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HomeMy WebLinkAbout1302_CabarrusCountyUnits2&3_GWMR_DIN28215_20161101C a b a r r u s C o u n t y S a n i t a r y L a n d f i l l - U n i t s 2 a n d 3 S e m i - A n n u a l S a m p l i n g R e p o r t F a c i l i t y P e r m i t s # 1 3 0 2 - M S W L F - a n d 1 3 0 2 - C D L F - 1 9 9 8 ( N o v e m b e r 2 0 1 6 S a m p l i n g E v e n t ) P r e p a r e d F e b r u a r y 2 0 1 7 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919 325-3500 fax: 919 781-5730 February 9, 2017 Ms. Jaclynne Drummond North Carolina Department of Environmental Quality Division of Waste Management Solid Waste Section 2090 U.S. 70 Highway Swannanoa, North Carolina 28778 Subject: November 2016 Semi-Annual Sampling Report Cabarrus County Landfill Units 2 and 3 Facility Permit No. 1302-MSWLF- and 1302-CDLF-1998 Dear Ms. Drummond: CDM Smith Inc. (CDM Smith), on behalf of Cabarrus County, is submitting an electronic copy of the November 2016 semi-annual sampling event report. This letter report presents the results of the recently completed sampling at Units 2 and 3 of the Cabarrus County Landfill and constitutes the second semi-annual sampling event for 2016. The approved groundwater monitoring network consists of the following wells: MW-1, -3, -3 deep, -A, -B, -C, -C Rep, -D, -E Rep, -E deep, -F, -G, -H, -H deep, -I, -J, -K, -L, -L deep, -M, -X, CD-6, assessment wells AMW-1s, -1d, -2s, and -2d, and background wells CD-1s and CD-1d. CD-4 Rep was installed in January 2009 as part of the proposed Phase I C&D Landfill expansion. Surface water sample locations include SW-1 and -2, which also monitor the Unit 1 Landfill. Assessment wells CD-4, -5, and -6 were added to the groundwater monitoring network in September 2006 during the Phase I C&D Landfill expansion. Assessment wells CD-4 and -5 were abandoned in July 2010 in preparation of the Phase II C&D Landfill expansion. Assessment wells AMW-1s, -1d, -2s, and -2d were added to the groundwater monitoring network in October 2009 as part of the Corrective Action Plan (CAP) implementation. Field activities, sampling results, and an evaluation of corrective action activities are discussed below. Field Activities Groundwater samples from Units 2 & 3 of the Cabarrus County Landfill were collected on November 1-3, 2016. Groundwater samples were collected from the monitoring wells by use of disposable, laboratory decontaminated Teflon™ bailers or a QED bladder pump system using low-flow sampling techniques. Monitoring well and surface water locations for Units 2 & 3 are provided on Figure 1. Construction details for each monitoring well are summarized in Table 1. Groundwater elevations were measured at each well prior to sampling and are presented in Table 2. These groundwater elevations were used to construct potentiometric contours for this sampling event Ms. Jaclynne Drummond February 9, 2017 Page 2 and are presented on Figure 1. The groundwater elevations and potentiometric contours were used to estimate groundwater velocities at each well, which are presented in Table 3. After depth to groundwater was measured, three well volumes of water were removed from each well prior to sampling to provide fresh formation water within the well water column. Low-flow sampling techniques were used to purge and sample wells used to monitor natural attenuation. Each well volume was measured in the field for pH, conductivity, turbidity, temperature, dissolved oxygen (DO), and oxidation- reduction potential (ORP) using a YSI-556 multi-parameter water quality meter and Oakton T100 and Lamonte 2020 turbidity meters. Wells with elevated turbidity were allowed to settle prior to sampling. The water quality parameters at the time of sampling are presented in Table 4. The headspace of each monitoring well was screened for methane gas using a RKI Eagle multi-gas monitor. Screening results are provided in Appendix A. Sampling Results Pace Analytical Services, Inc., located in Peachtree Corners, Georgia, analyzed the groundwater samples for North Carolina Appendix I volatile organic compounds (VOCs) and metals. Samples for the North Carolina Appendix II constituent, bis (2-ethylhexyl) phthalate, are collected annually during the spring sampling event. Additional groundwater samples were collected to evaluate the effectiveness of natural attenuation and the Phase II injection event and are discussed in the Corrective Action Evaluation section of this letter report. In accordance with the North Carolina Department of Environmental Quality’s Solid Waste Section (SWS) guidelines the analytical results were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or below SWS Limits (SWSLs). All monitoring wells for Units 2 and 3 with detections of analytes above the MDL but below the SWSL were qualified as estimated or “J” flags. The following list indicates the analytes detected above the laboratory specific MDL at each sampling location. No “J” flag or general chemistry detections are provided. Underlined analytes exceeded the 15A NCAC 02L .020 (NC 2L) Groundwater Quality Standard, Groundwater Protection Standard, or the 15A NCAC 02B (NC 2B) Surface Water Quality Standard for Class C Waters. CD-1s (Background) Metals: Iron, Manganese Volatile Organic Compounds: None Detected CD-1d (Background) Metals: Iron Volatile Organic Compounds: None Detected Ms. Jaclynne Drummond February 9, 2017 Page 3 CD-4 Rep Metals: None Detected Volatile Organic Compounds: None Detected CD-6 Metals: Cobalt, Zinc Volatile Organic Compounds: None Detected AMW-1s Metals: None Detected Volatile Organic Compounds: 1,1-Dichloroethane, cis-1,2-Dichloroethene, Tetrachloroethene (PCE), Trichloroethene (TCE) AMW-1d Metals: Barium Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis-1,2-Dichloroethene, Vinyl Chloride AMW-2s Metals: None Detected Volatile Organic Compounds: 1,1-Dichloroethane, cis-1,2-Dichloroethene, PCE, TCE AMW-2d Metals: None Detected Volatile Organic Compounds: 1,1-Dichloroethane, cis-1,2-Dichloroethene, PCE, TCE MW-1 Metals: Barium, Cobalt Volatile Organic Compounds: None Detected MW-3 Metals: None Detected Volatile Organic Compounds: 1,1-Dichloroethane, PCE, TCE, Trichlorofluoromethane MW-3 deep Metals: Not Sampled Volatile Organic Compounds: Not Sampled Ms. Jaclynne Drummond February 9, 2017 Page 4 MW-A Metals: None Detected Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,2-Dichloropropane, cis-1,2-Dichloroethene, Methylene Chloride, PCE, TCE MW-B Metals: Barium, Cobalt Volatile Organic Compounds: None Detected MW-C Metals: Cobalt Volatile Organic Compounds: None Detected MW-D Metals: Barium Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene, cis-1,2-Dichloroethene, TCE, Vinyl Chloride MW-E Rep Metals: Barium Volatile Organic Compounds: Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, 1,2-Dichloroethane, cis-1,2-Dichloroethene, Vinyl Chloride MW-E deep Metals: Barium, Cobalt, Lead, Zinc Volatile Organic Compounds: Chloroethane, 1,4-Dichlorobenzene MW-F Metals: Barium Volatile Organic Compounds: None Detected MW-G Metals: Barium Volatile Organic Compounds: Chlorobenzene, 1,4-Dichlorobenzene MW-H Metals: Zinc Volatile Organic Compounds: None Detected Ms. Jaclynne Drummond February 9, 2017 Page 5 MW-H deep Metals: None Detected Volatile Organic Compounds: None Detected MW-I Metals: None Detected Volatile Organic Compounds: PCE, TCE MW-J Metals: Zinc Volatile Organic Compounds: None Detected MW-K Metals: None Detected Volatile Organic Compounds: None Detected MW-L Metals: None Detected Volatile Organic Compounds: None Detected MW-L deep Metals: Not Sampled Volatile Organic Compounds: Not Sampled MW-M Metals: None Detected Volatile Organic Compounds: None Detected MW-X Metals: None Detected Volatile Organic Compounds: None Detected SW-1 Metals: Dry Volatile Organic Compounds: Dry SW-2 Metals: Dry Volatile Organic Compounds: Dry Ms. Jaclynne Drummond February 9, 2017 Page 6 “J” flags were not included in the previous list, but several locations had “J” flag detections that exceeded the standards. These constituents along with their location are listed below. Cobalt: CD-1s, -4 Rep, AMW-1d, MW-A, -D, -E Rep, -F, -G, -H, and -J Vanadium: CD-1d, -4 Rep, -6, MW-H, -J, and -M 1,2-Dichloroethane: MW-E Deep Vinyl Chloride: MW-A The duplicate sample, identified as Duplicate, was collected from MW-K and had similar concentrations of all compounds detected in the primary sample with the exceptions of beryllium and copper. Beryllium and copper were detected in the primary sample as estimated concentrations, but not detected in the duplicate sample. No analytes were detected in the trip blank. Barium, copper, lead, and methylene chloride were detected below the NC 2L Standard in the equipment blank. Metals detected above the standards are likely natural occurring based on concentrations in the background monitoring wells or are from elevated turbidity at the time of sample collection. A summary of detected constituents from the May 2011 to the November 2016 sampling events is presented in Table 5. Laboratory analytical reports are provided in Appendix A. Corrective Action Evaluation In December 2008, CDM Smith, on behalf of the County, submitted an Assessment of Corrective Measures Report to the SWS for the closed landfill Units 2 and 3 in accordance with North Carolina Solid Waste Management Rule 15 NCAC 13B .1635. Monitored natural attenuation and institutional controls paired with in situ remediation by enhanced bioremediation was selected as the remedy to address groundwater contamination by select VOCs at the facility. In situ remediation efforts were to be focused on the bedrock contamination near monitoring wells MW-E Rep and -E deep. Groundwater contamination in the area of MW-E deep is caused by migration of leachate from the closed landfill Units 2 and 3 downward into the shallow fractured bedrock, thereby allowing low-level VOCs to migrate into this area prior to being attenuated below NC 2L Standards. Following approval of the CAP in September 2009 and the Phase I injection permit, six injection wells were installed upgradient of the MW-E cluster in October 2009 as shown on Figure 2. A 3% solution of potable water and EOS® 450, which is an emulsion of soybean oil and water, was injected simultaneously into the injection wells from November 2-6, 2009. A total of 38,100 gallons of the solution were injected with each well receiving approximately 6,350 gallons. The initial injection of EOS® 450 successfully degraded PCE and TCE to daughter products in the injection area and neither compound has been detected above the NC 2L Standards in MW-E deep since the Phase I injection in November 2009. It was assumed that the EOS® 450 would be viable for a period of 3 to 5 years. However, samples collected from the MW-E cluster and wells downgradient of the injection Ms. Jaclynne Drummond February 9, 2017 Page 7 area during the November 2013 sampling event showed that groundwater contaminant concentrations had increased and levels exceeding the applicable NC 2L Standards had been detected in monitoring wells near the property line. Due to the increasing downgradient contaminant concentrations and NC 2L exceedances near the property line the groundwater conditions were re-evaluated in accordance with the CAP and a Phase II injection was implemented. In order to assess the biological conditions in the injection area prior to initiating the Phase II injection, groundwater samples were collected from MW-E Rep, -E deep, AMW-1s, -1d, -2s, and -2d in January 2014 and analyzed for Dehalococcoides spp (DHC), the bacteria responsible for degrading the chlorinated ethene species of VOCs. The specific genes of the bacteria that promote dechlorination were also analyzed. Analytical results for the DHC analyses are summarized in Table 7 and show that a sufficient population exists at monitoring wells MW-E, -E deep, and assessment monitoring well AMW-2s for reductive dechlorination by enhanced anaerobic bioremediation. DHC was detected at low concentrations in assessment monitoring wells AMW-1d and -2d and was not detected at AMW-1s. The absence of DHC at AMW-1s is likely associated with relatively low VOC concentrations. Following approval of the injection permit in January 2014, the Phase II injection was completed from February 10-18, 2014, using potable water and a 10% solution of 60% SRS®-FR large droplet emulsified vegetable oil substrate. SRS®-FR is specifically designed for use in fractured bedrock environments and is a mixture of 60% emulsified vegetable oil, 20% water, 5-15% of proprietary emulsifiers and nutrients, and 5% sodium lactate. The nutrient component of SRS®-FR further enhances the microbial population growth. A total of 9,966 gallons of the solution were injected during the Phase II event with each well receiving approximately 1,661 gallons. In order to monitor the progress of the Phase II injection and the geochemical and biological response of the aquifer, groundwater samples were collected quarterly from monitoring wells MW-E Rep and -E deep and assessment wells AMW-1s, -1d, -2s, and -2d. The first and third quarterly sampling events were completed in conjunction with the May and November 2014 semi-annual sampling events respectively. The second quarterly sampling event was completed in August 2014 and the fourth quarterly sampling event was completed in March 2015. A 15 month post-injection sampling event was completed in May 2015. Water quality measurements of pH, temperature, ORP, DO, conductivity, turbidity, and ferrous iron were collected during each sampling event. In addition, the quarterly samples were submitted to an analytical laboratory for analysis of nitrate, sulfate, alkalinity, chloride, chemical oxygen demand (COD), VOCs, dissolved gases (i.e. methane, ethane, ethene, carbon dioxide), and metabolic acids (i.e. acetic acid, butyric acid, lactic acid, propionic acid, and pyruvic acid). North Carolina Appendix I metals were collected during events that corresponded with the semi-annual sampling program. Ms. Jaclynne Drummond February 9, 2017 Page 8 Additional samples were collected during the fourth quarterly sampling event (March 2015) from monitoring wells MW-E Rep and -E deep and assessment wells AMW-1s, -1d, -2s, and -2d and analyzed for DHC to assess the biological conditions in the injection area after initiating the Phase II injection. A sufficient population of DHC existed at assessment monitoring well AMW-1d for reductive dechlorination by enhanced anaerobic bioremediation and DHC was detected at low concentrations in monitoring well MW-E deep. Detections of DHC in AMW-1d indicated a healthy population of DHC in the primary bedrock treatment zone surrounding the injection wells. DHC detections in MW-E deep was an indication that active treatment in bedrock was also occurring downgradient. DHC was not detected at MW-E Rep, AMW-1s, -2s, or -2d and was likely due to reduced VOC concentrations from upgradient treatment. Analytical results for the DHC analyses are summarized in Table 7. On September 28, 2015, a report summarizing the results of the Phase II injection was submitted to the SWS. The report stated that the Phase II injection of emulsified vegetable oil replenished the carbon source and complete reductive dechlorination is occurring at MW-E, -E Deep, and AMW-1d. The presence of DHC populations and functional genes in MW-E Deep and AMW-1d demonstrate that the treatment process is capable of achieving complete chlorinated VOC degradation as long as a sufficient carbon donor is present. As part of the semi-annual monitoring program, additional groundwater samples were collected from the background well CD-1s; monitoring wells MW-A, -E Rep, -E deep, -L, and -3; and assessment wells AMW-1s, -1d, -2s, and -2d. Samples were analyzed for alkalinity, biochemical oxygen demand, COD, carbon dioxide, chloride, dissolved hydrogen, ethane, ethene, volatile fatty acids (i.e. acetic, butyric, hexanoic, lactic, pentanoic, propionic, and pyruvic), ferrous iron, methane, nitrate, sulfate, sulfide, and total organic carbon. Note that ferrous iron was analyzed in the field using a Hach test kit due to the short hold time of 15 minutes. These additional samples were collected to evaluate natural attenuation and the effectiveness of the Phase II injection as part of the CAP. A complete summary of the geochemical results is provided in Table 5. Contaminant concentration trends for MW-A, -3, -E Rep, -E deep, AMW-1s, -1d, -2s, and -2d were evaluated to determine the effectiveness of natural attenuation and the Phase II injection. Figures 3 through 10 present total VOC contaminant concentration data for each well. An isoconcentration contour map with data from the November 2016 sampling event is provided on Figure 11. The total VOC trend analysis for MW-A is presented on Figure 3. Total VOC concentrations increased in MW-A between June 1995 and April 2003. A decreasing trend began after the April 2003 sampling event but total VOC concentrations show an increasing trend between the May 2011 and November 2016 events. Although total VOC concentrations in MW-A show an increasing trend, concentrations of 1,1-dichloroethane, PCE, and TCE show a decreasing trend. Ms. Jaclynne Drummond February 9, 2017 Page 9 Figure 4 presents the total VOC trend analysis for MW-3. Total VOC concentrations show an increasing trend between the October 2006 and the November 2016 sampling events. 1,1-Dichloroethane, PCE, and TCE are the only compounds that have been detected in MW-3 above the NC 2L Standards. The geochemical data indicates aerobic conditions at MW-3. VOC concentrations in MW-3 deep have never been detected above the standards. The total VOC trend analyses for MW-E Rep and -E deep are presented on Figures 5 and 6, respectively. Total VOC concentrations in MW-E Rep and -E deep have decreased since the November 2009 Phase I injection and are expected to continue to decrease. PCE and TCE have not been detected above the NC 2L Standards in MW-E deep since the Phase I injection and have not been detected above the MDL since the August 2010 sampling event. Delivery of the carbon substrate (i.e. SRS®-FR) during the Phase II injection was effective based on the increase in COD at MW-E deep. Reducing conditions exist at the MW-E cluster based on low DO, a negative ORP, and high methane concentrations. The increase in metabolic acids and ferrous iron at MW-E deep also indicates that a reducing subsurface environment exists. A geochemically reducing environment is favorable for anaerobic reductive dechlorination. Figures 7 and 8 present the total VOC trend analyses for assessment wells AMW-1s and -1d, respectively. Total VOC concentrations in AMW-1s show an increasing trend from November 2010 to May 2013 but show a decreasing trend from the May 2013 to the May 2016 sampling event. Total VOC concentrations increased during the November 2016 sampling event. Total VOC concentrations in AMW- 1d show an increasing trend between May 2010 and November 2014. Total VOC concentrations show a decreasing trend since the November 2014 sampling event. Reducing conditions exist at AMW-1d. The concentration of vinyl chloride has generally increased at AMW-1d since the Phase II injection while the concentration of TCE has decreased. The increased concentration of vinyl chloride indicates that anaerobic reductive dechlorination is occurring as vinyl chloride is a daughter product of TCE. The total VOC trend analyses for AMW-2s and -2d are presented on Figures 9 and 10, respectively. Total VOC concentrations at AMW-2s show an increasing trend between the initial sampling event in October 2009 and November 2014, but show a fluctuating trend since the November 2014 sampling event. Total VOC concentrations show an increasing trend at AMW-2d from the November 2010 sampling event to the November 2013 sampling event, but have fluctuated since the Phase II injection. The AMW-2 cluster is located farthest downgradient of the injection area and the shallow well is screened in partially weathered rock. Geochemical results indicate an aerobic subsurface environment, but contaminant concentrations are expected to decrease. Recommendations Units 2&3 of the Cabarrus County Landfill are unlined and are the source of VOC concentrations that are above the NC 2L Standards in downgradient monitoring wells. The injection remedy successfully reduced the contaminant concentrations in bedrock monitoring well MW-E deep and developed a primary VOC Ms. Jaclynne Drummond February 9, 2017 Page 10 treatment zone in the vicinity of the injection wells and MW-E Rep. Downgradient VOC concentrations in bedrock and saprolite should continue to decrease due to reduced VOC concentrations in the primary treatment zone. Additional injections will be necessary in the future once all electron donors have been consumed and complete dechlorination stalls. The County will continue with the semi-annual assessment monitoring program. In addition to sampling for Appendix I VOCs and metals, and the Appendix II constituent, bis(2-ethylhexyl) phthalate (sampled at CD-1s, -1d, MW-C, -E deep, -H, -I, and AMW-2d during the spring sampling event), samples collected from CD-1s, MW-A, -E Rep, -E deep, -L, -3, AMW-1s, -1d, -2s, and -2d will continue to be analyzed for natural attenuation parameters during the semi-annual sampling events. Future analytical results will be monitored to see if another injection will be needed. The next sampling event will be completed in the spring of 2017. In accordance with recent changes to the SWS reporting requirements, a 14-Day Notification will be submitted with the Spring 2017 sampling report, if constituents exceed their respective limits. CDM Smith will prepare an Alternate Source Demonstration (ASD) for inorganics in groundwater at the Unit 2&3 landfill prior to the next sampling event. If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3569 or by email at colonemf@cdmsmith.com. Very truly yours, Mathew F. Colone, P.G. CDM Smith Inc. cc: Kevin Grant, Cabarrus County Table 1 Monitoring Well Construction Summary Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 6-inch Casing Screen Interval Filter Interval Seal Interval 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well)8/7/2006 35.47788 80.52334 Saprolite 29.53 --18.0-28.0 16.0-28.0 14.0-16.0 2.0 1302-MSWLF- & 1302-CDLF-1998 CD-1d (background well)7/21/2004 35.47788 80.52340 PWR 52.15 --40.0-50.0 38.0-50.0 36.0-38.0 2.0 1302-MSWLF- & 1302-CDLF-1998 AMW-1 10/6/2009 35.46915 80.52225 PWR 67.57 --50.0-65.0 48.0-65.0 46.0-48.0 2.0 1302-MSWLF- & 1302-CDLF-1998 AMW-1d 10/8/2009 35.46914 80.52227 Bedrock 96.93 0-78.0 84.0-94.0 82.0-94.0 80.0-82.0 2.0 1302-MSWLF- & 1302-CDLF-1998 AMW-2 10/6/2009 35.46829 80.52232 PWR 39.90 --22.0-37.0 20.0-37.0 18.0-20.0 2.0 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 10/8/2009 35.46831 80.52233 Bedrock 63.55 0-51.0 55.0-60.0 53.0-60.0 51.0-53.0 2.0 1302-MSWLF- & 1302-CDLF-1998 CD-6 9/11/2006 35.47556 80.52420 PWR 41.49 --23.5-38.5 21.5-38.5 19.5-21.5 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-1 1990s 35.47355 80.52105 Saprolite/PWR 29.93 --18.0-28.0 16.0-28.0 14.0-16.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-3 2/17/1992 35.46794 80.52120 Saprolite/PWR 35.10 --19.0-34.0 17.0-34.0 15.0-17.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep 6/3/2003 35.46785 80.52133 Bedrock 93.76 0-44.0 75.0-90.0 71.0-75.0 68.0-71.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-9 1990s 35.47706 80.51740 Saprolite/PWR 51.15 --39.0-49.0 37.0-49.0 35.0-37.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-A 9/16/1994 35.47289 80.52524 Saprolite/PWR 50.42 --33.0-48.0 31.0-49.9 29.0-31.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-B 9/16/1994 35.47165 80.52081 Saprolite/PWR 15.22 --2.5-12.5 2.0-13.0 1.0-2.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-C 9/16/1994 35.47042 80.52556 Saprolite/PWR 18.50 --2.5-15.0 2.0-15.0 1.0-2.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-D 9/16/1994 35.47021 80.52394 Saprolite/PWR 30.15 --18.0-28.0 16.0-28.0 14.0-16.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 4/9/1996 35.46983 80.52212 PWR/Bedrock 45.65 --28.0-43.0 25.0-45.0 23.0-25.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-E deep 9/2/1999 35.46974 80.52220 Bedrock 59.57 --41.0-56.0 39.0-56.0 37.0-39.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-F 9/15/1994 35.47050 80.52040 Saprolite/PWR 20.08 --3.0-18.0 1.5-18.0 0.5-1.5 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-G 9/15/1994 35.47290 80.52121 Saprolite/PWR 20.25 --3.0-18.0 1.5-18.0 0.5-1.5 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-H 9/3/1999 35.46861 80.52310 Saprolite/PWR 32.70 --19.5-29.5 17.5-29.5 15.5-17.5 2.0 Facility Permit Numbers Total Depth (feet BTOC) Monitoring Well Diameter (inches) Monitoring Well Code Geology of Screened Interval Installation Date Latitude Longitude Depth (feet bgs) Page 1 of 2 January 2017 Table 1 Monitoring Well Construction Summary Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 6-inch Casing Screen Interval Filter Interval Seal Interval Facility Permit Numbers Total Depth (feet BTOC) Monitoring Well Diameter (inches) Monitoring Well Code Geology of Screened Interval Installation Date Latitude Longitude Depth (feet bgs) 1302-MSWLF- & 1302-CDLF-1998 MW-H deep 9/2/1999 35.46851 80.52317 Bedrock 59.67 --41.0-56.0 39.0-56.0 37.0-39.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-I 9/3/1999 35.46928 80.52076 Saprolite/PWR 65.18 --47.0-62.0 45.0-62.0 43.0-45.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-J 9/3/1999 35.47403 80.52647 Saprolite/PWR 34.90 --29.0-32.0 28.0-32.0 25.0-28.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-K 9/3/1999 35.46978 80.52467 Saprolite/PWR 36.08 --18.0-33.0 16.0-33.0 14.0-16.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-L 9/2/1999 35.46771 80.52168 Saprolite/PWR 26.90 --14.0-24.0 12.0-24.0 10.0-12.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-L deep 6/3/2003 35.46778 80.52168 Bedrock 65.20 0-48.0 53.0-63.0 50.0-63.0 47.0-50.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-M 6/2/2003 35.46743 80.52026 PWR 39.80 --21.0-36.0 18.0-36.0 16.0-18.0 2.0 1302-MSWLF- & 1302-CDLF-1998 MW-X 12/1/1993 35.47225 80.52664 Saprolite/PWR 31.79 --20.0-30.0 18.0-30.0 16.0-18.0 2.0 Notes: 1. BTOC - Below Top of Casing 2. bgs - Below Ground Surface 3. PWR - Partially Weathered Rock Page 2 of 2 January 2017 Table 2 Groundwater Elevations November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 MW-1 701.37 689.08 689.35 689.82 688.87 690.81 689.03 689.32 690.73 689.22 688.97 688.94 688.76 1302-MSWLF- & 1302-CDLF-1998 MW-3 670.37 652.20 651.67 654.06 652.48 654.70 654.34 656.75 652.60 655.97 654.26 657.31 655.78 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep 668.33 655.15 NS 656.74 NS 657.43 NS 659.63 NS 658.99 657.48 660.27 659.10 1302-MSWLF- & 1302-CDLF-1998 MW-9 780.25 736.07 734.92 735.84 NS NS NS NS NS NS NS NS NS 1302-MSWLF- & 1302-CDLF-1998 MW-A 746.80 703.02 702.39 703.59 703.09 702.45 703.45 705.01 702.49 703.28 702.60 704.73 704.39 1302-MSWLF- & 1302-CDLF-1998 MW-B 681.66 679.04 679.56 678.34 677.44 679.71 678.96 678.96 675.25 679.06 678.86 678.89 678.77 1302-MSWLF- & 1302-CDLF-1998 MW-C 694.98 686.66 683.43 684.58 682.88 690.12 683.78 688.55 682.14 688.33 682.70 688.74 683.29 1302-MSWLF- & 1302-CDLF-1998 MW-D 720.28 692.88 691.48 693.12 691.60 692.15 692.58 696.21 692.98 692.78 691.53 694.50 693.39 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 712.58 679.94 679.07 682.38 NS 680.25 682.53 685.83 682.49 683.00 680.93 684.97 683.18 1302-MSWLF- & 1302-CDLF-1998 MW-E deep 705.70 669.66 668.80 671.10 669.31 670.05 672.21 675.55 672.75 672.71 670.65 674.67 672.88 1302-MSWLF- & 1302-CDLF-1998 MW-F 681.06 672.27 672.60 671.61 667.86 673.91 671.41 672.51 668.38 672.66 671.66 672.46 670.61 1302-MSWLF- & 1302-CDLF-1998 MW-G 695.19 685.79 686.40 685.46 685.72 686.74 685.69 685.78 685.11 685.68 685.68 685.62 685.65 1302-MSWLF- & 1302-CDLF-1998 MW-H 699.23 670.19 669.25 671.30 669.74 670.32 672.62 675.66 672.74 672.67 671.03 674.90 673.29 1302-MSWLF- & 1302-CDLF-1998 MW-H deep 699.17 669.30 668.54 670.81 669.32 669.72 672.17 675.17 672.33 672.32 670.62 674.52 672.96 1302-MSWLF- & 1302-CDLF-1998 MW-I 709.30 661.43 660.65 662.40 660.82 662.70 662.90 665.83 662.00 664.00 662.17 665.50 663.72 1302-MSWLF- & 1302-CDLF-1998 MW-J 728.47 698.68 697.11 698.49 696.45 698.77 698.02 700.14 696.55 699.10 696.77 699.52 698.05 1302-MSWLF- & 1302-CDLF-1998 MW-K 702.91 679.22 676.91 679.73 676.51 679.51 679.09 682.24 677.86 680.25 676.84 681.21 678.35 1302-MSWLF- & 1302-CDLF-1998 MW-L 669.54 653.13 651.96 654.24 652.71 655.24 654.74 657.83 654.03 656.54 654.39 657.90 655.72 10/31/2016 Groundwater Elevation (AMSL) 10/26/2015Sampling Event 5/5/20145/3/2011 5/7/2012 11/26/201211/7/2011 Facility Permit Numbers Monitoring Well Code Top of Casing Elevation (AMSL) 5/16/20165/4/201511/3/201411/4/20135/6/2013 Page 1 of 2 January 2017 Table 2 Groundwater Elevations November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 10/31/2016 Groundwater Elevation (AMSL) 10/26/2015Sampling Event 5/5/20145/3/2011 5/7/2012 11/26/201211/7/2011 Facility Permit Numbers Monitoring Well Code Top of Casing Elevation (AMSL) 5/16/20165/4/201511/3/201411/4/20135/6/2013 1302-MSWLF- & 1302-CDLF-1998 MW-L deep 672.51 654.62 NS 655.81 NS 656.74 NS 659.35 NS 658.15 656.14 659.50 657.51 1302-MSWLF- & 1302-CDLF-1998 MW-M 668.49 647.85 NS 648.19 NS 649.98 NS 650.69 NS 649.52 648.01 649.94 648.79 1302-MSWLF- & 1302-CDLF-1998 MW-X 710.28 697.62 700.80 697.38 695.25 699.28 696.54 698.95 695.53 698.02 696.14 698.64 696.83 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well)755.00 730.81 729.60 730.65 728.94 729.28 730.20 731.82 730.20 730.42 728.55 731.10 729.77 1302-MSWLF- & 1302-CDLF-1998 CD-1d (background well)757.40 730.49 729.46 730.96 728.75 729.09 730.00 731.54 729.95 730.20 728.33 730.89 729.57 1302-MSWLF- & 1302-CDLF-1998 CD-4 755.50 ------------------------ 1302-MSWLF- & 1302-CDLF-1998 CD-4 Rep 739.15 729.45 728.68 730.45 728.90 1302-MSWLF- & 1302-CDLF-1998 CD-5 758.70 ------------------------ 1302-MSWLF- & 1302-CDLF-1998 CD-6 741.40 707.71 706.81 707.55 706.10 706.02 704.04 710.20 709.30 707.64 706.65 708.75 708.44 1302-MSWLF- & 1302-CDLF-1998 AMW-1s 725.30 670.87 670.00 672.32 670.00 671.30 673.57 676.79 674.05 674.06 672.00 676.07 674.31 1302-MSWLF- & 1302-CDLF-1998 AMW-1d 725.80 670.58 669.77 672.03 670.34 671.05 673.31 676.62 673.02 673.85 671.73 675.85 674.09 1302-MSWLF- & 1302-CDLF-1998 AMW-2s 694.50 668.16 667.10 669.38 667.78 671.47 670.43 673.40 670.29 671.07 669.09 672.97 671.18 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 694.50 668.49 667.68 669.90 668.32 669.12 671.05 673.95 670.70 671.60 669.65 673.53 671.82 Notes: 1. AMSL - Above Mean Sea Level 2. Blank Cells - Water level not measured or well not installed 3. MW-E deep, -H, -H deep, -I, -J, -K, -L, were installed in June 1999. 4. Asessment wells CD-4, -5, and -6 were installed in September 2006. 5. Assessment wells AMW-1s, -1d, -2s, and -2d were installed in October 2009. 6. CD-4 and CD-5 were abandoned in July 2010. 7. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 8. MW-9 was removed from the monitoring program in November 2012. 9. MW-E Rep was not sampled during the Novemver 2012 sampling event due to laboratory oversight. Page 2 of 2 January 2017 Table 3 Summary of Groundwater Velocities November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 MW-A 0.0157 6.12E+00 0.0162 6.31E+00 0.0164 6.40E+00 0.0181 7.06E+00 1302-MSWLF- & 1302-CDLF-1998 MW-B 0.0171 1.27E+00 0.0163 1.20E+00 0.0180 1.33E+00 0.0183 1.35E+00 1302-MSWLF- & 1302-CDLF-1998 MW-C 0.0182 3.98E+00 0.0211 4.61E+00 0.0211 4.62E+00 0.0225 4.91E+00 1302-MSWLF- & 1302-CDLF-1998 MW-D 0.0097 3.42E+00 0.0104 3.68E+00 0.0100 3.53E+00 0.0109 3.88E+00 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 0.0154 5.36E+01 0.0155 5.42E+01 0.0141 4.93E+01 1302-MSWLF- & 1302-CDLF-1998 MW-F 0.0181 1.65E+00 0.0175 1.60E+00 0.0188 1.72E+00 0.0207 1.89E+00 1302-MSWLF- & 1302-CDLF-1998 MW-G 0.0265 2.92E+00 0.0255 2.82E+00 0.0265 2.93E+00 0.0227 2.51E+00 1302-MSWLF- & 1302-CDLF-1998 MW-1 0.0276 6.05E+00 0.0268 5.87E+00 0.0271 5.92E+00 0.0236 5.16E+00 1302-MSWLF- & 1302-CDLF-1998 MW-9 0.0185 4.05E+00 0.0187 4.08E+00 0.0190 4.16E+00 1302-MSWLF- & 1302-CDLF-1998 CD-1s 0.0196 2.35E-02 (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-4 1302-MSWLF- & 1302-CDLF-1998 CD-5 Notes: 1. CD-4 and CD-5 were installed in September 2006. 2. CD-4 and CD-5 were abandoned in July 2010. 