2904_DavidsonCoMSWLF_GWMR_DIN28618_20170302

15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
Benzene ug/L 12/09/03 1.6 BRL BRL 1.0
11/30/04 BRL BRL BRL
05/26/05 1.7 BRL BRL
11/08/05 2.0 BRL BRL
06/01/06 1.9 BRL BRL
06/26/07 1.8 BRL BRL
11/27/07 1.3 BRL BRL
05/22/08 1.6 BRL BRL
11/20/08 1.4 BRL BRL
10/06/09 2.0 BRL BRL
12/01/09 2.2 BRL BRL
07/20/10 2.6 BRL BRL
01/25/11 2.1 BRL BRL
07/14/11 2.2 BRL BRL
02/21/12 2.2 BRL BRL
08/14/12 2.1 BRL BRL
02/14/13 2.1 BRL BRL
08/22/13 2.5 BRL BRL
02/25/14 2.8 BRL BRL
08/21/14 2.0 BRL BRL
04/09/15 3.1 BRL BRL
08/11/16 2.1 BRL BRL
02/09/17 1.2 BRL BRL
Toluene ug/L 12/09/03 BRL BRL BRL 1,000
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Volatile Organic Compounds (ug/L)
Page 1 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Toluene 12/01/09 BRL BRL BRL
ug/L 07/20/10 BRL BRL BRL 1,000
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Ethylbenzene ug/L 12/09/03 BRL BRL BRL 600
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Page 2 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Total Xylenes ug/L 12/09/03 BRL BRL BRL 500
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 0.5J BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Chlorobenzene ug/L 12/09/03 10 BRL BRL 50
11/30/04 8.3 BRL BRL
05/26/05 12.0 BRL BRL
11/08/05 7.1 BRL BRL
06/01/06 12.0 BRL BRL
06/26/07 11.0 1.2 0.7J
11/27/07 7.0 0.90J BRL
05/22/08 10.0 BRL BRL
11/20/08 8.8 BRL BRL
10/06/09 9.3 1.2 0.84J
12/01/09 12.0 BRL BRL
Page 3 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Chlorobenzene ug/L 07/20/10 10.0 1.5 0.57J
01/25/11 7.9 0.72J BRL
07/14/11 11.6 BRL BRL 50
02/21/12 10.50 BRL BRL
08/14/12 8.50 BRL BRL
02/14/13 7.90 BRL BRL
08/22/13 10.20 BRL BRL
02/25/14 9.80 BRL BRL
08/21/14 7.50 1.1 BRL
04/09/15 8.60 BRL BRL
08/11/16 10.90 BRL BRL
02/09/17 7.9 1.6 BRL
1,2-Dichlorobenzene ug/L 12/09/03 BRL BRL BRL 20.0
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 0.51J BRL BRL
06/26/07 0.6J BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Page 4 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
1,4-Dichlorobenzene ug/L 12/09/03 1.8 BRL BRL 6.0
11/30/04 BRL BRL BRL
05/26/05 2.7 BRL BRL
11/08/05 1.8 BRL BRL
06/01/06 2.0 BRL BRL
06/26/07 2.2 BRL BRL
11/27/07 1.8 BRL BRL
05/22/08 BRL BRL BRL
11/20/08 2.6 BRL BRL
10/06/09 2.1 BRL BRL
12/01/09 2.0 BRL BRL
07/20/10 1.5 0.75J BRL
01/25/11 2.0 BRL BRL
07/14/11 2.1 BRL BRL
02/21/12 1.6 BRL BRL
08/14/12 2.2 BRL BRL
02/14/13 1.9 BRL BRL
08/22/13 2.6 BRL BRL
02/25/14 2.1 BRL BRL
08/21/14 2.3 BRL BRL
04/09/15 2.1 BRL BRL
08/11/16 2.3 BRL BRL
02/09/17 1.5 BRL BRL
1,1-Dichloroethane ug/L 12/09/03 1.3 BRL BRL 6.0
11/30/04 1.0 BRL BRL
05/26/05 1.2 BRL BRL
11/08/05 BRL BRL BRL
06/01/06 0.86J BRL BRL
06/26/07 0.69J 0.65J BRL
11/27/07 BRL 0.65J BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
Page 5 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
1,1-Dichloroethane ug/L 07/14/11 BRL BRL BRL 6.0
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
1,2-Dichloroethene (cis) ug/L 12/09/03 0.96J BRL BRL 70
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 0.61J BRL BRL
06/26/07 0.59J BRL BRL
11/27/07 BRL BRL BRL
05/22/08 0.62J BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Page 6 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Isopropylbenzene ug/L 12/09/03 BRL BRL BRL 70
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 0.52J BRL BRL
06/26/07 0.53J BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Trichloroethylene ug/L 12/09/03 BRL BRL BRL 3.0
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
Page 7 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Trichloroethylene ug/L 07/14/11 BRL BRL BRL 3.0
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Vinyl Chloride ug/L 12/09/03 4.6 BRL BRL 0.03
11/30/04 2.6 BRL BRL
05/26/05 2.4 BRL BRL
11/08/05 2.2 BRL BRL
06/01/06 BRL BRL BRL
06/26/07 0.64J BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Page 8 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
MTBE ug/L 12/09/03 1.9 BRL BRL 20
11/30/04 BRL BRL BRL
05/26/05 1.3 BRL BRL
11/08/05 1.3 BRL BRL
06/01/06 2.8 BRL BRL
06/26/07 1.4 BRL BRL
11/27/07 1.1 BRL BRL
05/22/08 1.1 BRL BRL
11/20/08 0.94J BRL BRL
10/06/09 1.2 BRL BRL
12/01/09 1.0 BRL BRL
07/20/10 1.2 BRL BRL
01/25/11 0.96J BRL BRL
07/14/11 1.1 BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL 20
08/21/14 BRL BRL BRL
04/09/15 1.1 BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Page 9 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
IPE ug/L 12/09/03 BRL BRL BRL 70.0
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Page 10 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Arsenic, Total mg/L 12/09/03 BRL BRL BRL 0.010
11/30/04 BRL BRL BRL
05/26/05 0.01 0.01 BRL
11/08/05 BRL BRL BRL
06/01/06 0.0048J BRL 0.0060J
