg/L SW-43.5 3.64.14.41 600 µg/L Toluene1 600 µg/L MW-2R0.271 600 µg/L MW-10 0.270.631 600 µg/L SW-20.521 3 µg/L Trichloroethene1 3 µg/L MW-2R11.20.71 0.66 0.79 0.85 0.71 0.89 0.68 0.77 0.820.88 0.651 2000 µg/L Trichlorofluoromethane1 2000 µg/L GP-A-7 (20.5-24.5)0.25c:\pwworking\tpa\d0269489\W-S GW Revised7 of 8
Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple Items)Selected groundwater detections of concern within the last 6 yearsQualifier (Multiple Items) Highlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsJun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11May-11MCL1 2000 µg/L MW-2R0.71 1 1.5 2.4 3.7 12 12.1 16.9 20.920.1 31.61 2000 µg/L MW-70.91 1.50.92 1.4 0.79 1.2 0.62 0.47 0.25 0.290.34 0.481 2000 µg/L MW-91.4 11.3 1.1 0.98 0.96 0.47 0.69 0.36 0.490.42 0.261 2000 µg/L MW-100.2 0.33 0.38 0.490.68 0.521 2000 µg/L MW-121 2.81.4 0.82 0.22 0.321 2000 #### MW-140.75 0.581.1 0.54 0.59 0.57 0.341 2000 #### MW-152.1 4.45.1 4.8 4.4 3.9 5.3 7.6 4.3 8.1 7.31 2000 #### SW-40.27 0.251.41 0.03 µg/L Vinyl chloride1 0.03 #### MW-2R10.72 0.75 0.7 1.2 0.955 500 µg/L Xylenes (Total)5 500 #### MW-2R0.98 1.65 500 #### MW-71.2 0.79c:\pwworking\tpa\d0269489\W-S GW Revised8 of 8
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Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12µg/L
MW-1R
NE NE µg/L Alkalinity, Total as CaCO3 68600 64300 54900 48100 39600 37600 30000 28100 29800 26300
10 10 µg/L Arsenic
100 700 µg/L Barium 272 241 228 207 164 142 124 106 109 91.7
10 0.05 µg/L Benzo(a)anthracene 1.4
15 3 µg/L bis(2-Ethylhexyl)phthalate 2.4
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 8860 9630 9000 8510 7640 7090 5600 5880 5910 5320
10 10 µg/L Chromium
10 5 µg/L Chrysene 1.5
5 70 µg/L cis-1,2-Dichloroethene 0.38 0.2
10 70 µg/L Cyanide 4.4
1 600 µg/L Ethylbenzene 0.38
300 300 µg/L Iron 54.8 96.2 78.8 82.8 85.8 52.9
10 15 µg/L Lead
50.0 50.0 µg/L Manganese 12.5 7.3 7.2 2.8 2.9
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 2.3
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 15800 14600 13300 13200 11600 10600 10800 9940 9080 9180
250000 250000 µg/L Sulfate 1380 1080 1070 1700 1720
1 600 µg/L Toluene
NE 500000 µg/L Total Dissolved Solids 165000 154000 138000 78000 133000 120000 91000 103000 84000 95000
10 1000 µg/L Zinc 5.5 5.7 5.6
MW-2R
5 6 µg/L 1,1-Dichloroethane 0.48 0.53 0.49 1.1 0.83 1.3 1.2 1.2
5 350 µg/L 1,1-Dichloroethene
1 0.4 µg/L 1,2-Dichloroethane 0.24
1 6 µg/L 1,4-Dichlorobenzene 0.39 0.38 0.4
2 50 µg/L 2,4,5-TP (Silvex)0.14 0.23
270µg/L2,4-D 0.43 1.1
10 NE µg/L 2,4-Dinitrotoluene 5.9
10 NE µg/L 2,6-Dinitrotoluene 8.1
100 4000 µg/L 2-Butanone (MEK)
50 NE µg/L 2-Hexanone 0.48
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 10.3 20.3
0.05 2 µg/L Aldrin
NE NE µg/L Alkalinity, Total as CaCO3 587000 571000 482000 440000 358000 453000 344000 349000 363000 277000
0.05 0.006 µg/L alpha-BHC
6 1000 µg/L Antimony 4.7 5.4
10 10 µg/L Arsenic
100 700 µg/L Barium 323 272 324 279 287 339 324 311 324 335
1 1 µg/L Benzene 2.1 2.2 1.7 1.5 1.7 2.5 1.8 1.9 1.4 1.3
15 3 µg/L bis(2-Ethylhexyl)phthalate 1.1
1 2 µg/L Cadmium
NE 250000 µg/L Chloride 50400 47600 47700 48700 44200 49800 50500 56700 50000 64000
10 3000 µg/L Chloroethane 2.1
5 70 µg/L Chloroform 0.16
1 3 µg/L Chloromethane 0.25
10 10 µg/L Chromium 2.8 2.6 3.4
5 70 µg/L cis-1,2-Dichloroethene 0.51 0.47 0.26 0.5 0.38 0.41 0.26 0.25
10 1000 µg/L Cobalt 20.6 16.5 18 17.4 20.3 25 22.8 19.2 18.2 15.2
10 1000 µg/L Copper 6.3 9.6
10 70 µg/L Cyanide 5.1 7.5 4.2
0.05 0.019 µg/L delta-BHC
5 1000 µg/L Dichlorodifluoromethane 0.26
0.1 2 µg/L Endrin 0.27
0.1 2 µg/L Endrin aldehyde 0.23
0.05 0.008 µg/L Heptachlor
300 300 µg/L Iron 3870 1780 4360 3080 9560 2580 1650 766 877 1730
10 15 µg/L Lead 3.3
5 500 µg/L m&p-Xylene
50 50 µg/L Manganese 9200 8570 10900 9010 11900 9880 7950 8710 7880 8400
0.2 1 µg/L Mercury
NS NS µg/L Methane
1 40 µg/L Methoxychlor
1 5 µg/L Methylene Chloride 4.4 1.3 2.3 3.7 3.7 3 4.2 4.5
10 6 µg/L Naphthalene 0.86 1.3 1.6
50 100 µg/L Nickel 17 18.5 17.9 18 17 25.9 20.6 27.1 20.7 21.8
NS NS µg/L Nitrogen, Ammonia
NE NE µg/L o-Xylene 0.33 0.31 0.54 0.54 0.63
10 20 µg/L Selenium 16.5
10 20 µg/L Silver
MCL
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
µg/L
MW-1R
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
bis(2-Ethylhexyl)phthalate
Carbon disulfide
Chloride
Chromium
Chrysene
cis-1,2-Dichloroethene
Cyanide
Ethylbenzene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Toluene
Total Dissolved Solids
Zinc
MW-2R
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
1,4-Dichlorobenzene
2,4,5-TP (Silvex)
2,4-D
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Butanone (MEK)
2-Hexanone
4,4'-DDT
Acetone
Aldrin
Alkalinity, Total as CaCO3
alpha-BHC
Antimony
Arsenic
Barium
Benzene
bis(2-Ethylhexyl)phthalate
Cadmium
Chloride
Chloroethane
Chloroform
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
delta-BHC
Dichlorodifluoromethane
Endrin
Endrin aldehyde
Heptachlor
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methane
Methoxychlor
Methylene Chloride
Naphthalene
Nickel
Nitrogen, Ammonia
o-Xylene
Selenium
Silver
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-0427100 27500
93.8 82.6 84.7 85.4 85.3 92.8 74 85 90 105 81 94 82 78 48 95 96
5350
1.4 0.96 1.4 2 0.9 0.6 0.5 2 3.5
5.5
0.51 0.29 0.48 0.6 0.4
9440 7670
93000 95000
1.1 1.2 1.1
36.6 38.7
0.54
3.7
0.12
196000 219000 165000
0.12
366 351 273 223 103 80.7 89 99 102 107 79 90 52 62 43 52 55
1.5 2 1.6 1.3
61500 62400 39900
0.26 0.36 3.4
5.4 0.49 1.2 1.6 0.5 0.8
0.33 0.46 0.26
14.8 11.8
0.18
0.28
0.48
3190 2980
0.66 0.74
8280 7920
0.34
1280
0.83
3.2 3.5 4.1 4.2
1.9
22.3 20.9
0.12
1 1.2 0.84
5.2 5 2.5 0.85 0.67 0.68 0.6 1.2 0.9
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
µg/L
MW-1R
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
bis(2-Ethylhexyl)phthalate
Carbon disulfide
Chloride
Chromium
Chrysene
cis-1,2-Dichloroethene
Cyanide
Ethylbenzene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Toluene
Total Dissolved Solids
Zinc
MW-2R
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
1,4-Dichlorobenzene
2,4,5-TP (Silvex)
2,4-D
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Butanone (MEK)
2-Hexanone
4,4'-DDT
Acetone
Aldrin
Alkalinity, Total as CaCO3
alpha-BHC
Antimony
Arsenic
Barium
Benzene
bis(2-Ethylhexyl)phthalate
Cadmium
Chloride
Chloroethane
Chloroform
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
delta-BHC
Dichlorodifluoromethane
Endrin
Endrin aldehyde
Heptachlor
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methane
Methoxychlor
Methylene Chloride
Naphthalene
Nickel
Nitrogen, Ammonia
o-Xylene
Selenium
Silver
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Nov-03May-03Dec-02Apr-02Nov-01Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-965.8
460 120 100 130 280 87 150 110 130 150 160 100 290 100 180 224
28 23
4.3 2.3 5 22 6.6 6.6 5.2 7.8 12 49 11 36
22 10 12 6
0.2 1.8
13
21
86
11
60 56 140 100 160 280 61 180 120 150 1100 190 340 200 160 350
1.9 3
2.2 2.1 16 16 3.9 3 14 7.8 210 34 43 4912
7 8.9 6.5 6.9 68 19 31 14 8 26
0.4
13
6
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
NE NE µg/L Sodium 72400 70200 61500 61400 51400 58300 59700 46200 45700 43400
250000 250000 µg/L Sulfate 110000 121000 115000 115000 98400 117000 136000 128000 115000 79500
1 0.7 µg/L Tetrachloroethene 1.8 1.3 0.95 1.2 2 1.8 2.2 1.5 1.8
NS NS µg/L Tetrahydrofuran 36.3 39.1 49.6 35.8 34.6 79.2 72.6 99.6 111 93.2
5.5 200 µg/L Thallium 5.1
1 600 µg/L Toluene 0.27
NE 500000 µg/L Total Dissolved Solids 796000 831000 769000 806000 632000 769000 549000 654000 589000 564000
1 3µg/L Trichloroethene 1 1.2 0.710.660.790.850.710.890.680.77
1 2000 µg/L Trichlorofluoromethane 0.71 1 1.5 2.4 3.7 12 12.1 16.9
25 300 µg/L Vanadium 11.9 11.4 5.5
1 0.03 µg/L Vinyl chloride 1 0.72 0.75 0.7 1.2 0.95
5 500 µg/L Xylenes (Total)0.98
10 1000 µg/L Zinc 5.8 8.7 16.8 12.2 21.1 24.5
MW-3R
100 6000 µg/L Acetone 21.4
NE NE µg/L Alkalinity, Total as CaCO3 114000 133000 87800 102000 107000 177000 155000 155000 175000 142000
10 10 µg/L Arsenic 5.5 3.9 3.3 8.9
100 700 µg/L Barium 309 297 278 271 214 221 205 201 216 173
10 200 µg/L Benzo(g,h,i)perylene 1
15 3 µg/L bis(2-Ethylhexyl)phthalate
1 2 µg/L Cadmium
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 2520 2050 2470 2990 2990 2940 3260 3620 3860 3920
10 10 µg/L Chromium
10 1000 µg/L Cobalt 11.5 9.8 10.2 9.1 10.1 13.3 53.5 64.1
10 1000 µg/L Copper 6.2
10 70 µg/L Cyanide 4.4 4.7 10.4 7.1 8.1 9.1
10 0.005 µg/L Dibenz(a,h)anthracene 1
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.1
300 300 µg/L Iron 89300 86400 77200 68200 56000 49700 38200 31300 34100 25300
10 15 µg/L Lead 3.4 3.5 3.8 2.7 2.7
50 50 µg/L Manganese 6460 5920 6800 7100 7980 9380 9260 9990 9630 11600
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 3.4 2.3
10 20 µg/L Selenium 5 5.5
10 20 µg/L Silver
NE NE µg/L Sodium 2240 2450 2310 2590 2770
250000 250000 µg/L Sulfate 1530 1800 2200 3000 3740 4230 3400 5070 5420
100 2000000 µg/L Tin 5.8
NE 500000 µg/L Total Dissolved Solids 133000 168000 188000 137000 182000 191000 187000 193000 175000 172000
25 300 µg/L Vanadium 9.9 8.8 2.8
10 1000 µg/L Zinc 8.7 10.5
MW-4R
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 11
NE NE µg/L Alkalinity, Total as CaCO3 315000 454000 99000 144000 117000 286000 222000 224000 203000 174000
10 10 µg/L Arsenic
100 700 µg/L Barium 343 255 210 184 306 305 264 296 375 400
1 1 µg/L Benzene 0.38 0.42 0.28 0.27
1 2 µg/L Cadmium
NE 250000 µg/L Chloride 35800 58400 13800 16900 22200 50500 29700 36500 33700 34500
1 3 µg/L Chloromethane
10 10 µg/L Chromium 3.2
10 1000 µg/L Cobalt 59.9 100 10.5 28.3 15.2 82 46.6 49.4 35.3 35.5
10 1000 µg/L Copper 2.8
10 70 µg/L Cyanide 4.2 4.3 5.9
0.05 0.019 µg/L delta-BHC
0.1 42 µg/L Endosulfan II 0.12
300 300 µg/L Iron 302 214 1550 312 292 126 89.5 158 344
10 15 µg/L Lead
50 50 µg/L Manganese 801 1320 515 407 315 1040 641 688 496 541
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 2.9
50 100 µg/L Nickel 5.8 8 3.2 3.7 2.8 7.2 5.3
10 20 µg/L Selenium 11.5
10 20 µg/L Silver
NE NE µg/L Sodium 42100 71000 14500 23800 23000 55400 39700 42600 42600 43600
250000 250000 µg/L Sulfate 125000 193000 48700 70300 72700 143000 85200 113000 97600 73600
NS NS µg/L Tetrahydrofuran 9.3 13.6 3.5 7 5.8 15.9 11.8 11.7 8.5 13.5
NE 500000 µg/L Total Dissolved Solids 552000 824000 241000 161000 304000 692000 445000 496000 413000 435000
25 300 µg/L Vanadium 4.2 2.7
10 1000 µg/L Zinc 8.6 8.4 17.8 5.9 7.5 7.2 13.6
MW-5R
100 6000 µg/L Acetone 18.4
NE NE µg/L Alkalinity, Total as CaCO3 32300 32700 30800 32300 28600 24000 31900 31700 34800 31200
10 10 µg/L Arsenic
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Thallium
Toluene
Total Dissolved Solids
Trichloroethene
Trichlorofluoromethane
Vanadium
Vinyl chloride
Xylenes (Total)
Zinc
MW-3R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Tin
Total Dissolved Solids
Vanadium
Zinc
MW-4R
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Cadmium
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
delta-BHC
Endosulfan II
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Vanadium
Zinc
MW-5R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-0438400 31800 27200
95000 96300
1.7 1.8 1.6 1.4
152 197 274 226
531000 498000
0.82 0.88 0.65
20.9 20.1 31.6 36.1 21.9 22.2
1.6
35.2 33.3
150000 155000
4
228 237 301 302 314 289 252 231 293 273 310 230 290 300 300 340 270
5.5
0.82 2
26.1 3.3
0.6 2.3 3.7
16.4
6.5
41500 40300
14
9310 7310
12 4.9 18.1 24
0.6 0.45 1 0.3 1.5 0.9
6860
168000 180000
0.14
64300 143000
9.2
407 328 126 335 55.9 334 58 263 172 287 200 220 220 180 150 140 380
33200 29200
0.15
1.3 0.68 1.3 5.4 1.2 0.6 0.4 14
21.5 15
0.069
145 368
4.8 18
370 257
0.88 1.3 2.4 2.6 0.9
40400 35300
98700 61800
8.8
374000 345000
134000 32800
4.2 5.1 5
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Thallium
Toluene
Total Dissolved Solids
Trichloroethene
Trichlorofluoromethane
Vanadium
Vinyl chloride
Xylenes (Total)
Zinc
MW-3R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Tin
Total Dissolved Solids
Vanadium
Zinc
MW-4R
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Cadmium
Chloride
Chloromethane
Chromium
Cobalt
Copper
Cyanide
delta-BHC
Endosulfan II
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Vanadium
Zinc
MW-5R
Acetone
Alkalinity, Total as CaCO3
Arsenic
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Nov-03May-03Dec-02Apr-02Nov-01Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-967.4 8.4 18 31 5.9
200 220 13 370 400 950 1500 300 52 1400 860 620 800 790 1230
2.3 15 19 50 100 24 77 25 16 28 20 9
21 35 53 80 40 39 32 26 27 15 15
0.2 0.7
12 5.6 7.5
97 94 86 61 900 550 350 570 860 950 2000 850 650 280 720 595
7
2.6 5.5 5 95 38 28 60 110 300 130 55 47 21
5.3 6 36 14 8.1 9.5 40 50 76 43 29 12 16 17
0.36 0.21 0.3 1.7
10
6
150
75 5
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
100 700 µg/L Barium 57.1 55.9 55.9 92.7 54 58.2 54.4 53.9 57.7 53.4
15 3 µg/L bis(2-Ethylhexyl)phthalate 1
1 2 µg/L Cadmium
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 15100 16400 15300 16200 15700 15500 13900 15200 16200 16100
1 3 µg/L Chloromethane
10 10 µg/L Chromium 4.6 5.8 5.1 4.8 4.8 5.6
10 1000 µg/L Cobalt 2.5
10 70 µg/L Cyanide 4.4 5.1
300 300 µg/L Iron 68.4 87.8 32600 113 221 123 126 102
10 15 µg/L Lead
50 50 µg/L Manganese 1890 2.6 6.1
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 3.2
10 20 µg/L Silver
NE NE µg/L Sodium 13900 14200 13100 11300 13100 13700 13600 13800 13000 14500
250000 250000 µg/L Sulfate 7740 8450 7620 7430 8000 8180 8060 8310 11200 8400
NE 500000 µg/L Total Dissolved Solids 156000 145000 154000 104000 166000 163000 167000 154000 131000 157000
25 300 µg/L Vanadium 4.4 5 4.2 3.7 4.3 5.6
10 1000 µg/L Zinc 7.3 11.4
MW-6R
10 10 µg/L Arsenic
100 700 µg/L Barium
10 10 µg/L Chromium
10 15 µg/L Lead
0.2 1 µg/L Mercury
MW-7
1 200 µg/L 1,1,1-Trichloroethane
5 6 µg/L 1,1-Dichloroethane 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.84 1.2
0.1 0.1 µg/L 4,4'-DDD
100 6000 µg/L Acetone 15.7
NE NE µg/L Alkalinity, Total as CaCO3 85000 80100 71700 67300 64100 62400 51900 51600 63500 51900
10 10 µg/L Arsenic
100 700 µg/L Barium 163 140 129 140 122 111 90.8 98.8 115 95.1
1 1 µg/L Benzene 0.43 0.42 0.26 0.29
1 4000 µg/L Beryllium 0.58
0.05 0.019 µg/L beta-BHC
100 700 µg/L Carbon disulfide
NE 250000 µg/L Chloride 5290 4820 4430 6050 4340 4300 3600 5160 5340 3810
10 3000 µg/L Chloroethane 1.3
1 3 µg/L Chloromethane 0.13
10 10 µg/L Chromium
5 70 µg/L cis-1,2-Dichloroethene 1.1 1.1 0.77 0.8 0.73 0.73 0.37 0.54 0.72 0.62
10 70 µg/L Cyanide 5
5 1000 µg/L Dichlorodifluoromethane 0.62 1
0.002 0.002 µg/L Dieldrin 0.11
0.1 40 µg/L Endosulfan I 0.15
0.075 0.004 µg/L Heptachlor epoxide 0.12
300 300 µg/L Iron 25.2 76.5
10 15 µg/L Lead
5 500 µg/L m&p-Xylene 1.2 2.2 1.8 0.84 1.5 1.1 0.96
50 50 µg/L Manganese 51.9 35.6 28.8 33.6 27.1 22.9 15.5 19.4 24.9 17.4
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 3.1 4.2 3.7 9.5 3.9 2.1 2.9
NE NE µg/L o-Xylene 0.46 0.63 0.47 0.27 0.4 0.36 0.27
10 20 µg/L Silver
NE NE µg/L Sodium 17800 16200 16400 15700 16300 16600 14200 13000 14300 13900
250000 250000 µg/L Sulfate 6720 3800 2930 10100 1850 1360 2090
1 0.7 µg/L Tetrachloroethene 0.48
NS NS µg/L Tetrahydrofuran 32 21.7 13.5 17.7 14.1 8.8 5.2 13.7 24.2 26
NE 500000 µg/L Total Dissolved Solids 175000 153000 137000 78000 145000 138000 126000 116000 108000 111000
1 2000 µg/L Trichlorofluoromethane 0.91 1.5 0.92 1.4 0.79 1.2 0.62 0.47 0.250.29
5 500 µg/L Xylenes (Total)1.2 0.79
10 1000 µg/L Zinc 8.9 5.7 5.2 6.8
MW-8
100 6000 µg/L Acetone 15.8
NE NE µg/L Alkalinity, Total as CaCO3 20800 25800 24800 23200 20000 22800 21300 19700 22800 19500
10 10 µg/L Arsenic 2.6
100 700 µg/L Barium 42.9 44 38.3 34.4 30 38 30.7 25.4 28.5 26.9
NE 250000 µg/L Chloride 3060 2670 1960 2040 1960 1350 1800 1510 2070 1860
10 10 µg/L Chromium 4.1
10 70 µg/L Cyanide 9.9 4.3 5.1
10 100 µg/L Di-n-octylphthalate 5.6
300 300 µg/L Iron 48.6 54 529 136 61.5 60.8
10 15 µg/L Lead
50 50 µg/L Manganese 3 2.7 2.9 3.3 3.4 19.9 6.8
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Barium
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chloromethane
Chromium
Cobalt
Cyanide
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
MW-6R
Arsenic
Barium
Chromium
Lead
Mercury
MW-7
1,1,1-Trichloroethane
1,1-Dichloroethane
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
beta-BHC
Carbon disulfide
Chloride
Chloroethane
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cyanide
Dichlorodifluoromethane
Dieldrin
Endosulfan I
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
o-Xylene
Silver
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Xylenes (Total)
Zinc
MW-8
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chromium
Cyanide
Di-n-octylphthalate
Iron
Lead
Manganese
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-0457.5 85.2 63.7 53 54.3 66.8 53 56 58 70.6 58 58 57 54 53 80 76
16100 16400
5.4
5.2 14.7 7.6 5.8 5 8.6 5.2 5.3 5.6 8.4 6.4 6.2 6.2 3.5 5.6 14 7.3
209 3540
5.1
43.5
0.4
0.57 0.16 0.46 0.6 0.3 0.8 0.6
14200 13300
7910 7020
149000 139000
13
15.3
28
2.2
0.82
1.2 1.9 3.8
0.13
50200 47700
3.4
100 97.1 104 100 99.3 104 87 99 96 101 89 76 74 60 53 63 180
0.1
12.5
0.55 0.65 0.9 7.3 4.4 26
0.5 0.67 0.71
0.081
0.066
1.4
10.2 12.7
0.24
0.39
0.84 0.23 0.56 0.88 0.4 1 0.7
13700 12000
18.9
109000 124000
0.34 0.48
3.8
20100 19600
6
27.5 24.4 27.3 26.8 28.8 27.2 25 33 24 26.6 30 29 29 26 25 30 480
0.96 0.62 1.4 0.8 1 0.4 2.4 28
57.8 151
41
7
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Barium
bis(2-Ethylhexyl)phthalate
Cadmium
Carbon disulfide
Chloride
Chloromethane
Chromium
Cobalt
Cyanide
Iron
Lead
Manganese
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
MW-6R
Arsenic
Barium
Chromium
Lead
Mercury
MW-7
1,1,1-Trichloroethane
1,1-Dichloroethane
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
beta-BHC
Carbon disulfide
Chloride
Chloroethane
Chloromethane
Chromium
cis-1,2-Dichloroethene
Cyanide
Dichlorodifluoromethane
Dieldrin
Endosulfan I
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
o-Xylene
Silver
Sodium
Sulfate
Tetrachloroethene
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Xylenes (Total)
Zinc
MW-8
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chromium
Cyanide
Di-n-octylphthalate
Iron
Lead
Manganese
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Nov-03May-03Dec-02Apr-02Nov-01Jul-01Dec-00Jun-00Nov-99Jun-99Nov-98May-98Oct-97May-97Oct-96Jan-9665 72 65 150 610 270 400 200 200 240 480 820 610 330 620 1000
2.7
25
8.7 9.5 7.4 23 140 49 82 8.1 29 38 96 170 16 70 43 96
13 7.6 7.6 8.2 16 29 69 31 14 20 19
0.8
10
16
25 24 41 180 530 62 41 82 59 160 360 260 300 590 1400
2.4 3.2 26 95 4.1 2.6 2.8 12 33 14 21 10 12
7.6 38 5.8 20 14 14 11 18
1.4
8.6 17 16 45 9.8
820 130 210 84 1300 1300 2600 360 390 960 1300 1200 1800 750 970 1930
9
150 17 32 6.8 270 210 580 2.5 62 190 350 430 410 180 21 28
24 5.3 6 36 26 65 8.7 12 30 36 38 53 23 6 17
0.2 0.4 1.4
10
2.6
36 46 89
52 77 48 150 2700 2600 4200
3.2 3.8 2 23 94 92 240
6.7 150 210 400
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 1.1
10 20 µg/L Silver
NE NE µg/L Sodium 9240 9700 8280 7940 6940 7810 6160 5580 6120 6980
250000 250000 µg/L Sulfate 2700 4090 1630 1350 1860 2100
NE 500000 µg/L Total Dissolved Solids 67000 67000 87000 79000 61000 64000 50000 61000 51000 58000
10 1000 µg/L Zinc 7.1 15.2
MW-9
NE NE µg/L Alkalinity, Total as CaCO3 25400 23300 21200 23400 18900 18300 18300 18400 21700 17200
10 10 µg/L Arsenic 3.5
100 700 µg/L Barium 207 195 197 186 182 193 168 170 174 142
15 3 µg/L bis(2-Ethylhexyl)phthalate 13
NE 250000 µg/L Chloride 4610 4360 6850 4710 4290 3610 3610 3950 4300 3560
10 10 µg/L Chromium
10 70 µg/L Cyanide 4.7
5 1000 µg/L Dichlorodifluoromethane 1.5 0.88 0.76 0.28 0.28
300 300 µg/L Iron 149 128 55.9 136 867
10 15 µg/L Lead
50 50 µg/L Manganese 4.6 8.5 6.3 4 3.5 7.6 6.9 16.6
10 20 µg/L Silver
NE NE µg/L Sodium 15400 15700 14200 14500 14500 14600 12400 13500 12900 13100
250000 250000 µg/L Sulfate 960 3440 1110 2030 2100 3200
NE 500000 µg/L Total Dissolved Solids 141000 135000 103000 142000 134000 141000 107000 124000 100000 118000
1 2000 µg/L Trichlorofluoromethane 1.4 1 1.3 1.1 0.98 0.96 0.47 0.69 0.36 0.49
10 1000 µg/L Zinc 5.1 5.3
MW-10
50 NE µg/L 2-Hexanone 0.69 0.96
100 NE µg/L 4-Methyl-2-pentanone (MIBK)2.8 2.5 2.6 5.6 2.2
100 6000 µg/L Acetone 22.5 14.1 11.8
NE NE µg/L Alkalinity, Total as CaCO3 446000 626000 29000 48200 47300 42200 31400 26700 32100 25500
10 10 µg/L Arsenic 2.6 5.2
100 700 µg/L Barium 221 148 292 241 660 262 132 112 115 101
1 1 µg/L Benzene 0.83 0.46 0.44
1 4000 µg/L Beryllium 3.2 1.9 2.8 1.4
100 700 µg/L Carbon disulfide 2 5.2
NE 250000 µg/L Chloride 318000 202000 9640 47400 51800 2220 1820 1790 2040 1800
10 10 µg/L Chromium 4.2 6.4 9.1 3.5 6.7
5 70 µg/L cis-1,2-Dichloroethene 0.2 0.33 0.35
10 1000 µg/L Cobalt 21.8 39.5 3.1 3.1 4.8
10 1000 µg/L Copper 16.4 6.3 3.8
10 70 µg/L Cyanide 5.4 4.1 9.8
0.1 40 µg/L Endosulfan I 0.17
1 600 µg/L Ethylbenzene 0.53 0.55 0.4 1 0.73
0.05 0.008 µg/L Heptachlor 0.21 0.12
0.075 0.004 µg/L Heptachlor epoxide 0.17 0.093
300 300 µg/L Iron 2400 2430 11800 3690 3650 1160 84.3 92.8 218
10 15 µg/L Lead 4.1 2.6 19.1 8.5 11.6 4.1
5 500 µg/L m&p-Xylene 1.2 2.1 0.68 1.2 1.1
50 50 µg/L Manganese 8390 12300 530 587 736 130 10.9 7.9 5.1
0.2 1µg/L Mercury 0.120.120.290.330.51
1 5 µg/L Methylene Chloride 2.8 1.2
50 100 µg/L Nickel 6.9 10.7 4.7 3.9 5.9
NE NE µg/L o-Xylene 1 2.1 0.43 0.85 0.65
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 123000 184000 10300 19800 14100 6860 5280
250000 250000 µg/L Sulfate 333000 555000 15800 63600 8770
1000 NE µg/L Sulfide 260
NS NS µg/L Tetrahydrofuran 182 237 6.1 120 145 106 18.6 5
5.5 200 µg/L Thallium 0.043
100 2000000 µg/L Tin 3.1 8.5
1 600 µg/L Toluene 0.27 0.63
NE 500000 µg/L Total Dissolved Solids 1150000 2040000 311000 403000 279000 86000 63000 66000 46000 63000
1 2000 µg/L Trichlorofluoromethane 0.20.330.380.49
25 300 µg/L Vanadium 2.7 20 5.6 4.9
10 1000 µg/L Zinc 5.4 5.1 34 27.2 21.2 6.2
MW-11
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 21.1
NE NE µg/L Alkalinity, Total as CaCO3 135000 107000 104000 127000 132000 143000 175000 161000 189000 153000
100 700 µg/L Barium 102 93.1 103 97.2 93.7 96.8 94.3 87.8 87 76.8
10 200 µg/L Benzo(g,h,i)perylene
NE 250000 µg/L Chloride 13500 14500 14500 14900 14400 15000 12400 14000 14200 12900
1 3 µg/L Chloromethane 0.23
10 10 µg/L Chromium
10 1000 µg/L Cobalt 2.9 2.5 2.6 47.5 65.1
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Mercury
Methylene Chloride
Silver
Sodium
Sulfate
Total Dissolved Solids
Zinc
MW-9
Alkalinity, Total as CaCO3
Arsenic
Barium
bis(2-Ethylhexyl)phthalate
Chloride
Chromium
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Silver
Sodium
Sulfate
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-10
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzene
Beryllium
Carbon disulfide
Chloride
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
Endosulfan I
Ethylbenzene
Heptachlor
Heptachlor epoxide
Iron
Lead
m&p-Xylene
Manganese
Mercury
Methylene Chloride
Nickel
o-Xylene
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Tin
Toluene
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-11
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Benzo(g,h,i)perylene
Chloride
Chloromethane
Chromium
Cobalt
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-040.1 0.26
0.1 0.16 0.2 0.1 0.16
6250 5410
52000 81000
45.4
20100 17400
142 141 153 157 134 128 173 124 124 117 140 140 100 100 85 95 240
7.6 0.5 14
14
0.43 0.27 0.32 0.2 0.4 0.2 0.32
12600 11900
123000 128000
0.42 0.26
413000 21700
96.5 91.3 80.7 38.9 46.6 39.1 39 42 42 40.8 52 71 48 46 82 55 98
13
0.63 0.7 13
55.1 424
6.8
6.8
0.2
6.2
0.12 0.19
49000 89000
0.68 0.52
0.05
120000 122000
70.3 57.5 56.2 48.1 37.6 31.8 28 29 29 23.1 25 24 26 27 24 28 47
1.3
10800 8480
3.9 3.3
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
10 1000 µg/L Copper 2.8
10 70 µg/L Cyanide 4.1 4.2
300 300 µg/L Iron 26700 32400 29400 34600 31400 35700 33400 32100 30700 29000
10 15 µg/L Lead 2.9 3.6
50 50 µg/L Manganese 1720 1670 1820 2020 1990 2030 1960 1920 1890 1740
1 5 µg/L Methylene Chloride 1.4
10 20 µg/L Selenium 5.6
10 20 µg/L Silver
NE NE µg/L Sodium 11700 12000 11200 12000 9460 10000 8490 9070 8290 8770
250000 250000 µg/L Sulfate 14100 17100 15200 19100 15300 12800 10700 10400 11000 10400
1000 NE µg/L Sulfide 130
NS NS µg/L Tetrahydrofuran 4.5
5.5 200 µg/L Thallium 8.8
NE 500000 µg/L Total Dissolved Solids 226000 189000 236000 281000 239000 228000 207000 236000 228000 220000
25 300 µg/L Vanadium 3.5 3.2 3.6
10 1000 µg/L Zinc 92
MW-12
100 6000 µg/L Acetone 12.1
NE NE µg/L Alkalinity, Total as CaCO3 64500 72900 55900 41000 19200 40500 45500 39300 29600 40200
10 10 µg/L Arsenic
100 700 µg/L Barium 113 144 190 95.7 60.9 59.2 61.1 47.6 50.1 50.5
10 200 µg/L Benzo(g,h,i)perylene
NE 250000 µg/L Chloride 19700 23300 26000 9000 8070 8240 6180 6230 5820 4900
1 3 µg/L Chloromethane
10 10 µg/L Chromium
10 70 µg/L Cyanide 5.3
5 1000 µg/L Dichlorodifluoromethane 0.23
10 100 µg/L Di-n-octylphthalate 5.6
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
300 300 µg/L Iron 714 274 312 523 524 758 348 253 324 1430
50 50 µg/L Manganese 134 148 90.8 49.6 9.7 199 14.6 86.1 13.2 33.6
1 5 µg/L Methylene Chloride 2 2
50 100 µg/L Nickel 4.4 6.2 5.5 3.2 4.1
10 20 µg/L Silver
NE NE µg/L Sodium 16200 19200 19200 13700 11200 12800 11000 10500 11100 11000
250000 250000 µg/L Sulfate 86100 129000 169000 70800 73600 32800 48000 27400 51800 24200
NS NS µg/L Tetrahydrofuran 11.4 26.8 12.4
5.5 200 µg/L Thallium 0.021
NE 500000 µg/L Total Dissolved Solids 288000 286000 382000 234000 163000 135000 149000 126000 138000 127000
1 2000 µg/L Trichlorofluoromethane 1 2.8 1.4 0.82 0.22 0.32
10 1000 µg/L Zinc 30.8
MW-13
5 350 µg/L 1,1-Dichloroethene
100 6000 µg/L Acetone 17.3
NE NE µg/L Alkalinity, Total as CaCO3 42400 42300 41000 37100 36900 36200 46400 43200 58700 43900
10 10 µg/L Arsenic 2.6
100 700 µg/L Barium 120 91.6 210 71.5 89.3 130 77.1 106 176 279
10 0.005 µg/L Benzo(a)pyrene
10 0.05 µg/L Benzo(b)fluoranthene
10 200 µg/L Benzo(g,h,i)perylene
1 4000 µg/L Beryllium 2.2 0.68 0.66 1.2 2.4 3.5
NE 250000 µg/L Chloride 4310 4100 4590 3270 3760 5870 3880 5700 3820 6150
10 10 µg/L Chromium 13.6 2.9 3 7.1 11.8
10 1000 µg/L Cobalt 6.6
10 1000 µg/L Copper 8.5 3.8 7.6 6.9
10 70 µg/L Cyanide 5
10 0.005 µg/L Dibenz(a,h)anthracene
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
300 300 µg/L Iron 58 343 11000 790 1400 2720 232 1330 8610 11300
10 15 µg/L Lead 8 2.9 5.4 6.5 7.5
50 50 µg/L Manganese 9.7 26.7 284 62.1 41.2 55.6 34.1 48.8 158 301
50 100 µg/L Nickel 6.4
10 20 µg/L Silver
NE NE µg/L Sodium 10000 9380 9420 12200 10700 10700 11200 11700 19100 14600
250000 250000 µg/L Sulfate 5670 5390 7280 10100 9330 8660 8680 9360 7820 9770
1000 NE µg/L Sulfide 151 106
NS NS µg/L Tetrahydrofuran
100 2000000 µg/L Tin 2.5
NE 500000 µg/L Total Dissolved Solids 89000 79000 145000 110000 107000 119000 113000 114000 87000 144000
1 2000 µg/L Trichlorofluoromethane
25 300 µg/L Vanadium 22.6 2.6 3.4 7.1 14.6 18.7
10 1000 µg/L Zinc 5.7 12.8 40.5 8.6 7.9 13.7 17.2 37.3 51
MW-14
100 6000 µg/L Acetone 14.7
NE NE µg/L Alkalinity, Total as CaCO3 55300 59700 50400 51500 45200 42300 37400 32800 35600 28900
10 10 µg/L Arsenic
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Copper
Cyanide
Iron
Lead
Manganese
Methylene Chloride
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Total Dissolved Solids
Vanadium
Zinc
MW-12
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(g,h,i)perylene
Chloride
Chloromethane
Chromium
Cyanide
Dichlorodifluoromethane
Di-n-octylphthalate
Indeno(1,2,3-cd)pyrene
Iron
Manganese
Methylene Chloride
Nickel
Silver
Sodium
Sulfate
Tetrahydrofuran
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Zinc
MW-13
1,1-Dichloroethene
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Beryllium
Chloride
Chromium
Cobalt
Copper
Cyanide
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Nickel
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Tin
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-14
Acetone
Alkalinity, Total as CaCO3
Arsenic
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-0426300 23000
1580 1250
8.7
1.2 0.48 0.5 0.8 0.4 0.39
7460 6480
9700 7590
4.4 12.1
161000 165000
37200 40200
2.7
46.9 60.1 39.1 44.9 40.6 38 35 58 61 47.3 31 66 55 77 50 77 74
1.2
8200 8030
0.21
2.6 1.1 2.4 2 1.8 4 2.1
1.2
539 3030
15.7 58.3
0.7 0.2 0.39 0.4 0.2 0.26
11600 9980
20500 15300
130000 124000
19.8
52200 44500
144 139 164 176 126 117 79 89 65 85.6 79 62 65 59 46 57 160
1.1
1
1.5
1.4 2.3
5380
5.5 3.9 4 1.7 0.8 1.6 2.2 1.1 2 4.8 9.2
6.1
1.2
1.5
3760 6140
6.4 4.3 11
91.5 140
0.72 0.4 0.41 0.4 0.2
16700 20200
9420 9460
178
18.6
110000 159000
18.6
7.2 10.8
20 31.6
30100 30400
7.3 8.3
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
100 700 µg/L Barium 221 188 188 183 179 193 163 140 254 160
1 4000 µg/L Beryllium 0.6 0.57 0.83 0.63 0.54 0.6
15 3 µg/L bis(2-Ethylhexyl)phthalate 9.8
NE 250000 µg/L Chloride 3260 3410 3470 3930 3510 3720 3630 4100 4290 4790
1 3 µg/L Chloromethane
10 10 µg/L Chromium 4.5 6.6 6
10 1000 µg/L Copper 4.8 9.5 5.8
10 70 µg/L Cyanide 4.3 5.3 6
5 1000 µg/L Dichlorodifluoromethane 3.6 2.3 3.6 2.1
300 300 µg/L Iron 134 123 312 466 695 2620 142 915 5820 4520
10 15 µg/L Lead
50 50 µg/L Manganese 18.1 13.7 21.6 69.3 25.7 120 40.2 110 240 251
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 1.6
50 100 µg/L Nickel 2.7 2.8 2.8 5.3 8.6 13.7
10 20 µg/L Silver
NE NE µg/L Sodium 16900 16200 15400 15800 14500 14400 12800 12300 13500 15000
250000 250000 µg/L Sulfate 663 1400 1080 1790
1 0.7 µg/L Tetrachloroethene 0.61
5.5 200 µg/L Thallium 0.048
NE 500000 µg/L Total Dissolved Solids 130000 118000 85000 135000 131000 119000 124000 123000 102000 127000
1 2000 µg/L Trichlorofluoromethane 0.75 0.58 1.1 0.54 0.59 0.57 0.34
25 300 µg/L Vanadium 5.5 9.9 8
10 1000 µg/L Zinc 6.3 13.3 11.7 27.4 23
MW-15
5 350 µg/L 1,1-Dichloroethene
0.1 0.1 µg/L 4,4'-DDD 0.062
100 6000 µg/L Acetone 13.2
NE NE µg/L Alkalinity, Total as CaCO3 98100 101000 104000 103000 91500 54700 96600 64300 78900 77600
10 10 µg/L Arsenic 4.5 7.1
100 700 µg/L Barium 22.7 14 11 74 105 41.5 8.6 23.8 59.6 143
NE 250000 µg/L Chloride 104000 98000 94000 113000 98200 146000 83400 124000 124000 143000
5 70 µg/L Chloroform 0.4 0.44 0.7 0.44 0.26 0.49 0.77 0.63 0.49
10 10 µg/L Chromium 5.4 7.6 6.7
10 1000 µg/L Copper 2.6 7.1 8.8 10.5
10 70 µg/L Cyanide 5.2
300 300 µg/L Iron 1740 781 227 8180 10600 233 292 239 4140 12300
10 15 µg/L Lead 66.8 9.5
50 50 µg/L Manganese 359 259 116 297 271 33 34.7 14 160 317
1 5 µg/L Methylene Chloride 2.4
50 100 µg/L Nickel 2.7 3.9 4.3
NE NE µg/L Sodium 21600 20200 20100 21800 20300 24000 24200 25300 26700 21200
250000 250000 µg/L Sulfate 58300 58700 63700 70000 65400 43800 59500 53200 41200 35600
1000 NE µg/L Sulfide 100
NS NS µg/L Tetrahydrofuran 12 16.8 27.3 19.8 16.9 15.5 21.4 14.7 7.4 6.3
5.5 200 µg/L Thallium 0.049
NE 500000 µg/L Total Dissolved Solids 410000 371000 418000 362000 360000 464000 373000 410000 442000 298000
1 2000 µg/L Trichlorofluoromethane 2.1 4.4 5.1 4.8 4.4 3.9 5.3 7.6 4.3 8.1
25 300 µg/L Vanadium 5 18.9 24.7 8.6 28.6
10 1000 µg/L Zinc 16.2 6.3 5.9 35.4 49 5.3 17.1 22.7 45.6
SW-1
100 6000 µg/L Acetone 11.2
NE NE µg/L Alkalinity, Total as CaCO3 33200 57400 27700 35100 44500 63700 45200 72700 58000 79700
10 10 µg/L Arsenic 3.6 5.9
100 700 µg/L Barium 86.8 65.9 69.5 65 72.2 276 65.8 71.1 58.9 63.3
1 4000 µg/L Beryllium 1.1
1 2 µg/L Cadmium 0.7
NE 250000 µg/L Chloride 49200 26800 26000 21600 31500 19500 23700 18100 20600 19700
10 10 µg/L Chromium 13
10 1000 µg/L Cobalt 9 14.6
10 1000 µg/L Copper 8.6 3.9 16.4
10 70 µg/L Cyanide 4.4 4.7
0.1 2 µg/L Endrin 0.08
300 300 µg/L Iron 5040 5660 5520 9830 8870 155000 8210 22800 6900 25500
10 15 µg/L Lead 18.3
50 50 µg/L Manganese 804 1050 465 688 1160 1760 749 1530 855 1720
0.2 1 µg/L Mercury
1 5 µg/L Methylene Chloride 2
50 100 µg/L Nickel 8.7
10 20 µg/L Selenium 7
10 20 µg/L Silver
NE NE µg/L Sodium 23000 14200 13000 12800 16000 12500 14500 13000 12400 15500
250000 250000 µg/L Sulfate 2530 3410 4320 4460 3690 3130 2820 2190 2700 2090
NE 500000 µg/L Total Dissolved Solids 143000 116000 118000 113000 140000 122000 126000 125000 104000 131000
25 300 µg/L Vanadium 4.3 37
10 1000 µg/L Zinc 10.1 7.2 7.5 69.8
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Barium
Beryllium
bis(2-Ethylhexyl)phthalate
Chloride
Chloromethane
Chromium
Copper
Cyanide
Dichlorodifluoromethane
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Silver
Sodium
Sulfate
Tetrachloroethene
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
MW-15
1,1-Dichloroethene
4,4'-DDD
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Chloride
Chloroform
Chromium
Copper
Cyanide
Iron
Lead
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Thallium
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
SW-1
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Beryllium
Cadmium
Chloride
Chromium
Cobalt
Copper
Cyanide
Endrin
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Total Dissolved Solids
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-04122 143 125 129 130 242 98 583 186 130 210 460 250 120 69 66 170
0.24
1.8 2.3 3 10.7 0.4 40 4.1 1.7 6.6 35 15 3.9 3.2
1140 2050
7.2 26 5.2 23 13 5.9 8
170 71
0.1 0.44
12.5
0.74 0.39 0.54 0.5 0.6 0.48
14300 12700
145000 138000
12
3.1
75300
5.7
115
60600
1.4
7.2
10000
7.6
327
16300
25800
260000
7.3
23.4
51.1
2.2 22.7
47200 19600
3.7 23 20
70.4 42.5 69.9 61.9 92.5 77.7 46 78 80 70.3 88 54 120 73 750 53 500
25300 19100
0.6 0.7 1.2 0.61 4.2 52 3.2 36
11400 2290
17.5 57 38
1040 130
1.1
0.4 0.28 0.62 0.4 0.4 0.51
14300 9390
98000 140000
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
SW-2
50 NE µg/L 2-Hexanone 1.8
20 NE µg/L 3,3'-Dichlorobenzidine
10 NE µg/L 3-Methylcholanthrene
100 6000 µg/L Acetone
NE NE µg/L Alkalinity, Total as CaCO3 46200 58800 32300 43200 33200 2390 41300 48900 48600 44700
10 10 µg/L Arsenic 3.7 17 6.2
100 700 µg/L Barium 77.5 108 73.1 70 700 171 59.7 50.1 51.7 46.5
10 0.05 µg/L Benzo(a)anthracene
10 0.005 µg/L Benzo(a)pyrene
10 0.05 µg/L Benzo(b)fluoranthene
10 200 µg/L Benzo(g,h,i)perylene
10 0.5 µg/L Benzo(k)fluoranthene
1 4000 µg/L Beryllium 3.7 0.64
15 3 µg/L bis(2-Ethylhexyl)phthalate
NE 250000 µg/L Chloride 13800 6190 9720 12500 4050 28200 10700 11600 10800 10300
10 10 µg/L Chromium 40.3 3.2
10 5 µg/L Chrysene
10 1000 µg/L Cobalt 5.9 4.4
10 1000 µg/L Copper 81.6 3.2
10 0.005 µg/L Dibenz(a,h)anthracene
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
300 300 µg/L Iron 1790 29900 1510 2070 226000 75000 2130 3360 1400 1280
10 15 µg/L Lead 2.7 75 7.4
50 50 µg/L Manganese 304 1160 317 291 1020 1010 219 152 153 106
0.2 1 µg/L Mercury 0.2
1 5 µg/L Methylene Chloride 3.1
50 100 µg/L Nickel 16.4 3.1
10 20 µg/L Selenium
10 20 µg/L Silver
NE NE µg/L Sodium 11600 10200 8420 11300 8390 17600 9840 10300 9160 9990
250000 250000 µg/L Sulfate 10900 6270 17100 11600 7280 5620 12700 5490 5090 4240
1000 NE µg/L Sulfide 142
NS NS µg/L Tetrahydrofuran 18.4
1 600 µg/L Toluene 0.52
NE 500000 µg/L Total Dissolved Solids 129000 106000 113000 105000 125000 117000 120000 114000 91000 101000
25 300 µg/L Vanadium 127 11.6
10 1000 µg/L Zinc 249 28
SW-3
10 40 µg/L 3&4-Methylphenol(m&p Cresol)3.6
0.1 0.1 µg/L 4,4'-DDD 0.079
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 16.2
NE NE µg/L Alkalinity, Total as CaCO3 251000 520000 161000 210000 118000 389000 259000 516000 293000 317000
100 700 µg/L Barium 173 270 114 152 105 206 181 348 185 315
1 1 µg/L Benzene 0.42 0.54 0.32 0.88 0.34
NE 250000 µg/L Chloride 18400 34000 10500 16300 27000 27000 16900 34800 20000 24300
10 10 µg/L Chromium 3.4
5 70 µg/L cis-1,2-Dichloroethene 0.26
10 1000 µg/L Cobalt 3 6.8 3.4 14.8 14.4 25.3 13
10 1000 µg/L Copper 4.4
10 70 µg/L Cyanide 4.6 6
0.1 42 µg/L Endosulfan II 0.071
300 300 µg/L Iron 8240 10500 3390 4160 4940 5270 8890 11700 9560 16500
10 15 µg/L Lead 2.7
50 50 µg/L Manganese 4750 8350 2310 3860 1420 5080 4320 8930 3990 5200
1 5 µg/L Methylene Chloride 1
50 100 µg/L Nickel 3.6 6.8 2.8 2.8 4.8 12
NE NE µg/L Sodium 24600 38400 14700 20900 18200 29900 29900 41100 25000 33800
250000 250000 µg/L Sulfate 15200 18500 11400 27000 17000 16800 26300 62500 20100 36400
NS NS µg/L Tetrahydrofuran 6.3 3.3 10.2 9.7 18.9 5.1 4.8
100 2000000 µg/L Tin 2.8
NE 500000 µg/L Total Dissolved Solids 321000 623000 231000 300000 233000 473000 319000 705000 327000 432000
25 300 µg/L Vanadium 5.6 9.7 9.8
10 1000 µg/L Zinc 9.6 13.6 10.8
SW-4
5 350 µg/L 1,1-Dichloroethene
50 NE µg/L 2-Hexanone 3.1
0.1 0.1 µg/L 4,4'-DDD 0.11
0.1 0.1 µg/L 4,4'-DDT
100 6000 µg/L Acetone 16
NE NE µg/L Alkalinity, Total as CaCO3 187000 240000 148000 187000 242000 140000 158000 152000 147000 220000
100 700 µg/L Barium 121 128 113 115 187 82.8 126 101 106 151
NE 250000 µg/L Chloride 27400 27900 20300 19800 19000 24300 30800 31000 26900 28800
5 70 µg/L Chloroform
10 1000 µg/L Cobalt 5.9 10.4
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
SW-2
2-Hexanone
3,3'-Dichlorobenzidine
3-Methylcholanthrene
Acetone
Alkalinity, Total as CaCO3
Arsenic
Barium
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Beryllium
bis(2-Ethylhexyl)phthalate
Chloride
Chromium
Chrysene
Cobalt
Copper
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Iron
Lead
Manganese
Mercury
Methylene Chloride
Nickel
Selenium
Silver
Sodium
Sulfate
Sulfide
Tetrahydrofuran
Toluene
Total Dissolved Solids
Vanadium
Zinc
SW-3
3&4-Methylphenol(m&p Cresol)
4,4'-DDD
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Benzene
Chloride
Chromium
cis-1,2-Dichloroethene
Cobalt
Copper
Cyanide
Endosulfan II
Iron
Lead
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Tetrahydrofuran
Tin
Total Dissolved Solids
Vanadium
Zinc
SW-4
1,1-Dichloroethene
2-Hexanone
4,4'-DDD
4,4'-DDT
Acetone
Alkalinity, Total as CaCO3
Barium
Chloride
Chloroform
Cobalt
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-043.6
2.9
4
44200 26100
5.5
53.4 81 49.2 57.6 59.4 52.1 46 51 51 49.4 300 44 150 51 47 65 63
1.1
2.5
2.8
1.8
2.5
1.1
11300 10900
0.4 17 4.7
1.1
2.1
2.2
1720 4170
11 7.6
157 280
0.081
21
0.2 0.2 0.36 0.5 0.3 0.26
9890 8650
6180 38300
101000 189000
7.5
13.5
0.09
221000 160000
179 123
0.25
22800 20900
5.5
0.085
9370 3230
3760 1890
21300 18500
26400 19800
4.5
329000 237000
0.58
0.062
0.054
158000 131000
136 105
30900 23600
0.97
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Historic Detections Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.
