1107_BuncombeCounty_GWMR_DIN28199_20161007

SCS Engineers, P.C. Environmental Consultants 4767 New Broad Street 407 514-2766 and Contractors Suite 222 FAX [phone] Orlando, FL 32814 www.scsengineers.com

Offices Nationwide
January 23, 2017
File No. 09204072.13
Mrs. Jackie Drummond Compliance Hydrogeologist
Division of Waste Management - Solid Waste Section NC Department of Environmental Quality Asheville Regional Office 2090 US Highway 70, Swannanoa, NC 28778 Subject: Sampling Report Buncombe County Solid Waste Management Facility Landfill
Buncombe County Permit No. 1107 Dear Mrs. Drummond:

The purpose of this letter is to notify the Solid Waste Section that semi-annual sampling has been completed at the Buncombe County Solid Waste Management Facility Landfill. Water quality samples were collected from each of the monitoring wells, surface water sampling locations in addition to leachate samples.

Metals and sulfate were the only constituents detected in monitoring well samples which exceeded North Carolina 2L (NC2L) Groundwater and Surface Water Standards (SWS) in concentrations which are consistent with previous sampling results and are generally recognized as naturally occurring. Leachate sampling demonstrated no constituents were above their SWS
reporting limits.
Currently 25 monitoring wells are sampled semi-annually. Groundwater samples were collected from October 7th through 12th, 2016. The six surface water and six leachate samples were collected on April 4th, 2016. All samples were collected and analyzed by Pace Laboratories in
Asheville, NC for analysis of the current landfill constituents list (Appendix I VOC (EPA 8260);
Appendix I Metals (EPA 6010) plus mercury (EPA 7470), sulfate (EPA 300.0), chloride (SM 4500-Cl-E), Alkalinity (SM 2320B), and Total Dissolved Solids (SM 2540C)). Groundwater elevations were also measured and groundwater contour maps for both the shallow
and deep flow regimes as presented in Attachment A. Field parameters and the well condition
were evaluated as presented in Attachment B Well Condition Summary and Attachment C Sampling Forms. Field parameters included: pH, specific conductivity, temperature, dissolved oxygen, and oxidation/reduction potential, temperature, and turbidity. Field parameters were also measured at the surface water sampling locations.

Twelve of the 25 monitoring wells (including the two background wells) had concentrations in excess of the North Carolina 2L Groundwater Standards. One surface water samples had

Jackie Drummond
January 23, 2017
Page 2
concentrations in excess of the SWS reporting limits. A summary of detections is provided in Attachment D, a summary of exceedances is provided as Attachment E. Total Dissolved Solids was detected above the maximum contaminant level of 500,000 µg/L in
MW-12 (528,000 µg/L). Metal constituents detected include barium, chromium, cobalt, copper, iron, manganese, nickel, thallium, vanadium, and zinc. Chromium was detected above the maximum contaminant level of 10 µg/L in MW-12 (15.1 µg/L). Cobalt was detected above the maximum contaminant level of 1 µg/L in MW-12 (19.5 µg/L), MW-13 (31.7 µg/L), MW-13D (23.5 µg/L), and MW-15S (74.8 µg/L). Iron was detected above the maximum contaminant level
of 300 µg/L in MW-1 (1,160 µg/L), MW-1D (1,060 µg/L), MW-12D (917 µg/L), MW-14 (1,620 µg/L), MW-15S (5,030 µg/L), and MW-15D (349 µg/L). Manganese was detected above the maximum contaminant level of 50 µg/L in MW-12 (413 µg/L), MW-12D (65.1 µg/L), MW-15S (12,100 µg/L), and MW-15D (239 µg/L). Thallium was detected above the maximum contaminant level of 0.28 µg/L in MW-12 (6.6 µg/L). Vanadium was detected above the
maximum contaminant level of 0.3 µg/L in MW-1 (7.6 µg/L), MW-3R (8.4 µg/L), MW-5 (5.6 µg/L), MW-10 (16.3 µg/L), MW-12D (31.2 µg/L), MW-14 (6.7 µg/L), MW-15S (6.1 µg/L), and MW-15D (5.6 µg/L). No Appendix I VOCs were detected in groundwater samples. Metal constituents detected in surface water samples include antimony, arsenic, barium,
chromium, cobalt, nickel, vanadium and zinc. No Appendix I VOCs were detected in surface water samples. One surface water sample, SW-6, had concentrations in excess of the SWS reporting limits for chromium, cobalt, and vanadium which has been associated with high turbidity (95.7 NTUs) upon sample collection October 7, 2016. The field sampler reported very low flow conditions with sediment being disturbed to collect sufficient sample volumes. SW-6
was subsequently re-sampled on December 14th, 2016 which confirmed an exceedance for cobalt. A geochemical atlas of North Carolina, U.S.A. was prepared using National Uranium Resource Evaluation (NURE) stream-sediment data. Stream sediment of weathered bedrock typical of the
nearby source formations was developed to assist mineral exploration. These data also serve to provide a baseline from which to assess naturally occurring metals in landfill saprolite and PWR. Naturally occurring cobalt has been documented in stream sediments in North Carolina, with higher concentrations noted in Buncombe County. This stream data was presented in the Alternate Source Demonstration (ASD) submitted January 4, 2017
Metal constituents detected in leachate samples include arsenic, barium, chromium, cobalt, copper, nickel, thallium, and zinc. VOC constituents detected in leachate samples include 1,1-dichloroethane, benzene, toluene, and vinyl chloride.
Metals detected in monitoring well samples and surface water sample SW-6 which exceeded NC2L Standards are consistent with previous sampling results. Based on the ASD it appears that our previous notations noting naturally occurring metals have been confirmed. The next Semi-Annual sampling event is scheduled for Spring 2017. This submittal, which
included a discussion of the sampling of the approved groundwater and surface water quality

Jackie Drummond
January 23, 2017
Page 3
monitoring network, satisfies the groundwater and surface water monitoring criteria necessary to operate the Buncombe County Landfill.
Sincerely,

C. Ed Hilton, Jr. P.E. Brooke Fait, MPH
Vice President/Project Director Environmental Health & Safety Project
Manager
SCS ENGINEERS SCS ENGINEERS
BLF/CEH
Buncombe County, North Carolina
Attachment A- Figures
Buncombe County, North Carolina
Attachment B- Well Condition Summary
Buncombe County, North Carolina
Attachment C- Field Reports
Buncombe County, North Carolina
Attachment D- Detection Table
Analytical Results Summary
Buncombe County New Facility
From:06/01/2016 To:12/31/2016
Well ID Parameter Sample Date Result Flags Units
MW‐1
Alkalinity, Total
10/12/2016 43800 ug/L
Barium, Dissolved
10/12/2016 103 ug/L
Barium, Total
10/12/2016 136 ug/L
Chloride
10/12/2016 4360 ug/L
Dissolved Oxygen
10/12/2016 6.43 mg/L
Iron, Total
10/12/2016 1160 ug/L
Manganese, Total
10/12/2016 14.8 ug/L
ORP ‐ Field
10/12/2016 156.7 mV
pH ‐ Field
10/12/2016 6.8 Std. Units
Specific Conductivity ‐ Field
10/12/2016 155 umhos/cm
Sulfate
10/12/2016 15400 ug/L
Temperature ‐ Field
10/12/2016 16.2 deg C
Total Dissolved Solids
10/12/2016 135000 ug/L
Turbidity ‐ Field
10/12/2016 14.09 NTU
Vanadium, Total
10/12/2016 7.6 ug/L
MW‐10
Barium, Dissolved
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 1 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐10
Barium, Dissolved
10/11/2016 132 ug/L
Barium, Total
10/11/2016 148 ug/L
Dissolved Oxygen
10/11/2016 3.44 mg/L
ORP ‐ Field
10/11/2016 101.1 mV
pH ‐ Field
10/11/2016 6.5 Std. Units
Specific Conductivity ‐ Field
10/11/2016 305 umhos/cm
Temperature ‐ Field
10/11/2016 15 deg C
Turbidity ‐ Field
10/11/2016 3.6 NTU
Vanadium, Dissolved
10/11/2016 10.6 ug/L
Vanadium, Total
10/11/2016 16.3 ug/L
Zinc, Dissolved
10/11/2016 10.4 ug/L
Zinc, Total
10/11/2016 12 ug/L
MW‐10D
Barium, Dissolved
10/11/2016 13.7 ug/L
Barium, Total
10/11/2016 15.4 ug/L
Dissolved Oxygen
10/11/2016 3.42 mg/L
Nickel, Dissolved
10/11/2016 5.5 ug/L
Nickel, Total
10/11/2016 6 ug/L
ORP ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 2 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐10D
ORP ‐ Field
10/11/2016 107.6 mV
pH ‐ Field
10/11/2016 6.4 Std. Units
Specific Conductivity ‐ Field
10/11/2016 280 umhos/cm
Temperature ‐ Field
10/11/2016 14.7 deg C
Turbidity ‐ Field
10/11/2016 2.36 NTU
MW‐11
Barium, Dissolved
10/11/2016 81.8 ug/L
Barium, Total
10/11/2016 89.6 ug/L
Dissolved Oxygen
10/11/2016 5.23 mg/L
Nickel, Dissolved
10/11/2016 8.6 ug/L
Nickel, Total
10/11/2016 9.9 ug/L
ORP ‐ Field
10/11/2016 130.4 mV
pH ‐ Field
10/11/2016 6.6 Std. Units
Specific Conductivity ‐ Field
10/11/2016 407 umhos/cm
Temperature ‐ Field
10/11/2016 16.2 deg C
Turbidity ‐ Field
10/11/2016 1.38 NTU
MW‐11D
Barium, Dissolved
10/11/2016 15.1 ug/L
Barium, Total
10/11/2016 16.5 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 3 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐11D
Dissolved Oxygen
10/11/2016 2.03 mg/L
ORP ‐ Field
10/11/2016 125.9 mV
pH ‐ Field
10/11/2016 6.6 Std. Units
Specific Conductivity ‐ Field
10/11/2016 387 umhos/cm
Temperature ‐ Field
10/11/2016 15.8 deg C
Turbidity ‐ Field
10/11/2016 0.74 NTU
MW‐12
Alkalinity, Total
10/12/2016 183000 ug/L
Barium, Dissolved
10/12/2016 70 ug/L
Barium, Total
10/12/2016 287 ug/L
Chloride
10/12/2016 35000 ug/L
Chromium, Total
10/12/2016 15.1 ug/L
Cobalt, Total
10/12/2016 19.5 ug/L
Copper, Total
10/12/2016 20.4 ug/L
Dissolved Oxygen
10/12/2016 2.44 mg/L
Iron, Total
10/12/2016 84.7 ug/L
Manganese, Total
10/12/2016 413 ug/L
Nickel, Dissolved
10/12/2016 14.9 ug/L
Nickel, Total
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 4 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐12
Nickel, Total
10/12/2016 30.9 ug/L
ORP ‐ Field
10/12/2016 165.4 mV
pH ‐ Field
10/12/2016 6.3 Std. Units
Specific Conductivity ‐ Field
10/12/2016 890 umhos/cm
Sulfate
10/12/2016 171000 ug/L
Temperature ‐ Field
10/12/2016 18.5 deg C
Thallium, Total
10/12/2016 6.6 ug/L
Total Dissolved Solids
10/12/2016 528000 ug/L
Turbidity ‐ Field
10/12/2016 2.54 NTU
Vanadium, Total
10/12/2016 31.2 ug/L
Zinc, Total
10/12/2016 28.5 ug/L
MW‐12D
Alkalinity, Total
10/12/2016 162000 ug/L
Barium, Dissolved
10/12/2016 39.4 ug/L
Barium, Total
10/12/2016 46.5 ug/L
Chloride
10/12/2016 14000 ug/L
Dissolved Oxygen
10/12/2016 1.8 mg/L
Iron, Total
10/12/2016 917 ug/L
Manganese, Total
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 5 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐12D
Manganese, Total
10/12/2016 65.1 ug/L
ORP ‐ Field
10/12/2016 156.9 mV
pH ‐ Field
10/12/2016 6.6 Std. Units
Specific Conductivity ‐ Field
10/12/2016 498 umhos/cm
Sulfate
10/12/2016 53100 ug/L
Temperature ‐ Field
10/12/2016 17.6 deg C
Total Dissolved Solids
10/12/2016 292000 ug/L
Turbidity ‐ Field
10/12/2016 13.47 NTU
MW‐13
Barium, Dissolved
10/11/2016 222 ug/L
Barium, Total
10/11/2016 248 ug/L
Cobalt, Dissolved
10/11/2016 29.6 ug/L
Cobalt, Total
10/11/2016 31.7 ug/L
Dissolved Oxygen
10/11/2016 1.8 mg/L
ORP ‐ Field
10/11/2016 ‐43.6 mV
pH ‐ Field
10/11/2016 6.5 Std. Units
Specific Conductivity ‐ Field
10/11/2016 400 umhos/cm
Temperature ‐ Field
10/11/2016 17.7 deg C
Turbidity ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 6 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐13
Turbidity ‐ Field
10/11/2016 4.82 NTU
MW‐13D
Barium, Dissolved
10/11/2016 312 ug/L
Barium, Total
10/11/2016 348 ug/L
Cobalt, Dissolved
10/11/2016 21.6 ug/L
Cobalt, Total
10/11/2016 23.5 ug/L
Dissolved Oxygen
10/11/2016 2 mg/L
Nickel, Dissolved
10/11/2016 20.8 ug/L
Nickel, Total
10/11/2016 22.2 ug/L
ORP ‐ Field
10/11/2016 26.4 mV
pH ‐ Field
10/11/2016 6.2 Std. Units
Specific Conductivity ‐ Field
10/11/2016 431 umhos/cm
Temperature ‐ Field
10/11/2016 18 deg C
Turbidity ‐ Field
10/11/2016 3.12 NTU
Zinc, Total
10/11/2016 10.9 ug/L
MW‐14
Alkalinity, Total
10/12/2016 64500 ug/L
Barium, Dissolved
10/12/2016 42.3 ug/L
Barium, Total
10/12/2016 60 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 7 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐14
Chloride
10/12/2016 2390 ug/L
Dissolved Oxygen
10/12/2016 7.75 mg/L
Iron, Total
10/12/2016 1620 ug/L
Manganese, Total
10/12/2016 12.8 ug/L
ORP ‐ Field
10/12/2016 169.6 mV
pH ‐ Field
10/12/2016 6.7 Std. Units
Specific Conductivity ‐ Field
10/12/2016 196 umhos/cm
Sulfate
10/12/2016 23300 ug/L
Temperature ‐ Field
10/12/2016 14.7 deg C
Total Dissolved Solids
10/12/2016 174000 ug/L
Turbidity ‐ Field
10/12/2016 33.28 NTU
Vanadium, Total
10/12/2016 6.7 ug/L
MW‐14D
Alkalinity, Total
10/12/2016 125000 ug/L
Chloride
10/12/2016 2370 ug/L
Dissolved Oxygen
10/12/2016 9.57 mg/L
ORP ‐ Field
10/12/2016 164.7 mV
pH ‐ Field
10/12/2016 6.5 Std. Units
Specific Conductivity ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 8 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐14D
Specific Conductivity ‐ Field
10/12/2016 275 umhos/cm
Sulfate
10/12/2016 17200 ug/L
Temperature ‐ Field
10/12/2016 15 deg C
Total Dissolved Solids
10/12/2016 199000 ug/L
Turbidity ‐ Field
10/12/2016 0.82 NTU
MW‐15D
Alkalinity, Total
10/12/2016 140000 ug/L
Barium, Dissolved
10/12/2016 161 ug/L
Barium, Total
10/12/2016 173 ug/L
Chloride
10/12/2016 12600 ug/L
Dissolved Oxygen
10/12/2016 3.39 mg/L
Iron, Total
10/12/2016 349 ug/L
Manganese, Total
10/12/2016 239 ug/L
Nickel, Dissolved
10/12/2016 6.7 ug/L
Nickel, Total
10/12/2016 7.6 ug/L
ORP ‐ Field
10/12/2016 131.8 mV
pH ‐ Field
10/12/2016 6.3 Std. Units
Specific Conductivity ‐ Field
10/12/2016 421 umhos/cm
Sulfate
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 9 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐15D
Sulfate
10/12/2016 54200 ug/L
Temperature ‐ Field
10/12/2016 15.4 deg C
Total Dissolved Solids
10/12/2016 297000 ug/L
Turbidity ‐ Field
10/12/2016 6.53 NTU
MW‐15S
Alkalinity, Total
10/12/2016 185000 ug/L
Barium, Dissolved
10/12/2016 162 ug/L
Barium, Total
10/12/2016 198 ug/L
Chloride
10/12/2016 16800 ug/L
Chromium, Total
10/12/2016 5.6 ug/L
Cobalt, Dissolved
10/12/2016 66.4 ug/L
Cobalt, Total
10/12/2016 74.8 ug/L
Dissolved Oxygen
10/12/2016 2.4 mg/L
Iron, Total
10/12/2016 5030 ug/L
Manganese, Total
10/12/2016 12100 ug/L
Nickel, Dissolved
10/12/2016 6 ug/L
Nickel, Total
10/12/2016 9 ug/L
ORP ‐ Field
10/12/2016 94 mV
pH ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 10 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐15S
pH ‐ Field
10/12/2016 6.3 Std. Units
Specific Conductivity ‐ Field
10/12/2016 443 umhos/cm
Sulfate
10/12/2016 27800 ug/L
Temperature ‐ Field
10/12/2016 17.2 deg C
Total Dissolved Solids
10/12/2016 266000 ug/L
Turbidity ‐ Field
10/12/2016 9.21 NTU
Vanadium, Total
10/12/2016 6.1 ug/L
Zinc, Total
10/12/2016 12.8 ug/L
MW‐1D
Alkalinity, Total
10/12/2016 72400 ug/L
Barium, Dissolved
10/12/2016 23.3 ug/L
Barium, Total
10/12/2016 35.3 ug/L
Chloride
10/12/2016 2280 ug/L
Chromium, Total
10/12/2016 6.7 ug/L
Dissolved Oxygen
10/12/2016 5.46 mg/L
Iron, Total
10/12/2016 1060 ug/L
Manganese, Total
10/12/2016 16 ug/L
Nickel, Total
10/12/2016 7 ug/L
ORP ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 11 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐1D
ORP ‐ Field
10/12/2016 166.6 mV
pH ‐ Field
10/12/2016 6.7 Std. Units
Specific Conductivity ‐ Field
10/12/2016 242 umhos/cm
Sulfate
10/12/2016 40500 ug/L
Temperature ‐ Field
10/12/2016 15.7 deg C
Total Dissolved Solids
10/12/2016 196000 ug/L
Turbidity ‐ Field
10/12/2016 33.78 NTU
Zinc, Total
10/12/2016 11.1 ug/L
MW‐2
Barium, Dissolved
10/11/2016 61 ug/L
Barium, Total
10/11/2016 68.1 ug/L
Dissolved Oxygen
10/11/2016 4.55 mg/L
ORP ‐ Field
10/11/2016 97.4 mV
pH ‐ Field
10/11/2016 6.8 Std. Units
Specific Conductivity ‐ Field
10/11/2016 189 umhos/cm
Temperature ‐ Field
10/11/2016 14.3 deg C
Turbidity ‐ Field
10/11/2016 1.93 NTU
MW‐2D
Barium, Dissolved
10/11/2016 96 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 12 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐2D
Barium, Total
10/11/2016 104 ug/L
Dissolved Oxygen
10/11/2016 4.03 mg/L
ORP ‐ Field
10/11/2016 112.2 mV
pH ‐ Field
10/11/2016 6.7 Std. Units
Specific Conductivity ‐ Field
10/11/2016 266 umhos/cm
Temperature ‐ Field
10/11/2016 14.4 deg C
Turbidity ‐ Field
10/11/2016 1.59 NTU
