1803_BlackburnCDLF_GWMR_DIN28244_20150324

1st Semi-Annual
2015Groundwater
MonitoringReport
forthe
BlackburnLandfill
(Subtitle-D/C&D/ClosedPortion)
Permit 18-03
GroundwaterMonitoringProgram
March 2015
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TABLEOFCONTENTS
EXECUTIVESUMMARY……………………………………..……..…………..1
1.0INTRODUCTION……………………………………………………………......6
2.0SITEDESCRIPTION….………………………………………………………......7
2.1PhysicalSetting…………………………………………………………………7
2.2GeologyandHydrogeology……………………….………………….….…….7
2.3MonitoringNetwork………………………….………………..………….8
3.0HYDROLOGICEVALUATION………………………………………………….8
3.1StaticWaterLevelsandGroundwater Elevations ...……………………….8
3.2GroundwaterFlowRateandDirection ..…………………………………....8
4.0SAMPLINGANDLABORATORYANALYSIS……………….……………….10
4.1FieldSamplingSummary…………..………………………………………….10
4.2LaboratoryAnalysisSummary .……………………………………………....11
4.3QualityAssurance/QualityControl…....………………………………….12
4.4AnalyticalResults ..…………………………………………………………….12
5.0FINDINGSANDCONCLUSIONS ..…………….……………….……………….15
5.1SummaryofFindings ..….…………..………………………………………….15
5.2Conclusions…….……………….……………………………………………....15
FIGURES
GroundwaterPotentiometricContours–UppermostAquifer
GroundwaterPotentiometricContours–DeeperAquifer
APPENDICES
AppendixAStaticWaterLevelSummary
AppendixBSubtitleD–Unit2andUnit3
1.1stSemi-Annual2015SummaryofDetections
2.SummaryofDissolvedMetalsandTSSDetections
3.HistoricalSummaryofDetections
4.LeachateAnalysisSummary
5.SummaryofDataPre-DatingUnit3Construction/WastePlacement
6.AnalyticalReportandChain-of-CustodyRecord
7.FieldSamplingSummaryandFieldSampleLogs
8.HistoricalResults
AppendixCClosedPortion–Unit1
1.1stSemi-Annual2015SummaryofDetections
2.SummaryofDissolvedMetalsandTSSDetections
3.HistoricalSummaryofDetections
4.AnalyticalReportandChain-of-CustodyRecord
5.FieldSamplingSummaryandFieldSampleLogs
6.HistoricalResults
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TABLEOFCONTENTS(cont’d)
AppendixDC&D–Unit1andUnit2
1.1stSemi-Annual2015SummaryofDetections
2.SummaryofDissolvedMetalsandTSSDetections
3.HistoricalSummaryofDetections
4.AnalyticalReportandChain-of-CustodyRecord
5.FieldSamplingSummaryandFieldSampleLogs
6.HistoricalResults
AppendixE AlternateSourceDemonstration
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EXECUTIVESUMMARY
REIConsultants,Inc.(REIC)haspreparedthisreportforthe 1st semi-annual2015water
qualitymonitoringeventfortheBlackburnResourceRecoveryFacility,operatedbyCatawba
County,NorthCarolina.ThemonitoringeventwasperformedinaccordancewithNorth
Carolinaregulationsin15ANCAC13B,directivesandapprovalsfromtheNorthCarolina
DepartmentofEnvironmentandNaturalResources(NCDENR),andthefacilityWaterQuality
MonitoringPlan.
BlackburnResourceRecoveryFacilityconsistsoffourmainareas,aSubtitleDLandfill(Units
2and3),aClosedPortion(Unit1),andaConstructionandDemolitionLandfill(C&DUnit2
Landfill),allofwhichoperateunderPermit#18-03,andaformerC&DLandfill(C&DUnit
1Landfill).
Waterqualitymonitoringisconductedonasemi-annualbasisatthefacility.Fieldsampling
forthe 1st semi-annualeventwasconductedbyREIConMarch24-25,2015.Samplesfrom
theSubtitleDandC&Dareas,currentlyindetectionmonitoring,andsamplesfromthe
ClosedPortion,currentlyinassessmentmonitoring,wereanalyzedforconstituentsappropriate
totherespectiveprograms.GroundwatersamplesassociatedwiththeC&Dlandfillswere
analyzedfortetrahydrofuraninadditiontotheroutinemonitoringparameterlistpertheJune
25,2010memofromNCDENR.
ResultsfromallwellswerecompareddirectlytoNorthCarolinagroundwaterstandards.The
regulationsat15ANCAC13Bnolongerrequirestatisticalanalysistobeperformedduring
detectionandassessmentmonitoring.However,duetometalsdetectionsthatexceeded
groundwaterstandards,statisticalanalysiswasutilizedtodemonstratethatmetals
concentrationswerelessthanbackgroundlevels.Theresultsofthe 1st semi-annual2015
monitoringeventforeachareaofthefacilityarediscussedbelow.
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SubtitleDUnit2
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeSubtitle
DUnit2areaduringtheeventwiththeexceptionofunderdrainsU-1,U-2,andU-3,allof
whichweredry.Allwellpurgingand samplingwasperformedwithnounusualcharacteristics
observedwiththeexceptionof significantsuspendedsolidsinseveralgroundwatersamples.
LaboratoryanalysesforNorthCarolinaAppendixIparametersyieldednodetectionsabovethe
NCDENRSolidWasteSectionLimits(SWSLs)forallvolatileorganiccompounds(VOCs).
NometalsconstituentsweredetectedaboveNorthCarolinagroundwaterstandardswiththe
exceptionofcobaltinwellsMW-12andMW-16,andvanadiuminwellMW-16.Astatistical
evaluationwasperformedutilizingpredictionintervals,whichwereconstructedfrom
backgroundhistoricaldataandcomparedtoindividualwellconstituentresultsfromthe 1st
semi-annual2015monitoringevent.Thisevaluationindicatesthatthemetalsobservedin
compliancewellsarenotstatisticallyelevatedoverbackgroundlevels(see“AlternateSource
Demonstration”intheappendix).
Basedontheresultsofthecurrentgroundwatermonitoringevent,andpursuanttoNorth
CarolinaSub-Chapter13B,Rule .1633,itisrecommendedthattheBlackburnSubtitleDUnit2
Landfillremaininadetectionmonitoringprogramforthe 2nd semi-annualmonitoringeventof
2015.
SubtitleDUnit 3
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeSubtitle
DUnit3areaduringtheevent.Allwellpurgingandsamplingwasperformedwithnounusual
characteristicsobservedwiththeexceptionofsignificantsuspendedsolidsinseveral
groundwatersamples.
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LaboratoryanalysesforNorthCarolinaAppendixIconstituentsyieldednodetectionsabove
NCDENRSWSLsforVOCsinanyofthewells.MetalsparametersthatexceededNorth
CarolinagroundwaterstandardsintheUnit3monitoringwellsincludedbariuminwellMW-
33;chromiuminwellsMW-31,MW-32,MW-33,andMW-34;cobaltandvanadiuminwells
MW-31,MW-32,andMW-33;andleadinwellMW-33.Astatisticalevaluationwas
performedutilizingpredictionintervals,whichwereconstructedfrombackgroundhistorical
dataandcomparedtoindividualwellconstituentresultsfromthe 1st semi-annualmonitoring
eventof2015.Thisevaluationindicatesthatthemetalsobservedincompliancewellsarenot
statisticallyelevatedoverbackgroundlevels(see“AlternateSourceDemonstration”inthe
appendix).
Basedontheresultsofthecurrentgroundwatermonitoringevent,andpursuanttoNorth
CarolinaSub-Chapter13B,Rule .1633,itisrecommendedthattheBlackburnSubtitleDUnit3
landfillremaininadetectionmonitoringprogramforthe 2nd semi-annualmonitoringeventof
2015.
ClosedUnit1
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeClosed
Unit1areaduringtheevent.Allwellpurgingandsamplingwasperformedwithnounusual
characteristicsobservedwiththeexceptionofsignificantsuspendedsolidsinseveral
groundwatersamples.
SampleswereanalyzedforNorthCarolinaAppendixIIconstituents.Parametersobservedat
concentrationsaboveNorthCarolinagroundwaterstandardsincompliancewellsareas
follows:
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Parameter MonitoringWell
Benzene MW-5A, MW-6,MW-7, MW-11
Chromium MW-5,MW-7
Cobalt MW-6,MW-7,MW-11
1,4-Dichlorobenzene MW-6,MW-7
1,1-Dichloroethane MW-5A, MW-6
Tetrachloroethene MW-5A
Trichloroethene MW-5A
Vanadium MW-5,MW-7,MW-11
Vinylchloride MW-7,MW-11
AllotherparameterswereeithernotdetectedorwerebelowNorthCarolinagroundwater
standards.NoparametersweredetectedaboveSWSLsbeyondtheAppendixIlist.
The 1st semi-annualassessmentmonitoringeventof2015includedanalysisofNorthCarolina
AppendixIconstituents.PerthefacilityWaterQualityMonitoringPlan,theClosedPortion
facilitywillcontinueassessmentmonitoringduringthe 2nd semi-annualsamplingeventof
2015,withanalysisofAppendixIparameters.
C&DUnits1and2
SampleswerecollectedfromallwaterqualitymonitoringlocationsassociatedwiththeC&D
Unit1andUnit2areasduringtheevent.Allwellpurgingandsamplingwasperformedwith
nounusualcharacteristicsobservedwiththeexceptionofsignificantsuspendedsolidsin
severalgroundwatersamples.
AreviewofthegroundwaterdatafortheC&DLandfillsyieldeddetectionsaboveNorth
CarolinagroundwaterstandardsofbariuminwellMW-27andchromiuminwellsMW-21,
MW-24,MW-26,MW-29andMW-30(notethatwellMW-21isanupgradientbackground
well).Astatisticalevaluationwasperformedutilizingpredictionintervals,whichwere
constructedfrombackgroundhistoricaldataandcomparedtoindividualwellconstituent
resultsfromthe 1st semi-annualmonitoringeventof2015.Thisevaluationindicatesthatthe
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metalsobservedincompliancewellsarenotstatisticallyelevatedoverbackgroundlevels(see
“AlternateSourceDemonstration”intheappendix).Tetrahydrofuranwasnotdetectedabove
thelaboratorypracticalquantitationlimit(PQL)inanyoftheC&Dwellsamples.
Basedontheresultsofthecurrentgroundwatermonitoringevent,andperthefacility’sWater
QualityMonitoringPlan,itisrecommendedthattheBlackburnC&DUnit1andUnit 2
landfillsremaininadetectionmonitoringprogramforthe 2nd semi-annualmonitoringeventof
2015.
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1.0INTRODUCTION
REIConsultants,Inc.(REIC)haspreparedthe 1st Semi-AnnualGroundwaterMonitoring
Reportfor2015fortheBlackburnResourceRecoveryFacility,anactivemunicipalsolidwaste
(MSW)andconstructionanddemolition(C&D)landfilllocatedinCatawbaCounty,North
Carolina.ThreesolidwastedisposalfacilitiesaremaintainedbyCatawbaCountyunderNorth
CarolinaSolidWastePermit#18-03. The sitesincludedinthepermitareasfollows:
·BlackburnSubtitleDFacility(Units2and3):anactiveMSW
landfillonthesouth sideofNorthCarolinaRoute2019.
·BlackburnClosedPortion(Unit1):aclosedlandfillarea,whichis
contiguouswiththesoutheast sideofUnit2andsouth sideofUnit3.
·BlackburnNewC&DFacility(C&DUnit2):aC&Dlandfill
locatedtothesouthoftheactiveSubtitleDdisposalareaandwestofthe
ClosedPortion.
Inaddition,CatawbaCountymaintainstheOldC&DFacility(C&DUnit1),aformerC&
DlandfilllocatedacrossRoute2019tothenorthoftheactiveSubtitleDdisposalarea.
Overtheyears,thewaterqualitymonitoringnetworkatBlackburnResourceRecoveryFacility
hasevolvedandadaptedasthefacilityhasundergonechangesandexpansions.NCDENRhas
beeninvolvedthroughoutthemonitoringhistory,throughmeetingsandperiodicdiscussions,
toissuerecommendations,requirements,andapprovalstochangesinthemonitoringprogram.
In2003,REICpreparedacomprehensiveWaterQualityMonitoringPlanattherequestof
NCDENRinordertoincorporateallpriordiscussions,directives,andrequirementsforthe
individualsitesintoonedocument.REICsubmittedanupdatedWaterQualityMonitoring
PlaninJune2013(approvedbyNCDENRinJuly2013)toincorporateprogramchangesand
amendmentstotheNorthCarolinaSolidWasteManagementRulesthathadoccurredsince
2003.MonitoringisconductedonasemiannualbasispertheWaterQualityMonitoringPlan.
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Forthe 1st semiannual2015event,REICcollectedgroundwatersamplesfromtwenty-six(26)
monitoringwells,two(2)piezometers,andfour(4)surfacewaterlocationsatthefacility.In
addition,asamplewascollectedfromthefacility’sleachate.
2.0SITEDESCRIPTION
2.1PhysicalSetting
BlackburnResourceRecoveryFacilityislocatedonRockyFordRoadapproximatelysixmiles
southwestofNewton,NorthCarolina.Localtopographyinthevicinityofthefacilityis
characterizedbygentlyrollinghills.Elevationsintheareaofthelandfillrangefrom
approximately930feetabovemeansealevel(MSL)onknollstoaminimumelevationatan
unnamedtributarystreamtoSouthForkCatawbaRiverthatexitsthepropertyat
approximately790feetaboveMSL.Landusesurroundingthefacilityisindustrialtothe
north,residentialtothesouthandwest,andagriculturaltotheeast.
2.2GeologyandHydrogeology
ThefacilityislocatedwithintheInnerPiedmontBeltofthePiedmontPhysiographicProvince
ofNorthCarolina.GeologyintheregionischaracterizedbyCambrian/Proterozoic
amphibolitewithbiotitegneiss. Extensivecharacterizationofon-sitesoilsandrockhavebeen
performedthroughcoringprogramsandloggingofboringsconductedatthefacility.Soilsin
thevicinitybeginwithclayeysiltnearthesurface,whiledeepersoilsaremoresiltyandsandy.
Thetransitionalboundaryfromsoiltorockistypicallycharacterizedbypartiallyweathered
rockabovebedrock.Thissoiltorockboundaryinthevicinityofthelandfillgenerallyranges
fromapproximately10to70feetdeep.Groundwateroftheupper-mostaquiferexistsunder
watertableconditions.Infiltrationofprecipitationistheprimarysourceofrechargeof
groundwater.Hydraulicgradientsaregenerallyinthedirectionofthetopographicsurface
gradients,resultinginadischargeconditionatstreams,wherethewatertableintersectsthe
topographiclowpointsinthearea.
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2.3MonitoringNetwork
TheUnit1monitoringnetworkincludeswellsMW-5,MW-5A,MW-6,MW-6D,MW-7,and
MW-11,andsurfacewaterlocationsSW-1andSW-3. Twopiezometers,PZ-85BandPZ-86B,
locatedalongtheeasternsideofUnit1,areincludedinthenetworkinordertomonitor
impactsoflandfillgasfromtheclosedareatogroundwaterinthevicinity.TheUnit2
monitoringnetworkincludeswellsMW-12,MW-13,MW-14,MW-15,MW-16,andMW-17,
andunderdrainsU-1,U-2,andU-3.TheUnit3monitoringnetworkincludeswellsMW-31,
MW-32, MW-33,and MW-34,andsurfacewaterlocationsSW-4andSW-5.TheC&DUnit1
monitoringsystemincludeswellsMW-2,MW-26,andMW-27.WellMW-20servesasthe
backgroundmonitoringwellforUnit1,Unit2,Unit3,andC&DUnit1.TheC&DUnit2
monitoringsystemincludeswellMW-21,thebackgroundwell,andwellsMW-24,MW-25,
MW-28,MW-29,andMW-30.Inadditiontotheabovegroundwatersamplingpoints,several
wellsacrossthesiteareutilizedonlyforwaterlevelmonitoring.Samplinglocationsare
indicatedongroundwaterpotentiometricmapsincludedinthisreport.
3.0HYDROLOGICEVALUATION
3.1StaticWaterLevelsandGroundwaterElevations
StaticwaterlevelsweremeasuredfromthetopofcasingpriortopurginginallwellsonMarch
24-25,2015.Thesewaterlevelmeasurements,inconjunctionwithsurveyedcasingelevation
data,wereusedtocalculategroundwaterelevationsineachwell.Thisdataispresentedin
AppendixA.
3.2Groundwater FlowRateandDirection
Theelevationdatahavebeenutilizedtodeveloppotentiometricmapsforthefacility.The
BlackburnSubtitleD(Units2and3),ClosedPortion(Unit1),NewC&D(C&DUnit2),
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andOldC&D(C&DUnit1)facilitiesareshowntogetherontheresultingmapsthatare
includedinthisreport.Separatemapsareprovidedfortheshalloworupper-mostaquiferand
thepotentiometricsurfacedefinedbythedeeperwellscreens.
Theshallowaquiferisthemost significantwater-bearingzoneoftheprogramandthemajority
ofthewellscreensaresetinthislayer.Theaquiferlithologyconsistsofsandwithminorsilt,
althoughtwoofthewellshavescreenswithextremelowerportionspenetratingthebedrock.
Theshallowaquiferisunconfinedandthephreaticsurfacegenerallyfollowstopographical
contours.Therefore,theinfluenceofsurfacetopographyandelevationsalongthecreek,the
localdischargepoint,wereutilizedindevelopingthepotentiometricmapfortheshallow
aquifer.
Thepotentiometricmapconstructedfromwaterlevelmeasurementstakenatthedeeperwell
screensisbasedonfourdatapoints.Thefourwellsutilizedarethosewithrelativelydeeper
wellscreenslocatedatclusteredwellsetsintheSubtitleDandClosedPortionareas.These
wellshavescreensthatarefullylocatedinthebedrockorhavescreenslocatedinweathered
bedrock.Noclearlydefinedaquitardsarediscernablebetweentheshallowanddeeperwell
screenzones.Thegeneraldeepergroundwaterflowdirectionissimilartothatoftheshallow
aquifer.
Thepotentiometricmapscreatedfortheupper-mostaquiferanddeeperwellscreenzoneare
includedinthisreport.Thehorizontalcomponentsofthehydraulicgradientshavebeen
determinedbyfollowingflowpathsthatarenormaltotheshallowpotentiometriccontours.
Theseflowpathsareshownontheshallowpotentiometricmap.Hydraulicgradientsand
groundwatervelocitieswerenotcalculatedforthedeeperwellscreenzone.
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GroundwaterhorizontalflowvelocitieswereestimatedusingaformofDarcy’s Law:
V=(Kh *i)/ ne
where:
V=groundwatervelocity
Kh=horizontalhydraulicconductivity
i=hydraulicgradient
ne=effectiveporosity
Hydraulicparametersandestimatedflowvelocitiesoftheupper-mostaquiferforeachareaare
providedinthefollowingtable:
Area
Groundwater
Velocity
(ft/yr)
Hydraulic
Conductivity
(cm/sec)
Hydraulic
Gradient
(ft/ft)
Effective
Porosity
(unitless)
ClosedUnit1 250 1.9x10-3 0.027 0.21
SubtitleDUnit2 97 7.7x10-4 0.026 0.21
C&DUnit1 360 1.9x10-3 0.038 0.21
C&DUnit2 510 1.9x10-3 0.055 0.21
Thehorizontalplacementofdowngradientwellsisdeemedsufficienttoprovideearlydetection
ofpotentialreleasesfromthewasteunits.Verticalplacementofwatertablewellscreens
allowsmonitoringofgroundwateroftheuppermostaquifer.WellsMW-5AandMW-6D
allowmonitoringofverticalflowconditionsandverticaldistributionofgroundwater
constituentsinthedischargeregionalongthestreamdowngradientofUnit1.Thewell
monitoringnetworkoftheBlackburnResourceRecoveryFacilityappearstoremainadequate
tomonitorgroundwaterhydraulicallyupgradientanddowngradientofthelandfillunitsatthe
facility.
4.0SAMPLINGANDLABORATORYANALYSIS
4.1FieldSamplingSummary
The 1st semi-annual2015samplingeventwasperformedattheBlackburnResourceRecovery
FacilityonMarch24-25,2015.Alllocationsinthemonitoringnetworkweresampledduring
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themonitoringeventwiththeexceptionofunderdrainsU-1,U-2,andU-3associatedwith
SubtitleDUnit2,allofwhichweredryduringthesamplingevent.Aleachatesamplewas
collectedfromthefacility’sleachatecollectionsystemduringtheevent.Fieldsamplingwas
performedinaccordancewithstateandfederalguidelinesandthefacility’sWaterQuality
MonitoringPlan.Monitoringwellswereinspectedpriortosampling,andnosecurityissuesor
damagetothewellswerenotedwiththeexceptionofabentinnercasingatwellMW-28.
Staticwaterlevelsweremeasuredineachwellpriortopurgingutilizingadecontaminated
electronicmeasuringtape.
Monitoringwellswerepurgedandsampledusinglaboratorydecontaminatedpolytetra-
fluoroethylenebailers.FieldtestingofpH,temperature,conductivity,andturbiditywere
measuredtoensureadequatepurgingandtoverifystabilization.Sampleswerecollectedinto
pre-cleanedandappropriatelypreservedcontainers,placedinicedcoolers,andtransported
underproperchain-of-custodyprotocoltothelaboratory.SamplepH,temperature,
conductivity,andturbidityweremeasuredinthefieldusingcalibratedinstruments.Allwell
purgingandsamplingwasperformedwithnounusualcharacteristicsobservedwiththe
exceptionofsignificantsuspendedsolidsinseveralgroundwatersamples.Fieldsamplinglogs
areincludedinAppendixB(SubtitleDUnits2and3),AppendixC(ClosedUnit1),and
AppendixD(C&DUnits1and2).
4.2LaboratoryAnalysisSummary
Samplescollectedduringthe 1st semi-annual2015eventwereanalyzedbyREIC.Allsamples
collectedduringthemonitoringeventwerereceivedbythelaboratoryingoodconditionandat
propertemperatures.SampleswereanalyzedutilizingU.S.EPAapprovedmethodswithin
requiredholdingtimes.SamplesassociatedwiththeSubtitleDUnits2and3andClosedUnit
1areaswereanalyzedforNorthCarolinaAppendixIparameters.Groundwatersamples
associatedwiththeC&DlandfillswereanalyzedforNorthCarolinaAppendixIVOCsand
eightRCRAmetalspertheWaterQualityMonitoringPlan,inadditiontotetrahydrofuranper
theJune25,2010memofromNCDENR.
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4.3QualityAssurance/QualityControl
Fieldqualitycontrolsamplesincludedduplicatesamplesandtripblanks.Duplicatesample
resultsgenerallyagreedwellwithparentsampleresults.Analysisofthetripblanksamplesdid
notindicateanycontaminationissuesviathefieldsampling,sampletransportation,or
laboratoryhandlingprocesses.
Thelaboratoryqualityassurance/qualitycontrol(QA/QC)programincludedallappropriate,
methodspecificqualitycontrols.Laboratorydatametthenecessaryqualitycontrolcriteria.
Laboratorycontrolsamplespikerecoveriesandsurrogaterecoverieswerewithinrequired
limits,andlaboratoryduplicate,matrixspike,andmethodblankanalyseswereacceptable.
4.4AnalyticalResults
Laboratoryreportsandchain-of-custodyrecordsareincludedinAppendixB(SubtitleDUnits
2and3),AppendixC(ClosedUnit1),andAppendixD(C&DUnits1and2).Datahave
beenreportedtomethoddetectionlimits(MDLs)asrequestedbyNCDENR.However,note
thatanyvaluesreportedbelowSolidWasteSectionLimits(SWSLs),flaggedwitha“J”
qualifier,areonlyestimates,arenotquantitative,andshouldnotbeusednumericallyinany
way.
LaboratoryanalysisforsamplesassociatedwithSubtitleDUnit2indicatedthatno
constituentsweredetectedaboveNorthCarolinagroundwaterstandardsinmonitoringwells
withtheexceptionofcobaltinwells MW-12and MW-16,andvanadiuminwell MW-16.
ParametersthatexceededNorthCarolinagroundwaterstandardsintheSubtitleDUnit3
monitoringwellsincludedbariuminwellMW-33;chromiuminwellsMW-31,MW-32,MW-
33,and MW-34;cobaltandvanadiuminwellsMW-31, MW-32,and MW-33;andleadinwell
MW-33.NoparametersweredetectedaboveNorthCarolinagroundwater/surfacewater
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standardsinsurfacewatersamplesSW-4andSW-5withtheexceptionoftetrachloroethenein
sampleSW-4.
ParametersobservedatconcentrationsaboveNorthCarolinagroundwaterstandardsin
compliancewellsassociatedwithClosedUnit1areasfollows:
Parameter MonitoringWell
Benzene MW-5A, MW-6,MW-7, MW-11
Chromium MW-5,MW-7
Cobalt MW-6,MW-7,MW-11
1,4-Dichlorobenzene MW-6,MW-7
1,1-Dichloroethane MW-5A, MW-6
Tetrachloroethene MW-5A
Trichloroethene MW-5A
Vanadium MW-5,MW-7,MW-11
Vinylchloride MW-7,MW-11
Theparametersandconcentrationsobservedduringthe 1st semiannual2015eventinwells
associatedwithClosedUnit1aregenerallyconsistentwithrecenthistoricaldata.Inaddition,
VOCsobservedduringthe 1st semiannual2015eventinpiezometersPZ-85BandPZ-86Bare
consistentwithrecenthistoricaldata.NoparametersweredetectedaboveSWSLsinthe
surfacewatersamplesSW-1andSW-3.
AreviewofthegroundwaterdatafortheC&DLandfillsindicateddetectionsaboveNorth
CarolinagroundwaterstandardsofbariuminwellMW-27andchromiuminwellsMW-21,
MW-24,MW-26,MW-29andMW-30(notethatwellMW-21isanupgradientbackground
well).
AnalyticalparametersthatweredetectedaboveSWSLsaresummarizedintablesincludedin
AppendixB(SubtitleDUnits2and3),AppendixC(ClosedUnit1),andAppendixD(C&D
Units1and2).Asummaryofdetectionstableisincludedforeacharea.Valuesgreaterthan
theNorthCarolinagroundwaterstandardsareshowninredprint.Dissolvedmetalsdetections
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andtotalsuspendedsolidsresults,aswellashistoricaldatasummaries,areincludedinthe
appendicesforeachareaofthefacility.
DuetochangesinNorthCarolinasolidwasterules,statisticalanalysisofgroundwaterdatais
nolongerrequired.However,statisticalanalysiswasutilizedtodemonstratethatmetals
concentrationsexceedinggroundwaterstandardswereactuallylessthanbackgroundlevels.
Thisevaluationindicatesthatthemetalsobservedabovegroundwaterstandardsincompliance
wellsassociatedwiththeSubtitleDUnit2,SubtitleDUnit3,C&DUnit1,andC&DUnit2
areasarenotstatisticallyelevatedoverbackgroundlevels.TheStatisticalAnalysisSummary
isincludedinAppendix E, “AlternateSourceDemonstration”.
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5.0FINDINGSANDCONCLUSIONS
5.1 SummaryofFindings
·The 1st semi-annual2015waterqualitymonitoringeventatBlackburnResource
RecoveryFacilityhasbeenperformedinaccordancewithNorthCarolinaregulations
andthefacility’sWaterQualityMonitoringPlan.
·Thehorizontalgroundwaterflowrateoftheuppermostaquiferhasbeenestimatedto
rangefrom97to510ft/yearthroughoutthesite.Thewellsinthemonitoringnetwork
appeartobeadequatetomonitorgroundwaterhydraulicallyupgradientand
downgradientofthefacility.
·Fieldsamplingandlaboratoryanalysisactivitieswereperformedwithnosignificant
proceduraldeviationsandwithinacceptableQA/QCparameters.
·Severalparametersexceededgroundwaterstandardsinwellsassociatedwiththe
ClosedUnit1area.However,resultsareconsistentwithdatafrompreviousevents.
·Severalmetalsparametersexceededgroundwaterstandardsinwellsassociatedwith
theSubtitleDUnit2and3andC&DUnit1and2areas.However,statistical
analysisindicatedthatthemetalsconcentrationswerelessthanbackgroundlevels.
5.2Conclusions
Areviewofthemonitoringwellnetwork,fieldsamplingandlaboratoryanalysisactivities,and
QA/QCprogramindicatesthatthe 1st semi-annual2015groundwatermonitoringeventatthe
BlackburnResourceRecoveryFacilityyieldedsamplesrepresentativeoftheuppermostaquifer
inthevicinityofthefacility.Basedontheresultsofthecurrentgroundwatermonitoring
event,andpursuanttoNorthCarolinaSub-Chapter13B,Rule.1633,itisrecommendedthat
theBlackburnSubtitleDlandfillsremaininadetectionmonitoringprogramforthe 2nd semi-
1st Semi-Annual2015Groundwater MonitoringReport
___________________________________________________________________________________________
REIConsultants,Inc.P.O.Box286,Beaver,WV25813800-999-0105 www.reiclabs.com
16
annualmonitoringeventof2015.Inaddition,itisrecommendedthattheC&DLandfills
remaininadetectionmonitoringprogramforthe 2nd semi-annualmonitoringeventof2015.It
isalsorecommendedthatassessmentmonitoringcontinueattheClosedUnit1facilityduring
the 2nd semi-annualeventof2015withanalysisofAppendixIparameters.
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Potentiometric Contour Maps
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
AppendixA:
Static Water Level Summary
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Subtitle D
AppendixB1:
1st Semi-Annual 2015
Summary of Detections
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
B la
c k b u r n
L an
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fi
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:
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:
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#:
1 5 03
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CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Subtitle D
AppendixB2:
Summary ofDissolvedMetalsand
TotalSuspendedSolid(TSS)
Detections
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Su
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-
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(m
g /L)
2.
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re
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a b o ve
S WS
Ls
sh
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S P E CI
AL
NO
T E S:
A ll
d a ta
re
p o r t ed
in
m g /L.
Su
mm
a r y
o f
Di
ss
o lv
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Me
t a l s
a nd
T SS
D e t e c ti
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a nd
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,
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,
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0 .01
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0 .01
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d,
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0 .01
Ni
c k e l,
D i ss
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0 .05
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,
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0 .01
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v e r ,
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0 .01
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0 .0 0 55
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S
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(T SS
)
1
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3 63
1 1 80
2 00
-
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F OO
T NO
T E S:
1.
S W SL
-
S o l id
W a s te
Se
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(m
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2.
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a b o ve
S WS
Ls
sh
o wn
S P E CI
AL
NO
T E S:
A ll
d a ta
re
p o r t ed
in
m g /L.
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB3:
HistoricalSummaryofDetections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Subtitle D -Unit 2
HistoricalSummary ofDetections
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
Subtitle D -Unit 3
HistoricalSummary ofDetections
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page20
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB4:
LeachateAnalysisSummary
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
REICJobNumber:1503V17
SampleDate:3-2015
Units PQL Result
Volatiles by GCMS
1 1,1,1,2-Tetrachloroethane mg/L 0.005 ND
2 1,1,1-Trichloroethane mg/L 0.001 ND
3 1,1,2,2-Tetrachloroethane mg/L 0.003 ND
4 1,1,2-Trichloroethane mg/L 0.001 ND
5 1,1-Dichloroethane mg/L 0.005 ND
6 1,1-Dichloroethene mg/L 0.005 ND
7 1,2,3-Trichloropropane mg/L 0.001 ND
8 1,2-Dibromo-3-Chloropropane (DBCP)mg/L 0.013 ND
9 1,2-Dibromoethane (EDB)mg/L 0.001 ND
10 1,2-Dichlorobenzene mg/L 0.005 ND
11 1,2-Dichloroethane mg/L 0.001 ND
12 1,2-Dichloropropane mg/L 0.001 ND
13 1,4-Dichlorobenzene mg/L 0.001 0.0024
14 2-Butanone(Methylethylketone)mg/L 0.100 ND
15 2-Hexanone mg/L 0.050 ND
16 4-Methyl-2-pentanone mg/L 0.100 ND
17 Acetone mg/L 0.100 ND
18 Acrylonitrile mg/L 0.20 ND
19 Benzene mg/L 0.001 0.0030
20 Bromochloromethane mg/L 0.003 ND
21 Bromodichloromethane mg/L 0.001 ND
22 Bromoform mg/L 0.003 ND
23 Bromomethane (Methyl bromide)mg/L 0.010 ND
24 Carbon disulfide mg/L 0.100 ND
25 Carbon tetrachloride mg/L 0.001 ND
26 Chlorobenzene mg/L 0.003 ND
27 Chloroethane mg/L 0.010 ND
28 Chloroform mg/L 0.005 ND
29 Chloromethane (Methyl chloride)mg/L 0.001 ND
30 cis-1,2-Dichloroethene mg/L 0.005 ND
31 cis-1,3-Dichloropropene mg/L 0.001 ND
32 Dibromochloromethane mg/L 0.003 ND
33 Dibromomethane(Methylenebromide)mg/L 0.010 ND
34 Ethylbenzene mg/L 0.001 0.0088
35 Iodomethane(Methyliodide)mg/L 0.010 ND
36 Methylene chloride mg/L 0.001 ND
37 Styrene mg/L 0.001 ND
38 Tetrachloroethene mg/L 0.001 ND
39 Toluene mg/L 0.001 0.0012
40 trans-1,2-Dichloroethene mg/L 0.005 ND
41 trans-1,3-Dichloropropene mg/L 0.001 ND
42 trans-1,4-Dichloro-2-butene mg/L 0.100 ND
43 Trichloroethene mg/L 0.001 ND
44 Trichlorofluoromethane mg/L 0.001 ND
45 Vinyl acetate mg/L 0.050 ND
46 Vinyl chloride mg/L 0.001 ND
47 Xylenes mg/L 0.005 0.0098
DATA SUMMARY
CatawbaCounty,NC-SubtitleD Landfill- Leachate
Parameter
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
REICJobNumber:1503V17
SampleDate:3-2015
Units PQL Result
DATA SUMMARY
CatawbaCounty,NC-SubtitleD Landfill- Leachate
Parameter
Inorganics (Metals)
48 Antimony mg/L 0.006 ND
49 Arsenic mg/L 0.010 ND
50 Barium mg/L 0.100 0.120
51 Beryllium mg/L 0.001 ND
52 Cadmium mg/L 0.001 ND
53 Chromium mg/L 0.010 0.0218
54 Cobalt mg/L 0.010 0.0132
55 Copper mg/L 0.010 ND
56 Lead mg/L 0.010 ND
57 Nickel mg/L 0.050 ND
58 Selenium mg/L 0.010 ND
59 Silver mg/L 0.010 ND
60 Thallium mg/L 0.006 ND
61 Vanadium mg/L 0.025 ND
62 Zinc mg/L 0.010 0.0817
Additional Parameters
Biochemical OxygenDemand(BOD)mg/L 2.0 27
Chemical OxygenDemand(COD)mg/L 10.0 298
Nitrate mg/L 0.1 ND
ortho-Phosphate mg/L 0.1 ND
Sulfate mg/L 5.0 6.52
NOTES:
ND-NotDetectedatPQL
PQL-PracticalQuantitationLimits (PQLs)arethe lowestconcentraitonofanalytes ingroundwaterthatcanbereliably
determinedwithinspecified limitsofprecisionandaccuracybyaparticularmethodunderroutine laboratoryconditions.
IfthePQL foraparticularmethod isahighervaluethanthegroundwaterstandard forthatparameter, itmustbenbe
equalorbe lessthanthePQLsstated intheNorthCarolinaAppendixIIMonitoringandAppendixIOrganicConsituents
Guidelines.