3. Blanks indicate no data. 4. Hydraulic conductivity and effective porosity values are estimated from previously performed slug tests and grain size analyses. 5. The gradient and linear velocity values shown for MW-9 and CD-1s are based on the average of all the listed wells. 6. The gradient and linear velocity values shown for MW-A are based on the average of MW-B, -C, -D, -E, and -F. 7. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 8. MW-9 was removed from the monitoring program in November 2012. 9. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. 5/7/2012 11/26/2012 Gradient Gradient Average Linear Velocity feet/day Average Linear Velocity feet/day Facility Permit Numbers Monitoring Well Code Gradient Gradient Average Linear Velocity feet/day Average Linear Velocity feet/day 5/3/2011 11/7/2011 Page 1 of 3 January 2017 Table 3 Summary of Groundwater Velocities November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 MW-A 1302-MSWLF- & 1302-CDLF-1998 MW-B 1302-MSWLF- & 1302-CDLF-1998 MW-C 1302-MSWLF- & 1302-CDLF-1998 MW-D 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 1302-MSWLF- & 1302-CDLF-1998 MW-F 1302-MSWLF- & 1302-CDLF-1998 MW-G 1302-MSWLF- & 1302-CDLF-1998 MW-1 1302-MSWLF- & 1302-CDLF-1998 MW-9 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-4 1302-MSWLF- & 1302-CDLF-1998 CD-5 Facility Permit Numbers Monitoring Well Code 0.0143 5.56E+00 0.0165 6.43E+00 0.0154 6.02E+00 0.0169 6.59E+00 0.0162 1.20E+00 0.0175 1.29E+00 0.0186 1.37E+00 0.0195 1.44E+00 0.0137 3.00E+00 0.0219 4.78E+00 0.0183 4.00E+00 0.0226 4.95E+00 0.0098 3.47E+00 0.0104 3.67E+00 0.0084 2.97E+00 0.0091 3.21E+00 0.0148 5.16E+01 0.0139 4.86E+01 0.0128 4.46E+01 0.0133 4.65E+01 0.0168 1.53E+00 0.0188 1.72E+00 0.0191 1.74E+00 0.0201 1.83E+00 0.0224 2.47E+00 0.0234 2.59E+00 0.0242 2.68E+00 0.0237 2.62E+00 0.0226 4.95E+00 0.0242 5.30E+00 0.0250 5.47E+00 0.0232 5.08E+00 0.0163 1.96E-02 0.0183 2.20E-02 0.0177 2.13E-02 0.0185 2.23E-02 Notes: 1. CD-4 and CD-5 were installed in September 2006. 2. CD-4 and CD-5 were abandoned in July 2010. 3. Blanks indicate no data. 4. Hydraulic conductivity and effective porosity values are estimated from previously performed slug tests and grain size analyses. 5. The gradient and linear velocity values shown for MW-9 and CD-1s are based on the average of all the listed wells. 6. The gradient and linear velocity values shown for MW-A are based on the average of MW-B, -C, -D, -E, and -F. 7. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 8. MW-9 was removed from the monitoring program in November 2012. 9. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. 5/6/2013 11/4/2013 5/5/2014 11/3/2014 GradientGradientGradientGradient Average Linear Velocity feet/day Average Linear Velocity feet/day Average Linear Velocity feet/day Average Linear Velocity feet/day Page 2 of 3 January 2017 Table 3 Summary of Groundwater Velocities November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 MW-A 1302-MSWLF- & 1302-CDLF-1998 MW-B 1302-MSWLF- & 1302-CDLF-1998 MW-C 1302-MSWLF- & 1302-CDLF-1998 MW-D 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 1302-MSWLF- & 1302-CDLF-1998 MW-F 1302-MSWLF- & 1302-CDLF-1998 MW-G 1302-MSWLF- & 1302-CDLF-1998 MW-1 1302-MSWLF- & 1302-CDLF-1998 MW-9 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-4 1302-MSWLF- & 1302-CDLF-1998 CD-5 Facility Permit Numbers Monitoring Well Code 0.0151 5.88E+00 0.0165 6.42E+00 0.0156 6.09E+00 0.0172 6.73E+00 0.0173 1.28E+00 0.0170 1.25E+00 0.0185 1.36E+00 0.0183 1.35E+00 0.0166 3.63E+00 0.0221 4.84E+00 0.0178 3.89E+00 0.0234 5.13E+00 0.0100 3.54E+00 0.0105 3.73E+00 0.0097 3.45E+00 0.0105 3.71E+00 0.0135 4.71E+01 0.0144 5.03E+01 0.0132 4.59E+01 0.0141 4.93E+01 0.0180 1.64E+00 0.0182 1.66E+00 0.0190 1.73E+00 0.0199 1.81E+00 0.0235 2.60E+00 0.0226 2.49E+00 0.0239 2.64E+00 0.0232 2.56E+00 0.0242 5.30E+00 0.0233 5.09E+00 0.0248 5.43E+00 0.0241 5.28E+00 0.0173 2.07E-02 0.0181 2.17E-02 0.0178 2.14E-02 0.0189 2.26E-02 Notes: 1. CD-4 and CD-5 were installed in September 2006. 2. CD-4 and CD-5 were abandoned in July 2010. 3. Blanks indicate no data. 4. Hydraulic conductivity and effective porosity values are estimated from previously performed slug tests and grain size analyses. 5. The gradient and linear velocity values shown for MW-9 and CD-1s are based on the average of all the listed wells. 6. The gradient and linear velocity values shown for MW-A are based on the average of MW-B, -C, -D, -E, and -F. 7. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 8. MW-9 was removed from the monitoring program in November 2012. 9. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. 5/16/2016 Gradient Average Linear Velocity feet/day Gradient Average Linear Velocity feet/day 10/26/2015 Gradient 5/4/2015 Average Linear Velocity feet/day 10/31/2016 Gradient Average Linear Velocity feet/day Page 3 of 3 January 2017 Table 4 Water Quality Parameters November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb. (S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs) 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well)5.58 158 16.0 5.96 191 87 5.65 120 17.5 3.83 182 59 5.86 111 16.3 1.51 181 10 1302-MSWLF- & 1302-CDLF-1998 CD-1d (background well)5.55 171 16.2 8.22 191 280 5.80 132 17.9 2.70 171 84 6.27 121 17.3 1.41 150 73 1302-MSWLF- & 1302-CDLF-1998 CD-4 (abandoned)------------------------------------ 1302-MSWLF- & 1302-CDLF-1998 CD-4 Rep 1302-MSWLF- & 1302-CDLF-1998 CD-5 (abandoned)------------------------------------ 1302-MSWLF- & 1302-CDLF-1998 CD-6 5.55 257 16.8 3.19 130 55 5.49 269 16.4 4.19 183 13 5.76 208 18.4 0.78 202 7 1302-MSWLF- & 1302-CDLF-1998 AMW-1s 5.23 225 21.9 1.22 176 10 6.36 237 17.8 0.17 12 7 5.67 292 27.4 0.02 121 9 1302-MSWLF- & 1302-CDLF-1998 AMW-1d 6.09 569 22.0 0.01 89 4 7.60 638 17.3 0.00 -112 3 6.00 651 24.1 0.24 95 8 1302-MSWLF- & 1302-CDLF-1998 AMW-2s 5.65 135 17.8 2.10 128 36 7.72 148 17.0 2.47 -30 10 5.74 171 18.6 0.42 195 29 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 6.24 241 19.1 0.75 107 3 6.96 167 13.9 1.07 -29 3 5.78 195 17.4 0.00 195 4 1302-MSWLF- & 1302-CDLF-1998 MW-1 6.03 1,870 16.6 2.96 -77 78 6.01 1,570 16.3 2.44 139 4 6.37 1,794 16.1 0.00 -22 2 1302-MSWLF- & 1302-CDLF-1998 MW-3 5.57 127 18.1 2.60 164 27 6.01 174 17.8 4.05 198 32 5.73 155 19.5 2.76 113 9 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep 7.09 469 18.3 3.98 81 242 NS NS NS NS NS NS 7.93 329 17.1 0.39 21 191 1302-MSWLF- & 1302-CDLF-1998 MW-9 6.08 90 18.9 3.45 139 4 5.91 107 18.9 4.70 212 0 6.05 106 19.1 1.82 127 3 1302-MSWLF- & 1302-CDLF-1998 MW-A 5.01 292 17.3 1.08 113 4 5.47 324 17.9 0.06 205 1 5.47 411 17.1 0.00 103 3 1302-MSWLF- & 1302-CDLF-1998 MW-B 6.45 1,350 14.2 3.70 -116 25 6.26 1,070 15.8 2.39 -78 5 6.70 1,097 14.8 0.00 -49 7 1302-MSWLF- & 1302-CDLF-1998 MW-C 5.37 152 13.8 5.23 136 54 5.79 394 16.9 4.01 130 12 5.89 200 18.3 0.83 -16 46 1302-MSWLF- & 1302-CDLF-1998 MW-D 5.36 610 16.7 3.14 87 135 5.26 501 16.5 1.99 79 4 5.36 460 16.9 0.00 79 4 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 5.73 586 17.7 0.01 34 9 5.69 659 19.0 0.00 -115 4 5.96 785 19.3 0.00 13 6 1302-MSWLF- & 1302-CDLF-1998 MW-E deep 6.40 738 15.9 0 -51 7 6.54 823 18.7 0.00 -67 3 6.50 842 21.1 2.51 -76 9 1302-MSWLF- & 1302-CDLF-1998 MW-F 6.35 1,120 14.3 2.43 -139 10 6.40 979 16.9 1.53 -95 4 6.30 826 16.2 0.00 -57 7 1302-MSWLF- & 1302-CDLF-1998 MW-G 6.11 1,110 16.5 5.79 -99 29 5.91 917 17.4 2.85 -61 2 6.21 861 14.1 0.00 -63 3 1302-MSWLF- & 1302-CDLF-1998 MW-H 5.29 230 14.5 9.03 197 212 5.82 176 14.9 6.13 193 7 5.20 145 15.0 3.90 74 13 1302-MSWLF- & 1302-CDLF-1998 MW-H deep 5.53 369 15.1 5.97 192 43 5.83 263 15.1 6.91 186 6 5.74 270 14.6 0.96 35 11 1302-MSWLF- & 1302-CDLF-1998 MW-I 5.46 99 16.2 3.44 164 10 5.67 113 15.8 4.67 114 3 5.92 109 17.9 2.58 147 3 1302-MSWLF- & 1302-CDLF-1998 MW-J 6.25 341 16.2 4.62 156 86 5.78 343 16.9 6.14 111 1 6.49 247 16.1 1.09 21 4 1302-MSWLF- & 1302-CDLF-1998 MW-K 5.47 269 15.6 4.74 153 38 5.09 311 16.4 4.32 47 8 5.75 200 15.8 1.90 143 8 1302-MSWLF- & 1302-CDLF-1998 MW-L 5.38 91 14.3 2.31 206 4 5.66 106 16.4 2.59 222 3 5.44 112 16.4 0.04 214 5 1302-MSWLF- & 1302-CDLF-1998 MW-L deep 6.65 368 18.7 3.49 103 18 NS NS NS NS NS NS 6.20 279 18.5 0.87 75 14 1302-MSWLF- & 1302-CDLF-1998 MW-M 5.53 301 14.4 6.58 194 26 NS NS NS NS NS NS 6.09 221 15.4 1.47 91 59 1302-MSWLF- & 1302-CDLF-1998 MW-X 5.93 338 15.3 4.29 174 51 6.01 260 16.6 6.51 33 20 5.13 241 14.9 0.91 69 4 1302-MSWLF- & 1302-CDLF-1998 SW-1 6.14 685 10.5 6.58 78 18 6.14 424 16.8 6.01 170 2 DRY DRY DRY DRY DRY DRY 1302-MSWLF- & 1302-CDLF-1998 SW-2 5.05 667.00 9.67 6.06 121 196 DRY DRY DRY DRY DRY DRY 6.36 455 22.3 2.49 114 13 Notes: 1. NS - Not Sampled 2. CD-4, CD-5, and CD-6 were installed in September 2006. 3. AMW-1s, -1d, -2s, and -2d were installed in October 2009. 4. CD-4 and CD-5 were abandoned in July 2010. 5. MW-3 deep, -L deep, -and -M are sampled annually during the spring event. 7. µs/cm- Microsiemens per centimeter 8. mg/L - milligrams per liter 9. ORP - Oxidation-Reduction Potential 10. Turb. - Turbidity; NTUs - Nephelometric Turbidity Units 11. mVs - millivolts 12. DO - Dissolved Oxygen 13. S.U. - Standard Units 14. Temp. - Temperature; Deg. C - Degrees Celsius 15. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 16. MW-9 was removed from the monitoring program in November 2012. 17. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. 5/3-5/2011 No. 32 Surface Water Sample Locations No. 34 5/7-9/2012 No. 33 Facility Permit Numbers Sampling Event: Sampling Date: Monitoring Well Code 11/7-9/2011 Page 1 of 4 January 2017 Table 4 Water Quality Parameters November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-1d (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-4 (abandoned) 1302-MSWLF- & 1302-CDLF-1998 CD-4 Rep 1302-MSWLF- & 1302-CDLF-1998 CD-5 (abandoned) 1302-MSWLF- & 1302-CDLF-1998 CD-6 1302-MSWLF- & 1302-CDLF-1998 AMW-1s 1302-MSWLF- & 1302-CDLF-1998 AMW-1d 1302-MSWLF- & 1302-CDLF-1998 AMW-2s 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 1302-MSWLF- & 1302-CDLF-1998 MW-1 1302-MSWLF- & 1302-CDLF-1998 MW-3 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep 1302-MSWLF- & 1302-CDLF-1998 MW-9 1302-MSWLF- & 1302-CDLF-1998 MW-A 1302-MSWLF- & 1302-CDLF-1998 MW-B 1302-MSWLF- & 1302-CDLF-1998 MW-C 1302-MSWLF- & 1302-CDLF-1998 MW-D 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 1302-MSWLF- & 1302-CDLF-1998 MW-E deep 1302-MSWLF- & 1302-CDLF-1998 MW-F 1302-MSWLF- & 1302-CDLF-1998 MW-G 1302-MSWLF- & 1302-CDLF-1998 MW-H 1302-MSWLF- & 1302-CDLF-1998 MW-H deep 1302-MSWLF- & 1302-CDLF-1998 MW-I 1302-MSWLF- & 1302-CDLF-1998 MW-J 1302-MSWLF- & 1302-CDLF-1998 MW-K 1302-MSWLF- & 1302-CDLF-1998 MW-L 1302-MSWLF- & 1302-CDLF-1998 MW-L deep 1302-MSWLF- & 1302-CDLF-1998 MW-M 1302-MSWLF- & 1302-CDLF-1998 MW-X 1302-MSWLF- & 1302-CDLF-1998 SW-1 1302-MSWLF- & 1302-CDLF-1998 SW-2 Surface Water Sample Locations Facility Permit Numbers Sampling Event: Sampling Date: Monitoring Well Code pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb. (S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs) 6.06 116 13.8 15.50 139 7 6.02 104 15.1 1.96 206 5 6.06 100 13.0 1.74 348 42 6.16 125 16.4 9.53 140 5 6.06 117 16.9 1.11 242 27 6.03 119 14.5 1.71 320 32 ------------------------------------ ------------------------------------ 6.03 221 16.2 0.00 71 1 5.75 223 16.9 0.60 166 11 6.15 994 17.1 1.24 -17 60 5.89 230 15.5 3.81 44 5 5.56 256 16.4 0.34 523 1 5.72 249 17.9 1.05 149 9 6.47 573 14.5 7.00 169 5 6.20 755 17.9 0.46 -53 2 6.08 727 19.6 1.40 -23 9 6.16 149 15.0 5.36 38 5 5.60 157 16.7 0.88 153 9 5.69 159 17.7 1.51 75 9 6.37 183 15.0 3.47 149 1 5.83 192 17.1 0.36 126 0 6.26 203 18.5 1.40 138 1 6.57 1,480 15.4 0.00 31 9 6.19 1,817 15.0 0.77 43 1 6.30 1,381 15.7 1.99 144 22 6.19 160 15.8 12.31 73 8 5.76 149 16.0 1.88 188 40 5.87 160 17.0 1.99 301 40 NS NS NS NS NS NS 7.76 348 16.4 0.39 -153 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 5.47 371 14.7 2.66 140 2 5.42 309 16.5 0.25 -34 0 5.40 333 15.3 1.89 291 1 6.87 958 15.2 0.00 -82 10 6.44 1,037 13.1 1.09 -88 1 6.33 817 16.4 1.35 -67 15 5.93 187 15.2 0.00 28 4 5.35 100 13.2 1.06 104 43 5.90 206 16.7 1.31 233 72 5.66 467 15.6 0.00 90 8 5.48 462 16.7 0.26 60 9 5.66 490 16.1 1.04 295 51 DRY DRY DRY DRY DRY DRY 6.17 991 16.8 0.47 -81 0 6.11 959 16.5 1.64 -40 3 6.50 822 16.5 1.70 78 >800 6.51 803 18.1 0.51 -80 3 6.35 836 17.1 1.21 -82 3 6.81 1,050 15.4 0.00 -92 12 6.30 745 13.7 0.64 -89 3 6.52 877 15.8 1.47 -100 10 6.51 997 16.1 0.00 -84 2 6.10 930 14.0 0.49 -98 0 6.15 1,430 16.7 1.60 -83 23 6.45 171 14.6 0.00 -22 2 5.79 149 15.7 1.77 60 9 6.04 160 15.2 2.04 335 96 6.40 251 16.1 6.27 17 1 6.13 255 16.0 1.23 130 2 6.14 259 15.1 2.75 332 15 6.14 116 14.4 0.00 84 8 5.74 112 15.3 0.21 159 1 5.97 116 15.1 1.61 311 1 6.57 251 14.1 0.00 125 1 6.40 236 15.5 1.45 223 14 6.42 242 14.7 1.64 346 37 6.00 235 14.8 0.00 103 9 5.72 207 15.2 0.66 175 1 5.79 199 15.2 1.40 266 33 6.70 227 14.9 3.03 3 5 5.30 96 15.1 1.09 188 8 5.54 106 14.6 1.39 258 68 NS NS NS NS NS NS 6.02 208 17.1 1.49 133 2 NS NS NS NS NS NS NS NS NS NS NS NS 6.34 297 15.3 1.51 54 1 NS NS NS NS NS NS 6.37 253 14.3 0.00 145 1 6.15 222 14.6 1.20 117 2 6.25 236 15.4 1.45 348 36 DRY DRY DRY DRY DRY DRY 7.02 466 16.0 4.10 -17 15 6.16 560 11.0 2.12 341 11 DRY DRY DRY DRY DRY DRY 7.10 333 15.5 4.46 -7 6 DRY DRY DRY DRY DRY DRY Notes: 1. NS - Not Sampled ` 2. CD-4, CD-5, and CD-6 were installed in September 2006. 3. AMW-1s, -1d, -2s, and -2d were installed in October 2009. 4. CD-4 and CD-5 were abandoned in July 2010. 5. MW-3 deep, -L deep, -and -M are sampled annually during the spring event. 7. µs/cm- Microsiemens per centimeter 8. mg/L - milligrams per liter 9. ORP - Oxidation-Reduction Potential 10. Turb. - Turbidity; NTUs - Nephelometric Turbidity Units 11. mVs - millivolts 12. DO - Dissolved Oxygen 13. S.U. - Standard Unit 14. Temp. - Temperature; Deg. C - Degrees Celsius 15. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 16. MW-9 was removed from the monitoring program in November 2012. No. 35 5/6-10/1311/27-29/2012 No. 37 11/4-7/13 No. 36 Page 2 of 4 January 2017 Table 4 Water Quality Parameters November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-1d (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-4 (abandoned) 1302-MSWLF- & 1302-CDLF-1998 CD-4 Rep 1302-MSWLF- & 1302-CDLF-1998 CD-5 (abandoned) 1302-MSWLF- & 1302-CDLF-1998 CD-6 1302-MSWLF- & 1302-CDLF-1998 AMW-1s 1302-MSWLF- & 1302-CDLF-1998 AMW-1d 1302-MSWLF- & 1302-CDLF-1998 AMW-2s 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 1302-MSWLF- & 1302-CDLF-1998 MW-1 1302-MSWLF- & 1302-CDLF-1998 MW-3 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep 1302-MSWLF- & 1302-CDLF-1998 MW-9 1302-MSWLF- & 1302-CDLF-1998 MW-A 1302-MSWLF- & 1302-CDLF-1998 MW-B 1302-MSWLF- & 1302-CDLF-1998 MW-C 1302-MSWLF- & 1302-CDLF-1998 MW-D 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 1302-MSWLF- & 1302-CDLF-1998 MW-E deep 1302-MSWLF- & 1302-CDLF-1998 MW-F 1302-MSWLF- & 1302-CDLF-1998 MW-G 1302-MSWLF- & 1302-CDLF-1998 MW-H 1302-MSWLF- & 1302-CDLF-1998 MW-H deep 1302-MSWLF- & 1302-CDLF-1998 MW-I 1302-MSWLF- & 1302-CDLF-1998 MW-J 1302-MSWLF- & 1302-CDLF-1998 MW-K 1302-MSWLF- & 1302-CDLF-1998 MW-L 1302-MSWLF- & 1302-CDLF-1998 MW-L deep 1302-MSWLF- & 1302-CDLF-1998 MW-M 1302-MSWLF- & 1302-CDLF-1998 MW-X 1302-MSWLF- & 1302-CDLF-1998 SW-1 1302-MSWLF- & 1302-CDLF-1998 SW-2 Surface Water Sample Locations Facility Permit Numbers Sampling Event: Sampling Date: Monitoring Well Code pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb. (S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs) 6.15 119 15.9 0.02 353 9 6.10 129 15.1 6.06 135 2 6.00 115 15.5 3.99 281 7 6.21 134 19.2 4.56 293 9 6.18 139 16.5 4.68 109 14 5.97 123 16.4 4.84 186 13 ------------------------------------ 6.29 495 13.5 2.75 70.4 4 ------------------------------------ 5.84 217 17.7 2.86 137 4 5.77 253 16.4 3.35 45 67 5.79 372 17.4 2.04 142 5 5.83 251 16.8 0.02 400 10 5.72 251 17.5 3.25 132 8 4.58 243 14.9 2.00 592 6 6.04 650 20.1 2.05 -28 604 6.13 643 18.0 1.36 -68 29 5.94 518 15.9 1.78 -52 16 5.76 178 18.8 2.08 114 6 5.77 182 15.2 3.48 121 6 5.07 160 14.2 3.50 562 6 6.30 231 16.9 3.88 95 1 6.26 252 16.0 4.19 104 1 5.77 230 15.2 2.51 391 1 6.36 1,361 15.0 2.84 37 3 6.34 1,511 15.4 2.59 -37 0 6.29 2,379 14.9 2.69 -19 6 6.05 180 18.5 0.04 150 8 5.97 202 16.3 5.94 466 4 5.42 166 17.6 2.29 260 14 7.75 385 16.5 4.04 -65 4 NS NS NS NS NS NS 7.49 368 20.5 1.50 -198 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 5.42 432 16.9 0.04 -17 1 5.47 451 16.4 1.70 45 2 4.78 390 15.6 2.34 27 2 6.66 1,033 12.6 2.58 -67 10 6.62 922 16.6 3.00 -101 1 6.70 1,485 13.0 3.03 -68 9 5.64 108 12.3 2.23 44 4 6.02 428 16.0 2.58 47 3 5.94 162 12.9 3.89 -181 8 5.85 705 17.2 1.85 -17 2 5.71 471 15.7 3.39 35 4 5.86 745 16.8 3.66 15 3 5.99 831 19.0 0.07 -24 2 6.25 1,180 17.6 1.62 -54 3 6.04 1,095 17.3 3.61 -38 9 5.60 1,042 20.2 0.09 -41 800 6.34 1,198 18.0 1.09 -82 13 6.41 1,027 18.4 0.88 -100 15 6.57 726 13.8 2.74 -81 5 6.46 919 15.4 2.18 -104 6 6.51 1,270 13.9 3.58 -58 3 6.27 1,542 13.7 2.29 -106 8 6.30 1,794 16.3 1.97 -124 14 6.31 2,445 13.9 2.66 -78 6 5.92 161 14.5 2.39 230 19 5.92 199 14.2 3.70 466 11 5.51 174 15.0 2.71 136-5 10 6.25 269 15.4 2.10 260 4 6.24 317 14.3 3.81 427 4 6.12 285 15.4 1.62 137 4 5.95 118 15.3 2.59 84 3 6.11 133 14.4 4.12 199 3 5.64 134 15.3 2.82 132 3 6.39 259 15.8 2.05 36 5 6.53 245 14.2 3.75 155 14 6.54 402 14.9 3.13 137 7 5.81 202 16.0 2.88 96 6 5.83 229 14.6 2.65 187 10 5.56 239 14.9 1.50 95 5 5.80 99 16.6 2.12 379 4 5.78 122 16.4 4.03 59 3 5.29 97 17.5 4.15 131 3 6.88 201 17.5 2.70 380 3 NS NS NS NS NS NS 6.61 341 17.5 4.79 190 3 6.31 271 15.3 2.45 211 4 NS NS NS NS NS NS 6.31 334 15.4 1.49 116 4 6.28 216 15.2 2.07 106 21 6.31 228 14.5 4.53 131 2 6.19 341 13.5 3.23 140 4 7.24 502 24.6 0.07 -26 22 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY 7.50 604 25.4 4.48 3 8 6.50 325 10.4 -69.80 2 43 6.89 520 24.7 2.19 4 7 Notes: 1. NS - Not Sampled 2. CD-4, CD-5, and CD-6 were installed in September 2006. 3. AMW-1s, -1d, -2s, and -2d were installed in October 2009. 4. CD-4 and CD-5 were abandoned in July 2010. 5. MW-3 deep, -L deep, -and -M are sampled annually during the spring event.` 7. µs/cm- Microsiemens per centimeter 8. mg/L - milligrams per liter 9. ORP - Oxidation-Reduction Potential 10. Turb. - Turbidity; NTUs - Nephelometric Turbidity Units 11. mVs - millivolts 12. DO - Dissolved Oxygen 13. S.U. - Standard Unit 14. Temp. - Temperature; Deg. C - Degrees Celsius 15. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 16. MW-9 was removed from the monitoring program in November 2012. No. 40 5/4-7/15 No. 39 11/3-6/14 No. 38 5/5-8/14 Page 3 of 4 January 2017 Table 4 Water Quality Parameters November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 CD-1s (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-1d (background well) 1302-MSWLF- & 1302-CDLF-1998 CD-4 (abandoned) 1302-MSWLF- & 1302-CDLF-1998 CD-4 Rep 1302-MSWLF- & 1302-CDLF-1998 CD-5 (abandoned) 1302-MSWLF- & 1302-CDLF-1998 CD-6 1302-MSWLF- & 1302-CDLF-1998 AMW-1s 1302-MSWLF- & 1302-CDLF-1998 AMW-1d 1302-MSWLF- & 1302-CDLF-1998 AMW-2s 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 1302-MSWLF- & 1302-CDLF-1998 MW-1 1302-MSWLF- & 1302-CDLF-1998 MW-3 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep 1302-MSWLF- & 1302-CDLF-1998 MW-9 1302-MSWLF- & 1302-CDLF-1998 MW-A 1302-MSWLF- & 1302-CDLF-1998 MW-B 1302-MSWLF- & 1302-CDLF-1998 MW-C 1302-MSWLF- & 1302-CDLF-1998 MW-D 1302-MSWLF- & 1302-CDLF-1998 MW-E Rep 1302-MSWLF- & 1302-CDLF-1998 MW-E deep 1302-MSWLF- & 1302-CDLF-1998 MW-F 1302-MSWLF- & 1302-CDLF-1998 MW-G 1302-MSWLF- & 1302-CDLF-1998 MW-H 1302-MSWLF- & 1302-CDLF-1998 MW-H deep 1302-MSWLF- & 1302-CDLF-1998 MW-I 1302-MSWLF- & 1302-CDLF-1998 MW-J 1302-MSWLF- & 1302-CDLF-1998 MW-K 1302-MSWLF- & 1302-CDLF-1998 MW-L 1302-MSWLF- & 1302-CDLF-1998 MW-L deep 1302-MSWLF- & 1302-CDLF-1998 MW-M 1302-MSWLF- & 1302-CDLF-1998 MW-X 1302-MSWLF- & 1302-CDLF-1998 SW-1 1302-MSWLF- & 1302-CDLF-1998 SW-2 Surface Water Sample Locations Facility Permit Numbers Sampling Event: Sampling Date: Monitoring Well Code pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb.pH Conductivity Temp.DO ORP Turb. (S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs)(S.U.)(µS/cm)(deg. C)(mg/L)(mVs)(NTUs) 5.73 132 15.0 3.84 519 3 5.91 103 15.7 3.45 245 4 5.81 136 14.5 6.96 507 7 6.06 115 15.8 4.50 210 20 5.34 124 15.9 3.10 330 8 ------------------------------------ 6.06 231 16.4 3.19 31.2 3 6.90 242 14.2 2.68 -54 28 5.05 113 16.1 4.49 360 6 ------------------------------------ 5.90 244 16.3 3.92 111 >800 6.20 271 16.9 1.50 -48 23 5.62 292 16.9 1.38 -4 29 5.80 443 16.0 2.68 253 3 6.07 224 16.5 3.77 222 8 5.02 297 18.8 1.65 377 6 6.11 1,004 15.8 2.55 -42 5 6.13 477 18.1 1.51 -28 4 5.00 583 13.3 1.73 199 8 5.92 173 16.2 4.19 187 3 5.78 154 15.8 3.22 51 7 4.92 164 16.4 3.38 235 8 6.36 260 17.2 3.90 158 2 6.04 229 15.9 2.69 88 1 5.52 356 16.5 2.15 346 4 6.31 1,743 15.5 1.94 21 7 8.05 1,515 15.4 3.48 94 4 6.13 1,812 16.2 1.03 34 8 6.20 178 19.5 3.85 166 3 6.04 167 16.5 3.18 101 1 5.52 246 20.6 3.50 439 5 7.63 387 19.5 1.67 -165 3 7.48 362 15.6 2.26 -130 0 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 5.30 402 15.5 1.41 29 3 5.48 394 16.1 1.27 -55 1 4.77 412 16.5 1.65 205 4 6.00 833 16.9 3.91 -51 6 8.32 976 14.0 3.73 53 17 6.44 1,085 17.5 2.11 -79 9 5.21 186 16.7 1.73 153 37 6.50 126 14.0 3.48 -78 6 5.52 243 17.4 2.58 49 7 5.19 520 16.5 2.60 85 14 7.26 617 16.3 1.23 -84 4 5.43 627 16.5 1.51 69 6 6.10 1,076 16.2 1.25 -36 3 6.27 1,088 17.1 1.40 -59 1 5.59 1,139 17.6 3.79 48 5 6.44 979 16.2 1.21 -71 5 6.63 1,017 17.5 3.08 -95 9 5.89 959 18.1 2.30 -39 8 6.61 1,134 15.5 2.71 -136 3 8.12 796 14.4 2.65 -47 6 6.25 1,141 16.6 1.23 -71 6 6.32 1,372 16.8 2.28 -135 0 7.96 1,671 15.0 2.40 49 12 6.07 2,320 17.6 1.09 -80 1 5.15 203 15.3 0.81 168 43 6.06 162 14.2 5.40 204 38 5.53 211 15.3 1.63 118 59 5.72 280 15.3 0.64 146 4 6.82 272 14.9 4.99 145 18 5.91 337 15.0 2.21 105 16 5.13 128 15.2 0.76 104 3 6.86 127 15.0 4.40 164 7 5.65 164 15.0 1.35 68 9 6.48 274 14.3 0.38 210 7 6.92 265 14.8 4.20 28 58 6.05 311 14.8 2.65 21 36 4.93 253 15.2 3.43 167 6 7.03 208 15.0 4.34 21 14 5.47 283 15.4 1.89 149 21 5.92 93 18.5 3.80 89 4 5.80 95 14.2 3.66 192 2 5.11 146 18.1 3.49 486 5 5.49 395 15.8 0.80 155 2 6.82 209 15.0 3.88 149 2 NS NS NS NS NS NS 5.67 334 15.7 0.49 151 10 7.97 320 15.3 4.02 -3 8 NS NS NS NS NS NS 5.03 234 15.3 2.53 342 3 7.19 210 13.9 3.98 20 6 5.94 275 15.3 1.62 78 2 6.83 840 16.0 1.04 -54 0 6.99 342 15.4 4.99 360.3 >800 DRY DRY DRY DRY DRY DRY 5.55 788 15.4 1.34 158 7 6.80 241 15.6 3.51 181 590 DRY DRY DRY DRY DRY DRY Notes: 1. NS - Not Sampled 2. CD-4, CD-5, and CD-6 were installed in September 2006. 3. AMW-1s, -1d, -2s, and -2d were installed in October 2009. 4. CD-4 and CD-5 were abandoned in July 2010. 5. MW-3 deep, -L deep, -and -M are sampled annually during the spring event. 6. µs/cm- Microsiemens per centimeter 7. mg/L - milligrams per liter 8. ORP - Oxidation-Reduction Potential 9. Turb. - Turbidity; NTUs - Nephelometric Turbidity Units 10. mVs - millivolts 11. DO - Dissolved Oxygen 12. S.U. - Standard Unit 13. Temp. - Temperature; Deg. C - Degrees Celsius 14. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 15. MW-9 was removed from the monitoring program in November 2012. No. 43 10/31/16 - 11/3/16 No. 42 5/16-19/16 No. 41 10/26-29/15 Page 4 of 4 January 2017 Table 5a Detected Groundwater Constituents - Metals November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Number 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t Nu m b e r s Mo n i t o r i n g We l l C o d e Sa m p l e D a t e An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Ir o n Le a d Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zin c 1*10 700 4*2 10 1*1,000 300 15 50 1 100 20 20 0.2*0.3*1,000 6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 CD-1s 3-May-11 81.4J 0.19J 5.45JB 4.23J 16.0 2.32J 5.93J 0.14J 20.6J 26.5 CD-1s 8-Nov-11 59.7J 0.25JB 4.46J 2.67J 12.4 1.9J 4.41J 0.08J 11.2J 18.2 CD-1s 7-May-12 45.5J 3.30J 1.19J 8.75J 1.12J 3.01J 12.7J 12.6B CD-1s 28-Nov-12 63.8J 0.11J 5.65J 3.05J 11.6 1.43J 4.66J 17.1J 16.9 CD-1s 7-May-13 0.94J 2.4JB 35.6J 0.88J 0.67J 4.04J 0.39J 1.78J 0.13J 6.06J 5.08J CD-1s 5-Nov-13 46.8J 0.12J 3.59J 1.63J 10.2 1.35J 3.50J 18.4JB 15.4B CD-1s 6-May-14 28.8J 4.14JB 1.48J 0.11J 1.03J 0.31J 3.40J 2.98JB CD-1s 4-Nov-14 28.7J 0.13J 1.31J 0.06J 1.04J 0.11J 2.57JB 1.58J CD-1s 5-May-15 1.63J 29.5JB 1.33J 371 0.15J 13.8 0.103JB 1.17J 2.40J 2.75JB CD-1s 27-Oct-15 1.00J 28.4J 0.80J 0.39J 0.75J 234 0.12J 35.9 1.21J 4.19CN,J 0.15J 4.10J 3.36B-01,J CD-1s 17-May-16 29.3J 0.94J 0.99J 446 0.12J 17.0J 1.01J 4.70J 1.93J CD-1s 1-Nov-16 30.5J 1.23J 1.32J 1.36J 647 0.28J 70.8 1.35J 4.30J CD-1d 3-May-11 2.44J 231 2.03 16.7 18.6 112 14.0 22.3J 0.11J 101 103 CD-1d 8-Nov-11 74.5J 0.51J 4.08J 4.27J 27 2.84J 5.68J 24.6J 26.3 CD-1d 7-May-12 72.4J 0.58J 3.91J 4.67J 25 2.81J 5.58J 26 27.9B CD-1d 28-Nov-12 0.33J 37.7J 0.07J 2.38J 0.94J 12.6 1.14J 2.50J 8.90J 13 CD-1d 8-May-13 0.88J 1.02JB 31.2J 0.07J 0.78J 4.5J 0.49J 1.92J 6.18J 13.1 CD-1d 5-Nov-13 35J 0.86J 4.34J 1.13J 1.90J 17.1JB 10.8B CD-1d 6-May-14 1.14J 37.8J 0.07J 0.05J 3.22JB 1.16J 7.34J 0.81J 2.74J 0.12J 6.16J 9.41JB CD-1d 4-Nov-14 43.1J 0.16J 0.11J 2.25J 9.09J 0.87J 2.88J 10.2JB 10.7 CD-1d 5-May-15 34.5JB 0.84J 3.63J 1,320 0.39J 32.5 1.42J 5.18J 3.68JB CD-1d 27-Oct-15 0.42J 42.3J 0.13J 1.87J 2.15J 8.18J 3,170 0.97J 87.4 2.49J 4.37CN,J 0.06J 10.9J 14.0B-01 CD-1d 17-May-16 81.3J 0.46J 4.86J 7.42J 26.0 12,000 3.13J 287 7.11J 2.11J 0.07J 29.3 29.7 CD-1d 1-Nov-16 32.6J 1.19J 0.77J 2.82J 1,200 0.33J 31.3J 1.24J 7.96J 4.29J CD-4 Rep 3-May-11 206 0.9JB 17.6 0.62J 8.39J 2.72JB CD-4 Rep (dup)3-May-11 0.21J 206 17.9 0.68J 8.98J 0.17J 2.85J CD-4 Rep 8-Nov-11 0.14J 191 0.93J 18.2 1.00J 8.86J 9.44J CD-4 Rep 9-May-12 184 1.69J 18.1 1.70J 0.17J 11.3J 3.03J 16.1B CD-4 Rep 29-Nov-12 172 13.7 0.62J 7.03J 2.84J 2.14JB CD-4 Rep 10-May-13 75.5J 0.5J 2.71J 7.87J 1.94J 0.88J 11.2J 11.1J 10.3 CD-4 Rep 7-Nov-13 1.36J 60.4J 0.35J 0.07J 0.77J 5.31J 1.83J 0.57J 5.11J 0.13J 32 4.40JB CD-4 Rep 7-May-14 62.4J 0.31J 0.05J 3.25JB 5.02J 1.70J 0.32J 6.52J 22.2J 2.97JB CD-4 Rep 5-Nov-14 70.0J 0.31J 2.59J 1.46J 0.72J 4.29J 14.8JB 6.85J CD-4 Rep 6-May-15 58.4J 0.39J 1.13J 5.94J 1.90J 0.53J 4.72J 14.0J 2.99J CD-4 Rep 28-Oct-15 0.79J 57.9J 0.32J 2.18J 5.86J 8.95J 1.26J 10.7J 4.14CN,J 13.9J 8.34B-01,J CD-4 Rep 18-May-16 1.09J 56.2J 0.46J 1.24J 7.31J 1.02J 0.66J 5.43J 18.0J 3.70J CD-4 Rep 2-Nov-16 46.3J 0.27J 1.35J 1.59J 1.18J 0.90J 4.18J 1.11J 18.1J 8.81J CD-6 4-May-11 66.6J 0.42J 6.74J 4.08J 4.6J 2.01J 5.34J 0.1J 24.7J 14 CD-6 9-Nov-11 59.6J 0.26J 4.71J 2.62J 7.89J 1.31J 5.22J 15.8J 9.62J CD-6 9-May-12 57.8J 0.20J 4.20J 2.08J 3.63J 1.21J 4.48J 17.2J 17.7B CD-6 29-Nov-12 50.8J 0.13J 2.25J 1.80J 1.86J 0.73J 3.73J 12.3J 6.61JB CD-6 10-May-13 61.4J 0.36J 5.89J 3.02J 4.12J 1.43J 4.77J 20.4J 13.8 CD-6 7-Nov-13 0.57J 3.77J 298 0.14J 18.3 36.9 2.13J 11.7J 1.07J 14.6J 6.88JB CD-6 7-May-14 38.5J 0.10J 3.42JB 1.04J 0.07J 2.30J 4.39J 2.40JB CD-6 5-Nov-14 120 0.88J 7.64J 8.02J 8.02J 3.83J 9.04J 0.14J 50.6B 25.7 CD-6 6-May-15 47.4J 0.20J 1.60J 1.84J 2.77J 0.81J 3.29J 10.5J 5.40J CD-6 28-Oct-15 4.97J 215 2.03 32.3 19.5 25.6 16.1 21.6J 8.64J 4.05CN,J 0.37J 107 73.9B-01 CD-6 18-May-16 1.92J 62.2J 0.23J 3.46J 13.2 2.57J 1.58J 8.70J 1.01J 12.6J 7.94J CD-6 2-Nov-16 1.89J 63.7J 0.33J 6.18J 13.3 3.12J 2.87J 9.12J 1.29J 17.3J 10.1 AMW-1s 3-May-11 104 0.92J 1.4JB 0.31J 2.08J 0.5J 3.59J 0.08J 8.1JB AMW-1s 8-Nov-11 105 0.90J 1.43J 0.46J 1.94J 0.44J 3.67J 0.10J 8.47J AMW-1s 7-May-12 103 0.86J 2.39J 1.87J 0.22J 3.87J 2.98J 8.49JB AMW-1s 28-Nov-12 0.19J 97.4J 0.83J 0.78J 0.78J 0.11J 3.31J 2.41J 4.79J AMW-1s 8-May-13 101 0.87J 1.98J 0.09J 4.05J 2.24J 6.13J AMW-1s 6-Nov-13 98J 0.91J 0.22J 2.91J 0.32J 4.06J 16.7JB 6.70JB AMW-1s 7-May-14 93.0J 0.95J 2.44JB 0.28J 2.27J 0.47J 3.91J 1.39J 6.35JB AMW-1s 5-Nov-14 89.2J 1.06 0.50J 3.37J 0.78J 4.15J 4.01JB 7.60J AMW-1s 7-May-15 87.6J 0.97J 3.78J 0.31J 2.72J 0.68J 5.86J 3.31J 6.51J AMW-1s 29-Oct-15 82.5J 0.78J 1.03J 0.71J 0.19J 4.03J 3.18CN,J 4.22J 9.82B-01,J AMW-1s 18-May-16 0.27J 0.82J 85.4J 1.03 1.43J 0.38J 2.47J 0.92J 4.16J 5.18J 7.43J AMW-1s 2-Nov-16 71.7J 0.56J 0.55J 3.19J 5.78J AMW-1d 3-May-11 0.24J 129 0.12J 4.67J 2.08J 0.25J 9.16J 0.19J 9.17JB AMW-1d 8-Nov-11 0.18J 140 0.07J 0.94J 5.78J 1.64J 0.21J 10.2J 0.25J 7J AMW-1d 7-May-12 0.29J 135 5.20J 2.17J 0.27J 9.17J 2.69J 8.98JB AMW-1d 28-Nov-12 0.41J 106 0.14J 1.38JB 3.27J 2.26J 0.52J 6.21J 5.50J AMW-1d 8-May-13 1.05JB 133 4.53J 1.63J 0.25J 7.81J 3.08J AMW-1d 6-Nov-13 133 1.88J 4.31J 1.77J 0.45J 7.45J 20.5JB 4.30JB AMW-1d 7-May-14 143 0.50J 0.05J 11.4B 5.48J 4.90J 3.01J 9.84J 5.89J 27.9B AMW-1d 5-Nov-14 1.46J 168 0.69J 0.05J 4.49J 6.70J 6.53J 4.14J 11.8J 13.8JB 20.8 AMW-1d 7-May-15 133 0.40J 4.08J 5.51J 3.58J 2.14J 9.83J 5.47J 10.3 AMW-1d 29-Oct-15 1.41J 123 0.18J 3.02J 5.32J 1.06J 0.93J 8.61J 3.57CN,J 4.00J 6.79B-01,J AMW-1d 18-May-16 1.01J 131 0.19J 2.09J 6.06J 1.52J 0.84J 9.03J 2.52J 6.84J AMW-1d 3-Nov-16 128 0.17J 2.20J 6.09J 1.12J 0.81J 9.30J 6.65J North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 1 of 14 January 2017 Table 5a Detected Groundwater Constituents - Metals November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Number 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t Nu m b e r s Mo n i t o r i n g We l l C o d e Sa m p l e D a t e An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Ir o n Le a d Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zin c 1*10 700 4*2 10 1*1,000 300 15 50 1 100 20 20 0.2*0.3*1,000 6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 AMW-2s 3-May-11 52.1J 0.92J 2.49JB 1.10J 1.41J 2.2J 2.54J 7.17J 6.47JB AMW-2s 8-Nov-11 42.3J 0.50J 1.36J 0.29J 0.82J 2.19J 1.36J 5.08J AMW-2s 8-May-12 42.8J 0.45J 1.48J 0.23J 2.85J 0.66J 1.47J 3.77J 5.92JB AMW-2s 29-Nov-12 45.3J 0.48J 1.02J 0.23J 0.62J 0.32J 1.19J 1.41J AMW-2s 9-May-13 42.6J 0.57J 1.11J 0.52J 1.06J 0.63J 1.95J 3.09J 3.63J AMW-2s 6-Nov-13 40.1J 0.54J 0.27J 0.64J 0.42J 1.48J 16.8JB 3.51JB AMW-2s 7-May-14 43.7J 0.56J 2.16JB 0.30J 0.87J 0.35J 1.41J 1.96JB AMW-2s 5-Nov-14 46.0J 0.69J 0.44J 1.01J 0.59J 1.88J 2.84J AMW-2s 6-May-15 2.72J 43.4J 0.51J 1.07J 0.39J 1.46J 2.07J 2.37J AMW-2s 28-Oct-15 1.02J 50.6J 0.88J 1.56J 0.75J 0.50J 1.23J 1.96J 6.12CN,J 6.23J 6.14B-01,J AMW-2s (dup)28-Oct-15 1.00J 51.1J 0.85J 1.79J 0.87J 0.57J 1.34J 2.10J 3.34CN,J 7.01J 7.01B-01,J AMW-2s 17-May-16 1.21J 45.8J 0.69J 1.15J 0.65J 0.48J 0.71J 1.63J 0.10J 4.51J 3.93J AMW-2s 1-Nov-16 46.5J 0.73J 1.60J 0.58J 0.57J 0.74J 1.81J 5.17J AMW-2d 3-May-11 55.2J 2.86JB 0.83J 1.03J AMW-2d 8-Nov-11 47.5J 1.08J 0.12J 0.77J 1.23J AMW-2d 8-May-12 78.2J 1.26J 3.20J 0.33J 1.22J 2.79J 10.5B AMW-2d 28-Nov-12 69.1J 0.88J 2.34J 0.39J 2.56J 4.76J AMW-2d 9-May-13 54.7J 1.75J 0.06J 1.42J 4.03J 2.4J AMW-2d 6-Nov-13 71.1J 2.43J 2.69J 18.5JB 7.86JB AMW-2d 7-May-14 57.0J 0.10J 2.08JB 0.84J 1.24J 0.76JB AMW-2d 5-Nov-14 60.4J 0.07J 1.25J 2.33J 1.09JB 5.04J AMW-2d 6-May-15 1.28J 67.4J 0.85J 1.67J AMW-2d 28-Oct-15 0.25J 63.9J 0.45J 0.14J 1.50J 2.79CN,J 2.65J 7.41B-01,J AMW-2d 17-May-16 64.5J 0.13J 1.37J 1.07J 1.38J AMW-2d 2-Nov-16 67.7J 0.10J 0.66J 1.90J 5.02J MW-1 4-May-11 0.46J 5.08J 360 0.9J 0.09J 9.05J 19.7 11.8 4.59J 20.8J 2.39J 0.09J 35.7 40.4 MW-1 9-Nov-11 2.22J 187 0.52J 16.8 6.67J 0.64J 37.7J 3.35J 3.71J MW-1 9-May-12 201 0.16J 0.06J 2.26J 17.8 17.0 3.61J 42.4J 6.90J 12.2J 13.9B MW-1 28-Nov-12 153 1.03J 0.75J 12.6 5.54J 0.75J 29.9J 5.75J 4.86J 3.55J MW-1 10-May-13 172 0.12J 0.26J 0.87J 15.9 9.48J 0.3J 35.1J 8.86J 8.67J MW-1 6-Nov-13 127 0.31J 11.5 8.66J 1.12J 28J 5.89J 11.9JB 2.64JB MW-1 7-May-14 1.99J 120 0.06J 0.28J 10.3 10.2 0.28J 28.2J 5.61J 0.10J 6.99J 1.93J MW-1 (dup)7-May-14 119 0.05J 0.31J 10.5 10.2 0.29J 28.0J 5.70J 6.16J 1.91J MW-1 4-Nov-14 2.27J 126 0.05J 0.44J 12.5 9.07J 0.95J 31.1J 2.40J 5.47JB 1.72J MW-1 5-May-15 0.83J 128 0.17J 11.6 7.74J 0.23J 29.9J 2.99J 3.77J 1.88J MW-1 28-Oct-15 144 0.36J 1.52J 14.4 8.26J 1.15J 33.3J 4.32CN,J 3.63J 4.24B-01,J MW-1 19-May-16 144 0.34J 0.51J 12.8 12.0 0.28J 29.4J 2.59J 1.99J MW-1 2-Nov-16 143 0.39J 13.7 8.64J 0.63J 30.4J 3.02J MW-3 4-May-11 36.2J 0.32J 4.19JB 1.56J 1.64J 1.14J 2.34J 0.11J 6.8J 7.68J MW-3 9-Nov-11 35.2J 0.25J 2.56J 1.22J 1.60J 1J 2.03J 8.1J MW-3 (dup)9-Nov-11 37.1J 0.24JB 2.30J 1.20J 1.55J 1.01J 2.00J 6.29J MW-3 8-May-12 30.1J 2.07J 0.64J 1.69J 0.79J 2.23J 3.76J 7.63JB MW-3 28-Nov-12 28.6J 2.30J 0.32J 0.84J 0.43J 1.20J 3.54J 1.98J MW-3 9-May-13 37.9J 0.51J 3.28J 1.53J 1.81J 2.21J 2.36J 6.15J 8.1J MW-3 7-Nov-13 0.50J 37.9J 0.47J 0.09J 3.93J 1.78J 3.55J 4.17J 4.47J 24.7J 82B MW-3 8-May-14 56.2J 0.70J 3.32J 2.45J 3.08J 3.28J 3.54J 8.62J 36.6 MW-3 6-Nov-14 30.8J 0.05J 1.14JB 0.40J 1.03J 