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Home My WebLink About8301_ScotlandCDoverMSW_WQMonitoring_April2017_DIN28108_20170630DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF April 2017 Groundwater Monitoring Report Scotland County Landfill Laurinburg, North Carolina NC Solid Waste Permit # 83-01 Prepared for: Scotland County Public Works Department 507 W. Covington Street Laurinburg, North Carolina 28352 June 2017 Prepared by: © 2017 Smith Gardner, Inc. This document is intended for the sole use of the client for which it was prepared and for the purpose agreed on by the client and Smith Gardner, Inc. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF April 2017 Groundwater Monitoring Report Scotland County Landfill NC Solid Waste Permit #83-01 Prepared For: Scotland County Public Works Department Laurinburg, North Carolina 28352 S+G Project No. SCOT-2 Madeline German, P.G. Project Geologist Joan Smyth, P.G. Senior Hydrogeologist June 2017 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Table of Contents Page i Scotland County Landfill Solid Waste Permit No. 83-01 April 2017 Water Quality Monitoring Report Table of Contents Page 1.0INTRODUCTION ......................................................................................................... 2 2.0SITE GEOLOGY ........................................................................................................... 2 3.0SAMPLING LOCATIONS ............................................................................................. 2 4.0SAMPLING PROCEDURES ......................................................................................... 3 5.0FIELD & LABORATORY RESULTS .............................................................................. 3 5.1Laboratory Analysis ................................................................................................... 3 5.2Field Results .............................................................................................................. 4 5.3Inorganic Constituent Laboratory Results ............................................................... 4 5.4Organic Constituent Laboratory Results .................................................................. 5 5.5Surface Water Analytical Results ............................................................................. 5 6.0CORRECTIVE MEASURES UPDATE ............................................................................ 5 7.0STATISTICAL ANALYSIS AND RESULTS .................................................................... 6 7.1Statistical Analysis .................................................................................................... 6 7.2Statistical Results ..................................................................................................... 6 8.0GROUNDWATER CHARACTERIZATION ...................................................................... 6 9.0CONCLUSIONS .......................................................................................................... 7 FIGURES Figure 1 Groundwater Potentiometric Surface Map Figure 2 Total VOC Isoconcentration Map TABLES Table 1 Groundwater Elevations Table 2 Field Parameter Results Table 3 Detected Inorganic Constituents Table 4 Detected Organic Constituents Table 5 Indicator Parameters Table 6 Statistical Analysis Summary Table 7 Conductivity and Velocity Calculations APPENDICES Appendix A Monitoring Well Information Appendix B Laboratory Analytical Report Appendix C Biochlor Models Appendix D Time vs. Concentration Graphs DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Page 2 