8401_CityofAlbemarleMSWLF_LeachateAssmt_DIN28452_20170816

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FIGURES

APPENDIX A
PHOTOGRAPH LOG

APPENDIX B
LABORATORY ANALYTICAL REPORT

#=CL#
August 08, 2017
LIMS USE: FR - AYLA HOMER
LIMS OBJECT ID: 92349769
92349769
Project:
Pace Project No.:
RE:
Ayla Homer
Shield
4301 Taggart Creek Road
Charlotte, NC 28208
Leachate
Dear Ayla Homer:
Enclosed are the analytical results for sample(s) received by the laboratory on August 01, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
cc:Mr. James Gamertsfelder, Shield Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92349769
Leachate
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92349769
Leachate
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92349769001 SB-1 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769002 SB-2 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769003 SB-3 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769004 SB-4 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769005 SB-5 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769006 SB-6 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769007 SB-7 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769008 SB-8 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769009 SB-9 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92349769010 SB-10 EPA 8260 52 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-1 Lab ID:92349769001 Collected:07/31/17 16:30 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 16:34 67-64-11711
Acrylonitrile ND ug/kg 08/02/17 16:34 107-13-11711
Benzene ND ug/kg 08/02/17 16:34 71-43-28.5 1
Bromochloromethane ND ug/kg 08/02/17 16:34 74-97-58.5 1
Bromodichloromethane ND ug/kg 08/02/17 16:34 75-27-48.5 1
Bromoform ND ug/kg 08/02/17 16:34 75-25-28.5 1
Bromomethane ND ug/kg 08/02/17 16:34 74-83-917.1 1
2-Butanone (MEK)ND ug/kg 08/02/17 16:34 78-93-31711
Carbon disulfide ND ug/kg 08/02/17 16:34 75-15-017.1 1
Carbon tetrachloride ND ug/kg 08/02/17 16:34 56-23-58.5 1
Chlorobenzene ND ug/kg 08/02/17 16:34 108-90-78.5 1
Chloroethane ND ug/kg 08/02/17 16:34 75-00-317.1 1
Chloroform ND ug/kg 08/02/17 16:34 67-66-38.5 1
Chloromethane ND ug/kg 08/02/17 16:34 74-87-317.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 16:34 96-12-88.5 1
Dibromochloromethane ND ug/kg 08/02/17 16:34 124-48-18.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 16:34 106-93-48.5 1
Dibromomethane ND ug/kg 08/02/17 16:34 74-95-38.5 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 16:34 95-50-18.5 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 16:34 106-46-78.5 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 16:34 110-57-68.5 1
1,1-Dichloroethane ND ug/kg 08/02/17 16:34 75-34-38.5 1
1,2-Dichloroethane ND ug/kg 08/02/17 16:34 107-06-28.5 1
1,1-Dichloroethene ND ug/kg 08/02/17 16:34 75-35-48.5 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 16:34 156-59-28.5 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 16:34 156-60-58.5 1
1,2-Dichloropropane ND ug/kg 08/02/17 16:34 78-87-58.5 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 16:34 10061-01-58.5 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 16:34 10061-02-68.5 1
Ethylbenzene ND ug/kg 08/02/17 16:34 100-41-48.5 1
2-Hexanone ND ug/kg 08/02/17 16:34 591-78-685.3 1
Iodomethane ND ug/kg 08/02/17 16:34 74-88-417.1 1
Methylene Chloride ND ug/kg 08/02/17 16:34 75-09-234.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 16:34 108-10-185.3 1
Styrene 9.0 ug/kg 08/02/17 16:34 100-42-58.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 16:34 630-20-68.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 16:34 79-34-58.5 1
Tetrachloroethene ND ug/kg 08/02/17 16:34 127-18-48.5 1
Toluene ND ug/kg 08/02/17 16:34 108-88-38.5 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 16:34 71-55-68.5 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 16:34 79-00-58.5 1
Trichloroethene ND ug/kg 08/02/17 16:34 79-01-68.5 1
Trichlorofluoromethane ND ug/kg 08/02/17 16:34 75-69-48.5 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 16:34 96-18-48.5 1
Vinyl acetate ND ug/kg 08/02/17 16:34 108-05-485.3 1
Vinyl chloride ND ug/kg 08/02/17 16:34 75-01-417.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-1 Lab ID:92349769001 Collected:07/31/17 16:30 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 16:34 1330-20-717.1 1
m&p-Xylene ND ug/kg 08/02/17 16:34 179601-23-117.1 1
o-Xylene ND ug/kg 08/02/17 16:34 95-47-68.5 1
Surrogates
Toluene-d8 (S)97 %08/02/17 16:34 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %08/02/17 16:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %08/02/17 16:34 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.8 %08/02/17 08:580.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-2 Lab ID:92349769002 Collected:07/31/17 16:35 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 16:54 67-64-1 M11311
Acrylonitrile ND ug/kg 08/02/17 16:54 107-13-1 M11311
Benzene ND ug/kg 08/02/17 16:54 71-43-26.6 1
Bromochloromethane ND ug/kg 08/02/17 16:54 74-97-56.6 1
Bromodichloromethane ND ug/kg 08/02/17 16:54 75-27-46.6 1
Bromoform ND ug/kg 08/02/17 16:54 75-25-2 M16.6 1
Bromomethane ND ug/kg 08/02/17 16:54 74-83-913.1 1
2-Butanone (MEK)ND ug/kg 08/02/17 16:54 78-93-31311
Carbon disulfide ND ug/kg 08/02/17 16:54 75-15-013.1 1
Carbon tetrachloride ND ug/kg 08/02/17 16:54 56-23-56.6 1
Chlorobenzene ND ug/kg 08/02/17 16:54 108-90-76.6 1
Chloroethane ND ug/kg 08/02/17 16:54 75-00-313.1 1
Chloroform ND ug/kg 08/02/17 16:54 67-66-36.6 1
Chloromethane ND ug/kg 08/02/17 16:54 74-87-313.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 16:54 96-12-86.6 1
Dibromochloromethane ND ug/kg 08/02/17 16:54 124-48-16.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 16:54 106-93-46.6 1
Dibromomethane ND ug/kg 08/02/17 16:54 74-95-36.6 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 16:54 95-50-1 M16.6 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 16:54 106-46-7 M16.6 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 16:54 110-57-6 M16.6 1
1,1-Dichloroethane ND ug/kg 08/02/17 16:54 75-34-36.6 1
1,2-Dichloroethane ND ug/kg 08/02/17 16:54 107-06-26.6 1
1,1-Dichloroethene ND ug/kg 08/02/17 16:54 75-35-46.6 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 16:54 156-59-26.6 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 16:54 156-60-56.6 1
1,2-Dichloropropane ND ug/kg 08/02/17 16:54 78-87-56.6 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 16:54 10061-01-5 M16.6 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 16:54 10061-02-6 M16.6 1
Ethylbenzene ND ug/kg 08/02/17 16:54 100-41-46.6 1
2-Hexanone ND ug/kg 08/02/17 16:54 591-78-6 M165.6 1
Iodomethane ND ug/kg 08/02/17 16:54 74-88-4 M113.1 1
Methylene Chloride ND ug/kg 08/02/17 16:54 75-09-226.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 16:54 108-10-165.6 1
