7803_Roberson_Subtitle DMSWLF_LeachateReleaseReport_DIN28588_20171009

2211 W. Meadowview Rd., #101
Greensboro, NC 27409
tel: [phone]
fax: [phone]
www.JoyceEngineering.com

October 9, 2017

Ms. Jackie Drummond
Compliance Hydrogeologist
NCDEQ/Solid Waste Section
Asheville Regional Office (ARO)
2090 US Highway 70
Swannanoa, NC 28778
Via email: [e-mail]

RE: Leachate Release Assessment Report
Robeson County Landfill, Permit No. 7803-MSWLF-1997
Robeson County, North Carolina

Dear Mrs. Drummond:

Joyce Engineering (JOYCE) presents this report on the results of the environmental
assessment conducted at the July 2017 leachate release area at the Robeson Municipal Solid
Waste (MSW) landfill, Permit No. 7803-MSWLF-1997. The environmental assessment was
conducted to evaluate the extent of potential environmental impacts resulting from a recent
leachate release due to a leaking force main. The location of the release is shown on the attached
Drawing 1.

METHODOLOGY
The environmental assessment followed the Sampling Plan for Leachate Release
Assessment, prepared by JOYCE, dated July 28, 2017, and approved by the North Carolina
Department of Environmental Quality (NCDEQ), Division of Waste Management, Solid Waste
Section (SWS) in a letter dated August 1, 2017 and incorporated here by reference.

FIELD ACTIVITIES
Hunt Environmental Associates lead the field activities and completed them between
August 14 and 15, 2017. The field activities consisted of collecting a background soil sample
and 14 environmental samples, which consisted of six soil samples from three soil borings (SB-1
through SB-3), five shallow soil samples from the stormwater ditch (SS-4 through SS-8), a
surface water sample from the small pond located at the outfall of the Sediment Basin (SW-A)
and two groundwater samples (SB-1-GW and MW-17R). All the samples were analyzed for the
constituents included in Appendix I of 40 CFR Part 258 (Appendix I). In addition, to assess the
adequacy of the decontamination process, an Equipment Blank was collected and analyzed for
Appendix I VOCs.

Ms. Jackie Drummond
October 9, 2017
Page 2 of 5

A summary of the collected environmental samples is included in the following table.
The attached Drawing 1 shows the locations of the samples, as well as the approximate surface
water flow path into Sediment Basin. Groundwater and surface water sample logs are included
as Attachment A.
SUMMARY OF ENVIRONMENTAL SAMPLES
Sample ID Matrix Sample Depth
(Below Ground Surface)
SB-1 (7 ft) Soil 7 feet
SB-1 (10 ft) Soil 10 feet
SB-2 (7 ft) Soil 7 feet
SB-2 (10 ft) Soil 10 feet
SB-3 (7 ft) Soil 7 feet
SB-3 (10 ft) Soil 10 feet
SS-4 Soil 6 – 12 inches
SS-5 Soil 6 – 12 inches
SS-6 Soil 6 – 12 inches
SS-7 Soil 6 – 12 inches
SS-8 Soil 6 – 12 inches
SW-A Surface Water NA
MW-17R Groundwater 16.5 feeta
SB-1-GW Groundwater 11.0 feeta

The soil, surface water, and groundwater samples were placed in laboratory-prepared
containers and put immediately into a cooler with ice and transported to the laboratory under
chain-of-custody control. The samples were transported to ESC Lab Sciences in Mt. Juliet,
Tennessee for analysis. As previously stated, the samples were analyzed for the Appendix I
constituents following the Environmental Protection Agency approve method (EPA Method)
7471B (mercury), Metals (ICP) by EPA Method 6010D or 6020B and Volatile Organic
Compounds (VOCs) by EPA Method 8260B).

LABORATORY ANALYTICAL RESULTS
The laboratory analytical report was received on August 30, 2017, and is included as Attachment
B.

SOIL SAMPLES ANALYTICAL RESULTS
Table 1 summarizes the analytical results for the soil samples and includes the
Preliminary Soil Remediation Goals (PSRGs) from the NCDEQ Inactive Hazardous Sites
Branch. The soil analytical results were compared to both the Industrial Health-based PSRG
a Depth to Groundwater from measuring point.
NA – Not Applicable
Ms. Jackie Drummond
October 9, 2017
Page 3 of 5

and the Protection of Groundwater PSRG. Based on the analytical test reports, VOCs
concentrations for all the soil samples were below the Reported Detection Limit (RDL).

Three metals (arsenic, cobalt, and vanadium) were detected above the lowest applicable
PSRG in one or more soil samples. Arsenic exceeded the PSRG in SB-2-10’, SB-3-7’, SB-3-
10’, and SS-7. Arsenic was not detected in the background sample (SB-BG). Cobalt exceeded
the PSRG in SB-2-10’, SB-3-7’, SB-3-10’, SS-4, SS-5, and SS-7. Cobalt was not detected in the
background sample (SB-BG). Vanadium exceeded the PSRG in the background sample (SB-
BG) and in all other soil samples except SS-6. Vanadium concentrations exceeded the
background in SB-2-10’, SB-3-7’, SS-4, SS-5, and SS-7; however, they were all within the same
order-of-magnitude (less than three times the concentration in SB-BG).

It is important to indicate that the RDLs for cobalt were above the PSRG in soil samples
SB-BG (background), SB-17’, SB-1 10’, SB-2 7’, SS-6, and SS-8; therefore, those soil samples
concentrations were compared to the background’s RDL concentration and were found to be at
or below the background RDL.

GROUNDWATER SAMPLES ANALYTICAL RESULTS
Groundwater samples were collected from a temporary well (SB-1); which is located
adjacent to the release area, and monitoring well MW-17R and their analytical result are
summarized in Table 2. The analytical test reports are included as Attachment B. The location
of groundwater samples are depicted on Drawing 1.

The analytical test reports reported concentrations of arsenic (17.4 µg/L), cobalt
(10.6 µg/L), vanadium (56.0 µg/L), and lead (15.4 µg/L) above the North Carolina Groundwater
Standards (15A NCAC 2L (NC2L)) in the temporary well SB-1. The concentrations are just
above NC2L of 10 µg/L, 10 µg/L and 150 µg/L, respectively. Cobalt was also reported in the
groundwater sample collected from monitoring well MW-17R (27.3 µg/L) at a concentration
above its NC2L. The other Appendix I constituents were reported to be below their respective
RDL.

SURFACE WATER SAMPLES ANALYTICAL RESULTS
A surface water sample (SW-A) was collected from the small pond located at the outfall
of the stormwater ditch, approximately 620 feet southeast of the release area and analyzed for
Appendix I constituents. The analytical test reports show that all the Appendix I constituents
concentrations were below their respective North Carolina Surface Water Standard (15A NCAC
2B). The analytical test results are summarized in Table 2 and the analytical reports are included
as Attachment B. The approximate location of the pond is depicted on Drawing 1.

Ms. Jackie Drummond
October 9, 2017
Page 4 of 5

QUALITY CONTROL SAMPLES ANALYTICAL RESULTS
As stated before, an Equipment Blank sample was collected and analyzed for the
Appendix I VOCs constituents to assess the adequacy of the decontamination process. Based on
the analytical results, the concentrations of all the Appendix I VOC constituents were below their
respective RDL.

QUALITY CONTROL
Based on the Quality Control data submitted with the Analytical Reports, all Method and
Batch Quality Control are within established criteria; however, J and B qualifiers were reported
for some of the constituents. The qualifier and description of the affected analyte are included in
Tables 1 and 2.

CONCLUSIONS
The results of this environmental assessment indicate that concentrations of the Appendix
I VOCs for the soil, groundwater and surface samples collected are below the NCDEQ
SWSDWM standards; therefore, the potential impact of any released VOCs to groundwater,
receptors, or the environment appears to be negligible, if any.

Arsenic, cobalt, and vanadium were detected in most of the soil samples above their
respective PSRG; however, vanadium was also detected in the background soil sample above the
PSRG. Concentrations of vanadium above the background concentrations were detected in five
of the nine soil samples with detectable concentrations; however, the concentrations were of the
same magnitude as the background concentrations. Since these metals occur naturally in the
mineralogy of the North Carolina soils, their concentrations are just above the PSRG and
vanadium concentrations are within the same magnitude of the background concentrations, we
suspect that the metals reported above the PSRG concentrations may be associated to
background concentrations and not to the release; however, since neither arsenic nor cobalt was
detected in the background sample, this is not conclusive.

Arsenic, cobalt, vanadium, and lead were detected in the groundwater samples at
concentrations above the NC2L; however, since the metals occur naturally in the North Carolina
groundwater and the reported concentrations are just above their respective standards, these
concentrations may be representative of natural groundwater conditions at the site; nevertheless,
the data is not conclusive.

Based on these conclusions, it is recommended to continue monitoring well MW-17R for
the Appendix I metals for the next four quarters. If there is no significate increase from the
historical mean during those four quarters, the sampling should return to its regular sampling
schedule and constituents.

Ms. Jackie Drummond
October 9, 2017
Page 5 of 5

Please contact me at [phone] or [e-mail] if you have
any questions regarding this sampling letter report.

Sincerely,
JOYCE ENGINEERING

Miguel A Vázquez, P.G.
Technical Consultant

Attachments:
Drawing 1, Table1, Table 2
Attachments 1 & 2

cc: Steve Edge, Robeson County
Gene Walters, Robeson County
Amy Davis, Joyce Engineering

DRAWING

160 160170180190200210210200190190150
170
180
190
200
210
1501501
4
0
1
5
0
MW-16
MW-17R
MW-18
MW-4A
MW-25
SW-2
MMW-11
MMW-10
MMW-9MMW-8
MMW-14
MMW-13
MMW-18R
EXISTING LEACHATE
STORAGE TANKS
FMFMFMFMFMFM
EXISTING LEACHATE
FORCEMAIN
PERMITTED LIMITS OF WASTE
CULVERT (TYP)
POND
SURFACE WATER
FLOW DIRECTION (TYP)
SB-3
SB-1
SB-2
SS-4
SS-5
SS-6
SS-7
SS-8
SS-8
SB1-GW
SS-8
SS-5
SB-1
SB1-GW
SAMPLE LOCATIONS
SOIL BORING LOCATION AND ID
SHALLOW SOIL SAMPLE LOCATION AND ID
SURFACE WATER SAMPLE LOCATION AND ID
GROUND WATER SAMPLE LOCATION AND ID
APPROXIMATE LOCATION
OF LEACHATE RELEASE 9731-F SOUTHERN PINE BLVD.CHARLOTTE, NC 28273PHONE: [phone]NC CORP LIC: C-07820
(FEET)
GRAPHIC SCALE
20010050
820.1801.11ROBESON COUNTY LANDFILLST. PAULS, NORTH CAROLINA1
AS SHOWNLEACHATE RELEASE ASSESMENT VBRWHVBVB09/14/17PROJECT NO.APPROVEDCHECKEDDRAWNDESIGNEDDATEDATEREVISIONS AND RECORD OF ISSUEBYNOAPPCKSCALE All rights reserved.Ó Joyce Engineering, Inc.DRAWING NO.2017LETTER REPORT

