2903_DavidsonCoMSWLF_GWMR_DIN28617_20170524

May 31, 2017

Ms. Jackie Drummond, Hydrogeologist
NC Solid Waste Section, Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

Re: 2017 First Semi-Annual Monitoring Report
City of Lexington Closed Landfill
Lexington, North Carolina
Permit #29-03

Dear Jackie:

Babb & Associates, P.A. has completed the 2017 first semi-annual monitoring event at
the City of Lexington Closed Landfill. On May 1, 2017 ten groundwater monitoring
wells were sampled and analyzed for Appendix I parameters. One upgradient surface
water monitoring station (SW-1) and one downgradient surface water monitoring station
(SW-4) were also sampled for Appendix I parameters during this monitoring event. The
Appendix I samples were analyzed for volatile organic compounds (VOCs) by EPA
Method 8260B and inorganic compounds by EPA Method 6010B.

In accordance with the approved February 2016 City of Lexington Closed Landfill Water
Quality Monitoring Plan, semi-annual monitoring will not be required in the fall of 2017.
As no volatile organic compounds were reported above the 2L Groundwater Standards
during this monitoring event, the landfill will perform annual water quality monitoring at
the site. If future water quality monitoring events indicate volatile organic compounds
are present above the 2L Groundwater Standards, the site will revert back to semi-annual
monitoring.

A site map is provided with this report which shows the groundwater and surface water
sample locations and shallow potentiometric surface (Figure 1). An isoconcentration
map showing the estimated volatile organic compound concentrations is provided as
Figure 2. Additional attachments to this report include tables summarizing the
groundwater and surface water analytical results (Tables 1, 2, and 3), field parameters
collected during the monitoring event (Table 4), well construction information (Table 5),
and groundwater flow rates (Table 6). The laboratory analytical report, in pdf and EDD
formats, is included as Appendix A.

If you have any questions or if additional information is needed, please contact me at
[phone].

Respectfully,

Babb & Associates, P.A.

Gary D. Babb, P.G.
President

Attachments

cc: Mr. Wes Kimbrell
City of Lexington

Water Quality Monitoring Report

City of Lexington Closed Solid Waste Landfill
State Road 2001
Lexington, North Carolina
Permit No. 29-03

Prepared for:

City of Lexington Public Works
28 West Center Street
Lexington, North Carolina 27292

Prepared by:

Babb & Associates, P.A.
P.O. Box 37697
Raleigh, North Carolina 27627

May 2017

___________________________________
Gary D. Babb, Licensed Geologist

Table of Contents

1.0 Introduction 1
1.1 Site Information
1.2 Site Geology
1.3 Site Hydrogeology

2.0 Water Quality Monitoring Program 4
2.1 Groundwater Monitoring Network
2.2 Surface Water Monitoring Network

3.0 Water Quality Sample Collection 6
3.1 Field Sample Procedures
3.2 Field Quality Assurance
3.3 Sample Delivery/Chain-of-Custody

4.0 Laboratory Analysis 8

5.0 Hydrogeological Conditions 9

6.0 Laboratory Analytical Results 10
6.1 Groundwater Analytical Results
6.2 Surface Water Analytical Results
6.3 Quality Control Sample

7.0 Conclusions 12

Figure 1 Water Quality Monitoring Sample Locations/Potentiometric Map
Figure 2 TVOC Isoconcentration Map

Table 1 Groundwater Analytical Results – Inorganics
Table 2 Groundwater Analytical Results - Organics
Table 3 Surface Water Analytical Results
Table 4 Field Parameter Measurements
Table 5 Well Construction Information/Elevations
Table 6 Groundwater Flow Rates

Appendix A ENCO Laboratory Analytical Report

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1.0 Introduction

1.1 Site Information

The City of Lexington Closed Landfill is located approximately two miles northeast of
downtown Lexington, North Carolina on State Road 2001 in Davidson County, North
Carolina. The landfill ceased operation on May 1, 1990 and was closed by capping the
fill with a four-foot thick final cover using native soils. The northern boundary of the
landfill is established by the Southern Railroad which traverses the property from
southwest to the northeast. The eastern, southern, and western portions of the landfill are
bordered by Abbotts Creek which flows in a general southwesterly direction.

Properties adjacent to the closed landfill are either undeveloped woodland or farmland.
Property usage to the south and east is primarily undeveloped woodland, farmland, and
residential. Undeveloped woodland and residential properties are also present to the
north of the landfill. Properties to the immediate west are undeveloped woodland.
Several industrial/commercial facilities are located along US Highway 64, located
approximately 2,300 feet west/northwest of the landfill.

1.2 Site Geology

The subject property is located in the Carolina Slate Belt, which is part of the Piedmont
Physiographic Province of North Carolina. The geology of the Carolina Slate Belt is
characterized by metavolcanic and metamorphosed intrusive rock sequences. According
to the Geologic Map of North Carolina published by the Department of Natural
Resources and Community Development (Brown, 1985), the rocks underlying the subject
property are metavolcanic rocks consisting of interbedded felsic to mafic tuffs and
flowrock.

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According to the Geologic Map of The Charlotte Quadrangle, North Carolina and South
Carolina (Goldsmith, Milton, and Horton, 1988), the rocks underlying the landfill are
interbedded felsic and mafic metavolcanic rocks. The metavolcanic rocks are fine to
medium grained with locally coarse grained or agglomeratic rocks of basaltic, andesitic,
and dacitic composition. This report identified a fault located between the landfill
property and US Highway 64 which is oriented in a northeast/southwest direction. The
general course of Abbotts Creek changes from a southwesterly direction to a
south/southwest direction at the landfill following this fault.

1.3 Site Hydrogeology

The observed subsurface conditions at the landfill consist of white to gray/green
metavolcanic bedrock overlain by weathered saprolitic soil. The soil at the site is
comprised of a mixture of clay, silt, and sand. The majority of the original soil profile on
the landfill property has been altered during landfill operations to the extent that it is no
longer recognizable.

The northern section of the landfill is characterized by a layer of silty clay and sandy silt
soil that overlies metavolcanic bedrock. The thickness of the soil varies from greater
than 43' at monitoring well MW-5 to 9' at monitoring well MW-6. The eastern section of
the landfill is characterized by a layer of silty clay and silty sand soil that also overlies
metavolcanic bedrock. The thickness of the soil in this area varies from 18' at monitoring
well MW-8 to 38' at monitoring well MW-7. The southern section of the landfill is
characterized by a layer of sandy clay to clayey silt soil. Fine sandy clay was present
beneath these layers in monitoring well MW-10. Bedrock was not encountered during
well installation activities in the southern section of the landfill.

A series of rising head slug tests were conducted in nine of the landfill monitoring wells
on October 23-24, 1996. An In-Situ model SE 1000C Hermit Data Logger system with

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May 2017 Page 3

submersible pressure transducers was used to record the water level changes in each well
during the slug tests. The transducers were first lowered into the well and placed a
minimum of ten feet below the static water level. A disposable bailer was then placed in
the well so that the top of the bailer was just below the groundwater surface. The aquifer
was allowed to stabilize for approximately 30 minutes prior to starting each test. After
stabilization the bailer was quickly removed from the well causing a rapid change in the
groundwater level. The data logger recorded changes in the water table every five
seconds and the levels stabilized. The Bouwer and Rice method was used to evaluate the
results and calculate hydraulic conductivity (K).

The calculated K for the nine wells resulted in the following:

MW-2: K = 0.438 ft/day
MW-3: K = 0.0494 ft/day
MW-4: K = 0.323 ft/day
MW-5: K = 0.0812 ft/day
MW-6: K = 1.04 ft/day
MW-7 K = 0.0127 ft/day
MW-8: K = 0.0565 ft/day
MW-9: K = 2.66 ft/day
MW-10: K = 0.327 ft/day

The hydraulic conductivity (K) represents an approximation of the permeability of the subsurface
materials which transmit groundwater. In the monitoring wells evaluated at the landfill, the
estimated permeability values ranged from a minimum of 0.0127 ft/day to a maximum of 2.66
ft/day, with the average value of 0.506 ft/day. These values are within the typical range for
saprolitic soil. The variability of the values seen here may reflect the various geologic features
encountered, including drainage features, fractured bedrock, and/or floodplain sediments.

City of Lexington Closed Landfill Water Quality Monitoring Report
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2.0 Water Quality Monitoring Program

The water quality monitoring network at the closed City of Lexington Landfill is evaluated on a
semi-annual basis. The locations of the groundwater and surface water samples collected during
the semi-annual monitoring events are shown on the attached Figure 1.

2.1 Groundwater Monitoring Network

There are thirteen groundwater monitoring wells located at the facility that comprise the
existing groundwater monitoring network (Figure 1). Monitoring well MW-12 is the
upgradient sampling point which represents background groundwater quality. The
northern boundary of the landfill is monitored by five wells; MW-4, MW-5, MW-6, MW-
11, and MW-12. The eastern boundary of the landfill is monitored by four wells; MW-7,
MW-7D, MW-8, and MW-3. The southern boundary of the landfill, along Abbotts
Creek, is monitored by four wells; MW-2, MW-9, MW-10, and MW-10D.

Information regarding the date of installation, construction specifics, formation material
encountered, and Lat/Long location of the thirteen groundwater monitoring wells is
provided on Table 5.

Monitoring wells MW-4, MW-5, and MW-12 are located on the hydraulically upgradient
portion of the property, however, the water quality in these wells may be impacted by
their close proximity to the former landfill disposal areas. As such, these three well are
gauged for water levels only, no sample is collected for laboratory analyses.

The monitoring wells evaluated by laboratory analyses during each monitoring event
include:

MW-2 MW-3 MW-6 MW-7 MW-7D
MW-8 MW-9 MW-10 MW-10D MW-11

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2.2 Surface Water Monitoring Network

In addition to the on-site groundwater monitoring wells, two surface water samples are
collected from Abbotts Creek. A surface water sample is collected upstream (SW-1) and
downstream (SW-4) of the landfill from Abbotts Creek. The location of the surface
water samples is shown on Figure 1.

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3.0 Water Quality Sample Collection

Samples of groundwater and surface water were collected in accordance with the 2008 NC Solid
Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling Guidance
Document and the approved February 2016 City of Lexington Closed Landfill Water Quality
Monitoring Plan. A brief description of the sample collection procedure is provided below.

3.1 Field Sample Procedures

Prior to groundwater sampling, water levels are obtained from each of the thirteen
monitoring wells using an electric water level meter capable of measuring the depth to
water to the nearest 0.01 feet. This information is later used to determine the elevation of
the water table in each monitoring well relative to surveyed datum (Table 4). The depth
to water in each well is also used to determine the volume of standing water in the well
casing. This information allows for the purging of a minimum of three casing volumes
from each well prior to sampling to assure a fresh groundwater sample is collected. New
disposable laboratory gloves are worn by sampling personnel and each well is purged and
sampled with a new disposable bailer which is discarded after use.

After the monitoring wells have been allowed to recover from purging, samples are
collected in the following order:

 Volatile organic compounds
 Inorganic compounds
 Field Parameters (pH, Conductivity, Temperature)

The samples are collected directly in the laboratory-supplied containers which are pre-
filled with the appropriate preservative. No filtering of the samples is performed prior to
collection. After collection, the samples are placed in a cooler on ice for overnight
shipment to the analytical laboratory.

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Surface water samples are collected directly into the laboratory-supplied containers as
grab samples. Sampling personnel wear new disposable laboratory gloves for each
surface water sample collected. As with the groundwater samples, these samples are
stored in a cooler on ice prior to overnight delivery to the analytical laboratory.

3.2 Field Quality Assurance

One trip blank sample is prepared by the analytical laboratory and accompanies the
sample shipment until receipt back at the laboratory. The trip blank sample is analyzed
for volatile organic compounds. Temperature blanks are also provided with the sample
shipments to assure the proper temperature is maintained until delivery to the analytical
laboratory.