Styrene ND ug/kg 08/02/17 16:54 100-42-5 M16.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 16:54 630-20-66.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 16:54 79-34-56.6 1
Tetrachloroethene ND ug/kg 08/02/17 16:54 127-18-46.6 1
Toluene ND ug/kg 08/02/17 16:54 108-88-36.6 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 16:54 71-55-66.6 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 16:54 79-00-56.6 1
Trichloroethene ND ug/kg 08/02/17 16:54 79-01-66.6 1
Trichlorofluoromethane ND ug/kg 08/02/17 16:54 75-69-46.6 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 16:54 96-18-46.6 1
Vinyl acetate ND ug/kg 08/02/17 16:54 108-05-4 M165.6 1
Vinyl chloride ND ug/kg 08/02/17 16:54 75-01-413.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-2 Lab ID:92349769002 Collected:07/31/17 16:35 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 16:54 1330-20-713.1 1
m&p-Xylene ND ug/kg 08/02/17 16:54 179601-23-113.1 1
o-Xylene ND ug/kg 08/02/17 16:54 95-47-66.6 1
Surrogates
Toluene-d8 (S)98 %08/02/17 16:54 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %08/02/17 16:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %08/02/17 16:54 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.8 %08/02/17 08:590.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-3 Lab ID:92349769003 Collected:07/31/17 16:42 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 17:13 67-64-11261
Acrylonitrile ND ug/kg 08/02/17 17:13 107-13-11261
Benzene ND ug/kg 08/02/17 17:13 71-43-26.3 1
Bromochloromethane ND ug/kg 08/02/17 17:13 74-97-56.3 1
Bromodichloromethane ND ug/kg 08/02/17 17:13 75-27-46.3 1
Bromoform ND ug/kg 08/02/17 17:13 75-25-26.3 1
Bromomethane ND ug/kg 08/02/17 17:13 74-83-912.6 1
2-Butanone (MEK)ND ug/kg 08/02/17 17:13 78-93-31261
Carbon disulfide ND ug/kg 08/02/17 17:13 75-15-012.6 1
Carbon tetrachloride ND ug/kg 08/02/17 17:13 56-23-56.3 1
Chlorobenzene ND ug/kg 08/02/17 17:13 108-90-76.3 1
Chloroethane ND ug/kg 08/02/17 17:13 75-00-312.6 1
Chloroform ND ug/kg 08/02/17 17:13 67-66-36.3 1
Chloromethane ND ug/kg 08/02/17 17:13 74-87-312.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 17:13 96-12-86.3 1
Dibromochloromethane ND ug/kg 08/02/17 17:13 124-48-16.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 17:13 106-93-46.3 1
Dibromomethane ND ug/kg 08/02/17 17:13 74-95-36.3 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 17:13 95-50-16.3 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 17:13 106-46-76.3 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 17:13 110-57-66.3 1
1,1-Dichloroethane ND ug/kg 08/02/17 17:13 75-34-36.3 1
1,2-Dichloroethane ND ug/kg 08/02/17 17:13 107-06-26.3 1
1,1-Dichloroethene ND ug/kg 08/02/17 17:13 75-35-46.3 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 17:13 156-59-26.3 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 17:13 156-60-56.3 1
1,2-Dichloropropane ND ug/kg 08/02/17 17:13 78-87-56.3 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 17:13 10061-01-56.3 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 17:13 10061-02-66.3 1
Ethylbenzene ND ug/kg 08/02/17 17:13 100-41-46.3 1
2-Hexanone ND ug/kg 08/02/17 17:13 591-78-662.9 1
Iodomethane ND ug/kg 08/02/17 17:13 74-88-412.6 1
Methylene Chloride ND ug/kg 08/02/17 17:13 75-09-225.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 17:13 108-10-162.9 1
Styrene ND ug/kg 08/02/17 17:13 100-42-56.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 17:13 630-20-66.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 17:13 79-34-56.3 1
Tetrachloroethene ND ug/kg 08/02/17 17:13 127-18-46.3 1
Toluene ND ug/kg 08/02/17 17:13 108-88-36.3 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 17:13 71-55-66.3 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 17:13 79-00-56.3 1
Trichloroethene ND ug/kg 08/02/17 17:13 79-01-66.3 1
Trichlorofluoromethane ND ug/kg 08/02/17 17:13 75-69-46.3 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 17:13 96-18-46.3 1
Vinyl acetate ND ug/kg 08/02/17 17:13 108-05-462.9 1
Vinyl chloride ND ug/kg 08/02/17 17:13 75-01-412.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-3 Lab ID:92349769003 Collected:07/31/17 16:42 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 17:13 1330-20-712.6 1
m&p-Xylene ND ug/kg 08/02/17 17:13 179601-23-112.6 1
o-Xylene ND ug/kg 08/02/17 17:13 95-47-66.3 1
Surrogates
Toluene-d8 (S)97 %08/02/17 17:13 2037-26-570-130 1
4-Bromofluorobenzene (S)92 %08/02/17 17:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %08/02/17 17:13 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.3 %08/02/17 08:590.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-4 Lab ID:92349769004 Collected:07/31/17 16:50 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 17:33 67-64-11481
Acrylonitrile ND ug/kg 08/02/17 17:33 107-13-11481
Benzene ND ug/kg 08/02/17 17:33 71-43-27.4 1
Bromochloromethane ND ug/kg 08/02/17 17:33 74-97-57.4 1
Bromodichloromethane ND ug/kg 08/02/17 17:33 75-27-47.4 1
Bromoform ND ug/kg 08/02/17 17:33 75-25-27.4 1
Bromomethane ND ug/kg 08/02/17 17:33 74-83-914.8 1
2-Butanone (MEK)ND ug/kg 08/02/17 17:33 78-93-31481
Carbon disulfide ND ug/kg 08/02/17 17:33 75-15-014.8 1
Carbon tetrachloride ND ug/kg 08/02/17 17:33 56-23-57.4 1
Chlorobenzene ND ug/kg 08/02/17 17:33 108-90-77.4 1
Chloroethane ND ug/kg 08/02/17 17:33 75-00-314.8 1
Chloroform ND ug/kg 08/02/17 17:33 67-66-37.4 1
Chloromethane ND ug/kg 08/02/17 17:33 74-87-314.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 17:33 96-12-87.4 1
Dibromochloromethane ND ug/kg 08/02/17 17:33 124-48-17.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 17:33 106-93-47.4 1
Dibromomethane ND ug/kg 08/02/17 17:33 74-95-37.4 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 17:33 95-50-17.4 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 17:33 106-46-77.4 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 17:33 110-57-67.4 1
1,1-Dichloroethane ND ug/kg 08/02/17 17:33 75-34-37.4 1
1,2-Dichloroethane ND ug/kg 08/02/17 17:33 107-06-27.4 1
1,1-Dichloroethene ND ug/kg 08/02/17 17:33 75-35-47.4 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 17:33 156-59-27.4 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 17:33 156-60-57.4 1
1,2-Dichloropropane ND ug/kg 08/02/17 17:33 78-87-57.4 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 17:33 10061-01-57.4 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 17:33 10061-02-67.4 1
Ethylbenzene ND ug/kg 08/02/17 17:33 100-41-47.4 1
2-Hexanone ND ug/kg 08/02/17 17:33 591-78-673.9 1
Iodomethane ND ug/kg 08/02/17 17:33 74-88-414.8 1
Methylene Chloride ND ug/kg 08/02/17 17:33 75-09-229.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 17:33 108-10-173.9 1
Styrene ND ug/kg 08/02/17 17:33 100-42-57.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 17:33 630-20-67.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 17:33 79-34-57.4 1