MW‐3R
Barium, Dissolved
10/11/2016 90.6 ug/L
Barium, Total
10/11/2016 119 ug/L
Chromium, Total
10/11/2016 5.2 ug/L
Dissolved Oxygen
10/11/2016 5.28 mg/L
Nickel, Dissolved
10/11/2016 5.8 ug/L
Nickel, Total
10/11/2016 7.7 ug/L
ORP ‐ Field
10/11/2016 112.7 mV
pH ‐ Field
10/11/2016 6.5 Std. Units
Specific Conductivity ‐ Field
10/11/2016 176 umhos/cm
Temperature ‐ Field
10/11/2016 14 deg C
Turbidity ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 13 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐3R
Turbidity ‐ Field
10/11/2016 25.1 NTU
Vanadium, Total
10/11/2016 8.4 ug/L
MW‐4
Barium, Dissolved
10/11/2016 63.3 ug/L
Barium, Total
10/11/2016 69.5 ug/L
Dissolved Oxygen
10/11/2016 2.95 mg/L
ORP ‐ Field
10/11/2016 134.3 mV
pH ‐ Field
10/11/2016 6.4 Std. Units
Specific Conductivity ‐ Field
10/11/2016 213 umhos/cm
Temperature ‐ Field
10/11/2016 16.1 deg C
Turbidity ‐ Field
10/11/2016 8.31 NTU
MW‐4D
Barium, Dissolved
10/11/2016 26.5 ug/L
Barium, Total
10/11/2016 29.5 ug/L
Dissolved Oxygen
10/11/2016 2.7 mg/L
ORP ‐ Field
10/11/2016 138.4 mV
pH ‐ Field
10/11/2016 6.3 Std. Units
Specific Conductivity ‐ Field
10/11/2016 252 umhos/cm
Temperature ‐ Field
10/11/2016 16.5 deg C
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 14 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐4D
Turbidity ‐ Field
10/11/2016 3.06 NTU
MW‐5
Barium, Dissolved
10/11/2016 102 ug/L
Barium, Total
10/11/2016 119 ug/L
Dissolved Oxygen
10/11/2016 2.65 mg/L
ORP ‐ Field
10/11/2016 146.4 mV
pH ‐ Field
10/11/2016 6.2 Std. Units
Specific Conductivity ‐ Field
10/11/2016 214 umhos/cm
Temperature ‐ Field
10/11/2016 15.9 deg C
Turbidity ‐ Field
10/11/2016 10.89 NTU
Vanadium, Total
10/11/2016 5.6 ug/L
MW‐5D
Barium, Dissolved
10/11/2016 61.8 ug/L
Barium, Total
10/11/2016 66.7 ug/L
Dissolved Oxygen
10/11/2016 2.4 mg/L
ORP ‐ Field
10/11/2016 147 mV
pH ‐ Field
10/11/2016 6.1 Std. Units
Specific Conductivity ‐ Field
10/11/2016 202 umhos/cm
Temperature ‐ Field
10/11/2016 15.8 deg C
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 15 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐5D
Turbidity ‐ Field
10/11/2016 2.42 NTU
MW‐6
Barium, Dissolved
10/11/2016 48.6 ug/L
Barium, Total
10/11/2016 61.8 ug/L
Dissolved Oxygen
10/11/2016 2.32 mg/L
ORP ‐ Field
10/11/2016 150.4 mV
pH ‐ Field
10/11/2016 6.5 Std. Units
Specific Conductivity ‐ Field
10/11/2016 151 umhos/cm
Temperature ‐ Field
10/11/2016 15.3 deg C
Turbidity ‐ Field
10/11/2016 23.13 NTU
MW‐7
Barium, Dissolved
10/11/2016 123 ug/L
Barium, Total
10/11/2016 136 ug/L
Dissolved Oxygen
10/11/2016 2.01 mg/L
Nickel, Dissolved
10/11/2016 10.5 ug/L
Nickel, Total
10/11/2016 12.1 ug/L
ORP ‐ Field
10/11/2016 58.1 mV
pH ‐ Field
10/11/2016 6.1 Std. Units
Specific Conductivity ‐ Field
10/11/2016 588 umhos/cm
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 16 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐7
Temperature ‐ Field
10/11/2016 16.5 deg C
Turbidity ‐ Field
10/11/2016 4.61 NTU
MW‐8
Barium, Dissolved
10/11/2016 125 ug/L
Barium, Total
10/11/2016 142 ug/L
Dissolved Oxygen
10/11/2016 4.26 mg/L
ORP ‐ Field
10/11/2016 138.6 mV
pH ‐ Field
10/11/2016 6.6 Std. Units
Specific Conductivity ‐ Field
10/11/2016 374 umhos/cm
Temperature ‐ Field
10/11/2016 16.3 deg C
Turbidity ‐ Field
10/11/2016 9.43 NTU
MW‐8D
Barium, Dissolved
10/11/2016 156 ug/L
Barium, Total
10/11/2016 172 ug/L
Dissolved Oxygen
10/11/2016 2.14 mg/L
ORP ‐ Field
10/11/2016 137.6 mV
pH ‐ Field
10/11/2016 6.5 Std. Units
Specific Conductivity ‐ Field
10/11/2016 408 umhos/cm
Temperature ‐ Field
10/11/2016 16.3 deg C
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 17 of 18
Well ID Parameter Sample Date Result Flags Units
MW‐8D
Turbidity ‐ Field
10/11/2016 1.2 NTU
Zinc, Total
10/11/2016 13.4 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 18 of 18
Analytical Results Summary
Buncombe County New Facility
From:06/01/2016 To:12/31/2016
Well ID Parameter Sample Date Result Flags Units
LD‐1
1,1‐Dichloroethane
10/7/2016 2.3 ug/L
Barium, Total
10/7/2016 72.3 ug/L
Cobalt, Total
10/7/2016 255 ug/L
Dissolved Oxygen
10/7/2016 0.81 mg/L
Nickel, Total
10/7/2016 59.5 ug/L
ORP ‐ Field
10/7/2016 53.2 mV
pH ‐ Field
10/7/2016 5.9 Std. Units
Specific Conductivity ‐ Field
10/7/2016 527 umhos/cm
Temperature ‐ Field
10/7/2016 17.9 deg C
Turbidity ‐ Field
10/7/2016 0.83 NTU
LD‐2
1,1‐Dichloroethane
10/7/2016 2.8 ug/L
Barium, Total
10/7/2016 155 ug/L
Cobalt, Total
10/7/2016 27.8 ug/L
Dissolved Oxygen
10/7/2016 4.5 mg/L
Nickel, Total
10/7/2016 7.3 ug/L
ORP ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 1 of 5
Well ID Parameter Sample Date Result Flags Units
LD‐2
ORP ‐ Field
10/7/2016 ‐16.5 mV
pH ‐ Field
10/7/2016 6.1 Std. Units
Specific Conductivity ‐ Field
10/7/2016 382 umhos/cm
Temperature ‐ Field
10/7/2016 17.1 deg C
Turbidity ‐ Field
10/7/2016 10.14 NTU
LD‐3
Barium, Total
10/7/2016 288 ug/L
Benzene
10/7/2016 1.7 ug/L
Cobalt, Total
10/7/2016 11.5 ug/L
Dissolved Oxygen
10/7/2016 1.8 mg/L
Nickel, Total
10/7/2016 8.3 ug/L
ORP ‐ Field
10/7/2016 3.5 mV
pH ‐ Field
10/7/2016 6.2 Std. Units
Specific Conductivity ‐ Field
10/7/2016 528 umhos/cm
Temperature ‐ Field
10/7/2016 16.7 deg C
Turbidity ‐ Field
10/7/2016 9 NTU
LD‐4
1,1‐Dichloroethane
10/7/2016 1.5 ug/L
Barium, Total
10/7/2016 420 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 2 of 5
Well ID Parameter Sample Date Result Flags Units
LD‐4
Benzene
10/7/2016 3 ug/L
Chromium, Total
10/7/2016 199 ug/L
Copper, Total
10/7/2016 54.1 ug/L
Dissolved Oxygen
10/7/2016 2.2 mg/L
Nickel, Total
10/7/2016 60.2 ug/L
ORP ‐ Field
10/7/2016 57.8 mV
pH ‐ Field
10/7/2016 5.8 Std. Units
Specific Conductivity ‐ Field
10/7/2016 207 umhos/cm
Temperature ‐ Field
10/7/2016 17.4 deg C
Toluene
10/7/2016 1.2 ug/L
Turbidity ‐ Field
10/7/2016 54.8 NTU
Vinyl chloride
10/7/2016 1.2 ug/L
Zinc, Total
10/7/2016 12.2 ug/L
LD‐5
Barium, Total
10/7/2016 215 ug/L
Cobalt, Total
10/7/2016 85.4 ug/L
Dissolved Oxygen
10/7/2016 3.4 mg/L
Nickel, Total
10/7/2016 26 ug/L
ORP ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 3 of 5
Well ID Parameter Sample Date Result Flags Units
LD‐5
ORP ‐ Field
10/7/2016 201.1 mV
pH ‐ Field
10/7/2016 6.4 Std. Units
Specific Conductivity ‐ Field
10/7/2016 751 umhos/cm
Temperature ‐ Field
10/7/2016 20.1 deg C
Turbidity ‐ Field
10/7/2016 43.89 NTU
LD‐6
Barium, Total
10/7/2016 456 ug/L
Cobalt, Total
10/7/2016 62.9 ug/L
Dissolved Oxygen
10/7/2016 1.5 mg/L
ORP ‐ Field
10/7/2016 10.9 mV
pH ‐ Field
10/7/2016 6.4 Std. Units
Specific Conductivity ‐ Field
10/7/2016 551 umhos/cm
Temperature ‐ Field
10/7/2016 18.5 deg C
Thallium, Total
10/7/2016 5.6 ug/L
Turbidity ‐ Field
10/7/2016 1.6 NTU
Leachate LD
Arsenic, Total
10/7/2016 26.1 ug/L
Barium, Total
10/7/2016 16.8 ug/L
Cobalt, Total
10/7/2016 117 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 4 of 5
Well ID Parameter Sample Date Result Flags Units
Leachate LD
Copper, Total
10/7/2016 36.6 ug/L
Dissolved Oxygen
10/7/2016 5.33 mg/L
Nickel, Total
10/7/2016 691 ug/L
ORP ‐ Field
10/7/2016 347.4 mV
pH ‐ Field
10/7/2016 4.6 Std. Units
Specific Conductivity ‐ Field
10/7/2016 734 umhos/cm
Temperature ‐ Field
10/7/2016 17 deg C
Turbidity ‐ Field
10/7/2016 3.8 NTU
Zinc, Total
10/7/2016 276 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 5 of 5
Analytical Results Summary
Buncombe County New Facility
From:06/01/2016 To:12/31/2016
Well ID Parameter Sample Date Result Flags Units
SW‐2
Barium, Total
10/7/2016 52.2 ug/L
Dissolved Oxygen
10/7/2016 9.65 mg/L
ORP ‐ Field
10/7/2016 149.3 mV
pH ‐ Field
10/7/2016 7.8 Std. Units
Specific Conductivity ‐ Field
10/7/2016 161 umhos/cm
Temperature ‐ Field
10/7/2016 14.9 deg C
Turbidity ‐ Field
10/7/2016 6.8 NTU
SW‐4
Barium, Total
10/7/2016 131 ug/L
Dissolved Oxygen
10/7/2016 6.98 mg/L
ORP ‐ Field
10/7/2016 149.2 mV
pH ‐ Field
10/7/2016 8.1 Std. Units
Specific Conductivity ‐ Field
10/7/2016 366 umhos/cm
Temperature ‐ Field
10/7/2016 16.6 deg C
Turbidity ‐ Field
10/7/2016 149.3 NTU
Zinc, Total
10/7/2016 12.1 ug/L
SW‐5
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 1 of 5
Well ID Parameter Sample Date Result Flags Units
SW‐5
Barium, Total
10/7/2016 60.6 ug/L
Dissolved Oxygen
10/7/2016 8.01 mg/L
Nickel, Total
10/7/2016 15.5 ug/L
ORP ‐ Field
10/7/2016 21.7 mV
pH ‐ Field
10/7/2016 8.4 Std. Units
Specific Conductivity ‐ Field
10/7/2016 160 umhos/cm
Temperature ‐ Field
10/7/2016 16.9 deg C
Turbidity ‐ Field
10/7/2016 4.34 NTU
SW‐6
Barium, Total
10/7/2016 155 ug/L
Chromium, Total
10/7/2016 10.6 ug/L
Cobalt, Total
10/7/2016 7.7 ug/L
Copper, Total
10/7/2016 6.9 ug/L
Dissolved Oxygen
10/7/2016 4.9 mg/L
Nickel, Total
10/7/2016 9.7 ug/L
ORP ‐ Field
10/7/2016 104.5 mV
pH ‐ Field
10/7/2016 7.5 Std. Units
Specific Conductivity ‐ Field
10/7/2016 315 umhos/cm
Temperature ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 2 of 5
Well ID Parameter Sample Date Result Flags Units
SW‐6
Temperature ‐ Field
10/7/2016 17.7 deg C
Turbidity ‐ Field
10/7/2016 95.65 NTU
Vanadium, Total
10/7/2016 22 ug/L
Zinc, Total
10/7/2016 25.2 ug/L
SW‐6 Resample
Antimony, Total
12/14/2016 5 ug/L
Arsenic, Total
12/14/2016 10 ug/L
Barium, Total
12/14/2016 105 ug/L
Beryllium, Total
12/14/2016 1 ug/L
Cadmium, Total
12/14/2016 1 ug/L
Chromium, Total
12/14/2016 5 ug/L
Cobalt, Total
12/14/2016 7 ug/L
Copper, Total
12/14/2016 5 ug/L
Dissolved Oxygen
12/14/2016 8 mg/L
Lead, Total
12/14/2016 5 ug/L
Nickel, Total
12/14/2016 5 ug/L
ORP ‐ Field
12/14/2016 78.7 mV
pH ‐ Field
12/14/2016 6.3 Std. Units
Selenium, Total
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 3 of 5
Well ID Parameter Sample Date Result Flags Units
SW‐6 Resample
Selenium, Total
12/14/2016 10 ug/L
Silver, Total
12/14/2016 5 ug/L
Specific Conductivity ‐ Field
12/14/2016 255.7 umhos/cm
Temperature ‐ Field
12/14/2016 13 deg C
Thallium, Total
12/14/2016 5.4 ug/L
Turbidity ‐ Field
12/14/2016 0.6 NTU
Vanadium, Total
12/14/2016 5 ug/L
Zinc, Total
12/14/2016 10 ug/L
SW‐Leachate
Antimony, Total
10/7/2016 10.7 ug/L
Arsenic, Total
10/7/2016 14.2 ug/L
Barium, Total
10/7/2016 240 ug/L
Chromium, Total
10/7/2016 38.4 ug/L
Cobalt, Total
10/7/2016 15.7 ug/L
Dissolved Oxygen
10/7/2016 17.01 mg/L
Nickel, Total
10/7/2016 81.6 ug/L
ORP ‐ Field
10/7/2016 168.3 mV
pH ‐ Field
10/7/2016 8.4 Std. Units
Specific Conductivity ‐ Field
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 4 of 5
Well ID Parameter Sample Date Result Flags Units
SW‐Leachate
Specific Conductivity ‐ Field
10/7/2016 5305 umhos/cm
Temperature ‐ Field
10/7/2016 22.3 deg C
Turbidity ‐ Field
10/7/2016 82.89 NTU
Vanadium, Total
10/7/2016 23.5 ug/L
Zinc, Total
10/7/2016 12.9 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 5 of 5
Buncombe County, North Carolina
Attachment E- Exceedances Table
Analytical Results Summary
Buncombe County New Facility
From:06/01/2016 To:12/31/2016
Well ID Parameter Sample Date Result Flags UnitsMCL
MW‐1
Iron, Total 300
10/12/2016 1160 ug/L
Vanadium, Total 0.3
10/12/2016 7.6 ug/L
MW‐10
Vanadium, Total 0.3
10/11/2016 16.3 ug/L
MW‐12
Chromium, Total 10
10/12/2016 15.1 ug/L
Cobalt, Total 1
10/12/2016 19.5 ug/L
Manganese, Total 50
10/12/2016 413 ug/L
Thallium, Total 0.28
10/12/2016 6.6 ug/L
Total Dissolved Solids 500000
10/12/2016 528000 ug/L
Vanadium, Total 0.3
10/12/2016 31.2 ug/L
MW‐12D
Iron, Total 300
10/12/2016 917 ug/L
Manganese, Total 50
10/12/2016 65.1 ug/L
MW‐13
Cobalt, Total 1
10/11/2016 31.7 ug/L
MW‐13D
Cobalt, Total 1
10/11/2016 23.5 ug/L
MW‐14
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 1 of 2
Well ID Parameter Sample Date Result Flags UnitsMCL
MW‐14
Iron, Total 300
10/12/2016 1620 ug/L
Vanadium, Total 0.3
10/12/2016 6.7 ug/L
MW‐15D
Iron, Total 300
10/12/2016 349 ug/L
Manganese, Total 50
10/12/2016 239 ug/L
MW‐15S
Cobalt, Total 1
10/12/2016 74.8 ug/L
Iron, Total 300
10/12/2016 5030 ug/L
Manganese, Total 50
10/12/2016 12100 ug/L
Vanadium, Total 0.3
10/12/2016 6.1 ug/L
MW‐1D
Iron, Total 300
10/12/2016 1060 ug/L
MW‐3R
Vanadium, Total 0.3
10/11/2016 8.4 ug/L
MW‐5
Vanadium, Total 0.3
10/11/2016 5.6 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 2 of 2
Analytical Results Summary
Buncombe County New Facility
From:06/01/2016 To:12/31/2016
Well ID Parameter Sample Date Result Flags UnitsMCL
SW‐6
Chromium, Total 10
10/7/2016 10.6 ug/L
Cobalt, Total 1
10/7/2016 7.7 ug/L
Vanadium, Total 0.3
10/7/2016 22 ug/L
SW‐6 Resample
Antimony, Total 1
12/14/2016 5 ug/L
Cobalt, Total 1
12/14/2016 7 ug/L
Thallium, Total 0.28
12/14/2016 5.4 ug/L
Vanadium, Total 0.3
12/14/2016 5 ug/L
SW‐Leachate
Antimony, Total 1
10/7/2016 10.7 ug/L
Arsenic, Total 10
10/7/2016 14.2 ug/L
Chromium, Total 10
10/7/2016 38.4 ug/L
Cobalt, Total 1
10/7/2016 15.7 ug/L
Vanadium, Total 0.3
10/7/2016 23.5 ug/L
U  =     Indicates that the compound wasd analyzed for but not detected.
BDL =  Indicates that the compound wasd analyzed for but not detected.
I    =     The reported value is between the laboratory method detection limit and the laboratory practical quatitation limit.
V  =     Indicates the anlyte was detected in both the sample and the associated method blank.
Wednesday, January 18, 2017 Page 1 of 1
Page 112 of 124
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Page 26 of 27
Page 27 of 27
Page 9 of 11
Page 10 of 11
Page 11 of 11
#=CL#
October 24, 2016
LIMS USE: FR - ED HILTON
LIMS OBJECT ID: 92315782
92315782
Project:
Pace Project No.:
RE:
Mr. Ed Hilton
SCS Engineers
4041 Park Oaks Blvd.
Suite 100
Tampa, FL 33610
BUNCOMBE NEW LF C&D Wells
Dear Mr. Hilton:
Enclosed are the analytical results for sample(s) received by the laboratory on October 12, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92315782001 1107-MW1 EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782002 1107-MW1D EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMLS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782003 1107-MW12 EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782004 1107-MW12D EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782005 1107-MW14 EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782006 1107-MW14D EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782007 1107-MW15S EPA 6010 2 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
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Page 3 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
92315782008 1107-MW15D EPA 6010 2 PASI-ASH1
EPA 7470 1 PASI-AWAB
SM 2320B 1 PASI-AKDF
SM 2540C 1 PASI-AMJS1
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW1 Lab ID:92315782001 Collected:10/12/16 13:15 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 1160 ug/L 10/20/16 20:21 7439-89-610/14/16 20:1050.0 1
Manganese 14.8 ug/L 10/20/16 20:21 7439-96-510/14/16 20:105.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/17/16 12:09 7439-97-610/15/16 01:450.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 43800 ug/L 10/18/16 15:4650001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 135000 ug/L 10/13/16 17:39250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 15400 ug/L 10/15/16 16:54 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4360 ug/L 10/24/16 13:44 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/24/2016 04:54 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW1D Lab ID:92315782002 Collected:10/12/16 13:30 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 1060 ug/L 10/18/16 06:26 7439-89-610/13/16 20:3050.0 1
Manganese 16.0 ug/L 10/18/16 06:26 7439-96-510/13/16 20:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/17/16 12:12 7439-97-610/15/16 01:450.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 72400 ug/L 10/18/16 15:5750001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 196000 ug/L 10/17/16 11:59250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 40500 ug/L 10/17/16 19:11 14808-79-840002
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2280 ug/L 10/24/16 13:03 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/24/2016 04:54 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW12 Lab ID:92315782003 Collected:10/12/16 12:00 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 84.7 ug/L 10/18/16 06:29 7439-89-610/13/16 20:3050.0 1
