9003_GriffinFarmsCDLF_April2016GWMR_28435_20161028

Griffin Farms C&D Landfill
Union County, North Carolina
April 2016
Permit Number: 90-03
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.
Garner and Boone, North Carolina
MESCO Project Number: G15011.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 3
Surface Water Samples Page 3
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 3
FIGURES
Single-Day Potentiometric Map of Uppermost Aquifer Figure 1
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, 2B or MCL Table 5
APPENDICIES
Laboratory Analysis Report, Chains of Custody Appendix A
Field Parameter Data Sheet(s) Appendix B
October 28, 2016
Mr. Ervin Lane
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
217 West Jones Street
Raleigh, NC 27603
Re: Semi-Annual Water Quality Monitoring Report
Griffin Farms Inactive Construction and Demolition Landfill
Permit No. 90-03
MESCO Project No. G15011.0
Event Date: April 7, 2016
Dear Mr. Lane:
Introduction
On behalf of Griffin Farms Incorporated, Municipal Engineering Services Company, P.A. (MESCO) is pleased to
present this Semi-Annual Water Quality Report for the spring 2016 event performed at the Inactive Construction and
Demolition (C&D) Landfill. NCDENR (now NCDEQ) Solid Waste Rules 15A NCAC 13B.0601 requires that
Griffin Farms provide this report to the SWS on a semi-annual basis. This report documents the quality of the
ground and surface waters during this monitoring event performed on April 7, 2016. During this event, there were
no constituents detected in any water sample in concentrations above applicable water quality Standards.
Background
The Griffin Farms Inactive C&D Landfill is located at 4242 Morgan Mill Road (NC 200), Unionville, Union
County, North Carolina. The C&D landfill footprint is less then 15 acres and the property encompasses
approximately 131 acres. The landfill stopped receiving waste prior to June 30, 2008. Water quality detection
monitoring has been performed at this facility on at least a semi-annual basis with historical data since prior to 1999
reviewed in support of this report.
As specified in rules 15A NCAC 13B.0601, the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization, and findings. Well construction summary table, field observations table, field parameter data table,
sampling and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates
table, potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed
herein.

Sampling Procedure
MESCO personnel performed this sampling event utilizing portable monitoring methodology in accordance with the
site-specific, approved Sampling and Analysis Plans (SAP) and the NCDENR SWS guidance document Solid Waste
Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. Water samples were
collected from six groundwater monitoring wells (MW-2R, MW-3, MW-4S, MW-4D, MW-5, MW-6R), one
background well (MW-1), and both surface water points (SW-3 and SW-4). Quality control measures were
implemented which included analysis of an equipment blank (EB) and a trip blank (TB). Groundwater depths were
also recorded from P-23 and PW-6D to better characterize flow directions and gradients. Water monitoring locations
are shown on the single-day potentiometric map, Figure 1.
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated and no significant deficiencies identified as documented
on Table 2. The depth to water in each well was electronically gaged prior to purging to quantify the static water
level elevation. Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum
of three times the volume of standing water in the well or until dry. Surface water samples were collected from
Chinkapin Creek at previously designated locations. During well purging and surface water sample collection the
stabilized field parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved
containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-
certified laboratory under proper C-O-C protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature, total
dissolved solids (TDS), visual turbidity and methane gas in well headspace. A summary of the field parameter data is
presented in Table 3 and the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratory Inc. (PACE) of Huntersville and Asheville, NC, performed the laboratory analysis. All
water samples were analyzed for the Appendix I list of VOCs and total metals as listed in the current 40 CFR 258,
total mercury and tetrahydrofuran. Additionally, two groundwater samples (MW-3R, MW-4R) were analyzed for
Appendix I dissolved metals since a few total metal concentrations were elevated. A table summarizing the monitored
locations, targeted constituents, and laboratory methods is presented on Table 4.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 2 summarizes constituents detected in groundwater and surface
water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North Carolina
Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a class C waterbody, and
Maximum Contaminant Levels (MCL) also known as “Federal Primary Drinking Water Standards”. Laboratory
results and C-O-Cs are presented in Appendix A.
Quality Control Samples
Both quality control samples TB and EB contained methylene chloride. Methylene chloride was also detected in
samples MW-4R, MW-7, SW-3 and SW-4 in levels comparable to those reported in the blanks. All of the detections
of methylene chloride were below applicable Standards and were flagged by the laboratory as C9 indicating a
“common laboratory contaminant”. Methylene chloride detections are considered false positives attributed to the
identified laboratory induced artifact contamination and should not be misconstrued as evidence of a release.
2
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Tables
Griffin Farms C&D Landfill Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
April 7, 2016
Latitude Longitude
(inches)(ft)
MW-1 10/24/95 2 42.5 534.83 531.94 518.74 16.09 33.859417 -85.264933
MW-2 12/5/95 2 45 545.99 543.63 501.79 44.2 33.859806 -85.262269
MW-3R 1/5/98 2 15 Sandy silty clay 498.05 494.76 492.02 6.03 33.861206 -85.261497
MW-4R 1/5/98 2 16 Sandy silty clay 498.52*495.45 494.01 4.51 33.853692 -85.261847
MW-5 11/22/95 2 16 501.52 498.78 494.99 6.53 33.863058 -85.262992
MW-6 12/6/95 2 21 514.02 511.22 504.97 9.05 33.861911 -85.264478
MW-7 10/25/95 2 22 520.17 517.18 514.72 5.45 33.860736 -85.264781
P-23 1/6/98 2 15.5 Sandy silty clay 496.59 493.55 488.47 8.12 33.858967 -85.260808
* = MW-4R stickup repaired between April-October 2013; therefore casing elevation may have changed
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length Geology of
Screened Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
na na Weathered argillite
na na Weathered argillite
na na
na na
na na Weathered argillite
na na Weathered argillite
na na Weathered argillite
na na
na = Not available
Griffin Farms C&D Landfill Page 1 of 1
Table 2
Field Observations of Monitoring Locations
April 7, 2016
Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes Slight constriction.