TABLES

TABLE 1: SOIL CONSTITUENT CONCENTRATIONSResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgResult (dry) mg/kgQRDL (dry) mg/kgMercury7471B 1.00 ND 0.0234 0.0238 0.0224 ND 0.023 ND 0.023 0.0393 0.0238 ND 0.0247 ND 0.0228 0.0677 0.0304 0.0597 0.0297 ND 0.0235 ND 0.024 ND 0.0236Antimony6010D0.90 ND J6 2.34 ND 2.24 ND 2.3 ND 2.3 ND 2.38 ND 2.47 ND 2.28 ND 3.04 ND 2.97 ND 2.35 ND 2.4 ND 2.36Arsenic6010D3.00 ND 2.34 2.75 2.24 2.41 2.3 ND 2.313.12.384.862.473.692.286.63.046.422.97 ND 2.354.062.4 ND 2.36Barium6010D580 21.2 0.586 15.8 0.561 28.3 0.576 14.3 0.575 45.9 0.594 31.7 0.618 19.4 0.571 76.9 0.76 70.8 0.743 15 0.588 31.5 0.601 5.86 0.591Beryllium6010D63 0.268 0.234 ND 0.224 ND 0.23 ND 0.23 ND 0.238 ND 0.247 ND 0.228 0.52 0.304 0.534 0.297 ND 0.235 0.251 0.24 ND 0.236Cadmium6010D3.00 ND 0.586 ND 0.561 ND 0.576 ND 0.575 ND 0.594 ND 0.618 ND 0.571 ND 0.76 ND 0.743 ND 0.588 ND 0.601 ND 0.591Chromium6010D100,000 17.8 1.17 15.3 1.12 19.5 1.15 10.2 1.15 41 1.19 28.2 1.24 19.4 1.14 48.3 1.52 44.9 1.49 1.57 1.18251.2 6.1 1.18Cobalt6010D0.90 ND 1.17 ND 1.12 ND 1.15 ND 1.152.561.191.841.242.681.144.91.527.711.49 ND 1.181.821.2 ND 1.18Copper6010D700 3.33 2.34 4.27 2.24 5.5 2.3 2.71 2.3 15.5 2.38 9.04 2.47 5.78 2.28 22.1 3.04 19.5 2.97 ND 2.35 7.89 2.4 ND 2.36Lead6010D270 5.76 0.586 3.39 0.561 5.46 0.576 2.98 0.575 4.29 0.594 4.36 0.618 7.64 0.571 18.5 0.76 20.5 0.743 0.78 0.588 11.5 0.601 1.87 0.591Nickel6010D130 4.37 2.34 4.59 2.24 5.86 2.3 3.69 2.3 11.6 2.38 7.91 2.47 5.23 2.28 15.3 3.04 14.9 2.97 ND 2.35 7.33 2.4 ND 2.36Selenium6010D2.10 ND 2.34 ND 2.24 ND 2.3 ND 2.3 ND 2.38 ND 2.47 ND 2.28 ND 3.04 ND 2.97 ND 2.35 ND 2.4 ND 2.36Silver6010D3.40 ND 1.17 ND 1.12 ND 1.15 ND 1.15 ND 1.19 ND 1.24 ND 1.14 ND 1.52 ND 1.49 ND 1.18 ND 1.2 ND 1.18Thallium6010D0.28 ND 2.34 ND 2.24 ND 2.3 ND 2.3 ND 2.38 ND 2.47 ND 2.28 ND 3.04 ND 2.97 ND 2.35 ND 2.4 ND 2.36Vanadium6010D6.0034.52.3426.72.2430.92.3172.386.42.3854.92.4731.92.2893.33.0484.92.97 5.15 2.3543.22.4 9.56 2.36Zinc6010D1200 7.95 B 5.86 8.49 B 5.61 9.53 B 5.76 9.47 B 5.75 19.9 B 5.94 13.3 B 6.18 8.29 B 5.71 70.5 7.6 93.9 7.43 7.36 B 5.88 24.6 6.01 6.65 B 5.91Acetone8260B24.00 ND 0.0586 ND 0.0561 ND 0.0576 ND 0.0575 ND 0.0594 ND 0.0618 ND 0.0571 ND 0.076 ND 0.0743 ND 0.0588 ND 0.0601 ND 0.0591Acrylonitrile8260B1.10 ND 0.0117 ND 0.0112 ND 0.0115 ND 0.0115 ND 0.0119 ND 0.0124 ND 0.0114 ND 0.0152 ND 0.0149 ND 0.0118 ND 0.012 ND 0.0118Benzene8260B0.01 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Bromochloromethane8260B126.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Bromodichloromethane8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Bromoform8260B0.02 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Bromomethane8260B6.00 ND 0.00586 ND 0.00561 ND 0.00576 ND 0.00575 ND 0.00594 ND 0.00618 ND 0.00571 ND 0.0076 ND 0.00743 ND 0.00588 ND 0.00601 ND 0.00591Carbon disulfide8260B3.80 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Carbon tetrachloride8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Chlorobenzene8260B0.44 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Chlorodibromomethane8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Chloroethane8260B16.00 ND 0.00586 ND 0.00561 ND 0.00576 ND 0.00575 ND 0.00594 ND 0.00618 ND 0.00571 ND 0.0076 ND 0.00743 ND 0.00588 ND 0.00601 ND 0.00591Chloroform8260B0.34 ND 0.00586 ND 0.00561 ND 0.00576 ND 0.00575 ND 0.00594 ND 0.00618 ND 0.00571 ND 0.0076 ND 0.00743 ND 0.00588 ND 0.00601 ND 0.00591Chloromethane8260B0.02 ND 0.00293 ND 0.00281 ND 0.00288 ND 0.00287 ND 0.00297 ND 0.00309 ND 0.00285 ND 0.0038 ND 0.00372 ND 0.00294 ND 0.003 ND 0.00296Dibromomethane8260B0.31 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,2-Dichlorobenzene8260B0.24 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,4-Dichlorobenzene8260B0.07 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118trans-1,4-Dichloro-2-butene8260B0.03 ND 0.00293 ND 0.00281 ND 0.00288 ND 0.00287 ND 0.00297 ND 0.00309 ND 0.00285 ND 0.0038 ND 0.00372 ND 0.00294 ND 0.003 ND 0.002961,1-Dichloroethane8260B0.03 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,2-Dichloroethane8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,1-Dichloroethene8260B0.05 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118cis-1,2-Dichloroethene8260B0.36 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118trans-1,2-Dichloroethene8260B0.55 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,2-Dichloropropane8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118cis-1,3-Dichloropropene8260B1490 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118trans-1,3-Dichloropropene8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Ethylbenzene8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001182-Hexanone8260B0.17 ND 0.0117 ND 0.0112 ND 0.0115 ND 0.0115 ND 0.0119 ND 0.0124 ND 0.0114 ND 0.0152 ND 0.0149 ND 0.0118 ND 0.012 ND 0.0118Iodomethane8260BNL ND 0.0117 ND 0.0112 ND 0.0115 ND 0.0115 ND 0.0119 ND 0.0124 ND 0.0114 ND 0.0152 ND 0.0149 ND 0.0118 ND 0.012 ND 0.01182-Butanone (MEK)8260B16.00 ND 0.0117 ND 0.0112 ND 0.0115 ND 0.0115 ND 0.0119 ND 0.0124 ND 0.0114 ND 0.0152 ND 0.0149 ND 0.0118 ND 0.012 ND 0.0118Methylene Chloride8260B0.02 ND 0.00586 ND 0.00561 ND 0.00576 ND 0.00575 ND 0.00594 ND 0.00618 ND 0.00571 ND 0.0076 ND 0.00743 ND 0.00588 ND 0.00601 ND 0.005914-Methyl-2-pentanone (MIBK)8260B0.43 ND 0.0117 ND 0.0112 ND 0.0115 ND 0.0115 ND 0.0119 ND 0.0124 ND 0.0114 ND 0.0152 ND 0.0149 ND 0.0118 ND 0.012 ND 0.0118Styrene8260B0.92 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,1,1,2-Tetrachloroethane8260B0.01 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,1,2,2-Tetrachloroethane8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Tetrachloroethene8260B0.01 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Toluene8260B5.50 ND 0.00586 ND 0.00561 ND 0.00576 ND 0.00575 ND 0.00594 ND 0.00618 ND 0.00571 ND 0.0076 ND 0.00743 ND 0.00588 ND 0.00601 ND 0.005911,1,1-Trichloroethane8260B1.20 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.001181,1,2-Trichloroethane8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Trichloroethene8260B0.02 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Trichlorofluoromethane8260B24.00 ND 0.00586 ND 0.00561 ND 0.00576 ND 0.00575 ND 0.00594 ND 0.00618 ND 0.00571 ND 0.0076 ND 0.00743 ND 0.00588 ND 0.00601 ND 0.005911,2,3-Trichloropropane8260B0.00 ND 0.00293 ND 0.00281 ND 0.00288 ND 0.00287 ND 0.00297 ND 0.00309 ND 0.00285 ND 0.0038 ND 0.00372 ND 0.00294 ND 0.003 ND 0.00296Vinyl acetate8260B0.37 ND 0.0117 ND 0.0112 ND 0.0115 ND 0.0115 ND 0.0119 ND 0.0124 ND 0.0114 ND 0.0152 ND 0.0149 ND 0.0118 ND 0.012 ND 0.0118Vinyl chloride8260B0.00 ND 0.00117 ND 0.00112 ND 0.00115 ND 0.00115 ND 0.00119 ND 0.00124 ND 0.00114 ND 0.00152 ND 0.00149 ND 0.00118 ND 0.0012 ND 0.00118Xylenes, Total8260B6.10 ND 0.00351 ND 0.00337 ND 0.00346 ND 0.00345 ND 0.00356 ND 0.00371 ND 0.00342 ND 0.00456 ND 0.00446 ND 0.00353 ND 0.0036 ND 0.00355Notes:PSRG = Lowest of Industrial Health-Based or Protection of Groundwater Q = Qualifiermg/kg = miligrams per kilograms J6 = The sample matrix interfered with the ability to make any accurate determination; spike value is low.RDL = Report Detection Limit. B = The same analyte is found in the associated blank. NL = Not Listed 15.3 = Bold blue concentration above the PSRG but below concentration of background soils ND = Not Detected Above the Reported Detection Limit (RDL) 86.4 = Bold Concentration above the PSRGAnalyteEPA Method SS-5 SS-6 SS-7PRELIMINARY SOIL REMEDIATION GOALS (PSRG) mg.kgSS-8SB-BG SB-1 7' SB-1 10' SB-2 7' SB-2 10' SB-3 7' SB-3 10' SS-4Robeson County Landfill, Permit No. 7803‐MSWLF‐1997 Robeson County, North CarolinaPage 1 of 1Joyce Engineering
TABLE 2: SURFACE WATER AND GROUNDWATER CONSTITUENT CONCENTRATIONS
Result
µg/l Q RDL
mg/l
Result
µg/l Q RDL
mg/l
Result
µg/l Q RDL
mg/l
Mercury 7470A 0.012 ND 0.0002 1 ND 0.0002 ND 0.0002
Arsenic 6010D 10 ND 0.01 10 ND 0.01 17.4 0.01
Barium 6010D 1000 4.51 0.005 700 113 0.005 282 0.005
Chromium 6010D 11 ND 0.01 10* ND 0.01 34.1 0.01
Cobalt 6010D 10* ND 0.01 1*273 0.01 10.6 0.01
Nickel 6010D 16.1 ND 0.01 100 ND 0.01 54.3 0.01
Silver 6010D 0.3 ND 0.005 20 ND 0.005 ND 0.005
Vanadium 6010D 0.3* ND 0.02 25* ND 0.02 56 0.02
Antimony 6020B NL ND 0.002 6* ND 0.002 ND 0.002
Beryllium 6020B 6.5 ND 0.002 1 ND 0.002 ND 0.002
Cadmium 6020B 0.15 ND 0.001 2 ND 0.001 ND 0.001
Copper 6020B 2.74 ND 0.005 1000 ND 0.005 19.5 0.005
Lead 6020B 0.54 ND 0.002 15 ND 0.002 15.4 0.002
Selenium 6020B 5 ND 0.002 20 ND 0.002 3.82 0.002
Thallium 6020B NL ND 0.002 5.5* ND 0.002 ND 0.002
Zinc 6020B 36.2 25.6 0.025 1000 ND 0.025 27.1 0.025
Acetone 8260B NL ND 0.05 6000 ND 0.05 ND J3 0.05
Acrylonitrile 8260B NL ND 0.01 200* ND 0.01 ND 0.01
Benzene 8260B 1.19 ND 0.001 1 ND 0.001 ND 0.001
Bromochloromethane 8260B NL ND 0.001 0.06 ND 0.001 ND 0.001
Bromodichloromethane 8260B NL ND 0.001 0.06 ND 0.001 ND 0.001
Bromoform 8260B NL ND 0.001 4 ND 0.001 ND 0.001
Bromomethane 8260B NL ND 0.005 10 ND 0.005 ND 0.005
Carbon disulfide 8260B NL ND 0.001 700 ND 0.001 ND 0.001
Carbon tetrachloride 8260B 0.254 ND 0.001 0.3 ND 0.001 ND J4 0.001
Chlorobenzene 8260B 488 ND 0.001 50 ND 0.001 ND 0.001
Chlorodibromomethane 8260B NL ND 0.001 0.4 ND 0.001 ND 0.001
Chloroethane 8260B NL ND 0.005 3000 ND 0.005 ND 0.005
Chloroform 8260B NL ND 0.005 70 ND 0.005 ND 0.005
Chloromethane 8260B NL ND 0.0025 3 ND 0.0025 ND 0.0025
Dibromomethane 8260B NL ND 0.001 10* ND 0.001 ND 0.001
1,2-Dichlorobenzene 8260B NL ND 0.001 20 ND 0.001 ND 0.001
1,4-Dichlorobenzene 8260B NL ND 0.001 6 ND 0.001 ND 0.001
trans-1,4-Dichloro-2-butene 8260B NL ND 0.0025 100* ND 0.0025 ND 0.0025
1,1-Dichloroethane 8260B NL ND 0.001 6 ND 0.001 ND 0.001
1,2-Dichloroethane 8260B NL ND 0.001 0.4 ND 0.001 ND 0.001
1,1-Dichloroethene 8260B NL ND 0.001 350 ND 0.001 ND 0.001
cis-1,2-Dichloroethene 8260B NL ND 0.001 70 ND 0.001 ND 0.001
trans-1,2-Dichloroethene 8260B NL ND 0.001 100 ND 0.001 ND 0.001
1,2-Dichloropropane 8260B NL ND 0.001 6 ND 0.001 ND 0.001
cis-1,3-Dichloropropene 8260B NL ND 0.001 0.4 ND 0.001 ND 0.001
trans-1,3-Dichloropropene 8260B NL ND 0.001 0.4 ND 0.001 ND 0.001
Ethylbenzene 8260B NL ND 0.001 600 ND 0.001 2.38 0.001
2-Hexanone 8260B NL ND 0.01 4000 ND 0.01 ND 0.01
Iodomethane 8260B NL ND J3 0.01 10* ND J3 0.01 ND J3,J4 0.01
2-Butanone (MEK)8260B NL ND 0.01 4000 ND 0.01 ND 0.01
Methylene Chloride 8260B NL ND 0.005 5 ND 0.005 ND 0.005
4-Methyl-2-pentanone (MIBK)8260B NL ND 0.01 100* ND 0.01 ND 0.01
Styrene 8260B NL ND 0.001 70 ND 0.001 ND 0.001
1,1,1,2-Tetrachloroethane 8260B NL ND 0.001 5* ND 0.001 ND 0.001
1,1,2,2-Tetrachloroethane 8260B NL ND 0.001 0.2 ND 0.001 ND 0.001
Tetrachloroethene 8260B NL ND 0.001 0.7 ND 0.001 ND 0.001
Toluene 8260B 11 ND 0.001 600 ND 0.001 26.4 0.001
1,1,1-Trichloroethane 8260B NL ND 0.001 200 ND 0.001 ND 0.001
1,1,2-Trichloroethane 8260B NL ND 0.001 1* ND 0.001 ND 0.001
Trichloroethene 8260B NL ND 0.001 3 ND 0.001 ND 0.001
Trichlorofluoromethane 8260B NL ND 0.005 2000 ND 0.005 ND 0.005
1,2,3-Trichloropropane 8260B NL ND 0.0025 0.005 ND 0.0025 ND 0.0025
Vinyl acetate 8260B NL ND 0.01 50* ND 0.01 ND 0.01
Vinyl chloride 8260B NL ND 0.001 0.03 ND 0.001 ND 0.001
Xylenes, Total 8260B NL ND 0.003 500 0.00515 0.003 19.1 0.003
NL = Not Listed .NC 2B = Surface Water Standards from 15A NCAC 2B.
ND = Not Detected Above the Reported Detection Limit (RDL).NC 2L = Groundwater Standards from 15A NCAC 2L.
Bold = Detected above the North Carolina Surface Water or Groundwater Standards.* = NC-DEQ Solid Waste Section Reporting Limits.
J3 = The associated batch QC was outside the established quality control range for precision.
J4 = The associated batch QC was outside the established quality control range for accuracy.
NC 2B µg/l NC 2L
µg/l
SW-A MW-17R SB-1-GWEPA
Method Analyte
Robeson County Landfill, Permit No. 7803‐MSWLF‐1997
 Robeson County, North Carolina Page 1 of 1Joyce Engineering

ATTACHMENT A

GROUNDWATER SAMPLING LOG

SITE
NAME: RCL Landfill
SITE
LOCATION: 246 Landfill Rd, St Pauls, NC 28384
WELL NO: SAMPLE ID: SW-A DATE: 8 -14-2 0 1 7
PURGING DATA
WELL
DIAMETER (inches): N/A WELL SCREEN INTERVAL
DEPTH: feet to feet
STATIC DEPTH
TO WATER (feet):
PURGE PUMP TYPE
OR BAILER: Pump
PuPumpPeristaltiPPu WELL VOLUME PURGE: 1 WELL VOLUME = (TOTAL WELL DEPTH – STATIC DEPTH TO WATER) X WELL CAPACITY
(only fill out if applicable)
= ( feet – feet) X gallons/foot = gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL. = PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable) = gallons + ( gallons/foot X feet) + gallons = gallons
FINAL BOTTOM
DEPTH IN WELL (feet): PURGING
INITIATED AT: 1:45
PM
PURGING
ENDED AT: 1:55
TOTAL VOLUME
PURGED (gallons): 3

TIME
PURGE
PUMP RATE

ORP
(mV)

pH
(standard
units)

TEMP.
(OC)
COND. (circle units) mhos/cm
or S/cm
DISSOLVED
OXYGEN
(circle units)
mg/L or
% saturation

TURBIDITY
(NTUs)

COLOR
(describe)

ODOR
(describe)
12:15 A M N/A 153.7 7.75 30.1 0.223 8.34 mg/l 41.4 Cloudy None

WELL CAPACITY (Gallons Per Foot): 0.75” = 0.02; 1” = 0.04; 1.25” = 0.06; 2” = 0.16; 3” = 0.37; 4” = 0.65; 5” = 1.02; 6” = 1.47; 12” = 5.88
TUBING INSIDE DIA. CAPACITY (Gal./Ft.): 1/8" = 0.0006; 3/16" = 0.0014; 1/4" = 0.0026; 5/16" = 0.004; 3/8" = 0.006; 1/2" = 0.010; 5/8" = 0.016
PURGING EQUIPMENT CODES: B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Other (Specify)

NOTES:
STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS:
pH: + 0.1 units Temperature: + 0.2 oC(+3%) Specific Conductance: + 3% Dissolved Oxygen: all readings + 10% saturation; optionally, + 0.2 mg/L or
+ 10% (whichever is greater) Turbidity: optionally + 5 NTU or + 10% (whichever is greater) ORP: + 10 millivolts
GROUNDWATER SAMPLING LOG

SITE
NAME: RCL Landfill
SITE
LOCATION: 246 Landfill Rd, St Pauls, NC 28384
WELL NO: MW-17R SAMPLE ID: MW-17R DATE: 8 -14-2 0 1 7
PURGING DATA
WELL
DIAMETER (inches): 2 WELL SCREEN INTERVAL
DEPTH: 7.5 feet to 17.5 feet
STATIC DEPTH
TO WATER (feet): 13.4’
PURGE PUMP TYPE
OR BAILER: Pump
PuPumpPeristaltiPPu WELL VOLUME PURGE: 1 WELL VOLUME = (TOTAL WELL DEPTH – STATIC DEPTH TO WATER) X WELL CAPACITY
(only fill out if applicable)
= ( 20 feet – 13.4 feet) X 0.1356 gallons/foot = 0.89496 gallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL. = PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable) = 0.89496 gallons + (0.0057 gallons/foot X 25 feet) + 0.25 gallons = 1.2875 gallons
FINAL BOTTOM
DEPTH IN WELL (feet): PURGING
INITIATED AT: 1:45
PM
PURGING
ENDED AT: 1:55
TOTAL VOLUME
PURGED (gallons): 3

TIME
PURGE
PUMP RATE

ORP
(mV)

pH
(standard
units)

TEMP.
(OC)
COND. (circle units) mhos/cm
or S/cm
DISSOLVED
OXYGEN
(circle units)
mg/L or
% saturation

TURBIDITY
(NTUs)

COLOR
(describe)

ODOR
(describe)
2:00 P M 0.3 185 4.2 24.7 0.373 1.77 mg/l 3.39 Clear None

WELL CAPACITY (Gallons Per Foot): 0.75” = 0.02; 1” = 0.04; 1.25” = 0.06; 2” = 0.16; 3” = 0.37; 4” = 0.65; 5” = 1.02; 6” = 1.47; 12” = 5.88
TUBING INSIDE DIA. CAPACITY (Gal./Ft.): 1/8" = 0.0006; 3/16" = 0.0014; 1/4" = 0.0026; 5/16" = 0.004; 3/8" = 0.006; 1/2" = 0.010; 5/8" = 0.016
PURGING EQUIPMENT CODES: B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Other (Specify)

NOTES:
STABILIZATION CRITERIA FOR RANGE OF VARIATION OF LAST THREE CONSECUTIVE READINGS:
pH: + 0.1 units Temperature: + 0.2 oC(+3%) Specific Conductance: + 3% Dissolved Oxygen: all readings + 10% saturation; optionally, + 0.2 mg/L or
+ 10% (whichever is greater) Turbidity: optionally + 5 NTU or + 10% (whichever is greater) ORP: + 10 millivolts