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 2
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB5:
SummaryofDataPre-DatingUnit3
Construction/Waste Placement
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
SUMMARY OF VOC DATA
PRE-DATING UNIT 3 CONSTRUCTION/WASTE PLACEMENT
Blackburn Landfill
Permit:#18-03
Analyte SWSL Units Sep-04 Mar-05 Sep-05 Mar-06 Sep-06 Mar-07 Sep-07
Acetone 0.1 mg/L ND ND ND ND ND ND ND
Acrylonitrile 0.2 mg/L ND ND ND ND ND ND ND
Benzene 0.001 mg/L ND ND ND ND ND ND ND
Bromochloromethane 0.003 mg/L ND ND ND ND ND ND ND
Bromodichloromethane 0.001 mg/L ND ND ND ND ND ND ND
Bromoform 0.003 mg/L ND ND ND ND ND ND ND
Bromomethane 0.01 mg/L ND ND ND ND ND ND ND
2-Butanone 0.1 mg/L ND ND ND ND ND ND ND
Carbondisulfide 0.1 mg/L ND ND ND ND ND ND ND
Carbontetrachloride 0.001 mg/L ND ND ND ND ND ND ND
Chlorobenzene 0.003 mg/L ND ND ND ND ND ND ND
Chloroethane 0.01 mg/L ND ND ND ND ND ND ND
Chloroform 0.005 mg/L ND ND ND ND ND ND ND
Chloromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromo-3-chloropropane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromoethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dichlorobenzene 0.005 mg/L ND ND ND ND ND ND ND
1,4-Dichlorobenzene 0.001 mg/L ND ND ND ND ND ND ND
trans-1,4-Dichloro-2-butene 0.1 mg/L ND ND ND ND ND ND ND
1,1-Dichloroethane 0.005 mg/L ND 0.007 0.014 0.019 0.025 0.0134 0.007
1,2-Dichloroethane 0.001 mg/L ND ND ND ND ND ND ND
1,1-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
cis-1,2-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
trans-1,2-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
1,2-Dichloropropane 0.001 mg/L ND ND ND ND ND ND ND
cis-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
trans-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
Dibromochloromethane 0.001 mg/L ND ND ND ND ND ND ND
Dibromomethane 0.01 mg/L ND ND ND ND ND ND ND
Ethylbenzene 0.001 mg/L ND ND ND ND ND ND ND
2-Hexanone 0.05 mg/L ND ND ND ND ND ND ND
Iodomethane 0.01 mg/L ND ND ND ND ND ND ND
Methylenechloride 0.001 mg/L ND ND ND ND ND ND ND
4-Methyl-2-pentanone 0.1 mg/L ND ND ND ND ND ND ND
Styrene 0.001 mg/L ND ND ND ND ND ND ND
1,1,1,2-Tetrachloroethane 0.005 mg/L ND ND ND ND ND ND ND
1,1,2,2-Tetrachloroethane 0.001 mg/L ND ND ND ND ND ND ND
Tetrachloroethene 0.001 mg/L 0.025 0.031 0.024 0.034 0.039 0.035 0.018
Toluene 0.001 mg/L ND ND ND ND ND ND ND
1,1,1-Trichloroethane 0.001 mg/L ND ND ND ND ND ND ND
1,1,2-Trichloroethane 0.005 mg/L ND ND ND ND ND ND ND
Trichloroethene 0.001 mg/L 0.030 0.055 0.042 0.061 0.070 0.039 0.018
Trichlorofluoromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2,3-Trichloropropane 0.001 mg/L ND ND ND ND ND ND ND
Vinylacetate 0.05 mg/L ND ND ND ND ND ND ND
Vinylchloride 0.001 mg/L ND ND 0.005 0.002 ND ND ND
Xylenes,Total 0.003 mg/L ND ND ND ND ND ND ND
FOOTNOTES:
SWSL-SolidWasteSectionLimits(mg/L)
ND-notdetectedatorabovetheSWSL
PZ-83B
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page 1
SUMMARY OF VOC DATA
PRE-DATING UNIT 3 CONSTRUCTION/WASTE PLACEMENT
Blackburn Landfill
Permit:#18-03
Analyte SWSL Units Sep-04 Mar-05 Sep-05 Mar-06 Sep-06 Mar-07 Sep-07
Acetone 0.1 mg/L ND ND ND ND ND ND ND
Acrylonitrile 0.2 mg/L ND ND ND ND ND ND ND
Benzene 0.001 mg/L 0.010 0.008 0.010 0.009 0.011 0.0106 0.0108
Bromochloromethane 0.003 mg/L ND ND ND ND ND ND ND
Bromodichloromethane 0.001 mg/L ND ND ND ND ND ND ND
Bromoform 0.003 mg/L ND ND ND ND ND ND ND
Bromomethane 0.01 mg/L ND ND ND ND ND ND ND
2-Butanone 0.1 mg/L ND ND ND ND ND ND ND
Carbondisulfide 0.1 mg/L ND ND ND ND ND ND ND
Carbontetrachloride 0.001 mg/L ND ND ND ND ND ND ND
Chlorobenzene 0.003 mg/L ND ND ND 0.006 0.007 0.007 0.008
Chloroethane 0.01 mg/L ND ND ND ND ND ND ND
Chloroform 0.005 mg/L ND ND ND ND ND ND ND
Chloromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromo-3-chloropropane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dibromoethane 0.001 mg/L ND ND ND ND ND ND ND
1,2-Dichlorobenzene 0.005 mg/L ND ND ND ND ND ND ND
1,4-Dichlorobenzene 0.001 mg/L 0.013 0.015 0.017 0.018 0.018 0.015 0.015
trans-1,4-Dichloro-2-butene 0.1 mg/L ND ND ND ND ND ND ND
1,1-Dichloroethane 0.005 mg/L 0.090 0.087 0.075 0.075 0.081 0.052 0.034
1,2-Dichloroethane 0.001 mg/L ND ND 0.002 ND ND ND ND
1,1-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
cis-1,2-Dichloroethene 0.005 mg/L 0.094 0.098 0.091 0.163 0.213 0.16 0.142
trans-1,2-Dichloroethene 0.005 mg/L ND ND ND ND ND ND ND
1,2-Dichloropropane 0.001 mg/L 0.009 0.007 0.008 0.006 0.006 0.005 0.004
cis-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
trans-1,3-Dichloropropene 0.001 mg/L ND ND ND ND ND ND ND
Dibromochloromethane 0.001 mg/L ND ND ND ND ND ND ND
Dibromomethane 0.01 mg/L ND ND ND ND ND ND ND
Ethylbenzene 0.001 mg/L ND ND ND ND ND ND ND
2-Hexanone 0.05 mg/L ND ND ND ND ND ND ND
Iodomethane 0.01 mg/L ND ND ND ND ND ND ND
Methylenechloride 0.001 mg/L 0.235 0.105 0.082 ND 0.026 0.030 0.015
4-Methyl-2-pentanone 0.1 mg/L ND ND ND ND ND ND ND
Styrene 0.001 mg/L ND ND ND ND ND ND ND
1,1,1,2-Tetrachloroethane 0.005 mg/L ND ND ND ND ND ND ND
1,1,2,2-Tetrachloroethane 0.001 mg/L ND ND ND ND ND ND ND
Tetrachloroethene 0.001 mg/L 0.154 0.092 0.107 0.028 0.023 0.0198 0.011
Toluene 0.001 mg/L ND ND ND ND ND 0.0033 0.0047
1,1,1-Trichloroethane 0.001 mg/L ND ND ND ND ND ND ND
1,1,2-Trichloroethane 0.005 mg/L ND ND ND ND ND ND ND
Trichloroethene 0.001 mg/L 0.160 0.156 0.111 0.048 0.030 0.017 0.014
Trichlorofluoromethane 0.001 mg/L ND ND ND ND ND ND ND
1,2,3-Trichloropropane 0.001 mg/L ND ND ND ND ND ND ND
Vinylacetate 0.05 mg/L ND ND ND ND ND ND ND
Vinylchloride 0.001 mg/L ND ND 0.005 0.003 0.003 ND ND
Xylenes,Total 0.003 mg/L 0.059 0.044 0.067 0.052 0.061 0.070 0.070
FOOTNOTES:
SWSL-SolidWasteSectionLimits(mg/L)
ND-notdetectedatorabovetheSWSL
PZ-84B
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page 2
SUMMARY OF VOC DATA
PRE-DATING UNIT 3 CONSTRUCTION/WASTE PLACEMENT
Blackburn Landfill
Permit:#18-03
Analyte SWSL Units Mar-08 Sep-08 Mar-09 Apr-09
1,1,1,2-Tetrachloroethane 0.005 mg/L ND ND ND ND
1,1,1-Trichloroethane 0.001 mg/L ND ND ND ND
1,1,2,2-Tetrachloroethane 0.001 mg/L ND ND ND ND
1,1,2-Trichloroethane 0.005 mg/L ND ND ND ND
1,1-Dichloroethane 0.005 mg/L ND 0.0070 0.0128 0.0182
1,1-Dichloroethene 0.005 mg/L ND ND ND ND
1,2,3-Trichloropropane 0.001 mg/L ND ND ND ND
1,2-Dibromo-3-chloropropane 0.001 mg/L ND ND ND ND
1,2-Dibromoethane 0.001 mg/L ND ND ND ND
1,2-Dichlorobenzene 0.005 mg/L ND ND ND ND
1,2-Dichloroethane 0.001 mg/L ND ND ND ND
1,2-Dichloropropane 0.001 mg/L ND ND ND ND
1,4-Dichlorobenzene 0.001 mg/L ND 0.0033 0.0044 0.0039
2-Butanone 0.1 mg/L ND ND ND ND
2-Hexanone 0.05 mg/L ND ND ND ND
4-Methyl-2-pentanone 0.1 mg/L ND ND ND ND
Acetone 0.1 mg/L ND ND ND ND
Acrylonitrile 0.2 mg/L ND ND ND ND
Benzene 0.001 mg/L ND ND 0.0011 0.0017
Bromochloromethane 0.003 mg/L ND ND ND ND
Bromodichloromethane 0.001 mg/L ND ND ND ND
Bromoform 0.003 mg/L ND ND ND ND
Bromomethane 0.01 mg/L ND ND ND ND
Carbondisulfide 0.1 mg/L ND ND ND ND
Carbontetrachloride 0.001 mg/L ND ND ND ND
Chlorobenzene 0.003 mg/L ND ND ND ND
Chloroethane 0.01 mg/L ND ND ND ND
Chloroform 0.005 mg/L ND ND ND ND
Chloromethane 0.001 mg/L ND ND ND ND
cis-1,2-Dichloroethene 0.005 mg/L ND 0.0081 0.0160 0.0243
cis-1,3-Dichloropropene 0.001 mg/L ND ND ND ND
Dibromochloromethane 0.001 mg/L ND ND ND ND
Dibromomethane 0.01 mg/L ND ND ND ND
Ethylbenzene 0.001 mg/L ND ND ND ND
Iodomethane 0.01 mg/L ND ND ND ND
Methylenechloride 0.001 mg/L ND 0.0020 0.0056 0.0079
Styrene 0.001 mg/L ND ND ND ND
Tetrachloroethene 0.001 mg/L ND 0.0039 0.0076 0.0157
Toluene 0.001 mg/L ND ND ND ND
trans-1,2-Dichloroethene 0.005 mg/L ND ND ND ND
trans-1,3-Dichloropropene 0.001 mg/L ND ND ND ND
trans-1,4-Dichloro-2-butene 0.1 mg/L ND ND ND ND
Trichloroethene 0.001 mg/L ND 0.0045 0.0120 0.0200
Trichlorofluoromethane 0.001 mg/L ND ND ND ND
Vinylacetate 0.05 mg/L ND ND ND ND
Vinylchloride 0.001 mg/L ND ND 0.0015 ND
Xylenes,Total 0.003 mg/L ND ND ND ND
FOOTNOTES:
SWSL-SolidWasteSectionLimits(mg/L)
ND-notdetectedatorabovetheSWSL
MW-31
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page 3
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB6:
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Tuesday, April 07, 2015
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:BLACKBURN SUBTITLE D - 1SA 2015
Work Order #:1503V10
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 8 sample(s) on 3/26/2015 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Case Narrative
Client:
Project:BLACKBURN SUBTITLE D - 1SA 2015
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:50:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-01A Matrix:Groundwater
MW-12Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 1:41 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Barium 0.0778 0.100 J mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:41 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:41 PM
Chromium ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Cobalt 0.0248 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Copper 0.0032 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/2/2015 1:41 PM
Nickel 0.0027 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 1:41 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 1:41 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 1:41 PM
Vanadium ND 0.0250 mg/L0.0010 NA PA/VA4/2/2015 1:41 PM
Zinc 0.0072 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 1:41 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 10:38 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 10:38 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 10:38 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 10:38 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 10:38 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 10:38 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 10:38 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 10:38 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 10:38 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 10:38 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 10:38 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 10:38 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 10:38 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 10:38 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 10:38 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 10:38 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 10:38 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 10:38 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 10:38 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 10:38 AM
Page 3 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:50:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-01A Matrix:Groundwater
MW-12Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 10:38 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 10:38 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 10:38 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 10:38 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 10:38 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 10:38 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 10:38 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 10:38 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 10:38 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 10:38 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 10:38 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 10:38 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 10:38 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 10:38 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 10:38 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 10:38 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 10:38 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 10:38 AM
Toluene 0.560 1.00 J µg/L0.167 NA PA/VA3/28/2015 10:38 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 10:38 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 10:38 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 10:38 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 10:38 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 10:38 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 10:38 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 10:38 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 10:38 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 10:38 AM
Surr: 1,2-Dichloroethane-d4 100 68.7-129 %RECNANA 3/28/2015 10:38 AM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 3/28/2015 10:38 AM
Surr: Dibromofluoromethane 95.2 74.3-124 %RECNANA 3/28/2015 10:38 AM
Surr: Toluene-d8 98.8 71.4-129 %RECNANA 3/28/2015 10:38 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 16.0 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 4 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:08:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-02A Matrix:Groundwater
MW-13Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 1:47 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Barium 0.106 0.100 mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:47 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:47 PM
Chromium 0.0096 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Cobalt 0.0035 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Copper 0.0231 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Lead 0.0006 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 1:47 PM
Nickel 0.0047 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 1:47 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 1:47 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 1:47 PM
Vanadium 0.0204 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 1:47 PM
Zinc 0.0253 0.0100 mg/L0.0030 NA PA/VA4/2/2015 1:47 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 11:12 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 11:12 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 11:12 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 11:12 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 11:12 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 11:12 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 11:12 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 11:12 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 11:12 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 11:12 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 11:12 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 11:12 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 11:12 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 11:12 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 11:12 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 11:12 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 11:12 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 11:12 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 11:12 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 11:12 AM
Page 5 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:08:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-02A Matrix:Groundwater
MW-13Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 11:12 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 11:12 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 11:12 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 11:12 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 11:12 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 11:12 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 11:12 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 11:12 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 11:12 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 11:12 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 11:12 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 11:12 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 11:12 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 11:12 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 11:12 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 11:12 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 11:12 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 11:12 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 11:12 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 11:12 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 11:12 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 11:12 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 11:12 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 11:12 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 11:12 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 11:12 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 11:12 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 11:12 AM
Surr: 1,2-Dichloroethane-d4 101 68.7-129 %RECNANA 3/28/2015 11:12 AM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 3/28/2015 11:12 AM
Surr: Dibromofluoromethane 98.8 74.3-124 %RECNANA 3/28/2015 11:12 AM
Surr: Toluene-d8 100 71.4-129 %RECNANA 3/28/2015 11:12 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 69.0 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 6 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:49:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-03A Matrix:Groundwater
MW-14Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 1:52 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Barium 0.0481 0.100 J mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:52 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:52 PM
Chromium 0.0019 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Cobalt 0.0020 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Copper 0.0050 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Lead 0.0003 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 1:52 PM
Nickel 0.0027 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 1:52 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 1:52 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 1:52 PM
Vanadium 0.0090 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 1:52 PM
Zinc 0.0075 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 1:52 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 9:30 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 9:30 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 9:30 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 9:30 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 9:30 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 9:30 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 9:30 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 9:30 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 9:30 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 9:30 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 9:30 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 9:30 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 9:30 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 9:30 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 9:30 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 9:30 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 9:30 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 9:30 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 9:30 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 9:30 AM
Page 7 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:49:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-03A Matrix:Groundwater
MW-14Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 9:30 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 9:30 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 9:30 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 9:30 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 9:30 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 9:30 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 9:30 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 9:30 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 9:30 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 9:30 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 9:30 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 9:30 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 9:30 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 9:30 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 9:30 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 9:30 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 9:30 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 9:30 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 9:30 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 9:30 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 9:30 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 9:30 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 9:30 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 9:30 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 9:30 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 9:30 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 9:30 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 9:30 AM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 3/28/2015 9:30 AM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 3/28/2015 9:30 AM
Surr: Dibromofluoromethane 97.9 74.3-124 %RECNANA 3/28/2015 9:30 AM
Surr: Toluene-d8 96.8 71.4-129 %RECNANA 3/28/2015 9:30 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 11.5 5.0 mg/L1.0 NA PA/VA3/27/2015 1:23 PM
Page 8 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:20:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-04A Matrix:Groundwater
MW-15Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 1:58 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Barium 0.0252 0.100 J mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:58 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 1:58 PM
Chromium 0.0031 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Copper 0.0027 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/2/2015 1:58 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/2/2015 1:58 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 1:58 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 1:58 PM
Vanadium 0.0014 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 1:58 PM
Zinc 0.0040 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 1:58 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 10:04 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 10:04 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 10:04 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 10:04 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 10:04 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 10:04 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 10:04 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 10:04 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 10:04 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 10:04 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 10:04 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 10:04 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 10:04 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 10:04 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 10:04 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 10:04 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 10:04 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 10:04 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 10:04 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 10:04 AM
Page 9 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:20:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-04A Matrix:Groundwater
MW-15Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 10:04 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 10:04 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 10:04 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 10:04 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 10:04 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 10:04 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 10:04 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 10:04 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 10:04 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 10:04 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 10:04 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 10:04 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 10:04 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 10:04 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 10:04 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 10:04 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 10:04 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 10:04 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 10:04 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 10:04 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 10:04 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 10:04 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 10:04 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 10:04 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 10:04 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 10:04 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 10:04 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 10:04 AM
Surr: 1,2-Dichloroethane-d4 101 68.7-129 %RECNANA 3/28/2015 10:04 AM
Surr: 4-Bromofluorobenzene 111 71.8-127 %RECNANA 3/28/2015 10:04 AM
Surr: Dibromofluoromethane 97.0 74.3-124 %RECNANA 3/28/2015 10:04 AM
Surr: Toluene-d8 100 71.4-129 %RECNANA 3/28/2015 10:04 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 10.5 5.0 mg/L1.0 NA PA/VA3/27/2015 1:23 PM
Page 10 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:00:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-05A Matrix:Groundwater
MW-16Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 2:03 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Barium 0.206 0.100 mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Beryllium 0.0008 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 2:03 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:03 PM
Chromium 0.0079 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Cobalt 0.0230 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Copper 0.0138 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Lead 0.0023 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 2:03 PM
Nickel 0.0050 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 2:03 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 2:03 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 2:03 PM
Vanadium 0.0351 0.0250 mg/L0.0010 NA PA/VA4/2/2015 2:03 PM
Zinc 0.0326 0.0100 mg/L0.0030 NA PA/VA4/2/2015 2:03 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 11:46 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 11:46 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 11:46 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 11:46 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 11:46 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 11:46 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 11:46 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 11:46 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 11:46 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 11:46 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 11:46 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 11:46 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 11:46 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 11:46 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 11:46 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 11:46 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 11:46 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 11:46 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 11:46 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 11:46 AM
Page 11 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:00:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-05A Matrix:Groundwater
MW-16Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 11:46 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 11:46 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 11:46 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 11:46 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 11:46 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 11:46 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 11:46 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 11:46 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 11:46 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 11:46 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 11:46 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 11:46 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 11:46 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 11:46 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 11:46 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 11:46 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 11:46 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 11:46 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 11:46 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 11:46 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 11:46 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 11:46 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 11:46 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 11:46 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 11:46 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 11:46 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 11:46 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 11:46 AM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 3/28/2015 11:46 AM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 3/28/2015 11:46 AM
Surr: Dibromofluoromethane 96.7 74.3-124 %RECNANA 3/28/2015 11:46 AM
Surr: Toluene-d8 98.6 71.4-129 %RECNANA 3/28/2015 11:46 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 74.0 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 12 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 7:39:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-06A Matrix:Groundwater
MW-17Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 2:09 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Barium 0.0610 0.100 J mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:09 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:09 PM
Chromium 0.0034 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Cobalt 0.0035 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Copper 0.0049 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Lead 0.0010 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 2:09 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/2/2015 2:09 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 2:09 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 2:09 PM
Vanadium 0.0137 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 2:09 PM
Zinc 0.0096 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 2:09 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 12:21 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 12:21 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 12:21 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 12:21 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 12:21 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 12:21 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 12:21 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 12:21 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 12:21 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 12:21 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 12:21 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 12:21 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 12:21 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 12:21 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 12:21 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 12:21 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 12:21 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 12:21 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 12:21 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 12:21 PM
Page 13 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 7:39:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-06A Matrix:Groundwater
MW-17Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 12:21 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 12:21 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 12:21 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 12:21 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 12:21 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 12:21 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 12:21 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 12:21 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 12:21 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 12:21 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 12:21 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 12:21 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 12:21 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 12:21 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 12:21 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 12:21 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 12:21 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 12:21 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 12:21 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 12:21 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 12:21 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 12:21 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 12:21 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 12:21 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 12:21 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 12:21 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 12:21 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 12:21 PM
Surr: 1,2-Dichloroethane-d4 104 68.7-129 %RECNANA 3/28/2015 12:21 PM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 3/28/2015 12:21 PM
Surr: Dibromofluoromethane 99.3 74.3-124 %RECNANA 3/28/2015 12:21 PM
Surr: Toluene-d8 98.0 71.4-129 %RECNANA 3/28/2015 12:21 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 97.0 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 14 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:20:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-07A Matrix:Groundwater
MW-15 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 2:15 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Barium 0.0243 0.100 J mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:15 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:15 PM
Chromium 0.0029 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Copper 0.0024 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/2/2015 2:15 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/2/2015 2:15 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 2:15 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 2:15 PM
Vanadium 0.0013 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 2:15 PM
Zinc 0.0082 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 2:15 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 12:55 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 12:55 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 12:55 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 12:55 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 12:55 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 12:55 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 12:55 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 12:55 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 12:55 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 12:55 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 12:55 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 12:55 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 12:55 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 12:55 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 12:55 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 12:55 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 12:55 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 12:55 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 12:55 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 12:55 PM
Page 15 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:20:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-07A Matrix:Groundwater
MW-15 DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 12:55 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 12:55 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 12:55 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 12:55 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 12:55 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 12:55 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 12:55 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 12:55 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 12:55 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 12:55 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 12:55 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 12:55 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 12:55 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 12:55 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 12:55 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 12:55 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 12:55 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 12:55 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 12:55 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 12:55 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 12:55 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 12:55 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 12:55 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 12:55 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 12:55 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 12:55 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 12:55 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 12:55 PM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 3/28/2015 12:55 PM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 3/28/2015 12:55 PM
Surr: Dibromofluoromethane 99.3 74.3-124 %RECNANA 3/28/2015 12:55 PM
Surr: Toluene-d8 98.8 71.4-129 %RECNANA 3/28/2015 12:55 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 4.0 5.0 J mg/L1.0 NA PA/VA3/27/2015 1:23 PM
Page 16 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:00:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-08A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 2:37 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 2:37 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 2:37 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 2:37 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 2:37 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 2:37 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 2:37 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 2:37 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 2:37 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 2:37 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 2:37 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 2:37 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 2:37 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 2:37 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 2:37 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 2:37 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 2:37 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 2:37 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 2:37 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 2:37 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 2:37 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 2:37 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 2:37 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 2:37 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 2:37 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 2:37 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 2:37 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 2:37 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 2:37 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 2:37 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 2:37 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 2:37 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 2:37 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 2:37 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 2:37 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 2:37 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 2:37 PM
Page 17 of 18
WO#: 1503V10
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:00:00 AM
Project:BLACKBURN SUBTITLE D - 1SA 2015
Lab ID:1503V10-08A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 2:37 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 2:37 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 2:37 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 2:37 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 2:37 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 2:37 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 2:37 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 2:37 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 2:37 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 2:37 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 2:37 PM
Surr: 1,2-Dichloroethane-d4 102 68.7-129 %RECNANA 3/28/2015 2:37 PM
Surr: 4-Bromofluorobenzene 113 71.8-127 %RECNANA 3/28/2015 2:37 PM
Surr: Dibromofluoromethane 97.3 74.3-124 %RECNANA 3/28/2015 2:37 PM
Surr: Toluene-d8 98.3 71.4-129 %RECNANA 3/28/2015 2:37 PM
Page 18 of 18
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
Unit 3
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver, WV 25813 800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Tuesday, April 07, 2015
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:UNIT 3 - 1SA 2015
Work Order #:1503V11
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 8 sample(s) on 3/26/2015 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Case Narrative
Client:
Project:UNIT 3 - 1SA 2015
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 10:56:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-01A Matrix:Groundwater
MW-31Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0003 0.0060 J mg/L0.0002 NA PA/VA4/2/2015 2:43 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Barium 0.520 0.100 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Beryllium 0.0004 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 2:43 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:43 PM
Chromium 0.0428 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Cobalt 0.0151 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Copper 0.0665 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Lead 0.0041 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 2:43 PM
Nickel 0.0257 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 2:43 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 2:43 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Thallium 0.0002 0.0055 J mg/L0.0002 NA PA/VA4/2/2015 2:43 PM
Vanadium 0.0488 0.0250 mg/L0.0010 NA PA/VA4/2/2015 2:43 PM
Zinc 0.0279 0.0100 mg/L0.0030 NA PA/VA4/2/2015 2:43 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/27/2015 8:27 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/27/2015 8:27 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/27/2015 8:27 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/27/2015 8:27 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/27/2015 8:27 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/27/2015 8:27 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/27/2015 8:27 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/27/2015 8:27 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/27/2015 8:27 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/27/2015 8:27 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/27/2015 8:27 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/27/2015 8:27 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/27/2015 8:27 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/27/2015 8:27 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/27/2015 8:27 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/27/2015 8:27 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/27/2015 8:27 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/27/2015 8:27 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/27/2015 8:27 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/27/2015 8:27 PM
Page 3 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 10:56:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-01A Matrix:Groundwater
MW-31Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/27/2015 8:27 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/27/2015 8:27 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/27/2015 8:27 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/27/2015 8:27 PM
cis-1,2-Dichloroethene 0.570 5.00 J µg/L0.226 NA PA/VA3/27/2015 8:27 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/27/2015 8:27 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/27/2015 8:27 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/27/2015 8:27 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/27/2015 8:27 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/27/2015 8:27 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/27/2015 8:27 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/27/2015 8:27 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/27/2015 8:27 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/27/2015 8:27 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/27/2015 8:27 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/27/2015 8:27 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/27/2015 8:27 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/27/2015 8:27 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/27/2015 8:27 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/27/2015 8:27 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/27/2015 8:27 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/27/2015 8:27 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/27/2015 8:27 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/27/2015 8:27 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/27/2015 8:27 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/27/2015 8:27 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/27/2015 8:27 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/27/2015 8:27 PM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 3/27/2015 8:27 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 3/27/2015 8:27 PM
Surr: Dibromofluoromethane 98.5 74.3-124 %RECNANA 3/27/2015 8:27 PM
Surr: Toluene-d8 96.6 71.4-129 %RECNANA 3/27/2015 8:27 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 289 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 4 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:34:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-02A Matrix:Groundwater
MW-32Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 2:48 PM
Arsenic 0.0011 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Barium 0.329 0.100 mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Beryllium 0.0009 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 2:48 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:48 PM
Chromium 0.0298 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Cobalt 0.0116 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Copper 0.0142 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Lead 0.0062 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 2:48 PM
Nickel 0.0076 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 2:48 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 2:48 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 2:48 PM
Vanadium 0.0740 0.0250 mg/L0.0010 NA PA/VA4/2/2015 2:48 PM
Zinc 0.0235 0.0100 mg/L0.0030 NA PA/VA4/3/2015 2:20 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 5:20 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/29/2015 5:20 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/29/2015 5:20 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/29/2015 5:20 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/29/2015 5:20 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/29/2015 5:20 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/29/2015 5:20 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/29/2015 5:20 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/29/2015 5:20 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/29/2015 5:20 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:20 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/29/2015 5:20 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/29/2015 5:20 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/29/2015 5:20 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/29/2015 5:20 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/29/2015 5:20 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/29/2015 5:20 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/29/2015 5:20 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/29/2015 5:20 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/29/2015 5:20 PM
Page 5 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:34:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-02A Matrix:Groundwater
MW-32Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/29/2015 5:20 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/29/2015 5:20 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 5:20 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/29/2015 5:20 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/29/2015 5:20 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/29/2015 5:20 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/29/2015 5:20 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/29/2015 5:20 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/29/2015 5:20 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/29/2015 5:20 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/29/2015 5:20 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/29/2015 5:20 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/29/2015 5:20 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/29/2015 5:20 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/29/2015 5:20 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/29/2015 5:20 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/29/2015 5:20 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/29/2015 5:20 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/29/2015 5:20 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/29/2015 5:20 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/29/2015 5:20 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/29/2015 5:20 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/29/2015 5:20 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/29/2015 5:20 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/29/2015 5:20 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/29/2015 5:20 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/29/2015 5:20 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/29/2015 5:20 PM
Surr: 1,2-Dichloroethane-d4 96.3 68.7-129 %RECNANA 3/29/2015 5:20 PM
Surr: 4-Bromofluorobenzene 123 71.8-127 %RECNANA 3/29/2015 5:20 PM
Surr: Dibromofluoromethane 96.1 74.3-124 %RECNANA 3/29/2015 5:20 PM
Surr: Toluene-d8 107 71.4-129 %RECNANA 3/29/2015 5:20 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 363 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 6 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:57:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-03A Matrix:Groundwater
MW-33Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 2:54 PM
Arsenic 0.0051 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Barium 0.726 0.100 mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Beryllium 0.0031 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:54 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:54 PM
Chromium 0.0440 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Cobalt 0.0374 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Copper 0.0281 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Lead 0.0170 0.0100 mg/L0.0002 NA PA/VA4/2/2015 2:54 PM
Nickel 0.0170 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 2:54 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 2:54 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Thallium 0.0002 0.0055 J mg/L0.0002 NA PA/VA4/2/2015 2:54 PM
Vanadium 0.257 0.0250 mg/L0.0010 NA PA/VA4/2/2015 2:54 PM
Zinc 0.0607 0.0100 mg/L0.0030 NA PA/VA4/2/2015 2:54 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 5:53 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/29/2015 5:53 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/29/2015 5:53 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/29/2015 5:53 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/29/2015 5:53 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/29/2015 5:53 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/29/2015 5:53 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/29/2015 5:53 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/29/2015 5:53 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/29/2015 5:53 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:53 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/29/2015 5:53 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/29/2015 5:53 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/29/2015 5:53 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/29/2015 5:53 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/29/2015 5:53 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/29/2015 5:53 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/29/2015 5:53 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/29/2015 5:53 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/29/2015 5:53 PM
Page 7 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:57:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-03A Matrix:Groundwater
MW-33Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/29/2015 5:53 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/29/2015 5:53 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 5:53 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/29/2015 5:53 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/29/2015 5:53 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/29/2015 5:53 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/29/2015 5:53 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/29/2015 5:53 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/29/2015 5:53 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/29/2015 5:53 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/29/2015 5:53 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/29/2015 5:53 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/29/2015 5:53 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/29/2015 5:53 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/29/2015 5:53 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/29/2015 5:53 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/29/2015 5:53 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/29/2015 5:53 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/29/2015 5:53 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/29/2015 5:53 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/29/2015 5:53 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/29/2015 5:53 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/29/2015 5:53 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/29/2015 5:53 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/29/2015 5:53 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/29/2015 5:53 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/29/2015 5:53 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/29/2015 5:53 PM
Surr: 1,2-Dichloroethane-d4 98.7 68.7-129 %RECNANA 3/29/2015 5:53 PM
Surr: 4-Bromofluorobenzene 126 71.8-127 %RECNANA 3/29/2015 5:53 PM
Surr: Dibromofluoromethane 92.8 74.3-124 %RECNANA 3/29/2015 5:53 PM
Surr: Toluene-d8 107 71.4-129 %RECNANA 3/29/2015 5:53 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 1,180 20.0 mg/L4.0 NA PA/VA3/27/2015 1:23 PM
Page 8 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:22:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-04A Matrix:Groundwater
MW-34Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 2:59 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Barium 0.119 0.100 mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:59 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 2:59 PM
