20094_Belmont_Dyers_Summary_Report_20170926

Licensure: NC Geology C-520 5113 Yachtsman Court Raleigh, North Carolina 27615 919-630-0721
September 26, 2017
Mr. Kim T. Caulk, PG VIA EMAIL: [e-mail]
Inactive Hazardous Sites Branch
Registered Environmental Consultant Program North Carolina Department of Environmental Quality 1601 Mail Service Center Raleigh, NC 27699
Subject: Site Activities Report Former Belmont Dyers 18 Linestowe Drive
Belmont, Gaston County, North Carolina
Site ID No.: NONCD 0001335
Dear Mr. Caulk: Please find enclosed herein the required and executed certification statements and our
Site Activities Report for assessment activities conducted during August 2017. If you should have questions regarding this submittal or associated documentation, please feel free to contact us at [phone] at your convenience.
Sincerely,
PROCTOR ENVIRONMENTAL SERVICES, INC.

Tom Proctor, P.G. RSM
Principal Environmental Geologist
Enclosures
North Carolina Corporate License C-520 5113 Yachtsman Court
Raleigh, North Carolina 27615 919-630-0721

September 26, 2017 Mr. Derr Leonhardt Leonhardt Environmental 8392 Six Forks Road, Suite 101
Raleigh, North Carolina 27615 Subject: SITE ACTIVITIES REPORT FORMER BELMONT DYERS SITE 18 LINESTOWE DRIVE BELMONT, NORTH CAROLINA SITE ID NO. NONCD0001335 Dear Mr. Leonhardt:
In accordance with the recently submitted Remedial Investigation Work Plan,
Proctor Environmental Services has conducted additional assessment work at the
Belmont Dyers site in Belmont, North Carolina (Figure 1). These assessment
activities do not complete the assessment work proposed in the Work Plan. The
remaining items in the Plan will be completed once site access agreements are
reached and a separate report will be issued.

During August of 2017, the following activities were performed:

• Constructed and sampled monitoring wells MW-8, MW-9, and MW-13;
• Sampled existing monitoring well PMW-5sR;
• Collected two soil samples and a duplicate sample from the boring for
well MW-9; and
• Collected soil gas samples for analysis at three locations.
The remainder of this letter report summarizes the findings of these assessment
activities.

Site Activities Report September 26, 2017 Former Belmont Dyers Site Page 2
Belmont, North Carolina Monitoring Well Construction and Sampling On August 21, 2017, groundwater monitoring well MW-8, MW-9 and MW-13 were
constructed near the southwestern corner of the site, located as shown on Figure 2.
The wells are 2-inch diameter Type II well and are screened from 35 to 45 feet below
land surface (bls). North Carolina Well Construction Records (form GW-1) for the wells
are located in Appendix A. Investigation derived soil cuttings from the well borings
were drummed and left on the site for subsequent off-site disposal.

Subsequent to installation, the three new wells and existing well PMW-5sR were
developed by removing three well volumes of groundwater from each. Investigation
derived development water from the wells was drummed and left on the site for
subsequent off-site disposal. Subsequent to purging the wells, a handheld YSI
multiparameter instrument was used to measure temperature, dissolved oxygen,
conductivity, specific conductance and pH of the water extracted for analysis. A
summary of these measurements can be found in Table 1.

A groundwater sample was collected from each well on August 21, 2017 and submitted
to the analytical laboratory under chain-of-custody protocols for analysis of volatile
organic compounds (VOCs) by SW-846 Method 8260. A duplicate sample (Dupe-W)
was collected for analysis from PMW-5sR. A laboratory-prepared trip blank was also
transported with the groundwater samples and submitted for analysis for QA/QC
purposes. As shown on the laboratory data sheets in Appendix B and summarized in Table 2, several detectable concentrations of constituents of concern, including 1,1-
dichloroethylene, tetrachloroethylene (PCE), trichloroethene (TCE), chloroform, and
trichlorofluoromethane were exhibited by the monitoring well samples in excess of their
respective North Carolina Groundwater Quality Standards and/or their residential
groundwater vapor intrusion screening levels. Concentrations of the most prevalent
constituent, tetrachloroethylene, are shown on Figure 3 for the four wells sampled in
August of 2017 along with the groundwater data for the other site wells from the March
2016 sampling event conducted by Mid-Atlantic Associates. The 2016 sampling event
is the most recent groundwater data prior to the August 2017 sampling efforts. Figure
3 also shows the estimated shallow groundwater flow direction determined during the
March 2016 sampling event. As shown, groundwater under the site was migrating
towards the east at the time of that sampling event.
Soil Sample Collection and Analysis

As summarized in the Work Plan, a July 1991 Environmental Phase 2 Assessment by
Westinghouse documented adversely-impacted soil associated with a former 10,000-
gallon aboveground heating oil tank. Specifically, Westinghouse sample BH105 was
Site Activities Report September 26, 2017 Former Belmont Dyers Site Page 3
Belmont, North Carolina collected from an area of semi-volatile-impacted soil (currently referred to as Diesel Range Organics (DRO)) Total Petroleum Hydrocarbons (TPH) and exhibited 9,970 mg/kg of DRO, which exceeds the current NCDEQ Action Level of 100 mg/kg for TPH-DRO.

The boring for new monitoring well MW-9, located as shown on Figure 2, was
advanced in the immediate vicinity of Westinghouse sample BH105 and soil samples were collected at 14 feet below land surface (bls) and 24 feet bls to determine whether
the soil is still impacted in excess of the Preliminary Soil Remedial Goals (PSRG)
established by the NCDEQ. The soil samples were analyzed for VOCs by Method 8260,
semi-volatile organic compounds (SVOCs) by Method 8270, and volatile and extractable
petroleum hydrocarbons (VPH and EPH by the MADEP method). As documented in the
laboratory data report in Appendix B, the sample collected from the 14-foot bls interval
(MW9/BH105A) exhibited 2.9 mg/Kg of MADEP EPH and the sample collected from the
24-foot bls interval (MW9/BH105B) exhibited on 2.7 mg/Kg of MADEP EPH. A duplicate
sample, Dupe-S, was collected and analyzed from the 24-foot bls interval. It exhibited
2.9 mg/Kg of MADEP EPH. All of these results were reported by the laboratory to be
“J” values, or estimated concentrations as they were detected at concentrations below
the laboratory’s reporting limit. They are also below the NCDEQ soil-to-water MSCC
(540 mg/Kg), residential cleanup level (1500 mg/Kg) and residential PSRG of 6.9
mg/Kg for C9-C18 aliphatics. In addition, acetone, a common laboratory artifact, was
detected at a concentration of 0.12 mg/Kg in duplicate sample Dupe-S. The residential
health-based PSRG for acetone is 12,000 mg/Kg. None of the results exceed their
respective NCDEQ PSRG values.
Vapor Intrusion Soil Gas Sampling Results

Our August 3, 2017 vapor intrusion soil gas sampling work plan called for the collection
and analysis of eight soil gas samples near the southern property boundary. These
locations were based on the findings from Hart & Hickman’s recent soil gas sampling
on May 16, 2017. However, it was determined to reduce the initial sample locations to
three, located as shown on Figure 4, since the results from the newly installed
groundwater monitoring wells (discussed above) would sufficiently characterize the
potential soil gas risk in the vicinity of the property’s southwest corner.

Soil gas samples PES-SG-6, 7, and 8A and 8B were collected and analyzed in
accordance with the vapor intrusion soil gas sampling work plan and exhibited the
following constituents of concern:

Site Activities Report September 26, 2017 Former Belmont Dyers Site Page 4
Belmont, North Carolina
Sample ID Date Analytical
Method
Constituent and Concentration (ug/m3)
Tetrachloroethylene Trichloroethylene
PES-SG-6
8/3/17 TO-15
1,400 20
PES-SG-7 1,000 3.4
PES-SG-8A 33 2.1
PES-SG-8B 47 2.0
Residential Soil Gas Screening Level 278 13.9

As summarized above and documented in the analytical report in Appendix C, the soil
gas samples collected on the property and north of the apartment buildings, PES-SG-
6 and 7, exhibited exceedances of tetrachloroethylene and trichloroethylene (PES-SG-
6 and 7) or just trichloroethylene (PES-SG-6). Tetrachloroethylene and
trichloroethylene were also detected in samples PES-SG-8A and 8B but at
concentrations less than their respective screening levels.

Summary and Conclusions Based on our observations, the activities conducted at the site, and the laboratory analytical results, Proctor Environmental offers the following summary and conclusions: Groundwater
• PCE was detected in each of the four groundwater samples collected near the property’s southwestern corner at concentrations in excess of its
groundwater quality standard. The sample from the newly installed off-site
well, MW-13, exhibited the highest PCE concentration, 95 ug/L, of the four
wells sampled. The horizontal and vertical extent of PCE impacted
groundwater has not been determined in this area of the site. Based upon the
site’s topography (Figure 1), it’s feasible that groundwater in this area of the
site is migrating towards the south, unlike the groundwater flow direction from
2016 shown in Figure 3; and
• The concentrations of PCE (all four wells sampled) and 1,1-Dichloroethylene (wells PMW-5sR and MW-13) exceed their respective residential vapor intrusion screening levels. MW-13 is within 100 feet of residential homes at 25,
27 and 29 Linestowe Drive and the currently vacant lot located at 31 Linestowe
Drive.

Site Activities Report September 26, 2017 Former Belmont Dyers Site Page 5
Belmont, North Carolina Soil

• The soil sample collected from the area previously assessed by
Westinghouse and documented in their 1991 assessment report did not
exhibit petroleum-related constituents at concentrations in excess of their
respective PSRGs.

Vapor Intrusion Soil Gas Sampling

• Soil gas sample location PES-SG-6 exceeded the respective residential vapor intrusion screening levels for PCE and TCE. This sample location is within 100 feet of the easternmost apartment building (River Ridge Condo, 1442 - 1452
River Drive);
• Soil gas sample location PES-SG-7 exceeded the respective residential vapor intrusion screening levels for PCE. This sample location is within 100 feet of the River Ridge Condo apartment building (River Ridge Condo, 1428 - 1438 River Drive);
• Crawlspace soil gas sampling should be conducted at the nearby residences along Linestowe Drive to determine if they are being adversely exposed to volatile organic vapors; and
• Soil gas sampling should be considered for the nearby apartments adjacent to
the southeastern property corner (i.e., the two easternmost River Ridge Condo
buildings) and the vacant property at 31 Linestowe Drive.
If you have any questions or comments regarding this report or the activities conducted
at the site to date, please contact me at [phone].

Best Regards,
PROCTOR ENVIRONMENTAL SERVICES, INC.

Thomas A. Proctor, P.G., RSM President
Attachments: Figures, Tables, Appendices

FIGURES

Figure 1 – Site Location Map Source: USGS Quadrangle Map Scale: As Shown

Former Belmont Dyers Site
18 Linestowe Drive
Belmont, North Carolina
PES Project Number: R17-207

Figure 2 – Monitoring Well Location Map Source: MAA Site Activities Report, June 2016 Scale: 1” ~ 135’

Former Belmont Dyers Site
18 Linestowe Drive
Belmont, North Carolina
PES Project Number: R17-20

MW-8 MW-9
MW-13
Legend: Existing Monitoring Well Location Newly Installed Monitoring Well Location

Figure 3 – PCE Concentrations Map Source: MAA Site Activities Report, June 2016 Scale: 1” ~ 90’

Former Belmont Dyers Site 18 Linestowe Drive Belmont, North Carolina PES Project Number: R17-207

#26 #27 #28 #29
PMW-5Sr 110 (3/16) 73 (8/17)
WHSE
MW-8 14 (8/17) MW-9 56 (8/17)
MW-13 95 (8/17)
5.6 ug/L (3/16)
200 (3/16)
91 (3/16)
ND (3/16)
Legend 96 = PCE (ug/L) GW Flow (3/16) Newly Installed Well #27 Linestowe Address
PMW-1iR 3.2 (3/16)
PMW-1sR 6.2 (3/16) PMW-1dR 9.0 (3/16)

Figure 4 – Vapor Intrusion Sample Locations Source: Hart & Hickman BF Assessment Report, June 12, 2017 Scale: 1” ~ 110’

Former Belmont Dyers Site
18 Linestowe Drive
Belmont, North Carolina PES Project Number: R17-207

PES-SG-6
PES-SG-7
PES-SG8A, 8B
Legend:
Soil Gas Sample Location and ID
TABLES

Well ID °C DO (mg/L)SC (mS/m)pH ORP (mV)
PMW-5sR 22.7 6.40 0.225 6.00 163
MW-8 21.9 6.88 0.092 5.60 173
MW-9 22.5 5.45 2.34 5.59 197
MW-13 21.4 6.70 0.225 6.13 186
NOTES:
DO - Dissolved Oxygen (in milligrams per liter or mg/L)
SC - Specific Conductance (in milliSeimens/meter)
pH - measureed in Standard Units
ORP - Oxygen Reducing Potential (in millivolts)
Table 1
Summary of Groundwater Field Parameters
Former Belmont Dyers Site
Belmont, North Carolina
August 21, 2017
Constituent
North Carolina
Groundwater
Quality
Standard
(ug/L)
Residential
Screening
Level (ug/L)
Non-
Residential
Screening
Level (ug/L)
PMW-5sR PMW-5sR
(Duplicate)MW-8 MW-9 MW-13
VOCs by Method 8260B (ug/L)
1,1-Dichloroethylene 350 4 164 4.8 5.6 BRL 0.54 14
Chloroform 70 8 35.5 BRL BRL BRL 0.60 1.4
Tetrachloroethylene 0.7 11.5 48.4 73 86 14 56 95
Trichloroethylene 3 1 4.35 0.70 0.92 BRL BRL 0.84
Trichlorofluoromethane 2,000 NSL NSL 0.96 BRL BRL 1.0 BRL
NOTES:
BRL - Below Laboratory Reporting Limit
NSL - No applicable screening level
Bolded concentrations exceed North Carolina Groundwater Quality Standard
Shaded concentrations exceed Residential Screening Level
Table 2
Groundwater Sample Analytical ResultsFormer Belmont Dyers Site
Belmont, North CarolinaAugust 21, 2017

APPENDIX A
WELL CONSTRUCTION RECORDS
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_______________
Mike Tynan
2725-A
Innovative Environmental Technologies, Inc.
✔
8/22/17 MW-9
Former Belmont Dyers
18 Linestowe Drive, Belmont 28012
Gaston
35 14 21.46 81 00 52.43
✔
✔
one
45
37
8.25
auger
37 45 silty sand
0 35 2 Sch40 PVC
35 45 2 0.010 Sch40 PVC
0 30 neat cement tremie - 70 gals
30 33 bentonite pour through augers -100 lbs
33 45 #2 silica sand pour through augers
0 45 reddish brown silty sand
8/24/17
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_______________
Mike Tynan
2725-A
Innovative Environmental Technologies, Inc.
✔
8/22/17 MW-13
Former Belmont Dyers
18 Linestowe Drive, Belmont 28012
Gaston
35 14 20.95 81 00 53.04
✔
✔
one
45
37
8.25
auger
37 45 silty sand
0 35 2 Sch40 PVC
35 45 2 0.010 Sch40 PVC
0 30 neat cement tremie - 70 gals
30 33 bentonite pour through augers -100 lbs
33 45 #2 silica sand pour through augers
0 45 reddish brown silty sand
8/24/17