06/26/07 0.0025J BRL BRL
11/27/07 BRL 0.0041J BRL
05/22/08 0.011 0.0098J 0.0038J
11/20/08 BRL 0.0023J BRL
10/06/09 0.0067J 0.0058J 0.0051J
12/01/09 0.0034J 0.0052J 0.0016J
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL 0.0107 0.0053
08/14/12 BRL BRL 0.0084
02/14/13 BRL BRL 0.0106
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL 0.0128 BRL
04/09/15 BRL 0.0183 BRL
08/11/16 BRL 0.0146 BRL
02/09/17 BRL 0.0223 BRL
Cadmium, Total mg/L 12/09/03 0.007 0.006 BRL 0.002
11/30/04 0.0011 0.0011 BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL 0.0005J
12/01/09 BRL BRL 0.002
Metals (Results and 2L Standards in mg/L)
Page 11 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Cadmium, Total mg/L 07/20/10 BRL BRL BRL 0.002
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL 0.0013
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Chromium, Total mg/L 12/09/03 BRL BRL BRL 0.010
11/30/04 BRL BRL BRL
05/26/05 0.0053 0.0058 BRL
11/08/05 BRL BRL 0.0059
06/01/06 BRL BRL 0.0031J
06/26/07 BRL BRL 0.0036J
11/27/07 0.0059 0.015 0.0030J
05/22/08 BRL BRL 0.0008J
11/20/08 0.0004J 0.0007J 0.0018J
10/06/09 0.0005J 0.0014J 0.0014J
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL 0.0086
02/25/14 BRL BRL BRL
08/21/14 BRL 0.0082 0.0057
04/09/15 BRL 0.0089 BRL
08/11/16 BRL 0.0057 BRL
02/09/17 BRL 0.0075 BRL
Page 12 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Copper, Total mg/L 12/09/03 BRL BRL BRL 1.0
11/30/04 BRL BRL BRL
05/26/05 BRL 0.012 BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 0.0054J 0.012 0.011
11/27/07 BRL 0.0091J 0.0029J
05/22/08 BRL 0.0013J 0.0024J
11/20/08 0.0050J 0.0090J 0.0033J
10/06/09 0.0019J 0.0023J BRL
12/01/09 0.0067J 0.0070J 0.0032J
07/20/10 BRL BRL BRL
01/25/11 BRL 0.014 BRL
07/14/11 BRL BRL BRL
02/21/12 0.0078 0.012 0.0094
08/14/12 BRL BRL 0.0109
02/14/13 BRL BRL 0.0146
08/22/13 BRL 0.0098 0.0135
02/25/14 BRL BRL BRL
08/21/14 BRL 0.0104 BRL
04/09/15 BRL 0.0243 BRL
08/11/16 BRL 0.0092 BRL
02/09/17 BRL 0.0146 BRL
Lead, Total mg/L 12/09/03 BRL BRL BRL 0.015
11/30/04 0.0052 BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 0.0033J 0.0025J BRL
06/26/07 BRL BRL BRL
11/27/07 BRL 0.007 BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
01/25/11 BRL BRL BRL
Page 13 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Lead, Total mg/L 07/14/11 BRL BRL BRL 0.015
02/21/12 BRL BRL BRL
08/14/12 BRL BRL 0.0060
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 BRL BRL BRL
04/09/15 BRL 0.0063 BRL
08/11/16 BRL 0.0064 BRL
02/09/17 BRL BRL BRL
Nickel, Total mg/L 12/09/03 0.019 0.011 0.012 0.100
11/30/04 0.025 0.02 BRL
05/26/05 BRL BRL BRL
11/08/05 0.016 BRL 0.014
06/01/06 0.0092J BRL 0.014
06/26/07 0.013 0.0064J 0.011
11/27/07 0.014 0.0066J 0.0061J
05/22/08 0.0069J 0.0016J 0.0054J
11/20/08 0.01 0.0006J 0.0021J
10/06/09 0.014 0.0048J 0.01
12/01/09 0.0052J BRL BRL
07/20/10 0.011 BRL BRL
01/25/11 0.010 BRL BRL
07/14/11 BRL BRL BRL
02/21/12 0.0087 BRL BRL
08/14/12 0.0110 0.0069 BRL
02/14/13 0.0127 BRL BRL
08/22/13 0.0084 BRL BRL
02/25/14 0.0118 BRL BRL
08/21/14 0.0124 0.0053 0.0078
04/09/15 0.0103 0.0073 BRL
08/11/16 0.0119 BRL BRL
02/09/17 0.0189 0.0115 BRL
Page 14 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Selenium, Total mg/L 12/09/03 BRL BRL BRL 0.0200
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 0.013J 0.019J 0.019J 0.0200
11/27/07 BRL BRL 0.0089J
05/22/08 BRL BRL 0.0089J
11/20/08 BRL 0.011J BRL
10/06/09 BRL 0.006J BRL
12/01/09 0.016J 0.019J BRL
07/20/10 0.030 0.032 BRL
01/25/11 BRL BRL BRL
07/14/11 BRL BRL BRL
02/21/12 BRL BRL BRL
08/14/12 BRL BRL BRL
02/14/13 BRL BRL BRL
08/22/13 BRL BRL BRL
02/25/14 BRL BRL BRL
08/21/14 0.0369 0.0171 0.0193
04/09/15 BRL BRL BRL
08/11/16 BRL BRL BRL
02/09/17 BRL BRL BRL
Zinc, Total mg/L 12/09/03 BRL BRL BRL 1.0
11/30/04 BRL BRL BRL
05/26/05 BRL BRL BRL
11/08/05 BRL BRL BRL
06/01/06 BRL BRL BRL
06/26/07 BRL BRL BRL
11/27/07 BRL BRL BRL
05/22/08 BRL BRL BRL
11/20/08 BRL BRL BRL
10/06/09 BRL BRL BRL
12/01/09 BRL BRL BRL
07/20/10 BRL BRL BRL
Page 15 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Zinc, Total mg/L 01/25/11 BRL 0.069 BRL
07/14/11 BRL 0.049 0.016
02/21/12 0.016 0.0359 0.0266
08/14/12 BRL 0.01 0.0606
02/14/13 BRL 0.0224 0.0335
08/22/13 0.0203 0.0754 0.0386
02/25/14 BRL 0.0945 0.0160 1.0
08/21/14 BRL 0.0657 0.0242
04/09/15 BRL 0.0851 0.0256
08/11/16 0.0292 0.0599 0.0384
02/09/17 0.0169 0.0854 0.0339
pH 12/09/03 6.76 6.61 6.99 6.0-9.0
11/30/04 5.93 5.70 5.31
05/26/05 6.45 6.23 6.46
11/08/05 6.90 6.74 7.10
06/01/06 6.26 6.17 6.50
06/26/07 7.60 7.44 7.64
11/27/07 7.93 7.43 7.70
05/22/08 8.11 7.73 8.12
11/20/08 7.42 7.34 7.95
10/06/09 6.30 6.09 6.38
12/01/09 NR NR NR
07/20/10 5.79 5.75 5.68
01/25/11 7.80 7.64 8.01
07/14/11 6.35 6.22 6.40
02/21/12 6.29 6.16 6.24
08/14/12 6.23 6.35 6.10
02/14/13 6.57 6.29 6.33