Chromium 0.0180 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Cobalt 0.0040 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Copper 0.0108 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Lead 0.0010 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 2:59 PM
Nickel 0.0079 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 2:59 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 2:59 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 2:59 PM
Vanadium 0.0181 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 2:59 PM
Zinc 0.0134 0.0100 mg/L0.0030 NA PA/VA4/3/2015 2:26 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 6:27 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/29/2015 6:27 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/29/2015 6:27 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/29/2015 6:27 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/29/2015 6:27 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/29/2015 6:27 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/29/2015 6:27 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/29/2015 6:27 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/29/2015 6:27 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/29/2015 6:27 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:27 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/29/2015 6:27 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/29/2015 6:27 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/29/2015 6:27 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/29/2015 6:27 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/29/2015 6:27 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/29/2015 6:27 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/29/2015 6:27 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/29/2015 6:27 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/29/2015 6:27 PM
Page 9 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:22:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-04A Matrix:Groundwater
MW-34Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/29/2015 6:27 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/29/2015 6:27 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 6:27 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/29/2015 6:27 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/29/2015 6:27 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/29/2015 6:27 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/29/2015 6:27 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/29/2015 6:27 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/29/2015 6:27 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/29/2015 6:27 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/29/2015 6:27 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/29/2015 6:27 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/29/2015 6:27 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/29/2015 6:27 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/29/2015 6:27 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/29/2015 6:27 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/29/2015 6:27 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/29/2015 6:27 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/29/2015 6:27 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/29/2015 6:27 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/29/2015 6:27 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/29/2015 6:27 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/29/2015 6:27 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/29/2015 6:27 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/29/2015 6:27 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/29/2015 6:27 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/29/2015 6:27 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/29/2015 6:27 PM
Surr: 1,2-Dichloroethane-d4 94.5 68.7-129 %RECNANA 3/29/2015 6:27 PM
Surr: 4-Bromofluorobenzene 125 71.8-127 %RECNANA 3/29/2015 6:27 PM
Surr: Dibromofluoromethane 94.7 74.3-124 %RECNANA 3/29/2015 6:27 PM
Surr: Toluene-d8 105 71.4-129 %RECNANA 3/29/2015 6:27 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 200 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 10 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:52:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-05A Matrix:Groundwater
SW-4Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 3:05 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Barium 0.0339 0.100 J mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:05 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:05 PM
Chromium 0.0014 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Copper 0.0013 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/2/2015 3:05 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/2/2015 3:05 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 3:05 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 3:05 PM
Vanadium 0.0010 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 3:05 PM
Zinc 0.0049 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 3:05 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 7:01 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/29/2015 7:01 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/29/2015 7:01 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/29/2015 7:01 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/29/2015 7:01 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/29/2015 7:01 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/29/2015 7:01 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/29/2015 7:01 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/29/2015 7:01 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/29/2015 7:01 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:01 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/29/2015 7:01 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/29/2015 7:01 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/29/2015 7:01 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/29/2015 7:01 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/29/2015 7:01 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/29/2015 7:01 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/29/2015 7:01 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/29/2015 7:01 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/29/2015 7:01 PM
Page 11 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:52:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-05A Matrix:Groundwater
SW-4Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/29/2015 7:01 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/29/2015 7:01 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 7:01 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/29/2015 7:01 PM
cis-1,2-Dichloroethene 0.500 5.00 J µg/L0.226 NA PA/VA3/29/2015 7:01 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/29/2015 7:01 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/29/2015 7:01 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/29/2015 7:01 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/29/2015 7:01 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/29/2015 7:01 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/29/2015 7:01 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/29/2015 7:01 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/29/2015 7:01 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/29/2015 7:01 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/29/2015 7:01 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/29/2015 7:01 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/29/2015 7:01 PM
Tetrachloroethene 1.74 1.00 µg/L0.196 NA PA/VA3/29/2015 7:01 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/29/2015 7:01 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/29/2015 7:01 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/29/2015 7:01 PM
Trichloroethene 0.860 1.00 J µg/L0.302 NA PA/VA3/29/2015 7:01 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/29/2015 7:01 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/29/2015 7:01 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/29/2015 7:01 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/29/2015 7:01 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/29/2015 7:01 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/29/2015 7:01 PM
Surr: 1,2-Dichloroethane-d4 95.0 68.7-129 %RECNANA 3/29/2015 7:01 PM
Surr: 4-Bromofluorobenzene 117 71.8-127 %RECNANA 3/29/2015 7:01 PM
Surr: Dibromofluoromethane 93.7 74.3-124 %RECNANA 3/29/2015 7:01 PM
Surr: Toluene-d8 105 71.4-129 %RECNANA 3/29/2015 7:01 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids ND 5.0 mg/L1.0 NA PA/VA3/27/2015 1:23 PM
Page 12 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 1:02:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-06A Matrix:Groundwater
SW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 3:11 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Barium 0.0632 0.100 J mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:11 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:11 PM
Chromium 0.0050 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Cobalt 0.0019 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Copper 0.0024 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Lead 0.0007 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 3:11 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/2/2015 3:11 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 3:11 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 3:11 PM
Vanadium 0.0081 0.0250 J mg/L0.0010 NA PA/VA4/2/2015 3:11 PM
Zinc 0.0059 0.0100 J mg/L0.0030 NA PA/VA4/2/2015 3:11 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 7:35 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/29/2015 7:35 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/29/2015 7:35 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/29/2015 7:35 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/29/2015 7:35 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/29/2015 7:35 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/29/2015 7:35 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/29/2015 7:35 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/29/2015 7:35 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/29/2015 7:35 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:35 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/29/2015 7:35 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/29/2015 7:35 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/29/2015 7:35 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/29/2015 7:35 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/29/2015 7:35 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/29/2015 7:35 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/29/2015 7:35 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/29/2015 7:35 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/29/2015 7:35 PM
Page 13 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 1:02:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-06A Matrix:Groundwater
SW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/29/2015 7:35 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/29/2015 7:35 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 7:35 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/29/2015 7:35 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/29/2015 7:35 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/29/2015 7:35 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/29/2015 7:35 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/29/2015 7:35 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/29/2015 7:35 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/29/2015 7:35 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/29/2015 7:35 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/29/2015 7:35 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/29/2015 7:35 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/29/2015 7:35 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/29/2015 7:35 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/29/2015 7:35 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/29/2015 7:35 PM
Tetrachloroethene 0.700 1.00 J µg/L0.196 NA PA/VA3/29/2015 7:35 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/29/2015 7:35 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/29/2015 7:35 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/29/2015 7:35 PM
Trichloroethene 1.02 1.00 µg/L0.302 NA PA/VA3/29/2015 7:35 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/29/2015 7:35 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/29/2015 7:35 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/29/2015 7:35 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/29/2015 7:35 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/29/2015 7:35 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/29/2015 7:35 PM
Surr: 1,2-Dichloroethane-d4 99.8 68.7-129 %RECNANA 3/29/2015 7:35 PM
Surr: 4-Bromofluorobenzene 120 71.8-127 %RECNANA 3/29/2015 7:35 PM
Surr: Dibromofluoromethane 95.2 74.3-124 %RECNANA 3/29/2015 7:35 PM
Surr: Toluene-d8 105 71.4-129 %RECNANA 3/29/2015 7:35 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 30.0 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 14 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:22:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-07A Matrix:Groundwater
MW-34 DUPLICATE MS/MSDClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/2/2015 3:16 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Barium 0.174 0.100 mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Beryllium 0.0003 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 3:16 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:16 PM
Chromium 0.0256 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Cobalt 0.0062 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Copper 0.0166 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Lead 0.0017 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 3:16 PM
Nickel 0.0119 0.0500 J mg/L0.0020 NA PA/VA4/2/2015 3:16 PM
Selenium ND 0.0100 mg/L0.0050 NA PA/VA4/2/2015 3:16 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/2/2015 3:16 PM
Vanadium 0.0276 0.0250 mg/L0.0010 NA PA/VA4/2/2015 3:16 PM
Zinc 0.0197 0.0100 mg/L0.0030 NA PA/VA4/3/2015 2:58 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 8:09 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/29/2015 8:09 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/29/2015 8:09 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/29/2015 8:09 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/29/2015 8:09 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/29/2015 8:09 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/29/2015 8:09 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/29/2015 8:09 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/29/2015 8:09 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/29/2015 8:09 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:09 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/29/2015 8:09 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/29/2015 8:09 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/29/2015 8:09 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/29/2015 8:09 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/29/2015 8:09 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/29/2015 8:09 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/29/2015 8:09 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/29/2015 8:09 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/29/2015 8:09 PM
Page 15 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:22:00 PM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-07A Matrix:Groundwater
MW-34 DUPLICATE MS/MSDClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/29/2015 8:09 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/29/2015 8:09 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 8:09 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/29/2015 8:09 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/29/2015 8:09 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/29/2015 8:09 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/29/2015 8:09 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/29/2015 8:09 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/29/2015 8:09 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/29/2015 8:09 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/29/2015 8:09 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/29/2015 8:09 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/29/2015 8:09 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/29/2015 8:09 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/29/2015 8:09 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/29/2015 8:09 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/29/2015 8:09 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/29/2015 8:09 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/29/2015 8:09 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/29/2015 8:09 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/29/2015 8:09 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/29/2015 8:09 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/29/2015 8:09 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/29/2015 8:09 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/29/2015 8:09 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/29/2015 8:09 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/29/2015 8:09 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/29/2015 8:09 PM
Surr: 1,2-Dichloroethane-d4 95.8 68.7-129 %RECNANA 3/29/2015 8:09 PM
Surr: 4-Bromofluorobenzene 117 71.8-127 %RECNANA 3/29/2015 8:09 PM
Surr: Dibromofluoromethane 93.7 74.3-124 %RECNANA 3/29/2015 8:09 PM
Surr: Toluene-d8 108 71.4-129 %RECNANA 3/29/2015 8:09 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 211 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 16 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:00:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-08A Matrix:Trip Blank
TRIP BLANK #5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 8:56 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 8:56 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 8:56 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/28/2015 8:56 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 8:56 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 8:56 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 8:56 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 8:56 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/28/2015 8:56 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 8:56 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 8:56 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/28/2015 8:56 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 8:56 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 8:56 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 8:56 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 8:56 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 8:56 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 8:56 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 8:56 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 8:56 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/28/2015 8:56 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 8:56 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 8:56 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 8:56 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 8:56 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 8:56 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 8:56 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 8:56 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 8:56 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/28/2015 8:56 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 8:56 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 8:56 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 8:56 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 8:56 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 8:56 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 8:56 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 8:56 AM
Page 17 of 18
WO#: 1503V11
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:00:00 AM
Project:UNIT 3 - 1SA 2015
Lab ID:1503V11-08A Matrix:Trip Blank
TRIP BLANK #5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.CSite ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 8:56 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/28/2015 8:56 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 8:56 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 8:56 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 8:56 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 8:56 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 8:56 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 8:56 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 8:56 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/28/2015 8:56 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/28/2015 8:56 AM
Surr: 1,2-Dichloroethane-d4 108 68.7-129 %RECNANA 3/28/2015 8:56 AM
Surr: 4-Bromofluorobenzene 104 71.8-127 %RECNANA 3/28/2015 8:56 AM
Surr: Dibromofluoromethane 99.6 74.3-124 %RECNANA 3/28/2015 8:56 AM
Surr: Toluene-d8 94.7 71.4-129 %RECNANA 3/28/2015 8:56 AM
Page 18 of 18
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
Leachate
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver, WV 25813 800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Tuesday, April 07, 2015
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:SUBTITLE LEACHATE - 1SA 2015
Work Order #:1503V17
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 1 sample(s) on 3/26/2015 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 6
WO#: 1503V17
Date Reported: 4/7/2015
REI Consultants, Inc. - Case Narrative
Client:
Project:SUBTITLE LEACHATE - 1SA 2015
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 6
WO#: 1503V17
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:45:00 PM
Project:SUBTITLE LEACHATE - 1SA 2015
Lab ID:1503V17-01A Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0043 0.0060 J mg/L0.0002 NA PA/VA4/3/2015 6:19 PM
Arsenic 0.0051 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Barium 0.120 0.100 mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 6:19 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 6:19 PM
Chromium 0.0218 0.0100 mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Cobalt 0.0132 0.0100 mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Copper 0.0064 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Lead 0.0008 0.0100 J mg/L0.0002 NA PA/VA4/3/2015 6:19 PM
Nickel 0.0489 0.0500 J mg/L0.0020 NA PA/VA4/3/2015 6:19 PM
Selenium 0.0013 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 6:19 PM
Vanadium 0.0083 0.0250 J mg/L0.0010 NA PA/VA4/3/2015 6:19 PM
Zinc 0.0817 0.0100 mg/L0.0030 NA PA/VA4/3/2015 6:19 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/28/2015 3:11 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/28/2015 3:11 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/28/2015 3:11 PM
Benzene 2.96 1.00 µg/L0.129 NA PA/VA3/28/2015 3:11 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/28/2015 3:11 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/28/2015 3:11 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/28/2015 3:11 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/28/2015 3:11 PM
2-Butanone 21.8 100 J µg/L4.68 NA PA/VA3/28/2015 3:11 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/28/2015 3:11 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/28/2015 3:11 PM
Chlorobenzene 0.930 3.00 J µg/L0.177 NA PA/VA3/28/2015 3:11 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/28/2015 3:11 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/28/2015 3:11 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/28/2015 3:11 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/28/2015 3:11 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/28/2015 3:11 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/28/2015 3:11 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/28/2015 3:11 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/28/2015 3:11 PM
Page 3 of 6
WO#: 1503V17
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:45:00 PM
Project:SUBTITLE LEACHATE - 1SA 2015
Lab ID:1503V17-01A Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
1,4-Dichlorobenzene 2.38 1.00 µg/L0.287 NA PA/VA3/28/2015 3:11 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/28/2015 3:11 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/28/2015 3:11 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/28/2015 3:11 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/28/2015 3:11 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/28/2015 3:11 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/28/2015 3:11 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/28/2015 3:11 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/28/2015 3:11 PM
Ethylbenzene 8.79 1.00 µg/L0.178 NA PA/VA3/28/2015 3:11 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/28/2015 3:11 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/28/2015 3:11 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/28/2015 3:11 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/28/2015 3:11 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/28/2015 3:11 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/28/2015 3:11 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/28/2015 3:11 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/28/2015 3:11 PM
Toluene 1.23 1.00 µg/L0.167 NA PA/VA3/28/2015 3:11 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/28/2015 3:11 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/28/2015 3:11 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/28/2015 3:11 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/28/2015 3:11 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/28/2015 3:11 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/28/2015 3:11 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/28/2015 3:11 PM
o-Xylene 3.12 1.00 µg/L0.186 NA PA/VA3/28/2015 3:11 PM
m,p-Xylene 6.72 2.00 µg/L0.287 NA PA/VA3/28/2015 3:11 PM
Surr: 1,2-Dichloroethane-d4 100 68.7-129 %RECNANA 3/28/2015 3:11 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 3/28/2015 3:11 PM
Surr: Dibromofluoromethane 99.8 74.3-124 %RECNANA 3/28/2015 3:11 PM
Surr: Toluene-d8 98.3 71.4-129 %RECNANA 3/28/2015 3:11 PM
BOD, 5 Day, 20°C Method: SM5210 B-2001 Analyst: CB
Biochemical Oxygen Demand 27 5 mg/L2NA PA/VA3/26/2015 4:32 PM
Chemical Oxygen Demand Method: EPA 410.4, Rev. 2
(1993)
Analyst: SF
Chemical Oxygen Demand 298 50 mg/L20NA PA/VA3/27/2015 7:46 AM
Page 4 of 6
WO#: 1503V17
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:45:00 PM
Project:SUBTITLE LEACHATE - 1SA 2015
Lab ID:1503V17-01A Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
ANIONS by ION CHROMATOGRAPHY Method: EPA 300.0, Rev.2.1
(1993)
Analyst: CF
Sulfate 6.52 5.00 mg/L1.00 NA 3/26/2015 9:11 PM
ANIONS by ION CHROMATOGRAPHY-48 HOUR Method: EPA 300.0, Rev.2.1
(1993)
Analyst: CF
Nitrogen, Nitrate 0.05 0.10 J mg/L0.02 NA 3/26/2015 3:42 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 60.0 20.0 mg/L4.0 NA PA/VA3/27/2015 2:25 PM
Page 5 of 6
WO#: 1503V17
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:45:00 PM
Project:SUBTITLE LEACHATE - 1SA 2015
Lab ID:1503V17-01B Matrix:Waste Water
LEACHATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
DISSOLVED ANIONS by ION
CHROMATOGRAPHY
Method: EPA 300.0, Rev.2.1
(1993)
Analyst: CF
Orthophosphate (As P)ND 0.10 mg/L0.05 NA 3/26/2015 4:05 PM
Page 6 of 6
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Subtitle D
AppendixB7:
FieldSamplingSummaries
and
FieldSampleLogs
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Unit 2
FieldSamplingSummaries
and
FieldSampleLogs
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Lt.RainandCloudy52-55°F
Property Units MW-12 MW-13 MW-14 MW-15
SamplingDepth Feet 20.03 7.18 6.69 4.03
StaticDepth Feet 16.19 6.04 6.01 3.88
WellDepth Feet 22.95 18.60 14.60 14.50
WaterColumnHeight Feet 6.76 12.56 8.59 10.62
VolumePurged Liters 24 22 15 20
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-12 MW-13 MW-14 MW-15
pH SU 5.81 5.83 5.91 6.04Dup6.03
Temperature oC 17.1 12.6 11.8 12.2Dup12.2
Conductivity umhos/cm 271 139 242 87.7Dup87.5
Turbidity NTU 4.52 102 25.0 7.62Dup7.67
Appearance -Clear Cloudy Cloudy Clear
Odor -Slight Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 16 69 11.5 10.5
Property Units MW-16 MW-17
SamplingDepth Feet 7.49 17.26
StaticDepth Feet 6.79 7.25
WellDepth Feet 21.77 20.60
WaterColumnHeight Feet 14.98 13.35
VolumePurged Liters 26 10
PurgingStatus -FinishedPurging PurgedDry
PhysicalProperty Units MW-16 MW-17
pH SU 5.77 5.52
Temperature oC 13.7 13.5
Conductivity umhos/cm 102 60.2
Turbidity NTU 200 82.9
Appearance -Cloudy Cloudy
Odor -No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 74 97
SAMPLING LOG SUMMARY
CountyofCatawba
1504V11
3/25/2015
SubtitleD-Unit2(Permit:#18-03)
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 2
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Lt.RainandCloudy52-55°F
SAMPLING LOG SUMMARY
CountyofCatawba
1504V11
3/25/2015
SubtitleD-Unit2(Permit:#18-03)
Property Units U-1 U-2 U-3 Leachate
SamplingDepth Feet ----
StaticDepth Feet ----
WellDepth Feet ----
WaterColumnHeight Feet ----
VolumePurged Liters ----
PurgingStatus -----
PhysicalProperty Units U-1 U-2 U-3 Leachate
pH SU ---7.21
Temperature oC ---26.3
Conductivity umhos/cm ---4390
Turbidity NTU ---25.5
Appearance ----Lt. Gray
Odor ----Strong Odor
TotalSuspendedSolids(TSS)mg/L ---60
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 3
ProjectName:Project :Well#:MW-12
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 52 °F
16.19 (Ft)3.91 (Liters)
22.95 (Ft)11.74 (Liters)
6.76 (Ft)24.00 (Liters)
pH
Time (SU)
09:37 6.11
09:39 6.22
09:41 6.17
09:43 6.04
09:44 6.00
09:46 5.96
09:47
Date:Time:09:50
Method:SamplingDepth:20.03'
pH:5.81 (SU)Conductivity:271 (umhos/cm)
Temperature:17.1 (o C)Turbidity:4.52 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 1stSemi2015
RodneyHamby 704-462-1348
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELLCONDITIONDATA
PURGINGDATA
Cap onWellRiser 2"PVCCasing
3/25/201509:32 WeatherConditions:
StaticDepth(DepthtoWater)Volume
WaterColumnHeight VolumePurged
WellDepth 3Volumes
VolumePurged
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity
481.0 16.1 16.01 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
495.0 16.8 23.00 4
364.0 17.1 14.81 12
444.0 17.0 19.72 8
338.0 17.2 11.72 16
FinishedPurging 24
312.0 17.3 11.73 20
PHYSICALCHARACTERISTICSOFSAMPLE
TeflonBailer
SAMPLINGDATA
3/25/2015
Appearance:Clear Odor:SlightOdor
3/25/2015
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 4
ProjectName:Project :Well#:MW-13
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 55 °F
6.04 (Ft)7.27 (Liters)
18.60 (Ft)21.81 (Liters)
12.56 (Ft)22.00 (Liters)
pH
Time (SU)
09:00 6.19
09:01 6.14
09:02 6.04
09:03 6.00
09:04 5.88
09:05 5.87
09:06
Date:Time:09:08
Method:SamplingDepth:7.18'
pH:5.83 (SU)Conductivity:139.3 (umhos/cm)
Temperature:12.6 (o C)Turbidity:102 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
1stSemi2015BlackburnSubtitleD-Unit 2
WELLCONDITIONDATA
RodneyHamby 704-462-1348
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
WeatherConditions:
Volume
2"PVCCasing
PURGINGDATA
Cap onWellRiser
3/25/201508:56
StaticDepth(DepthtoWater)
WaterColumnHeight
WellDepth
VolumePurged
3Volumes
TemperatureCorrected Temperature
EVACUATION/STABILIZATIONTESTDATA
(NTU)(Liters)
Turbidity
Conductivity(umhos/cm)
VolumePurged
(oC)
89.1 11.0
89.8 42.5 4
6.67 1
11.3
12.1 160
129.5 12.3
8
117 12
108.8
16143.0 12.5 97.4
137 20
22FinishedPurging
147.8 12.5
PHYSICALCHARACTERISTICSOFSAMPLE
TeflonBailer
SAMPLINGDATA
3/25/2015
NoOdorAppearance:Cloudy Odor:
3/25/2015
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 5
ProjectName:Project :Well#:MW-14
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 55 °F
6.01 (Ft)4.97 (Liters)
14.60 (Ft)14.92 (Liters)
8.59 (Ft)15.00 (Liters)
pH
Time (SU)
08:39 5.86
08:40 5.90
08:42 5.98
08:43 5.89
08:44 5.89
08:46 5.92
08:46
Date:Time:08:49
Method:SamplingDepth:6.69'
pH:5.91 (SU)Conductivity:242 (umhos/cm)
Temperature:11.8 (o C)Turbidity:25 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 1stSemi2015
WELLCONDITIONDATA
RodneyHamby
ProtectiveCasingPresent PhysicalDamage
704-462-1348
StaticDepth(DepthtoWater)Volume
Cap onWellRiser
ProtectiveCasingLocked Concrete/GroutPadPresent
3/25/201508:37 WeatherConditions:
PURGINGDATA
2"PVCCasing
WaterColumnHeight VolumePurged
WellDepth 3Volumes
EVACUATION/STABILIZATIONTESTDATA
VolumePurgedTurbidityTemperatureCorrected
(NTU)
Temperature
(Liters)Conductivity(umhos/cm)(oC)
11.8 11.51252.0
252.0
11.6 109
311.6 >800
247.0
245.0
11.7 55.9
6
9
243.0 11.7 59.8 12
244.0 11.8 33.5 15
15FinishedPurging
SAMPLINGDATA
PHYSICALCHARACTERISTICSOFSAMPLE
TeflonBailer
3/25/2015
Appearance:Cloudy Odor:NoOdor
3/25/2015
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 6
ProjectName:Project :Well#:MW-15
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 54 °F
3.88 (Ft)6.14 (Liters)
14.50 (Ft)18.44 (Liters)
10.62 (Ft)20.00 (Liters)
pH
Time (SU)
08:12 6.11
08:13 6.07
08:14 6.04
08:16 6.05
08:17 6.02
08:18 6.04
08:18
Date:Time:08:20
Method:SamplingDepth:4.03'
pH:6.04Dup6.03 (SU)Conductivity:87.7Dup87.5 (umhos/cm)
Temperature:12.2Dup12.2 (o C)Turbidity:7.62Dup7.67 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 1stSemi2015
ProtectiveCasingPresent PhysicalDamage
704-462-1348RodneyHamby
Concrete/GroutPadPresent
WELLCONDITIONDATA
Cap onWellRiser 2"PVCCasing
ProtectiveCasingLocked
3/25/201508:09 WeatherConditions:
Volume
PURGINGDATA
StaticDepth(DepthtoWater)
WaterColumnHeight VolumePurged
WellDepth 3Volumes
Temperature Turbidity
EVACUATION/STABILIZATIONTESTDATA
VolumePurgedTemperatureCorrected
Conductivity(umhos/cm)(oC)(NTU)(Liters)
81.3 12.3 13.52
7.39 481.0
8
12.0
82.4 12.1 6.83
10.14
85.9
1284.6 12.1
1612.1 11.77
12.1 14.3586.6 20
FinishedPurging
SAMPLINGDATA
PHYSICALCHARACTERISTICSOFSAMPLE
20
TeflonBailer
3/25/2015
Clear Odor:Appearance:NoOdor
3/25/2015
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 7
ProjectName:Project :Well#:MW-16
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 54 °F
6.79 (Ft)8.67 (Liters)
21.77 (Ft)26.02 (Liters)
14.98 (Ft)26.00 (Liters)
pH
Time (SU)
07:51 5.71
07:52 5.68
07:54 5.72
07:55 5.74
07:57 5.75
07:58 5.73
07:58
Date:Time:08:00
Method:SamplingDepth:7.49'
pH:5.77 (SU)Conductivity:101.5 (umhos/cm)
Temperature:13.7 (o C)Turbidity:200 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 1stSemi2015
RodneyHamby 704-462-1348
WELLCONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked
PURGINGDATA
Volume
3/25/201507:47
Concrete/GroutPadPresent
2"PVCCasingCap onWellRiser
WeatherConditions:
WellDepth
WaterColumnHeight
StaticDepth(DepthtoWater)
VolumePurged
3Volumes
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity VolumePurged
(oC)(NTU)(Liters)
94.8 12.3 3.14 1
Conductivity(umhos/cm)
91.7 29.8 5
15
12.6
93.0 13.1 87.1 10
94.7 13.3 159
215 2013.393.2
13.4 270 2594.2
3/25/2015
SAMPLINGDATA
PHYSICALCHARACTERISTICSOFSAMPLE
TeflonBailer
FinishedPurging 26
Cloudy NoOdorAppearance:
3/25/2015
Odor:
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 8
ProjectName:Project :Well#:MW-17
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 54 °F
7.25 (Ft)7.72 (Liters)
20.60 (Ft)23.18 (Liters)
13.35 (Ft)10.00 (Liters)
pH
Time (SU)
07:27 5.09
07:29 4.84
07:30 4.96
07:31
Date:Time:07:39
Method:SamplingDepth:17.26'
pH:5.52 (SU)Conductivity:60.2 (umhos/cm)
Temperature:13.5 (o C)Turbidity:82.9 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 2 1stSemi2015
PhysicalDamage
WELLCONDITIONDATA
ProtectiveCasingPresent
704-462-1348RodneyHamby
Volume
PURGINGDATA
StaticDepth(DepthtoWater)
2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
Cap onWellRiser
3/25/201507:22
3Volumes
VolumePurgedWaterColumnHeight
WeatherConditions:
WellDepth
TemperatureCorrected Temperature Turbidity
EVACUATION/STABILIZATIONTESTDATA
VolumePurged
(Liters)Conductivity(umhos/cm)(oC)(NTU)
176.3 12.7 53.8
12.5 51072.4
870.4 13.4 >800
4
PHYSICALCHARACTERISTICSOFSAMPLE
SAMPLINGDATA
TeflonBailer
10PurgedDry
3/25/2015
3/25/2015
NoOdorOdor:Appearance:Cloudy
RandyFarley/AllenMcBride/RickyTalley/J.D.Bennett
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 9
Outlet:
Date:08:08
pH:Conductivity:umhos/cm
Flow:NoFlow Temperature:o C
/
Turbidity=NTU
Outlet:
Date:07:59
pH:Conductivity:umhos/cm
Flow:NoFlow Temperature:o C
/
Turbidity=NTU
Outlet:
Date:07:35
pH:Conductivity:umhos/cm
Flow:NoFlow Temperature:o C
/
Turbidity=NTU
Time:
SampleOdorand PhysicalAppearance:
Comments:
U-3
U-2
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnSubtitleD-Unit 2
SampleOdorand PhysicalAppearance:
Contact Person:RodneyHamby Phone/Fax:
U-1
704-462-1348
3/25/2015 Time:
Comments:
3/25/2015
SampleOdorand PhysicalAppearance:
3/25/2015 Time:
Comments:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page10
Outlet:
Date:12:45
pH:7.21 Conductivity:4390 umhos/cm
Flow:N/A Temperature:26.3 o C
Lt.Gray /StrongOdor
Turbidity=25.5 NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
/
Turbidity=NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
/
Turbidity=NTU
Comments:
SampleOdorand PhysicalAppearance:
Time:
SampleOdorand PhysicalAppearance:
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnSubtitleD-Unit 2
Contact Person:RodneyHamby Phone/Fax:[phone]
Leachate
3/25/2015
Comments:
Time:
SampleOdorand PhysicalAppearance:
Comments:
Time:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page11
Unit 3
FieldSamplingSummaries
and
FieldSampleLogs
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page12
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley
WeatherConditions:RainandLt.Rain48-50°F
Property Units MW-31 MW-32 MW-33 MW-34
SamplingDepth Feet 24.02 24.21 26.31 19.91
StaticDepth Feet 22.35 24.11 20.91 19.58
WellDepth Feet 32.70 32.75 29.75 28.05
WaterColumnHeight Feet 10.35 8.64 8.84 8.47
VolumePurged Liters 20 15 15 15
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-31 MW-32 MW-33 MW-34
pH SU 5.71 5.57 5.77 6.15Dup6.12
Temperature oC 16.0 15.5 16.0 16.0Dup16.0
Conductivity umhos/cm 134 59.5 34.6 56.9Dup57.0
Turbidity NTU 335 >800 >800 437Dup429
Appearance -Cloudy Muddy Muddy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 289 363 1,180 200
Property Units SW-4 SW-5
SamplingDepth Feet --
StaticDepth Feet --
WellDepth Feet --
WaterColumnHeight Feet --
VolumePurged Liters --
PurgingStatus ---
PhysicalProperty Units SW-4 SW-5
pH SU 6.73 6.89
Temperature oC 13.8 13.1
Conductivity umhos/cm 90.4 110.8
Turbidity NTU 7.66 35.1
Appearance -Clear Cloudy
Odor -No Odor No Odor
TotalSuspendedSolids(TSS)mg/L -30
3/25/2015
SAMPLING LOG SUMMARY
CountyofCatawba
SubtitleD-Unit3(Permit:#18-03)
1503V11
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page13
ProjectName:Project :Well#:MW-31
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Rain 50 °F
22.35 (Ft)5.99 (Liters)
32.70 (Ft)17.97 (Liters)
10.35 (Ft)20.00 (Liters)
pH
Time (SU)
10:45 5.77
10:47 5.72
10:48 5.70
10:49 5.70
10:51 5.71
10:53 5.71
10:53
Date:Time:10:56
Method:SamplingDepth:24.02'
pH:5.71 (SU)Conductivity:133.5 (umhos/cm)
Temperature:16.0 (o C)Turbidity:335 (NTU)
Comments:
SampledBy:RandyFarley/AllenMcBride/RickyTalley
Sampler'sSignature:Date:3/25/2015
NoOdor
Conductivity(umhos/cm)
604 12
VolumePurged
FinishedPurging 20
TeflonBailer
PHYSICALCHARACTERISTICSOFSAMPLE
Appearance:Cloudy Odor:
3/25/2015
139.4
8
136.1 16.3
591 16
132.6
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
PURGINGDATA
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity
BlackburnSubtitleD-Unit 3 1stSemi2015
WELLCONDITIONDATA
RodneyHamby 704-462-1348
Cap onWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
134.8 16.3 535 20
138.2 16.3
16.3 460
534 4
(oC)(NTU)(Liters)
SAMPLINGDATA
131.2 15.7 42.2 1
16.1
3/25/201510:40 WeatherConditions:
WellDepth 3Volumes
WaterColumnHeight VolumePurged
StaticDepth(DepthtoWater)Volume
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page14
ProjectName:Project :Well#:MW-32
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Rain 49 °F
24.11 (Ft)5.00 (Liters)
32.75 (Ft)15.00 (Liters)
8.64 (Ft)15.00 (Liters)
pH
Time (SU)
11:21 5.61
11:23 5.49
11:24 5.53
11:25 5.55
11:26 5.60
11:27 5.64
11:27
Date:Time:11:34
Method:SamplingDepth:24.21'
pH:5.57 (SU)Conductivity:59.5 (umhos/cm)
Temperature:15.5 (o C)Turbidity:>800 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
BlackburnSubtitleD-Unit 3 1stSemi2015
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
WELLCONDITIONDATA
RodneyHamby 704-462-1348
Cap onWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
15.6
60.0 15.6
60.4 15.6
60.0
15.460.2
60.2 15.6
Conductivity(umhos/cm)(oC)
63.4 14.8
3/25/201511:17 WeatherConditions:
Temperature
WellDepth 3Volumes
>800
>800
>800
>800
>800
FinishedPurging
PURGINGDATA
TemperatureCorrected VolumePurged
WaterColumnHeight VolumePurged
EVACUATION/STABILIZATIONTESTDATA
StaticDepth(DepthtoWater)Volume
(NTU)(Liters)
Turbidity
11.12 1
3
12
6
9
15
15
3/25/2015
SAMPLINGDATA
Appearance:Muddy
PHYSICALCHARACTERISTICSOFSAMPLE
Odor:NoOdor
TeflonBailer
3/25/2015
RandyFarley/AllenMcBride/RickyTalley
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page15
ProjectName:Project :Well#:MW-33
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 48 °F
20.91 (Ft)5.11 (Liters)
29.75 (Ft)15.35 (Liters)
8.84 (Ft)15.00 (Liters)
pH
Time (SU)
11:48 5.55
11:49 5.57
11:50 5.71
11:51 5.81
11:53 5.83
11:54 5.82
11:54
Date:Time:11:57
Method:SamplingDepth:26.31'
pH:5.77 (SU)Conductivity:34.6 (umhos/cm)
Temperature:16.0 (o C)Turbidity:>800 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
BlackburnSubtitleD-Unit 3 1stSemi2015
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
RodneyHamby 704-462-1348
ProtectiveCasingLocked
Cap onWellRiser 2"PVCCasing
Concrete/GroutPadPresent
WELLCONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
3/25/201411:44 WeatherConditions:
StaticDepth(DepthtoWater)Volume
PURGINGDATA
TemperatureCorrected Temperature
WaterColumnHeight VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
Conductivity(umhos/cm)(oC)
Turbidity VolumePurged
(Liters)(NTU)
33.7 15.3 13.12 1
681 335.9 15.8
37.9
16.2
643.1 16.0 >800
941.0 >800
1516.1 >800
16.2 >800 12
FinishedPurging 15
36.2
3/25/2015
SAMPLINGDATA
PHYSICALCHARACTERISTICSOFSAMPLE
Appearance:Muddy Odor:NoOdor
TeflonBailer
3/25/2015
RandyFarley/AllenMcBride/RickyTalley
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page16
ProjectName:Project :Well#:MW-34
ContactPerson:Phone#:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 50 °F
19.58 (Ft)4.90 (Liters)
28.05 (Ft)14.71 (Liters)
8.47 (Ft)15.00 (Liters)
pH
Time (SU)
12:11 6.05
12:12 6.03
12:13 6.27
12:15 6.58
12:16 5.99
12:18 6.05
12:18
Date:Time:12:22
Method:SamplingDepth:19.91'
pH:6.15Dup6.12 (SU)Conductivity:56.9Dup57.0 (umhos/cm)
Temperature:16.0Dup16.0 (o C)Turbidity:437Dup429 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:
RodneyHamby 704-462-1348
Cap onWellRiser 2"PVCCasing
REICONSULTANTS,INC.GROUNDWATERSAMPLINGLOG
BlackburnSubtitleD-Unit 3 1stSemi2015
WELLCONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
3/25/201512:08 WeatherConditions:
StaticDepth(DepthtoWater)Volume
PURGINGDATA
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
VolumePurged
(NTU)(Liters)
WellDepth 3Volumes
Turbidity
51.8 15.8 74.4 1
16.4
16.4
TemperatureCorrected Temperature
Conductivity(umhos/cm)(oC)
543 6
9
52.8 16.3 378 3
678
53.0
54.1
12
15FinishedPurging
16.4 782
16.4 781 1555.8
54.8
3/25/2015
SAMPLINGDATA
Appearance:Cloudy Odor:NoOdor
PHYSICALCHARACTERISTICSOFSAMPLE
TeflonBailer
3/25/2015
RandyFarley/AllenMcBride/RickyTalley
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page17
Outlet:
Date:12:52
pH:6.73 Conductivity:90.4 umhos/cm
Flow:N/A Temperature:13.8 o C
Clear /NoOdor
Turbidity=7.66 NTU
Outlet:
Date:13:02
pH:6.89 Conductivity:110.8 umhos/cm
Flow:N/A Temperature:13.1 o C
Cloudy /NoOdor
Turbidity=35.1 NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
/
Turbidity=NTU
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnSubtitleD-Unit 3
3/25/2015 Time:
Contact Person:RodneyHamby Phone/Fax:
SW-4
704-462-1348
3/25/2015 Time:
SampleOdorand PhysicalAppearance:
SampleOdorand PhysicalAppearance:
Comments:
SW-5
SampleOdorand PhysicalAppearance:
Comments:
Comments:
Time:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813Phone:[phone] www.reiclabs.com Page18
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Subtitle D
AppendixB8:
HistoricalDataSummary
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-10
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-12
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 8
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-13
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page13
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-14
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page18
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-15
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page23
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-16
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page28
SubtitleD-Unit 2
HistoricalDataSummary
MonitoringWell:MW-17
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page33
SubtitleD-Unit 2
HistoricalDataSummary
Underdrain:U-1
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page38
SubtitleD-Unit 2
HistoricalDataSummary
Underdrain:U-2
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page43
SubtitleD-Unit 2
HistoricalDataSummary
Underdrain:U-3
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page48
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-31
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page53
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-32
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page56
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-33
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page59
SubtitleD-Unit 3
HistoricalDataSummary
MonitoringWell:MW-34
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page62
SubtitleD-Unit 3
HistoricalDataSummary
SurfaceWater:SW-4
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page65
SubtitleD-Unit 3
HistoricalDataSummary
SurfaceWater:SW-5
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page68
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C1:
1stSemi-Annual2015
Summary of Detections
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
P a r a m e t er
G W S
td
1
S W SL
2
M W -5
M W-
5A
M W -6
M W-
6D
M W -7
M W-
11
M W-
20
S W -1
S W -3
P Z-
85
B
P Z-
86
B
1
39
1
<5
<5
<5
21
6
11
3
12
1
<5
<5
-
-
F OO
T NO
T E S:
S PE
CI
A L
NO
T E S:
1
G W S
t d
-
N o rt
h Ca
r o li
na
g r o u nd
w a t e r
s t a n da
r d s (m g /L ).
-O n l y
r es
u lt
s
a b ov
e
S W SL
's
s ho
wn
2
S W S L
- So
li
d
W a s t e S
ec
t i on
L i m i t s
(m g /L)
-A
ll
c on
ce
n tr
a t i on
s d
e t ec
t e d a
b ov
e t h e
G W S
t d a
r e h
i g h li
g h t e d
i n
r e d an
d
b o l d
t e x t.
-A
ll
da
t a r e po
rt
e d
i n
m g /L.
-T r i p
Bl
a nk
r es
u l t s
f o r a
ll
vo
l a t il
e an
a
l y se
s
w e r e
ND
(no
t d
e t ec
t e d ) a
t
t h e
P Q L.
T o t a l
S us
p en
d e d
S o li
d s
(T SS
)
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C2:
Summary of Dissolved Metals and
TotalSuspendedSolid(TSS)
Detections
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
Su
mm
a r y
o f
Di
ss
o lv
e d
Me
t a l s
a nd
T SS
D e t e c ti
o
ns
B l a c kb
u
r n
L
a nd
f il
l
:
C l o s e d
P
o r ti
on
P e r m i t :
#18
-03
R E I C
J o b
N u m b e r :
1 5 03
V 15
S a m p l e
D a t e :
3 -2 0 15
A n t i m o n y ,
D i ss
o l v ed
0 .0 06
A r s e n i c ,
D i ss
o l v ed
0 .01
B a r i um
,
D i ss
o l v ed
0 .1
0 .1 76
0 .1 97
0 .2 34
0 .2 00
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CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C3:
HistoricalSummary ofDetections
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
AppendixC4:
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Friday, April 10, 2015
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:BLACKBURN CLOSED - 1SA 2015
Work Order #:1503V15
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 13 sample(s) on 3/26/2015 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Case Narrative
Client:
Project:BLACKBURN CLOSED - 1SA 2015
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0003 0.0060 J mg/L0.0002 NA PA/VA4/3/2015 4:50 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Barium 0.396 0.100 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Beryllium 0.0004 0.0010 J mg/L0.0002 NA PA/VA4/3/2015 4:50 PM
Cadmium 0.0003 0.0010 J mg/L0.0002 NA PA/VA4/3/2015 4:50 PM
Chromium 0.0316 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Cobalt 0.0054 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Copper 0.0346 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Lead 0.0037 0.0100 J mg/L0.0002 NA PA/VA4/3/2015 4:50 PM
Nickel 0.0073 0.0500 J mg/L0.0020 NA PA/VA4/3/2015 4:50 PM
Selenium 0.0010 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 4:50 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Vanadium 0.0531 0.0250 mg/L0.0010 NA PA/VA4/3/2015 4:50 PM
Zinc 0.0166 0.0100 mg/L0.0030 NA PA/VA4/3/2015 4:50 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:30 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
alpha-BHC ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
beta-BHC ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
delta-BHC ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
gamma-BHC ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
Chlordane ND 0.00512 mg/L0.00256 0.00050 3/31/2015 5:19 PM
4,4´-DDD ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
4,4´-DDE ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
4,4´-DDT ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
Dieldrin ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
Endosulfan I ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
Endosulfan II ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
Endosulfan sulfate ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
Endrin ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
Endrin aldehyde ND 0.000512 mg/L0.000256 0.00010 3/31/2015 5:19 PM
Heptachlor ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
Page 3 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000512 mg/L0.000256 0.00005 3/31/2015 5:19 PM
Methoxychlor ND 0.000512 mg/L0.000256 0.00100 3/31/2015 5:19 PM
Toxaphene ND 0.00512 mg/L0.00256 0.00100 3/31/2015 5:19 PM
Surr: Tetrachloro-m-xylene 99.5 30.6-137 %RECNANA 3/31/2015 5:19 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Aroclor 1221 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Aroclor 1232 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Aroclor 1242 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Aroclor 1248 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Aroclor 1254 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Aroclor 1260 ND 0.00051 mg/L0.00026 NA 3/31/2015 5:19 PM
Surr: Tetrachloro-m-xylene 69.5 23.9-150 %RECNANA 3/31/2015 5:19 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00240 mg/L0.000003 NA 4/8/2015 2:29 PM
2,4,5-TP (Silvex)ND 0.00240 mg/L0.000003 NA 4/8/2015 2:29 PM
2,4-D ND 0.00240 mg/L0.000005 NA 4/8/2015 2:29 PM
Dinoseb ND 0.00120 mg/L0.000005 NA 4/8/2015 2:29 PM
Surr: 2,4-Dichlorophenylacetic acid 44.3 21.8-182 %RECNANA 4/8/2015 2:29 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
1,3-Dinitrobenzene ND 0.0219 mg/L0.0055 NA 3/31/2015 6:52 PM
1,4-Napthoquinone ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
1-Naphthylamine ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
2,6-Dichlorophenol ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
2-Acetylaminofluorene ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
2-Naphthylamine ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
2-Picoline ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
3,3´-Dimethylbenzidine ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
3-Methylcholanthrene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
4-Aminobiphenyl ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
4-Nitroquinoline-1-oxide ND 0.0548 mg/LNANA 3/31/2015 6:52 PM
Page 4 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
7,12-Dimethylbenz(a)anthracene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Acetophenone ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Chlorobenzilate ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Diallate ND 0.0110 mg/L0.0022 NA 3/31/2015 6:52 PM
Dimethoate ND 0.0219 mg/L0.0055 NA 3/31/2015 6:52 PM
Diphenylamine ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Disulfoton ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Ethyl methacrylate ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Ethyl methanesulfonate ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
Famphur ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
Hexachlorophene ND 0.110 mg/LNANA 3/31/2015 6:52 PM
Hexachloropropene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Isodrin ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
Isosafrole ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Kepone ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
Methapyrilene ND 0.110 mg/LNANA 3/31/2015 6:52 PM
Methyl methacrylate ND 0.0329 mg/LNANA 4/4/2015 7:40 PM
Methyl methanesulfonate ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Methyl parathion ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
N-Nitroso-di-n-butylamine ND 0.0110 mg/L0.0022 NA 3/31/2015 6:52 PM
N-Nitrosodiethylamine ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
n-Nitrosomethylethylamine ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
N-Nitrosopiperidine ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
N-Nitrosopyrrolidine ND 0.0110 mg/L0.0022 NA 3/31/2015 6:52 PM
o,o,o-Triethylphosphorothioate ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0219 mg/LNANA 3/31/2015 6:52 PM
o-Toluidine ND 0.0110 mg/L0.0022 NA 3/31/2015 6:52 PM
p-Dimethylaminoazobenzene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
p-Phenylenediamine ND 0.0110 mg/LNANA 4/4/2015 7:40 PM
Parathion ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Pentachlorobenzene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Pentachloronitrobenzene ND 0.0219 mg/L0.0022 NA 3/31/2015 6:52 PM
Phenacetin ND 0.0219 mg/L0.0022 NA 3/31/2015 6:52 PM
Phorate ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Pronamide ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Safrole ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
sym-Trinitrobenzene ND 0.0110 mg/LNANA 3/31/2015 6:52 PM
Page 5 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0110 mg/L0NA PA/VA3/31/2015 6:52 PM
Acenaphthylene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Anthracene ND 0.0110 mg/LNANA PA/VA3/31/2015 6:52 PM
Benzo(a)anthracene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Benzo(a)pyrene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Benzo(b)fluoranthene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Benzo(g,h,i)perylene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Benzo(k)fluoranthene ND 0.0110 mg/L0.0033 NA PA/VA3/31/2015 6:52 PM
Benzyl alcohol ND 0.0219 mg/L0.0022 NA 3/31/2015 6:52 PM
Bis(2-chloroethoxy)methane ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Bis(2-chloroethyl)ether ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Bis(2-chloroisopropyl)ether ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Bis(2-ethylhexyl)phthalate ND 0.0164 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
4-Bromophenyl phenyl ether ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Butyl benzyl phthalate ND 0.0110 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
4-Chloroaniline ND 0.0219 mg/L0.0055 NA 3/31/2015 6:52 PM
4-Chloro-3-methylphenol ND 0.0219 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2-Chloronaphthalene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2-Chlorophenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
4-Chlorophenyl phenyl ether ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Chrysene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
o-Cresol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
m,p-Cresol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Dibenzo(a,h)anthracene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Dibenzofuran ND 0.0110 mg/LNANA PA/VA3/31/2015 6:52 PM
Di-n-butyl phthalate ND 0.0110 mg/LNANA PA/VA3/31/2015 6:52 PM
3,3´-Dichlorobenzidine ND 0.0219 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
2,4-Dichlorophenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Diethyl phthalate ND 6.58 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Dimethyl phthalate ND 0.0110 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