3.3 Sample Delivery/Chain of Custody

All groundwater and surface water samples are stored in coolers on ice immediately after
collection. Individual sample containers for each well or surface water sample are placed
in individual zip lock plastic bags to reduce the potential for cross contamination. Chain-
of-Custody control documents are prepared and shipped with each cooler. Custody seals
are also used for each cooler to maintain sample integrity until delivery to the analytical
laboratory. The sample coolers are shipped via Federal Express for next morning
delivery to the analytical laboratory.

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4.0 Laboratory Analysis

The samples were analyzed for parameters specified by the NC Solid Waste Section for
Detection Monitoring at permitted solid waste facilities. The standard Detection Monitoring
Program for groundwater and surface water samples consists of the Appendix I parameters. The
Appendix I analysis consists of volatile organic compounds by EPA Method 8260B and select
inorganic compounds by EPA Methods 6010C/6020A.

The laboratory performing the water quality analysis is Environmental Conservation
Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory.
Internal quality control samples, including matrix spikes/matrix spike duplicates, are performed
by ENCO for each set of samples. The ENCO laboratory report, including internal quality
control samples, is provided with this report in Appendix A.

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May 2017 Page 9

5.0 Hydrogeological Conditions

The depth to groundwater was measured in all thirteen compliance monitoring wells during the
May 1, 2017 monitoring event. The groundwater elevations were calculated relative to the
surveyed measuring point (top of casing) for each monitoring well. The groundwater elevations
are summarized on Table 4 and the potentiometric surface of the shallow water table is shown on
Figure 1.

The general direction of groundwater flow, based on the water level information collected during
this monitoring event, is also shown on Figure 1. Groundwater flow direction is generally to the
south, toward Abbotts Creek. Based on the observed groundwater elevations at the site, the
hydraulic gradient of the shallow water table from north to south is 0.0142 ft/ft. The vertical
component of groundwater flow was evaluated using the two nested pairs of landfill monitoring
wells. The following vertical groundwater gradients were observed:

MW-7/MW-7D 0.047 ft/ft downward (groundwater recharge zone)
MW-10/MW-10D 0.031 ft/ft downward (groundwater recharge zone)

Based on the results of prior field tests performed at the site, the estimated groundwater flow rate
in the saprolitic soil ranges from 0.0127 ft/day to 2.66 ft/day, with an average value of 0.506
ft/day. The estimated hydraulic conductivity values for the monitoring wells at the site are
provided on Table 6.

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May 2017 Page 10

6.0 Laboratory Analytical Results

Final laboratory analytical results for the samples collected on May 1, 2017 were received from
the analytical laboratory on May 18, 2017. A summary of the analytical results are provided on
Tables 1 and 2 (groundwater), Table 3 (surface water), and Table 4 (field parameters).

6.1 Groundwater Analytical Results

Inorganic compounds were detected at concentrations exceeding the Solid Waste Section
Limits (SWSLs) and/or laboratory detection limits in five of the ten groundwater
monitoring wells sampled during this monitoring event. Only one inorganic compound
was detected at a concentration that exceeded the established NC 2L Groundwater
Standards. The concentration of chromium in monitoring wells MW-6 (22.6 ug/l), MW-
9 (15.9 ug/l), and MW-10 (13.8 ug/l) slightly exceeds the established 2L Groundwater
Standard for chromium of 10.0 ug/l. No other inorganic compounds were reported above
the established 2L Groundwater Standards in any of the ten landfill groundwater
monitoring wells. A summary of the detected inorganic compounds and the respective
2L Groundwater Standards is provided on Table 1.

The groundwater analytical results indicate two volatile organic compounds (VOCs)
present at concentrations exceeding the SWSLs. The chlorinated compound 1,4-
dichlorobenzene was reported in monitoring well MW-7d (1.4 ug/l), and MW-8 (1.1
ug/l). The reported concentrations of 1,4-diclorobenzene in these two monitoring wells
do not exceed the NC 2L Groundwater Standard of 6.0 ug/l. The compound
chlorobenzene was reported in monitoring well MW-8 (14.0 ug/l), which is also below
the NC 2L Groundwater Standard of 50.0 ug/l. No other VOCs were reported above the
laboratory reporting limits or SWSLs in any of the remaining monitoring wells at the site.
A summary of the detected volatile organic compounds and the respective 2L
Groundwater Standards is provided on Table 2 with this report.

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May 2017 Page 11

6.2 Surface Water Analytical Results

Surface water samples were collected from the SW-1 upstream monitoring station and the
SW-4 downstream monitoring station (Figure 1). No VOCs were detected above the
SWSLs or laboratory reporting limits in the upstream or downstream surface water
samples. Several inorganic compounds were reported above the SWSLs or laboratory
reporting limits in the upstream surface water sample. The inorganic compounds barium,
chromium, cobalt, copper, lead, vanadium, and zinc were reported above the laboratory
reporting limit and SWSLs in the upstream SW-1 sample. Three of these inorganic
compounds (cobalt – 17.7 ug/l; copper – 28.4 ug/l; and zinc – 72.9 ug/l) exceed the
established 2B Surface Water Standards in the upstream surface water sample.

No inorganic compounds were reported above the laboratory reporting limits or SWSLs
in the downgradient SW-2 surface water sample. A summary of the laboratory analytical
results and the applicable 2B Surface Water Standards are provided on Table 3.

6.3 Quality Control Sample

One trip blank was submitted and analyzed for quality assurance purposes. No VOCs
were detected at a concentration equaling or exceeding laboratory quantitation limits in
the trip blank.

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7.0 Conclusions

The results of this monitoring event reported only minor variants from the established NC 2L
Groundwater Standards in five of the ten groundwater monitoring wells sampled at the landfill.
Surface water samples collected on Abbotts Creek did not report any detectable concentrations
above the laboratory detection limits or the NC 2B Surface Water Standards in the surface water
sample collected downgradient of the landfill.

Based on the results of this water quality monitoring event the closed City of Lexington Landfill
will remain in Detection Monitoring pursuant to Title 15A NCAC 13B .0601. In accordance
with the approved February 2016 City of Lexington Closed Landfill Water Quality Monitoring
Plan, semi-annual monitoring will not be required in the fall of 2017. As no volatile organic
compounds were reported above the 2L Groundwater Standards during this monitoring event, the
landfill will perform annual water quality monitoring at the site. If future water quality
monitoring events indicate volatile organic compounds are present above the 2L Groundwater
Standards, the site will revert back to semi-annual monitoring. The 2018 spring annual water
quality monitoring event is tentatively scheduled for April/May 2018.

Attachments to this report include tables summarizing the groundwater and surface water
analytical results (Tables 1, 2, and 3), field parameters collected during the monitoring event
(Table 4), well construction information (Table 5), and hydrologic test results (Table 6). A
potentiometric map of the shallow water table is provided as Figure 1 and an isoconcentration
map of the total volatile organic compounds is provided as Figure 2. A copy of the laboratory
analytical report in pdf and EDD formats is also included with this report in Appendix A.