08/22/13 6.43 6.33 6.51
02/25/14 6.90 6.79 7.04
08/21/14 7.01 7.46 7.81
04/09/15 7.70 6.56 4.26
08/11/16 5.81 5.95 6.23
02/09/17 NR NR NR
Field Parameters
Page 16 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Conductivity 12/09/03 0.248 0.102 0.165 NA
11/30/04 0.26 99.9 39.3
05/26/05 0.252 80 42.1
11/08/05 0.262 0.14 0.2
06/01/06 0.269 0.154 0.2
06/26/07 0.102 0.159 0.192
11/27/07 0.306 0.128 79.7
05/22/08 0.287 0.141 83.5
11/20/08 0.301 0.123 47.6
10/06/09 0.327 0.18 0.254 NA
12/01/09 NR NR NR
07/20/10 2.37 1.31 1.51
01/25/11 0.299 0.133 67.7
07/14/11 5.640 2.170 1.5
02/21/12 2.51 0.601 0.462
08/14/12 2.55 2.070 1.120
02/14/13 2.53 0.253 0.472
08/22/13 2.630 0.519 0.470
02/25/14 3.04 0.623 0.292
08/21/14 2.81 1.36 2.14
04/09/15 2.89 1.16 0.386
08/11/16 2.56 0.763 0.236
02/09/17 NR NR NR
Turbidity (NTU) 12/09/03 201 69.8 117 NA
11/30/04 NR NR NR
05/26/05 NR NR NR
11/08/05 NR NR NR
06/01/06 NR NR NR
06/26/07 -5 -5 -5
11/27/07 537 -5 -5
05/22/08 -5 -5 -5
11/20/08 -5 -5 -5
10/06/09 -5 -5 -5
12/01/09 NR NR NR
Page 17 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Turbidity 07/20/10 25.3 6.4 6.8
01/25/11 637 876 230
07/14/11 25 177 399
02/21/12 76 187 364
08/14/12 38 517 314
02/14/13 48 647 285
08/22/13 62 237 333
02/25/14 89 283 279
08/21/14 68 267 290
04/09/15 51 366 500
08/11/16 152 145 269
02/09/17 NR NR NR
Dissolved Oxygen 12/09/03 0 0 0.44 NA
11/30/04 0 0.45 0.41
05/26/05 0 0 0.31
11/08/05 9.26 1.67 0
06/01/06 2.45 4.53 0.11
06/26/07 2.52 7.94 5.08
11/27/07 5.32 2.43 4.16
05/22/08 3.71 2.50 3.26
11/20/08 7.19 0.34 9.62
10/06/09 5.31 6.33 4.38
12/01/09 NR NR NR
07/20/10 0.57 0.63 4.30
01/25/11 5.58 5.30 6.15
07/14/11 1.91 1.52 1.29
02/21/12 3.51 2.49 2.83
08/14/12 2.50 2.75 1.95
02/14/13 3.69 4.69 2.78
08/22/13 3.22 2.46 2.55
02/25/14 10.38 5.00 2.58
08/21/14 2.61 2.06 2.99
04/09/15 3.08 2.18 2.68
08/11/16 7.29 4.52 2.21
02/09/17 NR NR NR
Page 18 of 19
15A NCAC
PARAMETER UNITS Date MW-3 MW-4 MW-6 2L Standard
TABLE 1
Pyramid Project 2016-203
Groundwater Monitoring Results
Winding Creek Golf Course - Former City of Thomasville Landfill
72 Winding Creek Road, Thomasville, NC
Monitoring Well Numbers
Water Temperature C 12/09/03 18.2 16.1 14.8 NA
11/30/04 18.8 16.4 14.6
05/26/05 15.8 13.8 13.7
11/08/05 20 16.8 17.3
06/01/06 16.5 14.1 14.4
06/26/07 17.5 14.8 16.6
11/27/07 18 16.3 15.7
05/22/08 15.9 13.9 14.5
11/20/08 18.2 16.1 14.9
10/06/09 20.1 16.3 17.7
12/01/09 NR NR NR
07/20/10 19.8 16.1 17.4
01/25/11 14.5 13.4 9.5
07/14/11 21.9 18.7 21.3 NA
02/21/12 12.95 11.41 9.90
08/14/12 21.61 19.25 18.02
02/14/13 14.81 10.92 13.01
08/22/13 21.98 18.62 20.87
02/25/14 12.68 10.60 9.65
08/21/14 21.85 17.58 20.74
04/09/15 15.28 13.48 12.88
08/11/16 23.62 20.66 21.73
02/09/17 NR NR NR
Shaded values exceed the applicable standard J = Estimated Value
µg/L = Micrograms per liter NS = No Standard Established
mg/L = Milligrams per liter BRL = Below Reporting Limit
HT= Received and analyzed out of hold time NA = Not analyzed for this parameter
NR = Not Recorded
Page 19 of 19
#=CL#
February 17, 2017
LIMS USE: FR - BRETT HIGGINS
LIMS OBJECT ID: 92329570
92329570
Project:
Pace Project No.:
RE:
Mr. Brett Higgins
Pyramid Environmental
P.O. Box 16265
503 Industrial Avenue
Greensboro, NC 27416
Winding Creek GC
Dear Mr. Higgins:
Enclosed are the analytical results for sample(s) received by the laboratory on February 10, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92329570
Winding Creek GC
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92329570
Winding Creek GC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92329570001 MW-3 EPA 6010 8 PASI-ASH1
EPA 8260 63 PASI-CGAW
92329570002 MW-4 EPA 6010 8 PASI-ASH1
EPA 8260 63 PASI-CGAW
92329570003 MW-6 EPA 6010 8 PASI-ASH1
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92329570
Winding Creek GC
Sample:MW-3 Lab ID:92329570001 Collected:02/09/17 12:00 Received:02/10/17 10:14 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 02/15/17 19:25 7440-38-202/13/17 23:0510.0 1
Cadmium ND ug/L 02/15/17 19:25 7440-43-902/13/17 23:051.0 1
Chromium ND ug/L 02/15/17 19:25 7440-47-302/13/17 23:055.0 1
Copper ND ug/L 02/15/17 19:25 7440-50-802/13/17 23:055.0 1
Lead ND ug/L 02/15/17 19:25 7439-92-102/13/17 23:055.0 1
Nickel 18.9 ug/L 02/15/17 19:25 7440-02-002/13/17 23:055.0 1
Selenium ND ug/L 02/15/17 19:25 7782-49-202/13/17 23:0510.0 1
Zinc 16.9 ug/L 02/15/17 19:25 7440-66-602/13/17 23:0510.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 02/15/17 22:06 67-64-125.0 1
Benzene 1.2 ug/L 02/15/17 22:06 71-43-21.0 1
Bromobenzene ND ug/L 02/15/17 22:06 108-86-11.0 1
Bromochloromethane ND ug/L 02/15/17 22:06 74-97-51.0 1
Bromodichloromethane ND ug/L 02/15/17 22:06 75-27-41.0 1
Bromoform ND ug/L 02/15/17 22:06 75-25-21.0 1
Bromomethane ND ug/L 02/15/17 22:06 74-83-9 L1,L32.0 1