0.42J 1.56J 3.85J 3.57JB MW-3 6-May-15 0.81J 55.4J 0.71J 4.14JB 2.59J 3.17J 3.69J 4.36J 0.07J 11.3J 15.3 MW-3 28-Oct-15 25.0J 1.23J 0.25J 0.83J 4.17CN,J 3.12J 5.43B-01,J MW-3 18-May-16 1.46J 0.35J 0.99J 3.48J 2.10J MW-3 2-Nov-16 27.4J 1.60J 0.25J 1.00J 2.36J MW-3 Deep 5-May-11 2.47J 3.11J 195 1.73 1.24 52.1 16 26 14 55.4 0.17J 0.55J 77.3 81 MW-3 Deep 9-May-12 0.35J 38.3J 0.93J 2.12J 1.71JB MW-3 Deep 10-May-13 0.41J 37.7J 0.12J 0.09J 2.18JB 0.13J 1.32J 0.17J 2.49J 2.57J MW-3 Deep 8-May-14 40.8J 0.13J 4.10J 1.59J 0.98J 2.78J 5.44J MW-3 Deep 6-May-15 0.26J 2.16J 44.0J 0.13J 0.29J 1.90J 1.72J 2.47J 33.2 MW-3 Deep 28-Oct-15 1.02J 42.2J 0.70J 0.50J 0.64J 0.57J 3.00CN,J 5.87B-01,J MW-3 Deep 19-May-16 1.50J 43.0J 0.69J 0.61J 0.40J 0.58J 2.37J 3.26J MW-9 3-May-11 11.8J 1.44JB 0.27J 3.87J 0.61J 5.87J 4.62JB MW-9 9-Nov-11 9.87J 1.73J 0.16J 2.04J 0.54J 4.77J MW-9 9-May-12 13.7J 1.33J 0.34J 5.65J 0.09J 0.80J 8.37J 6.19JB MW-A 3-May-11 40J 0.15J 1.38JB 3.48J 0.87J 12.5J 3.86JB MW-A 9-Nov-11 0.36JB 44.2J 0.13J 1.81J 0.76J 9.32J 2.82J MW-A 9-May-12 42.4J 0.10J 1.14J 8.20J 0.91J 15.5J 4.53JB MW-A 27-Nov-12 0.36JB 45.6J 0.13J 0.97J 2.86J 1.17J 11.6J 1.86J 2.63J MW-A 7-May-13 43.7J 0.14J 0.64J 1.48J 1.48J 0.07J 9.14J 1.09J 2.31J MW-A 5-Nov-13 43.4J 1.65J 2.05J 0.76J 9.93J 20.3JB 3.37JB MW-A 6-May-14 44.2J 0.14J 3.73JB 8.88J 0.84J 16.6J 1.15J 2.10JB MW-A 4-Nov-14 45.1J 0.20J 6.14J 0.94J 18.7J 1.41J 1.87J MW-A 5-May-15 46.9J 0.15J 3.44J 0.84J 13.4J 1.41J 1.82J MW-A 27-Oct-15 0.26J 47.2J 0.14J 3.15J 1.18J 0.17J 12.9J 2.25CN,J 2.14J 5.23B-01,J MW-A 17-May-16 0.35J 1.01J 44.3J 0.17J 9.54J 0.48J 19.8J 2.40J 1.64J MW-A 1-Nov-16 48.6J 0.17J 7.25J 19.2J 3.85J 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 2 of 14 January 2017 Table 5a Detected Groundwater Constituents - Metals November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Number 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t Nu m b e r s Mo n i t o r i n g We l l C o d e Sa m p l e D a t e An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Ir o n Le a d Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zin c 1*10 700 4*2 10 1*1,000 300 15 50 1 100 20 20 0.2*0.3*1,000 6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 MW-B 4-May-11 2.35J 269 0.28J 3.78JB 18 3.45J 1.36J 11.3J 3.18J 0.14J 14.3J 9.95J MW-B 9-Nov-11 2.59J 249 0.06J 8.75J 1.51J 0.70J 8.91J 3.54J 0.13J 3.6J MW-B 9-May-12 191 8.68J 0.89J 0.09J 6.35J 15.9B MW-B 29-Nov-12 5.88J 268 23.5 1.08J 0.20J 9.10J 2.29J 3.58J MW-B 10-May-13 2.55J 197 9.39J 1.1J 0.29J 6.4J 2.89J 10.7 MW-B 6-Nov-13 2.02J 225 11.7 0.97J 0.23J 6.72J 1.49J 15.9JB 3.77JB MW-B 8-May-14 2.73J 236 0.08J 11.5 1.25J 0.55J 8.80J 1.48J 5.81J 3.14J MW-B 4-Nov-14 6.04J 226 0.06J 21.0 1.12J 0.18J 12.1J 2.75J 2.62JB 1.52J MW-B 5-May-15 0.30J 1.50J 160 8.50J 1.25J 0.34J 7.05J 2.25J 1.97J MW-B 29-Oct-15 2.61J 171 0.52J 16.5 0.53J 0.31J 5.45J 2.39CN,J 0.07J 7.39B-01,J MW-B 19-May-16 0.30B-01,J 2.16J 225 1.05J 11.7 0.81J 0.39J 6.53J 0.06J 4.64J 3.54J MW-B 3-Nov-16 2.43J 196 13.5 0.24J 6.84J 2.71J MW-C 4-May-11 42.3J 0.44J 0.07J 7.32J 5.63J 2.58J 1.45J 4.14J 0.08J 7.26J 9.97J MW-C 9-Nov-11 15.5J 0.15J 0.10J 0.62J 3.43J 1.06J 0.43J 4.19J 8.62J MW-C 9-May-12 43.5J 0.43J 7.45J 17 3.94J 2.30J 6.85J 10.4J 22.2B MW-C 29-Nov-12 35.8J 0.13J 2.75J 9.05J 1.17J 0.71J 3.94J 4.87J 8.07J MW-C 9-May-13 19.7J 0.24J 2.96J 0.75J 1.36J 0.8J 1.77J 3.48J 10.1 MW-C 6-Nov-13 31.7J 0.26J 3.77J 9.54J 1.79J 0.82J 3.74J 23.5JB 18.8B MW-C 7-May-14 19.6J 0.17J 2.98JB 3.20J 0.79J 0.26J 1.65J 3.08JB MW-C 5-Nov-14 47.2J 0.10J 0.57J 1.68J 4.20J 1.30J 0.29J 4.74J 2.11JB 3.06J MW-C 6-May-15 20.4J 0.30J 2.38J 2.26J 1.66J 0.91J 2.34J 3.53J 3.43J MW-C 29-Oct-15 1.42J 47.9J 0.68J 11.6 7.47J 4.52J 3.04J 9.28J 1.15J 3.79CN,J 0.10J 19.4J 14.4B-01 MW-C 18-May-16 21.4J 0.21J 0.71J 1.78J 0.47J 0.25J 1.69J 4.11J 2.01J MW-C 2-Nov-16 2.16J 34.0J 0.18J 1.30J 10.3 0.55J 0.33J 3.79J 3.51J MW-D 4-May-11 193 0.81J 0.12J 32.3 11.7 30.2 5.28J 30.4J 0.25J 41.7 37.3 MW-D 9-Nov-11 0.36JB 118 0.25J 8.02J 3.05J 8.5J 1.47J 15.3J 0.07J 5.68J 12.1 MW-D 9-May-12 124 3J 8.97J 3.94J 0.61J 15.7J 5.12J 9.33JB MW-D 28-Nov-12 0.98J 1.83J 117 0.11J 0.06J 2.31J 3.01J 3.63J 0.61J 13.8J 12.1J 5.11JB MW-D 9-May-13 140 0.21J 0.08J 6.4J 6.72J 7.78J 0.94J 17.3J 25.8 10.8 MW-D 6-Nov-13 194 0.86J 0.25J 28.6 12.8 35.5 7.32J 27J 105B 37.9B MW-D 7-May-14 169 0.21J 3.74JB 19.0 1.16J 20.7J 8.02J 1.43JB MW-D 5-Nov-14 121 0.11J 0.06J 1.62J 7.61J 3.41J 0.72J 18.3J 0.95JB 7.00J MW-D 5-May-15 1.79J 164 14.2 1.06J 21.7J 4.51J 1.62J MW-D 29-Oct-15 0.30J 5.11J 199 0.74J 0.12J 39.0 10.4 32.7 6.25J 37.0J 5.92J 3.91CN,J 0.37J 50.7 48.5B-01 MW-D 18-May-16 1.65J 157 0.11J 0.85J 17.0 0.92J 0.19J 21.0J 3.92J 1.72J MW-D 3-Nov-16 134 0.09J 8.75J 0.85J 0.21J 19.9J 3.64J MW-E Rep 4-May-11 262 0.57J 1.18JB 12.4 1.09J 0.62J 15.1J 6.4J MW-E Rep 8-Nov-11 1.07JB 267 0.41J 9.28J 0.83J 13.2J 0.07J 2.88J MW-E Rep 8-May-12 303 0.31J 12.6 0.85J 0.32J 15.2J 1.72J 10.3B MW-E Rep 8-May-13 286 0.34J 8.29J 1.08J 0.08J 14J 0.89J 3.71J MW-E Rep 5-Nov-13 294 15.5 0.84J 0.22J 15.8J 14JB 6.38JB MW-E Rep 6-May-14 342 0.44J 16.8 1.45J 0.67J 15.9J 7.58J 6.46JB MW-E Rep 4-Nov-14 326 0.21J 8.39J 0.89J 0.28J 15.9J 1.57J 2.99JB 4.31J MW-E Rep 5-May-15 348 0.30J 7.48J 1.02J 0.62J 14.5J 1.44J 12.2J 4.46J MW-E Rep 27-Oct-15 0.91J 294 0.26J 1.12J 10.2 0.39J 12.3J 2.07CN,J 4.84B-01,J MW-E Rep 18-May-16 1.11J 365 0.27J 12.0 0.32J 12.9J 2.31J 2.99J MW-E Rep 1-Nov-16 297 0.15J 5.44J 0.17J 11.4J 5.13J MW-E Deep 4-May-11 2.96J 2,530 0.25J 0.18J 1.14JB 66.4 3.11J 20 30.8J 57.9 MW-E Deep 8-Nov-11 3.66J 2,280 0.16J 0.22J 54.2 1.38J 16.4 26J 43.5 MW-E Deep 8-May-12 2.51J 2,210 0.53J 0.36J 50.1 31.6 94 24.9J 7.65J 60.9B MW-E Deep 28-Nov-12 0.71J 3.86J 1,820 0.84J 1.99 4.56J 39.6 22.3 213 26.1J 0.18J 9.20J 67.2 MW-E Deep 8-May-13 4.56JB 1,730 0.34J 0.71J 37.9 4.7J 74.5 20J 43 MW-E Deep 6-Nov-13 1.09J 2,240 0.19J 0.32J 39.7 2.34J 39.3 20.5J 16JB 41.2B MW-E Deep 6-May-14 2.69J 2,080 0.60J 0.44J 63.4 6.29J 60.9 32.7J 2.49J 32.2B MW-E Deep 4-Nov-14 3.29J 2,000 0.31J 0.47J 43.6 6.41J 55.6 20.4J 3.75JB 30.0 MW-E Deep 5-May-15 2.42J 2,040 0.25J 0.19J 34.4 2.70J 22.2 17.3J 0.87J 2.54J 19.3 MW-E Deep 27-Oct-15 2.55J 1,900 0.28J 0.23J 34.3 4.34J 38.2 14.2J 2.81CN,J 2.97J 24.3B-01 MW-E Deep 18-May-16 3.54J 2,150 0.48J 0.67J 0.93J 37.0 8.73J 76.4 16.0J 1.07J 8.52J 30.6 MW-E Deep 1-Nov-16 2.43J 1,960 0.22J 0.18J 34.5 2.34J 18.5 14.6J 19.3 MW-F 4-May-11 136 0.14J 0.75JB 1.29J 0.91J 3.15J 2.24J MW-F 9-Nov-11 0.17J 5.42J 219 0.06J 10.6 1.06J 4.44J 1.57J MW-F 9-May-12 3.19J 242 8.35J 1.27J 3.33J 0.92J 2.85J 2.34JB MW-F 29-Nov-12 283 0.15J 1.86J 8.50J 1.07J 0.59J 5.00J 1.52J 3.76J 4.46J MW-F 10-May-13 1.55J 1.17J 154 0.21J 1.63JB 5.16J 1.56J 0.15J 2.78J 2J 0.12J 4.86J MW-F 6-Nov-13 2.01J 255 11.2 0.82J 0.19J 3.45J 0.83J 12.7JB 2.43JB MW-F 8-May-14 5.17J 213 0.16J 10.4 0.97J 0.54J 4.88J 1.04J 6.84J 1.77J MW-F 4-Nov-14 2.92J 262 0.23J 11.3 0.80J 0.45J 5.51J 3.09J 1.25J MW-F 5-May-15 0.31J 2.29J 129 0.11J 1.39J 0.73J 0.10J 4.57J 1.85J MW-F 28-Oct-15 5.94J 262 0.45J 13.0 0.79J 0.14J 4.80J 1.92CN,J 3.67B-01,J MW-F 18-May-16 3.40J 214 9.62J 3.84J MW-F 3-Nov-16 231 0.14J 7.64J 4.63J 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 3 of 14 January 2017 Table 5a Detected Groundwater Constituents - Metals November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Number 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t Nu m b e r s Mo n i t o r i n g We l l C o d e Sa m p l e D a t e An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Ir o n Le a d Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zin c 1*10 700 4*2 10 1*1,000 300 15 50 1 100 20 20 0.2*0.3*1,000 6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 MW-G 4-May-11 148 0.08J 0.19J 1.07JB 14.6 12.6 1.15J 32.5J 8.16J 6.12J 4.01J MW-G 9-Nov-11 0.14J 2.75J 420 0.12J 4.99J 0.87JB 3.17J 2.79J 2.51J MW-G 9-May-12 4.45J 302 2.19J 0.86J 4.40J 1.41J 4.25J 13.7B MW-G 29-Nov-12 2.03J 385 0.15J 2.14J 0.96J 0.12J 3.69J 3.03J 2.79J 2.86J MW-G 10-May-13 354 0.18J 5.08J 1.19J 0.14J 2.43J 1.51J 2.11J 5.14J MW-G 6-Nov-13 5.44J 346 3.09J 0.81J 0.09J 4.81J 2.75J 12.4JB 2.49JB MW-G 8-May-14 4.42J 373 0.20J 6.69J 1.31J 0.27J 5.00J 2.95J 7.99J 4.08J MW-G 4-Nov-14 12.3 480 0.26J 7.02J 2.57J 0.61J 9.32J 2.96J 0.17J 10.6JB 6.72J MW-G 5-May-15 2.13J 340 0.18J 5.62J 2.30J 0.37J 5.29J 4.79J 4.85J 4.16J MW-G 28-Oct-15 4.45J 387 0.14J 1.23J 5.01J 0.74J 0.19J 4.88J 2.09CN,J 2.76J 3.69B-01,J MW-G 19-May-16 3.19J 412 0.15J 1.31J 6.07J 0.89J 0.26J 5.07J 4.72J 4.62J MW-G (dup)19-May-16 0.31B-01,J 3.51J 417 0.11J 1.05J 5.37J 0.09J 3.64J 2.55J 2.08J MW-G 3-Nov-16 6.65J 418 0.09J 1.23J 3.67J 1.00J 5.36J 5.04J MW-H 5-May-11 62.2J 0.31J 9.05J 2.05J 6.94J 1.68J 6.89J 0.08J 9.85J 16.9 MW-H 9-Nov-11 0.14J 32.6J 0.13J 2.69J 0.71J 2.93J 0.59J 2.83J 7.37J MW-H 9-May-12 44.9J 0.13J 3.58J 0.89J 4.23J 1.17J 3.17J 5.79J 12.1B MW-H 29-Nov-12 37.8J 1.68J 0.25J 1.62J 0.29J 1.13J 2.89J 5.65J MW-H 9-May-13 27.9J 1.94J 0.21J 1.33J 0.22J 1.1J 2.68J 5.45J MW-H 7-Nov-13 72J 0.38J 4.94J 2.51J 6.39J 2.65J 5.96J 15.4J 16.4B MW-H 8-May-14 67.0J 0.47J 3.48J 1.73J 6.34J 2.12J 4.49J 9.00J 14.2 MW-H 6-Nov-14 49.8J 0.17J 2.04JB 0.95J 3.67J 0.95J 2.97J 5.33J 7.55JB MW-H 5-May-15 1.20J 52.5J 0.20J 0.50JB 0.89J 4.34J 1.27J 2.94J 4.63J 7.65J MW-H 29-Oct-15 1.85J 78.1J 0.48J 8.22J 2.56J 8.56J 2.51J 7.19J 2.57J 4.20CN,J 0.09J 14.7J 22.9B-01 MW-H 19-May-16 1.24J 52.3J 0.25J 4.01J 1.16J 3.62J 1.26J 3.27J 1.52J 8.62J 9.43J MW-H 3-Nov-16 67.8J 0.33J 5.81J 1.96J 5.86J 1.78J 5.59J 2.87J 10.7J 15.7 MW-H Deep 5-May-11 57.5J 0.22J 4.33JB 0.82J 4.35J 1.57J 2.65J 7.23J 7.84J MW-H Deep 9-Nov-11 29.2J 0.05J 1.17J 0.71J 2.07J 0.45J 1.62J 2.55J MW-H Deep 9-May-12 0.74J 49.6J 0.18J 3.41J 0.95J 5.67J 1.42J 2.91J 7.53J 13.2B MW-H Deep 28-Nov-12 52.4J 1.28J 1.59J 0.96J 2.44J 2.62J MW-H Deep 9-May-13 0.83J 43J 0.47J 2.2J 0.22J 1.45J 6.98J MW-H Deep (dup)9-May-13 0.24J 44.1J 1.05J 0.19J 1.72J 0.22J 1.4J 3.34J 13.3 MW-H Deep 7-Nov-13 40.9J 0.28J 1.85J 0.23J 1.39J 12.1J 5.29JB MW-H Deep 8-May-14 55.0J 0.10J 0.32J 2.03J 0.37J 1.63J 3.89J MW-H Deep 6-Nov-14 49.9J 0.08J 1.33JB 1.45J 0.19J 2.00J 4.18J 9.25JB MW-H Deep (dup)6-Nov-14 49.4J 1.54JB 0.50J 1.74J 0.27J 1.93J 6.32JB MW-H Deep 5-May-15 1.84J 44.4J 0.29J 2.69J 0.38J 1.97J 2.00J 2.00J MW-H Deep (dup)5-May-15 1.42J 39.8J 0.13J 1.08J 0.31J 2.88J 0.37J 2.26J 3.23J MW-H Deep 29-Oct-15 45.9J 0.64J 1.49JB 0.23J 1.57J 3.82CN,J 4.80J 3.06B-01,J MW-H Deep 19-May-16 1.10B-01,J 55.9J 0.12J 0.87J 2.36J 0.45J 1.33J 0.10J 5.45J 2.27J MW-H Deep 3-Nov-16 54.7J 1.14J 0.25J 0.89J MW-I 4-May-11 26.3J 0.16J 4.87JB 0.29J 0.94J 0.44J 2.44J 4.15J 3.14J MW-I 9-Nov-11 0.30JB 12J 0.12JB 0.66J 0.11J 0.81J 1.24J 0.28J 3.36J MW-I 9-May-12 0.25J 17.6J 0.33J 1.80J 0.20J 1.65J 0.27J 3.01J 3.53J 11.5B MW-I (dup)9-May-12 16.2J 0.31J 1.71J 1.11J 0.23J 2.39J 8.56JB MW-I 28-Nov-12 0.30J 14.3J 0.73J 0.44J 0.94J 2.49J 1.05JB MW-I 10-May-13 0.49J 17.8J 0.22J 0.07J 1.38JB 0.34J 0.79J 0.31J 1.32J 3.39J MW-I 7-Nov-13 14.2J 0.12J 0.21J 0.59J 0.20J 1.41J 6.83J 2.61JB MW-I 7-May-14 13.9J 0.13J 3.44JB 0.77J 0.19J 1.31J 1.31J 1.53JB MW-I 5-Nov-14 20.7J 0.16J 0.05J 0.82J 0.26J 0.90J 0.31J 1.56J 2.55JB 1.70J MW-I 5-May-15 0.50J 15.4J 0.17J 1.81J 1.71J 0.33J 1.85J 1.86J MW-I 29-Oct-15 21.1J 0.21J 1.10J 0.62J 0.28J 1.57J 4.40CN,J 4.71J 4.32B-01,J MW-I 19-May-16 0.37B-01,J 20.7J 0.20J 1.07J 0.33J 1.75J 3.09J 2.42J MW-I 3-Nov-16 24.2J 0.29J 0.07J 1.30J 0.55J 0.84J 1.43J 3.58J MW-J 4-May-11 38.4J 0.31J 6.14J 2.01J 3J 2.4J 5.47J 0.08J 13J 11.2 MW-J 9-Nov-11 0.16JB 35.3J 1.55J 0.44J 1.26J 0.27JB 5.84J 0.12J 5.98J MW-J 9-May-12 15.2J 1.64J 0.38J 1.41J 0.52J 2.76J 3.35J 15B MW-J 29-Nov-12 16.4J 1.39J 0.30J 2.54J 0.30J 1.20J 3.93J 4.89J MW-J 8-May-13 10.6J 0.86J 0.31J 1.16J 0.27J 1.38J 4.81J 2.7J MW-J 6-Nov-13 17.8J 0.79J 1.43J 0.91J 2.28J 21.4JB 4.73JB MW-J 7-May-14 31.6J 3.02JB 0.52J 1.41J 0.83J 2.03J 3.40J 4.24JB MW-J 4-Nov-14 27.4J 0.17J 1.45J 1.24J 2.00J 1.16J 3.54J 9.58JB 6.38JB MW-J 6-May-15 10.7J 1.38J 0.51J 2.00J 0.63J 2.48J 3.51J 3.36J MW-J 28-Oct-15 1.21J 11.0J 0.58B-01,J 0.45J 1.64J 0.38J 2.06J 3.59CN,J 2.47J 5.91J MW-J 18-May-16 0.96J 28.2J 0.25J 3.11J 1.40J 1.62J 1.99J 3.55J 0.90J 12.0J 6.86J MW-J 2-Nov-16 32.2J 0.28J 4.86J 2.51J 2.38J 2.74J 5.69J 1.66J 14.9J 11.0 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 4 of 14 January 2017 Table 5a Detected Groundwater Constituents - Metals November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Number 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t Nu m b e r s Mo n i t o r i n g We l l C o d e Sa m p l e D a t e An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Ir o n Le a d Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zin c 1*10 700 4*2 10 1*1,000 300 15 50 1 100 20 20 0.2*0.3*1,000 6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 MW-K 4-May-11 25.2J 0.26J 6.52J 1.57J 2.25J 1.53J 3.65J 11J 7.96J MW-K 9-Nov-11 17.7J 0.14JB 2.51J 0.73J 3.67J 0.73J 2.07J 0.07J 4.96J 4.09J MW-K 9-May-12 35.2J 0.22J 7.59J 2.98J 3.66J 1.92J 6.06J 13.8J 20.1B MW-K 28-Nov-12 16.1J 1.35J 0.28J 0.74J 0.28J 1.42J 2.53J 4.44JB MW-K 8-May-13 1.02JB 17J 0.15J 1.91J 0.71J 1.33J 0.69J 2.24J 6.05J 5.28J MW-K 6-Nov-13 13.9J 2.68J 0.76J 1.26J 0.43J 1.94J 23JB 4.68JB MW-K 7-May-14 17.5J 0.12J 4.27JB 0.49J 1.30J 0.70J 1.83J 3.49J 2.46JB MW-K 5-Nov-14 13.3J 0.13J 1.21J 0.53J 1.20J 0.43J 1.97J 3.82JB 3.19J MW-K 5-May-15 1.16J 1.42J 15.3J 0.14J 0.49J 1.99J 0.71J 2.54J 4.66J 2.95J MW-K 29-Oct-15 0.35J 26.2J 0.19J 2.54B-01,J 1.16J 2.41J 1.04J 4.17J 2.87CN,J 6.18J 5.60J MW-K 18-May-16 1.43J 17.8J 0.16J 3.25J 0.89J 1.03J 0.83J 2.28J 1.18J 8.68J 5.35J MW-K 2-Nov-16 17.8J 0.16J 2.60J 0.87J 0.94J 0.72J 2.04J 1.78J 4.01J MW-K (dup)2-Nov-16 4.05J 1.31J 0.63J 0.18J 1.17J 1.08J 2.18J MW-L 4-May-11 45.7J 2.67JB 0.35J 0.7J 0.2J 1.64J 3.96J MW-L 9-Nov-11 0.19J 40.9J 0.06J 1.64J 0.41J 0.93J 0.37J 1.49J 3.72J MW-L 9-May-12 43.8J 1.20J 0.52J 0.09J 1.27J 1.93J 2.16JB MW-L 28-Nov-12 0.82J 23.0J 1.74J 0.32J 0.39J 2.21J 6.47J 3.75J MW-L 9-May-13 1.24JB 43.5J 1.12J 0.49J 0.83J 0.22J 1.95J 2.9J 3.29J MW-L 7-Nov-13 49.2J 0.19J 0.88J 1.20J 2.49J 0.85J 3.62J 11.8J 11.5B MW-L 8-May-14 43.7J 0.07J 0.67J 0.14J 1.28J 1.95J MW-L 5-Nov-14 38.6J 0.76J 0.14J 1.32J 2.44J 2.28JB MW-L 6-May-15 40J 0.81J 0.16J 1.27J 2.23J MW-L 28-Oct-15 33.5J 1.05J 0.29J 0.31J 1.07J 4.04CN,J 2.87J 6.06B-01-J MW-L 19-May-16 38.4J 0.88J 1.01J 2.23J 1.48J MW-L 2-Nov-16 35.2J 1.00J 1.04J 2.46J MW-L Deep 4-May-11 0.44J 56.8J 0.34J 14.7 2.86J 3.62J 3.39J 13.6J 15.2J 12.7 MW-L Deep 9-May-12 0.62J 23J 2.03J 0.83J 1.60J 0.68J 3.14J 8.53J 7.99JB MW-L Deep 10-May-13 0.41J 19.2J 0.24J 1.89J 0.27J 1.63J 2.08J 21.8 MW-L Deep 8-May-14 27.9J 1.34JB 0.11J 1.32J 6.06J MW-L Deep 6-May-15 0.36J 23.1J 0.90J 1.24J 1.50J 2.45J 45.1 MW-L Deep 29-Oct-15 0.58J 23.0J 0.47B-01,J 1.23J 0.09J 1.62J 3.73CN,J 81.1 MW-L Deep 19-May-16 0.46J 30.8J 0.44J 1.87J 0.17J 1.27J 4.59J 116 MW-M 5-May-11 0.92J 64.2J 0.56J 2.68J 2.64J 15.6 4.83J 5.84J 0.14J 18.2J 15.2 MW-M 9-May-12 40.3J 0.26J 2.46J 1.38J 8.56J 3.07J 3.80J 11.8J 15.2B MW-M 10-May-13 34.9J 0.16J 1.44JB 0.69J 2.21J 0.5J 1.68J 2.2J MW-M 8-May-14 37.1J 0.10J 0.80J 0.30J 2.00J 0.63J 1.91J 2.42J MW-M 5-May-15 1.93J 39.4J 0.88J 2.02J 0.51J 2.18J 4.07J 1.71J MW-M 29-Oct-15 38.9J 0.10J 1.56B-01,J 0.39J 2.10J 0.62J 2.10J 3.09CN,J 1.78J 4.96J MW-M 18-May-16 0.92J 38.8J 0.60J 0.46J 1.60J 0.58J 1.47J 6.84J 1.54J MW-X 4-May-11 0.32J 51.5J 0.21J 7.8J 2.79J 2.91J 1.49JB 11J 0.08J 12.2J 12.3 MW-X 9-Nov-11 23.1J 0.22JB 2.97J 1.21J 2.46J 1.77J 4.34J 0.07J 10.5J 6.75J MW-X 9-May-12 34.9J 1.52J 1.37J 5.63J 8.77JB MW-X 29-Nov-12 29.3J 1.80J 0.33J 1.31J 0.25J 4.74J 5.19J 2.17JB MW-X 29-Nov-12 32.0J 3.20J 0.75J 1.54J 0.39J 5.79J 5.63J 4.82JB MW-X 8-May-13 1.53JB 35.4J 0.77J 0.73J 1.8J 0.24J 6.37J 3.12J 4.55J MW-X 6-Nov-13 24.1J 1.12J 0.35J 1.04J 0.32J 4.27J 18.2JB 3.96JB MW-X 7-May-14 37.0J 0.05J 4.91JB 0.73J 1.25J 0.44J 5.74J 4.70J 3.84JB MW-X 5-Nov-14 26.8J 2.58JB 0.36J 0.97J 0.19J 3.67J 11.2J 2.10JB MW-X 6-May-15 28.9J 1.86J 0.32J 2.68J 0.21J 4.33J 2.51J 1.42J MW-X 29-Oct-15 27.8J 2.08B-01,J 1.29J 4.65J 3.24CN,J 1.74J MW-X 18-May-16 0.86J 32.0J 1.71J 0.52J 0.68J 0.34J 4.38J 6.50J 2.22J MW-X 2-Nov-16 32.3J 1.70J 1.60J 0.29J 3.56J 2.69J Notes: 1. All units are in micrograms per liter (parts per billion). 2. Monitoring wells MW-3 Deep, -L Deep, -and -M are sampled annually during the spring event. 3. * - Groundwater Protection Standard 4. (dup) - Duplicate 5. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 6. B/B-01 - Indicates constituent was detected in the batch blank above the method detection limit. 7. CN - Detected silver concentrations were determined to be the result of contamination from the preservative acid used. 8. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 9. MW-9 was removed from the monitoring program in November 2012. 10. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. - Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard - Indicates the result is below the detection limit or not analyzed . 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 5 of 14 January 2017 Table 5b Detected Groundwater Constituents - Volatile Organic Compounds November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l e D a t e Ac e t o n e Be n z e n e 2-B u t a n o n e 2- H e x a n o n e Ca r b o n D i s u l f i d e Ch l o r o b e n z e n e Ch l o r o e t h a n e Ch l o r o f o r m 1, 2 - D i c h l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e 1,1 - D i c h l o r o e t h a n e 1,2 - D i c h l o r o e t h a n e 1,1 - D i c h l o r o e t h e n e 1, 2 - D i c h l o r o p r o p a n e cis - 1 , 2 - D i c h l o r o e t h e n e Et h y l b e n z e n e Me t h y l e n e C h l o r i d e 4- M e t h y l - 2 - P e n t a n o n e tra n s - 1 , 2 - D i c h l o r o e t h e n e Te t r a c h l o r o e t h e n e To l u e n e To t a l X y l e n e s 1, 1 , 1 - T r i c h l o r o e t h a n e Tr i c h l o r o e t h e n e Tri c h l o r o f l u o r o m e t h a n e Vin y l C h l o r i d e bi s ( 2 - E t h y l h e x y l ) P h t h a l a t e 6,000 1 4,000 40*700 50 3,000 70 20 6 6 0.4 7 0.6 70 600 5 560*100 0.7 600 500 200 3 2,000 0.03 3 100 1 100 50 100 3 10 5 5 1 5 1 5 1 5 1 1 100 5 1 1 5 1 1 1 1 15 CD-1s 3-May-11 CD-1s 8-Nov-11 CD-1s 7-May-12 CD-1s 27-Nov-12 0.4J 0.2J CD-1s 7-May-13 CD-1s 5-Nov-13 CD-1s 6-May-14 CD-1s 4-Nov-14 CD-1s 5-May-15 CD-1s 27-Oct-15 CD-1s 17-May-16 CD-1s 1-Nov-16 CD-1d 3-May-11 CD-1d 8-Nov-11 CD-1d 7-May-12 CD-1d 27-Nov-12 CD-1d 7-May-13 CD-1d 5-Nov-13 CD-1d 6-May-14 CD-1d 4-Nov-14 CD-1d 5-May-15 CD-1d 27-Oct-15 CD-1d 17-May-16 CD-1d 1-Nov-16 CD-4 Rep 3-May-11 CD-4 Rep (dup)3-May-11 CD-4 Rep 8-Nov-11 CD-4 Rep 8-May-12 CD-4 Rep 28-Nov-12 0.3J CD-4 Rep 9-May-13 CD-4 Rep 7-Nov-13 0.6J CD-4 Rep 6-May-14 CD-4 Rep 4-Nov-14 CD-4 Rep 6-May-15 CD-4 Rep 27-Oct-15 CD-4 Rep 17-May-16 CD-4 Rep 2-Nov-16 CD-6 3-May-11 0.7J 0.9J CD-6 8-Nov-11 1.7J 1.4 0.6J CD-6 8-May-12 2.2J 1.7 0.9J CD-6 28-Nov-12 2.8J 0.4J 1.2 0.8J CD-6 9-May-13 3.6J 1.6 1.3 CD-6 7-Nov-13 36J 1.2 0.6J 1.4J 7.8 8.4 0.6J 1.2 57 0.5J 4.6 2.4 1.7 CD-6 6-May-14 5.2 0.3J 1.1 1.2 CD-6 4-Nov-14 4.7J 0.3J 1.4 1.2 CD-6 6-May-15 3.7J 1.5 1.1 CD-6 27-Oct-15 3.1J 1.0 0.9J CD-6 17-May-16 1.5J 0.5J 0.7J CD-6 1-Nov-16 2.2J 0.6J 0.9J AMW-1s 3-May-11 0.5J 1J 0.9J 9.2 1J 15 0.7J 3.0 3.8 AMW-1s 8-Nov-11 0.5J 0.7J 0.9J 11 0.7J 15 0.7J 3.1 3.1 AMW-1s 7-May-12 0.7J 1J 1 12 0.8J 16 0.8J 3.5 3.9 AMW-1s 28-Nov-12 0.6J 0.8J 1.1 10 0.7J 14 0.6J 3.2 3.4 AMW-1s 8-May-13 0.9J 0.9J 1.4 13 0.9J 18 1J 4.1 4.3 AMW-1s 6-Nov-13 0.9J 0.9J 1.3 13 0.9J 15 1J 3.8 3.9 AMW-1s 7-May-14 0.9J 0.9J 1.1 9.8 0.7J 12 1.4 3.6 2.8 AMW-1s 5-Nov-14 0.6J 1.0J 9.0 0.5J 10 2.5 2.8 AMW-1s 7-May-15 0.8J 1.3 8.1 0.5J 9.9 0.9J 3.1 2.6 AMW-1s 29-Oct-15 0.4J 0.8J 0.8J 5.8 6.1 1.6 1.4 AMW-1s 18-May-16 0.6J 0.5J 0.9J 5.7 7.6 0.6J 1.8 1.7 AMW-1s 2-Nov-16 0.2J 1.1J 24 2.8J 15 10 7.1 0.9J AMW-1d 3-May-11 1.1 2J 1.1J,B 0.8J 24 1.9J 28 0.3J 4.2 4.7 0.3J AMW-1d 8-Nov-11 1.2 1.4J 0.8J 28 1.8J 30 0.5J 0.6J 5.8 0.3J 0.4J AMW-1d 7-May-12 1.2 1.7J 0.9J 27 1.8J 35 0.4J 0.4J 1.7 4.8 0.4J AMW-1d 28-Nov-12 1.2 5.0J 1.3J 0.9J 29 1.9J 36 0.4J 0.6J 2.0 5.0 AMW-1d 8-May-13 1.1 2J 1.7 26 0.2J 2J 0.6J 40 0.6J 6.2 0.4J AMW-1d 6-Nov-13 1.1 2.6J 0.8J 29 2.2J 38 0.4J 0.5J 5.2 0.5J AMW-1d 7-May-14 1.2 2.2J 1.0 30 2.3J 36 0.6J 1.6 7.3 0.6J AMW-1d 5-Nov-14 1.3 1.7J 1.0J 31 1.3J 13 0.5J 0.7J 3.2 0.3J 29 AMW-1d 7-May-15 1.2 1.2J 1.1 24 0.7J 7.1 0.4J 1.2 1.9 18 AMW-1d 29-Oct-15 1.0 2.0J 0.7J 23 2.8J 20 AMW-1d 18-May-16 1.1 0.9J 23 9.7 1.6 8.0 AMW-1d 3-Nov-16 1.4 2.2J 1.0 26 0.8J 7.0 0.5J 13 AMW-2s 3-May-11 0.8J 10 1J 2.8J 2.5 5.4 3 0.7J AMW-2s 8-Nov-11 0.8J 11 1J 3.8J 2.9 5 3.2 0.8J AMW-2s 8-May-12 0.8J 12 1.2J 4.3J 2.7 5.8 3.8 0.9J AMW-2s 29-Nov-12 0.7J 12 1.1J 4.9J 2.2 6.4 4.1 0.8J AMW-2s 9-May-13 9 0.8J 4.7J 1.4 5.2 3.4 0.6J AMW-2s 6-Nov-13 10 0.9J 4.8J 1.3 4.9 3.4 0.7J AMW-2s 7-May-14 0.5J 12 0.8J 5.2 1.2 4.6 3.3 0.5J AMW-2s 5-Nov-14 12 0.9J 6.4 0.9J 5.5 4.2 0.6J AMW-2s 6-May-15 9.3 0.6J 5.5 0.6J 4.2 3.1 0.4J AMW-2s 28-Oct-15 8.4 5.7 0.7J 3.3 2.6 AMW-2s (dup)28-Oct-15 8.4 0.7J 5.9 0.7J 3.7 2.9 AMW-2s 17-May-16 8.5 6.4 0.7J 3.5 3.0 AMW-2s 1-Nov-16 10 0.8J 8.0 0.9J 4.1 3.2 1302-MSWLF- & 1302-CDLF-1998 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 6 of 14 January 2017 Table 5b Detected Groundwater Constituents - Volatile Organic Compounds November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l e D a t e Ac e t o n e Be n z e n e 2-B u t a n o n e 2- H e x a n o n e Ca r b o n D i s u l f i d e Ch l o r o b e n z e n e Ch l o r o e t h a n e Ch l o r o f o r m 1, 2 - D i c h l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e 1,1 - D i c h l o r o e t h a n e 1,2 - D i c h l o r o e t h a n e 1,1 - D i c h l o r o e t h e n e 1, 2 - D i c h l o r o p r o p a n e cis - 1 , 2 - D i c h l o r o e t h e n e Et h y l b e n z e n e Me t h y l e n e C h l o r i d e 4- M e t h y l - 2 - P e n t a n o n e tra n s - 1 , 2 - D i c h l o r o e t h e n e Te t r a c h l o r o e t h e n e To l u e n e To t a l X y l e n e s 1, 1 , 1 - T r i c h l o r o e t h a n e Tr i c h l o r o e t h e n e Tri c h l o r o f l u o r o m e t h a n e Vin y l C h l o r i d e bi s ( 2 - E t h y l h e x y l ) P h t h a l a t e 6,000 1 4,000 40*700 50 3,000 70 20 6 6 0.4 7 0.6 70 600 5 560*100 0.7 600 500 200 3 2,000 0.03 3 100 1 100 50 100 3 10 5 5 1 5 1 5 1 5 1 1 100 5 1 1 5 1 1 1 1 15 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 AMW-2d 3-May-11 5.6 0.9J 1.4J 2 4.0 2.3 1.4 AMW-2d 8-Nov-11 8.8 1J 1.9J 1.2 6.5 2.8 1.3 AMW-2d 8-May-12 9.7 1J 2J 1 6.1 3.1 1.1 AMW-2d 28-Nov-12 11 1.2J 2.5J 6.6 3.2 0.7J AMW-2d 9-May-13 12 1.2J 4.6J 1.1 7.8 4 1.2 AMW-2d 6-Nov-13 9.4 0.6J 9.1 0.7J 2.9 1.9 0.6J AMW-2d 7-May-14 0.7J 19 1.8J 6.0 2.0 8.5 5.6 1.4 AMW-2d 5-Nov-14 15 5.7 1.4 4.7 4.2 0.9J AMW-2d 6-May-15 19 1.5J 8.4 1.3 9.8 6.3 0.8J AMW-2d 28-Oct-15 14 0.8J 6.3 1.3 4.3 3.7 0.6J AMW-2d 17-May-16 0.5J 0.3J 17 1.0J 9.2 1.3 7.6 5.2 0.7J AMW-2d 2-Nov-16 0.4J 0.5J 5.0 6.2 2.0 1.2 MW-1 3-May-11 0.7J MW-1 8-Nov-11 0.4J MW-1 8-May-12 0.4J 0.7J MW-1 27-Nov-12 0.4J 0.8J MW-1 9-May-13 MW-1 5-Nov-13 1.0J 0.4J MW-1 7-May-14 0.4J 0.4J 2.4J 0.9J 0.5J 0.4J MW-1 (dup)7-May-14 0.3J 0.4J 2.4J 0.9J 0.5J 0.4J MW-1 3-Nov-14 1.3J 0.4J 0.4J MW-1 5-May-15 0.4J 1.1J 0.4J MW-1 27-Oct-15 0.5J MW-1 18-May-16 1.2J 0.6J MW-1 1-Nov-16 1.0J MW-3 4-May-11 7.4 1.4J 0.8J 13 4 1.1 MW-3 9-Nov-11 12 1.7J 1.8J 0.7J 16 5.3 1.2 MW-3 (dup)9-Nov-11 13 2J 1.8J 0.7J 15 5.3 1.6 MW-3 8-May-12 9.6 1.7J 1.2J 0.5J 17 5.4 1.3 MW-3 28-Nov-12 12 1.4J 1.9J 0.9J 15 5.2 MW-3 9-May-13 10 1.4J 1.7J 0.6J 18 5.7 1.1 MW-3 7-Nov-13 12 1.5J 1.7J 0.6J 15 5.1 1.0 MW-3 8-May-14 15 2.0J 2.6J 0.7J 17 6.1 1.0 MW-3 6-Nov-14 16 1.8J 3.6J 0.7J 18 7.4 1.2 MW-3 6-May-15 14 0.8J 3.1J 0.6J 17 5.9 0.9J MW-3 28-Oct-15 13 1.4J 3.8J 13 5.2 0.8J MW-3 18-May-16 13 1.3J 4.1J 0.6J 15 6.0 0.8J MW-3 2-Nov-16 14 2.4J 4.8J 0.6J 14 5.7 1.2 MW-3 Deep 4-May-11 0.5J MW-3 Deep 8-May-12 0.4J MW-3 Deep 10-May-13 1J 0.6J 0.4J MW-3 Deep 8-May-14 0.4J MW-3 Deep 6-May-15 1.2J 0.4J 0.4J MW-3 Deep 28-Oct-15 1.4J 0.4J MW-3 Deep 19-May-16 1.2J MW-9 3-May-11 0.8J MW-9 9-Nov-11 1.1 MW-9 9-May-12 1.4 MW-A 3-May-11 7.4 1J 4.7J 12 14 2.2 2.2 110 0.8J 0.4J 3.9 3.1J 3.2 0.7J MW-A 9-Nov-11 9.2 1.4J 6.5J 16 18 2.8 2.4 120 2 0.6J 6.5 5.2 3.8 1J MW-A 9-May-12 8.8 1.1J 6.5J 17 26 3.8 0.5J 2 110 0.9J 0.4J 6.5 2.6J 0.5J 4.5 0.2J 1.1 MW-A 27-Nov-12 9.3 1.6J 6.9J 15 25 3.9 0.6J 2.2 130 0.4J 0.5J 0.5J 4.7 1.7J 0.4J 4.4 0.8J MW-A 7-May-13 9.1 1.3J 5.1J 22 23 3 0.4J 2.4 120 0.6J 0.8J 0.5J 6.2 0.3J 8.0 4.3 MW-A 5-Nov-13 11 1.4J 5.7J 0.4J 25 22 4.1 130 1.4 6.2 6.0 3.8 1.0 MW-A 6-May-14 11 1.3J 5.6J 0.3J 28 18 3.6 0.2J 2.1 120 0.7J 4.6 0.4J 5.3 0.4J 5.8 3.3 1.0 MW-A 4-Nov-14 9.5 1.6J 5.6J 0.3J 31 21 2.6 130 0.4J 1.1 0.5J 5.7 2.0J 4.5 1.0J MW-A 5-May-15 9.3 1.4J 5.0J 0.3J 24 16 2.5 2.1 110 0.8J 0.8J 0.5J 5.6 0.4J 5.3 3.6 0.6J MW-A 27-Oct-15 9.1 1.4J 5.4J 28 15 2.3 110 0.7J 0.8J 5.9 0.3J 4.4J 3.4 0.7J MW-A 17-May-16 9.7 1.5J 31 15 1.3 2.2 120 1.1 1.4 4.8 0.6J 5.2 3.7 0.8J MW-A 1-Nov-16 11 1.6J 5.7J 36 17 1.6 2.6 140 0.7J 1.4 0.5J 5.7 4.7J 3.8 0.9J MW-B 3-May-11 MW-B 8-Nov-11 MW-B 8-May-12 MW-B 28-Nov-12 0.9J MW-B 9-May-13 MW-B 5-Nov-13 MW-B 7-May-14 MW-B 3-Nov-14 MW-B 5-May-15 MW-B 28-Oct-15 MW-B 18-May-16 MW-B 2-Nov-16 MW-C 3-May-11 MW-C 8-Nov-11 1.4J MW-C 8-May-12 MW-C 28-Nov-12 0.6J 0.5J MW-C 8-May-13 MW-C 5-Nov-13 11 MW-C 6-May-14 MW-C 4-Nov-14 0.3J 4.6J MW-C 6-May-15 MW-C 28-Oct-15 0.7J MW-C 17-May-16 MW-C 1-Nov-16 1.4J 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 7 of 14 January 2017 Table 5b Detected Groundwater Constituents - Volatile Organic Compounds November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l e D a t e Ac e t o n e Be n z e n e 2-B u t a n o n e 2- H e x a n o n e Ca r b o n D i s u l f i d e Ch l o r o b e n z e n e Ch l o r o e t h a n e Ch l o r o f o r m 1, 2 - D i c h l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e 1,1 - D i c h l o r o e t h a n e 1,2 - D i c h l o r o e t h a n e 1,1 - D i c h l o r o e t h e n e 1, 2 - D i c h l o r o p r o p a n e cis - 1 , 2 - D i c h l o r o e t h e n e Et h y l b e n z e n e Me t h y l e n e C h l o r i d e 4- M e t h y l - 2 - P e n t a n o n e tra n s - 1 , 2 - D i c h l o r o e t h e n e Te t r a c h l o r o e t h e n e To l u e n e To t a l X y l e n e s 1, 1 , 1 - T r i c h l o r o e t h a n e Tr i c h l o r o e t h e n e Tri c h l o r o f l u o r o m e t h a n e Vin y l C h l o r i d e bi s ( 2 - E t h y l h e x y l ) P h t h a l a t e 6,000 1 4,000 40*700 50 3,000 70 20 6 6 0.4 7 0.6 70 600 5 560*100 0.7 600 500 200 3 2,000 0.03 3 100 1 100 50 100 3 10 5 5 1 5 1 5 1 5 1 1 100 5 1 1 5 1 1 1 1 15 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 MW-D 3-May-11 5.5 3.2J 1.9 1.9J 37 0.7J 1.6J 5.5 0.8J MW-D 8-Nov-11 5.7 3.2J 2.9 1.8J 57 0.7J 0.4J 0.9J 1.5J 3.9 0.9J MW-D 8-May-12 7 0.3J 2.7J 6.2 1.3J 56 1 1J 1.7J 5.3 0.8J MW-D 27-Nov-12 6.5 0.3J 1.1J 6.4 1.3J 54 1.5 0.7J 0.2J 5.3 4.0 0.6J MW-D 8-May-13 6.8 0.4J 1.6J 8.4 1.2J 56 0.8J 1.2 2.7J 5.9 0.7J MW-D 5-Nov-13 7.2 0.5J 1.8J 9.3 1.0J 57 0.8J 1.8J 4.6 0.9J MW-D 6-May-14 5.1 0.4J 1.1J 7.8 0.7J 39 3.3J 3.9 0.6J MW-D 4-Nov-14 6.9 0.5J 0.9J 10 0.9J 53 0.2J 0.4J 1.5J 4.6 0.6J MW-D 5-May-15 5.9 0.6J 7.3 0.5J 38 0.2J 1.8J 3.3 0.5J MW-D 28-Oct-15 5.3 0.9J 8.1 0.5J 37 1.5J 2.7 0.6J MW-D 17-May-16 5.0 0.7J 9.9 39 1.7J 2.8 MW-D 2-Nov-16 6.5 0.8J 1.3J 12 0.5J 48 3.2J 2.6 1.1 MW-E Rep 4-May-11 6 2.5J 4.5J 14 20 1J 1J 75 0.9J 3.6 6.3 MW-E Rep 8-Nov-11 3.3 0.7J 2.1J 4.2J 11 20 0.8J 1.1 54 0.8J 2.2 5 MW-E Rep 8-May-12 2.5 2.4J 5.7J 13 23 1.1 1.1 47 0.4J 0.9J 0.3J 1.8 6.6 MW-E Rep 8-May-13 1.3 2.78J 3.7J 14 19 0.7J 1.2 21 0.7J 0.5J 4.4 MW-E Rep 5-Nov-13 2.3 3.2 3.7J 16 19 1.2 41 0.7J 1.0 7.6 MW-E Rep 6-May-14 2.9 3.2 2.9J 16 14 1.0 1.0 53 0.7J 0.2J 1.4 9.3 MW-E Rep 4-Nov-14 1.5 4.1 3.6J 18 15 1.1 43 0.7J 1.0 7.5 MW-E Rep 5-May-15 3.4J 0.8J 3.1 4.2J 0.3J 15 8.8 1.0J 1.1 25 0.4J 0.5J 3.8 MW-E Rep 27-Oct-15 1.0 3.9 5.1J 0.3J 15 9.0 1.1 27 0.4J 0.6J 4.3 MW-E Rep 18-May-16 0.8J 2.3J 7.6J 8.2 0.9J 0.9J 12 3.2 MW-E Rep 1-Nov-16 0.6J 3.2 8.0J 15 11 1.1 18 0.5J 4.5 MW-E Deep 4-May-11 1.9 11 3.9 32 0.9J 1.1 1J 0.5J 1.8 MW-E Deep 8-Nov-11 1.5 0.6J 9.5J 3.9 34 0.8J 1.3 1.1J 0.6J 1.3 MW-E Deep 8-May-12 1 0.5J 12 4.3 29 0.9J 1.2 0.4J 0.5J 0.3J 0.6J MW-E Deep 27-Nov-12 0.9J 1.2J 14 4.5 30 0.9J 1.1 1.0J 0.4J 0.4J 0.9J MW-E Deep 8-May-13 0.8J 0.7J 6.8J 4.1 30 0.8J 1.3 0.5J 0.4J 0.5J MW-E Deep 6-Nov-13 1.2 0.8J 12 5.1 26 0.7J 0.4J 1.2 MW-E Deep 6-May-14 85J 2.6 18J 15J 1.0J 9.5J 9.3 8.9 0.8J 0.7J 2.0J 10J 1.2 3.1J 0.4J MW-E Deep 4-Nov-14 18J 0.7J 4.3J 5.4J 0.9J 17 4.1 10 0.6J 0.3J 3.4 1.0J MW-E Deep 5-May-15 0.7J 1.1J 14 5.9 8.5 0.7J 1.9 1.4J MW-E Deep 27-Oct-15 0.4J 0.9J 16 4.9 7.0 0.6J 0.8J 1.0J MW-E Deep 18-May-16 0.4J 0.8J 11 4.2 1.0J 0.5J 0.5J 0.5J 0.8J MW-E Deep 1-Nov-16 0.6J 1.1J 26 5.9 1.7J 0.8J 0.7J 4.8J MW-F 3-May-11 MW-F 8-Nov-11 MW-F 8-May-12 MW-F 28-Nov-12 0.6J MW-F 9-May-13 MW-F 5-Nov-13 MW-F 7-May-14 MW-F 3-Nov-14 MW-F 5-May-15 3.1J MW-F 27-Oct-15 0.7J MW-F 17-May-16 MW-F 2-Nov-16 0.6J MW-G 3-May-11 0.6J 1.6J MW-G 8-Nov-11 1.5 2.1J MW-G 8-May-12 0.6J 1.1J 0.3J MW-G 28-Nov-12 1.6J 1.1 0.7J MW-G 9-May-13 2.8J 0.5J 1.6J MW-G 5-Nov-13 3.1J 2.3J 0.9J 0.4J 1.5 0.4J MW-G 7-May-14 0.2J 2.4J 0.8J 0.4J 1.4 0.5J MW-G 3-Nov-14 0.3J 2.6J 1.0J 0.5J 2.0 0.6J 0.4J MW-G 5-May-15 0.2J 2.4J 0.4J 1.9 0.5J MW-G 27-Oct-15 1.0 5.5 0.6J 2.9 MW-G 19-May-16 0.2J 2.2J 0.7J 1.4 0.6J MW-G (dup)19-May-16 0.2J 2.1J 1.3 0.5J MW-G 2-Nov-16 0.6J 5.6 1.2J 0.7J 3.4 0.6J MW-H 4-May-11 MW-H 8-Nov-11 MW-H 8-May-12 MW-H 28-Nov-12 0.7J MW-H 8-May-13 MW-H 7-Nov-13 MW-H 7-May-14 MW-H 5-Nov-14 MW-H 5-May-15 MW-H 28-Oct-15 MW-H 18-May-16 2.7J MW-H 2-Nov-16 MW-H Deep 4-May-11 MW-H Deep 8-Nov-11 MW-H Deep 8-May-12 MW-H Deep 28-Nov-12 0.4J MW-H Deep 8-May-13 MW-H Deep (dup)8-May-13 MW-H Deep 7-Nov-13 MW-H Deep 7-May-14 MW-H Deep 5-Nov-14 MW-H Deep (dup)5-Nov-14 MW-H Deep 5-May-15 MW-H Deep (dup)5-May-15 MW-H Deep 28-Oct-15 MW-H Deep 18-May-16 MW-H Deep 2-Nov-16 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 8 of 14 January 2017 Table 5b Detected Groundwater Constituents - Volatile Organic Compounds November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l e D a t e Ac e t o n e Be n z e n e 2-B u t a n o n e 2- H e x a n o n e Ca r b o n D i s u l f i d e Ch l o r o b e n z e n e Ch l o r o e t h a n e Ch l o r o f o r m 1, 2 - D i c h l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e 1,1 - D i c h l o r o e t h a n e 1,2 - D i c h l o r o e t h a n e 1,1 - D i c h l o r o e t h e n e 1, 2 - D i c h l o r o p r o p a n e cis - 1 , 2 - D i c h l o r o e t h e n e Et h y l b e n z e n e Me t h y l e n e C h l o r i d e 4- M e t h y l - 2 - P e n t a n o n e tra n s - 1 , 2 - D i c h l o r o e t h e n e Te t r a c h l o r o e t h e n e To l u e n e To t a l X y l e n e s 1, 1 , 1 - T r i c h l o r o e t h a n e Tr i c h l o r o e t h e n e Tri c h l o r o f l u o r o m e t h a n e Vin y l C h l o r i d e bi s ( 2 - E t h y l h e x y l ) P h t h a l a t e 6,000 1 4,000 40*700 50 3,000 70 20 6 6 0.4 7 0.6 70 600 5 560*100 0.7 600 500 200 3 2,000 0.03 3 100 1 100 50 100 3 10 5 5 1 5 1 5 1 5 1 1 100 5 1 1 5 1 1 1 1 15 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit 1302-MSWLF- & 1302-CDLF-1998 MW-I 4-May-11 4J 0.8J 2.9 1.3 0.7J MW-I 8-Nov-11 10J 3.5J 0.8J 2.5 1 0.6J MW-I 8-May-12 3.3J 0.2J 0.8J 0.4J 2.8 1.1 0.7J MW-I (dup)8-May-12 3.3J 0.3J 0.9J 0.4J 2.6 1.1 0.7J MW-I 27-Nov-12 4.0J 0.3J 0.9J 1.2 2.4 1.1 MW-I 9-May-13 3.6J 1.3J 0.4J 2.8 1.4 0.6J MW-I 7-Nov-13 3.9J 1.3J 0.4J 2.8 1.4 0.6J MW-I 6-May-14 4.7J 0.2J 1.4J 2.9 1.4 0.6J MW-I 4-Nov-14 4.9J 0.4J 1.7J 3.4 1.7 0.6J MW-I 5-May-15 4.4J 1.4J 0.4J 3.1 1.5 0.6J MW-I 28-Oct-15 4.6J 1.9J 3.2 1.5 0.5J MW-I 18-May-16 3.9J 1.8J 2.9 1.5 0.5J 2.9J MW-I 2-Nov-16 4.6J 1.0J 2.0J 0.6J 3.5 1.3 0.8J MW-J 3-May-11 MW-J 8-Nov-11 MW-J 8-May-12 MW-J 28-Nov-12 0.8J MW-J 7-May-13 MW-J 5-Nov-13 MW-J 6-May-14 MW-J 4-Nov-14 MW-J 6-May-15 MW-J 27-Oct-15 MW-J 17-May-16 MW-J 1-Nov-16 MW-K 3-May-11 0.6J MW-K 8-Nov-11 5.1J 1J MW-K 8-May-12 0.4J MW-K 27-Nov-12 1.6J 0.3J 0.7J 0.3J 0.3J MW-K 7-May-13 1.3J 0.4J MW-K 5-Nov-13 MW-K 6-May-14 0.5J MW-K 4-Nov-14 1.1J 0.5J MW-K 5-May-15 0.6J MW-K 28-Oct-15 1.4J 0.8J 0.4J MW-K 17-May-16 MW-K 1-Nov-16 0.6J 0.6J MW-K (dup)1-Nov-16 0.5J 0.9J 0.6J MW-L 4-May-11 MW-L 9-Nov-11 MW-L 9-May-12 MW-L 28-Nov-12 11 1.0J 1.1J 1.2 2.5 2.4 MW-L 9-May-13 MW-L 7-Nov-13 MW-L 8-May-14 MW-L 5-Nov-14 MW-L 6-May-15 MW-L 28-Oct-15 MW-L 19-May-16 MW-L 2-Nov-16 MW-L Deep 4-May-11 9.4 1.4J 1.2J 0.7J 13 3.7 1.6 MW-L Deep 8-May-12 5.8 0.4J 0.6J 0.4J 1.4 1.2 0.6J MW-L Deep 9-May-13 11 1.2J 1.8J 0.9J 16 5.1 1.5 MW-L Deep 8-May-14 0.4J 6.8 0.5J 0.8J 2.2 1.7 0.4J MW-L Deep 6-May-15 5.6 0.5J 0.6J 0.4J 3.5 1.8 0.6J MW-L Deep 29-Oct-15 4.6J 0.6J 2.2 1.5 0.5J MW-L Deep 19-May-16 3.2J 2.0 0.9J MW-M 4-May-11 0.4J MW-M 8-May-12 0.9J 0.3J MW-M 9-May-13 1.1J 0.5J MW-M 8-May-14 1.1J MW-M 5-May-15 1.0J 0.4J MW-M 28-Oct-15 0.9J MW-M 17-May-16 0.8J MW-X 3-May-11 MW-X 8-Nov-11 MW-X 8-May-12 MW-X 28-Nov-12 0.6J MW-X (dup)28-Nov-12 0.6J MW-X 7-May-13 MW-X 5-Nov-13 MW-X 6-May-14 MW-X 4-Nov-14 MW-X 6-May-15 MW-X 28-Oct-15 MW-X 17-May-16 MW-X 1-Nov-16 Notes:1. All units are in micrograms per liter (parts per billion). 