2,4-Dimethylphenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
4,6-Dinitro-2-methylphenol ND 0.0548 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2,4-Dinitrophenol ND 0.0548 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2,4-Dinitrotoluene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2,6-Dinitrotoluene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Di-n-octyl phthalate ND 0.0110 mg/LNANA PA/VA3/31/2015 6:52 PM
Fluoranthene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Fluorene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Page 6 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Hexachlorobutadiene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Hexachlorocyclopentadiene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Hexachloroethane ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Indeno(1,2,3-cd)pyrene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Isophorone ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2-Methylnaphthalene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Naphthalene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2-Nitroaniline ND 0.0548 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
3-Nitroaniline ND 0.0548 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
4-Nitroaniline ND 0.0219 mg/L0.0055 NA PA/VA3/31/2015 6:52 PM
Nitrobenzene ND 0.0110 mg/LNANA PA/VA3/31/2015 6:52 PM
2-Nitrophenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
4-Nitrophenol ND 0.0548 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
N-Nitrosodimethylamine ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
N-Nitrosodiphenylamine ND 0.0110 mg/L0NA PA/VA3/31/2015 6:52 PM
N-Nitrosodi-n-propylamine ND 0.0110 mg/L0NA PA/VA3/31/2015 6:52 PM
Pentachlorophenol ND 0.0274 mg/L0NA PA/VA3/31/2015 6:52 PM
Phenanthrene ND 0.0110 mg/L0NA PA/VA3/31/2015 6:52 PM
Phenol ND 0.0110 mg/L0NA PA/VA3/31/2015 6:52 PM
Pyrene ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2,3,4,6-Tetrachlorophenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
1,2,4-Trichlorobenzene ND 0.0110 mg/L0.0022 NA 3/31/2015 6:52 PM
2,4,5-Trichlorophenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
2,4,6-Trichlorophenol ND 0.0110 mg/L0.0022 NA PA/VA3/31/2015 6:52 PM
Surr: 2-Fluorophenol 38.2 32.9-110 %RECNANA 3/31/2015 6:52 PM
Surr: Phenol-d5 29.7 25.8-110 %RECNANA 3/31/2015 6:52 PM
Surr: 2,4,6-Tribromophenol 69.9 63.8-110 %RECNANA 3/31/2015 6:52 PM
Surr: Nitrobenzene-d5 88.7 61.8-110 %RECNANA 3/31/2015 6:52 PM
Surr: 2-Fluorobiphenyl 76.2 58.6-110 %RECNANA 3/31/2015 6:52 PM
Surr: 4-Terphenyl-d14 75.7 55.1-110 %RECNANA 3/31/2015 6:52 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/30/2015 11:53 PM
Acetone ND 100 µg/L4.88 NA PA/VA3/30/2015 11:53 PM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/30/2015 11:53 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/30/2015 11:53 PM
Benzene 0.890 1.00 J µg/L0.129 NA PA/VA3/30/2015 11:53 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/30/2015 11:53 PM
Page 7 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/30/2015 11:53 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/30/2015 11:53 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/30/2015 11:53 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/30/2015 11:53 PM
Carbon disulfide ND 100 µg/L1.27 NA 3/30/2015 11:53 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/30/2015 11:53 PM
Chlorobenzene 2.43 3.00 J µg/L0.177 NA PA/VA3/30/2015 11:53 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/30/2015 11:53 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/30/2015 11:53 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/30/2015 11:53 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/30/2015 11:53 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/30/2015 11:53 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/30/2015 11:53 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/30/2015 11:53 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/30/2015 11:53 PM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/30/2015 11:53 PM
1,4-Dichlorobenzene 1.88 1.00 µg/L0.287 NA PA/VA3/30/2015 11:53 PM
Dichlorodifluoromethane 3.03 5.00 J µg/L0.714 NA PA/VA3/30/2015 11:53 PM
1,1-Dichloroethane 2.88 5.00 J µg/L0.383 NA PA/VA3/30/2015 11:53 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/30/2015 11:53 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/30/2015 11:53 PM
cis-1,2-Dichloroethene 1.60 5.00 J µg/L0.226 NA PA/VA3/30/2015 11:53 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/30/2015 11:53 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/30/2015 11:53 PM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/30/2015 11:53 PM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/30/2015 11:53 PM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/30/2015 11:53 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/30/2015 11:53 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/30/2015 11:53 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/30/2015 11:53 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/30/2015 11:53 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/30/2015 11:53 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/30/2015 11:53 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/30/2015 11:53 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/30/2015 11:53 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/30/2015 11:53 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/30/2015 11:53 PM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/30/2015 11:53 PM
Page 8 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-01A Matrix:Groundwater
MW-5Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/30/2015 11:53 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/30/2015 11:53 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/30/2015 11:53 PM
Trichloroethene 1.52 1.00 µg/L0.302 NA PA/VA3/30/2015 11:53 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/30/2015 11:53 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/30/2015 11:53 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/30/2015 11:53 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/30/2015 11:53 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/30/2015 11:53 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/30/2015 11:53 PM
Surr: 1,2-Dichloroethane-d4 95.0 68.7-129 %RECNANA 3/30/2015 11:53 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 3/30/2015 11:53 PM
Surr: Dibromofluoromethane 98.5 74.3-124 %RECNANA 3/30/2015 11:53 PM
Surr: Toluene-d8 97.3 71.4-129 %RECNANA 3/30/2015 11:53 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/30/2015 11:53 PM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/30/2015 11:53 PM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/30/2015 11:53 PM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/30/2015 11:53 PM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/30/2015 11:53 PM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/30/2015 11:53 PM
Surr: 1,2-Dichloroethane-d4 88.2 80-120 %RECNANA 3/30/2015 11:53 PM
Surr: 4-Bromofluorobenzene 98.2 80-120 %RECNANA 3/30/2015 11:53 PM
Surr: Dibromofluoromethane 90.6 80-120 %RECNANA 3/30/2015 11:53 PM
Surr: Toluene-d8 99.9 80-120 %RECNANA 3/30/2015 11:53 PM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 10:16 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 391 10 mg/L2.0 NA PA/VA3/27/2015 2:04 PM
Page 9 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 4:56 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Barium 0.203 0.100 mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 4:56 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 4:56 PM
Chromium 0.0018 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Copper 0.0020 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/3/2015 4:56 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/3/2015 4:56 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 4:56 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Vanadium 0.0076 0.0250 J mg/L0.0010 NA PA/VA4/3/2015 4:56 PM
Zinc 0.0078 0.0100 J mg/L0.0030 NA PA/VA4/3/2015 4:56 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury 0.0001 0.0010 J mg/L0.0001 NA PA/VA3/31/2015 10:32 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
alpha-BHC ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
beta-BHC ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
delta-BHC ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
gamma-BHC ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
Chlordane ND 0.00499 mg/L0.00250 0.00050 3/31/2015 5:34 PM
4,4´-DDD ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
4,4´-DDE ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
4,4´-DDT ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
Dieldrin ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
Endosulfan I ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
Endosulfan II ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
Endosulfan sulfate ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
Endrin ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
Endrin aldehyde ND 0.000499 mg/L0.000250 0.00010 3/31/2015 5:34 PM
Heptachlor ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
Page 10 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000499 mg/L0.000250 0.00005 3/31/2015 5:34 PM
Methoxychlor ND 0.000499 mg/L0.000250 0.00100 3/31/2015 5:34 PM
Toxaphene ND 0.00499 mg/L0.00250 0.00100 3/31/2015 5:34 PM
Surr: Tetrachloro-m-xylene 109 30.6-137 %RECNANA 3/31/2015 5:34 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Aroclor 1221 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Aroclor 1232 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Aroclor 1242 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Aroclor 1248 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Aroclor 1254 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Aroclor 1260 ND 0.00050 mg/L0.00025 NA 3/31/2015 5:34 PM
Surr: Tetrachloro-m-xylene 73.5 23.9-150 %RECNANA 3/31/2015 5:34 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00239 mg/L0.000003 NA 4/8/2015 3:20 PM
2,4,5-TP (Silvex)ND 0.00239 mg/L0.000003 NA 4/8/2015 3:20 PM
2,4-D ND 0.00239 mg/L0.000005 NA 4/8/2015 3:20 PM
Dinoseb ND 0.00119 mg/L0.000005 NA 4/8/2015 3:20 PM
Surr: 2,4-Dichlorophenylacetic acid 68.4 21.8-182 %RECNANA 4/8/2015 3:20 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
1,3-Dinitrobenzene ND 0.0207 mg/L0.0052 NA 3/31/2015 7:19 PM
1,4-Napthoquinone ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
1-Naphthylamine ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
2,6-Dichlorophenol ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
2-Acetylaminofluorene ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
2-Naphthylamine ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
2-Picoline ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
3,3´-Dimethylbenzidine ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
3-Methylcholanthrene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
4-Aminobiphenyl ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
4-Nitroquinoline-1-oxide ND 0.0518 mg/LNANA 3/31/2015 7:19 PM
Page 11 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
7,12-Dimethylbenz(a)anthracene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Acetophenone ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Chlorobenzilate ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Diallate ND 0.0104 mg/L0.0021 NA 3/31/2015 7:19 PM
Dimethoate ND 0.0207 mg/L0.0052 NA 3/31/2015 7:19 PM
Diphenylamine ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Disulfoton ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Ethyl methacrylate ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Ethyl methanesulfonate ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
Famphur ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
Hexachlorophene ND 0.104 mg/LNANA 3/31/2015 7:19 PM
Hexachloropropene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Isodrin ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
Isosafrole ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Kepone ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
Methapyrilene ND 0.104 mg/LNANA 3/31/2015 7:19 PM
Methyl methacrylate ND 0.0311 mg/LNANA 4/4/2015 8:02 PM
Methyl methanesulfonate ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Methyl parathion ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
N-Nitroso-di-n-butylamine ND 0.0104 mg/L0.0021 NA 3/31/2015 7:19 PM
N-Nitrosodiethylamine ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
n-Nitrosomethylethylamine ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
N-Nitrosopiperidine ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
N-Nitrosopyrrolidine ND 0.0104 mg/L0.0021 NA 3/31/2015 7:19 PM
o,o,o-Triethylphosphorothioate ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0207 mg/LNANA 3/31/2015 7:19 PM
o-Toluidine ND 0.0104 mg/L0.0021 NA 3/31/2015 7:19 PM
p-Dimethylaminoazobenzene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
p-Phenylenediamine ND 0.0104 mg/LNANA 4/4/2015 8:02 PM
Parathion ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Pentachlorobenzene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Pentachloronitrobenzene ND 0.0207 mg/L0.0021 NA 3/31/2015 7:19 PM
Phenacetin ND 0.0207 mg/L0.0021 NA 3/31/2015 7:19 PM
Phorate ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Pronamide ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Safrole ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
sym-Trinitrobenzene ND 0.0104 mg/LNANA 3/31/2015 7:19 PM
Page 12 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0104 mg/L0NA PA/VA3/31/2015 7:19 PM
Acenaphthylene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Anthracene ND 0.0104 mg/LNANA PA/VA3/31/2015 7:19 PM
Benzo(a)anthracene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Benzo(a)pyrene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Benzo(b)fluoranthene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Benzo(g,h,i)perylene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Benzo(k)fluoranthene ND 0.0104 mg/L0.0031 NA PA/VA3/31/2015 7:19 PM
Benzyl alcohol ND 0.0207 mg/L0.0021 NA 3/31/2015 7:19 PM
Bis(2-chloroethoxy)methane ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Bis(2-chloroethyl)ether ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Bis(2-chloroisopropyl)ether ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Bis(2-ethylhexyl)phthalate ND 0.0155 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
4-Bromophenyl phenyl ether ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Butyl benzyl phthalate ND 0.0104 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
4-Chloroaniline ND 0.0207 mg/L0.0052 NA 3/31/2015 7:19 PM
4-Chloro-3-methylphenol ND 0.0207 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2-Chloronaphthalene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2-Chlorophenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
4-Chlorophenyl phenyl ether ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Chrysene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
o-Cresol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
m,p-Cresol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Dibenzo(a,h)anthracene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Dibenzofuran ND 0.0104 mg/LNANA PA/VA3/31/2015 7:19 PM
Di-n-butyl phthalate ND 0.0104 mg/LNANA PA/VA3/31/2015 7:19 PM
3,3´-Dichlorobenzidine ND 0.0207 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
2,4-Dichlorophenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Diethyl phthalate ND 6.21 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Dimethyl phthalate ND 0.0104 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
2,4-Dimethylphenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
4,6-Dinitro-2-methylphenol ND 0.0518 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2,4-Dinitrophenol ND 0.0518 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2,4-Dinitrotoluene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2,6-Dinitrotoluene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Di-n-octyl phthalate ND 0.0104 mg/LNANA PA/VA3/31/2015 7:19 PM
Fluoranthene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Fluorene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Page 13 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Hexachlorobutadiene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Hexachlorocyclopentadiene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Hexachloroethane ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Indeno(1,2,3-cd)pyrene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Isophorone ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2-Methylnaphthalene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Naphthalene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2-Nitroaniline ND 0.0518 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
3-Nitroaniline ND 0.0518 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
4-Nitroaniline ND 0.0207 mg/L0.0052 NA PA/VA3/31/2015 7:19 PM
Nitrobenzene ND 0.0104 mg/LNANA PA/VA3/31/2015 7:19 PM
2-Nitrophenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
4-Nitrophenol ND 0.0518 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
N-Nitrosodimethylamine ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
N-Nitrosodiphenylamine ND 0.0104 mg/L0NA PA/VA3/31/2015 7:19 PM
N-Nitrosodi-n-propylamine ND 0.0104 mg/L0NA PA/VA3/31/2015 7:19 PM
Pentachlorophenol ND 0.0259 mg/L0NA PA/VA3/31/2015 7:19 PM
Phenanthrene ND 0.0104 mg/L0NA PA/VA3/31/2015 7:19 PM
Phenol ND 0.0104 mg/L0NA PA/VA3/31/2015 7:19 PM
Pyrene ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2,3,4,6-Tetrachlorophenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
1,2,4-Trichlorobenzene ND 0.0104 mg/L0.0021 NA 3/31/2015 7:19 PM
2,4,5-Trichlorophenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
2,4,6-Trichlorophenol ND 0.0104 mg/L0.0021 NA PA/VA3/31/2015 7:19 PM
Surr: 2-Fluorophenol 39.7 32.9-110 %RECNANA 3/31/2015 7:19 PM
Surr: Phenol-d5 30.7 25.8-110 %RECNANA 3/31/2015 7:19 PM
Surr: 2,4,6-Tribromophenol 77.2 63.8-110 %RECNANA 3/31/2015 7:19 PM
Surr: Nitrobenzene-d5 93.4 61.8-110 %RECNANA 3/31/2015 7:19 PM
Surr: 2-Fluorobiphenyl 80.2 58.6-110 %RECNANA 3/31/2015 7:19 PM
Surr: 4-Terphenyl-d14 83.8 55.1-110 %RECNANA 3/31/2015 7:19 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 12:26 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 12:26 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 12:26 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 12:26 AM
Benzene 2.14 1.00 µg/L0.129 NA PA/VA3/31/2015 12:26 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 12:26 AM
Page 14 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 12:26 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 12:26 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 12:26 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 12:26 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 12:26 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 12:26 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/31/2015 12:26 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 12:26 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 12:26 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 12:26 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 12:26 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 12:26 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 12:26 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 12:26 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 12:26 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 12:26 AM
1,4-Dichlorobenzene 0.980 1.00 J µg/L0.287 NA PA/VA3/31/2015 12:26 AM
Dichlorodifluoromethane 3.08 5.00 J µg/L0.714 NA PA/VA3/31/2015 12:26 AM
1,1-Dichloroethane 19.8 5.00 µg/L0.383 NA PA/VA3/31/2015 12:26 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 12:26 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 12:26 AM
cis-1,2-Dichloroethene 21.6 5.00 µg/L0.226 NA PA/VA3/31/2015 12:26 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 12:26 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 12:26 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 12:26 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 12:26 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 12:26 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 12:26 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 12:26 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 12:26 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 12:26 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 12:26 AM
Methylene chloride 1.35 1.00 µg/L0.539 NA PA/VA3/31/2015 12:26 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 12:26 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 12:26 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 12:26 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 12:26 AM
Tetrachloroethene 10.1 1.00 µg/L0.196 NA PA/VA3/31/2015 12:26 AM
Page 15 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-02A Matrix:Groundwater
MW-5AClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 12:26 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 12:26 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 12:26 AM
Trichloroethene 21.6 1.00 µg/L0.302 NA PA/VA3/31/2015 12:26 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 12:26 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 12:26 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 12:26 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 12:26 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 12:26 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 12:26 AM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 3/31/2015 12:26 AM
Surr: 4-Bromofluorobenzene 103 71.8-127 %RECNANA 3/31/2015 12:26 AM
Surr: Dibromofluoromethane 98.2 74.3-124 %RECNANA 3/31/2015 12:26 AM
Surr: Toluene-d8 95.1 71.4-129 %RECNANA 3/31/2015 12:26 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 12:26 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 12:26 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 12:26 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 12:26 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 12:26 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 12:26 AM
Surr: 1,2-Dichloroethane-d4 94.5 80-120 %RECNANA 3/31/2015 12:26 AM
Surr: 4-Bromofluorobenzene 94.3 80-120 %RECNANA 3/31/2015 12:26 AM
Surr: Dibromofluoromethane 76.7 80-120 S %RECNANA 3/31/2015 12:26 AM
Surr: Toluene-d8 97.8 80-120 %RECNANA 3/31/2015 12:26 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 10:17 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 4.0 5.0 J mg/L1.0 NA PA/VA3/27/2015 2:04 PM
Page 16 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0002 0.0060 J mg/L0.0002 NA PA/VA4/3/2015 5:12 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Barium 0.285 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:12 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:12 PM
Chromium 0.0044 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Cobalt 0.0254 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Copper 0.0016 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/3/2015 5:12 PM
Nickel 0.0148 0.0500 J mg/L0.0020 NA PA/VA4/3/2015 5:12 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:12 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Vanadium 0.0012 0.0250 J mg/L0.0010 NA PA/VA4/3/2015 5:12 PM
Zinc 0.0104 0.0100 mg/L0.0030 NA PA/VA4/3/2015 5:12 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:39 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
alpha-BHC ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
beta-BHC ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
delta-BHC ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
gamma-BHC ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
Chlordane ND 0.00510 mg/L0.00255 0.00050 3/31/2015 5:48 PM
4,4´-DDD ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
4,4´-DDE ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
4,4´-DDT ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
Dieldrin ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
Endosulfan I ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
Endosulfan II ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
Endosulfan sulfate ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
Endrin ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
Endrin aldehyde ND 0.00102 mg/L0.000510 0.00010 4/1/2015 9:44 AM
Heptachlor ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
Page 17 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.00102 mg/L0.000510 0.00005 4/1/2015 9:44 AM
Methoxychlor ND 0.00102 mg/L0.000510 0.00100 4/1/2015 9:44 AM
Toxaphene ND 0.00510 mg/L0.00255 0.00100 3/31/2015 5:48 PM
Surr: Tetrachloro-m-xylene 184 30.6-137 S %RECNANA 4/1/2015 9:44 AM
Notes:
Elevated PQLs are due to matrix interference.
Surrogate recovery exceeded REIC control limits due to sample dilution and does not reflect extraction efficiency.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00408 mg/L0.00015 NA 4/2/2015 2:31 PM
Aroclor 1221 ND 0.00408 mg/L0.00026 NA 4/2/2015 2:31 PM
Aroclor 1232 ND 0.00408 mg/L0.00020 NA 4/2/2015 2:31 PM
Aroclor 1242 ND 0.00408 mg/L0.00022 NA 4/2/2015 2:31 PM
Aroclor 1248 ND 0.00408 mg/L0.00014 NA 4/2/2015 2:31 PM
Aroclor 1254 ND 0.00408 mg/L0.00013 NA 4/2/2015 2:31 PM
Aroclor 1260 ND 0.00408 mg/L0.00003 NA 4/2/2015 2:31 PM
Surr: Tetrachloro-m-xylene 142 23.9-150 %RECNANA 3/31/2015 5:48 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.0119 mg/L0.000013 NA 4/8/2015 3:03 PM
2,4,5-TP (Silvex)ND 0.0119 mg/L0.000013 NA 4/8/2015 3:03 PM
2,4-D ND 0.0119 mg/L0.000024 NA 4/8/2015 3:03 PM
Dinoseb ND 0.00597 mg/L0.000024 NA 4/8/2015 3:03 PM
Surr: 2,4-Dichlorophenylacetic acid 108 21.8-182 %RECNANA 4/8/2015 3:03 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
1,3-Dinitrobenzene ND 0.0213 mg/L0.0053 NA 3/31/2015 7:45 PM
1,4-Napthoquinone ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
1-Naphthylamine ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
2,6-Dichlorophenol ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
2-Acetylaminofluorene ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
2-Naphthylamine ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
2-Picoline ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
3,3´-Dimethylbenzidine ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
3-Methylcholanthrene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
4-Aminobiphenyl ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
Page 18 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
4-Nitroquinoline-1-oxide ND 0.0531 mg/LNANA 3/31/2015 7:45 PM
5-Nitro-o-toluidine ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
7,12-Dimethylbenz(a)anthracene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Acetophenone ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Chlorobenzilate ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Diallate ND 0.0106 mg/L0.0021 NA 3/31/2015 7:45 PM
Dimethoate ND 0.0213 mg/L0.0053 NA 3/31/2015 7:45 PM
Diphenylamine ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Disulfoton ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Ethyl methacrylate ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Ethyl methanesulfonate ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
Famphur ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
Hexachlorophene ND 0.106 mg/LNANA 3/31/2015 7:45 PM
Hexachloropropene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Isodrin ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
Isosafrole ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Kepone ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
Methapyrilene ND 0.106 mg/LNANA 3/31/2015 7:45 PM
Methyl methacrylate ND 0.0319 mg/LNANA 4/4/2015 8:23 PM
Methyl methanesulfonate ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Methyl parathion ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
N-Nitroso-di-n-butylamine ND 0.0106 mg/L0.0021 NA 3/31/2015 7:45 PM
N-Nitrosodiethylamine ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
n-Nitrosomethylethylamine ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
N-Nitrosopiperidine ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
N-Nitrosopyrrolidine ND 0.0106 mg/L0.0021 NA 3/31/2015 7:45 PM
o,o,o-Triethylphosphorothioate ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0213 mg/LNANA 3/31/2015 7:45 PM
o-Toluidine ND 0.0106 mg/L0.0021 NA 3/31/2015 7:45 PM
p-Dimethylaminoazobenzene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
p-Phenylenediamine ND 0.0106 mg/LNANA 4/4/2015 8:23 PM
Parathion ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Pentachlorobenzene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Pentachloronitrobenzene ND 0.0213 mg/L0.0021 NA 3/31/2015 7:45 PM
Phenacetin ND 0.0213 mg/L0.0021 NA 3/31/2015 7:45 PM
Phorate ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Pronamide ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Safrole ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Page 19 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
sym-Trinitrobenzene ND 0.0106 mg/LNANA 3/31/2015 7:45 PM
Acenaphthene ND 0.0106 mg/L0NA PA/VA3/31/2015 7:45 PM
Acenaphthylene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Anthracene ND 0.0106 mg/LNANA PA/VA3/31/2015 7:45 PM
Benzo(a)anthracene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Benzo(a)pyrene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Benzo(b)fluoranthene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Benzo(g,h,i)perylene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Benzo(k)fluoranthene ND 0.0106 mg/L0.0032 NA PA/VA3/31/2015 7:45 PM
Benzyl alcohol ND 0.0213 mg/L0.0021 NA 3/31/2015 7:45 PM
Bis(2-chloroethoxy)methane ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Bis(2-chloroethyl)ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Bis(2-chloroisopropyl)ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Bis(2-ethylhexyl)phthalate ND 0.0159 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
4-Bromophenyl phenyl ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Butyl benzyl phthalate ND 0.0106 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
4-Chloroaniline ND 0.0213 mg/L0.0053 NA 3/31/2015 7:45 PM
4-Chloro-3-methylphenol ND 0.0213 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2-Chloronaphthalene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2-Chlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
4-Chlorophenyl phenyl ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Chrysene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
o-Cresol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
m,p-Cresol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Dibenzo(a,h)anthracene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Dibenzofuran ND 0.0106 mg/LNANA PA/VA3/31/2015 7:45 PM
Di-n-butyl phthalate ND 0.0106 mg/LNANA PA/VA3/31/2015 7:45 PM
3,3´-Dichlorobenzidine ND 0.0213 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
2,4-Dichlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Diethyl phthalate ND 6.38 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Dimethyl phthalate ND 0.0106 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
2,4-Dimethylphenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
4,6-Dinitro-2-methylphenol ND 0.0531 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2,4-Dinitrophenol ND 0.0531 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2,4-Dinitrotoluene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2,6-Dinitrotoluene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Di-n-octyl phthalate ND 0.0106 mg/LNANA PA/VA3/31/2015 7:45 PM
Fluoranthene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Page 20 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Fluorene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Hexachlorobenzene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Hexachlorobutadiene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Hexachlorocyclopentadiene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Hexachloroethane ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Indeno(1,2,3-cd)pyrene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Isophorone ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2-Methylnaphthalene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Naphthalene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2-Nitroaniline ND 0.0531 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
3-Nitroaniline ND 0.0531 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
4-Nitroaniline ND 0.0213 mg/L0.0053 NA PA/VA3/31/2015 7:45 PM
Nitrobenzene ND 0.0106 mg/LNANA PA/VA3/31/2015 7:45 PM
2-Nitrophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
4-Nitrophenol ND 0.0531 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
N-Nitrosodimethylamine ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
N-Nitrosodiphenylamine ND 0.0106 mg/L0NA PA/VA3/31/2015 7:45 PM
N-Nitrosodi-n-propylamine ND 0.0106 mg/L0NA PA/VA3/31/2015 7:45 PM
Pentachlorophenol ND 0.0266 mg/L0NA PA/VA3/31/2015 7:45 PM
Phenanthrene ND 0.0106 mg/L0NA PA/VA3/31/2015 7:45 PM
Phenol ND 0.0106 mg/L0NA PA/VA3/31/2015 7:45 PM
Pyrene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2,3,4,6-Tetrachlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
1,2,4-Trichlorobenzene ND 0.0106 mg/L0.0021 NA 3/31/2015 7:45 PM
2,4,5-Trichlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
2,4,6-Trichlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 7:45 PM
Surr: 2-Fluorophenol 40.6 32.9-110 %RECNANA 3/31/2015 7:45 PM
Surr: Phenol-d5 33.4 25.8-110 %RECNANA 3/31/2015 7:45 PM
Surr: 2,4,6-Tribromophenol 78.2 63.8-110 %RECNANA 3/31/2015 7:45 PM
Surr: Nitrobenzene-d5 95.1 61.8-110 %RECNANA 3/31/2015 7:45 PM
Surr: 2-Fluorobiphenyl 80.7 58.6-110 %RECNANA 3/31/2015 7:45 PM
Surr: 4-Terphenyl-d14 80.6 55.1-110 %RECNANA 3/31/2015 7:45 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 12:59 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 12:59 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 12:59 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 12:59 AM
Benzene 4.00 1.00 µg/L0.129 NA PA/VA3/31/2015 12:59 AM
Page 21 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 12:59 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 12:59 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 12:59 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 12:59 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 12:59 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 12:59 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 12:59 AM
Chlorobenzene 3.01 3.00 µg/L0.177 NA PA/VA3/31/2015 12:59 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 12:59 AM
Chloroform 0.960 5.00 J µg/L0.253 NA PA/VA3/31/2015 12:59 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 12:59 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 12:59 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 12:59 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 12:59 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 12:59 AM
1,2-Dichlorobenzene 0.540 5.00 J µg/L0.450 NA PA/VA3/31/2015 12:59 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 12:59 AM
1,4-Dichlorobenzene 8.39 1.00 µg/L0.287 NA PA/VA3/31/2015 12:59 AM
Dichlorodifluoromethane 4.07 5.00 J µg/L0.714 NA PA/VA3/31/2015 12:59 AM
1,1-Dichloroethane 14.3 5.00 µg/L0.383 NA PA/VA3/31/2015 12:59 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 12:59 AM
1,1-Dichloroethene 0.890 5.00 J µg/L0.328 NA PA/VA3/31/2015 12:59 AM
cis-1,2-Dichloroethene 4.29 5.00 J µg/L0.226 NA PA/VA3/31/2015 12:59 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 12:59 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 12:59 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 12:59 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 12:59 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 12:59 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 12:59 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 12:59 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 12:59 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 12:59 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 12:59 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/31/2015 12:59 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 12:59 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 12:59 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 12:59 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 12:59 AM
Page 22 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:27:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-03A Matrix:Groundwater
MW-6Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Tetrachloroethene 0.910 1.00 J µg/L0.196 NA PA/VA3/31/2015 12:59 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 12:59 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 12:59 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 12:59 AM
Trichloroethene 2.18 1.00 µg/L0.302 NA PA/VA3/31/2015 12:59 AM
Trichlorofluoromethane 13.8 1.00 µg/L0.299 NA PA/VA3/31/2015 12:59 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 12:59 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 12:59 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 12:59 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 12:59 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 12:59 AM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 3/31/2015 12:59 AM
Surr: 4-Bromofluorobenzene 100 71.8-127 %RECNANA 3/31/2015 12:59 AM
Surr: Dibromofluoromethane 98.9 74.3-124 %RECNANA 3/31/2015 12:59 AM
Surr: Toluene-d8 93.3 71.4-129 %RECNANA 3/31/2015 12:59 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 12:59 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 12:59 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 12:59 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 12:59 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 12:59 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 12:59 AM
Surr: 1,2-Dichloroethane-d4 108 80-120 %RECNANA 3/31/2015 12:59 AM
Surr: 4-Bromofluorobenzene 97.3 80-120 %RECNANA 3/31/2015 12:59 AM
Surr: Dibromofluoromethane 104 80-120 %RECNANA 3/31/2015 12:59 AM
Surr: Toluene-d8 96.1 80-120 %RECNANA 3/31/2015 12:59 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 10:18 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 5.0 5.0 mg/L1.0 NA PA/VA3/27/2015 2:04 PM
Page 23 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 5:18 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Barium 0.0750 0.100 J mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:18 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:18 PM
Chromium 0.0018 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Copper 0.0015 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/3/2015 5:18 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/3/2015 5:18 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:18 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Vanadium 0.0093 0.0250 J mg/L0.0010 NA PA/VA4/3/2015 5:18 PM
Zinc 0.0068 0.0100 J mg/L0.0030 NA PA/VA4/3/2015 5:18 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:41 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
alpha-BHC ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
beta-BHC ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
delta-BHC ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
gamma-BHC ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
Chlordane ND 0.00502 mg/L0.00251 0.00050 3/31/2015 6:02 PM
4,4´-DDD ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
4,4´-DDE ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
4,4´-DDT ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
Dieldrin ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
Endosulfan I ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
Endosulfan II ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
Endosulfan sulfate ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
Endrin ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
Endrin aldehyde ND 0.000502 mg/L0.000251 0.00010 3/31/2015 6:02 PM
Heptachlor ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
Page 24 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000502 mg/L0.000251 0.00005 3/31/2015 6:02 PM
Methoxychlor ND 0.000502 mg/L0.000251 0.00100 3/31/2015 6:02 PM
Toxaphene ND 0.00502 mg/L0.00251 0.00100 3/31/2015 6:02 PM
Surr: Tetrachloro-m-xylene 97.0 30.6-137 %RECNANA 3/31/2015 6:02 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Aroclor 1221 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Aroclor 1232 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Aroclor 1242 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Aroclor 1248 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Aroclor 1254 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Aroclor 1260 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:02 PM
Surr: Tetrachloro-m-xylene 67.0 23.9-150 %RECNANA 3/31/2015 6:02 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00245 mg/L0.000003 NA 4/8/2015 3:37 PM
2,4,5-TP (Silvex)ND 0.00245 mg/L0.000003 NA 4/8/2015 3:37 PM
2,4-D ND 0.00245 mg/L0.000005 NA 4/8/2015 3:37 PM
Dinoseb ND 0.00123 mg/L0.000005 NA 4/8/2015 3:37 PM
Surr: 2,4-Dichlorophenylacetic acid 75.0 21.8-182 %RECNANA 4/8/2015 3:37 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
1,3-Dinitrobenzene ND 0.0205 mg/L0.0051 NA 3/31/2015 8:12 PM
1,4-Napthoquinone ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
1-Naphthylamine ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
2,6-Dichlorophenol ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
2-Acetylaminofluorene ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
2-Naphthylamine ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
2-Picoline ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
3,3´-Dimethylbenzidine ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
3-Methylcholanthrene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
4-Aminobiphenyl ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
4-Nitroquinoline-1-oxide ND 0.0512 mg/LNANA 3/31/2015 8:12 PM
Page 25 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
7,12-Dimethylbenz(a)anthracene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Acetophenone ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Chlorobenzilate ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Diallate ND 0.0102 mg/L0.0020 NA 3/31/2015 8:12 PM
Dimethoate ND 0.0205 mg/L0.0051 NA 3/31/2015 8:12 PM
Diphenylamine ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Disulfoton ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Ethyl methacrylate ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Ethyl methanesulfonate ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
Famphur ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
Hexachlorophene ND 0.102 mg/LNANA 3/31/2015 8:12 PM
Hexachloropropene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Isodrin ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
Isosafrole ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Kepone ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
Methapyrilene ND 0.102 mg/LNANA 3/31/2015 8:12 PM
Methyl methacrylate ND 0.0307 mg/LNANA 4/4/2015 8:45 PM
Methyl methanesulfonate ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Methyl parathion ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
N-Nitroso-di-n-butylamine ND 0.0102 mg/L0.0020 NA 3/31/2015 8:12 PM
N-Nitrosodiethylamine ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
n-Nitrosomethylethylamine ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
N-Nitrosopiperidine ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
N-Nitrosopyrrolidine ND 0.0102 mg/L0.0020 NA 3/31/2015 8:12 PM
o,o,o-Triethylphosphorothioate ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0205 mg/LNANA 3/31/2015 8:12 PM
o-Toluidine ND 0.0102 mg/L0.0020 NA 3/31/2015 8:12 PM
p-Dimethylaminoazobenzene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
p-Phenylenediamine ND 0.0102 mg/LNANA 4/4/2015 8:45 PM
Parathion ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Pentachlorobenzene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Pentachloronitrobenzene ND 0.0205 mg/L0.0020 NA 3/31/2015 8:12 PM
Phenacetin ND 0.0205 mg/L0.0020 NA 3/31/2015 8:12 PM
Phorate ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Pronamide ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Safrole ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
sym-Trinitrobenzene ND 0.0102 mg/LNANA 3/31/2015 8:12 PM
Page 26 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0102 mg/L0NA PA/VA3/31/2015 8:12 PM
Acenaphthylene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Anthracene ND 0.0102 mg/LNANA PA/VA3/31/2015 8:12 PM
Benzo(a)anthracene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Benzo(a)pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Benzo(b)fluoranthene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Benzo(g,h,i)perylene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Benzo(k)fluoranthene ND 0.0102 mg/L0.0031 NA PA/VA3/31/2015 8:12 PM
Benzyl alcohol ND 0.0205 mg/L0.0020 NA 3/31/2015 8:12 PM
Bis(2-chloroethoxy)methane ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Bis(2-chloroethyl)ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Bis(2-chloroisopropyl)ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Bis(2-ethylhexyl)phthalate ND 0.0154 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
4-Bromophenyl phenyl ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Butyl benzyl phthalate ND 0.0102 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
4-Chloroaniline ND 0.0205 mg/L0.0051 NA 3/31/2015 8:12 PM
4-Chloro-3-methylphenol ND 0.0205 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2-Chloronaphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2-Chlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
4-Chlorophenyl phenyl ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Chrysene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
o-Cresol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
m,p-Cresol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Dibenzo(a,h)anthracene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Dibenzofuran ND 0.0102 mg/LNANA PA/VA3/31/2015 8:12 PM
Di-n-butyl phthalate ND 0.0102 mg/LNANA PA/VA3/31/2015 8:12 PM
3,3´-Dichlorobenzidine ND 0.0205 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
2,4-Dichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Diethyl phthalate ND 6.15 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Dimethyl phthalate ND 0.0102 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
2,4-Dimethylphenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
4,6-Dinitro-2-methylphenol ND 0.0512 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2,4-Dinitrophenol ND 0.0512 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2,4-Dinitrotoluene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2,6-Dinitrotoluene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Di-n-octyl phthalate ND 0.0102 mg/LNANA PA/VA3/31/2015 8:12 PM
Fluoranthene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Fluorene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Page 27 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Hexachlorobutadiene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Hexachlorocyclopentadiene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Hexachloroethane ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Indeno(1,2,3-cd)pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Isophorone ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2-Methylnaphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Naphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2-Nitroaniline ND 0.0512 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
3-Nitroaniline ND 0.0512 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
4-Nitroaniline ND 0.0205 mg/L0.0051 NA PA/VA3/31/2015 8:12 PM
Nitrobenzene ND 0.0102 mg/LNANA PA/VA3/31/2015 8:12 PM
2-Nitrophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
4-Nitrophenol ND 0.0512 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
N-Nitrosodimethylamine ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
N-Nitrosodiphenylamine ND 0.0102 mg/L0NA PA/VA3/31/2015 8:12 PM
N-Nitrosodi-n-propylamine ND 0.0102 mg/L0NA PA/VA3/31/2015 8:12 PM
Pentachlorophenol ND 0.0256 mg/L0NA PA/VA3/31/2015 8:12 PM
Phenanthrene ND 0.0102 mg/L0NA PA/VA3/31/2015 8:12 PM
Phenol ND 0.0102 mg/L0NA PA/VA3/31/2015 8:12 PM
Pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2,3,4,6-Tetrachlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
1,2,4-Trichlorobenzene ND 0.0102 mg/L0.0020 NA 3/31/2015 8:12 PM
2,4,5-Trichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
2,4,6-Trichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 8:12 PM
Surr: 2-Fluorophenol 37.0 32.9-110 %RECNANA 3/31/2015 8:12 PM
Surr: Phenol-d5 29.9 25.8-110 %RECNANA 3/31/2015 8:12 PM
Surr: 2,4,6-Tribromophenol 76.5 63.8-110 %RECNANA 3/31/2015 8:12 PM
Surr: Nitrobenzene-d5 90.8 61.8-110 %RECNANA 3/31/2015 8:12 PM
Surr: 2-Fluorobiphenyl 79.1 58.6-110 %RECNANA 3/31/2015 8:12 PM
Surr: 4-Terphenyl-d14 83.1 55.1-110 %RECNANA 3/31/2015 8:12 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 1:32 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 1:32 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 1:32 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 1:32 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/31/2015 1:32 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 1:32 AM
Page 28 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 1:32 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 1:32 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 1:32 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 1:32 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 1:32 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 1:32 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/31/2015 1:32 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 1:32 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 1:32 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 1:32 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 1:32 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 1:32 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 1:32 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 1:32 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 1:32 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 1:32 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/31/2015 1:32 AM
Dichlorodifluoromethane 0.800 5.00 J µg/L0.714 NA PA/VA3/31/2015 1:32 AM
1,1-Dichloroethane 0.780 5.00 J µg/L0.383 NA PA/VA3/31/2015 1:32 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 1:32 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 1:32 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/31/2015 1:32 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 1:32 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 1:32 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 1:32 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 1:32 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 1:32 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 1:32 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 1:32 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 1:32 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 1:32 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 1:32 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/31/2015 1:32 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 1:32 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 1:32 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 1:32 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 1:32 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/31/2015 1:32 AM
Page 29 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:04:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-04A Matrix:Groundwater
MW-6DClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 1:32 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 1:32 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 1:32 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/31/2015 1:32 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 1:32 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 1:32 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 1:32 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 1:32 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 1:32 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 1:32 AM
Surr: 1,2-Dichloroethane-d4 109 68.7-129 %RECNANA 3/31/2015 1:32 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 3/31/2015 1:32 AM
Surr: Dibromofluoromethane 104 74.3-124 %RECNANA 3/31/2015 1:32 AM
Surr: Toluene-d8 91.7 71.4-129 %RECNANA 3/31/2015 1:32 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 1:32 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 1:32 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 1:32 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 1:32 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 1:32 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 1:32 AM
Surr: 1,2-Dichloroethane-d4 108 80-120 %RECNANA 3/31/2015 1:32 AM
Surr: 4-Bromofluorobenzene 94.0 80-120 %RECNANA 3/31/2015 1:32 AM
Surr: Dibromofluoromethane 86.8 80-120 %RECNANA 3/31/2015 1:32 AM
Surr: Toluene-d8 94.2 80-120 %RECNANA 3/31/2015 1:32 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 10:18 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 4.5 5.0 J mg/L1.0 NA PA/VA3/27/2015 2:04 PM
Page 30 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony 0.0003 0.0060 J mg/L0.0002 NA PA/VA4/3/2015 5:24 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Barium 0.304 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Beryllium 0.0008 0.0010 J mg/L0.0002 NA PA/VA4/3/2015 5:24 PM
Cadmium 0.0008 0.0010 J mg/L0.0002 NA PA/VA4/3/2015 5:24 PM
Chromium 0.0308 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Cobalt 0.124 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Copper 0.0118 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Lead 0.0037 0.0100 J mg/L0.0002 NA PA/VA4/3/2015 5:24 PM
Nickel 0.0487 0.0500 J mg/L0.0020 NA PA/VA4/3/2015 5:24 PM
Selenium 0.0018 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Thallium 0.0003 0.0055 J mg/L0.0002 NA PA/VA4/3/2015 5:24 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Vanadium 0.0291 0.0250 mg/L0.0010 NA PA/VA4/3/2015 5:24 PM
Zinc 0.0930 0.0100 mg/L0.0030 NA PA/VA4/3/2015 5:24 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:43 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
alpha-BHC ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
beta-BHC ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
delta-BHC ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
gamma-BHC ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
Chlordane ND 0.00499 mg/L0.00250 0.00050 3/31/2015 6:17 PM
4,4´-DDD ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
4,4´-DDE ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
4,4´-DDT ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
Dieldrin ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
Endosulfan I ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
Endosulfan II ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
Endosulfan sulfate ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
Endrin ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
Endrin aldehyde ND 0.000998 mg/L0.000499 0.00010 4/1/2015 9:58 AM
Heptachlor ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
Page 31 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000998 mg/L0.000499 0.00005 4/1/2015 9:58 AM
Methoxychlor ND 0.000998 mg/L0.000499 0.00100 4/1/2015 9:58 AM
Toxaphene ND 0.00499 mg/L0.00250 0.00100 3/31/2015 6:17 PM
Surr: Tetrachloro-m-xylene 127 30.6-137 %RECNANA 3/31/2015 6:17 PM
Notes:
Elevated PQLs are due to matrix interference.
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Aroclor 1221 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Aroclor 1232 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Aroclor 1242 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Aroclor 1248 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Aroclor 1254 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Aroclor 1260 ND 0.00050 mg/L0.00025 NA 3/31/2015 6:17 PM
Surr: Tetrachloro-m-xylene 87.0 23.9-150 %RECNANA 3/31/2015 6:17 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.0119 mg/L0.000013 NA 4/8/2015 3:54 PM
2,4,5-TP (Silvex)ND 0.0119 mg/L0.000013 NA 4/8/2015 3:54 PM
2,4-D ND 0.0119 mg/L0.000024 NA 4/8/2015 3:54 PM
Dinoseb ND 0.00597 mg/L0.000024 NA 4/8/2015 3:54 PM
Surr: 2,4-Dichlorophenylacetic acid 94.4 21.8-182 J %RECNANA 4/8/2015 3:54 PM
Notes:
Surrogate recovery exceeded REIC control limits due to sample dilution and does not reflect extraction efficiency.