ATTACHMENT B
ANALYTICAL REPORT
August 28, 2017
Hunt Environmental Associates
Sample Delivery Group:L930565
Samples Received:08/18/2017
Project Number:17-0801245
Description:RCL Leachate Spill
Report To:Cody Hunt
1730 Rennert Road
Lumberton, NC 28360
Entire Report Reviewed By:
August 28, 2017
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
August 28, 2017
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
SB-BG L930565-01 7
SB-1 7' L930565-02 9
SB-1 10' L930565-03 11
SB-2 7' L930565-04 13
SB-2 10' L930565-05 15
SB-3 7' L930565-06 17
SB-3 10' L930565-07 19
SS-4 L930565-08 21
SS-5 L930565-09 23
SS-6 L930565-10 25
SS-7 L930565-11 27
SS-8 L930565-12 29
SW-A L930565-13 31
MW-17R L930565-14 33
SB-1-GW L930565-15 35
EQUIPMENT BLANK L930565-16 37
Qc: Quality Control Summary 38
Total Solids by Method 2540 G-2011 38
Mercury by Method 7470A 41
Mercury by Method 7471B 43
Metals (ICP) by Method 6010D 44
Metals (ICPMS) by Method 6020B 47
Volatile Organic Compounds (GC/MS) by Method 8260B 50
Gl: Glossary of Terms 59
Al: Accreditations & Locations 60
Sc: Chain of Custody 61
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-BG L930565-01 Solid Michael C Hurt 08/14/17 10:30 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:29 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:03 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 10:30 08/22/17 14:07 JAH
Collected by Collected date/time Received date/time
SB-1 7' L930565-02 Solid Michael C Hurt 08/14/17 11:05 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012670 1 08/23/17 10:46 08/23/17 11:01 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:41 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:19 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 11:05 08/22/17 14:27 JAH
Collected by Collected date/time Received date/time
SB-1 10' L930565-03 Solid Michael C Hurt 08/14/17 11:20 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012670 1 08/23/17 10:46 08/23/17 11:01 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:43 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:23 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 11:20 08/22/17 14:46 JAH
Collected by Collected date/time Received date/time
SB-2 7' L930565-04 Solid Michael C Hurt 08/14/17 13:45 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012670 1 08/23/17 10:46 08/23/17 11:01 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:45 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:32 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 13:45 08/22/17 15:06 JAH
Collected by Collected date/time Received date/time
SB-2 10' L930565-05 Solid Michael C Hurt 08/14/17 14:20 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012743 1 08/24/17 12:48 08/24/17 13:07 KDW
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:48 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:36 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 14:20 08/22/17 16:05 JAH
Collected by Collected date/time Received date/time
SB-3 7' L930565-06 Solid Michael C Hurt 08/15/17 09:05 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012743 1 08/24/17 12:48 08/24/17 13:07 KDW
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:50 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:39 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/15/17 09:05 08/22/17 16:45 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-3 10' L930565-07 Solid Michael C Hurt 08/15/17 09:35 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:53 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:42 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/15/17 09:35 08/22/17 17:04 BMB
Collected by Collected date/time Received date/time
SS-4 L930565-08 Solid Michael C Hurt 08/14/17 10:45 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:55 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:45 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 10:45 08/22/17 17:24 BMB
Collected by Collected date/time Received date/time
SS-5 L930565-09 Solid Michael C Hurt 08/14/17 10:55 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 09:57 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:49 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 15:55 08/22/17 17:44 BMB
Collected by Collected date/time Received date/time
SS-6 L930565-10 Solid Michael C Hurt 08/14/17 11:10 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 10:00 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:52 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 11:10 08/22/17 18:04 BMB
Collected by Collected date/time Received date/time
SS-7 L930565-11 Solid Michael C Hurt 08/14/17 11:25 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 10:02 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:55 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 11:25 08/27/17 18:45 JHH
Collected by Collected date/time Received date/time
SS-8 L930565-12 Solid Michael C Hurt 08/14/17 11:45 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1012140 1 08/22/17 14:03 08/22/17 14:21 JD
Mercury by Method 7471B WG1011876 1 08/21/17 13:41 08/22/17 10:12 ABL
Metals (ICP) by Method 6010D WG1012952 1 08/24/17 15:19 08/28/17 02:59 CCE
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011691 1 08/14/17 14:05 08/22/17 18:43 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-A L930565-13 GW Michael C Hurt 08/14/17 12:15 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG1012561 1 08/23/17 08:41 08/23/17 12:50 ABL
Metals (ICP) by Method 6010D WG1013097 1 08/25/17 13:19 08/25/17 17:07 ST
Metals (ICPMS) by Method 6020B WG1012187 1 08/24/17 15:19 08/24/17 19:51 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011888 1 08/20/17 22:29 08/20/17 22:29 JAH
Collected by Collected date/time Received date/time
MW-17R L930565-14 GW Michael C Hurt 08/14/17 14:10 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG1011867 1 08/21/17 15:26 08/22/17 00:00 EL
Metals (ICP) by Method 6010D WG1013097 1 08/25/17 13:19 08/25/17 17:10 ST
Metals (ICPMS) by Method 6020B WG1012187 1 08/24/17 15:19 08/24/17 18:55 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG1011888 1 08/20/17 22:51 08/20/17 22:51 JAH
Collected by Collected date/time Received date/time
SB-1-GW L930565-15 GW Michael C Hurt 08/14/17 13:05 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG1012561 1 08/23/17 08:41 08/23/17 12:53 ABL
Metals (ICP) by Method 6010D WG1013097 1 08/25/17 13:19 08/25/17 17:14 ST
Metals (ICPMS) by Method 6020B WG1013102 1 08/25/17 15:09 08/26/17 11:51 JPD
Metals (ICPMS) by Method 6020B WG1013541 1 08/28/17 07:44 08/28/17 12:24 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG1012744 1 08/23/17 12:12 08/23/17 12:12 LRL
Collected by Collected date/time Received date/time
EQUIPMENT BLANK L930565-16 GW Michael C Hurt 08/14/17 00:00 08/18/17 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG1012744 1 08/23/17 11:53 08/23/17 11:53 LRL
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
VOC pH outside of method requirement.
ESC Sample ID Project Sample ID Method
L930565-15 SB-1-GW 8260B
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 6 of 65
Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 6 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L930565
SB-BG
Collected date/time: 08/14/17 10:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.4 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0234 1 08/22/2017 09:29 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND J6 2.34 1 08/28/2017 02:03 WG1012952
Arsenic ND 2.34 1 08/28/2017 02:03 WG1012952
Barium 21.2 0.586 1 08/28/2017 02:03 WG1012952
Beryllium 0.268 0.234 1 08/28/2017 02:03 WG1012952
Cadmium ND 0.586 1 08/28/2017 02:03 WG1012952
Chromium 17.8 1.17 1 08/28/2017 02:03 WG1012952
Cobalt ND 1.17 1 08/28/2017 02:03 WG1012952
Copper 3.33 2.34 1 08/28/2017 02:03 WG1012952
Lead 5.76 0.586 1 08/28/2017 02:03 WG1012952
Nickel 4.37 2.34 1 08/28/2017 02:03 WG1012952
Selenium ND 2.34 1 08/28/2017 02:03 WG1012952
Silver ND 1.17 1 08/28/2017 02:03 WG1012952
Thallium ND 2.34 1 08/28/2017 02:03 WG1012952
Vanadium 34.5 2.34 1 08/28/2017 02:03 WG1012952
Zinc 7.95 B 5.86 1 08/28/2017 02:03 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0586 1 08/22/2017 14:07 WG1011691
Acrylonitrile ND 0.0117 1 08/22/2017 14:07 WG1011691
Benzene ND 0.00117 1 08/22/2017 14:07 WG1011691
Bromochloromethane ND 0.00117 1 08/22/2017 14:07 WG1011691
Bromodichloromethane ND 0.00117 1 08/22/2017 14:07 WG1011691
Bromoform ND 0.00117 1 08/22/2017 14:07 WG1011691
Bromomethane ND 0.00586 1 08/22/2017 14:07 WG1011691
Carbon disulfide ND 0.00117 1 08/22/2017 14:07 WG1011691
Carbon tetrachloride ND 0.00117 1 08/22/2017 14:07 WG1011691
Chlorobenzene ND 0.00117 1 08/22/2017 14:07 WG1011691
Chlorodibromomethane ND 0.00117 1 08/22/2017 14:07 WG1011691
Chloroethane ND 0.00586 1 08/22/2017 14:07 WG1011691
Chloroform ND 0.00586 1 08/22/2017 14:07 WG1011691
Chloromethane ND 0.00293 1 08/22/2017 14:07 WG1011691
Dibromomethane ND 0.00117 1 08/22/2017 14:07 WG1011691
1,2-Dichlorobenzene ND 0.00117 1 08/22/2017 14:07 WG1011691
1,4-Dichlorobenzene ND 0.00117 1 08/22/2017 14:07 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00293 1 08/22/2017 14:07 WG1011691
1,1-Dichloroethane ND 0.00117 1 08/22/2017 14:07 WG1011691
1,2-Dichloroethane ND 0.00117 1 08/22/2017 14:07 WG1011691
1,1-Dichloroethene ND 0.00117 1 08/22/2017 14:07 WG1011691
cis-1,2-Dichloroethene ND 0.00117 1 08/22/2017 14:07 WG1011691
trans-1,2-Dichloroethene ND 0.00117 1 08/22/2017 14:07 WG1011691
1,2-Dichloropropane ND 0.00117 1 08/22/2017 14:07 WG1011691
cis-1,3-Dichloropropene ND 0.00117 1 08/22/2017 14:07 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 7 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 7 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L930565
SB-BG
Collected date/time: 08/14/17 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00117 1 08/22/2017 14:07 WG1011691
Ethylbenzene ND 0.00117 1 08/22/2017 14:07 WG1011691
2-Hexanone ND 0.0117 1 08/22/2017 14:07 WG1011691
Iodomethane ND 0.0117 1 08/22/2017 14:07 WG1011691
2-Butanone (MEK)ND 0.0117 1 08/22/2017 14:07 WG1011691
Methylene Chloride ND 0.00586 1 08/22/2017 14:07 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0117 1 08/22/2017 14:07 WG1011691
Styrene ND 0.00117 1 08/22/2017 14:07 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00117 1 08/22/2017 14:07 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00117 1 08/22/2017 14:07 WG1011691
Tetrachloroethene ND 0.00117 1 08/22/2017 14:07 WG1011691
Toluene ND 0.00586 1 08/22/2017 14:07 WG1011691
1,1,1-Trichloroethane ND 0.00117 1 08/22/2017 14:07 WG1011691
1,1,2-Trichloroethane ND 0.00117 1 08/22/2017 14:07 WG1011691
Trichloroethene ND 0.00117 1 08/22/2017 14:07 WG1011691
Trichlorofluoromethane ND 0.00586 1 08/22/2017 14:07 WG1011691
1,2,3-Trichloropropane ND 0.00293 1 08/22/2017 14:07 WG1011691
Vinyl acetate ND 0.0117 1 08/22/2017 14:07 WG1011691
Vinyl chloride ND 0.00117 1 08/22/2017 14:07 WG1011691
Xylenes, Total ND 0.00351 1 08/22/2017 14:07 WG1011691
(S) Toluene-d8 111 80.0-120 08/22/2017 14:07 WG1011691
(S) Dibromofluoromethane 104 74.0-131 08/22/2017 14:07 WG1011691
(S) a,a,a-Trifluorotoluene 99.1 80.0-120 08/22/2017 14:07 WG1011691
(S) 4-Bromofluorobenzene 110 64.0-132 08/22/2017 14:07 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 8 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 8 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L930565
SB-1 7'
Collected date/time: 08/14/17 11:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.1 1 08/23/2017 11:01 WG1012670
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury 0.0238 0.0224 1 08/22/2017 09:41 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.24 1 08/28/2017 02:19 WG1012952
Arsenic 2.75 2.24 1 08/28/2017 02:19 WG1012952
Barium 15.8 0.561 1 08/28/2017 02:19 WG1012952
Beryllium ND 0.224 1 08/28/2017 02:19 WG1012952
Cadmium ND 0.561 1 08/28/2017 02:19 WG1012952
Chromium 15.3 1.12 1 08/28/2017 02:19 WG1012952
Cobalt ND 1.12 1 08/28/2017 02:19 WG1012952
Copper 4.27 2.24 1 08/28/2017 02:19 WG1012952
Lead 3.39 0.561 1 08/28/2017 02:19 WG1012952
Nickel 4.59 2.24 1 08/28/2017 02:19 WG1012952
Selenium ND 2.24 1 08/28/2017 02:19 WG1012952
Silver ND 1.12 1 08/28/2017 02:19 WG1012952
Thallium ND 2.24 1 08/28/2017 02:19 WG1012952
Vanadium 26.7 2.24 1 08/28/2017 02:19 WG1012952
Zinc 8.49 B 5.61 1 08/28/2017 02:19 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0561 1 08/22/2017 14:27 WG1011691
Acrylonitrile ND 0.0112 1 08/22/2017 14:27 WG1011691
Benzene ND 0.00112 1 08/22/2017 14:27 WG1011691
Bromochloromethane ND 0.00112 1 08/22/2017 14:27 WG1011691
Bromodichloromethane ND 0.00112 1 08/22/2017 14:27 WG1011691
Bromoform ND 0.00112 1 08/22/2017 14:27 WG1011691
Bromomethane ND 0.00561 1 08/22/2017 14:27 WG1011691
Carbon disulfide ND 0.00112 1 08/22/2017 14:27 WG1011691
Carbon tetrachloride ND 0.00112 1 08/22/2017 14:27 WG1011691
Chlorobenzene ND 0.00112 1 08/22/2017 14:27 WG1011691
Chlorodibromomethane ND 0.00112 1 08/22/2017 14:27 WG1011691
Chloroethane ND 0.00561 1 08/22/2017 14:27 WG1011691
Chloroform ND 0.00561 1 08/22/2017 14:27 WG1011691
Chloromethane ND 0.00281 1 08/22/2017 14:27 WG1011691
Dibromomethane ND 0.00112 1 08/22/2017 14:27 WG1011691
1,2-Dichlorobenzene ND 0.00112 1 08/22/2017 14:27 WG1011691
1,4-Dichlorobenzene ND 0.00112 1 08/22/2017 14:27 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00281 1 08/22/2017 14:27 WG1011691
1,1-Dichloroethane ND 0.00112 1 08/22/2017 14:27 WG1011691
1,2-Dichloroethane ND 0.00112 1 08/22/2017 14:27 WG1011691
1,1-Dichloroethene ND 0.00112 1 08/22/2017 14:27 WG1011691
cis-1,2-Dichloroethene ND 0.00112 1 08/22/2017 14:27 WG1011691
trans-1,2-Dichloroethene ND 0.00112 1 08/22/2017 14:27 WG1011691
1,2-Dichloropropane ND 0.00112 1 08/22/2017 14:27 WG1011691
cis-1,3-Dichloropropene ND 0.00112 1 08/22/2017 14:27 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 9 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 9 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L930565
SB-1 7'
Collected date/time: 08/14/17 11:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00112 1 08/22/2017 14:27 WG1011691
Ethylbenzene ND 0.00112 1 08/22/2017 14:27 WG1011691
2-Hexanone ND 0.0112 1 08/22/2017 14:27 WG1011691
Iodomethane ND 0.0112 1 08/22/2017 14:27 WG1011691
2-Butanone (MEK)ND 0.0112 1 08/22/2017 14:27 WG1011691
Methylene Chloride ND 0.00561 1 08/22/2017 14:27 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0112 1 08/22/2017 14:27 WG1011691
Styrene ND 0.00112 1 08/22/2017 14:27 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00112 1 08/22/2017 14:27 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00112 1 08/22/2017 14:27 WG1011691
Tetrachloroethene ND 0.00112 1 08/22/2017 14:27 WG1011691
Toluene ND 0.00561 1 08/22/2017 14:27 WG1011691
1,1,1-Trichloroethane ND 0.00112 1 08/22/2017 14:27 WG1011691
1,1,2-Trichloroethane ND 0.00112 1 08/22/2017 14:27 WG1011691
Trichloroethene ND 0.00112 1 08/22/2017 14:27 WG1011691
Trichlorofluoromethane ND 0.00561 1 08/22/2017 14:27 WG1011691
1,2,3-Trichloropropane ND 0.00281 1 08/22/2017 14:27 WG1011691
Vinyl acetate ND 0.0112 1 08/22/2017 14:27 WG1011691
Vinyl chloride ND 0.00112 1 08/22/2017 14:27 WG1011691
Xylenes, Total ND 0.00337 1 08/22/2017 14:27 WG1011691
(S) Toluene-d8 110 80.0-120 08/22/2017 14:27 WG1011691
(S) Dibromofluoromethane 105 74.0-131 08/22/2017 14:27 WG1011691
(S) a,a,a-Trifluorotoluene 101 80.0-120 08/22/2017 14:27 WG1011691
(S) 4-Bromofluorobenzene 106 64.0-132 08/22/2017 14:27 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 10 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 10 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L930565
SB-1 10'
Collected date/time: 08/14/17 11:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.8 1 08/23/2017 11:01 WG1012670
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0230 1 08/22/2017 09:43 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.30 1 08/28/2017 02:23 WG1012952
Arsenic 2.41 2.30 1 08/28/2017 02:23 WG1012952
Barium 28.3 0.576 1 08/28/2017 02:23 WG1012952
Beryllium ND 0.230 1 08/28/2017 02:23 WG1012952
Cadmium ND 0.576 1 08/28/2017 02:23 WG1012952