Value Column Labels
SWSL 2L units Row Labels Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12MCL
10 70 µg/L Cyanide 5.6
0.1 42 µg/L Endosulfan II
0.1 2 µg/L Endrin aldehyde
300 300 µg/L Iron 1480 1520 1520 2240 9220 638 2520 1790 4180 1640
50 50 µg/L Manganese 2900 2930 1930 2550 5050 739 2250 1080 1650 2430
1 5 µg/L Methylene Chloride 1.2
50 100 µg/L Nickel 2.5 3.6
NE NE µg/L Sodium 23400 26000 16900 20200 23800 17800 24400 20100 18200 29000
250000 250000 µg/L Sulfate 18200 28600 16600 24900 23500 17600 23500 23000 13200 32300
NS NS µg/L Tetrahydrofuran 3.5 3.6 4.1 4.4
NE 500000 µg/L Total Dissolved Solids 289000 325000 229000 267000 371000 222000 257000 270000 255000 349000
1 2000 µg/L Trichlorofluoromethane 0.27 0.25
25 300 µg/L Vanadium 3.5 5.9
10 1000 µg/L Zinc 7.3
c:\pwworking\tpa\d0269489\W-S GW Revised
Facility Permit
Historic Detections
Value
Row Labels
Cyanide
Endosulfan II
Endrin aldehyde
Iron
Manganese
Methylene Chloride
Nickel
Sodium
Sulfate
Tetrahydrofuran
Total Dissolved Solids
Trichlorofluoromethane
Vanadium
Zinc
Old Salisbury Road Landfill (C&D)
Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND.Apr-12Dec-11Nov-11Jun-11May-11Nov-10Apr-10Mar-10Sep-09Mar-09Dec-08Mar-08Nov-07Apr-07Nov-06Apr-06Nov-05Jun-05Nov-04Aug-04May-040.066
0.061
2140 1060
2420 1290
20000 17900
23600 19500
272000 234000
1.4
c:\pwworking\tpa\d0269489\W-S GW Revised
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
June-17
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 110000 125000 333000 14100
EPA 6010
µg/L
100 700 µg/L Barium 323 343 221 102
10 10 µg/L Chromium 4.2
10 1000 µg/L Cobalt 20.6 59.9 21.8
300 300 µg/L Iron 3870 302 2400 26700
10 15 µg/L Lead 4.1
50 50 µg/L Manganese 9200 801 8390 1720
50 100 µg/L Nickel 17 5.8 6.9
NE NE µg/L Sodium 72400 42100 123000 11700
5.5 200 µg/L Thallium 0.043
25 300 µg/L Vanadium 2.7
10 1000 µg/L Zinc 8.6 5.4
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.48
1 0.4 µg/L 1,2-Dichloroethane 0.24
100 NE µg/L 4-Methyl-2-pentanone (MIB 2.8
100 6000 µg/L Acetone 10.3 11 22.5 21.1
1 1 µg/L Benzene 2.1
100 700 µg/L Carbon disulfide 2
1 3 µg/L Chloromethane 0.23
5 70 µg/L cis-1,2-Dichloroethene 0.51 0.2
1 600 µg/L Ethylbenzene 0.53
5 500 µg/L m&p-Xylene 1.2
NE NE µg/L o-Xylene 1
NS NS µg/L Tetrahydrofuran 36.3 9.3 182 4.5
1 600 µg/L Toluene 0.27
1 3 µg/L Trichloroethene 1
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 587000 315000 446000 135000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 796000 552000 1E+06 226000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 50400 35800 318000 13500
(blank)
feet
Static Water Level 7.88 8.1 11.39 3.92
Total Well Depth 21 20 21 20
mg/L
Oxygen, Dissolved 1.9 0.1 0.6 0.3
NTU
Turbidity 3.4 9.93 34.3 8.58
Std. Units
Field pH 6.1 6 6.1 5.9
mV
REDOX -62.6 154.4 -58.5 -10.4
(blank)
Appearance
Collected By
Odor
umhos/cm
Field Specific Conductance 1246 756 1714 354.9
deg C
Field Temperature 24.3 14.8 23 16.6
May-17
MCL
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 7740 6720 2700 960
EPA 6010
µg/L
10 10 µg/L Arsenic 5.5
100 700 µg/L Barium 272 309 57.1 163 42.9 207
1 4000 µg/L Beryllium
10 10 µg/L Chromium 4.6
10 1000 µg/L Cobalt 11.5
10 1000 µg/L Copper
300 300 µg/L Iron 54.8 89300 68.4 25.2
10 15 µg/L Lead 3.4
50 50 µg/L Manganese 12.5 6460 51.9 3 4.6
50 100 µg/L Nickel
NE NE µg/L Sodium 15800 2240 13900 17800 9240 15400
5.5 200 µg/L Thallium
100 2000000 µg/L Tin
25 300 µg/L Vanadium 4.4
10 1000 µg/L Zinc 5.5 8.9 5.1
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.3
100 6000 µg/L Acetone 21.4 18.4 15.7 15.8
1 1 µg/L Benzene 0.43
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.38 1.1
5 1000 µg/L Dichlorodifluoromethane 1.5
5 500 µg/L m&p-Xylene 1.2
1 5 µg/L Methylene Chloride 3.1
NE NE µg/L o-Xylene 0.46
1 0.7 µg/L Tetrachloroethene
NS NS µg/L Tetrahydrofuran 32
1 2000 µg/L Trichlorofluoromethane 0.91 1.4
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 68600 114000 32300 85000 20800 25400
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 165000 133000 156000 175000 67000 141000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 8860 2520 15100 5290 3060 4610
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 4.4 4.4 9.9
(blank)
feet
Static Water Level 35.05 18.43 10.6 36.56 15.16 52.82
Total Well Depth 60 27 50 48 27 60
mg/L
Oxygen, Dissolved 1.3 0.5 5.4 0.4 5.4 6.51
NTU
Turbidity 3.5 5.3 3.1 4.2 1.16 0.4
Std. Units
Field pH 5.5 6.3 5.9 5.5 5.6 5.5
mV
REDOX 179.6 -60 182.6 210.2 195 178.8
(blank)
Appearance
Collected By
Odor
umhos/cm
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
86100 5670 663 58300 2530 10900 15200 18200
113 120 221 22.7 86.8 77.5 173 121
0.6
3
2.6 761
714 58 134 1740 5040 1790 8240 1480 27.1
18.2
134 9.7 18.1 359 804 304 4750 2900
4.4 2.7 3.6
16200 10000 16900 21600 23000 11600 24600 23400
0.021 0.048 0.049
4
5
5.7 16.2 10.1 455
12.1 17.3 14.7 13.2 11.2 16.2 16 18.7 18.3
0.4
3.6
0.61
11.4 12 3.5
1 0.75 2.1
64500 42400 55300 98100 33200 46200 251000 187000
288000 89000 130000 410000 143000 129000 321000 289000
19700 4310 3260 104000 49200 13800 18400 27400
4.3 4.4 4.6
4.64 8.7 51.86 38.85
15.7 20 60 50.85
0.3 4.03 3.28 3.06 4.7 6.3 4.3 6
9.26 1.75 5.42 23.24 15.12 14.72 7.94 7.13
5.9 5.6 5.5 6.3 6.5 6.8 6.6 7.3
107.5 138.8 147 121 -7.1 -15.2 -49.6 -38.5
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
Field Specific Conductance 209.7 392.9 175.5 220.7 68.1 159
deg C
Field Temperature 20.3 20.4 21.2 19.7 17 19.8
November-16
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1380 121000 1530 193000 8450 3800 4090 3440 555000 17100
EPA 6010
µg/L
10 10 µg/L Arsenic 3.9 2.6
100 700 µg/L Barium 241 272 297 255 55.9 140 44 195 148 93.1
1 4000 µg/L Beryllium 0.58
10 10 µg/L Chromium 2.8 5.8 4.1 6.4
10 1000 µg/L Cobalt 16.5 9.8 100 39.5
300 300 µg/L Iron 96.2 1780 86400 214 149 2430 32400
10 15 µg/L Lead 3.5 2.6
50 50 µg/L Manganese 7.3 8570 5920 1320 35.6 2.7 8.5 12300 1670
50 100 µg/L Nickel 18.5 8 10.7
10 20 µg/L Selenium 5
NE NE µg/L Sodium 14600 70200 2450 71000 14200 16200 9700 15700 184000 12000
25 300 µg/L Vanadium 5
10 1000 µg/L Zinc 5.7 8.4 7.3 5.7 5.1
EPA 8081
µg/L
0.05 0.008 µg/L Heptachlor 0.21
0.075 0.004 µg/L Heptachlor epoxide 0.17
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.53 1.5
1 6 µg/L 1,4-Dichlorobenzene 0.39
100 NE µg/L 4-Methyl-2-pentanone (MIB 2.5
100 6000 µg/L Acetone 14.1
1 1 µg/L Benzene 2.2 0.38 0.42 0.83
100 700 µg/L Carbon disulfide 5.2
5 70 µg/L Chloroform
1 3 µg/L Chloromethane
5 70 µg/L cis-1,2-Dichloroethene 0.2 0.47 1.1 0.33
5 1000 µg/L Dichlorodifluoromethane 0.62 0.88
1 600 µg/L Ethylbenzene 0.38 0.55
5 500 µg/L m&p-Xylene 2.2 2.1
1 5 µg/L Methylene Chloride 4.2
NE NE µg/L o-Xylene 0.63 2.1
1 0.7 µg/L Tetrachloroethene 1.8 0.48
NS NS µg/L Tetrahydrofuran 39.1 13.6 21.7 237
1 600 µg/L Toluene
1 3 µg/L Trichloroethene 1.2
1 2000 µg/L Trichlorofluoromethane 1.5 1
1 0.03 µg/L Vinyl chloride 1
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 154000 831000 168000 824000 145000 153000 67000 135000 2E+06 189000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 9630 47600 2050 58400 16400 4820 2670 4360 202000 14500
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 5.4
Field
feet
Static Water Level 34.35 8.32 20.47 8.88 11.08 36.41 17.1 52.04 12.07 4.37
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
367.4 116.5 173.7 690 250.9 172 549 461
17.4 16.9 18.4 17.6 21 21 21.2 20.4
129000 5390 1400 58700 3410 6270 18500 28600
3.6 3.7
144 91.6 188 14 65.9 108 270 128
0.57
6.8
274 343 123 781 5660 29900 10500 1520
2.7
148 26.7 13.7 259 1050 1160 8350 2930
6.2 6.8
19200 9380 16200 20200 14200 10200 38400 26000
12.8 6.3
25.4
0.42
0.44
0.4
0.26
2.3
26.8 16.8 6.3 3.6
0.52
2.8 0.58 4.4
72900 42300 59700 101000 57400 58800 520000 240000
286000 79000 118000 371000 116000 106000 623000 325000
23300 4100 3410 98000 26800 6190 34000 27900
5.38 9.22 51.5 39.3
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 1.52 1.18 2.9 3.5 5.73 1.2 7.7 8.26 1.16 4.39
NTU
Turbidity 0.72 1.51 5.3 7.03 0.31 0.25 0.31 4.61 6.38 5.81
Std. Units
Field pH 5.6 6.2 6.3 6.1 5.9 5.6 5.7 5.5 6.2 6
mV
REDOX 137.2 24.1 -61.4 176.7 242.9 152 217.5 272 62.3 16.7
umhos/cm
Field Specific Conductance 202.8 1262 380.4 1204 176 203.1 73.7 167.8 2535 355
deg C
Field Temperature 16.6 15.9 15 16 16.3 15.3 16.5 17.1 17.2 16.1
June-16
EPA 8260
µg/L
1 5 µg/L Methylene Chloride 3.7
Field
feet
Static Water Level 34.65 7.68 36.15
Total Well Depth 60 20 48
mg/L
Oxygen, Dissolved 1.7 0.2 0.3
NTU
Turbidity 1.4 4.26 0.42
Std. Units
Field pH 5.4 6 5.6
mV
REDOX 242.6 212.4 257.5
umhos/cm
Field Specific Conductance 194.3 981 198.4
deg C
Field Temperature 22 15.9 17
May-16
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1080 115000 1800 48700 7620 2930 1630 15800 15200
EPA 6010
µg/L
6 1000 µg/L Antimony 4.7
10 10 µg/L Arsenic 3.3 5.2
100 700 µg/L Barium 228 324 278 210 55.9 129 38.3 197 292 103
1 4000 µg/L Beryllium 3.2
10 10 µg/L Chromium 2.6 3.2 5.1 9.1
10 1000 µg/L Cobalt 18 10.2 10.5 3.1
10 1000 µg/L Copper 2.8 16.4
300 300 µg/L Iron 78.8 4360 77200 1550 87.8 128 11800 29400
10 15 µg/L Lead 19.1
50 50 µg/L Manganese 7.2 10900 6800 515 28.8 2.9 6.3 530 1820
50 100 µg/L Nickel 17.9 3.2 4.7
10 20 µg/L Selenium 5.5
NE NE µg/L Sodium 13300 61500 2310 14500 13100 16400 8280 14200 10300 11200
100 2000000 µg/L Tin 3.1
25 300 µg/L Vanadium 4.2 4.2 20
10 1000 µg/L Zinc 17.8 5.2 34
EPA 7470
µg/L
0.2 1 µg/L Mercury 0.12
EPA 8081
µg/L
0.1 40 µg/L Endosulfan I 0.15
EPA 8260
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
15.58 20 60 50.85
1.34 4.6 4 3.19 3.25 1.91 2.81 6.33
2.97 7.23 1.95 44.5 19.33 34.84 13.52 6.16
5.9 5.7 5.6 6.4 6.4 6.5 6.5 7.2
175.1 241.4 270.5 177.6 14.7 -57 -23.6 -72.6
463.1 106.2 158.6 609.9 208.3 208.7 1006 549.9
16.7 16.4 17.1 15.2 17.2 21.5 15.6 17
169000 7280 63700 4320 17100 11400 16600
190 210 188 11 69.5 73.1 114 113
2.2 0.83
13.6
8.5 8.6
312 11000 312 227 5520 1510 3390 1520
8
90.8 284 21.6 116 465 317 2310 1930
5.5 6.4 2.7 2.5
19200 9420 15400 20100 13000 8420 14700 16900
2.5 2.8 2.8
22.6
40.5 5.9 7.2 9.6 7.3 6
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2
1 1 µg/L Benzene 1.7 0.26
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.77
5 1000 µg/L Dichlorodifluoromethane
5 500 µg/L m&p-Xylene 1.8
1 5 µg/L Methylene Chloride 2.3 4.4 3.4 2.9 3.2 9.5 1.1 2.8 1.4
NE NE µg/L o-Xylene 0.47
1 0.7 µg/L Tetrachloroethene 1.3
NS NS µg/L Tetrahydrofuran 49.6 3.5 13.5 6.1
1 3 µg/L Trichloroethene 0.71
1 2000 µg/L Trichlorofluoromethane 0.71 0.92 1.3
1 0.03 µg/L Vinyl chloride 0.72
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 54900 482000 87800 99000 30800 71700 24800 21200 29000 104000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 138000 769000 188000 241000 154000 137000 87000 103000 311000 236000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 9000 47700 2470 13800 15300 4430 1960 6850 9640 14500
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 5.1 4.7 4.2 4.3 4.1 4.1
December-15
Field
feet
Static Water Level 20.86
Total Well Depth 27
mg/L
Oxygen, Dissolved 1
NTU
Turbidity 7.8
Std. Units
Field pH 6
mV
REDOX -71.6
µmhos/cm
Field Specific Conductance 365.6
°C
Field Temperature 13.6
November-15
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1070 115000 2200 70300 7430 10100 1350 1110 63600 19100
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 207 279 271 184 92.7 140 34.4 186 241 97.2
1 4000 µg/L Beryllium 1.9
10 10 µg/L Chromium 3.5
10 1000 µg/L Cobalt 17.4 9.1 28.3 2.5 3.1 2.9
10 1000 µg/L Copper 6.2 6.3 2.8
300 300 µg/L Iron 82.8 3080 68200 312 32600 48.6 3690 34600
10 15 µg/L Lead 3.8 8.5
50 50 µg/L Manganese 2.8 9010 7100 407 1890 33.6 3.3 4 587 2020
50 100 µg/L Nickel 18 3.7 3.9
10 20 µg/L Selenium 5.6
NE NE µg/L Sodium 13200 61400 2590 23800 11300 15700 7940 14500 19800 12000
5.5 200 µg/L Thallium 8.8
100 2000000 µg/L Tin 8.5
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
0.7
3.6
2 1.6 2.4 2 3.1 1 1.2 2.3 6
12.4 27.3 3.7 3.2
1.4 1.1 5.1
55900 41000 50400 104000 27700 32300 161000 148000
382000 145000 85000 418000 118000 113000 231000 229000
26000 4590 3470 94000 26000 9720 10500 20300
4.7 6 5.6
70800 10100 1080 70000 4460 11600 27000 24900
2.6 4.5
95.7 71.5 183 74 65 70 152 115
0.68 0.63
5.4
7.1 3.9
523 790 466 8180 9830 2070 4160 2240
6
49.6 62.1 69.3 297 688 291 3860 2550
3.2 2.8 3.9 2.8
13700 12200 15800 21800 12800 11300 20900 20200
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
10 1000 µg/L Zinc 5.6 5.8 8.7 5.9 7.1 27.2
EPA 7470
µg/L
0.2 1 µg/L Mercury 0.12
EPA 8081
µg/L
0.1 40 µg/L Endosulfan I 0.17
0.05 0.008 µg/L Heptachlor 0.12
0.075 0.004 µg/L Heptachlor epoxide 0.093
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.91
1 6 µg/L 1,4-Dichlorobenzene 0.38
50 NE µg/L 2-Hexanone 0.69
100 NE µg/L 4-Methyl-2-pentanone (MIB 2.6
100 6000 µg/L Acetone 11.8
1 1 µg/L Benzene 1.5
5 70 µg/L Chloroform
1 3 µg/L Chloromethane 0.25
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.8
5 1000 µg/L Dichlorodifluoromethane 0.26 1 0.76
1 600 µg/L Ethylbenzene 0.4
5 500 µg/L m&p-Xylene 0.84 0.68
1 5 µg/L Methylene Chloride 1.3 2.3 3.9 1.2
NE NE µg/L o-Xylene 0.27 0.43
1 0.7 µg/L Tetrachloroethene 0.95
NS NS µg/L Tetrahydrofuran 35.8 7 17.7 120
1 600 µg/L Toluene 0.27
1 3 µg/L Trichloroethene 0.66
1 2000 µg/L Trichlorofluoromethane 1 1.4 1.1
1 0.03 µg/L Vinyl chloride 0.75
EPA 8270
µg/L
10 NE µg/L 2,4-Dinitrotoluene 5.9
10 NE µg/L 2,6-Dinitrotoluene 8.1
10 200 µg/L Benzo(g,h,i)perylene 1
10 0.005 µg/L Dibenz(a,h)anthracene 1
10 100 µg/L Di-n-octylphthalate 5.6
10 0.05 µg/L Indeno(1,2,3-cd)pyrene 1.1
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 78000 806000 137000 161000 104000 78000 79000 142000 403000 281000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 8510 48700 2990 16900 16200 6050 2040 4710 47400 14900
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 7.5 5.1 4.7 9.8 4.2
Field
feet
Static Water Level 72.25 16.3 43.76 20.31 23.2 76.9 36.73 107.71 24.15 7.17
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 2.2 2 0.2 3.3 5.9 0.7 4.4 6.3 0.2 0.1
NTU
Turbidity 1 5.6 3 9.6 1 1 1.6 2.6 295 9.3
Std. Units
Field pH 5.4 6.1 6.3 5.8 5.8 5.5 5.4 5.3 5.4 5.9
mV
REDOX 34.8 -35.2 -91.6 48.8 52.6 30.9 4 54.3 -77.7 -38.7
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
8.6 6.3 35.4 7.5
0.44
0.23 2.1
2 1.1
19.8 3.3
0.82 0.54 4.8
5.6
41000 37100 51500 103000 35100 43200 210000 187000
234000 110000 135000 362000 113000 105000 300000 267000
9000 3270 3930 113000 21600 12500 16300 19800
5.3 5 5.3
9.51 17.47 104.89 78.88
15.58 20 60 50.85
3.4 1.2 4.8 2.8 5.5 3.5 3.2 7.6
8.9 51.6 5.9 154.9 48.7 20.5 9.1 3.2
5.8 5.5 5.4 6.2 6.7 6.6 6.4 7
-23.3 5.2 49.6 34.8 -78.3 -84.6 -90 -87.1
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
µmhos/cm
Field Specific Conductance 163.2 1044 211.4 395.9 164.5 196.6 58.4 151.5 365.1 400.8
°C
Field Temperature 16 15.9 15.2 15.5 15.9 15.3 15.6 15.9 16.5 15.8
May-15
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1700 98400 3000 72700 8000 1850 1860 2030 8770 15300
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 164 287 214 306 54 122 30 182 660 93.7
1 4000 µg/L Beryllium 2.8
10 10 µg/L Chromium 4.8 6.7
10 1000 µg/L Cobalt 20.3 10.1 15.2 4.8 2.5
10 1000 µg/L Copper 6.3 3.8
300 300 µg/L Iron 9560 56000 292 113 54 3650 31400
10 15 µg/L Lead 3.3 2.7 11.6 2.9
50 50 µg/L Manganese 11900 7980 315 27.1 3.4 3.5 736 1990
50 100 µg/L Nickel 17 2.8 5.9
NE NE µg/L Sodium 11600 51400 23000 13100 16300 6940 14500 14100 9460
5.5 200 µg/L Thallium 5.1
25 300 µg/L Vanadium 11.4 8.8 4.3 4.9 3.2
10 1000 µg/L Zinc 8.7 7.5 6.8 21.2
EPA 7470
µg/L
0.2 1 µg/L Mercury 0.29
EPA 8151
µg/L
2 50 µg/L 2,4,5-TP (Silvex)0.14
2 70 µg/L 2,4-D 0.43
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.49 1.1
50 NE µg/L 2-Hexanone 0.96
100 NE µg/L 4-Methyl-2-pentanone (MIB 5.6
1 1 µg/L Benzene 1.7 0.29 0.46
5 70 µg/L Chloroform
1 3 µg/L Chloromethane 0.13
5 70 µg/L cis-1,2-Dichloroethene 0.73
1 600 µg/L Ethylbenzene 1
5 500 µg/L m&p-Xylene 1.5 1.2
1 5 µg/L Methylene Chloride 2.3 2.1
NE NE µg/L o-Xylene 0.4 0.85
1 0.7 µg/L Tetrachloroethene 1.2
NS NS µg/L Tetrahydrofuran 34.6 5.8 14.1 145
1 600 µg/L Toluene 0.63
1 3 µg/L Trichloroethene 0.79
1 2000 µg/L Trichlorofluoromethane 1.5 0.79 0.98
1 0.03 µg/L Vinyl chloride 0.7
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 39600 358000 107000 117000 28600 64100 20000 18900 47300 132000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 133000 632000 182000 304000 166000 145000 61000 134000 279000 239000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 7640 44200 2990 22200 15700 4340 1960 4290 51800 14400
Field
feet
Static Water Level 71.44 16.32 42.18 18.28 21.85 75.46 16.85 53.36 23.35 8.07
Total Well Depth 60 21 27 20 30 48 27 60 21 20
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
281.5 108.9 152.1 596.2 92.6 88.6 274.8 247.9
16.2 16.2 16.3 15.6 9.4 11.9 8.2 9
73600 9330 1790 65400 3690 7280 17000 23500
17
60.9 89.3 179 105 72.2 700 105 187
0.66 0.54 3.7
2.9 7.6 40.3 3.4
5.9 5.9
8.8 81.6 4.4
524 1400 695 10600 8870 226000 4940 9220
2.9 6.8 75 2.7
9.7 41.2 25.7 271 1160 1020 1420 5050
2.8 4.3 16.4 2.8 3.6
11200 10700 14500 20300 16000 8390 18200 23800
3.4 24.7 127 9.7 5.9
7.9 49 249 13.6
0.2
1.8 3.1
0.26
1.5 1.8
16.9 4.1
0.22 0.59 4.4
19200 36900 45200 91500 44500 33200 118000 242000
163000 107000 131000 360000 140000 125000 233000 371000
8070 3760 3510 98200 31500 4050 27000 19000
9.8 8.98 52.23 39.21
15.58 20 60 50.85
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
Turbidity 1.2 8.8 6.2 12.2 2.2 1.2 2.3 1.4 246.4 8
Std. Units
Field pH 5.5 6.1 6.1 5.9 5.9 5.6 5.7 5.5 5.2 6
mV
REDOX 265.1 15.4 -1.1 262.8 244.4 228.8 255.2 206.8 244.7 -34.3
µmhos/cm
Field Specific Conductance 153.1 985 363.4 422 175.1 194.8 50.9 148.3 297.2 407.8
°C
Field Temperature 18 13.7 15 13.3 14.7 16.7 16.1 17.5 17.1 13.4
November-14
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 1720 117000 3740 143000 8180 1360 2100 12800
EPA 6010
µg/L
10 10 µg/L Arsenic 2.6 3.5
100 700 µg/L Barium 142 339 221 305 58.2 111 38 193 262 96.8
1 4000 µg/L Beryllium 1.4
1 2 µg/L Cadmium
10 10 µg/L Chromium 3.4 4.8
10 1000 µg/L Cobalt 25 13.3 82 2.6
10 1000 µg/L Copper 9.6
300 300 µg/L Iron 85.8 2580 49700 126 221 76.5 529 55.9 1160 35700
10 15 µg/L Lead 2.7 4.1 3.6
50 50 µg/L Manganese 2.9 9880 9380 1040 2.6 22.9 19.9 7.6 130 2030
50 100 µg/L Nickel 25.9 7.2
10 20 µg/L Selenium
NE NE µg/L Sodium 10600 58300 2770 55400 13700 16600 7810 14600 6860 10000
25 300 µg/L Vanadium 2.8 2.7 5.6 3.6
10 1000 µg/L Zinc 16.8 7.2 5.3 6.2
EPA 7470
µg/L
0.2 1 µg/L Mercury 0.33
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.1 1.3
1 6 µg/L 1,4-Dichlorobenzene 0.4
100 NE µg/L 4-Methyl-2-pentanone (MIB 2.2
1 1 µg/L Benzene 2.5 0.42 0.44
10 3000 µg/L Chloroethane 2.1
5 70 µg/L cis-1,2-Dichloroethene 0.5 0.73 0.35
1 600 µg/L Ethylbenzene 0.73
5 500 µg/L m&p-Xylene 1.1 1.1
1 5 µg/L Methylene Chloride 3.7 2.9
NE NE µg/L o-Xylene 0.33 0.36 0.65
1 0.7 µg/L Tetrachloroethene 2
NS NS µg/L Tetrahydrofuran 79.2 15.9 8.8 106
1 3 µg/L Trichloroethene 0.85
1 2000 µg/L Trichlorofluoromethane 2.4 1.2 0.96
1 0.03 µg/L Vinyl chloride 1.2
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 120000 769000 191000 692000 163000 138000 64000 141000 86000 228000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 7090 49800 2940 50500 15500 4300 1350 3610 2220 15000
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 4.4 4.2 10.4 4.3 5.1
SM 4500-S2D
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
7.7 32.7 26.1 81.7 26.5 385.5 42.7 18.6
6 5.7 5.6 6.2 6.3 6.5 6.9 6.5
230.6 218.9 221.2 176 11 -79.4 -15.8 -25.5
234.3 115 150.1 611 228.7 185.9 364.2 603
14.9 18.7 17.1 17.3 20.4 19.7 17.5 18.2
32800 8660 43800 3130 5620 16800 17600
5.9 6.2
59.2 130 193 41.5 276 171 206 82.8
1.2 0.6 1.1 0.64
0.7
3 4.5 13 3.2
4.4 3.4
3.8 4.8 16.4 3.2
758 2720 2620 233 155000 75000 5270 638
5.4 18.3 7.4
199 55.6 120 33 1760 1010 5080 739
4.1 5.3 8.7 3.1 4.8
7
12800 10700 14400 24000 12500 17600 29900 17800
7.1 5.5 37 11.6
13.7 13.3 5.3 69.8 28
0.54
15.5 18.4 10.2
0.57 3.9 0.27
40500 36200 42300 54700 63700 2390 389000 140000
135000 119000 119000 464000 122000 117000 473000 222000
8240 5870 3720 146000 19500 28200 27000 24300
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
1000 NE µg/L Sulfide 260 130
Field
feet
Static Water Level 69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 1 0.5 6.3 0.5 5 0.5 2.3 8.3 0.5
NTU
Turbidity 1.7 3.53 5.2 10 3.6 1.2 9.1 2 98 9.9
Std. Units
Field pH 5.6 6.1 6 5.9 6 5.6 5.7 5.5 5.1 5.9
mV
REDOX 194 38 13 158 198 184 224 252 198 -61
µmhos/cm
Field Specific Conductance 138 1150 363 971 184 186 59 161 106 440
°C
Field Temperature 14.8 13.2 13.2 13.7 12.9 13.7 13 12.4 15.3 15.4
May-14
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 136000 4230 85200 8060 10700
EPA 6010
µg/L
6 1000 µg/L Antimony 5.4
10 10 µg/L Arsenic 8.9
100 700 µg/L Barium 124 324 205 264 54.4 90.8 30.7 168 132 94.3
10 10 µg/L Chromium 5.6
10 1000 µg/L Cobalt 22.8 46.6
300 300 µg/L Iron 52.9 1650 38200 123 33400
50 50 µg/L Manganese 7950 9260 641 6.1 15.5 10.9 1960
50 100 µg/L Nickel 20.6
10 20 µg/L Selenium 16.5 11.5
NE NE µg/L Sodium 10800 59700 39700 13600 14200 6160 12400 8490
10 1000 µg/L Zinc 11.4
EPA 7470
µg/L
0.2 1 µg/L Mercury 0.51
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 0.83 0.81
1 1 µg/L Benzene 1.8 0.28
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.38 0.37
1 5 µg/L Methylene Chloride 3.7
NE NE µg/L o-Xylene 0.31
1 0.7 µg/L Tetrachloroethene 1.8
NS NS µg/L Tetrahydrofuran 72.6 11.8 5.2 18.6
1 3 µg/L Trichloroethene 0.71
1 2000 µg/L Trichlorofluoromethane 3.7 0.62 0.47 0.2
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 91000 549000 187000 445000 167000 126000 50000 107000 63000 207000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5600 50500 3260 29700 13900 3600 1800 3610 1820 12400
Field
feet
Static Water Level 70.78 14.24 37.86 14.47 20.22 74.12 26.82 52.72 11.34 8.55
Total Well Depth 60 21 27 20 30 37.05 27 60 21 20
mg/L
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
151 142
10.76 18.48 103.8 79
15.58 20 60 50.85
0.5 0.5 3.8 1.25 0.5 2.11 4.5 8.18
5.2 152 7.8 20.1 363.9 136.9 16.6 28.3
5.9 5.6 5.6 6.2 6.1 6.3 6.6 6.7
101 232 242 182 7 -36 -45 27
203 120 159 647 247 324 885 344
15.4 13.8 11.9 16.7 10.8 11.2 12.5 10
48000 8680 59500 2820 12700 26300 23500
61.1 77.1 163 8.6 65.8 59.7 181 126
9 14.8
348 232 142 292 8210 2130 8890 2520
14.6 34.1 40.2 34.7 749 219 4320 2250
11000 11200 12800 24200 14500 9840 29900 24400
17.2 11.7
0.32
0.49
1.1
21.4 9.7 4.4
0.32 0.34 5.3
45500 46400 37400 96600 45200 41300 259000 158000
149000 113000 124000 373000 126000 120000 319000 257000
6180 3880 3630 83400 23700 10700 16900 30800
9.77 17.91 103.61 76.95
15.58 20 60 50.85
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
Oxygen, Dissolved 5.3 4.8 6.3 6.2 8.6 3.8 8.4 8.7 8.3 7.5
NTU
Turbidity 3 11 6 17 10 6 8 5 4 22
Std. Units
Field pH 5.6 5.8 6 5.7 5.7 5.3 5 5.2 5 6
mV
REDOX 411 243 146 374 389 363 389 436 436 27
µmhos/cm
Field Specific Conductance 137 1040 367 715 194 171 64 155 86 430
°C
Field Temperature 18.4 19.6 18.7 14.8 14.7 17.2 16 17.7 15 14.4
November-13
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 128000 3400 113000 8310 10400
EPA 6010
µg/L
100 700 µg/L Barium 106 311 201 296 53.9 98.8 25.4 170 112 87.8
10 1000 µg/L Cobalt 19.2 53.5 49.4 47.5
300 300 µg/L Iron 766 31300 89.5 136 136 84.3 32100
50 50 µg/L Manganese 8710 9990 688 19.4 6.8 6.9 7.9 1920
50 100 µg/L Nickel 27.1 5.3
NE NE µg/L Sodium 9940 46200 42600 13800 13000 5580 13500 9070
25 300 µg/L Vanadium 5.5
10 1000 µg/L Zinc 12.2
EPA 8151
µg/L
2 50 µg/L 2,4,5-TP (Silvex)0.23
2 70 µg/L 2,4-D 1.1
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.3 0.9
1 1 µg/L Benzene 1.9 0.27
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.41 0.54
5 1000 µg/L Dichlorodifluoromethane 0.28
1 5 µg/L Methylene Chloride 3
10 6 µg/L Naphthalene 0.86
NE NE µg/L o-Xylene 0.54
1 0.7 µg/L Tetrachloroethene 2.2
NS NS µg/L Tetrahydrofuran 99.6 11.7 13.7 5
1 3 µg/L Trichloroethene 0.89
1 2000 µg/L Trichlorofluoromethane 12 0.47 0.69 0.33
1 0.03 µg/L Vinyl chloride 0.95
EPA 8270
µg/L
10 40 µg/L 3&4-Methylphenol(m&p Cre
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 28100 349000 155000 224000 31700 51600 19700 18400 26700 161000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 103000 654000 193000 496000 154000 116000 61000 124000 66000 236000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5880 56700 3620 36500 15200 5160 1510 3950 1790 14000
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 7.1 5.9
Field
feet
Static Water Level 71.87 16.65 45.08 18.63 22.73 76.44 36.08 106.03 24.77 9.1
Total Well Depth 60 21 27 20 30 48 27 60 21 20
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
8.4 6.8 8.1 5.4 5.5 7.3 2.9 7
15 147 118 50 51 23 14 33
5.9 5.6 5.5 6.3 6.4 6.8 6.5 6.8
315 367 437 406 284 252 127 262
243 149 156 623 205 183 649 478
15 16.6 17.7 17.8 21.2 19.7 18.9 19.3
27400 9360 53200 2190 5490 62500 23000
47.6 106 140 23.8 71.1 50.1 348 101
14.4
253 1330 915 239 22800 3360 11700 1790
86.1 48.8 110 14 1530 152 8930 1080
12
10500 11700 12300 25300 13000 10300 41100 20100
9.8
17.1 10.8
0.88
0.77
14.7 18.9
7.6 0.25
3.6
39300 43200 32800 64300 72700 48900 516000 152000
126000 114000 123000 410000 125000 114000 705000 270000
6230 5700 4100 124000 18100 11600 34800 31000
6 5.2
10.56 18.83 104.66 79.28
15.58 20 60 50.85
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
Oxygen, Dissolved 8.7 0.9 0.7 7.5 5.6 0.5 10.2 9.2 2.2 0.5
NTU
Turbidity 1 3 1 12 3 2 5 11 4 8
Std. Units
Field pH 5.6 5.6 5.9 5.8 5.9 5.5 5.4 5.2 5.2 5.9
mV
REDOX 228 68 -8 207 239 200 357 363 327 -66
µmhos/cm
Field Specific Conductance 104 840 316 678 168 144 48 138 63 385
°C
Field Temperature 18.3 13.8 15.9 17.2 17.4 16.5 15.1 16.3 16.7 16.7
May-13
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 115000 5070 97600 11200 2100 3200 11000
EPA 6010
µg/L
100 700 µg/L Barium 109 324 216 375 57.7 115 28.5 174 115 87
1 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 18.2 64.1 35.3 65.1
10 1000 µg/L Copper
300 300 µg/L Iron 877 34100 158 126 61.5 867 92.8 30700
10 15 µg/L Lead
50 50 µg/L Manganese 7880 9630 496 24.9 16.6 1890
50 100 µg/L Nickel 20.7
NE NE µg/L Sodium 9080 45700 42600 13000 14300 6120 12900 8290
100 2000000 µg/L Tin 5.8
25 300 µg/L Vanadium
10 1000 µg/L Zinc 21.1 10.5 13.6
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2 0.84
50 NE µg/L 2-Hexanone 0.48
100 6000 µg/L Acetone 20.3
1 1 µg/L Benzene 1.4
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.72
5 500 µg/L m&p-Xylene 0.96
1 5 µg/L Methylene Chloride 4.2
10 6 µg/L Naphthalene 1.3
NE NE µg/L o-Xylene 0.54 0.27
1 0.7 µg/L Tetrachloroethene 1.5
NS NS µg/L Tetrahydrofuran 111 8.5 24.2
1 3 µg/L Trichloroethene 0.68
1 2000 µg/L Trichlorofluoromethane 12.1 0.25 0.36 0.38
5 500 µg/L Xylenes (Total)1.2
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 29800 363000 175000 203000 34800 63500 22800 21700 32100 189000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 84000 589000 175000 413000 131000 108000 51000 100000 46000 228000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5910 50000 3860 33700 16200 5340 2070 4300 2040 14200
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 8.1 5
Field
feet
Static Water Level 73 15.54 21.94 17.53 21.44 38.62 31.43 106.24 23.65 8.13
Total Well Depth 60 21 27 20 30 48 27 60 21 20
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
6.5 1.3 6.5 2.8 3 4 2.5 4.3
9 123 250 21 35 2 57 4
5.8 5.4 5.4 6.2 6.2 6.7 6.2 6.8
189 280 355 241 -31 -12 -15 61
153 115 123 614 246 134 899 369
17.1 14.8 16.7 17 13.7 12.7 15.1 12.8
51800 7820 41200 2700 5090 20100 13200
50.1 176 254 59.6 58.9 51.7 185 106
2.4
7.1 6.6
6.6 14.6 25.3 10.4
7.6 9.5
324 8610 5820 4140 6900 1400 9560 4180
6.5
13.2 158 240 160 855 153 3990 1650
8.6
11100 19100 13500 26700 12400 9160 25000 18200
14.6 9.9 8.6
37.3 27.4 22.7
0.63
7.4 5.1
4.3
29600 58700 35600 78900 58000 48600 293000 147000
138000 87000 102000 442000 104000 91000 327000 255000
5820 3820 4290 124000 20600 10800 20000 26900
9.59 17.62 104.48 78.61
15.58 20 60 50.85
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
Oxygen, Dissolved 8.3 1.9 6 2.7 7.1 0.9 7.2 7.4 3.1 6.4
NTU
Turbidity 1 1 1 36 1 1 1 44 1 6
Std. Units
Field pH 5.6 5.8 5.8 5.6 6 5.3 5.5 5 5.2 6.2
mV
REDOX 263 10 21 246 274 211 260 282 267 -22
µmhos/cm
Field Specific Conductance 68 802 217 382 116 106 31 88 43 400
°C
Field Temperature 20.9 19.7 15.7 15.6 15.2 16.3 17.5 18.1 16.3 14.7
November-12
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 79500 5420 73600 8400 2090 10400
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 91.7 335 173 400 53.4 95.1 26.9 142 101 76.8
1 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 15.2 35.5
10 1000 µg/L Copper
300 300 µg/L Iron 1730 25300 344 102 60.8 218 29000
10 15 µg/L Lead
50 50 µg/L Manganese 8400 11600 541 17.4 5.1 1740
50 100 µg/L Nickel 21.8
NE NE µg/L Sodium 9180 43400 43600 14500 13900 6980 13100 5280 8770
25 300 µg/L Vanadium
10 1000 µg/L Zinc 24.5 15.2 92
EPA 8081
µg/L
0.1 0.1 µg/L 4,4'-DDD
0.002 0.002 µg/L Dieldrin 0.11
0.1 42 µg/L Endosulfan II 0.12
0.1 2 µg/L Endrin 0.27
0.1 2 µg/L Endrin aldehyde 0.23
0.075 0.004 µg/L Heptachlor epoxide 0.12
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2 1.2
1 1 µg/L Benzene 1.3
10 3000 µg/L Chloroethane 1.3
5 70 µg/L Chloroform 0.16
5 70 µg/L cis-1,2-Dichloroethene 0.25 0.62
5 1000 µg/L Dichlorodifluoromethane 0.28
1 5 µg/L Methylene Chloride 4.5
10 6 µg/L Naphthalene 1.6
NE NE µg/L o-Xylene 0.63
1 0.7 µg/L Tetrachloroethene 1.8
NS NS µg/L Tetrahydrofuran 93.2 13.5 26
1 3 µg/L Trichloroethene 0.77
1 2000 µg/L Trichlorofluoromethane 16.9 0.29 0.49 0.49
5 500 µg/L Xylenes (Total)0.98 0.79
EPA 8270
µg/L
10 0.05 µg/L Benzo(a)anthracene 1.4
15 3 µg/L bis(2-Ethylhexyl)phthalate 2.4 1.1 1 13
10 5 µg/L Chrysene 1.5
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 26300 277000 142000 174000 31200 51900 19500 17200 25500 153000
SM 2540C
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
9.3 1.3 6.4 2.5 5 9.5 1.9 5.8
5 587 446 190 45 11 13 15
5.8 5.6 5.5 6.1 6.4 7 6.3 6.9
185 204 254 224 -13 -10 -53 -31
197 136 81 403 208 144 575 367
14.7 16.5 18.2 17.9 22.4 23 22.4 23.3
24200 9770 35600 2090 4240 36400 32300
7.1
50.5 279 160 143 63.3 46.5 315 151
3.5
11.8 6 6.7
13
6.9 5.8 10.5
1430 11300 4520 12300 25500 1280 16500 1640
7.5 9.5
33.6 301 251 317 1720 106 5200 2430
13.7
11000 14600 15000 21200 15500 9990 33800 29000
18.7 8 28.6
30.8 51 23 45.6
0.062 0.079 0.11
0.071
0.08
0.34
0.49
6.3 4.8
8.1
9.8
40200 43900 28900 77600 79700 44700 317000 220000
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
µg/L
NE 500000 µg/L Total Dissolved Solids 95000 564000 172000 435000 157000 111000 58000 118000 63000 220000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5320 64000 3920 34500 16100 3810 1860 3560 1800 12900
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 9.1
SM 4500-S2D
µg/L
1000 NE µg/L Sulfide
Field
feet
Static Water Level 72.24 17.78 45.36 19.26 22.81 77.49 37.56 105.53 25.13 8.94
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 5.5 1.5 1.2 2.3 6.4 1.8 9.8 7.3 4.4 0.9
NTU
Turbidity 1 1 25 14 14 7 1 1 1 25
Std. Units
Field pH 5.7 5.8 5.6 5.7 5.8 5.4 5.7 5.5 5 6.1
mV
REDOX 236 77 16 181 245 197 260 352 366 -61
µmhos/cm
Field Specific Conductance 100 842 283 655 175 147 49 134 63 354
°C
Field Temperature 16 14 15.2 13.3 15.9 14.5 15.6 16 16.3 16
April-12
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 95000 6860 98700 7910 9700
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 93.8 366 228 407 57.5 100 27.5 142 96.5 70.3
1 4000 µg/L Beryllium
10 10 µg/L Chromium 5.2
10 1000 µg/L Cobalt 14.8 16.4 21.5
300 300 µg/L Iron 3190 41500 145 209 57.8 55.1 26300
10 15 µg/L Lead
50 50 µg/L Manganese 8280 9310 370 10.2 1580
50 100 µg/L Nickel 22.3
10 20 µg/L Silver 5.2
NE NE µg/L Sodium 9440 38400 40400 14200 13700 6250 12600 7460
25 300 µg/L Vanadium
10 1000 µg/L Zinc 35.2
EPA 8081
µg/L
0.1 0.1 µg/L 4,4'-DDD 0.13
0.1 0.1 µg/L 4,4'-DDT 0.54 0.14 0.05
0.05 2 µg/L Aldrin 0.12
0.05 0.006 µg/L alpha-BHC 0.12
0.05 0.019 µg/L beta-BHC 0.1
0.05 0.019 µg/L delta-BHC 0.18 0.069
0.002 0.002 µg/L Dieldrin 0.081
0.1 42 µg/L Endosulfan II
0.1 2 µg/L Endrin aldehyde 0.28
0.05 0.008 µg/L Heptachlor 0.48
0.075 0.004 µg/L Heptachlor epoxide 0.066
1 40 µg/L Methoxychlor 0.83
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.1 1.2
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
127000 144000 127000 298000 131000 101000 432000 349000
4900 6150 4790 143000 19700 10300 24300 28800
106 100
10.71 18.71 104.68 79.91
15.58 20 60 50.85
3 2.3 6.4 2.3 8.7 6.7 2.1 6.7
1 605 329 456 3 1 14 92
5.9 5.5 5.5 6.5 6.1 6.7 6.2 6.8
150 246 365 160 -21 -21 -26 83
158 136 137 434 261 135 700 523
16.1 15.8 15.8 15.5 14.7 12.7 10 12.4
20500 9420 25800 6180 26400 23600
5.7
46.9 144 122 115 70.4 53.4 179 136
1.4
7.2
5.5
539 3760 1140 10000 11400 1720 9370 2140
7.6
15.7 91.5 170 327 1040 157 3760 2420
12.5
11600 16700 14300 16300 14300 9890 21300 20000
7.2 23.4
20 51.1
0.062
0.09 0.054
0.085 0.066
0.061
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
5 350 µg/L 1,1-Dichloroethene 36.6
1 1 µg/L Benzene 1.5
5 70 µg/L Chloroform
5 70 µg/L cis-1,2-Dichloroethene 0.33 0.5
1 5 µg/L Methylene Chloride 3.2
10 6 µg/L Naphthalene 1.9
NE NE µg/L o-Xylene 1
1 0.7 µg/L Tetrachloroethene 1.7
NS NS µg/L Tetrahydrofuran 152 8.8 18.9 4.4
1 3 µg/L Trichloroethene 0.82
1 2000 µg/L Trichlorofluoromethane 20.9
5 500 µg/L Xylenes (Total)1.6
EPA 8270
µg/L
20 NE µg/L 3,3'-Dichlorobenzidine
10 NE µg/L 3-Methylcholanthrene
10 0.05 µg/L Benzo(a)anthracene
10 0.005 µg/L Benzo(a)pyrene
10 0.05 µg/L Benzo(b)fluoranthene
10 200 µg/L Benzo(g,h,i)perylene 1.3
10 0.5 µg/L Benzo(k)fluoranthene
15 3 µg/L bis(2-Ethylhexyl)phthalate 5.5
10 5 µg/L Chrysene
10 0.005 µg/L Dibenz(a,h)anthracene
10 0.05 µg/L Indeno(1,2,3-cd)pyrene
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 27100 196000 150000 64300 134000 50200 20100 20100 413000 120000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 93000 531000 168000 374000 149000 109000 52000 123000 49000 161000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 5350 61500 33200 16100 10800
SM 4500-CN-E
µg/L
10 70 µg/L Cyanide 6.5
SM 4500-S2D
µg/L
1000 NE µg/L Sulfide
Field
feet
Static Water Level 36.43 7.99 21.01 8.24 10.55 38.23 15.03 52.4 11.92 4.13
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 5 2.9 0.8 0.7 8.7 0.8 6.7 7.2 4.8 0.5
NTU
Turbidity 1 4 3 7 2 1 7 2 2 14
Std. Units
Field pH 5.2 5.8 5.8 5.5 5.4 5.5 5.5 5.2 5.2 5.5
mV
REDOX 166 43 -24 156 189 185 176 180 196 -78
µmhos/cm
Field Specific Conductance 102 809 329 568 182 149 52 140 66 325
°C
Field Temperature 16.7 15.2 13.8 13 13.9 14.7 14.4 16 14.5 14.2
December-11
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 61800 7020
EPA 6010
µg/L
100 700 µg/L Barium 82.6 328 85.2
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
3.1
0.25
1.4 0.97
4.5
7.3 1.4
3.6
2.9
1.1
1.1 2.5
1 2.8
1.2 1.5 1.8
2.5
1.1
1.1
1.2 2.1
1.2 1.5 2.2
37200 52200 30100 75300 47200 44200 221000 158000
130000 110000 145000 260000 98000 101000 329000 272000
8200 5380 60600 25300 11300 22800 30900
178
5.04 8.92 52.03 39.39
15.58 20 60 50.85
5.4 1.6 6.9 2.5 7.1 8.5 4.1 7.7
8 150 32 112 21 16 12 10
6.1 5.9 5.8 6.4 6.5 7.1 6.4 6.5
166 189 177 121 -6 -36 -62 -23
176 144 150 404 194 142 570 454
15.1 15 16.4 16.7 19.9 18 18.5 18.9
19800 19500
123 105
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
10 10 µg/L Chromium 14.7
10 1000 µg/L Cobalt 15
300 300 µg/L Iron 368 3540
50 50 µg/L Manganese 257 43.5
NE NE µg/L Sodium 7670 35300 13300
25 300 µg/L Vanadium 13
10 1000 µg/L Zinc 15.3
EPA 8260
µg/L
5 350 µg/L 1,1-Dichloroethene
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 27500 143000 32800
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 95000 345000 139000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 29200 16400
Field
feet
Static Water Level 36.8 9.33 11.2
Total Well Depth 60 20 30
mg/L
Oxygen, Dissolved 5.4 2.3 6.2
NTU
Turbidity 2 40 90
Std. Units
Field pH 5.8 5.9 5.7
mV
REDOX 218 175 200
µmhos/cm
Field Specific Conductance 97 490 177
°C
Field Temperature 15.4 12.5 15.2
November-11
EPA 300.0
µg/L
250000 250000 µg/L Sulfate 96300 7590
EPA 6010
µg/L
100 700 µg/L Barium 351 237 97.1 24.4 141 91.3 57.5
1 4000 µg/L Beryllium
10 10 µg/L Chromium
10 1000 µg/L Cobalt 11.8
10 1000 µg/L Copper
300 300 µg/L Iron 2980 40300 151 424 23000
10 15 µg/L Lead
50 50 µg/L Manganese 7920 7310 12.7 7 6.8 1250
50 100 µg/L Nickel 20.9
10 20 µg/L Silver 5
NE NE µg/L Sodium 31800 12000 5410 11900 6480
25 300 µg/L Vanadium
10 1000 µg/L Zinc 33.3 45.4
EPA 8260
µg/L
5 6 µg/L 1,1-Dichloroethane 1.2 1.9
5 350 µg/L 1,1-Dichloroethene 38.7
100 6000 µg/L Acetone 3.7
1 1 µg/L Benzene 2
5 70 µg/L Chloroform 0.26
5 70 µg/L cis-1,2-Dichloroethene 0.46 0.67
5 500 µg/L m&p-Xylene 0.66
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
3230 1060
1890 1290
18500 17900
0.58
160000 131000
237000 234000
20900 23600
5.1 8.3
14 7
6.4 6.7
-1 66
415 370
11.4 11.5
15300 9460 38300
60.1 139 143 42.5 81
2.3
5.5
6.1
3030 6140 2050 2290 4170
6.4
58.3 140 71 130 280
9980 20200 12700 9390 8650
10.8 7.5
31.6 12 13.5
2.2 4 6.6 5.5
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
1 5 µg/L Methylene Chloride 3.5
NE NE µg/L o-Xylene 1.2
1 0.7 µg/L Tetrachloroethene 1.8
NS NS µg/L Tetrahydrofuran 197
1 3 µg/L Trichloroethene 0.88
1 2000 µg/L Trichlorofluoromethane 20.1 0.34 0.42 0.68
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 219000 155000 47700 19600 17400 21700 122000
SM 2540C
µg/L
NE 500000 µg/L Total Dissolved Solids 498000 180000 124000 81000 128000 89000 165000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 62400 8480
Field
feet
Static Water Level 36.52 16.58 44.06 9.04 11.1 77.6 17.03 52.19 12.24 7.38
Total Well Depth 21 27 48 27 60 21 20
mg/L
Oxygen, Dissolved 1.7 3.1 4 5.8 6.8 4.5 0.6
NTU
Turbidity 1 4 3 4 1 2 37
Std. Units
Field pH 5.9 6 5.8 5.6 5.6 5.6 6.3
mV
REDOX 95 71 207 206 205 223 -148
µmhos/cm
Field Specific Conductance 762 306 158 48 141 58 289
°C
Field Temperature 12.7 13.8 12.3 15.2 14.9 14.2 13.5
June-11
EPA 350.1
µg/L
NS NS µg/L Nitrogen, Ammonia 0.12
EPA 6010
µg/L
NE NE µg/L Sodium 27200
EPA 8260
µg/L
1 1 µg/L Benzene 1.6
1 0.7 µg/L Tetrachloroethene 1.6
NS NS µg/L Tetrahydrofuran 274
RSK 175
µg/L
NS NS µg/L Methane 1280
SM 2320B
µg/L
NE NE µg/L Alkalinity, Total as CaCO3 165000
SM 4500-Cl-E
µg/L
NE 250000 µg/L Chloride 39900
Field
feet
Static Water Level 8.31
Total Well Depth 21
mg/L
Oxygen, Dissolved 4.2
NTU
Turbidity 3
Std. Units
Field pH 5.8
mV
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
3.2
40200 44500 30400 19600 26100
124000 159000 138000 140000 189000
8030 19100 10900
9.19 17.83 52.08
15.58 20 60
2 6.9 6.2 7.7 7.3
54 223 154 36 103
6 5.9 5.8 6.4 6.6
216 239 218 112 88
155 127 139 116 177
13 13.3 14.3 10.9 11.5
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
10 10 µg/L Chromium 1.4 5.4 1.3 7.6 0.96 0.63