MW-3R Yes Yes Yes Yes Yes Yes Lock rusty
MW-4R Yes Yes Yes Yes Yes Yes Slight constriction
MW-5 Yes Yes Yes Yes Yes Yes
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes Under trash can
PW-6D Yes Yes Yes -Yes Yes
SW-3 Yes -----Low seasonal gage height & flow
SW-4 Yes -----Low seasonal gage height & flow
Any unusual field conditions, observations, or events:
C&D Landfill still inactive.
MW-4R was damaged and repaired since April 2013. Top of casing datum elevation may have changed.
Pump barely descends past PVC constriction in MW-4R. Pump needs pushed with bailer to descend.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Effective
Griffin Farms C&D Landfill Page 1 of 1
Table 3
Field Parameter Data Summary
April 7, 2016
Parameter DO ORP pH Temp.TDS
Units mg/L SU C mg/L %/Vol Visual
MW-1 16.09 518.74 534.83 NR NR 6.6 16.1 200 NR 0 Clear
MW-2 44.20 501.79 545.99 NR NR 6.4 15.9 500 NR 0 Slight
MW-3R 6.03 492.02 498.05 NR NR 6.6 14.2 210 NR 0 Clear
MW-4R 4.51 494.01*498.52 *NR NR 6.5 14.1 60 NR 0 Clear
MW-5 6.53 494.99 501.52 NR NR 6.1 13.9 1300 NR 0 Slight
MW-6 9.05 504.97 514.02 NR NR 6.1 16.1 690 NR 0 Clear
MW-7 5.45 514.72 520.17 NR NR 6.4 15.2 1510 NR 0 Clear
PW-6D 5.54 508.12 513.66 NR NR NR NR 90 NR NR NR
P-19
P-23 8.12 488.47 496.59 NR NR NR NR NR NR 0 NR
Minimum 5.73 490.57 498.05 NR NR 6.1 13.9 60 NR 0 Clear
Average 14.85 499.34 515.49 NR NR 6.4 15.1 493 NR 0 Clear
Maximum 45.45 515.73 545.99 NR NR 6.6 16.1 1510 NR 0 Slight
SW-3 ---NR NR 6.9 18.2 90 NR -Clear
SW-4 ---NR NR 6.9 18.1 70 NR -Clear
Minimum ---NR NR 6.9 18.1 70 NR -Clear
Average ---NR NR 6.9 18.2 80 NR -Clear
Maximum ---NR NR 6.9 18.2 90 NR -Clear
NR = No Reading Attempted
* = TOC elevation at MW-4R may have changed since 4/24/13 due to repair.
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane
Gas in
Headspace
Degree of
Visual
Turbidity of
Collected
Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
No Readings since piezometer has been destroyed since 4/24/13
Griffin Farms C&D Landfill Page 1 of 1
Table 4
Sampling and Analysis Summary
April 7, 2016
Misc.C&D Field Parameter
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MW-1 x x x x x x x x x x
MW-2 x x x x x x x x x x
MW-3R x x x x x x x x x x x
MW-4R x x x x x x x x x x x
MW-5 x x x x x x x x x x
MW-6 x x x x x x x x x x
MW-7 x x x x x x x x x x
SW-3 x x x x x x x x
SW-4 x x x x x x x x
EB x x
TB x x
Appendix I = List from current 40 CFR 258
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Griffin Farms C&D Landfill Page 1 of 1
Table 5
Detections in Water Samples Above Established SWSL, GWP, 2L, 2B, or MCL
April 7, 2016
Result Unit
MW-3R Cadmium, total 4/07/16 1.6 0.5 1 2 5
MW-4R Methylene Chloride 4/07/16 1.9 (C9)0.97 1 4.6 5
MW-5 4/07/16 7.3J 3.1 NE NE NE NE
MW-5 Cobalt, total 4/07/16 59.3 2.5 10 70 NE
MW-5 Barium, total 4/07/16 136 2.5 100 700 2000
MW-6 4/07/16 3.2J 3.1 NE NE NE NE
MW-6 Cobalt, total 4/07/16 15.8 2.5 10 70 NE
MW-7 Cobalt, total 4/07/16 15.1 2.5 10 70 NE
MW-7 Methylene Chloride 4/07/16 2.6 (C9)0.97 1 4.6 5
SW-3 Methylene Chloride 4/07/16 2.4 (C9)0.97 1 4.6 4.6 5
SW-4 Methylene Chloride 4/07/16 3.4 (C9)0.97 1 4.6 4.6 5
TB Methylene Chloride 4/07/16 2.4 (C9)0.97 1 4.6 5
EB Methylene Chloride 4/07/16 2.1 (C9)0.97 1 4.6 5
A definitive source of the detection was not determined as part of this report.