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
1,3-Dinitrobenzene ND 0.0203 mg/L0.0051 NA 3/31/2015 8:39 PM
1,4-Napthoquinone ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
1-Naphthylamine ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
2,6-Dichlorophenol ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
2-Acetylaminofluorene ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
2-Naphthylamine ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
2-Picoline ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
3,3´-Dimethylbenzidine ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
3-Methylcholanthrene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Page 32 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
4-Aminobiphenyl ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
4-Nitroquinoline-1-oxide ND 0.0507 mg/LNANA 3/31/2015 8:39 PM
5-Nitro-o-toluidine ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
7,12-Dimethylbenz(a)anthracene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Acetophenone ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Chlorobenzilate ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Diallate ND 0.0101 mg/L0.0020 NA 3/31/2015 8:39 PM
Dimethoate ND 0.0203 mg/L0.0051 NA 3/31/2015 8:39 PM
Diphenylamine ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Disulfoton ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Ethyl methacrylate ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Ethyl methanesulfonate ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
Famphur ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
Hexachlorophene ND 0.101 mg/LNANA 3/31/2015 8:39 PM
Hexachloropropene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Isodrin ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
Isosafrole ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Kepone ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
Methapyrilene ND 0.101 mg/LNANA 3/31/2015 8:39 PM
Methyl methacrylate ND 0.0304 mg/LNANA 4/4/2015 9:07 PM
Methyl methanesulfonate ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Methyl parathion ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
N-Nitroso-di-n-butylamine ND 0.0101 mg/L0.0020 NA 3/31/2015 8:39 PM
N-Nitrosodiethylamine ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
n-Nitrosomethylethylamine ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
N-Nitrosopiperidine ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
N-Nitrosopyrrolidine ND 0.0101 mg/L0.0020 NA 3/31/2015 8:39 PM
o,o,o-Triethylphosphorothioate ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0203 mg/LNANA 3/31/2015 8:39 PM
o-Toluidine ND 0.0101 mg/L0.0020 NA 3/31/2015 8:39 PM
p-Dimethylaminoazobenzene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
p-Phenylenediamine ND 0.0101 mg/LNANA 4/4/2015 9:07 PM
Parathion ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Pentachlorobenzene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Pentachloronitrobenzene ND 0.0203 mg/L0.0020 NA 3/31/2015 8:39 PM
Phenacetin ND 0.0203 mg/L0.0020 NA 3/31/2015 8:39 PM
Phorate ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Pronamide ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Page 33 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Safrole ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
sym-Trinitrobenzene ND 0.0101 mg/LNANA 3/31/2015 8:39 PM
Acenaphthene ND 0.0101 mg/L0NA PA/VA3/31/2015 8:39 PM
Acenaphthylene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Anthracene ND 0.0101 mg/LNANA PA/VA3/31/2015 8:39 PM
Benzo(a)anthracene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Benzo(a)pyrene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Benzo(b)fluoranthene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Benzo(g,h,i)perylene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Benzo(k)fluoranthene ND 0.0101 mg/L0.0030 NA PA/VA3/31/2015 8:39 PM
Benzyl alcohol ND 0.0203 mg/L0.0020 NA 3/31/2015 8:39 PM
Bis(2-chloroethoxy)methane ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Bis(2-chloroethyl)ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Bis(2-chloroisopropyl)ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Bis(2-ethylhexyl)phthalate ND 0.0152 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
4-Bromophenyl phenyl ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Butyl benzyl phthalate ND 0.0101 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
4-Chloroaniline ND 0.0203 mg/L0.0051 NA 3/31/2015 8:39 PM
4-Chloro-3-methylphenol ND 0.0203 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2-Chloronaphthalene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2-Chlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
4-Chlorophenyl phenyl ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Chrysene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
o-Cresol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
m,p-Cresol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Dibenzo(a,h)anthracene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Dibenzofuran ND 0.0101 mg/LNANA PA/VA3/31/2015 8:39 PM
Di-n-butyl phthalate ND 0.0101 mg/LNANA PA/VA3/31/2015 8:39 PM
3,3´-Dichlorobenzidine ND 0.0203 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
2,4-Dichlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Diethyl phthalate ND 6.08 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Dimethyl phthalate ND 0.0101 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
2,4-Dimethylphenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
4,6-Dinitro-2-methylphenol ND 0.0507 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2,4-Dinitrophenol ND 0.0507 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2,4-Dinitrotoluene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2,6-Dinitrotoluene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Di-n-octyl phthalate ND 0.0101 mg/LNANA PA/VA3/31/2015 8:39 PM
Page 34 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Fluoranthene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Fluorene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Hexachlorobenzene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Hexachlorobutadiene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Hexachlorocyclopentadiene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Hexachloroethane ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Indeno(1,2,3-cd)pyrene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Isophorone ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2-Methylnaphthalene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Naphthalene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2-Nitroaniline ND 0.0507 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
3-Nitroaniline ND 0.0507 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
4-Nitroaniline ND 0.0203 mg/L0.0051 NA PA/VA3/31/2015 8:39 PM
Nitrobenzene ND 0.0101 mg/LNANA PA/VA3/31/2015 8:39 PM
2-Nitrophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
4-Nitrophenol ND 0.0507 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
N-Nitrosodimethylamine ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
N-Nitrosodiphenylamine ND 0.0101 mg/L0NA PA/VA3/31/2015 8:39 PM
N-Nitrosodi-n-propylamine ND 0.0101 mg/L0NA PA/VA3/31/2015 8:39 PM
Pentachlorophenol ND 0.0253 mg/L0NA PA/VA3/31/2015 8:39 PM
Phenanthrene ND 0.0101 mg/L0NA PA/VA3/31/2015 8:39 PM
Phenol ND 0.0101 mg/L0NA PA/VA3/31/2015 8:39 PM
Pyrene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2,3,4,6-Tetrachlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
1,2,4-Trichlorobenzene ND 0.0101 mg/L0.0020 NA 3/31/2015 8:39 PM
2,4,5-Trichlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
2,4,6-Trichlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 8:39 PM
Surr: 2-Fluorophenol 41.0 32.9-110 %RECNANA 3/31/2015 8:39 PM
Surr: Phenol-d5 31.6 25.8-110 %RECNANA 3/31/2015 8:39 PM
Surr: 2,4,6-Tribromophenol 82.1 63.8-110 %RECNANA 3/31/2015 8:39 PM
Surr: Nitrobenzene-d5 99.3 61.8-110 %RECNANA 3/31/2015 8:39 PM
Surr: 2-Fluorobiphenyl 86.1 58.6-110 %RECNANA 3/31/2015 8:39 PM
Surr: 4-Terphenyl-d14 82.4 55.1-110 %RECNANA 3/31/2015 8:39 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 2:05 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 2:05 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 2:05 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 2:05 AM
Page 35 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Benzene 8.15 1.00 µg/L0.129 NA PA/VA3/31/2015 2:05 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 2:05 AM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 2:05 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 2:05 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 2:05 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 2:05 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 2:05 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 2:05 AM
Chlorobenzene 3.14 3.00 µg/L0.177 NA PA/VA3/31/2015 2:05 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 2:05 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 2:05 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 2:05 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 2:05 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 2:05 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 2:05 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 2:05 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 2:05 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 2:05 AM
1,4-Dichlorobenzene 9.99 1.00 µg/L0.287 NA PA/VA3/31/2015 2:05 AM
Dichlorodifluoromethane ND 5.00 µg/L0.714 NA PA/VA3/31/2015 2:05 AM
1,1-Dichloroethane 1.09 5.00 J µg/L0.383 NA PA/VA3/31/2015 2:05 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 2:05 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 2:05 AM
cis-1,2-Dichloroethene 4.53 5.00 J µg/L0.226 NA PA/VA3/31/2015 2:05 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 2:05 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 2:05 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 2:05 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 2:05 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 2:05 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 2:05 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 2:05 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 2:05 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 2:05 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 2:05 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/31/2015 2:05 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 2:05 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 2:05 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 2:05 AM
Page 36 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:02:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-05A Matrix:Groundwater
MW-7Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 2:05 AM
Tetrachloroethene 0.520 1.00 J µg/L0.196 NA PA/VA3/31/2015 2:05 AM
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 2:05 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 2:05 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 2:05 AM
Trichloroethene 0.910 1.00 J µg/L0.302 NA PA/VA3/31/2015 2:05 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 2:05 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 2:05 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 2:05 AM
Vinyl chloride 1.29 1.00 µg/L0.223 NA PA/VA3/31/2015 2:05 AM
o-Xylene 4.34 1.00 µg/L0.186 NA PA/VA3/31/2015 2:05 AM
m,p-Xylene 2.93 2.00 µg/L0.287 NA PA/VA3/31/2015 2:05 AM
Surr: 1,2-Dichloroethane-d4 106 68.7-129 %RECNANA 3/31/2015 2:05 AM
Surr: 4-Bromofluorobenzene 102 71.8-127 %RECNANA 3/31/2015 2:05 AM
Surr: Dibromofluoromethane 99.4 74.3-124 %RECNANA 3/31/2015 2:05 AM
Surr: Toluene-d8 93.1 71.4-129 %RECNANA 3/31/2015 2:05 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 2:05 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 2:05 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 2:05 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 2:05 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 2:05 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 2:05 AM
Surr: 1,2-Dichloroethane-d4 99.3 80-120 %RECNANA 3/31/2015 2:05 AM
Surr: 4-Bromofluorobenzene 103 80-120 %RECNANA 3/31/2015 2:05 AM
Surr: Dibromofluoromethane 90.3 80-120 %RECNANA 3/31/2015 2:05 AM
Surr: Toluene-d8 96.0 80-120 %RECNANA 3/31/2015 2:05 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 10:21 AM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 216 10 mg/L2.0 NA PA/VA3/27/2015 2:04 PM
Page 37 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 5:29 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Barium 0.210 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Beryllium 0.0003 0.0010 J mg/L0.0002 NA PA/VA4/3/2015 5:29 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:29 PM
Chromium 0.0048 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Cobalt 0.0115 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Copper 0.0091 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Lead 0.0008 0.0100 J mg/L0.0002 NA PA/VA4/3/2015 5:29 PM
Nickel 0.0032 0.0500 J mg/L0.0020 NA PA/VA4/3/2015 5:29 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:29 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Vanadium 0.0259 0.0250 mg/L0.0010 NA PA/VA4/3/2015 5:29 PM
Zinc 0.0137 0.0100 mg/L0.0030 NA PA/VA4/3/2015 5:29 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:45 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
alpha-BHC ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
beta-BHC ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
delta-BHC ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
gamma-BHC ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
Chlordane ND 0.00506 mg/L0.00253 0.00050 3/31/2015 6:31 PM
4,4´-DDD ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
4,4´-DDE ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
4,4´-DDT ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
Dieldrin ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
Endosulfan I ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
Endosulfan II ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
Endosulfan sulfate ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
Endrin ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
Endrin aldehyde ND 0.000506 mg/L0.000253 0.00010 3/31/2015 6:31 PM
Heptachlor ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
Page 38 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000506 mg/L0.000253 0.00005 3/31/2015 6:31 PM
Methoxychlor ND 0.000506 mg/L0.000253 0.00100 3/31/2015 6:31 PM
Toxaphene ND 0.00506 mg/L0.00253 0.00100 3/31/2015 6:31 PM
Surr: Tetrachloro-m-xylene 102 30.6-137 %RECNANA 3/31/2015 6:31 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Aroclor 1221 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Aroclor 1232 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Aroclor 1242 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Aroclor 1248 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Aroclor 1254 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Aroclor 1260 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:31 PM
Surr: Tetrachloro-m-xylene 71.5 23.9-150 %RECNANA 3/31/2015 6:31 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00246 mg/L0.000003 NA 4/8/2015 4:12 PM
2,4,5-TP (Silvex)ND 0.00246 mg/L0.000003 NA 4/8/2015 4:12 PM
2,4-D ND 0.00246 mg/L0.000005 NA 4/8/2015 4:12 PM
Dinoseb ND 0.00123 mg/L0.000005 NA 4/8/2015 4:12 PM
Surr: 2,4-Dichlorophenylacetic acid 73.4 21.8-182 %RECNANA 4/8/2015 4:12 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
1,3-Dinitrobenzene ND 0.0212 mg/L0.0053 NA 3/31/2015 9:06 PM
1,4-Napthoquinone ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
1-Naphthylamine ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
2,6-Dichlorophenol ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
2-Acetylaminofluorene ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
2-Naphthylamine ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
2-Picoline ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
3,3´-Dimethylbenzidine ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
3-Methylcholanthrene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
4-Aminobiphenyl ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
4-Nitroquinoline-1-oxide ND 0.0529 mg/LNANA 3/31/2015 9:06 PM
Page 39 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
7,12-Dimethylbenz(a)anthracene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Acetophenone ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Chlorobenzilate ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Diallate ND 0.0106 mg/L0.0021 NA 3/31/2015 9:06 PM
Dimethoate ND 0.0212 mg/L0.0053 NA 3/31/2015 9:06 PM
Diphenylamine ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Disulfoton ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Ethyl methacrylate ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Ethyl methanesulfonate ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
Famphur ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
Hexachlorophene ND 0.106 mg/LNANA 3/31/2015 9:06 PM
Hexachloropropene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Isodrin ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
Isosafrole ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Kepone ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
Methapyrilene ND 0.106 mg/LNANA 3/31/2015 9:06 PM
Methyl methacrylate ND 0.0318 mg/LNANA 4/4/2015 9:28 PM
Methyl methanesulfonate ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Methyl parathion ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
N-Nitroso-di-n-butylamine ND 0.0106 mg/L0.0021 NA 3/31/2015 9:06 PM
N-Nitrosodiethylamine ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
n-Nitrosomethylethylamine ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
N-Nitrosopiperidine ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
N-Nitrosopyrrolidine ND 0.0106 mg/L0.0021 NA 3/31/2015 9:06 PM
o,o,o-Triethylphosphorothioate ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0212 mg/LNANA 3/31/2015 9:06 PM
o-Toluidine ND 0.0106 mg/L0.0021 NA 3/31/2015 9:06 PM
p-Dimethylaminoazobenzene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
p-Phenylenediamine ND 0.0106 mg/LNANA 4/4/2015 9:28 PM
Parathion ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Pentachlorobenzene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Pentachloronitrobenzene ND 0.0212 mg/L0.0021 NA 3/31/2015 9:06 PM
Phenacetin ND 0.0212 mg/L0.0021 NA 3/31/2015 9:06 PM
Phorate ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Pronamide ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Safrole ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
sym-Trinitrobenzene ND 0.0106 mg/LNANA 3/31/2015 9:06 PM
Page 40 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0106 mg/L0NA PA/VA3/31/2015 9:06 PM
Acenaphthylene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Anthracene ND 0.0106 mg/LNANA PA/VA3/31/2015 9:06 PM
Benzo(a)anthracene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Benzo(a)pyrene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Benzo(b)fluoranthene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Benzo(g,h,i)perylene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Benzo(k)fluoranthene ND 0.0106 mg/L0.0032 NA PA/VA3/31/2015 9:06 PM
Benzyl alcohol ND 0.0212 mg/L0.0021 NA 3/31/2015 9:06 PM
Bis(2-chloroethoxy)methane ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Bis(2-chloroethyl)ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Bis(2-chloroisopropyl)ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Bis(2-ethylhexyl)phthalate ND 0.0159 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
4-Bromophenyl phenyl ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Butyl benzyl phthalate ND 0.0106 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
4-Chloroaniline ND 0.0212 mg/L0.0053 NA 3/31/2015 9:06 PM
4-Chloro-3-methylphenol ND 0.0212 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2-Chloronaphthalene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2-Chlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
4-Chlorophenyl phenyl ether ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Chrysene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
o-Cresol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
m,p-Cresol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Dibenzo(a,h)anthracene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Dibenzofuran ND 0.0106 mg/LNANA PA/VA3/31/2015 9:06 PM
Di-n-butyl phthalate ND 0.0106 mg/LNANA PA/VA3/31/2015 9:06 PM
3,3´-Dichlorobenzidine ND 0.0212 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
2,4-Dichlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Diethyl phthalate ND 6.35 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Dimethyl phthalate ND 0.0106 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
2,4-Dimethylphenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
4,6-Dinitro-2-methylphenol ND 0.0529 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2,4-Dinitrophenol ND 0.0529 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2,4-Dinitrotoluene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2,6-Dinitrotoluene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Di-n-octyl phthalate ND 0.0106 mg/LNANA PA/VA3/31/2015 9:06 PM
Fluoranthene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Fluorene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Page 41 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Hexachlorobutadiene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Hexachlorocyclopentadiene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Hexachloroethane ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Indeno(1,2,3-cd)pyrene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Isophorone ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2-Methylnaphthalene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Naphthalene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2-Nitroaniline ND 0.0529 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
3-Nitroaniline ND 0.0529 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
4-Nitroaniline ND 0.0212 mg/L0.0053 NA PA/VA3/31/2015 9:06 PM
Nitrobenzene ND 0.0106 mg/LNANA PA/VA3/31/2015 9:06 PM
2-Nitrophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
4-Nitrophenol ND 0.0529 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
N-Nitrosodimethylamine ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
N-Nitrosodiphenylamine ND 0.0106 mg/L0NA PA/VA3/31/2015 9:06 PM
N-Nitrosodi-n-propylamine ND 0.0106 mg/L0NA PA/VA3/31/2015 9:06 PM
Pentachlorophenol ND 0.0265 mg/L0NA PA/VA3/31/2015 9:06 PM
Phenanthrene ND 0.0106 mg/L0NA PA/VA3/31/2015 9:06 PM
Phenol ND 0.0106 mg/L0NA PA/VA3/31/2015 9:06 PM
Pyrene ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2,3,4,6-Tetrachlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
1,2,4-Trichlorobenzene ND 0.0106 mg/L0.0021 NA 3/31/2015 9:06 PM
2,4,5-Trichlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
2,4,6-Trichlorophenol ND 0.0106 mg/L0.0021 NA PA/VA3/31/2015 9:06 PM
Surr: 2-Fluorophenol 40.2 32.9-110 %RECNANA 3/31/2015 9:06 PM
Surr: Phenol-d5 32.0 25.8-110 %RECNANA 3/31/2015 9:06 PM
Surr: 2,4,6-Tribromophenol 80.1 63.8-110 %RECNANA 3/31/2015 9:06 PM
Surr: Nitrobenzene-d5 97.2 61.8-110 %RECNANA 3/31/2015 9:06 PM
Surr: 2-Fluorobiphenyl 85.0 58.6-110 %RECNANA 3/31/2015 9:06 PM
Surr: 4-Terphenyl-d14 88.5 55.1-110 %RECNANA 3/31/2015 9:06 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 2:38 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 2:38 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 2:38 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 2:38 AM
Benzene 6.25 1.00 µg/L0.129 NA PA/VA3/31/2015 2:38 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 2:38 AM
Page 42 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 2:38 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 2:38 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 2:38 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 2:38 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 2:38 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 2:38 AM
Chlorobenzene 2.53 3.00 J µg/L0.177 NA PA/VA3/31/2015 2:38 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 2:38 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 2:38 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 2:38 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 2:38 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 2:38 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 2:38 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 2:38 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 2:38 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 2:38 AM
1,4-Dichlorobenzene 4.66 1.00 µg/L0.287 NA PA/VA3/31/2015 2:38 AM
Dichlorodifluoromethane ND 5.00 µg/L0.714 NA PA/VA3/31/2015 2:38 AM
1,1-Dichloroethane 0.800 5.00 J µg/L0.383 NA PA/VA3/31/2015 2:38 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 2:38 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 2:38 AM
cis-1,2-Dichloroethene 5.01 5.00 µg/L0.226 NA PA/VA3/31/2015 2:38 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 2:38 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 2:38 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 2:38 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 2:38 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 2:38 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 2:38 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 2:38 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 2:38 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 2:38 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 2:38 AM
Methylene chloride 3.34 1.00 µg/L0.539 NA PA/VA3/31/2015 2:38 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 2:38 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 2:38 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 2:38 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 2:38 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/31/2015 2:38 AM
Page 43 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:37:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-06A Matrix:Groundwater
MW-11Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 2:38 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 2:38 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 2:38 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/31/2015 2:38 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 2:38 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 2:38 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 2:38 AM
Vinyl chloride 1.20 1.00 µg/L0.223 NA PA/VA3/31/2015 2:38 AM
o-Xylene 1.24 1.00 µg/L0.186 NA PA/VA3/31/2015 2:38 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 2:38 AM
Surr: 1,2-Dichloroethane-d4 99.7 68.7-129 %RECNANA 3/31/2015 2:38 AM
Surr: 4-Bromofluorobenzene 103 71.8-127 %RECNANA 3/31/2015 2:38 AM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 3/31/2015 2:38 AM
Surr: Toluene-d8 93.7 71.4-129 %RECNANA 3/31/2015 2:38 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 2:38 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 2:38 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 2:38 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 2:38 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 2:38 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 2:38 AM
Surr: 1,2-Dichloroethane-d4 97.3 80-120 %RECNANA 3/31/2015 2:38 AM
Surr: 4-Bromofluorobenzene 98.2 80-120 %RECNANA 3/31/2015 2:38 AM
Surr: Dibromofluoromethane 90.2 80-120 %RECNANA 3/31/2015 2:38 AM
Surr: Toluene-d8 96.3 80-120 %RECNANA 3/31/2015 2:38 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 12:02 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 113 10 mg/L2.0 NA PA/VA3/27/2015 2:04 PM
Page 44 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 5:35 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Barium 0.0322 0.100 J mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:35 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:35 PM
Chromium 0.0020 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Copper 0.0042 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/3/2015 5:35 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/3/2015 5:35 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:35 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Vanadium ND 0.0250 mg/L0.0010 NA PA/VA4/3/2015 5:35 PM
Zinc 0.0036 0.0100 J mg/L0.0030 NA PA/VA4/3/2015 5:35 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:47 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
alpha-BHC ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
beta-BHC ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
delta-BHC ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
gamma-BHC ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
Chlordane ND 0.00507 mg/L0.00253 0.00050 3/31/2015 6:46 PM
4,4´-DDD ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
4,4´-DDE ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
4,4´-DDT ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
Dieldrin ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
Endosulfan I ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
Endosulfan II ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
Endosulfan sulfate ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
Endrin ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
Endrin aldehyde ND 0.000507 mg/L0.000253 0.00010 3/31/2015 6:46 PM
Heptachlor ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
Page 45 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000507 mg/L0.000253 0.00005 3/31/2015 6:46 PM
Methoxychlor ND 0.000507 mg/L0.000253 0.00100 3/31/2015 6:46 PM
Toxaphene ND 0.00507 mg/L0.00253 0.00100 3/31/2015 6:46 PM
Surr: Tetrachloro-m-xylene 106 30.6-137 %RECNANA 3/31/2015 6:46 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Aroclor 1221 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Aroclor 1232 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Aroclor 1242 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Aroclor 1248 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Aroclor 1254 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Aroclor 1260 ND 0.00051 mg/L0.00025 NA 3/31/2015 6:46 PM
Surr: Tetrachloro-m-xylene 72.5 23.9-150 %RECNANA 3/31/2015 6:46 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00247 mg/L0.000003 NA 4/8/2015 4:29 PM
2,4,5-TP (Silvex)ND 0.00247 mg/L0.000003 NA 4/8/2015 4:29 PM
2,4-D ND 0.00247 mg/L0.000005 NA 4/8/2015 4:29 PM
Dinoseb ND 0.00124 mg/L0.000005 NA 4/8/2015 4:29 PM
Surr: 2,4-Dichlorophenylacetic acid 71.2 21.8-182 %RECNANA 4/8/2015 4:29 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
1,3-Dinitrobenzene ND 0.0214 mg/L0.0053 NA 3/31/2015 9:33 PM
1,4-Napthoquinone ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
1-Naphthylamine ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
2,6-Dichlorophenol ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
2-Acetylaminofluorene ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
2-Naphthylamine ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
2-Picoline ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
3,3´-Dimethylbenzidine ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
3-Methylcholanthrene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
4-Aminobiphenyl ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
4-Nitroquinoline-1-oxide ND 0.0535 mg/LNANA 3/31/2015 9:33 PM
Page 46 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
7,12-Dimethylbenz(a)anthracene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Acetophenone ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Chlorobenzilate ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Diallate ND 0.0107 mg/L0.0021 NA 3/31/2015 9:33 PM
Dimethoate ND 0.0214 mg/L0.0053 NA 3/31/2015 9:33 PM
Diphenylamine ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Disulfoton ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Ethyl methacrylate ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Ethyl methanesulfonate ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
Famphur ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
Hexachlorophene ND 0.107 mg/LNANA 3/31/2015 9:33 PM
Hexachloropropene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Isodrin ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
Isosafrole ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Kepone ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
Methapyrilene ND 0.107 mg/LNANA 3/31/2015 9:33 PM
Methyl methacrylate ND 0.0321 mg/LNANA 4/4/2015 9:50 PM
Methyl methanesulfonate ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Methyl parathion ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
N-Nitroso-di-n-butylamine ND 0.0107 mg/L0.0021 NA 3/31/2015 9:33 PM
N-Nitrosodiethylamine ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
n-Nitrosomethylethylamine ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
N-Nitrosopiperidine ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
N-Nitrosopyrrolidine ND 0.0107 mg/L0.0021 NA 3/31/2015 9:33 PM
o,o,o-Triethylphosphorothioate ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0214 mg/LNANA 3/31/2015 9:33 PM
o-Toluidine ND 0.0107 mg/L0.0021 NA 3/31/2015 9:33 PM
p-Dimethylaminoazobenzene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
p-Phenylenediamine ND 0.0107 mg/LNANA 4/4/2015 9:50 PM
Parathion ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Pentachlorobenzene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Pentachloronitrobenzene ND 0.0214 mg/L0.0021 NA 3/31/2015 9:33 PM
Phenacetin ND 0.0214 mg/L0.0021 NA 3/31/2015 9:33 PM
Phorate ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Pronamide ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Safrole ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
sym-Trinitrobenzene ND 0.0107 mg/LNANA 3/31/2015 9:33 PM
Page 47 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0107 mg/L0NA PA/VA3/31/2015 9:33 PM
Acenaphthylene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Anthracene ND 0.0107 mg/LNANA PA/VA3/31/2015 9:33 PM
Benzo(a)anthracene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Benzo(a)pyrene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Benzo(b)fluoranthene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Benzo(g,h,i)perylene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Benzo(k)fluoranthene ND 0.0107 mg/L0.0032 NA PA/VA3/31/2015 9:33 PM
Benzyl alcohol ND 0.0214 mg/L0.0021 NA 3/31/2015 9:33 PM
Bis(2-chloroethoxy)methane ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Bis(2-chloroethyl)ether ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Bis(2-chloroisopropyl)ether ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Bis(2-ethylhexyl)phthalate ND 0.0160 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
4-Bromophenyl phenyl ether ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Butyl benzyl phthalate ND 0.0107 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
4-Chloroaniline ND 0.0214 mg/L0.0053 NA 3/31/2015 9:33 PM
4-Chloro-3-methylphenol ND 0.0214 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2-Chloronaphthalene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2-Chlorophenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
4-Chlorophenyl phenyl ether ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Chrysene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
o-Cresol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
m,p-Cresol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Dibenzo(a,h)anthracene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Dibenzofuran ND 0.0107 mg/LNANA PA/VA3/31/2015 9:33 PM
Di-n-butyl phthalate ND 0.0107 mg/LNANA PA/VA3/31/2015 9:33 PM
3,3´-Dichlorobenzidine ND 0.0214 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
2,4-Dichlorophenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Diethyl phthalate ND 6.42 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Dimethyl phthalate ND 0.0107 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
2,4-Dimethylphenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
4,6-Dinitro-2-methylphenol ND 0.0535 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2,4-Dinitrophenol ND 0.0535 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2,4-Dinitrotoluene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2,6-Dinitrotoluene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Di-n-octyl phthalate ND 0.0107 mg/LNANA PA/VA3/31/2015 9:33 PM
Fluoranthene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Fluorene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Page 48 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Hexachlorobutadiene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Hexachlorocyclopentadiene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Hexachloroethane ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Indeno(1,2,3-cd)pyrene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Isophorone ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2-Methylnaphthalene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Naphthalene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2-Nitroaniline ND 0.0535 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
3-Nitroaniline ND 0.0535 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
4-Nitroaniline ND 0.0214 mg/L0.0053 NA PA/VA3/31/2015 9:33 PM
Nitrobenzene ND 0.0107 mg/LNANA PA/VA3/31/2015 9:33 PM
2-Nitrophenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
4-Nitrophenol ND 0.0535 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
N-Nitrosodimethylamine ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
N-Nitrosodiphenylamine ND 0.0107 mg/L0NA PA/VA3/31/2015 9:33 PM
N-Nitrosodi-n-propylamine ND 0.0107 mg/L0NA PA/VA3/31/2015 9:33 PM
Pentachlorophenol ND 0.0267 mg/L0NA PA/VA3/31/2015 9:33 PM
Phenanthrene ND 0.0107 mg/L0NA PA/VA3/31/2015 9:33 PM
Phenol ND 0.0107 mg/L0NA PA/VA3/31/2015 9:33 PM
Pyrene ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2,3,4,6-Tetrachlorophenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
1,2,4-Trichlorobenzene ND 0.0107 mg/L0.0021 NA 3/31/2015 9:33 PM
2,4,5-Trichlorophenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
2,4,6-Trichlorophenol ND 0.0107 mg/L0.0021 NA PA/VA3/31/2015 9:33 PM
Surr: 2-Fluorophenol 42.0 32.9-110 %RECNANA 3/31/2015 9:33 PM
Surr: Phenol-d5 31.8 25.8-110 %RECNANA 3/31/2015 9:33 PM
Surr: 2,4,6-Tribromophenol 77.9 63.8-110 %RECNANA 3/31/2015 9:33 PM
Surr: Nitrobenzene-d5 98.0 61.8-110 %RECNANA 3/31/2015 9:33 PM
Surr: 2-Fluorobiphenyl 83.7 58.6-110 %RECNANA 3/31/2015 9:33 PM
Surr: 4-Terphenyl-d14 78.6 55.1-110 %RECNANA 3/31/2015 9:33 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 3:11 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 3:11 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 3:11 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 3:11 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/31/2015 3:11 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 3:11 AM
Page 49 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 3:11 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 3:11 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 3:11 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 3:11 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 3:11 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 3:11 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/31/2015 3:11 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 3:11 AM
Chloroform 1.60 5.00 J µg/L0.253 NA PA/VA3/31/2015 3:11 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 3:11 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 3:11 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 3:11 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 3:11 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 3:11 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 3:11 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 3:11 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/31/2015 3:11 AM
Dichlorodifluoromethane ND 5.00 µg/L0.714 NA PA/VA3/31/2015 3:11 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/31/2015 3:11 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 3:11 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 3:11 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/31/2015 3:11 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 3:11 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 3:11 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 3:11 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 3:11 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 3:11 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 3:11 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 3:11 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 3:11 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 3:11 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 3:11 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/31/2015 3:11 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 3:11 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 3:11 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 3:11 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 3:11 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/31/2015 3:11 AM
Page 50 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:40:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-07A Matrix:Groundwater
MW-20Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 3:11 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 3:11 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 3:11 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/31/2015 3:11 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 3:11 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 3:11 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 3:11 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 3:11 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 3:11 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 3:11 AM
Surr: 1,2-Dichloroethane-d4 109 68.7-129 %RECNANA 3/31/2015 3:11 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 3/31/2015 3:11 AM
Surr: Dibromofluoromethane 110 74.3-124 %RECNANA 3/31/2015 3:11 AM
Surr: Toluene-d8 90.4 71.4-129 %RECNANA 3/31/2015 3:11 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 3:11 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 3:11 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 3:11 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 3:11 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 3:11 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 3:11 AM
Surr: 1,2-Dichloroethane-d4 112 80-120 %RECNANA 3/31/2015 3:11 AM
Surr: 4-Bromofluorobenzene 92.9 80-120 %RECNANA 3/31/2015 3:11 AM
Surr: Dibromofluoromethane 95.3 80-120 %RECNANA 3/31/2015 3:11 AM
Surr: Toluene-d8 93.1 80-120 %RECNANA 3/31/2015 3:11 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 12:03 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 121 10 mg/L2.0 NA PA/VA3/27/2015 2:04 PM
Page 51 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 5:40 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Barium 0.0559 0.100 J mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:40 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:40 PM
Chromium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Cobalt 0.0016 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Copper 0.0013 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/3/2015 5:40 PM
Nickel 0.0021 0.0500 J mg/L0.0020 NA PA/VA4/3/2015 5:40 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:40 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Vanadium ND 0.0250 mg/L0.0010 NA PA/VA4/3/2015 5:40 PM
Zinc 0.0049 0.0100 J mg/L0.0030 NA PA/VA4/3/2015 5:40 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:50 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
alpha-BHC ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
beta-BHC ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
delta-BHC ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
gamma-BHC ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
Chlordane ND 0.00505 mg/L0.00253 0.00050 3/31/2015 7:00 PM
4,4´-DDD ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
4,4´-DDE ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
4,4´-DDT ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
Dieldrin ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
Endosulfan I ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
Endosulfan II ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
Endosulfan sulfate ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
Endrin ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
Endrin aldehyde ND 0.000505 mg/L0.000253 0.00010 3/31/2015 7:00 PM
Heptachlor ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
Page 52 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000505 mg/L0.000253 0.00005 3/31/2015 7:00 PM
Methoxychlor ND 0.000505 mg/L0.000253 0.00100 3/31/2015 7:00 PM
Toxaphene ND 0.00505 mg/L0.00253 0.00100 3/31/2015 7:00 PM
Surr: Tetrachloro-m-xylene 102 30.6-137 %RECNANA 3/31/2015 7:00 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Aroclor 1221 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Aroclor 1232 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Aroclor 1242 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Aroclor 1248 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Aroclor 1254 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Aroclor 1260 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:00 PM
Surr: Tetrachloro-m-xylene 70.5 23.9-150 %RECNANA 3/31/2015 7:00 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00237 mg/L0.000003 NA 4/8/2015 4:46 PM
2,4,5-TP (Silvex)ND 0.00237 mg/L0.000002 NA 4/8/2015 4:46 PM
2,4-D ND 0.00237 mg/L0.000005 NA 4/8/2015 4:46 PM
Dinoseb ND 0.00119 mg/L0.000005 NA 4/8/2015 4:46 PM
Surr: 2,4-Dichlorophenylacetic acid 62.1 21.8-182 %RECNANA 4/8/2015 4:46 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
1,3-Dinitrobenzene ND 0.0205 mg/L0.0051 NA 3/31/2015 9:59 PM
1,4-Napthoquinone ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
1-Naphthylamine ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
2,6-Dichlorophenol ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
2-Acetylaminofluorene ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
2-Naphthylamine ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
2-Picoline ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
3,3´-Dimethylbenzidine ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
3-Methylcholanthrene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
4-Aminobiphenyl ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
4-Nitroquinoline-1-oxide ND 0.0512 mg/LNANA 3/31/2015 9:59 PM
Page 53 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
7,12-Dimethylbenz(a)anthracene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Acetophenone ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Chlorobenzilate ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Diallate ND 0.0102 mg/L0.0020 NA 3/31/2015 9:59 PM
Dimethoate ND 0.0205 mg/L0.0051 NA 3/31/2015 9:59 PM
Diphenylamine ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Disulfoton ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Ethyl methacrylate ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Ethyl methanesulfonate ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
Famphur ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
Hexachlorophene ND 0.102 mg/LNANA 3/31/2015 9:59 PM
Hexachloropropene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Isodrin ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
Isosafrole ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Kepone ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
Methapyrilene ND 0.102 mg/LNANA 3/31/2015 9:59 PM
Methyl methacrylate ND 0.0307 mg/LNANA 4/4/2015 10:11 PM
Methyl methanesulfonate ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Methyl parathion ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
N-Nitroso-di-n-butylamine ND 0.0102 mg/L0.0020 NA 3/31/2015 9:59 PM
N-Nitrosodiethylamine ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
n-Nitrosomethylethylamine ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
N-Nitrosopiperidine ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
N-Nitrosopyrrolidine ND 0.0102 mg/L0.0020 NA 3/31/2015 9:59 PM
o,o,o-Triethylphosphorothioate ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0205 mg/LNANA 3/31/2015 9:59 PM
o-Toluidine ND 0.0102 mg/L0.0020 NA 3/31/2015 9:59 PM
p-Dimethylaminoazobenzene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
p-Phenylenediamine ND 0.0102 mg/LNANA 4/4/2015 10:11 PM
Parathion ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Pentachlorobenzene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Pentachloronitrobenzene ND 0.0205 mg/L0.0020 NA 3/31/2015 9:59 PM
Phenacetin ND 0.0205 mg/L0.0020 NA 3/31/2015 9:59 PM
Phorate ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Pronamide ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Safrole ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
sym-Trinitrobenzene ND 0.0102 mg/LNANA 3/31/2015 9:59 PM
Page 54 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0102 mg/L0NA PA/VA3/31/2015 9:59 PM
Acenaphthylene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Anthracene ND 0.0102 mg/LNANA PA/VA3/31/2015 9:59 PM
Benzo(a)anthracene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Benzo(a)pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Benzo(b)fluoranthene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Benzo(g,h,i)perylene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Benzo(k)fluoranthene ND 0.0102 mg/L0.0031 NA PA/VA3/31/2015 9:59 PM
Benzyl alcohol ND 0.0205 mg/L0.0020 NA 3/31/2015 9:59 PM
Bis(2-chloroethoxy)methane ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Bis(2-chloroethyl)ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Bis(2-chloroisopropyl)ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Bis(2-ethylhexyl)phthalate ND 0.0154 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
4-Bromophenyl phenyl ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Butyl benzyl phthalate ND 0.0102 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
4-Chloroaniline ND 0.0205 mg/L0.0051 NA 3/31/2015 9:59 PM
4-Chloro-3-methylphenol ND 0.0205 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2-Chloronaphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2-Chlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
4-Chlorophenyl phenyl ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Chrysene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
o-Cresol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
m,p-Cresol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Dibenzo(a,h)anthracene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Dibenzofuran ND 0.0102 mg/LNANA PA/VA3/31/2015 9:59 PM
Di-n-butyl phthalate ND 0.0102 mg/LNANA PA/VA3/31/2015 9:59 PM
3,3´-Dichlorobenzidine ND 0.0205 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
2,4-Dichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Diethyl phthalate ND 6.14 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Dimethyl phthalate ND 0.0102 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
2,4-Dimethylphenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
4,6-Dinitro-2-methylphenol ND 0.0512 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2,4-Dinitrophenol ND 0.0512 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2,4-Dinitrotoluene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2,6-Dinitrotoluene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Di-n-octyl phthalate ND 0.0102 mg/LNANA PA/VA3/31/2015 9:59 PM
Fluoranthene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Fluorene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Page 55 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Hexachlorobutadiene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Hexachlorocyclopentadiene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Hexachloroethane ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Indeno(1,2,3-cd)pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Isophorone ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2-Methylnaphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Naphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2-Nitroaniline ND 0.0512 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
3-Nitroaniline ND 0.0512 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
4-Nitroaniline ND 0.0205 mg/L0.0051 NA PA/VA3/31/2015 9:59 PM
Nitrobenzene ND 0.0102 mg/LNANA PA/VA3/31/2015 9:59 PM
2-Nitrophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
4-Nitrophenol ND 0.0512 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
N-Nitrosodimethylamine ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
N-Nitrosodiphenylamine ND 0.0102 mg/L0NA PA/VA3/31/2015 9:59 PM
N-Nitrosodi-n-propylamine ND 0.0102 mg/L0NA PA/VA3/31/2015 9:59 PM
Pentachlorophenol ND 0.0256 mg/L0NA PA/VA3/31/2015 9:59 PM
Phenanthrene ND 0.0102 mg/L0NA PA/VA3/31/2015 9:59 PM
Phenol ND 0.0102 mg/L0NA PA/VA3/31/2015 9:59 PM
Pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2,3,4,6-Tetrachlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
1,2,4-Trichlorobenzene ND 0.0102 mg/L0.0020 NA 3/31/2015 9:59 PM
2,4,5-Trichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
2,4,6-Trichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 9:59 PM
Surr: 2-Fluorophenol 40.3 32.9-110 %RECNANA 3/31/2015 9:59 PM
Surr: Phenol-d5 30.7 25.8-110 %RECNANA 3/31/2015 9:59 PM
Surr: 2,4,6-Tribromophenol 76.4 63.8-110 %RECNANA 3/31/2015 9:59 PM
Surr: Nitrobenzene-d5 99.3 61.8-110 %RECNANA 3/31/2015 9:59 PM
Surr: 2-Fluorobiphenyl 82.3 58.6-110 %RECNANA 3/31/2015 9:59 PM
Surr: 4-Terphenyl-d14 83.6 55.1-110 %RECNANA 3/31/2015 9:59 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 3:44 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 3:44 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 3:44 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 3:44 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/31/2015 3:44 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 3:44 AM
Page 56 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 3:44 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 3:44 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 3:44 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 3:44 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 3:44 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 3:44 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/31/2015 3:44 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 3:44 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 3:44 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 3:44 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 3:44 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 3:44 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 3:44 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 3:44 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 3:44 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 3:44 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/31/2015 3:44 AM
Dichlorodifluoromethane ND 5.00 µg/L0.714 NA PA/VA3/31/2015 3:44 AM
1,1-Dichloroethane 0.860 5.00 J µg/L0.383 NA PA/VA3/31/2015 3:44 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 3:44 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 3:44 AM
cis-1,2-Dichloroethene 0.710 5.00 J µg/L0.226 NA PA/VA3/31/2015 3:44 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 3:44 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 3:44 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 3:44 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 3:44 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 3:44 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 3:44 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 3:44 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 3:44 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 3:44 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 3:44 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/31/2015 3:44 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 3:44 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 3:44 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 3:44 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 3:44 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/31/2015 3:44 AM
Page 57 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:50:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-08A Matrix:Groundwater
SW-1Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 3:44 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 3:44 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 3:44 AM
Trichloroethene 0.700 1.00 J µg/L0.302 NA PA/VA3/31/2015 3:44 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 3:44 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 3:44 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 3:44 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 3:44 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 3:44 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 3:44 AM