10 20 µg/L Silver 0.51 2.5 0.6 0.88 0.57 0.84 0.1 0.43 0.12 1.2
EPA 8260
µg/L
1 200 µg/L 1,1,1-Trichloroethane 0.82
5 6 µg/L 1,1-Dichloroethane 1.1 3.8
100 6000 µg/L Acetone 3.8
1 1 µg/L Benzene 1.3
5 70 µg/L Chloroform 0.36
1 3 µg/L Chloromethane 0.15
5 70 µg/L cis-1,2-Dichloroethene 0.26 0.71
5 500 µg/L m&p-Xylene 0.74 1.4
1 5 µg/L Methylene Chloride 4.1
NE NE µg/L o-Xylene 0.84 0.39
1 0.7 µg/L Tetrachloroethene 1.4
NS NS µg/L Tetrahydrofuran 226 12.1
1 3 µg/L Trichloroethene 0.65
1 2000 µg/L Trichlorofluoromethane 31.6 0.48 0.26 0.52
Field
feet
Static Water Level 35.93 8.17 20.56 8.34 10.44 37.99 15.08 51.11 11.72 4
Total Well Depth 60 21 27 20 19.56 48 27 60 21 20
mg/L
Oxygen, Dissolved 6.3 3.9 6.3 5.3 9 3.2 8.7 7.3 7.1 4.3
NTU
Turbidity 55 57 70 96 85 40 18 1 4 23
Std. Units
Field pH 5.8 5.9 6.2 5.7 6.1 5.6 5.1 5.6 5.5 6.2
mV
REDOX 263 71 -43 271 141 245 272 265 279 -36
µmhos/cm
Field Specific Conductance 110 687 409 174 208 193 10 153 55 321
°C
Field Temperature 17 16 14.6 14.3 15.5 16.2 16.6 18.7 16.6 15.6
November-10
EPA 6010
µg/L
100 700 µg/L Barium 85.4 223 302 335 53 100 26.8 157 38.9 48.1
10 10 µg/L Chromium 0.96 0.49 0.68 5.8 0.55 0.62
10 15 µg/L Lead
10 20 µg/L Silver 0.85 1.3 0.16 0.23
EPA 8260
µg/L
1 5 µg/L Methylene Chloride 4.2
1 2000 µg/L Trichlorofluoromethane 36.1
Field
feet
Static Water Level 35.62 8.39 19.97 8.49 10.5 37.48 16.12 50.02 12.04 4.03
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 6.8 4.3 4.8 3.6 8.1 4 7.9 7.8 7.8 5.1
NTU
Turbidity 3 6 99 40 3 1.5 1 1 0.5 80
Std. Units
Field pH 5.13 5.05 5.22 6.16 5.13 5.81 5.56 5.38 5.31 5.91
mV
REDOX 282 99 -14 260 212 261 329 334 329 -27
µmhos/cm
Field Specific Conductance 109 543 369 562 204 191 60 193 42 267
°C
Field Temperature 16.8 16.3 15.9 16.4 16.2 15.1 17.5 16.2 18.5 17
April-10
EPA 8260
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
2.6 3.9 1.8
0.7 0.72 0.74 0.4 0.2
0.21 0.24
18.6
4.91 8.85 51.45
15.58 20 60
7.4 5.2 7.8 6.6 9.1
25 177 39 50 52
6 5.6 5.5 6.4 6.5
188 245 272 -15 23
179 171 140 295 129
15 15 17.1 19.7 18.6
44.9 176 129 61.9 57.6
1.1 4 2.3
4.3
4.97 9.04 51
15.58 20 60
4.9 5.2 7.7 6.7 8.8
7 200 24 7 8
5.82 5.45 5.42 6.37 6.09
183 251 335 9 60
183 168 167 307 183
18.1 17.2 17.2 14 13.4
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
1 2000 µg/L Trichlorofluoromethane 21.9
Field
feet
Static Water Level 7.15
Total Well Depth 21
mg/L
Oxygen, Dissolved 2.7
NTU
Turbidity 2
Std. Units
Field pH 5.46
mV
REDOX -7
µmhos/cm
Field Specific Conductance 255
°C
Field Temperature 14.3
March-10
EPA 6010
µg/L
10 10 µg/L Arsenic 4 4.2 3.4
100 700 µg/L Barium 85.3 103 314 55.9 54.3 99.3 28.8 134 46.6 37.6
1 2 µg/L Cadmium 0.82
10 10 µg/L Chromium 1.4 1.2 1.3 5 1.4
10 20 µg/L Silver 0.29 0.67 0.45 0.46 0.56 0.27 0.48
EPA 8260
µg/L
1 2000 µg/L Trichlorofluoromethane 22.2
Field
feet
Static Water Level 36.62 7.16 18.22 8.22 9.99 38.71 13.23 51.31 11.18 3.55
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 5.9 4.8 3.7 4.4 6.1 2.2 7.2 8.5 7.4 1.9
NTU
Turbidity 2 4 6 45 3 2 7 6 2 13
Std. Units
Field pH 5.74 5.31 5.61 5.56 5.96 5.55 5.21 5.32 5.18 5.97
mV
REDOX 262 191 31 262 260 213 303 309 300 -60
µmhos/cm
Field Specific Conductance 90 230 330 90 170 160 60 140 40 190
°C
Field Temperature 20.7 14.8 16.4 14.6 19.2 16.8 13.7 14.6 17.1 13.4
November-09
Field
feet
Static Water Level
Total Well Depth
mg/L
Oxygen, Dissolved
NTU
Turbidity
Std. Units
Field pH
mV
REDOX
µmhos/cm
Field Specific Conductance
°C
Field Temperature
September-09
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
2.7 3.7
40.6 126 130 92.5 59.4
2.4 1.7 3
0.2 0.4 0.39 0.28 0.2
4.15 8.05 51.21
15.58 20 60
6.8 5.4 7.9 6.8 8.8
31 11 29 8 13
5.73 5.5 5.35 7.05 6.77
197 237 292 53 82
140 120 150 230 170
13 13.6 14.4 17.1 17.9
8.55
20
2.6
65
5.23
386
105
15.9
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
EPA 6010
µg/L
100 700 µg/L Barium 92.8 80.7 289 334 66.8 104 27.2 128 39.1 31.8
10 10 µg/L Chromium 2 5.4 8.6 0.65
10 15 µg/L Lead 4.8
10 20 µg/L Silver 0.48 0.68 1 2.4 0.6 0.88 0.16 0.32 0.19 0.5
EPA 7470
µg/L
0.2 1 µg/L Mercury
EPA 8260
µg/L
5 350 µg/L 1,1-Dichloroethene
100 700 µg/L Carbon disulfide 26.1 12.5 13
1 5 µg/L Methylene Chloride
1 2000 µg/L Trichlorofluoromethane
Field
feet
Static Water Level 37.16 8.89 22.73 9.59 11.33 39.87 16.7 51.52 12.36 4.48
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 3.6 1 0.5 1.8 6.3 1 5.4 6.1 6.9 1
NTU
Turbidity 38 12 40 247 62 21 27 28 2 13
Std. Units
Field pH 5.61 5.65 5.88 5.77 6.11 5.47 5.43 5.45 5.35 6.15
mV
REDOX 334 175 37 259 362 292 342 353 371 -22
µmhos/cm
Field Specific Conductance 107 228 366 391 195 170 60 141 42 171
°C
Field Temperature 18.1 18.8 17.6 19.2 16.6 18.9 16.1 16.9 18.9 19.3
March-09
EPA 6010
µg/L
100 700 µg/L Barium 74.3 88.5 252 58.3 52.6 86.9 25 173 38.9 28.4
10 10 µg/L Chromium 0.88 1.6 1.2 5.2 0.78 7.6 0.65
10 20 µg/L Silver 0.58 0.29 0.28 0.42 0.18
EPA 8260
µg/L
100 700 µg/L Carbon disulfide 3.3
Field
feet
Static Water Level 38.27 8.14 22.29 10.07 11.14 40.61 15.86 52.36 11.7 3.73
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 4.5 2.6 1.3 4.9 6.6 0.9 7.8 6.4 7.2 2.4
Std. Units
Field pH 5.7 5.59 5.92 5.51 6.01 5.62 5.38 5.37 5.58 5.84
mV
REDOX 585 198 1 433 517 355 523 466 353 -122
µmhos/cm
Field Specific Conductance 94 222 349 60 175 152 54 115 37 137
°C
Field Temperature 15.4 13 14.7 11 13.6 15 14.8 15.5 13.9 13.5
December-08
EPA 6010
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 85 98.8 231 263 56.1 99 32.8 124 41.9 28.6
10 10 µg/L Chromium 0.64 0.5 0.58 5.3 0.91 0.97 0.47
10 15 µg/L Lead
10 20 µg/L Selenium 11.8 8.7
10 20 µg/L Silver 0.62 1.2 1.5 2.6 0.78 0.96 0.15 0.36 0.79
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
38 117 242 77.7 52.1
0.8 10.7
7.2 17.5
0.39 0.41 0.54 0.62 0.36
0.081
19.8
2.6
18.6
4.85 9.35 51.28
15.58 20 60
2.4 4.1 6 0.6 8.4
19 63 598 65 30
5.83 5.56 5.53 6.16 6.55
197 290 364 28 111
139 124 147 255 148
19.5 17.9 16.8 19.8 20.9
34.5 79.2 97.9 45.6 46.3
2 1.6 0.4 0.61 0.42
4.13 8.34 51.52
15.58 20 60
7.1 4.2 8.3 6.4 8.6
5.79 5.4 5.5 6.07 7.01
181 241 390 53 117
114 89 140 146 126
12.4 12.8 15 15.5 15.9
7.3
57.9 88.7 583 78.2 50.6
2.2 40.2 0.67
26.2
0.37 0.44 0.46 0.39 0.5
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
EPA 8260
µg/L
5 70 µg/L Chloroform 3.4
Field
feet
Static Water Level 38.39 9.13 22.72 11.18 11.78 40.61 17.8 52.11 12.33 4.24
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 4.43 0.64 0.62 0.81 6.83 1.88 6.01 6.19 6.73 0.35
Std. Units
Field pH 5.79 5.76 5.79 5.88 6.08 5.64 5.85 5.7 5.73 6.33
mV
REDOX 217 185 45 178 197 220 199 203 222 -79
µmhos/cm
Field Specific Conductance 93 218 268 422 176 152 53 117 35 133
°C
Field Temperature 14.8 13.3 14.6 14.7 15 12.8 15.3 15 15.6 14.7
March-08
EPA 6010
µg/L
100 700 µg/L Barium 90.3 102 293 172 57.5 95.7 24 124 42 29.2
10 10 µg/L Chromium 0.49 0.79 0.63 0.4 5.6 7.3 0.42
10 20 µg/L Selenium 4.9
10 20 µg/L Silver 0.43 0.93 0.87 0.94 0.56 0.66 0.13 0.22 0.41
EPA 7470
µg/L
0.2 1 µg/L Mercury 0.1
EPA 8260
µg/L
100 4000 µg/L 2-Butanone (MEK)
100 6000 µg/L Acetone
Field
feet
Static Water Level 38.28 8.83 22.71 10.49 11.13 40.6 15.22 51.33 11.77 4.08
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 4.61 1.46 3.08 3.69 6.77 3.04 6.44 7.8 7.08 0.33
Std. Units
Field pH 6.04 6.14 6.08 6.75 6.56 5.84 7.39 5.66 6.81 7.12
mV
REDOX 56 29 -43 24 33 52 50 191 123 -172
µmhos/cm
Field Specific Conductance 91 234 258 254 172 141 51 123 36 125
°C
Field Temperature 16.62 16.47 14.41 11.87 14.15 15.59 14 17.68 14.52 13.95
November-07
(blank)
µg/L
100 6000 µg/L Acetone
100 700 µg/L Barium 105 107 273 287 70.6 101 26.6 117 40.8 23.1
10 10 µg/L Chromium 8.4
0.2 1 µg/L Mercury
10 20 µg/L Selenium 18.1
10 20 µg/L Silver 0.16 0.32 0.39
Field
feet
Static Water Level 38.12 9.32 22.72 10.65 11.65 40.4 16.78 50.38 12.34 4.33
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 5.08 0.72 1.69 1.32 6.5 0.85 7.12 7.32 6.59 1.02
Std. Units
Field pH 6.52 6.67 6.21 6.35 7 6.07 6.27 5.73 5.95 6.67
mV
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
4.51 8.91 51.81
15.58 20 60
2.52 4.2 6.68 5.58 8.4
5.98 5.68 5.81 5.04 6.19
-30 190 215 145 88
118 84 135 196 130
14.3 14.5 14.8 8.1 7
60.5 64.6 186 79.7 50.6
1.8 1.1 4.1 1.2
0.15 0.21 0.56 0.37 0.26
0.26
4.6
15
4.47 8.78 51.11
15.58 20 60
5.27 5.85 6.69 7.5 7.28
7.22 6.45 5.82 7.69 8.54
18 74 124 197 195
99 72 136 194 122
12.86 15.63 16.47 14.74 13.5
22.7
47.3 85.6 130 70.3 49.4
1.7 0.61
0.098
0.26 0.48 0.51 0.26
4.95 9.27 50.78
15.58 20 60
2.01 5.16 7.33 5 6.93
6.48 6.83 5.82 6.18 7.35
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
REDOX 59 61 66 43 61 53 66 56 73 -80
µmhos/cm
Field Specific Conductance 85 176 217 394 161 126 51 121 36 121
°C
Field Temperature 15.42 14.08 13.22 16.04 14.9 14.16 15.48 15.75 16.38 16.33
April-07
(blank)
µg/L
100 4000 µg/L 2-Butanone (MEK)
10 10 µg/L Arsenic
100 700 µg/L Barium 81 79 310 200 58 89 30 140 52 25
10 10 µg/L Chromium 6.4
10 15 µg/L Lead
10 20 µg/L Selenium 24
Field
feet
Static Water Level 37.43 8.58 20.12 8.71 10.33 39.81 14.14 49.98 11.43 2.66
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 3.82 0.48 290 1.07 5.55 0.67 5.14 5.35 5.53 280
Std. Units
Field pH 5.86 5.59 5.81 6 6.17 5.66 5.03 5.86 5.62 5.96
mV
REDOX 58 50 -3 -8 36 30 48 90 124 -114
µmhos/cm
Field Specific Conductance 91 151 324 333 171 139 52 115 39 125
°C
Field Temperature 15.4 12.4 14.2 12.1 13.5 15.4 14.3 15.5 14 13.9
November-06
(blank)
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 94 90 230 220 58 76 29 140 71 24
1 2 µg/L Cadmium 2
10 10 µg/L Chromium 6.2
10 15 µg/L Lead
Field
feet
Static Water Level 38.17 8.74 22.3 9.81 11.17 40.13 16.19 49.85 11.94 3.41
Total Well Depth 60 21 27 20 30 48 27 60 21 20
mg/L
Oxygen, Dissolved 4.28 0.31 1.15 0.42 5.88 1.21 6.2 5.44 5.67 0.31
Std. Units
Field pH 6.29 5.97 5.94 6.16 6.49 5.94 6.15 5.94 5.84 6.64
mV
REDOX -13 114 160 59 59 95 35 90 221 67
µmhos/cm
Field Specific Conductance 104 235 266 196 196 155 60 136 45 145
°F
Field Temperature 58.8 59.3 59.5 59.9 60.2 58.1 59.9 59.7 60.7 60.4
April-06
(blank)
µg/L
100 700 µg/L Barium 82 52 290 220 57 74 29 100 48 26
10 10 µg/L Chromium 6.2
10 15 µg/L Lead
November-05
EPA 6010
µg/L
100 700 µg/L Barium 78 62 300 180 54 60 26 100 46 27
10 10 µg/L Chromium 3.5
10 15 µg/L Lead
EPA 7470
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
21 73 58 34 48
114 65 140 218 112
16.3 15.32 15.75 15.64 17.53
11
5.5
31 79 210 88 300
6.6 17
5.2 11
21
4.21 8.67 49.43
15.7 20 60
6.57 4.59 5.7 5.5 6.16
6.02 5.72 5.79 6.63 6.32
87 110 99 27 86
105 72 140 314 130
13.5 12.9 15.4 22.3 20.8
8.3
66 62 460 54 44
35
23
4.65 8.92 40.93
15.6 20 60
0.85 4.54 6.41 7.91 5.26
6.24 5.84 6 7.28 6.65
132 235 171 130 233
127 80 152 66 140
60.3 60.7 59.2 55.4 62.2
55 65 250 120 150
4215 4.2 4.7
13 7.6
77 59 120 73 51
3.9
5.9
7/14/2017
Summary of Detected Constituents
Facility Permit 34-12 Old Salisbury Road Landfill (C&D)
Qualifier (Multiple Items)
SWSL 2L Units Concentration
MW-1R MW-2R MW-3R MW-4R MW-5R
MW-
6R MW-7 MW-8 MW-9 MW-10 MW-11
MCL
µg/L
0.2 1 µg/L Mercury 0.34 0.4 0.24 0.26 0.2
EPA 8260
µg/L
1 3 µg/L Chloromethane 5.4
June-05
(blank)
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 48 43 300 150 53 53 25 85 82 24
10 10 µg/L Chromium 5.6
10 15 µg/L Lead
10 20 µg/L Selenium 5.5
November-04
(blank)
µg/L
10 10 µg/L Arsenic 5.1
100 700 µg/L Barium 95 52 340 140 80 63 30 95 55 28
10 10 µg/L Chromium 2 2.3 14 4.4 2.4 3.9
August-04
(blank)
µg/L
10 10 µg/L Arsenic
100 700 µg/L Barium 240 98 47
10 10 µg/L Chromium 14 13 3.3
10 15 µg/L Lead 14 6.8
10 20 µg/L Selenium 6.2
7/14/2017
Summary of Detected Constituents
MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4
Trip
Blank
Equipment
Blank
0.44 1.1
23
50 46 69 750 47
52
57
77 57 66 53 65
2.1 4.8 3.2
20
74 160 170 500 63
9.2 3.2 36
11 8 38
7/14/2017

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Appendix B – Laboratory Groundwater Report

B
Appendix B – Laboratory
Groundwater Report

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#=CL#
June 15, 2017
LIMS USE: FR - SEAN QUARRY
LIMS OBJECT ID: 92342317
92342317
Project:
Pace Project No.:
RE:
Sean Quarry
HDR Engineering
440 South Church Street
Suite 1000
Charlotte, NC 28202
OSR
Dear Sean Quarry:
Enclosed are the analytical results for sample(s) received by the laboratory between May 31, 2017
and June 02, 2017. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 199
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342317
OSR
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 199
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342317001 3412-EQUIPMENT BLANK EPA 8081 14 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 3 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 11 PASI-CRES
EPA 8260 53 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342317002 3412-MW8 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AAES2
SM 4500-CN-E 1 PASI-AAES2
92342317003 3412-MW9 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AAES2
SM 4500-CN-E 1 PASI-AAES2
92342317004 3412-MW13 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 199
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AAES2
SM 4500-CN-E 1 PASI-AAES2
92342317005 3412-MW14 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ANAL
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-AAES2
SM 4500-CN-E 1 PASI-AAES2
92342317006 3412-MW1R EPA 8081 14 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 3 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 8 PASI-CBPJ
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317007 3412-MW15 EPA 8081 14 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 3 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 8 PASI-CBPJ
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 199
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317008 3412-MW3R EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 8 PASI-CBPJ
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317009 3412-MW7 EPA 8081 14 PASI-CRES
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317010 3412-SW2 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 8 PASI-CBPJ
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 199
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342317011 3412-MW5R EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317012 3412-MW12 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317013 3412-SW1 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317014 3412-SW3 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 199
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317015 3412-SW4 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CZDO
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 4500-CN-E 1 PASI-AAES2
92342317016 3412-TRIP BLANK EPA 8260 53 PASI-CGAW
92342317017 3412-MW2R EPA 8081 14 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 3 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 8 PASI-CRES
EPA 8260 53 PASI-CGAW
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 4500-CN-E 1 PASI-AAES2
92342317018 3412-MW4R EPA 8081 14 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 3 PASI-OLJM
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 8 PASI-CRES
EPA 8260 53 PASI-CGAW
SM 2320B 1 PASI-AKDF1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 199
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 4500-CN-E 1 PASI-AAES2
92342317019 3412-MW10 EPA 8081 14 PASI-CRES
EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CGAW
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 4500-CN-E 1 PASI-AAES2
92342317020 3412-MW11 EPA 6010 18 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 53 PASI-CGAW
SM 2320B 1 PASI-AKDF1
SM 2540C 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92342317001 Collected:05/30/17 09:15 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/07/17 23:28 309-00-206/02/17 13:290.050 1
alpha-BHC ND ug/L 06/07/17 23:28 319-84-606/02/17 13:290.050 1
delta-BHC ND ug/L 06/07/17 23:28 319-86-806/02/17 13:290.050 1
4,4'-DDD ND ug/L 06/07/17 23:28 72-54-806/02/17 13:290.050 1
4,4'-DDT ND ug/L 06/07/17 23:28 50-29-306/02/17 13:290.050 1
Endosulfan I ND ug/L 06/07/17 23:28 959-98-806/02/17 13:290.050 1
Endosulfan II ND ug/L 06/07/17 23:28 33213-65-906/02/17 13:290.050 1
Endrin ND ug/L 06/07/17 23:28 72-20-806/02/17 13:290.050 1
Endrin aldehyde ND ug/L 06/07/17 23:28 7421-93-406/02/17 13:290.050 1
Heptachlor ND ug/L 06/07/17 23:28 76-44-806/02/17 13:290.050 1
Heptachlor epoxide ND ug/L 06/07/17 23:28 1024-57-306/02/17 13:290.050 1
Methoxychlor ND ug/L 06/07/17 23:28 72-43-506/02/17 13:290.15 1
Surrogates
Tetrachloro-m-xylene (S)98 %06/07/17 23:28 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)38 %06/07/17 23:28 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/01/17 21:57 12674-11-205/31/17 16:500.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/01/17 21:57 11104-28-205/31/17 16:500.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/01/17 21:57 11141-16-505/31/17 16:500.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/01/17 21:57 53469-21-905/31/17 16:500.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/01/17 21:57 12672-29-605/31/17 16:500.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/01/17 21:57 11097-69-105/31/17 16:500.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/01/17 21:57 11096-82-505/31/17 16:500.50 1
Surrogates
Decachlorobiphenyl (S)72 %06/01/17 21:57 2051-24-305/31/17 16:5010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/06/17 07:15 94-75-706/02/17 16:300.90 1
2,4,5-TP (Silvex)ND ug/L 06/06/17 07:15 93-72-106/02/17 16:300.18 1
Surrogates
2,4-DCAA (S)76 %06/06/17 07:15 19719-28-906/02/17 16:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 07:32 7440-36-006/02/17 15:205.0 1
Arsenic ND ug/L 06/10/17 07:32 7440-38-206/02/17 15:2010.0 1
Barium ND ug/L 06/10/17 07:32 7440-39-306/02/17 15:205.0 1
Beryllium ND ug/L 06/10/17 07:32 7440-41-706/02/17 15:201.0 1
Cadmium ND ug/L 06/10/17 07:32 7440-43-906/02/17 15:201.0 1
Chromium ND ug/L 06/10/17 07:32 7440-47-306/02/17 15:205.0 1
Cobalt ND ug/L 06/10/17 07:32 7440-48-406/02/17 15:205.0 1
Copper 761 ug/L 06/10/17 07:32 7440-50-8 M106/02/17 15:205.0 1
Iron 27.1J ug/L 06/10/17 07:32 7439-89-606/02/17 15:2050.0 1
Lead 18.2 ug/L 06/10/17 07:32 7439-92-106/02/17 15:205.0 1
Manganese ND ug/L 06/10/17 07:32 7439-96-506/02/17 15:205.0 1
Nickel ND ug/L 06/10/17 07:32 7440-02-006/02/17 15:205.0 1
Selenium ND ug/L 06/10/17 07:32 7782-49-206/02/17 15:2010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92342317001 Collected:05/30/17 09:15 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Silver ND ug/L 06/10/17 07:32 7440-22-406/02/17 15:205.0 1
Sodium ND ug/L 06/10/17 07:32 7440-23-506/02/17 15:2050001
Tin 4.0J ug/L 06/10/17 07:32 7440-31-506/02/17 15:205.0 1
Vanadium ND ug/L 06/10/17 07:32 7440-62-206/02/17 15:205.0 1
Zinc 455 ug/L 06/10/17 07:32 7440-66-6 M106/02/17 15:2010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 13:39 7440-28-006/01/17 11:300.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/02/17 03:13 7439-97-606/01/17 13:380.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/02/17 17:07 56-55-305/31/17 13:3810.0 1
Chrysene ND ug/L 06/02/17 17:07 218-01-905/31/17 13:3810.0 1
Dibenz(a,h)anthracene ND ug/L 06/02/17 17:07 53-70-305/31/17 13:3810.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/02/17 17:07 117-81-705/31/17 13:386.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/02/17 17:07 193-39-505/31/17 13:3810.0 1
Surrogates
Nitrobenzene-d5 (S)80 %06/02/17 17:07 4165-60-005/31/17 13:3821-110 1
2-Fluorobiphenyl (S)91 %06/02/17 17:07 321-60-805/31/17 13:3827-110 1
Terphenyl-d14 (S)93 %06/02/17 17:07 1718-51-005/31/17 13:3831-107 1
Phenol-d6 (S)26 %06/02/17 17:07 13127-88-305/31/17 13:3810-110 1
2-Fluorophenol (S)39 %06/02/17 17:07 367-12-405/31/17 13:3812-110 1
2,4,6-Tribromophenol (S)88 %06/02/17 17:07 118-79-605/31/17 13:3827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 18.3J ug/L 05/31/17 16:10 67-64-125.0 1
Acrylonitrile ND ug/L 05/31/17 16:10 107-13-110.0 1
Benzene ND ug/L 05/31/17 16:10 71-43-21.0 1
Bromochloromethane ND ug/L 05/31/17 16:10 74-97-51.0 1
Bromodichloromethane ND ug/L 05/31/17 16:10 75-27-41.0 1
Bromoform ND ug/L 05/31/17 16:10 75-25-21.0 1
Bromomethane ND ug/L 05/31/17 16:10 74-83-92.0 1
2-Butanone (MEK)ND ug/L 05/31/17 16:10 78-93-35.0 1
Carbon disulfide ND ug/L 05/31/17 16:10 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/31/17 16:10 56-23-51.0 1
Chlorobenzene ND ug/L 05/31/17 16:10 108-90-71.0 1
Chloroethane ND ug/L 05/31/17 16:10 75-00-31.0 1
Chloroform ND ug/L 05/31/17 16:10 67-66-31.0 1
Chloromethane ND ug/L 05/31/17 16:10 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 16:10 96-12-82.0 1
Dibromochloromethane ND ug/L 05/31/17 16:10 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 16:10 106-93-41.0 1
Dibromomethane ND ug/L 05/31/17 16:10 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/31/17 16:10 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-EQUIPMENT BLANK Lab ID:92342317001 Collected:05/30/17 09:15 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 05/31/17 16:10 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 16:10 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 05/31/17 16:10 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/31/17 16:10 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/31/17 16:10 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/31/17 16:10 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/31/17 16:10 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/31/17 16:10 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/31/17 16:10 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 16:10 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 16:10 10061-02-61.0 1
Ethylbenzene ND ug/L 05/31/17 16:10 100-41-41.0 1
2-Hexanone ND ug/L 05/31/17 16:10 591-78-65.0 1
Iodomethane ND ug/L 05/31/17 16:10 74-88-45.0 1
Methylene Chloride ND ug/L 05/31/17 16:10 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 16:10 108-10-15.0 1
Styrene ND ug/L 05/31/17 16:10 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 16:10 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 16:10 79-34-51.0 1
Tetrachloroethene ND ug/L 05/31/17 16:10 127-18-41.0 1
Tetrahydrofuran ND ug/L 05/31/17 16:10 109-99-910.0 1
Toluene ND ug/L 05/31/17 16:10 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/31/17 16:10 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/31/17 16:10 79-00-51.0 1
Trichloroethene ND ug/L 05/31/17 16:10 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/31/17 16:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/31/17 16:10 96-18-41.0 1
Vinyl acetate ND ug/L 05/31/17 16:10 108-05-42.0 1
Vinyl chloride ND ug/L 05/31/17 16:10 75-01-41.0 1
m&p-Xylene ND ug/L 05/31/17 16:10 179601-23-12.0 1
o-Xylene ND ug/L 05/31/17 16:10 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %05/31/17 16:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %05/31/17 16:10 17060-07-070-130 1
Toluene-d8 (S)108 %05/31/17 16:10 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-81001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:17 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW8 Lab ID:92342317002 Collected:05/30/17 14:05 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/30/17 14:051
Field pH 5.6 Std. Units 05/30/17 14:050.10 1
Field Temperature 17.0 deg C 05/30/17 14:050.50 1
Static Water Level 15.16 feet 05/30/17 14:051
Field Specific Conductance 68.1 umhos/cm 05/30/17 14:051.0 1
Oxygen, Dissolved 5.40 mg/L 05/30/17 14:05 7782-44-71
Total Well Depth 27 feet 05/30/17 14:051
REDOX 195.0 mV 05/30/17 14:051
Turbidity 1.16 NTU 05/30/17 14:051.0 1
Odor NONE 05/30/17 14:051
Appearance CLEAR 05/30/17 14:051
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 07:50 7440-36-006/02/17 15:205.0 1
Arsenic ND ug/L 06/10/17 07:50 7440-38-206/02/17 15:2010.0 1
Barium 42.9 ug/L 06/10/17 07:50 7440-39-306/02/17 15:205.0 1
Beryllium ND ug/L 06/10/17 07:50 7440-41-706/02/17 15:201.0 1
Cadmium ND ug/L 06/10/17 07:50 7440-43-906/02/17 15:201.0 1
Chromium ND ug/L 06/10/17 07:50 7440-47-306/02/17 15:205.0 1
Cobalt ND ug/L 06/10/17 07:50 7440-48-406/02/17 15:205.0 1
Copper ND ug/L 06/10/17 07:50 7440-50-806/02/17 15:205.0 1
Iron ND ug/L 06/10/17 07:50 7439-89-606/02/17 15:2050.0 1
Lead ND ug/L 06/10/17 07:50 7439-92-106/02/17 15:205.0 1
Manganese 3.0J ug/L 06/10/17 07:50 7439-96-506/02/17 15:205.0 1
Nickel ND ug/L 06/10/17 07:50 7440-02-006/02/17 15:205.0 1
Selenium ND ug/L 06/10/17 07:50 7782-49-206/02/17 15:2010.0 1
Silver ND ug/L 06/10/17 07:50 7440-22-406/02/17 15:205.0 1
Sodium 9240 ug/L 06/10/17 07:50 7440-23-506/02/17 15:2050001
Tin ND ug/L 06/10/17 07:50 7440-31-506/02/17 15:205.0 1
Vanadium ND ug/L 06/10/17 07:50 7440-62-206/02/17 15:205.0 1
Zinc ND ug/L 06/10/17 07:50 7440-66-606/02/17 15:2010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 13:41 7440-28-006/01/17 11:300.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/02/17 03:15 7439-97-606/01/17 13:380.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 15.8J ug/L 05/31/17 16:27 67-64-125.0 1
Acrylonitrile ND ug/L 05/31/17 16:27 107-13-110.0 1
Benzene ND ug/L 05/31/17 16:27 71-43-21.0 1
Bromochloromethane ND ug/L 05/31/17 16:27 74-97-51.0 1
Bromodichloromethane ND ug/L 05/31/17 16:27 75-27-41.0 1
Bromoform ND ug/L 05/31/17 16:27 75-25-21.0 1
Bromomethane ND ug/L 05/31/17 16:27 74-83-9 M12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW8 Lab ID:92342317002 Collected:05/30/17 14:05 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 05/31/17 16:27 78-93-35.0 1
Carbon disulfide ND ug/L 05/31/17 16:27 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/31/17 16:27 56-23-51.0 1
Chlorobenzene ND ug/L 05/31/17 16:27 108-90-71.0 1
Chloroethane ND ug/L 05/31/17 16:27 75-00-31.0 1
Chloroform ND ug/L 05/31/17 16:27 67-66-31.0 1
Chloromethane ND ug/L 05/31/17 16:27 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 16:27 96-12-82.0 1
Dibromochloromethane ND ug/L 05/31/17 16:27 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 16:27 106-93-41.0 1
Dibromomethane ND ug/L 05/31/17 16:27 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/31/17 16:27 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/31/17 16:27 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 16:27 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 05/31/17 16:27 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/31/17 16:27 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/31/17 16:27 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/31/17 16:27 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/31/17 16:27 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/31/17 16:27 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/31/17 16:27 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 16:27 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 16:27 10061-02-61.0 1
Ethylbenzene ND ug/L 05/31/17 16:27 100-41-41.0 1
2-Hexanone ND ug/L 05/31/17 16:27 591-78-6 M15.0 1
Iodomethane ND ug/L 05/31/17 16:27 74-88-45.0 1
Methylene Chloride ND ug/L 05/31/17 16:27 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 16:27 108-10-15.0 1
Styrene ND ug/L 05/31/17 16:27 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 16:27 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 16:27 79-34-51.0 1
Tetrachloroethene ND ug/L 05/31/17 16:27 127-18-41.0 1
Tetrahydrofuran ND ug/L 05/31/17 16:27 109-99-910.0 1
Toluene ND ug/L 05/31/17 16:27 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/31/17 16:27 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/31/17 16:27 79-00-51.0 1
Trichloroethene ND ug/L 05/31/17 16:27 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/31/17 16:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/31/17 16:27 96-18-41.0 1
Vinyl acetate ND ug/L 05/31/17 16:27 108-05-42.0 1
Vinyl chloride ND ug/L 05/31/17 16:27 75-01-41.0 1
m&p-Xylene ND ug/L 05/31/17 16:27 179601-23-12.0 1
o-Xylene ND ug/L 05/31/17 16:27 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %05/31/17 16:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %05/31/17 16:27 17060-07-070-130 1
Toluene-d8 (S)90 %05/31/17 16:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW8 Lab ID:92342317002 Collected:05/30/17 14:05 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 20800 ug/L 06/01/17 18:0150001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 67000 ug/L 06/05/17 17:43250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2700 ug/L 06/03/17 19:35 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3060 ug/L 06/02/17 11:26 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 9.9 ug/L 06/01/17 17:18 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW9 Lab ID:92342317003 Collected:05/30/17 15:10 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/30/17 15:101
Field pH 5.5 Std. Units 05/30/17 15:100.10 1
Field Temperature 19.8 deg C 05/30/17 15:100.50 1
Static Water Level 52.82 feet 05/30/17 15:101
Field Specific Conductance 159.0 umhos/cm 05/30/17 15:101.0 1
Oxygen, Dissolved 6.51 mg/L 05/30/17 15:10 7782-44-71
Total Well Depth 60.0 feet 05/30/17 15:101
REDOX 178.8 mV 05/30/17 15:101
Turbidity 0.40 NTU 05/30/17 15:101.0 1
Odor NONE 05/30/17 15:101
Appearance CLEAR 05/30/17 15:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 07:53 7440-36-006/02/17 15:205.0 1
Arsenic ND ug/L 06/10/17 07:53 7440-38-206/02/17 15:2010.0 1
Barium 207 ug/L 06/10/17 07:53 7440-39-306/02/17 15:205.0 1
Beryllium ND ug/L 06/10/17 07:53 7440-41-706/02/17 15:201.0 1
Cadmium ND ug/L 06/10/17 07:53 7440-43-906/02/17 15:201.0 1
Chromium ND ug/L 06/10/17 07:53 7440-47-306/02/17 15:205.0 1
Cobalt ND ug/L 06/10/17 07:53 7440-48-406/02/17 15:205.0 1
Copper ND ug/L 06/10/17 07:53 7440-50-806/02/17 15:205.0 1
Iron ND ug/L 06/10/17 07:53 7439-89-606/02/17 15:2050.0 1
Lead ND ug/L 06/10/17 07:53 7439-92-106/02/17 15:205.0 1
Manganese 4.6J ug/L 06/10/17 07:53 7439-96-506/02/17 15:205.0 1
Nickel ND ug/L 06/10/17 07:53 7440-02-006/02/17 15:205.0 1
Selenium ND ug/L 06/10/17 07:53 7782-49-206/02/17 15:2010.0 1
Silver ND ug/L 06/10/17 07:53 7440-22-406/02/17 15:205.0 1
Sodium 15400 ug/L 06/10/17 07:53 7440-23-506/02/17 15:2050001
Tin ND ug/L 06/10/17 07:53 7440-31-506/02/17 15:205.0 1
Vanadium ND ug/L 06/10/17 07:53 7440-62-206/02/17 15:205.0 1
Zinc 5.1J ug/L 06/10/17 07:53 7440-66-606/02/17 15:2010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 13:43 7440-28-006/01/17 11:300.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/02/17 03:18 7439-97-606/01/17 13:380.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/31/17 16:44 67-64-125.0 1
Acrylonitrile ND ug/L 05/31/17 16:44 107-13-110.0 1
Benzene ND ug/L 05/31/17 16:44 71-43-21.0 1
Bromochloromethane ND ug/L 05/31/17 16:44 74-97-51.0 1
Bromodichloromethane ND ug/L 05/31/17 16:44 75-27-41.0 1
Bromoform ND ug/L 05/31/17 16:44 75-25-21.0 1
Bromomethane ND ug/L 05/31/17 16:44 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW9 Lab ID:92342317003 Collected:05/30/17 15:10 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 05/31/17 16:44 78-93-35.0 1
Carbon disulfide ND ug/L 05/31/17 16:44 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/31/17 16:44 56-23-51.0 1
Chlorobenzene ND ug/L 05/31/17 16:44 108-90-71.0 1
Chloroethane ND ug/L 05/31/17 16:44 75-00-31.0 1
Chloroform ND ug/L 05/31/17 16:44 67-66-31.0 1
Chloromethane ND ug/L 05/31/17 16:44 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 16:44 96-12-82.0 1
Dibromochloromethane ND ug/L 05/31/17 16:44 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 16:44 106-93-41.0 1
Dibromomethane ND ug/L 05/31/17 16:44 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/31/17 16:44 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/31/17 16:44 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 16:44 110-57-6 L11.0 1
Dichlorodifluoromethane 1.5 ug/L 05/31/17 16:44 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/31/17 16:44 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/31/17 16:44 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/31/17 16:44 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/31/17 16:44 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/31/17 16:44 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/31/17 16:44 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 16:44 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 16:44 10061-02-61.0 1
Ethylbenzene ND ug/L 05/31/17 16:44 100-41-41.0 1
2-Hexanone ND ug/L 05/31/17 16:44 591-78-65.0 1
Iodomethane ND ug/L 05/31/17 16:44 74-88-45.0 1
Methylene Chloride ND ug/L 05/31/17 16:44 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 16:44 108-10-15.0 1
Styrene ND ug/L 05/31/17 16:44 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 16:44 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 16:44 79-34-51.0 1
Tetrachloroethene ND ug/L 05/31/17 16:44 127-18-41.0 1
Tetrahydrofuran ND ug/L 05/31/17 16:44 109-99-910.0 1
Toluene ND ug/L 05/31/17 16:44 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/31/17 16:44 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/31/17 16:44 79-00-51.0 1
Trichloroethene ND ug/L 05/31/17 16:44 79-01-61.0 1
Trichlorofluoromethane 1.4 ug/L 05/31/17 16:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/31/17 16:44 96-18-41.0 1
Vinyl acetate ND ug/L 05/31/17 16:44 108-05-42.0 1
Vinyl chloride ND ug/L 05/31/17 16:44 75-01-41.0 1
m&p-Xylene ND ug/L 05/31/17 16:44 179601-23-12.0 1
o-Xylene ND ug/L 05/31/17 16:44 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %05/31/17 16:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %05/31/17 16:44 17060-07-070-130 1
Toluene-d8 (S)108 %05/31/17 16:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW9 Lab ID:92342317003 Collected:05/30/17 15:10 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 25400 ug/L 06/01/17 18:1250001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 141000 ug/L 06/05/17 17:43250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 960J ug/L 06/03/17 19:52 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4610 ug/L 06/02/17 11:27 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:21 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW13 Lab ID:92342317004 Collected:05/30/17 17:10 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/30/17 17:101
Field pH 5.6 Std. Units 05/30/17 17:100.10 1
Field Temperature 16.9 deg C 05/30/17 17:100.50 1
Static Water Level 8.70 feet 05/30/17 17:101
Field Specific Conductance 116.5 umhos/cm 05/30/17 17:101.0 1
Oxygen, Dissolved 4.03 mg/L 05/30/17 17:10 7782-44-71
Total Well Depth 20 feet 05/30/17 17:101
REDOX 138.8 mV 05/30/17 17:101
Turbidity 1.75 NTU 05/30/17 17:101.0 1
Odor NONE 05/30/17 17:101
Appearance CLEAR 05/30/17 17:101
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 07:57 7440-36-006/02/17 15:205.0 1
Arsenic ND ug/L 06/10/17 07:57 7440-38-206/02/17 15:2010.0 1
Barium 120 ug/L 06/10/17 07:57 7440-39-306/02/17 15:205.0 1
Beryllium ND ug/L 06/10/17 07:57 7440-41-706/02/17 15:201.0 1
Cadmium ND ug/L 06/10/17 07:57 7440-43-906/02/17 15:201.0 1
Chromium ND ug/L 06/10/17 07:57 7440-47-306/02/17 15:205.0 1
Cobalt ND ug/L 06/10/17 07:57 7440-48-406/02/17 15:205.0 1
Copper ND ug/L 06/10/17 07:57 7440-50-806/02/17 15:205.0 1
Iron 58.0 ug/L 06/10/17 07:57 7439-89-606/02/17 15:2050.0 1
Lead ND ug/L 06/10/17 07:57 7439-92-106/02/17 15:205.0 1
Manganese 9.7 ug/L 06/10/17 07:57 7439-96-506/02/17 15:205.0 1
Nickel ND ug/L 06/10/17 07:57 7440-02-006/02/17 15:205.0 1
Selenium ND ug/L 06/10/17 07:57 7782-49-206/02/17 15:2010.0 1
Silver ND ug/L 06/10/17 07:57 7440-22-406/02/17 15:205.0 1
Sodium 10000 ug/L 06/10/17 07:57 7440-23-506/02/17 15:2050001
Tin ND ug/L 06/10/17 07:57 7440-31-506/02/17 15:205.0 1
Vanadium ND ug/L 06/10/17 07:57 7440-62-206/02/17 15:205.0 1
Zinc 5.7J ug/L 06/10/17 07:57 7440-66-606/02/17 15:2010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 13:44 7440-28-006/01/17 11:300.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/02/17 03:20 7439-97-606/01/17 13:380.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 17.3J ug/L 05/31/17 17:19 67-64-125.0 1
Acrylonitrile ND ug/L 05/31/17 17:19 107-13-110.0 1
Benzene ND ug/L 05/31/17 17:19 71-43-21.0 1
Bromochloromethane ND ug/L 05/31/17 17:19 74-97-51.0 1
Bromodichloromethane ND ug/L 05/31/17 17:19 75-27-41.0 1
Bromoform ND ug/L 05/31/17 17:19 75-25-21.0 1
Bromomethane ND ug/L 05/31/17 17:19 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW13 Lab ID:92342317004 Collected:05/30/17 17:10 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 05/31/17 17:19 78-93-35.0 1
Carbon disulfide ND ug/L 05/31/17 17:19 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/31/17 17:19 56-23-51.0 1
Chlorobenzene ND ug/L 05/31/17 17:19 108-90-71.0 1
Chloroethane ND ug/L 05/31/17 17:19 75-00-31.0 1
Chloroform ND ug/L 05/31/17 17:19 67-66-31.0 1
Chloromethane ND ug/L 05/31/17 17:19 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 17:19 96-12-82.0 1
Dibromochloromethane ND ug/L 05/31/17 17:19 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 17:19 106-93-41.0 1
Dibromomethane ND ug/L 05/31/17 17:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/31/17 17:19 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/31/17 17:19 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 17:19 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 05/31/17 17:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/31/17 17:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/31/17 17:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/31/17 17:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/31/17 17:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/31/17 17:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/31/17 17:19 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 17:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 17:19 10061-02-61.0 1
Ethylbenzene ND ug/L 05/31/17 17:19 100-41-41.0 1
2-Hexanone ND ug/L 05/31/17 17:19 591-78-65.0 1
Iodomethane ND ug/L 05/31/17 17:19 74-88-45.0 1
Methylene Chloride ND ug/L 05/31/17 17:19 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 17:19 108-10-15.0 1
Styrene ND ug/L 05/31/17 17:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 17:19 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 17:19 79-34-51.0 1
Tetrachloroethene ND ug/L 05/31/17 17:19 127-18-41.0 1
Tetrahydrofuran ND ug/L 05/31/17 17:19 109-99-910.0 1
Toluene ND ug/L 05/31/17 17:19 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/31/17 17:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/31/17 17:19 79-00-51.0 1
Trichloroethene ND ug/L 05/31/17 17:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 05/31/17 17:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/31/17 17:19 96-18-41.0 1
Vinyl acetate ND ug/L 05/31/17 17:19 108-05-42.0 1
Vinyl chloride ND ug/L 05/31/17 17:19 75-01-41.0 1
m&p-Xylene ND ug/L 05/31/17 17:19 179601-23-12.0 1