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
(C9) = Laboratory flagged as “common laboratory contaminant”
NE = Not Established
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
Tetrahydrofuran ug/L
ug/L
ug/L
Tetrahydrofuran ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, 2L, 2B, GWP or MCL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
April 21, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92293142
92293142
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
GRIFFIN FARMS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on April 08, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 36
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Lab ID Sample ID Matrix Date Collected Date Received
92293142001 MW-1 Water 04/07/16 14:15 04/08/16 08:17
92293142002 MW-2 Water 04/07/16 13:45 04/08/16 08:17
92293142003 MW-3R Water 04/07/16 13:10 04/08/16 08:17
92293142004 MW-4R Water 04/07/16 12:35 04/08/16 08:17
92293142005 MW-5 Water 04/07/16 12:00 04/08/16 08:17
92293142006 MW-6 Water 04/07/16 10:10 04/08/16 08:17
92293142007 MW-7 Water 04/07/16 10:50 04/08/16 08:17
92293142008 SW-3 Water 04/07/16 11:15 04/08/16 08:17
92293142009 SW-4 Water 04/07/16 14:35 04/08/16 08:17
92293142010 TB Water 04/07/16 00:00 04/08/16 08:17
92293142011 EB Water 04/07/16 14:50 04/08/16 08:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92293142001 MW-1 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142002 MW-2 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142003 MW-3R EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142004 MW-4R EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142005 MW-5 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142006 MW-6 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142007 MW-7 EPA 6010 15 PASI-ACDF
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92293142008 SW-3 EPA 6010 15 PASI-ACDF
EPA 8260 51 PASI-CGAW
92293142009 SW-4 EPA 6010 15 PASI-ACDF
EPA 8260 51 PASI-CGAW
92293142010 TB EPA 8260 51 PASI-CGAW
92293142011 EB EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-1 Lab ID:92293142001 Collected:04/07/16 14:15 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 18:47 7440-36-004/11/16 23:506.0 3.8 1
Arsenic ND ug/L 04/13/16 18:47 7440-38-204/11/16 23:5010.0 2.5 1
Barium 4.9J ug/L 04/13/16 18:47 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 18:47 7440-41-704/11/16 23:501.0 0.50 1
Cadmium 0.80J ug/L 04/13/16 18:47 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 18:47 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt ND ug/L 04/13/16 18:47 7440-48-404/11/16 23:5010.0 2.5 1
Copper 5.4J ug/L 04/13/16 18:47 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 18:47 7439-92-104/11/16 23:5010.0 2.5 1
Nickel ND ug/L 04/13/16 18:47 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 18:47 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 18:47 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 18:47 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 18:47 7440-62-204/11/16 23:5025.0 2.5 1
Zinc 5.3J ug/L 04/13/16 18:47 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:16 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 15:14 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 15:14 107-13-12001.9 1
Benzene ND ug/L 04/14/16 15:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 15:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 15:14 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 15:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 15:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 15:14 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 15:14 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 15:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 15:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 15:14 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 15:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 15:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 15:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 15:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 15:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 15:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 15:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 15:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 15:14 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 15:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 15:14 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 15:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 15:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 15:14 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-1 Lab ID:92293142001 Collected:04/07/16 14:15 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 15:14 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 15:14 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 15:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 15:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 15:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 15:14 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/16 15:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 15:14 108-10-11000.33 1
Styrene ND ug/L 04/14/16 15:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 15:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 15:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 15:14 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 15:14 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 15:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 15:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 15:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 15:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 15:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 15:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 15:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 15:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 15:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %04/14/16 15:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %04/14/16 15:14 17060-07-070-130 1
Toluene-d8 (S)102 %04/14/16 15:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-2 Lab ID:92293142002 Collected:04/07/16 13:45 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 18:50 7440-36-004/11/16 23:506.0 3.8 1
Arsenic ND ug/L 04/13/16 18:50 7440-38-204/11/16 23:5010.0 2.5 1
Barium 3.5J ug/L 04/13/16 18:50 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 18:50 7440-41-704/11/16 23:501.0 0.50 1
Cadmium 0.99J ug/L 04/13/16 18:50 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 18:50 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt ND ug/L 04/13/16 18:50 7440-48-404/11/16 23:5010.0 2.5 1
Copper 4.0J ug/L 04/13/16 18:50 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 18:50 7439-92-104/11/16 23:5010.0 2.5 1
Nickel ND ug/L 04/13/16 18:50 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 18:50 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 18:50 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 18:50 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 18:50 7440-62-204/11/16 23:5025.0 2.5 1
Zinc ND ug/L 04/13/16 18:50 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:19 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 15:30 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 15:30 107-13-12001.9 1
Benzene ND ug/L 04/14/16 15:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 15:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 15:30 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 15:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 15:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 15:30 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 15:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 15:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 15:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 15:30 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 15:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 15:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 15:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 15:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 15:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 15:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 15:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 15:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 15:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 15:30 75-34-35.0 0.32 1
1,2-Dichloroethane 0.34J ug/L 04/14/16 15:30 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 15:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 15:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 15:30 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-2 Lab ID:92293142002 Collected:04/07/16 13:45 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 15:30 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 15:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 15:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 15:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 15:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 15:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/16 15:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 15:30 108-10-11000.33 1