APPENDIX B GROUNDWATER LABORATORY ANALYTICAL RESULTS
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
09/05/2017
Proctor Environmental Services, Inc.
Tom Proctor
5113 Yachtsman Ct.
Raleigh, NC 27615
Project: Belmont Dyers
Lab Submittal Date: 08/23/2017
Prism Work Order: 7080385
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
RLM Sample container suspected to have low methanol content. Results possibly biased high.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 47
Sample Receipt Summary
09/05/2017
Prism Work Order: 7080385
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7080385-01 08/21/17PMW-5SR 08/23/17Water
7080385-02 08/21/17MW-8 08/23/17Water
7080385-03 08/21/17MW-9 08/23/17Water
7080385-04 08/21/17MW-13 08/23/17Water
7080385-05 08/21/17Dupe-W 08/23/17Water
7080385-06 08/21/17Trip Blank 08/23/17Water
7080385-07 08/21/17MW9/BH105A 08/23/17Solid
7080385-08 08/21/17MW9/BH105B 08/23/17Solid
7080385-09 08/21/17Dupe-5 08/23/17Solid
Samples were received in good condition at 5.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 47
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7080385
09/05/2017
Summary of Detections
4.8 ug/L7080385-01 PMW-5SR 1,1-Dichloroethylene 8260B
73 ug/L7080385-01 PMW-5SR Tetrachloroethylene 8260B
0.70 ug/L7080385-01 PMW-5SR Trichloroethylene 8260B
0.96 ug/L7080385-01 PMW-5SR Trichlorofluoromethane 8260B
14 ug/L7080385-02 MW-8 Tetrachloroethylene 8260B
0.54 ug/L7080385-03 MW-9 1,1-Dichloroethylene 8260B
0.60 ug/L7080385-03 MW-9 Chloroform 8260B
56 ug/L7080385-03 MW-9 Tetrachloroethylene 8260B
1.0 ug/L7080385-03 MW-9 Trichlorofluoromethane 8260B
14 ug/L7080385-04 MW-13 1,1-Dichloroethylene 8260B
1.4 ug/L7080385-04 MW-13 Chloroform 8260B
95 ug/L7080385-04 MW-13 Tetrachloroethylene 8260B
0.84 ug/L7080385-04 MW-13 Trichloroethylene 8260B
5.6 ug/L7080385-05 Dupe-W 1,1-Dichloroethylene 8260B
86 ug/L7080385-05 Dupe-W Tetrachloroethylene 8260B
0.92 ug/L7080385-05 Dupe-W Trichloroethylene 8260B
2.9 J mg/kg dry7080385-07 MW9/BH105A C9-C18 Aliphatics MADEP EPH
2.7 J mg/kg dry7080385-08 MW9/BH105B C9-C18 Aliphatics MADEP EPH
2.9 J mg/kg dry7080385-09 Dupe-5 C9-C18 Aliphatics MADEP EPH
0.12 mg/kg dry7080385-09 Dupe-5 Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: PMW-5SR
Prism Sample ID: 7080385-01
Prism Work Order: 7080385
Time Collected: 08/21/17 12:00
Time Submitted: 08/23/17 08:40
Volatile Organic Compounds by GC/MS
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0831,1-Dichloroethane
4.8 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7H045012.0 8/24/17 17:10 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7H045012.0 8/24/17 17:10 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7H045012.0 8/24/17 17:10 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7H045015.0 8/24/17 17:10 KDMug/L 0.31Acetone
BRL 8260B P7H04501208/24/17 17:10 KDMug/L 0.20Acrolein
BRL 8260B P7H04501208/24/17 17:10 KDMug/L 0.20Acrylonitrile
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.048Benzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.057Bromobenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.14Bromochloromethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.040Bromoform
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.18Bromomethane
BRL 8260B P7H045015.0 8/24/17 17:10 KDMug/L 0.075Carbon disulfide
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.062Chlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.22Chloroethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.076Chloroform
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.079Chloromethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: PMW-5SR
Prism Sample ID: 7080385-01
Prism Work Order: 7080385
Time Collected: 08/21/17 12:00
Time Submitted: 08/23/17 08:40
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.065Dibromomethane
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.061Ethylbenzene
BRL 8260B P7H045012.0 8/24/17 17:10 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7H045015.0 8/24/17 17:10 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7H045015.0 8/24/17 17:10 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7H045015.0 8/24/17 17:10 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.083Methylene Chloride
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.19Naphthalene
BRL 8260B P7H045011.0 8/24/17 17:10 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.044o-Xylene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.047Styrene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.088tert-Butylbenzene
73 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.044Toluene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.070trans-1,3-Dichloropropylene
0.70 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.078Trichloroethylene
0.96 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7H045012.0 8/24/17 17:10 KDMug/L 0.060Vinyl acetate
BRL 8260B P7H045010.50 8/24/17 17:10 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-124102 %4-Bromofluorobenzene
75-12996 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: MW-8
Prism Sample ID: 7080385-02
Prism Work Order: 7080385
Time Collected: 08/21/17 15:10
Time Submitted: 08/23/17 08:40
Volatile Organic Compounds by GC/MS
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7H045012.0 8/24/17 17:36 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7H045012.0 8/24/17 17:36 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7H045012.0 8/24/17 17:36 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7H045015.0 8/24/17 17:36 KDMug/L 0.31Acetone
BRL 8260B P7H04501208/24/17 17:36 KDMug/L 0.20Acrolein
BRL 8260B P7H04501208/24/17 17:36 KDMug/L 0.20Acrylonitrile
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.048Benzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.057Bromobenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.14Bromochloromethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.040Bromoform
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.18Bromomethane
BRL 8260B P7H045015.0 8/24/17 17:36 KDMug/L 0.075Carbon disulfide
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.062Chlorobenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.22Chloroethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.076Chloroform
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.079Chloromethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: MW-8
Prism Sample ID: 7080385-02
Prism Work Order: 7080385
Time Collected: 08/21/17 15:10
Time Submitted: 08/23/17 08:40
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.065Dibromomethane
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.061Ethylbenzene
BRL 8260B P7H045012.0 8/24/17 17:36 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7H045015.0 8/24/17 17:36 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7H045015.0 8/24/17 17:36 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7H045015.0 8/24/17 17:36 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.083Methylene Chloride
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.19Naphthalene
BRL 8260B P7H045011.0 8/24/17 17:36 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.044o-Xylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.047Styrene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.088tert-Butylbenzene
14 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.044Toluene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.078Trichloroethylene
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7H045012.0 8/24/17 17:36 KDMug/L 0.060Vinyl acetate
BRL 8260B P7H045010.50 8/24/17 17:36 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-124100 %4-Bromofluorobenzene
75-12998 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 7080385-03
Prism Work Order: 7080385
Time Collected: 08/21/17 15:30
Time Submitted: 08/23/17 08:40
Volatile Organic Compounds by GC/MS
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0831,1-Dichloroethane
0.54 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7H045012.0 8/24/17 18:02 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7H045012.0 8/24/17 18:02 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7H045012.0 8/24/17 18:02 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7H045015.0 8/24/17 18:02 KDMug/L 0.31Acetone
BRL 8260B P7H04501208/24/17 18:02 KDMug/L 0.20Acrolein
BRL 8260B P7H04501208/24/17 18:02 KDMug/L 0.20Acrylonitrile
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.048Benzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.057Bromobenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.14Bromochloromethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.040Bromoform
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.18Bromomethane
BRL 8260B P7H045015.0 8/24/17 18:02 KDMug/L 0.075Carbon disulfide
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.062Chlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.22Chloroethane
0.60 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.076Chloroform
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.079Chloromethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 7080385-03
Prism Work Order: 7080385
Time Collected: 08/21/17 15:30
Time Submitted: 08/23/17 08:40
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.065Dibromomethane
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.061Ethylbenzene
BRL 8260B P7H045012.0 8/24/17 18:02 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7H045015.0 8/24/17 18:02 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7H045015.0 8/24/17 18:02 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7H045015.0 8/24/17 18:02 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.083Methylene Chloride
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.19Naphthalene
BRL 8260B P7H045011.0 8/24/17 18:02 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.044o-Xylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.047Styrene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.088tert-Butylbenzene
56 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.044Toluene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.078Trichloroethylene
1.0 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7H045012.0 8/24/17 18:02 KDMug/L 0.060Vinyl acetate
BRL 8260B P7H045010.50 8/24/17 18:02 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-12997 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 7080385-04
Prism Work Order: 7080385
Time Collected: 08/21/17 15:50
Time Submitted: 08/23/17 08:40
Volatile Organic Compounds by GC/MS
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0831,1-Dichloroethane
14 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7H045012.0 8/24/17 23:09 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7H045012.0 8/24/17 23:09 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7H045012.0 8/24/17 23:09 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7H045015.0 8/24/17 23:09 KDMug/L 0.31Acetone
BRL 8260B P7H04501208/24/17 23:09 KDMug/L 0.20Acrolein
BRL 8260B P7H04501208/24/17 23:09 KDMug/L 0.20Acrylonitrile
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.048Benzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.057Bromobenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.14Bromochloromethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.040Bromoform
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.18Bromomethane
BRL 8260B P7H045015.0 8/24/17 23:09 KDMug/L 0.075Carbon disulfide
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.062Chlorobenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.22Chloroethane
1.4 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.076Chloroform
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.079Chloromethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 7080385-04
Prism Work Order: 7080385
Time Collected: 08/21/17 15:50
Time Submitted: 08/23/17 08:40
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.065Dibromomethane
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.061Ethylbenzene
BRL 8260B P7H045012.0 8/24/17 23:09 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7H045015.0 8/24/17 23:09 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7H045015.0 8/24/17 23:09 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7H045015.0 8/24/17 23:09 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.083Methylene Chloride
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.19Naphthalene
BRL 8260B P7H045011.0 8/24/17 23:09 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.044o-Xylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.047Styrene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.088tert-Butylbenzene
95 8260B P7H0450105.0 8/24/17 23:35 KDMug/L 0.98Tetrachloroethylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.044Toluene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.070trans-1,3-Dichloropropylene
0.84 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.078Trichloroethylene
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7H045012.0 8/24/17 23:09 KDMug/L 0.060Vinyl acetate
BRL 8260B P7H045010.50 8/24/17 23:09 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: Dupe-W
Prism Sample ID: 7080385-05
Prism Work Order: 7080385
Time Collected: 08/21/17 00:00
Time Submitted: 08/23/17 08:40
Volatile Organic Compounds by GC/MS
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0831,1-Dichloroethane
5.6 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7H045012.0 8/24/17 18:27 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7H045012.0 8/24/17 18:27 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7H045012.0 8/24/17 18:27 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7H045015.0 8/24/17 18:27 KDMug/L 0.31Acetone
BRL 8260B P7H04501208/24/17 18:27 KDMug/L 0.20Acrolein
BRL 8260B P7H04501208/24/17 18:27 KDMug/L 0.20Acrylonitrile
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.048Benzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.057Bromobenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.14Bromochloromethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.040Bromoform
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.18Bromomethane
BRL 8260B P7H045015.0 8/24/17 18:27 KDMug/L 0.075Carbon disulfide
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.062Chlorobenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.22Chloroethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.076Chloroform
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.079Chloromethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: Dupe-W
Prism Sample ID: 7080385-05
Prism Work Order: 7080385
Time Collected: 08/21/17 00:00
Time Submitted: 08/23/17 08:40
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.065Dibromomethane
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.061Ethylbenzene
BRL 8260B P7H045012.0 8/24/17 18:27 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7H045015.0 8/24/17 18:27 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7H045015.0 8/24/17 18:27 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7H045015.0 8/24/17 18:27 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.083Methylene Chloride
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.19Naphthalene
BRL 8260B P7H045011.0 8/24/17 18:27 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.044o-Xylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.047Styrene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.088tert-Butylbenzene
86 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.044Toluene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.070trans-1,3-Dichloropropylene
0.92 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.078Trichloroethylene
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7H045012.0 8/24/17 18:27 KDMug/L 0.060Vinyl acetate
BRL 8260B P7H045010.50 8/24/17 18:27 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-124123 %4-Bromofluorobenzene
75-129119 %Dibromofluoromethane
77-123122 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: Trip Blank
Prism Sample ID: 7080385-06
Prism Work Order: 7080385
Time Collected: 08/21/17 12:00
Time Submitted: 08/23/17 08:40
Volatile Organic Compounds by GC/MS
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7H045012.0 8/24/17 15:03 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7H045012.0 8/24/17 15:03 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7H045012.0 8/24/17 15:03 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7H045015.0 8/24/17 15:03 KDMug/L 0.31Acetone
BRL 8260B P7H04501208/24/17 15:03 KDMug/L 0.20Acrolein
BRL 8260B P7H04501208/24/17 15:03 KDMug/L 0.20Acrylonitrile
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.048Benzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.057Bromobenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.14Bromochloromethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.040Bromoform
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.18Bromomethane
BRL 8260B P7H045015.0 8/24/17 15:03 KDMug/L 0.075Carbon disulfide
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.062Chlorobenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.22Chloroethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.076Chloroform
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.079Chloromethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Water
Client Sample ID: Trip Blank
Prism Sample ID: 7080385-06
Prism Work Order: 7080385
Time Collected: 08/21/17 12:00
Time Submitted: 08/23/17 08:40
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.065Dibromomethane
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.061Ethylbenzene
BRL 8260B P7H045012.0 8/24/17 15:03 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7H045015.0 8/24/17 15:03 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7H045015.0 8/24/17 15:03 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7H045015.0 8/24/17 15:03 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.083Methylene Chloride
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.19Naphthalene
BRL 8260B P7H045011.0 8/24/17 15:03 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.044o-Xylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.047Styrene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.044Toluene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.078Trichloroethylene
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7H045012.0 8/24/17 15:03 KDMug/L 0.060Vinyl acetate
BRL 8260B P7H045010.50 8/24/17 15:03 KDMug/L 0.097Vinyl chloride
Surrogate Recovery Control Limits
80-124101 %4-Bromofluorobenzene
75-12996 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105A
Prism Sample ID: 7080385-07