2-Butanone (MEK)ND ug/L 02/15/17 22:06 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/15/17 22:06 56-23-51.0 1
Chlorobenzene 7.9 ug/L 02/15/17 22:06 108-90-71.0 1
Chloroethane ND ug/L 02/15/17 22:06 75-00-31.0 1
Chloroform ND ug/L 02/15/17 22:06 67-66-31.0 1
Chloromethane ND ug/L 02/15/17 22:06 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/15/17 22:06 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/15/17 22:06 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/15/17 22:06 96-12-82.0 1
Dibromochloromethane ND ug/L 02/15/17 22:06 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/15/17 22:06 106-93-41.0 1
Dibromomethane ND ug/L 02/15/17 22:06 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/15/17 22:06 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/15/17 22:06 541-73-11.0 1
1,4-Dichlorobenzene 1.5 ug/L 02/15/17 22:06 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/15/17 22:06 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/15/17 22:06 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/15/17 22:06 107-06-21.0 1
1,1-Dichloroethene ND ug/L 02/15/17 22:06 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/15/17 22:06 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/15/17 22:06 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/15/17 22:06 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/15/17 22:06 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/15/17 22:06 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/15/17 22:06 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/15/17 22:06 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/15/17 22:06 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/15/17 22:06 108-20-31.0 1
Ethylbenzene ND ug/L 02/15/17 22:06 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/15/17 22:06 87-68-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92329570
Winding Creek GC
Sample:MW-3 Lab ID:92329570001 Collected:02/09/17 12:00 Received:02/10/17 10:14 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
2-Hexanone ND ug/L 02/15/17 22:06 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/15/17 22:06 99-87-61.0 1
Methylene Chloride ND ug/L 02/15/17 22:06 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/15/17 22:06 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/15/17 22:06 1634-04-41.0 1
Naphthalene ND ug/L 02/15/17 22:06 91-20-31.0 1
Styrene ND ug/L 02/15/17 22:06 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/15/17 22:06 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/15/17 22:06 79-34-51.0 1
Tetrachloroethene ND ug/L 02/15/17 22:06 127-18-41.0 1
Toluene ND ug/L 02/15/17 22:06 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/15/17 22:06 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/15/17 22:06 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/15/17 22:06 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/15/17 22:06 79-00-51.0 1
Trichloroethene ND ug/L 02/15/17 22:06 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/15/17 22:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/15/17 22:06 96-18-41.0 1
Vinyl acetate ND ug/L 02/15/17 22:06 108-05-42.0 1
Vinyl chloride ND ug/L 02/15/17 22:06 75-01-41.0 1
Xylene (Total)ND ug/L 02/15/17 22:06 1330-20-71.0 1
m&p-Xylene ND ug/L 02/15/17 22:06 179601-23-12.0 1
o-Xylene ND ug/L 02/15/17 22:06 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %02/15/17 22:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/15/17 22:06 17060-07-070-130 1
Toluene-d8 (S)100 %02/15/17 22:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92329570
Winding Creek GC
Sample:MW-4 Lab ID:92329570002 Collected:02/09/17 10:30 Received:02/10/17 10:14 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic 22.3 ug/L 02/15/17 19:29 7440-38-202/13/17 23:0510.0 1
Cadmium ND ug/L 02/15/17 19:29 7440-43-902/13/17 23:051.0 1
Chromium 7.5 ug/L 02/15/17 19:29 7440-47-302/13/17 23:055.0 1
Copper 14.6 ug/L 02/15/17 19:29 7440-50-802/13/17 23:055.0 1
Lead ND ug/L 02/15/17 19:29 7439-92-102/13/17 23:055.0 1
Nickel 11.5 ug/L 02/15/17 19:29 7440-02-002/13/17 23:055.0 1
Selenium ND ug/L 02/15/17 19:29 7782-49-202/13/17 23:0510.0 1
Zinc 85.4 ug/L 02/15/17 19:29 7440-66-602/13/17 23:0510.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 02/15/17 22:22 67-64-125.0 1
Benzene ND ug/L 02/15/17 22:22 71-43-21.0 1
Bromobenzene ND ug/L 02/15/17 22:22 108-86-11.0 1
Bromochloromethane ND ug/L 02/15/17 22:22 74-97-51.0 1
Bromodichloromethane ND ug/L 02/15/17 22:22 75-27-41.0 1
Bromoform ND ug/L 02/15/17 22:22 75-25-21.0 1
Bromomethane ND ug/L 02/15/17 22:22 74-83-9 L1,L32.0 1
2-Butanone (MEK)ND ug/L 02/15/17 22:22 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/15/17 22:22 56-23-51.0 1
Chlorobenzene 1.6 ug/L 02/15/17 22:22 108-90-71.0 1