Chromium 19.5 1.15 1 08/28/2017 02:23 WG1012952
Cobalt ND 1.15 1 08/28/2017 02:23 WG1012952
Copper 5.50 2.30 1 08/28/2017 02:23 WG1012952
Lead 5.46 0.576 1 08/28/2017 02:23 WG1012952
Nickel 5.86 2.30 1 08/28/2017 02:23 WG1012952
Selenium ND 2.30 1 08/28/2017 02:23 WG1012952
Silver ND 1.15 1 08/28/2017 02:23 WG1012952
Thallium ND 2.30 1 08/28/2017 02:23 WG1012952
Vanadium 30.9 2.30 1 08/28/2017 02:23 WG1012952
Zinc 9.53 B 5.76 1 08/28/2017 02:23 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0576 1 08/22/2017 14:46 WG1011691
Acrylonitrile ND 0.0115 1 08/22/2017 14:46 WG1011691
Benzene ND 0.00115 1 08/22/2017 14:46 WG1011691
Bromochloromethane ND 0.00115 1 08/22/2017 14:46 WG1011691
Bromodichloromethane ND 0.00115 1 08/22/2017 14:46 WG1011691
Bromoform ND 0.00115 1 08/22/2017 14:46 WG1011691
Bromomethane ND 0.00576 1 08/22/2017 14:46 WG1011691
Carbon disulfide ND 0.00115 1 08/22/2017 14:46 WG1011691
Carbon tetrachloride ND 0.00115 1 08/22/2017 14:46 WG1011691
Chlorobenzene ND 0.00115 1 08/22/2017 14:46 WG1011691
Chlorodibromomethane ND 0.00115 1 08/22/2017 14:46 WG1011691
Chloroethane ND 0.00576 1 08/22/2017 14:46 WG1011691
Chloroform ND 0.00576 1 08/22/2017 14:46 WG1011691
Chloromethane ND 0.00288 1 08/22/2017 14:46 WG1011691
Dibromomethane ND 0.00115 1 08/22/2017 14:46 WG1011691
1,2-Dichlorobenzene ND 0.00115 1 08/22/2017 14:46 WG1011691
1,4-Dichlorobenzene ND 0.00115 1 08/22/2017 14:46 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00288 1 08/22/2017 14:46 WG1011691
1,1-Dichloroethane ND 0.00115 1 08/22/2017 14:46 WG1011691
1,2-Dichloroethane ND 0.00115 1 08/22/2017 14:46 WG1011691
1,1-Dichloroethene ND 0.00115 1 08/22/2017 14:46 WG1011691
cis-1,2-Dichloroethene ND 0.00115 1 08/22/2017 14:46 WG1011691
trans-1,2-Dichloroethene ND 0.00115 1 08/22/2017 14:46 WG1011691
1,2-Dichloropropane ND 0.00115 1 08/22/2017 14:46 WG1011691
cis-1,3-Dichloropropene ND 0.00115 1 08/22/2017 14:46 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 11 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 11 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L930565
SB-1 10'
Collected date/time: 08/14/17 11:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00115 1 08/22/2017 14:46 WG1011691
Ethylbenzene ND 0.00115 1 08/22/2017 14:46 WG1011691
2-Hexanone ND 0.0115 1 08/22/2017 14:46 WG1011691
Iodomethane ND 0.0115 1 08/22/2017 14:46 WG1011691
2-Butanone (MEK)ND 0.0115 1 08/22/2017 14:46 WG1011691
Methylene Chloride ND 0.00576 1 08/22/2017 14:46 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0115 1 08/22/2017 14:46 WG1011691
Styrene ND 0.00115 1 08/22/2017 14:46 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00115 1 08/22/2017 14:46 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00115 1 08/22/2017 14:46 WG1011691
Tetrachloroethene ND 0.00115 1 08/22/2017 14:46 WG1011691
Toluene ND 0.00576 1 08/22/2017 14:46 WG1011691
1,1,1-Trichloroethane ND 0.00115 1 08/22/2017 14:46 WG1011691
1,1,2-Trichloroethane ND 0.00115 1 08/22/2017 14:46 WG1011691
Trichloroethene ND 0.00115 1 08/22/2017 14:46 WG1011691
Trichlorofluoromethane ND 0.00576 1 08/22/2017 14:46 WG1011691
1,2,3-Trichloropropane ND 0.00288 1 08/22/2017 14:46 WG1011691
Vinyl acetate ND 0.0115 1 08/22/2017 14:46 WG1011691
Vinyl chloride ND 0.00115 1 08/22/2017 14:46 WG1011691
Xylenes, Total ND 0.00346 1 08/22/2017 14:46 WG1011691
(S) Toluene-d8 112 80.0-120 08/22/2017 14:46 WG1011691
(S) Dibromofluoromethane 103 74.0-131 08/22/2017 14:46 WG1011691
(S) a,a,a-Trifluorotoluene 97.6 80.0-120 08/22/2017 14:46 WG1011691
(S) 4-Bromofluorobenzene 107 64.0-132 08/22/2017 14:46 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 12 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 12 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L930565
SB-2 7'
Collected date/time: 08/14/17 13:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.0 1 08/23/2017 11:01 WG1012670
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0230 1 08/22/2017 09:45 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.30 1 08/28/2017 02:32 WG1012952
Arsenic ND 2.30 1 08/28/2017 02:32 WG1012952
Barium 14.3 0.575 1 08/28/2017 02:32 WG1012952
Beryllium ND 0.230 1 08/28/2017 02:32 WG1012952
Cadmium ND 0.575 1 08/28/2017 02:32 WG1012952
Chromium 10.2 1.15 1 08/28/2017 02:32 WG1012952
Cobalt ND 1.15 1 08/28/2017 02:32 WG1012952
Copper 2.71 2.30 1 08/28/2017 02:32 WG1012952
Lead 2.98 0.575 1 08/28/2017 02:32 WG1012952
Nickel 3.69 2.30 1 08/28/2017 02:32 WG1012952
Selenium ND 2.30 1 08/28/2017 02:32 WG1012952
Silver ND 1.15 1 08/28/2017 02:32 WG1012952
Thallium ND 2.30 1 08/28/2017 02:32 WG1012952
Vanadium 17.0 2.30 1 08/28/2017 02:32 WG1012952
Zinc 9.47 B 5.75 1 08/28/2017 02:32 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0575 1 08/22/2017 15:06 WG1011691
Acrylonitrile ND 0.0115 1 08/22/2017 15:06 WG1011691
Benzene ND 0.00115 1 08/22/2017 15:06 WG1011691
Bromochloromethane ND 0.00115 1 08/22/2017 15:06 WG1011691
Bromodichloromethane ND 0.00115 1 08/22/2017 15:06 WG1011691
Bromoform ND 0.00115 1 08/22/2017 15:06 WG1011691
Bromomethane ND 0.00575 1 08/22/2017 15:06 WG1011691
Carbon disulfide ND 0.00115 1 08/22/2017 15:06 WG1011691
Carbon tetrachloride ND 0.00115 1 08/22/2017 15:06 WG1011691
Chlorobenzene ND 0.00115 1 08/22/2017 15:06 WG1011691
Chlorodibromomethane ND 0.00115 1 08/22/2017 15:06 WG1011691
Chloroethane ND 0.00575 1 08/22/2017 15:06 WG1011691
Chloroform ND 0.00575 1 08/22/2017 15:06 WG1011691
Chloromethane ND 0.00287 1 08/22/2017 15:06 WG1011691
Dibromomethane ND 0.00115 1 08/22/2017 15:06 WG1011691
1,2-Dichlorobenzene ND 0.00115 1 08/22/2017 15:06 WG1011691
1,4-Dichlorobenzene ND 0.00115 1 08/22/2017 15:06 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00287 1 08/22/2017 15:06 WG1011691
1,1-Dichloroethane ND 0.00115 1 08/22/2017 15:06 WG1011691
1,2-Dichloroethane ND 0.00115 1 08/22/2017 15:06 WG1011691
1,1-Dichloroethene ND 0.00115 1 08/22/2017 15:06 WG1011691
cis-1,2-Dichloroethene ND 0.00115 1 08/22/2017 15:06 WG1011691
trans-1,2-Dichloroethene ND 0.00115 1 08/22/2017 15:06 WG1011691
1,2-Dichloropropane ND 0.00115 1 08/22/2017 15:06 WG1011691
cis-1,3-Dichloropropene ND 0.00115 1 08/22/2017 15:06 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 13 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 13 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L930565
SB-2 7'
Collected date/time: 08/14/17 13:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00115 1 08/22/2017 15:06 WG1011691
Ethylbenzene ND 0.00115 1 08/22/2017 15:06 WG1011691
2-Hexanone ND 0.0115 1 08/22/2017 15:06 WG1011691
Iodomethane ND 0.0115 1 08/22/2017 15:06 WG1011691
2-Butanone (MEK)ND 0.0115 1 08/22/2017 15:06 WG1011691
Methylene Chloride ND 0.00575 1 08/22/2017 15:06 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0115 1 08/22/2017 15:06 WG1011691
Styrene ND 0.00115 1 08/22/2017 15:06 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00115 1 08/22/2017 15:06 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00115 1 08/22/2017 15:06 WG1011691
Tetrachloroethene ND 0.00115 1 08/22/2017 15:06 WG1011691
Toluene ND 0.00575 1 08/22/2017 15:06 WG1011691
1,1,1-Trichloroethane ND 0.00115 1 08/22/2017 15:06 WG1011691
1,1,2-Trichloroethane ND 0.00115 1 08/22/2017 15:06 WG1011691
Trichloroethene ND 0.00115 1 08/22/2017 15:06 WG1011691
Trichlorofluoromethane ND 0.00575 1 08/22/2017 15:06 WG1011691
1,2,3-Trichloropropane ND 0.00287 1 08/22/2017 15:06 WG1011691
Vinyl acetate ND 0.0115 1 08/22/2017 15:06 WG1011691
Vinyl chloride ND 0.00115 1 08/22/2017 15:06 WG1011691
Xylenes, Total ND 0.00345 1 08/22/2017 15:06 WG1011691
(S) Toluene-d8 108 80.0-120 08/22/2017 15:06 WG1011691
(S) Dibromofluoromethane 106 74.0-131 08/22/2017 15:06 WG1011691
(S) a,a,a-Trifluorotoluene 101 80.0-120 08/22/2017 15:06 WG1011691
(S) 4-Bromofluorobenzene 110 64.0-132 08/22/2017 15:06 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 14 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 14 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L930565
SB-2 10'
Collected date/time: 08/14/17 14:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.2 1 08/24/2017 13:07 WG1012743
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury 0.0393 0.0238 1 08/22/2017 09:48 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.38 1 08/28/2017 02:36 WG1012952
Arsenic 13.1 2.38 1 08/28/2017 02:36 WG1012952
Barium 45.9 0.594 1 08/28/2017 02:36 WG1012952
Beryllium ND 0.238 1 08/28/2017 02:36 WG1012952
Cadmium ND 0.594 1 08/28/2017 02:36 WG1012952
Chromium 41.0 1.19 1 08/28/2017 02:36 WG1012952
Cobalt 2.56 1.19 1 08/28/2017 02:36 WG1012952
Copper 15.5 2.38 1 08/28/2017 02:36 WG1012952
Lead 4.29 0.594 1 08/28/2017 02:36 WG1012952
Nickel 11.6 2.38 1 08/28/2017 02:36 WG1012952
Selenium ND 2.38 1 08/28/2017 02:36 WG1012952
Silver ND 1.19 1 08/28/2017 02:36 WG1012952
Thallium ND 2.38 1 08/28/2017 02:36 WG1012952
Vanadium 86.4 2.38 1 08/28/2017 02:36 WG1012952
Zinc 19.9 B 5.94 1 08/28/2017 02:36 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0594 1 08/22/2017 16:05 WG1011691
Acrylonitrile ND 0.0119 1 08/22/2017 16:05 WG1011691
Benzene ND 0.00119 1 08/22/2017 16:05 WG1011691
Bromochloromethane ND 0.00119 1 08/22/2017 16:05 WG1011691
Bromodichloromethane ND 0.00119 1 08/22/2017 16:05 WG1011691
Bromoform ND 0.00119 1 08/22/2017 16:05 WG1011691
Bromomethane ND 0.00594 1 08/22/2017 16:05 WG1011691
Carbon disulfide ND 0.00119 1 08/22/2017 16:05 WG1011691
Carbon tetrachloride ND 0.00119 1 08/22/2017 16:05 WG1011691
Chlorobenzene ND 0.00119 1 08/22/2017 16:05 WG1011691
Chlorodibromomethane ND 0.00119 1 08/22/2017 16:05 WG1011691
Chloroethane ND 0.00594 1 08/22/2017 16:05 WG1011691
Chloroform ND 0.00594 1 08/22/2017 16:05 WG1011691
Chloromethane ND 0.00297 1 08/22/2017 16:05 WG1011691
Dibromomethane ND 0.00119 1 08/22/2017 16:05 WG1011691
1,2-Dichlorobenzene ND 0.00119 1 08/22/2017 16:05 WG1011691
1,4-Dichlorobenzene ND 0.00119 1 08/22/2017 16:05 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00297 1 08/22/2017 16:05 WG1011691
1,1-Dichloroethane ND 0.00119 1 08/22/2017 16:05 WG1011691
1,2-Dichloroethane ND 0.00119 1 08/22/2017 16:05 WG1011691
1,1-Dichloroethene ND 0.00119 1 08/22/2017 16:05 WG1011691
cis-1,2-Dichloroethene ND 0.00119 1 08/22/2017 16:05 WG1011691
trans-1,2-Dichloroethene ND 0.00119 1 08/22/2017 16:05 WG1011691
1,2-Dichloropropane ND 0.00119 1 08/22/2017 16:05 WG1011691
cis-1,3-Dichloropropene ND 0.00119 1 08/22/2017 16:05 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 15 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 15 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L930565
SB-2 10'
Collected date/time: 08/14/17 14:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00119 1 08/22/2017 16:05 WG1011691
Ethylbenzene ND 0.00119 1 08/22/2017 16:05 WG1011691
2-Hexanone ND 0.0119 1 08/22/2017 16:05 WG1011691
Iodomethane ND 0.0119 1 08/22/2017 16:05 WG1011691
2-Butanone (MEK)ND 0.0119 1 08/22/2017 16:05 WG1011691
Methylene Chloride ND 0.00594 1 08/22/2017 16:05 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0119 1 08/22/2017 16:05 WG1011691
Styrene ND 0.00119 1 08/22/2017 16:05 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00119 1 08/22/2017 16:05 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00119 1 08/22/2017 16:05 WG1011691
Tetrachloroethene ND 0.00119 1 08/22/2017 16:05 WG1011691
Toluene ND 0.00594 1 08/22/2017 16:05 WG1011691
1,1,1-Trichloroethane ND 0.00119 1 08/22/2017 16:05 WG1011691
1,1,2-Trichloroethane ND 0.00119 1 08/22/2017 16:05 WG1011691
Trichloroethene ND 0.00119 1 08/22/2017 16:05 WG1011691
Trichlorofluoromethane ND 0.00594 1 08/22/2017 16:05 WG1011691
1,2,3-Trichloropropane ND 0.00297 1 08/22/2017 16:05 WG1011691
Vinyl acetate ND 0.0119 1 08/22/2017 16:05 WG1011691
Vinyl chloride ND 0.00119 1 08/22/2017 16:05 WG1011691
Xylenes, Total ND 0.00356 1 08/22/2017 16:05 WG1011691
(S) Toluene-d8 109 80.0-120 08/22/2017 16:05 WG1011691
(S) Dibromofluoromethane 99.8 74.0-131 08/22/2017 16:05 WG1011691
(S) a,a,a-Trifluorotoluene 98.4 80.0-120 08/22/2017 16:05 WG1011691
(S) 4-Bromofluorobenzene 106 64.0-132 08/22/2017 16:05 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 16 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 16 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L930565
SB-3 7'
Collected date/time: 08/15/17 09:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.9 1 08/24/2017 13:07 WG1012743
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0247 1 08/22/2017 09:50 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.47 1 08/28/2017 02:39 WG1012952
Arsenic 4.86 2.47 1 08/28/2017 02:39 WG1012952
Barium 31.7 0.618 1 08/28/2017 02:39 WG1012952
Beryllium ND 0.247 1 08/28/2017 02:39 WG1012952
Cadmium ND 0.618 1 08/28/2017 02:39 WG1012952
Chromium 28.2 1.24 1 08/28/2017 02:39 WG1012952
Cobalt 1.84 1.24 1 08/28/2017 02:39 WG1012952
Copper 9.04 2.47 1 08/28/2017 02:39 WG1012952
Lead 4.36 0.618 1 08/28/2017 02:39 WG1012952
Nickel 7.91 2.47 1 08/28/2017 02:39 WG1012952
Selenium ND 2.47 1 08/28/2017 02:39 WG1012952
Silver ND 1.24 1 08/28/2017 02:39 WG1012952
Thallium ND 2.47 1 08/28/2017 02:39 WG1012952
Vanadium 54.9 2.47 1 08/28/2017 02:39 WG1012952
Zinc 13.3 B 6.18 1 08/28/2017 02:39 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0618 1 08/22/2017 16:45 WG1011691
Acrylonitrile ND 0.0124 1 08/22/2017 16:45 WG1011691
Benzene ND 0.00124 1 08/22/2017 16:45 WG1011691
Bromochloromethane ND 0.00124 1 08/22/2017 16:45 WG1011691
Bromodichloromethane ND 0.00124 1 08/22/2017 16:45 WG1011691
Bromoform ND 0.00124 1 08/22/2017 16:45 WG1011691
Bromomethane ND 0.00618 1 08/22/2017 16:45 WG1011691
Carbon disulfide ND 0.00124 1 08/22/2017 16:45 WG1011691
Carbon tetrachloride ND 0.00124 1 08/22/2017 16:45 WG1011691
Chlorobenzene ND 0.00124 1 08/22/2017 16:45 WG1011691
Chlorodibromomethane ND 0.00124 1 08/22/2017 16:45 WG1011691
Chloroethane ND 0.00618 1 08/22/2017 16:45 WG1011691
Chloroform ND 0.00618 1 08/22/2017 16:45 WG1011691
Chloromethane ND 0.00309 1 08/22/2017 16:45 WG1011691
Dibromomethane ND 0.00124 1 08/22/2017 16:45 WG1011691
1,2-Dichlorobenzene ND 0.00124 1 08/22/2017 16:45 WG1011691
1,4-Dichlorobenzene ND 0.00124 1 08/22/2017 16:45 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00309 1 08/22/2017 16:45 WG1011691
1,1-Dichloroethane ND 0.00124 1 08/22/2017 16:45 WG1011691
1,2-Dichloroethane ND 0.00124 1 08/22/2017 16:45 WG1011691
1,1-Dichloroethene ND 0.00124 1 08/22/2017 16:45 WG1011691
cis-1,2-Dichloroethene ND 0.00124 1 08/22/2017 16:45 WG1011691
trans-1,2-Dichloroethene ND 0.00124 1 08/22/2017 16:45 WG1011691
1,2-Dichloropropane ND 0.00124 1 08/22/2017 16:45 WG1011691
cis-1,3-Dichloropropene ND 0.00124 1 08/22/2017 16:45 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 17 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 17 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L930565
SB-3 7'
Collected date/time: 08/15/17 09:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00124 1 08/22/2017 16:45 WG1011691
Ethylbenzene ND 0.00124 1 08/22/2017 16:45 WG1011691
2-Hexanone ND 0.0124 1 08/22/2017 16:45 WG1011691
Iodomethane ND 0.0124 1 08/22/2017 16:45 WG1011691
2-Butanone (MEK)ND 0.0124 1 08/22/2017 16:45 WG1011691
Methylene Chloride ND 0.00618 1 08/22/2017 16:45 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0124 1 08/22/2017 16:45 WG1011691
Styrene ND 0.00124 1 08/22/2017 16:45 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00124 1 08/22/2017 16:45 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00124 1 08/22/2017 16:45 WG1011691
Tetrachloroethene ND 0.00124 1 08/22/2017 16:45 WG1011691
Toluene ND 0.00618 1 08/22/2017 16:45 WG1011691
1,1,1-Trichloroethane ND 0.00124 1 08/22/2017 16:45 WG1011691
1,1,2-Trichloroethane ND 0.00124 1 08/22/2017 16:45 WG1011691
Trichloroethene ND 0.00124 1 08/22/2017 16:45 WG1011691
Trichlorofluoromethane ND 0.00618 1 08/22/2017 16:45 WG1011691
1,2,3-Trichloropropane ND 0.00309 1 08/22/2017 16:45 WG1011691
Vinyl acetate ND 0.0124 1 08/22/2017 16:45 WG1011691
Vinyl chloride ND 0.00124 1 08/22/2017 16:45 WG1011691
Xylenes, Total ND 0.00371 1 08/22/2017 16:45 WG1011691
(S) Toluene-d8 111 80.0-120 08/22/2017 16:45 WG1011691
