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HomeMy WebLinkAbout0302_AlleghanyCoGWMR_Spring2017_DIN28325 ASSESSMENT/DETECTION MONITORING REPORT FOR THE ALLEGHANY COUNTY MUNICIPAL SOLID WASTE LANDFILL (CLOSED) SPARTA, NORTH CAROLINA Permit #03-03-T Land Use: Municipal Solid Waste Landfill. Prop. Owner:Alleghany County 348 South Main Street Sparta, North Carolina 28675 (336) 372-4179 Site Operator:Alleghany County 348 South Main Street Sparta, North Carolina 28675 (336) 372-4179 Date:June 5, 2017 Nat. of Release:Suspected hydrocarbon leachate discharge from landfill disposal Coordinates:Latitude(North): 36 29' 26" N Longitude(West): 81 08' 58" W Prepared By:Applied Resource Management, PC 257 Transfer Station Road P. O. Box 882 Hampstead, North Carolina 28443 (910) 270-2919 Fax (910) 270-2988 ARM Project #9625 ASSESSMENT/DETECTION MONITORING REPORT FOR THE SPARTA, NORTH CAROLINA ALLEGHANY COUNTY MUNICIPAL SOLID WASTE LANDFILL (CLOSED) Permit #03-03-T Land Use: Municipal Solid Waste Landfill. Prop. Owner:Alleghany County 348 South Main Street Sparta, North Carolina 28675 (336) 372-4179 Site Operator:Alleghany County 348 South Main Street Sparta, North Carolina 28675 (336) 372-4179 Date:June 5, 2017 Nat. of Release:Suspected hydrocarbon leachate discharge from landfill disposal Coordinates:Latitude(North): 36 29' 26" N Longitude(West): 81 08' 58" W Prepared By:Applied Resource Management, PC 257 Transfer Station Road P. O. Box 882 Hampstead, North Carolina 28443 (910) 270-2919 Fax (910) 270-2988 ARM Project #9625 TABLE OF CONTENTS Page 1.0 SUMMARY OF SAMPLING RESULTS 1 1.1 Summary of Analytical Results .................................1 1.2 Proximity of the Plume to the Nearest Receptor....................4 1.3 Description of Current Plume Size..............................5 1.4 Groundwater Flow Direction...................................5 1.5 Predictive Rate of Contaminant Transport........................6 2.0 CONCLUSIONS AND RECOMMENDATIONS 6 3.0 REFERENCES 7 TABLES TABLE 1 SEMI-ANNUAL MONITORING WELL, METHANE SCREENING, AND STREAM SAMPLING DATA SUMMARY TABLE 2 QUARTERLY METHANE MONITORING DATA SUMMARY TABLE 3 HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY FIGURES FIGURE 1 SITE MAP WITH MONITORING WELL AND STREAM SAMPLE LOCATIONS FIGURE 2 SITE MAP WITH DOMESTIC WELL LOCATIONS FIGURE 3 GROUNDWATER TABLE CONTOURS AS OF 6/21/17 APPENDICES APPENDIX A LABORATORY REPORTS APPENDIX B LANDFILL EDD ASSESSMENT/DETECTION MONITORING REPORT FOR THE ALLEGHANY COUNTY MUNICIPAL SOLID WASTE LANDFILL (CLOSED) SPARTA, NORTH CAROLINA PERMIT # 03-03-T PREPARED FOR: ALLEGHANY COUNTY SPARTA, NORTH CAROLINA JULY 11, 2017 1.0 SUMMARY OF SAMPLING RESULTS 1.1 Summary of Analytical Results (Refer to Tables 1, 2, and Appendix A) As summarized on the referenced tables, numerous sampling events have been conducted at the site on a semi-annual schedule. This event included the sampling of the five monitoring wells (0303T-MW1 thru 0303T-MW5), and two stream samples (0303T-ST1 and 0303T-ST2). Also, methane monitoring was conducted on-site at designated locations. Figure 1 is a Site Map With Monitoring Well And Stream Sample Locations. A Semi-Annual Monitoring Well, Methane Screening, And Stream Sampling Data Summary is provided in Table 1. Quarterly Methane Monitoring is summarized in Table 2. A Historical Groundwater Sampling Results Summary is provided in Table 3. Due to the accumulation of data over several years, the summary has been revised to include the previous three years of data. Review of the current analytical results for Appendix I Volatiles indicate that all monitoring wells were found to be compliant for all hydrocarbon compounds with the exception of 0303T-MW3 which contained a non-compliant vinyl chloride estimated concentration at 0.91 ppb, exceeding the NCAC 02L Groundwater Quality Standard at 0.03 ppb. Appendix I metals cobalt and barium were found during this event at non- compliant concentrations. 0303T-MW2 revealed cobalt at an estimated 0.0044 ppm. Also, 0303T-MW3 revealed a non-compliant barium concentration at 1.43 ppm, exceeding the NCAC 2L Groundwater Standard 1 July 11, 2017 of 0.7 ppm, and a non-complaint cobalt concentration at 0.0274 ppm, exceeding the Groundwater Protection Standard at 0.001 ppm. All other monitoring wells and stream samples were found to be compliant for all Appendix I Volatiles and Appendix I Metals. Historical results have revealed both 0303T-MW1 and 0303T-MW3 to contain fluctuating low compliant and non-compliant vinyl chloride and benzene concentrations. Benzene concentrations at 0303T-MW1 have ranged from below laboratory quantitation limits to 5.02 ppb, with this and several previous benzene concentrations found to be non-detected through June, 2011. 0303T-MW2 has historically revealed non-compliant methylene chloride concentrations ranging from 5.34 to 17.1 ppb. This event as well as the two previous events both revealed a non-detect concentration. 0303T- MW3 was found to be compliant for all Appendix I volatile compounds tested with the exception of vinyl chloride. Upgradient well, 0303T-MW4 previously revealed a non-compliant 2-Hexanone concentration of 55.4 ppb. This compound was found to be compliant during the last three consecutive events. The downgradient well, 0303T-MW5, located between 0303T-MW1 and Vile Creek, has consistently revealed all target compounds to be compliant. The previous event revealed a low level non-complaint chloromethane concentration at 6.8 ppb; however, this event revealed a compliant chloromethane concentration. All other monitoring wells and stream samples collected during this event and previous events were found to be compliant for Appendix I Volatiles. The Appendix I metals barium and cobalt were both found at 0303T-MW3 at non-compliant concentrations. Barium was identified at 1.43 ppm, slightly exceeding the State action limit of 0.7 ppm. Cobalt was found at 0.0274 ppm at 0303T-MW3, and estimated 0.0044 ppm at 0303T-MW2, both exceeding the Groundwater Protection Standards at 0.001 ppm. All other monitoring well and stream samples collected during this event for Appendix I metals were found to be compliant as compared with the NCAC 02L Groundwater Standards and Groundwater Protection Standards. Methane monitoring was conducted during this event at all five monitoring wells, the on-site methane well, and the enclosed structures identified as the scale house, the recycling center, and the tipping scale area. No measurable methane concentrations were found to be present at any of the monitoring well locations (see Table 1). Historically, low level methane readings have been periodically found in the wells ranging from 0 to 120 ppm. LEL readings were consistent at 0% during this event. No detectable methane levels were found at the scale house, the recycling/storage center, 2 July 11, 2017 or the tipping scale area. The methane well, located in the central portion of the landfill, revealed methane concentrations ranging from 70 to 400 ppm and a LEL between 1% and 12%. A Quarterly Methane Monitoring Data Summary is provided in Table 2. Results of Well Gauging A Semi-Annual Monitoring Well and Stream Sampling Data Summary is presented in Table 1. Depth to the groundwater table, as measured on 6/21/17, ranged from 4.02 to 33.11 feet. Sampling Methods and Results (Refer to Table 3 and Appendix A) As part of this monitoring event, five monitoring wells, 0303T-MW1 through 0303T-MW5 were purged of at least three well volumes of groundwater and sampled. Also, two stream samples, 0303T-ST1 and 0303T-ST2 were collected. All of the monitoring well groundwater samples and stream samples were analyzed by Pace Analytical Services, LLC for Appendix I Volatiles and Appendix I Metals. Review of historical results have shown low level hydrocarbon concentrations of benzene and vinyl chloride exceeding NCAC 02L Groundwater Standards at monitoring well 0303T-MW1. Benzene concentrations at 0303T-MW1 have historically ranged from below laboratory quantitation limits to 5.02 ppb, exceeding the State action limit of 1 ppb. Both compounds at this well location have been non-detected for the past several events. This event revealed two monitoring wells, 0303T-MW2 and 0303T-MW3 to be non-compliant. 0303T-MW2 revealed the Appendix I metal cobalt at an estimated concentration of 0.0044 ppm. Also, 0303T-MW3 revealed a non- compliant barium concentration at 1.43 ppm, exceeding the NCAC 2L Groundwater Standard of 0.7 ppm, and a non-complaint cobalt concentration at 0.0274 ppm, exceeding the Groundwater Protection Standard at 0.001 ppm. All other monitoring well and stream samples collected during this event for Appendix I metals were found to be compliant as compared with the NCAC 02L Groundwater Standards and Groundwater Protection Standards. Review of the current analytical results for Appendix I Volatiles indicate that all monitoring wells and stream samples were found to be below their respective action levels for all hydrocarbon compounds with the exception of 0303T-MW3 which contained a non-compliant vinyl chloride estimated 3 July 11, 2017 concentration at 0.91 ppb, exceeding the NCAC 02L Groundwater Quality Standard at 0.03 ppb. 0303T-MW3 historically revealed vinyl chloride concentrations above the State action limit during several of the previous sampling events, although six of the previous or alternating events revealed vinyl chloride to be either below quantitation limits or not detected. 0303T- MW2 has been compliant for all hydrocarbon compounds during previous sampling events through June of 2010. Low levels of methylene chloride, 1,1 dichloroethane, and chloromethane have been detected in the well since that time. This event has revealed all hydrocarbon compounds to be at compliant levels. Up gradient well, 0303T-MW4 previously revealed a non- compliant 2-Hexanone concentration at 55.4 ppb, slightly exceeding the Groundwater Protection Standard at 40 ppb. The well has remained compliant during this and two previous events. The down gradient well, 0303T-MW5, located between 0303T-MW1 and Vile Creek, has revealed consistently compliant hydrocarbon concentrations with the exception of a low level non-compliant chloromethane concentration at 6.8 ppb during the previous sampling event. All other monitoring wells and stream samples collected during this event and previous events were found to be compliant for Appendix I Volatiles. Laboratory results are enclosed as Appendix A. Methane monitoring was conducted at the site utilizing an RKI Instruments Gas Tracer. No measurable methane concentrations were detected in any of the monitoring wells during this event. Historically, the monitoring wells were found to contain low level methane readings ranging from 0 to 120 ppm. LEL readings were consistent at 0%. The methane well, located in the central portion of the landfill, revealed methane concentrations ranging from 70 to 400 ppm, with a LEL between 1% and 12%. In addition, methane monitoring was conducted inside the enclosed structures identified as the scale house, the recycling center/storage area, and the tipping scale area. No measurable methane levels were detected at these locations. 1.2 Proximity of the Plume to the Nearest Receptor (Refer to Figure 2) Sensitive receptors of contamination, as defined by the NCDENR, include groundwater supply wells and subsurface building structures, as well as any potential for adverse impact to humans, plants, or animals. Five surrounding water supply wells were identified in 2008 by Alleghany County personnel within a 500 foot buffer of the former landfill. Figure 2 is a Site Map With Domestic Well Locations. A summary of surrounding water wells are as follows: 4 July 11, 2017 WELL # OWNER/ ADDRESS WELL TYPE/ USE MUNICIPAL WATER AVAILABLE MUNICIPAL WATER CONNECTION APPROXIMATE DISTANCE FROM SOURCE AREA OF RELEASE (ft.) 1 Alleghany Co. P.O. Box 366 Sparta, NC 28675 Drinking & Irrigation NO NO <200' 2 Marry Perry 501 Osborne Rd. Sparta, NC 28675 Drinking & Irrigation NO NO 490' 3 Mary & Rick Perry 464 Osborne Rd. Sparta, NC 28675 Drinking & Irrigation NO NO 420' 4 Billy Dale Alley 264 Osborne Road Sparta, NC 28675 Drinking & Irrigation NO NO 420' 5 Edwin & Laura Bloodworth 231 Osborne Rd. Sparta, NC 28675 Drinking & Irrigation NO NO 400' 1.3 Description of Current Plume Size Review of historical results have shown varying low level hydrocarbon concentrations of benzene and vinyl chloride exceeding NCAC T:15A 02L Groundwater Standards at monitoring well 0303T-MW1 and 0303T-MW3. Also, 0303T-MW2 has revealed low level methylene chloride and 1,1 dichloroethane concentrations during several previous events above the State action limit. This event revealed two monitoring wells, 0303T-MW2 and 0303T-MW3 to be non-compliant with low levels of cobalt within each well, and low levels of barium and vinyl chloride present at 0303T-MW-3. 1.4 Groundwater Flow Direction (Refer to Figure 3) As presented on Figure 3, groundwater flow appears consistent with historical data and remains toward the southeast under the site. 1.5 Predictive Rate of Contaminant Transport As shown on Figure 3, an overall groundwater flow toward the southeast was identified within the area of investigation. A hydraulic gradient (dh/dl) of 4.3% was calculated between 0303T-MW2 and 0303T-MW4. No slug testing or other hydrogeological testing has been conducted as of this date. In the event contaminant concentrations significantly increase or begin to 5 July 11, 2017 appear within down gradient wells, additional hydrogeological analyses could become necessary. 