Manganese 413 ug/L 10/18/16 06:29 7439-96-510/13/16 20:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/17/16 12:14 7439-97-610/15/16 01:450.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 183000 ug/L 10/18/16 16:0750001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 528000 ug/L 10/13/16 17:39250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 171000 ug/L 10/15/16 17:15 14808-79-82000010
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 35000 ug/L 10/24/16 13:04 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/24/2016 04:54 PM
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[phone]
Page 7 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW12D Lab ID:92315782004 Collected:10/12/16 12:10 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 917 ug/L 10/18/16 06:32 7439-89-610/13/16 20:3050.0 1
Manganese 65.1 ug/L 10/18/16 06:32 7439-96-510/13/16 20:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/17/16 12:16 7439-97-610/15/16 01:450.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 162000 ug/L 10/18/16 16:4150001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 292000 ug/L 10/13/16 17:39250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 53100 ug/L 10/15/16 17:47 14808-79-8100005
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 14000 ug/L 10/24/16 13:05 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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Page 8 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW14 Lab ID:92315782005 Collected:10/12/16 11:30 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 1620 ug/L 10/18/16 06:35 7439-89-610/13/16 20:3050.0 1
Manganese 12.8 ug/L 10/18/16 06:35 7439-96-510/13/16 20:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/17/16 12:19 7439-97-610/15/16 01:450.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 64500 ug/L 10/18/16 16:5450001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 174000 ug/L 10/13/16 17:40 D6250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 23300 ug/L 10/15/16 17:57 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2390 ug/L 10/24/16 13:06 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/24/2016 04:54 PM
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Page 9 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW14D Lab ID:92315782006 Collected:10/12/16 11:40 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron ND ug/L 10/18/16 06:38 7439-89-610/13/16 20:3050.0 1
Manganese ND ug/L 10/18/16 06:38 7439-96-510/13/16 20:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/17/16 12:26 7439-97-610/15/16 01:450.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 125000 ug/L 10/18/16 17:0650001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 199000 ug/L 10/13/16 17:40250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 17200 ug/L 10/15/16 18:08 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2370 ug/L 10/24/16 13:08 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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Page 10 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW15S Lab ID:92315782007 Collected:10/12/16 12:25 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 5030 ug/L 10/18/16 06:41 7439-89-610/13/16 20:3050.0 1
Manganese 12100 ug/L 10/18/16 16:15 7439-96-510/13/16 20:3025.0 5
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/19/16 10:41 7439-97-610/17/16 16:000.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 185000 ug/L 10/18/16 17:1950001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 266000 ug/L 10/13/16 17:40250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 27800 ug/L 10/15/16 18:18 14808-79-820001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 16800 ug/L 10/24/16 13:15 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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Page 11 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Sample:1107-MW15D Lab ID:92315782008 Collected:10/12/16 12:35 Received:10/12/16 14:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Iron 349 ug/L 10/18/16 06:45 7439-89-610/13/16 20:3050.0 1
Manganese 239 ug/L 10/18/16 06:45 7439-96-510/13/16 20:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 10/19/16 10:43 7439-97-610/17/16 16:000.20 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 140000 ug/L 10/18/16 17:3350001
Analytical Method: SM 2540C2540C Total Dissolved Solids
Total Dissolved Solids 297000 ug/L 10/13/16 17:41250001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 54200 ug/L 10/15/16 18:29 14808-79-8100005
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 12600 ug/L 10/24/16 13:16 16887-00-610001
REPORT OF LABORATORY ANALYSIS
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Page 12 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333122
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005, 92315782006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1846056
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005, 92315782006
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 10/17/16 11:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1846057LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1846058MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315870003
1846059
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12591 12.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/24/2016 04:54 PM
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Page 13 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333431
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92315782007, 92315782008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1847825
Associated Lab Samples:92315782007, 92315782008
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 10/19/16 10:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1847826LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1847827MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92316027001
1847828
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 95 75-125239 782.50.47 2.8 6.4
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
332926
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92315782002, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007, 92315782008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1845029
Associated Lab Samples:92315782002, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007, 92315782008
Matrix:Water
Analyzed
Iron ug/L ND 50.0 10/18/16 16:06
Manganese ug/L ND 5.0 10/18/16 16:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1845030LABORATORY CONTROL SAMPLE:
LCSSpike
Iron ug/L 49505000 99 80-120
Manganese ug/L 507500 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1845031MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315771001
1845032
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Iron ug/L 5000 100 75-12599 1500068.4J 5060 5010
Manganese ug/L 500 101 75-125100 1500ND509504
REPORT OF LABORATORY ANALYSIS
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Page 15 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333148
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92315782001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1846092
Associated Lab Samples:92315782001
Matrix:Water
Analyzed
Iron ug/L ND 50.0 10/20/16 20:15
Manganese ug/L ND 5.0 10/20/16 20:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1846093LABORATORY CONTROL SAMPLE:
LCSSpike
Iron ug/L 48305000 97 80-120
Manganese ug/L 499500 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1846094MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315782001
1846095
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Iron ug/L 5000 97 75-12599 15000116060306100
Manganese ug/L 500 100 75-125100 150014.8 512 516
REPORT OF LABORATORY ANALYSIS
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Page 16 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333499
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007,
92315782008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1848139
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007,
92315782008
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 10/18/16 14:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1848140LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4960050000 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1848141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92316191002
1848142
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 96 80-12099 25000049.7
mg/L 97500 99400
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1848143MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315782008
1848144
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 96 80-12097 050000140000188000188000
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333077
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92315782001, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007, 92315782008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1845870
Associated Lab Samples:92315782001, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007, 92315782008
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 10/13/16 17:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1845871LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 250000250000 100 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92315615003
1845872SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 1060000 41100 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92315782005
1845873SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 186000 D67174000
REPORT OF LABORATORY ANALYSIS
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Page 18 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333349
SM 2540C
SM 2540C
2540C Total Dissolved Solids
Associated Lab Samples:92315782002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1847340
Associated Lab Samples:92315782002
Matrix:Water
Analyzed
Total Dissolved Solids ug/L ND 25000 10/17/16 11:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1847341LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids ug/L 232000250000 93 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92316023001
1847342SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 94000 391.0 mg/L
Parameter Units
Dup
Result QualifiersRPDResult
92315887002
1847343SAMPLE DUPLICATE:
Total Dissolved Solids ug/L 215000 5204 mg/L
REPORT OF LABORATORY ANALYSIS
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Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333243
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007,
92315782008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1846773
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005, 92315782006, 92315782007,
92315782008
Matrix:Water
Analyzed
Sulfate ug/L ND 2000 10/15/16 13:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1846774LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 1990020000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1846775MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315263001
1846776
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L M1200009690-11089 22000056.4
mg/L 75600 74300
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1846777MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315855001
1846778
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate ug/L 20000 91 90-11090 1200002.3
mg/L 20400 20300
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333555
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1848368
Associated Lab Samples:92315782001, 92315782002, 92315782003, 92315782004, 92315782005
Matrix:Water
Analyzed
Chloride ug/L ND 1000 10/24/16 12:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1848369LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2100020000 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1848370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92316183002
1848371
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L M1100008490-11082 01000023.0
mg/L 31400 31300
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1848372MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92316048001
1848373
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 105 90-110104 1100001.2
mg/L 11700 11600
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
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Page 21 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333556
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92315782006, 92315782007, 92315782008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1848374
Associated Lab Samples:92315782006, 92315782007, 92315782008
Matrix:Water
Analyzed
Chloride ug/L ND 1000 10/24/16 13:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1848375LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2110020000 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1848376MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315782006
1848377
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 106 90-110108 21000023701290013100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1848378MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92316026001
1848379
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride ug/L 10000 110 90-110110 0100002.9
mg/L 13900 13900
REPORT OF LABORATORY ANALYSIS
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Page 22 of 27
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 23 of 27
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92315782001 333148 3332971107-MW1 EPA 3010A EPA 6010
92315782002 332926 3331381107-MW1D EPA 3010A EPA 6010
92315782003 332926 3331381107-MW12 EPA 3010A EPA 6010
92315782004 332926 3331381107-MW12D EPA 3010A EPA 6010
92315782005 332926 3331381107-MW14 EPA 3010A EPA 6010
92315782006 332926 3331381107-MW14D EPA 3010A EPA 6010
92315782007 332926 3331381107-MW15S EPA 3010A EPA 6010
92315782008 332926 3331381107-MW15D EPA 3010A EPA 6010
92315782001 333122 3333081107-MW1 EPA 7470 EPA 7470
92315782002 333122 3333081107-MW1D EPA 7470 EPA 7470
92315782003 333122 3333081107-MW12 EPA 7470 EPA 7470
92315782004 333122 3333081107-MW12D EPA 7470 EPA 7470
92315782005 333122 3333081107-MW14 EPA 7470 EPA 7470
92315782006 333122 3333081107-MW14D EPA 7470 EPA 7470
92315782007 333431 3334901107-MW15S EPA 7470 EPA 7470
92315782008 333431 3334901107-MW15D EPA 7470 EPA 7470
92315782001 3334991107-MW1 SM 2320B
92315782002 3334991107-MW1D SM 2320B
92315782003 3334991107-MW12 SM 2320B
92315782004 3334991107-MW12D SM 2320B
92315782005 3334991107-MW14 SM 2320B
92315782006 3334991107-MW14D SM 2320B
92315782007 3334991107-MW15S SM 2320B
92315782008 3334991107-MW15D SM 2320B
92315782001 3330771107-MW1 SM 2540C
92315782002 3333491107-MW1D SM 2540C
92315782003 3330771107-MW12 SM 2540C
92315782004 3330771107-MW12D SM 2540C
92315782005 3330771107-MW14 SM 2540C
92315782006 3330771107-MW14D SM 2540C
92315782007 3330771107-MW15S SM 2540C
92315782008 3330771107-MW15D SM 2540C
92315782001 3332431107-MW1 EPA 300.0
92315782002 3332431107-MW1D EPA 300.0
92315782003 3332431107-MW12 EPA 300.0
92315782004 3332431107-MW12D EPA 300.0
92315782005 3332431107-MW14 EPA 300.0
92315782006 3332431107-MW14D EPA 300.0
92315782007 3332431107-MW15S EPA 300.0
92315782008 3332431107-MW15D EPA 300.0
92315782001 3335551107-MW1 SM 4500-Cl-E
92315782002 3335551107-MW1D SM 4500-Cl-E
92315782003 3335551107-MW12 SM 4500-Cl-E
92315782004 3335551107-MW12D SM 4500-Cl-E
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92315782
BUNCOMBE NEW LF C&D Wells
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92315782005 3335551107-MW14 SM 4500-Cl-E
92315782006 3335561107-MW14D SM 4500-Cl-E
92315782007 3335561107-MW15S SM 4500-Cl-E
92315782008 3335561107-MW15D SM 4500-Cl-E
REPORT OF LABORATORY ANALYSIS
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Page 26 of 27
Page 27 of 27
#=CL#
October 17, 2016
LIMS USE: FR - ED HILTON
LIMS OBJECT ID: 92315333
92315333
Project:
Pace Project No.:
RE:
Mr. Ed Hilton
SCS Engineers
4041 Park Oaks Blvd.
Suite 100
Tampa, FL 33610
BUNCOMBE NEW LF LDS
Dear Mr. Hilton:
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92315333001 1107-LD1 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315333002 1107-LD2 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315333003 1107-LD3 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315333004 1107-LD4 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315333005 1107-LD5 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315333006 1107-LD6 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315333007 1107-Leachate LD EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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Page 3 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD1 Lab ID:92315333001 Collected:10/07/16 10:30 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 10:301
Field pH 5.9 Std. Units 10/07/16 10:300.10 1
Field Temperature 17.9 deg C 10/07/16 10:300.50 1
Field Specific Conductance 527 umhos/cm 10/07/16 10:301.0 1
Oxygen, Dissolved 0.81 mg/L 10/07/16 10:30 7782-44-71
REDOX 53.2 mV 10/07/16 10:301
Turbidity 0.83 NTU 10/07/16 10:301.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 06:50 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 06:50 7440-38-210/13/16 01:3010.0 1
Barium 72.3 ug/L 10/16/16 06:50 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 06:50 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 06:50 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 06:50 7440-47-310/13/16 01:305.0 1
Cobalt 255 ug/L 10/16/16 06:50 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 06:50 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 06:50 7439-92-110/13/16 01:305.0 1
Nickel 59.5 ug/L 10/16/16 06:50 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 06:50 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 06:50 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 06:50 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 06:50 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/16/16 06:50 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/12/16 22:42 67-64-125.0 1
Acrylonitrile ND ug/L 10/12/16 22:42 107-13-110.0 1
Benzene ND ug/L 10/12/16 22:42 71-43-21.0 1
Bromochloromethane ND ug/L 10/12/16 22:42 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/16 22:42 75-27-41.0 1
Bromoform ND ug/L 10/12/16 22:42 75-25-21.0 1
Bromomethane ND ug/L 10/12/16 22:42 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/16 22:42 78-93-35.0 1
Carbon disulfide ND ug/L 10/12/16 22:42 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/12/16 22:42 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/16 22:42 108-90-71.0 1
Chloroethane ND ug/L 10/12/16 22:42 75-00-31.0 1
Chloroform ND ug/L 10/12/16 22:42 67-66-31.0 1
Chloromethane ND ug/L 10/12/16 22:42 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/16 22:42 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/16 22:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/16 22:42 106-93-41.0 1
Dibromomethane ND ug/L 10/12/16 22:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/16 22:42 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/16 22:42 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD1 Lab ID:92315333001 Collected:10/07/16 10:30 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/12/16 22:42 110-57-61.0 1
1,1-Dichloroethane 2.3 ug/L 10/12/16 22:42 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/16 22:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/16 22:42 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/16 22:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/16 22:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/16 22:42 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/16 22:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/16 22:42 10061-02-61.0 1
Ethylbenzene ND ug/L 10/12/16 22:42 100-41-41.0 1
2-Hexanone ND ug/L 10/12/16 22:42 591-78-65.0 1
Iodomethane ND ug/L 10/12/16 22:42 74-88-45.0 1
Methylene Chloride ND ug/L 10/12/16 22:42 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/16 22:42 108-10-15.0 1
Styrene ND ug/L 10/12/16 22:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/16 22:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/16 22:42 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/16 22:42 127-18-41.0 1
Toluene ND ug/L 10/12/16 22:42 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/12/16 22:42 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/16 22:42 79-00-51.0 1
Trichloroethene ND ug/L 10/12/16 22:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/16 22:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/16 22:42 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/16 22:42 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/16 22:42 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/16 22:42 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/16 22:42 179601-23-12.0 1
o-Xylene ND ug/L 10/12/16 22:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/16 22:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/12/16 22:42 17060-07-070-130 1
Toluene-d8 (S)100 %10/12/16 22:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD2 Lab ID:92315333002 Collected:10/07/16 11:40 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 11:401
Field pH 6.1 Std. Units 10/07/16 11:400.10 1
Field Temperature 17.1 deg C 10/07/16 11:400.50 1
Field Specific Conductance 382 umhos/cm 10/07/16 11:401.0 1
Oxygen, Dissolved 4.50 mg/L 10/07/16 11:40 7782-44-71
REDOX -16.5 mV 10/07/16 11:401
Turbidity 10.14 NTU 10/07/16 11:401.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 06:53 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 06:53 7440-38-210/13/16 01:3010.0 1
Barium 155 ug/L 10/16/16 06:53 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 06:53 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 06:53 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 06:53 7440-47-310/13/16 01:305.0 1
Cobalt 27.8 ug/L 10/16/16 06:53 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 06:53 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 06:53 7439-92-110/13/16 01:305.0 1
Nickel 7.3 ug/L 10/16/16 06:53 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 06:53 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 06:53 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 06:53 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 06:53 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/16/16 06:53 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/12/16 22:59 67-64-125.0 1
Acrylonitrile ND ug/L 10/12/16 22:59 107-13-110.0 1
Benzene ND ug/L 10/12/16 22:59 71-43-21.0 1
Bromochloromethane ND ug/L 10/12/16 22:59 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/16 22:59 75-27-41.0 1
Bromoform ND ug/L 10/12/16 22:59 75-25-21.0 1
Bromomethane ND ug/L 10/12/16 22:59 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/16 22:59 78-93-35.0 1
Carbon disulfide ND ug/L 10/12/16 22:59 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/12/16 22:59 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/16 22:59 108-90-71.0 1
Chloroethane ND ug/L 10/12/16 22:59 75-00-31.0 1
Chloroform ND ug/L 10/12/16 22:59 67-66-31.0 1
Chloromethane ND ug/L 10/12/16 22:59 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/16 22:59 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/16 22:59 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/16 22:59 106-93-41.0 1
Dibromomethane ND ug/L 10/12/16 22:59 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/16 22:59 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/16 22:59 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD2 Lab ID:92315333002 Collected:10/07/16 11:40 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/12/16 22:59 110-57-61.0 1
1,1-Dichloroethane 2.8 ug/L 10/12/16 22:59 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/16 22:59 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/16 22:59 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/16 22:59 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/16 22:59 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/16 22:59 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/16 22:59 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/16 22:59 10061-02-61.0 1
Ethylbenzene ND ug/L 10/12/16 22:59 100-41-41.0 1
2-Hexanone ND ug/L 10/12/16 22:59 591-78-65.0 1
Iodomethane ND ug/L 10/12/16 22:59 74-88-45.0 1
Methylene Chloride ND ug/L 10/12/16 22:59 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/16 22:59 108-10-15.0 1
Styrene ND ug/L 10/12/16 22:59 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/16 22:59 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/16 22:59 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/16 22:59 127-18-41.0 1
Toluene ND ug/L 10/12/16 22:59 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/12/16 22:59 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/16 22:59 79-00-51.0 1
Trichloroethene ND ug/L 10/12/16 22:59 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/16 22:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/16 22:59 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/16 22:59 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/16 22:59 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/16 22:59 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/16 22:59 179601-23-12.0 1
o-Xylene ND ug/L 10/12/16 22:59 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %10/12/16 22:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/12/16 22:59 17060-07-070-130 1
Toluene-d8 (S)102 %10/12/16 22:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD3 Lab ID:92315333003 Collected:10/07/16 13:00 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 06:131
Field pH 6.2 Std. Units 10/07/16 06:130.10 1
Field Temperature 16.7 deg C 10/07/16 06:130.50 1
Field Specific Conductance 528 umhos/cm 10/07/16 06:131.0 1
Oxygen, Dissolved 1.80 mg/L 10/07/16 06:13 7782-44-71
REDOX 3.5 mV 10/07/16 06:131
Turbidity 9.0 NTU 10/07/16 06:131.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 06:56 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 06:56 7440-38-210/13/16 01:3010.0 1
Barium 288 ug/L 10/16/16 06:56 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 06:56 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 06:56 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 06:56 7440-47-310/13/16 01:305.0 1
Cobalt 11.5 ug/L 10/16/16 06:56 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 06:56 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 06:56 7439-92-110/13/16 01:305.0 1
Nickel 8.3 ug/L 10/16/16 06:56 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 06:56 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 06:56 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 06:56 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 06:56 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/16/16 06:56 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/12/16 23:16 67-64-125.0 1
Acrylonitrile ND ug/L 10/12/16 23:16 107-13-110.0 1
Benzene 1.7 ug/L 10/12/16 23:16 71-43-21.0 1
Bromochloromethane ND ug/L 10/12/16 23:16 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/16 23:16 75-27-41.0 1
Bromoform ND ug/L 10/12/16 23:16 75-25-21.0 1
Bromomethane ND ug/L 10/12/16 23:16 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/16 23:16 78-93-35.0 1
Carbon disulfide ND ug/L 10/12/16 23:16 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/12/16 23:16 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/16 23:16 108-90-71.0 1
Chloroethane ND ug/L 10/12/16 23:16 75-00-31.0 1
Chloroform ND ug/L 10/12/16 23:16 67-66-31.0 1
Chloromethane ND ug/L 10/12/16 23:16 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/16 23:16 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/16 23:16 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/16 23:16 106-93-41.0 1
Dibromomethane ND ug/L 10/12/16 23:16 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/16 23:16 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/16 23:16 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD3 Lab ID:92315333003 Collected:10/07/16 13:00 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/12/16 23:16 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/12/16 23:16 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/16 23:16 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/16 23:16 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/16 23:16 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/16 23:16 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/16 23:16 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/16 23:16 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/16 23:16 10061-02-61.0 1
Ethylbenzene ND ug/L 10/12/16 23:16 100-41-41.0 1
2-Hexanone ND ug/L 10/12/16 23:16 591-78-65.0 1
Iodomethane ND ug/L 10/12/16 23:16 74-88-45.0 1
Methylene Chloride ND ug/L 10/12/16 23:16 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/16 23:16 108-10-15.0 1
Styrene ND ug/L 10/12/16 23:16 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/16 23:16 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/16 23:16 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/16 23:16 127-18-41.0 1
Toluene ND ug/L 10/12/16 23:16 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/12/16 23:16 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/16 23:16 79-00-51.0 1
Trichloroethene ND ug/L 10/12/16 23:16 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/16 23:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/16 23:16 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/16 23:16 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/16 23:16 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/16 23:16 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/16 23:16 179601-23-12.0 1
o-Xylene ND ug/L 10/12/16 23:16 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/12/16 23:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/12/16 23:16 17060-07-070-130 1
Toluene-d8 (S)99 %10/12/16 23:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD4 Lab ID:92315333004 Collected:10/07/16 13:10 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 13:101
Field pH 5.8 Std. Units 10/07/16 13:100.10 1
Field Temperature 17.4 deg C 10/07/16 13:100.50 1
Field Specific Conductance 207 umhos/cm 10/07/16 13:101.0 1
Oxygen, Dissolved 2.20 mg/L 10/07/16 13:10 7782-44-71
REDOX 57.8 mV 10/07/16 13:101
Turbidity 54.8 NTU 10/07/16 13:101.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 07:00 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 07:00 7440-38-210/13/16 01:3010.0 1
Barium 420 ug/L 10/16/16 07:00 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 07:00 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 07:00 7440-43-910/13/16 01:301.0 1
Chromium 199 ug/L 10/16/16 07:00 7440-47-310/13/16 01:305.0 1
Cobalt ND ug/L 10/16/16 07:00 7440-48-410/13/16 01:305.0 1
Copper 54.1 ug/L 10/16/16 07:00 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 07:00 7439-92-110/13/16 01:305.0 1
Nickel 60.2 ug/L 10/16/16 07:00 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 07:00 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 07:00 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 07:00 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 07:00 7440-62-210/13/16 01:305.0 1
Zinc 12.2 ug/L 10/16/16 07:00 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/12/16 23:33 67-64-125.0 1
Acrylonitrile ND ug/L 10/12/16 23:33 107-13-110.0 1
Benzene 3.0 ug/L 10/12/16 23:33 71-43-21.0 1
Bromochloromethane ND ug/L 10/12/16 23:33 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/16 23:33 75-27-41.0 1
Bromoform ND ug/L 10/12/16 23:33 75-25-21.0 1
Bromomethane ND ug/L 10/12/16 23:33 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/16 23:33 78-93-35.0 1
Carbon disulfide ND ug/L 10/12/16 23:33 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/12/16 23:33 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/16 23:33 108-90-71.0 1
Chloroethane ND ug/L 10/12/16 23:33 75-00-31.0 1
Chloroform ND ug/L 10/12/16 23:33 67-66-31.0 1
Chloromethane ND ug/L 10/12/16 23:33 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/16 23:33 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/16 23:33 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/16 23:33 106-93-41.0 1
Dibromomethane ND ug/L 10/12/16 23:33 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/16 23:33 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/16 23:33 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD4 Lab ID:92315333004 Collected:10/07/16 13:10 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/12/16 23:33 110-57-61.0 1
1,1-Dichloroethane 1.5 ug/L 10/12/16 23:33 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/16 23:33 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/16 23:33 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/16 23:33 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/16 23:33 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/16 23:33 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/16 23:33 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/16 23:33 10061-02-61.0 1