o-Xylene ND ug/L 05/31/17 17:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %05/31/17 17:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %05/31/17 17:19 17060-07-070-130 1
Toluene-d8 (S)107 %05/31/17 17:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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Page 19 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW13 Lab ID:92342317004 Collected:05/30/17 17:10 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 42400 ug/L 06/01/17 18:2450001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 89000 ug/L 06/05/17 17:44250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 5670 ug/L 06/03/17 20:09 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4310 ug/L 06/02/17 11:28 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:22 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW14 Lab ID:92342317005 Collected:05/30/17 16:15 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/30/17 16:151
Field pH 5.5 Std. Units 05/30/17 16:150.10 1
Field Temperature 18.4 deg C 05/30/17 16:150.50 1
Static Water Level 51.86 feet 05/30/17 16:151
Field Specific Conductance 173.7 umhos/cm 05/30/17 16:151.0 1
Oxygen, Dissolved 3.28 mg/L 05/30/17 16:15 7782-44-71
Total Well Depth 60 feet 05/30/17 16:151
REDOX 147.0 mV 05/30/17 16:151
Turbidity 5.42 NTU 05/30/17 16:151.0 1
Odor NONE 05/30/17 16:151
Appearance CLEAR 05/30/17 16:151
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 08:00 7440-36-006/02/17 15:205.0 1
Arsenic ND ug/L 06/10/17 08:00 7440-38-206/02/17 15:2010.0 1
Barium 221 ug/L 06/10/17 08:00 7440-39-306/02/17 15:205.0 1
Beryllium 0.60J ug/L 06/10/17 08:00 7440-41-706/02/17 15:201.0 1
Cadmium ND ug/L 06/10/17 08:00 7440-43-906/02/17 15:201.0 1
Chromium ND ug/L 06/10/17 08:00 7440-47-306/02/17 15:205.0 1
Cobalt ND ug/L 06/10/17 08:00 7440-48-406/02/17 15:205.0 1
Copper ND ug/L 06/10/17 08:00 7440-50-806/02/17 15:205.0 1
Iron 134 ug/L 06/10/17 08:00 7439-89-606/02/17 15:2050.0 1
Lead ND ug/L 06/10/17 08:00 7439-92-106/02/17 15:205.0 1
Manganese 18.1 ug/L 06/10/17 08:00 7439-96-506/02/17 15:205.0 1
Nickel ND ug/L 06/10/17 08:00 7440-02-006/02/17 15:205.0 1
Selenium ND ug/L 06/10/17 08:00 7782-49-206/02/17 15:2010.0 1
Silver ND ug/L 06/10/17 08:00 7440-22-406/02/17 15:205.0 1
Sodium 16900 ug/L 06/10/17 08:00 7440-23-506/02/17 15:2050001
Tin ND ug/L 06/10/17 08:00 7440-31-506/02/17 15:205.0 1
Vanadium ND ug/L 06/10/17 08:00 7440-62-206/02/17 15:205.0 1
Zinc ND ug/L 06/10/17 08:00 7440-66-606/02/17 15:2010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.048J ug/L 06/06/17 16:42 7440-28-006/01/17 11:300.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:28 7439-97-606/06/17 14:590.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 14.7J ug/L 05/31/17 17:36 67-64-125.0 1
Acrylonitrile ND ug/L 05/31/17 17:36 107-13-110.0 1
Benzene ND ug/L 05/31/17 17:36 71-43-21.0 1
Bromochloromethane ND ug/L 05/31/17 17:36 74-97-51.0 1
Bromodichloromethane ND ug/L 05/31/17 17:36 75-27-41.0 1
Bromoform ND ug/L 05/31/17 17:36 75-25-21.0 1
Bromomethane ND ug/L 05/31/17 17:36 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW14 Lab ID:92342317005 Collected:05/30/17 16:15 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 05/31/17 17:36 78-93-35.0 1
Carbon disulfide ND ug/L 05/31/17 17:36 75-15-02.0 1
Carbon tetrachloride ND ug/L 05/31/17 17:36 56-23-51.0 1
Chlorobenzene ND ug/L 05/31/17 17:36 108-90-71.0 1
Chloroethane ND ug/L 05/31/17 17:36 75-00-31.0 1
Chloroform ND ug/L 05/31/17 17:36 67-66-31.0 1
Chloromethane ND ug/L 05/31/17 17:36 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 17:36 96-12-82.0 1
Dibromochloromethane ND ug/L 05/31/17 17:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 17:36 106-93-41.0 1
Dibromomethane ND ug/L 05/31/17 17:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 05/31/17 17:36 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 05/31/17 17:36 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 17:36 110-57-6 L11.0 1
Dichlorodifluoromethane 3.6 ug/L 05/31/17 17:36 75-71-81.0 1
1,1-Dichloroethane ND ug/L 05/31/17 17:36 75-34-31.0 1
1,2-Dichloroethane ND ug/L 05/31/17 17:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 05/31/17 17:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 05/31/17 17:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 05/31/17 17:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 05/31/17 17:36 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 17:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 17:36 10061-02-61.0 1
Ethylbenzene ND ug/L 05/31/17 17:36 100-41-41.0 1
2-Hexanone ND ug/L 05/31/17 17:36 591-78-65.0 1
Iodomethane ND ug/L 05/31/17 17:36 74-88-45.0 1
Methylene Chloride ND ug/L 05/31/17 17:36 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 17:36 108-10-15.0 1
Styrene ND ug/L 05/31/17 17:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 17:36 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 17:36 79-34-51.0 1
Tetrachloroethene 0.61J ug/L 05/31/17 17:36 127-18-41.0 1
Tetrahydrofuran ND ug/L 05/31/17 17:36 109-99-910.0 1
Toluene ND ug/L 05/31/17 17:36 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 05/31/17 17:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 05/31/17 17:36 79-00-51.0 1
Trichloroethene ND ug/L 05/31/17 17:36 79-01-61.0 1
Trichlorofluoromethane 0.75J ug/L 05/31/17 17:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/31/17 17:36 96-18-41.0 1
Vinyl acetate ND ug/L 05/31/17 17:36 108-05-42.0 1
Vinyl chloride ND ug/L 05/31/17 17:36 75-01-41.0 1
m&p-Xylene ND ug/L 05/31/17 17:36 179601-23-12.0 1
o-Xylene ND ug/L 05/31/17 17:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %05/31/17 17:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %05/31/17 17:36 17060-07-070-130 1
Toluene-d8 (S)108 %05/31/17 17:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW14 Lab ID:92342317005 Collected:05/30/17 16:15 Received:05/31/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 55300 ug/L 06/01/17 18:3650001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 130000 ug/L 06/05/17 17:45250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 663J ug/L 06/03/17 20:26 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3260 ug/L 06/02/17 11:30 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.3J ug/L 06/01/17 17:23 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW1R Lab ID:92342317006 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 05/31/17 11:451
Field pH 5.5 Std. Units 05/31/17 11:450.10 1
Field Temperature 20.3 deg C 05/31/17 11:450.50 1
Static Water Level 35.05 feet 05/31/17 11:451
Field Specific Conductance 209.7 umhos/cm 05/31/17 11:451.0 1
Oxygen, Dissolved 1.3 mg/L 05/31/17 11:45 7782-44-71
Total Well Depth 60 feet 05/31/17 11:451
REDOX 179.6 mV 05/31/17 11:451
Turbidity 3.5 NTU 05/31/17 11:451.0 1
Odor NONE 05/31/17 11:451
Appearance CLEAR 05/31/17 11:451
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 21:37 309-00-206/02/17 10:090.050 1
alpha-BHC ND ug/L 06/06/17 21:37 319-84-606/02/17 10:090.050 1
delta-BHC ND ug/L 06/06/17 21:37 319-86-806/02/17 10:090.050 1
4,4'-DDD ND ug/L 06/06/17 21:37 72-54-806/02/17 10:090.050 1
4,4'-DDT ND ug/L 06/06/17 21:37 50-29-306/02/17 10:090.050 1
Endosulfan I ND ug/L 06/06/17 21:37 959-98-806/02/17 10:090.050 1
Endosulfan II ND ug/L 06/06/17 21:37 33213-65-906/02/17 10:090.050 1
Endrin ND ug/L 06/06/17 21:37 72-20-806/02/17 10:090.050 1
Endrin aldehyde ND ug/L 06/06/17 21:37 7421-93-406/02/17 10:090.050 1
Heptachlor ND ug/L 06/06/17 21:37 76-44-806/02/17 10:090.050 1
Heptachlor epoxide ND ug/L 06/06/17 21:37 1024-57-306/02/17 10:090.050 1
Methoxychlor ND ug/L 06/06/17 21:37 72-43-506/02/17 10:090.15 1
Surrogates
Tetrachloro-m-xylene (S)35 %06/06/17 21:37 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)77 %06/06/17 21:37 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 20:55 12674-11-206/02/17 10:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 20:55 11104-28-206/02/17 10:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 20:55 11141-16-506/02/17 10:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 20:55 53469-21-906/02/17 10:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 20:55 12672-29-606/02/17 10:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 20:55 11097-69-106/02/17 10:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 20:55 11096-82-506/02/17 10:090.50 1
Surrogates
Decachlorobiphenyl (S)76 %06/02/17 20:55 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 11:57 94-75-7 L106/05/17 16:501.0 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 11:57 93-72-106/05/17 16:500.21 1
Surrogates
2,4-DCAA (S)92 %06/07/17 11:57 19719-28-906/05/17 16:5039-139 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW1R Lab ID:92342317006 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:20 7440-36-006/02/17 11:255.0 1
Arsenic ND ug/L 06/08/17 15:20 7440-38-206/02/17 11:2510.0 1
Barium 272 ug/L 06/08/17 15:20 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:20 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:20 7440-43-906/02/17 11:251.0 1
Chromium ND ug/L 06/08/17 15:20 7440-47-306/02/17 11:255.0 1
Cobalt ND ug/L 06/08/17 15:20 7440-48-406/02/17 11:255.0 1
Copper ND ug/L 06/08/17 15:20 7440-50-806/02/17 11:255.0 1
Iron 54.8 ug/L 06/08/17 15:20 7439-89-606/02/17 11:2550.0 1
Lead ND ug/L 06/08/17 15:20 7439-92-106/02/17 11:255.0 1
Manganese 12.5 ug/L 06/08/17 15:20 7439-96-506/02/17 11:255.0 1
Nickel ND ug/L 06/08/17 15:20 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:20 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:20 7440-22-406/02/17 11:255.0 1
Sodium 15800 ug/L 06/08/17 15:20 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 19:49 7440-31-506/02/17 11:255.0 1
Vanadium ND ug/L 06/08/17 15:20 7440-62-206/02/17 11:255.0 1
Zinc 5.5J ug/L 06/08/17 15:20 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 15:51 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:10 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/12/17 23:06 56-55-3 L206/05/17 11:4510.0 1
Chrysene ND ug/L 06/12/17 23:06 218-01-9 L206/05/17 11:4510.0 1
Dibenz(a,h)anthracene ND ug/L 06/12/17 23:06 53-70-306/05/17 11:4510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/17 23:06 117-81-706/05/17 11:456.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/17 23:06 193-39-5 L206/05/17 11:4510.0 1
Surrogates
Nitrobenzene-d5 (S)53 %06/12/17 23:06 4165-60-0 1g06/05/17 11:4521-110 1
2-Fluorobiphenyl (S)70 %06/12/17 23:06 321-60-806/05/17 11:4527-110 1
Terphenyl-d14 (S)62 %06/12/17 23:06 1718-51-006/05/17 11:4531-107 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 06:07 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 06:07 107-13-110.0 1
Benzene ND ug/L 06/02/17 06:07 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 06:07 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 06:07 75-27-41.0 1
Bromoform ND ug/L 06/02/17 06:07 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 06:07 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 06:07 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 06:07 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW1R Lab ID:92342317006 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/02/17 06:07 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 06:07 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 06:07 75-00-31.0 1
Chloroform ND ug/L 06/02/17 06:07 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 06:07 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 06:07 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 06:07 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 06:07 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 06:07 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 06:07 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 06:07 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 06:07 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 06:07 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 06:07 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 06:07 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 06:07 75-35-41.0 1
cis-1,2-Dichloroethene 0.38J ug/L 06/02/17 06:07 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 06:07 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 06:07 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 06:07 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 06:07 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 06:07 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 06:07 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 06:07 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 06:07 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 06:07 108-10-15.0 1
Styrene ND ug/L 06/02/17 06:07 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 06:07 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 06:07 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 06:07 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/02/17 06:07 109-99-910.0 1
Toluene ND ug/L 06/02/17 06:07 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 06:07 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 06:07 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 06:07 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 06:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 06:07 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 06:07 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 06:07 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 06:07 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 06:07 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)114 %06/02/17 06:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %06/02/17 06:07 17060-07-070-130 1
Toluene-d8 (S)115 %06/02/17 06:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW1R Lab ID:92342317006 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 68600 ug/L 06/05/17 14:0550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 165000 ug/L 06/06/17 02:05250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 06/03/17 19:58 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 8860 ug/L 06/05/17 11:09 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:12 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW15 Lab ID:92342317007 Collected:05/31/17 14:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 14:201
Field pH 6.3 Std. Units 05/31/17 14:200.10 1
Field Temperature 17.6 deg C 05/31/17 14:200.50 1
Static Water Level 38.85 feet 05/31/17 14:201
Field Specific Conductance 690 umhos/cm 05/31/17 14:201.0 1
Oxygen, Dissolved 3.06 mg/L 05/31/17 14:20 7782-44-71
Total Well Depth 50.85 feet 05/31/17 14:201
REDOX 121.0 mV 05/31/17 14:201
Turbidity 23.24 NTU 05/31/17 14:201.0 1
Odor NONE 05/31/17 14:201
Appearance MURKY 05/31/17 14:201
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 21:55 309-00-206/02/17 10:090.050 1
alpha-BHC ND ug/L 06/06/17 21:55 319-84-606/02/17 10:090.050 1
delta-BHC ND ug/L 06/06/17 21:55 319-86-806/02/17 10:090.050 1
4,4'-DDD ND ug/L 06/06/17 21:55 72-54-806/02/17 10:090.050 1
4,4'-DDT ND ug/L 06/06/17 21:55 50-29-306/02/17 10:090.050 1
Endosulfan I ND ug/L 06/06/17 21:55 959-98-806/02/17 10:090.050 1
Endosulfan II ND ug/L 06/06/17 21:55 33213-65-906/02/17 10:090.050 1
Endrin ND ug/L 06/06/17 21:55 72-20-806/02/17 10:090.050 1
Endrin aldehyde ND ug/L 06/06/17 21:55 7421-93-406/02/17 10:090.050 1
Heptachlor ND ug/L 06/06/17 21:55 76-44-806/02/17 10:090.050 1
Heptachlor epoxide ND ug/L 06/06/17 21:55 1024-57-306/02/17 10:090.050 1
Methoxychlor ND ug/L 06/06/17 21:55 72-43-506/02/17 10:090.15 1
Surrogates
Tetrachloro-m-xylene (S)74 %06/06/17 21:55 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)70 %06/06/17 21:55 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 21:15 12674-11-206/02/17 10:090.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 21:15 11104-28-206/02/17 10:090.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 21:15 11141-16-506/02/17 10:090.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 21:15 53469-21-906/02/17 10:090.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 21:15 12672-29-606/02/17 10:090.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 21:15 11097-69-106/02/17 10:090.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 21:15 11096-82-506/02/17 10:090.50 1
Surrogates
Decachlorobiphenyl (S)68 %06/02/17 21:15 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 12:27 94-75-7 L106/05/17 16:500.99 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 12:27 93-72-106/05/17 16:500.20 1
Surrogates
2,4-DCAA (S)91 %06/07/17 12:27 19719-28-906/05/17 16:5039-139 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW15 Lab ID:92342317007 Collected:05/31/17 14:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:23 7440-36-006/02/17 11:255.0 1
Arsenic ND ug/L 06/08/17 15:23 7440-38-206/02/17 11:2510.0 1
Barium 22.7 ug/L 06/08/17 15:23 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:23 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:23 7440-43-906/02/17 11:251.0 1
Chromium ND ug/L 06/08/17 15:23 7440-47-306/02/17 11:255.0 1
Cobalt ND ug/L 06/08/17 15:23 7440-48-406/02/17 11:255.0 1
Copper 2.6J ug/L 06/08/17 15:23 7440-50-806/02/17 11:255.0 1
Iron 1740 ug/L 06/08/17 15:23 7439-89-606/02/17 11:2550.0 1
Lead ND ug/L 06/08/17 15:23 7439-92-106/02/17 11:255.0 1
Manganese 359 ug/L 06/08/17 15:23 7439-96-506/02/17 11:255.0 1
Nickel 2.7J ug/L 06/08/17 15:23 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:23 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:23 7440-22-406/02/17 11:255.0 1
Sodium 21600 ug/L 06/08/17 15:23 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 19:52 7440-31-506/02/17 11:255.0 1
Vanadium 5.0J ug/L 06/08/17 15:23 7440-62-206/02/17 11:255.0 1
Zinc 16.2 ug/L 06/08/17 15:23 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.049J ug/L 06/06/17 15:53 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:13 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/12/17 23:34 56-55-3 L206/05/17 11:4510.0 1
Chrysene ND ug/L 06/12/17 23:34 218-01-9 L206/05/17 11:4510.0 1
Dibenz(a,h)anthracene ND ug/L 06/12/17 23:34 53-70-306/05/17 11:4510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/17 23:34 117-81-706/05/17 11:456.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/17 23:34 193-39-5 L206/05/17 11:4510.0 1
Surrogates
Nitrobenzene-d5 (S)52 %06/12/17 23:34 4165-60-0 1g06/05/17 11:4521-110 1
2-Fluorobiphenyl (S)64 %06/12/17 23:34 321-60-806/05/17 11:4527-110 1
Terphenyl-d14 (S)65 %06/12/17 23:34 1718-51-006/05/17 11:4531-107 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.2J ug/L 06/02/17 06:25 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 06:25 107-13-110.0 1
Benzene ND ug/L 06/02/17 06:25 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 06:25 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 06:25 75-27-41.0 1
Bromoform ND ug/L 06/02/17 06:25 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 06:25 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 06:25 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 06:25 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW15 Lab ID:92342317007 Collected:05/31/17 14:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/02/17 06:25 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 06:25 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 06:25 75-00-31.0 1
Chloroform 0.40J ug/L 06/02/17 06:25 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 06:25 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 06:25 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 06:25 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 06:25 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 06:25 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 06:25 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 06:25 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 06:25 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 06:25 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 06:25 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 06:25 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 06:25 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 06:25 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 06:25 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 06:25 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 06:25 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 06:25 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 06:25 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 06:25 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 06:25 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 06:25 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 06:25 108-10-15.0 1
Styrene ND ug/L 06/02/17 06:25 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 06:25 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 06:25 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 06:25 127-18-41.0 1
Tetrahydrofuran 12.0 ug/L 06/02/17 06:25 109-99-910.0 1
Toluene ND ug/L 06/02/17 06:25 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 06:25 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 06:25 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 06:25 79-01-61.0 1
Trichlorofluoromethane 2.1 ug/L 06/02/17 06:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 06:25 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 06:25 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 06:25 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 06:25 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 06:25 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)112 %06/02/17 06:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 06:25 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 06:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW15 Lab ID:92342317007 Collected:05/31/17 14:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 98100 ug/L 06/05/17 14:1750001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 410000 ug/L 06/06/17 02:06250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 58300 ug/L 06/03/17 20:51 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 104000 ug/L 06/05/17 11:35 16887-00-650005
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:13 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW3R Lab ID:92342317008 Collected:05/31/17 10:05 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 05/31/17 10:051
Field pH 6.3 Std. Units 05/31/17 10:050.10 1
Field Temperature 20.4 deg C 05/31/17 10:050.50 1
Static Water Level 18.43 feet 05/31/17 10:051
Field Specific Conductance 392.9 umhos/cm 05/31/17 10:051.0 1
Oxygen, Dissolved 0.5 mg/L 05/31/17 10:05 7782-44-71
Total Well Depth 27 feet 05/31/17 10:051
REDOX -60.0 mV 05/31/17 10:051
Turbidity 5.3 NTU 05/31/17 10:051.0 1
Odor Sulfuric 05/31/17 10:051
Appearance Clear 05/31/17 10:051
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:26 7440-36-006/02/17 11:255.0 1
Arsenic 5.5J ug/L 06/08/17 15:26 7440-38-206/02/17 11:2510.0 1
Barium 309 ug/L 06/08/17 15:26 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:26 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:26 7440-43-906/02/17 11:251.0 1
Chromium ND ug/L 06/08/17 15:26 7440-47-306/02/17 11:255.0 1
Cobalt 11.5 ug/L 06/08/17 15:26 7440-48-406/02/17 11:255.0 1
Copper ND ug/L 06/08/17 15:26 7440-50-806/02/17 11:255.0 1
Iron 89300 ug/L 06/08/17 15:26 7439-89-606/02/17 11:2550.0 1
Lead 3.4J ug/L 06/08/17 15:26 7439-92-106/02/17 11:255.0 1
Manganese 6460 ug/L 06/08/17 15:26 7439-96-506/02/17 11:255.0 1
Nickel ND ug/L 06/08/17 15:26 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:26 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:26 7440-22-406/02/17 11:255.0 1
Sodium 2240J ug/L 06/08/17 15:26 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 19:55 7440-31-506/02/17 11:255.0 1
Vanadium ND ug/L 06/08/17 15:26 7440-62-206/02/17 11:255.0 1
Zinc ND ug/L 06/08/17 15:26 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 15:55 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:15 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/13/17 00:03 56-55-3 L206/05/17 11:4510.0 1
Chrysene ND ug/L 06/13/17 00:03 218-01-9 L206/05/17 11:4510.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 00:03 53-70-306/05/17 11:4510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 00:03 117-81-706/05/17 11:456.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 00:03 193-39-5 L206/05/17 11:4510.0 1
Surrogates
Nitrobenzene-d5 (S)27 %06/13/17 00:03 4165-60-0 1g06/05/17 11:4521-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW3R Lab ID:92342317008 Collected:05/31/17 10:05 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
2-Fluorobiphenyl (S)36 %06/13/17 00:03 321-60-806/05/17 11:4527-110 1
Terphenyl-d14 (S)41 %06/13/17 00:03 1718-51-006/05/17 11:4531-107 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 21.4J ug/L 06/02/17 06:42 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 06:42 107-13-110.0 1
Benzene ND ug/L 06/02/17 06:42 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 06:42 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 06:42 75-27-41.0 1
Bromoform ND ug/L 06/02/17 06:42 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 06:42 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 06:42 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 06:42 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/02/17 06:42 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 06:42 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 06:42 75-00-31.0 1
Chloroform ND ug/L 06/02/17 06:42 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 06:42 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 06:42 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 06:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 06:42 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 06:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 06:42 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 06:42 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 06:42 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 06:42 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 06:42 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 06:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 06:42 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 06:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 06:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 06:42 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 06:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 06:42 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 06:42 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 06:42 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 06:42 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 06:42 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 06:42 108-10-15.0 1
Styrene ND ug/L 06/02/17 06:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 06:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 06:42 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 06:42 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/02/17 06:42 109-99-910.0 1
Toluene ND ug/L 06/02/17 06:42 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 06:42 71-55-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW3R Lab ID:92342317008 Collected:05/31/17 10:05 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,2-Trichloroethane ND ug/L 06/02/17 06:42 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 06:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 06:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 06:42 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 06:42 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 06:42 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 06:42 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 06:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)108 %06/02/17 06:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/02/17 06:42 17060-07-070-130 1
Toluene-d8 (S)113 %06/02/17 06:42 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 114000 ug/L 06/05/17 14:2950001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 133000 ug/L 06/06/17 02:07250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 06/03/17 21:09 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2520 ug/L 06/05/17 11:14 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.4J ug/L 06/07/17 13:16 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW7 Lab ID:92342317009 Collected:05/31/17 16:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 05/31/17 16:201
Field pH 5.5 Std. Units 05/31/17 16:200.10 1
Field Temperature 19.7 deg C 05/31/17 16:200.50 1
Static Water Level 36.56 feet 05/31/17 16:201
Field Specific Conductance 220.7 umhos/cm 05/31/17 16:201.0 1
Oxygen, Dissolved 0.4 mg/L 05/31/17 16:20 7782-44-71
Total Well Depth 48 feet 05/31/17 16:201
REDOX 210.2 mV 05/31/17 16:201
Turbidity 4.2 NTU 05/31/17 16:201.0 1
Odor NONE 05/31/17 16:201
Appearance CLEAR 05/31/17 16:201
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/08/17 00:22 309-00-206/02/17 13:290.050 1
alpha-BHC ND ug/L 06/08/17 00:22 319-84-606/02/17 13:290.050 1
delta-BHC ND ug/L 06/08/17 00:22 319-86-806/02/17 13:290.050 1
4,4'-DDD ND ug/L 06/08/17 00:22 72-54-806/02/17 13:290.050 1
4,4'-DDT ND ug/L 06/08/17 00:22 50-29-306/02/17 13:290.050 1
Endosulfan I ND ug/L 06/08/17 00:22 959-98-806/02/17 13:290.050 1
Endosulfan II ND ug/L 06/08/17 00:22 33213-65-906/02/17 13:290.050 1
Endrin ND ug/L 06/08/17 00:22 72-20-806/02/17 13:290.050 1
Endrin aldehyde ND ug/L 06/08/17 00:22 7421-93-4 M106/02/17 13:290.050 1
Heptachlor ND ug/L 06/08/17 00:22 76-44-806/02/17 13:290.050 1
Heptachlor epoxide ND ug/L 06/08/17 00:22 1024-57-306/02/17 13:290.050 1
Methoxychlor ND ug/L 06/08/17 00:22 72-43-506/02/17 13:290.15 1
Surrogates
Tetrachloro-m-xylene (S)91 %06/08/17 00:22 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)69 %06/08/17 00:22 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:30 7440-36-006/02/17 11:255.0 1
Arsenic ND ug/L 06/08/17 15:30 7440-38-206/02/17 11:2510.0 1
Barium 163 ug/L 06/08/17 15:30 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:30 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:30 7440-43-906/02/17 11:251.0 1
Chromium ND ug/L 06/08/17 15:30 7440-47-306/02/17 11:255.0 1
Cobalt ND ug/L 06/08/17 15:30 7440-48-406/02/17 11:255.0 1
Copper ND ug/L 06/08/17 15:30 7440-50-806/02/17 11:255.0 1
Iron 25.2J ug/L 06/08/17 15:30 7439-89-606/02/17 11:2550.0 1
Lead ND ug/L 06/08/17 15:30 7439-92-106/02/17 11:255.0 1
Manganese 51.9 ug/L 06/08/17 15:30 7439-96-506/02/17 11:255.0 1
Nickel ND ug/L 06/08/17 15:30 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:30 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:30 7440-22-406/02/17 11:255.0 1
Sodium 17800 ug/L 06/08/17 15:30 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 19:59 7440-31-506/02/17 11:255.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW7 Lab ID:92342317009 Collected:05/31/17 16:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Vanadium ND ug/L 06/08/17 15:30 7440-62-206/02/17 11:255.0 1
Zinc 8.9J ug/L 06/08/17 15:30 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 15:56 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:17 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 15.7J ug/L 06/02/17 07:00 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 07:00 107-13-110.0 1
Benzene 0.43J ug/L 06/02/17 07:00 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 07:00 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 07:00 75-27-41.0 1
Bromoform ND ug/L 06/02/17 07:00 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 07:00 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 07:00 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 07:00 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/02/17 07:00 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 07:00 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 07:00 75-00-31.0 1
Chloroform ND ug/L 06/02/17 07:00 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 07:00 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 07:00 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 07:00 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 07:00 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 07:00 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 07:00 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 07:00 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 07:00 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 07:00 75-71-81.0 1
1,1-Dichloroethane 1.3 ug/L 06/02/17 07:00 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 07:00 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 07:00 75-35-41.0 1
cis-1,2-Dichloroethene 1.1 ug/L 06/02/17 07:00 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 07:00 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 07:00 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 07:00 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 07:00 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 07:00 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 07:00 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 07:00 74-88-45.0 1
Methylene Chloride 3.1 ug/L 06/02/17 07:00 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 07:00 108-10-15.0 1
Styrene ND ug/L 06/02/17 07:00 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW7 Lab ID:92342317009 Collected:05/31/17 16:20 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 07:00 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 07:00 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 07:00 127-18-41.0 1
Tetrahydrofuran 32.0 ug/L 06/02/17 07:00 109-99-910.0 1
Toluene ND ug/L 06/02/17 07:00 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 07:00 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 07:00 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 07:00 79-01-61.0 1
Trichlorofluoromethane 0.91J ug/L 06/02/17 07:00 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 07:00 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 07:00 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 07:00 75-01-41.0 1
m&p-Xylene 1.2J ug/L 06/02/17 07:00 179601-23-12.0 1
o-Xylene 0.46J ug/L 06/02/17 07:00 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)116 %06/02/17 07:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/02/17 07:00 17060-07-070-130 1
Toluene-d8 (S)95 %06/02/17 07:00 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 85000 ug/L 06/05/17 14:4250001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 175000 ug/L 06/06/17 02:08250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 6720 ug/L 06/03/17 21:27 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 5290 ug/L 06/05/17 11:15 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:17 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW2 Lab ID:92342317010 Collected:05/31/17 10:15 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 10:151
Field pH 6.8 Std. Units 05/31/17 10:150.10 1
Field Temperature 21.0 deg C 05/31/17 10:150.50 1
Field Specific Conductance 172.0 umhos/cm 05/31/17 10:151.0 1
Oxygen, Dissolved 6.3 mg/L 05/31/17 10:15 7782-44-71
REDOX -15.2 mV 05/31/17 10:151
Turbidity 14.72 NTU 05/31/17 10:151.0 1
Odor NONE 05/31/17 10:151
Appearance MURKY 05/31/17 10:151
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:33 7440-36-006/02/17 11:255.0 1
Arsenic ND ug/L 06/08/17 15:33 7440-38-206/02/17 11:2510.0 1
Barium 77.5 ug/L 06/08/17 15:33 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:33 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:33 7440-43-906/02/17 11:251.0 1
Chromium ND ug/L 06/08/17 15:33 7440-47-306/02/17 11:255.0 1
Cobalt ND ug/L 06/08/17 15:33 7440-48-406/02/17 11:255.0 1
Copper ND ug/L 06/08/17 15:33 7440-50-806/02/17 11:255.0 1
Iron 1790 ug/L 06/08/17 15:33 7439-89-606/02/17 11:2550.0 1
Lead ND ug/L 06/08/17 15:33 7439-92-106/02/17 11:255.0 1
Manganese 304 ug/L 06/08/17 15:33 7439-96-506/02/17 11:255.0 1
Nickel ND ug/L 06/08/17 15:33 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:33 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:33 7440-22-406/02/17 11:255.0 1
Sodium 11600 ug/L 06/08/17 15:33 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 20:02 7440-31-506/02/17 11:255.0 1
Vanadium ND ug/L 06/08/17 15:33 7440-62-206/02/17 11:255.0 1
Zinc ND ug/L 06/08/17 15:33 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 15:58 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:20 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/13/17 00:31 56-55-3 L206/05/17 11:4510.0 1
Chrysene ND ug/L 06/13/17 00:31 218-01-9 L206/05/17 11:4510.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 00:31 53-70-306/05/17 11:4510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 00:31 117-81-706/05/17 11:456.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 00:31 193-39-5 L206/05/17 11:4510.0 1
Surrogates
Nitrobenzene-d5 (S)30 %06/13/17 00:31 4165-60-0 1g06/05/17 11:4521-110 1
2-Fluorobiphenyl (S)35 %06/13/17 00:31 321-60-806/05/17 11:4527-110 1
Terphenyl-d14 (S)49 %06/13/17 00:31 1718-51-006/05/17 11:4531-107 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW2 Lab ID:92342317010 Collected:05/31/17 10:15 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 07:17 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 07:17 107-13-110.0 1
Benzene ND ug/L 06/02/17 07:17 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 07:17 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 07:17 75-27-41.0 1
Bromoform ND ug/L 06/02/17 07:17 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 07:17 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 07:17 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 07:17 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/02/17 07:17 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 07:17 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 07:17 75-00-31.0 1
Chloroform ND ug/L 06/02/17 07:17 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 07:17 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 07:17 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 07:17 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 07:17 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 07:17 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 07:17 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 07:17 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 07:17 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 07:17 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 07:17 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 07:17 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 07:17 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 07:17 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 07:17 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 07:17 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 07:17 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 07:17 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 07:17 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 07:17 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 07:17 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 07:17 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 07:17 108-10-15.0 1