2.0 CONCLUSIONS AND RECOMMENDATIONS Review of historical results have shown fluctuating low level hydrocarbon concentrations of benzene and vinyl chloride meeting and exceeding the NCAC T:15A 02L Groundwater Standards at monitoring wells 0303T-MW1 and 0303T-MW3. Review of the current analytical results for Appendix I Volatiles indicate all of the monitoring wells and stream samples to be compliant for all hydrocarbon compounds with the exception of 0303T-MW3 which contained a non-compliant vinyl chloride estimated concentration at 0.91 ppb, slightly exceeding the NCAC 02L Groundwater Quality Standard at 0.03 ppb. Non-compliant barium and cobalt concentrations at 1.43 and 0.0274 ppm were also found at 0303T-MW3, both exceeding their respective standards at 0.7 and 0.001 ppm. Cobalt was found at 0303T-MW2 at an estimated 0.0044 ppb, slightly exceeding the Groundwater Protection Standard of 0.001 ppm. All other monitoring wells and stream samples were found to be compliant for all Appendix I Volatiles and Appendix I Metals. Historical methane monitoring at the site revealed the monitoring wells to contain low level methane readings ranging from 0 to 120 ppm. This event revealed no detectable methane concentrations at any of the monitoring well locations. LEL readings were consistent at 0%. The methane well, located in the central portion of the landfill, revealed methane concentrations ranging from 70 to 400 ppm and a LEL between 1% and 12%. In addition, methane monitoring was conducted within the enclosed structures identified as the scale house, the recycling center/storage area, and the tipping scale area. No measurable methane levels were detected at these sites. It is recommended that the groundwater monitoring program continue on a semi-annual schedule. Methane monitoring for all five monitoring wells, the on-site methane well, and enclosed structures will continue on a quarterly basis. Also, it is recommended that the on-site water supply well, Well #1, be sampled during the next groundwater monitoring event in December 2017. The well should be sampled for Appendix I volatiles to verify no impacts have occurred since last sampled in July 2008. 6 July 11, 2017 3.0 REFERENCES North Carolina Department of Environment and Natural Resources, NC Solid Waste Program. Requirements For Municipal Solid Waste Landfill Facilities (MSWLFs). North Carolina Department of Environmental and Natural Resources, March 2007. Ground Water Section Guidelines for the Investigation and Remediation of Soil and Ground Water. North Carolina Department of Environment and Natural Resources, Waste Management - Constituent List Last Updated 11/20/13. 7 TABLES TABLE 1 SEMI-ANNUAL MONITORING WELL, METHANE SCREENING, AND STREAM SAMPLING DATA SUMMARY ALLEGHANY COUNTY CLOSED MSWLF JUNE 21, 2017 SAMPLE WELL DEPTH IN FEET TOP OF CASING ELEVATION DEPTH TO WATER IN FEET GROUND WATER TABLE ELEVATION BAILS REQ’D QUANTITY PURGED IN GALLONS (Three Volumes) pH TEMP. IN FE SPEC. CONDUCT IN umhos METHANE GAS LEL/ PPM 0303T-MW1 36 3,023.25 10.34 3,012.91 52 12.32 6.3 62.4 118.3 0/0 0303T-MW2 29 3,023.77 4.02 3,019.75 50 12.00 7.3 62.6 94.3 0/0 0303T-MW3 51 3,086.00*33.11 3,052.89 36 8.59 5.4 67.1 85.8 0/0 0303T-MW4 42 3,063.06 20.67 3,042.39 43 10.24 6.0 62.8 135.6 0/0 0303T-MW5 19 3,012.92 9.11 3,003.81 20 4.75 6.5 64.6 16.0 0/0 METHANE WELL Approx 160 NA NA NA NA NA NA NA NA 1-12% 70-400 0303T-ST1 NA NA NA NA NA NA 7.6 61.7 50.7 NA 0303T-ST2 NA NA NA NA NA NA 7.5 61.5 27.2 NA NOTES: MW = Monitoring Well Sample ST = Stream Sample NA = Not Applicable Methane Monitoring Conducted With RKI Instruments Gas Tracer * = Assumed Benchmark Elevation At MW-3 Adjusted From GPS TABLE 2 QUARTERLY METHANE MONITORING DATA SUMMARY ALLEGHANY COUNTY CLOSED MSWLF SAMPLE LOCATION/ SAMPLED BY DATE WELL DEPTH IN FEET METHANE GAS LEL METHANE GAS PPM 0303T-MW1 3/30/2017 36 0 0 0303T-MW2 3/30/2017 29 0 0 0303T-MW3 3/30/2017 51 0 0 0303T-MW4 3/30/2017 42 0 0 0303T-MW5 3/30/2017 19 0 0 METHANE WELL 3/30/2017 Approx 160 10%-18%40-1,740 SCALE HOUSE 3/30/2017 NA 0 0 RECYCLING CENTER 3/30/2017 NA 0 0 TIPPING SCALE 3/30/2017 NA 0 0 0303T-MW1 6/21/2017 36 0 0 0303T-MW2 6/21/2017 29 0 0 0303T-MW3 6/21/2017 51 0 0 0303T-MW4 6/21/2017 42 0 0 0303T-MW5 6/21/2017 19 0 0 METHANE WELL 6/21/2017 Approx 160 1%-12%70-400 SCALE HOUSE 6/21/2017 NA 0 0 RECYCLING CENTER 6/21/2017 NA 0 0 TIPPING SCALE 6/21/2017 NA 0 0 LEL = Lower explosive limit PPM = Parts per million NA = Not applicable TABLE 3 (PAGE 1 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-MW1 DATE SAMPLED 6/12/14 12/18/1 4 6/18/15 12/16/1 5 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND 17.2 J BENZENE 1 NE ND ND ND ND ND 2-BUTANONE 4,000 NE ND ND ND ND ND CARBON DISULFIDE 700 NE ND ND 1.2 J ND ND CHLOROBENZENE 50 NE ND ND ND ND ND CHLOROETHANE 3,000 NE ND ND ND ND ND CHLOROMETHANE 3 NE ND ND ND 0.66 J 0.35 J 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND ND ND ND ND 1,1-DICHLOROETHANE 6 NE ND ND ND ND ND 1,1-DICHLOROETHENE 7 NE ND ND ND ND ND CIS-1,2-DICHLOROETHENE 70 NE ND ND ND ND ND 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND METHYLENE CHLORIDE 5 NE ND ND ND ND ND 4-METHYL-2-PENTANONE NE 560 4.7J ND ND ND ND TETRACHLOROETHENE 0.7 NE ND ND ND ND ND 1,1,1-TRICHLOROETHANE 200 NE ND ND ND ND ND TRICHLOROFLOUROMETHANE 2,000 NE ND ND ND ND ND TOLUENE 600 NE ND ND ND ND ND TRICHLOROETHENE 3 NE ND ND ND ND ND VINYL CHLORIDE 0.03 NE ND ND ND ND ND TOTAL XYLENE 500 NE ND ND ND ND ND ALL OTHER COMPOUNDS Varies ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = Not Established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration ND = None Detected TABLE 3 (PAGE 2 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-MW2 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/17/1 5 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND ND 16.3 J 13.3 J BENZENE 1 NE ND 0.74 J 0.50 J ND 0.88 J 0.74 J 0.88 J 2-BUTANONE 4,000 NE ND ND ND ND ND ND ND CARBON DISULFIDE 700 NE ND 4.2 ND 2.5 4.3 1.6 J ND CHLOROBENZENE 50 NE ND ND ND ND ND ND ND CHLOROETHANE 3,000 NE ND 1.9 1.6 ND 1.4 1.4 1.5 CHLOROFORM 70 NE ND ND ND ND ND ND ND CHLOROMETHANE 3 NE ND ND ND ND ND 12.6 ND 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND 0.42 J 0.45 J 0.51 J 0.57 J 0.71 J 0.68 J 1,1-DICHLOROETHANE 6 NE 5.6 6.9 6.4 5.5 5.4 5.2 5.3 1,1-DICHLOROETHENE 7 NE 1.0 0.67 J 0.58 J 0.56 J ND ND ND CIS-1,2-DICHLOROETHENE 70 NE 0.55J 1.2 1.1 1.3 2.2 2.6 3.0 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND ND ND METHYLENE CHLORIDE 5 NE 17.1 10.2 3.4 5.0 ND ND ND TETRACHLOROETHENE 0.7 NE 0.46J 0.51 J ND ND ND ND 0.61 J 1,1,1-TRICHLOROETHANE 200 NE ND 0.98 J ND ND 0.50 J ND ND TRICHLOROFLOUROMETHANE 2,000 NE 5.5 2.7 1.9 1.7 1.6 1.3 0.86 J TOLUENE 600 NE ND ND ND ND ND ND ND TRICHLOROETHENE 3 NE 0.97J 1.1 0.63 J 0.59 J 0.85 J 0.90 J ND VINYL CHLORIDE 0.03 NE ND ND ND ND ND ND ND TOTAL XYLENE 500 NE ND ND ND ND ND ND ND ALL OTHER COMPOUNDS Varies Varies ND ND ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = not established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration ND = None Detected TABLE 3 (PAGE 3 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-MW3 DATE SAMPLED 6/12/14 12/18/1 4 6/18/15 12/17/1 5 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND ND ND ND BENZENE 1 NE ND 0.84 J 0.58 J ND 0.63 J 0.61 J 0.78 J 2-BUTANONE 4,000 NE ND ND ND ND ND ND ND CARBON DISULFIDE 700 NE ND 3.0 ND 1.7 J 5.6 4.5 ND CHLOROBENZENE 50 NE ND ND ND ND ND ND ND CHLOROETHANE 3,000 NE ND 1.6 1.3 ND 1.0 1.1 1.1 CHLOROMETHANE 3 NE ND ND ND ND ND 8.9 ND 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND ND ND ND ND ND ND 1,1-DICHLOROETHANE 6 NE ND 0.42 J ND ND ND ND ND 1,1-DICHLOROETHENE 7 NE ND ND ND ND ND ND ND CIS-1,2-DICHLOROETHENE 70 NE 5.3 8.0 8.4 6.0 7.1 6.8 6.8 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND ND ND METHYLENE CHLORIDE 5 NE ND 1.1 ND 1.8 ND ND ND TETRACHLOROETHENE 0.7 NE ND ND ND ND ND ND ND 1,1,1-TRICHLOROETHANE 200 NE ND ND ND ND ND ND ND TRICHLOROFLOUROMETHANE 2,000 NE ND ND ND ND ND ND ND TOLUENE 600 NE ND ND ND ND ND ND ND TRICHLOROETHENE 3 NE ND 0.47 J ND ND ND ND ND VINYL CHLORIDE 0.03 NE ND 0.75 J 0.70 J ND 0.76 J 0.73 J 0.91 J TOTAL XYLENE 500 NE ND ND ND ND ND ND ND ALL OTHER COMPOUNDS Varies ND ND ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = Not Established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration U = Undetected ND = None Detected TABLE 3 (PAGE 4 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-MW4 DATE SAMPLED 6/12/14 12/18/1 4 6/18/15 12/17/15 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND 10.1 J BENZENE 1 NE ND ND ND ND ND 2-BUTANONE 4,000 NE ND ND ND ND ND CARBON DISULFIDE 700 NE ND ND ND ND ND CHLOROBENZENE 50 NE ND ND ND ND ND CHLOROETHANE 3,000 NE ND ND ND ND ND CHLOROFORM 70 NE ND ND ND ND ND CHLOROMETHANE 3 NE ND ND ND ND ND 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND ND ND ND ND 1,1-DICHLOROETHANE 6 NE ND ND ND ND ND 1,1-DICHLOROETHENE 7 NE ND ND ND ND ND CIS-1,2-DICHLOROETHENE 70 NE ND ND ND ND ND 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND 2-HEXANONE NE 40 ND 55.4 ND 0.93 J ND METHYLENE CHLORIDE 5 NE ND ND ND ND ND TETRACHLOROETHENE 0.7 NE ND ND ND ND ND 1,1,1-TRICHLOROETHANE 200 NE ND ND ND ND ND TRICHLOROFLOUROMETHANE 2,000 NE ND ND ND ND ND TOLUENE 600 NE ND ND ND ND ND TRICHLOROETHENE 3 NE ND ND ND ND ND VINYL CHLORIDE 0.03 NE ND ND ND ND ND TOTAL XYLENE 500 NE ND ND ND ND ND ALL OTHER COMPOUNDS Varies ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = Not Established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration U = Undetected ND = None Detected TABLE 3 (PAGE 5 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-MW5 DATE SAMPLED 6/12/14 6/18/15 12/18/1 4 12/16/1 5 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND 12.3 J 13.7 J BENZENE 1 NE ND ND ND ND ND ND 2-BUTANONE 4,000 NE ND ND ND ND ND ND CARBON DISULFIDE 700 NE ND 2.4 ND 1.8 J ND ND CHLOROBENZENE 50 NE ND ND ND ND ND ND CHLOROETHANE 3,000 NE ND ND ND ND ND ND CHLOROFORM 70 NE ND ND ND ND ND ND CHLOROMETHANE 3 NE ND ND ND ND 6.8 ND 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND ND ND ND ND ND 1,1-DICHLOROETHANE 6 NE ND ND ND ND ND ND 1,1-DICHLOROETHENE 7 NE ND ND ND ND ND ND CIS-1,2-DICHLOROETHENE 70 NE ND ND ND ND ND ND 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND ND 2-HEXANONE NE 40 ND ND 14.6 ND ND ND METHYLENE CHLORIDE 5 NE ND ND ND ND ND ND TETRACHLOROETHENE 0.7 NE ND ND ND ND ND ND 1,1,1-TRICHLOROETHANE 200 NE ND ND ND ND ND ND TRICHLOROFLOUROMETHANE 2,000 NE ND ND ND ND ND ND TOLUENE 600 NE ND ND ND ND ND ND TRICHLOROETHENE 3 NE ND ND ND ND ND ND VINYL CHLORIDE 0.03 NE ND ND ND ND ND ND TOTAL XYLENE 500 NE ND ND ND ND ND ND ALL OTHER COMPOUNDS Varies Varies ND ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = Not Established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration U = Undetected ND = None Detected TABLE 3 (PAGE 6 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-ST1 DATE SAMPLED 6/12/14 12/15/1 1 12/18/1 4 6/18/15 12/16/1 5 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND ND ND ND ND BENZENE 1 NE ND ND ND ND ND ND ND ND 2-BUTANONE 4,000 NE ND ND ND ND ND ND ND ND CARBON DISULFIDE 700 NE ND 1.83J 5.1 1.2 J ND 1.2 J ND ND CHLOROBENZENE 50 NE ND ND ND ND ND ND ND ND CHLOROETHANE 3,000 NE ND ND ND ND ND ND ND ND CHLOROFORM 70 NE ND ND ND ND ND ND ND ND CHLOROMETHANE 3 NE ND ND ND ND ND ND ND ND 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND ND ND ND ND ND ND ND 1,1-DICHLOROETHANE 6 NE ND ND ND ND ND ND ND ND 1,1-DICHLOROETHENE 7 NE ND ND ND ND ND ND ND ND CIS-1,2-DICHLOROETHENE 70 NE ND ND ND ND ND ND ND ND 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND ND ND ND METHYLENE CHLORIDE 5 NE ND ND ND ND 1.3 ND ND ND TETRACHLOROETHENE 0.7 NE ND ND ND ND ND ND ND ND 1,1,1-TRICHLOROETHANE 200 NE ND ND ND ND ND ND ND ND TRICHLOROFLOUROMETHAN E 2,000 NE ND ND ND ND ND ND ND ND TOLUENE 600 NE ND ND ND ND ND ND ND ND TRICHLOROETHENE 3 NE ND ND ND ND ND ND ND ND VINYL CHLORIDE 0.03 NE ND ND ND ND ND ND ND ND TOTAL XYLENE 500 NE ND ND ND ND ND ND ND ND ALL OTHER COMPOUNDS Varie Varie ND ND ND ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = Not Established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration ND = None Detected TABLE 3 (PAGE 7 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD. 0303T-ST2 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/16/15 6/2/16 12/1/16 6/21/17 APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND ND ND ND ND ND BENZENE 1 NE ND ND ND ND ND ND 2-BUTANONE 4,000 NE ND ND ND ND ND ND CARBON DISULFIDE 700 NE ND 1.2 J ND ND ND ND CHLOROBENZENE 50 NE ND ND ND ND ND ND CHLOROETHANE 3,000 NE ND ND ND ND ND ND CHLOROFORM 70 NE ND ND ND ND ND ND CHLOROMETHANE 3 NE ND ND ND ND ND ND 1,2-DICHLOROBENZENE 20 NE ND ND ND ND ND ND 1,4-DICHLOROBENZENE 6 NE ND ND ND ND ND ND 1,1-DICHLOROETHANE 6 NE ND ND ND ND ND ND 1,1-DICHLOROETHENE 7 NE ND ND ND ND ND ND CIS-1,2-DICHLOROETHENE 70 NE ND ND ND ND ND ND 1,2-DICHLOROPROPANE 0.6 NE ND ND ND ND ND ND ETHYLBENZENE 600 NE ND ND ND ND ND ND METHYLENE CHLORIDE 5 NE ND ND 1.8 ND ND ND TETRACHLOROETHENE 0.7 NE ND ND ND ND ND ND 1,1,1-TRICHLOROETHANE 200 NE ND ND ND ND ND ND TRICHLOROFLOUROMETHAN E 2,000 NE ND ND ND ND ND ND TOLUENE 600 NE ND ND ND ND ND ND TRICHLOROETHENE 3 NE ND ND ND ND ND ND VINYL CHLORIDE 0.03 NE ND ND ND ND ND ND TOTAL XYLENE 500 NE ND ND ND ND ND ND ALL OTHER COMPOUNDS Varie Varie ND ND ND ND ND ND Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection Standard. BQL = Below Quantitation Limits ug/L = parts per billion NE = Not Established GWP = Groundwater Protection Standard NA = Not Analyzed J = Estimated Concentration ND = None Detected TABLE 3 (PAGE 8 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-MW1 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/16/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE ND ND ND