2. * - Groundwater Protection Standard 3. Monitoring wells MW-3 Deep, -L Deep, -and -M are sampled annually during the spring event. 4. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 5. B - Indicates constituent was detected in the batch blank above the method detection limit. 6. (dup) - Duplicate 7. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 8. MW-9 was removed from the monitoring program in November 2012. 9. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. - Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard - Indicates the result is below the detection limit. 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 9 of 14 January 2017 Table 5c Detected Surface Water Constituents - Volatile Organic Compounds and Metals November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Le a d Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zi n c Ac e t o n e St y r e n e To l u e n e 0.64*0.01*200*0.0065**0.00015**0.024**0.004*0.0027*0.00054**0.016**0.005**0.00006**0.00047*NS 0.036*2,000 NS 11 0.006 0.01 0.1 0.001 0.001 0.01 0.01 0.01 0.01 0.05 0.01 0.01 0.0055 0.025 0.01 100 1 1 SW-1 5-May-11 0.0002J 0.0718J 0.0012J 0.00381J 0.00115J 0.00623J 0.00248J 0.00369J SW-1 9-Nov-11 0.094J 0.00077J 0.0026J 0.00023J 0.00532J 0.00174J SW-1 10-May-13 0.0821J 0.00006J 0.00379J 0.00201J 0.00016J 0.0063J 0.00205J 0.00493J SW-1 5-Nov-13 0.00106J 0.139 0.00952J 0.00175J 0.00009J 0.00851J 0.00285J 0.00012J 0.00755JB 0.00938JB 2J 0.3J SW-1 5-May-14 0.00180J 0.146 0.00037J 0.00463JB 0.00117 0.00634J 0.00358JB 0.00979J 0.00283J 0.0144J 0.0343 SW-1 5-May-15 SW-1 29-Oct-15 0.00089J 0.0692J 0.00101J 0.00172J 0.00509J 0.00439J 0.00293CN,J 0.00237J SW-1 19-May-16 0.00352J 0.157 0.00144 0.0372 0.0156 0.0251 0.0148 0.0172J 0.00533J 0.00008J 0.0652 0.0640 SW-1 3-Nov-16 SW-2 5-May-11 0.00019J 0.091J 0.00018J 0.00251J 0.00425J 0.0034J 0.0013JB 0.00626J 0.00388J 0.00384J 0.00639J SW-2 9-May-12 0.0653J 0.00106J 0.00088J 0.00168J 0.00085J 0.00333J 0.00133J 0.00301J 0.00267J,B SW-2 10-May-13 0.00097J 0.0789J 0.00063J 0.00253J 0.0022J 0.00084J 0.00636J 0.00302J 0.00605J SW-2 6-May-14 0.00145J 0.137 0.00005J 0.00329J 0.00365J 0.00152JB 0.00699J 0.00368J 0.00711J 0.0245 SW-2 3-Nov-14 0.00188J 0.067J 0.0127 0.00057J 0.00005J 0.00142J 0.00108J 0.00515JB 6.0J 2 SW-2 5-May-15 0.00732JB 0.00316J 0.00121J 0.00634J 0.00340J 0.00136J SW-2 29-Oct-15 0.00168J 0.0811J 0.00010J 0.00069J 0.00364J 0.00095J 0.00460J 0.00650J 0.00328CN,J 0.00193J 0.00548J SW-2 19-May-16 0.00235J 0.0890J 0.00094J 0.0122 0.00721J 0.0119 0.00873J 0.00833J 0.00340J 0.0327 0.0350 SW-2 3-Nov-16 Notes: 1. All units for metals are in milligrams per liter (parts per million). All untis for volatile organic compounds are in micrograms per liter (parts per billion). 2. Standards obtained from 15A NCAC 02B .0211 (North Carolina 2B) Fresh Surface Water Quality Standards for Class C Waters - June 2016. 3. * - Human Health Standard 4. ** - Freshwater Aquatic Life Standard 5. NS - No Standard 6. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 7. B - Indicates constituent was detected in the batch blank above the method detection limit. 8. CN - Detected silver concentrations were determined to be the result of contamination from the preservative acid used. 9. SW-1 was dry during the Fall 2007, Fall 2009, Spring 2010, Fall 2011, Spring 2012, Fall 2012, Fall 2014, Spring 2015, and Fall 2016 sampling events. 10. SW-2 was dry during the Fall 2009, Spring 2010, Fall 2010, Fall 2011, Fall 2012, Fall 2013, and Fall 2016 sampling events. - Concentration exceeds North Carolina 2B Human Health or Freshwater Aquatic Life Standard for Class C Waters. - Indicates the result is below the detection limit. Volatile Organic Compounds Solid Waste Section Limit North Carolina 2B Human Health or Freshwater Aquatic Life Standard Metals 1302-MSWLF- & 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Su r f a c e W a t e r S a m p l e Lo c a t i o n Sa m p l e D a t e 1302-MSWLF- & 1302-CDLF-1998 DRY DRY DRY DRY Page 10 of 14 January 2017 Table 5d Geochemical Constituents in Groundwater November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l i n g D a t e Di s s o l v e d O x y g e n Ox i d a t i o n - R e d u c t i o n P o t e n t i a l Et h a n e Et h e n e Me t h a n e Ac e t i c A c i d Bu t y r i c A c i d Fo r m i c A c i d He x a n o i c A c i d i- H e x a n o i c A c i d i- P e n t a n o i c A c i d La c t i c A c i d a n d H I B A Pe n t a n o i c A c i d Pr o p i o n i c A c i d Py r u v u c A c i d Dis s o l v e d H y d r o g e n Ca r b o n D i o x i d e Al k a l i n i t y Bio c h e m i c a l O x y g e n D e m a n d (B O D ) Ch e m i c a l O x y g e n D e m a n d (C O D ) Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e Su l f i d e To t a l O r g a n i c C a r b o n ( T O C ) mg/l mVolts µg/l µg/l µg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l nM mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l MW-9 3-May-11 3.45 139 <0.010 0.004J 1.7 0.088 <0.05 <0.1 <0.05 <0.05 <0.15 0.14 <0.07 0.1 <0.15 0.65 37 50 <0.5 <6 1.3 0.16J 0.091 0.41J <0.6 3.1 MW-9 9-Nov-11 4.70 212 0.062 0.078 3.5 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.033J <0.07 <0.05 <0.15 1.4 53 35 <2 11 1.3 0.9JH 0.094 0.26J <1 0.4JB MW-9 9-May-12 1.82 127 0.11 0.012J 6.7 0.038J <0.05 0.051J <0.05 <0.05 <0.15 0.086J <0.07 <0.05 <0.15 2.8 41 36 <0.002 <10 1.6 <0.2H 0.180 <5 <0.2 0.484J CD-1s 3-May-11 47 3.6 1.2J CD-1s 8-Nov-11 40 4 1.1J CD-1s 7-May-12 46 3.9 CD-1s 27-Nov-12 15.56 139 <0.025 0.019J 1.1 <0.07 0.029J 0.019J <0.10 <0.05 <0.15 <0.10 <0.07 <0.05 <0.15 0.94 54 39 <2 <10 4.1 0 0.06 <5 <0.2 <1 CD-1s 7-May-13 1.96 206 0.21 0.14 3.8 <0.07 <0.05 0.062J <0.10 <0.05 <0.15 0.055J <0.07 <0.05 <0.15 0.82 30 42 <2 0.64 4 0.22 0.066 <5 <0.2 <1 CD-1s 5-Nov-13 1.74 348 0.0033J 0.0037J 0.33 0.034J 0.056 <0.5 <0.1 <0.15 0.20 <0.07 <0.05 <0.15 0.74 15 30 <2 <10 3.8 2.42 0.082 <5 <0.2 <1 CD-1s 6-May-14 0.02 353 0.0032J 0.010J 3.4 0.037J <0.05 <0.5 <0.1 <0.15 <0.10 <0.07 <0.05 <0.15 0.94 54 42 <2 <10 3.8 0 0.077 <5 <0.2 1.07 CD-1s 4-Nov-14 6.06 135 0.0061J 0.011J 1.8 0.041J <0.05 <0.5 <0.2 <0.15 0.037J <0.07 0.052 <0.15 1.7 62 41 <2 <10 3.9 0 0.065 <5 <0.2 <1 CD-1s 5-May-15 3.99 281 0.0034J 0.016J 0.060J 0.081 <0.05 0.10 <0.5 <0.2 <0.15 0.019J <0.07 <0.05 0.034J 26 42 38 <2 <10 3.8 0 0.120 <5 <0.2 3.48 CD-1s 27-Oct-15 3.84 519 <0.10 0.012J 0.12J 0.036J 0.0094J 0.033J <0.20 <0.20 <0.10 <0.20 <0.10 0.0024J <0.10 40 61 43 <2 30.6 3.8 0 0.130 <5 <0.2 <1 CD-1s 17-May-16 3.45 245 <0.10 <0.10 0.048J 0.020J <0.10 0.045J <0.20 <0.20 <0.10 0.011J <0.10 <0.10 <0.10 22 46 43 <2 <10 3.7 0 0.079 1 <0.2 <1 CD-1s 1-Nov-16 4.49 360.2 0.0031J 0.0099J 0.84 0.038J 0.0076J 0.059J <0.20 <0.20 <0.10 0.0090J <0.10 <0.10 <0.10 3.1 60 46 <2 26.5 4.2 0 0.067H-02 <5 <0.2 <1 CD-1d 3-May-11 57 2.6 3J CD-1d 8-Nov-11 30 2.9 3J CD-1d 7-May-12 50 2.8 <5 CD-1d 27-Nov-12 9.53 140 46 3 0 0.07 <5 CD-1d 7-May-13 1.11 242 0.015J 0.015J 0.31 0.021J <0.05 0.052J <0.10 <0.05 <0.15 0.06J <0.07 <0.05 <0.15 0.61 40 52 4 6.05 3 0.56 0.069 <5 <0.2 1.42 CD-1d 5-Nov-13 1.71 320.1 42 3 <5 CD-1d 6-May-14 4.56 293 46 2.9 0.077 <5 CD-1d 4-Nov-14 4.68 108.7 43 3.1 0 <5 CD-1d 5-May-15 4.84 186 44 2.9 0 0.086 <5 CD-1d 27-Oct-15 4.10 507 46 2.9 0 <5 CD-1d 17-May-16 4.50 210 96 18.0 0 <0.05 14 CD-1d 1-Nov-16 3.10 330 52 3.4 0 <5 AMW-1s 3-May-11 1.22 176 0.007J 0.004J 810 0.57J <0.05 <0.1 <0.05 <0.05 <0.15 0.13 <0.07 0.63 <0.15 1 250 114 <0.5 <6 3.2 0.13J <0.006 0.36J <0.6 1J AMW-1s 8-Nov-11 0.17 12 0.031 0.068 1,100 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.08J <0.07 <0.05 <0.15 1.1 320 95 3 9J 3.1 <0.2 <0.05 0.26J <1 0.7JB AMW-1s 7-May-12 0.02 121 0.043 0.047 1,300 0.061J <0.05 0.055J <0.05 <0.05 <0.15 0.089J <0.07 <0.05 <0.15 82 300 105 <0.002 <10 3.2 <0.2H <0.004 <0.18 <0.2 0.524J AMW-1s 28-Nov-12 3.81 44 0.064 0.031 1,000 <0.07 <0.05 0.036J <0.10 <0.05 <0.15 <0.10 <0.07 <0.05 <0.15 1.1 280 92 <2 <10 3.1 0.3 <0.05 <5 <0.2 <1 AMW-1s 8-May-13 0.34 523 0.11 0.054 1,600 0.029J <0.05 0.064J <0.10 <0.05 <0.15 0.073J <0.07 <0.05 <0.15 0.69 260 87 <2 14.4 3.5 0.11 <0.05 <5 <0.2 <1 AMW-1s 6-Nov-13 1.05 149 0.11 <0.025 1,400 0.041J 0.061 <0.5 <0.1 <0.15 0.15 <0.07 0.015J <0.15 0.85 270 107 <2 <10 3.6 0.34 <0.05 <5 <0.2 <1 AMW-1s 7-May-14 0.02 400 0.095 <0.025 1,200 0.054J <0.05 <0.5 <0.1 <0.15 0.026J <0.07 0.036J <0.15 0.86 280 105 <2 <10 3.4 0 <0.05 <5 <0.2 <1 AMW-1s 5-Nov-14 3.25 132.2 0.15 0.015J 1,000 0.055J <0.05 <0.5 <0.2 <0.15 0.031J <0.07 0.053 <0.15 1.7 280 120 <2 <10 3.7 0 <0.05 <5 <0.2 <1 AMW-1s 7-May-15 2.00 592 0.2 0.0073J 1,600 <0.07 <0.05 0.11 <0.5 <0.2 <0.15 0.031J <0.07 <0.05 <0.15 12 310 96 <2 <10 3.5 0 <0.5 <5 <0.2 <1 AMW-1s 29-Oct-15 2.68 253 0.21 0.0064J 1,100 0.028J 0.0052J 0.036J <0.20 <0.20 <0.10 0.0094J <0.10 0.0022J <0.10 8.2 300 10.5 <2 <10 3.7 0 <0.05 0.22J <0.2 <1 AMW-1s 18-May-16 3.77 222 0.17 <0.10 1,000 0.015J <0.10 0.030J <0.20 <0.20 <0.10 0.0072J 0.012J <0.10 <0.10 1.5 210 85 <2 <10 3.8 0 <0.05 <5 <0.2 1.44 AMW-1s 2-Nov-16 1.65 377.2 0.13 0.0064J 820 0.044J <0.10 0.048J <0.20 <0.20 <0.10 0.0092J <0.10 <0.10 <0.10 6.0 270 100 <2 23.6 3.3 0 <0.05 <5 <0.2 <1 1302-MSWLF- & 1302-CDLF-1998 Units 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 11 of 14 January 2017 Table 5d Geochemical Constituents in Groundwater November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l i n g D a t e Di s s o l v e d O x y g e n Ox i d a t i o n - R e d u c t i o n P o t e n t i a l Et h a n e Et h e n e Me t h a n e Ac e t i c A c i d Bu t y r i c A c i d Fo r m i c A c i d He x a n o i c A c i d i- H e x a n o i c A c i d i- P e n t a n o i c A c i d La c t i c A c i d a n d H I B A Pe n t a n o i c A c i d Pr o p i o n i c A c i d Py r u v u c A c i d Dis s o l v e d H y d r o g e n Ca r b o n D i o x i d e Al k a l i n i t y Bio c h e m i c a l O x y g e n D e m a n d (B O D ) Ch e m i c a l O x y g e n D e m a n d (C O D ) Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e Su l f i d e To t a l O r g a n i c C a r b o n ( T O C ) mg/l mVolts µg/l µg/l µg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l nM mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1302-MSWLF- & 1302-CDLF-1998 Units AMW-1d 3-May-11 0.01 89 0.059 0.71 1,100 0.11 <0.05 <0.1 <0.05 <0.05 <0.15 <0.1 <0.07 0.29 <0.15 0.89 170 295 1.8J <6 7.3 0.14J <0.006 31 3 1.3 AMW-1d 8-Nov-11 0.00 -112 0.18 1.4 2,900 0.23 <0.05 <0.1 <0.05 <0.05 <0.15 0.2 <0.07 <0.05 <0.15 0.89 280 320 4 19 6.8 1 <0.05 27 <1 4.6 AMW-1d 7-May-12 0.24 95 0.17 1.7 2,500 0.097 <0.05 0.058J <0.05 <0.05 <0.15 0.11 <0.07 <0.05 <0.15 480 270 230 6 <10 6.6 1.91H 0.006J 15 <0.2 4.11 AMW-1d 28-Nov-12 7.00 169 0.15 1.8 2,000 1.9 <0.05 0.039J <0.10 <0.05 <0.15 <0.10 <0.07 0.039J <0.15 0.51J 240 265 4 30.2 6.4 1.8 <0.05 9.2 0.434 3.02 AMW-1d 8-May-13 0.46 -53 0.32 1.6 3,800 0.054J <0.05 0.079J <0.10 <0.05 <0.15 0.089J <0.07 0.028J <0.15 1 300 375 4 8.99 7.1 3.3 <0.05 12 <0.2 4.95 AMW-1d 6-Nov-13 1.40 -22.7 0.28 1.1 3,400 0.033J 0.066 <0.5 <0.1 <0.15 0.12 <0.07 <0.05 <0.15 0.96 290 315 <2 19.7 5.6 2.91 <0.05 6.4 <0.2 3.4 AMW-1d 7-May-14 2.05 -28 0.32 0.82 3,700 0.082 <0.05 <0.5 <0.1 <0.15 0.047J <0.07 0.032J <0.15 1.3 330 230 2 <10 5.6 5 <0.05 <5 <0.2 2.16 AMW-1d 5-Nov-14 1.36 -67.7 0.33 1.3 3,000 0.34 <0.05 <0.5 <0.2 <0.15 0.042J <0.07 0.077 <0.15 2.0 320 375 2 44.9 5.4 4.0 <0.05 <5 0.241 2.15 AMW-1d 7-May-15 1.78 -52 0.5 2.2 3,400 0.15 <0.05 0.11 <0.5 <0.2 <0.15 0.014J <0.07 <0.05 0.035J 7.3 320 230 2 35.2 5.4 2.0 <0.5 <5 <0.2 3.41 AMW-1d 29-Oct-15 2.55 -42 0.79 4.0 4,000 0.27 0.0061J 0.038J <0.20 <0.20 <0.10 0.011J <0.10 0.0050J <0.10 8.2 330 255 9BOD-3 <10 5.5 2.5 <0.05 <5 <0.2 2.67 AMW-1d 18-May-16 1.51 -28 2 2.2 3,700 0.021J <0.10 0.040J <0.20 <0.20 <0.10 <0.20 <0.10 <0.10 <0.10 1.8 300 225 <2 13.2 5.9 3.0 <0.05 <5 <0.2 2.93 AMW-1d 3-Nov-16 1.73 199.2 2.2 3.4 3,900 0.045J <0.10 0.054J <0.20 <0.20 <0.10 0.0083J <0.10 <0.10 <0.10 19 350 215 10 41.6 5.9 2.0 <0.05 <5 <0.2 3.42 AMW-2s 3-May-11 2.10 128 0.003J 0.014 0.240 0.098 <0.05 <0.1 <0.05 <0.05 <0.15 0.12 <0.07 0.063 <0.15 1.2 130 77 <0.5 20 3.2 <0.07 0.086 0.2J <0.6 1.2 AMW-2s 8-Nov-11 2.47 -30 0.016J 0.076 4 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.092J <0.07 <0.05 <0.15 0.68 170 70 1J 10 3.2 0.2JH 0.1 0.097J <1 0.6JB AMW-2s 8-May-12 0.42 195 0.014J 0.022J 0.34 0.042J <0.05 0.066J <0.05 <0.05 <0.15 0.53 <0.07 <0.05 <0.15 9.7 170 70 1.29J <10 3.4 <0.2H 0.12 <5 <0.2 0.418J AMW-2s 29-Nov-12 5.36 38 <0.025 0.026 0.86 <0.07 0.025J 0.023J <0.10 <0.05 <0.15 <0.10 <0.07 <0.05 <0.15 0.41J 170 8 <2 <10 3.3 <0.2H 0.11 <5 <0.2 <1 AMW-2s 9-May-13 0.88 153 0.008J 0.022J 4.30 0.047J <0.05 0.066J 0.068J <0.05 <0.15 0.11 <0.07 <0.05 <0.15 0.87 160 46 4 13.5 3.5 0.43 0.13 <5 <0.2 1.52 AMW-2s 6-Nov-13 1.51 75.1 0.0045J <0.025 0.58 0.020J 0.068 <0.5 <0.1 <0.15 0.10 <0.07 <0.05 <0.15 0.94 140 63 <2 15.8 3.5 0.55 0.16 <5 <0.2 12.3 AMW-2s 7-May-14 2.08 114 0.022J 0.0081J 0.31 0.062J 0.033J <0.5 <0.1 <0.15 0.032J <0.07 0.032J <0.15 25 180 60.6 <2 <10 3.6 0 0.16 <5 <0.2 1.07 AMW-2s 5-Nov-14 3.48 120.5 0.0054J 0.014J 0.20 0.036J <0.05 <0.5 <0.2 <0.15 <0.10 <0.07 0.048J 0.046J 1.4 180 95 <2 <10 3.6 0 0.17 <5 <0.2 <1 AMW-2s 6-May-15 3.50 562 0.0044J 0.020J 1.10 <0.07 <0.05 0.088J <0.5 <0.2 <0.15 0.013J <0.07 <0.05 <0.15 52.0 180 53 <2 <10 3.5 0 0.22 <5 <0.2 1.05 AMW-2s 28-Oct-15 4.19 187 0.0048J 0.056J 0.26J 0.026J 0.0050J 0.044J <0.20 <0.20 <0.10 0.0087J <0.10 0.0016J <0.10 8.0 160 64 <2 <10 3.7 0 0.24 <5 <0.2 1.15 AMW-2s 17-May-16 3.22 51 <0.10 0.012J 4.60 0.017J <0.10 0.038J <0.20 <0.20 <0.10 <0.20 <0.10 <0.10 <0.10 1.9 180 65 <2 <10 3.4 0 0.29 <5 <0.2 <1 AMW-2s 1-Nov-16 3.38 235.1 0.0087J 0.014J 3.8 0.027J 0.0073J 0.051J <0.20 <0.20 <0.10 0.0077J <0.10 <0.10 <0.10 2.9 200 69 <2 25.8 3.7 0 0.31H-02 <5 <0.2 1.02 AMW-2d 3-May-11 0.75 107 0.005J 0.037 0.41 0.052J <0.05 <0.1 <0.05 <0.05 <0.15 0.12 <0.07 0.066 <0.15 0.86 44 129 <0.5 <6 3.1 0.08J 0.017J 4.3J <0.6 0.8J AMW-2d 8-Nov-11 1.07 -29 0.03 0.19 7.10 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.032J <0.07 <0.05 <0.15 1.4 96 75 <2 7 2.9 <0.2H 0.011J 3.5J <1 0.7JB AMW-2d 8-May-12 0.00 195 0.053 0.073 1 0.037J <0.05 0.053J <0.05 <0.05 <0.15 0.087J <0.07 <0.05 <0.15 31 98 80 <0.002 <10 3 <0.2H <0.05 <5 <0.2 0.932J AMW-2d 28-Nov-12 3.47 149 0.10 0.69 30 0.99 <0.05 0.031J <0.10 <0.05 <0.15 <0.10 <0.07 0.030J <0.15 0.68 110 79 <2 13.5 3.2 0.3 <0.05 <5 <0.2 <1 AMW-2d 9-May-13 0.36 126 0.013J 0.049 1.1 0.1 <0.05 0.064J <0.10 <0.05 <0.15 0.08J <0.07 <0.05 <0.15 1.5 110 65 1.48J 11.7 3 0.06 <0.05 <5 <0.2 <1 AMW-2d 6-Nov-13 1.40 137.7 0.0072J 0.048 0.48 0.027J 0.061 <0.5 <0.1 <0.15 0.12 <0.07 <0.05 <0.15 0.65 68 85 20.4 <10 3.1 0.16 0.18 <5 <0.2 <1 AMW-2d 7-May-14 3.88 95 0.0068J 0.021J 0.36 0.073 <0.05 <0.5 <0.1 <0.15 0.033J <0.07 0.030J <0.15 18 170 78.8 <2 <10 3.2 0.5 <0.05 <5 <0.2 <1 AMW-2d 5-Nov-14 4.19 103.5 0.016J 0.016J 0.27 0.040J <0.05 <0.5 <0.2 <0.15 0.016J 0.082 0.048J <0.15 1.3 100 130 <2 <10 3.3 0 <0.05 <5 <0.2 <1 AMW-2d 6-May-15 2.51 391 0.011J 0.035J 0.97 <0.07 <0.05 0.098J <0.5 <0.2 <0.15 <0.1 <0.07 <0.05 <0.15 23.0 200 90 <2 <10 3.4 0 <0.5 <5 <0.2 <1 AMW-2d 28-Oct-15 3.90 158 0.013J 0.039J 0.20J 0.030J 0.0075J 0.038J <0.20 <0.20 <0.10 0.0051J <0.10 0.0024J <0.10 9.0 120 98 <2 <10 3.3 0 <0.05 <5 <0.2 <1 AMW-2d 17-May-16 2.69 88 0.023J 0.012J 0.49J 0.036J <0.10 0.095J <0.20 <0.20 <0.10 <0.20 <0.10 <0.10 <0.10 1.0 160 110 <2 <10 3.5 0 <0.05 <5 <0.2 <1 AMW-2d 2-Nov-16 2.15 345.8 0.015J 0.20 2.0 0.020J <0.10 0.046J <0.20 <0.20 <0.10 0.075J <0.10 <0.10 <0.10 2.3 230 110 <2 31.2 4.2 0 <0.05 <5 <0.2 <1 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 12 of 14 January 2017 Table 5d Geochemical Constituents in Groundwater November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l i n g D a t e Di s s o l v e d O x y g e n Ox i d a t i o n - R e d u c t i o n P o t e n t i a l Et h a n e Et h e n e Me t h a n e Ac e t i c A c i d Bu t y r i c A c i d Fo r m i c A c i d He x a n o i c A c i d i- H e x a n o i c A c i d i- P e n t a n o i c A c i d La c t i c A c i d a n d H I B A Pe n t a n o i c A c i d Pr o p i o n i c A c i d Py r u v u c A c i d Dis s o l v e d H y d r o g e n Ca r b o n D i o x i d e Al k a l i n i t y Bio c h e m i c a l O x y g e n D e m a n d (B O D ) Ch e m i c a l O x y g e n D e m a n d (C O D ) Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e Su l f i d e To t a l O r g a n i c C a r b o n ( T O C ) mg/l mVolts µg/l µg/l µg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l nM mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1302-MSWLF- & 1302-CDLF-1998 Units MW-3 4-May-11 2.60 164 0.003J 0.006J 0.5 0.24 0.098 <0.1 <0.05 <0.05 <0.15 0.19 <0.07 0.094 <0.15 1.1 69 69 <0.5 <6 2.8 0.18J 0.022J 0.25J <0.6 0.3J MW-3 9-Nov-11 4.05 198 0.04 0.059 1.6 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.043J <0.07 <0.05 <0.15 0.8 120 65 <2 <10 2.9 0.18JH 0.019J 0.15J <1 0.4JB MW-3 8-May-12 2.76 113 <0.025 0.021J 0.14 0.072 <0.05 0.094J <0.05 <0.05 <0.15 0.13 <0.07 <0.05 <0.15 1.5 100 60 <0.002 <10 3.6 0.3H <0.05 <5 <0.2 0.303J MW-3 28-Nov-12 12.31 73 0.044 0.022J 0.83 <0.07 <0.05 0.038J <0.10 <0.05 <0.15 <0.10 <0.07 <0.05 <0.15 1.1 120 91 <2 <10 3.2 <0.2H <0.05 <5 <0.2 <1 MW-3 9-May-13 1.88 188 0.018J 0.0079J 0.40 0.025J <0.05 0.058J <0.10 <0.05 <0.15 0.082J <0.07 <0.05 <0.15 1.6 82 52 <2 10.1 3.1 1.11 <0.05 <5 <0.2 <1 MW-3 7-Nov-13 1.99 301.1 0.0035J 0.0075J 0.34 0.049J <0.05 <0.5 <0.1 <0.15 0.22 <0.07 0.015J <0.15 1.4 110 69 26 28.1 3.4 0.83 <0.05 <5 <0.2 9.12 MW-3 8-May-14 0.04 150 0.0062J 0.030 0.16 0.080 <0.05 <0.5 <0.1 <0.15 0.053J <0.07 0.034J <0.15 1.1 140 63.6 6 <10 3.2 0 <0.05 <5 <0.2 1.67 MW-3 6-Nov-14 5.94 465.6 0.0040J 0.015J 0.30 0.045J <0.05 <0.5 <0.2 <0.15 0.040J 0.068J 0.048J <0.15 1.6 140 61 <2 <10 3.3 0 <0.05 <5 <0.2 <1 MW-3 6-May-15 2.29 260 0.0085J 0.016J 0.18J <0.07 <0.05 0.077J <0.05 <0.02 <0.15 0.014J <0.07 <0.05 <0.15 14 140 65 <2 76.2 3.4 0 <0.5 <5 <0.2 1.43 MW-3 28-Oct-15 3.85 166 0.23 0.022J 0.20J 0.026J 0.0058J 0.043J <0.20 <0.20 <0.10 <0.20 <0.10 0.0016J <0.10 11 130 69 <2 <10 3.4 0 <0.05 <5 <0.2 <1 MW-3 18-May-16 3.18 101 <0.10 <0.10 0.87 0.015J <0.10 0.079J <0.20 <0.20 <0.10 0.0092J <0.10 <0.10 <0.10 9.6 120 75 <2 <10 3.7 0 <0.05 <5 <0.2 1.32 MW-3 2-Nov-16 3.50 438.8 0.020J 0.021J 0.72 0.031J <0.10 0.10 <0.20 <0.20 <0.10 0.0082J <0.10 <0.10 <0.10 1.9 130 60 <2 14.9 4.1 0 <0.05 <5 <0.2 <1 MW-A 3-May-11 1.08 113 0.018 <0.010 3,600 0.085 0.12 <0.1 <0.05 <0.05 <0.15 0.13 <0.07 0.063 <0.15 1.3 470 134 6 7J 11 0.14J <0.006 4.5J <0.6 7.6 MW-A 9-Nov-11 0.06 205 0.084 0.057 9,300 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.22 <0.07 <0.05 <0.15 1.3 610 115 2 <10 11 0.6H <0.05 4.3J <1 2.6 MW-A 9-May-12 0.00 103 0.11 0.027 8,000 0.16 <0.05 0.056J <0.05 <0.05 <0.15 0.11 <0.07 0.020J <0.15 3.2 560 146 6 <10 14 2.22H <0.05 <5 <0.2 0.364J MW-A 27-Nov-12 2.66 140 0.073 0.018J 9,000 <0.07 <0.05 0.016J <0.10 <0.05 <0.15 0.043J <0.07 <0.05 0.071J 4 530 127 8 13.3 19 0.60 <0.05 <5 0.228 2.52 MW-A 7-May-13 0.25 -34 0.11 0.033 7,500 0.03J <0.05 0.07J <0.10 <0.05 <0.15 0.07J <0.07 <0.05 <0.15 0.54J 470 131 5 5.15 16 0.28 <0.05 <5 <0.2 2.62 MW-A 5-Nov-13 1.89 290.8 0.051 <0.025 8,000 0.028J 0.044J <0.5 <0.1 <0.15 0.11 <0.07 <0.05 <0.15 0.84 530 128 6 <10 20 0.60 <0.05 3 <0.2 2.53 MW-A 6-May-14 0.04 -17 0.048 <0.025 11,000 0.21 0.077 <0.5 <0.1 <0.15 0.026J <0.07 0.050 <0.15 0.90 580 131 4 <10 29 2 <0.05 3.5J 0.232 3.1 MW-A 4-Nov-14 1.70 45 0.082 0.019J 10,000 0.038J <0.05 <0.5 <0.2 <0.15 <0.1 <0.07 0.048J <0.15 4.8 640 111 2 <10 32 1 <0.05 4.4J <0.2 2.32 MW-A 5-May-15 2.34 26 0.080J 0.015J 10,000 <0.07 <0.05 0.090J <0.5 <0.2 <0.15 0.027J <0.07 <0.05 <0.15 14.0 580 117 4 <10 28 1 <0.05 5.9 <0.2 3.15 MW-A 27-Oct-15 1.41 29 0.084J 0.011J 9,900 0.032J 0.0066J 0.022J <0.20 <0.20 <0.10 0.013J <0.10 0.0033J <0.10 7.2 600 123 11 <10 25 0.5 <0.05 7.4 <0.2 4.18 MW-A 17-May-16 1.27 -55 0.094J <0.10 11,000 0.21 0.084J 0.032J <0.20 <0.20 <0.10 0.0075J <0.10 <0.10 <0.10 1.3 540 85 6 <10 18 1.0 <0.05 13 <0.2 3.68 MW-A 1-Nov-16 1.65 205 0.087J 0.015J 9,500 0.040J <0.10 0.057J <0.20 <0.20 <0.10 <0.20 <0.10 <0.10 <0.10 1.8 640 129 12BOD-4 33.8 27 1.5 <0.05 19 <0.2 3.28 MW-E Rep 4-May-11 0.01 34 0.37 0.38 5,000 0.22 0.086 <0.1 <0.05 <0.05 0.092J 0.13 <0.07 0.092 0.18 1.4 410 261 5 13 30 <0.07H <0.006 13 <0.6 4.2 MW-E Rep 8-Nov-11 0.00 -115 4.9 0.36 4,300 <0.07 <0.05 <0.1 <0.05 <0.05 <0.15 0.21 <0.07 <0.05 <0.15 1.4 460 275 5 34 32 5.89H <0.05 11 <1 4 MW-E Rep 8-May-12 0.00 13 4.6 0.33 2,200 0.048J <0.05 0.052J <0.05 <0.05 <0.15 0.086J <0.07 <0.05 <0.15 2.1 430 285 4 <10 30 8.22H <0.05 8.1 <0.2 0.317J MW-E Rep 8-May-13 0.47 -81 6.6 0.5 1,600 0.048J <0.05 0.074J <0.05 <0.05 <0.15 0.072J <0.07 <0.05 <0.15 0.56J 350 405 2 16.9 52 3.3 <0.05 <5 <0.2 4.89 MW-E Rep 5-Nov-13 1.64 -39.8 4.2 0.36 1,700 0.038J 0.058 <0.5 <0.1 <0.15 0.11 <0.07 <0.05 <0.15 0.81 330 320 4.09 24.6 31 2.77 <0.05 5 <0.2 4.18 MW-E Rep 6-May-14 0.07 -24 2.6 0.27 2,400 0.095 0.091 <0.5 <0.1 <0.15 0.15 <0.07 0.048J <0.15 0.97 400 285 3 <10 28 5 <0.05 8.5 <0.2 4.08 MW-E Rep 4-Nov-14 1.62 -54 3.7 0.56 2,800 0.038J <0.05 <0.5 <0.2 <0.15 0.051J 0.070 <0.05 <0.15 1.4 430 610 3 <10 45 3.5 <0.05 11 <0.2 4.44 MW-E Rep 5-May-15 3.61 -38 3.4 0.47 1,700 <0.07 <0.05 0.12 <0.5 <0.2 <0.15 0.036J 0.028J <0.05 0.044J 13 340 415 4 11 48 2.5 <0.05 11 <0.2 6.14 MW-E Rep 27-Oct-15 1.25 -36 4.1 0.73 2,300 0.038J 0.0062J 0.049J <0.20 <0.20 <0.10 0.011J 0.011J 0.0026J <0.10 7.3 380 365 5 <10 48 2.0 <0.05 8.3 <0.2 4.82 MW-E Rep 18-May-16 1.40 -59 3.3 0.63 680 0.21 1 0.12 <0.20 <0.20 <0.10 <0.20 0.024J 0.021J 0.014J 1 250 425 3 <10 55 0.5 <0.05 6 <0.2 4.49 MW-E Rep 1-Nov-16 3.79 48.1 4.8 0.73 660 0.035J <0.10 0.056J <0.20 <0.20 <0.10 0.0060J0.0086J <0.10 0.012J 2.3 370 475 <2 33.4 50 3.0 <0.05 78 <0.2 5.06 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 13 of 14 January 2017 Table 5d Geochemical Constituents in Groundwater November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Fa c i l i t y P e r m i t N u m b e r s Mo n i t o r i n g W e l l C o d e Sa m p l i n g D a t e Di s s o l v e d O x y g e n Ox i d a t i o n - R e d u c t i o n P o t e n t i a l Et h a n e Et h e n e Me t h a n e Ac e t i c A c i d Bu t y r i c A c i d Fo r m i c A c i d He x a n o i c A c i d i- H e x a n o i c A c i d i- P e n t a n o i c A c i d La c t i c A c i d a n d H I B A Pe n t a n o i c A c i d Pr o p i o n i c A c i d Py r u v u c A c i d Dis s o l v e d H y d r o g e n Ca r b o n D i o x i d e Al k a l i n i t y Bio c h e m i c a l O x y g e n D e m a n d (B O D ) Ch e m i c a l O x y g e n D e m a n d (C O D ) Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e Su l f i d e To t a l O r g a n i c C a r b o n ( T O C ) mg/l mVolts µg/l µg/l µg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l nM mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1302-MSWLF- & 1302-CDLF-1998 Units MW-E Deep 4-May-11 0.00 -51 3.3 0.14 6,900 4.3 0.13 <0.1 <0.05 <0.05 <0.15 <0.1 <0.07 0.25 <0.15 2.3 100 401 7 37 27 2.7 <0.006 0.096J <0.6 5.4 MW-E Deep 8-Nov-11 0.00 -67 10 0.29 19,000 2.2 0.021J <0.1 <0.05 <0.05 <0.15 0.076J <0.07 <0.05 <0.15 2 160 345 16 33 26 2.2 0.007J <5 <1 2.9 MW-E Deep 8-May-12 2.51 -76 7.5 0.11 14,000 0.84 <0.05 0.090J <0.05 <0.05 <0.15 0.10 <0.07 0.024J <0.15 3.3 160 305 24 22.6 27 4.03H <0.05 <5 <0.2 0.207J MW-E Deep 27-Nov-12 1.70 78 9.8 0.14 16,000 0.19 <0.05 0.058J <0.10 <0.05 <0.15 0.034J <0.07 <0.05 0.11J 1.1 160 255 10 39.2 28 7H <0.05 <5 <0.2 1.37 MW-E Deep 8-May-13 0.51 -80 13 0.13 16,000 0.25 <0.05 0.12 <0.10 <0.05 <0.15 0.066J <0.07 0.028J <0.15 0.99 140 370 5 26.4 28 3.3 <0.05 <5 <0.2 2.3 MW-E Deep 6-Nov-13 1.21 -82.2 13 0.18 15,000 0.11 <0.05 <0.5 <0.1 <0.15 0.16 <0.07 <0.05 <0.15 1.5 170 345 5.97 23.1 31 3.3 <0.05 <5 <0.2 2.51 MW-E Deep 6-May-14 0.09 -41 4.6 0.13 19,000 120 20 2.9 <0.1 1.9 <1 20 100 4.0 1.3 480 320 1,580 2,410 20 5.5 <0.05 <5 <0.2 432 MW-E Deep 4-Nov-14 1.09 -82.3 2.8 0.056 22,000 52 2.3 0.44J <0.2 0.18 0.046J 0.37 5.4 0.21 6.7 310 625 208 355 30 1.5 <0.05 <5 <0.2 41.6 MW-E Deep 5-May-15 0.88 -100 9 0.059J 22,000 7.1 0.092 0.23 <0.5 <0.2 0.029J 0.019J <0.07 0.12 0.042J 17 220 410 47 59.2 35 1 <0.50 <5 <2 8.26 MW-E Deep 27-Oct-15 1.20 -71 8.1 <0.50 26,000 2.4 0.085J 0.035J 0.012J <0.20 <0.10 <0.20 <0.10 0.026J <0.10 8.7 170 415 36 22.4 34 3.0 0.13 <5 <0.2 4.52 MW-E Deep 18-May-16 3.08 -95 3.9 0.021J 16,000 2.8 0.2 0.064J <0.20 <0.20 <0.10 <0.20 <0.10 0.064J 0.012J 2.3 130 <1 28 63.8 37 3.0 <0.05 <5 <0.2 6.34 MW-E Deep 1-Nov-16 2.30 -39.0 12 0.063J 29,000 0.12 <0.10 0.072J <0.20 <0.20 <0.20 <0.20 <0.10 <0.10 <0.10 2.7 210 415 27BOD-4 62.5 44 2.0 <0.5 <5 <0.2 3.16 MW-L 4-May-11 2.31 206 <0.01J 0.003J 0.3 0.22 0.11 <0.1 <0.05 <0.05 <0.15 0.32 <0.07 0.097 <0.15 0.7 72 44 <0.5 <6 2.2 0.16J 0.13 1.8J <0.6 0.5J MW-L 9-Nov-11 2.59 222 <0.025 0.066 0.3 <0.07 0.019J <0.1 <0.05 <0.05 <0.15 0.16 <0.07 <0.05 <0.15 1.4 83 30 <2 10J 2.6 <0.2H 0.096 1.8J <1 0.5JB MW-L 9-May-12 0.04 214 <0.025 0.014J 0.69 0.049J <0.05 0.062J <0.05 <0.05 <0.15 0.11 <0.07 <0.05 <0.15 1.1 98 37 <0.002 <10 2.6 <0.2H 0.096 <5 <0.2 0.342J MW-L 28-Nov-12 3.03 3 0.22 0.037 2.8 <0.07 0.033J 0.031J <0.10 <0.05 <0.15 0.066J <0.07 <0.05 <0.15 0.43J 72 90 <2 <10 2.7 <0.2H 0.052 <5 <0.2 <1 MW-L 9-May-13 1.09 188 <0.025 0.024J 0.55 0.024J <0.05 0.056J 0.044J <0.05 <0.15 0.085J <0.07 <0.05 <0.15 1.2 79 28 1.91J 2.22 2.7 0 0.06 <5 <0.2 <1 MW-L 7-Nov-13 1.39 258.1 <0.025 <0.025 0.059J 0.034J <0.05 <0.5 <0.1 <0.15 0.12 <0.07 <0.05 <0.15 0.78 90 35 2 <10 2.8 0.61 0.065 <5 <0.2 1.43 MW-L 8-May-14 2.12 379 0.0030J 0.0038J 0.042J 0.063J <0.05 <0.5 <0.1 <0.15 0.033J <0.07 0.034J <0.15 0.79 100 34.3 <2 <10 2.8 0.5 0.061 <5 <0.2 <1 MW-L 5-Nov-14 4.03 59.2 0.0037J 0.014J 0.63 0.042J <0.05 <0.5 <0.2 <0.15 0.058J <0.07 0.049J <0.15 1.3 100 31 <2 <10 3.1 0 0.081 2.8J <0.2 <1 MW-L 6-May-15 4.15 131 0.0050J 0.016J 0.055J <0.07 <0.05 0.12 <0.5 <0.2 <0.15 0.014J <0.07 <0.05 <0.15 26 100 31 <2 11 2.7 0 <0.5 1.9J <0.2 <1 MW-L 28-Oct-15 3.80 89 0.0058J 0.019J 0.077J 0.029J 0.0081J 0.033J <0.20 <0.20 <0.10 <0.20 <0.10 0.0022J <0.10 8.9 94 39 <2 <10 3 0 0.054 1.5 <0.2 <1 MW-L 19-May-16 3.66 192 <0.10 <0.10 0.031J 0.012J <0.10 0.033J <0.20 <0.20 <0.10 0.0063J <0.10 <0.10 <0.10 0.63 98 35 <2 10 2.8 0 <0.05 1.4 <0.2 <10 MW-L 2-Nov-16 3.49 486.0 0.028J 0.013J 0.80 0.029J 0.0079J 0.046J <0.20 <0.20 <0.10 0.0062J <0.10 <0.10 <0.10 1.7 87 40 <2 12.9 3.2 0 0.085 <5 <0.2 <1 Notes: 1. Blank cells indicate parameter was not analyzed or the result was below the detection limit. 2. Assessment wells CD-4 and CD-5 were installed in September 2006. 3. Assessment wells AMW-1s, -1d, 2s, and 2d were installed in October 2009. 4. Assessment wells CD-4 and CD-5 were abandoned in July 2010. 5. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 6. BOD-1 - Indicates the dilutions selected for the BOD analysis based on screening COD values did not meet the oxygen depletion criteria of at least 2mg/L dissolved oxygen depletion. The result is reported as an estimated value or non-detect at the elevated reporting limit. 7. H, H-02 - Sample was analyzed outside the U.S. Environmental Protection Agency recommended holding time. 8. B - Indicates constituent was detected in the batch blank above the method detection limit. 9. BOD-3 - Lab control recovery was outside control limits biased low. Samples could not be reanalyzed due to holding time requirements. Sample values are reported as estimated values with possible low bias. 10 BOD-4 - Lab control recovery was outside control limits biased high. Samples are reported as estimated with possible high bias. 11. mg/l - milligrams per liter/µg/l - micrograms per liter/mVolts - millivolts/Nm - nanomoles 12. HIBA - Hydroxyisobutyric Acid 13. Alkalinity, chloride, ferrous iron, sulfate, and total dissolved solids were added to the sampling program in May 2010 for CD-1s and CD-1d. 14. The November 2012 sampling event was the first event that CD-1s/CD-1d replaced MW-9 as the background monitoring wells. 15. MW-9 was removed from the monitoring program in November 2012. 16. MW-E Rep was not sampled during the November 2012 sampling event due to laboratory oversight. 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Page 14 of 14 January 2017 Table 6 Constituents Detected Above Standards November 2016 Semi-Annual Sampling Event Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Notes: 1. MW-E deep, -H, -H deep, -I, -J, -K, -L are assessment wells installed in June 1999. 2. Assessment wells CD-4, CD-5, and CD-6 were installed in September 2006. 3. Assessment wells AMW-1s, -1d, -2s, and -2d were installed in October 2009. 4. Assessment wells CD-4 and CD-5 were abandoned in July 2010. 5. Monitoring wells MW-3 deep, -L deep, -and -M are sampled annually during the spring event. 6. * - Constituents exceed the Groundwater Protection Standard. 7. Bold - J Flag - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 8. The November 2012 sampling event was the first event that CD-1s/-1d replaced MW-9 as the background monitoring wells. 9. MW-9 was removed from the monitoring program in November 2012. Tetrachloroethene 1,1-Dichloroethane, Tetrachloroethene, Trichloroethene Cobalt*, Benzene, 1,4-Dichlorobenzene, Vinyl Chloride Cobalt* MW-E Rep None DetectedMW-K MW-J MW-I None DetectedMW-L Tetrachloroethene Cobalt*, Vanadium* MW-C MW-D Cobalt*, 1,4-Dichlorobenzene, 1,1-Dichloroethane, 1,2-Dichloroethane, Vinyl Chloride PARAMETERS EXCEEDING NORTH CAROLINA 2L OR GROUNDWATER PROTECTION STANDARD ASSESSMENT MONITORING - NOVEMBER 2016 MONITORING WELL FACILITY PERMIT NUMBERS MONITORING WELL 1302-MSWLF- & 1302-CDLF-1998 Not SampledMW-9 PARAMETERS EXCEEDING NORTH CAROLINA 2L OR GROUNDWATER PROTECTION STANDARD ASSESSMENT MONITORING - NOVEMBER 2016 1302-MSWLF- & 1302-CDLF-1998 AMW-1s 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 Cobalt*, Iron, Manganese Iron, Vanadium* 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 CD-5 Not Sampled 1302-MSWLF- & 1302-CDLF-1998 CD-6 CD-4 Rep 1,1-Dichloroethane, Tetrachloroethene, Trichloroethene CD-1s (background well) CD-1d (background well) 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 MW-3 deep Not Sampled MW-1 Cobalt* MW-3 1302-MSWLF- & 1302-CDLF-1998 MW-A 1302-MSWLF- & 1302-CDLF-1998 MW-B Cobalt* Cobalt*, Benzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,2-Dichloropropane, cis-1,2-Dichloroethene, Tetrachloroethene, Trichloroethene, Vinyl Chloride None Detected Not SampledMW-M MW-X MW-L deep Not Sampled 1302-MSWLF- & 1302-CDLF-1998 AMW-2d1302-MSWLF- & 1302-CDLF-1998 1302-MSWLF- & 1302-CDLF-1998 AWM-1d AMW-2s MW-E deepCobalt*, Vanadium* MW-F Barium, Cobalt*, Lead, 1,2-Dichloroethane Cobalt*, Vanadium* MW-GCobalt*, Vanadium* MW-H deep None Detected 1,1-Dichloroethane, Tetrachloroethene, Trichloroethene Cobalt* Cobalt* MW-H Cobalt*, Benzene, 1,1-Dichloroethane, Vinyl Chloride Page 1 of 1 January 2017 Table 7 DHC Sampling Summary Cabarrus County Landfill Units 2 and 3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Monitoring Well Code Sample Date DNA (ng/L) Universal PCR* DHC 16S rRNA Gene copy/L Functional Gene tceA copy/L Functional Gene bvcA copy/L Functional Gene vcrA copy/L MW-E Rep 9-Jan-14 1,958 +1.37E+06 + 1.81E+05 9.48E+05 + 8.02E+04 0.00E+00 + 0.00E+00 5.46E+02 + 1.02E+02 MW-E Rep 4-Mar-15 328 +0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 MW-E deep 9-Jan-14 3,524 +1.38E+07 + 2.23E+06 7.85E+05 + 1.10E+05 0.00E+00 + 0.00E+00 2.84E+06 + 4.53E+05 MW-E deep 4-Mar-15 6,848 +5.20E+03 ± 6.72E+02 9.00E+03 ± 8.24E+01 0.00E+00 ± 0.00E+00 7.06E+02 ± 1.28E02 AMW-1s 9-Jan-14 8,214 +0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 AMW-1s 4-Mar-15 538 +0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 AMW-1d 9-Jan-14 2,648 +3.53E+03 + 3.17E+03 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 AMW-1d 4-Mar-15 1,716 +1.03E+06 ± 1.12E+05 6.18E06 ± 2.89+05 0.00E+00 ± 0.00E+00 3.13E+04 ± 2.79+03 AMW-2s 9-Jan-14 1,917 +3.09E+05 + 5.12E+04 1.24E+06 + 2.26E+05 9.61E+04 + 1.86E+04 5.66E+04 + 1.12E+04 AMW-2s 4-Mar-15 1,564 +0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 AMW-2d 9-Jan-14 1,320 +8.81E+03 + 3.15E+02 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 0.00E+00 + 0.00E+00 AMW-2d 4-Mar-15 108 -0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 0.00E+00 ± 0.00E+00 Notes: 1. PCR - Polymearse chain reaction 2. DHC - Dehalococcoides spp 3. * - A "+" inidicates that amplication of bacteria was successful. "-" indicates that ampification was not successful. 