Styrene ND ug/L 06/02/17 07:17 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 07:17 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 07:17 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 07:17 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/02/17 07:17 109-99-910.0 1
Toluene ND ug/L 06/02/17 07:17 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 07:17 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 07:17 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 07:17 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 07:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 07:17 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 07:17 108-05-42.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW2 Lab ID:92342317010 Collected:05/31/17 10:15 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 06/02/17 07:17 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 07:17 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 07:17 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)114 %06/02/17 07:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/02/17 07:17 17060-07-070-130 1
Toluene-d8 (S)82 %06/02/17 07:17 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 46200 ug/L 06/05/17 14:5350001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 129000 ug/L 06/06/17 02:09250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 10900 ug/L 06/03/17 21:45 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 13800 ug/L 06/05/17 11:16 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:18 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW5R Lab ID:92342317011 Collected:05/31/17 13:40 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 05/31/17 13:401
Field pH 5.9 Std. Units 05/31/17 13:400.10 1
Field Temperature 21.2 deg C 05/31/17 13:400.50 1
Static Water Level 10.60 feet 05/31/17 13:401
Field Specific Conductance 175.5 umhos/cm 05/31/17 13:401.0 1
Oxygen, Dissolved 5.4 mg/L 05/31/17 13:40 7782-44-71
Total Well Depth 50 feet 05/31/17 13:401
REDOX 182.6 mV 05/31/17 13:401
Turbidity 3.1 NTU 05/31/17 13:401.0 1
Odor NONE 05/31/17 13:401
Appearance CLEAR 05/31/17 13:401
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:36 7440-36-006/02/17 11:255.0 1
Arsenic ND ug/L 06/08/17 15:36 7440-38-206/02/17 11:2510.0 1
Barium 57.1 ug/L 06/08/17 15:36 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:36 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:36 7440-43-906/02/17 11:251.0 1
Chromium 4.6J ug/L 06/08/17 15:36 7440-47-306/02/17 11:255.0 1
Cobalt ND ug/L 06/08/17 15:36 7440-48-406/02/17 11:255.0 1
Copper ND ug/L 06/08/17 15:36 7440-50-806/02/17 11:255.0 1
Iron 68.4 ug/L 06/08/17 15:36 7439-89-606/02/17 11:2550.0 1
Lead ND ug/L 06/08/17 15:36 7439-92-106/02/17 11:255.0 1
Manganese ND ug/L 06/08/17 15:36 7439-96-506/02/17 11:255.0 1
Nickel ND ug/L 06/08/17 15:36 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:36 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:36 7440-22-406/02/17 11:255.0 1
Sodium 13900 ug/L 06/08/17 15:36 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 20:05 7440-31-506/02/17 11:255.0 1
Vanadium 4.4J ug/L 06/08/17 15:36 7440-62-206/02/17 11:255.0 1
Zinc ND ug/L 06/08/17 15:36 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 16:00 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:22 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 18.4J ug/L 06/02/17 07:34 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 07:34 107-13-110.0 1
Benzene ND ug/L 06/02/17 07:34 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 07:34 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 07:34 75-27-41.0 1
Bromoform ND ug/L 06/02/17 07:34 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 07:34 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW5R Lab ID:92342317011 Collected:05/31/17 13:40 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 06/02/17 07:34 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 07:34 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/02/17 07:34 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 07:34 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 07:34 75-00-31.0 1
Chloroform ND ug/L 06/02/17 07:34 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 07:34 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 07:34 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 07:34 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 07:34 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 07:34 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 07:34 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 07:34 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 07:34 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 07:34 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 07:34 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 07:34 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 07:34 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 07:34 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 07:34 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 07:34 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 07:34 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 07:34 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 07:34 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 07:34 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 07:34 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 07:34 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 07:34 108-10-15.0 1
Styrene ND ug/L 06/02/17 07:34 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 07:34 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 07:34 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 07:34 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/02/17 07:34 109-99-910.0 1
Toluene ND ug/L 06/02/17 07:34 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 07:34 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 07:34 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 07:34 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 07:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 07:34 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 07:34 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 07:34 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 07:34 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 07:34 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)113 %06/02/17 07:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/02/17 07:34 17060-07-070-130 1
Toluene-d8 (S)119 %06/02/17 07:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW5R Lab ID:92342317011 Collected:05/31/17 13:40 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 32300 ug/L 06/05/17 15:0550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 156000 ug/L 06/06/17 02:09250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 7740 ug/L 06/03/17 22:03 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 15100 ug/L 06/05/17 11:17 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.4J ug/L 06/07/17 13:19 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW12 Lab ID:92342317012 Collected:05/31/17 15:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 15:451
Field pH 5.9 Std. Units 05/31/17 15:450.10 1
Field Temperature 17.4 deg C 05/31/17 15:450.50 1
Static Water Level 4.64 feet 05/31/17 15:451
Field Specific Conductance 367.4 umhos/cm 05/31/17 15:451.0 1
Oxygen, Dissolved 0.3 mg/L 05/31/17 15:45 7782-44-71
Total Well Depth 15.7 feet 05/31/17 15:451
REDOX 107.5 mV 05/31/17 15:451
Turbidity 9.26 NTU 05/31/17 15:451.0 1
Odor NONE 05/31/17 15:451
Appearance CLEAR 05/31/17 15:451
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/08/17 15:39 7440-36-006/02/17 11:255.0 1
Arsenic ND ug/L 06/08/17 15:39 7440-38-206/02/17 11:2510.0 1
Barium 113 ug/L 06/08/17 15:39 7440-39-306/02/17 11:255.0 1
Beryllium ND ug/L 06/08/17 15:39 7440-41-706/02/17 11:251.0 1
Cadmium ND ug/L 06/08/17 15:39 7440-43-906/02/17 11:251.0 1
Chromium ND ug/L 06/08/17 15:39 7440-47-306/02/17 11:255.0 1
Cobalt ND ug/L 06/08/17 15:39 7440-48-406/02/17 11:255.0 1
Copper ND ug/L 06/08/17 15:39 7440-50-806/02/17 11:255.0 1
Iron 714 ug/L 06/08/17 15:39 7439-89-606/02/17 11:2550.0 1
Lead ND ug/L 06/08/17 15:39 7439-92-106/02/17 11:255.0 1
Manganese 134 ug/L 06/08/17 15:39 7439-96-506/02/17 11:255.0 1
Nickel 4.4J ug/L 06/08/17 15:39 7440-02-006/02/17 11:255.0 1
Selenium ND ug/L 06/08/17 15:39 7782-49-206/02/17 11:2510.0 1
Silver ND ug/L 06/08/17 15:39 7440-22-406/02/17 11:255.0 1
Sodium 16200 ug/L 06/08/17 15:39 7440-23-506/02/17 11:2550001
Tin ND ug/L 06/09/17 20:08 7440-31-506/02/17 11:255.0 1
Vanadium ND ug/L 06/08/17 15:39 7440-62-206/02/17 11:255.0 1
Zinc ND ug/L 06/08/17 15:39 7440-66-606/02/17 11:2510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.021J ug/L 06/06/17 16:02 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:24 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.1J ug/L 06/02/17 07:52 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 07:52 107-13-110.0 1
Benzene ND ug/L 06/02/17 07:52 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 07:52 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 07:52 75-27-41.0 1
Bromoform ND ug/L 06/02/17 07:52 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 07:52 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW12 Lab ID:92342317012 Collected:05/31/17 15:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 06/02/17 07:52 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 07:52 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/02/17 07:52 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 07:52 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 07:52 75-00-31.0 1
Chloroform ND ug/L 06/02/17 07:52 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 07:52 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 07:52 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 07:52 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 07:52 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 07:52 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 07:52 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 07:52 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 07:52 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 07:52 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 07:52 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 07:52 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 07:52 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 07:52 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 07:52 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 07:52 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 07:52 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 07:52 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 07:52 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 07:52 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 07:52 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 07:52 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 07:52 108-10-15.0 1
Styrene ND ug/L 06/02/17 07:52 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 07:52 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 07:52 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 07:52 127-18-41.0 1
Tetrahydrofuran 11.4 ug/L 06/02/17 07:52 109-99-910.0 1
Toluene ND ug/L 06/02/17 07:52 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 07:52 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 07:52 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 07:52 79-01-61.0 1
Trichlorofluoromethane 1.0 ug/L 06/02/17 07:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 07:52 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 07:52 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 07:52 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 07:52 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 07:52 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)119 %06/02/17 07:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %06/02/17 07:52 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 07:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW12 Lab ID:92342317012 Collected:05/31/17 15:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 64500 ug/L 06/05/17 15:5550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 288000 ug/L 06/06/17 02:10250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 86100 ug/L 06/03/17 22:21 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 19700 ug/L 06/05/17 11:18 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:20 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW1 Lab ID:92342317013 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 11:451
Field pH 6.5 Std. Units 05/31/17 11:450.10 1
Field Temperature 21.0 deg C 05/31/17 11:450.50 1
Field Specific Conductance 250.9 umhos/cm 05/31/17 11:451.0 1
Oxygen, Dissolved 4.70 mg/L 05/31/17 11:45 7782-44-71
REDOX -7.1 mV 05/31/17 11:451
Turbidity 15.12 NTU 05/31/17 11:451.0 1
Odor NONE 05/31/17 11:451
Appearance MURKY 05/31/17 11:451
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 01:45 7440-36-006/02/17 12:055.0 1
Arsenic ND ug/L 06/09/17 01:45 7440-38-206/02/17 12:0510.0 1
Barium 86.8 ug/L 06/09/17 01:45 7440-39-306/02/17 12:055.0 1
Beryllium ND ug/L 06/09/17 01:45 7440-41-706/02/17 12:051.0 1
Cadmium ND ug/L 06/09/17 01:45 7440-43-906/02/17 12:051.0 1
Chromium ND ug/L 06/09/17 01:45 7440-47-306/02/17 12:055.0 1
Cobalt ND ug/L 06/09/17 01:45 7440-48-406/02/17 12:055.0 1
Copper ND ug/L 06/09/17 01:45 7440-50-806/02/17 12:055.0 1
Iron 5040 ug/L 06/09/17 01:45 7439-89-606/02/17 12:0550.0 1
Lead ND ug/L 06/09/17 01:45 7439-92-106/02/17 12:055.0 1
Manganese 804 ug/L 06/09/17 01:45 7439-96-506/02/17 12:055.0 1
Nickel ND ug/L 06/09/17 01:45 7440-02-006/02/17 12:055.0 1
Selenium ND ug/L 06/09/17 01:45 7782-49-206/02/17 12:0510.0 1
Silver ND ug/L 06/09/17 01:45 7440-22-406/02/17 12:055.0 1
Sodium 23000 ug/L 06/09/17 11:38 7440-23-506/02/17 12:0550001
Tin ND ug/L 06/09/17 01:45 7440-31-506/02/17 12:055.0 1
Vanadium ND ug/L 06/09/17 01:45 7440-62-206/02/17 12:055.0 1
Zinc 10.1 ug/L 06/09/17 01:45 7440-66-606/02/17 12:0510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 16:04 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:32 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.2J ug/L 06/02/17 08:27 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 08:27 107-13-110.0 1
Benzene ND ug/L 06/02/17 08:27 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 08:27 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 08:27 75-27-41.0 1
Bromoform ND ug/L 06/02/17 08:27 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 08:27 74-83-9 M12.0 1
2-Butanone (MEK)ND ug/L 06/02/17 08:27 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 08:27 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW1 Lab ID:92342317013 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/02/17 08:27 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 08:27 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 08:27 75-00-31.0 1
Chloroform ND ug/L 06/02/17 08:27 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 08:27 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 08:27 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 08:27 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 08:27 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 08:27 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 08:27 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 08:27 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 08:27 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 08:27 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 08:27 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 08:27 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 08:27 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 08:27 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 08:27 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 08:27 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 08:27 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 08:27 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 08:27 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 08:27 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 08:27 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 08:27 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 08:27 108-10-15.0 1
Styrene ND ug/L 06/02/17 08:27 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 08:27 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 08:27 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 08:27 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/02/17 08:27 109-99-910.0 1
Toluene ND ug/L 06/02/17 08:27 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 08:27 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 08:27 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 08:27 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 08:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 08:27 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 08:27 108-05-4 M12.0 1
Vinyl chloride ND ug/L 06/02/17 08:27 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 08:27 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 08:27 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %06/02/17 08:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %06/02/17 08:27 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 08:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW1 Lab ID:92342317013 Collected:05/31/17 11:45 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 33200 ug/L 06/03/17 08:5450001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 143000 ug/L 06/06/17 02:11250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2530 ug/L 06/03/17 22:39 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 49200 ug/L 06/05/17 11:53 16887-00-620002
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.4J ug/L 06/07/17 13:20 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW3 Lab ID:92342317014 Collected:05/31/17 12:25 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 12:251
Field pH 6.6 Std. Units 05/31/17 12:250.10 1
Field Temperature 21.2 deg C 05/31/17 12:250.50 1
Field Specific Conductance 549 umhos/cm 05/31/17 12:251.0 1
Oxygen, Dissolved 4.30 mg/L 05/31/17 12:25 7782-44-71
REDOX -49.6 mV 05/31/17 12:251
Turbidity 7.94 NTU 05/31/17 12:251.0 1
Odor NONE 05/31/17 12:251
Appearance CLEAR 05/31/17 12:251
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 02:03 7440-36-006/02/17 12:055.0 1
Arsenic ND ug/L 06/09/17 02:03 7440-38-206/02/17 12:0510.0 1
Barium 173 ug/L 06/09/17 02:03 7440-39-306/02/17 12:055.0 1
Beryllium ND ug/L 06/09/17 02:03 7440-41-706/02/17 12:051.0 1
Cadmium ND ug/L 06/09/17 02:03 7440-43-906/02/17 12:051.0 1
Chromium ND ug/L 06/09/17 02:03 7440-47-306/02/17 12:055.0 1
Cobalt 3.0J ug/L 06/09/17 02:03 7440-48-406/02/17 12:055.0 1
Copper ND ug/L 06/09/17 02:03 7440-50-806/02/17 12:055.0 1
Iron 8240 ug/L 06/09/17 02:03 7439-89-606/02/17 12:0550.0 1
Lead ND ug/L 06/09/17 02:03 7439-92-106/02/17 12:055.0 1
Manganese 4750 ug/L 06/09/17 02:03 7439-96-506/02/17 12:055.0 1
Nickel 3.6J ug/L 06/09/17 02:03 7440-02-006/02/17 12:055.0 1
Selenium ND ug/L 06/09/17 02:03 7782-49-206/02/17 12:0510.0 1
Silver ND ug/L 06/09/17 02:03 7440-22-406/02/17 12:055.0 1
Sodium 24600 ug/L 06/09/17 11:47 7440-23-506/02/17 12:0550001
Tin ND ug/L 06/09/17 02:03 7440-31-506/02/17 12:055.0 1
Vanadium ND ug/L 06/09/17 02:03 7440-62-206/02/17 12:055.0 1
Zinc ND ug/L 06/09/17 02:03 7440-66-606/02/17 12:0510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 16:06 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:34 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 16.2J ug/L 06/02/17 08:44 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 08:44 107-13-110.0 1
Benzene ND ug/L 06/02/17 08:44 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 08:44 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 08:44 75-27-41.0 1
Bromoform ND ug/L 06/02/17 08:44 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 08:44 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 08:44 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 08:44 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW3 Lab ID:92342317014 Collected:05/31/17 12:25 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/02/17 08:44 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 08:44 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 08:44 75-00-31.0 1
Chloroform ND ug/L 06/02/17 08:44 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 08:44 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 08:44 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 08:44 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 08:44 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 08:44 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 08:44 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 08:44 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 08:44 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 08:44 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 08:44 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 08:44 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 08:44 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 08:44 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 08:44 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 08:44 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 08:44 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 08:44 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 08:44 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 08:44 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 08:44 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 08:44 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 08:44 108-10-15.0 1
Styrene ND ug/L 06/02/17 08:44 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 08:44 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 08:44 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 08:44 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/02/17 08:44 109-99-910.0 1
Toluene ND ug/L 06/02/17 08:44 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 08:44 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 08:44 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 08:44 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 08:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 08:44 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 08:44 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 08:44 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 08:44 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 08:44 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %06/02/17 08:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 08:44 17060-07-070-130 1
Toluene-d8 (S)109 %06/02/17 08:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW3 Lab ID:92342317014 Collected:05/31/17 12:25 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 251000 ug/L 06/03/17 09:0350001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 321000 ug/L 06/06/17 02:12 D6250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 15200 ug/L 06/03/17 22:57 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 18400 ug/L 06/05/17 11:20 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.6J ug/L 06/07/17 13:21 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW4 Lab ID:92342317015 Collected:05/31/17 11:00 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 11:001
Field pH 7.3 Std. Units 05/31/17 11:000.10 1
Field Temperature 20.4 deg C 05/31/17 11:000.50 1
Field Specific Conductance 461.0 umhos/cm 05/31/17 11:001.0 1
Oxygen, Dissolved 6.00 mg/L 05/31/17 11:00 7782-44-71
REDOX -38.5 mV 05/31/17 11:001
Turbidity 7.13 NTU 05/31/17 11:001.0 1
Odor NONE 05/31/17 11:001
Appearance CLEAR 05/31/17 11:001
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 02:06 7440-36-006/02/17 12:055.0 1
Arsenic ND ug/L 06/09/17 02:06 7440-38-206/02/17 12:0510.0 1
Barium 121 ug/L 06/09/17 02:06 7440-39-306/02/17 12:055.0 1
Beryllium ND ug/L 06/09/17 02:06 7440-41-706/02/17 12:051.0 1
Cadmium ND ug/L 06/09/17 02:06 7440-43-906/02/17 12:051.0 1
Chromium ND ug/L 06/09/17 02:06 7440-47-306/02/17 12:055.0 1
Cobalt ND ug/L 06/09/17 02:06 7440-48-406/02/17 12:055.0 1
Copper ND ug/L 06/09/17 02:06 7440-50-806/02/17 12:055.0 1
Iron 1480 ug/L 06/09/17 02:06 7439-89-606/02/17 12:0550.0 1
Lead ND ug/L 06/09/17 02:06 7439-92-106/02/17 12:055.0 1
Manganese 2900 ug/L 06/09/17 02:06 7439-96-506/02/17 12:055.0 1
Nickel ND ug/L 06/09/17 02:06 7440-02-006/02/17 12:055.0 1
Selenium ND ug/L 06/09/17 02:06 7782-49-206/02/17 12:0510.0 1
Silver ND ug/L 06/09/17 02:06 7440-22-406/02/17 12:055.0 1
Sodium 23400 ug/L 06/09/17 11:50 7440-23-506/02/17 12:0550001
Tin ND ug/L 06/09/17 02:06 7440-31-506/02/17 12:055.0 1
Vanadium ND ug/L 06/09/17 02:06 7440-62-206/02/17 12:055.0 1
Zinc ND ug/L 06/09/17 02:06 7440-66-606/02/17 12:0510.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 16:14 7440-28-006/02/17 03:450.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:36 7439-97-606/05/17 20:000.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 16.0J ug/L 06/02/17 09:02 67-64-125.0 1
Acrylonitrile ND ug/L 06/02/17 09:02 107-13-110.0 1
Benzene ND ug/L 06/02/17 09:02 71-43-21.0 1
Bromochloromethane ND ug/L 06/02/17 09:02 74-97-51.0 1
Bromodichloromethane ND ug/L 06/02/17 09:02 75-27-41.0 1
Bromoform ND ug/L 06/02/17 09:02 75-25-21.0 1
Bromomethane ND ug/L 06/02/17 09:02 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/02/17 09:02 78-93-35.0 1
Carbon disulfide ND ug/L 06/02/17 09:02 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW4 Lab ID:92342317015 Collected:05/31/17 11:00 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/02/17 09:02 56-23-51.0 1
Chlorobenzene ND ug/L 06/02/17 09:02 108-90-71.0 1
Chloroethane ND ug/L 06/02/17 09:02 75-00-31.0 1
Chloroform ND ug/L 06/02/17 09:02 67-66-31.0 1
Chloromethane ND ug/L 06/02/17 09:02 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 09:02 96-12-82.0 1
Dibromochloromethane ND ug/L 06/02/17 09:02 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 09:02 106-93-41.0 1
Dibromomethane ND ug/L 06/02/17 09:02 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/02/17 09:02 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/02/17 09:02 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 09:02 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 09:02 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/02/17 09:02 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/02/17 09:02 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/02/17 09:02 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 09:02 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 09:02 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/02/17 09:02 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 09:02 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 09:02 10061-02-61.0 1
Ethylbenzene ND ug/L 06/02/17 09:02 100-41-41.0 1
2-Hexanone ND ug/L 06/02/17 09:02 591-78-65.0 1
Iodomethane ND ug/L 06/02/17 09:02 74-88-45.0 1
Methylene Chloride ND ug/L 06/02/17 09:02 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 09:02 108-10-15.0 1
Styrene ND ug/L 06/02/17 09:02 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 09:02 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 09:02 79-34-51.0 1
Tetrachloroethene ND ug/L 06/02/17 09:02 127-18-41.0 1
Tetrahydrofuran 3.5J ug/L 06/02/17 09:02 109-99-910.0 1
Toluene ND ug/L 06/02/17 09:02 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/02/17 09:02 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/02/17 09:02 79-00-51.0 1
Trichloroethene ND ug/L 06/02/17 09:02 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/02/17 09:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/02/17 09:02 96-18-41.0 1
Vinyl acetate ND ug/L 06/02/17 09:02 108-05-42.0 1
Vinyl chloride ND ug/L 06/02/17 09:02 75-01-41.0 1
m&p-Xylene ND ug/L 06/02/17 09:02 179601-23-12.0 1
o-Xylene ND ug/L 06/02/17 09:02 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)112 %06/02/17 09:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %06/02/17 09:02 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 09:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-SW4 Lab ID:92342317015 Collected:05/31/17 11:00 Received:06/01/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 187000 ug/L 06/03/17 09:1750001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 289000 ug/L 06/06/17 02:13250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 18200 ug/L 06/05/17 17:18 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 27400 ug/L 06/05/17 11:21 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:24 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-TRIP BLANK Lab ID:92342317016 Collected:05/30/17 00:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 18.7J ug/L 06/04/17 20:54 67-64-125.0 1
Acrylonitrile ND ug/L 06/04/17 20:54 107-13-110.0 1
Benzene ND ug/L 06/04/17 20:54 71-43-21.0 1
Bromochloromethane ND ug/L 06/04/17 20:54 74-97-51.0 1
Bromodichloromethane ND ug/L 06/04/17 20:54 75-27-41.0 1
Bromoform ND ug/L 06/04/17 20:54 75-25-21.0 1
Bromomethane ND ug/L 06/04/17 20:54 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/04/17 20:54 78-93-35.0 1
Carbon disulfide ND ug/L 06/04/17 20:54 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/04/17 20:54 56-23-51.0 1
Chlorobenzene ND ug/L 06/04/17 20:54 108-90-71.0 1
Chloroethane ND ug/L 06/04/17 20:54 75-00-31.0 1
Chloroform ND ug/L 06/04/17 20:54 67-66-31.0 1
Chloromethane ND ug/L 06/04/17 20:54 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 20:54 96-12-82.0 1
Dibromochloromethane ND ug/L 06/04/17 20:54 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 20:54 106-93-41.0 1
Dibromomethane ND ug/L 06/04/17 20:54 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/04/17 20:54 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/04/17 20:54 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 20:54 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 20:54 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/04/17 20:54 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/04/17 20:54 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/04/17 20:54 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 20:54 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 20:54 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/04/17 20:54 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 20:54 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 20:54 10061-02-61.0 1
Ethylbenzene ND ug/L 06/04/17 20:54 100-41-41.0 1
2-Hexanone ND ug/L 06/04/17 20:54 591-78-65.0 1
Iodomethane ND ug/L 06/04/17 20:54 74-88-45.0 1
Methylene Chloride ND ug/L 06/04/17 20:54 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 20:54 108-10-15.0 1
Styrene ND ug/L 06/04/17 20:54 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 20:54 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 20:54 79-34-51.0 1
Tetrachloroethene ND ug/L 06/04/17 20:54 127-18-41.0 1
Tetrahydrofuran ND ug/L 06/04/17 20:54 109-99-910.0 1
Toluene ND ug/L 06/04/17 20:54 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/04/17 20:54 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/04/17 20:54 79-00-51.0 1
Trichloroethene ND ug/L 06/04/17 20:54 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/04/17 20:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/04/17 20:54 96-18-41.0 1
Vinyl acetate ND ug/L 06/04/17 20:54 108-05-42.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-TRIP BLANK Lab ID:92342317016 Collected:05/30/17 00:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 06/04/17 20:54 75-01-41.0 1
m&p-Xylene ND ug/L 06/04/17 20:54 179601-23-12.0 1
o-Xylene ND ug/L 06/04/17 20:54 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)111 %06/04/17 20:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %06/04/17 20:54 17060-07-070-130 1
Toluene-d8 (S)113 %06/04/17 20:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW2R Lab ID:92342317017 Collected:06/01/17 10:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JJQ 05/31/17 10:151
Field pH 6.1 Std. Units 05/31/17 10:150.10 1
Field Temperature 24.3 deg C 05/31/17 10:150.50 1
Static Water Level 7.88 feet 05/31/17 10:151
Field Specific Conductance 1246 umhos/cm 05/31/17 10:151.0 1
Oxygen, Dissolved 1.9 mg/L 05/31/17 10:15 7782-44-71
Total Well Depth 21 feet 05/31/17 10:151
REDOX -62.6 mV 05/31/17 10:151
Turbidity 3.4 NTU 05/31/17 10:151.0 1
Odor Sulfuric 05/31/17 10:151
Appearance Clear 05/31/17 10:151
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/08/17 01:34 309-00-206/02/17 13:290.050 1
alpha-BHC ND ug/L 06/08/17 01:34 319-84-606/02/17 13:290.050 1
delta-BHC ND ug/L 06/08/17 01:34 319-86-806/02/17 13:290.050 1
4,4'-DDD ND ug/L 06/08/17 01:34 72-54-806/02/17 13:290.050 1
4,4'-DDT ND ug/L 06/08/17 01:34 50-29-306/02/17 13:290.050 1
Endosulfan I ND ug/L 06/08/17 01:34 959-98-806/02/17 13:290.050 1
Endosulfan II ND ug/L 06/08/17 01:34 33213-65-906/02/17 13:290.050 1
Endrin ND ug/L 06/08/17 01:34 72-20-806/02/17 13:290.050 1
Endrin aldehyde ND ug/L 06/08/17 01:34 7421-93-406/02/17 13:290.050 1
Heptachlor ND ug/L 06/08/17 01:34 76-44-806/02/17 13:290.050 1
Heptachlor epoxide ND ug/L 06/08/17 01:34 1024-57-306/02/17 13:290.050 1
Methoxychlor ND ug/L 06/08/17 01:34 72-43-506/02/17 13:290.15 1
Surrogates
Tetrachloro-m-xylene (S)46 %06/08/17 01:34 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)38 %06/08/17 01:34 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/05/17 18:51 12674-11-206/02/17 13:290.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/05/17 18:51 11104-28-206/02/17 13:290.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/05/17 18:51 11141-16-506/02/17 13:290.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/05/17 18:51 53469-21-906/02/17 13:290.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/05/17 18:51 12672-29-606/02/17 13:290.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/05/17 18:51 11097-69-106/02/17 13:290.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/05/17 18:51 11096-82-506/02/17 13:290.50 1
Surrogates
Decachlorobiphenyl (S)56 %06/05/17 18:51 2051-24-306/02/17 13:2910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 12:56 94-75-7 L106/05/17 16:501.1 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 12:56 93-72-106/05/17 16:500.22 1
Surrogates
2,4-DCAA (S)105 %06/07/17 12:56 19719-28-906/05/17 16:5039-139 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW2R Lab ID:92342317017 Collected:06/01/17 10:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 21:47 7440-36-006/04/17 16:405.0 1
Arsenic ND ug/L 06/14/17 21:47 7440-38-206/04/17 16:4010.0 1
Barium 323 ug/L 06/14/17 21:47 7440-39-306/04/17 16:405.0 1
Beryllium ND ug/L 06/14/17 21:47 7440-41-706/04/17 16:401.0 1
Cadmium ND ug/L 06/14/17 21:47 7440-43-906/04/17 16:401.0 1
Chromium ND ug/L 06/14/17 21:47 7440-47-306/04/17 16:405.0 1
Cobalt 20.6 ug/L 06/14/17 21:47 7440-48-406/04/17 16:405.0 1
Copper ND ug/L 06/14/17 21:47 7440-50-806/04/17 16:405.0 1
Iron 3870 ug/L 06/15/17 12:55 7439-89-606/04/17 16:4050.0 1
Lead ND ug/L 06/14/17 21:47 7439-92-106/04/17 16:405.0 1
Manganese 9200 ug/L 06/14/17 21:47 7439-96-506/04/17 16:405.0 1
Nickel 17.0 ug/L 06/14/17 21:47 7440-02-006/04/17 16:405.0 1
Selenium ND ug/L 06/14/17 21:47 7782-49-206/04/17 16:4010.0 1
Silver ND ug/L 06/14/17 21:47 7440-22-406/04/17 16:405.0 1
Sodium 72400 ug/L 06/14/17 21:47 7440-23-506/04/17 16:4050001
Tin ND ug/L 06/14/17 21:47 7440-31-506/04/17 16:405.0 1
Vanadium ND ug/L 06/14/17 21:47 7440-62-206/04/17 16:405.0 1
Zinc ND ug/L 06/14/17 21:47 7440-66-606/04/17 16:4010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 16:18 7440-28-006/03/17 02:250.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 02:58 7439-97-606/04/17 20:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/13/17 16:11 56-55-306/08/17 16:3210.0 1
Chrysene ND ug/L 06/13/17 16:11 218-01-906/08/17 16:3210.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 16:11 53-70-306/08/17 16:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 16:11 117-81-706/08/17 16:326.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 16:11 193-39-506/08/17 16:3210.0 1
Surrogates
Nitrobenzene-d5 (S)66 %06/13/17 16:11 4165-60-006/08/17 16:3221-110 1
2-Fluorobiphenyl (S)76 %06/13/17 16:11 321-60-806/08/17 16:3227-110 1
Terphenyl-d14 (S)61 %06/13/17 16:11 1718-51-006/08/17 16:3231-107 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.3J ug/L 06/04/17 13:13 67-64-125.0 1
Acrylonitrile ND ug/L 06/04/17 13:13 107-13-110.0 1
Benzene 2.1 ug/L 06/04/17 13:13 71-43-21.0 1
Bromochloromethane ND ug/L 06/04/17 13:13 74-97-51.0 1
Bromodichloromethane ND ug/L 06/04/17 13:13 75-27-41.0 1
Bromoform ND ug/L 06/04/17 13:13 75-25-21.0 1
Bromomethane ND ug/L 06/04/17 13:13 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/04/17 13:13 78-93-35.0 1
Carbon disulfide ND ug/L 06/04/17 13:13 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW2R Lab ID:92342317017 Collected:06/01/17 10:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/04/17 13:13 56-23-51.0 1
Chlorobenzene ND ug/L 06/04/17 13:13 108-90-71.0 1
Chloroethane ND ug/L 06/04/17 13:13 75-00-31.0 1
Chloroform ND ug/L 06/04/17 13:13 67-66-31.0 1
Chloromethane ND ug/L 06/04/17 13:13 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 13:13 96-12-82.0 1
Dibromochloromethane ND ug/L 06/04/17 13:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 13:13 106-93-41.0 1
Dibromomethane ND ug/L 06/04/17 13:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/04/17 13:13 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/04/17 13:13 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 13:13 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 13:13 75-71-81.0 1
1,1-Dichloroethane 0.48J ug/L 06/04/17 13:13 75-34-31.0 1
1,2-Dichloroethane 0.24J ug/L 06/04/17 13:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/04/17 13:13 75-35-41.0 1
cis-1,2-Dichloroethene 0.51J ug/L 06/04/17 13:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 13:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/04/17 13:13 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 13:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 13:13 10061-02-61.0 1
Ethylbenzene ND ug/L 06/04/17 13:13 100-41-41.0 1