Prism Work Order: 7080385
Time Collected: 08/21/17 14:00
Time Submitted: 08/23/17 08:40
Extractable Petroleum Hydrocarbons by GC/FID
2.9 MADEP EPH P7H04061298/24/17 23:53 ZRCJmg/kg dry 1.2C9-C18 Aliphatics
BRL MADEP EPH P7H04061298/24/17 23:53 ZRCmg/kg dry 2.3C19-C36 Aliphatics
BRL MADEP EPH P7H04061118/24/17 23:53 ZRCmg/kg dry 1.6C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14062 %1-Chlorooctadecane
40-14069 %o-Terphenyl
40-14087 %2-Fluorobiphenyl
40-140107 %2-Bromonaphthalene
General Chemistry Parameters
85.0 *SM2540 G P7H052610.100 8/28/17 16:00 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0601,2,4-Trichlorobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0581,2-Dichlorobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0541,3-Dichlorobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0561,4-Dichlorobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0741-Methylnaphthalene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0722,4,6-Trichlorophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0742,4-Dichlorophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0592,4-Dimethylphenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0532,4-Dinitrophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0512,6-Dinitrotoluene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0552-Chloronaphthalene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0542-Chlorophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0612-Methylnaphthalene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0492-Methylphenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0702-Nitrophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0763,3’-Dichlorobenzidine
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0473/4-Methylphenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0574,6-Dinitro-2-methylphenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0664-Bromophenyl phenyl ether
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0544-Chloro-3-methylphenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0464-Chloroaniline
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0504-Chlorophenyl phenyl ether
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.0594-Nitrophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.052Acenaphthene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.055Acenaphthylene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.062Anthracene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.051Azobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.050Benzo(a)anthracene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.041Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105A
Prism Sample ID: 7080385-07
Prism Work Order: 7080385
Time Collected: 08/21/17 14:00
Time Submitted: 08/23/17 08:40
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.044Benzo(b)fluoranthene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.042Benzo(g,h,i)perylene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.050Benzo(k)fluoranthene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.050Benzyl alcohol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.066bis(2-Chloroethoxy)methane
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.054Bis(2-Chloroethyl)ether
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.065Bis(2-chloroisopropyl)ether
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.057Bis(2-Ethylhexyl)phthalate
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.054Butyl benzyl phthalate
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.048Chrysene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.047Dibenzo(a,h)anthracene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.058Dibenzofuran
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.053Diethyl phthalate
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.051Dimethyl phthalate
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.054Di-n-butyl phthalate
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.047Di-n-octyl phthalate
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.049Fluoranthene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.055Fluorene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.061Hexachlorobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.069Hexachlorobutadiene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.068Hexachlorocyclopentadiene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.064Hexachloroethane
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.044Indeno(1,2,3-cd)pyrene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.052Isophorone
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.062Naphthalene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.054Nitrobenzene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.060N-Nitroso-di-n-propylamine
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.058N-Nitrosodiphenylamine
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.045Pentachlorophenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.050Phenanthrene
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.056Phenol
BRL 8270D P7H041010.38 8/23/17 16:02 JMVmg/kg dry 0.051Pyrene
Surrogate Recovery Control Limits
39-13262 %2,4,6-Tribromophenol
44-11558 %2-Fluorobiphenyl
35-11559 %2-Fluorophenol
37-12256 %Nitrobenzene-d5
34-12152 %Phenol-d5
54-12770 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000471,1,1,2-Tetrachloroethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000281,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105A
Prism Sample ID: 7080385-07
Prism Work Order: 7080385
Time Collected: 08/21/17 14:00
Time Submitted: 08/23/17 08:40
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000391,1,2,2-Tetrachloroethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000511,1,2-Trichloroethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000731,2,3-Trichloropropane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000441,2,4-Trimethylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000381,3-Dichlorobenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000344-Chlorotoluene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.000284-Isopropyltoluene
BRL 8260B P7I000110.057 9/1/17 11:46 ANGmg/kg dry 0.0014Acetone
BRL 8260B P7I000110.0034 9/1/17 11:46 ANGmg/kg dry 0.00033Benzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00048Bromobenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00031Bromochloromethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00065Bromoform
BRL 8260B P7I000110.011 9/1/17 11:46 ANGmg/kg dry 0.00070Bromomethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00030Chlorobenzene
BRL 8260B P7I000110.011 9/1/17 11:46 ANGmg/kg dry 0.00048Chloroethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00041Chloroform
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00038Chloromethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00022Ethylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00034Isopropylbenzene (Cumene)
BRL 8260B P7I000110.011 9/1/17 11:46 ANGmg/kg dry 0.00053m,p-Xylenes
BRL 8260B P7I000110.057 9/1/17 11:46 ANGmg/kg dry 0.00052Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7I000110.11 9/1/17 11:46 ANGmg/kg dry 0.00052Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105A
Prism Sample ID: 7080385-07
Prism Work Order: 7080385
Time Collected: 08/21/17 14:00
Time Submitted: 08/23/17 08:40
BRL 8260B P7I000110.057 9/1/17 11:46 ANGmg/kg dry 0.00049Methyl Isobutyl Ketone
BRL 8260B P7I000110.011 9/1/17 11:46 ANGmg/kg dry 0.00032Methylene Chloride
BRL 8260B P7I000110.011 9/1/17 11:46 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P7I000110.011 9/1/17 11:46 ANGmg/kg dry 0.00018Naphthalene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00034n-Propylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00023o-Xylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00028sec-Butylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00034Styrene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00033Toluene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00037Trichloroethylene
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P7I000110.029 9/1/17 11:46 ANGmg/kg dry 0.00078Vinyl acetate
BRL 8260B P7I000110.0057 9/1/17 11:46 ANGmg/kg dry 0.00028Vinyl chloride
BRL 8260B P7I000110.017 9/1/17 11:46 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12999 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID RLM
BRL MADEP VPH P7I00251004.5 9/5/17 11:17 ANGmg/kg dry 0.14C5-C8 Aliphatics
BRL MADEP VPH P7I00251004.5 9/5/17 11:17 ANGmg/kg dry 0.23C9-C12 Aliphatics
BRL MADEP VPH P7I00251004.5 9/5/17 11:17 ANGmg/kg dry 0.050C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130152 %2,5-Dibromotoluene (PID)SR
70-130173 %2,5-Dibromotoluene (FID)SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105B
Prism Sample ID: 7080385-08
Prism Work Order: 7080385
Time Collected: 08/21/17 14:10
Time Submitted: 08/23/17 08:40
Extractable Petroleum Hydrocarbons by GC/FID
2.7 MADEP EPH P7H04061288/25/17 0:30 ZRCJmg/kg dry 1.2C9-C18 Aliphatics
BRL MADEP EPH P7H04061288/25/17 0:30 ZRCmg/kg dry 2.2C19-C36 Aliphatics
BRL MADEP EPH P7H04061118/25/17 0:30 ZRCmg/kg dry 1.5C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14062 %1-Chlorooctadecane
40-14068 %o-Terphenyl
40-14084 %2-Fluorobiphenyl
40-140103 %2-Bromonaphthalene
General Chemistry Parameters
88.5 *SM2540 G P7H052610.100 8/28/17 16:00 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0581,2,4-Trichlorobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0561,2-Dichlorobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0521,3-Dichlorobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0541,4-Dichlorobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0711-Methylnaphthalene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0702,4,6-Trichlorophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0722,4-Dichlorophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0572,4-Dimethylphenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0522,4-Dinitrophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0452,4-Dinitrotoluene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0492,6-Dinitrotoluene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0542-Chloronaphthalene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0532-Chlorophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0592-Methylnaphthalene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0482-Methylphenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0672-Nitrophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0733,3’-Dichlorobenzidine
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0463/4-Methylphenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0644-Bromophenyl phenyl ether
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0524-Chloro-3-methylphenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0454-Chloroaniline
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0484-Chlorophenyl phenyl ether
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.0574-Nitrophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.050Acenaphthene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.054Acenaphthylene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.060Anthracene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.049Azobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.049Benzo(a)anthracene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.040Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105B
Prism Sample ID: 7080385-08
Prism Work Order: 7080385
Time Collected: 08/21/17 14:10
Time Submitted: 08/23/17 08:40
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.043Benzo(b)fluoranthene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.041Benzo(g,h,i)perylene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.049Benzo(k)fluoranthene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.031Benzoic Acid
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.049Benzyl alcohol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.064bis(2-Chloroethoxy)methane
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.052Bis(2-Chloroethyl)ether
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.063Bis(2-chloroisopropyl)ether
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.055Bis(2-Ethylhexyl)phthalate
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.053Butyl benzyl phthalate
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.047Chrysene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.045Dibenzo(a,h)anthracene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.056Dibenzofuran
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.051Diethyl phthalate
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.049Dimethyl phthalate
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.053Di-n-butyl phthalate
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.046Di-n-octyl phthalate
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.047Fluoranthene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.053Fluorene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.059Hexachlorobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.067Hexachlorobutadiene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.066Hexachlorocyclopentadiene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.062Hexachloroethane
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.050Isophorone
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.060Naphthalene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.053Nitrobenzene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.058N-Nitroso-di-n-propylamine
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.056N-Nitrosodiphenylamine
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.044Pentachlorophenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.048Phenanthrene
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.055Phenol
BRL 8270D P7H041010.37 8/23/17 16:24 JMVmg/kg dry 0.049Pyrene
Surrogate Recovery Control Limits
39-13270 %2,4,6-Tribromophenol
44-11566 %2-Fluorobiphenyl
35-11567 %2-Fluorophenol
37-12257 %Nitrobenzene-d5
34-12162 %Phenol-d5
54-12777 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000391,1,1,2-Tetrachloroethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000231,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105B
Prism Sample ID: 7080385-08
Prism Work Order: 7080385
Time Collected: 08/21/17 14:10
Time Submitted: 08/23/17 08:40
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000321,1,2,2-Tetrachloroethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000421,1,2-Trichloroethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000131,1-Dichloroethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000211,1-Dichloroethylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000261,1-Dichloropropylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000271,2,3-Trichlorobenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000601,2,3-Trichloropropane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000351,2,4-Trichlorobenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000361,2,4-Trimethylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000191,2-Dibromoethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000221,2-Dichlorobenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000281,2-Dichloroethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000291,2-Dichloropropane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000351,3,5-Trimethylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000311,3-Dichlorobenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000241,3-Dichloropropane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000181,4-Dichlorobenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000222,2-Dichloropropane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000242-Chlorotoluene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000284-Chlorotoluene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.000234-Isopropyltoluene
BRL 8260B P7I000110.047 9/1/17 12:14 ANGmg/kg dry 0.0011Acetone
BRL 8260B P7I000110.0028 9/1/17 12:14 ANGmg/kg dry 0.00027Benzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00039Bromobenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00026Bromochloromethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00026Bromodichloromethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00053Bromoform
BRL 8260B P7I000110.0094 9/1/17 12:14 ANGmg/kg dry 0.00058Bromomethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00023Carbon Tetrachloride
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00025Chlorobenzene
BRL 8260B P7I000110.0094 9/1/17 12:14 ANGmg/kg dry 0.00039Chloroethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00034Chloroform
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00032Chloromethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00020cis-1,2-Dichloroethylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00016cis-1,3-Dichloropropylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00019Dibromochloromethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00021Dichlorodifluoromethane
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00018Ethylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00019Isopropyl Ether
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00028Isopropylbenzene (Cumene)
BRL 8260B P7I000110.0094 9/1/17 12:14 ANGmg/kg dry 0.00043m,p-Xylenes
BRL 8260B P7I000110.047 9/1/17 12:14 ANGmg/kg dry 0.00042Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7I000110.094 9/1/17 12:14 ANGmg/kg dry 0.00042Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: MW9/BH105B
Prism Sample ID: 7080385-08
Prism Work Order: 7080385
Time Collected: 08/21/17 14:10
Time Submitted: 08/23/17 08:40
BRL 8260B P7I000110.047 9/1/17 12:14 ANGmg/kg dry 0.00040Methyl Isobutyl Ketone
BRL 8260B P7I000110.0094 9/1/17 12:14 ANGmg/kg dry 0.00026Methylene Chloride
BRL 8260B P7I000110.0094 9/1/17 12:14 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether
BRL 8260B P7I000110.0094 9/1/17 12:14 ANGmg/kg dry 0.00015Naphthalene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00024n-Butylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00028n-Propylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00019o-Xylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00023sec-Butylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00028Styrene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00016tert-Butylbenzene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00022Tetrachloroethylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00027Toluene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00028trans-1,2-Dichloroethylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00025trans-1,3-Dichloropropylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00030Trichloroethylene