Tetrachloroethene ND ug/kg 08/02/17 17:33 127-18-47.4 1
Toluene ND ug/kg 08/02/17 17:33 108-88-37.4 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 17:33 71-55-67.4 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 17:33 79-00-57.4 1
Trichloroethene ND ug/kg 08/02/17 17:33 79-01-67.4 1
Trichlorofluoromethane ND ug/kg 08/02/17 17:33 75-69-47.4 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 17:33 96-18-47.4 1
Vinyl acetate ND ug/kg 08/02/17 17:33 108-05-473.9 1
Vinyl chloride ND ug/kg 08/02/17 17:33 75-01-414.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-4 Lab ID:92349769004 Collected:07/31/17 16:50 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 17:33 1330-20-714.8 1
m&p-Xylene ND ug/kg 08/02/17 17:33 179601-23-114.8 1
o-Xylene ND ug/kg 08/02/17 17:33 95-47-67.4 1
Surrogates
Toluene-d8 (S)96 %08/02/17 17:33 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %08/02/17 17:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %08/02/17 17:33 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.0 %08/02/17 09:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-5 Lab ID:92349769005 Collected:07/31/17 16:56 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/03/17 21:16 67-64-11571
Acrylonitrile ND ug/kg 08/03/17 21:16 107-13-11571
Benzene ND ug/kg 08/03/17 21:16 71-43-27.9 1
Bromochloromethane ND ug/kg 08/03/17 21:16 74-97-57.9 1
Bromodichloromethane ND ug/kg 08/03/17 21:16 75-27-47.9 1
Bromoform ND ug/kg 08/03/17 21:16 75-25-27.9 1
Bromomethane ND ug/kg 08/03/17 21:16 74-83-915.7 1
2-Butanone (MEK)ND ug/kg 08/03/17 21:16 78-93-31571
Carbon disulfide ND ug/kg 08/03/17 21:16 75-15-015.7 1
Carbon tetrachloride ND ug/kg 08/03/17 21:16 56-23-57.9 1
Chlorobenzene ND ug/kg 08/03/17 21:16 108-90-77.9 1
Chloroethane ND ug/kg 08/03/17 21:16 75-00-315.7 1
Chloroform ND ug/kg 08/03/17 21:16 67-66-37.9 1
Chloromethane ND ug/kg 08/03/17 21:16 74-87-315.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/03/17 21:16 96-12-87.9 1
Dibromochloromethane ND ug/kg 08/03/17 21:16 124-48-17.9 1
1,2-Dibromoethane (EDB)ND ug/kg 08/03/17 21:16 106-93-47.9 1
Dibromomethane ND ug/kg 08/03/17 21:16 74-95-37.9 1
1,2-Dichlorobenzene ND ug/kg 08/03/17 21:16 95-50-17.9 1
1,4-Dichlorobenzene ND ug/kg 08/03/17 21:16 106-46-77.9 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/03/17 21:16 110-57-6 L17.9 1
1,1-Dichloroethane ND ug/kg 08/03/17 21:16 75-34-37.9 1
1,2-Dichloroethane ND ug/kg 08/03/17 21:16 107-06-27.9 1
1,1-Dichloroethene ND ug/kg 08/03/17 21:16 75-35-47.9 1
cis-1,2-Dichloroethene ND ug/kg 08/03/17 21:16 156-59-27.9 1
trans-1,2-Dichloroethene ND ug/kg 08/03/17 21:16 156-60-57.9 1
1,2-Dichloropropane ND ug/kg 08/03/17 21:16 78-87-57.9 1
cis-1,3-Dichloropropene ND ug/kg 08/03/17 21:16 10061-01-57.9 1
trans-1,3-Dichloropropene ND ug/kg 08/03/17 21:16 10061-02-67.9 1
Ethylbenzene ND ug/kg 08/03/17 21:16 100-41-47.9 1
2-Hexanone ND ug/kg 08/03/17 21:16 591-78-678.6 1
Iodomethane ND ug/kg 08/03/17 21:16 74-88-415.7 1
Methylene Chloride ND ug/kg 08/03/17 21:16 75-09-231.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/03/17 21:16 108-10-178.6 1
Styrene ND ug/kg 08/03/17 21:16 100-42-57.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/03/17 21:16 630-20-67.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/03/17 21:16 79-34-57.9 1
Tetrachloroethene ND ug/kg 08/03/17 21:16 127-18-47.9 1
Toluene ND ug/kg 08/03/17 21:16 108-88-37.9 1
1,1,1-Trichloroethane ND ug/kg 08/03/17 21:16 71-55-67.9 1
1,1,2-Trichloroethane ND ug/kg 08/03/17 21:16 79-00-57.9 1
Trichloroethene ND ug/kg 08/03/17 21:16 79-01-67.9 1
Trichlorofluoromethane ND ug/kg 08/03/17 21:16 75-69-47.9 1
1,2,3-Trichloropropane ND ug/kg 08/03/17 21:16 96-18-47.9 1
Vinyl acetate ND ug/kg 08/03/17 21:16 108-05-478.6 1
Vinyl chloride ND ug/kg 08/03/17 21:16 75-01-415.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-5 Lab ID:92349769005 Collected:07/31/17 16:56 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/03/17 21:16 1330-20-715.7 1
m&p-Xylene ND ug/kg 08/03/17 21:16 179601-23-115.7 1
o-Xylene ND ug/kg 08/03/17 21:16 95-47-67.9 1
Surrogates
Toluene-d8 (S)97 %08/03/17 21:16 2037-26-570-130 1
4-Bromofluorobenzene (S)89 %08/03/17 21:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %08/03/17 21:16 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.4 %08/02/17 09:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-6 Lab ID:92349769006 Collected:07/31/17 17:05 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/03/17 21:36 67-64-11391
Acrylonitrile ND ug/kg 08/03/17 21:36 107-13-11391
Benzene ND ug/kg 08/03/17 21:36 71-43-27.0 1
Bromochloromethane ND ug/kg 08/03/17 21:36 74-97-57.0 1
Bromodichloromethane ND ug/kg 08/03/17 21:36 75-27-47.0 1
Bromoform ND ug/kg 08/03/17 21:36 75-25-27.0 1
Bromomethane ND ug/kg 08/03/17 21:36 74-83-913.9 1
2-Butanone (MEK)ND ug/kg 08/03/17 21:36 78-93-31391
Carbon disulfide ND ug/kg 08/03/17 21:36 75-15-013.9 1
Carbon tetrachloride ND ug/kg 08/03/17 21:36 56-23-57.0 1
Chlorobenzene ND ug/kg 08/03/17 21:36 108-90-77.0 1
Chloroethane ND ug/kg 08/03/17 21:36 75-00-313.9 1
Chloroform ND ug/kg 08/03/17 21:36 67-66-37.0 1
Chloromethane ND ug/kg 08/03/17 21:36 74-87-313.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/03/17 21:36 96-12-87.0 1
Dibromochloromethane ND ug/kg 08/03/17 21:36 124-48-17.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/03/17 21:36 106-93-47.0 1
Dibromomethane ND ug/kg 08/03/17 21:36 74-95-37.0 1
1,2-Dichlorobenzene ND ug/kg 08/03/17 21:36 95-50-17.0 1
1,4-Dichlorobenzene ND ug/kg 08/03/17 21:36 106-46-77.0 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/03/17 21:36 110-57-6 L17.0 1
1,1-Dichloroethane ND ug/kg 08/03/17 21:36 75-34-37.0 1
1,2-Dichloroethane ND ug/kg 08/03/17 21:36 107-06-27.0 1
1,1-Dichloroethene ND ug/kg 08/03/17 21:36 75-35-47.0 1
cis-1,2-Dichloroethene ND ug/kg 08/03/17 21:36 156-59-27.0 1
trans-1,2-Dichloroethene ND ug/kg 08/03/17 21:36 156-60-57.0 1
1,2-Dichloropropane ND ug/kg 08/03/17 21:36 78-87-57.0 1
cis-1,3-Dichloropropene ND ug/kg 08/03/17 21:36 10061-01-57.0 1
trans-1,3-Dichloropropene ND ug/kg 08/03/17 21:36 10061-02-67.0 1
Ethylbenzene ND ug/kg 08/03/17 21:36 100-41-47.0 1
2-Hexanone ND ug/kg 08/03/17 21:36 591-78-669.6 1
Iodomethane ND ug/kg 08/03/17 21:36 74-88-413.9 1
Methylene Chloride ND ug/kg 08/03/17 21:36 75-09-227.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/03/17 21:36 108-10-169.6 1
Styrene ND ug/kg 08/03/17 21:36 100-42-57.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/03/17 21:36 630-20-67.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/03/17 21:36 79-34-57.0 1
Tetrachloroethene ND ug/kg 08/03/17 21:36 127-18-47.0 1
Toluene ND ug/kg 08/03/17 21:36 108-88-37.0 1
1,1,1-Trichloroethane ND ug/kg 08/03/17 21:36 71-55-67.0 1