FIGURES

TABLES
TABLE 12017 First Semi-Annual Groundwater Laboratory Analytical ResultsCity of Lexington Closed LandfillLexington, North CarolinaPermit #29-03Inorganic ParametersParameter MW-2 MW-3 MW-6 MW-7 MW-7d MW-8 MW-9 MW-10 MW-10d MW-11 2L Std.Metals (ug/l) Antimony BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NEBarium551 418 13169.2 J 26.1 J 70.4 J145 30521.4 J 84.1 J 700Beryllium 0.139 J BQL BQL BQL BQL BQL 0.491 J BQL BQL BQL NECadmium BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 2Chromium 1.99 J BQL22.7BQL BQL BQL15.9 13.8BQL BQL 10Cobalt11.1 13.8 15.28.61 J BQL 4.50 J14.75.48 J BQL BQL NECopper23.7BQL115.02.07 J BQL BQL23.9 26.12.75 J 1.86 J 1000Lead BQL BQL BQL BQL BQL BQL 3.82 J 5.57 J BQL BQL 15Nickel BQL BQL 20.6 J BQL BQL BQL 9.42 J 6.33 J BQL 4.06 J 100Selenium BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 20Silver BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 20Thallium 0.258 J 0.292 J 0.193 J 0.223 J 0.241 J 0.208 J 0.302 J 0.33 J0.213 J 0.221 J NEVanadium57.49.06 J66.7BQL 2.56 J BQL27.8 30.24.04 J 5.39 J NEZinc50.48.65 J69.05.70 J BQL 6.57 J86.3 26.09.98 J 6.11 J 1000Notes:Samples collected on May 1, 2017BQL - below laboratory quantitation limit.Bold concentrations equal or exceed laboratory quantitation limit.Shaded concentrations equal or exceed established or interim standards.J - Between MDL and RLB - Amount in Prep Blank > MDLNS - Not Sampled
TABLE 22017 First Semi-Annual Groundwater Monitoring Well Laboratory Analytical ResultsCity of Lexington Closed LandfillLexington, North CarolinaPermit #29-03Volatile Organic ParametersParameter MW-2 MW-3 MW-6 MW-7 MW-7d MW-8 MW-9 MW-10 MW-10d MW-11 2L Std.Method 8260B (ug/l) Acetone BQL150.0BQL 14.0 J BQL BQL BQL BQL BQL BQL 6000Benzene BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 1Chlorobenzene BQL BQL BQL BQL 1.2 J14.0BQL BQL BQL BQL 50Chloroethane BQL BQL BQL 2.3 J 1.2 J BQL BQL BQL BQL BQL 30001,4-Dichlorobenzene BQL BQL BQL BQL1.4 1.1BQL BQL BQL BQL 61,1-Dichloroethane BQL BQL BQL 0.87 J 1.4 J BQL BQL BQL BQL BQL 6cis-1,2-Dichloroethene BQL BQL BQL 2.0 J BQL BQL BQL BQL 0.89 J BQL 70Toluene BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 600Notes:Samples collected on May 1, 2017BQL - below laboratory quantitation limit.Bold concentrations equal or exceed laboratory quantitation limit.Shaded concentrations equal or exceed established or interim standards.J - Between MDL and RLB - Amount in Prep Blank > MDLNS - Not Sampled
TABLE 32017 First Semi-Annual Surface Water Laboratory Analytical ResultsCity of Lexington Closed LandfillLexington, North CarolinaPermit #29-03Parameter SW-1 SW-4 2B Std.App. I Metals (ug/l)Barium20341.8 J 1000Beryllium 0.161 J BQL 6.5Chromium14.3BQL 74Cobalt17.7BQL 4Copper28.43.55 J 7Lead16.2BQL 25Nickel 10.5 J BQL 88Thallium 0.223 J 0.148 J 0.24Vanadium45.84.46 J NEZinc72.9BQL 50Method 8260B (ug/l)BQL BQLNotes:Samples collected on May 1, 2017BQL - below laboratory quantitation limit.Bold concentrations equal or exceed laboratory quantitation limit.J - Between MDL and RLB - Amount in Prep Blank > MDLNE - Not EstablishedShaded concentrations equal or exceed established or interim standards.
TABLE 42017 First Semi-Annual Field ParametersCity of Lexington Closed LandfillLexington, North CarolinaPermit #29-03Field ParametersMonitoring WellSample Date Depth to GW GW Elevation Sample Time Conductivity Temperature - C pHMW-2 5/1/2017 27.31 638.11 1215 403 17.7 5.6MW-3 5/1/2017 15.18 639.29 1140 650 17.6 6.2MW-4 * 5/1/2017 40.36 651.62 ND ND ND NDMW-5 * 5/1/2017 35.84 654.65 ND ND ND NDMW-6 5/1/2017 6.11 653.40 1000 326 17.6 6.5MW-7 5/1/2017 39.62 638.18 1045 1302 8.6 5.7MW-7d 5/1/2017 41.01 636.95 1055 677 6.4 6.0MW-8 5/1/2017 25.81 635.51 1120 822 5.9 5.2MW-9 5/1/2017 3.91 634.71 1300 192 6.1 4.9MW-10 5/1/2017 3.75 636.82 1320 73 16.8 6.2MW-10d 5/1/2017 6.73 634.90 1340 423 5.9 6.7MW-11 5/1/2017 10.80 674.91 930 652 19.7 6.5MW-12 * 5/1/2017 Dry ND ND ND ND NDSW-1 5/1/2017 ND ND 1350 332 11.9 6.4SW-4 5/1/2017 ND ND 1405 144 19.3 7.2ND - Not Determined* Water Level Only, No Sample Collected
TABLE 5Groundwater Monitoring Well ConstructionCity of Lexington Closed LandfillLexington, North CaroliinaPermit #29-03Well ID Date DrilledWell DiameterTotal Depth TOS DepthScreened IntervalGround ElevationTOC ElevationLat/Long 1GeologyMW-2 6/23/89 2" 35.0' 25.0' 25' - 35' 662.92 665.42499948.185mE 231604.502mNNAMW-3 6/24/89 2" 25.0' 15.0' 15' - 35' 651.97 654.47500082.542mE 231652.174mNNAMW-4 2/20/95 2" 75.0' 60.0' 60' - 75' 689.38 691.98499603.675mE 231816.763mNsilty CLAYMW-5 2/21/95 2" 43.0' 28.0' 28' - 43' 687.99 690.49499888.474mE 231934.709mNsandy SILTMW-6 8/31/95 2" 11.5' 3.5' 3.5' - 11.5' 657.01 659.51500008.244mE 232000.743mNsandy SILTMW-7 2/23/95 2" 57.0' 37.0' 37' - 57' 675.30 677.80500058.708mE 231878.999mNfelsic/mafic MetavaolcanicsMW-7D 11/19/97 2" 81.0' 76.0' 76' - 81' 675.52 677.96500058.708mE 231878.999mNfelsic/mafic MetavaolcanicsMW-8 2/22/95 2" 47.0' 22.0' 22' - 47' 658.82 661.32500048.916mE 231734.876mNfelsic/mafic MetavaolcanicsMW-9 8/9/95 2" 8.0' 3.0' 3' - 8' 635.42 638.62499794.237mE 231514.847mNclayey SANDMW-10 8/8/95 2" 13.5' 3.5' 3.5' - 13.5' 638.07 640.57499697.167mE 231622.368mNsandy CLAYMW-10D 12/15/97 2" 73.0' 63.0' 63' - 73' 639.39 641.63499697.167mE 231622.368mNfelsic/mafic MetavaolcanicsMW-11 1/14/98 2" 27.0' 17.0' 17' - 27' 683.64 685.71499791.974mE 232006.470mNsilty SANDMW-12 11/18/97 2" 30.0' 15.0' 15' - 30' 665.21 667.83499379.189mE 231746.473mNfelsic/mafic MetavaolcanicsTOS - Top of ScreenTOC - Top of CasingNA - Not AvailableLat/Long approximated from Google Earth1 NC State Plane X Y (Meters)
TABLE 6Groundwater Flow Rates 1City of Lexington Closed LandfillLexington, North CarolinaPermit #29-03Test Piezometer Test Type 2Hydraulic Conductivity (feet/day) Geologic MaterialMW-2 Rising Head 0.438 NAMW-3 Rising Head 0.0494 NAMW-4 Rising Head 0.323 Silty CLAYMW-5 Rising Head 0.0812 sandy SILTMW-6 Rising Head 1.04 sandy SILTMW-7 Rising Head 0.0127 felsic/mafic MetavolcanicsMW-8 Rising Head 0.0565 felsic/mafic MetavolcanicsMW-9 Rising Head 2.66 clayey SANDMW-10 Rising Head 0.327 sandy CLAY1 Data from December 1996 Groundwater and Surface Water Assessment Report2 Aquifer Testing by rising head slug tests, analyzed using Bouwer and Rice methodNA - Not Available
Appendix A Laboratory Report
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CA05953
Raleigh, NC 27606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: City of Lexington Closed Landfill
Attn: Gary Babb
Babb & Associates (BA024)
3605 Country Cove Lane
Bill Scott
Project Manager
Thursday, May 18, 2017
RE: Laboratory Results for
Dear Gary Babb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, May 2, 2017.
The total number of pages in this report, including this page is 57.
Page 1 of 60
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SAMPLE SUMMARY/LABORATORY CHRONICLE
2903-MW2 CA05953-01 Sampled:05/01/17 12:15 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:25
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 12:22
EPA 8260B 05/15/17 05/09/17 00:00 5/9/2017 17:16
2903-MW3 CA05953-02 Sampled:05/01/17 11:40 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:27
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 12:40
EPA 8260B 05/15/17 05/09/17 00:00 5/9/2017 17:45
2903-MW6 CA05953-03 Sampled:05/01/17 10:00 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:29
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 12:44
EPA 8260B 05/15/17 05/09/17 00:00 5/9/2017 18:14
2903-MW7 CA05953-04 Sampled:05/01/17 10:45 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:32
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 12:47
EPA 8260B 05/15/17 05/09/17 00:00 5/9/2017 18:42
2903-MW7d CA05953-05 Sampled:05/01/17 10:55 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:34
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:05
EPA 8260B 05/15/17 05/10/17 00:00 5/10/2017 12:27
2903-MW8 CA05953-06 Sampled:05/01/17 11:20 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:37
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:09
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 06:50
Page 2 of 57
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2903-MW9 CA05953-07 Sampled:05/01/17 13:00 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:08 5/8/2017 16:39
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:13
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 00:58
2903-MW10 CA05953-08 Sampled:05/01/17 13:20 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:12 5/9/2017 14:22
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:16
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 01:27
2903-MW10d CA05953-09 Sampled:05/01/17 13:40 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:12 5/9/2017 14:41
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:20
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 01:57
2903-MW11 CA05953-10 Sampled:05/01/17 09:30 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:12 5/9/2017 14:43
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:24
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 02:26
2903-SW1 CA05953-11 Sampled:05/01/17 13:50 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:12 5/9/2017 14:46
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:27
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 02:55
2903-SW4 CA05953-12 Sampled:05/01/17 14:05 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/28/17 05/05/17 09:12 5/9/2017 14:48
EPA 6020B 10/28/17 05/08/17 14:46 5/17/2017 13:31
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 03:25
2903-Tripblank CA05953-13 Sampled:05/01/17 09:30 Received:05/02/17 10:45Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 05/15/17 05/09/17 00:00 5/10/2017 03:54
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW2 CA05953-01
Flag NotesMDLNC SWSLMRLDF
551 ug/L EPA 6010D 10010.01.001Barium - Total
0.139 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
1.99 ug/L EPA 6010DJ 1010.01.401Chromium - Total
11.1 ug/L EPA 6010D 1010.01.101Cobalt - Total
23.7 ug/L EPA 6010D 1010.01.601Copper - Total
0.258 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
57.4 ug/L EPA 6010D 2510.01.401Vanadium - Total
50.4 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW3 CA05953-02
Flag NotesMDLNC SWSLMRLDF
150 ug/L EPA 8260B O-0110020101Acetone
418 ug/L EPA 6010D 10010.01.001Barium - Total
13.8 ug/L EPA 6010D 1010.01.101Cobalt - Total
0.292 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
9.06 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
8.65 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW6 CA05953-03
Flag NotesMDLNC SWSLMRLDF
131 ug/L EPA 6010D 10010.01.001Barium - Total
22.7 ug/L EPA 6010D 1010.01.401Chromium - Total
15.2 ug/L EPA 6010D 1010.01.101Cobalt - Total
115 ug/L EPA 6010D 1010.01.601Copper - Total
20.6 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.193 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
66.7 ug/L EPA 6010D 2510.01.401Vanadium - Total
69.0 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW7 CA05953-04
Flag NotesMDLNC SWSLMRLDF
0.87 ug/L EPA 8260BJ 51.00.6211,1-Dichloroethane
14 ug/L EPA 8260BJ O-0110020101Acetone
69.2 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.3 ug/L EPA 8260BJ 101.00.981Chloroethane
2.0 ug/L EPA 8260BJ 51.00.531cis-1,2-Dichloroethene
8.61 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
2.07 ug/L EPA 6010DJ 1010.01.601Copper - Total
0.223 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
5.70 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW7d CA05953-05
Flag NotesMDLNC SWSLMRLDF
1.4 ug/L EPA 8260BJ 51.00.6211,1-Dichloroethane
1.4 ug/L EPA 8260B 11.00.7611,4-Dichlorobenzene
26.1 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.2 ug/L EPA 8260BJ 31.00.721Chlorobenzene
1.2 ug/L EPA 8260BJ 101.00.981Chloroethane
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Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW7d CA05953-05
Flag NotesMDLNC SWSLMRLDF
0.241 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
2.56 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW8 CA05953-06
Flag NotesMDLNC SWSLMRLDF
1.1 ug/L EPA 8260B 11.00.7611,4-Dichlorobenzene
70.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
14 ug/L EPA 8260B 31.00.721Chlorobenzene
4.50 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
0.208 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
6.57 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW9 CA05953-07
Flag NotesMDLNC SWSLMRLDF
145 ug/L EPA 6010D 10010.01.001Barium - Total
0.491 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
15.9 ug/L EPA 6010D 1010.01.401Chromium - Total
14.7 ug/L EPA 6010D 1010.01.101Cobalt - Total
23.9 ug/L EPA 6010D 1010.01.601Copper - Total
3.82 ug/L EPA 6010DJ 1010.03.101Lead - Total
9.42 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.302 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
27.8 ug/L EPA 6010D 2510.01.401Vanadium - Total
86.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW10 CA05953-08
Flag NotesMDLNC SWSLMRLDF
305 ug/L EPA 6010D 10010.01.001Barium - Total
13.8 ug/L EPA 6010D 1010.01.401Chromium - Total
5.48 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
26.1 ug/L EPA 6010D 1010.01.601Copper - Total
5.57 ug/L EPA 6010DJ 1010.03.101Lead - Total
6.33 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.330 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
30.2 ug/L EPA 6010D 2510.01.401Vanadium - Total
26.0 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW10d CA05953-09
Flag NotesMDLNC SWSLMRLDF
21.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.89 ug/L EPA 8260BJ 51.00.531cis-1,2-Dichloroethene
2.75 ug/L EPA 6010DJ 1010.01.601Copper - Total
0.213 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
4.04 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
9.98 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW11 CA05953-10
Flag NotesMDLNC SWSLMRLDF
84.1 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.86 ug/L EPA 6010DJ 1010.01.601Copper - Total
4.06 ug/L EPA 6010DJ 5010.02.201Nickel - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:2903-MW11 CA05953-10
Flag NotesMDLNC SWSLMRLDF
0.221 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
5.39 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
6.11 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-SW1 CA05953-11
Flag NotesMDLNC SWSLMRLDF
203 ug/L EPA 6010D 10010.01.001Barium - Total
0.161 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
14.3 ug/L EPA 6010D 1010.01.401Chromium - Total
17.7 ug/L EPA 6010D 1010.01.101Cobalt - Total
28.4 ug/L EPA 6010D 1010.01.601Copper - Total
16.2 ug/L EPA 6010D 1010.03.101Lead - Total
10.5 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.223 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
45.8 ug/L EPA 6010D 2510.01.401Vanadium - Total
72.9 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:2903-SW4 CA05953-12
Flag NotesMDLNC SWSLMRLDF
41.8 ug/L EPA 6010DJ 10010.01.001Barium - Total
3.55 ug/L EPA 6010DJ 1010.01.601Copper - Total
0.148 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
4.46 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
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ANALYTICAL RESULTS
2903-MW2Description:Lab Sample ID:CA05953-01 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 12:15 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 12:22Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:25Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:25Barium [7440-39-3] ^1.00 JMV10.0551 1001
ug/L EPA 6010D 05/08/17 16:25Beryllium [7440-41-7] ^0.130 JMV1.000.139 J 11
ug/L EPA 6010D 05/08/17 16:25Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:25Chromium [7440-47-3] ^1.40 JMV10.01.99 J 101
ug/L EPA 6010D 05/08/17 16:25Cobalt [7440-48-4] ^1.10 JMV10.011.1 101
ug/L EPA 6010D 05/08/17 16:25Copper [7440-50-8] ^1.60 JMV10.023.7 101