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00030Trichlorofluoromethane
BRL 8260B P7I000110.023 9/1/17 12:14 ANGmg/kg dry 0.00064Vinyl acetate
BRL 8260B P7I000110.0047 9/1/17 12:14 ANGmg/kg dry 0.00023Vinyl chloride
BRL 8260B P7I000110.014 9/1/17 12:14 ANGmg/kg dry 0.00088Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-129101 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID RLM
BRL MADEP VPH P7I00251004.2 9/5/17 11:48 ANGmg/kg dry 0.14C5-C8 Aliphatics
BRL MADEP VPH P7I00251004.2 9/5/17 11:48 ANGmg/kg dry 0.22C9-C12 Aliphatics
BRL MADEP VPH P7I00251004.2 9/5/17 11:48 ANGmg/kg dry 0.047C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130149 %2,5-Dibromotoluene (PID)SR
70-130170 %2,5-Dibromotoluene (FID)SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: Dupe-5
Prism Sample ID: 7080385-09
Prism Work Order: 7080385
Time Collected: 08/21/17 14:20
Time Submitted: 08/23/17 08:40
Extractable Petroleum Hydrocarbons by GC/FID
2.9 MADEP EPH P7H04061288/25/17 1:06 ZRCJmg/kg dry 1.2C9-C18 Aliphatics
BRL MADEP EPH P7H04061288/25/17 1:06 ZRCmg/kg dry 2.3C19-C36 Aliphatics
BRL MADEP EPH P7H04061118/25/17 1:06 ZRCmg/kg dry 1.5C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14060 %1-Chlorooctadecane
40-14073 %o-Terphenyl
40-14087 %2-Fluorobiphenyl
40-140106 %2-Bromonaphthalene
General Chemistry Parameters
83.1 *SM2540 G P7H052610.100 8/28/17 16:00 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0611,2,4-Trichlorobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0601,2-Dichlorobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0551,3-Dichlorobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0581,4-Dichlorobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0761-Methylnaphthalene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0742,4,6-Trichlorophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0762,4-Dichlorophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0602,4-Dimethylphenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0522,6-Dinitrotoluene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0562-Chlorophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0632-Methylnaphthalene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0502-Methylphenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0722-Nitrophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0783,3’-Dichlorobenzidine
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0474-Chloroaniline
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.0614-Nitrophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.063Anthracene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.052Azobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.043Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: Dupe-5
Prism Sample ID: 7080385-09
Prism Work Order: 7080385
Time Collected: 08/21/17 14:20
Time Submitted: 08/23/17 08:40
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.052Benzo(k)fluoranthene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.052Benzyl alcohol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.068bis(2-Chloroethoxy)methane
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.067Bis(2-chloroisopropyl)ether
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.056Butyl benzyl phthalate
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.050Chrysene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.060Dibenzofuran
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.048Di-n-octyl phthalate
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.050Fluoranthene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.057Fluorene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.063Hexachlorobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.071Hexachlorobutadiene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.070Hexachlorocyclopentadiene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.053Isophorone
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.063Naphthalene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.060N-Nitrosodiphenylamine
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.058Phenol
BRL 8270D P7H041010.39 8/23/17 16:46 JMVmg/kg dry 0.052Pyrene
Surrogate Recovery Control Limits
39-13249 %2,4,6-Tribromophenol
44-11546 %2-Fluorobiphenyl
35-11542 %2-Fluorophenol
37-12242 %Nitrobenzene-d5
34-12144 %Phenol-d5
54-12758 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000511,1,1,2-Tetrachloroethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000301,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: Dupe-5
Prism Sample ID: 7080385-09
Prism Work Order: 7080385
Time Collected: 08/21/17 14:20
Time Submitted: 08/23/17 08:40
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000551,1,2-Trichloroethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000791,2,3-Trichloropropane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000461,2,4-Trichlorobenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000411,3-Dichlorobenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000374-Chlorotoluene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.000304-Isopropyltoluene
0.12 8260B P7I000110.062 9/1/17 12:41 ANGmg/kg dry 0.0015Acetone
BRL 8260B P7I000110.0037 9/1/17 12:41 ANGmg/kg dry 0.00036Benzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00052Bromobenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00034Bromochloromethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00070Bromoform
BRL 8260B P7I000110.012 9/1/17 12:41 ANGmg/kg dry 0.00076Bromomethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00033Chlorobenzene
BRL 8260B P7I000110.012 9/1/17 12:41 ANGmg/kg dry 0.00052Chloroethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00045Chloroform
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00042Chloromethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00024Ethylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P7I000110.012 9/1/17 12:41 ANGmg/kg dry 0.00057m,p-Xylenes
BRL 8260B P7I000110.062 9/1/17 12:41 ANGmg/kg dry 0.00056Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7I000110.12 9/1/17 12:41 ANGmg/kg dry 0.00056Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 47
Laboratory Report
09/05/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: Dupe-5
Prism Sample ID: 7080385-09
Prism Work Order: 7080385
Time Collected: 08/21/17 14:20
Time Submitted: 08/23/17 08:40
BRL 8260B P7I000110.062 9/1/17 12:41 ANGmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P7I000110.012 9/1/17 12:41 ANGmg/kg dry 0.00035Methylene Chloride
BRL 8260B P7I000110.012 9/1/17 12:41 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P7I000110.012 9/1/17 12:41 ANGmg/kg dry 0.00020Naphthalene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00025o-Xylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00037Styrene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00035Toluene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00040Trichloroethylene
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00040Trichlorofluoromethane
BRL 8260B P7I000110.031 9/1/17 12:41 ANGmg/kg dry 0.00085Vinyl acetate
BRL 8260B P7I000110.0062 9/1/17 12:41 ANGmg/kg dry 0.00030Vinyl chloride
BRL 8260B P7I000110.019 9/1/17 12:41 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID RLM
BRL MADEP VPH P7I00251004.6 9/5/17 12:18 ANGmg/kg dry 0.15C5-C8 Aliphatics
BRL MADEP VPH P7I00251004.6 9/5/17 12:18 ANGmg/kg dry 0.24C9-C12 Aliphatics
BRL MADEP VPH P7I00251004.6 9/5/17 12:18 ANGmg/kg dry 0.052C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130171 %2,5-Dibromotoluene (PID)SR
70-130196 %2,5-Dibromotoluene (FID)SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7H0450 - 5030B
Blank (P7H0450-BLK1)Prepared & Analyzed: 08/24/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7H0450 - 5030B
Blank (P7H0450-BLK1)Prepared & Analyzed: 08/24/17
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10351.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9647.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10050.2
LCS (P7H0450-BS1)Prepared & Analyzed: 08/24/17
1,1,1,2-Tetrachloroethane ug/L17.4 0.50 20.00 79-13487
1,1,1-Trichloroethane ug/L18.2 0.50 20.00 75-13691
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 62-127107
1,1,2-Trichloroethane ug/L19.9 0.50 20.00 70-140100
1,1-Dichloroethane ug/L20.6 0.50 20.00 78-130103
1,1-Dichloroethylene ug/L20.2 0.50 20.00 70-154101
1,1-Dichloropropylene ug/L19.4 0.50 20.00 71-13697
1,2,3-Trichlorobenzene ug/L17.3 2.0 20.00 58-14487
1,2,3-Trichloropropane ug/L19.7 1.0 20.00 71-12798
1,2,4-Trichlorobenzene ug/L17.1 1.0 20.00 66-13986
1,2,4-Trimethylbenzene ug/L20.7 0.50 20.00 75-133103
1,2-Dibromo-3-chloropropane ug/L15.7 2.0 20.00 63-13478
1,2-Dibromoethane ug/L20.0 0.50 20.00 77-135100
1,2-Dichlorobenzene ug/L19.4 0.50 20.00 78-12897
1,2-Dichloroethane ug/L19.8 0.50 20.00 68-13199
1,2-Dichloropropane ug/L21.5 0.50 20.00 77-130108
1,3,5-Trimethylbenzene ug/L20.6 0.50 20.00 75-131103
1,3-Dichlorobenzene ug/L18.8 0.50 20.00 77-12594
1,3-Dichloropropane ug/L20.0 0.50 20.00 76-132100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7H0450 - 5030B
LCS (P7H0450-BS1)Prepared & Analyzed: 08/24/17
1,4-Dichlorobenzene ug/L19.1 0.50 20.00 75-12695
2,2-Dichloropropane ug/L19.6 2.0 20.00 29-14998
2-Chlorotoluene ug/L20.9 0.50 20.00 74-126104
4-Chlorotoluene ug/L20.7 0.50 20.00 78-129103
4-Isopropyltoluene ug/L20.2 0.50 20.00 69-132101
Acetone ug/L38.0 5.0 40.00 40-16695
Acrolein ug/L46.7 20 40.00 70-130117
Acrylonitrile ug/L42.2 20 40.00 81-127106
Benzene ug/L20.9 0.50 20.00 77-128105
Bromobenzene ug/L21.8 0.50 20.00 78-129109
Bromochloromethane ug/L18.9 0.50 20.00 78-13595
Bromodichloromethane ug/L20.0 0.50 20.00 76-138100
Bromoform ug/L14.3 1.0 20.00 71-13571
Bromomethane ug/L27.0 1.0 20.00 41-168135
Carbon disulfide ug/L19.3 5.0 20.00 59-13596
Carbon Tetrachloride ug/L15.7 0.50 20.00 72-14279
Chlorobenzene ug/L20.4 0.50 20.00 78-119102
Chloroethane ug/L24.9 0.50 20.00 57-142124
Chloroform ug/L20.0 0.50 20.00 77-130100
Chloromethane ug/L21.6 0.50 20.00 47-145108
cis-1,2-Dichloroethylene ug/L21.3 0.50 20.00 76-141106
cis-1,3-Dichloropropylene ug/L21.0 0.50 20.00 65-140105
Dibromochloromethane ug/L16.4 0.50 20.00 75-13482
Dibromomethane ug/L19.5 0.50 20.00 76-13898
Dichlorodifluoromethane ug/L16.5 1.0 20.00 28-16383
Ethylbenzene ug/L20.8 0.50 20.00 80-127104
Hexachlorobutadiene ug/L16.8 2.0 20.00 61-13484
Isopropyl Ether ug/L20.3 0.50 20.00 60-154101
Isopropylbenzene (Cumene)ug/L19.9 0.50 20.00 70-13099
m,p-Xylenes ug/L41.3 1.0 40.00 77-133103
Methyl Butyl Ketone (2-Hexanone)ug/L21.2 5.0 20.00 64-137106
Methyl Ethyl Ketone (2-Butanone)ug/L19.9 5.0 20.00 71-134100
Methyl Isobutyl Ketone ug/L22.5 5.0 20.00 69-134113
Methylene Chloride ug/L19.4 1.0 20.00 73-13197
Methyl-tert-Butyl Ether ug/L20.6 0.50 20.00 68-135103
Naphthalene ug/L18.8 1.0 20.00 64-13694
n-Butylbenzene ug/L21.4 1.0 20.00 68-134107
n-Propylbenzene ug/L21.1 0.50 20.00 72-132105
o-Xylene ug/L20.0 0.50 20.00 78-128100
sec-Butylbenzene ug/L19.9 0.50 20.00 71-13199
Styrene ug/L21.1 0.50 20.00 78-129105
tert-Butylbenzene ug/L18.8 0.50 20.00 70-13294
Tetrachloroethylene ug/L16.9 0.50 20.00 80-12984
Toluene ug/L20.6 0.50 20.00 76-131103
trans-1,2-Dichloroethylene ug/L20.8 0.50 20.00 76-135104
trans-1,3-Dichloropropylene ug/L20.1 0.50 20.00 67-140101
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7H0450 - 5030B
LCS (P7H0450-BS1)Prepared & Analyzed: 08/24/17
Trichloroethylene ug/L18.0 0.50 20.00 77-13390
Trichlorofluoromethane ug/L17.7 0.50 20.00 62-14889
Vinyl acetate ug/L23.3 2.0 20.00 34-167116
Vinyl chloride ug/L23.4 0.50 20.00 57-141117
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10050.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9648.1
ug/L 50.00 77-123Surrogate: Toluene-d8 10050.0
LCS Dup (P7H0450-BSD1)Prepared & Analyzed: 08/24/17
1,1,1,2-Tetrachloroethane ug/L16.9 0.50 20.00 2079-13484 3
1,1,1-Trichloroethane ug/L17.6 0.50 20.00 2075-13688 3
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 2062-127106 0.1
1,1,2-Trichloroethane ug/L19.9 0.50 20.00 2070-140100 0
1,1-Dichloroethane ug/L20.2 0.50 20.00 2078-130101 2
1,1-Dichloroethylene ug/L19.7 0.50 20.00 2070-15499 2
1,1-Dichloropropylene ug/L19.1 0.50 20.00 2071-13696 1
1,2,3-Trichlorobenzene ug/L17.1 2.0 20.00 2058-14485 2
1,2,3-Trichloropropane ug/L19.4 1.0 20.00 2071-12797 2
1,2,4-Trichlorobenzene ug/L16.6 1.0 20.00 2066-13983 3
1,2,4-Trimethylbenzene ug/L19.8 0.50 20.00 2075-13399 4
1,2-Dibromo-3-chloropropane ug/L16.4 2.0 20.00 2063-13482 5
1,2-Dibromoethane ug/L20.0 0.50 20.00 2077-135100 0.2
1,2-Dichlorobenzene ug/L18.9 0.50 20.00 2078-12895 2
1,2-Dichloroethane ug/L19.5 0.50 20.00 2068-13198 1
1,2-Dichloropropane ug/L20.7 0.50 20.00 2077-130104 4
1,3,5-Trimethylbenzene ug/L20.0 0.50 20.00 2075-131100 3
1,3-Dichlorobenzene ug/L18.3 0.50 20.00 2077-12592 3
1,3-Dichloropropane ug/L19.7 0.50 20.00 2076-13298 2
1,4-Dichlorobenzene ug/L18.3 0.50 20.00 2075-12692 4
2,2-Dichloropropane ug/L19.0 2.0 20.00 2029-14995 3
2-Chlorotoluene ug/L20.2 0.50 20.00 2074-126101 3
4-Chlorotoluene ug/L19.8 0.50 20.00 2078-12999 4
4-Isopropyltoluene ug/L19.6 0.50 20.00 2069-13298 3
Acetone ug/L38.5 5.0 40.00 2040-16696 1
Acrolein ug/L48.7 20 40.00 2070-130122 4
Acrylonitrile ug/L43.5 20 40.00 2081-127109 3
Benzene ug/L20.3 0.50 20.00 2077-128102 3
Bromobenzene ug/L21.2 0.50 20.00 2078-129106 3
Bromochloromethane ug/L18.7 0.50 20.00 2078-13594 1
Bromodichloromethane ug/L19.6 0.50 20.00 2076-13898 2
Bromoform ug/L14.4 1.0 20.00 2071-13572 0.7
Bromomethane ug/L25.6 1.0 20.00 2041-168128 5
Carbon disulfide ug/L18.8 5.0 20.00 2059-13594 2
Carbon Tetrachloride ug/L15.4 0.50 20.00 2072-14277 2
Chlorobenzene ug/L19.6 0.50 20.00 2078-11998 4
Chloroethane ug/L23.5 0.50 20.00 2057-142118 6
Chloroform ug/L19.6 0.50 20.00 2077-13098 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7H0450 - 5030B
LCS Dup (P7H0450-BSD1)Prepared & Analyzed: 08/24/17
Chloromethane ug/L20.4 0.50 20.00 2047-145102 5
cis-1,2-Dichloroethylene ug/L20.6 0.50 20.00 2076-141103 3
cis-1,3-Dichloropropylene ug/L20.6 0.50 20.00 2065-140103 2
Dibromochloromethane ug/L15.9 0.50 20.00 2075-13479 3
Dibromomethane ug/L19.8 0.50 20.00 2076-13899 1
Dichlorodifluoromethane ug/L16.3 1.0 20.00 2028-16382 1
Ethylbenzene ug/L19.9 0.50 20.00 2080-127100 4
Hexachlorobutadiene ug/L15.7 2.0 20.00 2061-13479 7
Isopropyl Ether ug/L20.1 0.50 20.00 2060-154100 1
Isopropylbenzene (Cumene)ug/L19.0 0.50 20.00 2070-13095 5
m,p-Xylenes ug/L40.0 1.0 40.00 2077-133100 3
Methyl Butyl Ketone (2-Hexanone)ug/L21.9 5.0 20.00 2064-137109 3
Methyl Ethyl Ketone (2-Butanone)ug/L19.7 5.0 20.00 2071-13499 1
Methyl Isobutyl Ketone ug/L22.8 5.0 20.00 2069-134114 1
Methylene Chloride ug/L18.9 1.0 20.00 2073-13195 2
Methyl-tert-Butyl Ether ug/L20.6 0.50 20.00 2068-135103 0.05
Naphthalene ug/L19.0 1.0 20.00 2064-13695 0.8
n-Butylbenzene ug/L20.3 1.0 20.00 2068-134102 5
n-Propylbenzene ug/L20.2 0.50 20.00 2072-132101 4
o-Xylene ug/L19.2 0.50 20.00 2078-12896 4
sec-Butylbenzene ug/L19.0 0.50 20.00 2071-13195 4
Styrene ug/L20.3 0.50 20.00 2078-129102 4
tert-Butylbenzene ug/L18.0 0.50 20.00 2070-13290 4
Tetrachloroethylene ug/L16.0 0.50 20.00 2080-12980 5
Toluene ug/L19.9 0.50 20.00 2076-13199 3
trans-1,2-Dichloroethylene ug/L20.3 0.50 20.00 2076-135102 2
trans-1,3-Dichloropropylene ug/L20.2 0.50 20.00 2067-140101 0.3
Trichloroethylene ug/L17.5 0.50 20.00 2077-13388 2
Trichlorofluoromethane ug/L16.8 0.50 20.00 2062-14884 5
Vinyl acetate ug/L23.4 2.0 20.00 2034-167117 0.4
Vinyl chloride ug/L22.4 0.50 20.00 2057-141112 4
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 77-123Surrogate: Toluene-d8 10050.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7I0001 - 5035
Blank (P7I0001-BLK1)Prepared & Analyzed: 09/01/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7I0001 - 5035
Blank (P7I0001-BLK1)Prepared & Analyzed: 09/01/17
Methylene Chloride mg/kg wetBRL0.010
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10250.9
ug/L 50.00 76-129Surrogate: Toluene-d8 9849.1
LCS (P7I0001-BS1)Prepared & Analyzed: 09/01/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0459 0.0050 0.05000 72-11592
1,1,1-Trichloroethane mg/kg wet0.0450 0.0050 0.05000 67-13190
1,1,2,2-Tetrachloroethane mg/kg wet0.0452 0.0050 0.05000 56-12690
1,1,2-Trichloroethane mg/kg wet0.0452 0.0050 0.05000 70-13390
1,1-Dichloroethane mg/kg wet0.0446 0.0050 0.05000 74-12789
1,1-Dichloroethylene mg/kg wet0.0454 0.0050 0.05000 67-14991
1,1-Dichloropropylene mg/kg wet0.0445 0.0050 0.05000 71-13089
1,2,3-Trichlorobenzene mg/kg wet0.0473 0.0050 0.05000 68-13095
1,2,3-Trichloropropane mg/kg wet0.0454 0.0050 0.05000 60-13791
1,2,4-Trichlorobenzene mg/kg wet0.0481 0.0050 0.05000 66-12596
1,2,4-Trimethylbenzene mg/kg wet0.0451 0.0050 0.05000 69-12990
1,2-Dibromoethane mg/kg wet0.0469 0.0050 0.05000 70-13294
1,2-Dichlorobenzene mg/kg wet0.0448 0.0050 0.05000 72-12390
1,2-Dichloroethane mg/kg wet0.0439 0.0050 0.05000 68-12888
1,2-Dichloropropane mg/kg wet0.0437 0.0050 0.05000 73-13087
1,3,5-Trimethylbenzene mg/kg wet0.0443 0.0050 0.05000 69-12889
1,3-Dichlorobenzene mg/kg wet0.0453 0.0050 0.05000 71-12091
1,3-Dichloropropane mg/kg wet0.0450 0.0050 0.05000 75-12490
1,4-Dichlorobenzene mg/kg wet0.0445 0.0050 0.05000 71-12389
2,2-Dichloropropane mg/kg wet0.0462 0.0050 0.05000 50-14292
2-Chlorotoluene mg/kg wet0.0437 0.0050 0.05000 67-12487
4-Chlorotoluene mg/kg wet0.0444 0.0050 0.05000 71-12689
4-Isopropyltoluene mg/kg wet0.0458 0.0050 0.05000 68-12992
Acetone mg/kg wet0.109 0.050 0.1000 29-198109
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7I0001 - 5035
LCS (P7I0001-BS1)Prepared & Analyzed: 09/01/17
Benzene mg/kg wet0.0442 0.0030 0.05000 74-12788
Bromobenzene mg/kg wet0.0424 0.0050 0.05000 73-12585
Bromochloromethane mg/kg wet0.0462 0.0050 0.05000 72-13492
Bromodichloromethane mg/kg wet0.0438 0.0050 0.05000 75-12288
Bromoform mg/kg wet0.0466 0.0050 0.05000 66-13593
Bromomethane mg/kg wet0.0502 0.010 0.05000 20-180100
Carbon Tetrachloride mg/kg wet0.0455 0.0050 0.05000 64-14391
Chlorobenzene mg/kg wet0.0446 0.0050 0.05000 74-11889
Chloroethane mg/kg wet0.0431 0.010 0.05000 33-14986
Chloroform mg/kg wet0.0446 0.0050 0.05000 73-12789
Chloromethane mg/kg wet0.0484 0.0050 0.05000 45-14397
cis-1,2-Dichloroethylene mg/kg wet0.0442 0.0050 0.05000 76-13488
cis-1,3-Dichloropropylene mg/kg wet0.0452 0.0050 0.05000 71-12590
Dibromochloromethane mg/kg wet0.0451 0.0050 0.05000 73-12290