1,1,2-Trichloroethane ND ug/kg 08/03/17 21:36 79-00-57.0 1
Trichloroethene ND ug/kg 08/03/17 21:36 79-01-67.0 1
Trichlorofluoromethane ND ug/kg 08/03/17 21:36 75-69-47.0 1
1,2,3-Trichloropropane ND ug/kg 08/03/17 21:36 96-18-47.0 1
Vinyl acetate ND ug/kg 08/03/17 21:36 108-05-469.6 1
Vinyl chloride ND ug/kg 08/03/17 21:36 75-01-413.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-6 Lab ID:92349769006 Collected:07/31/17 17:05 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/03/17 21:36 1330-20-713.9 1
m&p-Xylene ND ug/kg 08/03/17 21:36 179601-23-113.9 1
o-Xylene ND ug/kg 08/03/17 21:36 95-47-67.0 1
Surrogates
Toluene-d8 (S)96 %08/03/17 21:36 2037-26-570-130 1
4-Bromofluorobenzene (S)89 %08/03/17 21:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %08/03/17 21:36 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.7 %08/02/17 09:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-7 Lab ID:92349769007 Collected:07/31/17 17:12 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/03/17 21:55 67-64-11331
Acrylonitrile ND ug/kg 08/03/17 21:55 107-13-11331
Benzene ND ug/kg 08/03/17 21:55 71-43-26.7 1
Bromochloromethane ND ug/kg 08/03/17 21:55 74-97-56.7 1
Bromodichloromethane ND ug/kg 08/03/17 21:55 75-27-46.7 1
Bromoform ND ug/kg 08/03/17 21:55 75-25-26.7 1
Bromomethane ND ug/kg 08/03/17 21:55 74-83-913.3 1
2-Butanone (MEK)ND ug/kg 08/03/17 21:55 78-93-31331
Carbon disulfide ND ug/kg 08/03/17 21:55 75-15-013.3 1
Carbon tetrachloride ND ug/kg 08/03/17 21:55 56-23-56.7 1
Chlorobenzene ND ug/kg 08/03/17 21:55 108-90-76.7 1
Chloroethane ND ug/kg 08/03/17 21:55 75-00-313.3 1
Chloroform ND ug/kg 08/03/17 21:55 67-66-36.7 1
Chloromethane ND ug/kg 08/03/17 21:55 74-87-313.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/03/17 21:55 96-12-86.7 1
Dibromochloromethane ND ug/kg 08/03/17 21:55 124-48-16.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/03/17 21:55 106-93-46.7 1
Dibromomethane ND ug/kg 08/03/17 21:55 74-95-36.7 1
1,2-Dichlorobenzene ND ug/kg 08/03/17 21:55 95-50-16.7 1
1,4-Dichlorobenzene ND ug/kg 08/03/17 21:55 106-46-76.7 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/03/17 21:55 110-57-6 L16.7 1
1,1-Dichloroethane ND ug/kg 08/03/17 21:55 75-34-36.7 1
1,2-Dichloroethane ND ug/kg 08/03/17 21:55 107-06-26.7 1
1,1-Dichloroethene ND ug/kg 08/03/17 21:55 75-35-46.7 1
cis-1,2-Dichloroethene ND ug/kg 08/03/17 21:55 156-59-26.7 1
trans-1,2-Dichloroethene ND ug/kg 08/03/17 21:55 156-60-56.7 1
1,2-Dichloropropane ND ug/kg 08/03/17 21:55 78-87-56.7 1
cis-1,3-Dichloropropene ND ug/kg 08/03/17 21:55 10061-01-56.7 1
trans-1,3-Dichloropropene ND ug/kg 08/03/17 21:55 10061-02-66.7 1
Ethylbenzene ND ug/kg 08/03/17 21:55 100-41-46.7 1
2-Hexanone ND ug/kg 08/03/17 21:55 591-78-666.7 1
Iodomethane ND ug/kg 08/03/17 21:55 74-88-413.3 1
Methylene Chloride ND ug/kg 08/03/17 21:55 75-09-226.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/03/17 21:55 108-10-166.7 1
Styrene ND ug/kg 08/03/17 21:55 100-42-56.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/03/17 21:55 630-20-66.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/03/17 21:55 79-34-56.7 1
Tetrachloroethene ND ug/kg 08/03/17 21:55 127-18-46.7 1
Toluene ND ug/kg 08/03/17 21:55 108-88-36.7 1
1,1,1-Trichloroethane ND ug/kg 08/03/17 21:55 71-55-66.7 1
1,1,2-Trichloroethane ND ug/kg 08/03/17 21:55 79-00-56.7 1
Trichloroethene ND ug/kg 08/03/17 21:55 79-01-66.7 1
Trichlorofluoromethane ND ug/kg 08/03/17 21:55 75-69-46.7 1
1,2,3-Trichloropropane ND ug/kg 08/03/17 21:55 96-18-46.7 1
Vinyl acetate ND ug/kg 08/03/17 21:55 108-05-466.7 1
Vinyl chloride ND ug/kg 08/03/17 21:55 75-01-413.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
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Page 16 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-7 Lab ID:92349769007 Collected:07/31/17 17:12 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/03/17 21:55 1330-20-713.3 1
m&p-Xylene ND ug/kg 08/03/17 21:55 179601-23-113.3 1
o-Xylene ND ug/kg 08/03/17 21:55 95-47-66.7 1
Surrogates
Toluene-d8 (S)96 %08/03/17 21:55 2037-26-570-130 1
4-Bromofluorobenzene (S)90 %08/03/17 21:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %08/03/17 21:55 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.7 %08/02/17 09:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
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[phone]
Page 17 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-8 Lab ID:92349769008 Collected:07/31/17 17:20 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 19:00 67-64-11191
Acrylonitrile ND ug/kg 08/02/17 19:00 107-13-11191
Benzene ND ug/kg 08/02/17 19:00 71-43-25.9 1
Bromochloromethane ND ug/kg 08/02/17 19:00 74-97-55.9 1
Bromodichloromethane ND ug/kg 08/02/17 19:00 75-27-45.9 1
Bromoform ND ug/kg 08/02/17 19:00 75-25-25.9 1
Bromomethane ND ug/kg 08/02/17 19:00 74-83-911.9 1
2-Butanone (MEK)ND ug/kg 08/02/17 19:00 78-93-31191
Carbon disulfide ND ug/kg 08/02/17 19:00 75-15-011.9 1
Carbon tetrachloride ND ug/kg 08/02/17 19:00 56-23-55.9 1
Chlorobenzene ND ug/kg 08/02/17 19:00 108-90-75.9 1
Chloroethane ND ug/kg 08/02/17 19:00 75-00-311.9 1
Chloroform ND ug/kg 08/02/17 19:00 67-66-35.9 1
Chloromethane ND ug/kg 08/02/17 19:00 74-87-311.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 19:00 96-12-85.9 1
Dibromochloromethane ND ug/kg 08/02/17 19:00 124-48-15.9 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 19:00 106-93-45.9 1
Dibromomethane ND ug/kg 08/02/17 19:00 74-95-35.9 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 19:00 95-50-15.9 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 19:00 106-46-75.9 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 19:00 110-57-65.9 1
1,1-Dichloroethane ND ug/kg 08/02/17 19:00 75-34-35.9 1
1,2-Dichloroethane ND ug/kg 08/02/17 19:00 107-06-25.9 1
1,1-Dichloroethene ND ug/kg 08/02/17 19:00 75-35-45.9 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 19:00 156-59-25.9 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 19:00 156-60-55.9 1
1,2-Dichloropropane ND ug/kg 08/02/17 19:00 78-87-55.9 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 19:00 10061-01-55.9 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 19:00 10061-02-65.9 1
Ethylbenzene ND ug/kg 08/02/17 19:00 100-41-45.9 1
2-Hexanone ND ug/kg 08/02/17 19:00 591-78-659.5 1
Iodomethane ND ug/kg 08/02/17 19:00 74-88-411.9 1
Methylene Chloride ND ug/kg 08/02/17 19:00 75-09-223.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 19:00 108-10-159.5 1
Styrene ND ug/kg 08/02/17 19:00 100-42-55.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 19:00 630-20-65.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 19:00 79-34-55.9 1
Tetrachloroethene ND ug/kg 08/02/17 19:00 127-18-45.9 1
Toluene ND ug/kg 08/02/17 19:00 108-88-35.9 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 19:00 71-55-65.9 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 19:00 79-00-55.9 1