Chloroethane ND ug/L 02/15/17 22:22 75-00-31.0 1
Chloroform ND ug/L 02/15/17 22:22 67-66-31.0 1
Chloromethane ND ug/L 02/15/17 22:22 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/15/17 22:22 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/15/17 22:22 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/15/17 22:22 96-12-82.0 1
Dibromochloromethane ND ug/L 02/15/17 22:22 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/15/17 22:22 106-93-41.0 1
Dibromomethane ND ug/L 02/15/17 22:22 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/15/17 22:22 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/15/17 22:22 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/15/17 22:22 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/15/17 22:22 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/15/17 22:22 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/15/17 22:22 107-06-21.0 1
1,1-Dichloroethene ND ug/L 02/15/17 22:22 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/15/17 22:22 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/15/17 22:22 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/15/17 22:22 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/15/17 22:22 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/15/17 22:22 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/15/17 22:22 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/15/17 22:22 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/15/17 22:22 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/15/17 22:22 108-20-31.0 1
Ethylbenzene ND ug/L 02/15/17 22:22 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/15/17 22:22 87-68-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92329570
Winding Creek GC
Sample:MW-4 Lab ID:92329570002 Collected:02/09/17 10:30 Received:02/10/17 10:14 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
2-Hexanone ND ug/L 02/15/17 22:22 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/15/17 22:22 99-87-61.0 1
Methylene Chloride ND ug/L 02/15/17 22:22 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/15/17 22:22 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/15/17 22:22 1634-04-41.0 1
Naphthalene ND ug/L 02/15/17 22:22 91-20-31.0 1
Styrene ND ug/L 02/15/17 22:22 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/15/17 22:22 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/15/17 22:22 79-34-51.0 1
Tetrachloroethene ND ug/L 02/15/17 22:22 127-18-41.0 1
Toluene ND ug/L 02/15/17 22:22 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/15/17 22:22 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/15/17 22:22 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/15/17 22:22 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/15/17 22:22 79-00-51.0 1
Trichloroethene ND ug/L 02/15/17 22:22 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/15/17 22:22 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/15/17 22:22 96-18-41.0 1
Vinyl acetate ND ug/L 02/15/17 22:22 108-05-42.0 1
Vinyl chloride ND ug/L 02/15/17 22:22 75-01-41.0 1
Xylene (Total)ND ug/L 02/15/17 22:22 1330-20-71.0 1
m&p-Xylene ND ug/L 02/15/17 22:22 179601-23-12.0 1
o-Xylene ND ug/L 02/15/17 22:22 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %02/15/17 22:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %02/15/17 22:22 17060-07-070-130 1
Toluene-d8 (S)99 %02/15/17 22:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92329570
Winding Creek GC
Sample:MW-6 Lab ID:92329570003 Collected:02/09/17 11:20 Received:02/10/17 10:14 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 02/15/17 19:34 7440-38-202/13/17 23:0510.0 1
Cadmium ND ug/L 02/15/17 19:34 7440-43-902/13/17 23:051.0 1
Chromium ND ug/L 02/15/17 19:34 7440-47-302/13/17 23:055.0 1
Copper ND ug/L 02/15/17 19:34 7440-50-802/13/17 23:055.0 1
Lead ND ug/L 02/15/17 19:34 7439-92-102/13/17 23:055.0 1
Nickel ND ug/L 02/15/17 19:34 7440-02-002/13/17 23:055.0 1
Selenium ND ug/L 02/15/17 19:34 7782-49-202/13/17 23:0510.0 1
Zinc 33.9 ug/L 02/15/17 19:34 7440-66-602/13/17 23:0510.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 02/15/17 22:54 67-64-125.0 1
Benzene ND ug/L 02/15/17 22:54 71-43-21.0 1
Bromobenzene ND ug/L 02/15/17 22:54 108-86-11.0 1
Bromochloromethane ND ug/L 02/15/17 22:54 74-97-51.0 1
Bromodichloromethane ND ug/L 02/15/17 22:54 75-27-41.0 1
Bromoform ND ug/L 02/15/17 22:54 75-25-21.0 1
Bromomethane ND ug/L 02/15/17 22:54 74-83-9 L1,L3,
M0
2.0 1
2-Butanone (MEK)ND ug/L 02/15/17 22:54 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/15/17 22:54 56-23-51.0 1
Chlorobenzene ND ug/L 02/15/17 22:54 108-90-71.0 1
Chloroethane ND ug/L 02/15/17 22:54 75-00-31.0 1
Chloroform ND ug/L 02/15/17 22:54 67-66-31.0 1