Surr: 1,2-Dichloroethane-d4 107 68.7-129 %RECNANA 3/31/2015 3:44 AM
Surr: 4-Bromofluorobenzene 102 71.8-127 %RECNANA 3/31/2015 3:44 AM
Surr: Dibromofluoromethane 107 74.3-124 %RECNANA 3/31/2015 3:44 AM
Surr: Toluene-d8 93.6 71.4-129 %RECNANA 3/31/2015 3:44 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 3:44 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 3:44 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 3:44 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 3:44 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 3:44 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 3:44 AM
Surr: 1,2-Dichloroethane-d4 103 80-120 %RECNANA 3/31/2015 3:44 AM
Surr: 4-Bromofluorobenzene 90.2 80-120 %RECNANA 3/31/2015 3:44 AM
Surr: Dibromofluoromethane 101 80-120 %RECNANA 3/31/2015 3:44 AM
Surr: Toluene-d8 96.3 80-120 %RECNANA 3/31/2015 3:44 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 12:03 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 2.0 5.0 J mg/L1.0 NA PA/VA3/27/2015 2:04 PM
Page 58 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 5:46 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Barium 0.0256 0.100 J mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:46 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:46 PM
Chromium 0.0033 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Copper 0.0025 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Lead 0.0003 0.0100 J mg/L0.0002 NA PA/VA4/3/2015 5:46 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/3/2015 5:46 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:46 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Vanadium 0.0037 0.0250 J mg/L0.0010 NA PA/VA4/3/2015 5:46 PM
Zinc 0.0092 0.0100 J mg/L0.0030 NA PA/VA4/3/2015 5:46 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:52 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
alpha-BHC ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
beta-BHC ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
delta-BHC ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
gamma-BHC ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
Chlordane ND 0.00508 mg/L0.00254 0.00050 3/31/2015 7:15 PM
4,4´-DDD ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
4,4´-DDE ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
4,4´-DDT ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
Dieldrin ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
Endosulfan I ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
Endosulfan II ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
Endosulfan sulfate ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
Endrin ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
Endrin aldehyde ND 0.000508 mg/L0.000254 0.00010 3/31/2015 7:15 PM
Heptachlor ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
Page 59 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000508 mg/L0.000254 0.00005 3/31/2015 7:15 PM
Methoxychlor ND 0.000508 mg/L0.000254 0.00100 3/31/2015 7:15 PM
Toxaphene ND 0.00508 mg/L0.00254 0.00100 3/31/2015 7:15 PM
Surr: Tetrachloro-m-xylene 95.0 30.6-137 %RECNANA 3/31/2015 7:15 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Aroclor 1221 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Aroclor 1232 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Aroclor 1242 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Aroclor 1248 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Aroclor 1254 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Aroclor 1260 ND 0.00051 mg/L0.00025 NA 3/31/2015 7:15 PM
Surr: Tetrachloro-m-xylene 66.0 23.9-150 %RECNANA 3/31/2015 7:15 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00249 mg/L0.000003 NA 4/8/2015 5:04 PM
2,4,5-TP (Silvex)ND 0.00249 mg/L0.000003 NA 4/8/2015 5:04 PM
2,4-D ND 0.00249 mg/L0.000005 NA 4/8/2015 5:04 PM
Dinoseb ND 0.00125 mg/L0.000005 NA 4/8/2015 5:04 PM
Surr: 2,4-Dichlorophenylacetic acid 63.7 21.8-182 %RECNANA 4/8/2015 5:04 PM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
1,3-Dinitrobenzene ND 0.0203 mg/L0.0051 NA 3/31/2015 10:25 PM
1,4-Napthoquinone ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
1-Naphthylamine ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
2,6-Dichlorophenol ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
2-Acetylaminofluorene ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
2-Naphthylamine ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
2-Picoline ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
3,3´-Dimethylbenzidine ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
3-Methylcholanthrene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
4-Aminobiphenyl ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
4-Nitroquinoline-1-oxide ND 0.0507 mg/LNANA 3/31/2015 10:25 PM
Page 60 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
7,12-Dimethylbenz(a)anthracene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Acetophenone ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Chlorobenzilate ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Diallate ND 0.0101 mg/L0.0020 NA 3/31/2015 10:25 PM
Dimethoate ND 0.0203 mg/L0.0051 NA 3/31/2015 10:25 PM
Diphenylamine ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Disulfoton ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Ethyl methacrylate ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Ethyl methanesulfonate ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
Famphur ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
Hexachlorophene ND 0.101 mg/LNANA 3/31/2015 10:25 PM
Hexachloropropene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Isodrin ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
Isosafrole ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Kepone ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
Methapyrilene ND 0.101 mg/LNANA 3/31/2015 10:25 PM
Methyl methacrylate ND 0.0304 mg/LNANA 4/4/2015 10:33 PM
Methyl methanesulfonate ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Methyl parathion ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
N-Nitroso-di-n-butylamine ND 0.0101 mg/L0.0020 NA 3/31/2015 10:25 PM
N-Nitrosodiethylamine ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
n-Nitrosomethylethylamine ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
N-Nitrosopiperidine ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
N-Nitrosopyrrolidine ND 0.0101 mg/L0.0020 NA 3/31/2015 10:25 PM
o,o,o-Triethylphosphorothioate ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0203 mg/LNANA 3/31/2015 10:25 PM
o-Toluidine ND 0.0101 mg/L0.0020 NA 3/31/2015 10:25 PM
p-Dimethylaminoazobenzene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
p-Phenylenediamine ND 0.0101 mg/LNANA 4/4/2015 10:33 PM
Parathion ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Pentachlorobenzene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Pentachloronitrobenzene ND 0.0203 mg/L0.0020 NA 3/31/2015 10:25 PM
Phenacetin ND 0.0203 mg/L0.0020 NA 3/31/2015 10:25 PM
Phorate ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Pronamide ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Safrole ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
sym-Trinitrobenzene ND 0.0101 mg/LNANA 3/31/2015 10:25 PM
Page 61 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0101 mg/L0NA PA/VA3/31/2015 10:25 PM
Acenaphthylene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Anthracene ND 0.0101 mg/LNANA PA/VA3/31/2015 10:25 PM
Benzo(a)anthracene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Benzo(a)pyrene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Benzo(b)fluoranthene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Benzo(g,h,i)perylene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Benzo(k)fluoranthene ND 0.0101 mg/L0.0030 NA PA/VA3/31/2015 10:25 PM
Benzyl alcohol ND 0.0203 mg/L0.0020 NA 3/31/2015 10:25 PM
Bis(2-chloroethoxy)methane ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Bis(2-chloroethyl)ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Bis(2-chloroisopropyl)ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Bis(2-ethylhexyl)phthalate ND 0.0152 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
4-Bromophenyl phenyl ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Butyl benzyl phthalate ND 0.0101 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
4-Chloroaniline ND 0.0203 mg/L0.0051 NA 3/31/2015 10:25 PM
4-Chloro-3-methylphenol ND 0.0203 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2-Chloronaphthalene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2-Chlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
4-Chlorophenyl phenyl ether ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Chrysene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
o-Cresol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
m,p-Cresol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Dibenzo(a,h)anthracene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Dibenzofuran ND 0.0101 mg/LNANA PA/VA3/31/2015 10:25 PM
Di-n-butyl phthalate ND 0.0101 mg/LNANA PA/VA3/31/2015 10:25 PM
3,3´-Dichlorobenzidine ND 0.0203 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
2,4-Dichlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Diethyl phthalate ND 6.08 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Dimethyl phthalate ND 0.0101 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
2,4-Dimethylphenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
4,6-Dinitro-2-methylphenol ND 0.0507 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2,4-Dinitrophenol ND 0.0507 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2,4-Dinitrotoluene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2,6-Dinitrotoluene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Di-n-octyl phthalate ND 0.0101 mg/LNANA PA/VA3/31/2015 10:25 PM
Fluoranthene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Fluorene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Page 62 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Hexachlorobutadiene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Hexachlorocyclopentadiene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Hexachloroethane ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Indeno(1,2,3-cd)pyrene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Isophorone ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2-Methylnaphthalene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Naphthalene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2-Nitroaniline ND 0.0507 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
3-Nitroaniline ND 0.0507 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
4-Nitroaniline ND 0.0203 mg/L0.0051 NA PA/VA3/31/2015 10:25 PM
Nitrobenzene ND 0.0101 mg/LNANA PA/VA3/31/2015 10:25 PM
2-Nitrophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
4-Nitrophenol ND 0.0507 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
N-Nitrosodimethylamine ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
N-Nitrosodiphenylamine ND 0.0101 mg/L0NA PA/VA3/31/2015 10:25 PM
N-Nitrosodi-n-propylamine ND 0.0101 mg/L0NA PA/VA3/31/2015 10:25 PM
Pentachlorophenol ND 0.0253 mg/L0NA PA/VA3/31/2015 10:25 PM
Phenanthrene ND 0.0101 mg/L0NA PA/VA3/31/2015 10:25 PM
Phenol ND 0.0101 mg/L0NA PA/VA3/31/2015 10:25 PM
Pyrene ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2,3,4,6-Tetrachlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
1,2,4-Trichlorobenzene ND 0.0101 mg/L0.0020 NA 3/31/2015 10:25 PM
2,4,5-Trichlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
2,4,6-Trichlorophenol ND 0.0101 mg/L0.0020 NA PA/VA3/31/2015 10:25 PM
Surr: 2-Fluorophenol 40.7 32.9-110 %RECNANA 3/31/2015 10:25 PM
Surr: Phenol-d5 31.2 25.8-110 %RECNANA 3/31/2015 10:25 PM
Surr: 2,4,6-Tribromophenol 80.4 63.8-110 %RECNANA 3/31/2015 10:25 PM
Surr: Nitrobenzene-d5 97.8 61.8-110 %RECNANA 3/31/2015 10:25 PM
Surr: 2-Fluorobiphenyl 84.0 58.6-110 %RECNANA 3/31/2015 10:25 PM
Surr: 4-Terphenyl-d14 84.7 55.1-110 %RECNANA 3/31/2015 10:25 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 4:17 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 4:17 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 4:17 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 4:17 AM
Benzene ND 1.00 µg/L0.129 NA PA/VA3/31/2015 4:17 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 4:17 AM
Page 63 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 4:17 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 4:17 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 4:17 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 4:17 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 4:17 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 4:17 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/31/2015 4:17 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 4:17 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 4:17 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 4:17 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 4:17 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 4:17 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 4:17 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 4:17 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 4:17 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 4:17 AM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA3/31/2015 4:17 AM
Dichlorodifluoromethane ND 5.00 µg/L0.714 NA PA/VA3/31/2015 4:17 AM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA3/31/2015 4:17 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 4:17 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 4:17 AM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA3/31/2015 4:17 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 4:17 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 4:17 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 4:17 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 4:17 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 4:17 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 4:17 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 4:17 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 4:17 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 4:17 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 4:17 AM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA3/31/2015 4:17 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 4:17 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 4:17 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 4:17 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 4:17 AM
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA3/31/2015 4:17 AM
Page 64 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 3:00:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-09A Matrix:Groundwater
SW-3Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 4:17 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 4:17 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 4:17 AM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA3/31/2015 4:17 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 4:17 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 4:17 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 4:17 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 4:17 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 4:17 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 4:17 AM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 3/31/2015 4:17 AM
Surr: 4-Bromofluorobenzene 102 71.8-127 %RECNANA 3/31/2015 4:17 AM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 3/31/2015 4:17 AM
Surr: Toluene-d8 92.0 71.4-129 %RECNANA 3/31/2015 4:17 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 4:17 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 4:17 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 4:17 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 4:17 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 4:17 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 4:17 AM
Surr: 1,2-Dichloroethane-d4 97.8 80-120 %RECNANA 3/31/2015 4:17 AM
Surr: 4-Bromofluorobenzene 90.1 80-120 %RECNANA 3/31/2015 4:17 AM
Surr: Dibromofluoromethane 99.4 80-120 %RECNANA 3/31/2015 4:17 AM
Surr: Toluene-d8 94.4 80-120 %RECNANA 3/31/2015 4:17 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 4:34 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 4.0 5.0 J mg/L1.0 NA PA/VA3/27/2015 2:04 PM
Page 65 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Antimony ND 0.0060 mg/L0.0002 NA PA/VA4/3/2015 5:52 PM
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Barium 0.204 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Beryllium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:52 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/3/2015 5:52 PM
Chromium 0.0018 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Cobalt ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Copper 0.0014 0.0100 J mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Lead ND 0.0100 mg/L0.0002 NA PA/VA4/3/2015 5:52 PM
Nickel ND 0.0500 mg/L0.0020 NA PA/VA4/3/2015 5:52 PM
Selenium ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Thallium ND 0.0055 mg/L0.0002 NA PA/VA4/3/2015 5:52 PM
Tin ND 0.100 mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Vanadium 0.0075 0.0250 J mg/L0.0010 NA PA/VA4/3/2015 5:52 PM
Zinc 0.0045 0.0100 J mg/L0.0030 NA PA/VA4/3/2015 5:52 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury 0.0001 0.0010 J mg/L0.0001 NA PA/VA3/31/2015 10:54 AM
PESTICIDES Method: SW8081B (2000)Analyst: NC
Aldrin ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
alpha-BHC ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
beta-BHC ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
delta-BHC ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
gamma-BHC ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
Chlordane ND 0.00503 mg/L0.00251 0.00050 3/31/2015 7:29 PM
4,4´-DDD ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
4,4´-DDE ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
4,4´-DDT ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
Dieldrin ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
Endosulfan I ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
Endosulfan II ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
Endosulfan sulfate ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
Endrin ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
Endrin aldehyde ND 0.000503 mg/L0.000251 0.00010 3/31/2015 7:29 PM
Heptachlor ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
Page 66 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Heptachlor epoxide ND 0.000503 mg/L0.000251 0.00005 3/31/2015 7:29 PM
Methoxychlor ND 0.000503 mg/L0.000251 0.00100 3/31/2015 7:29 PM
Toxaphene ND 0.00503 mg/L0.00251 0.00100 3/31/2015 7:29 PM
Surr: Tetrachloro-m-xylene 105 30.6-137 %RECNANA 3/31/2015 7:29 PM
Notes:
The ending CCV for pesticides exceeded REIC control limits indicating a high bias. Since the analyte result was ND, this exceedance does
not adversely impact data usability.
PCBS Method: SW8082A (2/07)Analyst: NC
Aroclor 1016 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Aroclor 1221 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Aroclor 1232 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Aroclor 1242 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Aroclor 1248 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Aroclor 1254 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Aroclor 1260 ND 0.00050 mg/L0.00025 NA 3/31/2015 7:29 PM
Surr: Tetrachloro-m-xylene 72.0 23.9-150 %RECNANA 3/31/2015 7:29 PM
CHLORINATED HERBICIDES Method: SW8151A (1998)Analyst: TS
2,4,5-T ND 0.00238 mg/L0.000003 NA 4/7/2015 9:05 AM
2,4,5-TP (Silvex)ND 0.00238 mg/L0.000002 NA 4/7/2015 9:05 AM
2,4-D ND 0.00238 mg/L0.000005 NA 4/7/2015 9:05 AM
Dinoseb ND 0.00119 mg/L0.000005 NA 4/7/2015 9:05 AM
Surr: 2,4-Dichlorophenylacetic acid 68.6 21.8-182 %RECNANA 4/7/2015 9:05 AM
Notes:
The associated batch matrix spike exceeds REIC control limits.
SEMIVOLATILE ORGANIC COMPOUNDS Method: SW8270D (2007)Analyst: JD
1,2,4,5-Tetrachlorobenzene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
1,3-Dinitrobenzene ND 0.0204 mg/L0.0051 NA 3/31/2015 6:25 PM
1,4-Napthoquinone ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
1-Naphthylamine ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
2,6-Dichlorophenol ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
2-Acetylaminofluorene ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
2-Naphthylamine ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
2-Picoline ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
3,3´-Dimethylbenzidine ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
3-Methylcholanthrene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
4-Aminobiphenyl ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
4-Nitroquinoline-1-oxide ND 0.0509 mg/LNANA 3/31/2015 6:25 PM
Page 67 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
5-Nitro-o-toluidine ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
7,12-Dimethylbenz(a)anthracene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Acetophenone ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Chlorobenzilate ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Diallate ND 0.0102 mg/L0.0020 NA 3/31/2015 6:25 PM
Dimethoate ND 0.0204 mg/L0.0051 NA 3/31/2015 6:25 PM
Diphenylamine ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Disulfoton ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Ethyl methacrylate ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Ethyl methanesulfonate ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
Famphur ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
Hexachlorophene ND 0.102 mg/LNANA 3/31/2015 6:25 PM
Hexachloropropene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Isodrin ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
Isosafrole ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Kepone ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
Methapyrilene ND 0.102 mg/LNANA 3/31/2015 6:25 PM
Methyl methacrylate ND 0.0306 mg/LNANA 4/4/2015 10:55 PM
Methyl methanesulfonate ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Methyl parathion ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
N-Nitroso-di-n-butylamine ND 0.0102 mg/L0.0020 NA 3/31/2015 6:25 PM
N-Nitrosodiethylamine ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
n-Nitrosomethylethylamine ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
N-Nitrosopiperidine ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
N-Nitrosopyrrolidine ND 0.0102 mg/L0.0020 NA 3/31/2015 6:25 PM
o,o,o-Triethylphosphorothioate ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
o,o-Diethyl-o-2-pyrazinyl
phosphorothioate
ND 0.0204 mg/LNANA 3/31/2015 6:25 PM
o-Toluidine ND 0.0102 mg/L0.0020 NA 3/31/2015 6:25 PM
p-Dimethylaminoazobenzene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
p-Phenylenediamine ND 0.0102 mg/LNANA 4/4/2015 10:55 PM
Parathion ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Pentachlorobenzene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Pentachloronitrobenzene ND 0.0204 mg/L0.0020 NA 3/31/2015 6:25 PM
Phenacetin ND 0.0204 mg/L0.0020 NA 3/31/2015 6:25 PM
Phorate ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Pronamide ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Safrole ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
sym-Trinitrobenzene ND 0.0102 mg/LNANA 3/31/2015 6:25 PM
Page 68 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Acenaphthene ND 0.0102 mg/L0NA PA/VA3/31/2015 6:25 PM
Acenaphthylene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Anthracene ND 0.0102 mg/LNANA PA/VA3/31/2015 6:25 PM
Benzo(a)anthracene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Benzo(a)pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Benzo(b)fluoranthene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Benzo(g,h,i)perylene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Benzo(k)fluoranthene ND 0.0102 mg/L0.0031 NA PA/VA3/31/2015 6:25 PM
Benzyl alcohol ND 0.0204 mg/L0.0020 NA 3/31/2015 6:25 PM
Bis(2-chloroethoxy)methane ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Bis(2-chloroethyl)ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Bis(2-chloroisopropyl)ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Bis(2-ethylhexyl)phthalate ND 0.0153 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
4-Bromophenyl phenyl ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Butyl benzyl phthalate ND 0.0102 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
4-Chloroaniline ND 0.0204 mg/L0.0051 NA 3/31/2015 6:25 PM
4-Chloro-3-methylphenol ND 0.0204 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2-Chloronaphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2-Chlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
4-Chlorophenyl phenyl ether ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Chrysene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
o-Cresol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
m,p-Cresol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Dibenzo(a,h)anthracene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Dibenzofuran ND 0.0102 mg/LNANA PA/VA3/31/2015 6:25 PM
Di-n-butyl phthalate ND 0.0102 mg/LNANA PA/VA3/31/2015 6:25 PM
3,3´-Dichlorobenzidine ND 0.0204 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
2,4-Dichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Diethyl phthalate ND 6.11 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Dimethyl phthalate ND 0.0102 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
2,4-Dimethylphenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
4,6-Dinitro-2-methylphenol ND 0.0509 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2,4-Dinitrophenol ND 0.0509 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2,4-Dinitrotoluene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2,6-Dinitrotoluene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Di-n-octyl phthalate ND 0.0102 mg/LNANA PA/VA3/31/2015 6:25 PM
Fluoranthene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Fluorene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Page 69 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Hexachlorobenzene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Hexachlorobutadiene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Hexachlorocyclopentadiene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Hexachloroethane ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Indeno(1,2,3-cd)pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Isophorone ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2-Methylnaphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Naphthalene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2-Nitroaniline ND 0.0509 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
3-Nitroaniline ND 0.0509 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
4-Nitroaniline ND 0.0204 mg/L0.0051 NA PA/VA3/31/2015 6:25 PM
Nitrobenzene ND 0.0102 mg/LNANA PA/VA3/31/2015 6:25 PM
2-Nitrophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
4-Nitrophenol ND 0.0509 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
N-Nitrosodimethylamine ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
N-Nitrosodiphenylamine ND 0.0102 mg/L0NA PA/VA3/31/2015 6:25 PM
N-Nitrosodi-n-propylamine ND 0.0102 mg/L0NA PA/VA3/31/2015 6:25 PM
Pentachlorophenol ND 0.0255 mg/L0NA PA/VA3/31/2015 6:25 PM
Phenanthrene ND 0.0102 mg/L0NA PA/VA3/31/2015 6:25 PM
Phenol ND 0.0102 mg/L0NA PA/VA3/31/2015 6:25 PM
Pyrene ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2,3,4,6-Tetrachlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
1,2,4-Trichlorobenzene ND 0.0102 mg/L0.0020 NA 3/31/2015 6:25 PM
2,4,5-Trichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
2,4,6-Trichlorophenol ND 0.0102 mg/L0.0020 NA PA/VA3/31/2015 6:25 PM
Surr: 2-Fluorophenol 38.1 32.9-110 %RECNANA 3/31/2015 6:25 PM
Surr: Phenol-d5 29.2 25.8-110 %RECNANA 3/31/2015 6:25 PM
Surr: 2,4,6-Tribromophenol 72.1 63.8-110 %RECNANA 3/31/2015 6:25 PM
Surr: Nitrobenzene-d5 87.3 61.8-110 %RECNANA 3/31/2015 6:25 PM
Surr: 2-Fluorobiphenyl 76.1 58.6-110 %RECNANA 3/31/2015 6:25 PM
Surr: 4-Terphenyl-d14 79.2 55.1-110 %RECNANA 3/31/2015 6:25 PM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/31/2015 4:50 AM
Acetone ND 100 µg/L4.88 NA PA/VA3/31/2015 4:50 AM
Acrolein ND 53.0 µg/L4.36 NA PA/VA3/31/2015 4:50 AM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA3/31/2015 4:50 AM
Benzene 2.10 1.00 µg/L0.129 NA PA/VA3/31/2015 4:50 AM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA3/31/2015 4:50 AM
Page 70 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA3/31/2015 4:50 AM
Bromoform ND 3.00 µg/L0.400 NA PA/VA3/31/2015 4:50 AM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA3/31/2015 4:50 AM
2-Butanone ND 100 µg/L4.68 NA PA/VA3/31/2015 4:50 AM
Carbon disulfide ND 100 µg/L1.27 NA 3/31/2015 4:50 AM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA3/31/2015 4:50 AM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA3/31/2015 4:50 AM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA3/31/2015 4:50 AM
Chloroform ND 5.00 µg/L0.253 NA PA/VA3/31/2015 4:50 AM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA3/31/2015 4:50 AM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA3/31/2015 4:50 AM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA3/31/2015 4:50 AM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA3/31/2015 4:50 AM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA3/31/2015 4:50 AM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA3/31/2015 4:50 AM
1,3-Dichlorobenzene ND 5.00 µg/L0.136 NA PA/VA3/31/2015 4:50 AM
1,4-Dichlorobenzene 0.890 1.00 J µg/L0.287 NA PA/VA3/31/2015 4:50 AM
Dichlorodifluoromethane 3.06 5.00 J µg/L0.714 NA PA/VA3/31/2015 4:50 AM
1,1-Dichloroethane 19.7 5.00 µg/L0.383 NA PA/VA3/31/2015 4:50 AM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA3/31/2015 4:50 AM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA3/31/2015 4:50 AM
cis-1,2-Dichloroethene 21.5 5.00 µg/L0.226 NA PA/VA3/31/2015 4:50 AM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA3/31/2015 4:50 AM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA3/31/2015 4:50 AM
1,3-Dichloropropane ND 1.00 µg/L0.706 NA PA/VA3/31/2015 4:50 AM
2,2-Dichloropropane ND 15.0 µg/L0.229 NA PA/VA3/31/2015 4:50 AM
1,1-Dichloropropene ND 5.00 µg/L0.334 NA PA/VA3/31/2015 4:50 AM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA3/31/2015 4:50 AM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA3/31/2015 4:50 AM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA3/31/2015 4:50 AM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA3/31/2015 4:50 AM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA3/31/2015 4:50 AM
Methylene chloride 1.49 1.00 µg/L0.539 NA PA/VA3/31/2015 4:50 AM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA3/31/2015 4:50 AM
Styrene ND 1.00 µg/L0.240 NA PA/VA3/31/2015 4:50 AM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA3/31/2015 4:50 AM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA3/31/2015 4:50 AM
Tetrachloroethene 9.97 1.00 µg/L0.196 NA PA/VA3/31/2015 4:50 AM
Page 71 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 2:45:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-10A Matrix:Groundwater
MW-5A DUPLICATEClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Toluene ND 1.00 µg/L0.167 NA PA/VA3/31/2015 4:50 AM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA3/31/2015 4:50 AM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA3/31/2015 4:50 AM
Trichloroethene 21.4 1.00 µg/L0.302 NA PA/VA3/31/2015 4:50 AM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA3/31/2015 4:50 AM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA3/31/2015 4:50 AM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA3/31/2015 4:50 AM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA3/31/2015 4:50 AM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA3/31/2015 4:50 AM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA3/31/2015 4:50 AM
Surr: 1,2-Dichloroethane-d4 106 68.7-129 %RECNANA 3/31/2015 4:50 AM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 3/31/2015 4:50 AM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 3/31/2015 4:50 AM
Surr: Toluene-d8 95.3 71.4-129 %RECNANA 3/31/2015 4:50 AM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Acetonitrile ND 55.0 µg/L18.4 NA PA/VA3/31/2015 4:50 AM
Allyl chloride ND 10.0 µg/L0.829 NA PA/VA3/31/2015 4:50 AM
Chloroprene ND 20.0 µg/L1.25 NA PA/VA3/31/2015 4:50 AM
Isobutyl alcohol ND 100 µg/L16.1 NA PA/VA3/31/2015 4:50 AM
Methacrylonitrile ND 100 µg/L5.82 NA PA/VA3/31/2015 4:50 AM
Propionitrile ND 150 µg/L52.6 NA PA/VA3/31/2015 4:50 AM
Surr: 1,2-Dichloroethane-d4 102 80-120 %RECNANA 3/31/2015 4:50 AM
Surr: 4-Bromofluorobenzene 96.8 80-120 %RECNANA 3/31/2015 4:50 AM
Surr: Dibromofluoromethane 107 80-120 %RECNANA 3/31/2015 4:50 AM
Surr: Toluene-d8 97.7 80-120 %RECNANA 3/31/2015 4:50 AM
SULFIDE Method: SM4500-S-F-2000 Analyst: CC
Sulfide (As S)ND 1.00 mg/L0.40 NA PA/VA3/30/2015 3:10 PM
Cyanide Method: EPA 335.4, Rev. 1
(1993)
Analyst: JH
Cyanide, Total ND 0.020 mg/L0.005 NA PA/VA3/30/2015 4:37 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 3.0 5.0 J mg/L1.0 NA PA/VA3/27/2015 2:04 PM
Page 72 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:14:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-11A Matrix:Groundwater
PZ-85BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 4/3/2015 3:36 PM
Acetone ND 100 µg/L4.88 NA PA/VA4/3/2015 3:36 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA4/3/2015 3:36 PM
Benzene 0.500 1.00 J µg/L0.129 NA PA/VA4/3/2015 3:36 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA4/3/2015 3:36 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA4/3/2015 3:36 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA4/3/2015 3:36 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA4/3/2015 3:36 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA4/3/2015 3:36 PM
Carbon disulfide ND 100 µg/L1.27 NA 4/3/2015 3:36 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA4/3/2015 3:36 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA4/3/2015 3:36 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA4/3/2015 3:36 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA4/3/2015 3:36 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA4/3/2015 3:36 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA4/3/2015 3:36 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA4/3/2015 3:36 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA4/3/2015 3:36 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA4/3/2015 3:36 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA4/3/2015 3:36 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA4/3/2015 3:36 PM
1,1-Dichloroethane 1.87 5.00 J µg/L0.383 NA PA/VA4/3/2015 3:36 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA4/3/2015 3:36 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA4/3/2015 3:36 PM
cis-1,2-Dichloroethene 5.74 5.00 µg/L0.226 NA PA/VA4/3/2015 3:36 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA4/3/2015 3:36 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA4/3/2015 3:36 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA4/3/2015 3:36 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA4/3/2015 3:36 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA4/3/2015 3:36 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA4/3/2015 3:36 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA4/3/2015 3:36 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA4/3/2015 3:36 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA4/3/2015 3:36 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA4/3/2015 3:36 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA4/3/2015 3:36 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA4/3/2015 3:36 PM
Page 73 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 5:14:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-11A Matrix:Groundwater
PZ-85BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Tetrachloroethene 5.44 1.00 µg/L0.196 NA PA/VA4/3/2015 3:36 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA4/3/2015 3:36 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA4/3/2015 3:36 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA4/3/2015 3:36 PM
Trichloroethene 6.76 1.00 µg/L0.302 NA PA/VA4/3/2015 3:36 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA4/3/2015 3:36 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA4/3/2015 3:36 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA4/3/2015 3:36 PM
Vinyl chloride 1.76 1.00 µg/L0.223 NA PA/VA4/3/2015 3:36 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA4/3/2015 3:36 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA4/3/2015 3:36 PM
Surr: 1,2-Dichloroethane-d4 93.1 68.7-129 %RECNANA 4/3/2015 3:36 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 4/3/2015 3:36 PM
Surr: Dibromofluoromethane 94.5 74.3-124 %RECNANA 4/3/2015 3:36 PM
Surr: Toluene-d8 100 71.4-129 %RECNANA 4/3/2015 3:36 PM
Page 74 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:38:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-12A Matrix:Groundwater
PZ-86BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 4/3/2015 4:10 PM
Acetone ND 100 µg/L4.88 NA PA/VA4/3/2015 4:10 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA4/3/2015 4:10 PM
Benzene 4.85 1.00 µg/L0.129 NA PA/VA4/3/2015 4:10 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA4/3/2015 4:10 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA4/3/2015 4:10 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA4/3/2015 4:10 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA4/3/2015 4:10 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA4/3/2015 4:10 PM
Carbon disulfide ND 100 µg/L1.27 NA 4/3/2015 4:10 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA4/3/2015 4:10 PM
Chlorobenzene 0.670 3.00 J µg/L0.177 NA PA/VA4/3/2015 4:10 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA4/3/2015 4:10 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA4/3/2015 4:10 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA4/3/2015 4:10 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA4/3/2015 4:10 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA4/3/2015 4:10 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA4/3/2015 4:10 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA4/3/2015 4:10 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA4/3/2015 4:10 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA4/3/2015 4:10 PM
1,1-Dichloroethane 34.2 50.0 J µg/L3.83 NA PA/VA4/6/2015 4:20 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA4/3/2015 4:10 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA4/3/2015 4:10 PM
cis-1,2-Dichloroethene 25.8 50.0 J µg/L2.26 NA PA/VA4/6/2015 4:20 PM
trans-1,2-Dichloroethene 0.780 5.00 J µg/L0.392 NA PA/VA4/3/2015 4:10 PM
1,2-Dichloropropane 0.500 1.00 J µg/L0.461 NA PA/VA4/3/2015 4:10 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA4/3/2015 4:10 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA4/3/2015 4:10 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA4/3/2015 4:10 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA4/3/2015 4:10 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA4/3/2015 4:10 PM
Methylene chloride 26.5 10.0 µg/L5.39 NA PA/VA4/6/2015 4:20 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA4/3/2015 4:10 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA4/3/2015 4:10 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA4/3/2015 4:10 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA4/3/2015 4:10 PM
Page 75 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 4:38:00 PM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-12A Matrix:Groundwater
PZ-86BClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Tetrachloroethene 35.2 10.0 µg/L1.96 NA PA/VA4/6/2015 4:20 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA4/3/2015 4:10 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA4/3/2015 4:10 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA4/3/2015 4:10 PM
Trichloroethene 26.2 10.0 µg/L3.02 NA PA/VA4/6/2015 4:20 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA4/3/2015 4:10 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA4/3/2015 4:10 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA4/3/2015 4:10 PM
Vinyl chloride 5.47 1.00 µg/L0.223 NA PA/VA4/3/2015 4:10 PM
o-Xylene 1.84 1.00 µg/L0.186 NA PA/VA4/3/2015 4:10 PM
m,p-Xylene 1.44 2.00 J µg/L0.287 NA PA/VA4/3/2015 4:10 PM
Surr: 1,2-Dichloroethane-d4 97.2 68.7-129 %RECNANA 4/3/2015 4:10 PM
Surr: 4-Bromofluorobenzene 110 71.8-127 %RECNANA 4/3/2015 4:10 PM
Surr: Dibromofluoromethane 99.6 74.3-124 %RECNANA 4/3/2015 4:10 PM
Surr: Toluene-d8 99.8 71.4-129 %RECNANA 4/3/2015 4:10 PM
Page 76 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 12:00:00 AM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-13A Matrix:Trip Blank
TRIP BLANK # 2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: TC
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 4/3/2015 4:44 PM
Acetone ND 100 µg/L4.88 NA PA/VA4/3/2015 4:44 PM
Acrylonitrile ND 200 µg/L4.24 NA PA/VA4/3/2015 4:44 PM
Benzene ND 1.00 µg/L0.129 NA PA/VA4/3/2015 4:44 PM
Bromochloromethane ND 3.00 µg/L0.346 NA PA/VA4/3/2015 4:44 PM
Bromodichloromethane ND 1.00 µg/L0.162 NA PA/VA4/3/2015 4:44 PM
Bromoform ND 3.00 µg/L0.400 NA PA/VA4/3/2015 4:44 PM
Bromomethane ND 10.0 µg/L0.497 NA PA/VA4/3/2015 4:44 PM
2-Butanone ND 100 µg/L4.68 NA PA/VA4/3/2015 4:44 PM
Carbon disulfide ND 100 µg/L1.27 NA 4/3/2015 4:44 PM
Carbon tetrachloride ND 1.00 µg/L0.250 NA PA/VA4/3/2015 4:44 PM
Chlorobenzene ND 3.00 µg/L0.177 NA PA/VA4/3/2015 4:44 PM
Chloroethane ND 10.0 µg/L0.942 NA PA/VA4/3/2015 4:44 PM
Chloroform ND 5.00 µg/L0.253 NA PA/VA4/3/2015 4:44 PM
Chloromethane ND 1.00 µg/L0.327 NA PA/VA4/3/2015 4:44 PM
Dibromochloromethane ND 3.00 µg/L0.419 NA PA/VA4/3/2015 4:44 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.499 NA PA/VA4/3/2015 4:44 PM
1,2-Dibromoethane ND 1.00 µg/L0.341 NA PA/VA4/3/2015 4:44 PM
Dibromomethane ND 10.0 µg/L0.293 NA PA/VA4/3/2015 4:44 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.450 NA PA/VA4/3/2015 4:44 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.287 NA PA/VA4/3/2015 4:44 PM
1,1-Dichloroethane ND 5.00 µg/L0.383 NA PA/VA4/3/2015 4:44 PM
1,2-Dichloroethane ND 1.00 µg/L0.428 NA PA/VA4/3/2015 4:44 PM
1,1-Dichloroethene ND 5.00 µg/L0.328 NA PA/VA4/3/2015 4:44 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.226 NA PA/VA4/3/2015 4:44 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.392 NA PA/VA4/3/2015 4:44 PM
1,2-Dichloropropane ND 1.00 µg/L0.461 NA PA/VA4/3/2015 4:44 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.220 NA PA/VA4/3/2015 4:44 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.216 NA PA/VA4/3/2015 4:44 PM
Ethylbenzene ND 1.00 µg/L0.178 NA PA/VA4/3/2015 4:44 PM
2-Hexanone ND 50.0 µg/L4.11 NA PA/VA4/3/2015 4:44 PM
Iodomethane ND 10.0 µg/L3.44 NA PA/VA4/3/2015 4:44 PM
Methylene chloride ND 1.00 µg/L0.539 NA PA/VA4/3/2015 4:44 PM
4-Methyl-2-pentanone ND 100 µg/L4.40 NA PA/VA4/3/2015 4:44 PM
Styrene ND 1.00 µg/L0.240 NA PA/VA4/3/2015 4:44 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.360 NA PA/VA4/3/2015 4:44 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.384 NA PA/VA4/3/2015 4:44 PM
Page 77 of 78
WO#: 1503V15
Date Reported: 4/10/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/24/2015 12:00:00 AM
Project:BLACKBURN CLOSED - 1SA 2015
Lab ID:1503V15-13A Matrix:Trip Blank
TRIP BLANK # 2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA N.CSite ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.196 NA PA/VA4/3/2015 4:44 PM
Toluene ND 1.00 µg/L0.167 NA PA/VA4/3/2015 4:44 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.354 NA PA/VA4/3/2015 4:44 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.492 NA PA/VA4/3/2015 4:44 PM
Trichloroethene ND 1.00 µg/L0.302 NA PA/VA4/3/2015 4:44 PM
Trichlorofluoromethane ND 1.00 µg/L0.299 NA PA/VA4/3/2015 4:44 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.358 NA PA/VA4/3/2015 4:44 PM
Vinyl acetate ND 50.0 µg/L4.87 NA PA/VA4/3/2015 4:44 PM
Vinyl chloride ND 1.00 µg/L0.223 NA PA/VA4/3/2015 4:44 PM
o-Xylene ND 1.00 µg/L0.186 NA PA/VA4/3/2015 4:44 PM
m,p-Xylene ND 2.00 µg/L0.287 NA PA/VA4/3/2015 4:44 PM
Surr: 1,2-Dichloroethane-d4 96.3 68.7-129 %RECNANA 4/3/2015 4:44 PM
Surr: 4-Bromofluorobenzene 109 71.8-127 %RECNANA 4/3/2015 4:44 PM
Surr: Dibromofluoromethane 98.6 74.3-124 %RECNANA 4/3/2015 4:44 PM
Surr: Toluene-d8 100 71.4-129 %RECNANA 4/3/2015 4:44 PM
Page 78 of 78
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
CatawbaCounty,NorthCarolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
Appendix C5:
FieldSamplingSummaries
and
FieldSampleLogs
REIConsultants,Inc.P.OBox 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Cloudy,PartlyCloudy,andSunny68-74°F
Property Units MW-5 MW-5A MW-6 MW-6D
SamplingDepth Feet 6.65 17.58 6.22 6.18
StaticDepth Feet 6.06 5.18 5.89 5.38
WellDepth Feet 17.69 48.40 17.60 53.35
WaterColumnHeight Feet 11.63 43.22 11.71 47.97
VolumePurged Liters 24 76 21 84
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-5 MW-5A MW-6 MW-6D
pH SU 5.58 6.48Dup6.48 6.00 6.98
Temperature oC 14.5 16.8Dup16.7 15.0 17.2
Conductivity umhos/cm 270 235Dup235 1060 122
Turbidity NTU 154 4.41Dup4.41 28.2 2.89
Appearance -Cloudy Clear Cloudy Clear
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 391 <5.00 <5.00 <5.00
Property Units MW-7 MW-11 MW-20 PZ-85B
SamplingDepth Feet 12.51 15.82 38.66 20.85
StaticDepth Feet 10.77 15.25 37.96 19.32
WellDepth Feet 17.40 26.60 50.63 44.00
WaterColumnHeight Feet 6.63 11.35 12.67 24.68
VolumePurged Liters 12 20 25 43
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-7 MW-11 MW-20 PZ-85B
pH SU 5.22 5.44 5.70 5.87
Temperature oC 15.9 17.3 17.0 16.9
Conductivity umhos/cm 532 151 106 164
Turbidity NTU 46.8 110 332 324
Appearance -Cloudy Cloudy Cloudy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 216 113 121 -
SAMPLING LOG SUMMARY
Closed Portion(Permit:#18-03)
1503V15
3/24/2015
CountyofCatawba
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Cloudy,PartlyCloudy,andSunny68-74°F
SAMPLING LOG SUMMARY
Closed Portion(Permit:#18-03)
1503V15
3/24/2015
CountyofCatawba
Property Units PZ-86B SW-1 SW-3
SamplingDepth Feet 33.32 --
StaticDepth Feet 31.92 --
WellDepth Feet 57.78 --
WaterColumnHeight Feet 25.86 --
VolumePurged Liters 45 --
PurgingStatus -FinishedPurging --
PhysicalProperty Units PZ-86B SW-1 SW-3
pH SU 5.97 6.60 6.89
Temperature oC 16.6 15.0 16.1
Conductivity umhos/cm 357 182 71.2
Turbidity NTU 13.0 9.14 16.17
Appearance -Clear Clear Clear
Odor -No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L -<5.00 <5.00
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 2
ProjectName:Project :Well #:MW-5
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 72 °F
6.06 (Ft)6.73 (Liters)
17.69 (Ft)20.20 (Liters)
11.63 (Ft)24.00 (Liters)
pH
Time (SU)
15:25 5.61
15:26 5.62
15:27 5.61
15:28 5.61
15:30 5.58
15:31 5.59
15:32
Date:Time:15:37
Method:SamplingDepth:6.65'
pH:5.58 (SU)Conductivity:270 (umhos/cm)
Temperature:14.5 (oC)Turbidity:154 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:NoOdor
PHYSICAL CHARACTERISTICSOFSAMPLE
TeflonBailer
SAMPLINGDATA
3/24/2015
Finished Purging 24
238.0 13.5 322.00 20
249.0 13.6 244.00 16
258.0 13.5 129.00 12
278.0 13.3 140.00 8
311.0 13.6 184.00 4
323.0 13.6 84.20 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TemperatureCorrected Temperature Turbidity VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
3/24/201515:13 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
BlackburnClosed Portion 1stSemi2015
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 3
ProjectName:Project :Well #:MW-5A
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 72 °F
5.18 (Ft)25.02 (Liters)
48.40 (Ft)75.07 (Liters)
43.22 (Ft)76.00 (Liters)
pH
Time (SU)
14:19 6.97
14:23 7.15
14:27 6.56
14:31 6.45
14:36 6.47
14:40 6.49
14:42
Date:Time:14:45
Method:SamplingDepth:17.58'
pH:6.48Dup6.48 (SU)Conductivity:235Dup235 (umhos/cm)
Temperature:16.8Dup16.7 (oC)Turbidity:4.41Dup4.41 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
PHYSICAL CHARACTERISTICSOFSAMPLE
TeflonBailer
Odor:Appearance:Clear NoOdor
SAMPLINGDATA
3/24/2015
Finished Purging 76
243.0 16.9 13.11 70
246.0 16.9 569.58
248.0 16.9 2.17 42
220.0 17.0 10.61 28
137.6 16.8 141.21
138.1 14.8 0.76 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TurbidityTemperatureCorrectedTemperature VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
3/24/201514:10 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
BlackburnClosed Portion 1stSemi2015
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 4
ProjectName:Project :Well #:MW-6
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Pt.Cloudy 74 °F
5.89 (Ft)6.78 (Liters)
17.60 (Ft)20.34 (Liters)
11.71 (Ft)21.00 (Liters)
pH
Time (SU)
16:18 6.01
16:19 6.04
16:21 6.01
16:22 6.01
16:23 6.00
16:24 6.01
16:24
Date:Time:16:27
Method:SamplingDepth:6.22'
pH:6.00 (SU)Conductivity:1060 (umhos/cm)
Temperature:15.0 (oC)Turbidity:28.2 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
PHYSICAL CHARACTERISTICSOFSAMPLE
Cloudy Odor:NoOdorAppearance:
TeflonBailer
3/24/2015
SAMPLINGDATA
21Finished Purging
14.5 61.8 20
1,070.0 14.4 85.6 16
14.4 140 121,068.0
1,056.0 14.4 254 8
1,028.0 14.8 775 4
15.6 >800 11,019.0
(oC)(NTU)(Liters)Conductivity(umhos/cm)
TemperatureCorrected
VolumePurged
Temperature Turbidity VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
6/24/201516:15 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
RodneyHamby 704-462-1348
BlackburnClosed Portion 1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 5
ProjectName:Project :Well #:MW-6D
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Cloudy 72 °F
5.38 (Ft)27.77 (Liters)
53.35 (Ft)83.32 (Liters)
47.97 (Ft)84.00 (Liters)
pH
Time (SU)
16:39 6.96
16:43 6.69
16:48 6.86
16:52 6.95
16:56 6.98
17:00 6.99
17:02
Date:Time:17:04
Method:SamplingDepth:6.18'
pH:6.98 (SU)Conductivity:121.9 (umhos/cm)
Temperature:17.2 (oC)Turbidity:2.89 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Clear
PHYSICAL CHARACTERISTICSOFSAMPLE
Odor:Appearance:NoOdor
TeflonBailer
3/24/2015
SAMPLINGDATA
84Finished Purging
121.9 17.2 5.1 80
122.2 17.2 6.02 64
48122.8 17.2 4.72
123.5 17.0 5.12 32
124.3 16.9 2.26 16
1133.2 14.7 1.32
Conductivity(umhos/cm)(oC)(NTU)(Liters)
Temperature Turbidity VolumePurged
WaterColumnHeight VolumePurged
TemperatureCorrected
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
PURGINGDATA
3/24/201516:37 WeatherConditions:
CaponWellRiser 2"PVCCasing
WELL CONDITIONDATA
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
RodneyHamby 704-462-1348
BlackburnClosed Portion
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 6
ProjectName:Project :Well #:MW-7
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 73 °F
10.77 (Ft)3.83 (Liters)
17.40 (Ft)11.51 (Liters)
6.63 (Ft)12.00 (Liters)
pH
Time (SU)
15:53 5.21
15:54 5.07
15:55 5.06
15:56 5.06
15:58 5.07
15:59 5.10
15:59
Date:Time:16:02
Method:SamplingDepth:12.51'
pH:5.22 (SU)Conductivity:532 (umhos/cm)
Temperature:15.9 (oC)Turbidity:46.8 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
NoOdorAppearance:Cloudy Odor:
TeflonBailer
3/24/2015
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
12Finished Purging
15.6 301 11
9
471.0
537476.0 15.5
7489.0 15.6 612
508.0 15.6 671 5
3615540.0 15.9
1558.0 16.9 3.65
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TemperatureCorrected Temperature
WaterColumnHeight
EVACUATION/STABILIZATIONTESTDATA
Turbidity VolumePurged
VolumePurged
WellDepth 3Volumes
PURGINGDATA
StaticDepth(DepthtoWater)Volume
3/24/201515:50 WeatherConditions:
2"PVCCasingCaponWellRiser
ProtectiveCasingLocked Concrete/GroutPadPresent
WELL CONDITIONDATA
ProtectiveCasingPresent PhysicalDamage
BlackburnClosed Portion 1stSemi2015
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 7
ProjectName:Project :Well #:MW-11
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 72 °F
15.25 (Ft)6.57 (Liters)
26.60 (Ft)19.71 (Liters)
11.35 (Ft)20.00 (Liters)
pH
Time (SU)
15:27 5.35
15:28 5.39
15:30 5.42
15:31 5.43
15:33 5.47
15:34 5.46
15:34
Date:Time:15:37
Method:SamplingDepth:15.82'
pH:5.44 (SU)Conductivity:151.1 (umhos/cm)
Temperature:17.3 (oC)Turbidity:110 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:NoOdor
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
3/24/2015
SAMPLINGDATA
Finished Purging 20
17.3 34.3 20150.5
144.3 17.3 12.7 16
17.2 12.3 8
141.6 17.2 13.19 12
140.8
137.6 17.5 16.14 4
(oC)(NTU)(Liters)
139.0 18.2 9.55 1
Conductivity(umhos/cm)
VolumePurged
EVACUATION/STABILIZATIONTESTDATA
TemperatureCorrected Temperature Turbidity VolumePurged
WaterColumnHeight
WellDepth 3Volumes
PURGINGDATA
StaticDepth(DepthtoWater)Volume
3/24/201515:18 WeatherConditions:
CaponWellRiser 2"PVCCasing
Concrete/GroutPadPresent
WELL CONDITIONDATA
704-462-1348
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked
BlackburnClosed Portion
RodneyHamby
1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 8
ProjectName:Project :Well #:MW-20
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 68 °F
37.96 (Ft)7.33 (Liters)
50.63 (Ft)22.00 (Liters)
12.67 (Ft)25.00 (Liters)
pH
Time (SU)
14:17 5.49
14:19 5.54
14:21 5.70
14:23 5.77
14:25 5.80
14:29 5.78
14:29
Date:Time:14:40
Method:SamplingDepth:38.66'
pH:5.70 (SU)Conductivity:105.6 (umhos/cm)
Temperature:17.0 (oC)Turbidity:332 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Odor:NoOdor
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
Cloudy
3/24/2015
SAMPLINGDATA
25Finished Purging
16.8 69.3 25110.2
16.9 129 20111.0
15
111.1 16.9 224 10
113.3 16.8 205
17.2 510 5106.5
1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
113.3 17.7 43.6
Temperature Turbidity VolumePurgedTemperatureCorrected
WaterColumnHeight
EVACUATION/STABILIZATIONTESTDATA
VolumePurged
StaticDepth(DepthtoWater)Volume
WellDepth 3Volumes
WeatherConditions:
PURGINGDATA
3/24/201514:15
CaponWellRiser 2"PVCCasing
PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
RodneyHamby 704-462-1348
WELL CONDITIONDATA
ProtectiveCasingPresent
1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 9
ProjectName:Project :Well #:PZ-85B
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 72 °F
19.32 (Ft)14.28 (Liters)
44.00 (Ft)42.86 (Liters)
24.68 (Ft)43.00 (Liters)
pH
Time (SU)
16:52 6.83
16:55 6.80
16:58 6.24
17:02 5.90
17:06 5.92
17:10 5.89
17:11
Date:Time:17:14
Method:SamplingDepth:20.85'
pH:5.87 (SU)Conductivity:163.9 (umhos/cm)
Temperature:16.9 (oC)Turbidity:324 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:NoOdor
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
3/24/2015
SAMPLINGDATA
Finished Purging 43
16.5 311 40164.9
165.4 32300
164.2 16.5 274 24
16.6
16.6 102 16157.3
149.4 16.6 8
151.1 16.9 7.93 1
37.7
(oC)(NTU)(Liters)Conductivity(umhos/cm)
TemperatureCorrected Temperature Turbidity VolumePurged
EVACUATION/STABILIZATIONTESTDATA
VolumePurged
WellDepth
WaterColumnHeight
StaticDepth(DepthtoWater)Volume
3Volumes
WeatherConditions:3/24/201516:49
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
ProtectiveCasingLocked Concrete/GroutPadPresent
RodneyHamby
WELL CONDITIONDATA
704-462-1348
BlackburnClosed Portion 1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page10
ProjectName:Project :Well #:PZ-86B
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Sunny 72 °F
31.92 (Ft)14.97 (Liters)
57.78 (Ft)44.91 (Liters)
25.86 (Ft)45.00 (Liters)
pH
Time (SU)
16:15 6.15
16:18 6.14
16:22 6.07
16:25 6.02
16:29 5.99
16:33 6.01
16:35
Date:Time:16:38
Method:SamplingDepth:33.32'
pH:5.97 (SU)Conductivity:357 (umhos/cm)
Temperature:16.6 (oC)Turbidity:13.01 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/24/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
ClearAppearance:
SAMPLINGDATA
TeflonBailer
3/24/2015
PHYSICAL CHARACTERISTICSOFSAMPLE
Odor:NoOdor
45Finished Purging
40362.0 16.5 25.9
32
16.5 23.5 24364.0
361.0 16.5 20.8
16345.0 16.6 34
8
17.1 1.49 1310.0
312.0 16.6 15.91
(Liters)Conductivity(umhos/cm)(oC)(NTU)
TemperatureCorrected VolumePurgedTemperatureTurbidity
VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
PURGINGDATA
3/24/201516:10 WeatherConditions:
CaponWellRiser 2"PVCCasing
WELL CONDITIONDATA
704-462-1348
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
RodneyHamby
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnClosed Portion 1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page11
Outlet:
Date:15:50
pH:6.60 Conductivity:182.3 umhos/cm
Flow:N/A Temperature:15.0 o C
Clear /NoOdor
Turbidity=9.14NTU
Outlet:
Date:15:00
pH:6.89 Conductivity:71.2 umhos/cm
Flow:N/A Temperature:16.1 o C
Clear /NoOdor
Turbidity=16.17NTU
Outlet:
Date:
pH:Conductivity:umhos/cm
Flow:Temperature:o C
SampleOdorand PhysicalAppearance:
Comments:
3/24/2015 Time:
SampleOdorand PhysicalAppearance:
Comments:
Time:
SurfaceWaterSampling Log
REIConsultants,Inc.
ProjectName:BlackburnClosedPortion
SW-3
Contact Person:RodneyHamby Phone/Fax:[phone]
SW-1
3/24/2015 Time:
SampleOdorand PhysicalAppearance:
Comments:
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page12
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
Closed Portion
AppendixC6:
Historical Results
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-5
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-5A
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page17
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-6
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page33
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
C l o se
d P o r ti
o n
(P e r m it
:
#18
-0 3)
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-6D