4. ng/L - Nanogram per liter 5. copy/L - Copy per liter - Indicates the result is between the laboratory method detection limit and the reporting limit. Page 1 of 1 January 2017 1" = Approximately 100' MW - E R e p IW - 1 IW - 2 IW - 3 IW - 4 IW - 5 No t e s : 1. T h e i n j e c t i o n w e l l s w e r e i n s t a l l e d u s i n g a i r - r o t ar y d r i l l i n g m e t h o d s f r o m O c t o b e r 5 - 9 , 2 0 0 9 . 2. T h e i n j e c t i o n w e l l s a r e s p a c e d a p p r o x i m a t e l y 3 0 fe e t a p a r t p e r p e n d i c u l a r t o g r o u n d w a t e r f l o w a n d h a ve a r a d i u s o f i n f l u e n c e o f a p p r o x i m a t e l y 1 5 f e e t . 3. S u r f a c e a r e a o f t h e i n j e c t i o n w e l l n e t w o r k i s a p pr o x i m a t e l y 5 , 4 0 0 f e e t . 4 . T h e P h a s e I i n j e c t i o n e v e n t w a s c o m p l e t e d f r o m N o ve m b e r 2 - 6 , 2 0 0 9 . 5. T h e P h a s e I I i n j e c t i o n e v e n t w a s c o m p l e t e d f r o m Fe b r u a r y 1 0 - 1 8 , 2 0 1 4 . MW - E d e e p IW - 6 Fi g u r e 2 : I n j e c t i o n A r e a O v e r v i e w Closed Landfill Units 2 and 3 Cabarrus County, North Carolina Ma p S o u r c e : M i c r o s o f t B i n g , 2 0 1 0 A e r i a l , C o n c o r d , N or t h C a r o l i n a Figure 3 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 MW-A Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Note: Only detections above laboratory method detection limits represented in figure.Figure 3 (MW-A) 0 50 100 150 200 250 300 350 400 450 Se p - 9 4 Ap r - 9 5 No v - 9 5 Ju n - 9 6 Ja n - 9 7 Au g - 9 7 Ma r - 9 8 Oc t - 9 8 Ma y - 9 9 De c - 9 9 Ju l - 0 0 Fe b - 0 1 Se p - 0 1 Ap r - 0 2 No v - 0 2 Ju n - 0 3 Ja n - 0 4 Au g - 0 4 Ma r - 0 5 Oc t - 0 5 Ma y - 0 6 De c - 0 6 Ju l - 0 7 Fe b - 0 8 Se p - 0 8 Ap r - 0 9 No v - 0 9 Ju n - 1 0 Ja n - 1 1 Au g - 1 1 Ma r - 1 2 Oc t - 1 2 Ma y - 1 3 De c - 1 3 Ju l - 1 4 Fe b - 1 5 Se p - 1 5 Ap r - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Figure 4 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 MW-3 Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Note: Only detections above laboratory method detection limits represented in figure.Figure 4 (MW-3) 0 10 20 30 40 50 60 Ju l - 9 8 De c - 9 8 Ma y - 9 9 Oc t - 9 9 Ma r - 0 0 Au g - 0 0 Ja n - 0 1 Ju n - 0 1 No v - 0 1 Ap r - 0 2 Se p - 0 2 Fe b - 0 3 Ju l - 0 3 De c - 0 3 Ma y - 0 4 Oc t - 0 4 Ma r - 0 5 Au g - 0 5 Ja n - 0 6 Ju n - 0 6 No v - 0 6 Ap r - 0 7 Se p - 0 7 Fe b - 0 8 Ju l - 0 8 De c - 0 8 Ma y - 0 9 Oc t - 0 9 Ma r - 1 0 Au g - 1 0 Ja n - 1 1 Ju n - 1 1 No v - 1 1 Ap r - 1 2 Se p - 1 2 Fe b - 1 3 Ju l - 1 3 De c - 1 3 Ma y - 1 4 Oc t - 1 4 Ma r - 1 5 Au g - 1 5 Ja n - 1 6 Ju n - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Figure 5 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 MW-E Rep Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Notes: Only detections above laboratory method detection limits represented in figure. MW-E was not sampled during the November 2012 sampling event due to laboratory oversight.Figure 5 (MW-E Rep) 0 20 40 60 80 100 120 140 160 180 200 Se p - 9 4 Ap r - 9 5 No v - 9 5 Ju n - 9 6 Ja n - 9 7 Au g - 9 7 Ma r - 9 8 Oc t - 9 8 Ma y - 9 9 De c - 9 9 Ju l - 0 0 Fe b - 0 1 Se p - 0 1 Ap r - 0 2 No v - 0 2 Ju n - 0 3 Ja n - 0 4 Au g - 0 4 Ma r - 0 5 Oc t - 0 5 Ma y - 0 6 De c - 0 6 Ju l - 0 7 Fe b - 0 8 Se p - 0 8 Ap r - 0 9 No v - 0 9 Ju n - 1 0 Ja n - 1 1 Au g - 1 1 Ma r - 1 2 Oc t - 1 2 Ma y - 1 3 De c - 1 3 Ju l - 1 4 Fe b - 1 5 Se p - 1 5 Ap r - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Phase I Emulsified Oil Injection -November 2009 Phase II Injection - February 2014 Figure 6 Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 MW-E deep Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Note: Only detections above laboratory method detection lmits represented in figure.Figure 6 (MW-E deep) 0 20 40 60 80 100 120 140 160 180 No v - 9 9 Ma y - 0 0 No v - 0 0 Ma y - 0 1 No v - 0 1 Ma y - 0 2 No v - 0 2 Ma y - 0 3 No v - 0 3 Ma y - 0 4 No v - 0 4 Ma y - 0 5 No v - 0 5 Ma y - 0 6 No v - 0 6 Ma y - 0 7 No v - 0 7 Ma y - 0 8 No v - 0 8 Ma y - 0 9 No v - 0 9 Ma y - 1 0 No v - 1 0 Ma y - 1 1 No v - 1 1 Ma y - 1 2 No v - 1 2 Ma y - 1 3 No v - 1 3 Ma y - 1 4 No v - 1 4 Ma y - 1 5 No v - 1 5 Ma y - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / L ) Date Total VOC PCE TCE DCE VC Phase I Emulsified Oil Injection -November 2009 Phase II -February 2014 Figure 7 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 AMW-1s Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Notes: Only detections above laboratory method detection limits represented in figure. Figure 7 (AMW-1s) 0 20 40 60 80 100 120 Se p - 0 9 No v - 0 9 Ja n - 1 0 Ma r - 1 0 Ma y - 1 0 Ju l - 1 0 Se p - 1 0 No v - 1 0 Ja n - 1 1 Ma r - 1 1 Ma y - 1 1 Ju l - 1 1 Se p - 1 1 No v - 1 1 Ja n - 1 2 Ma r - 1 2 Ma y - 1 2 Ju l - 1 2 Se p - 1 2 No v - 1 2 Ja n - 1 3 Ma r - 1 3 Ma y - 1 3 Ju l - 1 3 Se p - 1 3 No v - 1 3 Ja n - 1 4 Ma r - 1 4 Ma y - 1 4 Ju l - 1 4 Se p - 1 4 No v - 1 4 Ja n - 1 5 Ma r - 1 5 Ma y - 1 5 Ju l - 1 5 Se p - 1 5 No v - 1 5 Ja n - 1 6 Ma r - 1 6 Ma y - 1 6 Ju l - 1 6 Se p - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Phase I Emulsified Oil Injection -November 2009 Phase II -February 2014 Figure 8 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 AMW-1d Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Notes: Only detections above laboratory method detection limits represented in figure. Figure 8 (AMW-1d) 0 20 40 60 80 100 120 Se p - 0 9 No v - 0 9 Ja n - 1 0 Ma r - 1 0 Ma y - 1 0 Ju l - 1 0 Se p - 1 0 No v - 1 0 Ja n - 1 1 Ma r - 1 1 Ma y - 1 1 Ju l - 1 1 Se p - 1 1 No v - 1 1 Ja n - 1 2 Ma r - 1 2 Ma y - 1 2 Ju l - 1 2 Se p - 1 2 No v - 1 2 Ja n - 1 3 Ma r - 1 3 Ma y - 1 3 Ju l - 1 3 Se p - 1 3 No v - 1 3 Ja n - 1 4 Ma r - 1 4 Ma y - 1 4 Ju l - 1 4 Se p - 1 4 No v - 1 4 Ja n - 1 5 Ma r - 1 5 Ma y - 1 5 Ju l - 1 5 Se p - 1 5 No v - 1 5 Ja n - 1 6 Ma r - 1 6 Ma y - 1 6 Ju l - 1 6 Se p - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Phase I Emulsified Oil Injection -November 2009 Phase II -February 2014 Figure 9 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 AMW-2s Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Notes: Only detections above laboratory method detection limits represented in figure. Figure 9 (AMW-2s) 0 5 10 15 20 25 30 35 Se p - 0 9 No v - 0 9 Ja n - 1 0 Ma r - 1 0 Ma y - 1 0 Ju l - 1 0 Se p - 1 0 No v - 1 0 Ja n - 1 1 Ma r - 1 1 Ma y - 1 1 Ju l - 1 1 Se p - 1 1 No v - 1 1 Ja n - 1 2 Ma r - 1 2 Ma y - 1 2 Ju l - 1 2 Se p - 1 2 No v - 1 2 Ja n - 1 3 Ma r - 1 3 Ma y - 1 3 Ju l - 1 3 Se p - 1 3 No v - 1 3 Ja n - 1 4 Ma r - 1 4 Ma y - 1 4 Ju l - 1 4 Se p - 1 4 No v - 1 4 Ja n - 1 5 Ma r - 1 5 Ma y - 1 5 Ju l - 1 5 Se p - 1 5 No v - 1 5 Ja n - 1 6 Ma r - 1 6 Ma y - 1 6 Ju l - 1 6 Se p - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Phase I Emulsified Oil Injection -November 2009 Phase II -February 2014 Figure 10 Total Detected Volatile Organic Compounds Cabarrus County Landfill Units 2 and 3 AMW-2d Facility Permit Numbers 1302-MSWLF- and 1302-CDLF-1998 Notes: Only detections above laboratory method detection limits represented in figure. Figure 10 (AMW-2d) 0 5 10 15 20 25 30 35 40 45 50 Se p - 0 9 No v - 0 9 Ja n - 1 0 Ma r - 1 0 Ma y - 1 0 Ju l - 1 0 Se p - 1 0 No v - 1 0 Ja n - 1 1 Ma r - 1 1 Ma y - 1 1 Ju l - 1 1 Se p - 1 1 No v - 1 1 Ja n - 1 2 Ma r - 1 2 Ma y - 1 2 Ju l - 1 2 Se p - 1 2 No v - 1 2 Ja n - 1 3 Ma r - 1 3 Ma y - 1 3 Ju l - 1 3 Se p - 1 3 No v - 1 3 Ja n - 1 4 Ma r - 1 4 Ma y - 1 4 Ju l - 1 4 Se p - 1 4 No v - 1 4 Ja n - 1 5 Ma r - 1 5 Ma y - 1 5 Ju l - 1 5 Se p - 1 5 No v - 1 5 Ja n - 1 6 Ma r - 1 6 Ma y - 1 6 Ju l - 1 6 Se p - 1 6 No v - 1 6 To t a l D e t e c t e d V O C s ( u g / l ) Date Phase I Emulsified Oil Injection -November 2009 Phase II -February 2014         Appendix A  P AC E AN A L YT I C A L S E R VI C E S , I N C . En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h Pr o j e c t : C a b a r r u s C o - 2 & 3 Ra l e i g h , N C 2 7 6 1 2 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 M r . M a t C o l o n e W e a p p r e c i a t e t h e o p p o r t u n i t y t o p r o v i d e t h e a n a l y t i c a l s u p p o r t f o r y o u r p r o j e c t . T h e a n a l y t i c a l r e s u l t s i n t h i s r e p o r t a r e b a s e d u p o n i n f o r m a t i o n s u p p l i e d b y y o u , t h e cl i e n t , a n d a r e f o r y o u r e x c l u s i v e u s e . I f y o u h a v e a n y q u e s t i o n s r e g a r d i n g t h i s d a t a p a c k a g e , p l e a s e d o n o t h e s i t a t e t o c a l l . Pa c e An a l y t i c a l S e r v i c e s , Inc. certifies that th e f o l l o w i n g a n a l y t i c a l r e s u l t s m e e t a l l r e q u i r e m e n t s o f t h e N a t i o n a l E n v i r o n m e n t a l L a b o r a t o r y Ac c r e d i t a t i o n C o n f e r e n c e (N E L A C ) . A l l t e s t r e s u l t s r e l a t e o n l y t o t h e sa m p l e s a n a l y z e d . La b o r a t o r y R e p o r t Pr o j e c t # : [ n o n e ] Pr e p a r e d F o r : At t e n t i o n : No v e m b e r 3 0 , 2 0 1 6 Re p o r t N u m b e r : AZ K 0 0 4 4 Ap p r o v e d : Th i s r e p o r t m a y n o t b e r e p r o d u c e d , e x c e p t i n f u l l , wi t h o u t w r i t t e n a p p r o v a l f r o m P a c e An a l y t i c a l S e r v i c e s , I n c . Page 1 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Sa m p l e I D La b o r a t o r y I D Ma t r i x Da t e S a m p l e d AN A L YT I C A L R E P O R T F O R S A M P L E S Date Received 13 0 2 - C D 1 S AZ K 0 0 4 4 - 0 1 1 1/ 0 1 / 1 6 0 9 : 1 3 1 1/02/16 09:20 Gr o u n d W at e r 13 0 2 - C D 1 D AZ K 0 0 4 4 - 0 2 1 1/ 0 1 / 1 6 1 0 : 0 3 1 1/02/16 09:20 Gr o u n d W at e r 13 0 2 - A M W 2 S AZ K 0 0 4 4 - 0 3 1 1/ 0 1 / 1 6 1 5 : 0 9 1 1/02/16 09:20 Gr o u n d W at e r 13 0 2 - M W A AZ K 0 0 4 4 - 0 4 1 1/ 0 1 / 1 6 1 1: 0 6 1 1/02/16 09:20 Gr o u n d W at e r 13 0 2 - M W E AZ K 0 0 4 4 - 0 5 1 1/ 0 1 / 1 6 1 2 : 2 1 1 1/02/16 09:20 Gr o u n d W at e r 13 0 2 - M W E D e e p AZ K 0 0 4 4 - 0 6 1 1/ 0 1 / 1 6 1 3 : 4 6 1 1/02/16 09:20 Gr o u n d W at e r 13 0 2 - A M W 2 d AZ K 0 0 4 4 - 0 7 1 1/ 0 2 / 1 6 1 0 : 4 3 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - A M W 1 s AZ K 0 0 4 4 - 0 8 1 1/ 0 2 / 1 6 1 4 : 5 7 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W 3 AZ K 0 0 4 4 - 0 9 1 1/ 0 2 / 1 6 1 3 : 1 9 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W L AZ K 0 0 4 4 - 1 0 1 1/ 0 2 / 1 6 1 1: 5 6 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 4 R e p AZ K 0 0 4 4 - 11 1 1/ 0 1 / 1 6 0 8 : 1 7 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 4 R e p AZ K 0 0 4 4 - 1 2 1 1/ 0 2 / 1 6 0 8 : 1 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 6 AZ K 0 0 4 4 - 1 3 1 1/ 0 1 / 1 6 0 9 : 1 9 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 6 AZ K 0 0 4 4 - 1 4 1 1/ 0 2 / 1 6 0 8 : 3 6 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W 1 AZ K 0 0 4 4 - 1 5 1 1/ 0 1 / 1 6 1 5 : 4 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W 1 AZ K 0 0 4 4 - 1 6 1 1/ 0 2 / 1 6 1 1: 2 3 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W C AZ K 0 0 4 4 - 1 7 1 1/ 0 1 / 1 6 1 3 : 5 9 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W C AZ K 0 0 4 4 - 1 8 1 1/ 0 2 / 1 6 1 0 : 4 5 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W J AZ K 0 0 4 4 - 1 9 1 1/ 0 1 / 1 6 1 1: 1 7 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W J AZ K 0 0 4 4 - 2 0 1 1/ 0 2 / 1 6 0 9 : 5 2 1 1/03/16 09:35 Gr o u n d W at e r Page 2 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Sa m p l e I D La b o r a t o r y I D Ma t r i x Da t e S a m p l e d AN A L YT I C A L R E P O R T F O R S A M P L E S Date Received 13 0 2 - M W K AZ K 0 0 4 4 - 2 1 1 1/ 0 1 / 1 6 1 3 : 3 7 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W K AZ K 0 0 4 4 - 2 2 1 1/ 0 2 / 1 6 1 0 : 5 6 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W X AZ K 0 0 4 4 - 2 3 1 1/ 0 1 / 1 6 1 1: 5 2 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - M W X AZ K 0 0 4 4 - 2 4 1 1/ 0 2 / 1 6 1 0 : 3 7 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - D u p l i c a t e AZ K 0 0 4 4 - 2 5 1 1/ 0 1 / 1 6 0 0 : 0 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - D u p l i c a t e AZ K 0 0 4 4 - 2 6 1 1/ 0 2 / 1 6 0 0 : 0 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - A M W 1 d AZ K 0 0 4 4 - 2 7 1 1/ 0 3 / 1 6 0 9 : 1 0 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - C D 1 S AZ K 0 0 4 4 - 2 8 1 1/ 0 3 / 1 6 1 3 : 0 7 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W B AZ K 0 0 4 4 - 2 9 1 1/ 0 2 / 1 6 1 2 : 0 3 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W B AZ K 0 0 4 4 - 3 0 1 1/ 0 3 / 1 6 0 8 : 1 2 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W D AZ K 0 0 4 4 - 3 1 1 1/ 0 2 / 1 6 1 1: 1 2 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W D AZ K 0 0 4 4 - 3 2 1 1/ 0 3 / 1 6 0 8 : 5 2 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W F AZ K 0 0 4 4 - 3 3 1 1/ 0 2 / 1 6 1 2 : 2 6 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W F AZ K 0 0 4 4 - 3 4 1 1/ 0 3 / 1 6 0 8 : 2 0 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W G AZ K 0 0 4 4 - 3 5 1 1/ 0 2 / 1 6 1 1: 3 7 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W G AZ K 0 0 4 4 - 3 6 1 1/ 0 3 / 1 6 0 8 : 0 5 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W H AZ K 0 0 4 4 - 3 7 1 1/ 0 2 / 1 6 1 4 : 1 7 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W H AZ K 0 0 4 4 - 3 8 1 1/ 0 3 / 1 6 0 9 : 0 5 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W H D e e p AZ K 0 0 4 4 - 3 9 1 1/ 0 2 / 1 6 1 4 : 5 4 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W H D e e p AZ K 0 0 4 4 - 4 0 1 1/ 0 3 / 1 6 0 9 : 0 7 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - M W I AZ K 0 0 4 4 - 4 1 1 1/ 0 2 / 1 6 1 3 : 4 0 1 1/03/16 17:30 Gr o u n d W at e r Page 3 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Sa m p l e I D La b o r a t o r y I D Ma t r i x Da t e S a m p l e d AN A L YT I C A L R E P O R T F O R S A M P L E S Date Received 13 0 2 - M W I AZ K 0 0 4 4 - 4 2 1 1/ 0 3 / 1 6 0 8 : 2 6 1 1/03/16 17:30 Gr o u n d W at e r 13 0 2 - T rip B l a n k AZ K 0 0 4 4 - 4 3 1 1/ 0 1 / 1 6 0 0 : 0 0 1 1/03/16 17:30 W at e r 13 0 2 - E q u i p m e n t B l a n k AZ K 0 0 4 4 - 4 4 1 1/ 0 3 / 1 6 1 7 : 2 7 1 1/03/16 17:30 W at e r Page 4 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Io n C h r o m a t o g r a p h An a l y s i s v i a E P A 90 5 6 A (H - 0 2 a n d Q M - 1 0 Q u a l i f i e r s ) : Or i g i n a l a n a l y s i s f o r s a m p l e s AZ K 00 4 4 - 0 1 ( C D - 1 S ) , A Z K 0 0 4 4 - 0 3 ( A M W - 2 S ) , an d AZ K 00 4 4 - 0 7 ( A M W - 2 d ) f o r N i t r a t e w a s p r e p a r e d w i t h i n t h e 4 8 - h o u r me t h o d - s p e c i f i e d h o l d i n g t i m e . H o w e v e r , t h e a n a l y t i c a l i n s t r u m e n t m a l f u n c t i o n e d , a n d a n a l y s i s c o u l d n o t b e c o m p l e t e d w i t h i n t h e h o l d i n g t i m e . Du e t o t h e i n s t r u m e n t m a l f u n c t i o n o n b a t c h 61 10 0 6 0 , t h e m a t r i x s p i k e a n d m a t r i x s p i k e d u p l i c a t e ( A Z K 0 0 4 4 - 0 3 , A M W - 2 S ) r e c o v e r i e s f e l l b e l o w t h e co n t r o l l i m i t s f o r c h l o r i d e , n i t r a t e , a n d s u l f a t e . Da t a p a s s e s o n t h e m e t h o d b l a n k a n d l a b o r a t o r y c o n t r o l s a m p l e r e c o v e r i e s , a n d q u a l i f i e r s a r e a p p l i e d a s a p p r o p r i a t e . Ca s e N a r r a t i v e Page 5 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 1 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 On S i t e EP A 9 0 5 0 A 11 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 SM 4 5 0 0 - O G 44 9 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 EP A 9 0 4 0 C 5. 0 5 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 NA 36 0 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 SM 2 5 5 0 B 16 . 1 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 EP A 1 8 0 . 1 5. 7 2 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 NA 25 . 2 3 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 46 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 5 2 2 0 D 26 5 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 71 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 ND EP A 9 0 6 0 A ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 17:56 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 42 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10060 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 14:40 1 1/ 0 2 / 1 6 1 4 : 2 8 EP A 9 0 5 6 A 67 ug / L 1 Ni t r a t e a s N 50 H- 0 2 61 10060 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/07/16 14:40 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10060 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 14:40 1 1/ 0 2 / 1 6 1 4 : 2 8 Me t a l s , T ot a l Page 6 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 1 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 30 . 5 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 2 3 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 2 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 6 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 8 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 5 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 3 0 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 64 7 ug / L 1 Ir o n 40 . 0 61 10182 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 70 . 8 ug / L 1 Ma n g a n e s e 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 13:21 1 1/ 0 4 / 1 6 0 8 : 4 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 7 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 1 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 8 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 1 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 9 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 1 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 96 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 10 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 0 4 4 - 0 2 AZK0044 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 On S i t e EP A 9 0 5 0 A 12 4 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 SM 4 5 0 0 - O G 31 0 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 EP A 9 0 4 0 C 5. 3 4 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 NA 33 0 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 SM 2 5 5 0 B 15 . 9 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 EP A 1 8 0 . 1 8. 2 7 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 NA 27 . 8 3 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 52 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 99 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 In o r g a n i c An i o n s EP A 9 0 5 6 A 34 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10060 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 15:00 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10060 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 15:00 1 1/ 0 2 / 1 6 1 4 : 2 8 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 32 . 6 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 11 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 0 4 4 - 0 2 AZK0044 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 Me t a l s , T ot a l EP A 6 0 2 0 B 1. 1 9 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 7 7 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 8 2 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 3 3 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 2 4 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 7. 9 6 ug / L 1 V an a d i u m 25 . 0 J 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 2 9 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 12 0 0 ug / L 1 Ir o n 40 . 0 61 10182 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 31 . 3 ug / L 1 Ma n g a n e s e 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 13:24 1 1/ 0 4 / 1 6 0 8 : 4 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 12 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 0 4 4 - 0 2 AZK0044 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 13 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 0 4 4 - 0 2 AZK0044 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 14 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 0 4 4 - 0 2 AZK0044 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 15 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 3 AZK0044 1 1/ 0 1 / 1 6 1 5 : 0 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 On S i t e EP A 9 0 5 0 A 16 4 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 SM 4 5 0 0 - O G 33 8 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 EP A 9 0 4 0 C 4. 9 2 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 NA 23 5 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 SM 2 5 5 0 B 16 . 4 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 EP A 1 8 0 . 1 7. 9 7 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 NA 23 . 3 2 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 15:09 1 1/ 0 1 / 1 6 1 5 : 0 9 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 69 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 BO D - 4 61 10082 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 10:47 1 1/ 0 3 / 1 6 0 9 : 5 4 SM 5 2 2 0 D 25 8 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 10 2 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 EP A 9 0 6 0 A 10 2 0 ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 18:13 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 37 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10060 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 15:21 1 1/ 0 2 / 1 6 1 4 : 2 8 EP A 9 0 5 6 A 31 0 ug / L 1 Ni t r a t e a s N 50 H- 0 2 61 10060 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/07/16 15:21 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10060 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 15:21 1 1/ 0 2 / 1 6 1 4 : 2 8 Page 16 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 3 AZK0044 1 1/ 0 1 / 1 6 1 5 : 0 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 46 . 5 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 7 3 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 6 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 5 8 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 5 7 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 7 4 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 8 1 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 19:45 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 1 7 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:08 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 17 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 3 AZK0044 1 1/ 0 1 / 1 6 1 5 : 0 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 10 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 8 ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 8. 0 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 18 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 3 AZK0044 1 1/ 0 1 / 1 6 1 5 : 0 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 9 ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 4. 1 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 3. 2 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 19 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 S Gr o u n d W at e r AZ K 0 0 4 4 - 0 3 AZK0044 1 1/ 0 1 / 1 6 1 5 : 0 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 2 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 13:56 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 20 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W A Gr o u n d W at e r AZ K 0 0 4 4 - 0 4 AZK0044 1 1/ 0 1 / 1 6 1 1: 0 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 On S i t e EP A 9 0 5 0 A 41 2 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 SM 4 5 0 0 - O G 16 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 NA 15 0 0 ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 EP A 9 0 4 0 C 4. 7 7 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 NA 20 5 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 SM 2 5 5 0 B 16 . 5 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 EP A 1 8 0 . 1 4. 0 9 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 NA 42 . 4 1 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 1 1:06 1 1/ 0 1 / 1 6 1 1:06 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 12 9 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 5 2 1 0 B 12 0 0 0 ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 BO D - 4 61 10082 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 10:47 1 1/ 0 3 / 1 6 0 9 : 5 4 SM 5 2 2 0 D 33 8 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 20 8 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 EP A 9 0 6 0 A 32 8 0 ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 27 0 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10060 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 15:41 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 61 10060 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/03/16 00:21 1 1/ 0 2 / 1 6 1 4 : 2 8 EP A 9 0 5 6 A 19 0 0 0 ug / L 1 Su l f a t e 50 0 0 61 10060 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 15:41 1 1/ 0 2 / 1 6 1 4 : 2 8 Page 21 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W A Gr o u n d W at e r AZ K 0 0 4 4 - 0 4 AZK0044 1 1/ 0 1 / 1 6 1 1: 0 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 19:51 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 48 . 6 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 19:51 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 7 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 19:51 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 7. 2 5 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 19:51 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 19 . 2 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 19:51 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 19:51 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 8 5 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:13 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 11 ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 22 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W A Gr o u n d W at e r AZ K 0 0 4 4 - 0 4 AZK0044 1 1/ 0 1 / 1 6 1 1: 0 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 6 ug / L 1 Ch l o r o b e n z e n e 3. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 5. 7 ug / L 1 Ch l o r o e t h a n e 10 J 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 36 ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 17 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 6 ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 14 0 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 2. 6 ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 23 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W A Gr o u n d W at e r AZ K 0 0 4 4 - 0 4 AZK0044 1 1/ 0 1 / 1 6 1 1: 0 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 7 ug / L 1 Et h y l b e n z e n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 4 ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 5. 7 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 3. 8 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 9 ug / L 1 V in y l C h l o r i d e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 4. 7 ug / L 1 Xy l e n e s , t o t a l 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 24 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W A Gr o u n d W at e r AZ K 0 0 4 4 - 0 4 AZK0044 1 1/ 0 1 / 1 6 1 1: 0 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 95 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 14:23 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 25 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E Gr o u n d W at e r AZ K 0 0 4 4 - 0 5 AZK0044 1 1/ 0 1 / 1 6 1 2 : 2 1 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 On S i t e EP A 9 0 5 0 A 1 14 0 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 SM 4 5 0 0 - O G 37 9 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 NA 30 0 0 ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 EP A 9 0 4 0 C 5. 5 9 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 NA 48 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 SM 2 5 5 0 B 17 . 6 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 EP A 1 8 0 . 1 5. 2 3 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 NA 29 . 4 0 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 12:21 1 1/ 0 1 / 1 6 1 2 : 2 1 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 47 5 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 BO D - 4 61 10082 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 10:47 1 1/ 0 3 / 1 6 0 9 : 5 4 SM 5 2 2 0 D 33 4 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 56 5 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 EP A 9 0 6 0 A 50 6 0 ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 18:45 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 50 0 0 0 ug / L 10 Ch l o r i d e 10 0 0 0 61 10060 EP A 9 0 5 6 A 10 0 0 0 16 8 8 7 - 0 0 - 6 1 1/15/16 06:35 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 61 10060 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/03/16 00:44 1 1/ 0 2 / 1 6 1 4 : 2 8 EP A 9 0 5 6 A 78 0 0 0 ug / L 10 Su l f a t e 50 0 0 0 61 10060 EP A 9 0 5 6 A 50 0 0 0 14 8 0 8 - 7 9 - 8 1 1/15/16 06:35 1 1/ 0 2 / 1 6 1 4 : 2 8 Page 26 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E Gr o u n d W at e r AZ K 0 0 4 4 - 0 5 AZK0044 1 1/ 0 1 / 1 6 1 2 : 2 1 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 29 7 ug / L 1 Ba r i u m 10 0 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 5 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 4 4 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 7 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1 1. 4 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 19:57 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 1 3 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:19 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 Be n z e n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 27 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E Gr o u n d W at e r AZ K 0 0 4 4 - 0 5 AZK0044 1 1/ 0 1 / 1 6 1 2 : 2 1 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 3. 2 ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 8. 0 ug / L 1 Ch l o r o e t h a n e 10 J 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 15 ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 11 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 1 ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 18 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 28 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E Gr o u n d W at e r AZ K 0 0 4 4 - 0 5 AZK0044 1 1/ 0 1 / 1 6 1 2 : 2 1 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 4. 5 ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 29 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E Gr o u n d W at e r AZ K 0 0 4 4 - 0 5 AZK0044 1 1/ 0 1 / 1 6 1 2 : 2 1 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 99 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 14:51 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 30 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 0 6 AZK0044 1 1/ 0 1 / 1 6 1 3 : 4 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 On S i t e EP A 9 0 5 0 A 95 9 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 SM 4 5 0 0 - O G 23 0 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 NA 20 0 0 ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 EP A 9 0 4 0 C 5. 8 9 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 NA -3 9 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 SM 2 5 5 0 B 18 . 1 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 EP A 1 8 0 . 1 7. 9 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 NA 59 . 