ND ND ND ND BARIUM 0.7 NE 0.0451 0.0254 0.0357 0.0273 0.0271 0.0271 0.0245 BERYLLIUM NE 0.004 ND ND ND ND 0.000081J ND ND CADMIUM 0.002 NE 0.00075J ND ND ND ND ND 0.0013 CHROMIUM 0.010 NE 0.0013J ND ND ND ND ND ND COBALT NE 0.001 0.0061 ND ND ND ND ND ND COPPER 1.0 NE 0.0036J 0.0032 J ND 0.0028 J 0.0047 J ND 0.0026J LEAD 0.015 NE ND ND ND ND 0.0032 J ND ND MERCURY 0.001 NE 0.000078J ND ND ND ND ND ND NICKEL 0.10 NE 0.0039J ND 00038 J ND 0.0035 J ND ND SELENIUM 0.020 NE ND ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 0.00028 ND ND ND ND ND ND ND VANADIUM NE 0.0003 0.0021J ND 0.0027 J ND 0.0039 J ND ND ZINC 1.0 NE 0.0076J 0.0048 J 0.0070 J 0.0053 J 0.0045 J 0.0052 J 0.222 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits, ppm = parts per million NE = Not Established, NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank, Amount in Prep Blank > MDL ND = None Detected TABLE 3 (PAGE 9 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-MW2 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/17/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE ND ND ND ND ND ND ND BARIUM 0.7 NE 0.0199 0.0203 0.0242 0.0238 0.0241 0.0262 0.0360 BERYLLIUM NE 0.004 ND 0.000057 J ND ND ND ND ND CADMIUM 0.002 NE ND ND ND ND ND ND ND CHROMIUM 0.010 NE 0.00072J ND ND ND ND ND 0.0028J COBALT NE 0.001 ND ND ND ND ND ND 0.0044J COPPER 1.0 NE ND ND ND ND ND ND ND LEAD 0.015 NE ND ND ND ND ND ND ND NICKEL 0.10 NE ND ND ND ND ND ND ND SELENIUM 0.020 NE ND ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 0.00028 ND ND ND ND ND ND ND VANADIUM NE 0.0003 ND ND ND ND ND ND ND ZINC 1.0 NE 0.0026J 0.0083 J 0.0080 J 0.0099 J 0.0033 J 0.0036 J 0.262 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits, ppm = parts per million NE = Not Established, NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank, Amount in Prep Blank > MDL ND = None Detected TABLE 3 (PAGE 10 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-MW3 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/17/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE 0.0044J ND ND ND ND 0.0057J ND BARIUM 0.7 NE 0.409 0.442 0.522 0.597 0.692 0.933 1.430 BERYLLIUM NE 0.004 0.00093J 0.0011 0.0012 0.0015 0.0016 0.0019 0.0012J CADMIUM 0.002 NE ND ND ND ND ND ND ND CHROMIUM 0.010 NE 0.0015J ND ND ND ND ND ND COBALT NE 0.001 0.0105 0.0089 0.0108 0.0122 0.0116 0.012 0.0274 COPPER 1.0 NE ND ND ND ND ND ND ND LEAD 0.015 NE ND ND ND ND 0.0028 J ND ND NICKEL 0.10 NE 0.0021J ND 0.0030 J ND 0.0038 J 0.004 J ND SELENIUM 0.020 NE ND ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 0.00028 ND ND ND ND ND ND ND VANADIUM NE 0.0003 0.0015J ND ND ND ND ND ND ZINC 1.0 NE 0.0156 0.0598 0.0200 0.0216 0.0288 0.0312 0.280 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits, ppm = parts per million NE = Not Established, NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank, Amount in Prep Blank > MDL ND = None Detected TABLE 3 (PAGE 11 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-MW4 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/17/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE ND ND ND ND ND ND ND BARIUM 0.7 NE 0.140 0.156 0.150 0.140 0.163 0.190 0.190 BERYLLIUM NE 0.004 ND 0.00014 J 0.00015J ND 0.00021J 0.00014J 0.0001J CADMIUM 0.002 NE ND ND ND ND ND ND ND CHROMIUM 0.010 NE 0.00080J ND ND ND ND ND 0.0032J COBALT NE 0.001 0.00077J ND ND ND ND ND ND COPPER 1.0 NE ND ND ND ND ND ND ND LEAD 0.015 NE ND ND ND ND ND ND ND NICKEL 0.10 NE ND ND ND ND ND ND ND SELENIUM 0.020 NE 0.0038J ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 0.00028 ND ND ND ND ND ND ND VANADIUM NE 0.0003 ND ND ND ND ND ND ND ZINC 1.0 NE 0.0013J 0.0062 J ND 0.0066 J ND ND 0.306 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits, ppm = parts per million NE = Not Established, NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank, Amount in Prep Blank > MDL ND = None Detected TABLE 3 (PAGE 12 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-MW5 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/16/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE 0.0031J ND ND ND ND ND ND BARIUM 0.7 NE 0.0182 0.0167 0.0162 0.0188 0.0188 0.0185 0.0162 BERYLLIUM NE 0.004 ND 0.000063 J 0.000080J ND ND 0.000086J 0.000058J CADMIUM 0.002 NE ND ND ND ND ND ND ND CHROMIUM 0.010 NE 0.00072J ND ND ND ND ND ND COBALT NE 0.001 0.00075J ND ND ND ND ND ND COPPER 1.0 NE ND ND ND ND ND ND ND LEAD 0.015 NE ND ND ND ND ND ND ND NICKEL 0.10 NE ND ND ND ND ND ND ND SELENIUM 0.020 NE ND ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 0.00028 ND ND ND ND ND ND ND VANADIUM NE 0.0003 ND ND ND ND ND ND ND ZINC 1.0 NE 0.0035J 0.0087 J 0.0085 J 0.0026 J ND ND 0.201 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits ppm = parts per million NE = Not Established NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank ND = None Detected TABLE 3 (PAGE 13 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-ST1 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/16/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE ND ND ND ND ND ND ND BARIUM 0.7 NE 0.0440 0.0349 0.0367 0.0412 0.0382 0.0393 0.0394 BERYLLIUM NE 0.002 ND ND ND ND 0.000055J 0.00018J ND CADMIUM 0.002 NE ND ND ND ND ND ND ND CHROMIUM 0.010 NE 0.0012J ND ND ND ND ND ND COBALT NE 0.002 ND ND ND ND ND ND ND COPPER 1.0 NE 0.00059J ND ND ND ND ND ND LEAD 0.015 NE ND ND ND ND ND ND ND NICKEL 0.10 NE ND ND ND ND ND ND ND SELENIUM 0.020 NE ND ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 2.0 ND ND ND ND ND ND ND VANADIUM NE 0.0003 0.00070J ND ND ND 0.0032 J ND ND ZINC 1.0 NE 0.0016J 0.0061 J 0.0031 J ND 0.0051 J ND 0.195 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits ppm = parts per million NE = Not Established NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank ND = None Detected TABLE 3 (PAGE 14 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD. GWP STD.0303T-ST2 DATE SAMPLED 6/12/14 12/18/14 6/18/15 12/16/15 6/2/16 12/1/16 6/21/17 APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE ND ND ND ND ND ND ND BARIUM 0.7 NE 0.0171 0.0122 0.0175 0.0168 0.0192 0.0167 0.0165 BERYLLIUM NE 0.002 0.00023J ND ND ND ND 0.00020J ND CADMIUM 0.002 NE ND ND ND ND ND ND ND CHROMIUM 0.010 NE 0.0012J ND ND ND ND ND ND COBALT NE 0.002 0.0012J ND ND ND ND ND ND COPPER 1.0 NE 0.0010J ND ND ND ND ND ND LEAD 0.015 NE ND ND ND ND ND ND ND NICKEL 0.10 NE ND ND ND ND ND ND ND SELENIUM 0.020 NE 0.0062J ND ND ND ND ND ND SILVER 0.020 NE ND ND ND ND ND ND ND THALLIUM NE 2.0 ND ND ND ND ND ND ND VANADIUM NE 0.0003 0.00089J ND ND ND ND ND ND ZINC 1.0 NE 0.0024J 0.0045 J 0.0035 J ND ND ND 0.192 Shaded areas represent non compliant concentrations. BQL = Below Quantitation Limits ppm = parts per million NE = Not Established NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit B = Compound Also Detected In Batch Blank ND = None Detected TABLE 3 (PAGE 15 OF 15) HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY ALLEGHANY COUNTY LANDFILL SPARTA, NORTH CAROLINA ANALYTE NCAC 02L STD.GWP STD.WATER SUPPLY WELL #5 DATE SAMPLED 12/14/12 APPENDIX I VOLATILES (CONCENTRATIONS IN ug/L) ACETONE 6,000 NE ND BENZENE 1 NE ND 2-BUTANONE 4,000 NE ND CARBON DISULFIDE 700 NE ND CHLOROBENZENE 50 NE ND CHLOROETHANE 3,000 NE ND CHLOROFORM 70 NE ND CHLOROMETHANE 3 NE ND 1,2-DICHLOROBENZENE 20 NE ND 1,4-DICHLOROBENZENE 6 NE ND 1,1-DICHLOROETHANE 6 NE ND 1,1-DICHLOROETHENE 7 NE ND CIS-1,2-DICHLOROETHENE 70 NE ND 1,2-DICHLOROPROPANE 0.6 NE ND ETHYLBENZENE 600 NE ND METHYLENE CHLORIDE 5 NE ND TETRACHLOROETHENE 0.7 NE ND 1,1,1-TRICHLOROETHANE 200 NE ND TRICHLOROFLOUROMETHANE 2,000 NE ND TOLUENE 600 NE ND TRICHLOROETHENE 3 NE ND VINYL CHLORIDE 0.03 NE ND TOTAL XYLENE 500 NE ND ALL OTHER COMPOUNDS Varies Varies ND APPENDIX I METALS (CONCENTRATIONS IN mg/L) ARSENIC 0.010 NE ND BARIUM 0.7 NE 0.0373J BERYLLIUM NE 0.002 ND CADMIUM 0.002 NE 0.00006J CHROMIUM 0.010 NE 0.00422J COBALT NE 0.002 ND COPPER 1.0 NE 0.0444 LEAD 0.015 NE 0.00914J NICKEL 0.10 NE 0.00414J SELENIUM 0.020 NE ND SILVER 0.020 NE 0.00368J THALLIUM NE 2.0 ND VANADIUM NE 0.0003 ND ZINC 1.0 NE 0.0227J Shaded areas represent non compliant concentrations. ND = None Detected NE = Not Established, NA = Not Analyzed J = Estimated Concentration, Below Calibration Range and Above Method Detection Limit Water Supply Well #5 not sampled during this monitoring event. FIGURES 1/6/17Approx: 1" = 200’ FIGURE: Adapted from the Alleghany County GIS On-Line Website Aerial Dated 2014. SITE MAP WITH MONITORING WELL AND STREAM SAMPLE LOCATIONS 19625 SCALE:JOB:DATE:DRAWN BY: TITLE: KLC/EFC LEGEND Monitoring Well Methane Well Stream Sampling locations Dan Osborne Rd 0303T-MW3 0303T-MW4 0303T-MW2 0303T-MW1 0303T-MW5 0303T-ST2 0303T-ST1 Former Landfill Former Landfill Vile Creek Scale House Recycle/Storage Center Methane Monitoring Well Tipping Scale Area Hampstead, NC 28443Hampstead, NC 28443 Applied Resource Management, P. C. Applied Resource Management, P. C. Adapted from Map provided by Alleghany County Manager’s Office,Tax Information re-verified 1/2017 SITE MAP WITH DOMESTIC WELL LOCATIONS LEGEND Surrounding Domestic Wells Former Landfill Alleghany County Poole Estate Poole Estate 1 2 3 4 5 391.15 ft 2 1/6/17Approx: 1" = 500’ FIGURE: 9625 SCALE:JOB:DATE:DRAWN BY: TITLE: KLC/EFCHampstead, NC 28443Hampstead, NC 28443 Applied Resource Management, P. C. Applied Resource Management, P. C. GROUNDWATER TABLE CONTOURS AS OF 6/21/17 3 (3,052.89) Monitoring Well Hydraulic Flow Direction Contour Interval = 10’ Groundwater Elevation In Feet AMSL, Adjusted From GPS 6/28/17Approx: 1" = 200’ FIGURE: Adapted from the Alleghany County GIS On-Line Website Aerial Dated 2014. 9625 SCALE:JOB:DATE:DRAWN BY: TITLE: JLZ Dan Osborne Rd Former Landfill Former Landfill Vile Creek Scale House Recycle/Storage Center Tipping Scale Area Hampstead, NC 28443Hampstead, NC 28443 Applied Resource Management, P. C. Applied Resource Management, P. C. (3,003.81) (3,05 0 .0 0 ) (3,04 0.00 ) (3,030.00) (3,020.00) (3,010.00) 0303T-MW5 0303T-MW1 0303T-MW2 0303T-MW4 0303T-MW3 (3,012.91) (3,019.75) (3,042.39) (3,052.89) LEGEND ATTACHMENT A #=CL# July 07, 2017 LIMS USE: FR - JOE ZUNCICH LIMS OBJECT ID: 92345424 92345424 Project: Pace Project No.: RE: Joe Zuncich ARM'S Waterworks PO Box 882 Hampstead, NC 28443 ALLEGHANY COUNTY LANDFILL 9625 Dear Joe Zuncich: Enclosed are the analytical results for sample(s) received by the laboratory on June 22, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com Project Manager (704)875-9092 Enclosures cc:Karen Corbett, ARM's Waterworks Ellen Cornette, ARM'S Waterworks James Cornette, ARM'S Waterworks REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 32 #=CP# CERTIFICATIONS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 32 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Lab ID Sample ID Matrix Date Collected Date Received 92345424001 0303T-MW1 Water 06/21/17 15:20 06/22/17 10:24 92345424002 0303T-MW2 Water 06/21/17 12:37 06/22/17 10:24 92345424003 0303T-MW3 Water 06/21/17 17:07 06/22/17 10:24 92345424004 0303T-MW4 Water 06/21/17 16:16 06/22/17 10:24 92345424005 0303T-MW5 Water 06/21/17 14:01 06/22/17 10:24 92345424006 0303T-ST1 Water 06/21/17 13:14 06/22/17 10:24 92345424007 0303T-ST2 Water 06/21/17 14:33 06/22/17 10:24 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 32 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92345424001 0303T-MW1 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO 92345424002 0303T-MW2 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO 92345424003 0303T-MW3 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO 92345424004 0303T-MW4 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO 92345424005 0303T-MW5 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO 92345424006 0303T-ST1 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO 92345424007 0303T-ST2 EPA 200.7 15 PASI-ASH1 EPA 245.1 1 PASI-AKAL EPA 8260 49 PASI-CZDO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW1 Lab ID:92345424001 Collected:06/21/17 15:20 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 00:58 7440-36-006/28/17 16:055.0 3.9 1 Arsenic ND ug/L 07/06/17 00:58 7440-38-206/28/17 16:0510.0 5.0 1 Barium 24.5 ug/L 07/06/17 00:58 7440-39-306/28/17 16:055.0 2.5 1 Beryllium ND ug/L 07/06/17 00:58 7440-41-706/28/17 16:051.0 0.050 1 Cadmium 1.3 ug/L 07/06/17 00:58 7440-43-906/28/17 16:051.0 0.50 1 Chromium ND ug/L 07/06/17 00:58 7440-47-306/28/17 16:055.0 2.5 1 Cobalt ND ug/L 07/06/17 00:58 7440-48-406/28/17 16:055.0 2.5 1 Copper 2.6J ug/L 07/06/17 00:58 7440-50-806/28/17 16:055.0 2.5 1 Lead ND ug/L 07/06/17 00:58 7439-92-106/28/17 16:055.0 2.5 1 Nickel ND ug/L 07/06/17 00:58 7440-02-006/28/17 16:055.0 2.5 1 Selenium ND ug/L 07/06/17 00:58 7782-49-206/28/17 16:0510.0 5.0 1 Silver ND ug/L 07/06/17 00:58 7440-22-406/28/17 16:055.0 2.5 1 Thallium ND ug/L 07/06/17 00:58 7440-28-006/28/17 16:0510.0 5.0 1 Vanadium ND ug/L 07/06/17 00:58 7440-62-206/28/17 16:055.0 2.5 1 Zinc 222 ug/L 07/06/17 00:58 7440-66-606/28/17 16:0510.0 2.5 1 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury 0.081J ug/L 07/05/17 03:16 7439-97-6 B07/03/17 04:000.