2-Hexanone ND ug/L 06/04/17 13:13 591-78-65.0 1
Iodomethane ND ug/L 06/04/17 13:13 74-88-45.0 1
Methylene Chloride ND ug/L 06/04/17 13:13 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 13:13 108-10-15.0 1
Styrene ND ug/L 06/04/17 13:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 13:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 13:13 79-34-51.0 1
Tetrachloroethene ND ug/L 06/04/17 13:13 127-18-41.0 1
Tetrahydrofuran 36.3 ug/L 06/04/17 13:13 109-99-910.0 1
Toluene ND ug/L 06/04/17 13:13 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/04/17 13:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/04/17 13:13 79-00-51.0 1
Trichloroethene 1.0J ug/L 06/04/17 13:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/04/17 13:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/04/17 13:13 96-18-41.0 1
Vinyl acetate ND ug/L 06/04/17 13:13 108-05-42.0 1
Vinyl chloride ND ug/L 06/04/17 13:13 75-01-41.0 1
m&p-Xylene ND ug/L 06/04/17 13:13 179601-23-12.0 1
o-Xylene ND ug/L 06/04/17 13:13 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %06/04/17 13:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %06/04/17 13:13 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 13:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW2R Lab ID:92342317017 Collected:06/01/17 10:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 587000 ug/L 06/05/17 21:1550001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 796000 ug/L 06/07/17 01:521000001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 110000 ug/L 06/06/17 03:20 14808-79-820002
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 50400 ug/L 06/14/17 03:56 16887-00-650005
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:42 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW4R Lab ID:92342317018 Collected:06/01/17 14:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 06/01/17 14:401
Field pH 6.0 Std. Units 06/01/17 14:400.10 1
Field Temperature 14.8 deg C 06/01/17 14:400.50 1
Static Water Level 8.10 feet 06/01/17 14:401
Field Specific Conductance 756.0 umhos/cm 06/01/17 14:401.0 1
Oxygen, Dissolved 0.1 mg/L 06/01/17 14:40 7782-44-71
Total Well Depth 20.0 feet 06/01/17 14:401
REDOX 154.4 mV 06/01/17 14:401
Turbidity 9.93 NTU 06/01/17 14:401.0 1
Odor NONE 06/01/17 14:401
Appearance CLEAR 06/01/17 14:401
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/08/17 01:52 309-00-206/02/17 13:290.050 1
alpha-BHC ND ug/L 06/08/17 01:52 319-84-606/02/17 13:290.050 1
delta-BHC ND ug/L 06/08/17 01:52 319-86-806/02/17 13:290.050 1
4,4'-DDD ND ug/L 06/08/17 01:52 72-54-806/02/17 13:290.050 1
4,4'-DDT ND ug/L 06/08/17 01:52 50-29-306/02/17 13:290.050 1
Endosulfan I ND ug/L 06/08/17 01:52 959-98-806/02/17 13:290.050 1
Endosulfan II ND ug/L 06/08/17 01:52 33213-65-906/02/17 13:290.050 1
Endrin ND ug/L 06/08/17 01:52 72-20-806/02/17 13:290.050 1
Endrin aldehyde ND ug/L 06/08/17 01:52 7421-93-406/02/17 13:290.050 1
Heptachlor ND ug/L 06/08/17 01:52 76-44-806/02/17 13:290.050 1
Heptachlor epoxide ND ug/L 06/08/17 01:52 1024-57-306/02/17 13:290.050 1
Methoxychlor ND ug/L 06/08/17 01:52 72-43-506/02/17 13:290.15 1
Surrogates
Tetrachloro-m-xylene (S)37 %06/08/17 01:52 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)34 %06/08/17 01:52 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/05/17 19:31 12674-11-206/02/17 13:290.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/05/17 19:31 11104-28-206/02/17 13:290.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/05/17 19:31 11141-16-506/02/17 13:290.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/05/17 19:31 53469-21-906/02/17 13:290.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/05/17 19:31 12672-29-606/02/17 13:290.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/05/17 19:31 11097-69-106/02/17 13:290.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/05/17 19:31 11096-82-506/02/17 13:290.50 1
Surrogates
Decachlorobiphenyl (S)41 %06/05/17 19:31 2051-24-306/02/17 13:2910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 13:26 94-75-7 L106/05/17 16:501.0 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 13:26 93-72-106/05/17 16:500.21 1
Surrogates
2,4-DCAA (S)95 %06/07/17 13:26 19719-28-906/05/17 16:5039-139 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW4R Lab ID:92342317018 Collected:06/01/17 14:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 21:50 7440-36-006/04/17 16:405.0 1
Arsenic ND ug/L 06/14/17 21:50 7440-38-206/04/17 16:4010.0 1
Barium 343 ug/L 06/14/17 21:50 7440-39-306/04/17 16:405.0 1
Beryllium ND ug/L 06/14/17 21:50 7440-41-706/04/17 16:401.0 1
Cadmium ND ug/L 06/14/17 21:50 7440-43-906/04/17 16:401.0 1
Chromium ND ug/L 06/14/17 21:50 7440-47-306/04/17 16:405.0 1
Cobalt 59.9 ug/L 06/14/17 21:50 7440-48-406/04/17 16:405.0 1
Copper ND ug/L 06/14/17 21:50 7440-50-806/04/17 16:405.0 1
Iron 302 ug/L 06/15/17 12:58 7439-89-606/04/17 16:4050.0 1
Lead ND ug/L 06/14/17 21:50 7439-92-106/04/17 16:405.0 1
Manganese 801 ug/L 06/14/17 21:50 7439-96-506/04/17 16:405.0 1
Nickel 5.8 ug/L 06/14/17 21:50 7440-02-006/04/17 16:405.0 1
Selenium ND ug/L 06/14/17 21:50 7782-49-206/04/17 16:4010.0 1
Silver ND ug/L 06/14/17 21:50 7440-22-406/04/17 16:405.0 1
Sodium 42100 ug/L 06/14/17 21:50 7440-23-506/04/17 16:4050001
Tin ND ug/L 06/14/17 21:50 7440-31-506/04/17 16:405.0 1
Vanadium ND ug/L 06/14/17 21:50 7440-62-206/04/17 16:405.0 1
Zinc 8.6J ug/L 06/14/17 21:50 7440-66-606/04/17 16:4010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 16:20 7440-28-006/03/17 02:250.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:00 7439-97-606/04/17 20:450.20 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Benzo(a)anthracene ND ug/L 06/13/17 16:44 56-55-306/08/17 16:3210.0 1
Chrysene ND ug/L 06/13/17 16:44 218-01-906/08/17 16:3210.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 16:44 53-70-306/08/17 16:3210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 16:44 117-81-706/08/17 16:326.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 16:44 193-39-506/08/17 16:3210.0 1
Surrogates
Nitrobenzene-d5 (S)69 %06/13/17 16:44 4165-60-006/08/17 16:3221-110 1
2-Fluorobiphenyl (S)80 %06/13/17 16:44 321-60-806/08/17 16:3227-110 1
Terphenyl-d14 (S)82 %06/13/17 16:44 1718-51-006/08/17 16:3231-107 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.0J ug/L 06/04/17 13:31 67-64-125.0 1
Acrylonitrile ND ug/L 06/04/17 13:31 107-13-110.0 1
Benzene ND ug/L 06/04/17 13:31 71-43-21.0 1
Bromochloromethane ND ug/L 06/04/17 13:31 74-97-51.0 1
Bromodichloromethane ND ug/L 06/04/17 13:31 75-27-41.0 1
Bromoform ND ug/L 06/04/17 13:31 75-25-21.0 1
Bromomethane ND ug/L 06/04/17 13:31 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/04/17 13:31 78-93-35.0 1
Carbon disulfide ND ug/L 06/04/17 13:31 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW4R Lab ID:92342317018 Collected:06/01/17 14:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 06/04/17 13:31 56-23-51.0 1
Chlorobenzene ND ug/L 06/04/17 13:31 108-90-71.0 1
Chloroethane ND ug/L 06/04/17 13:31 75-00-31.0 1
Chloroform ND ug/L 06/04/17 13:31 67-66-31.0 1
Chloromethane ND ug/L 06/04/17 13:31 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 13:31 96-12-82.0 1
Dibromochloromethane ND ug/L 06/04/17 13:31 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 13:31 106-93-41.0 1
Dibromomethane ND ug/L 06/04/17 13:31 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/04/17 13:31 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/04/17 13:31 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 13:31 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 13:31 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/04/17 13:31 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/04/17 13:31 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/04/17 13:31 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 13:31 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 13:31 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/04/17 13:31 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 13:31 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 13:31 10061-02-61.0 1
Ethylbenzene ND ug/L 06/04/17 13:31 100-41-41.0 1
2-Hexanone ND ug/L 06/04/17 13:31 591-78-65.0 1
Iodomethane ND ug/L 06/04/17 13:31 74-88-45.0 1
Methylene Chloride ND ug/L 06/04/17 13:31 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 13:31 108-10-15.0 1
Styrene ND ug/L 06/04/17 13:31 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 13:31 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 13:31 79-34-51.0 1
Tetrachloroethene ND ug/L 06/04/17 13:31 127-18-41.0 1
Tetrahydrofuran 9.3J ug/L 06/04/17 13:31 109-99-910.0 1
Toluene ND ug/L 06/04/17 13:31 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/04/17 13:31 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/04/17 13:31 79-00-51.0 1
Trichloroethene ND ug/L 06/04/17 13:31 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/04/17 13:31 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/04/17 13:31 96-18-41.0 1
Vinyl acetate ND ug/L 06/04/17 13:31 108-05-42.0 1
Vinyl chloride ND ug/L 06/04/17 13:31 75-01-41.0 1
m&p-Xylene ND ug/L 06/04/17 13:31 179601-23-12.0 1
o-Xylene ND ug/L 06/04/17 13:31 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)108 %06/04/17 13:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 13:31 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 13:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW4R Lab ID:92342317018 Collected:06/01/17 14:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 315000 ug/L 06/05/17 23:5050001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 552000 ug/L 06/07/17 01:54250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 125000 ug/L 06/06/17 03:37 14808-79-830003
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 35800 ug/L 06/14/17 02:36 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:42 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW10 Lab ID:92342317019 Collected:06/01/17 15:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 06/01/17 15:151
Field pH 6.1 Std. Units 06/01/17 15:150.10 1
Field Temperature 23.0 deg C 06/01/17 15:150.50 1
Static Water Level 11.39 feet 06/01/17 15:151
Field Specific Conductance 1714 umhos/cm 06/01/17 15:151.0 1
Oxygen, Dissolved 0.6 mg/L 06/01/17 15:15 7782-44-71
Total Well Depth 21 feet 06/01/17 15:151
REDOX -58.5 mV 06/01/17 15:151
Turbidity 34.3 NTU 06/01/17 15:151.0 1
Odor NONE 06/01/17 15:151
Appearance CLEAR 06/01/17 15:151
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/08/17 02:10 309-00-206/02/17 13:290.050 1
alpha-BHC ND ug/L 06/08/17 02:10 319-84-606/02/17 13:290.050 1
delta-BHC ND ug/L 06/08/17 02:10 319-86-806/02/17 13:290.050 1
4,4'-DDD ND ug/L 06/08/17 02:10 72-54-806/02/17 13:290.050 1
4,4'-DDT ND ug/L 06/08/17 02:10 50-29-306/02/17 13:290.050 1
Endosulfan I ND ug/L 06/08/17 02:10 959-98-806/02/17 13:290.050 1
Endosulfan II ND ug/L 06/08/17 02:10 33213-65-906/02/17 13:290.050 1
Endrin ND ug/L 06/08/17 02:10 72-20-806/02/17 13:290.050 1
Endrin aldehyde ND ug/L 06/08/17 02:10 7421-93-406/02/17 13:290.050 1
Heptachlor ND ug/L 06/08/17 02:10 76-44-806/02/17 13:290.050 1
Heptachlor epoxide ND ug/L 06/08/17 02:10 1024-57-306/02/17 13:290.050 1
Methoxychlor ND ug/L 06/08/17 02:10 72-43-506/02/17 13:290.15 1
Surrogates
Tetrachloro-m-xylene (S)101 %06/08/17 02:10 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)37 %06/08/17 02:10 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 21:53 7440-36-006/04/17 16:405.0 1
Arsenic ND ug/L 06/14/17 21:53 7440-38-206/04/17 16:4010.0 1
Barium 221 ug/L 06/14/17 21:53 7440-39-306/04/17 16:405.0 1
Beryllium ND ug/L 06/14/17 21:53 7440-41-706/04/17 16:401.0 1
Cadmium ND ug/L 06/14/17 21:53 7440-43-906/04/17 16:401.0 1
Chromium 4.2J ug/L 06/14/17 21:53 7440-47-306/04/17 16:405.0 1
Cobalt 21.8 ug/L 06/14/17 21:53 7440-48-406/04/17 16:405.0 1
Copper ND ug/L 06/14/17 21:53 7440-50-806/04/17 16:405.0 1
Iron 2400 ug/L 06/15/17 13:01 7439-89-606/04/17 16:4050.0 1
Lead 4.1J ug/L 06/14/17 21:53 7439-92-106/04/17 16:405.0 1
Manganese 8390 ug/L 06/14/17 21:53 7439-96-506/04/17 16:405.0 1
Nickel 6.9 ug/L 06/14/17 21:53 7440-02-006/04/17 16:405.0 1
Selenium ND ug/L 06/14/17 21:53 7782-49-206/04/17 16:4010.0 1
Silver ND ug/L 06/14/17 21:53 7440-22-406/04/17 16:405.0 1
Sodium 123000 ug/L 06/15/17 13:17 7440-23-506/04/17 16:405000010
Tin ND ug/L 06/14/17 21:53 7440-31-506/04/17 16:405.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW10 Lab ID:92342317019 Collected:06/01/17 15:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Vanadium 2.7J ug/L 06/14/17 21:53 7440-62-206/04/17 16:405.0 1
Zinc 5.4J ug/L 06/14/17 21:53 7440-66-606/04/17 16:4010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.043J ug/L 06/09/17 16:22 7440-28-006/03/17 02:250.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:02 7439-97-606/04/17 20:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 22.5J ug/L 06/04/17 13:48 67-64-125.0 1
Acrylonitrile ND ug/L 06/04/17 13:48 107-13-110.0 1
Benzene ND ug/L 06/04/17 13:48 71-43-21.0 1
Bromochloromethane ND ug/L 06/04/17 13:48 74-97-51.0 1
Bromodichloromethane ND ug/L 06/04/17 13:48 75-27-41.0 1
Bromoform ND ug/L 06/04/17 13:48 75-25-21.0 1
Bromomethane ND ug/L 06/04/17 13:48 74-83-92.0 1
2-Butanone (MEK)ND ug/L 06/04/17 13:48 78-93-35.0 1
Carbon disulfide 2.0 ug/L 06/04/17 13:48 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/04/17 13:48 56-23-51.0 1
Chlorobenzene ND ug/L 06/04/17 13:48 108-90-71.0 1
Chloroethane ND ug/L 06/04/17 13:48 75-00-31.0 1
Chloroform ND ug/L 06/04/17 13:48 67-66-31.0 1
Chloromethane ND ug/L 06/04/17 13:48 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 13:48 96-12-82.0 1
Dibromochloromethane ND ug/L 06/04/17 13:48 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 13:48 106-93-41.0 1
Dibromomethane ND ug/L 06/04/17 13:48 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/04/17 13:48 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/04/17 13:48 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 13:48 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 13:48 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/04/17 13:48 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/04/17 13:48 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/04/17 13:48 75-35-41.0 1
cis-1,2-Dichloroethene 0.20J ug/L 06/04/17 13:48 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 13:48 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/04/17 13:48 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 13:48 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 13:48 10061-02-61.0 1
Ethylbenzene 0.53J ug/L 06/04/17 13:48 100-41-41.0 1
2-Hexanone ND ug/L 06/04/17 13:48 591-78-65.0 1
Iodomethane ND ug/L 06/04/17 13:48 74-88-45.0 1
Methylene Chloride ND ug/L 06/04/17 13:48 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)2.8J ug/L 06/04/17 13:48 108-10-15.0 1
Styrene ND ug/L 06/04/17 13:48 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW10 Lab ID:92342317019 Collected:06/01/17 15:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 13:48 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 13:48 79-34-51.0 1
Tetrachloroethene ND ug/L 06/04/17 13:48 127-18-41.0 1
Tetrahydrofuran 182 ug/L 06/04/17 13:48 109-99-910.0 1
Toluene 0.27J ug/L 06/04/17 13:48 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/04/17 13:48 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/04/17 13:48 79-00-51.0 1
Trichloroethene ND ug/L 06/04/17 13:48 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/04/17 13:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/04/17 13:48 96-18-41.0 1
Vinyl acetate ND ug/L 06/04/17 13:48 108-05-42.0 1
Vinyl chloride ND ug/L 06/04/17 13:48 75-01-41.0 1
m&p-Xylene 1.2J ug/L 06/04/17 13:48 179601-23-12.0 1
o-Xylene 1.0 ug/L 06/04/17 13:48 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %06/04/17 13:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %06/04/17 13:48 17060-07-070-130 1
Toluene-d8 (S)107 %06/04/17 13:48 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 446000 ug/L 06/06/17 00:0650001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 1150000 ug/L 06/07/17 01:551000001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 333000 ug/L 06/11/17 09:41 14808-79-860006
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 318000 ug/L 06/14/17 03:58 16887-00-6 M6,R11000010
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:43 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW11 Lab ID:92342317020 Collected:06/01/17 12:05 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 06/01/17 12:051
Field pH 5.9 Std. Units 06/01/17 12:050.10 1
Field Temperature 16.6 deg C 06/01/17 12:050.50 1
Static Water Level 3.92 feet 06/01/17 12:051
Field Specific Conductance 354.9 umhos/cm 06/01/17 12:051.0 1
Oxygen, Dissolved 0.3 mg/L 06/01/17 12:05 7782-44-71
Total Well Depth 20.0 feet 06/01/17 12:051
REDOX -10.4 mV 06/01/17 12:051
Turbidity 8.58 NTU 06/01/17 12:051.0 1
Odor NONE 06/01/17 12:051
Appearance CLEAR 06/01/17 12:051
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 21:56 7440-36-006/04/17 16:405.0 1
Arsenic ND ug/L 06/14/17 21:56 7440-38-206/04/17 16:4010.0 1
Barium 102 ug/L 06/14/17 21:56 7440-39-306/04/17 16:405.0 1
Beryllium ND ug/L 06/14/17 21:56 7440-41-706/04/17 16:401.0 1
Cadmium ND ug/L 06/14/17 21:56 7440-43-906/04/17 16:401.0 1
Chromium ND ug/L 06/14/17 21:56 7440-47-306/04/17 16:405.0 1
Cobalt ND ug/L 06/14/17 21:56 7440-48-406/04/17 16:405.0 1
Copper ND ug/L 06/14/17 21:56 7440-50-806/04/17 16:405.0 1
Iron 26700 ug/L 06/15/17 13:14 7439-89-606/04/17 16:4050.0 1
Lead ND ug/L 06/14/17 21:56 7439-92-106/04/17 16:405.0 1
Manganese 1720 ug/L 06/14/17 21:56 7439-96-506/04/17 16:405.0 1
Nickel ND ug/L 06/14/17 21:56 7440-02-006/04/17 16:405.0 1
Selenium ND ug/L 06/14/17 21:56 7782-49-206/04/17 16:4010.0 1
Silver ND ug/L 06/14/17 21:56 7440-22-406/04/17 16:405.0 1
Sodium 11700 ug/L 06/14/17 21:56 7440-23-506/04/17 16:4050001
Tin ND ug/L 06/14/17 21:56 7440-31-506/04/17 16:405.0 1
Vanadium ND ug/L 06/14/17 21:56 7440-62-206/04/17 16:405.0 1
Zinc ND ug/L 06/14/17 21:56 7440-66-606/04/17 16:4010.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 16:24 7440-28-006/03/17 02:250.10 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:05 7439-97-606/04/17 20:450.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 21.1J ug/L 06/04/17 14:06 67-64-125.0 1
Acrylonitrile ND ug/L 06/04/17 14:06 107-13-110.0 1
Benzene ND ug/L 06/04/17 14:06 71-43-21.0 1
Bromochloromethane ND ug/L 06/04/17 14:06 74-97-51.0 1
Bromodichloromethane ND ug/L 06/04/17 14:06 75-27-41.0 1
Bromoform ND ug/L 06/04/17 14:06 75-25-21.0 1
Bromomethane ND ug/L 06/04/17 14:06 74-83-92.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 69 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW11 Lab ID:92342317020 Collected:06/01/17 12:05 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Butanone (MEK)ND ug/L 06/04/17 14:06 78-93-35.0 1
Carbon disulfide ND ug/L 06/04/17 14:06 75-15-02.0 1
Carbon tetrachloride ND ug/L 06/04/17 14:06 56-23-51.0 1
Chlorobenzene ND ug/L 06/04/17 14:06 108-90-71.0 1
Chloroethane ND ug/L 06/04/17 14:06 75-00-31.0 1
Chloroform ND ug/L 06/04/17 14:06 67-66-31.0 1
Chloromethane 0.23J ug/L 06/04/17 14:06 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 14:06 96-12-82.0 1
Dibromochloromethane ND ug/L 06/04/17 14:06 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 14:06 106-93-41.0 1
Dibromomethane ND ug/L 06/04/17 14:06 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/04/17 14:06 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 06/04/17 14:06 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 14:06 110-57-6 L11.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 14:06 75-71-81.0 1
1,1-Dichloroethane ND ug/L 06/04/17 14:06 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/04/17 14:06 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/04/17 14:06 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 14:06 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 14:06 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/04/17 14:06 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 14:06 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 14:06 10061-02-61.0 1
Ethylbenzene ND ug/L 06/04/17 14:06 100-41-41.0 1
2-Hexanone ND ug/L 06/04/17 14:06 591-78-65.0 1
Iodomethane ND ug/L 06/04/17 14:06 74-88-45.0 1
Methylene Chloride ND ug/L 06/04/17 14:06 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 14:06 108-10-15.0 1
Styrene ND ug/L 06/04/17 14:06 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 14:06 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 14:06 79-34-51.0 1
Tetrachloroethene ND ug/L 06/04/17 14:06 127-18-41.0 1
Tetrahydrofuran 4.5J ug/L 06/04/17 14:06 109-99-910.0 1
Toluene ND ug/L 06/04/17 14:06 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 06/04/17 14:06 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/04/17 14:06 79-00-51.0 1
Trichloroethene ND ug/L 06/04/17 14:06 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/04/17 14:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/04/17 14:06 96-18-41.0 1
Vinyl acetate ND ug/L 06/04/17 14:06 108-05-42.0 1
Vinyl chloride ND ug/L 06/04/17 14:06 75-01-41.0 1
m&p-Xylene ND ug/L 06/04/17 14:06 179601-23-12.0 1
o-Xylene ND ug/L 06/04/17 14:06 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %06/04/17 14:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 14:06 17060-07-070-130 1
Toluene-d8 (S)106 %06/04/17 14:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 199
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342317
OSR
Sample:3412-MW11 Lab ID:92342317020 Collected:06/01/17 12:05 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 135000 ug/L 06/06/17 00:26 M150001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 226000 ug/L 06/07/17 01:55250001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-81001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 14100 ug/L 06/10/17 19:28 14808-79-810001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 13500 ug/L 06/14/17 02:46 16887-00-610001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:44 57-12-58.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362989
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012264
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 06/02/17 02:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012265LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012266MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342318021
2012267
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 96 75-12594 22.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363241
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013873
Associated Lab Samples:92342317005
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 06/07/17 03:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013874LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013875MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281010
2013876
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12592 02.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363333
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014275
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 06/07/17 02:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014276LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342769001
2014278
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L M1125075-1250125NDNDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363457
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015058
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 06/07/17 00:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015059LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015060MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342619002
2015061
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-125101 12.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363006
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012403
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 06/10/17 07:26
Arsenic ug/L ND 10.0 06/10/17 07:26
Barium ug/L ND 5.0 06/10/17 07:26
Beryllium ug/L ND 1.0 06/10/17 07:26
Cadmium ug/L ND 1.0 06/10/17 07:26
Chromium ug/L ND 5.0 06/10/17 07:26
Cobalt ug/L ND 5.0 06/10/17 07:26
Copper ug/L ND 5.0 06/10/17 07:26
Iron ug/L ND 50.0 06/10/17 07:26
Lead ug/L ND 5.0 06/10/17 07:26
Manganese ug/L ND 5.0 06/10/17 07:26
Nickel ug/L ND 5.0 06/10/17 07:26
Selenium ug/L ND 10.0 06/10/17 07:26
Silver ug/L ND 5.0 06/10/17 07:26
Sodium ug/L ND 5000 06/10/17 07:26
Tin ug/L ND 5.0 06/10/17 07:26
Vanadium ug/L ND 5.0 06/10/17 07:26
Zinc ug/L ND 10.0 06/10/17 07:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012404LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 485500 97 80-120
Barium ug/L 523500 105 80-120
Beryllium ug/L 500500 100 80-120
Cadmium ug/L 526500 105 80-120
Chromium ug/L 508500 102 80-120
Cobalt ug/L 514500 103 80-120
Copper ug/L 509500 102 80-120
Iron ug/L 49205000 98 80-120
Lead ug/L 509500 102 80-120
Manganese ug/L 498500 100 80-120
Nickel ug/L 515500 103 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 251250 101 80-120
Sodium ug/L 50405000 101 80-120
Tin ug/L 514500 103 80-120
Vanadium ug/L 489500 98 80-120
Zinc ug/L 514500 103 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012405MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317001
2012406
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-125100 0500ND503501
Arsenic ug/L 500 96 75-12595 1500ND480475
Barium ug/L 500 103 75-125102 0500ND513511
Beryllium ug/L 500 98 75-12598 0500ND491490
Cadmium ug/L 500 104 75-125103 1500ND518516
Chromium ug/L 500 101 75-125100 0500ND504501
Cobalt ug/L 500 102 75-125101 0500ND509506
Copper ug/L M1500-52 75-125-52 0500761501501
Iron ug/L 5000 97 75-12596 1500027.1J 4870 4820
Lead ug/L 500 97 75-12597 150018.2 506 501
Manganese ug/L 500 99 75-12598 1500ND494491
Nickel ug/L 500 102 75-125101 0500ND508506
Selenium ug/L 500 100 75-125100 0500ND504503
Silver ug/L 250 100 75-12599 1250ND251248
Sodium ug/L 5000 102 75-125101 15000ND50905040
Tin ug/L 500 101 75-125101 15004.0J 511 508
Vanadium ug/L 500 97 75-12596 1500ND486482
Zinc ug/L M15001175-12510 1500455510507
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363145
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013273
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 06/08/17 14:18
Arsenic ug/L ND 10.0 06/08/17 14:18
Barium ug/L ND 5.0 06/08/17 14:18
Beryllium ug/L ND 1.0 06/08/17 14:18
Cadmium ug/L ND 1.0 06/08/17 14:18
Chromium ug/L 2.6J 5.0 06/08/17 14:18
Cobalt ug/L ND 5.0 06/08/17 14:18
Copper ug/L ND 5.0 06/08/17 14:18
Iron ug/L ND 50.0 06/08/17 14:18
Lead ug/L ND 5.0 06/08/17 14:18
Manganese ug/L ND 5.0 06/08/17 14:18
Nickel ug/L ND 5.0 06/08/17 14:18
Selenium ug/L ND 10.0 06/08/17 14:18
Silver ug/L ND 5.0 06/08/17 14:18
Sodium ug/L ND 5000 06/08/17 14:18
Tin ug/L ND 5.0 06/08/17 20:57
Vanadium ug/L ND 5.0 06/08/17 14:18
Zinc ug/L ND 10.0 06/08/17 14:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013274LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 512500 102 80-120
Arsenic ug/L 490500 98 80-120
Barium ug/L 507500 101 80-120
Beryllium ug/L 508500 102 80-120
Cadmium ug/L 507500 101 80-120
Chromium ug/L 505500 101 80-120
Cobalt ug/L 508500 102 80-120
Copper ug/L 511500 102 80-120
Iron ug/L 50005000 100 80-120
Lead ug/L 500500 100 80-120
Manganese ug/L 506500 101 80-120
Nickel ug/L 497500 99 80-120
Selenium ug/L 517500 103 80-120
Silver ug/L 254250 102 80-120
Sodium ug/L 4850J5000 97 80-120
Tin ug/L 510500 102 80-120
Vanadium ug/L 498500 100 80-120
Zinc ug/L 510500 102 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 78 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013275MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342480001
2013276
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-125100 1500ND493499
Arsenic ug/L 500 95 75-12596 1500ND477482
Barium ug/L 500 99 75-125100 150033.2 528 531
Beryllium ug/L 500 99 75-125100 1500ND495500
Cadmium ug/L 500 98 75-12599 1500ND491496
Chromium ug/L 500 98 75-12599 1500ND489494
Cobalt ug/L 500 98 75-12599 15004.9J 496 501
Copper ug/L 500 99 75-125100 1500ND498500
Iron ug/L 5000 97 75-12597 1500058354205450
Lead ug/L 500 96 75-12597 1500ND480486
Manganese ug/L 500 96 75-12594 1500349831819
Nickel ug/L 500 96 75-12597 1500ND484489
Selenium ug/L 500 98 75-125100 2500ND492501
Silver ug/L 250 98 75-12598 0250ND245246
Sodium ug/L 5000 96 75-12589 25000104001510014800
Tin ug/L 500 99 75-125100 1500ND495502
Vanadium ug/L 500 97 75-12597 0500ND484486
Zinc ug/L 500 99 75-125100 15005.2J 498 504
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363147
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013281
Associated Lab Samples:92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 06/09/17 11:23
Arsenic ug/L ND 10.0 06/09/17 11:23
Barium ug/L ND 5.0 06/09/17 11:23
Beryllium ug/L ND 1.0 06/09/17 11:23
Cadmium ug/L ND 1.0 06/09/17 11:23
Chromium ug/L ND 5.0 06/09/17 11:23
Cobalt ug/L ND 5.0 06/09/17 11:23
Copper ug/L ND 5.0 06/09/17 11:23
Iron ug/L ND 50.0 06/09/17 11:23
Lead ug/L ND 5.0 06/09/17 11:23
Manganese ug/L ND 5.0 06/09/17 11:23
Nickel ug/L ND 5.0 06/09/17 11:23
Selenium ug/L ND 10.0 06/09/17 11:23
Silver ug/L ND 5.0 06/09/17 11:23
Sodium ug/L ND 5000 06/09/17 11:23
Tin ug/L ND 5.0 06/09/17 11:23
Vanadium ug/L ND 5.0 06/09/17 11:23
Zinc ug/L ND 10.0 06/09/17 11:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013282LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 498500 100 80-120
Arsenic ug/L 476500 95 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 494500 99 80-120
Cadmium ug/L 502500 100 80-120
Chromium ug/L 496500 99 80-120
Cobalt ug/L 499500 100 80-120
Copper ug/L 500500 100 80-120
Iron ug/L 48605000 97 80-120
Lead ug/L 491500 98 80-120
Manganese ug/L 493500 99 80-120
Nickel ug/L 493500 99 80-120
Selenium ug/L 503500 101 80-120
Silver ug/L 248250 99 80-120
Sodium ug/L 4880J5000 98 80-120
Tin ug/L 499500 100 80-120
Vanadium ug/L 485500 97 80-120
Zinc ug/L 497500 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013283MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317013
2013284
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 100 75-125100 0500ND501500
Arsenic ug/L 500 98 75-12598 1500ND492488
Barium ug/L 500 100 75-125100 050086.8 589 587
Beryllium ug/L 500 104 75-125103 1500ND519516
Cadmium ug/L 500 99 75-12598 1500ND494491
Chromium ug/L 500 101 75-125100 1500ND505500
Cobalt ug/L 500 100 75-12599 1500ND498494
Copper ug/L 500 104 75-125103 0500ND519518
Iron ug/L 5000 101 75-125100 1500050401010010000
Lead ug/L 500 97 75-12596 1500ND487483
Manganese ug/L 500 99 75-12597 150080413001290
Nickel ug/L 500 96 75-12595 1500ND482478
Selenium ug/L 500 101 75-125100 1500ND507502
Silver ug/L 250 103 75-125102 0250ND257256
Sodium ug/L 5000 92 75-12589 15000230002760027500
Tin ug/L 500 101 75-125100 0500ND503501
Vanadium ug/L 500 101 75-125101 0500ND507505
Zinc ug/L 500 101 75-125100 150010.1 514 509
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 06/14/17 21:19
Arsenic ug/L ND 10.0 06/14/17 21:19
Barium ug/L ND 5.0 06/14/17 21:19
Beryllium ug/L ND 1.0 06/14/17 21:19
Cadmium ug/L ND 1.0 06/14/17 21:19
Chromium ug/L ND 5.0 06/14/17 21:19
Cobalt ug/L ND 5.0 06/14/17 21:19
Copper ug/L ND 5.0 06/14/17 21:19
Iron ug/L ND 50.0 06/14/17 21:19
Lead ug/L ND 5.0 06/14/17 21:19
Manganese ug/L ND 5.0 06/14/17 21:19
Nickel ug/L ND 5.0 06/14/17 21:19
Selenium ug/L ND 10.0 06/14/17 21:19
Silver ug/L ND 5.0 06/14/17 21:19
Sodium ug/L ND 5000 06/14/17 21:19
Tin ug/L ND 5.0 06/14/17 21:19
Vanadium ug/L ND 5.0 06/14/17 21:19
Zinc ug/L ND 10.0 06/14/17 21:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Iron ug/L 43505000 87 80-120
Lead ug/L 486500 97 80-120
Manganese ug/L 457500 91 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Sodium ug/L 4710J5000 94 80-120
Tin ug/L 485500 97 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3500ND517501
Arsenic ug/L 500 100 75-12597 2500174672657
Barium ug/L 500 108 75-125104 35008.0 546 530
Beryllium ug/L 500 96 75-12594 25000.73J 481 471
Cadmium ug/L 500 108 75-125105 35001.7 540 524
Chromium ug/L 500 97 75-12594 3500ND486470
Cobalt ug/L 500 104 75-125100 350075.0 594 577
Copper ug/L 500 104 75-125102 3500ND522509
Iron ug/L 5000 117 75-125101 15000843009010089400
Lead ug/L 500 100 75-12597 35004.4J 506 491
Manganese ug/L 500 103 75-12590 1500428047904730
Nickel ug/L 500 96 75-12593 35003.2J 481 466
Selenium ug/L 500 102 75-125100 2500ND511501
Silver ug/L 250 99 75-12595 4250ND246238
Sodium ug/L 5000 100 75-12596 1500074901250012300
Tin ug/L 500 101 75-12597 4500ND503484
Vanadium ug/L 500 96 75-12593 3500ND482466
Zinc ug/L 500 98 75-12595 35005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362965
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012152
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 06/06/17 12:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012153LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 99.4100 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012154MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342318021
2012155
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-125100 11000.061J 99.7 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362966
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012156
Associated Lab Samples:92342317005
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 06/06/17 16:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012157LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 98.2100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012158MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317005
2012159
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 95 75-12597 11000.048J 95.5 96.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363105
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013133
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 06/06/17 15:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013134LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.0100 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013135MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317006
2013136
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-12598 2100ND99.8 98.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363273
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014038
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Thallium ug/L ND 0.10 06/09/17 16:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014039LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 91.8100 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014040MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342600010
2014041
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Thallium ug/L 100 91 75-12593 3100ND90.7 93.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362875
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011671
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/31/17 15:18
1,1,1-Trichloroethane ug/L ND 1.0 05/31/17 15:18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/31/17 15:18
1,1,2-Trichloroethane ug/L ND 1.0 05/31/17 15:18
1,1-Dichloroethane ug/L ND 1.0 05/31/17 15:18
1,1-Dichloroethene ug/L ND 1.0 05/31/17 15:18
1,2,3-Trichloropropane ug/L ND 1.0 05/31/17 15:18
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/31/17 15:18
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/31/17 15:18
1,2-Dichlorobenzene ug/L ND 1.0 05/31/17 15:18
1,2-Dichloroethane ug/L ND 1.0 05/31/17 15:18
1,2-Dichloropropane ug/L ND 1.0 05/31/17 15:18
1,4-Dichlorobenzene ug/L ND 1.0 05/31/17 15:18
2-Butanone (MEK)ug/L ND 5.0 05/31/17 15:18
2-Hexanone ug/L ND 5.0 05/31/17 15:18
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/31/17 15:18
Acetone ug/L ND 25.0 05/31/17 15:18
Acrylonitrile ug/L ND 10.0 05/31/17 15:18
Benzene ug/L ND 1.0 05/31/17 15:18
Bromochloromethane ug/L ND 1.0 05/31/17 15:18
Bromodichloromethane ug/L ND 1.0 05/31/17 15:18
Bromoform ug/L ND 1.0 05/31/17 15:18
Bromomethane ug/L ND 2.0 05/31/17 15:18
Carbon disulfide ug/L ND 2.0 05/31/17 15:18
Carbon tetrachloride ug/L ND 1.0 05/31/17 15:18
Chlorobenzene ug/L ND 1.0 05/31/17 15:18
Chloroethane ug/L ND 1.0 05/31/17 15:18
Chloroform ug/L ND 1.0 05/31/17 15:18
Chloromethane ug/L ND 1.0 05/31/17 15:18
cis-1,2-Dichloroethene ug/L ND 1.0 05/31/17 15:18
cis-1,3-Dichloropropene ug/L ND 1.0 05/31/17 15:18
Dibromochloromethane ug/L ND 1.0 05/31/17 15:18
Dibromomethane ug/L ND 1.0 05/31/17 15:18
Dichlorodifluoromethane ug/L ND 1.0 05/31/17 15:18
Ethylbenzene ug/L ND 1.0 05/31/17 15:18
Iodomethane ug/L ND 5.0 05/31/17 15:18
m&p-Xylene ug/L ND 2.0 05/31/17 15:18
Methylene Chloride ug/L ND 1.0 05/31/17 15:18
o-Xylene ug/L ND 1.0 05/31/17 15:18
Styrene ug/L ND 1.0 05/31/17 15:18
Tetrachloroethene ug/L ND 1.0 05/31/17 15:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011671
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Tetrahydrofuran ug/L ND 10.0 05/31/17 15:18
Toluene ug/L ND 1.0 05/31/17 15:18
trans-1,2-Dichloroethene ug/L ND 1.0 05/31/17 15:18
trans-1,3-Dichloropropene ug/L ND 1.0 05/31/17 15:18
trans-1,4-Dichloro-2-butene ug/L ND 1.0 05/31/17 15:18
Trichloroethene ug/L ND 1.0 05/31/17 15:18
Trichlorofluoromethane ug/L ND 1.0 05/31/17 15:18
Vinyl acetate ug/L ND 2.0 05/31/17 15:18
Vinyl chloride ug/L ND 1.0 05/31/17 15:18
1,2-Dichloroethane-d4 (S)%104 70-130 05/31/17 15:18
4-Bromofluorobenzene (S)%101 70-130 05/31/17 15:18
Toluene-d8 (S)%108 70-130 05/31/17 15:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011672LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 80-125
1,1,1-Trichloroethane ug/L 51.150 102 71-129
1,1,2,2-Tetrachloroethane ug/L 51.650 103 79-124
1,1,2-Trichloroethane ug/L 49.950 100 85-125
1,1-Dichloroethane ug/L 48.150 96 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,2,3-Trichloropropane ug/L 51.350 103 75-130
1,2-Dibromo-3-chloropropane ug/L 57.750 115 71-133
1,2-Dibromoethane (EDB)ug/L 55.050 110 83-124
1,2-Dichlorobenzene ug/L 52.650 105 80-133
1,2-Dichloroethane ug/L 49.650 99 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
1,4-Dichlorobenzene ug/L 51.250 102 78-130
2-Butanone (MEK)ug/L 125100 125 61-144
2-Hexanone ug/L 119100 119 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 136100 136 48-146
Acrylonitrile ug/L 255250 102 40-160
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 49.250 98 71-125
Bromodichloromethane ug/L 53.250 106 78-124
Bromoform ug/L 45.350 91 71-128
Bromomethane ug/L 39.850 80 40-160
Carbon disulfide ug/L 52.650 105 50-160
Carbon tetrachloride ug/L 52.050 104 69-131
Chlorobenzene ug/L 51.350 103 81-122
Chloroethane ug/L 40.750 81 39-148
Chloroform ug/L 50.650 101 73-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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Page 89 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011672LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 53.750 107 44-146