9 0 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 13:46 1 1/ 0 1 / 1 6 1 3 : 4 6 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 41 5 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 5 2 1 0 B 27 0 0 0 ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 BO D - 4 61 10082 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 10:47 1 1/ 0 3 / 1 6 0 9 : 5 4 SM 5 2 2 0 D 62 5 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 47 5 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 EP A 9 0 6 0 A 31 6 0 ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 19:02 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 44 0 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10060 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 19:08 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 61 10060 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/03/16 01:07 1 1/ 0 2 / 1 6 1 4 : 2 8 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10060 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 19:08 1 1/ 0 2 / 1 6 1 4 : 2 8 Page 31 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 0 6 AZK0044 1 1/ 0 1 / 1 6 1 3 : 4 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:03 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 4 3 ug / L 1 Ar s e n i c 10 . 0 J 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 20:03 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 19 6 0 ug / L 50 Ba r i u m 50 0 0 J 61 10182 EP A 3 0 0 5 A 21 . 8 74 4 0 - 3 9 - 3 1 1/29/16 14:14 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 2 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:03 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 8 ug / L 1 Ca d m i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 34 . 5 ug / L 1 Co b a l t 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 3 4 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 18 . 5 ug / L 1 Le a d 10 . 0 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:03 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 14 . 6 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:03 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:03 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 19 . 3 ug / L 1 Zi n c 10 . 0 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:25 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 Be n z e n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 32 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 0 6 AZK0044 1 1/ 0 1 / 1 6 1 3 : 4 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 1 ug / L 1 Ch l o r o b e n z e n e 3. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 26 ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 5. 9 ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 7 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 8 ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 33 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 0 6 AZK0044 1 1/ 0 1 / 1 6 1 3 : 4 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 7 ug / L 1 T olu e n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 4. 8 ug / L 1 Xy l e n e s , t o t a l 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 34 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W E D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 0 6 AZK0044 1 1/ 0 1 / 1 6 1 3 : 4 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 2 / 1 6 0 9 : 2 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 15:18 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 35 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 d Gr o u n d W at e r AZ K 0 0 4 4 - 0 7 AZK0044 1 1/ 0 2 / 1 6 1 0 : 4 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 35 6 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 SM 4 5 0 0 - O G 21 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 EP A 9 0 4 0 C 5. 5 2 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 NA 34 6 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 SM 2 5 5 0 B 16 . 5 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 EP A 1 8 0 . 1 4. 1 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 NA 22 . 6 8 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 10:43 1 1/ 0 2 / 1 6 1 0 : 4 3 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 1 10 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 61 10108 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 12:45 1 1/ 0 3 / 1 6 1 4 : 0 0 SM 5 2 2 0 D 31 2 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 10 9 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 ND EP A 9 0 6 0 A ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 19:19 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 42 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10098 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/04/16 12:31 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 H- 0 2 61 10098 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/04/16 12:31 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10098 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/04/16 12:31 1 1/ 0 3 / 1 6 1 3 : 2 6 Page 36 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 d Gr o u n d W at e r AZ K 0 0 4 4 - 0 7 AZK0044 1 1/ 0 2 / 1 6 1 0 : 4 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 67 . 7 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 0 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:31 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:31 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 6 6 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:31 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 9 0 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:31 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:08 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:31 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 0 2 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:31 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 4 ug / L 1 Be n z e n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 37 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 d Gr o u n d W at e r AZ K 0 0 4 4 - 0 7 AZK0044 1 1/ 0 2 / 1 6 1 0 : 4 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 Ch l o r o e t h a n e 10 J 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 5. 0 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 6. 2 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 38 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 d Gr o u n d W at e r AZ K 0 0 4 4 - 0 7 AZK0044 1 1/ 0 2 / 1 6 1 0 : 4 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 2. 0 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 2 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 39 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 2 d Gr o u n d W at e r AZ K 0 0 4 4 - 0 7 AZK0044 1 1/ 0 2 / 1 6 1 0 : 4 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 15:46 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 40 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 s Gr o u n d W at e r AZ K 0 0 4 4 - 0 8 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 29 7 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 SM 4 5 0 0 - O G 16 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 EP A 9 0 4 0 C 5. 0 2 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 NA 37 7 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 SM 2 5 5 0 B 18 . 8 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 EP A 1 8 0 . 1 5. 9 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 NA 50 . 9 9 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 14:57 1 1/ 0 2 / 1 6 1 4 : 5 7 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 10 0 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 61 10108 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 12:45 1 1/ 0 3 / 1 6 1 4 : 0 0 SM 5 2 2 0 D 23 6 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 10 5 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 ND EP A 9 0 6 0 A ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 19:37 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 33 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10098 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/04/16 12:08 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 61 10098 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/04/16 12:08 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10098 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/04/16 12:08 1 1/ 0 3 / 1 6 1 3 : 2 6 Page 41 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 s Gr o u n d W at e r AZ K 0 0 4 4 - 0 8 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 71 . 7 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 5 6 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:36 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:36 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 5 5 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:36 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 1 9 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:36 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:14 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:36 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 7 8 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:36 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 2 ug / L 1 Be n z e n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 42 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 s Gr o u n d W at e r AZ K 0 0 4 4 - 0 8 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 1 ug / L 1 Ch l o r o e t h a n e 10 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 24 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 2. 8 ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 15 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 43 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 s Gr o u n d W at e r AZ K 0 0 4 4 - 0 8 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 7. 1 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 9 ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 44 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 s Gr o u n d W at e r AZ K 0 0 4 4 - 0 8 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 95 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 12:32 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 45 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 3 Gr o u n d W at e r AZ K 0 0 4 4 - 0 9 AZK0044 1 1/ 0 2 / 1 6 1 3 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 24 6 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 SM 4 5 0 0 - O G 35 0 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 EP A 9 0 4 0 C 5. 5 2 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 NA 43 9 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 SM 2 5 5 0 B 20 . 6 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 EP A 1 8 0 . 1 4. 8 7 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 NA 14 . 5 9 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 13:19 1 1/ 0 2 / 1 6 1 3 : 1 9 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 60 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 61 10108 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 12:45 1 1/ 0 3 / 1 6 1 4 : 0 0 SM 5 2 2 0 D 14 9 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 10 7 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 ND EP A 9 0 6 0 A ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 19:53 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 41 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10098 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/04/16 1 1:45 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 61 10098 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/04/16 1 1:45 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10098 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/04/16 1 1:45 1 1/ 0 3 / 1 6 1 3 : 2 6 Page 46 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 3 Gr o u n d W at e r AZ K 0 0 4 4 - 0 9 AZK0044 1 1/ 0 2 / 1 6 1 3 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 27 . 4 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 6 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 12:42 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 12:42 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 12:42 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 5 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 0 0 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 12:42 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:20 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 12:42 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 3 6 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 12:42 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 47 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 3 Gr o u n d W at e r AZ K 0 0 4 4 - 0 9 AZK0044 1 1/ 0 2 / 1 6 1 3 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 14 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 2. 4 ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 4. 8 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 48 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 3 Gr o u n d W at e r AZ K 0 0 4 4 - 0 9 AZK0044 1 1/ 0 2 / 1 6 1 3 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 14 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 5. 7 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 2 ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/09/16 21:37 1 1/ 0 9 / 1 6 2 1 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 0 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/09/16 21:37 1 1/ 0 9 / 1 6 2 1 : 0 0 80 - 1 2 0 Page 49 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 3 Gr o u n d W at e r AZ K 0 0 4 4 - 0 9 AZK0044 1 1/ 0 2 / 1 6 1 3 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 99 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/09/16 21:37 1 1/ 0 9 / 1 6 2 1 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 90 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 90 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/09/16 21:37 1 1/ 0 9 / 1 6 2 1 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/09/16 21:37 1 1/ 0 9 / 1 6 2 1 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 12:59 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 50 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W L Gr o u n d W at e r AZ K 0 0 4 4 - 1 0 AZK0044 1 1/ 0 2 / 1 6 1 1: 5 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 14 6 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 SM 4 5 0 0 - O G 34 9 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 EP A 9 0 4 0 C 5. 11 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 NA 48 6 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 SM 2 5 5 0 B 18 . 1 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 EP A 1 8 0 . 1 4. 7 3 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 NA 13 . 8 2 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 1 1:56 1 1/ 0 2 / 1 6 1 1:56 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 40 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 61 10108 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/08/16 12:45 1 1/ 0 3 / 1 6 1 4 : 0 0 SM 5 2 2 0 D 12 9 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 57 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 ND EP A 9 0 6 0 A ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 20:10 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 32 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10098 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/04/16 1 1:22 1 1/ 0 3 / 1 6 1 3 : 2 6 EP A 9 0 5 6 A 85 ug / L 1 Ni t r a t e a s N 50 61 10098 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/04/16 1 1:22 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10098 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/04/16 1 1:22 1 1/ 0 3 / 1 6 1 3 : 2 6 Page 51 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W L Gr o u n d W at e r AZ K 0 0 4 4 - 1 0 AZK0044 1 1/ 0 2 / 1 6 1 1: 5 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 35 . 2 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 0 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 0 4 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:37 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 4 6 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 13:27 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 52 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W L Gr o u n d W at e r AZ K 0 0 4 4 - 1 0 AZK0044 1 1/ 0 2 / 1 6 1 1: 5 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 53 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W L Gr o u n d W at e r AZ K 0 0 4 4 - 1 0 AZK0044 1 1/ 0 2 / 1 6 1 1: 5 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 54 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W L Gr o u n d W at e r AZ K 0 0 4 4 - 1 0 AZK0044 1 1/ 0 2 / 1 6 1 1: 5 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 20:19 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 55 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 11 AZK0044 1 1/ 0 1 / 1 6 0 8 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 20 9 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 SM 4 5 0 0 - O G 13 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 EP A 9 0 4 0 C 5. 2 8 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 NA 79 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 SM 2 5 5 0 B 17 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 NA 10 . 2 5 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 56 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 11 AZK0044 1 1/ 0 1 / 1 6 0 8 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 57 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 11 AZK0044 1 1/ 0 1 / 1 6 0 8 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 58 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 1 2 AZK0044 1 1/ 0 2 / 1 6 0 8 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 3. 2 1 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 08:10 1 1/ 0 2 / 1 6 0 8 : 1 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 46 . 3 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 7 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 5 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 5 9 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 1 8 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 9 0 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 1 8 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 11 ug / L 1 Se l e n i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 18 . 1 ug / L 1 V an a d i u m 25 . 0 J 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 8. 8 1 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 59 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 6 Gr o u n d W at e r AZ K 0 0 4 4 - 1 3 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 29 2 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 SM 4 5 0 0 - O G 13 8 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 EP A 9 0 4 0 C 5. 6 2 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 NA - 4 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 SM 2 5 5 0 B 16 . 9 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 NA 32 . 9 6 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 09:19 1 1/ 0 1 / 1 6 0 9 : 1 9 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 60 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 6 Gr o u n d W at e r AZ K 0 0 4 4 - 1 3 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 2. 2 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 61 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 6 Gr o u n d W at e r AZ K 0 0 4 4 - 1 3 AZK0044 1 1/ 0 1 / 1 6 0 9 : 1 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 9 ug / L 1 T ric h l o r o e t h e n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 14:22 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 62 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 6 Gr o u n d W at e r AZ K 0 0 4 4 - 1 4 AZK0044 1 1/ 0 2 / 1 6 0 8 : 3 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 29 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 08:36 1 1/ 0 2 / 1 6 0 8 : 3 6 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 8 9 ug / L 1 Ar s e n i c 10 . 0 J 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 63 . 7 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 3 3 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 6. 1 8 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 13:39 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 13 . 3 ug / L 1 Co b a l t 10 . 0 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 13:39 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 1 2 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 13:39 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 8 7 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 9. 1 2 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 13:39 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 2 9 ug / L 1 Se l e n i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 17 . 3 ug / L 1 V an a d i u m 25 . 0 J 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 13:39 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 10 . 1 ug / L 1 Zi n c 10 . 0 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 13:39 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 63 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 1 Gr o u n d W at e r AZ K 0 0 4 4 - 1 5 AZK0044 1 1/ 0 1 / 1 6 1 5 : 4 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 18 1 0 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 SM 4 5 0 0 - O G 10 3 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 EP A 9 0 4 0 C 6. 1 3 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 NA 34 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 SM 2 5 5 0 B 16 . 2 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 NA 12 . 6 1 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 15:40 1 1/ 0 1 / 1 6 1 5 : 4 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 64 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 1 Gr o u n d W at e r AZ K 0 0 4 4 - 1 5 AZK0044 1 1/ 0 1 / 1 6 1 5 : 4 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 0 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 65 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 1 Gr o u n d W at e r AZ K 0 0 4 4 - 1 5 AZK0044 1 1/ 0 1 / 1 6 1 5 : 4 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 14:49 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 66 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W 1 Gr o u n d W at e r AZ K 0 0 4 4 - 1 6 AZK0044 1 1/ 0 2 / 1 6 1 1: 2 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 8. 0 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 1 1:23 1 1/ 0 2 / 1 6 1 1:23 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 14 3 ug / L 1 Ba r i u m 10 0 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 3 9 ug / L 1 Ca d m i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 13 . 7 ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 8. 6 4 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 6 3 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 30 . 4 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 0 2 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 19:47 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 67 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W C Gr o u n d W at e r AZ K 0 0 4 4 - 1 7 AZK0044 1 1/ 0 1 / 1 6 1 3 : 5 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 24 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 SM 4 5 0 0 - O G 25 8 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 EP A 9 0 4 0 C 5. 5 2 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 NA 49 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 SM 2 5 5 0 B 17 . 4 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 NA 1 1. 6 9 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 13:59 1 1/ 0 1 / 1 6 1 3 : 5 9 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 68 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W C Gr o u n d W at e r AZ K 0 0 4 4 - 1 7 AZK0044 1 1/ 0 1 / 1 6 1 3 : 5 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 4 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 69 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W C Gr o u n d W at e r AZ K 0 0 4 4 - 1 7 AZK0044 1 1/ 0 1 / 1 6 1 3 : 5 9 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 10 0 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 15:17 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 70 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W C Gr o u n d W at e r AZ K 0 0 4 4 - 1 8 AZK0044 1 1/ 0 2 / 1 6 1 0 : 4 5 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 7. 0 7 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 10:45 1 1/ 0 2 / 1 6 1 0 : 4 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 1 6 ug / L 1 Ar s e n i c 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 34 . 0 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 8 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 10 . 3 ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 5 5 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 3 3 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 7 9 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 5 1 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 19:52 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 71 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W J Gr o u n d W at e r AZ K 0 0 4 4 - 1 9 AZK0044 1 1/ 0 1 / 1 6 1 1: 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 31 1 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 SM 4 5 0 0 - O G 26 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 EP A 9 0 4 0 C 6. 0 5 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 NA 21 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 SM 2 5 5 0 B 14 . 8 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 NA 30 . 4 2 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 1 1:17 1 1/ 0 1 / 1 6 1 1:17 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 72 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W J Gr o u n d W at e r AZ K 0 0 4 4 - 1 9 AZK0044 1 1/ 0 1 / 1 6 1 1: 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 73 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W J Gr o u n d W at e r AZ K 0 0 4 4 - 1 9 AZK0044 1 1/ 0 1 / 1 6 1 1: 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 15:44 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 74 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W J Gr o u n d W at e r AZ K 0 0 4 4 - 2 0 AZK0044 1 1/ 0 2 / 1 6 0 9 : 5 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 36 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 09:52 1 1/ 0 2 / 1 6 0 9 : 5 2 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 32 . 2 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 8 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 8 6 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 5 1 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 3 8 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 7 4 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 6 9 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 6 6 ug / L 1 Se l e n i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 14 . 9 ug / L 1 V an a d i u m 25 . 0 J 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1 1. 0 ug / L 1 Zi n c 10 . 0 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 19:58 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 75 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W K Gr o u n d W at e r AZ K 0 0 4 4 - 2 1 AZK0044 1 1/ 0 1 / 1 6 1 3 : 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 28 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 SM 4 5 0 0 - O G 18 9 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 EP A 9 0 4 0 C 5. 4 7 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 NA 14 9 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 SM 2 5 5 0 B 15 . 4 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 NA 24 . 5 6 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 13:37 1 1/ 0 1 / 1 6 1 3 : 3 7 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 76 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W K Gr o u n d W at e r AZ K 0 0 4 4 - 2 1 AZK0044 1 1/ 0 1 / 1 6 1 3 : 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 77 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W K Gr o u n d W at e r AZ K 0 0 4 4 - 2 1 AZK0044 1 1/ 0 1 / 1 6 1 3 : 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 96 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 16:12 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 78 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W K Gr o u n d W at e r AZ K 0 0 4 4 - 2 2 AZK0044 1 1/ 0 2 / 1 6 1 0 : 5 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 21 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 10:56 1 1/ 0 2 / 1 6 1 0 : 5 6 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 17 . 8 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 6 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 6 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 8 7 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 9 4 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 7 2 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 0 4 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 7 8 ug / L 1 Se l e n i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 0 1 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:04 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 79 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W X Gr o u n d W at e r AZ K 0 0 4 4 - 2 3 AZK0044 1 1/ 0 1 / 1 6 1 1: 5 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 27 5 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 SM 4 5 0 0 - O G 16 2 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 EP A 9 0 4 0 C 5. 9 4 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 NA 78 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 SM 2 5 5 0 B 15 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 NA 13 . 4 5 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 1 1:52 1 1/ 0 1 / 1 6 1 1:52 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 80 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W X Gr o u n d W at e r AZ K 0 0 4 4 - 2 3 AZK0044 1 1/ 0 1 / 1 6 1 1: 5 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 81 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W X Gr o u n d W at e r AZ K 0 0 4 4 - 2 3 AZK0044 1 1/ 0 1 / 1 6 1 1: 5 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 95 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 16:39 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 82 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W X Gr o u n d W at e r AZ K 0 0 4 4 - 2 4 AZK0044 1 1/ 0 2 / 1 6 1 0 : 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 3. 11 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 10:37 1 1/ 0 2 / 1 6 1 0 : 3 7 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 32 . 3 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 7 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 6 0 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 9 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 5 6 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 6 9 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:10 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 83 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 0 4 4 - 2 5 AZK0044 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 84 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 0 4 4 - 2 5 AZK0044 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 0. 9 ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 85 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 0 4 4 - 2 5 AZK0044 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 17:07 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 86 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 0 4 4 - 2 6 AZK0044 1 1/ 0 2 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 0 5 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 1 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 6 3 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 8 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 1 7 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 0 8 ug / L 1 Se l e n i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 1 8 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:27 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 87 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 d Gr o u n d W at e r AZ K 0 0 4 4 - 2 7 AZK0044 1 1/ 0 3 / 1 6 0 9 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 58 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 SM 4 5 0 0 - O G 17 3 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 NA 20 0 0 ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 EP A 9 0 4 0 C 5. 