ug/L EPA 6010D 05/08/17 16:25Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/08/17 16:25Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 12:22Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:25Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 12:22Thallium [7440-28-0] ^0.110 JDH1.000.258 J 5.51
ug/L EPA 6010D 05/08/17 16:25Vanadium [7440-62-2] ^1.40 JMV10.057.4 251
ug/L EPA 6010D 05/08/17 16:25Zinc [7440-66-6] ^4.40 JMV10.050.4 101
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2903-MW2Description:Lab Sample ID:CA05953-01 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 12:15 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/09/17 17:161,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/09/17 17:161,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 17:161,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/09/17 17:161,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 17:161,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/09/17 17:161,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U 51
ug/L EPA 8260B 05/09/17 17:161,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/09/17 17:161,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/09/17 17:161,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/09/17 17:161,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 17:161,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/09/17 17:161,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 17:161,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 17:162-Butanone [78-93-3] ^4.5 JAJ5.04.5 U 1001
ug/L EPA 8260B 05/09/17 17:162-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/09/17 17:164-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/09/17 17:16Acetone [67-64-1] ^10 JAJ2010U 1001
ug/L EPA 8260B 05/09/17 17:16Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U QL-022001
ug/L EPA 8260B 05/09/17 17:16Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 17:16Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/09/17 17:16Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/09/17 17:16Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/09/17 17:16Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U 101
ug/L EPA 8260B 05/09/17 17:16Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U 1001
ug/L EPA 8260B 05/09/17 17:16Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 17:16Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/09/17 17:16Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U 101
ug/L EPA 8260B 05/09/17 17:16Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/09/17 17:16Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/09/17 17:16cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/09/17 17:16cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/09/17 17:16Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/09/17 17:16Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/09/17 17:16Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/09/17 17:16Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U 101
ug/L EPA 8260B 05/09/17 17:16m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/09/17 17:16Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/09/17 17:16o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/09/17 17:16Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/09/17 17:16Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 17:16Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/09/17 17:16trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 17:16trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/09/17 17:16trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/09/17 17:16Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/09/17 17:16Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 17:16Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U 501
ug/L EPA 8260B 05/09/17 17:16Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 17:16Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW2Description:Lab Sample ID:CA05953-01 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 12:15 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-142100 %JAJEPA 8260B 05/09/17 17:167E090145050.0 1
Dibromofluoromethane 53-14686 %JAJEPA 8260B 05/09/17 17:167E090144350.0 1
Toluene-d8 41-14692 %JAJEPA 8260B 05/09/17 17:167E090144650.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW3Description:Lab Sample ID:CA05953-02 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 11:40 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 12:40Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:27Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:27Barium [7440-39-3] ^1.00 JMV10.0418 1001
ug/L EPA 6010D 05/08/17 16:27Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/08/17 16:27Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:27Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/08/17 16:27Cobalt [7440-48-4] ^1.10 JMV10.013.8 101
ug/L EPA 6010D 05/08/17 16:27Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/08/17 16:27Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/08/17 16:27Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 12:40Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:27Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 12:40Thallium [7440-28-0] ^0.110 JDH1.000.292 J 5.51
ug/L EPA 6010D 05/08/17 16:27Vanadium [7440-62-2] ^1.40 JMV10.09.06 J 251
ug/L EPA 6010D 05/08/17 16:27Zinc [7440-66-6] ^4.40 JMV10.08.65 J 101
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2903-MW3Description:Lab Sample ID:CA05953-02 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 11:40 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/09/17 17:451,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/09/17 17:451,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 17:451,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/09/17 17:451,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 17:451,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/09/17 17:451,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U 51
ug/L EPA 8260B 05/09/17 17:451,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/09/17 17:451,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/09/17 17:451,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/09/17 17:451,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 17:451,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/09/17 17:451,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 17:451,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 17:452-Butanone [78-93-3] ^4.5 JAJ5.04.5 U 1001
ug/L EPA 8260B 05/09/17 17:452-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/09/17 17:454-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/09/17 17:45Acetone [67-64-1] ^10 JAJ20150 O-011001
ug/L EPA 8260B 05/09/17 17:45Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U QL-022001
ug/L EPA 8260B 05/09/17 17:45Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 17:45Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/09/17 17:45Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/09/17 17:45Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/09/17 17:45Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U 101
ug/L EPA 8260B 05/09/17 17:45Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U 1001
ug/L EPA 8260B 05/09/17 17:45Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 17:45Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/09/17 17:45Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U 101
ug/L EPA 8260B 05/09/17 17:45Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/09/17 17:45Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/09/17 17:45cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/09/17 17:45cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/09/17 17:45Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/09/17 17:45Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/09/17 17:45Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/09/17 17:45Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U 101
ug/L EPA 8260B 05/09/17 17:45m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/09/17 17:45Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/09/17 17:45o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/09/17 17:45Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/09/17 17:45Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 17:45Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/09/17 17:45trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 17:45trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/09/17 17:45trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/09/17 17:45Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/09/17 17:45Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 17:45Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U 501
ug/L EPA 8260B 05/09/17 17:45Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 17:45Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW3Description:Lab Sample ID:CA05953-02 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 11:40 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-142101 %JAJEPA 8260B 05/09/17 17:457E090145150.0 1
Dibromofluoromethane 53-14687 %JAJEPA 8260B 05/09/17 17:457E090144450.0 1
Toluene-d8 41-14695 %JAJEPA 8260B 05/09/17 17:457E090144750.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW6Description:Lab Sample ID:CA05953-03 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:00 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 12:44Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:29Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:29Barium [7440-39-3] ^1.00 JMV10.0131 1001
ug/L EPA 6010D 05/08/17 16:29Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/08/17 16:29Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:29Chromium [7440-47-3] ^1.40 JMV10.022.7 101
ug/L EPA 6010D 05/08/17 16:29Cobalt [7440-48-4] ^1.10 JMV10.015.2 101
ug/L EPA 6010D 05/08/17 16:29Copper [7440-50-8] ^1.60 JMV10.0115 101
ug/L EPA 6010D 05/08/17 16:29Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/08/17 16:29Nickel [7440-02-0] ^2.20 JMV10.020.6 J 501
ug/L EPA 6020B 05/17/17 12:44Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:29Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 12:44Thallium [7440-28-0] ^0.110 JDH1.000.193 J 5.51
ug/L EPA 6010D 05/08/17 16:29Vanadium [7440-62-2] ^1.40 JMV10.066.7 251
ug/L EPA 6010D 05/08/17 16:29Zinc [7440-66-6] ^4.40 JMV10.069.0 101
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2903-MW6Description:Lab Sample ID:CA05953-03 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:00 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/09/17 18:141,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/09/17 18:141,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 18:141,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/09/17 18:141,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 18:141,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/09/17 18:141,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U 51
ug/L EPA 8260B 05/09/17 18:141,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/09/17 18:141,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/09/17 18:141,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/09/17 18:141,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 18:141,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/09/17 18:141,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 18:141,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 18:142-Butanone [78-93-3] ^4.5 JAJ5.04.5 U 1001
ug/L EPA 8260B 05/09/17 18:142-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/09/17 18:144-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/09/17 18:14Acetone [67-64-1] ^10 JAJ2010U 1001
ug/L EPA 8260B 05/09/17 18:14Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U QL-022001
ug/L EPA 8260B 05/09/17 18:14Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 18:14Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/09/17 18:14Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/09/17 18:14Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/09/17 18:14Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U 101
ug/L EPA 8260B 05/09/17 18:14Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U 1001
ug/L EPA 8260B 05/09/17 18:14Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 18:14Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/09/17 18:14Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U 101
ug/L EPA 8260B 05/09/17 18:14Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/09/17 18:14Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/09/17 18:14cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/09/17 18:14cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/09/17 18:14Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/09/17 18:14Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/09/17 18:14Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/09/17 18:14Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U 101
ug/L EPA 8260B 05/09/17 18:14m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/09/17 18:14Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/09/17 18:14o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/09/17 18:14Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/09/17 18:14Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 18:14Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/09/17 18:14trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 18:14trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/09/17 18:14trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/09/17 18:14Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/09/17 18:14Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 18:14Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U 501
ug/L EPA 8260B 05/09/17 18:14Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 18:14Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW6Description:Lab Sample ID:CA05953-03 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:00 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-142101 %JAJEPA 8260B 05/09/17 18:147E090145050.0 1
Dibromofluoromethane 53-14686 %JAJEPA 8260B 05/09/17 18:147E090144350.0 1
Toluene-d8 41-14693 %JAJEPA 8260B 05/09/17 18:147E090144650.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW7Description:Lab Sample ID:CA05953-04 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:45 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 12:47Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:32Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:32Barium [7440-39-3] ^1.00 JMV10.069.2 J 1001
ug/L EPA 6010D 05/08/17 16:32Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/08/17 16:32Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:32Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/08/17 16:32Cobalt [7440-48-4] ^1.10 JMV10.08.61 J 101
ug/L EPA 6010D 05/08/17 16:32Copper [7440-50-8] ^1.60 JMV10.02.07 J 101
ug/L EPA 6010D 05/08/17 16:32Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/08/17 16:32Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 12:47Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:32Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 12:47Thallium [7440-28-0] ^0.110 JDH1.000.223 J 5.51
ug/L EPA 6010D 05/08/17 16:32Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/08/17 16:32Zinc [7440-66-6] ^4.40 JMV10.05.70 J 101
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2903-MW7Description:Lab Sample ID:CA05953-04 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:45 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/09/17 18:421,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/09/17 18:421,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 18:421,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/09/17 18:421,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 18:421,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.87 J 51
ug/L EPA 8260B 05/09/17 18:421,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U 51