Chloromethane ND ug/L 02/15/17 22:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/15/17 22:54 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/15/17 22:54 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/15/17 22:54 96-12-82.0 1
Dibromochloromethane ND ug/L 02/15/17 22:54 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/15/17 22:54 106-93-41.0 1
Dibromomethane ND ug/L 02/15/17 22:54 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/15/17 22:54 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/15/17 22:54 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/15/17 22:54 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/15/17 22:54 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/15/17 22:54 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/15/17 22:54 107-06-21.0 1
1,1-Dichloroethene ND ug/L 02/15/17 22:54 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/15/17 22:54 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/15/17 22:54 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/15/17 22:54 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/15/17 22:54 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/15/17 22:54 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/15/17 22:54 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/15/17 22:54 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/15/17 22:54 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/15/17 22:54 108-20-31.0 1
Ethylbenzene ND ug/L 02/15/17 22:54 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92329570
Winding Creek GC
Sample:MW-6 Lab ID:92329570003 Collected:02/09/17 11:20 Received:02/10/17 10:14 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 02/15/17 22:54 87-68-31.0 1
2-Hexanone ND ug/L 02/15/17 22:54 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/15/17 22:54 99-87-61.0 1
Methylene Chloride ND ug/L 02/15/17 22:54 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/15/17 22:54 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/15/17 22:54 1634-04-41.0 1
Naphthalene ND ug/L 02/15/17 22:54 91-20-31.0 1
Styrene ND ug/L 02/15/17 22:54 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/15/17 22:54 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/15/17 22:54 79-34-51.0 1
Tetrachloroethene ND ug/L 02/15/17 22:54 127-18-41.0 1
Toluene ND ug/L 02/15/17 22:54 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/15/17 22:54 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/15/17 22:54 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/15/17 22:54 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/15/17 22:54 79-00-51.0 1
Trichloroethene ND ug/L 02/15/17 22:54 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/15/17 22:54 75-69-4 M11.0 1
1,2,3-Trichloropropane ND ug/L 02/15/17 22:54 96-18-41.0 1
Vinyl acetate ND ug/L 02/15/17 22:54 108-05-42.0 1
Vinyl chloride ND ug/L 02/15/17 22:54 75-01-41.0 1
Xylene (Total)ND ug/L 02/15/17 22:54 1330-20-71.0 1
m&p-Xylene ND ug/L 02/15/17 22:54 179601-23-12.0 1
o-Xylene ND ug/L 02/15/17 22:54 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %02/15/17 22:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/15/17 22:54 17060-07-070-130 1
Toluene-d8 (S)101 %02/15/17 22:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
348027
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92329570001, 92329570002, 92329570003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1931003
Associated Lab Samples:92329570001, 92329570002, 92329570003
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 02/15/17 18:44
Cadmium ug/L ND 1.0 02/15/17 18:44
Chromium ug/L ND 5.0 02/15/17 18:44
Copper ug/L ND 5.0 02/15/17 18:44
Lead ug/L ND 5.0 02/15/17 18:44
Nickel ug/L ND 5.0 02/15/17 18:44
Selenium ug/L ND 10.0 02/15/17 18:44
Zinc ug/L ND 10.0 02/15/17 18:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1931004LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 436500 87 80-120
Cadmium ug/L 456500 91 80-120
Chromium ug/L 459500 92 80-120
Copper ug/L 454500 91 80-120
Lead ug/L 444500 89 80-120
Nickel ug/L 446500 89 80-120
Selenium ug/L 451500 90 80-120
Zinc ug/L 458500 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1931005MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92329555005
1931006
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 95 75-12594 150033.3 510 504
Cadmium ug/L 500 88 75-12587 2500ND441434
Chromium ug/L 500 90 75-12589 2500ND450443
Copper ug/L 500 95 75-12595 1500ND479475
Lead ug/L 500 86 75-12585 15007.2 439 434
Nickel ug/L 500 86 75-12585 15005.3 433 428
Selenium ug/L 500 95 75-12594 150023.0 499 494
Zinc ug/L 500 94 75-12592 2500ND468459
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
348387
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92329570001, 92329570002, 92329570003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1932915