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page49
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-7
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page60
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-11
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page76
Closed Portion
HistoricalDataSummary
MonitoringWell:MW-20
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page87
Closed Portion
HistoricalDataSummary
SurfaceWater:SW-1
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page98
Closed Portion
HistoricalDataSummary
SurfaceWater:SW-3
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page109
Closed Portion
Historical Data Summary
Piezometer:PZ-85B
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page120
Closed Portion
Historical Data Summary
Piezometer:PZ-86B
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page125
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD1:
1stSemi-Annual2015
Summary of Detections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
1
-O n l y
re
s
u lt
s
a b ov
e
S W SL
's s ho
wn
2
1
2
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD2:
Summary of Dissolved Metals and
TotalSuspendedSolid(TSS)
Detections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
Su
mm
a r y
o f
Di
ss
o lv
e d
Me
t a l s
a nd
T SS
D e t e c ti
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B l a c kb
u
r n
L
a nd
f il
l
:
C
& D
P e r m i t :
#18
-03
R E I C
J o b
N u m b e r :
1 5 03
V 13
S a m p l e
D a t e :
03
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-2 0 15
A r s e n i c ,
D i ss
o l v ed
0 .01
B a r i um
,
D i ss
o l v ed
0 .1
0 .1 50
0 .9 56
0 .2 34
0 .2 64
C a d m i um
,
D i ss
o l v ed
0 .0 01
C h r o m i um
,
D i ss
o l v ed
0 .01
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d,
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0 .01
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,
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0 .01
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0 .01
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ry
,
D i ss
o l v ed
0 .0 0 02
T o t a l S
u
s p e nd
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S
o li
d s
(T SS
)
1
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2 67
13
6 10
2 03
40
2 50
2 05
4 44
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& D
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C
& D
F OO
T NO
T E S:
1.
S W SL
-
S o l id
W a s te
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on
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(m
g /L)
2.
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re
su
l ts
a b o ve
S WS
Ls
sh
o wn
S P E CI
AL
NO
T E S:
A ll
d a ta
re
p o r t ed
in
m g /L.
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD3:
HistoricalSummaryofDetections
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
H I S TO
R IC
AL
SU
MM
A R Y
O F
D E T E C T I ON
S
M o n it
o r i ng
W e ll
:
MW
-
2
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:
C
& D
P a r a m e t er
G W S
t d.
1
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2
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9
2
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9
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9
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9
9
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9
9
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0
0
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0
0
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0
1
B a ri
um
2 .0
0 .50
0
0 .64
9
C a d m i um
0 .00
1 75
0 .00
1
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9
Ch
r o m i um
0 .05
0 .05
0 .00
7
0 .03
7
0 .02
0
0 .04
3
0 .01
2
0 .10
5
0 .01
8
0 .03
3
T SS
1
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G W S
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2
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0
1
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20
0
2
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0
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20
0
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0
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1 75
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1
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0 .05
0 .01
36
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1
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58
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37
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7
7
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0 .7
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1
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1
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2
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1
Ch
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0 .01
0
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1
-
30
12
13
17
10
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li
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-
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s a
r e
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3
S W S L
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li
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(no
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t
t h e
P Q L.
HI
S T O R I C A L
S U MM
A R Y
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S
1
2
3
1
3
1
3
1
3
1 2 3
HI
S T O R I C A L
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A R Y
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ON
S
1
2
3
1
3
3
1
3
1 2 3
HI
S T O R I C A L
S U MM
A R Y
O F D
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ON
S
1
2
3
1
3
3
1
3
1 2 3
HI
S T O R I C A L
S U MM
A R Y
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ON
S
1
2
3
1
3
1
3
1 2 3
HI
S T O R I C A L
S U MM
A R Y
O F D
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ON
S
1
2
3
1
3
1
3
1 2 3
HI
S T O R I C A L
S U MM
A R Y
O F D
E T E C TI
ON
S
1
2
1
3
1
3
1 2 3
HI
S T O R I C A L
S U MM
A R Y
O F D
E T E C TI
ON
S
1
3
1
3
1
3
1 2 3
HI
S T O R I C A L
S U MM
A R Y
O F D
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ON
S
1
3
1
3
1
3
1 2 3
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD4:
LaboratoryAnalytical Reports
and
Chain-of-Custody Records
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
PO Box 286
Beaver, WV 25813
TEL: [phone]
Website: www.reiclabs.com
REI Consultants, Inc.
3029-C Peters Creek Road
Roanoke, VA 24019
TEL: [phone] TEL: [phone]
Ashland, KY 41101
101 17th Street
TEL: [phone]
Verona, VA 24482
1557 Commerce Road, Suite 201
TEL: [phone]
Westover, WV 26501
16 Commerce Drive
Tuesday, April 07, 2015
Mr. Rodney Hamby
COUNTY OF CATAWBA
P O BOX 389
NEWTON, NC 28658
TEL:
FAX:
[phone]
[phone]
RE:BLACKBURN C&D - 1SA 2015
Work Order #:1503V13
Dear Mr. Rodney Hamby:
REI Consultants, Inc. received 11 sample(s) on 3/26/2015 for the analyses presented in the following report.
Sincerely,
Michelle Ellison
Page 1 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Case Narrative
Client:
Project:BLACKBURN C&D - 1SA 2015
COUNTY OF CATAWBA
The analytical results presented in this report were produced using documented laboratory SOPs that incorporate appropriate quality control
procedures as described in the applicable methods. Verification of required sample preservation (as required) is recorded on associated
laboratory logs. Any deviation from compliance or method modification is identified within the body of this report by a qualifier footnote which is
defined at the bottom of this page.
All sample results for solid samples are reported on an "as-received" wet weight basis unless otherwise noted.
Results reported for sums of individual parameters, such as TTHM and HAA5, may vary slightly from the sum of the individual parameter results,
due to rounding of individual results, as required by EPA.
The test results in this report meet all NELAP (and/or VELAP) requirements for parameters except as noted in this report.
Please note if the sample collection time is not provided on the Chain of Custody, the default recording will be 0:00:00. This may cause some
tests to be apparently analyzed out of hold.
All tests performed by REIC Service Centers are designated by an annotation on the test code. All other tests were performed by REIC's Main
Laboratory in Beaver, WV.
This report may not be reproduced, except in full, without the written approval of REIC.
DEFINITIONS:
MCL: Maximum Contaminant Level
MDL: Method Detection Limit; The lowest concentration of analyte that can be detected by the method in the applicable matrix.
Mg/Kg or mg/L: Units of part per million (PPM) - milligram per Kilogram (weight/weight) or milligram per Liter (weight/volume).
NA: Not Applicable
ND: Not Detected at the PQL or MDL
PQL: Practical Quantitation Limit; The lowest verified limit to which data is quantified without qualifications. Analyte concentrations below PQL
are reported either as ND or as a number with a "J" qualifier.
Qual: Qualifier that applies to the analyte reported.
TIC: Tentatively Identified Compound, Estimated Concentration denoted by "J" qualifier.
Ug/Kg or ug/L: Units of part per billion (PPB) - microgram per kilogram (weight/weight) or microgram per liter (weight/volume).
QUALIFIERS:
X: Reported value exceeds required MCL
B: Analyte detected in the associated Method Blank at a concentration > 1/2 the PQL
E: Analyte concentration reported that exceeds the upper calibration standard. Greater uncertainty is associated with this result and data should
be consider estimated.
H: Holding time for preparation or analysis has been exceeded.
J: Analyte concentration is reported, and is less than the PQL and greater than or equal to the MDL. The result reported is an estimate.
S: % REC (% recovery) exceeds control limits
CERTIFICATIONS:
Beaver, WV: WVDHHR 00412CM, WVDEP 060, VADCLS 00281, KYDEP 90039, TNDEQ TN02926, NCDWQ 466, PADEP 68-00839, VADCLS
(VELAP)460148
Bioassay (Beaver, WV): WVDEP 060, VADCLS(VELAP) 460148, PADEP 68-00839
Roanoke, VA: VADCLS(VELAP) 460150
Verona, VA: VADCLS(VELAP) 460151
Ashland, KY: KYDEP 00094, WVDEP 389
Morgantown, WV: WVDHHR 003112M, WVDEP 387
Page 2 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 7:50:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-01A Matrix:Groundwater
MW-2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:44 PM
Barium 0.195 0.100 mg/L0.0010 NA PA/VA4/2/2015 3:44 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:44 PM
Chromium 0.0054 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:44 PM
Lead 0.0004 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 3:44 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 3:44 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:44 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 9:59 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 4:31 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 4:31 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 4:31 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 4:31 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 4:31 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 4:31 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 4:31 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 4:31 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 4:31 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 4:31 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 4:31 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 4:31 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 4:31 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 4:31 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 4:31 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 4:31 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 4:31 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 4:31 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 4:31 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 4:31 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 4:31 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 4:31 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 4:31 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 4:31 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 4:31 PM
Page 3 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 7:50:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-01A Matrix:Groundwater
MW-2Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 4:31 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 4:31 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 4:31 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 4:31 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 4:31 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 4:31 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 4:31 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 4:31 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 4:31 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 4:31 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 4:31 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 4:31 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 4:31 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 4:31 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 4:31 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 4:31 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 4:31 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 4:31 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 4:31 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 4:31 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 4:31 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 4:31 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 4:31 PM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 3/29/2015 4:31 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 3/29/2015 4:31 PM
Surr: Dibromofluoromethane 104 74.3-124 %RECNANA 3/29/2015 4:31 PM
Surr: Toluene-d8 95.0 71.4-129 %RECNANA 3/29/2015 4:31 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 4:31 PM
Surr: 1,2-Dichloroethane-d4 95.9 80-120 %RECNANA 3/29/2015 4:31 PM
Surr: 4-Bromofluorobenzene 96.4 80-120 %RECNANA 3/29/2015 4:31 PM
Surr: Dibromofluoromethane 102 80-120 %RECNANA 3/29/2015 4:31 PM
Surr: Toluene-d8 97.6 80-120 %RECNANA 3/29/2015 4:31 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 39.5 5.0 mg/L1.0 NA PA/VA3/27/2015 1:23 PM
Page 4 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:54:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-02A Matrix:Groundwater
MW-21Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic 0.0017 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:50 PM
Barium 0.354 0.100 mg/L0.0010 NA PA/VA4/2/2015 3:50 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 3:50 PM
Chromium 0.0257 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:50 PM
Lead 0.0057 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 3:50 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 3:50 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:50 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:01 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 5:04 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 5:04 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 5:04 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:04 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 5:04 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 5:04 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 5:04 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 5:04 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 5:04 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 5:04 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 5:04 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 5:04 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 5:04 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 5:04 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 5:04 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 5:04 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 5:04 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 5:04 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 5:04 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 5:04 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 5:04 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 5:04 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 5:04 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 5:04 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 5:04 PM
Page 5 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:54:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-02A Matrix:Groundwater
MW-21Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 5:04 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 5:04 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 5:04 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 5:04 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 5:04 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 5:04 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 5:04 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 5:04 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 5:04 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 5:04 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 5:04 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 5:04 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 5:04 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:04 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:04 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 5:04 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 5:04 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 5:04 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 5:04 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 5:04 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 5:04 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 5:04 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 5:04 PM
Surr: 1,2-Dichloroethane-d4 103 68.7-129 %RECNANA 3/29/2015 5:04 PM
Surr: 4-Bromofluorobenzene 108 71.8-127 %RECNANA 3/29/2015 5:04 PM
Surr: Dibromofluoromethane 102 74.3-124 %RECNANA 3/29/2015 5:04 PM
Surr: Toluene-d8 95.6 71.4-129 %RECNANA 3/29/2015 5:04 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 5:04 PM
Surr: 1,2-Dichloroethane-d4 93.7 80-120 %RECNANA 3/29/2015 5:04 PM
Surr: 4-Bromofluorobenzene 97.5 80-120 %RECNANA 3/29/2015 5:04 PM
Surr: Dibromofluoromethane 97.9 80-120 %RECNANA 3/29/2015 5:04 PM
Surr: Toluene-d8 98.8 80-120 %RECNANA 3/29/2015 5:04 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 610 10 mg/L2.0 NA PA/VA3/27/2015 1:23 PM
Page 6 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 10:37:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-03A Matrix:Groundwater
MW-24Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic 0.0012 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 3:55 PM
Barium 0.389 0.100 mg/L0.0010 NA PA/VA4/2/2015 3:55 PM
Cadmium 0.0004 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 3:55 PM
Chromium 0.0391 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:55 PM
Lead 0.0048 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 3:55 PM
Selenium 0.0022 0.0100 J mg/L0.0020 NA PA/VA4/2/2015 3:55 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 3:55 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:03 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 5:37 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 5:37 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 5:37 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:37 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 5:37 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 5:37 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 5:37 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 5:37 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 5:37 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 5:37 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 5:37 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 5:37 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 5:37 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 5:37 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 5:37 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 5:37 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 5:37 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 5:37 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 5:37 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 5:37 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 5:37 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 5:37 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 5:37 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 5:37 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 5:37 PM
Page 7 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 10:37:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-03A Matrix:Groundwater
MW-24Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 5:37 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 5:37 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 5:37 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 5:37 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 5:37 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 5:37 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 5:37 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 5:37 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 5:37 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 5:37 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 5:37 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 5:37 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 5:37 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:37 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 5:37 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 5:37 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 5:37 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 5:37 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 5:37 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 5:37 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 5:37 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 5:37 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 5:37 PM
Surr: 1,2-Dichloroethane-d4 124 68.7-129 %RECNANA 3/29/2015 5:37 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 3/29/2015 5:37 PM
Surr: Dibromofluoromethane 115 74.3-124 %RECNANA 3/29/2015 5:37 PM
Surr: Toluene-d8 93.5 71.4-129 %RECNANA 3/29/2015 5:37 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 5:37 PM
Surr: 1,2-Dichloroethane-d4 125 80-120 S %RECNANA 3/29/2015 5:37 PM
Surr: 4-Bromofluorobenzene 101 80-120 %RECNANA 3/29/2015 5:37 PM
Surr: Dibromofluoromethane 112 80-120 %RECNANA 3/29/2015 5:37 PM
Surr: Toluene-d8 96.2 80-120 %RECNANA 3/29/2015 5:37 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 203 10 mg/L2.0 NA PA/VA3/27/2015 1:38 PM
Page 8 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:07:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-04A Matrix:Groundwater
MW-25Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:01 PM
Barium 0.359 0.100 mg/L0.0010 NA PA/VA4/2/2015 4:01 PM
Cadmium 0.0002 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 4:01 PM
Chromium 0.0036 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 4:01 PM
Lead 0.0004 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 4:01 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 4:01 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:01 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:06 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 6:10 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 6:10 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 6:10 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:10 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 6:10 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 6:10 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 6:10 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 6:10 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 6:10 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 6:10 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 6:10 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 6:10 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 6:10 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 6:10 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 6:10 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 6:10 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 6:10 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 6:10 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 6:10 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 6:10 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 6:10 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 6:10 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 6:10 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 6:10 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 6:10 PM
Page 9 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:07:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-04A Matrix:Groundwater
MW-25Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 6:10 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 6:10 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 6:10 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 6:10 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 6:10 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 6:10 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 6:10 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 6:10 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 6:10 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 6:10 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 6:10 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 6:10 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 6:10 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:10 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:10 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 6:10 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 6:10 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 6:10 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 6:10 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 6:10 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 6:10 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 6:10 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 6:10 PM
Surr: 1,2-Dichloroethane-d4 102 68.7-129 %RECNANA 3/29/2015 6:10 PM
Surr: 4-Bromofluorobenzene 103 71.8-127 %RECNANA 3/29/2015 6:10 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 3/29/2015 6:10 PM
Surr: Toluene-d8 94.6 71.4-129 %RECNANA 3/29/2015 6:10 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 6:10 PM
Surr: 1,2-Dichloroethane-d4 104 80-120 %RECNANA 3/29/2015 6:10 PM
Surr: 4-Bromofluorobenzene 94.7 80-120 %RECNANA 3/29/2015 6:10 PM
Surr: Dibromofluoromethane 99.2 80-120 %RECNANA 3/29/2015 6:10 PM
Surr: Toluene-d8 96.6 80-120 %RECNANA 3/29/2015 6:10 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 40.0 10 mg/L2.0 NA PA/VA3/27/2015 1:38 PM
Page 10 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:05:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-05A Matrix:Groundwater
MW-26Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:06 PM
Barium 0.118 0.100 mg/L0.0010 NA PA/VA4/2/2015 4:06 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 4:06 PM
Chromium 0.0172 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:06 PM
Lead 0.0030 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 4:06 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 4:06 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:06 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury 0.0003 0.0010 J mg/L0.0001 NA PA/VA3/31/2015 10:12 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 6:43 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 6:43 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 6:43 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:43 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 6:43 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 6:43 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 6:43 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 6:43 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 6:43 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 6:43 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 6:43 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 6:43 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 6:43 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 6:43 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 6:43 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 6:43 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 6:43 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 6:43 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 6:43 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 6:43 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 6:43 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 6:43 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 6:43 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 6:43 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 6:43 PM
Page 11 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 9:05:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-05A Matrix:Groundwater
MW-26Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 6:43 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 6:43 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 6:43 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 6:43 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 6:43 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 6:43 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 6:43 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 6:43 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 6:43 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 6:43 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 6:43 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 6:43 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 6:43 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:43 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 6:43 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 6:43 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 6:43 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 6:43 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 6:43 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 6:43 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 6:43 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 6:43 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 6:43 PM
Surr: 1,2-Dichloroethane-d4 105 68.7-129 %RECNANA 3/29/2015 6:43 PM
Surr: 4-Bromofluorobenzene 106 71.8-127 %RECNANA 3/29/2015 6:43 PM
Surr: Dibromofluoromethane 104 74.3-124 %RECNANA 3/29/2015 6:43 PM
Surr: Toluene-d8 95.8 71.4-129 %RECNANA 3/29/2015 6:43 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 6:43 PM
Surr: 1,2-Dichloroethane-d4 104 80-120 %RECNANA 3/29/2015 6:43 PM
Surr: 4-Bromofluorobenzene 94.8 80-120 %RECNANA 3/29/2015 6:43 PM
Surr: Dibromofluoromethane 100 80-120 %RECNANA 3/29/2015 6:43 PM
Surr: Toluene-d8 98.5 80-120 %RECNANA 3/29/2015 6:43 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 267 10 mg/L2.0 NA PA/VA3/27/2015 1:38 PM
Page 12 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:30:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-06A Matrix:Groundwater
MW-27Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:46 PM
Barium 1.15 0.100 mg/L0.0010 NA PA/VA4/2/2015 4:46 PM
Cadmium 0.0003 0.0010 J mg/L0.0002 NA PA/VA4/2/2015 4:46 PM
Chromium 0.0044 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 4:46 PM
Lead 0.0002 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 4:46 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 4:46 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:46 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury 0.0001 0.0010 J mg/L0.0001 NA PA/VA3/31/2015 10:14 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 7:16 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 7:16 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 7:16 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:16 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 7:16 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 7:16 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 7:16 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 7:16 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 7:16 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 7:16 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 7:16 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 7:16 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 7:16 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 7:16 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 7:16 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 7:16 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 7:16 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 7:16 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 7:16 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 7:16 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 7:16 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 7:16 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 7:16 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 7:16 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 7:16 PM
Page 13 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 8:30:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-06A Matrix:Groundwater
MW-27Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 7:16 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 7:16 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 7:16 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 7:16 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 7:16 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 7:16 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 7:16 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 7:16 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 7:16 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 7:16 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 7:16 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 7:16 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 7:16 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:16 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:16 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 7:16 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 7:16 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 7:16 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 7:16 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 7:16 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 7:16 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 7:16 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 7:16 PM
Surr: 1,2-Dichloroethane-d4 111 68.7-129 %RECNANA 3/29/2015 7:16 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 3/29/2015 7:16 PM
Surr: Dibromofluoromethane 106 74.3-124 %RECNANA 3/29/2015 7:16 PM
Surr: Toluene-d8 92.5 71.4-129 %RECNANA 3/29/2015 7:16 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 7:16 PM
Surr: 1,2-Dichloroethane-d4 114 80-120 %RECNANA 3/29/2015 7:16 PM
Surr: 4-Bromofluorobenzene 98.5 80-120 %RECNANA 3/29/2015 7:16 PM
Surr: Dibromofluoromethane 111 80-120 %RECNANA 3/29/2015 7:16 PM
Surr: Toluene-d8 95.0 80-120 %RECNANA 3/29/2015 7:16 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 12.5 5.0 mg/L1.0 NA PA/VA3/27/2015 1:38 PM
Page 14 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:25:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-07A Matrix:Groundwater
MW-28Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic 0.0040 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 4:51 PM
Barium 0.0867 0.100 J mg/L0.0010 NA PA/VA4/2/2015 4:51 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 4:51 PM
Chromium 0.0087 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 4:51 PM
Lead 0.0057 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 4:51 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 4:51 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:51 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:17 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 7:49 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 7:49 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 7:49 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:49 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 7:49 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 7:49 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 7:49 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 7:49 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 7:49 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 7:49 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 7:49 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 7:49 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 7:49 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 7:49 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 7:49 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 7:49 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 7:49 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 7:49 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 7:49 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 7:49 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 7:49 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 7:49 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 7:49 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 7:49 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 7:49 PM
Page 15 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:25:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-07A Matrix:Groundwater
MW-28Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 7:49 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 7:49 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 7:49 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 7:49 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 7:49 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 7:49 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 7:49 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 7:49 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 7:49 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 7:49 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 7:49 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 7:49 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 7:49 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:49 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 7:49 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 7:49 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 7:49 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 7:49 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 7:49 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 7:49 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 7:49 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 7:49 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 7:49 PM
Surr: 1,2-Dichloroethane-d4 104 68.7-129 %RECNANA 3/29/2015 7:49 PM
Surr: 4-Bromofluorobenzene 102 71.8-127 %RECNANA 3/29/2015 7:49 PM
Surr: Dibromofluoromethane 103 74.3-124 %RECNANA 3/29/2015 7:49 PM
Surr: Toluene-d8 95.1 71.4-129 %RECNANA 3/29/2015 7:49 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 7:49 PM
Surr: 1,2-Dichloroethane-d4 108 80-120 %RECNANA 3/29/2015 7:49 PM
Surr: 4-Bromofluorobenzene 95.9 80-120 %RECNANA 3/29/2015 7:49 PM
Surr: Dibromofluoromethane 99.3 80-120 %RECNANA 3/29/2015 7:49 PM
Surr: Toluene-d8 98.1 80-120 %RECNANA 3/29/2015 7:49 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 250 20.0 mg/L4.0 NA PA/VA3/27/2015 1:38 PM
Page 16 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:55:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-08A Matrix:Groundwater
MW-29Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:57 PM
Barium 0.122 0.100 mg/L0.0010 NA PA/VA4/2/2015 4:57 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 4:57 PM
Chromium 0.0244 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:57 PM
Lead 0.0021 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 4:57 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 4:57 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 4:57 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:19 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 8:22 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 8:22 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 8:22 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:22 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 8:22 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 8:22 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 8:22 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 8:22 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 8:22 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 8:22 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 8:22 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 8:22 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 8:22 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 8:22 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 8:22 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 8:22 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 8:22 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 8:22 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 8:22 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 8:22 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 8:22 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 8:22 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 8:22 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 8:22 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 8:22 PM
Page 17 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 11:55:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-08A Matrix:Groundwater
MW-29Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 8:22 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 8:22 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 8:22 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 8:22 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 8:22 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 8:22 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 8:22 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 8:22 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 8:22 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 8:22 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 8:22 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 8:22 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 8:22 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:22 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:22 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 8:22 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 8:22 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 8:22 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 8:22 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 8:22 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 8:22 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 8:22 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 8:22 PM
Surr: 1,2-Dichloroethane-d4 108 68.7-129 %RECNANA 3/29/2015 8:22 PM
Surr: 4-Bromofluorobenzene 102 71.8-127 %RECNANA 3/29/2015 8:22 PM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 3/29/2015 8:22 PM
Surr: Toluene-d8 95.7 71.4-129 %RECNANA 3/29/2015 8:22 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 8:22 PM
Surr: 1,2-Dichloroethane-d4 106 80-120 %RECNANA 3/29/2015 8:22 PM
Surr: 4-Bromofluorobenzene 93.2 80-120 %RECNANA 3/29/2015 8:22 PM
Surr: Dibromofluoromethane 102 80-120 %RECNANA 3/29/2015 8:22 PM
Surr: Toluene-d8 98.5 80-120 %RECNANA 3/29/2015 8:22 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 205 10 mg/L2.0 NA PA/VA3/27/2015 1:38 PM
Page 18 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:16:00 PM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-09A Matrix:Groundwater
MW-30Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 5:03 PM
Barium 0.348 0.100 mg/L0.0010 NA PA/VA4/2/2015 5:03 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 5:03 PM
Chromium 0.0313 0.0100 mg/L0.0010 NA PA/VA4/2/2015 5:03 PM
Lead 0.0048 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 5:03 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 5:03 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 5:03 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:21 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 8:56 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 8:56 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 8:56 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:56 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 8:56 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 8:56 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 8:56 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 8:56 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 8:56 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 8:56 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 8:56 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 8:56 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 8:56 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 8:56 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 8:56 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 8:56 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 8:56 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 8:56 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 8:56 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 8:56 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 8:56 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 8:56 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 8:56 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 8:56 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 8:56 PM
Page 19 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:16:00 PM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-09A Matrix:Groundwater
MW-30Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 8:56 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 8:56 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 8:56 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 8:56 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 8:56 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 8:56 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 8:56 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 8:56 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 8:56 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 8:56 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 8:56 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 8:56 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 8:56 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:56 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 8:56 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 8:56 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 8:56 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 8:56 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 8:56 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 8:56 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 8:56 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 8:56 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 8:56 PM
Surr: 1,2-Dichloroethane-d4 106 68.7-129 %RECNANA 3/29/2015 8:56 PM
Surr: 4-Bromofluorobenzene 105 71.8-127 %RECNANA 3/29/2015 8:56 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 3/29/2015 8:56 PM
Surr: Toluene-d8 95.1 71.4-129 %RECNANA 3/29/2015 8:56 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 8:56 PM
Surr: 1,2-Dichloroethane-d4 103 80-120 %RECNANA 3/29/2015 8:56 PM
Surr: 4-Bromofluorobenzene 95.2 80-120 %RECNANA 3/29/2015 8:56 PM
Surr: Dibromofluoromethane 111 80-120 %RECNANA 3/29/2015 8:56 PM
Surr: Toluene-d8 97.9 80-120 %RECNANA 3/29/2015 8:56 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 444 10 mg/L2.0 NA PA/VA3/27/2015 1:38 PM
Page 20 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 7:50:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-10A Matrix:Groundwater
MW-2 DUPLICATE Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
TOTAL METALS by ICP-MS Method: SW6020A (1998)Analyst: LF
Arsenic ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 5:08 PM
Barium 0.197 0.100 mg/L0.0010 NA PA/VA4/2/2015 5:08 PM
Cadmium ND 0.0010 mg/L0.0002 NA PA/VA4/2/2015 5:08 PM
Chromium 0.0058 0.0100 J mg/L0.0010 NA PA/VA4/2/2015 5:08 PM
Lead 0.0005 0.0100 J mg/L0.0002 NA PA/VA4/2/2015 5:08 PM
Selenium ND 0.0100 mg/L0.0020 NA PA/VA4/2/2015 5:08 PM
Silver ND 0.0100 mg/L0.0010 NA PA/VA4/2/2015 5:08 PM
MERCURY, Total SW7470A Method: SW7470A (1994)Analyst: CR
Mercury ND 0.0010 mg/L0.0001 NA PA/VA3/31/2015 10:23 AM
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 9:29 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 9:29 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 9:29 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 9:29 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 9:29 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 9:29 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 9:29 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 9:29 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 9:29 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 9:29 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 9:29 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 9:29 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 9:29 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 9:29 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 9:29 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 9:29 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 9:29 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 9:29 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 9:29 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 9:29 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 9:29 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 9:29 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 9:29 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 9:29 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 9:29 PM
Page 21 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 7:50:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-10A Matrix:Groundwater
MW-2 DUPLICATE Client Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 9:29 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 9:29 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 9:29 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 9:29 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 9:29 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 9:29 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 9:29 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 9:29 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 9:29 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 9:29 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 9:29 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 9:29 PM
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 9:29 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 9:29 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 9:29 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 9:29 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 9:29 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 9:29 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 9:29 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 9:29 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 9:29 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 9:29 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 9:29 PM
Surr: 1,2-Dichloroethane-d4 111 68.7-129 %RECNANA 3/29/2015 9:29 PM
Surr: 4-Bromofluorobenzene 107 71.8-127 %RECNANA 3/29/2015 9:29 PM
Surr: Dibromofluoromethane 101 74.3-124 %RECNANA 3/29/2015 9:29 PM
Surr: Toluene-d8 93.9 71.4-129 %RECNANA 3/29/2015 9:29 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 9:29 PM
Surr: 1,2-Dichloroethane-d4 110 80-120 %RECNANA 3/29/2015 9:29 PM
Surr: 4-Bromofluorobenzene 96.7 80-120 %RECNANA 3/29/2015 9:29 PM
Surr: Dibromofluoromethane 94.0 80-120 %RECNANA 3/29/2015 9:29 PM
Surr: Toluene-d8 96.2 80-120 %RECNANA 3/29/2015 9:29 PM
TOTAL SUSPENDED SOLIDS Method: SM2540 D-1997 Analyst: SF
Total Suspended Solids 66.0 5.0 mg/L1.0 NA PA/VA3/27/2015 1:38 PM
Page 22 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:00:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-11A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
VOLATILE ORGANIC COMPOUNDS-8260 Method: SW8260B (1996)Analyst: JM
trans-1,4-Dichloro-2-butene ND 50.0 µg/L5.00 NA 3/29/2015 10:02 PM
Acetone ND 100 µg/L5.00 NA PA/VA3/29/2015 10:02 PM
Acrylonitrile ND 200 µg/L2.42 NA PA/VA3/29/2015 10:02 PM
Benzene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 10:02 PM
Bromochloromethane ND 3.00 µg/L0.213 NA PA/VA3/29/2015 10:02 PM
Bromodichloromethane ND 1.00 µg/L0.184 NA PA/VA3/29/2015 10:02 PM
Bromoform ND 3.00 µg/L0.482 NA PA/VA3/29/2015 10:02 PM
Bromomethane ND 10.0 µg/L0.420 NA PA/VA3/29/2015 10:02 PM
2-Butanone ND 100 µg/L4.74 NA PA/VA3/29/2015 10:02 PM
Carbon disulfide ND 100 µg/L2.25 NA 3/29/2015 10:02 PM
Carbon tetrachloride ND 1.00 µg/L0.166 NA PA/VA3/29/2015 10:02 PM
Chlorobenzene ND 3.00 µg/L0.350 NA PA/VA3/29/2015 10:02 PM
Chloroethane ND 10.0 µg/L0.270 NA PA/VA3/29/2015 10:02 PM
Chloroform ND 5.00 µg/L0.400 NA PA/VA3/29/2015 10:02 PM
Chloromethane ND 1.00 µg/L0.350 NA PA/VA3/29/2015 10:02 PM
Dibromochloromethane ND 3.00 µg/L0.415 NA PA/VA3/29/2015 10:02 PM
1,2-Dibromo-3-chloropropane ND 13.0 µg/L0.429 NA PA/VA3/29/2015 10:02 PM
1,2-Dibromoethane ND 1.00 µg/L0.399 NA PA/VA3/29/2015 10:02 PM
Dibromomethane ND 10.0 µg/L0.418 NA PA/VA3/29/2015 10:02 PM
1,2-Dichlorobenzene ND 5.00 µg/L0.480 NA PA/VA3/29/2015 10:02 PM
1,4-Dichlorobenzene ND 1.00 µg/L0.452 NA PA/VA3/29/2015 10:02 PM
1,1-Dichloroethane ND 5.00 µg/L0.250 NA PA/VA3/29/2015 10:02 PM
1,2-Dichloroethane ND 1.00 µg/L0.231 NA PA/VA3/29/2015 10:02 PM
1,1-Dichloroethene ND 5.00 µg/L0.280 NA PA/VA3/29/2015 10:02 PM
cis-1,2-Dichloroethene ND 5.00 µg/L0.200 NA PA/VA3/29/2015 10:02 PM
trans-1,2-Dichloroethene ND 5.00 µg/L0.250 NA PA/VA3/29/2015 10:02 PM
1,2-Dichloropropane ND 1.00 µg/L0.200 NA PA/VA3/29/2015 10:02 PM
cis-1,3-Dichloropropene ND 1.00 µg/L0.231 NA PA/VA3/29/2015 10:02 PM
trans-1,3-Dichloropropene ND 1.00 µg/L0.292 NA PA/VA3/29/2015 10:02 PM
Ethylbenzene ND 1.00 µg/L0.311 NA PA/VA3/29/2015 10:02 PM
2-Hexanone ND 50.0 µg/L3.12 NA PA/VA3/29/2015 10:02 PM
Iodomethane ND 10.0 µg/L2.22 NA PA/VA3/29/2015 10:02 PM
Methylene chloride ND 1.00 µg/L0.420 NA PA/VA3/29/2015 10:02 PM
4-Methyl-2-pentanone ND 100 µg/L3.15 NA PA/VA3/29/2015 10:02 PM
Styrene ND 1.00 µg/L0.346 NA PA/VA3/29/2015 10:02 PM
1,1,1,2-Tetrachloroethane ND 5.00 µg/L0.359 NA PA/VA3/29/2015 10:02 PM
1,1,2,2-Tetrachloroethane ND 3.00 µg/L0.497 NA PA/VA3/29/2015 10:02 PM
Page 23 of 24
WO#: 1503V13
Date Reported: 4/7/2015
REI Consultants, Inc. - Analytical Report
Client:COUNTY OF CATAWBA Collection Date:3/25/2015 12:00:00 AM
Project:BLACKBURN C&D - 1SA 2015
Lab ID:1503V13-11A Matrix:Trip Blank
TRIP BLANKClient Sample ID:
Analysis Date AnalyzedResultMDLQualUnitsPQLMCL
Date Received:3/26/2015
CATAWBA CO N.C.Site ID:
NELAP
Tetrachloroethene ND 1.00 µg/L0.290 NA PA/VA3/29/2015 10:02 PM
Toluene ND 1.00 µg/L0.250 NA PA/VA3/29/2015 10:02 PM
1,1,1-Trichloroethane ND 1.00 µg/L0.250 NA PA/VA3/29/2015 10:02 PM
1,1,2-Trichloroethane ND 1.00 µg/L0.307 NA PA/VA3/29/2015 10:02 PM
Trichloroethene ND 1.00 µg/L0.270 NA PA/VA3/29/2015 10:02 PM
Trichlorofluoromethane ND 1.00 µg/L0.223 NA PA/VA3/29/2015 10:02 PM
1,2,3-Trichloropropane ND 1.00 µg/L0.428 NA PA/VA3/29/2015 10:02 PM
Vinyl acetate ND 50.0 µg/L0.288 NA PA/VA3/29/2015 10:02 PM
Vinyl chloride ND 1.00 µg/L0.350 NA PA/VA3/29/2015 10:02 PM
o-Xylene ND 1.00 µg/L0.306 NA PA/VA3/29/2015 10:02 PM
m,p-Xylene ND 2.00 µg/L0.698 NA PA/VA3/29/2015 10:02 PM
Surr: 1,2-Dichloroethane-d4 106 68.7-129 %RECNANA 3/29/2015 10:02 PM
Surr: 4-Bromofluorobenzene 103 71.8-127 %RECNANA 3/29/2015 10:02 PM
Surr: Dibromofluoromethane 105 74.3-124 %RECNANA 3/29/2015 10:02 PM
Surr: Toluene-d8 94.8 71.4-129 %RECNANA 3/29/2015 10:02 PM
VOLATILE ORGANIC COMPOUNDS-
ADDITIONAL
Method: SW8260B (1996)Analyst: JM
Tetrahydrofuran ND 50.0 µg/L12.5 NA 3/29/2015 10:02 PM
Surr: 1,2-Dichloroethane-d4 95.2 80-120 %RECNANA 3/29/2015 10:02 PM
Surr: 4-Bromofluorobenzene 94.8 80-120 %RECNANA 3/29/2015 10:02 PM
Surr: Dibromofluoromethane 105 80-120 %RECNANA 3/29/2015 10:02 PM
Surr: Toluene-d8 97.4 80-120 %RECNANA 3/29/2015 10:02 PM
Page 24 of 24
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
DB
P i x
E v a l u a t i on
w w w.