cis-1,2-Dichloroethene ug/L 49.050 98 74-124
cis-1,3-Dichloropropene ug/L 56.150 112 72-132
Dibromochloromethane ug/L 51.750 103 78-125
Dibromomethane ug/L 51.150 102 82-120
Dichlorodifluoromethane ug/L 40.250 80 34-157
Ethylbenzene ug/L 52.050 104 79-121
Iodomethane ug/L 97.1100 97 39-154
m&p-Xylene ug/L 102100 102 81-124
Methylene Chloride ug/L 51.150 102 64-133
o-Xylene ug/L 51.150 102 79-131
Styrene ug/L 51.350 103 84-126
Tetrachloroethene ug/L 50.550 101 78-122
Tetrahydrofuran ug/L 561500 112 69-148
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 47.750 95 71-127
trans-1,3-Dichloropropene ug/L 57.350 115 69-141
trans-1,4-Dichloro-2-butene ug/L 98.6 L15019740-160
Trichloroethene ug/L 52.750 105 78-122
Trichlorofluoromethane ug/L 47.250 94 53-137
Vinyl acetate ug/L 118100 118 40-160
Vinyl chloride ug/L 45.450 91 58-137
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2011673MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317002
1,1,1,2-Tetrachloroethane ug/L 23.720 118 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.420 97 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 22.120 111 70-130ND
1,1-Dichloroethene ug/L 23.220 116 70-166ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 26.020 130 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.720 118 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 21.520 107 70-130ND
1,2-Dichloropropane ug/L 23.420 117 70-130ND
1,4-Dichlorobenzene ug/L 22.320 111 70-130ND
2-Butanone (MEK)ug/L 49.240 123 70-130ND
2-Hexanone ug/L 54.1 M14013570-130ND
4-Methyl-2-pentanone (MIBK)ug/L 48.640 121 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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Page 90 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2011673MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317002
Acetone ug/L 65.440 124 70-13015.8J
Acrylonitrile ug/L 118100 118 70-130ND
Benzene ug/L 23.420 117 70-148ND
Bromochloromethane ug/L 23.320 116 70-130ND
Bromodichloromethane ug/L 23.720 119 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 13.1 M1206670-130ND
Carbon disulfide ug/L 23.020 115 70-130ND
Carbon tetrachloride ug/L 23.320 116 70-130ND
Chlorobenzene ug/L 22.920 114 70-146ND
Chloroethane ug/L 20.720 103 70-130ND
Chloroform ug/L 23.120 116 70-130ND
Chloromethane ug/L 23.320 116 70-130ND
cis-1,2-Dichloroethene ug/L 22.220 111 70-130ND
cis-1,3-Dichloropropene ug/L 22.720 114 70-130ND
Dibromochloromethane ug/L 21.720 108 70-130ND
Dibromomethane ug/L 23.320 117 70-130ND
Dichlorodifluoromethane ug/L 18.820 94 70-130ND
Ethylbenzene ug/L 23.720 118 70-130ND
Iodomethane ug/L 35.740 89 70-130ND
m&p-Xylene ug/L 46.540 116 70-130ND
Methylene Chloride ug/L 22.620 113 70-130ND
o-Xylene ug/L 23.120 115 70-130ND
Styrene ug/L 22.520 112 70-130ND
Tetrachloroethene ug/L 22.920 114 70-130ND
Tetrahydrofuran ug/L 255200 128 70-130ND
Toluene ug/L 21.820 109 70-155ND
trans-1,2-Dichloroethene ug/L 22.220 111 70-130ND
trans-1,3-Dichloropropene ug/L 23.320 116 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.620 98 70-130ND
Trichloroethene ug/L 22.720 114 69-151ND
Trichlorofluoromethane ug/L 23.220 116 70-130ND
Vinyl acetate ug/L 42.440 106 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%91 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92342317003
2011674SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342317003
2011674SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L 1.3 161.5
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L 1.1 221.4
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%108 8100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342317003
2011674SAMPLE DUPLICATE:
4-Bromofluorobenzene (S)%104 2106
Toluene-d8 (S)%87 21108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363024
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012502
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/02/17 00:55
1,1,1-Trichloroethane ug/L ND 1.0 06/02/17 00:55
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/02/17 00:55
1,1,2-Trichloroethane ug/L ND 1.0 06/02/17 00:55
1,1-Dichloroethane ug/L ND 1.0 06/02/17 00:55
1,1-Dichloroethene ug/L ND 1.0 06/02/17 00:55
1,2,3-Trichloropropane ug/L ND 1.0 06/02/17 00:55
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/02/17 00:55
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/02/17 00:55
1,2-Dichlorobenzene ug/L ND 1.0 06/02/17 00:55
1,2-Dichloroethane ug/L ND 1.0 06/02/17 00:55
1,2-Dichloropropane ug/L ND 1.0 06/02/17 00:55
1,4-Dichlorobenzene ug/L ND 1.0 06/02/17 00:55
2-Butanone (MEK)ug/L ND 5.0 06/02/17 00:55
2-Hexanone ug/L ND 5.0 06/02/17 00:55
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/02/17 00:55
Acetone ug/L ND 25.0 06/02/17 00:55
Acrylonitrile ug/L ND 10.0 06/02/17 00:55
Benzene ug/L ND 1.0 06/02/17 00:55
Bromochloromethane ug/L ND 1.0 06/02/17 00:55
Bromodichloromethane ug/L ND 1.0 06/02/17 00:55
Bromoform ug/L ND 1.0 06/02/17 00:55
Bromomethane ug/L ND 2.0 06/02/17 00:55
Carbon disulfide ug/L ND 2.0 06/02/17 00:55
Carbon tetrachloride ug/L ND 1.0 06/02/17 00:55
Chlorobenzene ug/L ND 1.0 06/02/17 00:55
Chloroethane ug/L ND 1.0 06/02/17 00:55
Chloroform ug/L ND 1.0 06/02/17 00:55
Chloromethane ug/L ND 1.0 06/02/17 00:55
cis-1,2-Dichloroethene ug/L ND 1.0 06/02/17 00:55
cis-1,3-Dichloropropene ug/L ND 1.0 06/02/17 00:55
Dibromochloromethane ug/L ND 1.0 06/02/17 00:55
Dibromomethane ug/L ND 1.0 06/02/17 00:55
Dichlorodifluoromethane ug/L ND 1.0 06/02/17 00:55
Ethylbenzene ug/L ND 1.0 06/02/17 00:55
Iodomethane ug/L ND 5.0 06/02/17 00:55
m&p-Xylene ug/L ND 2.0 06/02/17 00:55
Methylene Chloride ug/L ND 1.0 06/02/17 00:55
o-Xylene ug/L ND 1.0 06/02/17 00:55
Styrene ug/L ND 1.0 06/02/17 00:55
Tetrachloroethene ug/L ND 1.0 06/02/17 00:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012502
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010
Matrix:Water
Analyzed
Tetrahydrofuran ug/L ND 10.0 06/02/17 00:55
Toluene ug/L ND 1.0 06/02/17 00:55
trans-1,2-Dichloroethene ug/L ND 1.0 06/02/17 00:55
trans-1,3-Dichloropropene ug/L ND 1.0 06/02/17 00:55
trans-1,4-Dichloro-2-butene ug/L ND 1.0 06/02/17 00:55
Trichloroethene ug/L ND 1.0 06/02/17 00:55
Trichlorofluoromethane ug/L ND 1.0 06/02/17 00:55
Vinyl acetate ug/L ND 2.0 06/02/17 00:55
Vinyl chloride ug/L ND 1.0 06/02/17 00:55
1,2-Dichloroethane-d4 (S)%99 70-130 06/02/17 00:55
4-Bromofluorobenzene (S)%115 70-130 06/02/17 00:55
Toluene-d8 (S)%110 70-130 06/02/17 00:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.950 102 80-125
1,1,1-Trichloroethane ug/L 46.350 93 71-129
1,1,2,2-Tetrachloroethane ug/L 54.250 108 79-124
1,1,2-Trichloroethane ug/L 50.150 100 85-125
1,1-Dichloroethane ug/L 44.050 88 73-126
1,1-Dichloroethene ug/L 38.450 77 66-135
1,2,3-Trichloropropane ug/L 54.550 109 75-130
1,2-Dibromo-3-chloropropane ug/L 46.850 94 71-133
1,2-Dibromoethane (EDB)ug/L 51.850 104 83-124
1,2-Dichlorobenzene ug/L 45.750 91 80-133
1,2-Dichloroethane ug/L 44.150 88 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
1,4-Dichlorobenzene ug/L 46.850 94 78-130
2-Butanone (MEK)ug/L 105100 105 61-144
2-Hexanone ug/L 99.7100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 107100 107 48-146
Acrylonitrile ug/L 234250 94 40-160
Benzene ug/L 47.550 95 80-125
Bromochloromethane ug/L 45.750 91 71-125
Bromodichloromethane ug/L 47.150 94 78-124
Bromoform ug/L 57.550 115 71-128
Bromomethane ug/L 50.350 101 40-160
Carbon disulfide ug/L 40.550 81 50-160
Carbon tetrachloride ug/L 47.050 94 69-131
Chlorobenzene ug/L 46.650 93 81-122
Chloroethane ug/L 46.950 94 39-148
Chloroform ug/L 42.950 86 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 52.850 106 44-146
cis-1,2-Dichloroethene ug/L 45.450 91 74-124
cis-1,3-Dichloropropene ug/L 50.650 101 72-132
Dibromochloromethane ug/L 53.650 107 78-125
Dibromomethane ug/L 45.150 90 82-120
Dichlorodifluoromethane ug/L 39.350 79 34-157
Ethylbenzene ug/L 48.150 96 79-121
Iodomethane ug/L 71.3100 71 39-154
m&p-Xylene ug/L 96.4100 96 81-124
Methylene Chloride ug/L 48.250 96 64-133
o-Xylene ug/L 50.750 101 79-131
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 49.050 98 78-122
Tetrahydrofuran ug/L 493500 99 69-148
Toluene ug/L 48.250 96 80-121
trans-1,2-Dichloroethene ug/L 44.550 89 71-127
trans-1,3-Dichloropropene ug/L 53.150 106 69-141
trans-1,4-Dichloro-2-butene ug/L 63.550 127 40-160
Trichloroethene ug/L 48.850 98 78-122
Trichlorofluoromethane ug/L 45.950 92 53-137
Vinyl acetate ug/L 92.9100 93 40-160
Vinyl chloride ug/L 41.950 84 58-137
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%113 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2012504MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478001
1,1,1,2-Tetrachloroethane ug/L 19.520 98 70-130ND
1,1,1-Trichloroethane ug/L 22.420 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.420 107 70-130ND
1,1,2-Trichloroethane ug/L 18.020 90 70-130ND
1,1-Dichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethene ug/L 25.920 129 70-166ND
1,2,3-Trichloropropane ug/L 20.920 105 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.920 85 70-130ND
1,2-Dibromoethane (EDB)ug/L 16.920 85 70-130ND
1,2-Dichlorobenzene ug/L 19.720 98 70-130ND
1,2-Dichloroethane ug/L 19.820 99 70-130ND
1,2-Dichloropropane ug/L 21.120 105 70-130ND
1,4-Dichlorobenzene ug/L 19.920 99 70-130ND
2-Butanone (MEK)ug/L 32.640 82 70-130ND
2-Hexanone ug/L 31.440 78 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 30.140 75 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2012504MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478001
Acetone ug/L 39.640 99 70-130ND
Acrylonitrile ug/L 94.7100 95 70-130ND
Benzene ug/L 21.020 105 70-148ND
Bromochloromethane ug/L 22.220 111 70-130ND
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 20.120 100 70-130ND
Bromomethane ug/L 22.620 113 70-130ND
Carbon disulfide ug/L 25.520 127 70-130ND
Carbon tetrachloride ug/L 21.620 108 70-130ND
Chlorobenzene ug/L 20.520 102 70-146ND
Chloroethane ug/L 23.920 119 70-130ND
Chloroform ug/L 20.520 102 70-130ND
Chloromethane ug/L 26.6 M12013370-130ND
cis-1,2-Dichloroethene ug/L 22.120 110 70-130ND
cis-1,3-Dichloropropene ug/L 16.120 80 70-130ND
Dibromochloromethane ug/L 16.720 83 70-130ND
Dibromomethane ug/L 19.520 98 70-130ND
Dichlorodifluoromethane ug/L 17.420 87 70-130ND
Ethylbenzene ug/L 21.720 109 70-130ND
Iodomethane ug/L 42.440 106 70-130ND
m&p-Xylene ug/L 43.440 109 70-130ND
Methylene Chloride ug/L 21.720 108 70-130ND
o-Xylene ug/L 23.220 116 70-130ND
Styrene ug/L 22.420 112 70-130ND
Tetrachloroethene ug/L 17.220 86 70-130ND
Tetrahydrofuran ug/L 181200 91 70-130ND
Toluene ug/L 18.620 93 70-155ND
trans-1,2-Dichloroethene ug/L 21.820 109 70-130ND
trans-1,3-Dichloropropene ug/L 17.120 85 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.920 94 70-130ND
Trichloroethene ug/L 21.920 109 69-151ND
Trichlorofluoromethane ug/L 23.620 118 70-130ND
Vinyl acetate ug/L 25.4 M1406470-130ND
Vinyl chloride ug/L 21.320 106 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%116 70-130
Toluene-d8 (S)%85 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L 0.48J0.43J
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L 0.43J0.39J
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%103 3100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
4-Bromofluorobenzene (S)%114 1113
Toluene-d8 (S)%113 1111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363026
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342317011, 92342317012, 92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012510
Associated Lab Samples:92342317011, 92342317012, 92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/02/17 01:12
1,1,1-Trichloroethane ug/L ND 1.0 06/02/17 01:12
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/02/17 01:12
1,1,2-Trichloroethane ug/L ND 1.0 06/02/17 01:12
1,1-Dichloroethane ug/L ND 1.0 06/02/17 01:12
1,1-Dichloroethene ug/L ND 1.0 06/02/17 01:12
1,2,3-Trichloropropane ug/L ND 1.0 06/02/17 01:12
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/02/17 01:12
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/02/17 01:12
1,2-Dichlorobenzene ug/L ND 1.0 06/02/17 01:12
1,2-Dichloroethane ug/L ND 1.0 06/02/17 01:12
1,2-Dichloropropane ug/L ND 1.0 06/02/17 01:12
1,4-Dichlorobenzene ug/L ND 1.0 06/02/17 01:12
2-Butanone (MEK)ug/L ND 5.0 06/02/17 01:12
2-Hexanone ug/L ND 5.0 06/02/17 01:12
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/02/17 01:12
Acetone ug/L ND 25.0 06/02/17 01:12
Acrylonitrile ug/L ND 10.0 06/02/17 01:12
Benzene ug/L ND 1.0 06/02/17 01:12
Bromochloromethane ug/L ND 1.0 06/02/17 01:12
Bromodichloromethane ug/L ND 1.0 06/02/17 01:12
Bromoform ug/L ND 1.0 06/02/17 01:12
Bromomethane ug/L ND 2.0 06/02/17 01:12
Carbon disulfide ug/L ND 2.0 06/02/17 01:12
Carbon tetrachloride ug/L ND 1.0 06/02/17 01:12
Chlorobenzene ug/L ND 1.0 06/02/17 01:12
Chloroethane ug/L ND 1.0 06/02/17 01:12
Chloroform ug/L ND 1.0 06/02/17 01:12
Chloromethane ug/L ND 1.0 06/02/17 01:12
cis-1,2-Dichloroethene ug/L ND 1.0 06/02/17 01:12
cis-1,3-Dichloropropene ug/L ND 1.0 06/02/17 01:12
Dibromochloromethane ug/L ND 1.0 06/02/17 01:12
Dibromomethane ug/L ND 1.0 06/02/17 01:12
Dichlorodifluoromethane ug/L ND 1.0 06/02/17 01:12
Ethylbenzene ug/L ND 1.0 06/02/17 01:12
Iodomethane ug/L ND 5.0 06/02/17 01:12
m&p-Xylene ug/L ND 2.0 06/02/17 01:12
Methylene Chloride ug/L ND 1.0 06/02/17 01:12
o-Xylene ug/L ND 1.0 06/02/17 01:12
Styrene ug/L ND 1.0 06/02/17 01:12
Tetrachloroethene ug/L ND 1.0 06/02/17 01:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012510
Associated Lab Samples:92342317011, 92342317012, 92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Tetrahydrofuran ug/L ND 10.0 06/02/17 01:12
Toluene ug/L ND 1.0 06/02/17 01:12
trans-1,2-Dichloroethene ug/L ND 1.0 06/02/17 01:12
trans-1,3-Dichloropropene ug/L ND 1.0 06/02/17 01:12
trans-1,4-Dichloro-2-butene ug/L ND 1.0 06/02/17 01:12
Trichloroethene ug/L ND 1.0 06/02/17 01:12
Trichlorofluoromethane ug/L ND 1.0 06/02/17 01:12
Vinyl acetate ug/L ND 2.0 06/02/17 01:12
Vinyl chloride ug/L ND 1.0 06/02/17 01:12
1,2-Dichloroethane-d4 (S)%102 70-130 06/02/17 01:12
4-Bromofluorobenzene (S)%114 70-130 06/02/17 01:12
Toluene-d8 (S)%111 70-130 06/02/17 01:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012511LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 80-125
1,1,1-Trichloroethane ug/L 45.550 91 71-129
1,1,2,2-Tetrachloroethane ug/L 55.150 110 79-124
1,1,2-Trichloroethane ug/L 51.250 102 85-125
1,1-Dichloroethane ug/L 43.350 87 73-126
1,1-Dichloroethene ug/L 37.050 74 66-135
1,2,3-Trichloropropane ug/L 55.250 110 75-130
1,2-Dibromo-3-chloropropane ug/L 48.050 96 71-133
1,2-Dibromoethane (EDB)ug/L 51.950 104 83-124
1,2-Dichlorobenzene ug/L 46.250 92 80-133
1,2-Dichloroethane ug/L 42.250 84 67-128
1,2-Dichloropropane ug/L 47.850 96 75-132
1,4-Dichlorobenzene ug/L 47.250 94 78-130
2-Butanone (MEK)ug/L 104100 104 61-144
2-Hexanone ug/L 104100 104 68-143
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 72-135
Acetone ug/L 103100 103 48-146
Acrylonitrile ug/L 230250 92 40-160
Benzene ug/L 47.950 96 80-125
Bromochloromethane ug/L 44.650 89 71-125
Bromodichloromethane ug/L 46.850 94 78-124
Bromoform ug/L 57.350 115 71-128
Bromomethane ug/L 51.450 103 40-160
Carbon disulfide ug/L 42.250 84 50-160
Carbon tetrachloride ug/L 47.050 94 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 47.250 94 39-148
Chloroform ug/L 44.050 88 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012511LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 51.050 102 44-146
cis-1,2-Dichloroethene ug/L 44.550 89 74-124
cis-1,3-Dichloropropene ug/L 51.450 103 72-132
Dibromochloromethane ug/L 54.750 109 78-125
Dibromomethane ug/L 45.750 91 82-120
Dichlorodifluoromethane ug/L 38.350 77 34-157
Ethylbenzene ug/L 48.250 96 79-121
Iodomethane ug/L 90.6100 91 39-154
m&p-Xylene ug/L 95.5100 96 81-124
Methylene Chloride ug/L 46.650 93 64-133
o-Xylene ug/L 51.750 103 79-131
Styrene ug/L 51.350 103 84-126
Tetrachloroethene ug/L 49.250 98 78-122
Tetrahydrofuran ug/L 498500 100 69-148
Toluene ug/L 48.650 97 80-121
trans-1,2-Dichloroethene ug/L 43.750 87 71-127
trans-1,3-Dichloropropene ug/L 53.550 107 69-141
trans-1,4-Dichloro-2-butene ug/L 61.650 123 40-160
Trichloroethene ug/L 49.450 99 78-122
Trichlorofluoromethane ug/L 41.050 82 53-137
Vinyl acetate ug/L 91.3100 91 40-160
Vinyl chloride ug/L 40.850 82 58-137
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%112 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013904MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317013
1,1,1,2-Tetrachloroethane ug/L 21.420 107 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.320 101 70-130ND
1,1,2-Trichloroethane ug/L 21.520 108 70-130ND
1,1-Dichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethene ug/L 24.020 120 70-166ND
1,2,3-Trichloropropane ug/L 19.820 99 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.620 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 21.020 105 70-130ND
1,2-Dichloroethane ug/L 22.020 110 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,4-Dichlorobenzene ug/L 19.920 99 70-130ND
2-Butanone (MEK)ug/L 40.840 102 70-130ND
2-Hexanone ug/L 39.540 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.240 103 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013904MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317013
Acetone ug/L 52.940 104 70-13011.2J
Acrylonitrile ug/L 102100 102 70-130ND
Benzene ug/L 21.920 110 70-148ND
Bromochloromethane ug/L 23.320 116 70-130ND
Bromodichloromethane ug/L 22.220 111 70-130ND
Bromoform ug/L 15.920 80 70-130ND
Bromomethane ug/L 27.0 M12013570-130ND
Carbon disulfide ug/L 22.820 114 70-130ND
Carbon tetrachloride ug/L 22.020 110 70-130ND
Chlorobenzene ug/L 21.020 105 70-146ND
Chloroethane ug/L 19.020 95 70-130ND
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 18.720 93 70-130ND
cis-1,2-Dichloroethene ug/L 23.120 115 70-130ND
cis-1,3-Dichloropropene ug/L 19.820 99 70-130ND
Dibromochloromethane ug/L 20.820 104 70-130ND
Dibromomethane ug/L 22.120 110 70-130ND
Dichlorodifluoromethane ug/L 18.720 93 70-130ND
Ethylbenzene ug/L 21.320 107 70-130ND
Iodomethane ug/L 42.340 106 70-130ND
m&p-Xylene ug/L 42.040 105 70-130ND
Methylene Chloride ug/L 18.520 92 70-130ND
o-Xylene ug/L 21.420 107 70-130ND
Styrene ug/L 20.820 104 70-130ND
Tetrachloroethene ug/L 19.020 95 70-130ND
Tetrahydrofuran ug/L 203200 101 70-130ND
Toluene ug/L 22.520 112 70-155ND
trans-1,2-Dichloroethene ug/L 22.520 112 70-130ND
trans-1,3-Dichloropropene ug/L 18.920 94 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.620 73 70-130ND
Trichloroethene ug/L 21.620 108 69-151ND
Trichlorofluoromethane ug/L 23.020 115 70-130ND
Vinyl acetate ug/L 23.3 M1405870-130ND
Vinyl chloride ug/L 21.020 105 70-130ND
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92342317012
2012513SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342317012
2012513SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L 10.4J12.1J
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L 11.9 411.4
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L 1.2 171.0
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%99 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342317012
2012513SAMPLE DUPLICATE:
4-Bromofluorobenzene (S)%112 7119
Toluene-d8 (S)%83 30112
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363311
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/04/17 06:59
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:59
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/04/17 06:59
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:59
1,1-Dichloroethane ug/L ND 1.0 06/04/17 06:59
1,1-Dichloroethene ug/L ND 1.0 06/04/17 06:59
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:59
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/04/17 06:59
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:59
1,2-Dichlorobenzene ug/L ND 1.0 06/04/17 06:59
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:59
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:59
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:59
2-Butanone (MEK)ug/L ND 5.0 06/04/17 06:59
2-Hexanone ug/L ND 5.0 06/04/17 06:59
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/04/17 06:59
Acetone ug/L ND 25.0 06/04/17 06:59
Acrylonitrile ug/L ND 10.0 06/04/17 06:59
Benzene ug/L ND 1.0 06/04/17 06:59
Bromochloromethane ug/L ND 1.0 06/04/17 06:59
Bromodichloromethane ug/L ND 1.0 06/04/17 06:59
Bromoform ug/L ND 1.0 06/04/17 06:59
Bromomethane ug/L ND 2.0 06/04/17 06:59
Carbon disulfide ug/L ND 2.0 06/04/17 06:59
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:59
Chlorobenzene ug/L ND 1.0 06/04/17 06:59
Chloroethane ug/L ND 1.0 06/04/17 06:59
Chloroform ug/L ND 1.0 06/04/17 06:59
Chloromethane ug/L ND 1.0 06/04/17 06:59
cis-1,2-Dichloroethene ug/L ND 1.0 06/04/17 06:59
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:59
Dibromochloromethane ug/L ND 1.0 06/04/17 06:59
Dibromomethane ug/L ND 1.0 06/04/17 06:59
Dichlorodifluoromethane ug/L ND 1.0 06/04/17 06:59
Ethylbenzene ug/L ND 1.0 06/04/17 06:59
Iodomethane ug/L ND 5.0 06/04/17 06:59
m&p-Xylene ug/L ND 2.0 06/04/17 06:59
Methylene Chloride ug/L ND 1.0 06/04/17 06:59
o-Xylene ug/L ND 1.0 06/04/17 06:59
Styrene ug/L ND 1.0 06/04/17 06:59
Tetrachloroethene ug/L ND 1.0 06/04/17 06:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Tetrahydrofuran ug/L ND 10.0 06/04/17 06:59
Toluene ug/L ND 1.0 06/04/17 06:59
trans-1,2-Dichloroethene ug/L ND 1.0 06/04/17 06:59
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:59
trans-1,4-Dichloro-2-butene ug/L ND 1.0 06/04/17 06:59
Trichloroethene ug/L ND 1.0 06/04/17 06:59
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:59
Vinyl acetate ug/L ND 2.0 06/04/17 06:59
Vinyl chloride ug/L ND 1.0 06/04/17 06:59
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:59
4-Bromofluorobenzene (S)%99 70-130 06/04/17 06:59
Toluene-d8 (S)%106 70-130 06/04/17 06:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 80-125
1,1,1-Trichloroethane ug/L 50.850 102 71-129
1,1,2,2-Tetrachloroethane ug/L 53.150 106 79-124
1,1,2-Trichloroethane ug/L 51.550 103 85-125
1,1-Dichloroethane ug/L 52.350 105 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,2,3-Trichloropropane ug/L 47.050 94 75-130
1,2-Dibromo-3-chloropropane ug/L 47.350 95 71-133
1,2-Dibromoethane (EDB)ug/L 54.150 108 83-124
1,2-Dichlorobenzene ug/L 48.250 96 80-133
1,2-Dichloroethane ug/L 48.450 97 67-128
1,2-Dichloropropane ug/L 52.750 105 75-132
1,4-Dichlorobenzene ug/L 45.650 91 78-130
2-Butanone (MEK)ug/L 138100 138 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 72-135
Acetone ug/L 123100 123 48-146
Acrylonitrile ug/L 286250 114 40-160
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 48.550 97 71-128
Bromomethane ug/L 44.850 90 40-160
Carbon disulfide ug/L 52.850 106 50-160
Carbon tetrachloride ug/L 44.250 88 69-131
Chlorobenzene ug/L 49.950 100 81-122
Chloroethane ug/L 43.650 87 39-148
Chloroform ug/L 52.250 104 73-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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Huntersville, NC 28078
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Page 107 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 58.150 116 44-146
cis-1,2-Dichloroethene ug/L 54.050 108 74-124
cis-1,3-Dichloropropene ug/L 52.450 105 72-132
Dibromochloromethane ug/L 48.750 97 78-125
Dibromomethane ug/L 46.050 92 82-120
Dichlorodifluoromethane ug/L 45.450 91 34-157
Ethylbenzene ug/L 48.050 96 79-121
Iodomethane ug/L 95.1100 95 39-154
m&p-Xylene ug/L 95.0100 95 81-124
Methylene Chloride ug/L 53.350 107 64-133
o-Xylene ug/L 46.150 92 79-131
Styrene ug/L 48.350 97 84-126
Tetrachloroethene ug/L 47.950 96 78-122
Tetrahydrofuran ug/L 629500 126 69-148
Toluene ug/L 48.350 97 80-121
trans-1,2-Dichloroethene ug/L 53.850 108 71-127
trans-1,3-Dichloropropene ug/L 51.450 103 69-141
trans-1,4-Dichloro-2-butene ug/L 99.7 L15019940-160
Trichloroethene ug/L 49.550 99 78-122
Trichlorofluoromethane ug/L 46.550 93 53-137
Vinyl acetate ug/L 103100 103 40-160
Vinyl chloride ug/L 46.950 94 58-137
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
1,1,1,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.320 106 70-130ND
1,1,2-Trichloroethane ug/L 21.120 105 70-130ND
1,1-Dichloroethane ug/L 24.120 120 70-130ND
1,1-Dichloroethene ug/L 24.120 120 70-166ND
1,2,3-Trichloropropane ug/L 20.320 102 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.720 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 20.720 104 70-130ND
1,2-Dichloropropane ug/L 22.820 114 70-130ND
1,4-Dichlorobenzene ug/L 21.820 109 70-130ND
2-Butanone (MEK)ug/L 46.840 117 70-130ND
2-Hexanone ug/L 41.240 103 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.340 106 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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Page 108 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
Acetone ug/L 49.140 90 70-13012.9J
Acrylonitrile ug/L 111100 111 70-130ND
Benzene ug/L 23.720 119 70-148ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 17.720 88 70-130ND
Bromomethane ug/L 23.220 116 70-130ND
Carbon disulfide ug/L 24.520 123 70-130ND
Carbon tetrachloride ug/L 21.220 106 70-130ND
Chlorobenzene ug/L 22.520 112 70-146ND
Chloroethane ug/L 18.920 94 70-130ND
Chloroform ug/L 22.320 111 70-130ND
Chloromethane ug/L 24.420 121 70-1300.14J
cis-1,2-Dichloroethene ug/L 24.820 123 70-1300.22J
cis-1,3-Dichloropropene ug/L 22.520 113 70-130ND
Dibromochloromethane ug/L 19.220 96 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Dichlorodifluoromethane ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 44.240 110 70-130ND
m&p-Xylene ug/L 42.540 106 70-130ND
Methylene Chloride ug/L 22.620 113 70-130ND
o-Xylene ug/L 21.020 105 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 20.720 103 70-130ND
Tetrahydrofuran ug/L 231200 116 70-130ND
Toluene ug/L 22.220 111 70-155ND
trans-1,2-Dichloroethene ug/L 23.720 118 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 24.720 124 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 22.520 112 70-130ND
Vinyl acetate ug/L 38.640 96 70-130ND
Vinyl chloride ug/L 21.520 107 70-130ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L 0.35J0.37J
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L 0.86JND
1,4-Dichlorobenzene ug/L 2.4 52.5
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L 13.9J21.4J
Acrylonitrile ug/L NDND
Benzene ug/L 0.52J0.62J
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 0.97J0.87J
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L 0.11JND
cis-1,2-Dichloroethene ug/L 1.0 31.0J
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L 0.31JND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L 0.91J0.88J
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%90 090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
4-Bromofluorobenzene (S)%98 299
Toluene-d8 (S)%105 3108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363328
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342317016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342317016
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/04/17 20:01
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 20:01
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/04/17 20:01
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 20:01
1,1-Dichloroethane ug/L ND 1.0 06/04/17 20:01
1,1-Dichloroethene ug/L ND 1.0 06/04/17 20:01
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 20:01
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/04/17 20:01
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 20:01
1,2-Dichlorobenzene ug/L ND 1.0 06/04/17 20:01
1,2-Dichloroethane ug/L ND 1.0 06/04/17 20:01
1,2-Dichloropropane ug/L ND 1.0 06/04/17 20:01
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 20:01
2-Butanone (MEK)ug/L ND 5.0 06/04/17 20:01
2-Hexanone ug/L ND 5.0 06/04/17 20:01
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/04/17 20:01
Acetone ug/L ND 25.0 06/04/17 20:01
Acrylonitrile ug/L ND 10.0 06/04/17 20:01
Benzene ug/L ND 1.0 06/04/17 20:01
Bromochloromethane ug/L ND 1.0 06/04/17 20:01
Bromodichloromethane ug/L ND 1.0 06/04/17 20:01
Bromoform ug/L ND 1.0 06/04/17 20:01
Bromomethane ug/L ND 2.0 06/04/17 20:01
Carbon disulfide ug/L ND 2.0 06/04/17 20:01
Carbon tetrachloride ug/L ND 1.0 06/04/17 20:01
Chlorobenzene ug/L ND 1.0 06/04/17 20:01
Chloroethane ug/L ND 1.0 06/04/17 20:01
Chloroform ug/L ND 1.0 06/04/17 20:01
Chloromethane ug/L ND 1.0 06/04/17 20:01
cis-1,2-Dichloroethene ug/L ND 1.0 06/04/17 20:01
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:01
Dibromochloromethane ug/L ND 1.0 06/04/17 20:01
Dibromomethane ug/L ND 1.0 06/04/17 20:01
Dichlorodifluoromethane ug/L ND 1.0 06/04/17 20:01
Ethylbenzene ug/L ND 1.0 06/04/17 20:01
Iodomethane ug/L ND 5.0 06/04/17 20:01
m&p-Xylene ug/L ND 2.0 06/04/17 20:01
Methylene Chloride ug/L ND 1.0 06/04/17 20:01
o-Xylene ug/L ND 1.0 06/04/17 20:01
Styrene ug/L ND 1.0 06/04/17 20:01
Tetrachloroethene ug/L ND 1.0 06/04/17 20:01
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342317016
Matrix:Water
Analyzed
Tetrahydrofuran ug/L ND 10.0 06/04/17 20:01
Toluene ug/L ND 1.0 06/04/17 20:01
trans-1,2-Dichloroethene ug/L ND 1.0 06/04/17 20:01
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:01
trans-1,4-Dichloro-2-butene ug/L ND 1.0 06/04/17 20:01
Trichloroethene ug/L ND 1.0 06/04/17 20:01
Trichlorofluoromethane ug/L ND 1.0 06/04/17 20:01
Vinyl acetate ug/L ND 2.0 06/04/17 20:01
Vinyl chloride ug/L ND 1.0 06/04/17 20:01
1,2-Dichloroethane-d4 (S)%85 70-130 06/04/17 20:01
4-Bromofluorobenzene (S)%100 70-130 06/04/17 20:01
Toluene-d8 (S)%115 70-130 06/04/17 20:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.650 93 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 48.950 98 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 46.950 94 66-135
1,2,3-Trichloropropane ug/L 46.550 93 75-130
1,2-Dibromo-3-chloropropane ug/L 46.750 93 71-133
1,2-Dibromoethane (EDB)ug/L 54.550 109 83-124
1,2-Dichlorobenzene ug/L 47.550 95 80-133
1,2-Dichloroethane ug/L 47.050 94 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2-Butanone (MEK)ug/L 126100 126 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 94.9100 95 72-135
Acetone ug/L 115100 115 48-146
Acrylonitrile ug/L 268250 107 40-160
Benzene ug/L 52.150 104 80-125
Bromochloromethane ug/L 48.950 98 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 43.150 86 71-128
Bromomethane ug/L 42.150 84 40-160
Carbon disulfide ug/L 49.350 99 50-160
Carbon tetrachloride ug/L 45.150 90 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 40.850 82 39-148
Chloroform ug/L 50.950 102 73-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 49.950 100 44-146
cis-1,2-Dichloroethene ug/L 52.550 105 74-124
cis-1,3-Dichloropropene ug/L 54.150 108 72-132
Dibromochloromethane ug/L 47.550 95 78-125
Dibromomethane ug/L 44.250 88 82-120
Dichlorodifluoromethane ug/L 41.150 82 34-157
Ethylbenzene ug/L 50.150 100 79-121
Iodomethane ug/L 91.7100 92 39-154
m&p-Xylene ug/L 99.4100 99 81-124
Methylene Chloride ug/L 53.650 107 64-133
o-Xylene ug/L 49.550 99 79-131
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 44.850 90 78-122
Tetrahydrofuran ug/L 580500 116 69-148
Toluene ug/L 46.450 93 80-121
trans-1,2-Dichloroethene ug/L 52.350 105 71-127
trans-1,3-Dichloropropene ug/L 52.450 105 69-141
trans-1,4-Dichloro-2-butene ug/L 68.350 137 40-160
Trichloroethene ug/L 50.450 101 78-122
Trichlorofluoromethane ug/L 45.450 91 53-137
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 41.950 84 58-137
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
1,1,1,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,1-Trichloroethane ug/L 23.020 115 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.120 110 70-130ND
1,1,2-Trichloroethane ug/L 22.220 111 70-130ND
1,1-Dichloroethane ug/L 23.120 116 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,2,3-Trichloropropane ug/L 19.520 98 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.220 91 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 20.920 105 70-130ND
1,2-Dichloroethane ug/L 21.320 106 70-130ND
1,2-Dichloropropane ug/L 24.120 120 70-130ND
1,4-Dichlorobenzene ug/L 21.120 105 70-130ND
2-Butanone (MEK)ug/L 47.740 119 70-130ND
2-Hexanone ug/L 40.940 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.240 108 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
Acetone ug/L 93.5 M14019870-13014.4J
Acrylonitrile ug/L 114100 114 70-130ND
Benzene ug/L 23.420 117 70-148ND
Bromochloromethane ug/L 21.420 107 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 16.520 83 70-130ND
Bromomethane ug/L 19.820 99 70-130ND
Carbon disulfide ug/L 23.420 117 70-130ND
Carbon tetrachloride ug/L 22.420 112 70-130ND
Chlorobenzene ug/L 22.120 110 70-146ND
Chloroethane ug/L 21.720 108 70-130ND
Chloroform ug/L 23.220 116 70-130ND
Chloromethane ug/L 25.820 129 70-130ND
cis-1,2-Dichloroethene ug/L 24.520 119 70-1300.64J
cis-1,3-Dichloropropene ug/L 23.420 117 70-130ND
Dibromochloromethane ug/L 18.420 92 70-130ND
Dibromomethane ug/L 21.720 108 70-130ND
Dichlorodifluoromethane ug/L 19.220 96 70-130ND
Ethylbenzene ug/L 23.020 115 70-130ND
Iodomethane ug/L 41.640 104 70-130ND
m&p-Xylene ug/L 46.140 115 70-130ND
Methylene Chloride ug/L 23.220 116 70-130ND
o-Xylene ug/L 22.220 111 70-130ND
Styrene ug/L 22.320 112 70-130ND
Tetrachloroethene ug/L 19.420 97 70-130ND
Tetrahydrofuran ug/L 233200 117 70-130ND
Toluene ug/L 22.720 113 70-155ND
trans-1,2-Dichloroethene ug/L 25.020 125 70-130ND
trans-1,3-Dichloropropene ug/L 21.820 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.320 106 70-130ND
Trichloroethene ug/L 23.820 119 69-151ND
Trichlorofluoromethane ug/L 22.120 111 70-130ND
Vinyl acetate ug/L 37.640 94 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,1-Dichloroethane ug/L 0.50J0.36J
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L 0.29JND
cis-1,2-Dichloroethene ug/L 0.88J0.65J
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%92 092
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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Page 116 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
4-Bromofluorobenzene (S)%105 2103
Toluene-d8 (S)%108 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363163
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342317006, 92342317007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013349
Associated Lab Samples:92342317006, 92342317007
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 06/06/17 20:06
4,4'-DDT ug/L ND 0.050 06/06/17 20:06
Aldrin ug/L ND 0.050 06/06/17 20:06
alpha-BHC ug/L ND 0.050 06/06/17 20:06
delta-BHC ug/L ND 0.050 06/06/17 20:06
Endosulfan I ug/L ND 0.050 06/06/17 20:06
Endosulfan II ug/L ND 0.050 06/06/17 20:06
Endrin ug/L ND 0.050 06/06/17 20:06
Endrin aldehyde ug/L ND 0.050 06/06/17 20:06
Heptachlor ug/L ND 0.050 06/06/17 20:06
Heptachlor epoxide ug/L ND 0.050 06/06/17 20:06
Methoxychlor ug/L ND 0.15 06/06/17 20:06
Decachlorobiphenyl (S)%95 20-130 06/06/17 20:06
Tetrachloro-m-xylene (S)%80 20-130 06/06/17 20:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013350LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.24.25 98 20-150
4,4'-DDT ug/L 0.26.25 105 20-150
Aldrin ug/L 0.18.25 73 20-150
alpha-BHC ug/L 0.20.25 79 20-150
delta-BHC ug/L 0.23.25 92 20-150
Endosulfan I ug/L 0.23.25 92 20-150
Endosulfan II ug/L 0.24.25 99 20-150
Endrin ug/L 0.25.25 100 20-150
Endrin aldehyde ug/L 0.23.25 94 20-150
Heptachlor ug/L 0.18.25 75 20-150
Heptachlor epoxide ug/L 0.21.25 83 20-150
Methoxychlor ug/L 0.76.74 102 20-150
Decachlorobiphenyl (S)%86 20-130
Tetrachloro-m-xylene (S)%54 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013351MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479004
4,4'-DDD ug/L 0.22.25 89 20-150ND
4,4'-DDT ug/L 0.24.25 98 20-150ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013351MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479004
Aldrin ug/L 0.18.25 71 20-150ND
alpha-BHC ug/L 0.19.25 77 20-150ND
delta-BHC ug/L 0.21.25 84 20-150ND
Endosulfan I ug/L 0.21.25 87 20-150ND
Endosulfan II ug/L 0.23.25 91 20-150ND
Endrin ug/L 0.23.25 93 20-150ND
Endrin aldehyde ug/L 0.23.25 95 20-150ND
Heptachlor ug/L 0.18.25 74 20-150ND
Heptachlor epoxide ug/L 0.20.25 83 20-150ND
Methoxychlor ug/L 0.70.74 94 20-150ND
Decachlorobiphenyl (S)%47 20-130
Tetrachloro-m-xylene (S)%76 20-130
Parameter Units
Dup
Result QualifiersRPDResult
92342479005
2013352SAMPLE DUPLICATE:
4,4'-DDD ug/L NDND
4,4'-DDT ug/L NDND
Aldrin ug/L NDND
alpha-BHC ug/L NDND
delta-BHC ug/L NDND
Endosulfan I ug/L NDND
Endosulfan II ug/L NDND
Endrin ug/L NDND
Endrin aldehyde ug/L NDND
Heptachlor ug/L NDND
Heptachlor epoxide ug/L NDND
Methoxychlor ug/L NDND
Decachlorobiphenyl (S)%68 2184
Tetrachloro-m-xylene (S)%87 15101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363212
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342317001, 92342317009, 92342317017, 92342317018, 92342317019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013628
Associated Lab Samples:92342317001, 92342317009, 92342317017, 92342317018, 92342317019
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 06/08/17 02:46
4,4'-DDT ug/L ND 0.050 06/08/17 02:46
Aldrin ug/L ND 0.050 06/08/17 02:46
alpha-BHC ug/L ND 0.050 06/08/17 02:46
delta-BHC ug/L ND 0.050 06/08/17 02:46
Endosulfan I ug/L ND 0.050 06/08/17 02:46
Endosulfan II ug/L ND 0.050 06/08/17 02:46
Endrin ug/L ND 0.050 06/08/17 02:46
Endrin aldehyde ug/L ND 0.050 06/08/17 02:46
Heptachlor ug/L ND 0.050 06/08/17 02:46
Heptachlor epoxide ug/L ND 0.050 06/08/17 02:46
Methoxychlor ug/L ND 0.15 06/08/17 02:46
Decachlorobiphenyl (S)%60 20-130 06/08/17 02:46
Tetrachloro-m-xylene (S)%79 20-130 06/08/17 02:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013629LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.11.12 87 20-150
4,4'-DDT ug/L 0.11.12 90 20-150
Aldrin ug/L 0.081.12 66 20-150
alpha-BHC ug/L 0.10.12 83 20-150
delta-BHC ug/L 0.11.12 88 20-150
Endosulfan I ug/L 0.11.12 88 20-150
Endosulfan II ug/L 0.11.12 90 20-150
Endrin ug/L 0.11.12 90 20-150
Endrin aldehyde ug/L 0.098.12 80 20-150
Heptachlor ug/L 0.099.12 80 20-150
Heptachlor epoxide ug/L 0.11.12 87 20-150
Methoxychlor ug/L 0.39.37 105 20-150
Decachlorobiphenyl (S)%54 20-130
Tetrachloro-m-xylene (S)%88 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013630MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317009
4,4'-DDD ug/L 0.13.12 105 20-150ND
4,4'-DDT ug/L 0.12.12 95 20-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013630MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317009
Aldrin ug/L 0.069.12 55 20-150ND
alpha-BHC ug/L 0.097.12 78 20-150ND
delta-BHC ug/L 0.081.12 65 20-150ND
Endosulfan I ug/L 0.12.12 97 20-150ND
Endosulfan II ug/L 0.091.12 73 20-150ND
Endrin ug/L 0.14.12 115 20-150ND
Endrin aldehyde ug/L 0.44 M1.12 359 20-150ND
Heptachlor ug/L 0.083.12 67 20-150ND
Heptachlor epoxide ug/L 0.12.12 98 20-150ND
Methoxychlor ug/L 0.31.37 85 20-150ND
Decachlorobiphenyl (S)%66 20-130