ug/L EPA 8260B 05/09/17 18:421,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/09/17 18:421,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/09/17 18:421,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/09/17 18:421,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 18:421,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/09/17 18:421,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/09/17 18:421,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 18:422-Butanone [78-93-3] ^4.5 JAJ5.04.5 U 1001
ug/L EPA 8260B 05/09/17 18:422-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/09/17 18:424-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/09/17 18:42Acetone [67-64-1] ^10 JAJ2014J O-011001
ug/L EPA 8260B 05/09/17 18:42Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U QL-022001
ug/L EPA 8260B 05/09/17 18:42Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 18:42Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/09/17 18:42Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/09/17 18:42Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/09/17 18:42Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U 101
ug/L EPA 8260B 05/09/17 18:42Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U 1001
ug/L EPA 8260B 05/09/17 18:42Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 18:42Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/09/17 18:42Chloroethane [75-00-3] ^0.98 JAJ1.02.3 J 101
ug/L EPA 8260B 05/09/17 18:42Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/09/17 18:42Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/09/17 18:42cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.02.0 J 51
ug/L EPA 8260B 05/09/17 18:42cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/09/17 18:42Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/09/17 18:42Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/09/17 18:42Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/09/17 18:42Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U 101
ug/L EPA 8260B 05/09/17 18:42m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/09/17 18:42Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/09/17 18:42o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/09/17 18:42Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/09/17 18:42Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/09/17 18:42Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/09/17 18:42trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/09/17 18:42trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/09/17 18:42trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/09/17 18:42Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/09/17 18:42Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/09/17 18:42Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U 501
ug/L EPA 8260B 05/09/17 18:42Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/09/17 18:42Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW7Description:Lab Sample ID:CA05953-04 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:45 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14299 %JAJEPA 8260B 05/09/17 18:427E090144950.0 1
Dibromofluoromethane 53-14686 %JAJEPA 8260B 05/09/17 18:427E090144350.0 1
Toluene-d8 41-14692 %JAJEPA 8260B 05/09/17 18:427E090144650.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 18 of 57
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2903-MW7dDescription:Lab Sample ID:CA05953-05 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:55 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:05Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:34Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:34Barium [7440-39-3] ^1.00 JMV10.026.1 J 1001
ug/L EPA 6010D 05/08/17 16:34Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/08/17 16:34Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:34Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/08/17 16:34Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/08/17 16:34Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/08/17 16:34Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/08/17 16:34Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 13:05Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:34Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:05Thallium [7440-28-0] ^0.110 JDH1.000.241 J 5.51
ug/L EPA 6010D 05/08/17 16:34Vanadium [7440-62-2] ^1.40 JMV10.02.56 J 251
ug/L EPA 6010D 05/08/17 16:34Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
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2903-MW7dDescription:Lab Sample ID:CA05953-05 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:55 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 12:271,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 12:271,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 12:271,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 12:271,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 12:271,1-Dichloroethane [75-34-3] ^0.62 JAJ1.01.4 J 51
ug/L EPA 8260B 05/10/17 12:271,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U 51
ug/L EPA 8260B 05/10/17 12:271,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 12:271,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 12:271,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 12:271,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 12:271,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 12:271,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 12:271,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.01.4 11
ug/L EPA 8260B 05/10/17 12:272-Butanone [78-93-3] ^4.5 JAJ5.04.5 U 1001
ug/L EPA 8260B 05/10/17 12:272-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 12:274-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 12:27Acetone [67-64-1] ^10 JAJ2010U 1001
ug/L EPA 8260B 05/10/17 12:27Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U QL-02,
QM-19
2001
ug/L EPA 8260B 05/10/17 12:27Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 12:27Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 12:27Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 12:27Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 12:27Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U 101
ug/L EPA 8260B 05/10/17 12:27Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U 1001
ug/L EPA 8260B 05/10/17 12:27Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 12:27Chlorobenzene [108-90-7] ^0.72 JAJ1.01.2 J 31
ug/L EPA 8260B 05/10/17 12:27Chloroethane [75-00-3] ^0.98 JAJ1.01.2 J 101
ug/L EPA 8260B 05/10/17 12:27Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 12:27Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 12:27cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 12:27cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 12:27Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 12:27Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 12:27Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 12:27Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U 101
ug/L EPA 8260B 05/10/17 12:27m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 12:27Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 12:27o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 12:27Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 12:27Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 12:27Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 12:27trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 12:27trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 12:27trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 12:27Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 12:27Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 12:27Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U 501
ug/L EPA 8260B 05/10/17 12:27Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 12:27Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW7dDescription:Lab Sample ID:CA05953-05 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 10:55 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14299 %JAJEPA 8260B 05/10/17 12:277E100114950.0 1
Dibromofluoromethane 53-14688 %JAJEPA 8260B 05/10/17 12:277E100114450.0 1
Toluene-d8 41-14692 %JAJEPA 8260B 05/10/17 12:277E100114650.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW8Description:Lab Sample ID:CA05953-06 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 11:20 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:09Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:37Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:37Barium [7440-39-3] ^1.00 JMV10.070.4 J 1001
ug/L EPA 6010D 05/08/17 16:37Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/08/17 16:37Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:37Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/08/17 16:37Cobalt [7440-48-4] ^1.10 JMV10.04.50 J 101
ug/L EPA 6010D 05/08/17 16:37Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/08/17 16:37Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/08/17 16:37Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 13:09Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:37Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:09Thallium [7440-28-0] ^0.110 JDH1.000.208 J 5.51
ug/L EPA 6010D 05/08/17 16:37Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/08/17 16:37Zinc [7440-66-6] ^4.40 JMV10.06.57 J 101
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2903-MW8Description:Lab Sample ID:CA05953-06 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 11:20 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 06:501,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 06:501,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 06:501,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 06:501,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 06:501,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 06:501,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 06:501,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 06:501,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 06:501,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 06:501,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 06:501,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 06:501,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 06:501,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.01.1 11
ug/L EPA 8260B 05/10/17 06:502-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 06:502-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 06:504-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 06:50Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 06:50Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 06:50Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 06:50Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 06:50Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 06:50Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 06:50Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 06:50Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 06:50Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 06:50Chlorobenzene [108-90-7] ^0.72 JAJ1.014 31
ug/L EPA 8260B 05/10/17 06:50Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 06:50Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 06:50Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 06:50cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 06:50cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 06:50Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 06:50Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 06:50Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 06:50Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 06:50m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 06:50Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 06:50o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 06:50Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 06:50Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 06:50Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 06:50trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 06:50trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 06:50trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 06:50Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 06:50Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 06:50Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 06:50Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 06:50Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW8Description:Lab Sample ID:CA05953-06 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 11:20 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14288 %JAJEPA 8260B 05/10/17 06:507E090264450.0 1
Dibromofluoromethane 53-14693 %JAJEPA 8260B 05/10/17 06:507E090264650.0 1
Toluene-d8 41-14696 %JAJEPA 8260B 05/10/17 06:507E090264850.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 24 of 57
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2903-MW9Description:Lab Sample ID:CA05953-07 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:00 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:13Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/08/17 16:39Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/08/17 16:39Barium [7440-39-3] ^1.00 JMV10.0145 1001
ug/L EPA 6010D 05/08/17 16:39Beryllium [7440-41-7] ^0.130 JMV1.000.491 J 11
ug/L EPA 6010D 05/08/17 16:39Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/08/17 16:39Chromium [7440-47-3] ^1.40 JMV10.015.9 101
ug/L EPA 6010D 05/08/17 16:39Cobalt [7440-48-4] ^1.10 JMV10.014.7 101
ug/L EPA 6010D 05/08/17 16:39Copper [7440-50-8] ^1.60 JMV10.023.9 101
ug/L EPA 6010D 05/08/17 16:39Lead [7439-92-1] ^3.10 JMV10.03.82 J 101
ug/L EPA 6010D 05/08/17 16:39Nickel [7440-02-0] ^2.20 JMV10.09.42 J 501
ug/L EPA 6020B 05/17/17 13:13Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/08/17 16:39Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:13Thallium [7440-28-0] ^0.110 JDH1.000.302 J 5.51
ug/L EPA 6010D 05/08/17 16:39Vanadium [7440-62-2] ^1.40 JMV10.027.8 251
ug/L EPA 6010D 05/08/17 16:39Zinc [7440-66-6] ^4.40 JMV10.086.3 101
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2903-MW9Description:Lab Sample ID:CA05953-07 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:00 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 00:581,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 00:581,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 00:581,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 00:581,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 00:581,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 00:581,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QM-07,
QV-01
51
ug/L EPA 8260B 05/10/17 00:581,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 00:581,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 00:581,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 00:581,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 00:581,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 00:581,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 00:581,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 00:582-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 00:582-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 00:584-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 00:58Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 00:58Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 00:58Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 00:58Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 00:58Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 00:58Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 00:58Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 00:58Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QM-07,
QV-01
1001