Trichloroethene ND ug/kg 08/02/17 19:00 79-01-65.9 1
Trichlorofluoromethane ND ug/kg 08/02/17 19:00 75-69-45.9 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 19:00 96-18-45.9 1
Vinyl acetate ND ug/kg 08/02/17 19:00 108-05-459.5 1
Vinyl chloride ND ug/kg 08/02/17 19:00 75-01-411.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 18 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-8 Lab ID:92349769008 Collected:07/31/17 17:20 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 19:00 1330-20-711.9 1
m&p-Xylene ND ug/kg 08/02/17 19:00 179601-23-111.9 1
o-Xylene ND ug/kg 08/02/17 19:00 95-47-65.9 1
Surrogates
Toluene-d8 (S)101 %08/02/17 19:00 2037-26-5 1g70-130 1
4-Bromofluorobenzene (S)91 %08/02/17 19:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %08/02/17 19:00 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.4 %08/02/17 09:010.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-9 Lab ID:92349769009 Collected:07/31/17 17:30 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 19:19 67-64-11211
Acrylonitrile ND ug/kg 08/02/17 19:19 107-13-11211
Benzene ND ug/kg 08/02/17 19:19 71-43-26.0 1
Bromochloromethane ND ug/kg 08/02/17 19:19 74-97-56.0 1
Bromodichloromethane ND ug/kg 08/02/17 19:19 75-27-46.0 1
Bromoform ND ug/kg 08/02/17 19:19 75-25-26.0 1
Bromomethane ND ug/kg 08/02/17 19:19 74-83-912.1 1
2-Butanone (MEK)ND ug/kg 08/02/17 19:19 78-93-31211
Carbon disulfide ND ug/kg 08/02/17 19:19 75-15-012.1 1
Carbon tetrachloride ND ug/kg 08/02/17 19:19 56-23-56.0 1
Chlorobenzene ND ug/kg 08/02/17 19:19 108-90-76.0 1
Chloroethane ND ug/kg 08/02/17 19:19 75-00-312.1 1
Chloroform ND ug/kg 08/02/17 19:19 67-66-36.0 1
Chloromethane ND ug/kg 08/02/17 19:19 74-87-312.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 19:19 96-12-86.0 1
Dibromochloromethane ND ug/kg 08/02/17 19:19 124-48-16.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 19:19 106-93-46.0 1
Dibromomethane ND ug/kg 08/02/17 19:19 74-95-36.0 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 19:19 95-50-16.0 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 19:19 106-46-76.0 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 19:19 110-57-66.0 1
1,1-Dichloroethane ND ug/kg 08/02/17 19:19 75-34-36.0 1
1,2-Dichloroethane ND ug/kg 08/02/17 19:19 107-06-26.0 1
1,1-Dichloroethene ND ug/kg 08/02/17 19:19 75-35-46.0 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 19:19 156-59-26.0 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 19:19 156-60-56.0 1
1,2-Dichloropropane ND ug/kg 08/02/17 19:19 78-87-56.0 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 19:19 10061-01-56.0 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 19:19 10061-02-66.0 1
Ethylbenzene ND ug/kg 08/02/17 19:19 100-41-46.0 1
2-Hexanone ND ug/kg 08/02/17 19:19 591-78-660.3 1
Iodomethane ND ug/kg 08/02/17 19:19 74-88-412.1 1
Methylene Chloride ND ug/kg 08/02/17 19:19 75-09-224.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 19:19 108-10-160.3 1
Styrene ND ug/kg 08/02/17 19:19 100-42-56.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 19:19 630-20-66.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 19:19 79-34-56.0 1
Tetrachloroethene ND ug/kg 08/02/17 19:19 127-18-46.0 1
Toluene ND ug/kg 08/02/17 19:19 108-88-36.0 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 19:19 71-55-66.0 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 19:19 79-00-56.0 1
Trichloroethene ND ug/kg 08/02/17 19:19 79-01-66.0 1
Trichlorofluoromethane ND ug/kg 08/02/17 19:19 75-69-46.0 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 19:19 96-18-46.0 1
Vinyl acetate ND ug/kg 08/02/17 19:19 108-05-460.3 1
Vinyl chloride ND ug/kg 08/02/17 19:19 75-01-412.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-9 Lab ID:92349769009 Collected:07/31/17 17:30 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 19:19 1330-20-712.1 1
m&p-Xylene ND ug/kg 08/02/17 19:19 179601-23-112.1 1
o-Xylene ND ug/kg 08/02/17 19:19 95-47-66.0 1
Surrogates
Toluene-d8 (S)101 %08/02/17 19:19 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %08/02/17 19:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %08/02/17 19:19 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %08/02/17 09:010.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-10 Lab ID:92349769010 Collected:07/31/17 17:40 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/02/17 19:39 67-64-11131
Acrylonitrile ND ug/kg 08/02/17 19:39 107-13-11131
Benzene ND ug/kg 08/02/17 19:39 71-43-25.7 1
Bromochloromethane ND ug/kg 08/02/17 19:39 74-97-55.7 1
Bromodichloromethane ND ug/kg 08/02/17 19:39 75-27-45.7 1
Bromoform ND ug/kg 08/02/17 19:39 75-25-25.7 1
Bromomethane ND ug/kg 08/02/17 19:39 74-83-911.3 1
2-Butanone (MEK)ND ug/kg 08/02/17 19:39 78-93-31131
Carbon disulfide ND ug/kg 08/02/17 19:39 75-15-011.3 1
Carbon tetrachloride ND ug/kg 08/02/17 19:39 56-23-55.7 1
Chlorobenzene ND ug/kg 08/02/17 19:39 108-90-75.7 1
Chloroethane ND ug/kg 08/02/17 19:39 75-00-311.3 1
Chloroform ND ug/kg 08/02/17 19:39 67-66-35.7 1
Chloromethane ND ug/kg 08/02/17 19:39 74-87-311.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/02/17 19:39 96-12-85.7 1
Dibromochloromethane ND ug/kg 08/02/17 19:39 124-48-15.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/02/17 19:39 106-93-45.7 1
Dibromomethane ND ug/kg 08/02/17 19:39 74-95-35.7 1
1,2-Dichlorobenzene ND ug/kg 08/02/17 19:39 95-50-15.7 1
1,4-Dichlorobenzene ND ug/kg 08/02/17 19:39 106-46-75.7 1
trans-1,4-Dichloro-2-butene ND ug/kg 08/02/17 19:39 110-57-65.7 1
1,1-Dichloroethane ND ug/kg 08/02/17 19:39 75-34-35.7 1
1,2-Dichloroethane ND ug/kg 08/02/17 19:39 107-06-25.7 1
1,1-Dichloroethene ND ug/kg 08/02/17 19:39 75-35-45.7 1
cis-1,2-Dichloroethene ND ug/kg 08/02/17 19:39 156-59-25.7 1
trans-1,2-Dichloroethene ND ug/kg 08/02/17 19:39 156-60-55.7 1
1,2-Dichloropropane ND ug/kg 08/02/17 19:39 78-87-55.7 1
cis-1,3-Dichloropropene ND ug/kg 08/02/17 19:39 10061-01-55.7 1
trans-1,3-Dichloropropene ND ug/kg 08/02/17 19:39 10061-02-65.7 1
Ethylbenzene ND ug/kg 08/02/17 19:39 100-41-45.7 1
2-Hexanone ND ug/kg 08/02/17 19:39 591-78-656.5 1
Iodomethane ND ug/kg 08/02/17 19:39 74-88-411.3 1
Methylene Chloride ND ug/kg 08/02/17 19:39 75-09-222.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/02/17 19:39 108-10-156.5 1
Styrene ND ug/kg 08/02/17 19:39 100-42-55.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/02/17 19:39 630-20-65.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/02/17 19:39 79-34-55.7 1
Tetrachloroethene ND ug/kg 08/02/17 19:39 127-18-45.7 1
Toluene ND ug/kg 08/02/17 19:39 108-88-35.7 1
1,1,1-Trichloroethane ND ug/kg 08/02/17 19:39 71-55-65.7 1
1,1,2-Trichloroethane ND ug/kg 08/02/17 19:39 79-00-55.7 1
Trichloroethene ND ug/kg 08/02/17 19:39 79-01-65.7 1
Trichlorofluoromethane ND ug/kg 08/02/17 19:39 75-69-45.7 1