Tetrachloro-m-xylene (S)%74 20-130
Parameter Units
Dup
Result QualifiersRPDResult
92342317019
2013631SAMPLE DUPLICATE:
4,4'-DDD ug/L NDND
4,4'-DDT ug/L NDND
Aldrin ug/L NDND
alpha-BHC ug/L NDND
delta-BHC ug/L NDND
Endosulfan I ug/L NDND
Endosulfan II ug/L NDND
Endrin ug/L NDND
Endrin aldehyde ug/L NDND
Heptachlor ug/L NDND
Heptachlor epoxide ug/L NDND
Methoxychlor ug/L NDND
Decachlorobiphenyl (S)%38 337
Tetrachloro-m-xylene (S)%75 30101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362866
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342317001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011591
Associated Lab Samples:92342317001
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/02/17 03:10
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/02/17 03:10
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/02/17 03:10
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/02/17 03:10
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/02/17 03:10
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/02/17 03:10
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/02/17 03:10
Decachlorobiphenyl (S)%34 10-132 06/02/17 03:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011592LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2011593
PCB-1016 (Aroclor 1016)ug/L 2.65 53 50-150552.7 3 30
PCB-1260 (Aroclor 1260)ug/L 2.55 50 50-150562.8 10 30
Decachlorobiphenyl (S)%35 10-13235
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
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[phone]
Page 122 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363162
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342317006, 92342317007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013345
Associated Lab Samples:92342317006, 92342317007
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/03/17 13:25
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/03/17 13:25
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/03/17 13:25
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/03/17 13:25
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/03/17 13:25
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/03/17 13:25
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/03/17 13:25
Decachlorobiphenyl (S)%93 10-132 06/03/17 13:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013346LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 1.92.5 76 50-150
PCB-1260 (Aroclor 1260)ug/L 2.32.5 91 50-150
Decachlorobiphenyl (S)%64 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013347MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530001
PCB-1016 (Aroclor 1016)ug/L 1.52.5 61 50-150ND
PCB-1260 (Aroclor 1260)ug/L 1.42.5 55 50-150ND
Decachlorobiphenyl (S)%32 10-132
Parameter Units
Dup
Result QualifiersRPDResult
92342530003
2013348SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L NDND
PCB-1221 (Aroclor 1221)ug/L NDND
PCB-1232 (Aroclor 1232)ug/L NDND
PCB-1242 (Aroclor 1242)ug/L NDND
PCB-1248 (Aroclor 1248)ug/L NDND
PCB-1254 (Aroclor 1254)ug/L NDND
PCB-1260 (Aroclor 1260)ug/L NDND
Decachlorobiphenyl (S)%59 2777
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 123 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363213
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342317017, 92342317018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013632
Associated Lab Samples:92342317017, 92342317018
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/05/17 20:11
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/05/17 20:11
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/05/17 20:11
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/05/17 20:11
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/05/17 20:11
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/05/17 20:11
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/05/17 20:11
Decachlorobiphenyl (S)%82 10-132 06/05/17 20:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013633LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 2.12.5 84 50-150
PCB-1260 (Aroclor 1260)ug/L 2.32.5 92 50-150
Decachlorobiphenyl (S)%91 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013634MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317017
PCB-1016 (Aroclor 1016)ug/L 1.62.5 63 50-150ND
PCB-1260 (Aroclor 1260)ug/L 1.62.5 62 50-150ND
Decachlorobiphenyl (S)%55 10-132
Parameter Units
Dup
Result QualifiersRPDResult
92342317018
2013635SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L NDND
PCB-1221 (Aroclor 1221)ug/L NDND
PCB-1232 (Aroclor 1232)ug/L NDND
PCB-1242 (Aroclor 1242)ug/L NDND
PCB-1248 (Aroclor 1248)ug/L NDND
PCB-1254 (Aroclor 1254)ug/L NDND
PCB-1260 (Aroclor 1260)ug/L NDND
Decachlorobiphenyl (S)%74 5741
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
372315
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342317001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012657
Associated Lab Samples:92342317001
Matrix:Water
Analyzed
2,4,5-TP (Silvex)ug/L ND 0.19 06/06/17 01:19
2,4-D ug/L ND 0.94 06/06/17 01:19
2,4-DCAA (S)%94 39-139 06/06/17 01:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012658LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2013105
2,4,5-TP (Silvex)ug/L 1.11.2 92 53-134971.2 5 40
2,4-D ug/L 5.56 91 35-124955.7 5 40
2,4-DCAA (S)%83 39-13985 40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
372862
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342317006, 92342317007, 92342317017, 92342317018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015492
Associated Lab Samples:92342317006, 92342317007, 92342317017, 92342317018
Matrix:Water
Analyzed
2,4,5-TP (Silvex)ug/L ND 0.19 06/07/17 01:34
2,4-D ug/L ND 0.94 06/07/17 01:34
2,4-DCAA (S)%93 39-139 06/07/17 01:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015493LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-TP (Silvex)ug/L 1.51.2 128 53-134
2,4-D ug/L 7.6 L1612635-124
2,4-DCAA (S)%114 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015674MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35315473004
2015675
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4,5-TP (Silvex)ug/L 1.5 125 53-134119 231.20.051U 1.8 1.4
2,4-D ug/L 7.3 120 35-124107 3060.23U 8.7 6.5
2,4-DCAA (S)%114 39-13998
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362852
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342317001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011539
Associated Lab Samples:92342317001
Matrix:Water
Analyzed
Benzo(a)anthracene ug/L ND 10.0 06/02/17 16:09
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/02/17 16:09
Chrysene ug/L ND 10.0 06/02/17 16:09
Dibenz(a,h)anthracene ug/L ND 10.0 06/02/17 16:09
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/02/17 16:09
2,4,6-Tribromophenol (S)%69 27-110 06/02/17 16:09
2-Fluorobiphenyl (S)%65 27-110 06/02/17 16:09
2-Fluorophenol (S)%33 12-110 06/02/17 16:09
Nitrobenzene-d5 (S)%59 21-110 06/02/17 16:09
Phenol-d6 (S)%23 10-110 06/02/17 16:09
Terphenyl-d14 (S)%76 31-107 06/02/17 16:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011540LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(a)anthracene ug/L 38.950 78 56-121
bis(2-Ethylhexyl)phthalate ug/L 43.950 88 50-145
Chrysene ug/L 37.950 76 58-127
Dibenz(a,h)anthracene ug/L 42.750 85 53-129
Indeno(1,2,3-cd)pyrene ug/L 41.550 83 55-128
2,4,6-Tribromophenol (S)%92 27-110
2-Fluorobiphenyl (S)%82 27-110
2-Fluorophenol (S)%38 12-110
Nitrobenzene-d5 (S)%74 21-110
Phenol-d6 (S)%27 10-110
Terphenyl-d14 (S)%82 31-107
Parameter Units
Dup
Result QualifiersRPDResult
92342317001
2011542SAMPLE DUPLICATE:
Benzo(a)anthracene ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Chrysene ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
2,4,6-Tribromophenol (S)%76 1488
2-Fluorobiphenyl (S)%61 3991
2-Fluorophenol (S)%20 6339
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92342317001
2011542SAMPLE DUPLICATE:
Nitrobenzene-d5 (S)%52 4380
Phenol-d6 (S)%20 2926
Terphenyl-d14 (S)%88 693
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363352
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014313
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317010
Matrix:Water
Analyzed
Benzo(a)anthracene ug/L ND 10.0 06/07/17 13:12
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/07/17 13:12
Chrysene ug/L ND 10.0 06/07/17 13:12
Dibenz(a,h)anthracene ug/L ND 10.0 06/07/17 13:12
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/07/17 13:12
2,4,6-Tribromophenol (S)%52 27-110 06/07/17 13:12
2-Fluorobiphenyl (S)%40 27-110 06/07/17 13:12
2-Fluorophenol (S)%18 12-110 06/07/17 13:12
Nitrobenzene-d5 (S)%37 21-110 06/07/17 13:12
Phenol-d6 (S)%14 10-110 06/07/17 13:12
Terphenyl-d14 (S)%50 31-107 06/07/17 13:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014314LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(a)anthracene ug/L 24.3 L2504956-121
bis(2-Ethylhexyl)phthalate ug/L 28.550 57 50-145
Chrysene ug/L 23.5 L2504758-127
Dibenz(a,h)anthracene ug/L 28.250 56 53-129
Indeno(1,2,3-cd)pyrene ug/L 25.5 L2505155-128
2,4,6-Tribromophenol (S)%54 27-110
2-Fluorobiphenyl (S)%41 27-110
2-Fluorophenol (S)%20 12-110
Nitrobenzene-d5 (S)%38 21-110
Phenol-d6 (S)%19 10-110
Terphenyl-d14 (S)%54 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014315MATRIX SPIKE SAMPLE:
MSSpike
Result
92342683001
Benzo(a)anthracene ug/L 30.550 61 22-117ND
bis(2-Ethylhexyl)phthalate ug/L 35.150 70 23-102ND
Chrysene ug/L 28.950 58 23-115ND
Dibenz(a,h)anthracene ug/L 33.250 66 21-112ND
Indeno(1,2,3-cd)pyrene ug/L 32.050 64 20-113ND
2,4,6-Tribromophenol (S)%72 27-110
2-Fluorobiphenyl (S)%67 27-110
2-Fluorophenol (S)%30 12-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014315MATRIX SPIKE SAMPLE:
MSSpike
Result
92342683001
Nitrobenzene-d5 (S)%60 21-110
Phenol-d6 (S)%25 10-110
Terphenyl-d14 (S)%54 31-107
Parameter Units
Dup
Result QualifiersRPDResult
92342683004
2014316SAMPLE DUPLICATE:
Benzo(a)anthracene ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Chrysene ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
2,4,6-Tribromophenol (S)%60 2049
2-Fluorobiphenyl (S)%46 4828
2-Fluorophenol (S)%21 5811
Nitrobenzene-d5 (S)%39 6320
Phenol-d6 (S)%17 1015
Terphenyl-d14 (S)%37 2045
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364045
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342317017, 92342317018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018661
Associated Lab Samples:92342317017, 92342317018
Matrix:Water
Analyzed
Benzo(a)anthracene ug/L ND 10.0 06/09/17 14:08
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/09/17 14:08
Chrysene ug/L ND 10.0 06/09/17 14:08
Dibenz(a,h)anthracene ug/L ND 10.0 06/09/17 14:08
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/09/17 14:08
2,4,6-Tribromophenol (S)%70 27-110 06/09/17 14:08
2-Fluorobiphenyl (S)%68 27-110 06/09/17 14:08
2-Fluorophenol (S)%36 12-110 06/09/17 14:08
Nitrobenzene-d5 (S)%62 21-110 06/09/17 14:08
Phenol-d6 (S)%23 10-110 06/09/17 14:08
Terphenyl-d14 (S)%80 31-107 06/09/17 14:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018662LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(a)anthracene ug/L 39.850 80 56-121
bis(2-Ethylhexyl)phthalate ug/L 44.050 88 50-145
Chrysene ug/L 38.650 77 58-127
Dibenz(a,h)anthracene ug/L 43.950 88 53-129
Indeno(1,2,3-cd)pyrene ug/L 43.750 87 55-128
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%95 27-110
2-Fluorophenol (S)%47 12-110
Nitrobenzene-d5 (S)%82 21-110
Phenol-d6 (S)%33 10-110
Terphenyl-d14 (S)%90 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362960
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012130
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 06/01/17 16:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012131LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4940050000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012132MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342466001
2012133
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 108 80-120107 15000031.2
mg/L 85300 84600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363125
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013190
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 06/05/17 12:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013191LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5110050000 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013192MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342496001
2013193
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 103 80-12095 55000019.6
mg/L 70800 67200
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013194MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317011
2013195
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 102 80-120100 150000323008310082500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363343
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014291
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 06/05/17 20:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014292LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5080050000 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014293MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317017
2014294
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 110 80-12097 150000587000642000636000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014295MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317020
2014296
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500006580-12068 150000135000167000169000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363435
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014862
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 06/05/17 17:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014863LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 240000250000 96 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92342281001
2014864SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 46000 D6743.0 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92342318002
2014865SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 726000 3748 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363475
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015131
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 06/06/17 02:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015132LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 246000250000 98 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92342480005
2015133SAMPLE DUPLICATE:
Total Dissolved Solids ug/L NDND
Parameter Units
Dup
Result QualifiersRPDResult
92342317014
2015134SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 373000 D615321000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363658
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016163
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 06/07/17 01:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016164LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 250000250000 100 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92342317017
2016165SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 812000 2796000
Parameter Units
Dup
Result QualifiersRPDResult
92342745004
2016166SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 172000 5163 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363078
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013020
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Sulfide ug/L ND 100 06/01/17 21:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013021LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 464500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013022MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281005
2013023
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 99 80-120102 3500ND501516
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013024MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342337001
2013025
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 80-120104 4500ND509532
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363621
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015987
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010
Matrix:Water
Analyzed
Sulfide ug/L ND 100 06/06/17 22:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015988LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 464500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015989MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281006
2015990
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L R15008780-120105 19500ND433524
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015991MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472017
2015992
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 85 80-12085 0500ND470468
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363623
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342317011, 92342317012, 92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016031
Associated Lab Samples:92342317011, 92342317012, 92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Sulfide ug/L ND 100 06/06/17 23:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016032LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 470500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016033MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317011
2016034
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 91 80-12093 2500ND454463
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016035MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342530004
2016036
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 82 80-12085 4500ND408423
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363631
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016072
Associated Lab Samples:92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Sulfide ug/L ND 100 06/06/17 23:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016073LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 497500 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016074MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342297009
2016075
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L M15006480-12067 5500ND319337
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342297016
2016077
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 80-12098 2500ND501490
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363280
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014066
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Sulfate ug/L ND 1000 06/03/17 12:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014067LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5190050000 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014068MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342413001
2014069
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1,R150000-22 90-11081 675000051500103000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014070MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342701002
2014071
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 100 90-110101 1500001.3
mg/L 51200 51900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363281
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014072
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014
Matrix:Water
Analyzed
Sulfate ug/L ND 1000 06/03/17 13:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014073LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5210050000 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014074MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342339001
2014075
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1500005190-11054 35000018600J4410045600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342710001
2014077
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M6,R150000-45 90-110155 1550000634
mg/L 611000 711000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363396
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342317015, 92342317017, 92342317018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014592
Associated Lab Samples:92342317015, 92342317017, 92342317018
Matrix:Water
Analyzed
Sulfate ug/L ND 1000 06/05/17 16:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014593LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5040050000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014594MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2014595
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 101 90-110103 250000182006860069700
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014596MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342600004
2014597
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1,R150000390-11078 4750000584006010097400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364291
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2020011
Associated Lab Samples:92342317019, 92342317020
Matrix:Water
Analyzed
Sulfate ug/L ND 1000 06/10/17 11:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2020012LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 5020050000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2020015MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343524006
2020016
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 50000 98 90-110101 25000014.8
mg/L 63800 65100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2020039MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343485001
2020040
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M6500005990-11057 0500001830
mg/L 1860000 1860000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363150
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013292
Associated Lab Samples:92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Chloride ug/L ND 1000 06/02/17 11:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013293LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2000020000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013294MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342580001
2013295
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 92 90-11092 010000ND95309490
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013296MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317004
2013297
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 99 90-11098 01000043101420014200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363371
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014368
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014, 92342317015
Matrix:Water
Analyzed
Chloride ug/L ND 1000 06/05/17 10:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014369LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1960020000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342674001
2014371
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L M11000048990-110492 01000080.8
mg/L 130000 130000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014372MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342496003
2014373
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 100 90-110100 0100002.3
mg/L 12300 12200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364537
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92342317017, 92342317018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2021014
Associated Lab Samples:92342317017, 92342317018
Matrix:Water
Analyzed
Chloride ug/L ND 1000 06/14/17 02:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2021015LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2060020000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021016MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342600008
2021017
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L M11000011390-110113 01000062801760017500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021018MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343524004
2021019
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 102 90-110101 01000022.1
mg/L 32300 32200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364538
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2021020
Associated Lab Samples:92342317019, 92342317020
Matrix:Water
Analyzed
Chloride ug/L ND 1000 06/14/17 03:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2021021LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2040020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021022MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317019
2021023
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L M6,R110000-22 90-110-1450 5810000318000315000173000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021024MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343251002
2021025
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 96 90-11096 01000023.3
mg/L 32900 32900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362991
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012281
Associated Lab Samples:92342317001, 92342317002, 92342317003, 92342317004, 92342317005
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 06/01/17 17:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012282LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 102100 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012283MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342135005
2012284
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M11005180-12055 21000.12
mg/L 168 172
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012285MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342417001
2012286
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M1100080-1200 41000.0093
mg/L 9.4 9.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363512
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015217
Associated Lab Samples:92342317006, 92342317007, 92342317008, 92342317009, 92342317010, 92342317011, 92342317012,
92342317013, 92342317014
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 06/07/17 12:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015218LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 98.3100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015219MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342571001
2015220
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M11007080-12062 81000.027
mg/L 97.6 89.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015221MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342619002
2015222
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 94 80-12094 0100ND95.9 96.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
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Page 151 of 199
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342317
OSR
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363513
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342317015, 92342317017, 92342317018, 92342317019, 92342317020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015224
Associated Lab Samples:92342317015, 92342317017, 92342317018, 92342317019, 92342317020
Matrix:Water
Analyzed
Cyanide ug/L ND 8.0 06/07/17 13:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015225LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015226MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2015227
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L 100 94 80-12091 2100ND97.6 95.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342712006
2015229
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11002980-12019 271000.013
mg/L 41.2 31.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 199
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342317
OSR
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
BATCH QUALIFIERS
Batch: 372970
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[M5]
ANALYTE QUALIFIERS
Sample re-extracted outside method hold time. Results of re-analysis confirmed original analysis performed within hold
time.1g
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 153 of 199
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342317002 3412-MW8
92342317003 3412-MW9
92342317004 3412-MW13
92342317005 3412-MW14
92342317006 3412-MW1R
92342317007 3412-MW15
92342317008 3412-MW3R
92342317009 3412-MW7
92342317010 3412-SW2
92342317011 3412-MW5R
92342317012 3412-MW12
92342317013 3412-SW1
92342317014 3412-SW3
92342317015 3412-SW4
92342317017 3412-MW2R
92342317018 3412-MW4R
92342317019 3412-MW10
92342317020 3412-MW11
92342317001 363212 3638093412-EQUIPMENT BLANK EPA 3510 EPA 8081
92342317006 363163 3635903412-MW1R EPA 3510 EPA 8081
92342317007 363163 3635903412-MW15 EPA 3510 EPA 8081
92342317009 363212 3638093412-MW7 EPA 3510 EPA 8081
92342317017 363212 3638093412-MW2R EPA 3510 EPA 8081
92342317018 363212 3638093412-MW4R EPA 3510 EPA 8081
92342317019 363212 3638093412-MW10 EPA 3510 EPA 8081
92342317001 362866 3630303412-EQUIPMENT BLANK EPA 3510 EPA 8082
92342317006 363162 3633493412-MW1R EPA 3510 EPA 8082
92342317007 363162 3633493412-MW15 EPA 3510 EPA 8082
92342317017 363213 3633483412-MW2R EPA 3510 EPA 8082
92342317018 363213 3633483412-MW4R EPA 3510 EPA 8082
92342317001 372315 3729703412-EQUIPMENT BLANK EPA 8151 EPA 8151
92342317006 372862 3732323412-MW1R EPA 8151 EPA 8151
92342317007 372862 3732323412-MW15 EPA 8151 EPA 8151
92342317017 372862 3732323412-MW2R EPA 8151 EPA 8151
92342317018 372862 3732323412-MW4R EPA 8151 EPA 8151
92342317001 363006 3636873412-EQUIPMENT BLANK EPA 3010A EPA 6010
92342317002 363006 3636873412-MW8 EPA 3010A EPA 6010
92342317003 363006 3636873412-MW9 EPA 3010A EPA 6010
92342317004 363006 3636873412-MW13 EPA 3010A EPA 6010
92342317005 363006 3636873412-MW14 EPA 3010A EPA 6010
92342317006 363145 3636903412-MW1R EPA 3010A EPA 6010
92342317007 363145 3636903412-MW15 EPA 3010A EPA 6010
92342317008 363145 3636903412-MW3R EPA 3010A EPA 6010
92342317009 363145 3636903412-MW7 EPA 3010A EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 154 of 199
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342317010 363145 3636903412-SW2 EPA 3010A EPA 6010
92342317011 363145 3636903412-MW5R EPA 3010A EPA 6010
92342317012 363145 3636903412-MW12 EPA 3010A EPA 6010
92342317013 363147 3637923412-SW1 EPA 3010A EPA 6010
92342317014 363147 3637923412-SW3 EPA 3010A EPA 6010
92342317015 363147 3637923412-SW4 EPA 3010A EPA 6010
92342317017 363321 3646213412-MW2R EPA 3010A EPA 6010
92342317018 363321 3646213412-MW4R EPA 3010A EPA 6010
92342317019 363321 3646213412-MW10 EPA 3010A EPA 6010
92342317020 363321 3646213412-MW11 EPA 3010A EPA 6010
92342317001 362965 3631793412-EQUIPMENT BLANK EPA 3010A EPA 6020B
92342317002 362965 3631793412-MW8 EPA 3010A EPA 6020B
92342317003 362965 3631793412-MW9 EPA 3010A EPA 6020B
92342317004 362965 3631793412-MW13 EPA 3010A EPA 6020B
92342317005 362966 3631813412-MW14 EPA 3010A EPA 6020B
92342317006 363105 3631133412-MW1R EPA 3010A EPA 6020B
92342317007 363105 3631133412-MW15 EPA 3010A EPA 6020B
92342317008 363105 3631133412-MW3R EPA 3010A EPA 6020B
92342317009 363105 3631133412-MW7 EPA 3010A EPA 6020B
92342317010 363105 3631133412-SW2 EPA 3010A EPA 6020B
92342317011 363105 3631133412-MW5R EPA 3010A EPA 6020B
92342317012 363105 3631133412-MW12 EPA 3010A EPA 6020B
92342317013 363105 3631133412-SW1 EPA 3010A EPA 6020B
92342317014 363105 3631133412-SW3 EPA 3010A EPA 6020B
92342317015 363105 3631133412-SW4 EPA 3010A EPA 6020B
92342317017 363273 3633783412-MW2R EPA 3010A EPA 6020B
92342317018 363273 3633783412-MW4R EPA 3010A EPA 6020B
92342317019 363273 3633783412-MW10 EPA 3010A EPA 6020B
92342317020 363273 3633783412-MW11 EPA 3010A EPA 6020B
92342317001 362989 3630883412-EQUIPMENT BLANK EPA 7470 EPA 7470
92342317002 362989 3630883412-MW8 EPA 7470 EPA 7470
92342317003 362989 3630883412-MW9 EPA 7470 EPA 7470
92342317004 362989 3630883412-MW13 EPA 7470 EPA 7470
92342317005 363241 3635713412-MW14 EPA 7470 EPA 7470
92342317006 363457 3634833412-MW1R EPA 7470 EPA 7470
92342317007 363457 3634833412-MW15 EPA 7470 EPA 7470
92342317008 363457 3634833412-MW3R EPA 7470 EPA 7470
92342317009 363457 3634833412-MW7 EPA 7470 EPA 7470
92342317010 363457 3634833412-SW2 EPA 7470 EPA 7470
92342317011 363457 3634833412-MW5R EPA 7470 EPA 7470
92342317012 363457 3634833412-MW12 EPA 7470 EPA 7470
92342317013 363457 3634833412-SW1 EPA 7470 EPA 7470
92342317014 363457 3634833412-SW3 EPA 7470 EPA 7470
92342317015 363457 3634833412-SW4 EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 155 of 199
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342317017 363333 3633343412-MW2R EPA 7470 EPA 7470
92342317018 363333 3633343412-MW4R EPA 7470 EPA 7470
92342317019 363333 3633343412-MW10 EPA 7470 EPA 7470
92342317020 363333 3633343412-MW11 EPA 7470 EPA 7470
92342317001 362852 3631853412-EQUIPMENT BLANK EPA 3510 EPA 8270
92342317006 363352 3637673412-MW1R EPA 3510 EPA 8270
92342317007 363352 3637673412-MW15 EPA 3510 EPA 8270
92342317008 363352 3637673412-MW3R EPA 3510 EPA 8270
92342317010 363352 3637673412-SW2 EPA 3510 EPA 8270
92342317017 364045 3642193412-MW2R EPA 3510 EPA 8270
92342317018 364045 3642193412-MW4R EPA 3510 EPA 8270
92342317001 3628753412-EQUIPMENT BLANK EPA 8260
92342317002 3628753412-MW8 EPA 8260
92342317003 3628753412-MW9 EPA 8260
92342317004 3628753412-MW13 EPA 8260
92342317005 3628753412-MW14 EPA 8260
92342317006 3630243412-MW1R EPA 8260
92342317007 3630243412-MW15 EPA 8260
92342317008 3630243412-MW3R EPA 8260
92342317009 3630243412-MW7 EPA 8260
92342317010 3630243412-SW2 EPA 8260
92342317011 3630263412-MW5R EPA 8260
92342317012 3630263412-MW12 EPA 8260
92342317013 3630263412-SW1 EPA 8260
92342317014 3630263412-SW3 EPA 8260
92342317015 3630263412-SW4 EPA 8260
92342317016 3633283412-TRIP BLANK EPA 8260
92342317017 3633113412-MW2R EPA 8260
92342317018 3633113412-MW4R EPA 8260
92342317019 3633113412-MW10 EPA 8260
92342317020 3633113412-MW11 EPA 8260
92342317002 3629603412-MW8 SM 2320B
92342317003 3629603412-MW9 SM 2320B
92342317004 3629603412-MW13 SM 2320B
92342317005 3629603412-MW14 SM 2320B
92342317006 3631253412-MW1R SM 2320B
92342317007 3631253412-MW15 SM 2320B
92342317008 3631253412-MW3R SM 2320B
92342317009 3631253412-MW7 SM 2320B
92342317010 3631253412-SW2 SM 2320B
92342317011 3631253412-MW5R SM 2320B
92342317012 3631253412-MW12 SM 2320B
92342317013 3631253412-SW1 SM 2320B
92342317014 3631253412-SW3 SM 2320B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 156 of 199
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342317015 3631253412-SW4 SM 2320B
92342317017 3633433412-MW2R SM 2320B
92342317018 3633433412-MW4R SM 2320B
92342317019 3633433412-MW10 SM 2320B
92342317020 3633433412-MW11 SM 2320B
92342317002 3634353412-MW8 SM 2540C
92342317003 3634353412-MW9 SM 2540C
92342317004 3634353412-MW13 SM 2540C
92342317005 3634353412-MW14 SM 2540C
92342317006 3634753412-MW1R SM 2540C
92342317007 3634753412-MW15 SM 2540C
92342317008 3634753412-MW3R SM 2540C
92342317009 3634753412-MW7 SM 2540C
92342317010 3634753412-SW2 SM 2540C
92342317011 3634753412-MW5R SM 2540C
92342317012 3634753412-MW12 SM 2540C
92342317013 3634753412-SW1 SM 2540C
92342317014 3634753412-SW3 SM 2540C
92342317015 3634753412-SW4 SM 2540C
92342317017 3636583412-MW2R SM 2540C
92342317018 3636583412-MW4R SM 2540C
92342317019 3636583412-MW10 SM 2540C
92342317020 3636583412-MW11 SM 2540C
92342317001 3630783412-EQUIPMENT BLANK SM 4500-S2D
92342317002 3630783412-MW8 SM 4500-S2D
92342317003 3630783412-MW9 SM 4500-S2D
92342317004 3630783412-MW13 SM 4500-S2D
92342317005 3630783412-MW14 SM 4500-S2D
92342317006 3636213412-MW1R SM 4500-S2D
92342317007 3636213412-MW15 SM 4500-S2D
92342317008 3636213412-MW3R SM 4500-S2D
92342317009 3636213412-MW7 SM 4500-S2D
92342317010 3636213412-SW2 SM 4500-S2D
92342317011 3636233412-MW5R SM 4500-S2D
92342317012 3636233412-MW12 SM 4500-S2D
92342317013 3636233412-SW1 SM 4500-S2D
92342317014 3636233412-SW3 SM 4500-S2D
92342317015 3636233412-SW4 SM 4500-S2D
92342317017 3636313412-MW2R SM 4500-S2D
92342317018 3636313412-MW4R SM 4500-S2D
92342317019 3636313412-MW10 SM 4500-S2D
92342317020 3636313412-MW11 SM 4500-S2D
92342317002 3632803412-MW8 EPA 300.0
92342317003 3632803412-MW9 EPA 300.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 157 of 199
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342317004 3632803412-MW13 EPA 300.0
92342317005 3632803412-MW14 EPA 300.0
92342317006 3632813412-MW1R EPA 300.0
92342317007 3632813412-MW15 EPA 300.0
92342317008 3632813412-MW3R EPA 300.0
92342317009 3632813412-MW7 EPA 300.0
92342317010 3632813412-SW2 EPA 300.0
92342317011 3632813412-MW5R EPA 300.0
92342317012 3632813412-MW12 EPA 300.0
92342317013 3632813412-SW1 EPA 300.0
92342317014 3632813412-SW3 EPA 300.0
92342317015 3633963412-SW4 EPA 300.0
92342317017 3633963412-MW2R EPA 300.0
92342317018 3633963412-MW4R EPA 300.0
92342317019 3642913412-MW10 EPA 300.0
92342317020 3642913412-MW11 EPA 300.0
92342317002 3631503412-MW8 SM 4500-Cl-E
92342317003 3631503412-MW9 SM 4500-Cl-E
92342317004 3631503412-MW13 SM 4500-Cl-E
92342317005 3631503412-MW14 SM 4500-Cl-E
92342317006 3633713412-MW1R SM 4500-Cl-E
92342317007 3633713412-MW15 SM 4500-Cl-E
92342317008 3633713412-MW3R SM 4500-Cl-E
92342317009 3633713412-MW7 SM 4500-Cl-E
92342317010 3633713412-SW2 SM 4500-Cl-E
92342317011 3633713412-MW5R SM 4500-Cl-E
92342317012 3633713412-MW12 SM 4500-Cl-E
92342317013 3633713412-SW1 SM 4500-Cl-E
92342317014 3633713412-SW3 SM 4500-Cl-E
92342317015 3633713412-SW4 SM 4500-Cl-E
92342317017 3645373412-MW2R SM 4500-Cl-E
92342317018 3645373412-MW4R SM 4500-Cl-E
92342317019 3645383412-MW10 SM 4500-Cl-E
92342317020 3645383412-MW11 SM 4500-Cl-E
92342317001 3629913412-EQUIPMENT BLANK SM 4500-CN-E
92342317002 3629913412-MW8 SM 4500-CN-E
92342317003 3629913412-MW9 SM 4500-CN-E
92342317004 3629913412-MW13 SM 4500-CN-E
92342317005 3629913412-MW14 SM 4500-CN-E
92342317006 3635123412-MW1R SM 4500-CN-E
92342317007 3635123412-MW15 SM 4500-CN-E
92342317008 3635123412-MW3R SM 4500-CN-E
92342317009 3635123412-MW7 SM 4500-CN-E
92342317010 3635123412-SW2 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 158 of 199
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342317
OSR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342317011 3635123412-MW5R SM 4500-CN-E
92342317012 3635123412-MW12 SM 4500-CN-E
92342317013 3635123412-SW1 SM 4500-CN-E
92342317014 3635123412-SW3 SM 4500-CN-E
92342317015 3635133412-SW4 SM 4500-CN-E
92342317017 3635133412-MW2R SM 4500-CN-E
92342317018 3635133412-MW4R SM 4500-CN-E
92342317019 3635133412-MW10 SM 4500-CN-E
92342317020 3635133412-MW11 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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Winston-Salem City/County Utilities | Assessment Monitoring Report
Appendix C – Field Data

C
Appendix C – Field Data

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Winston-Salem City/County Utilities | Assessment Monitoring Report
Appendix D – Electronic Files

D
Appendix D – Electronic Files
Portable Document Format (PDF) of this Report
Electronic Data Deliverable (EDD) of Groundwater
Results

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