1.0INTRODUCTION The Scotland County Landfill, operating under Solid Waste Permit #83-01, is required to submit semi-annual groundwater monitoring reports (15A NCAC 13B.0544) for assessment monitoring. This report presents the results from the sampling conducted on April 18-19, 2017. The Scotland County Landfill contains two disposal areas. Phase I is located north of Old Maxton Road. Phases II and III are located south of Old Maxton Road. C&D waste is currently accepted over the closed Phases II and III. Municipal Solid Waste (MSW) is presently transferred off-site to a lined landfill in another county. The MSW landfill was closed per Solid Waste Regulations and the certification report1 was submitted to the Solid Waste Section (SWS) in August 1999. In 2007 the Scotland County Landfill was assessed to determine if groundwater issues would require a remediation plan. The Corrective Action Plan2 was approved on February 3, 2009. SSection 8.0 of this report is an update regarding the current corrective action situation for this facility. This report includes a field procedure summary, laboratory and statistical analyses, groundwater characterization, summary tables, graphs and laboratory analytical reports. 2.0SITE GEOLOGY According to the 1985 Geologic Map of North Carolina, the Scotland County Landfill is located in an area underlain by the Middendorf Formation. The Geology of the Carolinas3 describes the Middendorf Formation as deeply weathered at its type locality which has caused considerable difficulty in identification. In North Carolina the Middendorf is described as interbedded sands and clays with laterally discontinuous beds and common cross-bedding. Sandstone is the dominant lithology with the basal portion being conglomeritic with quartz and white kaolin clay clasts; believed to have been deposited in a fluvial upper delta plain environment. 3.0SAMPLING LOCATIONS The groundwater monitoring network consists of twelve wells (MW-1 through MW-9 and MW-11 through MW-13) positioned around the landfill perimeter (FFigure 1). MW-2 and MW-11 are only sampled during the spring event as approved in the March 2012 Revised Corrective Action Update4. MW-1 and MW-8 serve as the background wells for this site. Two surface water sampling points are located up and downstream of the landfill on Shoe Heel Creek. An 1 Construction Quality Assurance Report, Scotland County Landfill Phase III Closure, G.N. Richardson & Associates, Inc. August 1999. 2 Corrective Action Plan, Scotland County Landfill, Richardson Smith Gardner and Associates, Approved February 2009. 3 Horton, J. Wright, and Zullo, Victor, A., The Geology of the Carolinas, University of Tennessee Press, 1991. 4 Revised Corrective Action Update, Scotland County Landfill. Richardson Smith Gardner and Associates. March 26, 2012. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Page 3 equipment blank (EB) and trip blank (TB) were also analyzed for quality control purposes. Well depths range from 14.5 to 40 feet below grade. Available boring logs, presented in AAppendix A, indicate wells were installed in varying amounts of sand, silt and clay. Well construction details are provided in TTable 1. 