1,2,3-Trichloropropane ND ug/kg 08/02/17 19:39 96-18-45.7 1
Vinyl acetate ND ug/kg 08/02/17 19:39 108-05-456.5 1
Vinyl chloride ND ug/kg 08/02/17 19:39 75-01-411.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92349769
Leachate
Sample:SB-10 Lab ID:92349769010 Collected:07/31/17 17:40 Received:08/01/17 12:31 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Xylene (Total)ND ug/kg 08/02/17 19:39 1330-20-711.3 1
m&p-Xylene ND ug/kg 08/02/17 19:39 179601-23-111.3 1
o-Xylene ND ug/kg 08/02/17 19:39 95-47-65.7 1
Surrogates
Toluene-d8 (S)97 %08/02/17 19:39 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %08/02/17 19:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %08/02/17 19:39 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.6 %08/02/17 09:010.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 23 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
371497
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92349769001, 92349769002, 92349769003, 92349769004, 92349769008, 92349769009, 92349769010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2058177
Associated Lab Samples:92349769001, 92349769002, 92349769003, 92349769004, 92349769008, 92349769009, 92349769010
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 6.2 08/02/17 13:56
1,1,1-Trichloroethane ug/kg ND 6.2 08/02/17 13:56
1,1,2,2-Tetrachloroethane ug/kg ND 6.2 08/02/17 13:56
1,1,2-Trichloroethane ug/kg ND 6.2 08/02/17 13:56
1,1-Dichloroethane ug/kg ND 6.2 08/02/17 13:56
1,1-Dichloroethene ug/kg ND 6.2 08/02/17 13:56
1,2,3-Trichloropropane ug/kg ND 6.2 08/02/17 13:56
1,2-Dibromo-3-chloropropane ug/kg ND 6.2 08/02/17 13:56
1,2-Dibromoethane (EDB)ug/kg ND 6.2 08/02/17 13:56
1,2-Dichlorobenzene ug/kg ND 6.2 08/02/17 13:56
1,2-Dichloroethane ug/kg ND 6.2 08/02/17 13:56
1,2-Dichloropropane ug/kg ND 6.2 08/02/17 13:56
1,4-Dichlorobenzene ug/kg ND 6.2 08/02/17 13:56
2-Butanone (MEK)ug/kg ND 124 08/02/17 13:56
2-Hexanone ug/kg ND 62.0 08/02/17 13:56
4-Methyl-2-pentanone (MIBK)ug/kg ND 62.0 08/02/17 13:56
Acetone ug/kg ND 124 08/02/17 13:56
Acrylonitrile ug/kg ND 124 08/02/17 13:56
Benzene ug/kg ND 6.2 08/02/17 13:56
Bromochloromethane ug/kg ND 6.2 08/02/17 13:56
Bromodichloromethane ug/kg ND 6.2 08/02/17 13:56
Bromoform ug/kg ND 6.2 08/02/17 13:56
Bromomethane ug/kg ND 12.4 08/02/17 13:56
Carbon disulfide ug/kg ND 12.4 08/02/17 13:56
Carbon tetrachloride ug/kg ND 6.2 08/02/17 13:56
Chlorobenzene ug/kg ND 6.2 08/02/17 13:56
Chloroethane ug/kg ND 12.4 08/02/17 13:56
Chloroform ug/kg ND 6.2 08/02/17 13:56
Chloromethane ug/kg ND 12.4 08/02/17 13:56
cis-1,2-Dichloroethene ug/kg ND 6.2 08/02/17 13:56
cis-1,3-Dichloropropene ug/kg ND 6.2 08/02/17 13:56
Dibromochloromethane ug/kg ND 6.2 08/02/17 13:56
Dibromomethane ug/kg ND 6.2 08/02/17 13:56
Ethylbenzene ug/kg ND 6.2 08/02/17 13:56
Iodomethane ug/kg ND 12.4 08/02/17 13:56
m&p-Xylene ug/kg ND 12.4 08/02/17 13:56
Methylene Chloride ug/kg ND 24.8 08/02/17 13:56
o-Xylene ug/kg ND 6.2 08/02/17 13:56
Styrene ug/kg ND 6.2 08/02/17 13:56
Tetrachloroethene ug/kg ND 6.2 08/02/17 13:56
Toluene ug/kg ND 6.2 08/02/17 13:56
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
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Page 24 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2058177
Associated Lab Samples:92349769001, 92349769002, 92349769003, 92349769004, 92349769008, 92349769009, 92349769010
Matrix:Solid
Analyzed
trans-1,2-Dichloroethene ug/kg ND 6.2 08/02/17 13:56
trans-1,3-Dichloropropene ug/kg ND 6.2 08/02/17 13:56
trans-1,4-Dichloro-2-butene ug/kg ND 6.2 08/02/17 13:56
Trichloroethene ug/kg ND 6.2 08/02/17 13:56
Trichlorofluoromethane ug/kg ND 6.2 08/02/17 13:56
Vinyl acetate ug/kg ND 62.0 08/02/17 13:56
Vinyl chloride ug/kg ND 12.4 08/02/17 13:56
Xylene (Total)ug/kg ND 12.4 08/02/17 13:56
1,2-Dichloroethane-d4 (S)%102 70-132 08/02/17 13:56
4-Bromofluorobenzene (S)%99 70-130 08/02/17 13:56
Toluene-d8 (S)%99 70-130 08/02/17 13:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2058178LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.656.7 93 74-137
1,1,1-Trichloroethane ug/kg 54.256.7 96 67-140
1,1,2,2-Tetrachloroethane ug/kg 43.456.7 77 72-141
1,1,2-Trichloroethane ug/kg 53.556.7 94 78-138
1,1-Dichloroethane ug/kg 55.856.7 98 69-134
1,1-Dichloroethene ug/kg 57.356.7 101 67-138
1,2,3-Trichloropropane ug/kg 56.556.7 100 69-144
1,2-Dibromo-3-chloropropane ug/kg 55.256.7 97 65-140
1,2-Dibromoethane (EDB)ug/kg 56.356.7 99 77-135
1,2-Dichlorobenzene ug/kg 55.956.7 99 77-141
1,2-Dichloroethane ug/kg 53.056.7 93 65-137
1,2-Dichloropropane ug/kg 55.556.7 98 72-136
1,4-Dichlorobenzene ug/kg 55.356.7 98 76-138
2-Butanone (MEK)ug/kg 111J113 98 58-147
2-Hexanone ug/kg 115113 101 62-145
4-Methyl-2-pentanone (MIBK)ug/kg 117113 103 64-149
Acetone ug/kg 131113 116 53-153
Acrylonitrile ug/kg 283283 100 56-153
Benzene ug/kg 55.256.7 97 73-135
Bromochloromethane ug/kg 54.356.7 96 73-134
Bromodichloromethane ug/kg 56.156.7 99 71-135
Bromoform ug/kg 51.256.7 90 66-141
Bromomethane ug/kg 60.156.7 106 53-160
Carbon disulfide ug/kg 54.856.7 97 63-140
Carbon tetrachloride ug/kg 56.056.7 99 60-145
Chlorobenzene ug/kg 55.456.7 98 78-130
Chloroethane ug/kg 59.456.7 105 64-149
Chloroform ug/kg 54.756.7 97 70-134
Chloromethane ug/kg 59.256.7 104 52-150
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
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9800 Kincey Ave. Suite 100
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Page 25 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2058178LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/kg 55.856.7 98 70-133
cis-1,3-Dichloropropene ug/kg 56.856.7 100 68-134
Dibromochloromethane ug/kg 55.656.7 98 71-138
Dibromomethane ug/kg 54.956.7 97 74-130
Ethylbenzene ug/kg 54.256.7 96 75-133
Iodomethane ug/kg 113113 99 69-144
m&p-Xylene ug/kg 107113 94 75-136
Methylene Chloride ug/kg 56.456.7 99 45-154
o-Xylene ug/kg 53.756.7 95 76-141
Styrene ug/kg 54.456.7 96 79-137
Tetrachloroethene ug/kg 50.556.7 89 71-138
Toluene ug/kg 55.656.7 98 74-131
trans-1,2-Dichloroethene ug/kg 55.456.7 98 67-135
trans-1,3-Dichloropropene ug/kg 57.356.7 101 65-146
trans-1,4-Dichloro-2-butene ug/kg 71.856.7 127 70-130
Trichloroethene ug/kg 61.856.7 109 67-135
Trichlorofluoromethane ug/kg 58.756.7 104 59-144
Vinyl acetate ug/kg 49J113 43 40-160
Vinyl chloride ug/kg 54.956.7 97 56-141
Xylene (Total)ug/kg 161170 94 76-137
1,2-Dichloroethane-d4 (S)%101 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2059352MATRIX SPIKE SAMPLE:
MSSpike
Result
92349769002
1,1,1,2-Tetrachloroethane ug/kg 22.026.7 82 70-130ND
1,1,1-Trichloroethane ug/kg 24.526.7 92 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 20.926.7 78 70-130ND
1,1,2-Trichloroethane ug/kg 20.726.7 77 70-130ND
1,1-Dichloroethane ug/kg 25.126.7 94 70-130ND
1,1-Dichloroethene ug/kg 26.026.7 97 49-180ND