Dichlorodifluoromethane mg/kg wet0.0469 0.0050 0.05000 26-14694
Ethylbenzene mg/kg wet0.0449 0.0050 0.05000 74-12890
Isopropyl Ether mg/kg wet0.0450 0.0050 0.05000 59-15990
Isopropylbenzene (Cumene)mg/kg wet0.0452 0.0050 0.05000 68-12690
m,p-Xylenes mg/kg wet0.0919 0.010 0.1000 75-12492
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0515 0.050 0.05000 61-157103
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0467 0.10 0.05000 J63-14993
Methyl Isobutyl Ketone mg/kg wet0.0485 0.050 0.05000 J57-16297
Methylene Chloride mg/kg wet0.0474 0.010 0.05000 74-12995
Methyl-tert-Butyl Ether mg/kg wet0.0429 0.010 0.05000 70-13086
Naphthalene mg/kg wet0.0486 0.010 0.05000 57-15797
n-Butylbenzene mg/kg wet0.0453 0.0050 0.05000 65-13591
n-Propylbenzene mg/kg wet0.0442 0.0050 0.05000 67-13088
o-Xylene mg/kg wet0.0454 0.0050 0.05000 74-12691
sec-Butylbenzene mg/kg wet0.0449 0.0050 0.05000 66-13190
Styrene mg/kg wet0.0469 0.0050 0.05000 77-12194
tert-Butylbenzene mg/kg wet0.0455 0.0050 0.05000 67-13291
Tetrachloroethylene mg/kg wet0.0462 0.0050 0.05000 68-13092
Toluene mg/kg wet0.0440 0.0050 0.05000 71-12988
trans-1,2-Dichloroethylene mg/kg wet0.0449 0.0050 0.05000 73-13290
trans-1,3-Dichloropropylene mg/kg wet0.0447 0.0050 0.05000 68-12389
Trichloroethylene mg/kg wet0.0463 0.0050 0.05000 75-13393
Trichlorofluoromethane mg/kg wet0.0487 0.0050 0.05000 44-14697
Vinyl acetate mg/kg wet0.0521 0.025 0.05000 85-161104
Vinyl chloride mg/kg wet0.0450 0.0050 0.05000 48-14790
Xylenes, total mg/kg wet0.137 0.015 0.1500 74-12692
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.7
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7I0001 - 5035
LCS Dup (P7I0001-BSD1)Prepared & Analyzed: 09/01/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0450 0.0050 0.05000 2072-11590 2
1,1,1-Trichloroethane mg/kg wet0.0429 0.0050 0.05000 2067-13186 5
1,1,2,2-Tetrachloroethane mg/kg wet0.0459 0.0050 0.05000 2056-12692 2
1,1,2-Trichloroethane mg/kg wet0.0447 0.0050 0.05000 2070-13389 1
1,1-Dichloroethane mg/kg wet0.0431 0.0050 0.05000 2074-12786 3
1,1-Dichloroethylene mg/kg wet0.0430 0.0050 0.05000 2067-14986 5
1,1-Dichloropropylene mg/kg wet0.0428 0.0050 0.05000 2071-13086 4
1,2,3-Trichlorobenzene mg/kg wet0.0476 0.0050 0.05000 2068-13095 0.7
1,2,3-Trichloropropane mg/kg wet0.0465 0.0050 0.05000 2060-13793 2
1,2,4-Trichlorobenzene mg/kg wet0.0479 0.0050 0.05000 2066-12596 0.5
1,2,4-Trimethylbenzene mg/kg wet0.0442 0.0050 0.05000 2069-12988 2
1,2-Dibromoethane mg/kg wet0.0466 0.0050 0.05000 2070-13293 0.5
1,2-Dichlorobenzene mg/kg wet0.0440 0.0050 0.05000 2072-12388 2
1,2-Dichloroethane mg/kg wet0.0434 0.0050 0.05000 2068-12887 1
1,2-Dichloropropane mg/kg wet0.0422 0.0050 0.05000 2073-13084 3
1,3,5-Trimethylbenzene mg/kg wet0.0438 0.0050 0.05000 2069-12888 1
1,3-Dichlorobenzene mg/kg wet0.0448 0.0050 0.05000 2071-12090 1
1,3-Dichloropropane mg/kg wet0.0445 0.0050 0.05000 2075-12489 1
1,4-Dichlorobenzene mg/kg wet0.0441 0.0050 0.05000 2071-12388 0.9
2,2-Dichloropropane mg/kg wet0.0441 0.0050 0.05000 2050-14288 5
2-Chlorotoluene mg/kg wet0.0428 0.0050 0.05000 2067-12486 2
4-Chlorotoluene mg/kg wet0.0429 0.0050 0.05000 2071-12686 3
4-Isopropyltoluene mg/kg wet0.0442 0.0050 0.05000 2068-12988 4
Acetone mg/kg wet0.110 0.050 0.1000 2029-198110 0.8
Benzene mg/kg wet0.0427 0.0030 0.05000 2074-12785 3
Bromobenzene mg/kg wet0.0421 0.0050 0.05000 2073-12584 0.7
Bromochloromethane mg/kg wet0.0448 0.0050 0.05000 2072-13490 3
Bromodichloromethane mg/kg wet0.0428 0.0050 0.05000 2075-12286 2
Bromoform mg/kg wet0.0473 0.0050 0.05000 2066-13595 1
Bromomethane mg/kg wet0.0476 0.010 0.05000 2020-18095 5
Carbon Tetrachloride mg/kg wet0.0436 0.0050 0.05000 2064-14387 4
Chlorobenzene mg/kg wet0.0431 0.0050 0.05000 2074-11886 4
Chloroethane mg/kg wet0.0398 0.010 0.05000 2033-14980 8
Chloroform mg/kg wet0.0432 0.0050 0.05000 2073-12786 3
Chloromethane mg/kg wet0.0431 0.0050 0.05000 2045-14386 12
cis-1,2-Dichloroethylene mg/kg wet0.0425 0.0050 0.05000 2076-13485 4
cis-1,3-Dichloropropylene mg/kg wet0.0436 0.0050 0.05000 2071-12587 4
Dibromochloromethane mg/kg wet0.0456 0.0050 0.05000 2073-12291 1
Dichlorodifluoromethane mg/kg wet0.0466 0.0050 0.05000 2026-14693 0.6
Ethylbenzene mg/kg wet0.0431 0.0050 0.05000 2074-12886 4
Isopropyl Ether mg/kg wet0.0437 0.0050 0.05000 2059-15987 3
Isopropylbenzene (Cumene)mg/kg wet0.0441 0.0050 0.05000 2068-12688 3
m,p-Xylenes mg/kg wet0.0889 0.010 0.1000 2075-12489 3
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0517 0.050 0.05000 2061-157103 0.5
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0480 0.10 0.05000 20 J63-14996 3
Methyl Isobutyl Ketone mg/kg wet0.0485 0.050 0.05000 20 J57-16297 0.04
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7I0001 - 5035
LCS Dup (P7I0001-BSD1)Prepared & Analyzed: 09/01/17
Methylene Chloride mg/kg wet0.0461 0.010 0.05000 2074-12992 3
Methyl-tert-Butyl Ether mg/kg wet0.0426 0.010 0.05000 2070-13085 0.5
Naphthalene mg/kg wet0.0489 0.010 0.05000 2057-15798 0.8
n-Butylbenzene mg/kg wet0.0436 0.0050 0.05000 2065-13587 4
n-Propylbenzene mg/kg wet0.0432 0.0050 0.05000 2067-13086 2
o-Xylene mg/kg wet0.0448 0.0050 0.05000 2074-12690 1
sec-Butylbenzene mg/kg wet0.0433 0.0050 0.05000 2066-13187 3
Styrene mg/kg wet0.0454 0.0050 0.05000 2077-12191 3
tert-Butylbenzene mg/kg wet0.0441 0.0050 0.05000 2067-13288 3
Tetrachloroethylene mg/kg wet0.0443 0.0050 0.05000 2068-13089 4
Toluene mg/kg wet0.0420 0.0050 0.05000 2071-12984 5
trans-1,2-Dichloroethylene mg/kg wet0.0430 0.0050 0.05000 2073-13286 4
trans-1,3-Dichloropropylene mg/kg wet0.0439 0.0050 0.05000 2068-12388 2
Trichloroethylene mg/kg wet0.0449 0.0050 0.05000 2075-13390 3
Trichlorofluoromethane mg/kg wet0.0473 0.0050 0.05000 2044-14695 3
Vinyl acetate mg/kg wet0.0536 0.025 0.05000 2085-161107 3
Vinyl chloride mg/kg wet0.0424 0.0050 0.05000 2048-14785 6
Xylenes, total mg/kg wet0.134 0.015 0.1500 2074-12689 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.7
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7H0410 - 3546
Blank (P7H0410-BLK1)Prepared & Analyzed: 08/23/17
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7H0410 - 3546
Blank (P7H0410-BLK1)Prepared & Analyzed: 08/23/17
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 752.49
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 661.11
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 722.38
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 641.07
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 672.22
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 861.44
LCS (P7H0410-BS1)Prepared & Analyzed: 08/23/17
1,2,4-Trichlorobenzene mg/kg wet1.05 0.33 1.667 34-11863
1,2-Dichlorobenzene mg/kg wet0.954 0.33 1.667 33-11757
1,3-Dichlorobenzene mg/kg wet1.03 0.33 1.667 30-11562
1,4-Dichlorobenzene mg/kg wet1.00 0.33 1.667 31-11560
1-Methylnaphthalene mg/kg wet1.19 0.33 1.667 40-11972
2,4,6-Trichlorophenol mg/kg wet1.26 0.33 1.667 39-12675
2,4-Dichlorophenol mg/kg wet1.18 0.33 1.667 40-12271
2,4-Dimethylphenol mg/kg wet1.36 0.33 1.667 30-12782
2,4-Dinitrophenol mg/kg wet0.974 0.33 1.667 27-12958
2,4-Dinitrotoluene mg/kg wet1.27 0.33 1.667 48-12676
2,6-Dinitrotoluene mg/kg wet1.30 0.33 1.667 46-12478
2-Chloronaphthalene mg/kg wet1.23 0.33 1.667 41-11474
2-Chlorophenol mg/kg wet1.18 0.33 1.667 34-12171
2-Methylnaphthalene mg/kg wet1.15 0.33 1.667 38-12269
2-Methylphenol mg/kg wet1.27 0.33 1.667 32-12276
2-Nitrophenol mg/kg wet1.14 0.33 1.667 36-12368
3,3’-Dichlorobenzidine mg/kg wet1.26 0.33 1.667 22-12176
3/4-Methylphenol mg/kg wet1.10 0.33 1.667 34-11966
4,6-Dinitro-2-methylphenol mg/kg wet1.12 0.33 1.667 29-13267
4-Bromophenyl phenyl ether mg/kg wet1.22 0.33 1.667 46-12473
4-Chloro-3-methylphenol mg/kg wet1.23 0.33 1.667 45-12274
4-Chloroaniline mg/kg wet1.46 0.33 1.667 17-10687
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7H0410 - 3546
LCS (P7H0410-BS1)Prepared & Analyzed: 08/23/17
4-Chlorophenyl phenyl ether mg/kg wet1.27 0.33 1.667 45-12176
4-Nitrophenol mg/kg wet1.22 0.33 1.667 30-13273
Acenaphthene mg/kg wet1.28 0.33 1.667 40-12377
Acenaphthylene mg/kg wet1.35 0.33 1.667 32-13281
Anthracene mg/kg wet1.41 0.33 1.667 47-12385
Azobenzene mg/kg wet1.31 0.33 1.667 39-12579
Benzo(a)anthracene mg/kg wet1.34 0.33 1.667 49-12680
Benzo(a)pyrene mg/kg wet1.32 0.33 1.667 45-12979
Benzo(b)fluoranthene mg/kg wet1.29 0.33 1.667 45-13278
Benzo(g,h,i)perylene mg/kg wet1.30 0.33 1.667 43-13478
Benzo(k)fluoranthene mg/kg wet1.35 0.33 1.667 47-13281
Benzoic Acid mg/kg wet0.703 0.33 1.667 10-8342
Benzyl alcohol mg/kg wet1.11 0.33 1.667 29-12266
bis(2-Chloroethoxy)methane mg/kg wet1.15 0.33 1.667 36-12169
Bis(2-Chloroethyl)ether mg/kg wet0.924 0.33 1.667 31-12055
Bis(2-chloroisopropyl)ether mg/kg wet1.08 0.33 1.667 33-13165
Bis(2-Ethylhexyl)phthalate mg/kg wet1.31 0.33 1.667 51-13379
Butyl benzyl phthalate mg/kg wet1.29 0.33 1.667 48-13277
Chrysene mg/kg wet1.39 0.33 1.667 50-12484
Dibenzo(a,h)anthracene mg/kg wet0.934 0.33 1.667 45-13456
Dibenzofuran mg/kg wet1.29 0.33 1.667 44-12077
Diethyl phthalate mg/kg wet1.29 0.33 1.667 50-12477
Dimethyl phthalate mg/kg wet1.25 0.33 1.667 48-12475
Di-n-butyl phthalate mg/kg wet1.30 0.33 1.667 51-12878
Di-n-octyl phthalate mg/kg wet1.33 0.33 1.667 45-14080
Fluoranthene mg/kg wet1.36 0.33 1.667 50-12781
Fluorene mg/kg wet1.32 0.33 1.667 43-12579
Hexachlorobenzene mg/kg wet1.31 0.33 1.667 45-12279
Hexachlorobutadiene mg/kg wet1.12 0.33 1.667 32-12367
Hexachlorocyclopentadiene mg/kg wet1.18 0.33 1.667 32-11771
Hexachloroethane mg/kg wet1.01 0.33 1.667 28-11761
Indeno(1,2,3-cd)pyrene mg/kg wet1.49 0.33 1.667 45-13390
Isophorone mg/kg wet1.27 0.33 1.667 30-12276
Naphthalene mg/kg wet1.20 0.33 1.667 35-12372
Nitrobenzene mg/kg wet1.14 0.33 1.667 34-12268
N-Nitroso-di-n-propylamine mg/kg wet1.14 0.33 1.667 36-12068
N-Nitrosodiphenylamine mg/kg wet1.62 0.33 1.667 38-12797
Pentachlorophenol mg/kg wet1.28 0.33 1.667 25-13377
Phenanthrene mg/kg wet1.35 0.33 1.667 50-12181
Phenol mg/kg wet1.13 0.33 1.667 34-12168
Pyrene mg/kg wet1.30 0.33 1.667 47-12778
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 812.69
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 761.27
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 732.44
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 681.14
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 662.20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7H0410 - 3546
LCS (P7H0410-BS1)Prepared & Analyzed: 08/23/17
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 911.51
LCS Dup (P7H0410-BSD1)Prepared & Analyzed: 08/23/17
1,2,4-Trichlorobenzene mg/kg wet0.849 0.33 1.667 20 D34-11851 21
1,2-Dichlorobenzene mg/kg wet0.758 0.33 1.667 20 D33-11745 23
1,3-Dichlorobenzene mg/kg wet0.840 0.33 1.667 2030-11550 20
1,4-Dichlorobenzene mg/kg wet0.819 0.33 1.667 2031-11549 20
1-Methylnaphthalene mg/kg wet0.970 0.33 1.667 20 D40-11958 21
2,4,6-Trichlorophenol mg/kg wet1.10 0.33 1.667 2039-12666 14
2,4-Dichlorophenol mg/kg wet1.09 0.33 1.667 2040-12265 8
2,4-Dimethylphenol mg/kg wet1.28 0.33 1.667 2030-12777 6
2,4-Dinitrophenol mg/kg wet0.943 0.33 1.667 2027-12957 3
2,4-Dinitrotoluene mg/kg wet1.25 0.33 1.667 2048-12675 2
2,6-Dinitrotoluene mg/kg wet1.21 0.33 1.667 2046-12473 7
2-Chloronaphthalene mg/kg wet1.01 0.33 1.667 2041-11460 20
2-Chlorophenol mg/kg wet1.02 0.33 1.667 2034-12161 14
2-Methylnaphthalene mg/kg wet0.941 0.33 1.667 2038-12256 20
2-Methylphenol mg/kg wet0.973 0.33 1.667 20 D32-12258 26
2-Nitrophenol mg/kg wet0.936 0.33 1.667 2036-12356 19
3,3’-Dichlorobenzidine mg/kg wet1.38 0.33 1.667 2022-12183 9
3/4-Methylphenol mg/kg wet0.871 0.33 1.667 20 D34-11952 23
4,6-Dinitro-2-methylphenol mg/kg wet1.23 0.33 1.667 2029-13274 10
4-Bromophenyl phenyl ether mg/kg wet1.19 0.33 1.667 2046-12471 3
4-Chloro-3-methylphenol mg/kg wet1.10 0.33 1.667 2045-12266 12
4-Chloroaniline mg/kg wet1.28 0.33 1.667 2017-10677 13
4-Chlorophenyl phenyl ether mg/kg wet1.15 0.33 1.667 2045-12169 10
4-Nitrophenol mg/kg wet1.28 0.33 1.667 2030-13277 5
Acenaphthene mg/kg wet1.10 0.33 1.667 2040-12366 15
Acenaphthylene mg/kg wet1.15 0.33 1.667 2032-13269 16
Anthracene mg/kg wet1.41 0.33 1.667 2047-12385 0.05
Azobenzene mg/kg wet1.24 0.33 1.667 2039-12575 5
Benzo(a)anthracene mg/kg wet1.36 0.33 1.667 2049-12682 2
Benzo(a)pyrene mg/kg wet1.38 0.33 1.667 2045-12983 4
Benzo(b)fluoranthene mg/kg wet1.29 0.33 1.667 2045-13277 0.4
Benzo(g,h,i)perylene mg/kg wet1.35 0.33 1.667 2043-13481 3
Benzo(k)fluoranthene mg/kg wet1.39 0.33 1.667 2047-13283 3
Benzoic Acid mg/kg wet0.615 0.33 1.667 2010-8337 13
Benzyl alcohol mg/kg wet0.915 0.33 1.667 2029-12255 19
bis(2-Chloroethoxy)methane mg/kg wet0.949 0.33 1.667 2036-12157 19
Bis(2-Chloroethyl)ether mg/kg wet0.864 0.33 1.667 2031-12052 7
Bis(2-chloroisopropyl)ether mg/kg wet0.820 0.33 1.667 20 D33-13149 27
Bis(2-Ethylhexyl)phthalate mg/kg wet1.38 0.33 1.667 2051-13383 5
Butyl benzyl phthalate mg/kg wet1.33 0.33 1.667 2048-13280 3
Chrysene mg/kg wet1.44 0.33 1.667 2050-12487 4
Dibenzo(a,h)anthracene mg/kg wet0.993 0.33 1.667 2045-13460 6
Dibenzofuran mg/kg wet1.13 0.33 1.667 2044-12068 13
Diethyl phthalate mg/kg wet1.27 0.33 1.667 2050-12476 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7H0410 - 3546
LCS Dup (P7H0410-BSD1)Prepared & Analyzed: 08/23/17
Dimethyl phthalate mg/kg wet1.16 0.33 1.667 2048-12470 7
Di-n-butyl phthalate mg/kg wet1.36 0.33 1.667 2051-12881 4
Di-n-octyl phthalate mg/kg wet1.37 0.33 1.667 2045-14082 3
Fluoranthene mg/kg wet1.37 0.33 1.667 2050-12782 1
Fluorene mg/kg wet1.20 0.33 1.667 2043-12572 9
Hexachlorobenzene mg/kg wet1.30 0.33 1.667 2045-12278 2
Hexachlorobutadiene mg/kg wet0.983 0.33 1.667 2032-12359 13
Hexachlorocyclopentadiene mg/kg wet0.945 0.33 1.667 20 D32-11757 22
Hexachloroethane mg/kg wet0.764 0.33 1.667 20 D28-11746 28
Indeno(1,2,3-cd)pyrene mg/kg wet1.51 0.33 1.667 2045-13391 1
Isophorone mg/kg wet1.19 0.33 1.667 2030-12271 6
Naphthalene mg/kg wet0.972 0.33 1.667 20 D35-12358 21
Nitrobenzene mg/kg wet0.871 0.33 1.667 20 D34-12252 26
N-Nitroso-di-n-propylamine mg/kg wet0.905 0.33 1.667 20 D36-12054 23
N-Nitrosodiphenylamine mg/kg wet1.61 0.33 1.667 2038-12797 0.7
Pentachlorophenol mg/kg wet1.49 0.33 1.667 2025-13389 15
Phenanthrene mg/kg wet1.35 0.33 1.667 2050-12181 0.1
Phenol mg/kg wet1.12 0.33 1.667 2034-12167 2
Pyrene mg/kg wet1.31 0.33 1.667 2047-12779 1
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 812.70
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 621.03
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 501.68
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 550.914
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 642.14
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 931.54
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P7I0025 - MADEP VPH (S)
Blank (P7I0025-BLK1)Prepared & Analyzed: 09/05/17
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)919120
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)10310300
LCS (P7I0025-BS1)Prepared & Analyzed: 09/05/17
C5-C8 Aliphatics mg/kg wet34.2 5.0 32.00 70-130107
C9-C10 Aromatics mg/kg wet10.0 5.0 10.67 70-13094
C9-C12 Aliphatic mg/kg wet34.3 5.0 32.00 70-130107
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)909030
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)10010000
LCS Dup (P7I0025-BSD1)Prepared & Analyzed: 09/05/17
C5-C8 Aliphatics mg/kg wet34.0 5.0 32.00 5070-130106 0.7
C9-C10 Aromatics mg/kg wet9.79 5.0 10.67 5070-13092 2
C9-C12 Aliphatic mg/kg wet33.8 5.0 32.00 5070-130106 1
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)898910
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)1009970
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P7H0406 - 3546
Blank (P7H0406-BLK1)Prepared: 08/23/17 Analyzed: 08/24/17
C9-C18 Aliphatics mg/kg wet2.64 25 J
C19-C36 Aliphatics mg/kg wetBRL25
C11-C22 Aromatics mg/kg wetBRL10
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 561.12
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 631.26
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 843.37
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 1034.10
LCS (P7H0406-BS1)Prepared: 08/23/17 Analyzed: 08/24/17
C9-C18 Aliphatics mg/kg wet33.7 25 60.00 40-14056
C19-C36 Aliphatics mg/kg wet58.3 25 80.00 40-14073
C11-C22 Aromatics mg/kg wet13910 170.0 40-14082
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 611.22
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 721.43
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 873.48
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 1024.08
LCS Dup (P7H0406-BSD1)Prepared: 08/23/17 Analyzed: 08/24/17
C9-C18 Aliphatics mg/kg wet35.5 25 60.00 5040-14059 5
C19-C36 Aliphatics mg/kg wet59.1 25 80.00 5040-14074 1
C11-C22 Aromatics mg/kg wet14410 170.0 5040-14084 3
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 651.30
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 731.46
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 883.54
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 1024.08
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 47
9/5/17
Level II QC Report
5113 Yachtsman Ct.
Project: Belmont DyersProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 7080385
Time Submitted: 8/23/2017 8:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7H0526 - Solids, Dry Weight
Duplicate (P7H0526-DUP3)Prepared & Analyzed: 08/28/17 Source: 7080385-09
% Solids % by Weight83.9 0.100 83.1 200.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 47
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7H04067080385-07 08/23/17 11:3010.24 2g mL
P7H04067080385-08 08/23/17 11:3010.25 2g mL
P7H04067080385-09 08/23/17 11:3010.64 2g mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P7H05267080385-07 08/28/17 16:0030 30g g
P7H05267080385-08 08/28/17 16:0030 30g g
P7H05267080385-09 08/28/17 16:0030 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7H04107080385-07 08/23/17 11:3030.45 1g mL
P7H04107080385-08 08/23/17 11:3030.19 1g mL
P7H04107080385-09 08/23/17 11:3030.26 1g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7H04507080385-01 08/24/17 10:4210 10mL mL
P7H04507080385-02 08/24/17 10:4210 10mL mL
P7H04507080385-03 08/24/17 10:4210 10mL mL
P7H04507080385-04 08/24/17 10:4210 10mL mL
P7H04507080385-04 08/24/17 10:4210 10mL mL
P7H04507080385-05 08/24/17 10:4210 10mL mL
P7H04507080385-06 08/24/17 10:4210 10mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7I00017080385-07 09/01/17 9:345.15 5g mL
P7I00017080385-08 09/01/17 9:346.02 5g mL
P7I00017080385-09 09/01/17 9:344.87 5g mL
Prep Method: MADEP VPH (S)
Lab Number Batch Date/TimeInitialFinal
P7I00257080385-07 09/05/17 8:1219.81 16g mL
P7I00257080385-08 09/05/17 8:1220.14 16g mL
P7I00257080385-09 09/05/17 8:1219.55 16g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 47
Page 47 of 47