Styrene ND ug/L 04/14/16 15:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 15:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 15:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 15:30 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 15:30 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 15:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 15:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 15:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 15:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 15:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 15:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 15:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 15:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 15:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %04/14/16 15:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %04/14/16 15:30 17060-07-070-130 1
Toluene-d8 (S)100 %04/14/16 15:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-3R Lab ID:92293142003 Collected:04/07/16 13:10 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 18:53 7440-36-004/11/16 23:506.0 3.8 1
Arsenic ND ug/L 04/13/16 18:53 7440-38-204/11/16 23:5010.0 2.5 1
Barium 35.9J ug/L 04/13/16 18:53 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 18:53 7440-41-704/11/16 23:501.0 0.50 1
Cadmium 1.6 ug/L 04/13/16 18:53 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 18:53 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt ND ug/L 04/13/16 18:53 7440-48-404/11/16 23:5010.0 2.5 1
Copper ND ug/L 04/13/16 18:53 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 18:53 7439-92-104/11/16 23:5010.0 2.5 1
Nickel ND ug/L 04/13/16 18:53 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 18:53 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 18:53 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 18:53 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 18:53 7440-62-204/11/16 23:5025.0 2.5 1
Zinc ND ug/L 04/13/16 18:53 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:21 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 15:47 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 15:47 107-13-12001.9 1
Benzene ND ug/L 04/14/16 15:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 15:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 15:47 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 15:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 15:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 15:47 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 15:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 15:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 15:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 15:47 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 15:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 15:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 15:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 15:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 15:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 15:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 15:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 15:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 15:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 15:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 15:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 15:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 15:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 15:47 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-3R Lab ID:92293142003 Collected:04/07/16 13:10 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 15:47 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 15:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 15:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 15:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 15:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 15:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/16 15:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 15:47 108-10-11000.33 1
Styrene ND ug/L 04/14/16 15:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 15:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 15:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 15:47 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 15:47 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 15:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 15:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 15:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 15:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 15:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 15:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 15:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 15:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 15:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %04/14/16 15:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %04/14/16 15:47 17060-07-070-130 1
Toluene-d8 (S)99 %04/14/16 15:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-4R Lab ID:92293142004 Collected:04/07/16 12:35 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 18:56 7440-36-004/11/16 23:506.0 3.8 1
Arsenic 3.1J ug/L 04/13/16 18:56 7440-38-204/11/16 23:5010.0 2.5 1
Barium 27.3J ug/L 04/13/16 18:56 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 18:56 7440-41-704/11/16 23:501.0 0.50 1
Cadmium 0.73J ug/L 04/13/16 18:56 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 18:56 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt 7.2J ug/L 04/13/16 18:56 7440-48-404/11/16 23:5010.0 2.5 1
Copper 2.6J ug/L 04/13/16 18:56 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 18:56 7439-92-104/11/16 23:5010.0 2.5 1
Nickel ND ug/L 04/13/16 18:56 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 18:56 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 18:56 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 18:56 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 18:56 7440-62-204/11/16 23:5025.0 2.5 1
Zinc ND ug/L 04/13/16 18:56 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:24 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 16:04 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 16:04 107-13-12001.9 1
Benzene ND ug/L 04/14/16 16:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 16:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 16:04 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 16:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 16:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 16:04 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 16:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 16:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 16:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 16:04 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 16:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 16:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 16:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 16:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 16:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 16:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 16:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 16:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 16:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 16:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 16:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 16:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 16:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 16:04 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-4R Lab ID:92293142004 Collected:04/07/16 12:35 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 16:04 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 16:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 16:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 16:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 16:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 16:04 74-88-410.0 0.32 1
Methylene Chloride 1.9 ug/L 04/14/16 16:04 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 16:04 108-10-11000.33 1
Styrene ND ug/L 04/14/16 16:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 16:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 16:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 16:04 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 16:04 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 16:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 16:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 16:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 16:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 16:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 16:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 16:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 16:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 16:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %04/14/16 16:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %04/14/16 16:04 17060-07-070-130 1
Toluene-d8 (S)105 %04/14/16 16:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-5 Lab ID:92293142005 Collected:04/07/16 12:00 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 18:59 7440-36-004/11/16 23:506.0 3.8 1