Ethylbenzene ND ug/L 10/12/16 23:33 100-41-41.0 1
2-Hexanone ND ug/L 10/12/16 23:33 591-78-65.0 1
Iodomethane ND ug/L 10/12/16 23:33 74-88-45.0 1
Methylene Chloride ND ug/L 10/12/16 23:33 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/16 23:33 108-10-15.0 1
Styrene ND ug/L 10/12/16 23:33 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/16 23:33 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/16 23:33 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/16 23:33 127-18-41.0 1
Toluene 1.2 ug/L 10/12/16 23:33 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/12/16 23:33 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/16 23:33 79-00-51.0 1
Trichloroethene ND ug/L 10/12/16 23:33 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/16 23:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/16 23:33 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/16 23:33 108-05-42.0 1
Vinyl chloride 1.2 ug/L 10/12/16 23:33 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/16 23:33 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/16 23:33 179601-23-12.0 1
o-Xylene ND ug/L 10/12/16 23:33 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %10/12/16 23:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/12/16 23:33 17060-07-070-130 1
Toluene-d8 (S)101 %10/12/16 23:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD5 Lab ID:92315333005 Collected:10/07/16 12:35 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 12:351
Field pH 6.4 Std. Units 10/07/16 12:350.10 1
Field Temperature 20.1 deg C 10/07/16 12:350.50 1
Field Specific Conductance 751 umhos/cm 10/07/16 12:351.0 1
Oxygen, Dissolved 3.4 mg/L 10/07/16 12:35 7782-44-71
REDOX 201.1 mV 10/07/16 12:351
Turbidity 43.89 NTU 10/07/16 12:351.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 07:03 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 07:03 7440-38-210/13/16 01:3010.0 1
Barium 215 ug/L 10/16/16 07:03 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 07:03 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 07:03 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 07:03 7440-47-310/13/16 01:305.0 1
Cobalt 85.4 ug/L 10/16/16 07:03 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 07:03 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 07:03 7439-92-110/13/16 01:305.0 1
Nickel 26.0 ug/L 10/16/16 07:03 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 07:03 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 07:03 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 07:03 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 07:03 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/16/16 07:03 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/12/16 23:50 67-64-125.0 1
Acrylonitrile ND ug/L 10/12/16 23:50 107-13-110.0 1
Benzene ND ug/L 10/12/16 23:50 71-43-21.0 1
Bromochloromethane ND ug/L 10/12/16 23:50 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/16 23:50 75-27-41.0 1
Bromoform ND ug/L 10/12/16 23:50 75-25-21.0 1
Bromomethane ND ug/L 10/12/16 23:50 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/16 23:50 78-93-35.0 1
Carbon disulfide ND ug/L 10/12/16 23:50 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/12/16 23:50 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/16 23:50 108-90-71.0 1
Chloroethane ND ug/L 10/12/16 23:50 75-00-31.0 1
Chloroform ND ug/L 10/12/16 23:50 67-66-31.0 1
Chloromethane ND ug/L 10/12/16 23:50 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/16 23:50 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/16 23:50 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/16 23:50 106-93-41.0 1
Dibromomethane ND ug/L 10/12/16 23:50 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/16 23:50 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/16 23:50 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD5 Lab ID:92315333005 Collected:10/07/16 12:35 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/12/16 23:50 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/12/16 23:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/16 23:50 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/16 23:50 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/16 23:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/16 23:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/16 23:50 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/16 23:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/16 23:50 10061-02-61.0 1
Ethylbenzene ND ug/L 10/12/16 23:50 100-41-41.0 1
2-Hexanone ND ug/L 10/12/16 23:50 591-78-65.0 1
Iodomethane ND ug/L 10/12/16 23:50 74-88-45.0 1
Methylene Chloride ND ug/L 10/12/16 23:50 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/16 23:50 108-10-15.0 1
Styrene ND ug/L 10/12/16 23:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/16 23:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/16 23:50 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/16 23:50 127-18-41.0 1
Toluene ND ug/L 10/12/16 23:50 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/12/16 23:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/16 23:50 79-00-51.0 1
Trichloroethene ND ug/L 10/12/16 23:50 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/16 23:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/16 23:50 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/16 23:50 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/16 23:50 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/16 23:50 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/16 23:50 179601-23-12.0 1
o-Xylene ND ug/L 10/12/16 23:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/16 23:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/12/16 23:50 17060-07-070-130 1
Toluene-d8 (S)102 %10/12/16 23:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD6 Lab ID:92315333006 Collected:10/07/16 13:20 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 12:201
Field pH 6.4 Std. Units 10/07/16 12:200.10 1
Field Temperature 18.5 deg C 10/07/16 12:200.50 1
Field Specific Conductance 551 umhos/cm 10/07/16 12:201.0 1
Oxygen, Dissolved 1.5 mg/L 10/07/16 12:20 7782-44-71
REDOX 10.9 mV 10/07/16 12:201
Turbidity 1.6 NTU 10/07/16 12:201.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 07:06 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 07:06 7440-38-210/13/16 01:3010.0 1
Barium 456 ug/L 10/16/16 07:06 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 07:06 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 07:06 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 07:06 7440-47-310/13/16 01:305.0 1
Cobalt 62.9 ug/L 10/16/16 07:06 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 07:06 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 07:06 7439-92-110/13/16 01:305.0 1
Nickel ND ug/L 10/16/16 07:06 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 07:06 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 07:06 7440-22-410/13/16 01:305.0 1
Thallium 5.6 ug/L 10/16/16 07:06 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 07:06 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/16/16 07:06 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 00:07 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 00:07 107-13-110.0 1
Benzene ND ug/L 10/13/16 00:07 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 00:07 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 00:07 75-27-41.0 1
Bromoform ND ug/L 10/13/16 00:07 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 00:07 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 00:07 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 00:07 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 00:07 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 00:07 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 00:07 75-00-31.0 1
Chloroform ND ug/L 10/13/16 00:07 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 00:07 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 00:07 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 00:07 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 00:07 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 00:07 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 00:07 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 00:07 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-LD6 Lab ID:92315333006 Collected:10/07/16 13:20 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 00:07 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 00:07 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 00:07 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 00:07 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 00:07 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 00:07 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 00:07 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 00:07 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 00:07 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 00:07 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 00:07 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 00:07 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 00:07 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 00:07 108-10-15.0 1
Styrene ND ug/L 10/13/16 00:07 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 00:07 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 00:07 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 00:07 127-18-41.0 1
Toluene ND ug/L 10/13/16 00:07 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 00:07 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 00:07 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 00:07 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 00:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 00:07 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 00:07 108-05-42.0 1
Vinyl chloride ND ug/L 10/13/16 00:07 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 00:07 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 00:07 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 00:07 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/13/16 00:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/13/16 00:07 17060-07-070-130 1
Toluene-d8 (S)102 %10/13/16 00:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-Leachate LD Lab ID:92315333007 Collected:10/07/16 12:00 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By M. Swann 10/07/16 12:001
Field pH 4.6 Std. Units 10/07/16 12:000.10 1
Field Temperature 17.0 deg C 10/07/16 12:000.50 1
Field Specific Conductance 734 umhos/cm 10/07/16 12:001.0 1
Oxygen, Dissolved 5.33 mg/L 10/07/16 12:00 7782-44-71
REDOX 347.4 mV 10/07/16 12:001
Turbidity 3.8 NTU 10/07/16 12:001.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 07:09 7440-36-010/13/16 01:305.0 1
Arsenic 26.1 ug/L 10/16/16 07:09 7440-38-210/13/16 01:3010.0 1
Barium 16.8 ug/L 10/16/16 07:09 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 07:09 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 07:09 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 07:09 7440-47-310/13/16 01:305.0 1
Cobalt 117 ug/L 10/16/16 07:09 7440-48-410/13/16 01:305.0 1
Copper 36.6 ug/L 10/16/16 07:09 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 07:09 7439-92-110/13/16 01:305.0 1
Nickel 691 ug/L 10/16/16 07:09 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 07:09 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 07:09 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 07:09 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 07:09 7440-62-210/13/16 01:305.0 1
Zinc 276 ug/L 10/16/16 07:09 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 00:24 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 00:24 107-13-110.0 1
Benzene ND ug/L 10/13/16 00:24 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 00:24 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 00:24 75-27-41.0 1
Bromoform ND ug/L 10/13/16 00:24 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 00:24 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 00:24 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 00:24 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 00:24 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 00:24 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 00:24 75-00-31.0 1
Chloroform ND ug/L 10/13/16 00:24 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 00:24 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 00:24 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 00:24 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 00:24 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 00:24 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 00:24 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 00:24 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
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Page 16 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Sample:1107-Leachate LD Lab ID:92315333007 Collected:10/07/16 12:00 Received:10/07/16 14:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 00:24 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 00:24 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 00:24 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 00:24 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 00:24 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 00:24 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 00:24 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 00:24 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 00:24 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 00:24 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 00:24 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 00:24 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 00:24 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 00:24 108-10-15.0 1
Styrene ND ug/L 10/13/16 00:24 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 00:24 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 00:24 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 00:24 127-18-41.0 1
Toluene ND ug/L 10/13/16 00:24 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 00:24 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 00:24 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 00:24 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 00:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 00:24 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 00:24 108-05-42.0 1
Vinyl chloride ND ug/L 10/13/16 00:24 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 00:24 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 00:24 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 00:24 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %10/13/16 00:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/13/16 00:24 17060-07-070-130 1
Toluene-d8 (S)101 %10/13/16 00:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
332783
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92315333001, 92315333002, 92315333003, 92315333004, 92315333005, 92315333006, 92315333007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1844063
Associated Lab Samples:92315333001, 92315333002, 92315333003, 92315333004, 92315333005, 92315333006, 92315333007
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 10/16/16 05:49
Arsenic ug/L ND 10.0 10/16/16 05:49
Barium ug/L ND 5.0 10/16/16 05:49
Beryllium ug/L ND 1.0 10/16/16 05:49
Cadmium ug/L ND 1.0 10/16/16 05:49
Chromium ug/L ND 5.0 10/16/16 05:49
Cobalt ug/L ND 5.0 10/16/16 05:49
Copper ug/L ND 5.0 10/16/16 05:49
Lead ug/L ND 5.0 10/16/16 05:49
Nickel ug/L ND 5.0 10/16/16 05:49
Selenium ug/L ND 10.0 10/16/16 05:49
Silver ug/L ND 5.0 10/16/16 05:49
Thallium ug/L ND 5.4 10/16/16 05:49
Vanadium ug/L ND 5.0 10/16/16 05:49
Zinc ug/L ND 10.0 10/16/16 05:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1844064LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 476500 95 80-120
Arsenic ug/L 467500 93 80-120
Barium ug/L 505500 101 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 487500 97 80-120
Chromium ug/L 503500 101 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 499500 100 80-120
Lead ug/L 482500 96 80-120
Nickel ug/L 483500 97 80-120
Selenium ug/L 481500 96 80-120
Silver ug/L 248250 99 80-120
Thallium ug/L 473500 95 80-120
Vanadium ug/L 492500 98 80-120
Zinc ug/L 498500 100 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1844065MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92314876001
1844066
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 93 75-12596 3500ND467480
Arsenic ug/L 500 92 75-12595 3500ND460476
Barium ug/L 500 100 75-125102 250019.9J 521 532
Beryllium ug/L 500 99 75-125100 2500ND494502
Cadmium ug/L 500 96 75-12599 2500ND482493
Chromium ug/L 500 100 75-125102 25002.9J 501 513
Cobalt ug/L 500 96 75-12599 3500ND484496
Copper ug/L 500 100 75-125102 2500ND500513
Lead ug/L 500 94 75-12597 3500ND471484
Nickel ug/L 500 95 75-12597 25002.9J 477 489
Selenium ug/L 500 94 75-12597 3500ND473488
Silver ug/L 250 98 75-125100 2250ND244250
Thallium ug/L 500 92 75-12596 4500ND462481