APPENDIX C

SOIL GAS LABORATORY ANALYTICAL RESULTS
Soil Gas Analytical Results
Former Belmont Dyers Site
Belmont, North Carolina
Residential
Vapor
Intrusion
Screening
Levels
Residential
Soil-Gas
ug/m3
PES-SG-6 PES-SG-7 PES-SG-8A PES-SG-8B
Sampling Date 8/3/2017 4:26 PM 8/3/2017 5:05 PM 8/3/2017 5:38 PM 8/3/2017 5:38 PM
Sample Depth - Feet - Feet - Feet - FeetEPA TO-15Acetone 216000 ND (33)57 J 60 ND (19)Benzene 120 6.5 3.1 J 3.7 3.8Benzyl Chloride 6.95 ND (2.3)ND (2.3)ND (1.5)ND (1.3)Bromodichloromethane 21.9 ND (4.3)ND (4.3)ND (2.7)ND (2.5)Bromoform ~ND (6.3)ND (6.3)ND (3.9)ND (3.6)Bromomethane 34.8 ND (3.1)ND (3.1)ND (1.9)ND (1.8)1,3-Butadiene 13.9 ND (1.7)ND (1.7)ND (1.1)ND (0.98)2-Butanone (MEK)34800 8.4 J 5.8 J 6.9 J 3.1 JCarbon Disulfide 4870 32 8.5 J 7.1 J 7.4 JCarbon Tetrachloride 156 ND (4.5)ND (4.5)ND (2.8)ND (2.6)
Chlorobenzene 348 ND (2.9)ND (2.9)ND (1.8)ND (1.7)
Chloroethane 69500 ND (2.2)ND (2.2)ND (1.3)ND (1.2)
Chloroform 40.7 ND (3.6)ND (3.6)ND (2.2)ND (2.1)
Chloromethane 626 6.3 ND (1.7)2.8 2.3 J
Cyclohexane 41700 75 ND (2.0)9.1 8.7
Dibromochloromethane 34.7 ND (5.6)ND (5.6)ND (3.5)ND (3.3)
1,2-Dibromoethane (EDB)1.56 ND (5.0)ND (5.0)ND (3.1)ND (2.9)
1,2-Dichlorobenzene 1390 ND (4.0)ND (4.0)ND (2.5)ND (2.3)
1,3-Dichlorobenzene ~26 14 15 16
1,4-Dichlorobenzene 73.7 ND (4.2)ND (4.2)ND (2.6)ND (2.4)
Dichlorodifluoromethane (Freon 12)695 ND (3.7)ND (3.7)ND (2.3)ND (2.2)
1,1-Dichloroethane 507 ND (2.8)ND (2.8)ND (1.8)ND (1.6)
1,2-Dichloroethane 36 ND (2.9)ND (2.9)ND (1.8)ND (1.7)
1,1-Dichloroethylene 1390 ND (2.9)ND (2.9)ND (1.8)ND (1.7)cis-1,2-Dichloroethylene ~ND (2.7)ND (2.7)ND (1.7)ND (1.6)trans-1,2-Dichloroethylene 417 ND (3.0)ND (3.0)ND (1.9)ND (1.7)1,2-Dichloropropane 27.8 ND (3.2)ND (3.2)ND (2.0)ND (1.8)cis-1,3-Dichloropropene ~ND (3.9)ND (3.9)ND (2.4)ND (2.3)trans-1,3-Dichloropropene ~ND (2.8)ND (2.8)ND (1.7)ND (1.6)1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)~ND (5.7)ND (5.7)ND (3.6)ND (3.3)1,4-Dioxane ~ND (23)ND (23)ND (14)ND (13)Ethanol ~ND (34)ND (34)ND (21)ND (19)Ethyl Acetate ~ND (3.1)ND (3.1)ND (1.9)ND (1.8)Ethylbenzene 374 ND (2.9)ND (2.9)2.8 2.5
Parameter
SAMPLING LOCATION
Page 1
Soil Gas Analytical Results
Former Belmont Dyers Site
Belmont, North Carolina
4-Ethyltoluene ~ND (3.2)ND (3.2)ND (2.0)ND (1.8)
Heptane ~11 ND (2.7)5.0 5.1
Hexachlorobutadiene ~ND (8.1)ND (8.1)ND (5.1)ND (4.7)
Hexane 4870 22 J 8.3 J 8.7 J 8.6 J
2-Hexanone (MBK)209 ND (2.4)ND (2.4)4.4 ND (1.4)
Isopropanol ~3.2 J ND (3.0)ND (1.9)ND (1.7)
Methyl tert-Butyl Ether (MTBE)3600 ND (2.5)3.5 J 2.2 J 1.5 J
Methylene Chloride 4170 ND (4.2)ND (4.2)ND (2.6)ND (2.4)
4-Methyl-2-pentanone (MIBK)20900 ND (3.5)ND (3.5)4.6 4.2
Naphthalene 20.9 9.1 Z-01, J 9.6 Z-01, J 7.6 Z-01, J 7.6 Z-01, J
Propene 20900 350 52 J 79 79
Styrene 6950 ND (2.8)ND (2.8)ND (1.7)ND (1.6)
1,1,2,2-Tetrachloroethane 16.1 ND (4.3)ND (4.3)ND (2.6)ND (2.5)Tetrachloroethylene 278 1400 1000 33 47Tetrahydrofuran13900ND (2.0)ND (2.0)ND (1.3)ND (1.2)Toluene 34800 9.3 9.6 24 241,2,4-Trichlorobenzene 13.9 20 Z-01 16 Z-01 12 Z-01 13 Z-011,1,1-Trichloroethane 34800 4.0 J ND (3.8)ND (2.4)ND (2.2)1,1,2-Trichloroethane 1.39 ND (3.5)ND (3.5)ND (2.2)ND (2.0)Trichloroethylene 13.9 20 ND (3.4)ND (2.1)ND (2.0)Trichlorofluoromethane 4870 13 J 4.9 J ND (2.9)ND (2.7)1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)209000 ND (5.3)ND (5.3)ND (3.3)ND (3.1)1,2,4-Trimethylbenzene 48.7 ND (3.2)ND (3.2)2.7 J 2.1 J1,3,5-Trimethylbenzene ~ND (3.4)ND (3.4)ND (2.1)ND (1.9)Vinyl Acetate 1390 ND (2.1)ND (2.1)ND (1.3)ND (1.2)
Vinyl Chloride 55.9 2.5 J ND (1.9)ND (1.2)1.3 J
Xylene, m&p 695 6.9 J ND (5.6)10 9.9
Xylene, o-695 3.5 J ND (2.7)3.6 3.3
NOTES:
1. ND = Not detected above the lab reporting limits shown in parenthesis.
2. NT = Not tested.
3. ~ = No IHSB Residential or Non-Residential screening limits limits.
4. Values in italics exceed the IHSB Residential Indoor Air Screening Limits.
5. Bold values exceed the IHSB Non-Residential Indoor Air Screening Limits.
6. Yellow Shaded values exceed the IHSB Residential Soil-Gas Screening Limits.
7. Red Shaded values exceed the IHSB Non-Residential Soil-Gas Screening Limits.8. IHSB Residential/Non-Residential screening limits displayed for Xylenes are for the summation of all isomers and not for the individual isomer. Cells for individual isomers might not be in italics, and/or
shaded when the summation (total amount of all isomers) exceeds the limits for these parameters. User discretion is advised when interpreting these results.
9. Con-Test Laboratory is not responsible for the regulatory content, data comparisons with regulations, or decisions made based on data comparisons shown in this deliverable. Please notify us should
you be aware of any regulatory information that may not be correct or that has changed.
10. Bolded and shaded concentrations exceed the IHSB residential vapor intrusion screening levels for the respective consitutent.
Page 2
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 16, 2017
Robert Hill
RDH Environmental Consulting
4012 Ridgebrook Bluffs Drive
Raleigh, NC 27603
Project Location: Belmont Dyers Site - Belmont, NC
Client Job Number:
Project Number: 1725.00
Laboratory Work Order Number: 17H0494
Enclosed are results of analyses for samples received by the laboratory on August 4, 2017. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/16/2017RDH Environmental Consulting
4012 Ridgebrook Bluffs Drive
Raleigh, NC 27603
ATTN: Robert Hill
1725.00
17H0494
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Belmont Dyers Site - Belmont, NC
PES-SG-6 17H0494-06 Soil Gas EPA TO-15
PES-SG-7 17H0494-07 Soil Gas EPA TO-15
PES-SG-8A 17H0494-08 Soil Gas EPA TO-15
PES-SG-8B 17H0494-09 Soil Gas EPA TO-15
Page 2 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method TO-15, Samples 17H0494-06,-07,-08,-09 couldn t be run at a lower dilution due to limited sample volume.
EPA TO-15
Qualifications:
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in
house limits of 50-150%.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene, Naphthalene
17H0494-06[PES-SG-6], 17H0494-07[PES-SG-7], 17H0494-08[PES-SG-8A], 17H0494-09[PES-SG-8B], B184271-BS1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 3 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-6
Sample ID: 17H0494-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -3.5
Sampled: 8/3/2017 16:26
Canister ID: 1590
Flow Controller ID: 4201
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 40 8/15/17 22:04 CMRND20951433
Benzene 2.0 1.0 8/15/17 22:04 CMR6.5 203.20.64 2.0
Benzyl chloride ND 1.0 8/15/17 22:04 CMRND205.20.45 2.3
Bromodichloromethane ND 1.0 8/15/17 22:04 CMRND206.70.65 4.3
Bromoform ND 1.0 8/15/17 22:04 CMRND20100.61 6.3
Bromomethane ND 1.0 8/15/17 22:04 CMRND203.90.79 3.1
1,3-Butadiene ND 1.0 8/15/17 22:04 CMRND202.20.76 1.7
2-Butanone (MEK)2.9 40 8/15/17 22:04 CMRJ8.4 201200.75 2.2
Carbon Disulfide 10 10 8/15/17 22:04 CMR32 20310.68 2.1
Carbon Tetrachloride ND 1.0 8/15/17 22:04 CMRND206.30.72 4.5
Chlorobenzene ND 1.0 8/15/17 22:04 CMRND204.60.63 2.9
Chloroethane ND 2.0 8/15/17 22:04 CMRND205.30.82 2.2
Chloroform ND 1.0 8/15/17 22:04 CMRND204.90.73 3.6
Chloromethane 3.1 2.0 8/15/17 22:04 CMR6.3 204.10.83 1.7
Cyclohexane 22 1.0 8/15/17 22:04 CMR75 203.40.58 2.0
Dibromochloromethane ND 1.0 8/15/17 22:04 CMRND208.50.66 5.6
1,2-Dibromoethane (EDB)ND 1.0 8/15/17 22:04 CMRND207.70.65 5.0
1,2-Dichlorobenzene ND 1.0 8/15/17 22:04 CMRND206.00.66 4.0
1,3-Dichlorobenzene 4.3 1.0 8/15/17 22:04 CMR26 206.00.60 3.6
1,4-Dichlorobenzene ND 1.0 8/15/17 22:04 CMRND206.00.69 4.2
Dichlorodifluoromethane (Freon 12)ND 1.0 8/15/17 22:04 CMRND204.90.76 3.7
1,1-Dichloroethane ND 1.0 8/15/17 22:04 CMRND204.00.70 2.8
1,2-Dichloroethane ND 1.0 8/15/17 22:04 CMRND204.00.71 2.9
1,1-Dichloroethylene ND 1.0 8/15/17 22:04 CMRND204.00.73 2.9
cis-1,2-Dichloroethylene ND 1.0 8/15/17 22:04 CMRND204.00.68 2.7
trans-1,2-Dichloroethylene ND 1.0 8/15/17 22:04 CMRND204.00.75 3.0
1,2-Dichloropropane ND 1.0 8/15/17 22:04 CMRND204.60.69 3.2
cis-1,3-Dichloropropene ND 1.0 8/15/17 22:04 CMRND204.50.87 3.9
trans-1,3-Dichloropropene ND 1.0 8/15/17 22:04 CMRND204.50.61 2.8
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 1.0 8/15/17 22:04 CMRND207.00.82 5.7
1,4-Dioxane ND 10 8/15/17 22:04 CMRND20366.4 23
Ethanol ND 40 8/15/17 22:04 CMRND20751834
Ethyl Acetate ND 2.0 8/15/17 22:04 CMRND207.20.85 3.1
Ethylbenzene ND 1.0 8/15/17 22:04 CMRND204.30.66 2.9
4-Ethyltoluene ND 1.0 8/15/17 22:04 CMRND204.90.65 3.2
Heptane 2.7 1.0 8/15/17 22:04 CMR11 204.10.66 2.7
Hexachlorobutadiene ND 1.0 8/15/17 22:04 CMRND20110.76 8.1
Hexane 6.2 40 8/15/17 22:04 CMRJ22 201401.8 6.2
2-Hexanone (MBK)ND 1.0 8/15/17 22:04 CMRND204.10.59 2.4
Isopropanol 1.3 40 8/15/17 22:04 CMRJ3.2 20981.2 3.0
Methyl tert-Butyl Ether (MTBE)ND 1.0 8/15/17 22:04 CMRND203.60.68 2.5
Methylene Chloride ND 10 8/15/17 22:04 CMRND20351.2 4.2
4-Methyl-2-pentanone (MIBK)ND 1.0 8/15/17 22:04 CMRND204.10.85 3.5
Naphthalene 1.7 4.0 8/15/17 22:04 CMRZ-01, J 9.1 20210.87 4.5
Propene 200 40 8/15/17 22:04 CMR350 20693.1 5.3
Styrene ND 1.0 8/15/17 22:04 CMRND204.30.65 2.8
1,1,2,2-Tetrachloroethane ND 1.0 8/15/17 22:04 CMRND206.90.62 4.3
Page 4 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-6
Sample ID: 17H0494-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -3.5
Sampled: 8/3/2017 16:26
Canister ID: 1590
Flow Controller ID: 4201
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 200 1.0 8/15/17 22:04 CMR1400 206.80.61 4.1
Tetrahydrofuran ND 2.0 8/15/17 22:04 CMRND205.90.69 2.0
Toluene 2.5 1.0 8/15/17 22:04 CMR9.3 203.80.63 2.4
1,2,4-Trichlorobenzene 2.6 1.0 8/15/17 22:04 CMRZ-01 20 207.40.74 5.5
1,1,1-Trichloroethane 0.74 1.0 8/15/17 22:04 CMRJ4.0 205.50.69 3.8
1,1,2-Trichloroethane ND 1.0 8/15/17 22:04 CMRND205.50.64 3.5
Trichloroethylene 3.7 1.0 8/15/17 22:04 CMR20 205.40.63 3.4
Trichlorofluoromethane (Freon 11)2.3 4.0 8/15/17 22:04 CMRJ13 20220.84 4.7
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 4.0 8/15/17 22:04 CMRND20310.69 5.3
1,2,4-Trimethylbenzene ND 1.0 8/15/17 22:04 CMRND204.90.65 3.2
1,3,5-Trimethylbenzene ND 1.0 8/15/17 22:04 CMRND204.90.68 3.4
Vinyl Acetate ND 20 8/15/17 22:04 CMRND20700.61 2.1
Vinyl Chloride 0.98 1.0 8/15/17 22:04 CMRJ2.5 202.60.74 1.9
m&p-Xylene 1.6 2.0 8/15/17 22:04 CMRJ6.9 208.71.3 5.6
o-Xylene 0.80 1.0 8/15/17 22:04 CMRJ3.5 204.30.62 2.7
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)100 8/15/17 22:0470-130
Page 5 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-7
Sample ID: 17H0494-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -6.2