4.0SAMPLING PROCEDURES Sampling procedures followed the protocols set forth in the site’s approved Water Quality Monitoring Plan2 and the North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities (North Carolina Department of Environment and Natural Resources, Division of Waste Management). Each well was gauged to determine groundwater depth and then purged three to five well volumes or until dry. Water table elevations and are included in TTable 1. Samples were collected in laboratory prepared containers for the specified analytical procedures. Sampling equipment, was brought to the site in sterile condition from the manufacturer or was cleaned in the laboratory and transported to the site in a condition to avoid potential contamination. Groundwater samples were properly preserved, placed on ice and transported to the laboratory facility within the specified hold times for analysis. 5.0FIELD & LABORATORY RESULTS Analytical results were compared to the NC DWM Solid Waste Section Quantitation Limits (SWSLs), 15A NCAC 2L.0200 (2LStandard) and Federal Maximum Contaminant Limits (MCL). Surface water results were compared with the NCAC 2B Standard for Class C waters (2B Standard). Constituents detected between the Method Detection Limit (MDL) and SWSL are a non- quantifiable value defined by the laboratory as “J” values. Values reported below the MDL are considered non-detect. The laboratory analytical report is included as AAppendix B. 5.1Laboratory Analysis Samples were collected and analyzed by Environment 1, Inc., Greenville, NC, a North Carolina certified laboratory (NC Wastewater ID #10). Laboratory analysis for sampled locations included: xmetals plus mercury xAppendix II volatile organic compounds (VOCs) xtetrahydrofuran. Select wells were also analyzed for: xPesticides & PCBs xsemi-volatile organics xacid fraction compounds DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Page 4 Monitored Natural Attenuation (MNA) sampling locations were also analyzed for: xbiochemical oxygen demand (BOD) xchemical oxygen demand (COD) xnitrate nitrogen xtotal organic carbon (TOC) xtotal alkalinity xiron xchloride xsulfate xsulfide xcarbon dioxide MNA compounds analyzed by Pace Analytical Energy Services, LLC. (220 William Pitt Way, Pittsburg, PA 15238) included: xdissolved methane xhydrogen xethane xethane xvolatile fatty acids Analysis for these constituents was performed via the EPA approved methods identified in the laboratory report. 5.2Field Results Field parameters pH, conductivity, temperature, turbidity, dissolved oxygen and oxygen reduction potential (ORP) were collected by Environment 1; data is presented in TTable 2. April 2017 data is generally consistent with previously recorded field measurements at the site. Turbidity concentrations in MW-2, MW-7 and MW-12 were reported at levels over 100 NTUs. 5.3Inorganic Constituent Laboratory Results The inorganic constituent Arsenic was detected at its 2L Standard in the sample collected from MW-4 this event. Iron was detected above its 2L Standard in samples (MW-1, MW-6, MW-7, MW-9, MW-12 and MW-13) collected during this event. Vanadium (MW-12) was the only inorganic constituent detected above its GWP Standard for this event. Elevated turbidity values likely contributed to the elevated inorganic detections this event. The influence of turbidity on inorganic results in general, and these constituents in particular, at this site was characterized in the Inorganic Constituent Alternate Source Demonstration Report5. This report summarized the results of both total and dissolved analysis samples collected during the fall 2016 monitoring event. In particular, the 5 Smith Gardner, Inc., Inorganic Constituent Alternate Source Demonstration Report, Scotland County Landfill Facility, April 2017. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Page 5 constituents detected above the groundwater standards were found to be naturally occurring with total concentrations that were biased high by turbidity in the samples. Most inorganic constituents were non-quantifiable “J-values” or reported below the MDL. Inorganic detections are presented on TTable 3. 