0 0 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 NA 19 9 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 SM 2 5 5 0 B 13 . 3 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 EP A 1 8 0 . 1 8. 0 5 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 NA 51 . 7 1 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/03/16 09:10 1 1/ 0 3 / 1 6 0 9 : 1 0 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 21 5 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 5 2 1 0 B 10 0 0 0 ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 6110115 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/09/16 07:52 1 1/ 0 4 / 1 6 0 8 : 5 6 SM 5 2 2 0 D 41 6 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 24 2 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 EP A 9 0 6 0 A 34 2 0 ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 20:26 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 59 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10098 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/04/16 17:32 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Ni t r a t e a s N 50 61 10098 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/04/16 17:32 1 1/ 0 3 / 1 6 1 3 : 2 6 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10098 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/04/16 17:32 1 1/ 0 3 / 1 6 1 3 : 2 6 Page 88 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 d Gr o u n d W at e r AZ K 0 0 4 4 - 2 7 AZK0044 1 1/ 0 3 / 1 6 0 9 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 12 8 ug / L 1 Ba r i u m 10 0 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 7 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 2 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 6. 0 9 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 1 2 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 8 1 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 9. 3 0 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 6. 6 5 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:33 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 4 ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 89 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 d Gr o u n d W at e r AZ K 0 0 4 4 - 2 7 AZK0044 1 1/ 0 3 / 1 6 0 9 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 2. 2 ug / L 1 Ch l o r o e t h a n e 10 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 0 ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 26 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 8 ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 7. 0 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 90 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 d Gr o u n d W at e r AZ K 0 0 4 4 - 2 7 AZK0044 1 1/ 0 3 / 1 6 0 9 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 T ric h l o r o e t h e n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 13 ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 91 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - A M W 1 d Gr o u n d W at e r AZ K 0 0 4 4 - 2 7 AZK0044 1 1/ 0 3 / 1 6 0 9 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 17:34 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 92 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 0 4 4 - 2 8 AZK0044 1 1/ 0 3 / 1 6 1 3 : 0 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 14 5 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 SM 4 5 0 0 - O G 47 1 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 EP A 9 0 4 0 C 5. 8 0 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 NA 23 7 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 SM 2 5 5 0 B 18 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 EP A 1 8 0 . 1 9. 2 6 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 NA 25 . 2 8 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/03/16 13:07 1 1/ 0 3 / 1 6 1 3 : 0 7 Ge n e r a l C h e m i s t r y ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 6110115 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/09/16 07:52 1 1/ 0 4 / 1 6 0 8 : 5 6 Page 93 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W B Gr o u n d W at e r AZ K 0 0 4 4 - 2 9 AZK0044 1 1/ 0 2 / 1 6 1 2 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 10 8 0 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 SM 4 5 0 0 - O G 21 1 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 EP A 9 0 4 0 C 6. 4 4 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 NA -7 9 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 SM 2 5 5 0 B 17 . 5 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 NA 2. 8 9 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 12:03 1 1/ 0 2 / 1 6 1 2 : 0 3 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 94 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W B Gr o u n d W at e r AZ K 0 0 4 4 - 2 9 AZK0044 1 1/ 0 2 / 1 6 1 2 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 95 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W B Gr o u n d W at e r AZ K 0 0 4 4 - 2 9 AZK0044 1 1/ 0 2 / 1 6 1 2 : 0 3 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 18:02 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 96 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W B Gr o u n d W at e r AZ K 0 0 4 4 - 3 0 AZK0044 1 1/ 0 3 / 1 6 0 8 : 1 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 8. 6 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 08:12 1 1/ 0 3 / 1 6 0 8 : 1 2 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 4 3 ug / L 1 Ar s e n i c 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 19 6 ug / L 1 Ba r i u m 10 0 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 13 . 5 ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 4 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 6. 8 4 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 7 1 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:38 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 97 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W D Gr o u n d W at e r AZ K 0 0 4 4 - 3 1 AZK0044 1 1/ 0 2 / 1 6 1 1: 1 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 62 7 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 SM 4 5 0 0 - O G 15 1 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 EP A 9 0 4 0 C 5. 4 3 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 NA 69 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 SM 2 5 5 0 B 16 . 5 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 NA 26 . 8 9 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 1 1:12 1 1/ 0 2 / 1 6 1 1:12 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 6. 5 ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 8 ug / L 1 Ch l o r o b e n z e n e 3. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 3 ug / L 1 Ch l o r o e t h a n e 10 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 98 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W D Gr o u n d W at e r AZ K 0 0 4 4 - 3 1 AZK0044 1 1/ 0 2 / 1 6 1 1: 1 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 12 ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 5 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 48 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 99 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W D Gr o u n d W at e r AZ K 0 0 4 4 - 3 1 AZK0044 1 1/ 0 2 / 1 6 1 1: 1 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 2. 6 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 1 ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 3. 2 ug / L 1 Xy l e n e s , t o t a l 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 95 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 18:29 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 100 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W D Gr o u n d W at e r AZ K 0 0 4 4 - 3 2 AZK0044 1 1/ 0 3 / 1 6 0 8 : 5 2 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 6. 3 1 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 08:52 1 1/ 0 3 / 1 6 0 8 : 5 2 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 13 4 ug / L 1 Ba r i u m 10 0 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 0 9 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 8. 7 5 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 8 5 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 1 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 19 . 9 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 6 4 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:44 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 101 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W F Gr o u n d W at e r AZ K 0 0 4 4 - 3 3 AZK0044 1 1/ 0 2 / 1 6 1 2 : 2 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 1 14 0 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 SM 4 5 0 0 - O G 12 3 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 EP A 9 0 4 0 C 6. 2 5 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 NA -7 2 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 SM 2 5 5 0 B 16 . 6 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 NA 10 . 4 5 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 12:26 1 1/ 0 2 / 1 6 1 2 : 2 6 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 Ch l o r o e t h a n e 10 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 102 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W F Gr o u n d W at e r AZ K 0 0 4 4 - 3 3 AZK0044 1 1/ 0 2 / 1 6 1 2 : 2 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 103 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W F Gr o u n d W at e r AZ K 0 0 4 4 - 3 3 AZK0044 1 1/ 0 2 / 1 6 1 2 : 2 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 18:57 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 104 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W F Gr o u n d W at e r AZ K 0 0 4 4 - 3 4 AZK0044 1 1/ 0 3 / 1 6 0 8 : 2 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 6. 3 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 08:20 1 1/ 0 3 / 1 6 0 8 : 2 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 23 1 ug / L 1 Ba r i u m 10 0 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 1 4 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 7. 6 4 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co p p e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 6 3 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Zi n c 10 . 0 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:50 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 105 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W G Gr o u n d W at e r AZ K 0 0 4 4 - 3 5 AZK0044 1 1/ 0 2 / 1 6 1 1: 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 23 2 0 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 SM 4 5 0 0 - O G 10 9 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 EP A 9 0 4 0 C 6. 0 7 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 NA -8 0 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 SM 2 5 5 0 B 17 . 6 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 NA 9. 5 4 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 1 1:37 1 1/ 0 2 / 1 6 1 1:37 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 Be n z e n e 1. 0 J 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 5. 6 ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 1. 2 ug / L 1 Ch l o r o e t h a n e 10 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 106 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W G Gr o u n d W at e r AZ K 0 0 4 4 - 3 5 AZK0044 1 1/ 0 2 / 1 6 1 1: 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 7 ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 3. 4 ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 107 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W G Gr o u n d W at e r AZ K 0 0 4 4 - 3 5 AZK0044 1 1/ 0 2 / 1 6 1 1: 3 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 19:25 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 108 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W G Gr o u n d W at e r AZ K 0 0 4 4 - 3 6 AZK0044 1 1/ 0 3 / 1 6 0 8 : 0 5 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 0. 6 2 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 08:05 1 1/ 0 3 / 1 6 0 8 : 0 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 6. 6 5 ug / L 1 Ar s e n i c 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 41 8 ug / L 1 Ba r i u m 10 0 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 0 9 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 2 3 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 6 7 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 0 0 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Le a d 10 . 0 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 3 6 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 0 4 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 20:55 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 109 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H Gr o u n d W at e r AZ K 0 0 4 4 - 3 7 AZK0044 1 1/ 0 2 / 1 6 1 4 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 21 1 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 SM 4 5 0 0 - O G 16 3 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 EP A 9 0 4 0 C 5. 5 3 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 NA 11 8 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 SM 2 5 5 0 B 15 . 3 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 NA 25 . 9 4 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 14:17 1 1/ 0 2 / 1 6 1 4 : 1 7 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 110 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H Gr o u n d W at e r AZ K 0 0 4 4 - 3 7 AZK0044 1 1/ 0 2 / 1 6 1 4 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 111 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H Gr o u n d W at e r AZ K 0 0 4 4 - 3 7 AZK0044 1 1/ 0 2 / 1 6 1 4 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 95 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 19:52 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 112 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H Gr o u n d W at e r AZ K 0 0 4 4 - 3 8 AZK0044 1 1/ 0 3 / 1 6 0 9 : 0 5 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 59 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 09:05 1 1/ 0 3 / 1 6 0 9 : 0 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 67 . 8 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 3 3 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 8 1 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 9 6 ug / L 1 Co b a l t 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 8 6 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 7 8 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 5. 5 9 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 8 7 ug / L 1 Se l e n i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 10 . 7 ug / L 1 V an a d i u m 25 . 0 J 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 15 . 7 ug / L 1 Zi n c 10 . 0 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 21:01 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 113 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 3 9 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 4 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 33 7 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 SM 4 5 0 0 - O G 22 1 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 EP A 9 0 4 0 C 5. 9 1 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 NA 10 5 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 SM 2 5 5 0 B 15 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 NA 26 . 2 1 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 14:54 1 1/ 0 2 / 1 6 1 4 : 5 4 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 114 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 3 9 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 4 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 115 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 3 9 AZK0044 1 1/ 0 2 / 1 6 1 4 : 5 4 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 2 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 21:14 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 116 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W H D e e p Gr o u n d W at e r AZ K 0 0 4 4 - 4 0 AZK0044 1 1/ 0 3 / 1 6 0 9 : 0 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 16 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 09:07 1 1/ 0 3 / 1 6 0 9 : 0 7 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 54 . 7 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 1 4 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 5 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 8 9 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Zi n c 10 . 0 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 21:07 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 117 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W I Gr o u n d W at e r AZ K 0 0 4 4 - 4 1 AZK0044 1 1/ 0 2 / 1 6 1 3 : 4 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 9 0 5 0 A 16 4 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 SM 4 5 0 0 - O G 13 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 EP A 9 0 4 0 C 5. 6 5 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 NA 68 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 SM 2 5 5 0 B 15 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 NA 45 . 5 8 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/02/16 13:40 1 1/ 0 2 / 1 6 1 3 : 4 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10254 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10254 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10254 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10254 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10254 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10254 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 Page 118 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W I Gr o u n d W at e r AZ K 0 0 4 4 - 4 1 AZK0044 1 1/ 0 2 / 1 6 1 3 : 4 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10254 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10254 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 4. 6 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 10254 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 1. 0 ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 J 61 10254 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 2. 0 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 10254 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10254 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 0. 6 ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 J 61 10254 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10254 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10254 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 Page 119 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W I Gr o u n d W at e r AZ K 0 0 4 4 - 4 1 AZK0044 1 1/ 0 2 / 1 6 1 3 : 4 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 3. 5 ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 1. 3 ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 0. 8 ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 J 61 10254 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10254 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10254 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10254 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10254 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10254 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/09/16 12:55 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 Page 120 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - M W I Gr o u n d W at e r AZ K 0 0 4 4 - 4 2 AZK0044 1 1/ 0 3 / 1 6 0 8 : 2 6 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 On S i t e EP A 1 8 0 . 1 8. 7 6 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/03/16 08:26 1 1/ 0 3 / 1 6 0 8 : 2 6 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 24 . 2 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 9 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 0 7 ug / L 1 Ca d m i u m 1. 0 0 J 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 5 5 ug / L 1 Co p p e r 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 8 4 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 4 3 ug / L 1 Ni c k e l 50 . 0 J 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 3. 5 8 ug / L 1 Zi n c 10 . 0 J 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 21:13 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 121 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - T ri p B l a n k W at e r AZ K 0 0 4 4 - 4 3 AZK0044 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10254 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10254 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10254 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10254 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10254 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10254 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10254 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10254 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 Page 122 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - T ri p B l a n k W at e r AZ K 0 0 4 4 - 4 3 AZK0044 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10254 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10254 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10254 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 Page 123 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - T ri p B l a n k W at e r AZ K 0 0 4 4 - 4 3 AZK0044 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10254 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10254 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10254 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10254 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10254 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/09/16 13:23 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 Page 124 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - E q u i p m e n t B l a n k W at e r AZ K 0 0 4 4 - 4 4 AZK0044 1 1/ 0 3 / 1 6 1 7 : 2 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10183 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10183 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 9 9 ug / L 1 Ba r i u m 10 0 J 61 10183 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10183 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10183 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 12 . 6 ug / L 1 Co p p e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 6 ug / L 1 Le a d 10 . 0 J 61 10183 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ni c k e l 50 . 0 61 10183 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10183 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10183 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10183 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10183 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Zi n c 10 . 0 61 10183 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/17/16 21:18 1 1/ 0 8 / 1 6 1 4 : 4 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10254 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10254 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10254 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 Page 125 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - E q u i p m e n t B l a n k W at e r AZ K 0 0 4 4 - 4 4 AZK0044 1 1/ 0 3 / 1 6 1 7 : 2 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10254 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10254 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10254 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10254 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10254 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 Page 126 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - E q u i p m e n t B l a n k W at e r AZ K 0 0 4 4 - 4 4 AZK0044 1 1/ 0 3 / 1 6 1 7 : 2 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10254 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10254 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 0. 5 ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 J 61 10254 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10254 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10254 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10254 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10254 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10254 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10254 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10254 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 Page 127 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - E q u i p m e n t B l a n k W at e r AZ K 0 0 4 4 - 4 4 AZK0044 1 1/ 0 3 / 1 6 1 7 : 2 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10254 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 10254 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10254 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/09/16 13:50 1 1/ 0 9 / 1 6 1 1:00 80 - 1 2 0 Page 128 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 0 8 2 - S M 5 2 1 0 B Bl a n k ( 6 1 10 0 8 2 - B L K 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/08/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L ND 20 0 0 LC S ( 6 1 10 0 8 2 - B S 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/08/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 23 4 0 0 0 20 0 0 19 8 0 0 0 BOD-4 85 - 11 5 11 8 Du p l i c a t e ( 6 1 10 0 8 2 - D U P 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/08/16 So u r ce : AZ K 0 1 0 3 - 0 1 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 14 5 0 0 0 20 0 0 ND 20 BOD-4 Ba t c h 6 1 10 1 0 8 - S M 5 2 1 0 B Bl a n k ( 6 1 10 1 0 8 - B L K 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/08/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L ND 20 0 0 LC S ( 6 1 10 1 0 8 - B S 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/08/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 22 6 0 0 0 20 0 0 19 8 0 0 0 85 - 11 5 11 4 Du p l i c a t e ( 6 1 10 1 0 8 - D U P 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/08/16 So u r ce : AZ K 0 1 2 3 - 0 3 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 16 0 0 0 20 0 0 14 0 0 0 20 13 Ba t c h 6 11 0 1 15 - S M 5 2 1 0 B Bl a n k ( 6 11 0 1 15 - B L K 1 ) Pr e p a r e d : 1 1/ 0 4 / 1 6 An a l y z e d : 1 1/09/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L ND 20 0 0 LC S ( 6 11 0 1 15 - B S 1 ) Pr e p a r e d : 1 1/ 0 4 / 1 6 An a l y z e d : 1 1/09/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 22 4 0 0 0 20 0 0 19 8 0 0 0 85 - 11 5 11 3 Page 129 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 11 0 1 15 - S M 5 2 1 0 B Du p l i c a t e ( 6 11 0 1 15 - D U P 1 ) Pr e p a r e d : 1 1/ 0 4 / 1 6 An a l y z e d : 1 1/09/16 So u r ce : AZ K 0 1 4 3 - 0 1 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 19 6 0 0 0 20 0 0 ND 20 Ba t c h 6 1 10 1 2 8 - S M 2 5 4 0 C Bl a n k ( 6 1 10 1 2 8 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 T ot a l D i s s o l v e d S o l i d s ug / L ND 10 0 0 0 LC S ( 6 1 10 1 2 8 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 T ot a l D i s s o l v e d S o l i d s ug / L 33 8 0 0 0 10 0 0 0 40 0 0 0 0 84 - 1 0 8 84 Du p l i c a t e ( 6 1 10 1 2 8 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 0 4 4 - 0 6 T ot a l D i s s o l v e d S o l i d s ug / L 42 3 0 0 0 10 0 0 0 47 5 0 0 0 10 QR-03 12 Du p l i c a t e ( 6 1 10 1 2 8 - D U P 2 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 2 0 - 0 7 T ot a l D i s s o l v e d S o l i d s ug / L 36 7 0 0 0 66 7 0 0 41 3 0 0 0 10 QR-03 12 Ba t c h 6 1 10 1 5 3 - E P A 4 1 0 . 4 Bl a n k ( 6 1 10 1 5 3 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 Ch e m i c a l O x y g e n D e m a n d ug / L ND 10 0 0 0 LC S ( 6 1 10 1 5 3 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 Ch e m i c a l O x y g e n D e m a n d ug / L 20 4 0 0 0 10 0 0 0 20 0 0 0 0 90 - 11 0 10 2 Du p l i c a t e ( 6 1 10 1 5 3 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 8 1 - 0 1 Ch e m i c a l O x y g e n D e m a n d ug / L 32 6 0 0 0 40 0 0 0 31 7 0 0 0 10 3 Page 130 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 5 3 - E P A 4 1 0 . 4 Ma t r i x S p i k e ( 6 1 10 1 5 3 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 1 Ch e m i c a l O x y g e n D e m a n d ug / L 23 6 0 0 0 10 0 0 0 20 0 0 0 0 26 5 0 0 90 - 11 0 10 5 Ma t r i x S p i k e ( 6 1 10 1 5 3 - M S 2 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 4 4 - 0 3 Ch e m i c a l O x y g e n D e m a n d ug / L 22 7 0 0 0 10 0 0 0 20 0 0 0 0 25 8 0 0 90 - 11 0 10 1 Ma t r i x S p i k e D u p ( 6 1 10 1 5 3 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 1 Ch e m i c a l O x y g e n D e m a n d ug / L 22 7 0 0 0 10 0 0 0 20 0 0 0 0 26 5 0 0 10 90 - 11 0 10 0 4 Ba t c h 6 1 10 1 5 4 - E P A 9 0 6 0 A Bl a n k ( 6 1 10 1 5 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l O r g a n i c C a r b o n ug / L ND 10 0 0 LC S ( 6 1 10 1 5 4 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l O r g a n i c C a r b o n ug / L 19 6 0 0 10 0 0 20 0 0 0 88 - 11 2 98 Ma t r i x S p i k e ( 6 1 10 1 5 4 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ J 0 8 4 1 - 0 1 T ot a l O r g a n i c C a r b o n ug / L 19 4 0 0 10 0 0 20 0 0 0 ND 67 - 1 4 1 97 Ma t r i x S p i k e D u p ( 6 1 10 1 5 4 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ J 0 8 4 1 - 0 1 T ot a l O r g a n i c C a r b o n ug / L 19 2 0 0 10 0 0 20 0 0 0 ND 16 67 - 1 4 1 96 0. 9 Ba t c h 6 1 10 1 6 4 - S M 2 3 2 0 B Bl a n k ( 6 1 10 1 6 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Al k a l i n i t y a s C a C O 3 ug / L ND 10 0 0 Page 131 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 4 - S M 2 3 2 0 B LC S ( 6 1 10 1 6 4 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Al k a l i n i t y a s C a C O 3 ug / L 10 0 0 0 0 10 0 0 10 0 0 0 0 85 - 11 5 10 0 Du p l i c a t e ( 6 1 10 1 6 4 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 1 Al k a l i n i t y a s C a C O 3 ug / L 45 0 0 0 10 0 0 46 0 0 0 10 2 Ba t c h 6 1 10 1 9 1 - S M 4 5 0 0 - S D Bl a n k ( 6 1 10 1 9 1 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l S u l f i d e ug / L ND 20 0 LC S ( 6 1 10 1 9 1 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l S u l f i d e ug / L 54 4 20 0 50 1 . 0 0 80 - 1 2 0 10 9 Ma t r i x S p i k e ( 6 1 10 1 9 1 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 1 5 1 - 0 1 T ot a l S u l f i d e ug / L 78 1 20 0 50 1 . 0 0 ND QM-05 30 - 1 2 9 15 6 Ma t r i x S p i k e D u p ( 6 1 10 1 9 1 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 1 5 1 - 0 1 T ot a l S u l f i d e ug / L 76 3 20 0 50 1 . 0 0 ND 10 QM-05 30 - 1 2 9 15 2 2. 3 3 Page 132 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e In o r g a n i c An i o n s - Q u a l i t y C o n t r o l Ba t c h 6 1 10 0 6 0 - E P A 9 0 5 6 A Bl a n k ( 6 1 10 0 6 0 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 2 / 1 6 Ch l o r i d e ug / L ND 10 0 0 Ni t r a t e a s N ug / L ND 50 Su l f a t e ug / L ND 50 0 0 LC S ( 6 1 10 0 6 0 - B S 1 ) Pr e p a r e d : 1 1/ 0 2 / 1 6 An a l y z e d : 1 1/03/16 Ch l o r i d e ug / L 10 5 0 0 10 0 0 10 0 1 0 90 - 11 0 10 5 Ni t r a t e a s N ug / L 10 4 0 0 50 10 0 2 0 90 - 11 0 10 4 Su l f a t e ug / L 10 4 0 0 50 0 0 10 0 2 0 90 - 11 0 10 4 Ma t r i x S p i k e ( 6 1 10 0 6 0 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 2 / 1 6 So u r ce : AZ K 0 0 4 4 - 0 3 Ch l o r i d e ug / L 19 9 0 10 0 0 10 0 1 0 ND QM-10 90 - 11 0 20 Ni t r a t e a s N ug / L 15 8 0 50 10 0 2 0 58 . 0 QM-10 90 - 11 0 15 Su l f a t e ug / L ND 50 0 0 10 0 2 0 ND QM-10 90 - 11 0 0 Ma t r i x S p i k e ( 6 1 10 0 6 0 - M S 2 ) Pr e p a r e d : 1 1/ 0 2 / 1 6 An a l y z e d : 1 1/03/16 So u r ce : AZ K 0 0 8 0 - 0 1 Ch l o r i d e ug / L ND 10 0 0 10 0 1 0 ND QM-10 90 - 11 0 0 Ni t r a t e a s N ug / L ND 50 10 0 2 0 ND QM-10 90 - 11 0 0 Su l f a t e ug / L ND 50 0 0 10 0 2 0 ND QM-10 90 - 11 0 0 Ma t r i x S p i k e D u p ( 6 1 10 0 6 0 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 2 / 1 6 So u r ce : AZ K 0 0 4 4 - 0 3 Ch l o r i d e ug / L ND 10 0 0 10 0 1 0 ND 15 QM-10 90 - 11 0 0 Ni t r a t e a s N ug / L 48 3 50 10 0 2 0 58 . 