1,2,3-Trichloropropane ug/kg 22.026.7 83 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 21.426.7 80 70-130ND
1,2-Dibromoethane (EDB)ug/kg 22.126.7 83 70-130ND
1,2-Dichlorobenzene ug/kg 15.0 M126.7 56 70-130ND
1,2-Dichloroethane ug/kg 24.626.7 92 70-130ND
1,2-Dichloropropane ug/kg 24.126.7 90 70-130ND
1,4-Dichlorobenzene ug/kg 16.4 M126.7 61 70-130ND
2-Butanone (MEK)ug/kg 41.6J53.4 78 70-130ND
2-Hexanone ug/kg 34.7J M153.4 65 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 46.5J53.4 87 70-130ND
Acetone ug/kg 88.1J M153.4 165 70-130ND
Acrylonitrile ug/kg 84.6J M11336370-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 26 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2059352MATRIX SPIKE SAMPLE:
MSSpike
Result
92349769002
Benzene ug/kg 24.226.7 91 50-166ND
Bromochloromethane ug/kg 22.826.7 85 70-130ND
Bromodichloromethane ug/kg 23.526.7 88 70-130ND
Bromoform ug/kg 17.5 M126.7 66 70-130ND
Bromomethane ug/kg 20.026.7 75 70-130ND
Carbon disulfide ug/kg 23.226.7 87 70-130ND
Carbon tetrachloride ug/kg 23.726.7 89 70-130ND
Chlorobenzene ug/kg 21.426.7 80 43-169ND
Chloroethane ug/kg 28.126.7 105 70-130ND
Chloroform ug/kg 23.526.7 88 70-130ND
Chloromethane ug/kg 28.126.7 105 70-130ND
cis-1,2-Dichloroethene ug/kg 24.826.7 93 70-130ND
cis-1,3-Dichloropropene ug/kg 17.2 M126.7 65 70-130ND
Dibromochloromethane ug/kg 21.926.7 82 70-130ND
Dibromomethane ug/kg 21.926.7 82 70-130ND
Ethylbenzene ug/kg 22.426.7 84 70-130ND
Iodomethane ug/kg 23.4 M153.4 44 70-130ND
m&p-Xylene ug/kg 43.553.4 81 70-130ND
Methylene Chloride ug/kg 28.426.7 107 70-130ND
o-Xylene ug/kg 20.926.7 78 70-130ND
Styrene ug/kg 18.3 M126.7 69 70-130ND
Tetrachloroethene ug/kg 21.526.7 81 70-130ND
Toluene ug/kg 22.826.7 85 52-163ND
trans-1,2-Dichloroethene ug/kg 24.826.7 93 70-130ND
trans-1,3-Dichloropropene ug/kg 17.4 M126.7 65 70-130ND
trans-1,4-Dichloro-2-butene ug/kg 10 M126.7 37 70-130ND
Trichloroethene ug/kg 22.526.7 84 49-167ND
Trichlorofluoromethane ug/kg 28.426.7 106 70-130ND
Vinyl acetate ug/kg 12.5J M153.4 23 70-130ND
Vinyl chloride ug/kg 25.726.7 96 70-130ND
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%92 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92349769001
2059351SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92349769001
2059351SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Hexanone ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Acrylonitrile ug/kg NDND
Benzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon disulfide ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Ethylbenzene ug/kg NDND
Iodomethane ug/kg NDND
m&p-Xylene ug/kg NDND
Methylene Chloride ug/kg NDND
o-Xylene ug/kg NDND
Styrene ug/kg ND9.0
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
trans-1,4-Dichloro-2-butene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%111 6106
4-Bromofluorobenzene (S)%97 693
Toluene-d8 (S)%98 997
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
371769
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92349769005, 92349769006, 92349769007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2059781
Associated Lab Samples:92349769005, 92349769006, 92349769007
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 6.0 08/03/17 14:02
1,1,1-Trichloroethane ug/kg ND 6.0 08/03/17 14:02
1,1,2,2-Tetrachloroethane ug/kg ND 6.0 08/03/17 14:02
1,1,2-Trichloroethane ug/kg ND 6.0 08/03/17 14:02
1,1-Dichloroethane ug/kg ND 6.0 08/03/17 14:02
1,1-Dichloroethene ug/kg ND 6.0 08/03/17 14:02
1,2,3-Trichloropropane ug/kg ND 6.0 08/03/17 14:02
1,2-Dibromo-3-chloropropane ug/kg ND 6.0 08/03/17 14:02
1,2-Dibromoethane (EDB)ug/kg ND 6.0 08/03/17 14:02
1,2-Dichlorobenzene ug/kg ND 6.0 08/03/17 14:02
1,2-Dichloroethane ug/kg ND 6.0 08/03/17 14:02
1,2-Dichloropropane ug/kg ND 6.0 08/03/17 14:02
1,4-Dichlorobenzene ug/kg ND 6.0 08/03/17 14:02
2-Butanone (MEK)ug/kg ND 119 08/03/17 14:02
2-Hexanone ug/kg ND 59.7 08/03/17 14:02
4-Methyl-2-pentanone (MIBK)ug/kg ND 59.7 08/03/17 14:02
Acetone ug/kg ND 119 08/03/17 14:02
Acrylonitrile ug/kg ND 119 08/03/17 14:02
Benzene ug/kg ND 6.0 08/03/17 14:02
Bromochloromethane ug/kg ND 6.0 08/03/17 14:02
Bromodichloromethane ug/kg ND 6.0 08/03/17 14:02
Bromoform ug/kg ND 6.0 08/03/17 14:02
Bromomethane ug/kg ND 11.9 08/03/17 14:02
Carbon disulfide ug/kg ND 11.9 08/03/17 14:02
Carbon tetrachloride ug/kg ND 6.0 08/03/17 14:02
Chlorobenzene ug/kg ND 6.0 08/03/17 14:02
Chloroethane ug/kg ND 11.9 08/03/17 14:02
Chloroform ug/kg ND 6.0 08/03/17 14:02
Chloromethane ug/kg ND 11.9 08/03/17 14:02
cis-1,2-Dichloroethene ug/kg ND 6.0 08/03/17 14:02
cis-1,3-Dichloropropene ug/kg ND 6.0 08/03/17 14:02
Dibromochloromethane ug/kg ND 6.0 08/03/17 14:02
Dibromomethane ug/kg ND 6.0 08/03/17 14:02
Ethylbenzene ug/kg ND 6.0 08/03/17 14:02
Iodomethane ug/kg ND 11.9 08/03/17 14:02
m&p-Xylene ug/kg ND 11.9 08/03/17 14:02
Methylene Chloride ug/kg ND 23.9 08/03/17 14:02
o-Xylene ug/kg ND 6.0 08/03/17 14:02
Styrene ug/kg ND 6.0 08/03/17 14:02
Tetrachloroethene ug/kg ND 6.0 08/03/17 14:02
Toluene ug/kg ND 6.0 08/03/17 14:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2059781
Associated Lab Samples:92349769005, 92349769006, 92349769007
Matrix:Solid
Analyzed
trans-1,2-Dichloroethene ug/kg ND 6.0 08/03/17 14:02
trans-1,3-Dichloropropene ug/kg ND 6.0 08/03/17 14:02
trans-1,4-Dichloro-2-butene ug/kg ND 6.0 08/03/17 14:02
Trichloroethene ug/kg ND 6.0 08/03/17 14:02
Trichlorofluoromethane ug/kg ND 6.0 08/03/17 14:02
Vinyl acetate ug/kg ND 59.7 08/03/17 14:02
Vinyl chloride ug/kg ND 11.9 08/03/17 14:02
Xylene (Total)ug/kg ND 11.9 08/03/17 14:02
1,2-Dichloroethane-d4 (S)%107 70-132 08/03/17 14:02
4-Bromofluorobenzene (S)%99 70-130 08/03/17 14:02
Toluene-d8 (S)%99 70-130 08/03/17 14:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2059782LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 58.462.5 93 74-137
1,1,1-Trichloroethane ug/kg 59.062.5 94 67-140
1,1,2,2-Tetrachloroethane ug/kg 55.262.5 88 72-141
1,1,2-Trichloroethane ug/kg 59.562.5 95 78-138
1,1-Dichloroethane ug/kg 59.762.5 95 69-134
1,1-Dichloroethene ug/kg 63.062.5 101 67-138
1,2,3-Trichloropropane ug/kg 63.062.5 101 69-144
1,2-Dibromo-3-chloropropane ug/kg 61.562.5 98 65-140
1,2-Dibromoethane (EDB)ug/kg 63.962.5 102 77-135
1,2-Dichlorobenzene ug/kg 61.362.5 98 77-141
1,2-Dichloroethane ug/kg 58.262.5 93 65-137
1,2-Dichloropropane ug/kg 61.562.5 98 72-136
1,4-Dichlorobenzene ug/kg 61.562.5 98 76-138
2-Butanone (MEK)ug/kg ND125 100 58-147
2-Hexanone ug/kg 136125 109 62-145
4-Methyl-2-pentanone (MIBK)ug/kg 137125 109 64-149
Acetone ug/kg 166125 133 53-153
Acrylonitrile ug/kg 321312 103 56-153
Benzene ug/kg 60.362.5 96 73-135
Bromochloromethane ug/kg 55.262.5 88 73-134
Bromodichloromethane ug/kg 62.962.5 101 71-135
Bromoform ug/kg 58.862.5 94 66-141
Bromomethane ug/kg 62.662.5 100 53-160
Carbon disulfide ug/kg 58.162.5 93 63-140
Carbon tetrachloride ug/kg 62.362.5 100 60-145