5.4Organic Constituent Laboratory Results Five organic constituents were detected above their 2L Standards: x1,1-Dichloroethane (MW-6), x1,4-Dichorobenzene (Mw-2, MW-6), xBenzene(MW-2, MW-3, MW-6,MW-7 and MW-13), xDieldrin (MW-7) xVinyl chloride (MW-3, MW-4, MW-6 and MW-13). Tetrahydrofuran was detected in the samples collected from MW-2 and MW-13 this event however; standards have not been established for this parameter. Organic detections are presented on TTable 4. Additionally, a total volatile organic compound (VOC) isopach map is presented as FFigure 2. This map shows where VOC concentrations have been detected around the site for this sampling event. 5.5Surface Water Analytical Results No inorganic or organic constituents were reported above the 2B Standard in samples collected this event. 6.0CORRECTIVE MEASURES UPDATE Scotland County is currently operating under a Corrective Action Plan (CAP)6 approved February 3, 2009, and a Revised Corrective Action Update letter7 to Brian Wootton at NCDENR SWS submitted on March 26, 2012. Adjustments to the MNA parameters were implemented starting with the spring 2012 sampling event based on verbal approval from NCDENR, including reduced sampling parameters, frequency and locations. This event is a third year event therefore samples from select locations were analyzed for the full suite of MNA indicator parameters. Laboratory results indicate methanogenic processes continue to be present on site, and natural attenuation is occurring. Results are summarized in Table 5. 6 Corrective Action Plan, Scotland County Landfill, Richardson Smith Gardner and Associates, Inc. January 2009, approved February 2009. 7 Letter from Joan Smyth of RSG to Brian Wootton of NCDENR dated March 26, 2012. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Page 6 Biochlor is an EPA screening tool, designed to simulate natural attenuation of chlorinated solvents. For this event biochlor was run on wells MW-4, MW-6, MW-12 and MW-13. Models indicate a slight decrease in parent compounds as the chlorinated solvents attenuate. Results are presented in AAppendix C. 7.0STATISTICAL ANALYSIS AND RESULTS 7.1Statistical Analysis Smith Gardner, Inc. (S+G) reviewed the laboratory data from this event to evaluate trends, examine major site changes and establish statistical significance while considering differences between up and down gradient wells. Data entry and analysis was performed using the Chempoint and Chemstat statistical software package developed specifically for RCRA Subtitle D sites (Starpoint Software, Cincinnati, OH). Chemstat follows EPA and DWM protocols for approved statistical analysis methods for groundwater data. The data from this event was added to our existing site database, reviewed to evaluate the most appropriate analysis methods and checked for outliers and erroneous results. Initial analysis to determine noteworthy changes or data trends involved basic data review and construction of a time-concentration graph for specific parameters (included in AAppendix D). A statistical analysis summary is presented as TTable 6. 7.2Statistical Results Statistical analysis was performed for arsenic, iron and vanadium for reported total metals concentrations at or above their 2L or GWP Standards this event. Statistical analysis was not performed on constituents detected in background wells. Wilcoxon Rand Individual Well Test (Intra-well) was completed for iron. Parametric Prediction Limit Test (Inter-well) was completed for arsenic and vanadium. No concentrations were determined to be statistically significant this event. 