Sampled: 8/3/2017 17:05
Canister ID: 1576
Flow Controller ID: 4213
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 24 40 8/15/17 21:27 CMRJ57 20951433
Benzene 0.98 1.0 8/15/17 21:27 CMRJ3.1 203.20.64 2.0
Benzyl chloride ND 1.0 8/15/17 21:27 CMRND205.20.45 2.3
Bromodichloromethane ND 1.0 8/15/17 21:27 CMRND206.70.65 4.3
Bromoform ND 1.0 8/15/17 21:27 CMRND20100.61 6.3
Bromomethane ND 1.0 8/15/17 21:27 CMRND203.90.79 3.1
1,3-Butadiene ND 1.0 8/15/17 21:27 CMRND202.20.76 1.7
2-Butanone (MEK)2.0 40 8/15/17 21:27 CMRJ5.8 201200.75 2.2
Carbon Disulfide 2.7 10 8/15/17 21:27 CMRJ8.5 20310.68 2.1
Carbon Tetrachloride ND 1.0 8/15/17 21:27 CMRND206.30.72 4.5
Chlorobenzene ND 1.0 8/15/17 21:27 CMRND204.60.63 2.9
Chloroethane ND 2.0 8/15/17 21:27 CMRND205.30.82 2.2
Chloroform ND 1.0 8/15/17 21:27 CMRND204.90.73 3.6
Chloromethane ND 2.0 8/15/17 21:27 CMRND204.10.83 1.7
Cyclohexane ND 1.0 8/15/17 21:27 CMRND203.40.58 2.0
Dibromochloromethane ND 1.0 8/15/17 21:27 CMRND208.50.66 5.6
1,2-Dibromoethane (EDB)ND 1.0 8/15/17 21:27 CMRND207.70.65 5.0
1,2-Dichlorobenzene ND 1.0 8/15/17 21:27 CMRND206.00.66 4.0
1,3-Dichlorobenzene 2.3 1.0 8/15/17 21:27 CMR14 206.00.60 3.6
1,4-Dichlorobenzene ND 1.0 8/15/17 21:27 CMRND206.00.69 4.2
Dichlorodifluoromethane (Freon 12)ND 1.0 8/15/17 21:27 CMRND204.90.76 3.7
1,1-Dichloroethane ND 1.0 8/15/17 21:27 CMRND204.00.70 2.8
1,2-Dichloroethane ND 1.0 8/15/17 21:27 CMRND204.00.71 2.9
1,1-Dichloroethylene ND 1.0 8/15/17 21:27 CMRND204.00.73 2.9
cis-1,2-Dichloroethylene ND 1.0 8/15/17 21:27 CMRND204.00.68 2.7
trans-1,2-Dichloroethylene ND 1.0 8/15/17 21:27 CMRND204.00.75 3.0
1,2-Dichloropropane ND 1.0 8/15/17 21:27 CMRND204.60.69 3.2
cis-1,3-Dichloropropene ND 1.0 8/15/17 21:27 CMRND204.50.87 3.9
trans-1,3-Dichloropropene ND 1.0 8/15/17 21:27 CMRND204.50.61 2.8
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 1.0 8/15/17 21:27 CMRND207.00.82 5.7
1,4-Dioxane ND 10 8/15/17 21:27 CMRND20366.4 23
Ethanol ND 40 8/15/17 21:27 CMRND20751834
Ethyl Acetate ND 2.0 8/15/17 21:27 CMRND207.20.85 3.1
Ethylbenzene ND 1.0 8/15/17 21:27 CMRND204.30.66 2.9
4-Ethyltoluene ND 1.0 8/15/17 21:27 CMRND204.90.65 3.2
Heptane ND 1.0 8/15/17 21:27 CMRND204.10.66 2.7
Hexachlorobutadiene ND 1.0 8/15/17 21:27 CMRND20110.76 8.1
Hexane 2.4 40 8/15/17 21:27 CMRJ8.3 201401.8 6.2
2-Hexanone (MBK)ND 1.0 8/15/17 21:27 CMRND204.10.59 2.4
Isopropanol ND 40 8/15/17 21:27 CMRND20981.2 3.0
Methyl tert-Butyl Ether (MTBE)0.96 1.0 8/15/17 21:27 CMRJ3.5 203.60.68 2.5
Methylene Chloride ND 10 8/15/17 21:27 CMRND20351.2 4.2
4-Methyl-2-pentanone (MIBK)ND 1.0 8/15/17 21:27 CMRND204.10.85 3.5
Naphthalene 1.8 4.0 8/15/17 21:27 CMRZ-01, J 9.6 20210.87 4.5
Propene 30 40 8/15/17 21:27 CMRJ52 20693.1 5.3
Styrene ND 1.0 8/15/17 21:27 CMRND204.30.65 2.8
1,1,2,2-Tetrachloroethane ND 1.0 8/15/17 21:27 CMRND206.90.62 4.3
Page 6 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-7
Sample ID: 17H0494-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -6.2
Sampled: 8/3/2017 17:05
Canister ID: 1576
Flow Controller ID: 4213
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 150 1.0 8/15/17 21:27 CMR1000 206.80.61 4.1
Tetrahydrofuran ND 2.0 8/15/17 21:27 CMRND205.90.69 2.0
Toluene 2.5 1.0 8/15/17 21:27 CMR9.6 203.80.63 2.4
1,2,4-Trichlorobenzene 2.2 1.0 8/15/17 21:27 CMRZ-01 16 207.40.74 5.5
1,1,1-Trichloroethane ND 1.0 8/15/17 21:27 CMRND205.50.69 3.8
1,1,2-Trichloroethane ND 1.0 8/15/17 21:27 CMRND205.50.64 3.5
Trichloroethylene ND 1.0 8/15/17 21:27 CMRND205.40.63 3.4
Trichlorofluoromethane (Freon 11)0.88 4.0 8/15/17 21:27 CMRJ4.9 20220.84 4.7
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 4.0 8/15/17 21:27 CMRND20310.69 5.3
1,2,4-Trimethylbenzene ND 1.0 8/15/17 21:27 CMRND204.90.65 3.2
1,3,5-Trimethylbenzene ND 1.0 8/15/17 21:27 CMRND204.90.68 3.4
Vinyl Acetate ND 20 8/15/17 21:27 CMRND20700.61 2.1
Vinyl Chloride ND 1.0 8/15/17 21:27 CMRND202.60.74 1.9
m&p-Xylene ND 2.0 8/15/17 21:27 CMRND208.71.3 5.6
o-Xylene ND 1.0 8/15/17 21:27 CMRND204.30.62 2.7
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)100 8/15/17 21:2770-130
Page 7 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-8A
Sample ID: 17H0494-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -7.7
Sampled: 8/3/2017 17:38
Canister ID: 1574
Flow Controller ID: 4040
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 25 25 8/15/17 20:47 CMR60 12.5598.6 21
Benzene 1.2 0.62 8/15/17 20:47 CMR3.7 12.52.00.40 1.3
Benzyl chloride ND 0.62 8/15/17 20:47 CMRND12.53.20.28 1.5
Bromodichloromethane ND 0.62 8/15/17 20:47 CMRND12.54.20.40 2.7
Bromoform ND 0.62 8/15/17 20:47 CMRND12.56.40.38 3.9
Bromomethane ND 0.62 8/15/17 20:47 CMRND12.52.40.49 1.9
1,3-Butadiene ND 0.62 8/15/17 20:47 CMRND12.51.40.48 1.1
2-Butanone (MEK)2.3 25 8/15/17 20:47 CMRJ6.9 12.5730.46 1.4
Carbon Disulfide 2.3 6.2 8/15/17 20:47 CMRJ7.1 12.5190.42 1.3
Carbon Tetrachloride ND 0.62 8/15/17 20:47 CMRND12.53.90.45 2.8
Chlorobenzene ND 0.62 8/15/17 20:47 CMRND12.52.90.39 1.8
Chloroethane ND 1.2 8/15/17 20:47 CMRND12.53.30.51 1.3
Chloroform ND 0.62 8/15/17 20:47 CMRND12.53.00.46 2.2
Chloromethane 1.3 1.2 8/15/17 20:47 CMR2.8 12.52.60.51 1.1
Cyclohexane 2.6 0.62 8/15/17 20:47 CMR9.1 12.52.10.36 1.3
Dibromochloromethane ND 0.62 8/15/17 20:47 CMRND12.55.30.41 3.5
1,2-Dibromoethane (EDB)ND 0.62 8/15/17 20:47 CMRND12.54.80.41 3.1
1,2-Dichlorobenzene ND 0.62 8/15/17 20:47 CMRND12.53.70.41 2.5
1,3-Dichlorobenzene 2.6 0.62 8/15/17 20:47 CMR15 12.53.70.37 2.2
1,4-Dichlorobenzene ND 0.62 8/15/17 20:47 CMRND12.53.70.43 2.6
Dichlorodifluoromethane (Freon 12)ND 0.62 8/15/17 20:47 CMRND12.53.10.47 2.3
1,1-Dichloroethane ND 0.62 8/15/17 20:47 CMRND12.52.50.44 1.8
1,2-Dichloroethane ND 0.62 8/15/17 20:47 CMRND12.52.50.44 1.8
1,1-Dichloroethylene ND 0.62 8/15/17 20:47 CMRND12.52.50.45 1.8
cis-1,2-Dichloroethylene ND 0.62 8/15/17 20:47 CMRND12.52.50.42 1.7
trans-1,2-Dichloroethylene ND 0.62 8/15/17 20:47 CMRND12.52.50.47 1.9
1,2-Dichloropropane ND 0.62 8/15/17 20:47 CMRND12.52.90.43 2.0
cis-1,3-Dichloropropene ND 0.62 8/15/17 20:47 CMRND12.52.80.54 2.4
trans-1,3-Dichloropropene ND 0.62 8/15/17 20:47 CMRND12.52.80.38 1.7
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.62 8/15/17 20:47 CMRND12.54.40.51 3.6
1,4-Dioxane ND 6.2 8/15/17 20:47 CMRND12.5224.0 14
Ethanol ND 25 8/15/17 20:47 CMRND12.5471121
Ethyl Acetate ND 1.2 8/15/17 20:47 CMRND12.54.50.53 1.9
Ethylbenzene 0.65 0.62 8/15/17 20:47 CMR2.8 12.52.70.41 1.8
4-Ethyltoluene ND 0.62 8/15/17 20:47 CMRND12.53.10.40 2.0
Heptane 1.2 0.62 8/15/17 20:47 CMR5.0 12.52.60.41 1.7
Hexachlorobutadiene ND 0.62 8/15/17 20:47 CMRND12.56.60.48 5.1
Hexane 2.5 25 8/15/17 20:47 CMRJ8.7 12.5881.1 3.9
2-Hexanone (MBK)1.1 0.62 8/15/17 20:47 CMR4.4 12.52.60.37 1.5
Isopropanol ND 25 8/15/17 20:47 CMRND12.5610.76 1.9
Methyl tert-Butyl Ether (MTBE)0.60 0.62 8/15/17 20:47 CMRJ2.2 12.52.20.42 1.5
Methylene Chloride ND 6.2 8/15/17 20:47 CMRND12.5220.76 2.6
4-Methyl-2-pentanone (MIBK)1.1 0.62 8/15/17 20:47 CMR4.6 12.52.60.53 2.2
Naphthalene 1.5 2.5 8/15/17 20:47 CMRZ-01, J 7.6 12.5130.54 2.8
Propene 46 25 8/15/17 20:47 CMR79 12.5431.9 3.3
Styrene ND 0.62 8/15/17 20:47 CMRND12.52.70.40 1.7
1,1,2,2-Tetrachloroethane ND 0.62 8/15/17 20:47 CMRND12.54.30.39 2.6
Page 8 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-8A
Sample ID: 17H0494-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -7.7
Sampled: 8/3/2017 17:38
Canister ID: 1574
Flow Controller ID: 4040
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 4.8 0.62 8/15/17 20:47 CMR33 12.54.20.38 2.6
Tetrahydrofuran ND 1.2 8/15/17 20:47 CMRND12.53.70.43 1.3
Toluene 6.4 0.62 8/15/17 20:47 CMR24 12.52.30.39 1.5
1,2,4-Trichlorobenzene 1.6 0.62 8/15/17 20:47 CMRZ-01 12 12.54.60.46 3.4
1,1,1-Trichloroethane ND 0.62 8/15/17 20:47 CMRND12.53.40.43 2.4
1,1,2-Trichloroethane ND 0.62 8/15/17 20:47 CMRND12.53.40.40 2.2
Trichloroethylene ND 0.62 8/15/17 20:47 CMRND12.53.30.39 2.1
Trichlorofluoromethane (Freon 11)ND 2.5 8/15/17 20:47 CMRND12.5140.52 2.9
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 2.5 8/15/17 20:47 CMRND12.5190.43 3.3
1,2,4-Trimethylbenzene 0.55 0.62 8/15/17 20:47 CMRJ2.7 12.53.10.40 2.0
1,3,5-Trimethylbenzene ND 0.62 8/15/17 20:47 CMRND12.53.10.42 2.1
Vinyl Acetate ND 12 8/15/17 20:47 CMRND12.5440.38 1.3
Vinyl Chloride ND 0.62 8/15/17 20:47 CMRND12.51.60.46 1.2
m&p-Xylene 2.4 1.2 8/15/17 20:47 CMR10 12.55.40.81 3.5
o-Xylene 0.83 0.62 8/15/17 20:47 CMR3.6 12.52.70.39 1.7
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)100 8/15/17 20:4770-130
Page 9 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-8B
Sample ID: 17H0494-09
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -7.7
Sampled: 8/3/2017 17:38
Canister ID: 1589
Flow Controller ID: 4040
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 23 8/15/17 20:04 CMRND11.6558.0 19
Benzene 1.2 0.58 8/15/17 20:04 CMR3.8 11.61.80.37 1.2
Benzyl chloride ND 0.58 8/15/17 20:04 CMRND11.63.00.26 1.3
Bromodichloromethane ND 0.58 8/15/17 20:04 CMRND11.63.90.37 2.5
Bromoform ND 0.58 8/15/17 20:04 CMRND11.66.00.35 3.6
Bromomethane ND 0.58 8/15/17 20:04 CMRND11.62.20.45 1.8
1,3-Butadiene ND 0.58 8/15/17 20:04 CMRND11.61.30.44 0.98
2-Butanone (MEK)1.1 23 8/15/17 20:04 CMRJ3.1 11.6680.43 1.3
Carbon Disulfide 2.4 5.8 8/15/17 20:04 CMRJ7.4 11.6180.39 1.2
Carbon Tetrachloride ND 0.58 8/15/17 20:04 CMRND11.63.60.41 2.6
Chlorobenzene ND 0.58 8/15/17 20:04 CMRND11.62.70.37 1.7
Chloroethane ND 1.2 8/15/17 20:04 CMRND11.63.00.47 1.2
Chloroform ND 0.58 8/15/17 20:04 CMRND11.62.80.42 2.1
Chloromethane 1.1 1.2 8/15/17 20:04 CMRJ2.3 11.62.40.48 0.99
Cyclohexane 2.5 0.58 8/15/17 20:04 CMR8.7 11.62.00.34 1.2
Dibromochloromethane ND 0.58 8/15/17 20:04 CMRND11.64.90.38 3.3
1,2-Dibromoethane (EDB)ND 0.58 8/15/17 20:04 CMRND11.64.40.38 2.9
1,2-Dichlorobenzene ND 0.58 8/15/17 20:04 CMRND11.63.50.38 2.3
1,3-Dichlorobenzene 2.6 0.58 8/15/17 20:04 CMR16 11.63.50.35 2.1
1,4-Dichlorobenzene ND 0.58 8/15/17 20:04 CMRND11.63.50.40 2.4
Dichlorodifluoromethane (Freon 12)ND 0.58 8/15/17 20:04 CMRND11.62.90.44 2.2
1,1-Dichloroethane ND 0.58 8/15/17 20:04 CMRND11.62.30.41 1.6
1,2-Dichloroethane ND 0.58 8/15/17 20:04 CMRND11.62.30.41 1.7
1,1-Dichloroethylene ND 0.58 8/15/17 20:04 CMRND11.62.30.42 1.7
cis-1,2-Dichloroethylene ND 0.58 8/15/17 20:04 CMRND11.62.30.39 1.6
trans-1,2-Dichloroethylene ND 0.58 8/15/17 20:04 CMRND11.62.30.43 1.7
1,2-Dichloropropane ND 0.58 8/15/17 20:04 CMRND11.62.70.40 1.8
cis-1,3-Dichloropropene ND 0.58 8/15/17 20:04 CMRND11.62.60.50 2.3
trans-1,3-Dichloropropene ND 0.58 8/15/17 20:04 CMRND11.62.60.35 1.6