Arsenic ND ug/L 04/13/16 18:59 7440-38-204/11/16 23:5010.0 2.5 1
Barium 136 ug/L 04/13/16 18:59 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 18:59 7440-41-704/11/16 23:501.0 0.50 1
Cadmium ND ug/L 04/13/16 18:59 7440-43-904/11/16 23:501.0 0.50 1
Chromium 2.9J ug/L 04/13/16 18:59 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt 59.3 ug/L 04/13/16 18:59 7440-48-404/11/16 23:5010.0 2.5 1
Copper 3.1J ug/L 04/13/16 18:59 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 18:59 7439-92-104/11/16 23:5010.0 2.5 1
Nickel 5.9J ug/L 04/13/16 18:59 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 18:59 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 18:59 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 18:59 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 18:59 7440-62-204/11/16 23:5025.0 2.5 1
Zinc ND ug/L 04/13/16 18:59 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:26 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 16:20 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 16:20 107-13-12001.9 1
Benzene 0.64J ug/L 04/14/16 16:20 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 16:20 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 16:20 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 16:20 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 16:20 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 16:20 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 16:20 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 16:20 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 16:20 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 16:20 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 16:20 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 16:20 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 16:20 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 16:20 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 16:20 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 16:20 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 16:20 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 16:20 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 16:20 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 16:20 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 16:20 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 16:20 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 16:20 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 16:20 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-5 Lab ID:92293142005 Collected:04/07/16 12:00 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 16:20 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 16:20 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 16:20 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 16:20 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 16:20 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 16:20 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/16 16:20 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 16:20 108-10-11000.33 1
Styrene ND ug/L 04/14/16 16:20 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 16:20 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 16:20 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 16:20 127-18-41.0 0.46 1
Tetrahydrofuran 7.3J ug/L 04/14/16 16:20 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 16:20 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 16:20 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 16:20 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 16:20 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 16:20 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 16:20 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 16:20 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 16:20 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 16:20 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %04/14/16 16:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %04/14/16 16:20 17060-07-070-130 1
Toluene-d8 (S)101 %04/14/16 16:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-6 Lab ID:92293142006 Collected:04/07/16 10:10 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 19:12 7440-36-004/11/16 23:506.0 3.8 1
Arsenic 3.5J ug/L 04/13/16 19:12 7440-38-204/11/16 23:5010.0 2.5 1
Barium 16.2J ug/L 04/13/16 19:12 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 19:12 7440-41-704/11/16 23:501.0 0.50 1
Cadmium ND ug/L 04/13/16 19:12 7440-43-904/11/16 23:501.0 0.50 1
Chromium 4.1J ug/L 04/13/16 19:12 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt 15.8 ug/L 04/13/16 19:12 7440-48-404/11/16 23:5010.0 2.5 1
Copper 2.8J ug/L 04/13/16 19:12 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 19:12 7439-92-104/11/16 23:5010.0 2.5 1
Nickel 4.6J ug/L 04/13/16 19:12 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 19:12 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 19:12 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 19:12 7440-28-004/11/16 23:505.5 5.0 1
Vanadium 3.1J ug/L 04/13/16 19:12 7440-62-204/11/16 23:5025.0 2.5 1
Zinc 7.6J ug/L 04/13/16 19:12 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:28 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 16:37 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 16:37 107-13-12001.9 1
Benzene ND ug/L 04/14/16 16:37 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 16:37 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 16:37 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 16:37 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 16:37 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 16:37 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 16:37 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 16:37 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 16:37 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 16:37 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 16:37 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 16:37 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 16:37 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 16:37 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 16:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 16:37 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 16:37 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 16:37 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 16:37 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 16:37 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 16:37 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 16:37 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 16:37 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 16:37 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-6 Lab ID:92293142006 Collected:04/07/16 10:10 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 16:37 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 16:37 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 16:37 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 16:37 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 16:37 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 16:37 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 04/14/16 16:37 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 16:37 108-10-11000.33 1
Styrene ND ug/L 04/14/16 16:37 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 16:37 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 16:37 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 16:37 127-18-41.0 0.46 1
Tetrahydrofuran 3.2J ug/L 04/14/16 16:37 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 16:37 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 16:37 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 16:37 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 16:37 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 16:37 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 16:37 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 16:37 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 16:37 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 16:37 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %04/14/16 16:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %04/14/16 16:37 17060-07-070-130 1
Toluene-d8 (S)101 %04/14/16 16:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-7 Lab ID:92293142007 Collected:04/07/16 10:50 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 3.9J ug/L 04/13/16 19:15 7440-36-004/11/16 23:506.0 3.8 1
Arsenic ND ug/L 04/13/16 19:15 7440-38-204/11/16 23:5010.0 2.5 1
Barium 24.2J ug/L 04/13/16 19:15 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 19:15 7440-41-704/11/16 23:501.0 0.50 1
Cadmium ND ug/L 04/13/16 19:15 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 19:15 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt 15.1 ug/L 04/13/16 19:15 7440-48-404/11/16 23:5010.0 2.5 1
Copper ND ug/L 04/13/16 19:15 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 19:15 7439-92-104/11/16 23:5010.0 2.5 1
Nickel 14.2J ug/L 04/13/16 19:15 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 19:15 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 19:15 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 19:15 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 19:15 7440-62-204/11/16 23:5025.0 2.5 1