Chlorobenzene ug/kg 61.762.5 99 78-130
Chloroethane ug/kg 63.562.5 102 64-149
Chloroform ug/kg 58.462.5 93 70-134
Chloromethane ug/kg 65.662.5 105 52-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2059782LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/kg 60.662.5 97 70-133
cis-1,3-Dichloropropene ug/kg 63.562.5 102 68-134
Dibromochloromethane ug/kg 60.862.5 97 71-138
Dibromomethane ug/kg 59.662.5 95 74-130
Ethylbenzene ug/kg 61.762.5 99 75-133
Iodomethane ug/kg 106125 84 69-144
m&p-Xylene ug/kg 121125 97 75-136
Methylene Chloride ug/kg 63.762.5 102 45-154
o-Xylene ug/kg 60.762.5 97 76-141
Styrene ug/kg 61.062.5 98 79-137
Tetrachloroethene ug/kg 56.862.5 91 71-138
Toluene ug/kg 61.662.5 99 74-131
trans-1,2-Dichloroethene ug/kg 59.962.5 96 67-135
trans-1,3-Dichloropropene ug/kg 64.262.5 103 65-146
trans-1,4-Dichloro-2-butene ug/kg 86.4 L162.5 138 70-130
Trichloroethene ug/kg 64.662.5 103 67-135
Trichlorofluoromethane ug/kg 64.862.5 104 59-144
Vinyl acetate ug/kg 93.2125 75 40-160
Vinyl chloride ug/kg 58.962.5 94 56-141
Xylene (Total)ug/kg 182188 97 76-137
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2060390MATRIX SPIKE SAMPLE:
MSSpike
Result
92349874001
1,1,1,2-Tetrachloroethane ug/kg 15.119.8 77 70-130<2.3
1,1,1-Trichloroethane ug/kg 18.319.8 93 70-130<1.9
1,1,2,2-Tetrachloroethane ug/kg 11.5 M119.8 58 70-130<2.0
1,1,2-Trichloroethane ug/kg 13.0 M119.8 66 70-130<2.3
1,1-Dichloroethane ug/kg 16.919.8 86 70-130<1.6
1,1-Dichloroethene ug/kg 19.819.8 100 49-180<1.9
1,2,3-Trichloropropane ug/kg 12.9 M119.8 65 70-130<1.7
1,2-Dibromo-3-chloropropane ug/kg 9.7 M119.8 49 70-130<3.9
1,2-Dibromoethane (EDB)ug/kg 13.3 M119.8 67 70-130<1.9
1,2-Dichlorobenzene ug/kg 7.7 M119.8 39 70-130<2.0
1,2-Dichloroethane ug/kg 15.319.8 77 70-130<2.4
1,2-Dichloropropane ug/kg 16.219.8 82 70-130<1.8
1,4-Dichlorobenzene ug/kg 8.4 M119.8 42 70-130<1.8
2-Butanone (MEK)ug/kg 27.7J39.5 70 70-130<3.1
2-Hexanone ug/kg 26.3J M139.5 67 70-130<4.2
4-Methyl-2-pentanone (MIBK)ug/kg 30.5J39.5 77 70-130<4.0
Acetone ug/kg 35J39.5 88 70-130<10.8
Acrylonitrile ug/kg 75.2J98.8 76 70-130<28.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
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Huntersville, NC 28078
[phone]
Page 31 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2060390MATRIX SPIKE SAMPLE:
MSSpike
Result
92349874001
Benzene ug/kg 16.719.8 84 50-166<1.7
Bromochloromethane ug/kg 14.519.8 73 70-130<1.8
Bromodichloromethane ug/kg 15.219.8 77 70-130<2.0
Bromoform ug/kg 9.9 M119.8 50 70-130<2.5
Bromomethane ug/kg 18.519.8 94 70-130<2.7
Carbon disulfide ug/kg 17.319.8 88 70-130<3.2
Carbon tetrachloride ug/kg 19.619.8 99 70-130<2.8
Chlorobenzene ug/kg 12.419.8 63 43-169<2.0
Chloroethane ug/kg 20.519.8 104 70-130<2.6
Chloroform ug/kg 16.719.8 84 70-130<1.7
Chloromethane ug/kg 20.419.8 103 70-130<2.6
cis-1,2-Dichloroethene ug/kg 16.219.8 82 70-130<1.5
cis-1,3-Dichloropropene ug/kg 12.7 M119.8 64 70-130<1.9
Dibromochloromethane ug/kg 12.7 M119.8 64 70-130<1.9
Dibromomethane ug/kg 13.1 M119.8 66 70-130<2.7
Ethylbenzene ug/kg 16.119.8 81 70-130<1.9
Iodomethane ug/kg 27.1 M139.5 68 70-130<10.7
m&p-Xylene ug/kg 30.939.5 78 70-130<3.9
Methylene Chloride ug/kg 29.119.8 81 70-13013.1J
o-Xylene ug/kg 13.819.8 70 70-130<2.0
Styrene ug/kg 9.6 M119.8 48 70-130<1.9
Tetrachloroethene ug/kg 17.519.8 89 70-130<1.8
Toluene ug/kg 15.819.8 80 52-163<1.9
trans-1,2-Dichloroethene ug/kg 17.719.8 90 70-130<2.0
trans-1,3-Dichloropropene ug/kg 10.9 M119.8 55 70-130<1.6
trans-1,4-Dichloro-2-butene ug/kg 6.1 M019.8 31 70-130<3.9
Trichloroethene ug/kg 16.219.8 82 49-167<2.3
Trichlorofluoromethane ug/kg 21.319.8 108 70-130<2.4
Vinyl acetate ug/kg 9.4J M139.5 24 70-130<9.5
Vinyl chloride ug/kg 18.819.8 95 70-130<1.9
1,2-Dichloroethane-d4 (S)%100 70-132
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result QualifiersRPDResult
35327344001
2060389SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND
1,1,1-Trichloroethane ug/kg ND
1,1,2,2-Tetrachloroethane ug/kg ND
1,1,2-Trichloroethane ug/kg ND
1,1-Dichloroethane ug/kg ND
1,1-Dichloroethene ug/kg ND
1,2,3-Trichloropropane ug/kg ND
1,2-Dibromo-3-chloropropane ug/kg ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
35327344001
2060389SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/kg ND
1,2-Dichlorobenzene ug/kg ND
1,2-Dichloroethane ug/kg ND
1,2-Dichloropropane ug/kg ND
1,4-Dichlorobenzene ug/kg ND
2-Butanone (MEK)ug/kg 4.9J
2-Hexanone ug/kg ND
4-Methyl-2-pentanone (MIBK)ug/kg ND
Acetone ug/kg 73.8J
Acrylonitrile ug/kg ND
Benzene ug/kg ND1.7U
Bromochloromethane ug/kg ND
Bromodichloromethane ug/kg ND
Bromoform ug/kg ND
Bromomethane ug/kg ND
Carbon disulfide ug/kg ND
Carbon tetrachloride ug/kg ND
Chlorobenzene ug/kg ND
Chloroethane ug/kg ND
Chloroform ug/kg ND
Chloromethane ug/kg ND
cis-1,2-Dichloroethene ug/kg ND
cis-1,3-Dichloropropene ug/kg ND
Dibromochloromethane ug/kg ND
Dibromomethane ug/kg ND
Ethylbenzene ug/kg ND1.9U
Iodomethane ug/kg ND
m&p-Xylene ug/kg ND3.7U
Methylene Chloride ug/kg ND
o-Xylene ug/kg ND2.0U
Styrene ug/kg ND
Tetrachloroethene ug/kg ND
Toluene ug/kg ND1.9U
trans-1,2-Dichloroethene ug/kg ND
trans-1,3-Dichloropropene ug/kg ND
trans-1,4-Dichloro-2-butene ug/kg ND
Trichloroethene ug/kg ND
Trichlorofluoromethane ug/kg ND
Vinyl acetate ug/kg ND
Vinyl chloride ug/kg ND
Xylene (Total)ug/kg ND3.7U
1,2-Dichloroethane-d4 (S)%107 4106
4-Bromofluorobenzene (S)%94 394
Toluene-d8 (S)%98 199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92349769
Leachate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
371434
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92349769001, 92349769002, 92349769003, 92349769004, 92349769005, 92349769006, 92349769007,
92349769008, 92349769009, 92349769010
Parameter Units
Dup
Result QualifiersRPDResult
92349769001
2057962SAMPLE DUPLICATE:
Percent Moisture %14.1 213.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92349769
Leachate
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92349769
Leachate
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92349769001 371497SB-1 EPA 8260
92349769002 371497SB-2 EPA 8260
92349769003 371497SB-3 EPA 8260
92349769004 371497SB-4 EPA 8260
92349769005 371769SB-5 EPA 8260
92349769006 371769SB-6 EPA 8260
92349769007 371769SB-7 EPA 8260
92349769008 371497SB-8 EPA 8260
92349769009 371497SB-9 EPA 8260
92349769010 371497SB-10 EPA 8260
92349769001 371434SB-1 ASTM D2974-87
92349769002 371434SB-2 ASTM D2974-87
92349769003 371434SB-3 ASTM D2974-87
92349769004 371434SB-4 ASTM D2974-87
92349769005 371434SB-5 ASTM D2974-87
92349769006 371434SB-6 ASTM D2974-87
92349769007 371434SB-7 ASTM D2974-87
92349769008 371434SB-8 ASTM D2974-87
92349769009 371434SB-9 ASTM D2974-87
92349769010 371434SB-10 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2017 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 37
Page 37 of 37