8.0GROUNDWATER CHARACTERIZATION A potentiometric surface map was prepared from groundwater elevations for this sampling event. In general, groundwater is flowing east toward Shoe Heel Creek Swamp. This is consistent with groundwater flow patterns previously reported for the site. The potentiometric surface map is attached as FFigure 1. Groundwater flow velocities were calculated for monitoring wells MW-1 through MW-8 using the equation: V = Ki/n Where: K = hydraulic conductivity i = groundwater gradient n = porosity DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Scotland County Landfill April 2017 Groundwater Monitoring Report June 2017 Page 7 Groundwater flow velocities ranged from 0.354 ft/day (MW-8) to 1.444 ft/day (MW-5), and averaged 0.749 ft/day. Calculated flow velocities are presented in TTable 7. 9.0CONCLUSIONS Laboratory results indicate that water quality at the Scotland County Landfill is generally consistent with reported historical detections. Groundwater analysis indicates that inorganic parameter concentrations were likely influenced by high turbidity of naturally occurring metals in samples collected this event. Flow direction and gradient remain consistent with reported historical observations. Natural attenuation continues to degrade chlorinated solvents on site. Overall total VOC concentrations have decreased since the last biochlor model. All four modeled locations have adequate to strong evidence for anaerobic biodegradation according to the Natural Attenuation Screening Protocol. The facility will continue semi-annual monitoring with the next event that will include full MNA analysis, scheduled for October 2017. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF FIGURES April 2017 Groundwater Monitoring Report Scotland County Landfill Solid Waste Permit No. 83-01 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF TABLES April 2017 Groundwater Monitoring Report Scotland County Landfill Solid Waste Permit No. 83-01 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 1 Groundwater Elevations Scotland County Landfill April 18-19, 2017 By:MG Date: 6/12/2017 Well Well Installation Date Latitude Longitude Well Diameter (inches) Total Well Depth (ft bgs) Ground Surface Elevation (ft amsl) TOC Elevation (ft amsl) Depth to Water (ft bgs) Water Table Elevation (ft bgs) Screen Interval (feet bgs) Screen Geology MW-1 11/15/1993 34.72284 79.38451 2.0 21.0 190.35 192.83 6.88 185.95 5-20 sand with clay MW-2 11/18/1993 34.72577 79.38255 2.0 30.0 195.85 197.62 20.41 177.21 14-29 sand MW-3 11/19/1993 34.72696 79.37951 2.0 30.0 190.41 192.92 22.83 170.09 14-29 clayey sand MW-4 11/22/1993 34.72575 79.37836 2.0 34.0 190.12 191.11 23.37 167.74 18-33 clayey sand MW-5 11/17/1993 34.72290 79.38181 2.0 28.0 190.29 193.69 15.12 178.57 12-27 clayey sand MW-6 11/22/1993 34.72599 79.37951 2.0 40.0 180.27 186.44 16.04 170.40 19-39 sand and clay MW-7 11/23/1993 34.72821 79.38067 2.0 30.0 191.99 194.53 18.12 176.41 14-29 sandy clay MW-8 11/23/1993 34.72479 79.38627 2.0 21.0 193.75 196.05 11.28 184.77 5-20 sand MW-9 9/17/1990 34.72625 79.37735 4.0 22.0 169.83 171.22 7.27 163.95 NA clay MW-10 NA 34.72227 79.38415 NA NA 192.00 193.31 7.70 185.61 NA NA MW-11 4/24/1981 34.72857 79.37891 4.0 40.0 177.13 179.82 17.18 162.64 30-40 sand MW-12* 8/27/2009 34.72760 79.37871 2.0 35.0 187.17 187.00 27.55 159.45 25-35 silty sand MW-13* 8/27/2009 34.72644 79.37724 2.0 14.5 162.00 162.00 3.30 158.70 4.5-14.5 silty sand Note: NA = not available bgs = below ground surface amsl = above mean sea level Water