Zinc 7.4J ug/L 04/13/16 19:15 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/20/16 14:35 7439-97-604/11/16 14:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 16:54 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 16:54 107-13-12001.9 1
Benzene ND ug/L 04/14/16 16:54 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 16:54 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 16:54 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 16:54 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 16:54 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 16:54 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 16:54 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 16:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 16:54 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 16:54 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 16:54 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 16:54 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 16:54 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 16:54 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 16:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 16:54 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 16:54 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 16:54 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 16:54 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 16:54 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 16:54 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 16:54 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 16:54 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 16:54 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:MW-7 Lab ID:92293142007 Collected:04/07/16 10:50 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 04/14/16 16:54 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 16:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 16:54 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 16:54 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 16:54 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 16:54 74-88-410.0 0.32 1
Methylene Chloride 2.6 ug/L 04/14/16 16:54 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 16:54 108-10-11000.33 1
Styrene ND ug/L 04/14/16 16:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 16:54 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 16:54 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 16:54 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 16:54 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 16:54 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 16:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 16:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 16:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 16:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 16:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 16:54 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 16:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 16:54 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %04/14/16 16:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %04/14/16 16:54 17060-07-070-130 1
Toluene-d8 (S)101 %04/14/16 16:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:SW-3 Lab ID:92293142008 Collected:04/07/16 11:15 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 19:18 7440-36-004/11/16 23:506.0 3.8 1
Arsenic ND ug/L 04/13/16 19:18 7440-38-204/11/16 23:5010.0 2.5 1
Barium 22.5J ug/L 04/13/16 19:18 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 19:18 7440-41-704/11/16 23:501.0 0.50 1
Cadmium ND ug/L 04/13/16 19:18 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 19:18 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt ND ug/L 04/13/16 19:18 7440-48-404/11/16 23:5010.0 2.5 1
Copper ND ug/L 04/13/16 19:18 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 19:18 7439-92-104/11/16 23:5010.0 2.5 1
Nickel ND ug/L 04/13/16 19:18 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 19:18 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 19:18 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 19:18 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 19:18 7440-62-204/11/16 23:5025.0 2.5 1
Zinc ND ug/L 04/13/16 19:18 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 17:11 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 17:11 107-13-12001.9 1
Benzene ND ug/L 04/14/16 17:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 17:11 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 17:11 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 17:11 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 17:11 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 17:11 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 17:11 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 17:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 17:11 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 17:11 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 17:11 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 17:11 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 17:11 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 17:11 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 17:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 17:11 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 17:11 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 17:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 17:11 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 17:11 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 17:11 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 17:11 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 17:11 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 17:11 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/16 17:11 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 17:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 17:11 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:SW-3 Lab ID:92293142008 Collected:04/07/16 11:15 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 04/14/16 17:11 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 17:11 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 17:11 74-88-410.0 0.32 1
Methylene Chloride 2.4 ug/L 04/14/16 17:11 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 17:11 108-10-11000.33 1
Styrene ND ug/L 04/14/16 17:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 17:11 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 17:11 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 17:11 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 17:11 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 17:11 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 17:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 17:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 17:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 17:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 17:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 17:11 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 17:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 17:11 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %04/14/16 17:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %04/14/16 17:11 17060-07-070-130 1
Toluene-d8 (S)103 %04/14/16 17:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:SW-4 Lab ID:92293142009 Collected:04/07/16 14:35 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 04/13/16 19:21 7440-36-004/11/16 23:506.0 3.8 1
Arsenic 3.6J ug/L 04/13/16 19:21 7440-38-204/11/16 23:5010.0 2.5 1
Barium 22.4J ug/L 04/13/16 19:21 7440-39-304/11/16 23:501002.5 1
Beryllium ND ug/L 04/13/16 19:21 7440-41-704/11/16 23:501.0 0.50 1
Cadmium ND ug/L 04/13/16 19:21 7440-43-904/11/16 23:501.0 0.50 1
Chromium ND ug/L 04/13/16 19:21 7440-47-304/11/16 23:5010.0 2.5 1
Cobalt ND ug/L 04/13/16 19:21 7440-48-404/11/16 23:5010.0 2.5 1
Copper 2.6J ug/L 04/13/16 19:21 7440-50-804/11/16 23:5010.0 2.5 1
Lead ND ug/L 04/13/16 19:21 7439-92-104/11/16 23:5010.0 2.5 1
Nickel ND ug/L 04/13/16 19:21 7440-02-004/11/16 23:5050.0 2.5 1
Selenium ND ug/L 04/13/16 19:21 7782-49-204/11/16 23:5010.0 5.0 1
Silver ND ug/L 04/13/16 19:21 7440-22-404/11/16 23:5010.0 2.5 1
Thallium ND ug/L 04/13/16 19:21 7440-28-004/11/16 23:505.5 5.0 1
Vanadium ND ug/L 04/13/16 19:21 7440-62-204/11/16 23:5025.0 2.5 1
Zinc ND ug/L 04/13/16 19:21 7440-66-604/11/16 23:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 17:28 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 17:28 107-13-12001.9 1