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone 17.2J ug/L 06/25/17 05:26 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 05:26 107-13-110.0 1.9 1 Benzene ND ug/L 06/25/17 05:26 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 05:26 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 05:26 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 05:26 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 05:26 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 05:26 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 05:26 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 05:26 108-90-71.0 0.23 1 Chloroethane ND ug/L 06/25/17 05:26 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 05:26 67-66-31.0 0.14 1 Chloromethane 0.35J ug/L 06/25/17 05:26 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 05:26 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 05:26 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 05:26 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 05:26 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 05:26 95-50-11.0 0.30 1 1,4-Dichlorobenzene ND ug/L 06/25/17 05:26 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 05:26 110-57-61.0 1.0 1 1,1-Dichloroethane ND ug/L 06/25/17 05:26 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 05:26 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 05:26 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 06/25/17 05:26 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 05:26 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 05:26 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW1 Lab ID:92345424001 Collected:06/21/17 15:20 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 05:26 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 05:26 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 05:26 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 05:26 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 05:26 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 05:26 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 05:26 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 05:26 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 05:26 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 05:26 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 06/25/17 05:26 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 05:26 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 05:26 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 05:26 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 05:26 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 06/25/17 05:26 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 05:26 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 05:26 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 06/25/17 05:26 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 05:26 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)95 %06/25/17 05:26 460-00-470-130 1 1,2-Dichloroethane-d4 (S)100 %06/25/17 05:26 17060-07-070-130 1 Toluene-d8 (S)107 %06/25/17 05:26 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW2 Lab ID:92345424002 Collected:06/21/17 12:37 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 01:01 7440-36-006/28/17 16:055.0 3.9 1 Arsenic ND ug/L 07/06/17 01:01 7440-38-206/28/17 16:0510.0 5.0 1 Barium 36.0 ug/L 07/06/17 01:01 7440-39-306/28/17 16:055.0 2.5 1 Beryllium ND ug/L 07/06/17 01:01 7440-41-706/28/17 16:051.0 0.050 1 Cadmium ND ug/L 07/06/17 01:01 7440-43-906/28/17 16:051.0 0.50 1 Chromium 2.8J ug/L 07/06/17 01:01 7440-47-306/28/17 16:055.0 2.5 1 Cobalt 4.4J ug/L 07/06/17 01:01 7440-48-406/28/17 16:055.0 2.5 1 Copper ND ug/L 07/06/17 01:01 7440-50-806/28/17 16:055.0 2.5 1 Lead ND ug/L 07/06/17 01:01 7439-92-106/28/17 16:055.0 2.5 1 Nickel ND ug/L 07/06/17 01:01 7440-02-006/28/17 16:055.0 2.5 1 Selenium ND ug/L 07/06/17 01:01 7782-49-206/28/17 16:0510.0 5.0 1 Silver ND ug/L 07/06/17 01:01 7440-22-406/28/17 16:055.0 2.5 1 Thallium ND ug/L 07/06/17 01:01 7440-28-006/28/17 16:0510.0 5.0 1 Vanadium ND ug/L 07/06/17 01:01 7440-62-206/28/17 16:055.0 2.5 1 Zinc 262 ug/L 07/06/17 01:01 7440-66-606/28/17 16:0510.0 2.5 1 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury 0.073J ug/L 07/05/17 03:18 7439-97-6 B07/03/17 04:000.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone 13.3J ug/L 06/25/17 05:44 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 05:44 107-13-110.0 1.9 1 Benzene 0.88J ug/L 06/25/17 05:44 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 05:44 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 05:44 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 05:44 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 05:44 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 05:44 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 05:44 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 05:44 108-90-71.0 0.23 1 Chloroethane 1.5 ug/L 06/25/17 05:44 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 05:44 67-66-31.0 0.14 1 Chloromethane ND ug/L 06/25/17 05:44 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 05:44 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 05:44 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 05:44 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 05:44 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 05:44 95-50-11.0 0.30 1 1,4-Dichlorobenzene 0.68J ug/L 06/25/17 05:44 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 05:44 110-57-61.0 1.0 1 1,1-Dichloroethane 5.3 ug/L 06/25/17 05:44 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 05:44 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 05:44 75-35-41.0 0.56 1 cis-1,2-Dichloroethene 3.0 ug/L 06/25/17 05:44 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 05:44 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 05:44 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW2 Lab ID:92345424002 Collected:06/21/17 12:37 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 05:44 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 05:44 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 05:44 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 05:44 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 05:44 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 05:44 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 05:44 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 05:44 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 05:44 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 05:44 79-34-51.0 0.40 1 Tetrachloroethene 0.61J ug/L 06/25/17 05:44 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 05:44 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 05:44 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 05:44 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 05:44 79-01-61.0 0.47 1 Trichlorofluoromethane 0.86J ug/L 06/25/17 05:44 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 05:44 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 05:44 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 06/25/17 05:44 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 05:44 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)102 %06/25/17 05:44 460-00-470-130 1 1,2-Dichloroethane-d4 (S)97 %06/25/17 05:44 17060-07-070-130 1 Toluene-d8 (S)102 %06/25/17 05:44 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW3 Lab ID:92345424003 Collected:06/21/17 17:07 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 14:50 7440-36-006/28/17 16:0525.0 19.4 5 Arsenic ND ug/L 07/06/17 14:50 7440-38-206/28/17 16:0550.0 25.0 5 Barium 1430 ug/L 07/06/17 14:50 7440-39-306/28/17 16:0525.0 12.5 5 Beryllium 1.2J ug/L 07/06/17 14:50 7440-41-706/28/17 16:055.0 0.25 5 Cadmium ND ug/L 07/06/17 14:50 7440-43-906/28/17 16:055.0 2.5 5 Chromium ND ug/L 07/06/17 14:50 7440-47-306/28/17 16:0525.0 12.5 5 Cobalt 27.4 ug/L 07/06/17 14:50 7440-48-406/28/17 16:0525.0 12.5 5 Copper ND ug/L 07/06/17 14:50 7440-50-806/28/17 16:0525.0 12.5 5 Lead ND ug/L 07/06/17 14:50 7439-92-106/28/17 16:0525.0 12.5 5 Nickel ND ug/L 07/06/17 14:50 7440-02-006/28/17 16:0525.0 12.5 5 Selenium ND ug/L 07/06/17 14:50 7782-49-206/28/17 16:0550.0 25.0 5 Silver ND ug/L 07/06/17 14:50 7440-22-406/28/17 16:0525.0 12.5 5 Thallium ND ug/L 07/06/17 14:50 7440-28-006/28/17 16:0550.0 25.0 5 Vanadium ND ug/L 07/06/17 14:50 7440-62-206/28/17 16:0525.0 12.5 5 Zinc 280 ug/L 07/06/17 14:50 7440-66-606/28/17 16:0550.0 12.5 5 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury 0.16J ug/L 07/05/17 03:21 7439-97-6 B07/03/17 04:000.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone ND ug/L 06/25/17 06:02 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 06:02 107-13-110.0 1.9 1 Benzene 0.78J ug/L 06/25/17 06:02 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 06:02 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 06:02 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 06:02 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 06:02 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 06:02 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 06:02 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 06:02 108-90-71.0 0.23 1 Chloroethane 1.1 ug/L 06/25/17 06:02 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 06:02 67-66-31.0 0.14 1 Chloromethane ND ug/L 06/25/17 06:02 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 06:02 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 06:02 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 06:02 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 06:02 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 06:02 95-50-11.0 0.30 1 1,4-Dichlorobenzene ND ug/L 06/25/17 06:02 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 06:02 110-57-61.0 1.0 1 1,1-Dichloroethane ND ug/L 06/25/17 06:02 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 06:02 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 06:02 75-35-41.0 0.56 1 cis-1,2-Dichloroethene 6.8 ug/L 06/25/17 06:02 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 06:02 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 06:02 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW3 Lab ID:92345424003 Collected:06/21/17 17:07 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 06:02 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 06:02 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 06:02 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 06:02 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 06:02 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 06:02 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 06:02 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 06:02 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 06:02 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 06:02 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 06/25/17 06:02 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 06:02 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 06:02 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 06:02 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 06:02 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 06/25/17 06:02 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 06:02 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 06:02 108-05-42.0 0.35 1 Vinyl chloride 0.91J ug/L 06/25/17 06:02 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 06:02 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)103 %06/25/17 06:02 460-00-470-130 1 1,2-Dichloroethane-d4 (S)89 %06/25/17 06:02 17060-07-070-130 1 Toluene-d8 (S)105 %06/25/17 06:02 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW4 Lab ID:92345424004 Collected:06/21/17 16:16 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 01:07 7440-36-006/28/17 16:055.0 3.9 1 Arsenic ND ug/L 07/06/17 01:07 7440-38-206/28/17 16:0510.0 5.0 1 Barium 190 ug/L 07/06/17 01:07 7440-39-306/28/17 16:055.0 2.5 1 Beryllium 0.11J ug/L 07/06/17 01:07 7440-41-706/28/17 16:051.0 0.050 1 Cadmium ND ug/L 07/06/17 01:07 7440-43-906/28/17 16:051.0 0.50 1 Chromium 3.2J ug/L 07/06/17 01:07 7440-47-306/28/17 16:055.0 2.5 1 Cobalt ND ug/L 07/06/17 01:07 7440-48-406/28/17 16:055.0 2.5 1 Copper ND ug/L 07/06/17 01:07 7440-50-806/28/17 16:055.0 2.5 1 Lead ND ug/L 07/06/17 01:07 7439-92-106/28/17 16:055.0 2.5 1 Nickel ND ug/L 07/06/17 01:07 7440-02-006/28/17 16:055.0 2.5 1 Selenium ND ug/L 07/06/17 01:07 7782-49-206/28/17 16:0510.0 5.0 1 Silver ND ug/L 07/06/17 01:07 7440-22-406/28/17 16:055.0 2.5 1 Thallium ND ug/L 07/06/17 01:07 7440-28-006/28/17 16:0510.0 5.0 1 Vanadium ND ug/L 07/06/17 01:07 7440-62-206/28/17 16:055.0 2.5 1 Zinc 306 ug/L 07/06/17 01:07 7440-66-606/28/17 16:0510.0 2.5 1 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury 0.085J ug/L 07/05/17 03:23 7439-97-6 B07/03/17 04:000.