ug/L EPA 8260B 05/10/17 00:58Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 00:58Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 00:58Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 00:58Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 00:58Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 00:58cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 00:58cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 00:58Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 00:58Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 00:58Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 00:58Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QM-19,
QV-01
101
ug/L EPA 8260B 05/10/17 00:58m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 00:58Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 00:58o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 00:58Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 00:58Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 00:58Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 00:58trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 00:58trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 00:58trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 00:58Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 00:58Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 00:58Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 00:58Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 00:58Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
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2903-MW9Description:Lab Sample ID:CA05953-07 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:00 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14287 %JAJEPA 8260B 05/10/17 00:587E090264450.0 1
Dibromofluoromethane 53-14694 %JAJEPA 8260B 05/10/17 00:587E090264750.0 1
Toluene-d8 41-14698 %JAJEPA 8260B 05/10/17 00:587E090264950.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW10Description:Lab Sample ID:CA05953-08 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:20 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:16Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/09/17 14:22Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/09/17 14:22Barium [7440-39-3] ^1.00 JMV10.0305 1001
ug/L EPA 6010D 05/09/17 14:22Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/09/17 14:22Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/09/17 14:22Chromium [7440-47-3] ^1.40 JMV10.013.8 101
ug/L EPA 6010D 05/09/17 14:22Cobalt [7440-48-4] ^1.10 JMV10.05.48 J 101
ug/L EPA 6010D 05/09/17 14:22Copper [7440-50-8] ^1.60 JMV10.026.1 101
ug/L EPA 6010D 05/09/17 14:22Lead [7439-92-1] ^3.10 JMV10.05.57 J 101
ug/L EPA 6010D 05/09/17 14:22Nickel [7440-02-0] ^2.20 JMV10.06.33 J 501
ug/L EPA 6020B 05/17/17 13:16Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/09/17 14:22Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:16Thallium [7440-28-0] ^0.110 JDH1.000.330 J 5.51
ug/L EPA 6010D 05/09/17 14:22Vanadium [7440-62-2] ^1.40 JMV10.030.2 251
ug/L EPA 6010D 05/09/17 14:22Zinc [7440-66-6] ^4.40 JMV10.026.0 101
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2903-MW10Description:Lab Sample ID:CA05953-08 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:20 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 01:271,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 01:271,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 01:271,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 01:271,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 01:271,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 01:271,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 01:271,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 01:271,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 01:271,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 01:271,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 01:271,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 01:271,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 01:271,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 01:272-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 01:272-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 01:274-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 01:27Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 01:27Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 01:27Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 01:27Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 01:27Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 01:27Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 01:27Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 01:27Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 01:27Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 01:27Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 01:27Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 01:27Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 01:27Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 01:27cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 01:27cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 01:27Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 01:27Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 01:27Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 01:27Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 01:27m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 01:27Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 01:27o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 01:27Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 01:27Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 01:27Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 01:27trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 01:27trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 01:27trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 01:27Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 01:27Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 01:27Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 01:27Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 01:27Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW10Description:Lab Sample ID:CA05953-08 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:20 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14285 %JAJEPA 8260B 05/10/17 01:277E090264350.0 1
Dibromofluoromethane 53-14697 %JAJEPA 8260B 05/10/17 01:277E090264950.0 1
Toluene-d8 41-14694 %JAJEPA 8260B 05/10/17 01:277E090264750.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW10dDescription:Lab Sample ID:CA05953-09 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:40 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:20Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/09/17 14:41Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/09/17 14:41Barium [7440-39-3] ^1.00 JMV10.021.4 J 1001
ug/L EPA 6010D 05/09/17 14:41Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/09/17 14:41Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/09/17 14:41Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/09/17 14:41Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/09/17 14:41Copper [7440-50-8] ^1.60 JMV10.02.75 J 101
ug/L EPA 6010D 05/09/17 14:41Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/09/17 14:41Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 13:20Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/09/17 14:41Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:20Thallium [7440-28-0] ^0.110 JDH1.000.213 J 5.51
ug/L EPA 6010D 05/09/17 14:41Vanadium [7440-62-2] ^1.40 JMV10.04.04 J 251
ug/L EPA 6010D 05/09/17 14:41Zinc [7440-66-6] ^4.40 JMV10.09.98 J 101
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2903-MW10dDescription:Lab Sample ID:CA05953-09 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:40 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 01:571,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 01:571,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 01:571,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 01:571,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 01:571,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 01:571,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 01:571,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 01:571,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 01:571,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 01:571,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 01:571,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 01:571,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 01:571,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 01:572-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 01:572-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 01:574-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 01:57Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 01:57Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 01:57Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 01:57Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 01:57Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 01:57Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 01:57Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 01:57Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 01:57Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 01:57Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 01:57Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 01:57Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 01:57Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 01:57cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.89 J 51
ug/L EPA 8260B 05/10/17 01:57cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 01:57Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 01:57Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 01:57Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 01:57Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 01:57m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 01:57Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 01:57o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 01:57Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 01:57Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 01:57Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 01:57trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 01:57trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 01:57trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 01:57Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 01:57Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 01:57Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 01:57Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 01:57Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW10dDescription:Lab Sample ID:CA05953-09 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:40 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14289 %JAJEPA 8260B 05/10/17 01:577E090264550.0 1
Dibromofluoromethane 53-146105 %JAJEPA 8260B 05/10/17 01:577E090265250.0 1
Toluene-d8 41-14695 %JAJEPA 8260B 05/10/17 01:577E090264850.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-MW11Description:Lab Sample ID:CA05953-10 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 09:30 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:24Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/09/17 14:43Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/09/17 14:43Barium [7440-39-3] ^1.00 JMV10.084.1 J 1001
ug/L EPA 6010D 05/09/17 14:43Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/09/17 14:43Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/09/17 14:43Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/09/17 14:43Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/09/17 14:43Copper [7440-50-8] ^1.60 JMV10.01.86 J 101
ug/L EPA 6010D 05/09/17 14:43Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/09/17 14:43Nickel [7440-02-0] ^2.20 JMV10.04.06 J 501
ug/L EPA 6020B 05/17/17 13:24Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/09/17 14:43Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:24Thallium [7440-28-0] ^0.110 JDH1.000.221 J 5.51
ug/L EPA 6010D 05/09/17 14:43Vanadium [7440-62-2] ^1.40 JMV10.05.39 J 251
ug/L EPA 6010D 05/09/17 14:43Zinc [7440-66-6] ^4.40 JMV10.06.11 J 101
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2903-MW11Description:Lab Sample ID:CA05953-10 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 09:30 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 02:261,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 02:261,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 02:261,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 02:261,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 02:261,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 02:261,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 02:261,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 02:261,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 02:261,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 02:261,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 02:261,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 02:261,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 02:261,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 02:262-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 02:262-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 02:264-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 02:26Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 02:26Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 02:26Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 02:26Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 02:26Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 02:26Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 02:26Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 02:26Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 02:26Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 02:26Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 02:26Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 02:26Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 02:26Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 02:26cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 02:26cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 02:26Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 02:26Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 02:26Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 02:26Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 02:26m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 02:26Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 02:26o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 02:26Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 02:26Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 02:26Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 02:26trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 02:26trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 02:26trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 02:26Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 02:26Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 02:26Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 02:26Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 02:26Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-MW11Description:Lab Sample ID:CA05953-10 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 09:30 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14285 %JAJEPA 8260B 05/10/17 02:267E090264250.0 1
Dibromofluoromethane 53-14699 %JAJEPA 8260B 05/10/17 02:267E090264950.0 1
Toluene-d8 41-146102 %JAJEPA 8260B 05/10/17 02:267E090265150.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-SW1Description:Lab Sample ID:CA05953-11 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:50 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:27Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/09/17 14:46Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/09/17 14:46Barium [7440-39-3] ^1.00 JMV10.0203 1001