Benzene ND ug/L 04/14/16 17:28 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 17:28 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 17:28 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 17:28 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 17:28 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 17:28 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 17:28 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 17:28 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 17:28 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 17:28 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 17:28 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 17:28 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 17:28 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 17:28 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 17:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 17:28 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 17:28 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 17:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 17:28 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 17:28 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 17:28 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 17:28 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 17:28 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 17:28 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/16 17:28 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 17:28 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 17:28 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:SW-4 Lab ID:92293142009 Collected:04/07/16 14:35 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 04/14/16 17:28 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 17:28 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 17:28 74-88-410.0 0.32 1
Methylene Chloride 3.4 ug/L 04/14/16 17:28 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 17:28 108-10-11000.33 1
Styrene ND ug/L 04/14/16 17:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 17:28 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 17:28 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 17:28 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 17:28 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 17:28 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 17:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 17:28 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 17:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 17:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 17:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 17:28 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 04/14/16 17:28 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 17:28 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %04/14/16 17:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %04/14/16 17:28 17060-07-070-130 1
Toluene-d8 (S)102 %04/14/16 17:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:TB Lab ID:92293142010 Collected:04/07/16 00:00 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 14:40 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 14:40 107-13-12001.9 1
Benzene ND ug/L 04/14/16 14:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 14:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 14:40 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 14:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 14:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 14:40 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 14:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 14:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 14:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 14:40 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 14:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 14:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 14:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 14:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 14:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 14:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 14:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 14:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 14:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 14:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 14:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 14:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 14:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 14:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/16 14:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 14:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 14:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 14:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 14:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 14:40 74-88-410.0 0.32 1
Methylene Chloride 2.4 ug/L 04/14/16 14:40 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 14:40 108-10-11000.33 1
Styrene ND ug/L 04/14/16 14:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 14:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 14:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 14:40 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 14:40 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 14:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 14:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 14:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 14:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 14:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 14:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 14:40 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:TB Lab ID:92293142010 Collected:04/07/16 00:00 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 04/14/16 14:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 14:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %04/14/16 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %04/14/16 14:40 17060-07-070-130 1
Toluene-d8 (S)101 %04/14/16 14:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:EB Lab ID:92293142011 Collected:04/07/16 14:50 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 04/14/16 14:57 67-64-110010.0 1
Acrylonitrile ND ug/L 04/14/16 14:57 107-13-12001.9 1
Benzene ND ug/L 04/14/16 14:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 04/14/16 14:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 04/14/16 14:57 75-27-41.0 0.18 1
Bromoform ND ug/L 04/14/16 14:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 04/14/16 14:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 04/14/16 14:57 78-93-31000.96 1
Carbon disulfide ND ug/L 04/14/16 14:57 75-15-01001.2 1
Carbon tetrachloride ND ug/L 04/14/16 14:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/14/16 14:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 04/14/16 14:57 75-00-310.0 0.54 1
Chloroform ND ug/L 04/14/16 14:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 04/14/16 14:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 04/14/16 14:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 04/14/16 14:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/14/16 14:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/14/16 14:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/14/16 14:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 04/14/16 14:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 04/14/16 14:57 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 04/14/16 14:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 04/14/16 14:57 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/14/16 14:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/14/16 14:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/14/16 14:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 04/14/16 14:57 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 04/14/16 14:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/14/16 14:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 04/14/16 14:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 04/14/16 14:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 04/14/16 14:57 74-88-410.0 0.32 1
Methylene Chloride 2.1 ug/L 04/14/16 14:57 75-09-2 C91.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/14/16 14:57 108-10-11000.33 1
Styrene ND ug/L 04/14/16 14:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/14/16 14:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/14/16 14:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 04/14/16 14:57 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 04/14/16 14:57 109-99-910.0 3.1 1
Toluene ND ug/L 04/14/16 14:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 04/14/16 14:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/14/16 14:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/14/16 14:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/14/16 14:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/14/16 14:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/14/16 14:57 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Sample:EB Lab ID:92293142011 Collected:04/07/16 14:50 Received:04/08/16 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 04/14/16 14:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/14/16 14:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %04/14/16 14:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %04/14/16 14:57 17060-07-070-130 1
Toluene-d8 (S)100 %04/14/16 14:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/9236
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1706336
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 04/20/16 13:390.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1706337LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1706338MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92292995005
1706339
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 96 75-12598 2 252.5ND 2.4 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/21326