level data collected by Environment 1 personnel. Available well logs provided in AAppendix A *GSE and TOC are approximate for MW-12 and MW-13 Z:\Projects\Groundwater Monitoring Reports\Scotland\20.Scotland 4-15\4-15-scot_gw_tables-1 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 2 Field Parameter Results Scotland County Landfill April 18-19, 2017 By:MG Date: 6/12/2017 Well pH (Std Units) Specific Conductivity (umhos/cm) Temperature (Celsius) Turbidity (NTU) DO (mg/l) ORP (mV) MW-1 5.5 114 19 16 6140 63 MW-2 5.8 538 19 320 200 84 MW-3 5.8 251 19 17 180 113 MW-4 5.8 188 18 70 410 58 MW-5 6.4 498 16 8.2 2860 86 MW-6 5.5 335 17 5.6 120 77 MW-7 6.2 1013 17 400 1100 35 MW-8 4.6 103 19 13 5940 101 MW-9 5.4 250 17 55 2190 95 MW-11 4.8 144 18 8.1 3620 180 MW-12 6.0 948 20 290 670 27 MW-13 5.6 366 17 55 170 70 Upstream 5.8 62 19 NA NA NA Downstream 6.3 123 20 NA NA NA Note: NA = Not Analyzed Field measurements collected by Environment 1, Inc. personnel; from reports dated: 5/22/2017 & 6/1/2017, Client Z:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\20. Scotland 4-15\4-15-scot_gw_tables-1 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 3 Detected Inorganic Constituents Scotland County Landfill April 18-19, 2017 By: MG Date: 6/13/2017 Parameter MDL SWSL 2L / GWP*MCL 2B MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-11 MW-12 MW-13 Upstream Downstream Antimony 0.06 6 1 *6 640 0.07 J 0.13 J 0.06 J <0.06 0.11 J <0.06 <0.06 <0.06 0.07 J <0.06 0.1 J <0.06 <0.06 <0.06 Arsenic 0.07 10 10 10 10 0.2 J 6.4 J 1.9 J 110 1.1 J 3.1 J 4.4 J <0.07 0.24 J 0.09 J 6.6 J 1.3 J 0.64 J 0.32 J Barium 0.07 100 700 2000 200000 12.4 J 30.1 J 36.1 J 18.6 J 25.4 J 30.6 J 66.6 J 53.2 J 17 J 27.3 J 12.7 J 40.8 J 16.6 J 13.3 J Beryllium 0.07 1 4 *4 6.5 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 0.14 J 0.18 J <0.07 <0.07 <0.07 Cadmium 0.08 1 2 5 2 0.08 J 0.16 J 0.28 J 0.12 J 0.13 J 0.09 J 0.13 J 0.59 J 0.25 J <0.08 0.52 J 0.12 J <0.08 <0.08 Cobalt 0.24 10 1 *NE 4 0.38 J 1.7 J 0.65 J <0.24 1.3 J <0.24 0.31 J 1.6 J <0.24 3.5 J <0.24 0.81 J 0.95 J 0.51 J Total Chromium 0.08 10 10 100 50 1 J 0.69 J 0.28 J 0.54 J 0.18 J <0.08 <0.08 0.15 J <0.08 4 J 9.6 J 0.41 J 0.78 J 0.31 J Copper 0.09 10 1000 1300 7 0.55 J 3.1 J 4.4 J 0.83 J 5.8 J 0.29 J 11 1.6 J 0.69 J 2.2 J 2.9 J 1.5 J 0.65 J 0.94 J Iron 13.27 300 300 300 1000 9972 NA NA 333426 NA 227552 87929 NA 111163 NA 335037 29610 NA NA Iron (dissolved) 13.27 300 300 300 1000 NA NA NA NA NA NA NA NA 186 J NA 228358 20637 NA NA Lead 0.08 10 15 15 25 1.3 J 1.7 J 1.6 J 0.97 J 1.1 J 0.13 J 0.85 J 1.8 J 0.89 J 7.3 J 4.5 J 1.6 J 0.79 J 1.1 J Mercury 0.07 0.2 1 2 0.012 <0.07 0.16 J <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 0.41 <0.07 2.34 NA NA Nickel 0.08 50 100 NE 88 0.69 J 1.2 J 1.4 J 0.42 J 1.7 J 0.54 J 1 J 1.7 J 0.68 J 1.2 J 0.84 J 0.61 J 1.5 J 0.98 J Selenium 0.51 10 20 50 5 <0.51 0.63 J <0.51 <0.51 0.69 J <0.51 0.52 J <0.51 <0.51 <0.51 1.9 J 0.53 J <0.51 <0.51 Thallium 0.08 6 0.28* 2 0.47 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 0.12 J <0.08 <0.08 0.09 J <0.08 <0.08 Tin 0.13 100 2000* NE 800 NA 0.26 J 1.6 J <0.13 NA <0.13 0.21 J NA <0.13 0.44 J <0.13 0.29 J NA NA Vanadium 0.24 25 0.3 *NE NE 2.9 J 4.6 J 1 J 6.2 J 1.4 J 3.1 J 0.62 J 0.53 J 0.91 J 0.28 J 227 3.3 J 0.57 J 0.49 J Zinc 0.66 10 1000 5000 50 1.7 J 102 14 2.7 J 4.4 J 2.9 J 8.8 J 66 1.3 J 9 J 6.6 J 0.72 J 6 J 8.9 J Note: MDL -Method Detection Limit Table units are presented in ug/l. SWSL -Solid Waste Section Quantitation Limits Lab analysis by Environment 1, Inc. reports dated 5/22/2017 & 6/1/2017, Client ID#6000. 