a mm
a r a .c om
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD5:
FieldSamplingSummaries
and
FieldSampleLogs
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Rain, LightRain,andOvercast 51-55°F
Property Units MW-2 MW-21 MW-24 MW-25
SamplingDepth Feet 18.02 51.91 11.73 6.92
StaticDepth Feet 17.21 51.13 10.93 5.86
WellDepth Feet 23.99 62.63 22.78 13.94
WaterColumnHeight Feet 6.78 11.50 11.85 8.08
VolumePurged Liters 13 20 22 15
PurgingStatus -FinishedPurgingFinishedPurgingFinishedPurgingFinishedPurging
PhysicalProperty Units MW-2 MW-21 MW-24 MW-25
pH SU 5.43Dup5.42 6.16 6.31 6.03
Temperature oC 15.3Dup15.3 15.5 13.8 12.0
Conductivity umhos/cm 241Dup242 51.1 1555 740
Turbidity NTU 56.5Dup56.9 359 203 35.3
Appearance -Cloudy Cloudy Cloudy Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 39.5 610 203 40
Property Units MW-26 MW-27 MW-28 MW-29
SamplingDepth Feet 6.78 12.59 4.87 10.36
StaticDepth Feet 4.67 12.27 4.87 9.59
WellDepth Feet 22.41 28.00 14.92 23.13
WaterColumnHeight Feet 17.74 15.73 10.05 13.54
VolumePurged Liters 31 28 0 24
PurgingStatus -FinishedPurgingFinishedPurging 0 FinishedPurging
PhysicalProperty Units MW-26 MW-27 MW-28 MW-29
pH SU 5.84 6.25 6.39 5.77
Temperature oC 10.3 15.4 12.1 13.2
Conductivity umhos/cm 94.1 1268 213 122
Turbidity NTU 239 26.9 >800 480
Appearance -Cloudy Cloudy Red Cloudy
Odor -No Odor No Odor No Odor No Odor
TotalSuspendedSolids(TSS)mg/L 267 12.5 250 205
SAMPLING LOG SUMMARY
BlackburnC&D Landfill(Permit:#18-03)
1503V13
3/25/2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
REICJob#:
Sampling Date:
Sampler(s):Randy Farley /AllenMcBride/RickyTalley / J.D.Bennett
WeatherConditions:Rain, LightRain,andOvercast 51-55°F
SAMPLING LOG SUMMARY
BlackburnC&D Landfill(Permit:#18-03)
1503V13
3/25/2015
Property Units MW-30
SamplingDepth Feet 16.57
StaticDepth Feet 14.34
WellDepth Feet 22.85
WaterColumnHeight Feet 8.51
VolumePurged Liters 15
PurgingStatus -FinishedPurging
PhysicalProperty Units MW-30
pH SU 5.80
Temperature oC 15.0
Conductivity umhos/cm 190
Turbidity NTU 466
Appearance -Cloudy
Odor -No Odor
TotalSuspendedSolids(TSS)mg/L 444
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 2
ProjectName:Project :Well #:MW-2
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Overcast 55 °F
17.21 (Ft)3.92 (Liters)
23.99 (Ft)11.77 (Liters)
6.78 (Ft)13.00 (Liters)
pH
Time (SU)
07:39 5.32
07:40 5.37
07:41 5.39
07:43 5.40
07:44 5.40
07:45 5.40
07:46
Date:Time:07:50
Method:SamplingDepth:18.02'
pH:5.43Dup5.42 (SU)Conductivity:241Dup242 (umhos/cm)
Temperature:15.3Dup15.3 (oC)Turbidity:56.5Dup56.9 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
NoOdor
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Cloudy Odor:Appearance:
PHYSICAL CHARACTERISTICSOFSAMPLE
3/25/2015
TeflonBailer
SAMPLINGDATA
Finished Purging 13
231.0 15.6 17.94 11
234.0 15.5 24.9 9
232.0 15.5 48.9 5
239.0 15.6 23.3 7
227.0 15.5 34.7 3
222.0 15.4 1.99 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TemperatureCorrected Temperature Turbidity VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
3/25/201507:30 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
RodneyHamby 704-462-1348
WELL CONDITIONDATA
BlackburnC&D 1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 3
ProjectName:Project :Well #:MW-21
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 53 °F
51.13 (Ft)6.65 (Liters)
62.63 (Ft)19.97 (Liters)
11.50 (Ft)20.00 (Liters)
pH
Time (SU)
09:41 6.03
09:43 6.07
09:45 6.12
09:47 6.13
09:49 6.12
09:51 6.12
09:51
Date:Time:09:54
Method:SamplingDepth:51.91'
pH:6.16 (SU)Conductivity:51.1 (umhos/cm)
Temperature:15.5 (oC)Turbidity:359 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:
TeflonBailer
NoOdor
PHYSICAL CHARACTERISTICSOFSAMPLE
3/25/2015
SAMPLINGDATA
Finished Purging 20
50.9 15.7 358 20
51.1 15.6 307 16
50.9
50.6 15.5 280 12
15.6 290 8
51.3 15.5 219 4
51.9 15.4 5.74 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
Turbidity VolumePurgedTemperatureCorrectedTemperature
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
WaterColumnHeight VolumePurged
StaticDepth(DepthtoWater)Volume
3/25/201509:35 WeatherConditions:
PURGINGDATA
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
BlackburnC&D 1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 4
ProjectName:Project :Well #:MW-24
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 53 °F
10.93 (Ft)6.86 (Liters)
22.78 (Ft)20.58 (Liters)
11.85 (Ft)22.00 (Liters)
pH
Time (SU)
10:26 5.63
10:27 6.09
10:29 6.23
10:31 6.28
10:33 6.27
10:34
Date:Time:10:37
Method:SamplingDepth:11.73'
pH:6.31 (SU)Conductivity:1555 (umhos/cm)
Temperature:13.8 (oC)Turbidity:203 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
TeflonBailer
Appearance:Cloudy Odor:NoOdor
PHYSICAL CHARACTERISTICSOFSAMPLE
3/25/2015
SAMPLINGDATA
22Finished Purging
201,589.0 14.0 308
1,140.0 13.8 289 15
1,527.0 14.0 192 10
5657.0 13.4 51
145.1 13.1 1.21 1
(oC)(NTU)Conductivity(umhos/cm)(Liters)
TemperatureCorrected Temperature Turbidity VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
WellDepth 3Volumes
3/25/201510:15 WeatherConditions:
StaticDepth(DepthtoWater)Volume
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby
1stSemi2015
704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 5
ProjectName:Project :Well #:MW-25
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Rain 51 °F
5.86 (Ft)4.67 (Liters)
13.94 (Ft)14.03 (Liters)
8.08 (Ft)15.00 (Liters)
pH
Time (SU)
10:55 6.04
10:56 6.03
10:57 6.03
10:59 6.03
11:00 6.01
11:02 6.06
11:02
Date:Time:11:07
Method:SamplingDepth:6.92'
pH:6.03 (SU)Conductivity:740 (umhos/cm)
Temperature:12.0 (oC)Turbidity:35.3 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
Cloudy
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
TeflonBailer
Odor:NoOdorAppearance:
PHYSICAL CHARACTERISTICSOFSAMPLE
3/25/2015
SAMPLINGDATA
Finished Purging 15
768.0 12.5 101 15
611.0 12.1 73.6 12
9534.0 11.6 243
11.3 >800 6623.0
590.0 11.2 >800 3
1636.0 11.1 288
Conductivity(umhos/cm)(oC)(NTU)(Liters)
TemperatureCorrected Temperature Turbidity VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
WaterColumnHeight VolumePurged
3/25/201510:50 WeatherConditions:
StaticDepth(DepthtoWater)Volume
PURGINGDATA
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
BlackburnC&D
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 6
ProjectName:Project :Well #:MW-26
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Overcast 54 °F
4.67 (Ft)10.27 (Liters)
22.41 (Ft)30.81 (Liters)
17.74 (Ft)31.00 (Liters)
pH
Time (SU)
08:32 6.20
08:53 5.83
08:54 5.78
08:56 5.76
08:58 5.74
09:00 5.75
09:00
Date:Time:09:05
Method:SamplingDepth:6.78'
pH:5.84 (SU)Conductivity:94.1 (umhos/cm)
Temperature:10.3 (oC)Turbidity:239 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
NoOdorOdor:Appearance:Cloudy
3/25/2015
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
31Finished Purging
108.7 11.5 798 30
24108.8 11.4 616
106.3 10.9 >800 18
104.6 10.7 543 12
6103.6 10.5 437
108.7 10.8 101 1
Conductivity(umhos/cm)(oC)(NTU)(Liters)
VolumePurgedTemperatureCorrectedTemperatureTurbidity
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
3/25/201508:43 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 7
ProjectName:Project :Well #:MW-27
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Overcast 55 °F
12.27 (Ft)9.10 (Liters)
28.00 (Ft)27.32 (Liters)
15.73 (Ft)28.00 (Liters)
pH
Time (SU)
08:18 6.29
08:19 6.35
08:20 6.30
08:22 6.30
08:23 6.30
08:26 6.29
08:27
Date:Time:08:30
Method:SamplingDepth:12.59'
pH:6.25 (SU)Conductivity:1268 (umhos/cm)
Temperature:15.4 (oC)Turbidity:26.9 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:NoOdor
3/25/2015
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
Finished Purging 28
15.2 48.7 251,384.0
1,443.0 15.2 38.1 20
151,401.0 15.0 36.5
101,410.0 14.9 29.6
1,274.0 14.2 42.6 5
11,244.0 14.2 6.97
(Liters)Conductivity(umhos/cm)
VolumePurged
(oC)(NTU)
TemperatureCorrected Temperature Turbidity
EVACUATION/STABILIZATIONTESTDATA
WaterColumnHeight VolumePurged
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
3/25/201508:13 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
704-462-1348RodneyHamby
BlackburnC&D 1stSemi2015
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 8
ProjectName:Project :Well #:MW-28
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 51 °F
4.87 (Ft)5.80 (Liters)
14.92 (Ft)17.45 (Liters)
10.05 (Ft)0.00 (Liters)
pH
Time (SU)
Date:Time:11:25
Method:SamplingDepth:4.87'
pH:6.39 (SU)Conductivity:213 (umhos/cm)
Temperature:12.1 (oC)Turbidity:>800 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:
SampledOnly-DidNot Purge
Red Odor:NoOdor
3/25/2015
PHYSICAL CHARACTERISTICSOFSAMPLE
DisposableBailer
SAMPLINGDATA
Conductivity(umhos/cm)
Temperature Turbidity VolumePurged
(Liters)
TemperatureCorrected
(oC)(NTU)
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
WaterColumnHeight VolumePurged
3/25/201511:17 WeatherConditions:
StaticDepth(DepthtoWater)Volume
PURGINGDATA
WellCasingBent-SampledOnly
ProtectiveCasingLocked Concrete/GroutPadPresent
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
BlackburnC&D
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 9
ProjectName:Project :Well #:MW-29
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 51 °F
9.59 (Ft)7.83 (Liters)
23.13 (Ft)23.51 (Liters)
13.54 (Ft)24.00 (Liters)
pH
Time (SU)
11:43 5.83
11:44 5.76
11:46 5.73
11:47 5.71
11:49 5.77
11:50 5.77
11:51
Date:Time:11:55
Method:SamplingDepth:10.36'
pH:5.77 (SU)Conductivity:122.3 (umhos/cm)
Temperature:13.2 (oC)Turbidity:480 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:NoOdor
3/25/2015
PHYSICAL CHARACTERISTICSOFSAMPLE
TeflonBailer
SAMPLINGDATA
Finished Purging 24
122.0 13.2 567 20
121.5 13.1
119.8 12.6 552 12
486 16
12.7 385 8
118.1 12.6
119.3
117.9 12.3 8.27 1
165 4
(oC)(NTU)(Liters)
TemperatureCorrected Temperature
Conductivity(umhos/cm)
Turbidity VolumePurged
WaterColumnHeight VolumePurged
EVACUATION/STABILIZATIONTESTDATA
WellDepth 3Volumes
StaticDepth(DepthtoWater)Volume
3/25/201511:37 WeatherConditions:
PURGINGDATA
CaponWellRiser 2"PVCCasing
ProtectiveCasingLocked Concrete/GroutPadPresent
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
RodneyHamby 704-462-1348
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page10
ProjectName:Project :Well #:MW-30
ContactPerson:Phone #:
Y N Y N
x x
x x
x x
Comments:
Date/Time:Lt.Rain 51 °F
14.34 (Ft)4.92 (Liters)
22.85 (Ft)14.78 (Liters)
8.51 (Ft)15.00 (Liters)
pH
Time (SU)
12:07 5.65
12:08 5.65
12:09 5.64
12:10 5.67
12:11 5.72
12:13 5.70
12:13
Date:Time:12:16
Method:SamplingDepth:16.57'
pH:5.80 (SU)Conductivity:190 (umhos/cm)
Temperature:15.0 (oC)Turbidity:466 (NTU)
Comments:
SampledBy:
Sampler'sSignature:Date:3/25/2015
RandyFarley /AllenMcBride /RickyTalley / J.D.Bennett
Appearance:Cloudy Odor:NoOdor
3/25/2015
TeflonBailer
PHYSICAL CHARACTERISTICSOFSAMPLE
SAMPLINGDATA
15Finished Purging
>800222.0 14.9
12
15
9198.8 14.9
212.0 14.9 >800
>800
196.6 14.9
3
6530
1197.3 14.5
193.3 14.6 464
139
Conductivity(umhos/cm)(oC)
VolumePurged
(Liters)
TemperatureCorrected Temperature Turbidity
(NTU)
EVACUATION/STABILIZATIONTESTDATA
3VolumesWellDepth
WaterColumnHeight VolumePurged
StaticDepth(DepthtoWater)Volume
WeatherConditions:3/25/201512:02
PURGINGDATA
Concrete/GroutPadPresentProtectiveCasingLocked
CaponWellRiser 2"PVCCasing
ProtectiveCasingPresent PhysicalDamage
WELL CONDITIONDATA
704-462-1348RodneyHamby
REICONSULTANTS,INC. GROUNDWATERSAMPLINGLOG
BlackburnC&D 1stSemi2015
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page11
Catawba County,North Carolina
BlackburnLandfill
Permit Number:18-03
C &D Landfill
AppendixD6:
Historical Results
REI Consultants, Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-2
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-21
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 6
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-24
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page11
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-25
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page16
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-26
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page21
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-27
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page24
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-28
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page27
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-29
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page30
C &D Landfills
HistoricalDataSummary
MonitoringWell:MW-30
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page33
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
AppendixE:
Alternate Source Demonstration
REIConsultants,Inc.P.OBox286,Beaver,WV25813800-999-0105 www.reiclabs.com
ALTERNATESOURCEDEMONSTRATION
1st Semiannual2015Event
BlackburnResourceRecoveryFacility,PermitNo.18-03
CatawbaCounty,NorthCarolina
Preparedfor:
CountyofCatawba
P.O.Box389
Newton,NC28658
Preparedby:
REIConsultantsofNorthCarolina,PLLC
LicenseNo.P-1018
P.O.Box286
Beaver,WV25813
MichaelP.Hofe,PE
LicenseNo.028029
Date:________________________May18,2015
1
1.0 EXCEEDANCEDESCRIPTION
REIConsultantsofNorthCarolina,PLLC(REICofNC),onbehalfofCatawbaCounty,
issubmittingthisAlternateSourceDemonstration(ASD)forBlackburnResource
RecoveryFacility,PermitNo.18-03,pursuanttoNorthCarolinawastemanagement
regulations15NCAC13B.1633,duetoexceedancesofNorthCarolinagroundwater
protectionstandardsformetalsduringthe 1st semi-annualmonitoringperiodof2015.
NorthCarolinagroundwaterprotectionstandardsincludebothgroundwaterstandardsand
interimmaximumallowableconcentrations(IMACs)givenin15ANCAC2L.0202,
effectiveApril1,2013.Thefollowingmetalsexceededgroundwaterprotection
standardsintheindicatedcompliancewells:
Parameter Well
SubtitleDUnit2
Cobalt MW-12,MW-16
Vanadium MW-16
SubtitleDUnit3
Barium MW-33
Chromium MW-31,MW-32,MW-33,MW-34
Cobalt MW-31,MW-32,MW-33
Lead MW-33
Vanadium MW-31,MW-32,MW-33
C&DUnit1
Barium MW-27
Chromium MW-26
C&DUnit2
Chromium MW-24,MW-29,MW-30
2.0 DATAEVALUATION
Statisticalanalysisofbackgrounddatafromupgradientwellsatthefacilityindicatesthat
alloftheaboveexceedancesarelowerthanbackgroundstatisticallimits.Statistical
analysisofgroundwaterdatawasconductedbyconstructingpredictionlimitsfrom
availableupgradientbackgrounddata.DatafromwellsMW-4andMW-10,whichhave
beenabandonedduetofacilityexpansion,andwellMW-20werepooledandutilizedfor
2
comparisontodatafromcompliancewellsassociatedwiththeSubtitleDUnit2andUnit
3landfillsandtheC&DUnit1landfill.DatafromwellMW-21wasutilizedfor
comparisontodatafromcompliancewellsassociatedwiththeC&DUnit2landfill.The
statisticalanalysisisincludedinthisreport.Thefollowingtablessummarize,forthose
compliancewellsandparametersforwhichgroundwaterprotectionstandardswere
exceededduringthe 1st semiannual2015event,thesampleresults,reportinglimits,
applicablegroundwaterprotectionstandards,andbackgroundstatisticallimits:
SubtitleDUnit 2
SWSL GPS UPL MW-12MW-16
Cobalt 0.010 0.001 0.230 0.0248 0.0230
Vanadium 0.025 0.0003 0.880 -0.0351
SubtitleDUnit 3
SWSL GPS UPL MW-31MW-32MW-33MW-34
Barium 0.100 0.7 5.44 --0.726 -
Chromium 0.010 0.01 0.860 0.0428 0.0298 0.0440 0.0180
Cobalt 0.010 0.001 0.230 0.0151 0.0116 0.0374 -
Lead 0.010 0.015 0.045 --0.0170 -
Vanadium 0.025 0.0003 0.880 0.0488 0.0740 0.257 -
C&DUnit 1
SWSL GPS UPL MW-26MW-27
Barium 0.100 0.7 5.44 -1.15
Chromium 0.010 0.01 0.860 0.0172 -
C&DUnit 2
SWSL GPS UPL MW-24MW-29MW-30
Chromium 0.010 0.01 0.110 0.0391 0.0244 0.0313
Notes:
Allvaluesinmg/L
SWSL–SolidWasteSectionLimit(reportinglimit)
GPS–15ANCAC2L.0202groundwaterprotectionstandard
UPL–upperpredictionlimit
“-“–notdetected aboveGPS
Notethatnoneoftheresultsexceededthestatisticalbackgroundlimits.Allofthe
parameterswhichexceededgroundwaterprotectionstandardshavebeenobservedinthe
upgradientbackgroundwellsatthefacilityathigherlevelsthanthoseexhibitedin
compliancewells.
3
3.0 CONCLUSIONS
ItistheprofessionalopinionofREICofNCthatthegroundwaterprotectionstandard
exceedancesofmetalsincompliancewellswerenottheresultofareleasefromthe
landfill,butratherareduetonaturalvariation.Thisconclusionisbaseduponthe
availabledatacollectedfrombackgroundandcompliancewellsatthefacility,and
applicationofstatisticalprocedurestocomparedataupgradientanddowngradientofthe
landfills.Barium,chromium,cobalt,lead,andvanadiumhavebeenobservedinsamples
collectedfrombackgroundwellsatthefacility,whichindicatesthatthesemetalsare
presentnaturallyinareasofthefacilityupgradientofwasteunits.Inaddition,the
statisticallimitsderivedfromupgradientdataareconsiderablyhigherthanconcentrations
ofthemetalsobservedduringthe 1st semiannual2015monitoringevent.Sincethe
metalsintheaffectedwellsdonotexceedbackground,thepresenceofthemetalsis
attributedtonaturalvariation.
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
C&D
StatisticalEvaluation
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 1
WellNumber Date Barium Chromium Lead
MW-21 Jul-02 0.51 0.016 0.010
MW-21 Sep-02 1.19 0.050 0.021
MW-21 Mar-03 1.94 0.048 0.028
MW-21 Sep-03 1.03 0.032 0.005
MW-21 Mar-04 1.47 0.110 0.027
MW-21 Sep-04 <0.5 0.005 0.005
MW-21 Mar-05 <0.5 0.005 0.005
MW-21 Sep-05 <0.5 0.005 0.005
MW-21 Mar-06 <0.5 0.005 0.005
MW-21 Sep-06 0.260 0.005 0.005
MW-21 Mar-07 0.295 0.005 0.005
MW-21 Sep-07 0.440 0.005 0.005
MW-21 Mar-08 0.199 0.005 0.005
MW-21 Sep-08 0.119 0.0412 0.0143
MW-21 Mar-09 1.34 0.005 0.005
MW-21 Sep-09 0.492 0.005 0.005
MW-21 Mar-10 0.525 0.0157 0.005
MW-21 Sep-10 0.286 0.005 0.005
MW-21 Mar-11 0.414 0.0229 0.005
MW-21 Sep-11 0.366 0.0116 0.005
MW-21 Mar-12 0.336 0.005 0.005
MW-21 Sep-12 0.348 0.005 0.005
MW-21 Mar-13 0.215 0.005 0.005
MW-21 Sep-13 0.416 0.0102 0.005
MW-21 Mar-14 0.601 0.0477 0.005
MW-21 Sep-14 0.232 0.0182 0.005
MW-21 Mar-15 0.354 0.0257 0.005
27 27 27
4 14 22
15%52%81%
Parametric Non-parametric Non-parametric
UpperPredictionLimit 1.62 0.110 0.028
Method
HISTORICALBACKGROUNDDATA
#Observations
# Non-detects
% Non-detects
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 2
Barium ln(Barium)Shapiro-Wilk Normality Test
0.119 -2.1286 0.6627 2.791 0.4366 1.219
0.199 -1.6145 0.3853 2.000 0.3018 0.604
0.215 -1.5371 0.2927 1.830 0.2522 0.461
0.232 -1.4610 0.1740 1.635 0.2152 0.352
0.25 -1.3863 0.0296 1.416 0.1848 0.262
0.25 -1.3863-0.5092 0.877 0.1584 0.139
0.25 -1.3863-0.6444 0.742 0.1346 0.100
0.25 -1.3863-0.6733 0.713 0.1128 0.080
0.26 -1.3471-0.7093 0.638 0.0923 0.059
0.286 -1.2518-0.8210 0.431 0.0728 0.031
0.295 -1.2208-0.8771 0.344 0.0540 0.019
0.336 -1.0906-0.8819 0.209 0.0358 0.007
0.348 -1.0556-1.0051 0.050 0.0178 0.001
0.354 -1.0385-1.0385 0.000 0.0000 0.000
0.366 -1.0051-1.0556 -0.050
0.414 -0.8819-1.0906 -0.209 b=3.334
0.416 -0.8771-1.2208 -0.344
0.44 -0.8210-1.2518 -0.431
0.492 -0.7093-1.3471 -0.638
0.51 -0.6733-1.3863 -0.713
0.525 -0.6444-1.3863 -0.742
0.601 -0.5092-1.3863 -0.877
1.03 0.0296-1.3863 -1.416
1.19 0.1740-1.4610 -1.635
1.34 0.2927-1.5371 -1.830
1.47 0.3853-1.6145 -2.000
1.94 0.6627-2.1286 -2.791
s=0.681
W=0.923greater than0.894,lognormalassumptionnotrejected
EPAUnified Guidance, Table19-1(8COCs,n=27,w=5):
COCs 25 27 30
5 1.90 1.88 1.86
8 2.01
10 2.11 2.09 2.06
mean=-0.884
s=0.681
=2.01
UPL=1.62
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 3
CatawbaCounty,NorthCarolina
Blackburn Landfill
Permit Number:18-03
Units 2 & 3
StatisticalEvaluation
REIConsultants,Inc.P.O.Box286,Beaver,WV25813 Phone:[phone] www.reiclabs.com Page 4
i xi i/(n+1)mi mi*xi mi2
1 0.005 0.017 -2.1213 -0.0106 4.4998
2 0.005 0.034 -1.8264 -0.0091 3.3356
3 0.005 0.051 -1.6367 -0.0082 2.6788
4 0.005 0.068 -1.4924 -0.0075 2.2273
5 0.005 0.085 -1.3738 -0.0069 1.8874
6 0.005 0.102 -1.2720 -0.0064 1.6179
7 0.0111 0.119 -1.1818 -0.0131 1.3966
8 0.0121 0.136 -1.1003 -0.0133 1.2107
9 0.0125 0.153 -1.0256 -0.0128 1.0518
10 0.0134 0.169 -0.9562 -0.0128 0.9143
11 0.0140 0.186 -0.8911 -0.0125 0.7940
12 0.0161 0.203 -0.8296 -0.0134 0.6882
13 0.0210 0.220 -0.7710 -0.0162 0.5945
14 0.025 0.237 -0.7151 -0.0179 0.5113
15 0.025 0.254 -0.6612 -0.0165 0.4372
16 0.025 0.271 -0.6092 -0.0152 0.3712
17 0.025 0.288 -0.5588 -0.0140 0.3123
18 0.025 0.305 -0.5098 -0.0127 0.2599
19 0.025 0.322 -0.4620 -0.0116 0.2135
20 0.025 0.339 -0.4152 -0.0104 0.1724
21 0.025 0.356 -0.3694 -0.0092 0.1364
22 0.025 0.373 -0.3242 -0.0081 0.1051
23 0.025 0.390 -0.2798 -0.0070 0.0783
24 0.025 0.407 -0.2358 -0.0059 0.0556
25 0.025 0.424 -0.1924 -0.0048 0.0370
26 0.025 0.441 -0.1493 -0.0037 0.0223
27 0.025 0.458 -0.1064 -0.0027 0.0113
28 0.025 0.475 -0.0638 -0.0016 0.0041
29 0.025 0.492 -0.0212 -0.0005 0.0005
30 0.025 0.508 0.0212 0.0005 0.0005
31 0.025 0.525 0.0638 0.0016 0.0041
32 0.025 0.542 0.1064 0.0027 0.0113
33 0.025 0.559 0.1493 0.0037 0.0223
34 0.025 0.576 0.1924 0.0048 0.0370
35 0.0327 0.593 0.2358 0.0077 0.0556
36 0.0336 0.610 0.2798 0.0094 0.0783
37 0.0350 0.627 0.3242 0.0113 0.1051
38 0.0368 0.644 0.3694 0.0136 0.1364
39 0.053 0.661 0.4152 0.0220 0.1724
40 0.056 0.678 0.4620 0.0259 0.2135
41 0.059 0.695 0.5098 0.0301 0.2599
42 0.066 0.712 0.5588 0.0367 0.3123
43 0.078 0.729 0.6092 0.0472 0.3712
44 0.084 0.746 0.6612 0.0557 0.4372
45 0.086 0.763 0.7151 0.0615 0.5113
46 0.100 0.780 0.7710 0.0771 0.5945
47 0.109 0.797 0.8296 0.0904 0.6882
48 0.116 0.814 0.8911 0.1034 0.7940
49 0.130 0.831 0.9562 0.1243 0.9143
50 0.140 0.847 1.0256 0.1436 1.0518
51 0.200 0.864 1.1003 0.2205 1.2107
52 0.213 0.881 1.1818 0.2517 1.3966
53 0.220 0.898 1.2720 0.2798 1.6179
54 0.223 0.915 1.3738 0.3064 1.8874
55 0.252 0.932 1.4924 0.3761 2.2273
56 0.471 0.949 1.6367 0.7709 2.6788
57 0.680 0.966 1.8264 1.2419 3.3356
58 0.695 0.983 2.1213 1.4743 4.4998
sum 5.5103 51.2506
S.D.=0.141
W'=0.520 Þ less than0.945,normalassumptionrejected
Zinc
Shapiro-FranciaTest-NormalAssumption
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Zinc
i yi i/(n+1)mi mi*yi mi2
1 -5.298 0.017 -2.1213 11.2392 4.4998
2 -5.298 0.034 -1.8264 9.6766 3.3356
3 -5.298 0.051 -1.6367 8.6717 2.6788
4 -5.298 0.068 -1.4924 7.9072 2.2273
5 -5.298 0.085 -1.3738 7.2790 1.8874
6 -4.501 0.102 -1.2720 5.7248 1.6179
7 -4.415 0.119 -1.1818 5.2171 1.3966
8 -4.382 0.136 -1.1003 4.8217 1.2107
9 -4.313 0.153 -1.0256 4.4229 1.0518
10 -4.269 0.169 -0.9562 4.0816 0.9143
11 -4.129 0.186 -0.8911 3.6792 0.7940
12 -3.863 0.203 -0.8296 3.2048 0.6882
13 -3.689 0.220 -0.7710 2.8443 0.5945
14 -3.689 0.237 -0.7151 2.6377 0.5113
15 -3.689 0.254 -0.6612 2.4391 0.4372
16 -3.689 0.271 -0.6092 2.2474 0.3712
17 -3.689 0.288 -0.5588 2.0615 0.3123
18 -3.689 0.305 -0.5098 1.8807 0.2599
19 -3.689 0.322 -0.4620 1.7043 0.2135
20 -3.689 0.339 -0.4152 1.5318 0.1724
21 -3.689 0.356 -0.3694 1.3625 0.1364
22 -3.689 0.373 -0.3242 1.1961 0.1051
23 -3.689 0.390 -0.2798 1.0320 0.0783
24 -3.689 0.407 -0.2358 0.8700 0.0556
25 -3.689 0.424 -0.1924 0.7096 0.0370
26 -3.689 0.441 -0.1493 0.5506 0.0223
27 -3.689 0.458 -0.1064 0.3925 0.0113
28 -3.689 0.475 -0.0638 0.2352 0.0041
29 -3.689 0.492 -0.0212 0.0784 0.0005
30 -3.689 0.508 0.0212 -0.0784 0.0005
31 -3.689 0.525 0.0638 -0.2352 0.0041
32 -3.689 0.542 0.1064 -0.3925 0.0113
33 -3.689 0.559 0.1493 -0.5506 0.0223
34 -3.689 0.576 0.1924 -0.7096 0.0370
35 -3.420 0.593 0.2358 -0.8067 0.0556
36 -3.393 0.610 0.2798 -0.9493 0.0783
37 -3.352 0.627 0.3242 -1.0870 0.1051
38 -3.302 0.644 0.3694 -1.2197 0.1364
39 -2.937 0.661 0.4152 -1.2198 0.1724
40 -2.882 0.678 0.4620 -1.3317 0.2135
41 -2.830 0.695 0.5098 -1.4429 0.2599
42 -2.723 0.712 0.5588 -1.5215 0.3123
43 -2.557 0.729 0.6092 -1.5581 0.3712
44 -2.473 0.746 0.6612 -1.6354 0.4372
45 -2.453 0.763 0.7151 -1.7543 0.5113
46 -2.303 0.780 0.7710 -1.7754 0.5945
47 -2.216 0.797 0.8296 -1.8387 0.6882
48 -2.154 0.814 0.8911 -1.9196 0.7940
49 -2.040 0.831 0.9562 -1.9508 0.9143
50 -1.966 0.847 1.0256 -2.0164 1.0518
51 -1.607 0.864 1.1003 -1.7687 1.2107
52 -1.546 0.881 1.1818 -1.8276 1.3966
53 -1.514 0.898 1.2720 -1.9259 1.6179
54 -1.501 0.915 1.3738 -2.0616 1.8874
55 -1.378 0.932 1.4924 -2.0570 2.2273
56 -0.753 0.949 1.6367 -1.2323 2.6788
57 -0.386 0.966 1.8264 -0.7044 3.3356
58 -0.364 0.983 2.1213 -0.7718 4.4998
sum 61.3569 51.2506
S.D.=1.180
W'=0.925 Þ less than0.945,lognormalassumptionrejected
usenonparametric limit
Shapiro-FranciaTest-LognormalAssumption
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