(S) Dibromofluoromethane 103 74.0-131 08/22/2017 16:45 WG1011691
(S) a,a,a-Trifluorotoluene 101 80.0-120 08/22/2017 16:45 WG1011691
(S) 4-Bromofluorobenzene 107 64.0-132 08/22/2017 16:45 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 18 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 18 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L930565
SB-3 10'
Collected date/time: 08/15/17 09:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.6 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0228 1 08/22/2017 09:53 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.28 1 08/28/2017 02:42 WG1012952
Arsenic 3.69 2.28 1 08/28/2017 02:42 WG1012952
Barium 19.4 0.571 1 08/28/2017 02:42 WG1012952
Beryllium ND 0.228 1 08/28/2017 02:42 WG1012952
Cadmium ND 0.571 1 08/28/2017 02:42 WG1012952
Chromium 19.4 1.14 1 08/28/2017 02:42 WG1012952
Cobalt 2.68 1.14 1 08/28/2017 02:42 WG1012952
Copper 5.78 2.28 1 08/28/2017 02:42 WG1012952
Lead 7.64 0.571 1 08/28/2017 02:42 WG1012952
Nickel 5.23 2.28 1 08/28/2017 02:42 WG1012952
Selenium ND 2.28 1 08/28/2017 02:42 WG1012952
Silver ND 1.14 1 08/28/2017 02:42 WG1012952
Thallium ND 2.28 1 08/28/2017 02:42 WG1012952
Vanadium 31.9 2.28 1 08/28/2017 02:42 WG1012952
Zinc 8.29 B 5.71 1 08/28/2017 02:42 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0571 1 08/22/2017 17:04 WG1011691
Acrylonitrile ND 0.0114 1 08/22/2017 17:04 WG1011691
Benzene ND 0.00114 1 08/22/2017 17:04 WG1011691
Bromochloromethane ND 0.00114 1 08/22/2017 17:04 WG1011691
Bromodichloromethane ND 0.00114 1 08/22/2017 17:04 WG1011691
Bromoform ND 0.00114 1 08/22/2017 17:04 WG1011691
Bromomethane ND 0.00571 1 08/22/2017 17:04 WG1011691
Carbon disulfide ND 0.00114 1 08/22/2017 17:04 WG1011691
Carbon tetrachloride ND 0.00114 1 08/22/2017 17:04 WG1011691
Chlorobenzene ND 0.00114 1 08/22/2017 17:04 WG1011691
Chlorodibromomethane ND 0.00114 1 08/22/2017 17:04 WG1011691
Chloroethane ND 0.00571 1 08/22/2017 17:04 WG1011691
Chloroform ND 0.00571 1 08/22/2017 17:04 WG1011691
Chloromethane ND 0.00285 1 08/22/2017 17:04 WG1011691
Dibromomethane ND 0.00114 1 08/22/2017 17:04 WG1011691
1,2-Dichlorobenzene ND 0.00114 1 08/22/2017 17:04 WG1011691
1,4-Dichlorobenzene ND 0.00114 1 08/22/2017 17:04 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00285 1 08/22/2017 17:04 WG1011691
1,1-Dichloroethane ND 0.00114 1 08/22/2017 17:04 WG1011691
1,2-Dichloroethane ND 0.00114 1 08/22/2017 17:04 WG1011691
1,1-Dichloroethene ND 0.00114 1 08/22/2017 17:04 WG1011691
cis-1,2-Dichloroethene ND 0.00114 1 08/22/2017 17:04 WG1011691
trans-1,2-Dichloroethene ND 0.00114 1 08/22/2017 17:04 WG1011691
1,2-Dichloropropane ND 0.00114 1 08/22/2017 17:04 WG1011691
cis-1,3-Dichloropropene ND 0.00114 1 08/22/2017 17:04 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 19 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 19 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L930565
SB-3 10'
Collected date/time: 08/15/17 09:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00114 1 08/22/2017 17:04 WG1011691
Ethylbenzene ND 0.00114 1 08/22/2017 17:04 WG1011691
2-Hexanone ND 0.0114 1 08/22/2017 17:04 WG1011691
Iodomethane ND 0.0114 1 08/22/2017 17:04 WG1011691
2-Butanone (MEK)ND 0.0114 1 08/22/2017 17:04 WG1011691
Methylene Chloride ND 0.00571 1 08/22/2017 17:04 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0114 1 08/22/2017 17:04 WG1011691
Styrene ND 0.00114 1 08/22/2017 17:04 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00114 1 08/22/2017 17:04 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00114 1 08/22/2017 17:04 WG1011691
Tetrachloroethene ND 0.00114 1 08/22/2017 17:04 WG1011691
Toluene ND 0.00571 1 08/22/2017 17:04 WG1011691
1,1,1-Trichloroethane ND 0.00114 1 08/22/2017 17:04 WG1011691
1,1,2-Trichloroethane ND 0.00114 1 08/22/2017 17:04 WG1011691
Trichloroethene ND 0.00114 1 08/22/2017 17:04 WG1011691
Trichlorofluoromethane ND 0.00571 1 08/22/2017 17:04 WG1011691
1,2,3-Trichloropropane ND 0.00285 1 08/22/2017 17:04 WG1011691
Vinyl acetate ND 0.0114 1 08/22/2017 17:04 WG1011691
Vinyl chloride ND 0.00114 1 08/22/2017 17:04 WG1011691
Xylenes, Total ND 0.00342 1 08/22/2017 17:04 WG1011691
(S) Toluene-d8 110 80.0-120 08/22/2017 17:04 WG1011691
(S) Dibromofluoromethane 103 74.0-131 08/22/2017 17:04 WG1011691
(S) a,a,a-Trifluorotoluene 103 80.0-120 08/22/2017 17:04 WG1011691
(S) 4-Bromofluorobenzene 108 64.0-132 08/22/2017 17:04 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 20 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 20 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L930565
SS-4
Collected date/time: 08/14/17 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 65.8 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury 0.0677 0.0304 1 08/22/2017 09:55 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 3.04 1 08/28/2017 02:45 WG1012952
Arsenic 6.60 3.04 1 08/28/2017 02:45 WG1012952
Barium 76.9 0.760 1 08/28/2017 02:45 WG1012952
Beryllium 0.520 0.304 1 08/28/2017 02:45 WG1012952
Cadmium ND 0.760 1 08/28/2017 02:45 WG1012952
Chromium 48.3 1.52 1 08/28/2017 02:45 WG1012952
Cobalt 4.90 1.52 1 08/28/2017 02:45 WG1012952
Copper 22.1 3.04 1 08/28/2017 02:45 WG1012952
Lead 18.5 0.760 1 08/28/2017 02:45 WG1012952
Nickel 15.3 3.04 1 08/28/2017 02:45 WG1012952
Selenium ND 3.04 1 08/28/2017 02:45 WG1012952
Silver ND 1.52 1 08/28/2017 02:45 WG1012952
Thallium ND 3.04 1 08/28/2017 02:45 WG1012952
Vanadium 93.3 3.04 1 08/28/2017 02:45 WG1012952
Zinc 70.5 7.60 1 08/28/2017 02:45 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0760 1 08/22/2017 17:24 WG1011691
Acrylonitrile ND 0.0152 1 08/22/2017 17:24 WG1011691
Benzene ND 0.00152 1 08/22/2017 17:24 WG1011691
Bromochloromethane ND 0.00152 1 08/22/2017 17:24 WG1011691
Bromodichloromethane ND 0.00152 1 08/22/2017 17:24 WG1011691
Bromoform ND 0.00152 1 08/22/2017 17:24 WG1011691
Bromomethane ND 0.00760 1 08/22/2017 17:24 WG1011691
Carbon disulfide ND 0.00152 1 08/22/2017 17:24 WG1011691
Carbon tetrachloride ND 0.00152 1 08/22/2017 17:24 WG1011691
Chlorobenzene ND 0.00152 1 08/22/2017 17:24 WG1011691
Chlorodibromomethane ND 0.00152 1 08/22/2017 17:24 WG1011691
Chloroethane ND 0.00760 1 08/22/2017 17:24 WG1011691
Chloroform ND 0.00760 1 08/22/2017 17:24 WG1011691
Chloromethane ND 0.00380 1 08/22/2017 17:24 WG1011691
Dibromomethane ND 0.00152 1 08/22/2017 17:24 WG1011691
1,2-Dichlorobenzene ND 0.00152 1 08/22/2017 17:24 WG1011691
1,4-Dichlorobenzene ND 0.00152 1 08/22/2017 17:24 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00380 1 08/22/2017 17:24 WG1011691
1,1-Dichloroethane ND 0.00152 1 08/22/2017 17:24 WG1011691
1,2-Dichloroethane ND 0.00152 1 08/22/2017 17:24 WG1011691
1,1-Dichloroethene ND 0.00152 1 08/22/2017 17:24 WG1011691
cis-1,2-Dichloroethene ND 0.00152 1 08/22/2017 17:24 WG1011691
trans-1,2-Dichloroethene ND 0.00152 1 08/22/2017 17:24 WG1011691
1,2-Dichloropropane ND 0.00152 1 08/22/2017 17:24 WG1011691
cis-1,3-Dichloropropene ND 0.00152 1 08/22/2017 17:24 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 21 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 21 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L930565
SS-4
Collected date/time: 08/14/17 10:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00152 1 08/22/2017 17:24 WG1011691
Ethylbenzene ND 0.00152 1 08/22/2017 17:24 WG1011691
2-Hexanone ND 0.0152 1 08/22/2017 17:24 WG1011691
Iodomethane ND 0.0152 1 08/22/2017 17:24 WG1011691
2-Butanone (MEK)ND 0.0152 1 08/22/2017 17:24 WG1011691
Methylene Chloride ND 0.00760 1 08/22/2017 17:24 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0152 1 08/22/2017 17:24 WG1011691
Styrene ND 0.00152 1 08/22/2017 17:24 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00152 1 08/22/2017 17:24 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00152 1 08/22/2017 17:24 WG1011691
Tetrachloroethene ND 0.00152 1 08/22/2017 17:24 WG1011691
Toluene ND 0.00760 1 08/22/2017 17:24 WG1011691
1,1,1-Trichloroethane ND 0.00152 1 08/22/2017 17:24 WG1011691
1,1,2-Trichloroethane ND 0.00152 1 08/22/2017 17:24 WG1011691
Trichloroethene ND 0.00152 1 08/22/2017 17:24 WG1011691
Trichlorofluoromethane ND 0.00760 1 08/22/2017 17:24 WG1011691
1,2,3-Trichloropropane ND 0.00380 1 08/22/2017 17:24 WG1011691
Vinyl acetate ND 0.0152 1 08/22/2017 17:24 WG1011691
Vinyl chloride ND 0.00152 1 08/22/2017 17:24 WG1011691
Xylenes, Total ND 0.00456 1 08/22/2017 17:24 WG1011691
(S) Toluene-d8 110 80.0-120 08/22/2017 17:24 WG1011691
(S) Dibromofluoromethane 105 74.0-131 08/22/2017 17:24 WG1011691
(S) a,a,a-Trifluorotoluene 98.1 80.0-120 08/22/2017 17:24 WG1011691
(S) 4-Bromofluorobenzene 115 64.0-132 08/22/2017 17:24 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 22 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 22 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L930565
SS-5
Collected date/time: 08/14/17 10:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 67.3 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury 0.0597 0.0297 1 08/22/2017 09:57 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.97 1 08/28/2017 02:49 WG1012952
Arsenic 6.42 2.97 1 08/28/2017 02:49 WG1012952
Barium 70.8 0.743 1 08/28/2017 02:49 WG1012952
Beryllium 0.534 0.297 1 08/28/2017 02:49 WG1012952
Cadmium ND 0.743 1 08/28/2017 02:49 WG1012952
Chromium 44.9 1.49 1 08/28/2017 02:49 WG1012952
Cobalt 7.71 1.49 1 08/28/2017 02:49 WG1012952
Copper 19.5 2.97 1 08/28/2017 02:49 WG1012952
Lead 20.5 0.743 1 08/28/2017 02:49 WG1012952
Nickel 14.9 2.97 1 08/28/2017 02:49 WG1012952
Selenium ND 2.97 1 08/28/2017 02:49 WG1012952
Silver ND 1.49 1 08/28/2017 02:49 WG1012952
Thallium ND 2.97 1 08/28/2017 02:49 WG1012952
Vanadium 84.9 2.97 1 08/28/2017 02:49 WG1012952
Zinc 93.9 7.43 1 08/28/2017 02:49 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0743 1 08/22/2017 17:44 WG1011691
Acrylonitrile ND 0.0149 1 08/22/2017 17:44 WG1011691
Benzene ND 0.00149 1 08/22/2017 17:44 WG1011691
Bromochloromethane ND 0.00149 1 08/22/2017 17:44 WG1011691
Bromodichloromethane ND 0.00149 1 08/22/2017 17:44 WG1011691
Bromoform ND 0.00149 1 08/22/2017 17:44 WG1011691
Bromomethane ND 0.00743 1 08/22/2017 17:44 WG1011691
Carbon disulfide ND 0.00149 1 08/22/2017 17:44 WG1011691
Carbon tetrachloride ND 0.00149 1 08/22/2017 17:44 WG1011691
Chlorobenzene ND 0.00149 1 08/22/2017 17:44 WG1011691
Chlorodibromomethane ND 0.00149 1 08/22/2017 17:44 WG1011691
Chloroethane ND 0.00743 1 08/22/2017 17:44 WG1011691
Chloroform ND 0.00743 1 08/22/2017 17:44 WG1011691
Chloromethane ND 0.00372 1 08/22/2017 17:44 WG1011691
Dibromomethane ND 0.00149 1 08/22/2017 17:44 WG1011691
1,2-Dichlorobenzene ND 0.00149 1 08/22/2017 17:44 WG1011691
1,4-Dichlorobenzene ND 0.00149 1 08/22/2017 17:44 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00372 1 08/22/2017 17:44 WG1011691
1,1-Dichloroethane ND 0.00149 1 08/22/2017 17:44 WG1011691
1,2-Dichloroethane ND 0.00149 1 08/22/2017 17:44 WG1011691
1,1-Dichloroethene ND 0.00149 1 08/22/2017 17:44 WG1011691
cis-1,2-Dichloroethene ND 0.00149 1 08/22/2017 17:44 WG1011691
trans-1,2-Dichloroethene ND 0.00149 1 08/22/2017 17:44 WG1011691
1,2-Dichloropropane ND 0.00149 1 08/22/2017 17:44 WG1011691
cis-1,3-Dichloropropene ND 0.00149 1 08/22/2017 17:44 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 23 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 23 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L930565
SS-5
Collected date/time: 08/14/17 10:55
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00149 1 08/22/2017 17:44 WG1011691
Ethylbenzene ND 0.00149 1 08/22/2017 17:44 WG1011691
2-Hexanone ND 0.0149 1 08/22/2017 17:44 WG1011691
Iodomethane ND 0.0149 1 08/22/2017 17:44 WG1011691
2-Butanone (MEK)ND 0.0149 1 08/22/2017 17:44 WG1011691
Methylene Chloride ND 0.00743 1 08/22/2017 17:44 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0149 1 08/22/2017 17:44 WG1011691
Styrene ND 0.00149 1 08/22/2017 17:44 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00149 1 08/22/2017 17:44 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00149 1 08/22/2017 17:44 WG1011691
Tetrachloroethene ND 0.00149 1 08/22/2017 17:44 WG1011691
Toluene ND 0.00743 1 08/22/2017 17:44 WG1011691
1,1,1-Trichloroethane ND 0.00149 1 08/22/2017 17:44 WG1011691
1,1,2-Trichloroethane ND 0.00149 1 08/22/2017 17:44 WG1011691
Trichloroethene ND 0.00149 1 08/22/2017 17:44 WG1011691
Trichlorofluoromethane ND 0.00743 1 08/22/2017 17:44 WG1011691
1,2,3-Trichloropropane ND 0.00372 1 08/22/2017 17:44 WG1011691
Vinyl acetate ND 0.0149 1 08/22/2017 17:44 WG1011691
Vinyl chloride ND 0.00149 1 08/22/2017 17:44 WG1011691
Xylenes, Total ND 0.00446 1 08/22/2017 17:44 WG1011691
(S) Toluene-d8 113 80.0-120 08/22/2017 17:44 WG1011691
(S) Dibromofluoromethane 104 74.0-131 08/22/2017 17:44 WG1011691
(S) a,a,a-Trifluorotoluene 98.1 80.0-120 08/22/2017 17:44 WG1011691
(S) 4-Bromofluorobenzene 108 64.0-132 08/22/2017 17:44 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 24 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 24 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L930565
SS-6
Collected date/time: 08/14/17 11:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.1 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0235 1 08/22/2017 10:00 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.35 1 08/28/2017 02:52 WG1012952
Arsenic ND 2.35 1 08/28/2017 02:52 WG1012952
Barium 15.0 0.588 1 08/28/2017 02:52 WG1012952
Beryllium ND 0.235 1 08/28/2017 02:52 WG1012952
Cadmium ND 0.588 1 08/28/2017 02:52 WG1012952
Chromium 1.57 1.18 1 08/28/2017 02:52 WG1012952
Cobalt ND 1.18 1 08/28/2017 02:52 WG1012952
Copper ND 2.35 1 08/28/2017 02:52 WG1012952
Lead 0.780 0.588 1 08/28/2017 02:52 WG1012952
Nickel ND 2.35 1 08/28/2017 02:52 WG1012952
Selenium ND 2.35 1 08/28/2017 02:52 WG1012952
Silver ND 1.18 1 08/28/2017 02:52 WG1012952
Thallium ND 2.35 1 08/28/2017 02:52 WG1012952
Vanadium 5.15 2.35 1 08/28/2017 02:52 WG1012952
Zinc 7.36 B 5.88 1 08/28/2017 02:52 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0588 1 08/22/2017 18:04 WG1011691
Acrylonitrile ND 0.0118 1 08/22/2017 18:04 WG1011691
Benzene ND 0.00118 1 08/22/2017 18:04 WG1011691
Bromochloromethane ND 0.00118 1 08/22/2017 18:04 WG1011691
Bromodichloromethane ND 0.00118 1 08/22/2017 18:04 WG1011691
Bromoform ND 0.00118 1 08/22/2017 18:04 WG1011691
Bromomethane ND 0.00588 1 08/22/2017 18:04 WG1011691
Carbon disulfide ND 0.00118 1 08/22/2017 18:04 WG1011691
Carbon tetrachloride ND 0.00118 1 08/22/2017 18:04 WG1011691
Chlorobenzene ND 0.00118 1 08/22/2017 18:04 WG1011691
Chlorodibromomethane ND 0.00118 1 08/22/2017 18:04 WG1011691
Chloroethane ND 0.00588 1 08/22/2017 18:04 WG1011691
Chloroform ND 0.00588 1 08/22/2017 18:04 WG1011691
Chloromethane ND 0.00294 1 08/22/2017 18:04 WG1011691
Dibromomethane ND 0.00118 1 08/22/2017 18:04 WG1011691
1,2-Dichlorobenzene ND 0.00118 1 08/22/2017 18:04 WG1011691
1,4-Dichlorobenzene ND 0.00118 1 08/22/2017 18:04 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00294 1 08/22/2017 18:04 WG1011691
1,1-Dichloroethane ND 0.00118 1 08/22/2017 18:04 WG1011691
1,2-Dichloroethane ND 0.00118 1 08/22/2017 18:04 WG1011691
1,1-Dichloroethene ND 0.00118 1 08/22/2017 18:04 WG1011691
cis-1,2-Dichloroethene ND 0.00118 1 08/22/2017 18:04 WG1011691
trans-1,2-Dichloroethene ND 0.00118 1 08/22/2017 18:04 WG1011691
1,2-Dichloropropane ND 0.00118 1 08/22/2017 18:04 WG1011691
cis-1,3-Dichloropropene ND 0.00118 1 08/22/2017 18:04 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 25 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 25 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L930565
SS-6
Collected date/time: 08/14/17 11:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00118 1 08/22/2017 18:04 WG1011691
Ethylbenzene ND 0.00118 1 08/22/2017 18:04 WG1011691
2-Hexanone ND 0.0118 1 08/22/2017 18:04 WG1011691
Iodomethane ND 0.0118 1 08/22/2017 18:04 WG1011691
2-Butanone (MEK)ND 0.0118 1 08/22/2017 18:04 WG1011691
Methylene Chloride ND 0.00588 1 08/22/2017 18:04 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0118 1 08/22/2017 18:04 WG1011691
Styrene ND 0.00118 1 08/22/2017 18:04 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00118 1 08/22/2017 18:04 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00118 1 08/22/2017 18:04 WG1011691