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone 10.1J ug/L 06/25/17 06:20 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 06:20 107-13-110.0 1.9 1 Benzene ND ug/L 06/25/17 06:20 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 06:20 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 06:20 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 06:20 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 06:20 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 06:20 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 06:20 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 06:20 108-90-71.0 0.23 1 Chloroethane ND ug/L 06/25/17 06:20 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 06:20 67-66-31.0 0.14 1 Chloromethane ND ug/L 06/25/17 06:20 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 06:20 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 06:20 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 06:20 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 06:20 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 06:20 95-50-11.0 0.30 1 1,4-Dichlorobenzene ND ug/L 06/25/17 06:20 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 06:20 110-57-61.0 1.0 1 1,1-Dichloroethane ND ug/L 06/25/17 06:20 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 06:20 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 06:20 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 06/25/17 06:20 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 06:20 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 06:20 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW4 Lab ID:92345424004 Collected:06/21/17 16:16 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 06:20 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 06:20 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 06:20 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 06:20 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 06:20 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 06:20 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 06:20 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 06:20 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 06:20 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 06:20 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 06/25/17 06:20 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 06:20 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 06:20 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 06:20 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 06:20 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 06/25/17 06:20 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 06:20 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 06:20 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 06/25/17 06:20 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 06:20 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)101 %06/25/17 06:20 460-00-470-130 1 1,2-Dichloroethane-d4 (S)99 %06/25/17 06:20 17060-07-070-130 1 Toluene-d8 (S)106 %06/25/17 06:20 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW5 Lab ID:92345424005 Collected:06/21/17 14:01 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 01:16 7440-36-006/28/17 16:055.0 3.9 1 Arsenic ND ug/L 07/06/17 01:16 7440-38-206/28/17 16:0510.0 5.0 1 Barium 16.2 ug/L 07/06/17 01:16 7440-39-306/28/17 16:055.0 2.5 1 Beryllium 0.058J ug/L 07/06/17 01:16 7440-41-706/28/17 16:051.0 0.050 1 Cadmium ND ug/L 07/06/17 01:16 7440-43-906/28/17 16:051.0 0.50 1 Chromium ND ug/L 07/06/17 01:16 7440-47-306/28/17 16:055.0 2.5 1 Cobalt ND ug/L 07/06/17 01:16 7440-48-406/28/17 16:055.0 2.5 1 Copper ND ug/L 07/06/17 01:16 7440-50-806/28/17 16:055.0 2.5 1 Lead ND ug/L 07/06/17 01:16 7439-92-106/28/17 16:055.0 2.5 1 Nickel ND ug/L 07/06/17 01:16 7440-02-006/28/17 16:055.0 2.5 1 Selenium ND ug/L 07/06/17 01:16 7782-49-206/28/17 16:0510.0 5.0 1 Silver ND ug/L 07/06/17 01:16 7440-22-406/28/17 16:055.0 2.5 1 Thallium ND ug/L 07/06/17 01:16 7440-28-006/28/17 16:0510.0 5.0 1 Vanadium ND ug/L 07/06/17 01:16 7440-62-206/28/17 16:055.0 2.5 1 Zinc 201 ug/L 07/06/17 01:16 7440-66-606/28/17 16:0510.0 2.5 1 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury 0.076J ug/L 07/05/17 03:26 7439-97-6 B07/03/17 04:000.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone 13.7J ug/L 06/25/17 06:37 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 06:37 107-13-110.0 1.9 1 Benzene ND ug/L 06/25/17 06:37 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 06:37 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 06:37 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 06:37 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 06:37 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 06:37 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 06:37 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 06:37 108-90-71.0 0.23 1 Chloroethane ND ug/L 06/25/17 06:37 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 06:37 67-66-31.0 0.14 1 Chloromethane ND ug/L 06/25/17 06:37 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 06:37 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 06:37 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 06:37 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 06:37 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 06:37 95-50-11.0 0.30 1 1,4-Dichlorobenzene ND ug/L 06/25/17 06:37 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 06:37 110-57-61.0 1.0 1 1,1-Dichloroethane ND ug/L 06/25/17 06:37 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 06:37 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 06:37 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 06/25/17 06:37 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 06:37 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 06:37 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-MW5 Lab ID:92345424005 Collected:06/21/17 14:01 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 06:37 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 06:37 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 06:37 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 06:37 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 06:37 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 06:37 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 06:37 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 06:37 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 06:37 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 06:37 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 06/25/17 06:37 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 06:37 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 06:37 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 06:37 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 06:37 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 06/25/17 06:37 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 06:37 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 06:37 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 06/25/17 06:37 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 06:37 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)104 %06/25/17 06:37 460-00-470-130 1 1,2-Dichloroethane-d4 (S)101 %06/25/17 06:37 17060-07-070-130 1 Toluene-d8 (S)108 %06/25/17 06:37 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-ST1 Lab ID:92345424006 Collected:06/21/17 13:14 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 01:28 7440-36-006/28/17 16:055.0 3.9 1 Arsenic ND ug/L 07/06/17 01:28 7440-38-206/28/17 16:0510.0 5.0 1 Barium 39.4 ug/L 07/06/17 01:28 7440-39-306/28/17 16:055.0 2.5 1 Beryllium ND ug/L 07/06/17 01:28 7440-41-706/28/17 16:051.0 0.050 1 Cadmium ND ug/L 07/06/17 01:28 7440-43-906/28/17 16:051.0 0.50 1 Chromium ND ug/L 07/06/17 01:28 7440-47-306/28/17 16:055.0 2.5 1 Cobalt ND ug/L 07/06/17 01:28 7440-48-406/28/17 16:055.0 2.5 1 Copper ND ug/L 07/06/17 01:28 7440-50-806/28/17 16:055.0 2.5 1 Lead ND ug/L 07/06/17 01:28 7439-92-106/28/17 16:055.0 2.5 1 Nickel ND ug/L 07/06/17 01:28 7440-02-006/28/17 16:055.0 2.5 1 Selenium ND ug/L 07/06/17 01:28 7782-49-206/28/17 16:0510.0 5.0 1 Silver ND ug/L 07/06/17 01:28 7440-22-406/28/17 16:055.0 2.5 1 Thallium ND ug/L 07/06/17 01:28 7440-28-006/28/17 16:0510.0 5.0 1 Vanadium ND ug/L 07/06/17 01:28 7440-62-206/28/17 16:055.0 2.5 1 Zinc 195 ug/L 07/06/17 01:28 7440-66-606/28/17 16:0510.0 2.5 1 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury ND ug/L 07/07/17 05:45 7439-97-607/06/17 15:020.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone ND ug/L 06/25/17 06:55 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 06:55 107-13-110.0 1.9 1 Benzene ND ug/L 06/25/17 06:55 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 06:55 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 06:55 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 06:55 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 06:55 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 06:55 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 06:55 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 06:55 108-90-71.0 0.23 1 Chloroethane ND ug/L 06/25/17 06:55 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 06:55 67-66-31.0 0.14 1 Chloromethane ND ug/L 06/25/17 06:55 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 06:55 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 06:55 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 06:55 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 06:55 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 06:55 95-50-11.0 0.30 1 1,4-Dichlorobenzene ND ug/L 06/25/17 06:55 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 06:55 110-57-61.0 1.0 1 1,1-Dichloroethane ND ug/L 06/25/17 06:55 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 06:55 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 06:55 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 06/25/17 06:55 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 06:55 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 06:55 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-ST1 Lab ID:92345424006 Collected:06/21/17 13:14 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 06:55 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 06:55 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 06:55 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 06:55 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 06:55 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 06:55 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 06:55 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 06:55 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 06:55 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 06:55 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 06/25/17 06:55 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 06:55 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 06:55 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 06:55 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 06:55 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 06/25/17 06:55 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 06:55 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 06:55 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 06/25/17 06:55 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 06:55 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)98 %06/25/17 06:55 460-00-470-130 1 1,2-Dichloroethane-d4 (S)99 %06/25/17 06:55 17060-07-070-130 1 Toluene-d8 (S)113 %06/25/17 06:55 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-ST2 Lab ID:92345424007 Collected:06/21/17 14:33 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP Antimony ND ug/L 07/06/17 01:32 7440-36-006/28/17 16:055.0 3.9 1 Arsenic ND ug/L 07/06/17 01:32 7440-38-206/28/17 16:0510.0 5.0 1 Barium 16.5 ug/L 07/06/17 01:32 7440-39-306/28/17 16:055.0 2.5 1 Beryllium ND ug/L 07/06/17 01:32 7440-41-706/28/17 16:051.0 0.050 1 Cadmium ND ug/L 07/06/17 01:32 7440-43-906/28/17 16:051.0 0.50 1 Chromium ND ug/L 07/06/17 01:32 7440-47-306/28/17 16:055.0 2.5 1 Cobalt ND ug/L 07/06/17 01:32 7440-48-406/28/17 16:055.0 2.5 1 Copper ND ug/L 07/06/17 01:32 7440-50-806/28/17 16:055.0 2.5 1 Lead ND ug/L 07/06/17 01:32 7439-92-106/28/17 16:055.0 2.5 1 Nickel ND ug/L 07/06/17 01:32 7440-02-006/28/17 16:055.0 2.5 1 Selenium ND ug/L 07/06/17 01:32 7782-49-206/28/17 16:0510.0 5.0 1 Silver ND ug/L 07/06/17 01:32 7440-22-406/28/17 16:055.0 2.5 1 Thallium ND ug/L 07/06/17 01:32 7440-28-006/28/17 16:0510.0 5.0 1 Vanadium ND ug/L 07/06/17 01:32 7440-62-206/28/17 16:055.0 2.5 1 Zinc 192 ug/L 07/06/17 01:32 7440-66-606/28/17 16:0510.0 2.5 1 Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury Mercury 0.078J ug/L 07/05/17 03:28 7439-97-6 B07/03/17 04:000.20 0.070 1 Analytical Method: EPA 82608260 MSV Low Level Landfill Acetone ND ug/L 06/25/17 07:13 67-64-125.0 10.0 1 Acrylonitrile ND ug/L 06/25/17 07:13 107-13-110.0 1.9 1 Benzene ND ug/L 06/25/17 07:13 71-43-21.0 0.25 1 Bromochloromethane ND ug/L 06/25/17 07:13 74-97-51.0 0.17 1 Bromodichloromethane ND ug/L 06/25/17 07:13 75-27-41.0 0.18 1 Bromoform ND ug/L 06/25/17 07:13 75-25-21.0 0.26 1 Bromomethane ND ug/L 06/25/17 07:13 74-83-92.0 0.29 1 Carbon disulfide ND ug/L 06/25/17 07:13 75-15-02.0 1.2 1 Carbon tetrachloride ND ug/L 06/25/17 07:13 56-23-51.0 0.25 1 Chlorobenzene ND ug/L 06/25/17 07:13 108-90-71.0 0.23 1 Chloroethane ND ug/L 06/25/17 07:13 75-00-31.0 0.54 1 Chloroform ND ug/L 06/25/17 07:13 67-66-31.0 0.14 1 Chloromethane ND ug/L 06/25/17 07:13 74-87-31.0 0.11 1 1,2-Dibromo-3-chloropropane ND ug/L 06/25/17 07:13 96-12-82.0 2.0 1 Dibromochloromethane ND ug/L 06/25/17 07:13 124-48-11.0 0.21 1 1,2-Dibromoethane (EDB)ND ug/L 06/25/17 07:13 106-93-41.0 0.27 1 Dibromomethane ND ug/L 06/25/17 07:13 74-95-31.0 0.21 1 1,2-Dichlorobenzene ND ug/L 06/25/17 07:13 95-50-11.0 0.30 1 1,4-Dichlorobenzene ND ug/L 06/25/17 07:13 106-46-71.0 0.33 1 trans-1,4-Dichloro-2-butene ND ug/L 06/25/17 07:13 110-57-61.0 1.0 1 1,1-Dichloroethane ND ug/L 06/25/17 07:13 75-34-31.0 0.32 1 1,2-Dichloroethane ND ug/L 06/25/17 07:13 107-06-21.0 0.24 1 1,1-Dichloroethene ND ug/L 06/25/17 07:13 75-35-41.0 0.56 1 cis-1,2-Dichloroethene ND ug/L 06/25/17 07:13 156-59-21.0 0.19 1 trans-1,2-Dichloroethene ND ug/L 06/25/17 07:13 156-60-51.0 0.49 1 1,2-Dichloropropane ND ug/L 06/25/17 07:13 78-87-51.0 0.27 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 32 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Sample:0303T-ST2 Lab ID:92345424007 Collected:06/21/17 14:33 Received:06/22/17 10:24 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 82608260 MSV Low Level Landfill cis-1,3-Dichloropropene ND ug/L 06/25/17 07:13 10061-01-51.0 0.13 1 trans-1,3-Dichloropropene ND ug/L 06/25/17 07:13 10061-02-61.0 0.26 1 Ethylbenzene ND ug/L 06/25/17 07:13 100-41-41.0 0.30 1 2-Hexanone ND ug/L 06/25/17 07:13 591-78-65.0 0.46 1 Iodomethane ND ug/L 06/25/17 07:13 74-88-45.0 0.32 1 Methylene Chloride ND ug/L 06/25/17 07:13 75-09-21.0 0.97 1 4-Methyl-2-pentanone (MIBK)ND ug/L 06/25/17 07:13 108-10-15.0 0.33 1 Styrene ND ug/L 06/25/17 07:13 100-42-51.0 0.26 1 1,1,1,2-Tetrachloroethane ND ug/L 06/25/17 07:13 630-20-61.0 0.33 1 1,1,2,2-Tetrachloroethane ND ug/L 06/25/17 07:13 79-34-51.0 0.40 1 Tetrachloroethene ND ug/L 06/25/17 07:13 127-18-41.0 0.46 1 Toluene ND ug/L 06/25/17 07:13 108-88-31.0 0.26 1 1,1,1-Trichloroethane ND ug/L 06/25/17 07:13 71-55-61.0 0.48 1 1,1,2-Trichloroethane ND ug/L 06/25/17 07:13 79-00-51.0 0.29 1 Trichloroethene ND ug/L 06/25/17 07:13 79-01-61.0 0.47 1 Trichlorofluoromethane ND ug/L 06/25/17 07:13 75-69-41.0 0.20 1 1,2,3-Trichloropropane ND ug/L 06/25/17 07:13 96-18-41.0 0.41 1 Vinyl acetate ND ug/L 06/25/17 07:13 108-05-42.0 0.35 1 Vinyl chloride ND ug/L 06/25/17 07:13 75-01-41.0 0.62 1 Xylene (Total)ND ug/L 06/25/17 07:13 1330-20-71.0 0.66 1 Surrogates 4-Bromofluorobenzene (S)99 %06/25/17 07:13 460-00-470-130 1 1,2-Dichloroethane-d4 (S)94 %06/25/17 07:13 17060-07-070-130 1 Toluene-d8 (S)104 %06/25/17 07:13 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 367467 EPA 245.1 EPA 245.1 245.1 Mercury Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2037018 Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424007 Matrix:Water AnalyzedMDL Mercury ug/L 0.077J 0.20 07/05/17 02:570.070 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2037019LABORATORY CONTROL SAMPLE: LCSSpike Mercury ug/L 2.42.5 96 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 2037020MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92345260001 2037021 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury ug/L 2.5 98 70-130101 3 202.5ND 2.5 2.6 Parameter Units MS Result % Rec Limits Qual% RecConc. 