0 15 QM-10 90 - 11 0 4 10 6 Su l f a t e ug / L ND 50 0 0 10 0 2 0 ND 15 QM-10 90 - 11 0 0 Ba t c h 6 1 10 0 9 8 - E P A 9 0 5 6 A Bl a n k ( 6 1 10 0 9 8 - B L K 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/04/16 Ch l o r i d e ug / L ND 10 0 0 Ni t r a t e a s N ug / L ND 50 Page 133 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e In o r g a n i c An i o n s - Q u a l i t y C o n t r o l Ba t c h 6 1 10 0 9 8 - E P A 9 0 5 6 A Bl a n k ( 6 1 10 0 9 8 - B L K 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/04/16 Su l f a t e ug / L ND 50 0 0 LC S ( 6 1 10 0 9 8 - B S 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/04/16 Ch l o r i d e ug / L 10 3 0 0 10 0 0 10 0 1 0 90 - 11 0 10 3 Ni t r a t e a s N ug / L 10 2 0 0 50 10 0 2 0 90 - 11 0 10 2 Su l f a t e ug / L 10 6 0 0 50 0 0 10 0 2 0 90 - 11 0 10 6 Ma t r i x S p i k e ( 6 1 10 0 9 8 - M S 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/04/16 So u r ce : AZ K 0 0 9 0 - 1 2 Ch l o r i d e ug / L 46 5 0 0 10 0 0 10 0 1 0 40 8 0 0 QM-05 90 - 11 0 57 Ni t r a t e a s N ug / L 10 2 0 0 50 10 0 2 0 ND 90 - 11 0 10 2 Su l f a t e ug / L 13 1 0 0 50 0 0 10 0 2 0 ND QM-05 90 - 11 0 13 1 Ma t r i x S p i k e ( 6 1 10 0 9 8 - M S 2 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/04/16 So u r ce : AZ K 0 1 16 - 0 2 Ch l o r i d e ug / L 52 0 0 0 10 0 0 10 0 1 0 46 9 0 0 QM-05 90 - 11 0 52 Ni t r a t e a s N ug / L 35 5 0 0 50 10 0 2 0 28 0 0 0 QM-05 90 - 11 0 74 Su l f a t e ug / L 94 2 0 0 50 0 0 10 0 2 0 94 1 0 0 QM-05 90 - 11 0 1 Ma t r i x S p i k e D u p ( 6 1 10 0 9 8 - M S D 1 ) Pr e p a r e d : 1 1/ 0 3 / 1 6 An a l y z e d : 1 1/04/16 So u r ce : AZ K 0 0 9 0 - 1 2 Ch l o r i d e ug / L 46 6 0 0 10 0 0 10 0 1 0 40 8 0 0 15 QM-05 90 - 11 0 57 0. 1 Ni t r a t e a s N ug / L 10 2 0 0 50 10 0 2 0 ND 15 90 - 11 0 10 1 0. 1 Su l f a t e ug / L 13 3 0 0 50 0 0 10 0 2 0 ND 15 QM-05 90 - 11 0 13 2 1 Page 134 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 0 1 - E P A 7 4 7 0 A Bl a n k ( 6 1 10 1 0 1 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 Me r c u r y ug / L ND 0. 2 0 0 LC S ( 6 1 10 1 0 1 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 Me r c u r y ug / L 2. 5 2 0. 2 0 0 2. 5 0 0 0 80 - 1 2 0 10 1 Ma t r i x S p i k e ( 6 1 10 1 0 1 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 0 9 - 0 7 Me r c u r y ug / L 1. 9 5 0. 2 0 0 2. 5 0 0 0 ND 75 - 1 2 5 78 Ma t r i x S p i k e D u p ( 6 1 10 1 0 1 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 0 9 - 0 7 Me r c u r y ug / L 1. 9 4 0. 2 0 0 2. 5 0 0 0 ND 20 75 - 1 2 5 78 0. 3 Po s t S p i k e ( 6 1 10 1 0 1 - P S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 0 9 - 0 7 Me r c u r y ug / L 1. 3 5 1. 6 6 6 7 0. 0 0 7 80 - 1 2 0 80 Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Bl a n k ( 6 1 10 1 8 2 - B L K 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 An t i m o n y ug / L ND 6. 0 0 Ar s e n i c ug / L ND 10 . 0 Ba r i u m ug / L ND 10 0 Be r y l l i u m ug / L ND 1. 0 0 Ca d m i u m ug / L ND 1. 0 0 Ch r o m i u m ug / L ND 10 . 0 Co b a l t ug / L ND 10 . 0 Co p p e r ug / L ND 10 . 0 Ir o n ug / L ND 40 . 0 Le a d ug / L ND 10 . 0 Ma n g a n e s e ug / L ND 10 . 0 Ni c k e l ug / L ND 50 . 0 Page 135 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Bl a n k ( 6 1 10 1 8 2 - B L K 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 Se l e n i u m ug / L ND 10 . 0 Si l v e r ug / L ND 10 . 0 Th a l l i u m ug / L ND 5. 5 0 V an a d i u m ug / L ND 25 . 0 Zi n c ug / L ND 10 . 0 LC S ( 6 1 10 1 8 2 - B S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 An t i m o n y ug / L 10 2 6. 0 0 10 0 . 0 0 80 - 1 2 0 10 2 Ar s e n i c ug / L 97 . 5 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Ba r i u m ug / L 94 . 5 10 0 10 0 . 0 0 J 80 - 1 2 0 95 Be r y l l i u m ug / L 95 . 1 1. 0 0 10 0 . 0 0 80 - 1 2 0 95 Ca d m i u m ug / L 95 . 2 1. 0 0 10 0 . 0 0 80 - 1 2 0 95 Ch r o m i u m ug / L 99 . 6 10 . 0 10 0 . 0 0 80 - 1 2 0 10 0 Co b a l t ug / L 10 1 10 . 0 10 0 . 0 0 80 - 1 2 0 10 1 Co p p e r ug / L 98 . 0 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Ir o n ug / L 10 6 0 40 . 0 10 0 0 . 0 80 - 1 2 0 10 6 Le a d ug / L 96 . 7 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Ma n g a n e s e ug / L 10 2 10 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Ni c k e l ug / L 10 2 50 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Se l e n i u m ug / L 99 . 5 10 . 0 10 0 . 0 0 80 - 1 2 0 99 Si l v e r ug / L 97 . 2 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Th a l l i u m ug / L 96 . 4 5. 5 0 10 0 . 0 0 80 - 1 2 0 96 V an a d i u m ug / L 98 . 9 25 . 0 10 0 . 0 0 80 - 1 2 0 99 Zi n c ug / L 10 3 10 . 0 10 0 . 0 0 80 - 1 2 0 10 3 Ma t r i x S p i k e ( 6 1 10 1 8 2 - M S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 An t i m o n y ug / L 10 3 6. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 3 Ar s e n i c ug / L 10 2 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 2 Page 136 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Ma t r i x S p i k e ( 6 1 10 1 8 2 - M S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 Ba r i u m ug / L 15 7 10 0 10 0 . 0 0 61 . 8 75 - 1 2 5 95 Be r y l l i u m ug / L 84 . 7 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 85 Ca d m i u m ug / L 95 . 7 1. 0 0 10 0 . 0 0 0. 1 4 75 - 1 2 5 96 Ch r o m i u m ug / L 10 7 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 7 Co b a l t ug / L 11 9 10 . 0 10 0 . 0 0 18 . 7 75 - 1 2 5 10 0 Co p p e r ug / L 10 2 10 . 0 10 0 . 0 0 4. 4 0 75 - 1 2 5 98 Ir o n ug / L 22 3 0 40 . 0 10 0 0 . 0 1 17 0 75 - 1 2 5 10 6 Le a d ug / L 94 . 0 10 . 0 10 0 . 0 0 0. 1 8 75 - 1 2 5 94 Ma n g a n e s e ug / L 51 0 0 10 . 0 10 0 . 0 0 50 3 0 QM-02 75 - 1 2 5 71 Ni c k e l ug / L 12 8 50 . 0 10 0 . 0 0 27 . 9 75 - 1 2 5 10 0 Se l e n i u m ug / L 10 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 4 Si l v e r ug / L 96 . 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 96 Th a l l i u m ug / L 96 . 9 5. 5 0 10 0 . 0 0 ND 75 - 1 2 5 97 V an a d i u m ug / L 10 7 25 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 7 Zi n c ug / L 23 0 10 . 0 10 0 . 0 0 11 9 75 - 1 2 5 11 1 Ma t r i x S p i k e D u p ( 6 1 10 1 8 2 - M S D 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 An t i m o n y ug / L 10 3 6. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 3 0. 0 3 Ar s e n i c ug / L 10 1 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 1 0. 2 Ba r i u m ug / L 15 3 10 0 10 0 . 0 0 61 . 8 20 75 - 1 2 5 91 3 Be r y l l i u m ug / L 84 . 6 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 85 0. 1 Ca d m i u m ug / L 98 . 7 1. 0 0 10 0 . 0 0 0. 1 4 20 75 - 1 2 5 99 3 Ch r o m i u m ug / L 10 0 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 0 6 Co b a l t ug / L 11 7 10 . 0 10 0 . 0 0 18 . 7 20 75 - 1 2 5 99 1 Co p p e r ug / L 10 5 10 . 0 10 0 . 0 0 4. 4 0 20 75 - 1 2 5 10 0 2 Ir o n ug / L 21 8 0 40 . 0 10 0 0 . 0 1 17 0 20 75 - 1 2 5 10 1 2 Le a d ug / L 94 . 2 10 . 0 10 0 . 0 0 0. 1 8 20 75 - 1 2 5 94 0. 2 Ma n g a n e s e ug / L 50 1 0 10 . 0 10 0 . 0 0 50 3 0 20 QM-02 75 - 1 2 5 0 2 Page 137 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Ma t r i x S p i k e D u p ( 6 1 10 1 8 2 - M S D 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 Ni c k e l ug / L 12 6 50 . 0 10 0 . 0 0 27 . 9 20 75 - 1 2 5 98 2 Se l e n i u m ug / L 10 4 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 4 0. 3 Si l v e r ug / L 95 . 0 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 95 1 Th a l l i u m ug / L 94 . 9 5. 5 0 10 0 . 0 0 ND 20 75 - 1 2 5 95 2 V an a d i u m ug / L 10 2 25 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 2 5 Zi n c ug / L 22 0 10 . 0 10 0 . 0 0 11 9 20 75 - 1 2 5 10 0 5 Po s t S p i k e ( 6 1 10 1 8 2 - P S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 An t i m o n y ug / L 10 2 10 0 . 0 0 0. 2 0 80 - 1 2 0 10 2 Ar s e n i c ug / L 10 4 10 0 . 0 0 0. 3 0 80 - 1 2 0 10 3 Ba r i u m ug / L 16 0 10 0 . 0 0 61 . 8 80 - 1 2 0 98 Be r y l l i u m ug / L 87 . 2 10 0 . 0 0 0. 0 2 80 - 1 2 0 87 Ca d m i u m ug / L 99 . 0 10 0 . 0 0 0. 1 4 80 - 1 2 0 99 Ch r o m i u m ug / L 99 . 7 10 0 . 0 0 0. 4 0 80 - 1 2 0 99 Co b a l t ug / L 11 9 10 0 . 0 0 18 . 7 80 - 1 2 0 10 0 Co p p e r ug / L 10 2 10 0 . 0 0 4. 4 0 80 - 1 2 0 98 Ir o n ug / L 21 8 0 10 0 0 . 0 1 17 0 80 - 1 2 0 10 1 Le a d ug / L 93 . 4 10 0 . 0 0 0. 1 8 80 - 1 2 0 93 Ma n g a n e s e ug / L 51 0 0 10 0 . 0 0 50 3 0 QM-02 80 - 1 2 0 66 Ni c k e l ug / L 12 6 10 0 . 0 0 27 . 9 80 - 1 2 0 98 Se l e n i u m ug / L 10 7 10 0 . 0 0 -0 . 2 2 80 - 1 2 0 10 7 Si l v e r ug / L 97 . 8 10 0 . 0 0 0. 0 2 80 - 1 2 0 98 Th a l l i u m ug / L 95 . 9 10 0 . 0 0 0. 0 3 80 - 1 2 0 96 V an a d i u m ug / L 10 5 10 0 . 0 0 0. 4 2 80 - 1 2 0 10 5 Zi n c ug / L 22 2 10 0 . 0 0 11 9 80 - 1 2 0 10 3 Ba t c h 6 1 10 1 8 3 - E P A 3 0 0 5 A Page 138 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 3 - E P A 3 0 0 5 A Bl a n k ( 6 1 10 1 8 3 - B L K 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 An t i m o n y ug / L ND 6. 0 0 Ar s e n i c ug / L ND 10 . 0 Ba r i u m ug / L ND 10 0 Be r y l l i u m ug / L ND 1. 0 0 Ca d m i u m ug / L ND 1. 0 0 Ch r o m i u m ug / L ND 10 . 0 Co b a l t ug / L ND 10 . 0 Co p p e r ug / L ND 10 . 0 Le a d ug / L ND 10 . 0 Ni c k e l ug / L ND 50 . 0 Se l e n i u m ug / L ND 10 . 0 Si l v e r ug / L ND 10 . 0 Th a l l i u m ug / L ND 5. 5 0 V an a d i u m ug / L ND 25 . 0 Zi n c ug / L ND 10 . 0 LC S ( 6 1 10 1 8 3 - B S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 An t i m o n y ug / L 10 5 6. 0 0 10 0 . 0 0 80 - 1 2 0 10 5 Ar s e n i c ug / L 10 1 10 . 0 10 0 . 0 0 80 - 1 2 0 10 1 Ba r i u m ug / L 96 . 6 10 0 10 0 . 0 0 J 80 - 1 2 0 97 Be r y l l i u m ug / L 97 . 9 1. 0 0 10 0 . 0 0 80 - 1 2 0 98 Ca d m i u m ug / L 10 4 1. 0 0 10 0 . 0 0 80 - 1 2 0 10 4 Ch r o m i u m ug / L 10 2 10 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Co b a l t ug / L 10 0 10 . 0 10 0 . 0 0 80 - 1 2 0 10 0 Co p p e r ug / L 10 2 10 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Le a d ug / L 98 . 3 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Ni c k e l ug / L 10 3 50 . 0 10 0 . 0 0 80 - 1 2 0 10 3 Se l e n i u m ug / L 97 . 5 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Page 139 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 3 - E P A 3 0 0 5 A LC S ( 6 1 10 1 8 3 - B S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 Si l v e r ug / L 99 . 8 10 . 0 10 0 . 0 0 80 - 1 2 0 10 0 Th a l l i u m ug / L 97 . 6 5. 5 0 10 0 . 0 0 80 - 1 2 0 98 V an a d i u m ug / L 10 3 25 . 0 10 0 . 0 0 80 - 1 2 0 10 3 Zi n c ug / L 10 4 10 . 0 10 0 . 0 0 80 - 1 2 0 10 4 Ma t r i x S p i k e ( 6 1 10 1 8 3 - M S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 So u r ce : AZ K 0 0 4 4 - 2 4 An t i m o n y ug / L 10 7 6. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 7 Ar s e n i c ug / L 10 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 4 Ba r i u m ug / L 13 7 10 0 10 0 . 0 0 32 . 3 75 - 1 2 5 10 4 Be r y l l i u m ug / L 96 . 1 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 96 Ca d m i u m ug / L 10 4 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 4 Ch r o m i u m ug / L 10 8 10 . 0 10 0 . 0 0 1. 7 0 75 - 1 2 5 10 6 Co b a l t ug / L 10 8 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 8 Co p p e r ug / L 10 8 10 . 0 10 0 . 0 0 1. 6 0 75 - 1 2 5 10 7 Le a d ug / L 99 . 3 10 . 0 10 0 . 0 0 0. 2 9 75 - 1 2 5 99 Ni c k e l ug / L 11 1 50 . 0 10 0 . 0 0 3. 5 6 75 - 1 2 5 10 8 Se l e n i u m ug / L 99 . 1 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 99 Si l v e r ug / L 97 . 7 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 98 Th a l l i u m ug / L 99 . 2 5. 5 0 10 0 . 0 0 ND 75 - 1 2 5 99 V an a d i u m ug / L 11 4 25 . 0 10 0 . 0 0 ND 75 - 1 2 5 11 4 Zi n c ug / L 10 8 10 . 0 10 0 . 0 0 2. 6 9 75 - 1 2 5 10 5 Ma t r i x S p i k e D u p ( 6 1 10 1 8 3 - M S D 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 So u r ce : AZ K 0 0 4 4 - 2 4 An t i m o n y ug / L 10 5 6. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 5 2 Ar s e n i c ug / L 10 2 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 2 1 Ba r i u m ug / L 13 2 10 0 10 0 . 0 0 32 . 3 20 75 - 1 2 5 99 4 Be r y l l i u m ug / L 94 . 3 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 94 2 Ca d m i u m ug / L 10 1 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 1 3 Page 140 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 3 - E P A 3 0 0 5 A Ma t r i x S p i k e D u p ( 6 1 10 1 8 3 - M S D 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 So u r ce : AZ K 0 0 4 4 - 2 4 Ch r o m i u m ug / L 10 8 10 . 0 10 0 . 0 0 1. 7 0 20 75 - 1 2 5 10 7 0. 6 Co b a l t ug / L 10 4 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 4 4 Co p p e r ug / L 10 4 10 . 0 10 0 . 0 0 1. 6 0 20 75 - 1 2 5 10 2 4 Le a d ug / L 10 0 10 . 0 10 0 . 0 0 0. 2 9 20 75 - 1 2 5 10 0 1 Ni c k e l ug / L 10 9 50 . 0 10 0 . 0 0 3. 5 6 20 75 - 1 2 5 10 6 2 Se l e n i u m ug / L 95 . 9 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 96 3 Si l v e r ug / L 97 . 4 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 97 0. 3 Th a l l i u m ug / L 10 0 5. 5 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 0 1 V an a d i u m ug / L 11 5 25 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 11 5 0. 7 Zi n c ug / L 10 3 10 . 0 10 0 . 0 0 2. 6 9 20 75 - 1 2 5 10 0 4 Po s t S p i k e ( 6 1 10 1 8 3 - P S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/17/16 So u r ce : AZ K 0 0 4 4 - 2 4 An t i m o n y ug / L 10 6 10 0 . 0 0 0. 0 5 80 - 1 2 0 10 6 Ar s e n i c ug / L 10 3 10 0 . 0 0 0. 4 3 80 - 1 2 0 10 2 Ba r i u m ug / L 13 2 10 0 . 0 0 32 . 3 80 - 1 2 0 10 0 Be r y l l i u m ug / L 98 . 0 10 0 . 0 0 0. 0 7 80 - 1 2 0 98 Ca d m i u m ug / L 10 6 10 0 . 0 0 0. 0 3 80 - 1 2 0 10 6 Ch r o m i u m ug / L 10 9 10 0 . 0 0 1. 7 0 80 - 1 2 0 10 7 Co b a l t ug / L 10 4 10 0 . 0 0 0. 3 0 80 - 1 2 0 10 3 Co p p e r ug / L 10 6 10 0 . 0 0 1. 6 0 80 - 1 2 0 10 5 Le a d ug / L 99 . 2 10 0 . 0 0 0. 2 9 80 - 1 2 0 99 Ni c k e l ug / L 10 9 10 0 . 0 0 3. 5 6 80 - 1 2 0 10 5 Se l e n i u m ug / L 99 . 0 10 0 . 0 0 0. 7 2 80 - 1 2 0 98 Si l v e r ug / L 98 . 3 10 0 . 0 0 0. 0 1 80 - 1 2 0 98 Th a l l i u m ug / L 99 . 7 10 0 . 0 0 0. 0 2 80 - 1 2 0 10 0 V an a d i u m ug / L 11 5 10 0 . 0 0 5. 6 1 80 - 1 2 0 10 9 Zi n c ug / L 10 4 10 0 . 0 0 2. 6 9 80 - 1 2 0 10 1 Page 141 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 1 6 6 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Ac e t o n e ug / L ND 10 0 Ac r y l o n i t r i l e ug / L ND 20 0 Be n z e n e ug / L ND 1. 0 Br o m o c h l o r o m e t h a n e ug / L ND 3. 0 Br o m o d i c h l o r o m e t h a n e ug / L ND 1. 0 Br o m o f o r m ug / L ND 3. 0 Br o m o m e t h a n e ug / L ND 10 Ca r b o n D i s u l f i d e ug / L ND 10 0 Ca r b o n T et r a c h l o r i d e ug / L ND 1. 0 Ch l o r o b e n z e n e ug / L ND 3. 0 Ch l o r o e t h a n e ug / L ND 10 Ch l o r o f o r m ug / L ND 5. 0 Ch l o r o m e t h a n e ug / L ND 1. 0 Di b r o m o c h l o r o m e t h a n e ug / L ND 1. 0 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e ug / L ND 13 1, 2 - D i b r o m o e t h a n e ug / L ND 1. 0 Di b r o m o m e t h a n e ug / L ND 10 1, 2 - D i c h l o r o b e n z e n e ug / L ND 5. 0 1, 4 - D i c h l o r o b e n z e n e ug / L ND 1. 0 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e ug / L ND 10 0 1, 1 - D i c h l o r o e t h a n e ug / L ND 5. 0 1, 2 - D i c h l o r o e t h a n e ug / L ND 1. 0 1, 1 - D i c h l o r o e t h e n e ug / L ND 5. 0 ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 tr a n s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 1, 2 - D i c h l o r o p r o p a n e ug / L ND 1. 0 ci s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Page 142 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 1 6 6 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Et h y l b e n z e n e ug / L ND 1. 0 Io d o m e t h a n e ug / L ND 10 Me t h y l B u t y l K e t o n e ( 2 - H e x a n o n e ) ug / L ND 50 Me t h y l e n e C h l o r i d e ug / L ND 1. 0 Me t h y l E t h y l K e t o n e ( 2 - B u t a n o n e ) ug / L ND 10 0 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) ug / L ND 10 0 St y r e n e ug / L ND 1. 0 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e ug / L ND 5. 0 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e ug / L ND 1. 0 T et r a c h l o r o e t h e n e ug / L ND 1. 0 T olu e n e ug / L ND 1. 0 1, 1 , 1 - T ri c h l o r o e t h a n e ug / L ND 1. 0 1, 1 , 2 - T ri c h l o r o e t h a n e ug / L ND 1. 0 T ri c h l o r o e t h e n e ug / L ND 1. 0 T ri c h l o r o f l u o r o m e t h a n e ug / L ND 1. 0 1, 2 , 3 - T ri c h l o r o p r o p a n e ug / L ND 1. 0 V in y l Ac e t a t e ug / L ND 50 V in y l C h l o r i d e ug / L ND 1. 0 Xy l e n e s , t o t a l ug / L ND 5. 0 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 99 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 92 46 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 94 47 LC S ( 6 1 10 1 6 6 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Be n z e n e ug / L 59 50 . 0 0 0 67 - 1 3 4 11 9 Page 143 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B LC S ( 6 1 10 1 6 6 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Ch l o r o b e n z e n e ug / L 59 50 . 0 0 0 69 - 1 2 2 11 8 1, 1 - D i c h l o r o e t h e n e ug / L 65 50 . 0 0 0 58 - 1 4 2 13 0 T olu e n e ug / L 54 50 . 0 0 0 68 - 1 2 7 10 9 T ri c h l o r o e t h e n e ug / L 51 50 . 0 0 0 72 - 1 3 2 10 3 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 1 50 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 1 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 46 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 91 46 Ma t r i x S p i k e ( 6 1 10 1 6 6 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 7 Be n z e n e ug / L 62 50 . 0 0 0 0. 0 67 - 1 3 4 12 5 Ch l o r o b e n z e n e ug / L 61 50 . 0 0 0 0. 0 QM-05 69 - 1 2 2 12 3 1, 1 - D i c h l o r o e t h e n e ug / L 85 50 . 0 0 0 0. 0 QM-05 58 - 1 4 2 16 9 T olu e n e ug / L 58 50 . 0 0 0 0. 0 68 - 1 2 7 11 6 T ri c h l o r o e t h e n e ug / L 56 50 . 0 0 0 0. 0 72 - 1 3 2 11 3 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 3 51 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 94 47 Ma t r i x S p i k e D u p ( 6 1 10 1 6 6 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 7 Be n z e n e ug / L 58 50 . 0 0 0 0. 0 9 67 - 1 3 4 11 6 7 Ch l o r o b e n z e n e ug / L 56 50 . 0 0 0 0. 0 13 69 - 1 2 2 11 3 8 1, 1 - D i c h l o r o e t h e n e ug / L 78 50 . 0 0 0 0. 0 9 QM-05 58 - 1 4 2 15 6 8 T olu e n e ug / L 54 50 . 0 0 0 0. 0 9 68 - 1 2 7 10 8 7 T ri c h l o r o e t h e n e ug / L 53 50 . 0 0 0 0. 0 11 72 - 1 3 2 10 6 6 Page 144 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B Ma t r i x S p i k e D u p ( 6 1 10 1 6 6 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 7 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 3 52 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 90 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 93 46 Ba t c h 6 11 0 2 1 1 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 2 1 1- B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 Ac e t o n e ug / L ND 10 0 Ac r y l o n i t r i l e ug / L ND 20 0 Be n z e n e ug / L ND 1. 0 Br o m o c h l o r o m e t h a n e ug / L ND 3. 0 Br o m o d i c h l o r o m e t h a n e ug / L ND 1. 0 Br o m o f o r m ug / L ND 3. 0 Br o m o m e t h a n e ug / L ND 10 Ca r b o n D i s u l f i d e ug / L ND 10 0 Ca r b o n T et r a c h l o r i d e ug / L ND 1. 0 Ch l o r o b e n z e n e ug / L ND 3. 0 Ch l o r o e t h a n e ug / L ND 10 Ch l o r o f o r m ug / L ND 5. 0 Ch l o r o m e t h a n e ug / L ND 1. 0 Di b r o m o c h l o r o m e t h a n e ug / L ND 1. 0 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e ug / L ND 13 1, 2 - D i b r o m o e t h a n e ug / L ND 1. 0 Di b r o m o m e t h a n e ug / L ND 10 1, 2 - D i c h l o r o b e n z e n e ug / L ND 5. 0 1, 4 - D i c h l o r o b e n z e n e ug / L ND 1. 0 Page 145 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 11 0 2 1 1 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 2 1 1- B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e ug / L ND 10 0 1, 1 - D i c h l o r o e t h a n e ug / L ND 5. 0 1, 2 - D i c h l o r o e t h a n e ug / L ND 1. 0 1, 1 - D i c h l o r o e t h e n e ug / L ND 5. 0 ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 tr a n s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 1, 2 - D i c h l o r o p r o p a n e ug / L ND 1. 0 ci s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Et h y l b e n z e n e ug / L ND 1. 0 Io d o m e t h a n e ug / L ND 10 Me t h y l B u t y l K e t o n e ( 2 - H e x a n o n e ) ug / L ND 50 Me t h y l e n e C h l o r i d e ug / L ND 1. 0 Me t h y l E t h y l K e t o n e ( 2 - B u t a n o n e ) ug / L ND 10 0 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) ug / L ND 10 0 St y r e n e ug / L ND 1. 0 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e ug / L ND 5. 0 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e ug / L ND 1. 0 T et r a c h l o r o e t h e n e ug / L ND 1. 0 T olu e n e ug / L ND 1. 0 1, 1 , 1 - T ri c h l o r o e t h a n e ug / L ND 1. 0 1, 1 , 2 - T ri c h l o r o e t h a n e ug / L ND 1. 0 T ri c h l o r o e t h e n e ug / L ND 1. 0 T ri c h l o r o f l u o r o m e t h a n e ug / L ND 1. 0 1, 2 , 3 - T ri c h l o r o p r o p a n e ug / L ND 1. 0 V in y l Ac e t a t e ug / L ND 50 V in y l C h l o r i d e ug / L ND 1. 0 Page 146 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 11 0 2 1 1 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 2 1 1- B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 Xy l e n e s , t o t a l ug / L ND 5. 0 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 99 50 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 0 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 92 46 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 95 47 LC S ( 6 1 10 2 1 1- B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 Be n z e n e ug / L 57 50 . 0 0 0 67 - 1 3 4 11 5 Ch l o r o b e n z e n e ug / L 58 50 . 0 0 0 69 - 1 2 2 11 6 1, 1 - D i c h l o r o e t h e n e ug / L 68 50 . 0 0 0 58 - 1 4 2 13 5 T olu e n e ug / L 54 50 . 0 0 0 68 - 1 2 7 10 8 T ri c h l o r o e t h e n e ug / L 53 50 . 0 0 0 72 - 1 3 2 10 6 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 0 50 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 1 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 94 47 Ma t r i x S p i k e ( 6 1 10 2 1 1- M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 0 4 2 - 1 3 Be n z e n e ug / L 61 50 . 0 0 0 0. 0 67 - 1 3 4 12 2 Ch l o r o b e n z e n e ug / L 60 50 . 0 0 0 0. 0 69 - 1 2 2 12 0 1, 1 - D i c h l o r o e t h e n e ug / L 83 50 . 0 0 0 0. 0 QM-05 58 - 1 4 2 16 6 T olu e n e ug / L 57 50 . 0 0 0 0. 0 68 - 1 2 7 11 5 T ri c h l o r o e t h e n e ug / L 56 50 . 0 0 0 0. 0 72 - 1 3 2 11 1 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 3 52 Page 147 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 11 0 2 1 1 - E P A 5 0 3 0 B Ma t r i x S p i k e ( 6 1 10 2 1 1- M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 0 4 2 - 1 3 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 93 46 Ma t r i x S p i k e D u p ( 6 1 10 2 1 1- M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 0 4 2 - 1 3 Be n z e n e ug / L 57 50 . 0 0 0 0. 0 9 67 - 1 3 4 11 3 8 Ch l o r o b e n z e n e ug / L 56 50 . 0 0 0 0. 0 13 69 - 1 2 2 11 2 7 1, 1 - D i c h l o r o e t h e n e ug / L 79 50 . 0 0 0 0. 0 9 QM-05 58 - 1 4 2 15 7 6 T olu e n e ug / L 54 50 . 0 0 0 0. 0 9 68 - 1 2 7 10 9 5 T ri c h l o r o e t h e n e ug / L 53 50 . 0 0 0 0. 0 11 72 - 1 3 2 10 6 4 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 97 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 2 51 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 92 46 Ba t c h 6 1 10 2 5 4 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 2 5 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 Ac e t o n e ug / L ND 10 0 Ac r y l o n i t r i l e ug / L ND 20 0 Be n z e n e ug / L ND 1. 0 Br o m o c h l o r o m e t h a n e ug / L ND 3. 0 Br o m o d i c h l o r o m e t h a n e ug / L ND 1. 0 Br o m o f o r m ug / L ND 3. 0 Br o m o m e t h a n e ug / L ND 10 Ca r b o n D i s u l f i d e ug / L ND 10 0 Ca r b o n T et r a c h l o r i d e ug / L ND 1. 0 Page 148 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 5 4 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 2 5 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 Ch l o r o b e n z e n e ug / L ND 3. 0 Ch l o r o e t h a n e ug / L ND 10 Ch l o r o f o r m ug / L ND 5. 0 Ch l o r o m e t h a n e ug / L ND 1. 0 Di b r o m o c h l o r o m e t h a n e ug / L ND 1. 0 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e ug / L ND 13 1, 2 - D i b r o m o e t h a n e ug / L ND 1. 0 Di b r o m o m e t h a n e ug / L ND 10 1, 2 - D i c h l o r o b e n z e n e ug / L ND 5. 0 1, 4 - D i c h l o r o b e n z e n e ug / L ND 1. 0 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e ug / L ND 10 0 1, 1 - D i c h l o r o e t h a n e ug / L ND 5. 0 1, 2 - D i c h l o r o e t h a n e ug / L ND 1. 0 1, 1 - D i c h l o r o e t h e n e ug / L ND 5. 0 ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 tr a n s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 1, 2 - D i c h l o r o p r o p a n e ug / L ND 1. 0 ci s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Et h y l b e n z e n e ug / L ND 1. 0 Io d o m e t h a n e ug / L ND 10 Me t h y l B u t y l K e t o n e ( 2 - H e x a n o n e ) ug / L ND 50 Me t h y l e n e C h l o r i d e ug / L ND 1. 0 Me t h y l E t h y l K e t o n e ( 2 - B u t a n o n e ) ug / L ND 10 0 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) ug / L ND 10 0 St y r e n e ug / L ND 1. 0 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e ug / L ND 5. 0 Page 149 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 5 4 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 2 5 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e ug / L ND 1. 0 T et r a c h l o r o e t h e n e ug / L ND 1. 0 T olu e n e ug / L ND 1. 0 1, 1 , 1 - T ri c h l o r o e t h a n e ug / L ND 1. 0 1, 1 , 2 - T ri c h l o r o e t h a n e ug / L ND 1. 0 T ri c h l o r o e t h e n e ug / L ND 1. 0 T ri c h l o r o f l u o r o m e t h a n e ug / L ND 1. 0 1, 2 , 3 - T ri c h l o r o p r o p a n e ug / L ND 1. 0 V in y l Ac e t a t e ug / L ND 50 V in y l C h l o r i d e ug / L ND 1. 0 Xy l e n e s , t o t a l ug / L ND 5. 0 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 0 50 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 0 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 92 46 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 93 46 LC S ( 6 1 10 2 5 4 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 Be n z e n e ug / L 56 1. 0 50 . 0 0 0 67 - 1 3 4 11 2 Ch l o r o b e n z e n e ug / L 56 3. 0 50 . 0 0 0 69 - 1 2 2 11 3 1, 1 - D i c h l o r o e t h e n e ug / L 60 5. 0 50 . 0 0 0 58 - 1 4 2 12 1 T olu e n e ug / L 54 1. 0 50 . 0 0 0 68 - 1 2 7 10 7 T ri c h l o r o e t h e n e ug / L 52 1. 0 50 . 0 0 0 72 - 1 3 2 10 4 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 7 53 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 0 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 90 45 Page 150 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 5 4 - E P A 5 0 3 0 B LC S ( 6 1 10 2 5 4 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 84 42 Ma t r i x S p i k e ( 6 1 10 2 5 4 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 So u r ce : AZ K 0 2 8 4 - 0 2 Be n z e n e ug / L 51 1. 0 50 . 0 0 0 ND 67 - 1 3 4 10 3 Ch l o r o b e n z e n e ug / L 50 3. 0 50 . 0 0 0 ND 69 - 1 2 2 10 0 1, 1 - D i c h l o r o e t h e n e ug / L 69 5. 0 50 . 0 0 0 ND 58 - 1 4 2 13 9 T olu e n e ug / L 50 1. 0 50 . 0 0 0 ND 68 - 1 2 7 10 0 T ri c h l o r o e t h e n e ug / L 51 1. 0 50 . 0 0 0 ND 72 - 1 3 2 10 2 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 4 52 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 1 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 86 43 Ma t r i x S p i k e D u p ( 6 1 10 2 5 4 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 9 / 1 6 So u r ce : AZ K 0 2 8 4 - 0 2 Be n z e n e ug / L 40 1. 0 50 . 0 0 0 ND 9 QR-02 67 - 1 3 4 80 25 Ch l o r o b e n z e n e ug / L 39 3. 0 50 . 0 0 0 ND 13 QR-02 69 - 1 2 2 78 25 1, 1 - D i c h l o r o e t h e n e ug / L 57 5. 0 50 . 0 0 0 ND 9 QR-02 58 - 1 4 2 11 3 20 T olu e n e ug / L 38 1. 0 50 . 0 0 0 ND 9 QR-02 68 - 1 2 7 76 27 T ri c h l o r o e t h e n e ug / L 37 1. 0 50 . 0 0 0 ND 11 QR-02 72 - 1 3 2 74 32 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 5 53 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 1 51 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 89 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 86 43 Page 151 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 La b o r a t o r y C e r t i f i c a t i o n s Co d e De s c r i p t i o n Nu m b e r Expires 81 2 Ge o r g i a D W I n o r g a n i c s E f f: 0 7 / 0 1 / 2 0 1 6 06/30/2017 GA D W 81 2 Ge o r g i a D W M i c r o b i o l o g y E f f: 0 7 / 0 1 / 2 0 1 5 12/09/2016 GA D W M 38 1 No r t h C a r o l i n a 12/31/2016 NC E8 7 3 1 5 F L D O H ( N o n - P o t . W at e r , S o l i d s ) E f f: : 0 7 / 0 1 / 2 0 1 6 06/30/2017 NE L A C E8 7 3 1 5 F L D O H N E L A C ( D r i n k i n g W at e r ) E f f: 0 7 / 0 1 / 2 0 1 6 06/30/2017 NE L D W 98 0 11 0 0 1 So u t h C a r o l i n a 06/30/2017 SC T1 0 4 7 0 4 3 9 7 - 0 8 - T X T ex a s 03/31/2017 TX 13 4 0 V ir g i n i a 12/14/2016 VA Page 152 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Le g e n d De f i n a t i o n o f L a b o r a t o r y T er m s - N o t D e t e c t e d a t l e v e l s g r e a t e r t h a n o r e q u a l t o S W S L / R L ND SW S L / R L MD L - NC D E N R S o l i d W as t e S e c t i o n L I m i t /R e p o r t i n g L i m i t ( A d j u s t e d f o r D F / P r e p F a c t o r ) - M e t h o d D e t e c t i o n L i m i t Qu a l i f i e r s - D i l u t i o n F a c t o r DF QR - 0 3 Th e R P D v a l u e f o r t h e s a m p l e d u p l i c a t e o r M S / M S D w a s o u t s i d e o f Q C a c c e p t a n c e l i m i t s d u e t o s u s p e c t e d m a t r i x i n t e r f e r e n c e a n d / o r n o n - h o m o g e n e o u s s a m p l e ma t r i x . QR - 0 2 Th e R P D r e s u l t e x c e e d e d t h e Q C c o n t r o l l i m i t s ; h o w e v e r , b o t h p e r c e n t r e c o v e r i e s w e r e a c c e p t a b l e . S a m p l e r e s u l t s f o r t h e Q C b a t c h w e r e a c c e p t e d b a s e d o n pe r c e n t r e c o v e r i e s . QM - 1 0 MS a n d / o r M S D r e c o v e r i e s n o t w i t h i n Q u a l i t y C o n t r o l Ac c e p t a n c e c r i t e r i a . S e e C a s e N a r r a t i v e . QM - 0 5 Th e s p i k e r e c o v e r y w a s o u t s i d e a c c e p t a n c e l i m i t s f o r t h e M S a n d / o r M S D a n d / o r P D S d u e t o s u s p e c t e d m a t r i x i n t e r f e r e n c e . S a m p l e r e s u l t s f o r t h e Q C b a t c h we r e a c c e p t e d b a s e d o n a c c e p t a b l e L C S r e c o v e r i e s . QM - 0 2 Th e s p i k e r e c o v e r y i s o u t s i d e a c c e p t a n c e l i m i t s d u e t o i n s i g n i f i c a n t s p i k e a m o u n t a s c o m p a r e d t o s a m p l e c o n c e n t r a t i o n . J Es t i m a t e d v a l u e l e s s t h a n R e p o r t i n g L i m i t ( R L ) b u t g r e a t e r t h a n M e t h o d D e t e c t i o n L i m i t ( M D L ) ( C L P J - F l a g ) . H- 0 2 Sa m p l e w a s p r e p a r e d a n d / o r a n a l y z e d o u t s i d e o f t h e E PA r e c o m m e n d e d h o l d i n g t i m e . S e e C a s e N a r r a t i v e . BO D - 4 La b C o n t r o l ( G G A ) r e c o v e r y w a s o u t s i d e c o n t r o l l i m i t s b i a s e d h i g h . A s t h e p o s s i b l e b i a s i s h i g h , v a l u e s r e p o r t e d a s N D a n d / o r t h o s e b e l o w p e r m i t l i m i t s w e r e n o t a f fe c t e d . O t h e r v a l u e s a r e r e p o r t e d a s e s t i m a t e d w i t h p o s s i b l e h i g h b i a s . > Gr e a t e r t h a n t h e r e s u l t v a l u e r e p o r t e d . Page 153 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 No t e : U n l e s s o t h e r w i s e n o t e d , a l l r e s u l t s a r e r e p o r t e d o n a n a s r e c e i v e d b a s i s . Page 154 of 155 cdmsmith.com