Tetrachloroethene ND 0.00118 1 08/22/2017 18:04 WG1011691
Toluene ND 0.00588 1 08/22/2017 18:04 WG1011691
1,1,1-Trichloroethane ND 0.00118 1 08/22/2017 18:04 WG1011691
1,1,2-Trichloroethane ND 0.00118 1 08/22/2017 18:04 WG1011691
Trichloroethene ND 0.00118 1 08/22/2017 18:04 WG1011691
Trichlorofluoromethane ND 0.00588 1 08/22/2017 18:04 WG1011691
1,2,3-Trichloropropane ND 0.00294 1 08/22/2017 18:04 WG1011691
Vinyl acetate ND 0.0118 1 08/22/2017 18:04 WG1011691
Vinyl chloride ND 0.00118 1 08/22/2017 18:04 WG1011691
Xylenes, Total ND 0.00353 1 08/22/2017 18:04 WG1011691
(S) Toluene-d8 112 80.0-120 08/22/2017 18:04 WG1011691
(S) Dibromofluoromethane 106 74.0-131 08/22/2017 18:04 WG1011691
(S) a,a,a-Trifluorotoluene 98.6 80.0-120 08/22/2017 18:04 WG1011691
(S) 4-Bromofluorobenzene 106 64.0-132 08/22/2017 18:04 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 14:47 26 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 26 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L930565
SS-7
Collected date/time: 08/14/17 11:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.2 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0240 1 08/22/2017 10:02 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.40 1 08/28/2017 02:55 WG1012952
Arsenic 4.06 2.40 1 08/28/2017 02:55 WG1012952
Barium 31.5 0.601 1 08/28/2017 02:55 WG1012952
Beryllium 0.251 0.240 1 08/28/2017 02:55 WG1012952
Cadmium ND 0.601 1 08/28/2017 02:55 WG1012952
Chromium 25.0 1.20 1 08/28/2017 02:55 WG1012952
Cobalt 1.82 1.20 1 08/28/2017 02:55 WG1012952
Copper 7.89 2.40 1 08/28/2017 02:55 WG1012952
Lead 11.5 0.601 1 08/28/2017 02:55 WG1012952
Nickel 7.33 2.40 1 08/28/2017 02:55 WG1012952
Selenium ND 2.40 1 08/28/2017 02:55 WG1012952
Silver ND 1.20 1 08/28/2017 02:55 WG1012952
Thallium ND 2.40 1 08/28/2017 02:55 WG1012952
Vanadium 43.2 2.40 1 08/28/2017 02:55 WG1012952
Zinc 24.6 6.01 1 08/28/2017 02:55 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0601 1 08/27/2017 18:45 WG1011691
Acrylonitrile ND 0.0120 1 08/27/2017 18:45 WG1011691
Benzene ND 0.00120 1 08/27/2017 18:45 WG1011691
Bromochloromethane ND 0.00120 1 08/27/2017 18:45 WG1011691
Bromodichloromethane ND 0.00120 1 08/27/2017 18:45 WG1011691
Bromoform ND 0.00120 1 08/27/2017 18:45 WG1011691
Bromomethane ND 0.00601 1 08/27/2017 18:45 WG1011691
Carbon disulfide ND 0.00120 1 08/27/2017 18:45 WG1011691
Carbon tetrachloride ND 0.00120 1 08/27/2017 18:45 WG1011691
Chlorobenzene ND 0.00120 1 08/27/2017 18:45 WG1011691
Chlorodibromomethane ND 0.00120 1 08/27/2017 18:45 WG1011691
Chloroethane ND 0.00601 1 08/27/2017 18:45 WG1011691
Chloroform ND 0.00601 1 08/27/2017 18:45 WG1011691
Chloromethane ND 0.00300 1 08/27/2017 18:45 WG1011691
Dibromomethane ND 0.00120 1 08/27/2017 18:45 WG1011691
1,2-Dichlorobenzene ND 0.00120 1 08/27/2017 18:45 WG1011691
1,4-Dichlorobenzene ND 0.00120 1 08/27/2017 18:45 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00300 1 08/27/2017 18:45 WG1011691
1,1-Dichloroethane ND 0.00120 1 08/27/2017 18:45 WG1011691
1,2-Dichloroethane ND 0.00120 1 08/27/2017 18:45 WG1011691
1,1-Dichloroethene ND 0.00120 1 08/27/2017 18:45 WG1011691
cis-1,2-Dichloroethene ND 0.00120 1 08/27/2017 18:45 WG1011691
trans-1,2-Dichloroethene ND 0.00120 1 08/27/2017 18:45 WG1011691
1,2-Dichloropropane ND 0.00120 1 08/27/2017 18:45 WG1011691
cis-1,3-Dichloropropene ND 0.00120 1 08/27/2017 18:45 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L930565
SS-7
Collected date/time: 08/14/17 11:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00120 1 08/27/2017 18:45 WG1011691
Ethylbenzene ND 0.00120 1 08/27/2017 18:45 WG1011691
2-Hexanone ND 0.0120 1 08/27/2017 18:45 WG1011691
Iodomethane ND 0.0120 1 08/27/2017 18:45 WG1011691
2-Butanone (MEK)ND 0.0120 1 08/27/2017 18:45 WG1011691
Methylene Chloride ND 0.00601 1 08/27/2017 18:45 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0120 1 08/27/2017 18:45 WG1011691
Styrene ND 0.00120 1 08/27/2017 18:45 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00120 1 08/27/2017 18:45 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00120 1 08/27/2017 18:45 WG1011691
Tetrachloroethene ND 0.00120 1 08/27/2017 18:45 WG1011691
Toluene ND 0.00601 1 08/27/2017 18:45 WG1011691
1,1,1-Trichloroethane ND 0.00120 1 08/27/2017 18:45 WG1011691
1,1,2-Trichloroethane ND 0.00120 1 08/27/2017 18:45 WG1011691
Trichloroethene ND 0.00120 1 08/27/2017 18:45 WG1011691
Trichlorofluoromethane ND 0.00601 1 08/27/2017 18:45 WG1011691
1,2,3-Trichloropropane ND 0.00300 1 08/27/2017 18:45 WG1011691
Vinyl acetate ND 0.0120 1 08/27/2017 18:45 WG1011691
Vinyl chloride ND 0.00120 1 08/27/2017 18:45 WG1011691
Xylenes, Total ND 0.00360 1 08/27/2017 18:45 WG1011691
(S) Toluene-d8 96.1 80.0-120 08/27/2017 18:45 WG1011691
(S) Dibromofluoromethane 105 74.0-131 08/27/2017 18:45 WG1011691
(S) a,a,a-Trifluorotoluene 99.1 80.0-120 08/27/2017 18:45 WG1011691
(S) 4-Bromofluorobenzene 102 64.0-132 08/27/2017 18:45 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L930565
SS-8
Collected date/time: 08/14/17 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.6 1 08/22/2017 14:21 WG1012140
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 0.0236 1 08/22/2017 10:12 WG1011876
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Antimony ND 2.36 1 08/28/2017 02:59 WG1012952
Arsenic ND 2.36 1 08/28/2017 02:59 WG1012952
Barium 5.86 0.591 1 08/28/2017 02:59 WG1012952
Beryllium ND 0.236 1 08/28/2017 02:59 WG1012952
Cadmium ND 0.591 1 08/28/2017 02:59 WG1012952
Chromium 6.10 1.18 1 08/28/2017 02:59 WG1012952
Cobalt ND 1.18 1 08/28/2017 02:59 WG1012952
Copper ND 2.36 1 08/28/2017 02:59 WG1012952
Lead 1.87 0.591 1 08/28/2017 02:59 WG1012952
Nickel ND 2.36 1 08/28/2017 02:59 WG1012952
Selenium ND 2.36 1 08/28/2017 02:59 WG1012952
Silver ND 1.18 1 08/28/2017 02:59 WG1012952
Thallium ND 2.36 1 08/28/2017 02:59 WG1012952
Vanadium 9.56 2.36 1 08/28/2017 02:59 WG1012952
Zinc 6.65 B 5.91 1 08/28/2017 02:59 WG1012952
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0591 1 08/22/2017 18:43 WG1011691
Acrylonitrile ND 0.0118 1 08/22/2017 18:43 WG1011691
Benzene ND 0.00118 1 08/22/2017 18:43 WG1011691
Bromochloromethane ND 0.00118 1 08/22/2017 18:43 WG1011691
Bromodichloromethane ND 0.00118 1 08/22/2017 18:43 WG1011691
Bromoform ND 0.00118 1 08/22/2017 18:43 WG1011691
Bromomethane ND 0.00591 1 08/22/2017 18:43 WG1011691
Carbon disulfide ND 0.00118 1 08/22/2017 18:43 WG1011691
Carbon tetrachloride ND 0.00118 1 08/22/2017 18:43 WG1011691
Chlorobenzene ND 0.00118 1 08/22/2017 18:43 WG1011691
Chlorodibromomethane ND 0.00118 1 08/22/2017 18:43 WG1011691
Chloroethane ND 0.00591 1 08/22/2017 18:43 WG1011691
Chloroform ND 0.00591 1 08/22/2017 18:43 WG1011691
Chloromethane ND 0.00296 1 08/22/2017 18:43 WG1011691
Dibromomethane ND 0.00118 1 08/22/2017 18:43 WG1011691
1,2-Dichlorobenzene ND 0.00118 1 08/22/2017 18:43 WG1011691
1,4-Dichlorobenzene ND 0.00118 1 08/22/2017 18:43 WG1011691
trans-1,4-Dichloro-2-butene ND 0.00296 1 08/22/2017 18:43 WG1011691
1,1-Dichloroethane ND 0.00118 1 08/22/2017 18:43 WG1011691
1,2-Dichloroethane ND 0.00118 1 08/22/2017 18:43 WG1011691
1,1-Dichloroethene ND 0.00118 1 08/22/2017 18:43 WG1011691
cis-1,2-Dichloroethene ND 0.00118 1 08/22/2017 18:43 WG1011691
trans-1,2-Dichloroethene ND 0.00118 1 08/22/2017 18:43 WG1011691
1,2-Dichloropropane ND 0.00118 1 08/22/2017 18:43 WG1011691
cis-1,3-Dichloropropene ND 0.00118 1 08/22/2017 18:43 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 29 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L930565
SS-8
Collected date/time: 08/14/17 11:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
trans-1,3-Dichloropropene ND 0.00118 1 08/22/2017 18:43 WG1011691
Ethylbenzene ND 0.00118 1 08/22/2017 18:43 WG1011691
2-Hexanone ND 0.0118 1 08/22/2017 18:43 WG1011691
Iodomethane ND 0.0118 1 08/22/2017 18:43 WG1011691
2-Butanone (MEK)ND 0.0118 1 08/22/2017 18:43 WG1011691
Methylene Chloride ND 0.00591 1 08/22/2017 18:43 WG1011691
4-Methyl-2-pentanone (MIBK)ND 0.0118 1 08/22/2017 18:43 WG1011691
Styrene ND 0.00118 1 08/22/2017 18:43 WG1011691
1,1,1,2-Tetrachloroethane ND 0.00118 1 08/22/2017 18:43 WG1011691
1,1,2,2-Tetrachloroethane ND 0.00118 1 08/22/2017 18:43 WG1011691
Tetrachloroethene ND 0.00118 1 08/22/2017 18:43 WG1011691
Toluene ND 0.00591 1 08/22/2017 18:43 WG1011691
1,1,1-Trichloroethane ND 0.00118 1 08/22/2017 18:43 WG1011691
1,1,2-Trichloroethane ND 0.00118 1 08/22/2017 18:43 WG1011691
Trichloroethene ND 0.00118 1 08/22/2017 18:43 WG1011691
Trichlorofluoromethane ND 0.00591 1 08/22/2017 18:43 WG1011691
1,2,3-Trichloropropane ND 0.00296 1 08/22/2017 18:43 WG1011691
Vinyl acetate ND 0.0118 1 08/22/2017 18:43 WG1011691
Vinyl chloride ND 0.00118 1 08/22/2017 18:43 WG1011691
Xylenes, Total ND 0.00355 1 08/22/2017 18:43 WG1011691
(S) Toluene-d8 114 80.0-120 08/22/2017 18:43 WG1011691
(S) Dibromofluoromethane 102 74.0-131 08/22/2017 18:43 WG1011691
(S) a,a,a-Trifluorotoluene 98.0 80.0-120 08/22/2017 18:43 WG1011691
(S) 4-Bromofluorobenzene 111 64.0-132 08/22/2017 18:43 WG1011691
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L930565
SW-A
Collected date/time: 08/14/17 12:15
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 08/23/2017 12:50 WG1012561
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Arsenic ND 0.0100 1 08/25/2017 17:07 WG1013097
Barium 0.0451 0.00500 1 08/25/2017 17:07 WG1013097
Chromium ND 0.0100 1 08/25/2017 17:07 WG1013097
Cobalt ND 0.0100 1 08/25/2017 17:07 WG1013097
Nickel ND 0.0100 1 08/25/2017 17:07 WG1013097
Silver ND 0.00500 1 08/25/2017 17:07 WG1013097
Vanadium ND 0.0200 1 08/25/2017 17:07 WG1013097
Metals (ICPMS) by Method 6020B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 08/24/2017 19:51 WG1012187
Beryllium ND 0.00200 1 08/24/2017 19:51 WG1012187
Cadmium ND 0.00100 1 08/24/2017 19:51 WG1012187
Copper ND 0.00500 1 08/24/2017 19:51 WG1012187
Lead ND 0.00200 1 08/24/2017 19:51 WG1012187
Selenium ND 0.00200 1 08/24/2017 19:51 WG1012187
Thallium ND 0.00200 1 08/24/2017 19:51 WG1012187
Zinc 0.0256 0.0250 1 08/24/2017 19:51 WG1012187
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 08/20/2017 22:29 WG1011888
Acrylonitrile ND 0.0100 1 08/20/2017 22:29 WG1011888
Benzene ND 0.00100 1 08/20/2017 22:29 WG1011888
Bromochloromethane ND 0.00100 1 08/20/2017 22:29 WG1011888
Bromodichloromethane ND 0.00100 1 08/20/2017 22:29 WG1011888
Bromoform ND 0.00100 1 08/20/2017 22:29 WG1011888
Bromomethane ND 0.00500 1 08/20/2017 22:29 WG1011888
Carbon disulfide ND 0.00100 1 08/20/2017 22:29 WG1011888
Carbon tetrachloride ND 0.00100 1 08/20/2017 22:29 WG1011888
Chlorobenzene ND 0.00100 1 08/20/2017 22:29 WG1011888
Chlorodibromomethane ND 0.00100 1 08/20/2017 22:29 WG1011888
Chloroethane ND 0.00500 1 08/20/2017 22:29 WG1011888
Chloroform ND 0.00500 1 08/20/2017 22:29 WG1011888
Chloromethane ND 0.00250 1 08/20/2017 22:29 WG1011888
Dibromomethane ND 0.00100 1 08/20/2017 22:29 WG1011888
1,2-Dichlorobenzene ND 0.00100 1 08/20/2017 22:29 WG1011888
1,4-Dichlorobenzene ND 0.00100 1 08/20/2017 22:29 WG1011888
trans-1,4-Dichloro-2-butene ND 0.00250 1 08/20/2017 22:29 WG1011888
1,1-Dichloroethane ND 0.00100 1 08/20/2017 22:29 WG1011888
1,2-Dichloroethane ND 0.00100 1 08/20/2017 22:29 WG1011888
1,1-Dichloroethene ND 0.00100 1 08/20/2017 22:29 WG1011888
cis-1,2-Dichloroethene ND 0.00100 1 08/20/2017 22:29 WG1011888
trans-1,2-Dichloroethene ND 0.00100 1 08/20/2017 22:29 WG1011888
1,2-Dichloropropane ND 0.00100 1 08/20/2017 22:29 WG1011888
cis-1,3-Dichloropropene ND 0.00100 1 08/20/2017 22:29 WG1011888
trans-1,3-Dichloropropene ND 0.00100 1 08/20/2017 22:29 WG1011888
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L930565
SW-A
Collected date/time: 08/14/17 12:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ethylbenzene ND 0.00100 1 08/20/2017 22:29 WG1011888
2-Hexanone ND 0.0100 1 08/20/2017 22:29 WG1011888
Iodomethane ND J3 0.0100 1 08/20/2017 22:29 WG1011888
2-Butanone (MEK)ND 0.0100 1 08/20/2017 22:29 WG1011888
Methylene Chloride ND 0.00500 1 08/20/2017 22:29 WG1011888
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 08/20/2017 22:29 WG1011888
Styrene ND 0.00100 1 08/20/2017 22:29 WG1011888
1,1,1,2-Tetrachloroethane ND 0.00100 1 08/20/2017 22:29 WG1011888
1,1,2,2-Tetrachloroethane ND 0.00100 1 08/20/2017 22:29 WG1011888
Tetrachloroethene ND 0.00100 1 08/20/2017 22:29 WG1011888
Toluene ND 0.00100 1 08/20/2017 22:29 WG1011888
1,1,1-Trichloroethane ND 0.00100 1 08/20/2017 22:29 WG1011888
1,1,2-Trichloroethane ND 0.00100 1 08/20/2017 22:29 WG1011888
Trichloroethene ND 0.00100 1 08/20/2017 22:29 WG1011888
Trichlorofluoromethane ND 0.00500 1 08/20/2017 22:29 WG1011888
1,2,3-Trichloropropane ND 0.00250 1 08/20/2017 22:29 WG1011888
Vinyl acetate ND 0.0100 1 08/20/2017 22:29 WG1011888
Vinyl chloride ND 0.00100 1 08/20/2017 22:29 WG1011888
Xylenes, Total ND 0.00300 1 08/20/2017 22:29 WG1011888
(S) Toluene-d8 114 80.0-120 08/20/2017 22:29 WG1011888
(S) Dibromofluoromethane 102 76.0-123 08/20/2017 22:29 WG1011888
(S) a,a,a-Trifluorotoluene 106 80.0-120 08/20/2017 22:29 WG1011888
(S) 4-Bromofluorobenzene 103 80.0-120 08/20/2017 22:29 WG1011888
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 32 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L930565
MW-17R
Collected date/time: 08/14/17 14:10
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 08/22/2017 00:00 WG1011867
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Arsenic ND 0.0100 1 08/25/2017 17:10 WG1013097
Barium 0.113 0.00500 1 08/25/2017 17:10 WG1013097
Chromium ND 0.0100 1 08/25/2017 17:10 WG1013097
Cobalt 0.0273 0.0100 1 08/25/2017 17:10 WG1013097
Nickel ND 0.0100 1 08/25/2017 17:10 WG1013097
Silver ND 0.00500 1 08/25/2017 17:10 WG1013097
Vanadium ND 0.0200 1 08/25/2017 17:10 WG1013097
Metals (ICPMS) by Method 6020B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 08/24/2017 18:55 WG1012187
Beryllium ND 0.00200 1 08/24/2017 18:55 WG1012187
Cadmium ND 0.00100 1 08/24/2017 18:55 WG1012187
Copper ND 0.00500 1 08/24/2017 18:55 WG1012187
Lead ND 0.00200 1 08/24/2017 18:55 WG1012187
Selenium ND 0.00200 1 08/24/2017 18:55 WG1012187
Thallium ND 0.00200 1 08/24/2017 18:55 WG1012187
Zinc ND 0.0250 1 08/24/2017 18:55 WG1012187
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 08/20/2017 22:51 WG1011888
Acrylonitrile ND 0.0100 1 08/20/2017 22:51 WG1011888
Benzene ND 0.00100 1 08/20/2017 22:51 WG1011888
Bromochloromethane ND 0.00100 1 08/20/2017 22:51 WG1011888
Bromodichloromethane ND 0.00100 1 08/20/2017 22:51 WG1011888
Bromoform ND 0.00100 1 08/20/2017 22:51 WG1011888
Bromomethane ND 0.00500 1 08/20/2017 22:51 WG1011888
Carbon disulfide ND 0.00100 1 08/20/2017 22:51 WG1011888
Carbon tetrachloride ND 0.00100 1 08/20/2017 22:51 WG1011888
Chlorobenzene ND 0.00100 1 08/20/2017 22:51 WG1011888
Chlorodibromomethane ND 0.00100 1 08/20/2017 22:51 WG1011888
Chloroethane ND 0.00500 1 08/20/2017 22:51 WG1011888
Chloroform ND 0.00500 1 08/20/2017 22:51 WG1011888
Chloromethane ND 0.00250 1 08/20/2017 22:51 WG1011888
Dibromomethane ND 0.00100 1 08/20/2017 22:51 WG1011888
1,2-Dichlorobenzene ND 0.00100 1 08/20/2017 22:51 WG1011888
1,4-Dichlorobenzene ND 0.00100 1 08/20/2017 22:51 WG1011888
trans-1,4-Dichloro-2-butene ND 0.00250 1 08/20/2017 22:51 WG1011888
1,1-Dichloroethane ND 0.00100 1 08/20/2017 22:51 WG1011888
1,2-Dichloroethane ND 0.00100 1 08/20/2017 22:51 WG1011888
1,1-Dichloroethene ND 0.00100 1 08/20/2017 22:51 WG1011888
cis-1,2-Dichloroethene ND 0.00100 1 08/20/2017 22:51 WG1011888
trans-1,2-Dichloroethene ND 0.00100 1 08/20/2017 22:51 WG1011888
1,2-Dichloropropane ND 0.00100 1 08/20/2017 22:51 WG1011888
cis-1,3-Dichloropropene ND 0.00100 1 08/20/2017 22:51 WG1011888
trans-1,3-Dichloropropene ND 0.00100 1 08/20/2017 22:51 WG1011888
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 17-0801245 L930565 08/28/17 15:06 33 of 65
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L930565
MW-17R
Collected date/time: 08/14/17 14:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ethylbenzene ND 0.00100 1 08/20/2017 22:51 WG1011888
2-Hexanone ND 0.0100 1 08/20/2017 22:51 WG1011888
Iodomethane ND J3 0.0100 1 08/20/2017 22:51 WG1011888
2-Butanone (MEK)ND 0.0100 1 08/20/2017 22:51 WG1011888