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007,
92293142008, 92293142009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1706990
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007,
92293142008, 92293142009
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 04/13/16 18:203.8
Arsenic ug/L ND 10.0 04/13/16 18:202.5
Barium ug/L ND 100 04/13/16 18:202.5
Beryllium ug/L ND 1.0 04/13/16 18:200.50
Cadmium ug/L ND 1.0 04/13/16 18:200.50
Chromium ug/L ND 10.0 04/13/16 18:202.5
Cobalt ug/L ND 10.0 04/13/16 18:202.5
Copper ug/L ND 10.0 04/13/16 18:202.5
Lead ug/L ND 10.0 04/13/16 18:202.5
Nickel ug/L ND 50.0 04/13/16 18:202.5
Selenium ug/L ND 10.0 04/13/16 18:205.0
Silver ug/L ND 10.0 04/13/16 18:202.5
Thallium ug/L ND 5.5 04/13/16 18:205.0
Vanadium ug/L ND 25.0 04/13/16 18:202.5
Zinc ug/L ND 10.0 04/13/16 18:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1706991LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 454500 91 80-120
Arsenic ug/L 433500 87 80-120
Barium ug/L 469500 94 80-120
Beryllium ug/L 468500 94 80-120
Cadmium ug/L 459500 92 80-120
Chromium ug/L 465500 93 80-120
Cobalt ug/L 449500 90 80-120
Copper ug/L 461500 92 80-120
Lead ug/L 450500 90 80-120
Nickel ug/L 457500 91 80-120
Selenium ug/L 445500 89 80-120
Silver ug/L 232250 93 80-120
Thallium ug/L 459500 92 80-120
Vanadium ug/L 461500 92 80-120
Zinc ug/L 445500 89 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1706992MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92293126001
1706993
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 86 75-12587 2 25500ND430439
Arsenic ug/L 500 83 75-12585 2 25500ND414423
Barium ug/L 500 88 75-12589 1 2550022.8 462 466
Beryllium ug/L 500 88 75-12589 1 25500ND441446
Cadmium ug/L 500 86 75-12588 2 25500ND430439
Chromium ug/L 500 87 75-12588 1 25500ND435441
Cobalt ug/L 500 83 75-12584 2 25500ND413422
Copper ug/L 500 86 75-12588 2 25500ND431440
Lead ug/L 500 84 75-12585 2 25500ND419427
Nickel ug/L 500 84 75-12585 2 25500ND420428
Selenium ug/L 500 85 75-12586 2 25500ND425432
Silver ug/L 250 88 75-12590 2 25250ND219224
Thallium ug/L 500 84 75-12586 1 25500ND425431
Vanadium ug/L 500 88 75-12589 1 25500ND442447
Zinc ug/L 500 83 75-12584 2 2550012.2 427 434
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36365
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007,
92293142008, 92293142009, 92293142010, 92293142011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1710314
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007,
92293142008, 92293142009, 92293142010, 92293142011
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/14/16 13:170.33
1,1,1-Trichloroethane ug/L ND 1.0 04/14/16 13:170.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 04/14/16 13:170.40
1,1,2-Trichloroethane ug/L ND 1.0 04/14/16 13:170.29
1,1-Dichloroethane ug/L ND 5.0 04/14/16 13:170.32
1,1-Dichloroethene ug/L ND 5.0 04/14/16 13:170.56
1,2,3-Trichloropropane ug/L ND 1.0 04/14/16 13:170.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 04/14/16 13:172.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/14/16 13:170.27
1,2-Dichlorobenzene ug/L ND 5.0 04/14/16 13:170.30
1,2-Dichloroethane ug/L 0.30J 1.0 04/14/16 13:170.24
1,2-Dichloropropane ug/L ND 1.0 04/14/16 13:170.27
1,4-Dichlorobenzene ug/L ND 1.0 04/14/16 13:170.33
2-Butanone (MEK)ug/L ND 100 04/14/16 13:170.96
2-Hexanone ug/L ND 50.0 04/14/16 13:170.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 04/14/16 13:170.33
Acetone ug/L ND 100 04/14/16 13:1710.0
Acrylonitrile ug/L ND 200 04/14/16 13:171.9
Benzene ug/L ND 1.0 04/14/16 13:170.25
Bromochloromethane ug/L ND 3.0 04/14/16 13:170.17
Bromodichloromethane ug/L ND 1.0 04/14/16 13:170.18
Bromoform ug/L ND 3.0 04/14/16 13:170.26
Bromomethane ug/L ND 10.0 04/14/16 13:170.29
Carbon disulfide ug/L ND 100 04/14/16 13:171.2
Carbon tetrachloride ug/L ND 1.0 04/14/16 13:170.25
Chlorobenzene ug/L ND 3.0 04/14/16 13:170.23
Chloroethane ug/L ND 10.0 04/14/16 13:170.54
Chloroform ug/L ND 5.0 04/14/16 13:170.14
Chloromethane ug/L ND 1.0 04/14/16 13:170.11
cis-1,2-Dichloroethene ug/L ND 5.0 04/14/16 13:170.19
cis-1,3-Dichloropropene ug/L ND 1.0 04/14/16 13:170.13
Dibromochloromethane ug/L ND 3.0 04/14/16 13:170.21
Dibromomethane ug/L ND 10.0 04/14/16 13:170.21
Ethylbenzene ug/L ND 1.0 04/14/16 13:170.30
Iodomethane ug/L ND 10.0 04/14/16 13:170.32
Methylene Chloride ug/L ND 1.0 04/14/16 13:170.97
Styrene ug/L ND 1.0 04/14/16 13:170.26
Tetrachloroethene ug/L ND 1.0 04/14/16 13:170.46
Tetrahydrofuran ug/L ND 10.0 04/14/16 13:173.1
Toluene ug/L ND 1.0 04/14/16 13:170.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1710314
Associated Lab Samples:92293142001, 92293142002, 92293142003, 92293142004, 92293142005, 92293142006, 92293142007,
92293142008, 92293142009, 92293142010, 92293142011
Matrix:Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L ND 5.0 04/14/16 13:170.49
trans-1,3-Dichloropropene ug/L ND 1.0 04/14/16 13:170.26
trans-1,4-Dichloro-2-butene ug/L ND 100 04/14/16 13:171.0
Trichloroethene ug/L ND 1.0 04/14/16 13:170.47
Trichlorofluoromethane ug/L ND 1.0 04/14/16 13:170.20
Vinyl acetate ug/L ND 50.0 04/14/16 13:170.35
Vinyl chloride ug/L ND 1.0 04/14/16 13:170.62
Xylene (Total)ug/L ND 5.0 04/14/16 13:170.66
1,2-Dichloroethane-d4 (S)%105 70-130 04/14/16 13:17
4-Bromofluorobenzene (S)%100 70-130 04/14/16 13:17
Toluene-d8 (S)%101 70-130 04/14/16 13:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1710315LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 43.950 88 80-125
1,1,1-Trichloroethane ug/L 47.250 94 71-129
1,1,2,2-Tetrachloroethane ug/L 43.850 88 79-124
1,1,2-Trichloroethane ug/L 45.750 91 85-125
1,1-Dichloroethane ug/L 45.850 92 73-126
1,1-Dichloroethene ug/L 49.150 98 66-135
1,2,3-Trichloropropane ug/L 45.950 92 75-130
1,2-Dibromo-3-chloropropane ug/L 48.150 96 71-133
1,2-Dibromoethane (EDB)ug/L 45.850 92 83-124
1,2-Dichlorobenzene ug/L 43.450 87 80-133
1,2-Dichloroethane ug/L 47.550 95 67-128
1,2-Dichloropropane ug/L 43.550 87 75-132
1,4-Dichlorobenzene ug/L 45.850 92 78-130
2-Butanone (MEK)ug/L 96.4J100 96 61-144
2-Hexanone ug/L 94.0100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 94.3J100 94 72-135
Acetone ug/L 110100 110 48-146
Acrylonitrile ug/L 288250 115 40-160
Benzene ug/L 45.150 90 80-125
Bromochloromethane ug/L 51.450 103 71-125
Bromodichloromethane ug/L 45.950 92 78-124
Bromoform ug/L 44.450 89 71-128
Bromomethane ug/L 45.150 90 40-160
Carbon disulfide ug/L 53.6J50 107 50-160
Carbon tetrachloride ug/L 50.350 101 69-131
Chlorobenzene ug/L 44.050 88 81-122
Chloroethane ug/L 50.750 101 39-148
Chloroform ug/L 43.850 88 73-127
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
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Page 31 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1710315LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/L 50.750 101 44-146
cis-1,2-Dichloroethene ug/L 45.050 90 74-124
cis-1,3-Dichloropropene ug/L 46.750 93 72-132
Dibromochloromethane ug/L 44.050 88 78-125
Dibromomethane ug/L 45.750 91 82-120
Ethylbenzene ug/L 45.750 91 79-121
Iodomethane ug/L 93.0100 93 39-154
Methylene Chloride ug/L 47.950 96 64-133
Styrene ug/L 44.850 90 84-126
Tetrachloroethene ug/L 41.750 83 78-122
Tetrahydrofuran ug/L 465500 93 69-148
Toluene ug/L 43.150 86 80-121
trans-1,2-Dichloroethene ug/L 45.450 91 71-127
trans-1,3-Dichloropropene ug/L 44.950 90 69-141
trans-1,4-Dichloro-2-butene ug/L 44.2J50 88 40-160
Trichloroethene ug/L 44.950 90 78-122
Trichlorofluoromethane ug/L 50.150 100 53-137
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 47.650 95 58-137
Xylene (Total)ug/L 138150 92 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 32 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 33 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92293142
GRIFFIN FARMS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92293142001 MPRP/21326 ICP/19164MW-1 EPA 3010A EPA 6010
92293142002 MPRP/21326 ICP/19164MW-2 EPA 3010A EPA 6010
92293142003 MPRP/21326 ICP/19164MW-3R EPA 3010A EPA 6010
92293142004 MPRP/21326 ICP/19164MW-4R EPA 3010A EPA 6010
92293142005 MPRP/21326 ICP/19164MW-5 EPA 3010A EPA 6010
92293142006 MPRP/21326 ICP/19164MW-6 EPA 3010A EPA 6010
92293142007 MPRP/21326 ICP/19164MW-7 EPA 3010A EPA 6010
92293142008 MPRP/21326 ICP/19164SW-3 EPA 3010A EPA 6010
92293142009 MPRP/21326 ICP/19164SW-4 EPA 3010A EPA 6010
92293142001 MERP/9236 MERC/8872MW-1 EPA 7470 EPA 7470
92293142002 MERP/9236 MERC/8872MW-2 EPA 7470 EPA 7470
92293142003 MERP/9236 MERC/8872MW-3R EPA 7470 EPA 7470
92293142004 MERP/9236 MERC/8872MW-4R EPA 7470 EPA 7470
92293142005 MERP/9236 MERC/8872MW-5 EPA 7470 EPA 7470
92293142006 MERP/9236 MERC/8872MW-6 EPA 7470 EPA 7470
92293142007 MERP/9236 MERC/8872MW-7 EPA 7470 EPA 7470
92293142001 MSV/36365MW-1 EPA 8260
92293142002 MSV/36365MW-2 EPA 8260
92293142003 MSV/36365MW-3R EPA 8260
92293142004 MSV/36365MW-4R EPA 8260
92293142005 MSV/36365MW-5 EPA 8260
92293142006 MSV/36365MW-6 EPA 8260
92293142007 MSV/36365MW-7 EPA 8260
92293142008 MSV/36365SW-3 EPA 8260
92293142009 MSV/36365SW-4 EPA 8260
92293142010 MSV/36365TBEPA 8260
92293142011 MSV/36365EBEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 04/21/2016 03:06 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 34 of 36
Page 35 of 36
Page 36 of 36
Appendix B
Field Sampling Parameter Data Sheet(s)