2037022MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92345800001 2037023 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury ug/L 2.5 97 70-13091 6 202.5ND 2.5 2.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 367889 EPA 245.1 EPA 245.1 245.1 Mercury Associated Lab Samples:92345424006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2038731 Associated Lab Samples:92345424006 Matrix:Water AnalyzedMDL Mercury ug/L ND 0.20 07/07/17 05:410.070 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2038732LABORATORY CONTROL SAMPLE: LCSSpike Mercury ug/L 2.62.5 104 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 2038733MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92345424006 2038734 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury ug/L 2.5 101 70-130102 1 202.5ND 2.5 2.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 366767 EPA 200.7 EPA 200.7 200.7 MET Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424006, 92345424007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2033097 Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424006, 92345424007 Matrix:Water AnalyzedMDL Antimony ug/L ND 5.0 07/06/17 00:143.9 Arsenic ug/L ND 10.0 07/06/17 00:145.0 Barium ug/L ND 5.0 07/06/17 00:142.5 Beryllium ug/L ND 1.0 07/06/17 00:140.050 Cadmium ug/L ND 1.0 07/06/17 00:140.50 Chromium ug/L ND 5.0 07/06/17 00:142.5 Cobalt ug/L ND 5.0 07/06/17 00:142.5 Copper ug/L ND 5.0 07/06/17 00:142.5 Lead ug/L ND 5.0 07/06/17 00:142.5 Nickel ug/L ND 5.0 07/06/17 00:142.5 Selenium ug/L ND 10.0 07/06/17 00:145.0 Silver ug/L ND 5.0 07/06/17 00:142.5 Thallium ug/L ND 10.0 07/06/17 00:145.0 Vanadium ug/L ND 5.0 07/06/17 00:142.5 Zinc ug/L ND 10.0 07/06/17 14:442.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2033098LABORATORY CONTROL SAMPLE: LCSSpike Antimony ug/L 532500 106 85-115 Arsenic ug/L 515500 103 85-115 Barium ug/L 534500 107 85-115 Beryllium ug/L 529500 106 85-115 Cadmium ug/L 523500 105 85-115 Chromium ug/L 532500 106 85-115 Cobalt ug/L 530500 106 85-115 Copper ug/L 542500 108 85-115 Lead ug/L 522500 104 85-115 Nickel ug/L 514500 103 85-115 Selenium ug/L 534500 107 85-115 Silver ug/L 273250 109 85-115 Thallium ug/L 477500 95 85-115 Vanadium ug/L 527500 105 85-115 Zinc ug/L 504500 101 85-115 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 2033099MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92345266001 2033100 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Antimony ug/L 500 97 70-130100 3 2050011.6 497 511 Arsenic ug/L 500 99 70-130101 3 20500ND495508 Barium ug/L 500 99 70-130102 3 2050090.8 586 601 Beryllium ug/L 500 98 70-130101 2 20500ND492504 Cadmium ug/L 500 98 70-130100 3 20500ND488500 Chromium ug/L 500 99 70-130102 3 20500ND498512 Cobalt ug/L 500 96 70-13098 3 20500ND481494 Copper ug/L 500 100 70-130102 2 20500ND503514 Lead ug/L 500 92 70-13094 3 205008.4 467 479 Nickel ug/L 500 93 70-13095 2 2050020.8 484 496 Selenium ug/L 500 97 70-13099 2 20500ND488498 Silver ug/L 250 102 70-130104 2 20250ND255261 Thallium ug/L 500 78 70-13079 2 20500ND388395 Vanadium ug/L 500 100 70-130102 2 20500ND502513 Zinc ug/L 500 112 70-130127 9 20500280838914 Parameter Units MS Result % Rec Limits Qual% RecConc. 2033101MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92345424004 2033102 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Antimony ug/L 500 101 70-130101 0 20500ND504504 Arsenic ug/L 500 97 70-13098 1 20500ND488493 Barium ug/L 500 103 70-130102 1 20500190707700 Beryllium ug/L 500 102 70-130102 0 205000.11J 509 509 Cadmium ug/L 500 99 70-130100 0 20500ND496498 Chromium ug/L 500 102 70-130102 1 205003.2J 515 511 Cobalt ug/L 500 101 70-130101 0 20500ND503504 Copper ug/L 500 107 70-130102 5 20500ND536512 Lead ug/L 500 99 70-13099 1 20500ND493497 Nickel ug/L 500 98 70-13098 0 20500ND489490 Selenium ug/L 500 101 70-130102 1 20500ND506509 Silver ug/L 250 104 70-130104 0 20250ND260260 Thallium ug/L 500 90 70-13090 1 20500ND448451 Vanadium ug/L 500 102 70-130101 0 20500ND509507 Zinc ug/L 500 92 70-13071 14 20500306764661 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 366363 EPA 8260 EPA 8260 8260 MSV Low Level Landfill Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424006, 92345424007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2031047 Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424006, 92345424007 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/25/17 01:180.33 1,1,1-Trichloroethane ug/L ND 1.0 06/25/17 01:180.48 1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/25/17 01:180.40 1,1,2-Trichloroethane ug/L ND 1.0 06/25/17 01:180.29 1,1-Dichloroethane ug/L ND 1.0 06/25/17 01:180.32 1,1-Dichloroethene ug/L ND 1.0 06/25/17 01:180.56 1,2,3-Trichloropropane ug/L ND 1.0 06/25/17 01:180.41 1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/25/17 01:182.0 1,2-Dibromoethane (EDB)ug/L ND 1.0 06/25/17 01:180.27 1,2-Dichlorobenzene ug/L ND 1.0 06/25/17 01:180.30 1,2-Dichloroethane ug/L ND 1.0 06/25/17 01:180.24 1,2-Dichloropropane ug/L ND 1.0 06/25/17 01:180.27 1,4-Dichlorobenzene ug/L ND 1.0 06/25/17 01:180.33 2-Hexanone ug/L ND 5.0 06/25/17 01:180.46 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/25/17 01:180.33 Acetone ug/L ND 25.0 06/25/17 01:1810.0 Acrylonitrile ug/L ND 10.0 06/25/17 01:181.9 Benzene ug/L ND 1.0 06/25/17 01:180.25 Bromochloromethane ug/L ND 1.0 06/25/17 01:180.17 Bromodichloromethane ug/L ND 1.0 06/25/17 01:180.18 Bromoform ug/L ND 1.0 06/25/17 01:180.26 Bromomethane ug/L ND 2.0 06/25/17 01:180.29 Carbon disulfide ug/L ND 2.0 06/25/17 01:181.2 Carbon tetrachloride ug/L ND 1.0 06/25/17 01:180.25 Chlorobenzene ug/L ND 1.0 06/25/17 01:180.23 Chloroethane ug/L ND 1.0 06/25/17 01:180.54 Chloroform ug/L ND 1.0 06/25/17 01:180.14 Chloromethane ug/L ND 1.0 06/25/17 01:180.11 cis-1,2-Dichloroethene ug/L ND 1.0 06/25/17 01:180.19 cis-1,3-Dichloropropene ug/L ND 1.0 06/25/17 01:180.13 Dibromochloromethane ug/L ND 1.0 06/25/17 01:180.21 Dibromomethane ug/L ND 1.0 06/25/17 01:180.21 Ethylbenzene ug/L ND 1.0 06/25/17 01:180.30 Iodomethane ug/L ND 5.0 06/25/17 01:180.32 Methylene Chloride ug/L ND 1.0 06/25/17 01:180.97 Styrene ug/L ND 1.0 06/25/17 01:180.26 Tetrachloroethene ug/L ND 1.0 06/25/17 01:180.46 Toluene ug/L ND 1.0 06/25/17 01:180.26 trans-1,2-Dichloroethene ug/L ND 1.0 06/25/17 01:180.49 trans-1,3-Dichloropropene ug/L ND 1.0 06/25/17 01:180.26 trans-1,4-Dichloro-2-butene ug/L ND 1.0 06/25/17 01:181.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:2031047 Associated Lab Samples:92345424001, 92345424002, 92345424003, 92345424004, 92345424005, 92345424006, 92345424007 Matrix:Water AnalyzedMDL Trichloroethene ug/L ND 1.0 06/25/17 01:180.47 Trichlorofluoromethane ug/L ND 1.0 06/25/17 01:180.20 Vinyl acetate ug/L ND 2.0 06/25/17 01:180.35 Vinyl chloride ug/L ND 1.0 06/25/17 01:180.62 Xylene (Total)ug/L ND 1.0 06/25/17 01:180.66 1,2-Dichloroethane-d4 (S)%100 70-130 06/25/17 01:18 4-Bromofluorobenzene (S)%96 70-130 06/25/17 01:18 Toluene-d8 (S)%104 70-130 06/25/17 01:18 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2031048LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 51.950 104 80-125 1,1,1-Trichloroethane ug/L 50.550 101 71-129 1,1,2,2-Tetrachloroethane ug/L 50.350 101 79-124 1,1,2-Trichloroethane ug/L 48.250 96 85-125 1,1-Dichloroethane ug/L 45.750 91 73-126 1,1-Dichloroethene ug/L 46.750 93 66-135 1,2,3-Trichloropropane ug/L 44.950 90 75-130 1,2-Dibromo-3-chloropropane ug/L 47.150 94 71-133 1,2-Dibromoethane (EDB)ug/L 52.050 104 83-124 1,2-Dichlorobenzene ug/L 47.650 95 80-133 1,2-Dichloroethane ug/L 49.250 98 67-128 1,2-Dichloropropane ug/L 46.450 93 75-132 1,4-Dichlorobenzene ug/L 45.050 90 78-130 2-Hexanone ug/L 96.6100 97 68-143 4-Methyl-2-pentanone (MIBK)ug/L 95.0100 95 72-135 Acetone ug/L 101100 101 48-146 Acrylonitrile ug/L 232250 93 40-160 Benzene ug/L 47.850 96 80-125 Bromochloromethane ug/L 46.850 94 71-125 Bromodichloromethane ug/L 47.750 95 78-124 Bromoform ug/L 40.750 81 71-128 Bromomethane ug/L 55.450 111 40-160 Carbon disulfide ug/L 44.250 88 50-160 Carbon tetrachloride ug/L 47.750 95 69-131 Chlorobenzene ug/L 49.350 99 81-122 Chloroethane ug/L 37.250 74 39-148 Chloroform ug/L 48.650 97 73-127 Chloromethane ug/L 44.350 89 44-146 cis-1,2-Dichloroethene ug/L 44.550 89 74-124 cis-1,3-Dichloropropene ug/L 48.050 96 72-132 Dibromochloromethane ug/L 46.750 93 78-125 Dibromomethane ug/L 44.450 89 82-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 2031048LABORATORY CONTROL SAMPLE: LCSSpike Ethylbenzene ug/L 48.350 97 79-121 Iodomethane ug/L 107100 107 39-154 Methylene Chloride ug/L 47.650 95 64-133 Styrene ug/L 47.450 95 84-126 Tetrachloroethene ug/L 46.850 94 78-122 Toluene ug/L 44.350 89 80-121 trans-1,2-Dichloroethene ug/L 44.750 89 71-127 trans-1,3-Dichloropropene ug/L 46.050 92 69-141 trans-1,4-Dichloro-2-butene ug/L 55.550 111 40-160 Trichloroethene ug/L 48.050 96 78-122 Trichlorofluoromethane ug/L 47.850 96 53-137 Vinyl acetate ug/L 91.2100 91 40-160 Vinyl chloride ug/L 38.250 76 58-137 Xylene (Total)ug/L 141150 94 81-126 1,2-Dichloroethane-d4 (S)%103 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%90 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 2031944MATRIX SPIKE SAMPLE: MSSpike Result 92345285001 1,1,1,2-Tetrachloroethane ug/L 21.520 107 70-130ND 1,1,1-Trichloroethane ug/L 22.520 113 70-130ND 1,1,2,2-Tetrachloroethane ug/L 21.320 106 70-130ND 1,1,2-Trichloroethane ug/L 22.220 111 70-130ND 1,1-Dichloroethane ug/L 21.720 109 70-130ND 1,1-Dichloroethene ug/L 22.720 113 70-166ND 1,2,3-Trichloropropane ug/L 22.620 113 70-130ND 1,2-Dibromo-3-chloropropane ug/L 23.020 115 70-130ND 1,2-Dibromoethane (EDB)ug/L 21.420 107 70-130ND 1,2-Dichlorobenzene ug/L 20.720 103 70-130ND 1,2-Dichloroethane ug/L 21.620 108 70-130ND 1,2-Dichloropropane ug/L 22.920 115 70-130ND 1,4-Dichlorobenzene ug/L 20.220 101 70-130ND 2-Hexanone ug/L 51.840 129 70-130ND 4-Methyl-2-pentanone (MIBK)ug/L 48.940 122 70-130ND Acetone ug/L 64.8 M14016270-130ND Acrylonitrile ug/L 127100 127 70-130ND Benzene ug/L 22.220 111 70-148ND Bromochloromethane ug/L 22.320 112 70-130ND Bromodichloromethane ug/L 22.720 114 70-130ND Bromoform ug/L 18.520 93 70-130ND Bromomethane ug/L 13.3 M1206670-130ND Carbon disulfide ug/L 20.120 100 70-130ND Carbon tetrachloride ug/L 22.620 113 70-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 2031944MATRIX SPIKE SAMPLE: MSSpike Result 92345285001 Chlorobenzene ug/L 20.620 103 70-146ND Chloroethane ug/L 17.920 89 70-130ND Chloroform ug/L 22.420 112 70-130ND Chloromethane ug/L 15.120 73 70-1300.40J cis-1,2-Dichloroethene ug/L 23.720 116 70-1300.58J cis-1,3-Dichloropropene ug/L 22.520 113 70-130ND Dibromochloromethane ug/L 22.120 110 70-130ND Dibromomethane ug/L 22.320 111 70-130ND Ethylbenzene ug/L 20.920 104 70-130ND Iodomethane ug/L 30.640 77 70-130ND Methylene Chloride ug/L 23.720 118 70-130ND Styrene ug/L 20.620 103 70-130ND Tetrachloroethene ug/L 18.220 91 70-130ND Toluene ug/L 22.220 111 70-155ND trans-1,2-Dichloroethene ug/L 22.520 113 70-130ND trans-1,3-Dichloropropene ug/L 22.920 114 70-130ND trans-1,4-Dichloro-2-butene ug/L 24.220 121 70-130ND Trichloroethene ug/L 22.120 110 69-151ND Trichlorofluoromethane ug/L 20.520 102 70-130ND Vinyl acetate ug/L 43.040 107 70-130ND Vinyl chloride ug/L 16.720 84 70-130ND 1,2-Dichloroethane-d4 (S)%110 70-130 4-Bromofluorobenzene (S)%105 70-130 Toluene-d8 (S)%104 70-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92345285002 2031945SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/L ND 30ND 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,2,3-Trichloropropane ug/L ND 30ND 1,2-Dibromo-3-chloropropane ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND 2-Hexanone ug/L ND 30ND 4-Methyl-2-pentanone (MIBK)ug/L ND 30ND Acetone ug/L 27.5 3010.3J Acrylonitrile ug/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 32 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92345285002 2031945SAMPLE DUPLICATE: Benzene ug/L ND 30ND Bromochloromethane ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND 30ND Carbon disulfide ug/L ND 30ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L ND 30ND Chloromethane ug/L 0.51J 30ND cis-1,2-Dichloroethene ug/L ND 30ND cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dibromomethane ug/L ND 30ND Ethylbenzene ug/L ND 30ND Iodomethane ug/L ND 30ND Methylene Chloride ug/L ND 30ND Styrene ug/L ND 