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.58 8/15/17 20:04 CMRND11.64.00.47 3.3
1,4-Dioxane ND 5.8 8/15/17 20:04 CMRND11.6213.7 13
Ethanol ND 23 8/15/17 20:04 CMRND11.6441019
Ethyl Acetate ND 1.2 8/15/17 20:04 CMRND11.64.20.49 1.8
Ethylbenzene 0.58 0.58 8/15/17 20:04 CMR2.5 11.62.50.38 1.7
4-Ethyltoluene ND 0.58 8/15/17 20:04 CMRND11.62.80.38 1.8
Heptane 1.2 0.58 8/15/17 20:04 CMR5.1 11.62.40.38 1.6
Hexachlorobutadiene ND 0.58 8/15/17 20:04 CMRND11.66.20.44 4.7
Hexane 2.4 23 8/15/17 20:04 CMRJ8.6 11.6811.0 3.6
2-Hexanone (MBK)ND 0.58 8/15/17 20:04 CMRND11.62.40.34 1.4
Isopropanol ND 23 8/15/17 20:04 CMRND11.6570.71 1.7
Methyl tert-Butyl Ether (MTBE)0.40 0.58 8/15/17 20:04 CMRJ1.5 11.62.10.39 1.4
Methylene Chloride ND 5.8 8/15/17 20:04 CMRND11.6200.70 2.4
4-Methyl-2-pentanone (MIBK)1.0 0.58 8/15/17 20:04 CMR4.2 11.62.40.49 2.0
Naphthalene 1.4 2.3 8/15/17 20:04 CMRZ-01, J 7.6 11.6120.50 2.6
Propene 46 23 8/15/17 20:04 CMR79 11.6401.8 3.0
Styrene ND 0.58 8/15/17 20:04 CMRND11.62.50.38 1.6
1,1,2,2-Tetrachloroethane ND 0.58 8/15/17 20:04 CMRND11.64.00.36 2.5
Page 10 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Belmont Dyers Site - Belmont, N
Date Received: 8/4/2017
Work Order: 17H0494Sample Description/Location:
Field Sample #: PES-SG-8B
Sample ID: 17H0494-09
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -7.7
Sampled: 8/3/2017 17:38
Canister ID: 1589
Flow Controller ID: 4040
Sub Description/Location:
Canister Size: 0.4 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 2 Min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 6.9 0.58 8/15/17 20:04 CMR47 11.63.90.35 2.4
Tetrahydrofuran ND 1.2 8/15/17 20:04 CMRND11.63.40.40 1.2
Toluene 6.4 0.58 8/15/17 20:04 CMR24 11.62.20.37 1.4
1,2,4-Trichlorobenzene 1.7 0.58 8/15/17 20:04 CMRZ-01 13 11.64.30.43 3.2
1,1,1-Trichloroethane ND 0.58 8/15/17 20:04 CMRND11.63.20.40 2.2
1,1,2-Trichloroethane ND 0.58 8/15/17 20:04 CMRND11.63.20.37 2.0
Trichloroethylene ND 0.58 8/15/17 20:04 CMRND11.63.10.37 2.0
Trichlorofluoromethane (Freon 11)ND 2.3 8/15/17 20:04 CMRND11.6130.49 2.7
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 2.3 8/15/17 20:04 CMRND11.6180.40 3.1
1,2,4-Trimethylbenzene 0.43 0.58 8/15/17 20:04 CMRJ2.1 11.62.80.38 1.8
1,3,5-Trimethylbenzene ND 0.58 8/15/17 20:04 CMRND11.62.80.39 1.9
Vinyl Acetate ND 12 8/15/17 20:04 CMRND11.6410.35 1.2
Vinyl Chloride 0.50 0.58 8/15/17 20:04 CMRJ1.3 11.61.50.43 1.1
m&p-Xylene 2.3 1.2 8/15/17 20:04 CMR9.9 11.65.00.75 3.3
o-Xylene 0.75 0.58 8/15/17 20:04 CMR3.3 11.62.50.36 1.6
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)99.9 8/15/17 20:0470-130
Page 11 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
17H0494-06 [PES-SG-6]B184271 4 1 N/A 1000 400 80 08/15/17
17H0494-07 [PES-SG-7]B184271 8 1 N/A 1000 400 160 08/15/17
17H0494-08 [PES-SG-8A]B184271 8 1 N/A 1000 400 257 08/15/17
17H0494-09 [PES-SG-8B]B184271 8 1 N/A 1000 400 277 08/15/17
Page 12 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B184271 - TO-15 Prep
Blank (B184271-BLK1)Prepared & Analyzed: 08/15/17
1.4NDAcetone
0.035NDBenzene
0.035NDBenzyl chloride
0.035NDBromodichloromethane
0.035NDBromoform
0.035NDBromomethane
0.035ND1,3-Butadiene
1.4ND2-Butanone (MEK)
0.35NDCarbon Disulfide
0.035NDCarbon Tetrachloride
0.035NDChlorobenzene
0.035NDChloroethane
0.035NDChloroform
0.070NDChloromethane
0.035NDCyclohexane
0.035NDDibromochloromethane
0.035ND1,2-Dibromoethane (EDB)
0.035ND1,2-Dichlorobenzene
0.035ND1,3-Dichlorobenzene
0.035ND1,4-Dichlorobenzene
0.035NDDichlorodifluoromethane (Freon 12)
0.035ND1,1-Dichloroethane
0.035ND1,2-Dichloroethane
0.035ND1,1-Dichloroethylene
0.035NDcis-1,2-Dichloroethylene
0.035NDtrans-1,2-Dichloroethylene
0.035ND1,2-Dichloropropane
0.035NDcis-1,3-Dichloropropene
0.035NDtrans-1,3-Dichloropropene
0.035ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.35ND1,4-Dioxane
1.4NDEthanol
0.035NDEthyl Acetate
0.035NDEthylbenzene
0.035ND4-Ethyltoluene
0.035NDHeptane
0.035NDHexachlorobutadiene
1.4NDHexane
0.035ND2-Hexanone (MBK)
1.4NDIsopropanol
0.035NDMethyl tert-Butyl Ether (MTBE)
0.35NDMethylene Chloride
0.035ND4-Methyl-2-pentanone (MIBK)
0.035NDNaphthalene
1.4NDPropene
0.035NDStyrene
Page 13 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B184271 - TO-15 Prep
Blank (B184271-BLK1)Prepared & Analyzed: 08/15/17
0.035ND1,1,2,2-Tetrachloroethane
0.035NDTetrachloroethylene
0.035NDTetrahydrofuran
0.035NDToluene
0.035ND1,2,4-Trichlorobenzene
0.035ND1,1,1-Trichloroethane
0.035ND1,1,2-Trichloroethane
0.035NDTrichloroethylene
0.14NDTrichlorofluoromethane (Freon 11)
0.14ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.035ND1,2,4-Trimethylbenzene
0.035ND1,3,5-Trimethylbenzene
0.70NDVinyl Acetate
0.035NDVinyl Chloride
0.070NDm&p-Xylene
0.035NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1008.04
LCS (B184271-BS1)Prepared & Analyzed: 08/15/17
5.00 70-13096.84.84Acetone
5.00 70-1301025.10Benzene
5.00 70-1301085.39Benzyl chloride
5.00 70-1301035.15Bromodichloromethane
5.00 70-1301165.79Bromoform
5.00 70-1301256.25Bromomethane
5.00 70-1301226.111,3-Butadiene
5.00 70-13091.04.552-Butanone (MEK)
5.00 70-1301135.65Carbon Disulfide
5.00 70-13094.04.70Carbon Tetrachloride
5.00 70-1301105.51Chlorobenzene
5.00 70-1301236.16Chloroethane
5.00 70-13098.24.91Chloroform
5.00 70-1301175.83Chloromethane
5.00 70-13095.44.77Cyclohexane
5.00 70-1301095.44Dibromochloromethane
5.00 70-1301085.401,2-Dibromoethane (EDB)
5.00 70-13094.94.741,2-Dichlorobenzene
5.00 70-1301035.171,3-Dichlorobenzene
5.00 70-1301085.401,4-Dichlorobenzene
5.00 70-13098.04.90Dichlorodifluoromethane (Freon 12)
5.00 70-1301005.011,1-Dichloroethane
5.00 70-13094.34.711,2-Dichloroethane
5.00 70-1301115.561,1-Dichloroethylene
5.00 70-1301015.04cis-1,2-Dichloroethylene
5.00 70-13096.04.80trans-1,2-Dichloroethylene
5.00 70-1301055.261,2-Dichloropropane
Page 14 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B184271 - TO-15 Prep
LCS (B184271-BS1)Prepared & Analyzed: 08/15/17
5.00 70-1301065.29cis-1,3-Dichloropropene
5.00 70-1301035.15trans-1,3-Dichloropropene
5.00 70-1301125.591,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-13094.14.711,4-Dioxane
5.00 70-1301025.11Ethanol
5.00 70-1301055.24Ethyl Acetate
5.00 70-1301035.15Ethylbenzene
5.00 70-1301005.014-Ethyltoluene
5.00 70-1301075.37Heptane
5.00 70-1301206.02Hexachlorobutadiene
5.00 70-13089.34.46Hexane
5.00 70-13089.54.472-Hexanone (MBK)
5.00 70-13091.84.59Isopropanol
5.00 70-13087.24.36Methyl tert-Butyl Ether (MTBE)
5.00 70-13095.24.76Methylene Chloride
5.00 70-13095.34.764-Methyl-2-pentanone (MIBK)
5.00 Z-0170-1301407.02Naphthalene *
5.00 70-13091.94.59Propene
5.00 70-1301125.59Styrene
5.00 70-1301045.221,1,2,2-Tetrachloroethane
5.00 70-1301135.64Tetrachloroethylene
5.00 70-13099.04.95Tetrahydrofuran
5.00 70-1301095.43Toluene
5.00 Z-0170-1301417.051,2,4-Trichlorobenzene *
5.00 70-13089.94.491,1,1-Trichloroethane
5.00 70-1301055.241,1,2-Trichloroethane
5.00 70-1301075.36Trichloroethylene
5.00 70-1301075.37Trichlorofluoromethane (Freon 11)
5.00 70-1301065.281,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13097.94.891,2,4-Trimethylbenzene
5.00 70-13099.95.001,3,5-Trimethylbenzene
5.00 70-13080.84.04Vinyl Acetate
5.00 70-1301226.08Vinyl Chloride
10.0 70-13010710.7m&p-Xylene
5.00 70-1301115.54o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1068.52
Page 15 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult
compound and passes the in house limits of 50-150%.
Z-01
ANALYST
Thomas P. HniteckiTPH
Paula E. BlakeboroughPEB
Kerry K. McGeeKKM
Emily E. SnyderEES
Catherine M. RouleauCMR
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,MEAcetone
AIHA,FL,NJ,NY,VA,MEBenzene
AIHA,FL,NJ,NY,VA,MEBenzyl chloride
AIHA,NJ,NY,VA,MEBromodichloromethane
AIHA,NJ,NY,VA,MEBromoform
AIHA,FL,NJ,NY,MEBromomethane
AIHA,NJ,NY,VA,ME1,3-Butadiene
AIHA,FL,NJ,NY,VA,ME2-Butanone (MEK)
AIHA,NJ,NY,VA,MECarbon Disulfide
AIHA,FL,NJ,NY,VA,MECarbon Tetrachloride
AIHA,FL,NJ,NY,VA,MEChlorobenzene
AIHA,FL,NJ,NY,VA,MEChloroethane
AIHA,FL,NJ,NY,VA,MEChloroform
AIHA,FL,NJ,NY,VA,MEChloromethane
AIHA,NJ,NY,VA,MECyclohexane
AIHA,NY,MEDibromochloromethane
AIHA,NJ,NY,ME1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,VA,ME1,2-Dichlorobenzene
AIHA,NJ,NY,ME1,3-Dichlorobenzene
AIHA,FL,NJ,NY,VA,ME1,4-Dichlorobenzene
AIHA,NY,MEDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,VA,ME1,1-Dichloroethane
AIHA,FL,NJ,NY,VA,ME1,2-Dichloroethane
AIHA,FL,NJ,NY,VA,ME1,1-Dichloroethylene
AIHA,FL,NY,VA,MEcis-1,2-Dichloroethylene
AIHA,NJ,NY,VA,MEtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,VA,ME1,2-Dichloropropane
AIHA,FL,NJ,NY,VA,MEcis-1,3-Dichloropropene
AIHA,NY,MEtrans-1,3-Dichloropropene
AIHA,NJ,NY,VA,ME1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,VA,ME1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,VA,MEEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,VA,MEHeptane
AIHA,NJ,NY,VA,MEHexachlorobutadiene
AIHA,FL,NJ,NY,VA,MEHexane
AIHA2-Hexanone (MBK)
AIHA,NY,MEIsopropanol
AIHA,FL,NJ,NY,VA,MEMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,VA,MEMethylene Chloride
AIHA,FL,NJ,NY,ME4-Methyl-2-pentanone (MIBK)
NY,MENaphthalene
AIHAPropene
AIHA,FL,NJ,NY,VA,MEStyrene
AIHA,FL,NJ,NY,VA,ME1,1,2,2-Tetrachloroethane
Page 17 of 21
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,VA,METetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,VA,METoluene
AIHA,NJ,NY,VA,ME1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,VA,ME1,1,1-Trichloroethane
AIHA,FL,NJ,NY,VA,ME1,1,2-Trichloroethane
AIHA,FL,NJ,NY,VA,METrichloroethylene
AIHA,NY,METrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,VA,ME1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,VA,MEVinyl Acetate
AIHA,FL,NJ,NY,VA,MEVinyl Chloride
AIHA,FL,NJ,NY,VA,MEm&p-Xylene
AIHA,FL,NJ,NY,VA,MEo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 02/1/2018
M-MA100Massachusetts DEPMA 06/30/2018
PH-0567Connecticut Department of Publilc HealthCT 09/30/2017
10899 NELAPNew York State Department of HealthNY 04/1/2018
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2018
LAO00112Rhode Island Department of HealthRI 12/30/2017
652North Carolina Div. of Water QualityNC 12/31/2017
MA007 NELAPNew Jersey DEPNJ 06/30/2018
E871027 NELAPFlorida Department of HealthFL 06/30/2018
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2018
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2017
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2017
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2018
25703North Carolina Department of HealthNC-DW 07/31/2018
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