ug/L EPA 6010D 05/09/17 14:46Beryllium [7440-41-7] ^0.130 JMV1.000.161 J 11
ug/L EPA 6010D 05/09/17 14:46Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/09/17 14:46Chromium [7440-47-3] ^1.40 JMV10.014.3 101
ug/L EPA 6010D 05/09/17 14:46Cobalt [7440-48-4] ^1.10 JMV10.017.7 101
ug/L EPA 6010D 05/09/17 14:46Copper [7440-50-8] ^1.60 JMV10.028.4 101
ug/L EPA 6010D 05/09/17 14:46Lead [7439-92-1] ^3.10 JMV10.016.2 101
ug/L EPA 6010D 05/09/17 14:46Nickel [7440-02-0] ^2.20 JMV10.010.5 J 501
ug/L EPA 6020B 05/17/17 13:27Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/09/17 14:46Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:27Thallium [7440-28-0] ^0.110 JDH1.000.223 J 5.51
ug/L EPA 6010D 05/09/17 14:46Vanadium [7440-62-2] ^1.40 JMV10.045.8 251
ug/L EPA 6010D 05/09/17 14:46Zinc [7440-66-6] ^4.40 JMV10.072.9 101
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2903-SW1Description:Lab Sample ID:CA05953-11 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:50 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 02:551,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 02:551,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 02:551,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 02:551,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 02:551,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 02:551,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 02:551,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 02:551,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 02:551,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 02:551,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 02:551,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 02:551,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 02:551,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 02:552-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 02:552-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 02:554-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 02:55Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 02:55Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 02:55Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 02:55Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 02:55Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 02:55Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 02:55Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 02:55Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 02:55Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 02:55Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 02:55Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 02:55Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 02:55Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 02:55cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 02:55cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 02:55Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 02:55Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 02:55Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 02:55Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 02:55m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 02:55Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 02:55o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 02:55Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 02:55Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 02:55Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 02:55trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 02:55trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 02:55trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 02:55Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 02:55Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 02:55Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 02:55Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 02:55Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-SW1Description:Lab Sample ID:CA05953-11 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 13:50 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14280 %JAJEPA 8260B 05/10/17 02:557E090264050.0 1
Dibromofluoromethane 53-14697 %JAJEPA 8260B 05/10/17 02:557E090264850.0 1
Toluene-d8 41-14696 %JAJEPA 8260B 05/10/17 02:557E090264850.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-SW4Description:Lab Sample ID:CA05953-12 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 14:05 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/17/17 13:31Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/09/17 14:48Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/09/17 14:48Barium [7440-39-3] ^1.00 JMV10.041.8 J 1001
ug/L EPA 6010D 05/09/17 14:48Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/09/17 14:48Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/09/17 14:48Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/09/17 14:48Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/09/17 14:48Copper [7440-50-8] ^1.60 JMV10.03.55 J 101
ug/L EPA 6010D 05/09/17 14:48Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/09/17 14:48Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/17/17 13:31Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/09/17 14:48Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/17/17 13:31Thallium [7440-28-0] ^0.110 JDH1.000.148 J 5.51
ug/L EPA 6010D 05/09/17 14:48Vanadium [7440-62-2] ^1.40 JMV10.04.46 J 251
ug/L EPA 6010D 05/09/17 14:48Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
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2903-SW4Description:Lab Sample ID:CA05953-12 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 14:05 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 03:251,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 03:251,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 03:251,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 03:251,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 03:251,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 03:251,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 03:251,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 03:251,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 03:251,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 03:251,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 03:251,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 03:251,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 03:251,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 03:252-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 03:252-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 03:254-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 03:25Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 03:25Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 03:25Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 03:25Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 03:25Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 03:25Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 03:25Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 03:25Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 03:25Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 03:25Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 03:25Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 03:25Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 03:25Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 03:25cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 03:25cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 03:25Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 03:25Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 03:25Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 03:25Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 03:25m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 03:25Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 03:25o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 03:25Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 03:25Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 03:25Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 03:25trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 03:25trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 03:25trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 03:25Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 03:25Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 03:25Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 03:25Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 03:25Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-SW4Description:Lab Sample ID:CA05953-12 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 14:05 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14280 %JAJEPA 8260B 05/10/17 03:257E090264050.0 1
Dibromofluoromethane 53-14690 %JAJEPA 8260B 05/10/17 03:257E090264550.0 1
Toluene-d8 41-14693 %JAJEPA 8260B 05/10/17 03:257E090264650.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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2903-TripblankDescription:Lab Sample ID:CA05953-13 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 09:30 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/10/17 03:541,1,1,2-Tetrachloroethane [630-20-6] ^0.61 JAJ1.00.61 U 51
ug/L EPA 8260B 05/10/17 03:541,1,1-Trichloroethane [71-55-6] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 03:541,1,2,2-Tetrachloroethane [79-34-5] ^0.54 JAJ1.00.54 U 31
ug/L EPA 8260B 05/10/17 03:541,1,2-Trichloroethane [79-00-5] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 03:541,1-Dichloroethane [75-34-3] ^0.62 JAJ1.00.62 U 51
ug/L EPA 8260B 05/10/17 03:541,1-Dichloroethene [75-35-4] ^0.94 JAJ1.00.94 U QV-0151
ug/L EPA 8260B 05/10/17 03:541,2,3-Trichloropropane [96-18-4] ^0.64 JAJ1.00.64 U 11
ug/L EPA 8260B 05/10/17 03:541,2-Dibromo-3-chloropropane [96-12-8] ^0.96 JAJ1.00.96 U 131
ug/L EPA 8260B 05/10/17 03:541,2-Dibromoethane [106-93-4] ^0.78 JAJ1.00.78 U 11
ug/L EPA 8260B 05/10/17 03:541,2-Dichlorobenzene [95-50-1] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 03:541,2-Dichloroethane [107-06-2] ^0.63 JAJ1.00.63 U 11
ug/L EPA 8260B 05/10/17 03:541,2-Dichloropropane [78-87-5] ^0.80 JAJ1.00.80 U 11
ug/L EPA 8260B 05/10/17 03:541,4-Dichlorobenzene [106-46-7] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 03:542-Butanone [78-93-3] ^4.5 JAJ5.04.5 U QV-011001
ug/L EPA 8260B 05/10/17 03:542-Hexanone [591-78-6] ^1.4 JAJ5.01.4 U 501
ug/L EPA 8260B 05/10/17 03:544-Methyl-2-pentanone [108-10-1] ^0.79 JAJ5.00.79 U 1001
ug/L EPA 8260B 05/10/17 03:54Acetone [67-64-1] ^10 JAJ2010U QV-011001
ug/L EPA 8260B 05/10/17 03:54Acrylonitrile [107-13-1] ^3.2 JAJ103.2 U 2001
ug/L EPA 8260B 05/10/17 03:54Benzene [71-43-2] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 03:54Bromochloromethane [74-97-5] ^0.94 JAJ1.00.94 U 31
ug/L EPA 8260B 05/10/17 03:54Bromodichloromethane [75-27-4] ^0.52 JAJ1.00.52 U 11
ug/L EPA 8260B 05/10/17 03:54Bromoform [75-25-2] ^0.75 JAJ1.00.75 U 31
ug/L EPA 8260B 05/10/17 03:54Bromomethane [74-83-9] ^0.95 JAJ1.00.95 U QV-01101
ug/L EPA 8260B 05/10/17 03:54Carbon disulfide [75-15-0] ^2.6 JAJ5.02.6 U QV-011001
ug/L EPA 8260B 05/10/17 03:54Carbon tetrachloride [56-23-5] ^0.94 JAJ1.00.94 U 11
ug/L EPA 8260B 05/10/17 03:54Chlorobenzene [108-90-7] ^0.72 JAJ1.00.72 U 31
ug/L EPA 8260B 05/10/17 03:54Chloroethane [75-00-3] ^0.98 JAJ1.00.98 U QV-01101
ug/L EPA 8260B 05/10/17 03:54Chloroform [67-66-3] ^0.80 JAJ1.00.80 U 51
ug/L EPA 8260B 05/10/17 03:54Chloromethane [74-87-3] ^0.82 JAJ1.00.82 U 11
ug/L EPA 8260B 05/10/17 03:54cis-1,2-Dichloroethene [156-59-2] ^0.53 JAJ1.00.53 U 51
ug/L EPA 8260B 05/10/17 03:54cis-1,3-Dichloropropene [10061-01-5] ^0.59 JAJ1.00.59 U 11
ug/L EPA 8260B 05/10/17 03:54Dibromochloromethane [124-48-1] ^0.44 JAJ1.00.44 U 31
ug/L EPA 8260B 05/10/17 03:54Dibromomethane [74-95-3] ^0.84 JAJ1.00.84 U 101
ug/L EPA 8260B 05/10/17 03:54Ethylbenzene [100-41-4] ^0.69 JAJ1.00.69 U 11
ug/L EPA 8260B 05/10/17 03:54Iodomethane [74-88-4] ^0.72 JAJ5.00.72 U QL-02,
QV-01
101
ug/L EPA 8260B 05/10/17 03:54m,p-Xylenes [108-38-3/106-42-3] ^1.3 JAJ2.01.3 U NE1
ug/L EPA 8260B 05/10/17 03:54Methylene chloride [75-09-2] ^2.0 JAJ5.02.0 U 11
ug/L EPA 8260B 05/10/17 03:54o-Xylene [95-47-6] ^0.53 JAJ1.00.53 U NE1
ug/L EPA 8260B 05/10/17 03:54Styrene [100-42-5] ^0.61 JAJ1.00.61 U 11
ug/L EPA 8260B 05/10/17 03:54Tetrachloroethene [127-18-4] ^0.76 JAJ1.00.76 U 11
ug/L EPA 8260B 05/10/17 03:54Toluene [108-88-3] ^0.72 JAJ1.00.72 U 11
ug/L EPA 8260B 05/10/17 03:54trans-1,2-Dichloroethene [156-60-5] ^0.73 JAJ1.00.73 U 51
ug/L EPA 8260B 05/10/17 03:54trans-1,3-Dichloropropene [10061-02-6] ^0.73 JAJ1.00.73 U 11
ug/L EPA 8260B 05/10/17 03:54trans-1,4-Dichloro-2-butene [110-57-6] ^0.79 JAJ1.00.79 U 1001
ug/L EPA 8260B 05/10/17 03:54Trichloroethene [79-01-6] ^0.89 JAJ1.00.89 U 11
ug/L EPA 8260B 05/10/17 03:54Trichlorofluoromethane [75-69-4] ^0.94 JAJ1.00.94 U QV-0111
ug/L EPA 8260B 05/10/17 03:54Vinyl acetate [108-05-4] ^0.60 JAJ5.00.60 U QV-01501
ug/L EPA 8260B 05/10/17 03:54Vinyl chloride [75-01-4] ^0.71 JAJ1.00.71 U 11
ug/L EPA 8260B 05/10/17 03:54Xylenes (Total) [1330-20-7] ^1.3 JAJ2.01.3 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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2903-TripblankDescription:Lab Sample ID:CA05953-13 05/02/17 10:45Received:
Matrix:Water Sampled:05/01/17 09:30 Work Order:CA05953
City of Lexington Closed LandfillProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 41-14280 %JAJEPA 8260B 05/10/17 03:547E090264050.0 1
Dibromofluoromethane 53-14695 %JAJEPA 8260B 05/10/17 03:547E090264850.0 1
Toluene-d8 41-14696 %JAJEPA 8260B 05/10/17 03:547E090264850.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E05014 - EPA 3005A
Prepared: 05/05/2017 09:08 Analyzed: 05/08/2017 12:59Blank (7E05014-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 05/05/2017 09:08 Analyzed: 05/08/2017 15:26LCS (7E05014-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12091181 Arsenic
ug/L10.0 200 80-12099197 Barium
ug/L1.00 20.0 80-1209819.6 Beryllium
ug/L1.00 20.0 80-1209719.5 Cadmium
ug/L10.0 200 80-12097193 Chromium
ug/L10.0 200 80-12097193 Cobalt
ug/L10.0 200 80-12095189 Copper
ug/L10.0 200 80-12098195 Lead
ug/L10.0 200 80-12099198 Nickel
ug/L10.0 200 80-12095190 Silver
ug/L10.0 200 80-12094187 Vanadium
ug/L10.0 200 80-120101201 Zinc
Prepared: 05/05/2017 09:08 Analyzed: 05/08/2017 15:31Matrix Spike (7E05014-MS1)
Source: CA05744-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-125856.80 U169 Arsenic
ug/L10.0 200 75-1259127.2209 Barium
ug/L1.00 20.0 75-125930.130 U18.5 Beryllium
ug/L1.00 20.0 75-125910.360 U18.3 Cadmium
ug/L10.0 200 75-125901.40 U180 Chromium
ug/L10.0 200 75-125911.10 U181 Cobalt
ug/L10.0 200 75-125884.98182 Copper
ug/L10.0 200 75-125903.10 U179 Lead
ug/L10.0 200 75-125922.20 U184 Nickel
ug/L10.0 200 75-125891.90 U177 Silver
ug/L10.0 200 75-125891.40 U178 Vanadium
ug/L10.0 200 75-1259112.3194 Zinc
Prepared: 05/05/2017 09:08 Analyzed: 05/08/2017 15:33Matrix Spike Dup (7E05014-MSD1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E05014 - EPA 3005A
Prepared: 05/05/2017 09:08 Analyzed: 05/08/2017 15:33Matrix Spike Dup (7E05014-MSD1) Continued
Source: CA05744-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-12587 36.80 U174 Arsenic
ug/L10.0 200 2075-12591 0.627.2210 Barium
ug/L1.00 20.0 2075-12594 20.130 U18.9 Beryllium
ug/L1.00 20.0 2075-12592 10.360 U18.5 Cadmium
ug/L10.0 200 2075-12591 11.40 U182 Chromium
ug/L10.0 200 2075-12592 11.10 U183 Cobalt
ug/L10.0 200 2075-12589 0.74.98183 Copper
ug/L10.0 200 2075-12591 13.10 U182 Lead
ug/L10.0 200 2075-12592 0.32.20 U185 Nickel
ug/L10.0 200 2075-12589 0.81.90 U179 Silver
ug/L10.0 200 2075-12590 11.40 U181 Vanadium
ug/L10.0 200 2075-12591 0.712.3195 Zinc
Prepared: 05/05/2017 09:08 Analyzed: 05/08/2017 15:36Post Spike (7E05014-PS1)
Source: CA05744-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-12096-0.003850.192 Arsenic
mg/L0.0100 0.200 80-1201030.02720.232 Barium
mg/L0.00100 0.0200 80-120105-3.32E-50.0210 Beryllium