30ND Tetrachloroethene ug/L ND 30ND Toluene ug/L ND 30ND trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND trans-1,4-Dichloro-2-butene ug/L ND 30ND Trichloroethene ug/L ND 30ND Trichlorofluoromethane ug/L ND 30ND Vinyl acetate ug/L ND 30ND Vinyl chloride ug/L ND 30ND Xylene (Total)ug/L ND 30ND 1,2-Dichloroethane-d4 (S)%110 1199 4-Bromofluorobenzene (S)%100 3102 Toluene-d8 (S)%105 2103 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 32 #=QL# QUALIFIERS Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Analyte was detected in the associated method blank.B Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 32 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92345424 ALLEGHANY COUNTY LANDFILL 9625 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92345424001 366767 3674550303T-MW1 EPA 200.7 EPA 200.7 92345424002 366767 3674550303T-MW2 EPA 200.7 EPA 200.7 92345424003 366767 3674550303T-MW3 EPA 200.7 EPA 200.7 92345424004 366767 3674550303T-MW4 EPA 200.7 EPA 200.7 92345424005 366767 3674550303T-MW5 EPA 200.7 EPA 200.7 92345424006 366767 3674550303T-ST1 EPA 200.7 EPA 200.7 92345424007 366767 3674550303T-ST2 EPA 200.7 EPA 200.7 92345424001 367467 3676770303T-MW1 EPA 245.1 EPA 245.1 92345424002 367467 3676770303T-MW2 EPA 245.1 EPA 245.1 92345424003 367467 3676770303T-MW3 EPA 245.1 EPA 245.1 92345424004 367467 3676770303T-MW4 EPA 245.1 EPA 245.1 92345424005 367467 3676770303T-MW5 EPA 245.1 EPA 245.1 92345424006 367889 3680260303T-ST1 EPA 245.1 EPA 245.1 92345424007 367467 3676770303T-ST2 EPA 245.1 EPA 245.1 92345424001 3663630303T-MW1 EPA 8260 92345424002 3663630303T-MW2 EPA 8260 92345424003 3663630303T-MW3 EPA 8260 92345424004 3663630303T-MW4 EPA 8260 92345424005 3663630303T-MW5 EPA 8260 92345424006 3663630303T-ST1 EPA 8260 92345424007 3663630303T-ST2 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/07/2017 07:50 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 32 Page 30 of 32 Page 31 of 32 Page 32 of 32 ATTACHMENT B FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-MW1 7440-36-0 13 Antimony 3.9 ug/L U EPA 200.7 3.9 5 6 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-38-2 14 Arsenic 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-39-3 15 Barium 24.5 ug/L EPA 200.7 2.5 5 100 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-41-7 23 Beryllium 0.05 ug/L U EPA 200.7 0.05 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-43-9 34 Cadmium 1.3 ug/L EPA 200.7 0.5 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-47-3 51 Chromium 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-48-4 53 Cobalt 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-50-8 54 Copper 2.6 ug/L J EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7439-92-1 131 Lead 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-02-0 152 Nickel 2.5 ug/L U EPA 200.7 2.5 5 50 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7782-49-2 183 Selenium 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-22-4 184 Silver 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-28-0 194 Thallium 5 ug/L U EPA 200.7 5 10 5.5 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-62-2 209 Vanadium 2.5 ug/L U EPA 200.7 2.5 5 25 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7440-66-6 213 Zinc 222 ug/L EPA 200.7 2.5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-36-0 13 Antimony 3.9 ug/L U EPA 200.7 3.9 5 6 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-38-2 14 Arsenic 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-39-3 15 Barium 36 ug/L EPA 200.7 2.5 5 100 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-41-7 23 Beryllium 0.05 ug/L U EPA 200.7 0.05 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-43-9 34 Cadmium 0.5 ug/L U EPA 200.7 0.5 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-47-3 51 Chromium 2.8 ug/L J EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-48-4 53 Cobalt 4.4 ug/L J EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-50-8 54 Copper 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7439-92-1 131 Lead 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-02-0 152 Nickel 2.5 ug/L U EPA 200.7 2.5 5 50 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7782-49-2 183 Selenium 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-22-4 184 Silver 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-28-0 194 Thallium 5 ug/L U EPA 200.7 5 10 5.5 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-62-2 209 Vanadium 2.5 ug/L U EPA 200.7 2.5 5 25 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW2 7440-66-6 213 Zinc 262 ug/L EPA 200.7 2.5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-36-0 13 Antimony 19.4 ug/L U EPA 200.7 19.4 25 6 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-38-2 14 Arsenic 25 ug/L U EPA 200.7 25 50 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-39-3 15 Barium 1430 ug/L EPA 200.7 12.5 25 100 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-41-7 23 Beryllium 1.2 ug/L J EPA 200.7 0.25 5 1 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-43-9 34 Cadmium 2.5 ug/L U EPA 200.7 2.5 5 1 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-47-3 51 Chromium 12.5 ug/L U EPA 200.7 12.5 25 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-48-4 53 Cobalt 27.4 ug/L EPA 200.7 12.5 25 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-50-8 54 Copper 12.5 ug/L U EPA 200.7 12.5 25 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7439-92-1 131 Lead 12.5 ug/L U EPA 200.7 12.5 25 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-02-0 152 Nickel 12.5 ug/L U EPA 200.7 12.5 25 50 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7782-49-2 183 Selenium 25 ug/L U EPA 200.7 25 50 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-22-4 184 Silver 12.5 ug/L U EPA 200.7 12.5 25 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-28-0 194 Thallium 25 ug/L U EPA 200.7 25 50 5.5 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-62-2 209 Vanadium 12.5 ug/L U EPA 200.7 12.5 25 25 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW3 7440-66-6 213 Zinc 280 ug/L EPA 200.7 12.5 50 10 5 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-36-0 13 Antimony 3.9 ug/L U EPA 200.7 3.9 5 6 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-38-2 14 Arsenic 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-39-3 15 Barium 190 ug/L EPA 200.7 2.5 5 100 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-41-7 23 Beryllium 0.11 ug/L J EPA 200.7 0.05 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-43-9 34 Cadmium 0.5 ug/L U EPA 200.7 0.5 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-MW4 7440-47-3 51 Chromium 3.2 ug/L J EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-48-4 53 Cobalt 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-50-8 54 Copper 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7439-92-1 131 Lead 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-02-0 152 Nickel 2.5 ug/L U EPA 200.7 2.5 5 50 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7782-49-2 183 Selenium 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-22-4 184 Silver 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-28-0 194 Thallium 5 ug/L U EPA 200.7 5 10 5.5 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-62-2 209 Vanadium 2.5 ug/L U EPA 200.7 2.5 5 25 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW4 7440-66-6 213 Zinc 306 ug/L EPA 200.7 2.5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-36-0 13 Antimony 3.9 ug/L U EPA 200.7 3.9 5 6 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-38-2 14 Arsenic 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-39-3 15 Barium 16.2 ug/L EPA 200.7 2.5 5 100 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-41-7 23 Beryllium 0.058 ug/L J EPA 200.7 0.05 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-43-9 34 Cadmium 0.5 ug/L U EPA 200.7 0.5 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-47-3 51 Chromium 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-48-4 53 Cobalt 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-50-8 54 Copper 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7439-92-1 131 Lead 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-02-0 152 Nickel 2.5 ug/L U EPA 200.7 2.5 5 50 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7782-49-2 183 Selenium 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-22-4 184 Silver 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-28-0 194 Thallium 5 ug/L U EPA 200.7 5 10 5.5 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-62-2 209 Vanadium 2.5 ug/L U EPA 200.7 2.5 5 25 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW5 7440-66-6 213 Zinc 201 ug/L EPA 200.7 2.5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-36-0 13 Antimony 3.9 ug/L U EPA 200.7 3.9 5 6 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-38-2 14 Arsenic 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-39-3 15 Barium 39.4 ug/L EPA 200.7 2.5 5 100 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-41-7 23 Beryllium 0.05 ug/L U EPA 200.7 0.05 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-43-9 34 Cadmium 0.5 ug/L U EPA 200.7 0.5 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-47-3 51 Chromium 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-48-4 53 Cobalt 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-50-8 54 Copper 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7439-92-1 131 Lead 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-02-0 152 Nickel 2.5 ug/L U EPA 200.7 2.5 5 50 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7782-49-2 183 Selenium 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-22-4 184 Silver 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-28-0 194 Thallium 5 ug/L U EPA 200.7 5 10 5.5 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-62-2 209 Vanadium 2.5 ug/L U EPA 200.7 2.5 5 25 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST1 7440-66-6 213 Zinc 195 ug/L EPA 200.7 2.5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-36-0 13 Antimony 3.9 ug/L U EPA 200.7 3.9 5 6 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-38-2 14 Arsenic 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-39-3 15 Barium 16.5 ug/L EPA 200.7 2.5 5 100 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-41-7 23 Beryllium 0.05 ug/L U EPA 200.7 0.05 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-43-9 34 Cadmium 0.5 ug/L U EPA 200.7 0.5 1 1 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-47-3 51 Chromium 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-48-4 53 Cobalt 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-50-8 54 Copper 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7439-92-1 131 Lead 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-02-0 152 Nickel 2.5 ug/L U EPA 200.7 2.5 5 50 1 6/21/2017 6/28/2017 7/6/2017 40 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-ST2 7782-49-2 183 Selenium 5 ug/L U EPA 200.7 5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-22-4 184 Silver 2.5 ug/L U EPA 200.7 2.5 5 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-28-0 194 Thallium 5 ug/L U EPA 200.7 5 10 5.5 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-62-2 209 Vanadium 2.5 ug/L U EPA 200.7 2.5 5 25 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-ST2 7440-66-6 213 Zinc 192 ug/L EPA 200.7 2.5 10 10 1 6/21/2017 6/28/2017 7/6/2017 40 0303T-MW1 7439-97-6 132 Mercury 0.081 ug/L J,B EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/3/2017 7/5/2017 40 0303T-MW2 7439-97-6 132 Mercury 0.073 ug/L J,B EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/3/2017 7/5/2017 40 0303T-MW3 7439-97-6 132 Mercury 0.16 ug/L J,B EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/3/2017 7/5/2017 40 0303T-MW4 7439-97-6 132 Mercury 0.085 ug/L J,B EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/3/2017 7/5/2017 40 0303T-MW5 7439-97-6 132 Mercury 0.076 ug/L J,B EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/3/2017 7/5/2017 40 0303T-ST1 7439-97-6 132 Mercury 0.07 ug/L U EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/6/2017 7/7/2017 40 0303T-ST2 7439-97-6 132 Mercury 0.078 ug/L J,B EPA 245.1 0.07 0.2 0.2 1 6/21/2017 7/3/2017 7/5/2017 40 0303T-MW1 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-MW1 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 75-34-3 75 1,1-Dichloroethane 0.32 ug/L U EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 0303T-MW1 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-MW1 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-MW1 67-64-1 3 Acetone 17.2 ug/L J EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-MW1 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-MW1 71-43-2 16 Benzene 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-MW1 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-MW1 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-MW1 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-MW1 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-MW1 75-00-3 41 Chloroethane 0.54 ug/L U EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-MW1 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 74-87-3 137 Chloromethane 0.35 ug/L J EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-MW1 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-MW1 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-MW1 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 127-18-4 192 Tetrachloroethene 0.46 ug/L U EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 75-69-4 203 Trichlorofluoromethane 0.2 ug/L U EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-MW1 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-MW1 75-01-4 211 Vinyl chloride 0.62 ug/L U EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 