Vanadium ug/L 500 97 75-125100 25006.8J 494 506
Zinc ug/L 500 97 75-125100 35005.2J 492 504
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
332894
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92315333001, 92315333002, 92315333003, 92315333004, 92315333005, 92315333006, 92315333007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1844806
Associated Lab Samples:92315333001, 92315333002, 92315333003, 92315333004, 92315333005, 92315333006, 92315333007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/16 18:46
1,1,1-Trichloroethane ug/L ND 1.0 10/12/16 18:46
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/12/16 18:46
1,1,2-Trichloroethane ug/L ND 1.0 10/12/16 18:46
1,1-Dichloroethane ug/L ND 1.0 10/12/16 18:46
1,1-Dichloroethene ug/L ND 1.0 10/12/16 18:46
1,2,3-Trichloropropane ug/L ND 1.0 10/12/16 18:46
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/12/16 18:46
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/12/16 18:46
1,2-Dichlorobenzene ug/L ND 1.0 10/12/16 18:46
1,2-Dichloroethane ug/L ND 1.0 10/12/16 18:46
1,2-Dichloropropane ug/L ND 1.0 10/12/16 18:46
1,4-Dichlorobenzene ug/L ND 1.0 10/12/16 18:46
2-Butanone (MEK)ug/L ND 5.0 10/12/16 18:46
2-Hexanone ug/L ND 5.0 10/12/16 18:46
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/12/16 18:46
Acetone ug/L ND 25.0 10/12/16 18:46
Acrylonitrile ug/L ND 10.0 10/12/16 18:46
Benzene ug/L ND 1.0 10/12/16 18:46
Bromochloromethane ug/L ND 1.0 10/12/16 18:46
Bromodichloromethane ug/L ND 1.0 10/12/16 18:46
Bromoform ug/L ND 1.0 10/12/16 18:46
Bromomethane ug/L ND 2.0 10/12/16 18:46
Carbon disulfide ug/L ND 2.0 10/12/16 18:46
Carbon tetrachloride ug/L ND 1.0 10/12/16 18:46
Chlorobenzene ug/L ND 1.0 10/12/16 18:46
Chloroethane ug/L ND 1.0 10/12/16 18:46
Chloroform ug/L ND 1.0 10/12/16 18:46
Chloromethane ug/L ND 1.0 10/12/16 18:46
cis-1,2-Dichloroethene ug/L ND 1.0 10/12/16 18:46
cis-1,3-Dichloropropene ug/L ND 1.0 10/12/16 18:46
Dibromochloromethane ug/L ND 1.0 10/12/16 18:46
Dibromomethane ug/L ND 1.0 10/12/16 18:46
Ethylbenzene ug/L ND 1.0 10/12/16 18:46
Iodomethane ug/L ND 5.0 10/12/16 18:46
m&p-Xylene ug/L ND 2.0 10/12/16 18:46
Methylene Chloride ug/L ND 1.0 10/12/16 18:46
o-Xylene ug/L ND 1.0 10/12/16 18:46
Styrene ug/L ND 1.0 10/12/16 18:46
Tetrachloroethene ug/L ND 1.0 10/12/16 18:46
Toluene ug/L ND 1.0 10/12/16 18:46
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1844806
Associated Lab Samples:92315333001, 92315333002, 92315333003, 92315333004, 92315333005, 92315333006, 92315333007
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 10/12/16 18:46
trans-1,3-Dichloropropene ug/L ND 1.0 10/12/16 18:46
trans-1,4-Dichloro-2-butene ug/L ND 1.0 10/12/16 18:46
Trichloroethene ug/L ND 1.0 10/12/16 18:46
Trichlorofluoromethane ug/L ND 1.0 10/12/16 18:46
Vinyl acetate ug/L ND 2.0 10/12/16 18:46
Vinyl chloride ug/L ND 1.0 10/12/16 18:46
Xylene (Total)ug/L ND 1.0 10/12/16 18:46
1,2-Dichloroethane-d4 (S)%99 70-130 10/12/16 18:46
4-Bromofluorobenzene (S)%97 70-130 10/12/16 18:46
Toluene-d8 (S)%102 70-130 10/12/16 18:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1844807LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 80-125
1,1,1-Trichloroethane ug/L 50.950 102 71-129
1,1,2,2-Tetrachloroethane ug/L 47.650 95 79-124
1,1,2-Trichloroethane ug/L 45.950 92 85-125
1,1-Dichloroethane ug/L 48.550 97 73-126
1,1-Dichloroethene ug/L 51.950 104 66-135
1,2,3-Trichloropropane ug/L 46.550 93 75-130
1,2-Dibromo-3-chloropropane ug/L 51.050 102 71-133
1,2-Dibromoethane (EDB)ug/L 50.750 101 83-124
1,2-Dichlorobenzene ug/L 51.950 104 80-133
1,2-Dichloroethane ug/L 47.450 95 67-128
1,2-Dichloropropane ug/L 45.750 91 75-132
1,4-Dichlorobenzene ug/L 48.950 98 78-130
2-Butanone (MEK)ug/L 95.9100 96 61-144
2-Hexanone ug/L 98.3100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 95.4100 95 72-135
Acetone ug/L 95.9100 96 48-146
Acrylonitrile ug/L 236250 95 40-160
Benzene ug/L 48.550 97 80-125
Bromochloromethane ug/L 48.450 97 71-125
Bromodichloromethane ug/L 49.750 99 78-124
Bromoform ug/L 48.350 97 71-128
Bromomethane ug/L 52.850 106 40-160
Carbon disulfide ug/L 48.750 97 50-160
Carbon tetrachloride ug/L 52.550 105 69-131
Chlorobenzene ug/L 49.750 99 81-122
Chloroethane ug/L 42.050 84 39-148
Chloroform ug/L 48.550 97 73-127
Chloromethane ug/L 47.550 95 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1844807LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 49.550 99 74-124
cis-1,3-Dichloropropene ug/L 48.650 97 72-132
Dibromochloromethane ug/L 49.950 100 78-125
Dibromomethane ug/L 45.950 92 82-120
Ethylbenzene ug/L 50.050 100 79-121
Iodomethane ug/L 136100 136 39-154
m&p-Xylene ug/L 100100 100 81-124
Methylene Chloride ug/L 51.950 104 64-133
o-Xylene ug/L 48.450 97 79-131
Styrene ug/L 51.450 103 84-126
Tetrachloroethene ug/L 46.750 93 78-122
Toluene ug/L 49.550 99 80-121
trans-1,2-Dichloroethene ug/L 50.150 100 71-127
trans-1,3-Dichloropropene ug/L 46.850 94 69-141
trans-1,4-Dichloro-2-butene ug/L 44.450 89 40-160
Trichloroethene ug/L 48.050 96 78-122
Trichlorofluoromethane ug/L 50.350 101 53-137
Vinyl acetate ug/L 104100 104 40-160
Vinyl chloride ug/L 40.850 82 58-137
Xylene (Total)ug/L 149150 99 81-126
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1844808MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92314840006
1844809
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 101 70-130104 320ND20.2 20.7
1,1,1-Trichloroethane ug/L 20 109 70-130109 020ND21.8 21.9
1,1,2,2-Tetrachloroethane ug/L 20 97 70-13097 020ND19.5 19.5
1,1,2-Trichloroethane ug/L 20 99 70-13097 220ND19.8 19.4
1,1-Dichloroethane ug/L 20 104 70-130102 220ND20.7 20.4
1,1-Dichloroethene ug/L 20 116 70-166115 120ND23.2 22.9
1,2,3-Trichloropropane ug/L 20 97 70-13096 220ND19.5 19.1
1,2-Dibromo-3-chloropropane ug/L 20 101 70-130103 220ND20.1 20.6
1,2-Dibromoethane (EDB)ug/L 20 105 70-130105 020ND21.1 21.0
1,2-Dichlorobenzene ug/L 20 107 70-130109 220ND21.4 21.9
1,2-Dichloroethane ug/L 20 99 70-13097 320ND20.0 19.5
1,2-Dichloropropane ug/L 20 99 70-13097 320ND19.9 19.4
1,4-Dichlorobenzene ug/L 20 100 70-130103 220ND20.1 20.5
2-Butanone (MEK)ug/L 40 97 70-13099 240ND38.9 39.6
2-Hexanone ug/L 40 96 70-13099 340ND38.6 39.7
4-Methyl-2-pentanone (MIBK)ug/L 40 102 70-130102 040ND40.8 40.9
Acetone ug/L 40 93 70-13093 040ND37.9 37.9
REPORT OF LABORATORY ANALYSIS
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Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1844808MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92314840006
1844809
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Acrylonitrile ug/L 100 99 70-13096 4100ND99.4 95.7
Benzene ug/L 20 106 70-148103 220ND21.1 20.7
Bromochloromethane ug/L 20 102 70-130100 220ND20.5 20.0
Bromodichloromethane ug/L 20 104 70-130103 120ND20.9 20.6
Bromoform ug/L 20 94 70-13093 120ND18.7 18.5
Bromomethane ug/L 20 87 70-13094 820ND17.4 18.8
Carbon disulfide ug/L 20 106 70-130103 320ND21.6 20.9
Carbon tetrachloride ug/L 20 117 70-130115 120ND23.3 23.0
Chlorobenzene ug/L 20 107 70-146107 120ND21.3 21.5
Chloroethane ug/L 20 103 70-13099 320ND20.6 19.9
Chloroform ug/L 20 103 70-130100 320ND20.5 19.9
Chloromethane ug/L 20 107 70-130102 520ND21.5 20.4
cis-1,2-Dichloroethene ug/L 20 107 70-130105 320ND21.5 20.9
cis-1,3-Dichloropropene ug/L 20 100 70-13097 320ND20.0 19.3
Dibromochloromethane ug/L 20 100 70-13099 120ND20.0 19.8
Dibromomethane ug/L 20 100 70-130101 120ND19.9 20.1
Ethylbenzene ug/L 20 107 70-130106 120ND21.4 21.2
Iodomethane ug/L M14013870-130155 1140ND55.4 61.8
m&p-Xylene ug/L 40 105 70-130105 040ND42.1 42.1
Methylene Chloride ug/L 20 109 70-130105 420ND21.9 20.9
o-Xylene ug/L 20 101 70-130100 120ND20.2 20.1
Styrene ug/L 20 107 70-130107 020ND21.4 21.3
Tetrachloroethene ug/L 20 100 70-130101 120ND20.0 20.2
Toluene ug/L 20 108 70-155107 120ND21.6 21.4
trans-1,2-Dichloroethene ug/L 20 110 70-130107 320ND22.1 21.5
trans-1,3-Dichloropropene ug/L 20 94 70-13093 120ND18.7 18.6
trans-1,4-Dichloro-2-butene ug/L 20 84 70-13083 120ND16.7 16.6
Trichloroethene ug/L 20 106 69-151102 320ND21.1 20.5
Trichlorofluoromethane ug/L 20 121 70-130116 420ND24.2 23.3
Vinyl acetate ug/L 40 89 70-13087 340ND35.7 34.7
Vinyl chloride ug/L 20 93 70-13091 220ND18.6 18.1
1,2-Dichloroethane-d4 (S)%97 70-13096
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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2225 Riverside Dr.
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Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92315333
BUNCOMBE NEW LF LDS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92315333001 1107-LD1
92315333002 1107-LD2
92315333003 1107-LD3
92315333004 1107-LD4
92315333005 1107-LD5
92315333006 1107-LD6
92315333007 1107-Leachate LD
92315333001 332783 3330521107-LD1 EPA 3010A EPA 6010
92315333002 332783 3330521107-LD2 EPA 3010A EPA 6010
92315333003 332783 3330521107-LD3 EPA 3010A EPA 6010
92315333004 332783 3330521107-LD4 EPA 3010A EPA 6010
92315333005 332783 3330521107-LD5 EPA 3010A EPA 6010
92315333006 332783 3330521107-LD6 EPA 3010A EPA 6010
92315333007 332783 3330521107-Leachate LD EPA 3010A EPA 6010
92315333001 3328941107-LD1 EPA 8260
92315333002 3328941107-LD2 EPA 8260
92315333003 3328941107-LD3 EPA 8260
92315333004 3328941107-LD4 EPA 8260
92315333005 3328941107-LD5 EPA 8260
92315333006 3328941107-LD6 EPA 8260
92315333007 3328941107-Leachate LD EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/17/2016 04:04 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 28
Page 26 of 28
Page 27 of 28
Page 28 of 28
#=CL#
October 18, 2016
LIMS USE: FR - ED HILTON
LIMS OBJECT ID: 92315343
92315343
Project:
Pace Project No.:
RE:
Mr. Ed Hilton
SCS Engineers
4041 Park Oaks Blvd.
Suite 100
Tampa, FL 33610
BUNCOMBE NEW LF SW's
Dear Mr. Hilton:
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92315343001 1107-SW2 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315343002 1107-SW4 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315343003 1107-SW5 EPA 6010 15 PASI-AJMW
EPA 8260 52 PASI-CCAH
92315343004 1107-SW6 EPA 6010 15 PASI-ASH1
EPA 8260 52 PASI-CCAH
92315343005 1107-Leachate Lagoon EPA 6010 15 PASI-ASH1
EPA 8260 52 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Asheville, NC 28804
[phone]
Page 3 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW2 Lab ID:92315343001 Collected:10/07/16 09:55 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Field Data
Collected By M. Swann 10/07/16 09:551
Field pH 7.8 Std. Units 10/07/16 09:550.10 1
Field Temperature 14.9 deg C 10/07/16 09:550.50 1
Field Specific Conductance 161 umhos/cm 10/07/16 09:551.0 1
Oxygen, Dissolved 9.65 mg/L 10/07/16 09:55 7782-44-71
REDOX 149.3 mV 10/07/16 09:551
Turbidity 6.80 NTU 10/07/16 09:551.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/17/16 12:49 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/17/16 12:49 7440-38-210/13/16 01:3010.0 1
Barium 52.2 ug/L 10/17/16 12:49 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/17/16 12:49 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/17/16 12:49 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/17/16 12:49 7440-47-310/13/16 01:305.0 1
Cobalt ND ug/L 10/17/16 12:49 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/17/16 12:49 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/17/16 12:49 7439-92-110/13/16 01:305.0 1
Nickel ND ug/L 10/17/16 12:49 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/17/16 12:49 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/17/16 12:49 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/17/16 12:49 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/17/16 12:49 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/17/16 12:49 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 16:39 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 16:39 107-13-110.0 1
Benzene ND ug/L 10/13/16 16:39 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 16:39 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 16:39 75-27-41.0 1
Bromoform ND ug/L 10/13/16 16:39 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 16:39 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 16:39 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 16:39 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 16:39 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 16:39 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 16:39 75-00-31.0 1
Chloroform ND ug/L 10/13/16 16:39 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 16:39 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 16:39 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 16:39 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 16:39 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 16:39 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 16:39 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 16:39 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW2 Lab ID:92315343001 Collected:10/07/16 09:55 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 16:39 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 16:39 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 16:39 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 16:39 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 16:39 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 16:39 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 16:39 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 16:39 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 16:39 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 16:39 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 16:39 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 16:39 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 16:39 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 16:39 108-10-15.0 1
Styrene ND ug/L 10/13/16 16:39 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 16:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 16:39 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 16:39 127-18-4 M11.0 1
Toluene ND ug/L 10/13/16 16:39 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 16:39 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 16:39 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 16:39 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 16:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 16:39 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 16:39 108-05-4 M12.0 1
Vinyl chloride ND ug/L 10/13/16 16:39 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 16:39 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 16:39 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 16:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %10/13/16 16:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/13/16 16:39 17060-07-070-130 1
Toluene-d8 (S)102 %10/13/16 16:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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Page 5 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW4 Lab ID:92315343002 Collected:10/07/16 12:20 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Field Data
Collected By M. Swann 10/07/16 12:201
Field pH 8.1 Std. Units 10/07/16 12:200.10 1
Field Temperature 16.6 deg C 10/07/16 12:200.50 1
Field Specific Conductance 366 umhos/cm 10/07/16 12:201.0 1
Oxygen, Dissolved 6.98 mg/L 10/07/16 12:20 7782-44-71
REDOX 149.2 mV 10/07/16 12:201
Turbidity 149.3 NTU 10/07/16 12:201.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 07:24 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 07:24 7440-38-210/13/16 01:3010.0 1
Barium 131 ug/L 10/16/16 07:24 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 07:24 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 07:24 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 07:24 7440-47-310/13/16 01:305.0 1
Cobalt ND ug/L 10/16/16 07:24 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 07:24 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 07:24 7439-92-110/13/16 01:305.0 1
Nickel ND ug/L 10/16/16 07:24 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 07:24 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 07:24 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 07:24 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 07:24 7440-62-210/13/16 01:305.0 1
Zinc 12.1 ug/L 10/16/16 07:24 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 16:56 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 16:56 107-13-110.0 1
Benzene ND ug/L 10/13/16 16:56 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 16:56 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 16:56 75-27-41.0 1
Bromoform ND ug/L 10/13/16 16:56 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 16:56 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 16:56 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 16:56 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 16:56 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 16:56 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 16:56 75-00-31.0 1