mg/L0.00100 0.0200 80-1201040.0001070.0209 Cadmium
mg/L0.0100 0.200 80-1201020.0004900.205 Chromium
mg/L0.0100 0.200 80-1201030.0007350.206 Cobalt
mg/L0.0100 0.200 80-1201000.004980.206 Copper
mg/L0.0100 0.200 80-120102-0.0003470.204 Lead
mg/L0.0100 0.200 80-1201040.0002650.209 Nickel
mg/L0.0100 0.200 80-120970.0009870.196 Silver
mg/L0.0100 0.200 80-1201010.0008150.202 Vanadium
mg/L0.0100 0.200 80-1201030.01230.219 Zinc
Batch 7E05015 - EPA 3005A
Prepared: 05/05/2017 09:12 Analyzed: 05/09/2017 14:05Blank (7E05015-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.02.25 J Copper
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E05015 - EPA 3005A
Prepared: 05/05/2017 09:12 Analyzed: 05/09/2017 14:19LCS (7E05015-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12089178 Arsenic
ug/L10.0 200 80-12091183 Barium
ug/L1.00 20.0 80-1209218.3 Beryllium
ug/L1.00 20.0 80-1209519.0 Cadmium
ug/L10.0 200 80-12090181 Chromium
ug/L10.0 200 80-12093187 Cobalt
ug/L10.0 200 80-12090179 Copper
ug/L10.0 200 80-12093186 Lead
ug/L10.0 200 80-12093186 Nickel
ug/L10.0 200 80-12091181 Silver
ug/L10.0 200 80-12089177 Vanadium
ug/L10.0 200 80-12096193 Zinc
Prepared: 05/05/2017 09:12 Analyzed: 05/09/2017 14:24Matrix Spike (7E05015-MS1)
Source: CA05953-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-125956.80 U190 Arsenic
ug/L10.0 200 75-12591305487 Barium
ug/L1.00 20.0 75-125980.130 U19.5 Beryllium
ug/L1.00 20.0 75-125990.360 U19.8 Cadmium
ug/L10.0 200 75-1259313.8199 Chromium
ug/L10.0 200 75-125975.48200 Cobalt
ug/L10.0 200 75-1259326.1212 Copper
ug/L10.0 200 75-125975.57199 Lead
ug/L10.0 200 75-125956.33197 Nickel
ug/L10.0 200 75-125931.90 U186 Silver
ug/L10.0 200 75-1259130.2213 Vanadium
ug/L10.0 200 75-1259526.0216 Zinc
Prepared: 05/05/2017 09:12 Analyzed: 05/09/2017 14:26Matrix Spike Dup (7E05015-MSD1)
Source: CA05953-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-12590 56.80 U180 Arsenic
ug/L10.0 200 2075-12589 1305482 Barium
ug/L1.00 20.0 2075-12594 40.130 U18.9 Beryllium
ug/L1.00 20.0 2075-12594 50.360 U18.8 Cadmium
ug/L10.0 200 2075-12591 213.8196 Chromium
ug/L10.0 200 2075-12593 45.48192 Cobalt
ug/L10.0 200 2075-12591 226.1208 Copper
ug/L10.0 200 2075-12592 55.57190 Lead
ug/L10.0 200 2075-12593 26.33193 Nickel
ug/L10.0 200 2075-12590 31.90 U181 Silver
ug/L10.0 200 2075-12590 130.2210 Vanadium
ug/L10.0 200 2075-12593 226.0212 Zinc
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E05015 - EPA 3005A
Prepared: 05/05/2017 09:12 Analyzed: 05/09/2017 14:29Post Spike (7E05015-PS1)
Source: CA05953-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120103-0.01100.206 Arsenic
mg/L0.0100 0.200 80-1201000.3050.504 Barium
mg/L0.00100 0.0200 80-1201050.0001030.0211 Beryllium
mg/L0.00100 0.0200 80-1201072.80E-60.0213 Cadmium
mg/L0.0100 0.200 80-1201010.01380.216 Chromium
mg/L0.0100 0.200 80-1201050.005480.215 Cobalt
mg/L0.0100 0.200 80-1201010.02610.229 Copper
mg/L0.0100 0.200 80-1201050.005570.216 Lead
mg/L0.0100 0.200 80-1201030.006330.211 Nickel
mg/L0.0100 0.200 80-120970.0005100.195 Silver
mg/L0.0100 0.200 80-1201010.03020.232 Vanadium
mg/L0.0100 0.200 80-1201030.02600.233 Zinc
Batch 7E08027 - EPA 3005A
Prepared: 05/08/2017 14:46 Analyzed: 05/17/2017 12:15Blank (7E08027-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 05/08/2017 14:46 Analyzed: 05/17/2017 12:18LCS (7E08027-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120100200 Antimony
ug/L3.00 200 80-120105209 Selenium
ug/L1.00 200 80-120102205 Thallium
Prepared: 05/08/2017 14:46 Analyzed: 05/17/2017 12:25Matrix Spike (7E08027-MS1)
Source: CA05953-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-125670.370 U134 QM-07Antimony
ug/L3.00 200 75-125800.910 U161 Selenium
ug/L1.00 200 75-125880.258177 Thallium
Prepared: 05/08/2017 14:46 Analyzed: 05/17/2017 12:29Matrix Spike Dup (7E08027-MSD1)
Source: CA05953-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-12567 0.80.370 U135 QM-07Antimony
ug/L3.00 200 2075-12579 20.910 U157 Selenium
ug/L1.00 200 2075-12587 20.258174 Thallium
Prepared: 05/08/2017 14:46 Analyzed: 05/17/2017 12:33Post Spike (7E08027-PS1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E08027 - EPA 3005A
Prepared: 05/08/2017 14:46 Analyzed: 05/17/2017 12:33Post Spike (7E08027-PS1) Continued
Source: CA05953-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201000.291201 Antimony
ug/L3.00 200 80-120970.254195 Selenium
ug/L1.00 200 75-125870.258174 Thallium
QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E09014 - EPA 5030B_MS
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 11:53Blank (7E09014-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.61 U 1,1,1,2-Tetrachloroethane
ug/L1.00.80 U 1,1,1-Trichloroethane
ug/L1.00.54 U 1,1,2,2-Tetrachloroethane
ug/L1.00.76 U 1,1,2-Trichloroethane
ug/L1.00.62 U 1,1-Dichloroethane
ug/L1.00.94 U 1,1-Dichloroethene
ug/L1.00.64 U 1,2,3-Trichloropropane
ug/L1.00.96 U 1,2-Dibromo-3-chloropropane
ug/L1.00.78 U 1,2-Dibromoethane
ug/L1.00.73 U 1,2-Dichlorobenzene
ug/L1.00.63 U 1,2-Dichloroethane
ug/L1.00.80 U 1,2-Dichloropropane
ug/L1.00.76 U 1,4-Dichlorobenzene
ug/L5.04.5 U 2-Butanone
ug/L5.01.4 U 2-Hexanone
ug/L5.00.79 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.2 U Acrylonitrile
ug/L1.00.71 U Benzene
ug/L1.00.94 U Bromochloromethane
ug/L1.00.52 U Bromodichloromethane
ug/L1.00.75 U Bromoform
ug/L1.00.95 U Bromomethane
ug/L5.02.6 U Carbon disulfide
ug/L1.00.94 U Carbon tetrachloride
ug/L1.00.72 U Chlorobenzene
ug/L1.00.98 U Chloroethane
ug/L1.00.80 U Chloroform
ug/L1.00.82 U Chloromethane
ug/L1.00.53 U cis-1,2-Dichloroethene
ug/L1.00.59 U cis-1,3-Dichloropropene
ug/L1.00.44 U Dibromochloromethane
ug/L1.00.84 U Dibromomethane
ug/L1.00.69 U Ethylbenzene
ug/L5.00.72 U Iodomethane
ug/L2.01.3 U m,p-Xylenes
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E09014 - EPA 5030B_MS
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 11:53Blank (7E09014-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5.02.0 U Methylene chloride
ug/L1.00.53 U o-Xylene
ug/L1.00.61 U Styrene
ug/L1.00.76 U Tetrachloroethene
ug/L1.00.72 U Toluene
ug/L1.00.73 U trans-1,2-Dichloroethene
ug/L1.00.73 U trans-1,3-Dichloropropene
ug/L1.00.79 U trans-1,4-Dichloro-2-butene
ug/L1.00.89 U Trichloroethene
ug/L1.00.94 U Trichlorofluoromethane
ug/L5.00.60 U Vinyl acetate
ug/L1.00.71 U Vinyl chloride
ug/L2.01.3 U Xylenes (Total)
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9849
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8643
ug/L 50.0 41-146Surrogate: Toluene-d8 9447
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 09:30LCS (7E09014-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 47-1398417 1,1-Dichloroethene
ug/L1.0 20.0 56-1369118 Benzene
ug/L1.0 20.0 51-13910020 Chlorobenzene
ug/L1.0 20.0 64-1319719 Toluene
ug/L1.0 20.0 62-1358918 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9849
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8744
ug/L 50.0 41-146Surrogate: Toluene-d8 9146
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 09:58Matrix Spike (7E09014-MS1)
Source: AA03147-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 47-139990.94 U20 1,1-Dichloroethene
ug/L1.0 20.0 56-1361030.71 U21 Benzene
ug/L1.0 20.0 51-1391100.72 U22 Chlorobenzene
ug/L1.0 20.0 64-1311050.72 U21 Toluene
ug/L1.0 20.0 62-135990.89 U20 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9849
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8542
ug/L 50.0 41-146Surrogate: Toluene-d8 9347
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 10:27Matrix Spike Dup (7E09014-MSD1)
Source: AA03147-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E09014 - EPA 5030B_MS
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 10:27Matrix Spike Dup (7E09014-MSD1) Continued
Source: AA03147-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 1647-13993 60.94 U19 1,1-Dichloroethene
ug/L1.0 20.0 1456-136100 30.71 U20 Benzene
ug/L1.0 20.0 1351-139108 20.72 U22 Chlorobenzene
ug/L1.0 20.0 1664-131104 0.20.72 U21 Toluene
ug/L1.0 20.0 2062-13595 30.89 U19 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9949
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8542
ug/L 50.0 41-146Surrogate: Toluene-d8 9447
Batch 7E09026 - EPA 5030B_MS
Prepared: 05/09/2017 00:00 Analyzed: 05/10/2017 00:28Blank (7E09026-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.61 U 1,1,1,2-Tetrachloroethane
ug/L1.00.80 U 1,1,1-Trichloroethane
ug/L1.00.54 U 1,1,2,2-Tetrachloroethane
ug/L1.00.76 U 1,1,2-Trichloroethane
ug/L1.00.62 U 1,1-Dichloroethane
ug/L1.00.94 U 1,1-Dichloroethene
ug/L1.00.64 U 1,2,3-Trichloropropane
ug/L1.00.96 U 1,2-Dibromo-3-chloropropane
ug/L1.00.78 U 1,2-Dibromoethane
ug/L1.00.73 U 1,2-Dichlorobenzene
ug/L1.00.63 U 1,2-Dichloroethane
ug/L1.00.80 U 1,2-Dichloropropane
ug/L1.00.76 U 1,4-Dichlorobenzene
ug/L5.04.5 U 2-Butanone
ug/L5.01.4 U 2-Hexanone
ug/L5.00.79 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.2 U Acrylonitrile
ug/L1.00.71 U Benzene
ug/L1.00.94 U Bromochloromethane
ug/L1.00.52 U Bromodichloromethane
ug/L1.00.75 U Bromoform
ug/L1.00.95 U Bromomethane
ug/L5.02.6 U Carbon disulfide
ug/L1.00.94 U Carbon tetrachloride
ug/L1.00.72 U Chlorobenzene
ug/L1.00.98 U Chloroethane
ug/L1.00.80 U Chloroform
ug/L1.00.82 U Chloromethane
ug/L1.00.53 U cis-1,2-Dichloroethene
ug/L1.00.59 U cis-1,3-Dichloropropene
ug/L1.00.44 U Dibromochloromethane
ug/L1.00.84 U Dibromomethane
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E09026 - EPA 5030B_MS
Prepared: 05/09/2017 00:00 Analyzed: 05/10/2017 00:28Blank (7E09026-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.69 U Ethylbenzene
ug/L5.00.72 U Iodomethane
ug/L2.01.3 U m,p-Xylenes
ug/L5.02.0 U Methylene chloride
ug/L1.00.53 U o-Xylene
ug/L1.00.61 U Styrene
ug/L1.00.76 U Tetrachloroethene
ug/L1.00.72 U Toluene
ug/L1.00.73 U trans-1,2-Dichloroethene
ug/L1.00.73 U trans-1,3-Dichloropropene
ug/L1.00.79 U trans-1,4-Dichloro-2-butene
ug/L1.00.89 U Trichloroethene
ug/L1.00.94 U Trichlorofluoromethane
ug/L5.00.60 U Vinyl acetate
ug/L1.00.71 U Vinyl chloride
ug/L2.01.3 U Xylenes (Total)
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 10452
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 9749
ug/L 50.0 41-146Surrogate: Toluene-d8 9648
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 22:01LCS (7E09026-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 47-13913026 1,1-Dichloroethene
ug/L1.0 20.0 56-1369319 Benzene
ug/L1.0 20.0 51-1399820 Chlorobenzene
ug/L1.0 20.0 64-1319218 Toluene
ug/L1.0 20.0 62-13510321 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 8643
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8844
ug/L 50.0 41-146Surrogate: Toluene-d8 9246
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 22:31Matrix Spike (7E09026-MS1)
Source: CA05953-07
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 47-1391490.94 U30 QM-071,1-Dichloroethene
ug/L1.0 20.0 56-1361100.71 U22 Benzene
ug/L1.0 20.0 51-1391100.72 U22 Chlorobenzene
ug/L1.0 20.0 64-1311070.72 U21 Toluene
ug/L1.0 20.0 62-1351240.89 U25 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9949
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 9347
ug/L 50.0 41-146Surrogate: Toluene-d8 8844
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 23:00Matrix Spike Dup (7E09026-MSD1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E09026 - EPA 5030B_MS
Prepared: 05/09/2017 00:00 Analyzed: 05/09/2017 23:00Matrix Spike Dup (7E09026-MSD1) Continued
Source: CA05953-07
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 1647-139148 0.50.94 U30 QM-071,1-Dichloroethene
ug/L1.0 20.0 1456-136111 10.71 U22 Benzene
ug/L1.0 20.0 1351-139107 30.72 U21 Chlorobenzene
ug/L1.0 20.0 1664-13197 100.72 U19 Toluene
ug/L1.0 20.0 2062-135121 30.89 U24 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9145
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 9748
ug/L 50.0 41-146Surrogate: Toluene-d8 9447
Batch 7E10011 - EPA 5030B_MS
Prepared: 05/10/2017 00:00 Analyzed: 05/10/2017 11:51Blank (7E10011-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.61 U 1,1,1,2-Tetrachloroethane
ug/L1.00.80 U 1,1,1-Trichloroethane
ug/L1.00.54 U 1,1,2,2-Tetrachloroethane
ug/L1.00.76 U 1,1,2-Trichloroethane
ug/L1.00.62 U 1,1-Dichloroethane
ug/L1.00.94 U 1,1-Dichloroethene
ug/L1.00.64 U 1,2,3-Trichloropropane
ug/L1.00.96 U 1,2-Dibromo-3-chloropropane
ug/L1.00.78 U 1,2-Dibromoethane
ug/L1.00.73 U 1,2-Dichlorobenzene
ug/L1.00.63 U 1,2-Dichloroethane
ug/L1.00.80 U 1,2-Dichloropropane
ug/L1.00.76 U 1,4-Dichlorobenzene
ug/L5.04.5 U 2-Butanone
ug/L5.01.4 U 2-Hexanone
ug/L5.00.79 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.2 U Acrylonitrile
ug/L1.00.71 U Benzene
ug/L1.00.94 U Bromochloromethane
ug/L1.00.52 U Bromodichloromethane
ug/L1.00.75 U Bromoform
ug/L1.00.95 U Bromomethane
ug/L5.02.6 U Carbon disulfide
ug/L1.00.94 U Carbon tetrachloride
ug/L1.00.72 U Chlorobenzene
ug/L1.00.98 U Chloroethane
ug/L1.00.80 U Chloroform
ug/L1.00.82 U Chloromethane
ug/L1.00.53 U cis-1,2-Dichloroethene
ug/L1.00.59 U cis-1,3-Dichloropropene
ug/L1.00.44 U Dibromochloromethane
ug/L1.00.84 U Dibromomethane
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Volatile Organic Compounds by GCMS - Quality Control
Batch 7E10011 - EPA 5030B_MS
Prepared: 05/10/2017 00:00 Analyzed: 05/10/2017 11:51Blank (7E10011-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.69 U Ethylbenzene
ug/L5.00.72 U Iodomethane
ug/L2.01.3 U m,p-Xylenes
ug/L5.02.0 U Methylene chloride
ug/L1.00.53 U o-Xylene
ug/L1.00.61 U Styrene
ug/L1.00.76 U Tetrachloroethene
ug/L1.00.72 U Toluene
ug/L1.00.73 U trans-1,2-Dichloroethene
ug/L1.00.73 U trans-1,3-Dichloropropene
ug/L1.00.79 U trans-1,4-Dichloro-2-butene
ug/L1.00.89 U Trichloroethene
ug/L1.00.94 U Trichlorofluoromethane
ug/L5.00.60 U Vinyl acetate
ug/L1.00.71 U Vinyl chloride
ug/L2.01.3 U Xylenes (Total)
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9949
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8844
ug/L 50.0 41-146Surrogate: Toluene-d8 9347
Prepared: 05/10/2017 00:00 Analyzed: 05/10/2017 09:28LCS (7E10011-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 47-1398417 1,1-Dichloroethene
ug/L1.0 20.0 56-1369218 Benzene
ug/L1.0 20.0 51-13910020 Chlorobenzene
ug/L1.0 20.0 64-1319619 Toluene
ug/L1.0 20.0 62-1358918 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9849
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8743
ug/L 50.0 41-146Surrogate: Toluene-d8 9447
Prepared: 05/10/2017 00:00 Analyzed: 05/10/2017 09:57Matrix Spike (7E10011-MS1)
Source: CA05953-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 47-139960.94 U19 1,1-Dichloroethene
ug/L1.0 20.0 56-1361000.71 U20 Benzene
ug/L1.0 20.0 51-1391061.222 Chlorobenzene
ug/L1.0 20.0 64-1311040.72 U21 Toluene
ug/L1.0 20.0 62-135980.89 U20 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 9949
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8643
ug/L 50.0 41-146Surrogate: Toluene-d8 9447
Prepared: 05/10/2017 00:00 Analyzed: 05/10/2017 10:25Matrix Spike Dup (7E10011-MSD1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E10011 - EPA 5030B_MS
Prepared: 05/10/2017 00:00 Analyzed: 05/10/2017 10:25Matrix Spike Dup (7E10011-MSD1) Continued
Source: CA05953-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 1647-13996 0.70.94 U19 1,1-Dichloroethene
ug/L1.0 20.0 1456-13697 30.71 U19 Benzene
ug/L1.0 20.0 1351-139106 0.41.222 Chlorobenzene
ug/L1.0 20.0 1664-131102 10.72 U20 Toluene
ug/L1.0 20.0 2062-13595 30.89 U19 Trichloroethene
ug/L 50.0 41-142Surrogate: 4-Bromofluorobenzene 10050
ug/L 50.0 53-146Surrogate: Dibromofluoromethane 8844
ug/L 50.0 41-146Surrogate: Toluene-d8 9447
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
This compound is a common laboratory contaminant.O-01
The associated laboratory control sample exhibited high bias; since the result is ND, there is no
impact.
QL-02
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
The spike recovery was outside acceptance limits for the MS and/or MSD.QM-19
The associated continuing calibration verification standard exhibited high bias; since the result is
ND, there is no impact.
QV-01
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