Associated Lab Samples:92329570001, 92329570002, 92329570003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/15/17 15:27
1,1,1-Trichloroethane ug/L ND 1.0 02/15/17 15:27
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/15/17 15:27
1,1,2-Trichloroethane ug/L ND 1.0 02/15/17 15:27
1,1-Dichloroethane ug/L ND 1.0 02/15/17 15:27
1,1-Dichloroethene ug/L ND 1.0 02/15/17 15:27
1,1-Dichloropropene ug/L ND 1.0 02/15/17 15:27
1,2,3-Trichlorobenzene ug/L ND 1.0 02/15/17 15:27
1,2,3-Trichloropropane ug/L ND 1.0 02/15/17 15:27
1,2,4-Trichlorobenzene ug/L ND 1.0 02/15/17 15:27
1,2-Dibromo-3-chloropropane ug/L ND 2.0 02/15/17 15:27
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/15/17 15:27
1,2-Dichlorobenzene ug/L ND 1.0 02/15/17 15:27
1,2-Dichloroethane ug/L ND 1.0 02/15/17 15:27
1,2-Dichloropropane ug/L ND 1.0 02/15/17 15:27
1,3-Dichlorobenzene ug/L ND 1.0 02/15/17 15:27
1,3-Dichloropropane ug/L ND 1.0 02/15/17 15:27
1,4-Dichlorobenzene ug/L ND 1.0 02/15/17 15:27
2,2-Dichloropropane ug/L ND 1.0 02/15/17 15:27
2-Butanone (MEK)ug/L ND 5.0 02/15/17 15:27
2-Chlorotoluene ug/L ND 1.0 02/15/17 15:27
2-Hexanone ug/L ND 5.0 02/15/17 15:27
4-Chlorotoluene ug/L ND 1.0 02/15/17 15:27
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/15/17 15:27
Acetone ug/L ND 25.0 02/15/17 15:27
Benzene ug/L ND 1.0 02/15/17 15:27
Bromobenzene ug/L ND 1.0 02/15/17 15:27
Bromochloromethane ug/L ND 1.0 02/15/17 15:27
Bromodichloromethane ug/L ND 1.0 02/15/17 15:27
Bromoform ug/L ND 1.0 02/15/17 15:27
Bromomethane ug/L ND 2.0 02/15/17 15:27
Carbon tetrachloride ug/L ND 1.0 02/15/17 15:27
Chlorobenzene ug/L ND 1.0 02/15/17 15:27
Chloroethane ug/L ND 1.0 02/15/17 15:27
Chloroform ug/L ND 1.0 02/15/17 15:27
Chloromethane ug/L ND 1.0 02/15/17 15:27
cis-1,2-Dichloroethene ug/L ND 1.0 02/15/17 15:27
cis-1,3-Dichloropropene ug/L ND 1.0 02/15/17 15:27
Dibromochloromethane ug/L ND 1.0 02/15/17 15:27
Dibromomethane ug/L ND 1.0 02/15/17 15:27
Dichlorodifluoromethane ug/L ND 1.0 02/15/17 15:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1932915
Associated Lab Samples:92329570001, 92329570002, 92329570003
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 02/15/17 15:27
Ethylbenzene ug/L ND 1.0 02/15/17 15:27
Hexachloro-1,3-butadiene ug/L ND 1.0 02/15/17 15:27
m&p-Xylene ug/L ND 2.0 02/15/17 15:27
Methyl-tert-butyl ether ug/L ND 1.0 02/15/17 15:27
Methylene Chloride ug/L ND 2.0 02/15/17 15:27
Naphthalene ug/L ND 1.0 02/15/17 15:27
o-Xylene ug/L ND 1.0 02/15/17 15:27
p-Isopropyltoluene ug/L ND 1.0 02/15/17 15:27
Styrene ug/L ND 1.0 02/15/17 15:27
Tetrachloroethene ug/L ND 1.0 02/15/17 15:27
Toluene ug/L ND 1.0 02/15/17 15:27
trans-1,2-Dichloroethene ug/L ND 1.0 02/15/17 15:27
trans-1,3-Dichloropropene ug/L ND 1.0 02/15/17 15:27
Trichloroethene ug/L ND 1.0 02/15/17 15:27
Trichlorofluoromethane ug/L ND 1.0 02/15/17 15:27
Vinyl acetate ug/L ND 2.0 02/15/17 15:27
Vinyl chloride ug/L ND 1.0 02/15/17 15:27
Xylene (Total)ug/L ND 1.0 02/15/17 15:27
1,2-Dichloroethane-d4 (S)%95 70-130 02/15/17 15:27
4-Bromofluorobenzene (S)%98 70-130 02/15/17 15:27
Toluene-d8 (S)%99 70-130 02/15/17 15:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1932916LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 70-130
1,1,1-Trichloroethane ug/L 55.050 110 70-130
1,1,2,2-Tetrachloroethane ug/L 50.150 100 70-130
1,1,2-Trichloroethane ug/L 52.750 105 70-130
1,1-Dichloroethane ug/L 52.950 106 70-130
1,1-Dichloroethene ug/L 61.350 123 70-132
1,1-Dichloropropene ug/L 56.250 112 70-130
1,2,3-Trichlorobenzene ug/L 54.250 108 70-135
1,2,3-Trichloropropane ug/L 48.750 97 70-130
1,2,4-Trichlorobenzene ug/L 54.250 108 70-134
1,2-Dibromo-3-chloropropane ug/L 49.950 100 70-130
1,2-Dibromoethane (EDB)ug/L 49.450 99 70-130
1,2-Dichlorobenzene ug/L 52.050 104 70-130
1,2-Dichloroethane ug/L 50.850 102 70-130
1,2-Dichloropropane ug/L 52.450 105 70-130
1,3-Dichlorobenzene ug/L 50.450 101 70-130
1,3-Dichloropropane ug/L 50.450 101 70-130
1,4-Dichlorobenzene ug/L 50.150 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1932916LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 55.350 111 58-145
2-Butanone (MEK)ug/L 91.1100 91 70-145
2-Chlorotoluene ug/L 49.750 99 70-130
2-Hexanone ug/L 96.0100 96 70-144
4-Chlorotoluene ug/L 49.650 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 70-140
Acetone ug/L 88.6100 89 50-175
Benzene ug/L 54.350 109 70-130
Bromobenzene ug/L 49.550 99 70-130
Bromochloromethane ug/L 50.550 101 70-130
Bromodichloromethane ug/L 53.450 107 70-130
Bromoform ug/L 48.250 96 70-130
Bromomethane ug/L 65.5 L15013154-130
Carbon tetrachloride ug/L 54.950 110 70-132
Chlorobenzene ug/L 52.050 104 70-130
Chloroethane ug/L 47.150 94 64-134
Chloroform ug/L 51.550 103 70-130
Chloromethane ug/L 48.250 96 64-130
cis-1,2-Dichloroethene ug/L 50.650 101 70-131
cis-1,3-Dichloropropene ug/L 54.450 109 70-130