156-59-2 78 cis-1,2-Dichloroethene 0.19 ug/L U EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-MW1 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW1 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12 0303T-MW2 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-MW2 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 75-34-3 75 1,1-Dichloroethane 5.3 ug/L EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 0303T-MW2 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 106-46-7 71 1,4-Dichlorobenzene 0.68 ug/L J EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-MW2 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-MW2 67-64-1 3 Acetone 13.3 ug/L J EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-MW2 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-MW2 71-43-2 16 Benzene 0.88 ug/L J EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-MW2 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-MW2 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-MW2 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-MW2 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-MW2 75-00-3 41 Chloroethane 1.5 ug/L EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-MW2 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 74-87-3 137 Chloromethane 0.11 ug/L U EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-MW2 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-MW2 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-MW2 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 127-18-4 192 Tetrachloroethene 0.61 ug/L J EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 75-69-4 203 Trichlorofluoromethane 0.86 ug/L J EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-MW2 75-01-4 211 Vinyl chloride 0.62 ug/L U EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 156-59-2 78 cis-1,2-Dichloroethene 3 ug/L EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-MW2 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-MW2 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW2 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12 0303T-MW3 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-MW3 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 75-34-3 75 1,1-Dichloroethane 0.32 ug/L U EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 0303T-MW3 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-MW3 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-MW3 67-64-1 3 Acetone 10 ug/L U EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-MW3 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-MW3 71-43-2 16 Benzene 0.78 ug/L J EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-MW3 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-MW3 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-MW3 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-MW3 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-MW3 75-00-3 41 Chloroethane 1.1 ug/L EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-MW3 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 74-87-3 137 Chloromethane 0.11 ug/L U EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-MW3 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-MW3 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-MW3 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 127-18-4 192 Tetrachloroethene 0.46 ug/L U EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 75-69-4 203 Trichlorofluoromethane 0.2 ug/L U EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-MW3 75-01-4 211 Vinyl chloride 0.91 ug/L J EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 156-59-2 78 cis-1,2-Dichloroethene 6.8 ug/L EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-MW3 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW3 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-MW4 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-MW4 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 75-34-3 75 1,1-Dichloroethane 0.32 ug/L U EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 0303T-MW4 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-MW4 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-MW4 67-64-1 3 Acetone 10.1 ug/L J EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-MW4 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-MW4 71-43-2 16 Benzene 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-MW4 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-MW4 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-MW4 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-MW4 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-MW4 75-00-3 41 Chloroethane 0.54 ug/L U EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-MW4 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 74-87-3 137 Chloromethane 0.11 ug/L U EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-MW4 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-MW4 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-MW4 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 127-18-4 192 Tetrachloroethene 0.46 ug/L U EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 75-69-4 203 Trichlorofluoromethane 0.2 ug/L U EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-MW4 75-01-4 211 Vinyl chloride 0.62 ug/L U EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 156-59-2 78 cis-1,2-Dichloroethene 0.19 ug/L U EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-MW4 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW4 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12 0303T-MW5 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-MW5 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-MW5 75-34-3 75 1,1-Dichloroethane 0.32 ug/L U EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 0303T-MW5 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-MW5 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-MW5 67-64-1 3 Acetone 13.7 ug/L J EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-MW5 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-MW5 71-43-2 16 Benzene 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-MW5 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-MW5 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-MW5 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-MW5 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-MW5 75-00-3 41 Chloroethane 0.54 ug/L U EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-MW5 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 74-87-3 137 Chloromethane 0.11 ug/L U EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-MW5 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-MW5 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-MW5 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 127-18-4 192 Tetrachloroethene 0.46 ug/L U EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 75-69-4 203 Trichlorofluoromethane 0.2 ug/L U EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-MW5 75-01-4 211 Vinyl chloride 0.62 ug/L U EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 156-59-2 78 cis-1,2-Dichloroethene 0.19 ug/L U EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-MW5 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-MW5 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12 0303T-ST1 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-ST1 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 75-34-3 75 1,1-Dichloroethane 0.32 ug/L U EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-ST1 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-ST1 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-ST1 67-64-1 3 Acetone 10 ug/L U EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-ST1 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-ST1 71-43-2 16 Benzene 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-ST1 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-ST1 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-ST1 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-ST1 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-ST1 75-00-3 41 Chloroethane 0.54 ug/L U EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-ST1 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 74-87-3 137 Chloromethane 0.11 ug/L U EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-ST1 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-ST1 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-ST1 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 127-18-4 192 Tetrachloroethene 0.46 ug/L U EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 75-69-4 203 Trichlorofluoromethane 0.2 ug/L U EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-ST1 75-01-4 211 Vinyl chloride 0.62 ug/L U EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 156-59-2 78 cis-1,2-Dichloroethene 0.19 ug/L U EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-ST1 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-ST1 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12 0303T-ST2 630-20-6 190 1,1,1,2-Tetrachloroethane 0.33 ug/L U EPA 8260 0.33 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 71-55-6 200 1,1,1-Trichloroethane 0.48 ug/L U EPA 8260 0.48 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 79-34-5 191 1,1,2,2-Tetrachloroethane 0.4 ug/L U EPA 8260 0.4 1 3 1 6/21/2017 6/25/2017 12 0303T-ST2 79-00-5 202 1,1,2-Trichloroethane 0.29 ug/L U EPA 8260 0.29 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 75-34-3 75 1,1-Dichloroethane 0.32 ug/L U EPA 8260 0.32 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 75-35-4 77 1,1-Dichloroethene 0.56 ug/L U EPA 8260 0.56 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 96-18-4 206 1,2,3-Trichloropropane 0.41 ug/L U EPA 8260 0.41 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 96-12-8 67 1,2-Dibromo-3-chloropropane 2 ug/L U EPA 8260 2 2 13 1 6/21/2017 6/25/2017 12 0303T-ST2 106-93-4 68 1,2-Dibromoethane (EDB)0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 95-50-1 69 1,2-Dichlorobenzene 0.3 ug/L U EPA 8260 0.3 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 107-06-2 76 1,2-Dichloroethane 0.24 ug/L U EPA 8260 0.24 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 78-87-5 82 1,2-Dichloropropane 0.27 ug/L U EPA 8260 0.27 1 1 1 6/21/2017 6/25/2017 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MDL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY 0303T-ST2 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260 0.33 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 591-78-6 124 2-Hexanone 0.46 ug/L U EPA 8260 0.46 5 50 1 6/21/2017 6/25/2017 12 0303T-ST2 108-10-1 147 4-Methyl-2-pentanone (MIBK)0.33 ug/L U EPA 8260 0.33 5 100 1 6/21/2017 6/25/2017 12 0303T-ST2 67-64-1 3 Acetone 10 ug/L U EPA 8260 10 25 100 1 6/21/2017 6/25/2017 12 0303T-ST2 107-13-1 8 Acrylonitrile 1.9 ug/L U EPA 8260 1.9 10 200 1 6/21/2017 6/25/2017 12 0303T-ST2 71-43-2 16 Benzene 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 74-97-5 28 Bromochloromethane 0.17 ug/L U EPA 8260 0.17 1 3 1 6/21/2017 6/25/2017 12 0303T-ST2 75-27-4 29 Bromodichloromethane 0.18 ug/L U EPA 8260 0.18 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 75-25-2 30 Bromoform 0.26 ug/L U EPA 8260 0.26 1 3 1 6/21/2017 6/25/2017 12 0303T-ST2 74-83-9 136 Bromomethane 0.29 ug/L U EPA 8260 0.29 2 10 1 6/21/2017 6/25/2017 12 0303T-ST2 75-15-0 35 Carbon disulfide 1.2 ug/L U EPA 8260 1.2 2 100 1 6/21/2017 6/25/2017 12 0303T-ST2 56-23-5 36 Carbon tetrachloride 0.25 ug/L U EPA 8260 0.25 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 108-90-7 39 Chlorobenzene 0.23 ug/L U EPA 8260 0.23 1 3 1 6/21/2017 6/25/2017 12 0303T-ST2 75-00-3 41 Chloroethane 0.54 ug/L U EPA 8260 0.54 1 10 1 6/21/2017 6/25/2017 12 0303T-ST2 67-66-3 44 Chloroform 0.14 ug/L U EPA 8260 0.14 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 74-87-3 137 Chloromethane 0.11 ug/L U EPA 8260 0.11 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 124-48-1 66 Dibromochloromethane 0.21 ug/L U EPA 8260 0.21 1 3 1 6/21/2017 6/25/2017 12 0303T-ST2 74-95-3 139 Dibromomethane 0.21 ug/L U EPA 8260 0.21 1 10 1 6/21/2017 6/25/2017 12 0303T-ST2 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260 0.3 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 74-88-4 142 Iodomethane 0.32 ug/L U EPA 8260 0.32 5 10 1 6/21/2017 6/25/2017 12 0303T-ST2 75-09-2 140 Methylene Chloride 0.97 ug/L U EPA 8260 0.97 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 100-42-5 186 Styrene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 127-18-4 192 Tetrachloroethene 0.46 ug/L U EPA 8260 0.46 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 108-88-3 196 Toluene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 79-01-6 201 Trichloroethene 0.47 ug/L U EPA 8260 0.47 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 75-69-4 203 Trichlorofluoromethane 0.2 ug/L U EPA 8260 0.2 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 108-05-4 210 Vinyl acetate 0.35 ug/L U EPA 8260 0.35 2 50 1 6/21/2017 6/25/2017 12 0303T-ST2 75-01-4 211 Vinyl chloride 0.62 ug/L U EPA 8260 0.62 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 1330-20-7 346 Xylene (Total)0.66 ug/L U EPA 8260 0.66 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 156-59-2 78 cis-1,2-Dichloroethene 0.19 ug/L U EPA 8260 0.19 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 10061-01-5 86 cis-1,3-Dichloropropene 0.13 ug/L U EPA 8260 0.13 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 156-60-5 79 trans-1,2-Dichloroethene 0.49 ug/L U EPA 8260 0.49 1 5 1 6/21/2017 6/25/2017 12 0303T-ST2 10061-02-6 87 trans-1,3-Dichloropropene 0.26 ug/L U EPA 8260 0.26 1 1 1 6/21/2017 6/25/2017 12 0303T-ST2 110-57-6 73 trans-1,4-Dichloro-2-butene 1 ug/L U EPA 8260 1 1 100 1 6/21/2017 6/25/2017 12