Methylene Chloride ND 0.00500 1 08/20/2017 22:51 WG1011888
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 08/20/2017 22:51 WG1011888
Styrene ND 0.00100 1 08/20/2017 22:51 WG1011888
1,1,1,2-Tetrachloroethane ND 0.00100 1 08/20/2017 22:51 WG1011888
1,1,2,2-Tetrachloroethane ND 0.00100 1 08/20/2017 22:51 WG1011888
Tetrachloroethene ND 0.00100 1 08/20/2017 22:51 WG1011888
Toluene ND 0.00100 1 08/20/2017 22:51 WG1011888
1,1,1-Trichloroethane ND 0.00100 1 08/20/2017 22:51 WG1011888
1,1,2-Trichloroethane ND 0.00100 1 08/20/2017 22:51 WG1011888
Trichloroethene ND 0.00100 1 08/20/2017 22:51 WG1011888
Trichlorofluoromethane ND 0.00500 1 08/20/2017 22:51 WG1011888
1,2,3-Trichloropropane ND 0.00250 1 08/20/2017 22:51 WG1011888
Vinyl acetate ND 0.0100 1 08/20/2017 22:51 WG1011888
Vinyl chloride ND 0.00100 1 08/20/2017 22:51 WG1011888
Xylenes, Total 0.00515 0.00300 1 08/20/2017 22:51 WG1011888
(S) Toluene-d8 114 80.0-120 08/20/2017 22:51 WG1011888
(S) Dibromofluoromethane 102 76.0-123 08/20/2017 22:51 WG1011888
(S) a,a,a-Trifluorotoluene 105 80.0-120 08/20/2017 22:51 WG1011888
(S) 4-Bromofluorobenzene 103 80.0-120 08/20/2017 22:51 WG1011888
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L930565
SB-1-GW
Collected date/time: 08/14/17 13:05
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Mercury ND 0.000200 1 08/23/2017 12:53 WG1012561
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Arsenic 0.0174 0.0100 1 08/25/2017 17:14 WG1013097
Barium 0.282 0.00500 1 08/25/2017 17:14 WG1013097
Chromium 0.0341 0.0100 1 08/25/2017 17:14 WG1013097
Cobalt 0.0106 0.0100 1 08/25/2017 17:14 WG1013097
Nickel 0.0543 0.0100 1 08/25/2017 17:14 WG1013097
Silver ND 0.00500 1 08/25/2017 17:14 WG1013097
Vanadium 0.0560 0.0200 1 08/25/2017 17:14 WG1013097
Metals (ICPMS) by Method 6020B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 08/26/2017 11:51 WG1013102
Beryllium ND 0.00200 1 08/28/2017 12:24 WG1013541
Cadmium ND 0.00100 1 08/26/2017 11:51 WG1013102
Copper 0.0195 0.00500 1 08/26/2017 11:51 WG1013102
Lead 0.0154 0.00200 1 08/26/2017 11:51 WG1013102
Selenium 0.00382 0.00200 1 08/26/2017 11:51 WG1013102
Thallium ND 0.00200 1 08/26/2017 11:51 WG1013102
Zinc 0.0271 0.0250 1 08/26/2017 11:51 WG1013102
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 0.0500 1 08/23/2017 12:12 WG1012744
Acrylonitrile ND 0.0100 1 08/23/2017 12:12 WG1012744
Benzene ND 0.00100 1 08/23/2017 12:12 WG1012744
Bromochloromethane ND 0.00100 1 08/23/2017 12:12 WG1012744
Bromodichloromethane ND 0.00100 1 08/23/2017 12:12 WG1012744
Bromoform ND 0.00100 1 08/23/2017 12:12 WG1012744
Bromomethane ND 0.00500 1 08/23/2017 12:12 WG1012744
Carbon disulfide ND 0.00100 1 08/23/2017 12:12 WG1012744
Carbon tetrachloride ND J4 0.00100 1 08/23/2017 12:12 WG1012744
Chlorobenzene ND 0.00100 1 08/23/2017 12:12 WG1012744
Chlorodibromomethane ND 0.00100 1 08/23/2017 12:12 WG1012744
Chloroethane ND 0.00500 1 08/23/2017 12:12 WG1012744
Chloroform ND 0.00500 1 08/23/2017 12:12 WG1012744
Chloromethane ND 0.00250 1 08/23/2017 12:12 WG1012744
Dibromomethane ND 0.00100 1 08/23/2017 12:12 WG1012744
1,2-Dichlorobenzene ND 0.00100 1 08/23/2017 12:12 WG1012744
1,4-Dichlorobenzene ND 0.00100 1 08/23/2017 12:12 WG1012744
trans-1,4-Dichloro-2-butene ND 0.00250 1 08/23/2017 12:12 WG1012744
1,1-Dichloroethane ND 0.00100 1 08/23/2017 12:12 WG1012744
1,2-Dichloroethane ND 0.00100 1 08/23/2017 12:12 WG1012744
1,1-Dichloroethene ND 0.00100 1 08/23/2017 12:12 WG1012744
cis-1,2-Dichloroethene ND 0.00100 1 08/23/2017 12:12 WG1012744
trans-1,2-Dichloroethene ND 0.00100 1 08/23/2017 12:12 WG1012744
1,2-Dichloropropane ND 0.00100 1 08/23/2017 12:12 WG1012744
cis-1,3-Dichloropropene ND 0.00100 1 08/23/2017 12:12 WG1012744
trans-1,3-Dichloropropene ND 0.00100 1 08/23/2017 12:12 WG1012744
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L930565
SB-1-GW
Collected date/time: 08/14/17 13:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Ethylbenzene 0.00238 0.00100 1 08/23/2017 12:12 WG1012744
2-Hexanone ND 0.0100 1 08/23/2017 12:12 WG1012744
Iodomethane ND J3 J4 0.0100 1 08/23/2017 12:12 WG1012744
2-Butanone (MEK)ND 0.0100 1 08/23/2017 12:12 WG1012744
Methylene Chloride ND 0.00500 1 08/23/2017 12:12 WG1012744
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 08/23/2017 12:12 WG1012744
Styrene ND 0.00100 1 08/23/2017 12:12 WG1012744
1,1,1,2-Tetrachloroethane ND 0.00100 1 08/23/2017 12:12 WG1012744
1,1,2,2-Tetrachloroethane ND 0.00100 1 08/23/2017 12:12 WG1012744
Tetrachloroethene ND 0.00100 1 08/23/2017 12:12 WG1012744
Toluene 0.0264 0.00100 1 08/23/2017 12:12 WG1012744
1,1,1-Trichloroethane ND 0.00100 1 08/23/2017 12:12 WG1012744
1,1,2-Trichloroethane ND 0.00100 1 08/23/2017 12:12 WG1012744
Trichloroethene ND 0.00100 1 08/23/2017 12:12 WG1012744
Trichlorofluoromethane ND 0.00500 1 08/23/2017 12:12 WG1012744
1,2,3-Trichloropropane ND 0.00250 1 08/23/2017 12:12 WG1012744
Vinyl acetate ND 0.0100 1 08/23/2017 12:12 WG1012744
Vinyl chloride ND 0.00100 1 08/23/2017 12:12 WG1012744
Xylenes, Total 0.0191 0.00300 1 08/23/2017 12:12 WG1012744
(S) Toluene-d8 103 80.0-120 08/23/2017 12:12 WG1012744
(S) Dibromofluoromethane 110 76.0-123 08/23/2017 12:12 WG1012744
(S) a,a,a-Trifluorotoluene 107 80.0-120 08/23/2017 12:12 WG1012744
(S) 4-Bromofluorobenzene 105 80.0-120 08/23/2017 12:12 WG1012744
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L930565
EQUIPMENT BLANK
Collected date/time: 08/14/17 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 0.0500 1 08/23/2017 11:53 WG1012744
Acrylonitrile ND 0.0100 1 08/23/2017 11:53 WG1012744
Benzene ND 0.00100 1 08/23/2017 11:53 WG1012744
Bromochloromethane ND 0.00100 1 08/23/2017 11:53 WG1012744
Bromodichloromethane ND 0.00100 1 08/23/2017 11:53 WG1012744
Bromoform ND 0.00100 1 08/23/2017 11:53 WG1012744
Bromomethane ND 0.00500 1 08/23/2017 11:53 WG1012744
Carbon disulfide ND 0.00100 1 08/23/2017 11:53 WG1012744
Carbon tetrachloride ND J4 0.00100 1 08/23/2017 11:53 WG1012744
Chlorobenzene ND 0.00100 1 08/23/2017 11:53 WG1012744
Chlorodibromomethane ND 0.00100 1 08/23/2017 11:53 WG1012744
Chloroethane ND 0.00500 1 08/23/2017 11:53 WG1012744
Chloroform ND 0.00500 1 08/23/2017 11:53 WG1012744
Chloromethane ND 0.00250 1 08/23/2017 11:53 WG1012744
Dibromomethane ND 0.00100 1 08/23/2017 11:53 WG1012744
1,2-Dichlorobenzene ND 0.00100 1 08/23/2017 11:53 WG1012744
1,4-Dichlorobenzene ND 0.00100 1 08/23/2017 11:53 WG1012744
trans-1,4-Dichloro-2-butene ND 0.00250 1 08/23/2017 11:53 WG1012744
1,1-Dichloroethane ND 0.00100 1 08/23/2017 11:53 WG1012744
1,2-Dichloroethane ND 0.00100 1 08/23/2017 11:53 WG1012744
1,1-Dichloroethene ND 0.00100 1 08/23/2017 11:53 WG1012744
cis-1,2-Dichloroethene ND 0.00100 1 08/23/2017 11:53 WG1012744
trans-1,2-Dichloroethene ND 0.00100 1 08/23/2017 11:53 WG1012744
1,2-Dichloropropane ND 0.00100 1 08/23/2017 11:53 WG1012744
cis-1,3-Dichloropropene ND 0.00100 1 08/23/2017 11:53 WG1012744
trans-1,3-Dichloropropene ND 0.00100 1 08/23/2017 11:53 WG1012744
Ethylbenzene ND 0.00100 1 08/23/2017 11:53 WG1012744
2-Hexanone ND 0.0100 1 08/23/2017 11:53 WG1012744
Iodomethane ND J3 J4 0.0100 1 08/23/2017 11:53 WG1012744
2-Butanone (MEK)ND 0.0100 1 08/23/2017 11:53 WG1012744
Methylene Chloride ND 0.00500 1 08/23/2017 11:53 WG1012744
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 08/23/2017 11:53 WG1012744
Styrene ND 0.00100 1 08/23/2017 11:53 WG1012744
1,1,1,2-Tetrachloroethane ND 0.00100 1 08/23/2017 11:53 WG1012744
1,1,2,2-Tetrachloroethane ND 0.00100 1 08/23/2017 11:53 WG1012744
Tetrachloroethene ND 0.00100 1 08/23/2017 11:53 WG1012744
Toluene ND 0.00100 1 08/23/2017 11:53 WG1012744
1,1,1-Trichloroethane ND 0.00100 1 08/23/2017 11:53 WG1012744
1,1,2-Trichloroethane ND 0.00100 1 08/23/2017 11:53 WG1012744
Trichloroethene ND 0.00100 1 08/23/2017 11:53 WG1012744
Trichlorofluoromethane ND 0.00500 1 08/23/2017 11:53 WG1012744
1,2,3-Trichloropropane ND 0.00250 1 08/23/2017 11:53 WG1012744
Vinyl acetate ND 0.0100 1 08/23/2017 11:53 WG1012744
Vinyl chloride ND 0.00100 1 08/23/2017 11:53 WG1012744
Xylenes, Total ND 0.00300 1 08/23/2017 11:53 WG1012744
(S) Toluene-d8 103 80.0-120 08/23/2017 11:53 WG1012744
(S) Dibromofluoromethane 108 76.0-123 08/23/2017 11:53 WG1012744
(S) a,a,a-Trifluorotoluene 107 80.0-120 08/23/2017 11:53 WG1012744
(S) 4-Bromofluorobenzene 107 80.0-120 08/23/2017 11:53 WG1012744
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012140
Total Solids by Method 2540 G-2011 L930565-01,07,08,09,10,11,12
Method Blank (MB)
(MB) R3243541-1 08/22/17 14:21
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000600
L930565-01 Original Sample (OS) • Duplicate (DUP)
(OS) L930565-01 08/22/17 14:21 • (DUP) R3243541-3 08/22/17 14:21
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 85.4 84.2 1 1.44 5
Laboratory Control Sample (LCS)
(LCS) R3243541-2 08/22/17 14:21
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012670
Total Solids by Method 2540 G-2011 L930565-02,03,04
Method Blank (MB)
(MB) R3243960-1 08/23/17 11:01
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000100
L930565-02 Original Sample (OS) • Duplicate (DUP)
(OS) L930565-02 08/23/17 11:01 • (DUP) R3243960-3 08/23/17 11:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 89.1 86.9 1 2.53 5
Laboratory Control Sample (LCS)
(LCS) R3243960-2 08/23/17 11:01
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012743
Total Solids by Method 2540 G-2011 L930565-05,06
Method Blank (MB)
(MB) R3244367-1 08/24/17 13:07
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000500
L930544-08 Original Sample (OS) • Duplicate (DUP)
(OS) L930544-08 08/24/17 13:07 • (DUP) R3244367-3 08/24/17 13:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 77.9 76.2 1 2.22 5
Laboratory Control Sample (LCS)
(LCS) R3244367-2 08/24/17 13:07
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011867
Mercury by Method 7470A L930565-14
Method Blank (MB)
(MB) R3243110-1 08/21/17 23:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000049 0.000200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243110-2 08/21/17 23:35 • (LCSD) R3243110-3 08/21/17 23:38
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Mercury 0.00300 0.00250 0.00244 83 81 80-120 2 20
L930492-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930492-01 08/22/17 00:28 • (MS) R3243110-6 08/22/17 00:31 • (MSD) R3243110-7 08/22/17 00:33
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.0000300 0.788 0.750 0.710 0 0 100 75-125 V V 5 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012561
Mercury by Method 7470A L930565-13,15
Method Blank (MB)
(MB) R3243716-1 08/23/17 12:15
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.000049 0.000200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243716-2 08/23/17 12:17 • (LCSD) R3243716-3 08/23/17 12:20
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Mercury 0.00300 0.00288 0.00314 96 105 80-120 8 20
L930855-33 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930855-33 08/23/17 12:22 • (MS) R3243716-4 08/23/17 12:24 • (MSD) R3243716-5 08/23/17 12:26
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.00300 U 0.00295 0.00312 98 104 1 75-125 5 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011876
Mercury by Method 7471B L930565-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3243310-1 08/22/17 09:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243310-2 08/22/17 09:24 • (LCSD) R3243310-3 08/22/17 09:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.259 0.263 86 88 80-120 2 20
L930565-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930565-01 08/22/17 09:29 • (MS) R3243310-4 08/22/17 09:31 • (MSD) R3243310-5 08/22/17 09:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.351 ND 0.314 0.339 83 91 1 75-125 8 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012952
Metals (ICP) by Method 6010D L930565-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3244837-1 08/28/17 01:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.75 2.00
Arsenic U 0.65 2.00
Barium U 0.17 0.500
Beryllium U 0.07 0.200
Cadmium U 0.07 0.500
Chromium U 0.14 1.00
Cobalt U 0.23 1.00
Copper U 0.53 2.00
Lead U 0.19 0.500
Nickel U 0.49 2.00
Selenium U 0.74 2.00
Silver U 0.28 1.00
Thallium U 0.65 2.00
Vanadium U 0.24 2.00
Zinc 1.8 J 0.59 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244837-2 08/28/17 01:57 • (LCSD) R3244837-3 08/28/17 02:00
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Antimony 100 102 102 102 102 80-120 0 20
Arsenic 100 101 101 101 101 80-120 1 20
Barium 100 109 109 109 109 80-120 1 20
Beryllium 100 105 108 105 108 80-120 2 20
Cadmium 100 102 102 102 102 80-120 1 20
Chromium 100 102 104 102 104 80-120 2 20
Cobalt 100 106 106 106 106 80-120 0 20
Copper 100 104 105 104 105 80-120 1 20
Lead 100 103 103 103 103 80-120 1 20
Nickel 100 104 104 104 104 80-120 1 20
Selenium 100 101 102 101 102 80-120 1 20
Silver 20.0 19.4 19.6 97 98 80-120 1 20
Thallium 100 106 107 106 107 80-120 1 20
Vanadium 100 105 107 105 107 80-120 1 20
Zinc 100 103 103 103 103 80-120 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012952
Metals (ICP) by Method 6010D L930565-01,02,03,04,05,06,07,08,09,10,11,12
L930565-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930565-01 08/28/17 02:03 • (MS) R3244837-6 08/28/17 02:13 • (MSD) R3244837-7 08/28/17 02:16
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 117 ND 57.2 57.3 49 49 1 75-125 J6 J6 0 20
Arsenic 117 ND 115 110 96 92 1 75-125 4 20
Barium 117 21.2 152 144 112 105 1 75-125 5 20
Beryllium 117 0.268 129 125 110 106 1 75-125 3 20
Cadmium 117 ND 119 114 102 98 1 75-125 4 20
Chromium 117 17.8 143 139 107 104 1 75-125 2 20
Cobalt 117 ND 128 123 108 104 1 75-125 4 20
Copper 117 3.33 131 127 109 105 1 75-125 3 20
Lead 117 5.76 129 124 105 101 1 75-125 4 20
Nickel 117 4.37 131 126 108 104 1 75-125 4 20
Selenium 117 ND 114 110 98 94 1 75-125 4 20
Silver 23.4 ND 23.1 22.6 99 96 1 75-125 2 20
Thallium 117 ND 125 121 107 103 1 75-125 4 20
Vanadium 117 34.5 163 162 110 108 1 75-125 1 20
Zinc 117 7.95 129 123 103 98 1 75-125 5 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1013097
Metals (ICP) by Method 6010D L930565-13,14,15
Method Blank (MB)
(MB) R3244791-1 08/25/17 16:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Arsenic U 0.0065 0.0100
Barium U 0.0017 0.00500
Chromium U 0.0014 0.0100
Cobalt U 0.0023 0.0100
Nickel U 0.0049 0.0100
Silver U 0.0028 0.00500
Vanadium U 0.0024 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244791-2 08/25/17 16:47 • (LCSD) R3244791-3 08/25/17 16:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Arsenic 1.00 0.992 0.995 99 100 80-120 0 20
Barium 1.00 1.03 1.03 103 103 80-120 1 20
Chromium 1.00 1.00 1.01 100 101 80-120 1 20
Cobalt 1.00 1.01 1.02 101 102 80-120 1 20
Nickel 1.00 0.998 1.00 100 100 80-120 1 20
Silver 0.200 0.187 0.187 93 93 80-120 0 20
Vanadium 1.00 0.971 0.977 97 98 80-120 1 20
L930627-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930627-09 08/25/17 16:54 • (MS) R3244791-5 08/25/17 17:00 • (MSD) R3244791-6 08/25/17 17:03
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 1.00 ND 1.00 1.02 100 101 1 75-125 2 20
Barium 1.00 0.0962 1.12 1.13 102 103 1 75-125 1 20
Chromium 1.00 ND 0.997 1.02 100 102 1 75-125 2 20
Cobalt 1.00 ND 1.01 1.02 101 102 1 75-125 1 20
Nickel 1.00 ND 0.992 0.997 99 100 1 75-125 1 20
Silver 0.200 ND 0.188 0.191 94 95 1 75-125 1 20
Vanadium 1.00 ND 0.981 0.994 98 99 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012187
Metals (ICPMS) by Method 6020B L930565-13,14
Method Blank (MB)
(MB) R3244384-7 08/24/17 18:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00200
Beryllium U 0.00012 0.00200
Cadmium U 0.00016 0.00100
Copper U 0.00052 0.00500
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc U 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244384-8 08/24/17 18:48 • (LCSD) R3244384-9 08/24/17 18:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0500 0.0504 0.0502 101 100 80-120 1 20
Beryllium 0.0500 0.0427 0.0416 85 83 80-120 3 20
Cadmium 0.0500 0.0507 0.0520 101 104 80-120 2 20
Copper 0.0500 0.0485 0.0483 97 97 80-120 0 20
Lead 0.0500 0.0448 0.0447 90 89 80-120 0 20
Selenium 0.0500 0.0472 0.0464 94 93 80-120 2 20
Thallium 0.0500 0.0461 0.0461 92 92 80-120 0 20