Chloroform ND ug/L 10/13/16 16:56 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 16:56 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 16:56 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 16:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 16:56 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 16:56 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 16:56 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 16:56 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW4 Lab ID:92315343002 Collected:10/07/16 12:20 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 16:56 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 16:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 16:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 16:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 16:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 16:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 16:56 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 16:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 16:56 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 16:56 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 16:56 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 16:56 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 16:56 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 16:56 108-10-15.0 1
Styrene ND ug/L 10/13/16 16:56 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 16:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 16:56 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 16:56 127-18-41.0 1
Toluene ND ug/L 10/13/16 16:56 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 16:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 16:56 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 16:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 16:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 16:56 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 16:56 108-05-42.0 1
Vinyl chloride ND ug/L 10/13/16 16:56 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 16:56 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 16:56 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 16:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/13/16 16:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/13/16 16:56 17060-07-070-130 1
Toluene-d8 (S)102 %10/13/16 16:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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Page 7 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW5 Lab ID:92315343003 Collected:10/07/16 10:55 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Field Data
Collected By M. Swann 10/07/16 10:551
Field pH 8.4 Std. Units 10/07/16 10:550.10 1
Field Temperature 16.9 deg C 10/07/16 10:550.50 1
Field Specific Conductance 160 umhos/cm 10/07/16 10:551.0 1
Oxygen, Dissolved 8.01 mg/L 10/07/16 10:55 7782-44-71
REDOX 21.7 mV 10/07/16 10:551
Turbidity 4.34 NTU 10/07/16 10:551.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/16/16 07:27 7440-36-010/13/16 01:305.0 1
Arsenic ND ug/L 10/16/16 07:27 7440-38-210/13/16 01:3010.0 1
Barium 60.6 ug/L 10/16/16 07:27 7440-39-310/13/16 01:305.0 1
Beryllium ND ug/L 10/16/16 07:27 7440-41-710/13/16 01:301.0 1
Cadmium ND ug/L 10/16/16 07:27 7440-43-910/13/16 01:301.0 1
Chromium ND ug/L 10/16/16 07:27 7440-47-310/13/16 01:305.0 1
Cobalt ND ug/L 10/16/16 07:27 7440-48-410/13/16 01:305.0 1
Copper ND ug/L 10/16/16 07:27 7440-50-810/13/16 01:305.0 1
Lead ND ug/L 10/16/16 07:27 7439-92-110/13/16 01:305.0 1
Nickel 15.5 ug/L 10/16/16 07:27 7440-02-010/13/16 01:305.0 1
Selenium ND ug/L 10/16/16 07:27 7782-49-210/13/16 01:3010.0 1
Silver ND ug/L 10/16/16 07:27 7440-22-410/13/16 01:305.0 1
Thallium ND ug/L 10/16/16 07:27 7440-28-010/13/16 01:305.4 1
Vanadium ND ug/L 10/16/16 07:27 7440-62-210/13/16 01:305.0 1
Zinc ND ug/L 10/16/16 07:27 7440-66-610/13/16 01:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 17:29 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 17:29 107-13-110.0 1
Benzene ND ug/L 10/13/16 17:29 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 17:29 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 17:29 75-27-41.0 1
Bromoform ND ug/L 10/13/16 17:29 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 17:29 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 17:29 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 17:29 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 17:29 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 17:29 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 17:29 75-00-31.0 1
Chloroform ND ug/L 10/13/16 17:29 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 17:29 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 17:29 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 17:29 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 17:29 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 17:29 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 17:29 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 17:29 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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Page 8 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW5 Lab ID:92315343003 Collected:10/07/16 10:55 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 17:29 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 17:29 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 17:29 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 17:29 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 17:29 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 17:29 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 17:29 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 17:29 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 17:29 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 17:29 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 17:29 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 17:29 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 17:29 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 17:29 108-10-15.0 1
Styrene ND ug/L 10/13/16 17:29 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 17:29 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 17:29 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 17:29 127-18-41.0 1
Toluene ND ug/L 10/13/16 17:29 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 17:29 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 17:29 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 17:29 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 17:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 17:29 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 17:29 108-05-42.0 1
Vinyl chloride ND ug/L 10/13/16 17:29 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 17:29 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 17:29 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 17:29 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %10/13/16 17:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/13/16 17:29 17060-07-070-130 1
Toluene-d8 (S)100 %10/13/16 17:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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Page 9 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW6 Lab ID:92315343004 Collected:10/07/16 11:20 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Field Data
Collected By M. Swann 10/07/16 11:201
Field pH 7.5 Std. Units 10/07/16 11:200.10 1
Field Temperature 17.7 deg C 10/07/16 11:200.50 1
Field Specific Conductance 315 umhos/cm 10/07/16 11:201.0 1
Oxygen, Dissolved 4.90 mg/L 10/07/16 11:20 7782-44-71
REDOX 104.5 mV 10/07/16 11:201
Turbidity 95.65 NTU 10/07/16 11:201.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/17/16 20:41 7440-36-010/13/16 20:305.0 1
Arsenic ND ug/L 10/17/16 20:41 7440-38-210/13/16 20:3010.0 1
Barium 155 ug/L 10/17/16 20:41 7440-39-310/13/16 20:305.0 1
Beryllium ND ug/L 10/17/16 20:41 7440-41-710/13/16 20:301.0 1
Cadmium ND ug/L 10/17/16 20:41 7440-43-910/13/16 20:301.0 1
Chromium 10.6 ug/L 10/17/16 20:41 7440-47-310/13/16 20:305.0 1
Cobalt 7.7 ug/L 10/17/16 20:41 7440-48-410/13/16 20:305.0 1
Copper 6.9 ug/L 10/17/16 20:41 7440-50-810/13/16 20:305.0 1
Lead ND ug/L 10/17/16 20:41 7439-92-110/13/16 20:305.0 1
Nickel 9.7 ug/L 10/17/16 20:41 7440-02-010/13/16 20:305.0 1
Selenium ND ug/L 10/17/16 20:41 7782-49-210/13/16 20:3010.0 1
Silver ND ug/L 10/17/16 20:41 7440-22-410/13/16 20:305.0 1
Thallium ND ug/L 10/17/16 20:41 7440-28-010/13/16 20:305.4 1
Vanadium 22.0 ug/L 10/17/16 20:41 7440-62-210/13/16 20:305.0 1
Zinc 25.2 ug/L 10/17/16 20:41 7440-66-610/13/16 20:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 17:46 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 17:46 107-13-110.0 1
Benzene ND ug/L 10/13/16 17:46 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 17:46 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 17:46 75-27-41.0 1
Bromoform ND ug/L 10/13/16 17:46 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 17:46 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 17:46 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 17:46 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 17:46 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 17:46 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 17:46 75-00-31.0 1
Chloroform ND ug/L 10/13/16 17:46 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 17:46 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 17:46 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 17:46 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 17:46 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 17:46 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 17:46 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 17:46 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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Page 10 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-SW6 Lab ID:92315343004 Collected:10/07/16 11:20 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 17:46 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 17:46 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 17:46 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 17:46 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 17:46 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 17:46 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 17:46 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 17:46 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 17:46 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 17:46 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 17:46 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 17:46 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 17:46 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 17:46 108-10-15.0 1
Styrene ND ug/L 10/13/16 17:46 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 17:46 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 17:46 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 17:46 127-18-41.0 1
Toluene ND ug/L 10/13/16 17:46 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 17:46 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 17:46 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 17:46 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 17:46 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 17:46 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 17:46 108-05-42.0 1
Vinyl chloride ND ug/L 10/13/16 17:46 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 17:46 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 17:46 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 17:46 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %10/13/16 17:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/13/16 17:46 17060-07-070-130 1
Toluene-d8 (S)102 %10/13/16 17:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-Leachate Lagoon Lab ID:92315343005 Collected:10/07/16 12:10 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Field Data
Collected By M. Swann 10/07/16 12:101
Field pH 8.4 Std. Units 10/07/16 12:100.10 1
Field Temperature 22.3 deg C 10/07/16 12:100.50 1
Field Specific Conductance 5305 umhos/cm 10/07/16 12:101.0 1
Oxygen, Dissolved 17.01 mg/L 10/07/16 12:10 7782-44-71
REDOX 168.3 mV 10/07/16 12:101
Turbidity 82.89 NTU 10/07/16 12:101.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 10.7 ug/L 10/17/16 20:59 7440-36-010/13/16 20:305.0 1
Arsenic 14.2 ug/L 10/17/16 20:59 7440-38-210/13/16 20:3010.0 1
Barium 240 ug/L 10/17/16 20:59 7440-39-310/13/16 20:305.0 1
Beryllium ND ug/L 10/17/16 20:59 7440-41-710/13/16 20:301.0 1
Cadmium ND ug/L 10/17/16 20:59 7440-43-910/13/16 20:301.0 1
Chromium 38.4 ug/L 10/17/16 20:59 7440-47-310/13/16 20:305.0 1
Cobalt 15.7 ug/L 10/17/16 20:59 7440-48-410/13/16 20:305.0 1
Copper ND ug/L 10/17/16 20:59 7440-50-810/13/16 20:305.0 1
Lead ND ug/L 10/17/16 20:59 7439-92-110/13/16 20:305.0 1
Nickel 81.6 ug/L 10/17/16 20:59 7440-02-010/13/16 20:305.0 1
Selenium ND ug/L 10/17/16 20:59 7782-49-210/13/16 20:3010.0 1
Silver ND ug/L 10/17/16 20:59 7440-22-410/13/16 20:305.0 1
Thallium ND ug/L 10/17/16 20:59 7440-28-010/13/16 20:305.4 1
Vanadium 23.5 ug/L 10/17/16 20:59 7440-62-210/13/16 20:305.0 1
Zinc 12.9 ug/L 10/17/16 20:59 7440-66-610/13/16 20:3010.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/13/16 18:03 67-64-125.0 1
Acrylonitrile ND ug/L 10/13/16 18:03 107-13-110.0 1
Benzene ND ug/L 10/13/16 18:03 71-43-21.0 1
Bromochloromethane ND ug/L 10/13/16 18:03 74-97-51.0 1
Bromodichloromethane ND ug/L 10/13/16 18:03 75-27-41.0 1
Bromoform ND ug/L 10/13/16 18:03 75-25-21.0 1
Bromomethane ND ug/L 10/13/16 18:03 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/13/16 18:03 78-93-35.0 1
Carbon disulfide ND ug/L 10/13/16 18:03 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/13/16 18:03 56-23-51.0 1
Chlorobenzene ND ug/L 10/13/16 18:03 108-90-71.0 1
Chloroethane ND ug/L 10/13/16 18:03 75-00-31.0 1
Chloroform ND ug/L 10/13/16 18:03 67-66-31.0 1
Chloromethane ND ug/L 10/13/16 18:03 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/13/16 18:03 96-12-82.0 1
Dibromochloromethane ND ug/L 10/13/16 18:03 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/13/16 18:03 106-93-41.0 1
Dibromomethane ND ug/L 10/13/16 18:03 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/13/16 18:03 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/13/16 18:03 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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[phone]
Page 12 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Sample:1107-Leachate Lagoon Lab ID:92315343005 Collected:10/07/16 12:10 Received:10/07/16 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 10/13/16 18:03 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/13/16 18:03 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/13/16 18:03 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/13/16 18:03 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/13/16 18:03 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/13/16 18:03 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/13/16 18:03 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/13/16 18:03 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/13/16 18:03 10061-02-61.0 1
Ethylbenzene ND ug/L 10/13/16 18:03 100-41-41.0 1
2-Hexanone ND ug/L 10/13/16 18:03 591-78-65.0 1
Iodomethane ND ug/L 10/13/16 18:03 74-88-45.0 1
Methylene Chloride ND ug/L 10/13/16 18:03 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/13/16 18:03 108-10-15.0 1
Styrene ND ug/L 10/13/16 18:03 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/13/16 18:03 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/13/16 18:03 79-34-51.0 1
Tetrachloroethene ND ug/L 10/13/16 18:03 127-18-41.0 1
Toluene ND ug/L 10/13/16 18:03 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/13/16 18:03 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/13/16 18:03 79-00-51.0 1
Trichloroethene ND ug/L 10/13/16 18:03 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/13/16 18:03 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/13/16 18:03 96-18-41.0 1
Vinyl acetate ND ug/L 10/13/16 18:03 108-05-42.0 1
Vinyl chloride ND ug/L 10/13/16 18:03 75-01-41.0 1
Xylene (Total)ND ug/L 10/13/16 18:03 1330-20-71.0 1
m&p-Xylene ND ug/L 10/13/16 18:03 179601-23-12.0 1
o-Xylene ND ug/L 10/13/16 18:03 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %10/13/16 18:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/13/16 18:03 17060-07-070-130 1
Toluene-d8 (S)101 %10/13/16 18:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
Page 13 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
332783
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92315343001, 92315343002, 92315343003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1844063
Associated Lab Samples:92315343001, 92315343002, 92315343003
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 10/16/16 05:49
Arsenic ug/L ND 10.0 10/16/16 05:49
Barium ug/L ND 5.0 10/16/16 05:49
Beryllium ug/L ND 1.0 10/16/16 05:49
Cadmium ug/L ND 1.0 10/16/16 05:49
Chromium ug/L ND 5.0 10/16/16 05:49
Cobalt ug/L ND 5.0 10/16/16 05:49
Copper ug/L ND 5.0 10/16/16 05:49
Lead ug/L ND 5.0 10/16/16 05:49
Nickel ug/L ND 5.0 10/16/16 05:49