Dibromochloromethane ug/L 50.950 102 70-130
Dibromomethane ug/L 52.250 104 70-131
Dichlorodifluoromethane ug/L 40.950 82 56-130
Diisopropyl ether ug/L 53.450 107 70-130
Ethylbenzene ug/L 51.050 102 70-130
Hexachloro-1,3-butadiene ug/L 57.150 114 70-130
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 52.750 105 70-130
Methylene Chloride ug/L 56.750 113 63-130
Naphthalene ug/L 53.850 108 70-138
o-Xylene ug/L 50.950 102 70-130
p-Isopropyltoluene ug/L 49.750 99 70-130
Styrene ug/L 51.050 102 70-130
Tetrachloroethene ug/L 51.750 103 70-130
Toluene ug/L 53.750 107 70-130
trans-1,2-Dichloroethene ug/L 55.350 111 70-130
trans-1,3-Dichloropropene ug/L 52.650 105 70-132
Trichloroethene ug/L 52.750 105 70-130
Trichlorofluoromethane ug/L 55.950 112 62-133
Vinyl acetate ug/L 101100 101 66-157
Vinyl chloride ug/L 43.650 87 50-150
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1932918MATRIX SPIKE SAMPLE:
MSSpike
Result
92329570003
1,1,1,2-Tetrachloroethane ug/L 21.620 108 70-130ND
1,1,1-Trichloroethane ug/L 23.320 116 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.620 103 70-130ND
1,1,2-Trichloroethane ug/L 22.120 111 70-130ND
1,1-Dichloroethane ug/L 23.620 118 70-130ND
1,1-Dichloroethene ug/L 27.720 138 70-166ND
1,1-Dichloropropene ug/L 25.620 128 70-130ND
1,2,3-Trichlorobenzene ug/L 21.220 106 70-130ND
1,2,3-Trichloropropane ug/L 20.420 102 70-130ND
1,2,4-Trichlorobenzene ug/L 21.420 107 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.320 101 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.520 103 70-130ND
1,2-Dichlorobenzene ug/L 21.520 108 70-130ND
1,2-Dichloroethane ug/L 22.420 112 70-130ND
1,2-Dichloropropane ug/L 22.520 113 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,3-Dichloropropane ug/L 21.420 107 70-130ND
1,4-Dichlorobenzene ug/L 21.120 106 70-130ND
2,2-Dichloropropane ug/L 22.620 113 70-130ND
2-Butanone (MEK)ug/L 44.040 110 70-130ND
2-Chlorotoluene ug/L 21.720 108 70-130ND
2-Hexanone ug/L 39.240 98 70-130ND
4-Chlorotoluene ug/L 21.520 107 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.740 107 70-130ND
Acetone ug/L 36.340 91 70-130ND
Benzene ug/L 24.320 121 70-148ND
Bromobenzene ug/L 21.120 106 70-130ND
Bromochloromethane ug/L 22.720 114 70-130ND
Bromodichloromethane ug/L 22.520 113 70-130ND
Bromoform ug/L 19.920 99 70-130ND
Bromomethane ug/L 26.3 M02013170-130ND
Carbon tetrachloride ug/L 24.720 124 70-130ND
Chlorobenzene ug/L 22.320 111 70-146ND
Chloroethane ug/L 25.320 127 70-130ND
Chloroform ug/L 22.120 110 70-130ND
Chloromethane ug/L 20.820 104 70-130ND
cis-1,2-Dichloroethene ug/L 22.620 113 70-130ND
cis-1,3-Dichloropropene ug/L 22.320 112 70-130ND
Dibromochloromethane ug/L 21.720 108 70-130ND
Dibromomethane ug/L 21.720 109 70-130ND
Dichlorodifluoromethane ug/L 24.820 124 70-130ND
Diisopropyl ether ug/L 22.720 114 70-130ND
Ethylbenzene ug/L 23.020 115 70-130ND
Hexachloro-1,3-butadiene ug/L 21.720 109 70-130ND
m&p-Xylene ug/L 45.240 113 70-130ND
Methyl-tert-butyl ether ug/L 21.720 108 70-130ND
Methylene Chloride ug/L 23.220 116 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1932918MATRIX SPIKE SAMPLE:
MSSpike
Result
92329570003
Naphthalene ug/L 22.920 115 70-130ND
o-Xylene ug/L 22.220 111 70-130ND
p-Isopropyltoluene ug/L 21.220 106 70-130ND
Styrene ug/L 21.620 108 70-130ND
Tetrachloroethene ug/L 22.020 110 70-130ND
Toluene ug/L 23.320 116 70-155ND
trans-1,2-Dichloroethene ug/L 24.620 123 70-130ND
trans-1,3-Dichloropropene ug/L 21.420 107 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 26.4 M12013270-130ND
Vinyl acetate ug/L 36.140 90 70-130ND
Vinyl chloride ug/L 21.020 105 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92329570002
1932917SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L .74JND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92329570
Winding Creek GC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92329570002
1932917SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 1.5 101.6
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%100 396
4-Bromofluorobenzene (S)%99 099
Toluene-d8 (S)%99 199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92329570
Winding Creek GC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92329570
Winding Creek GC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92329570001 348027 348069MW-3 EPA 3010A EPA 6010
92329570002 348027 348069MW-4 EPA 3010A EPA 6010
92329570003 348027 348069MW-6 EPA 3010A EPA 6010
92329570001 348387MW-3 EPA 8260
92329570002 348387MW-4 EPA 8260
92329570003 348387MW-6 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/17/2017 02:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
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8/31/16
2016-203
Hunts Fork
Hanks Branch
flow
direction
flow
direction
suspected grondwater
flow direction