Zinc 0.0500 0.0506 0.0505 101 101 80-120 0 20
L930565-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930565-14 08/24/17 18:55 • (MS) R3244384-11 08/24/17 19:02 • (MSD) R3244384-12 08/24/17 19:06
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0500 ND 0.0504 0.0502 101 100 1 75-125 0 20
Beryllium 0.0500 ND 0.0411 0.0418 82 83 1 75-125 2 20
Cadmium 0.0500 ND 0.0504 0.0514 101 103 1 75-125 2 20
Copper 0.0500 ND 0.0469 0.0471 92 92 1 75-125 1 20
Lead 0.0500 ND 0.0465 0.0464 90 89 1 75-125 0 20
Selenium 0.0500 ND 0.0472 0.0482 93 96 1 75-125 2 20
Thallium 0.0500 ND 0.0461 0.0464 92 93 1 75-125 1 20
Zinc 0.0500 ND 0.0519 0.0500 99 95 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1013102
Metals (ICPMS) by Method 6020B L930565-15
Method Blank (MB)
(MB) R3244703-1 08/26/17 11:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00200
Cadmium U 0.00016 0.00100
Copper U 0.00052 0.00500
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc U 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244703-2 08/26/17 11:44 • (LCSD) R3244703-3 08/26/17 11:48
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0500 0.0460 0.0455 92 91 80-120 1 20
Cadmium 0.0500 0.0543 0.0533 109 107 80-120 2 20
Copper 0.0500 0.0474 0.0462 95 92 80-120 3 20
Lead 0.0500 0.0477 0.0465 95 93 80-120 2 20
Selenium 0.0500 0.0492 0.0475 98 95 80-120 3 20
Thallium 0.0500 0.0493 0.0482 99 96 80-120 2 20
Zinc 0.0500 0.0474 0.0478 95 96 80-120 1 20
L930565-15 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930565-15 08/26/17 11:51 • (MS) R3244703-5 08/26/17 11:58 • (MSD) R3244703-6 08/26/17 12:02
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0500 ND 0.0430 0.0444 84 87 1 75-125 3 20
Cadmium 0.0500 ND 0.0528 0.0523 106 105 1 75-125 1 20
Copper 0.0500 0.0195 0.0615 0.0619 84 85 1 75-125 1 20
Lead 0.0500 0.0154 0.0636 0.0647 96 99 1 75-125 2 20
Selenium 0.0500 0.00382 0.0510 0.0529 94 98 1 75-125 4 20
Thallium 0.0500 ND 0.0494 0.0492 99 98 1 75-125 1 20
Zinc 0.0500 0.0271 0.0666 0.0697 79 85 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1013541
Metals (ICPMS) by Method 6020B L930565-15
Method Blank (MB)
(MB) R3244942-1 08/28/17 11:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Beryllium U 0.00012 0.00200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244942-2 08/28/17 11:29 • (LCSD) R3244942-3 08/28/17 11:33
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Beryllium 0.0500 0.0455 0.0419 91 84 80-120 8 20
L930476-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L930476-01 08/28/17 11:37 • (MS) R3244942-5 08/28/17 11:43 • (MSD) R3244942-6 08/28/17 11:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Beryllium 0.0500 ND 0.0439 0.0441 88 88 1 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011691
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3243408-3 08/22/17 12:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromochloromethane U 0.000390 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
Carbon disulfide U 0.000221 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
trans-1,4-Dichloro-2-butene U 0.000778 0.00250
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
Ethylbenzene U 0.000297 0.00100
2-Hexanone U 0.00137 0.0100
Iodomethane U 0.00253 0.0100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011691
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3243408-3 08/22/17 12:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
Vinyl acetate U 0.00239 0.0100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 118 80.0-120
(S) Dibromofluoromethane 99.1 74.0-131
(S) a,a,a-Trifluorotoluene 102 80.0-120
(S) 4-Bromofluorobenzene 105 64.0-132
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243408-1 08/22/17 11:27 • (LCSD) R3243408-2 08/22/17 11:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.0777 0.0829 62.2 66.3 11.0-160 6.45 23
Acrylonitrile 0.125 0.0872 0.0915 69.8 73.2 61.0-143 4.83 20
Benzene 0.0250 0.0218 0.0217 87.1 86.9 71.0-124 0.250 20
Bromodichloromethane 0.0250 0.0234 0.0236 93.6 94.5 75.0-120 0.960 20
Bromochloromethane 0.0250 0.0244 0.0251 97.6 100 80.0-121 2.89 20
Bromoform 0.0250 0.0249 0.0258 99.6 103 65.0-133 3.48 20
Bromomethane 0.0250 0.0190 0.0183 75.9 73.1 26.0-160 3.79 20
Carbon disulfide 0.0250 0.0206 0.0204 82.5 81.4 53.0-130 1.29 20
Carbon tetrachloride 0.0250 0.0200 0.0197 80.1 78.8 66.0-123 1.75 20
Chlorobenzene 0.0250 0.0265 0.0262 106 105 79.0-121 1.08 20
Chlorodibromomethane 0.0250 0.0253 0.0253 101 101 74.0-128 0.0600 20
Chloroethane 0.0250 0.0197 0.0193 78.9 77.3 51.0-147 2.05 20
Chloroform 0.0250 0.0220 0.0221 88.0 88.4 73.0-123 0.500 20
Chloromethane 0.0250 0.0207 0.0203 82.8 81.1 51.0-138 2.08 20
Dibromomethane 0.0250 0.0211 0.0216 84.5 86.4 79.0-120 2.24 20
1,2-Dichlorobenzene 0.0250 0.0230 0.0236 92.0 94.2 80.0-120 2.42 20
1,4-Dichlorobenzene 0.0250 0.0246 0.0247 98.5 98.8 77.0-120 0.330 20
trans-1,4-Dichloro-2-butene 0.0250 0.0198 0.0214 79.2 85.5 68.0-126 7.69 20
1,1-Dichloroethane 0.0250 0.0224 0.0222 89.8 88.7 70.0-128 1.22 20
1,2-Dichloroethane 0.0250 0.0202 0.0209 80.7 83.7 69.0-128 3.67 20
1,1-Dichloroethene 0.0250 0.0194 0.0194 77.4 77.4 63.0-131 0.0400 20
cis-1,2-Dichloroethene 0.0250 0.0227 0.0229 90.8 91.7 74.0-123 0.950 20
trans-1,2-Dichloroethene 0.0250 0.0241 0.0231 96.3 92.2 72.0-122 4.28 20
1,2-Dichloropropane 0.0250 0.0226 0.0226 90.6 90.5 75.0-126 0.120 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011691
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-01,02,03,04,05,06,07,08,09,10,11,12
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243408-1 08/22/17 11:27 • (LCSD) R3243408-2 08/22/17 11:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
cis-1,3-Dichloropropene 0.0250 0.0262 0.0264 105 105 80.0-125 0.710 20
trans-1,3-Dichloropropene 0.0250 0.0254 0.0260 102 104 75.0-129 2.37 20
Ethylbenzene 0.0250 0.0273 0.0264 109 106 77.0-120 3.40 20
2-Hexanone 0.125 0.0988 0.105 79.0 84.3 61.0-143 6.50 20
Iodomethane 0.125 0.106 0.106 85.1 84.8 67.0-132 0.390 20
2-Butanone (MEK)0.125 0.0790 0.0851 63.2 68.0 37.0-159 7.39 20
Methylene Chloride 0.0250 0.0205 0.0207 81.9 82.9 67.0-123 1.23 20
4-Methyl-2-pentanone (MIBK)0.125 0.0945 0.101 75.6 80.4 60.0-144 6.19 20
Styrene 0.0250 0.0243 0.0242 97.2 97.0 78.0-124 0.250 20
1,1,1,2-Tetrachloroethane 0.0250 0.0248 0.0242 99.1 96.8 74.0-124 2.36 20
1,1,2,2-Tetrachloroethane 0.0250 0.0201 0.0215 80.2 86.1 73.0-120 7.12 20
Tetrachloroethene 0.0250 0.0301 0.0294 121 118 70.0-127 2.31 20
Toluene 0.0250 0.0259 0.0254 104 102 77.0-120 1.93 20
1,1,1-Trichloroethane 0.0250 0.0204 0.0198 81.4 79.2 69.0-125 2.79 20
1,1,2-Trichloroethane 0.0250 0.0250 0.0257 100 103 78.0-120 2.65 20
Trichloroethene 0.0250 0.0242 0.0241 96.6 96.6 79.0-120 0.000 20
Trichlorofluoromethane 0.0250 0.0201 0.0195 80.4 77.9 59.0-136 3.23 20
1,2,3-Trichloropropane 0.0250 0.0205 0.0211 82.1 84.4 73.0-124 2.82 20
Vinyl acetate 0.125 0.0961 0.0974 76.9 77.9 58.0-156 1.32 20
Vinyl chloride 0.0250 0.0209 0.0205 83.8 81.9 63.0-134 2.22 20
Xylenes, Total 0.0750 0.0803 0.0789 107 105 77.0-120 1.76 20
(S) Toluene-d8 118 117 80.0-120
(S) Dibromofluoromethane 96.6 99.1 74.0-131
(S) a,a,a-Trifluorotoluene 99.8 100 80.0-120
(S) 4-Bromofluorobenzene 101 102 64.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011888
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-13,14
Method Blank (MB)
(MB) R3244575-3 08/20/17 19:54
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromochloromethane U 0.000520 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene 0.000435 J 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
Toluene U 0.000412 0.00100
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011888
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-13,14
Method Blank (MB)
(MB) R3244575-3 08/20/17 19:54
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Trichlorofluoromethane U 0.00120 0.00500
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl chloride U 0.000259 0.00100
Vinyl acetate U 0.00163 0.0100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 113 80.0-120
(S) Dibromofluoromethane 103 76.0-123
(S) a,a,a-Trifluorotoluene 104 80.0-120
(S) 4-Bromofluorobenzene 105 80.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244575-1 08/20/17 18:50 • (LCSD) R3244575-2 08/20/17 19:12
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.154 0.157 123 125 10.0-160 2.10 23
Acrylonitrile 0.125 0.126 0.130 101 104 60.0-142 3.18 20
Benzene 0.0250 0.0270 0.0269 108 108 69.0-123 0.0300 20
Bromodichloromethane 0.0250 0.0256 0.0254 103 102 76.0-120 0.740 20
Bromochloromethane 0.0250 0.0285 0.0295 114 118 76.0-122 3.23 20
Bromoform 0.0250 0.0274 0.0273 109 109 67.0-132 0.300 20
Bromomethane 0.0250 0.0157 0.0167 62.8 66.9 18.0-160 6.40 20
Carbon disulfide 0.0250 0.0280 0.0282 112 113 55.0-127 0.960 20
Carbon tetrachloride 0.0250 0.0279 0.0281 112 112 63.0-122 0.660 20
Chlorobenzene 0.0250 0.0293 0.0284 117 114 79.0-121 3.10 20
Chlorodibromomethane 0.0250 0.0283 0.0280 113 112 75.0-125 0.880 20
Chloroethane 0.0250 0.0257 0.0257 103 103 47.0-152 0.0700 20
Chloroform 0.0250 0.0264 0.0266 106 106 72.0-121 0.520 20
Chloromethane 0.0250 0.0218 0.0230 87.3 92.1 48.0-139 5.37 20
1,2-Dichlorobenzene 0.0250 0.0269 0.0272 108 109 80.0-120 1.13 20
Dibromomethane 0.0250 0.0263 0.0263 105 105 78.0-120 0.0100 20
1,4-Dichlorobenzene 0.0250 0.0266 0.0265 106 106 77.0-120 0.170 20
trans-1,4-Dichloro-2-butene 0.0250 0.0221 0.0225 88.4 90.0 55.0-134 1.89 20
1,1-Dichloroethane 0.0250 0.0274 0.0274 109 110 70.0-126 0.260 20
1,2-Dichloroethane 0.0250 0.0263 0.0268 105 107 67.0-126 1.83 20
1,1-Dichloroethene 0.0250 0.0278 0.0284 111 114 64.0-129 2.20 20
cis-1,2-Dichloroethene 0.0250 0.0271 0.0274 109 110 73.0-120 1.08 20
trans-1,2-Dichloroethene 0.0250 0.0274 0.0277 110 111 71.0-121 1.01 20
1,2-Dichloropropane 0.0250 0.0263 0.0262 105 105 75.0-125 0.360 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1011888
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-13,14
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3244575-1 08/20/17 18:50 • (LCSD) R3244575-2 08/20/17 19:12
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
cis-1,3-Dichloropropene 0.0250 0.0273 0.0269 109 108 79.0-123 1.36 20
trans-1,3-Dichloropropene 0.0250 0.0263 0.0260 105 104 74.0-127 1.45 20
Ethylbenzene 0.0250 0.0292 0.0282 117 113 77.0-120 3.74 20
2-Hexanone 0.125 0.144 0.143 115 114 58.0-147 0.860 20
Iodomethane 0.125 0.0802 0.112 64.2 89.4 57.0-140 J3 32.9 20
2-Butanone (MEK)0.125 0.144 0.149 115 119 37.0-158 3.08 20
Methylene Chloride 0.0250 0.0270 0.0271 108 108 66.0-121 0.280 20
4-Methyl-2-pentanone (MIBK)0.125 0.129 0.127 104 102 59.0-143 1.72 20
Styrene 0.0250 0.0273 0.0280 109 112 78.0-124 2.42 20
1,1,1,2-Tetrachloroethane 0.0250 0.0281 0.0276 112 110 75.0-122 1.95 20
1,1,2,2-Tetrachloroethane 0.0250 0.0254 0.0258 102 103 71.0-122 1.29 20
Tetrachloroethene 0.0250 0.0288 0.0279 115 112 70.0-127 3.12 20
Toluene 0.0250 0.0283 0.0274 113 110 77.0-120 3.20 20
1,1,1-Trichloroethane 0.0250 0.0272 0.0271 109 108 68.0-122 0.450 20
1,1,2-Trichloroethane 0.0250 0.0275 0.0270 110 108 78.0-120 1.85 20
Trichloroethene 0.0250 0.0290 0.0287 116 115 78.0-120 1.06 20
Trichlorofluoromethane 0.0250 0.0263 0.0266 105 106 56.0-137 1.28 20
1,2,3-Trichloropropane 0.0250 0.0271 0.0276 108 110 72.0-124 1.77 20
Vinyl acetate 0.125 0.108 0.110 86.7 88.4 46.0-160 1.85 20
Vinyl chloride 0.0250 0.0268 0.0270 107 108 64.0-133 0.610 20
Xylenes, Total 0.0750 0.0846 0.0823 113 110 77.0-120 2.76 20
(S) Toluene-d8 111 109 80.0-120
(S) Dibromofluoromethane 102 104 76.0-123
(S) a,a,a-Trifluorotoluene 104 104 80.0-120
(S) 4-Bromofluorobenzene 106 106 80.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012744
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-15,16
Method Blank (MB)
(MB) R3243713-3 08/23/17 10:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromochloromethane U 0.000520 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene U 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
Toluene U 0.000412 0.00100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012744
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-15,16
Method Blank (MB)
(MB) R3243713-3 08/23/17 10:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Trichlorofluoromethane U 0.00120 0.00500
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl acetate U 0.00163 0.0100
Vinyl chloride U 0.000259 0.00100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 104 80.0-120
(S) Dibromofluoromethane 109 76.0-123
(S) a,a,a-Trifluorotoluene 108 80.0-120
(S) 4-Bromofluorobenzene 106 80.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243713-1 08/23/17 09:27 • (LCSD) R3243713-2 08/23/17 09:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.103 0.131 82.5 105 10.0-160 J3 23.9 23
Acrylonitrile 0.125 0.156 0.151 125 121 60.0-142 3.17 20
Benzene 0.0250 0.0289 0.0282 116 113 69.0-123 2.51 20
Bromodichloromethane 0.0250 0.0261 0.0253 104 101 76.0-120 2.81 20
Bromochloromethane 0.0250 0.0287 0.0261 115 104 76.0-122 9.62 20
Bromoform 0.0250 0.0266 0.0250 106 100 67.0-132 6.09 20
Bromomethane 0.0250 0.0117 0.0125 46.7 49.9 18.0-160 6.66 20
Carbon disulfide 0.0250 0.0267 0.0260 107 104 55.0-127 2.73 20
Carbon tetrachloride 0.0250 0.0313 0.0307 125 123 63.0-122 J4 J4 1.65 20
Chlorobenzene 0.0250 0.0255 0.0249 102 99.6 79.0-121 2.49 20
Chlorodibromomethane 0.0250 0.0263 0.0252 105 101 75.0-125 4.13 20
Chloroethane 0.0250 0.0315 0.0283 126 113 47.0-152 10.5 20
Chloroform 0.0250 0.0276 0.0267 110 107 72.0-121 3.26 20
Chloromethane 0.0250 0.0208 0.0200 83.3 79.8 48.0-139 4.27 20
Dibromomethane 0.0250 0.0272 0.0261 109 105 78.0-120 4.12 20
1,2-Dichlorobenzene 0.0250 0.0255 0.0246 102 98.6 80.0-120 3.46 20
1,4-Dichlorobenzene 0.0250 0.0241 0.0230 96.2 91.9 77.0-120 4.60 20
trans-1,4-Dichloro-2-butene 0.0250 0.0267 0.0257 107 103 55.0-134 3.66 20
1,1-Dichloroethane 0.0250 0.0286 0.0275 114 110 70.0-126 3.88 20
1,2-Dichloroethane 0.0250 0.0295 0.0287 118 115 67.0-126 2.56 20
1,1-Dichloroethene 0.0250 0.0259 0.0253 103 101 64.0-129 2.38 20
cis-1,2-Dichloroethene 0.0250 0.0270 0.0275 108 110 73.0-120 1.80 20
trans-1,2-Dichloroethene 0.0250 0.0282 0.0268 113 107 71.0-121 4.99 20
1,2-Dichloropropane 0.0250 0.0282 0.0275 113 110 75.0-125 2.49 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1012744
Volatile Organic Compounds (GC/MS) by Method 8260B L930565-15,16
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3243713-1 08/23/17 09:27 • (LCSD) R3243713-2 08/23/17 09:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
cis-1,3-Dichloropropene 0.0250 0.0266 0.0258 106 103 79.0-123 3.10 20
trans-1,3-Dichloropropene 0.0250 0.0276 0.0267 110 107 74.0-127 3.05 20
Ethylbenzene 0.0250 0.0251 0.0245 100 98.0 77.0-120 2.25 20
2-Hexanone 0.125 0.128 0.131 102 105 58.0-147 2.64 20
Iodomethane 0.125 0.0548 0.0743 43.8 59.4 57.0-140 J4 J3 30.2 20
2-Butanone (MEK)0.125 0.139 0.150 111 120 37.0-158 7.64 20
Methylene Chloride 0.0250 0.0257 0.0247 103 98.9 66.0-121 3.64 20
4-Methyl-2-pentanone (MIBK)0.125 0.132 0.129 106 103 59.0-143 2.36 20
Styrene 0.0250 0.0270 0.0254 108 102 78.0-124 5.79 20
1,1,1,2-Tetrachloroethane 0.0250 0.0253 0.0246 101 98.4 75.0-122 2.87 20
1,1,2,2-Tetrachloroethane 0.0250 0.0264 0.0251 105 101 71.0-122 4.75 20
Tetrachloroethene 0.0250 0.0261 0.0254 104 102 70.0-127 2.73 20
Toluene 0.0250 0.0250 0.0243 100 97.0 77.0-120 2.99 20
1,1,1-Trichloroethane 0.0250 0.0280 0.0268 112 107 68.0-122 4.41 20
1,1,2-Trichloroethane 0.0250 0.0257 0.0246 103 98.4 78.0-120 4.40 20
Trichloroethene 0.0250 0.0273 0.0265 109 106 78.0-120 2.76 20
Trichlorofluoromethane 0.0250 0.0324 0.0311 130 125 56.0-137 4.05 20
1,2,3-Trichloropropane 0.0250 0.0266 0.0253 107 101 72.0-124 5.33 20
Vinyl acetate 0.125 0.175 0.165 140 132 46.0-160 5.83 20
Vinyl chloride 0.0250 0.0292 0.0290 117 116 64.0-133 0.590 20
Xylenes, Total 0.0750 0.0758 0.0743 101 99.1 77.0-120 2.00 20
(S) Toluene-d8 101 100 80.0-120
(S) Dibromofluoromethane 107 107 76.0-123
(S) a,a,a-Trifluorotoluene 106 106 80.0-120
(S) 4-Bromofluorobenzene 105 103 80.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL (dry)Reported Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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