Selenium ug/L ND 10.0 10/16/16 05:49
Silver ug/L ND 5.0 10/16/16 05:49
Thallium ug/L ND 5.4 10/16/16 05:49
Vanadium ug/L ND 5.0 10/16/16 05:49
Zinc ug/L ND 10.0 10/16/16 05:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1844064LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 476500 95 80-120
Arsenic ug/L 467500 93 80-120
Barium ug/L 505500 101 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 487500 97 80-120
Chromium ug/L 503500 101 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 499500 100 80-120
Lead ug/L 482500 96 80-120
Nickel ug/L 483500 97 80-120
Selenium ug/L 481500 96 80-120
Silver ug/L 248250 99 80-120
Thallium ug/L 473500 95 80-120
Vanadium ug/L 492500 98 80-120
Zinc ug/L 498500 100 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1844065MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92314876001
1844066
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 93 75-12596 3500ND467480
Arsenic ug/L 500 92 75-12595 3500ND460476
Barium ug/L 500 100 75-125102 250019.9J 521 532
Beryllium ug/L 500 99 75-125100 2500ND494502
Cadmium ug/L 500 96 75-12599 2500ND482493
Chromium ug/L 500 100 75-125102 25002.9J 501 513
Cobalt ug/L 500 96 75-12599 3500ND484496
Copper ug/L 500 100 75-125102 2500ND500513
Lead ug/L 500 94 75-12597 3500ND471484
Nickel ug/L 500 95 75-12597 25002.9J 477 489
Selenium ug/L 500 94 75-12597 3500ND473488
Silver ug/L 250 98 75-125100 2250ND244250
Thallium ug/L 500 92 75-12596 4500ND462481
Vanadium ug/L 500 97 75-125100 25006.8J 494 506
Zinc ug/L 500 97 75-125100 35005.2J 492 504
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
332925
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92315343004, 92315343005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1845025
Associated Lab Samples:92315343004, 92315343005
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 10/17/16 20:35
Arsenic ug/L ND 10.0 10/17/16 20:35
Barium ug/L ND 5.0 10/17/16 20:35
Beryllium ug/L ND 1.0 10/17/16 20:35
Cadmium ug/L ND 1.0 10/17/16 20:35
Chromium ug/L ND 5.0 10/17/16 20:35
Cobalt ug/L ND 5.0 10/17/16 20:35
Copper ug/L ND 5.0 10/17/16 20:35
Lead ug/L ND 5.0 10/17/16 20:35
Nickel ug/L ND 5.0 10/17/16 20:35
Selenium ug/L ND 10.0 10/17/16 20:35
Silver ug/L ND 5.0 10/17/16 20:35
Thallium ug/L ND 5.4 10/17/16 20:35
Vanadium ug/L ND 5.0 10/17/16 20:35
Zinc ug/L ND 10.0 10/17/16 20:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1845026LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 516500 103 80-120
Arsenic ug/L 495500 99 80-120
Barium ug/L 510500 102 80-120
Beryllium ug/L 518500 104 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 511500 102 80-120
Cobalt ug/L 513500 103 80-120
Copper ug/L 524500 105 80-120
Lead ug/L 504500 101 80-120
Nickel ug/L 498500 100 80-120
Selenium ug/L 520500 104 80-120
Silver ug/L 256250 102 80-120
Thallium ug/L 527500 105 80-120
Vanadium ug/L 504500 101 80-120
Zinc ug/L 503500 101 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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Page 16 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1845027MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92315343004
1845028
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-12599 1500ND495498
Arsenic ug/L 500 97 75-12597 0500ND486489
Barium ug/L 500 102 75-125103 0500155667670
Beryllium ug/L 500 104 75-125104 1500ND518521
Cadmium ug/L 500 100 75-125101 1500ND501505
Chromium ug/L 500 100 75-125101 150010.6 512 517
Cobalt ug/L 500 98 75-12599 15007.7 500 502
Copper ug/L 500 104 75-125105 05006.9 528 530
Lead ug/L 500 96 75-12597 1500ND483486
Nickel ug/L 500 96 75-12596 15009.7 489 492
Selenium ug/L 500 100 75-125102 2500ND504513
Silver ug/L 250 101 75-125101 1250ND252254
Thallium ug/L 500 101 75-125100 0500ND504504
Vanadium ug/L 500 100 75-125100 150022.0 520 524
Zinc ug/L 500 97 75-12598 150025.2 510 516
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
333044
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92315343001, 92315343002, 92315343003, 92315343004, 92315343005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1845688
Associated Lab Samples:92315343001, 92315343002, 92315343003, 92315343004, 92315343005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/13/16 16:05
1,1,1-Trichloroethane ug/L ND 1.0 10/13/16 16:05
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/13/16 16:05
1,1,2-Trichloroethane ug/L ND 1.0 10/13/16 16:05
1,1-Dichloroethane ug/L ND 1.0 10/13/16 16:05
1,1-Dichloroethene ug/L ND 1.0 10/13/16 16:05
1,2,3-Trichloropropane ug/L ND 1.0 10/13/16 16:05
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/13/16 16:05
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/13/16 16:05
1,2-Dichlorobenzene ug/L ND 1.0 10/13/16 16:05
1,2-Dichloroethane ug/L ND 1.0 10/13/16 16:05
1,2-Dichloropropane ug/L ND 1.0 10/13/16 16:05
1,4-Dichlorobenzene ug/L ND 1.0 10/13/16 16:05
2-Butanone (MEK)ug/L ND 5.0 10/13/16 16:05
2-Hexanone ug/L ND 5.0 10/13/16 16:05
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/13/16 16:05
Acetone ug/L ND 25.0 10/13/16 16:05
Acrylonitrile ug/L ND 10.0 10/13/16 16:05
Benzene ug/L ND 1.0 10/13/16 16:05
Bromochloromethane ug/L ND 1.0 10/13/16 16:05
Bromodichloromethane ug/L ND 1.0 10/13/16 16:05
Bromoform ug/L ND 1.0 10/13/16 16:05
Bromomethane ug/L ND 2.0 10/13/16 16:05
Carbon disulfide ug/L ND 2.0 10/13/16 16:05
Carbon tetrachloride ug/L ND 1.0 10/13/16 16:05
Chlorobenzene ug/L ND 1.0 10/13/16 16:05
Chloroethane ug/L ND 1.0 10/13/16 16:05
Chloroform ug/L ND 1.0 10/13/16 16:05
Chloromethane ug/L ND 1.0 10/13/16 16:05
cis-1,2-Dichloroethene ug/L ND 1.0 10/13/16 16:05
cis-1,3-Dichloropropene ug/L ND 1.0 10/13/16 16:05
Dibromochloromethane ug/L ND 1.0 10/13/16 16:05
Dibromomethane ug/L ND 1.0 10/13/16 16:05
Ethylbenzene ug/L ND 1.0 10/13/16 16:05
Iodomethane ug/L ND 5.0 10/13/16 16:05
m&p-Xylene ug/L ND 2.0 10/13/16 16:05
Methylene Chloride ug/L ND 1.0 10/13/16 16:05
o-Xylene ug/L ND 1.0 10/13/16 16:05
Styrene ug/L ND 1.0 10/13/16 16:05
Tetrachloroethene ug/L ND 1.0 10/13/16 16:05
Toluene ug/L ND 1.0 10/13/16 16:05
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1845688
Associated Lab Samples:92315343001, 92315343002, 92315343003, 92315343004, 92315343005
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 10/13/16 16:05
trans-1,3-Dichloropropene ug/L ND 1.0 10/13/16 16:05
trans-1,4-Dichloro-2-butene ug/L ND 1.0 10/13/16 16:05
Trichloroethene ug/L ND 1.0 10/13/16 16:05
Trichlorofluoromethane ug/L ND 1.0 10/13/16 16:05
Vinyl acetate ug/L ND 2.0 10/13/16 16:05
Vinyl chloride ug/L ND 1.0 10/13/16 16:05
Xylene (Total)ug/L ND 1.0 10/13/16 16:05
1,2-Dichloroethane-d4 (S)%99 70-130 10/13/16 16:05
4-Bromofluorobenzene (S)%96 70-130 10/13/16 16:05
Toluene-d8 (S)%102 70-130 10/13/16 16:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1845689LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.850 98 80-125
1,1,1-Trichloroethane ug/L 50.650 101 71-129
1,1,2,2-Tetrachloroethane ug/L 46.050 92 79-124
1,1,2-Trichloroethane ug/L 46.350 93 85-125
1,1-Dichloroethane ug/L 47.650 95 73-126
1,1-Dichloroethene ug/L 53.150 106 66-135
1,2,3-Trichloropropane ug/L 45.650 91 75-130
1,2-Dibromo-3-chloropropane ug/L 50.350 101 71-133
1,2-Dibromoethane (EDB)ug/L 49.950 100 83-124
1,2-Dichlorobenzene ug/L 50.550 101 80-133
1,2-Dichloroethane ug/L 46.850 94 67-128
1,2-Dichloropropane ug/L 45.250 90 75-132
1,4-Dichlorobenzene ug/L 48.750 97 78-130
2-Butanone (MEK)ug/L 96.0100 96 61-144
2-Hexanone ug/L 96.7100 97 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.0100 98 72-135
Acetone ug/L 98.5100 99 48-146
Acrylonitrile ug/L 233250 93 40-160
Benzene ug/L 48.050 96 80-125
Bromochloromethane ug/L 48.250 96 71-125
Bromodichloromethane ug/L 48.850 98 78-124
Bromoform ug/L 49.050 98 71-128
Bromomethane ug/L 47.450 95 40-160
Carbon disulfide ug/L 52.150 104 50-160
Carbon tetrachloride ug/L 52.650 105 69-131
Chlorobenzene ug/L 49.250 98 81-122
Chloroethane ug/L 46.150 92 39-148
Chloroform ug/L 47.650 95 73-127
Chloromethane ug/L 55.650 111 44-146
REPORT OF LABORATORY ANALYSIS
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Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1845689LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.950 98 74-124
cis-1,3-Dichloropropene ug/L 48.650 97 72-132
Dibromochloromethane ug/L 49.150 98 78-125
Dibromomethane ug/L 46.450 93 82-120
Ethylbenzene ug/L 48.950 98 79-121
Iodomethane ug/L 136100 136 39-154
m&p-Xylene ug/L 95.7100 96 81-124
Methylene Chloride ug/L 51.250 102 64-133
o-Xylene ug/L 46.750 93 79-131
Styrene ug/L 50.850 102 84-126
Tetrachloroethene ug/L 46.150 92 78-122
Toluene ug/L 48.450 97 80-121
trans-1,2-Dichloroethene ug/L 50.150 100 71-127
trans-1,3-Dichloropropene ug/L 46.850 94 69-141
trans-1,4-Dichloro-2-butene ug/L 46.250 92 40-160
Trichloroethene ug/L 47.750 95 78-122
Trichlorofluoromethane ug/L 52.750 105 53-137
Vinyl acetate ug/L 104100 104 40-160
Vinyl chloride ug/L 45.550 91 58-137
Xylene (Total)ug/L 142150 95 81-126
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1845690MATRIX SPIKE SAMPLE:
MSSpike
Result
92315343001
1,1,1,2-Tetrachloroethane ug/L 17.820 89 70-130ND
1,1,1-Trichloroethane ug/L 18.120 91 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 19.120 96 70-130ND
1,1-Dichloroethene ug/L 19.520 98 70-166ND
1,2,3-Trichloropropane ug/L 20.120 101 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.020 95 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 16.220 81 70-130ND
1,2-Dichloroethane ug/L 19.820 98 70-130ND
1,2-Dichloropropane ug/L 19.220 96 70-130ND
1,4-Dichlorobenzene ug/L 14.920 75 70-130ND
2-Butanone (MEK)ug/L 41.640 104 70-130ND
2-Hexanone ug/L 43.540 109 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.840 102 70-130ND
Acetone ug/L 49.140 119 70-130ND
Acrylonitrile ug/L 102100 102 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 20 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1845690MATRIX SPIKE SAMPLE:
MSSpike
Result
92315343001
Benzene ug/L 19.320 97 70-148ND
Bromochloromethane ug/L 19.720 98 70-130ND
Bromodichloromethane ug/L 20.120 101 70-130ND
Bromoform ug/L 17.420 87 70-130ND
Bromomethane ug/L 24.120 120 70-130ND
Carbon disulfide ug/L 20.220 101 70-130ND
Carbon tetrachloride ug/L 17.820 89 70-130ND
Chlorobenzene ug/L 16.420 82 70-146ND
Chloroethane ug/L 19.720 98 70-130ND
Chloroform ug/L 19.720 98 70-130ND
Chloromethane ug/L 21.220 106 70-130ND
cis-1,2-Dichloroethene ug/L 18.920 94 70-130ND
cis-1,3-Dichloropropene ug/L 14.320 72 70-130ND
Dibromochloromethane ug/L 18.120 90 70-130ND
Dibromomethane ug/L 19.020 95 70-130ND
Ethylbenzene ug/L 15.320 76 70-130ND
Iodomethane ug/L 40.740 102 70-130ND
m&p-Xylene ug/L 30.440 76 70-130ND
Methylene Chloride ug/L 18.520 92 70-130ND
o-Xylene ug/L 15.820 79 70-130ND
Styrene ug/L 16.220 81 70-130ND
Tetrachloroethene ug/L 13.0 M1206570-130ND
Toluene ug/L 16.820 84 70-155ND
trans-1,2-Dichloroethene ug/L 18.720 93 70-130ND
trans-1,3-Dichloropropene ug/L 14.920 74 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.920 70 70-130ND
Trichloroethene ug/L 17.120 85 69-151ND
Trichlorofluoromethane ug/L 18.320 91 70-130ND
Vinyl acetate ug/L 15.1 M1403870-130ND
Vinyl chloride ug/L 18.120 90 70-130ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92315343002
1845691SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2016 12:18 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92315343002
1845691SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%100 099
4-Bromofluorobenzene (S)%98 296
Toluene-d8 (S)%103 1102
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92315343
BUNCOMBE NEW LF SW's
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92315343001 1107-SW2
92315343002 1107-SW4
92315343003 1107-SW5
92315343004 1107-SW6
92315343005 1107-Leachate Lagoon
92315343001 332783 3330521107-SW2 EPA 3010A EPA 6010
92315343002 332783 3330521107-SW4 EPA 3010A EPA 6010
92315343003 332783 3330521107-SW5 EPA 3010A EPA 6010
92315343004 332925 3331371107-SW6 EPA 3010A EPA 6010
92315343005 332925 3331371107-Leachate Lagoon EPA 3010A EPA 6010
92315343001 3330441107-SW2 EPA 8260
92315343002 3330441107-SW4 EPA 8260
92315343003 3330441107-SW5 EPA 8260
92315343004 3330441107-SW6 EPA 8260
92315343005 3330441107-Leachate Lagoon EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 24 of 27
Page 25 of 27
Page 26 of 27
Page 27 of 27
#=CL#
December 25, 2016
LIMS USE: FR - ED HILTON
LIMS OBJECT ID: 92323365
92323365
Project:
Pace Project No.:
RE:
Mr. Ed Hilton
SCS Engineers
4041 Park Oaks Blvd.
Suite 100
Tampa, FL 33610
SW-6 Resample
Dear Mr. Hilton:
Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92323365
SW-6 Resample
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92323365
SW-6 Resample
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92323365001 SW-6 Resample EPA 6010 15 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92323365
SW-6 Resample
Sample:SW-6 Resample Lab ID:92323365001 Collected:12/14/16 12:20 Received:12/14/16 12:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By Armon
Waters 12/14/16 12:201
Field pH 6.3 Std. Units 12/14/16 12:200.10 1
Field Temperature 13.0 deg C 12/14/16 12:200.50 1
Field Specific Conductance 255.7 umhos/cm 12/14/16 12:201.0 1
Oxygen, Dissolved 8.0 mg/L 12/14/16 12:20 7782-44-71
REDOX 78.7 mV 12/14/16 12:201
Turbidity 0.6 NTU 12/14/16 12:201.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/23/16 21:25 7440-36-012/17/16 01:005.0 1
Arsenic ND ug/L 12/23/16 06:18 7440-38-212/17/16 01:0010.0 1
Barium 105 ug/L 12/23/16 06:18 7440-39-312/17/16 01:005.0 1
Beryllium ND ug/L 12/23/16 06:18 7440-41-712/17/16 01:001.0 1
Cadmium ND ug/L 12/23/16 21:25 7440-43-912/17/16 01:001.0 1
Chromium ND ug/L 12/23/16 06:18 7440-47-312/17/16 01:005.0 1
Cobalt 7.0 ug/L 12/23/16 06:18 7440-48-412/17/16 01:005.0 1
Copper ND ug/L 12/23/16 06:18 7440-50-812/17/16 01:005.0 1
Lead ND ug/L 12/23/16 21:25 7439-92-112/17/16 01:005.0 1
Nickel ND ug/L 12/23/16 21:25 7440-02-012/17/16 01:005.0 1
Selenium ND ug/L 12/23/16 06:18 7782-49-212/17/16 01:0010.0 1
Silver ND ug/L 12/23/16 06:18 7440-22-412/17/16 01:005.0 1
Thallium ND ug/L 12/23/16 06:18 7440-28-012/17/16 01:005.4 1
Vanadium ND ug/L 12/23/16 06:18 7440-62-212/17/16 01:005.0 1
Zinc ND ug/L 12/23/16 06:18 7440-66-612/17/16 01:0010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/25/2016 05:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323365
SW-6 Resample
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341173
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92323365001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1892896
Associated Lab Samples:92323365001
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 12/23/16 05:11
Arsenic ug/L ND 10.0 12/23/16 05:11
Barium ug/L ND 5.0 12/23/16 05:11
Beryllium ug/L ND 1.0 12/23/16 05:11
Cadmium ug/L ND 1.0 12/23/16 05:11
Chromium ug/L ND 5.0 12/23/16 05:11
Cobalt ug/L ND 5.0 12/23/16 05:11
Copper ug/L ND 5.0 12/23/16 05:11
Lead ug/L ND 5.0 12/23/16 05:11
Nickel ug/L ND 5.0 12/23/16 05:11
Selenium ug/L ND 10.0 12/23/16 05:11
Silver ug/L ND 5.0 12/23/16 05:11
Thallium ug/L ND 5.4 12/23/16 05:11
Vanadium ug/L ND 5.0 12/23/16 05:11
Zinc ug/L ND 10.0 12/23/16 05:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1892897LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 430500 86 80-120
Arsenic ug/L 435500 87 80-120
Barium ug/L 423500 85 80-120
Beryllium ug/L 443500 89 80-120
Cadmium ug/L 418500 84 80-120
Chromium ug/L 433500 87 80-120
Cobalt ug/L 429500 86 80-120
Copper ug/L 462500 92 80-120
Lead ug/L 426500 85 80-120
Nickel ug/L 406500 81 80-120
Selenium ug/L 446500 89 80-120
Silver ug/L 233250 93 80-120
Thallium ug/L 462500 92 80-120
Vanadium ug/L 435500 87 80-120
Zinc ug/L 433500 87 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/25/2016 05:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323365
SW-6 Resample
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1892898MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92323288001
1892899
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125102 3500ND491508
Arsenic ug/L 500 78 75-12583 6500ND393415
Barium ug/L 500 76 75-12580 6500ND378402
Beryllium ug/L 500 79 75-12584 5500ND397418
Cadmium ug/L 500 76 75-12580 5500ND380402
Chromium ug/L 500 78 75-12582 6500ND388412
Cobalt ug/L 500 76 75-12581 7500ND381407
Copper ug/L 500 82 75-12587 6500ND413438
Lead ug/L 500 99 75-125103 3500ND497514
Nickel ug/L M15007375-12577 6500ND364386
Selenium ug/L 500 81 75-12585 5500ND404425
Silver ug/L 250 88 75-12591 4250ND219227
Thallium ug/L 500 83 75-12589 65005.5J 422 448
Vanadium ug/L 500 78 75-12583 6500ND390413
Zinc ug/L 500 77 75-12583 7500ND387415
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/25/2016 05:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92323365
SW-6 Resample
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/25/2016 05:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92323365
SW-6 Resample
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92323365001 SW-6 Resample
92323365001 341173 341571SW-6 Resample EPA 3010A EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/25/2016 05:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 11
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