2L -Groundwater Standards (15A NCAC 2L 0200) GWP -Groundwater Protection Standards (noted by *) MCL - Federal Maximum Contaminant Level 2B -NCAC 2B Standard for Class C waters BOLD -Detection above 2L or GWP Standard J-Laboratory defined concentration, between MDL and SWSL < MDL -Not detected at or above MDL NE -Standard Not Established NA -Parameter Not Analyzed Z:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\20. Scotland 4-15\4-15-scot_gw_tables-1 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 4 Detected Organic Constituents Scotland County Landfill April 18-19, 2017 By: MG Date: 6/12/2017 Parameter MDL SWSL 2L/GWP* MCL 2B MW-2 MW-3 MW-4 MW-6 MW-7 MW-9 MW-13 Upstream 1,1-Dichloroethane 0.20 5 6 NE 100 6.4 1.7 J <0.2 77.9 0.3 J 0.7 J 4.2 J <0.2 1,1-Dichloroethene 0.17 5 7 100 1500 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 0.2 J <0.17 1,2-Dichloropropane 0.21 1 0.6 5 15 0.6 J <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 1,4-Dichlorobenzene 0.39 1 6 75 100 110.4 1 <0.39 113.1 1 <0.39 2.7 <0.39 Benzene 0.24 1 1 5 51 44.6 1 <0.24 55.1 3.5 <0.24 11.3 <0.24 Chlorobenzene 0.30 3 50 100 140 2.4 J <0.3 <0.3 0.6 J 3.1 <0.3 1.1 J <0.3 Chloroethane 0.48 10 3000 NE NE <0.48 <0.48 <0.48 0.6 J <0.48 <0.48 <0.48 <0.48 Cis-1,2-Dichloroethene 0.25 5 70 70 720 10.5 <0.25 <0.25 0.3 J <0.25 <0.25 4.2 J <0.25 Dichlorodifluoromethane 0.51 5 1000 NE NE <0.51 <0.51 <0.51 1.3 J <0.51 <0.51 <0.51 NA Dieldrin 0.04 0.075 0.002 NE NE <0.042 <0.042 <0.042 <0.042 00.0927 <0.042 <0.042 NA Ethylbenzene 0.21 1 600 700 97 3.2 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 Tetrachloroethene 0.17 1 0.7 5 3.3 0.5 J <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 Tetrahydrofuran 0.39 NE NE NE NE 6.4 <0.39 <0.39 <0.39 0.7 J <0.39 1.7 NA Toluene 0.23 1 600 1000 11 0.3 J 0.3 J <0.23 <0.23 <0.23 <0.23 <0.23 0.8 J Trichloroethene 0.23 1 3 5 30 1.3 <0.23 <0.23 <0.23 <0.23 <0.23 0.7 J <0.23 Vinyl Chloride 0.630 1 0.03 2 2.4 110.7 2.6 1.4 16.5 <0.63 <0.63 44.8 <0.63 Xylenes 0.68 5 500 10000 670 1.3 J <0.68 <0.68 <0.68 <0.68 <0.68 <0.68 <0.68 Note: MDL - Method Detection Limit Table units are presented in ug/l. SWSL - Solid Waste Section Quantitation Limits 2L - Groundwater Standards (15A NCAC 2L 0200) GWP -Groundwater Protection Standards (noted by *) MCL - Federal Maximum Contaminant Level BOLD - Detection above 2L or GWP Standard J - Laboratory defined concentration between MDL and SWSL < MDL - Not detected at or above MDL NE - Standard Not Established NA - Parameter Not Analyzed Lab data analysis by Environment 1, Inc. reports dated 5/22/2017 & 6/1/2017, Client H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\24. Scotland 4-17\4-17-scot_gw_tables.xlsx DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 5 Indicator Parameters Scotland County Landfill April 18-19, 2017 By: MG Date: 6/13/2017 Parameter (units)MDL MW-1 MW-2 MW-3 MW-4 MW-6 MW-7 MW-9 MW-12 MW-13 BOD (mg/l)2 <2 NA NA <2 <2 6.2 <2 5.8 <2 COD (mg/l)0.84 22 NA NA 25 28 43 27 43 26 Nitrate Nitrogen (mg/l)0.003 1.95 J NA NA <0.003 <0.003 <0.003 0.32 J <0.84 <0.84 Total Organic Carbon (mg/l)0.12 1.06 NA NA 1.78 4.04 5.95 2.62 4.64 2.88 Total Alkalinity (mg CaCO3/l)1 3 NA NA 55 99 391 6 228 55 Chloride (mg/l)5 16 NA NA 8 18 6 13 23 32 Sulfate (mg/l)5 18.3 J NA NA 13.8 J 23.8 J 9.6 J 70.2 J 128 J 58.7 J Sulfide (ug/l)100 <100 154 J 220 J <100 105 J <100 <100 <100 <100 Dissolved Oxygen (mg/l)0.1 6.14 0.2 0.18 0.41 0.12 1.1 2.19 0.67 0.17 Carbon Dioxide (mg/l)1 19 NA NA 212 365 484 85 380 197 ORP (MV)NE 63 84 113 58 77 35 95 27 70 Lactic Acid (mg/l)0.006 0.02 J NA NA 0.019 J 0.026 J 0.035 J 0.037 J 0.09 J 0.041 J Acetic Acid (mg/l)0.005 0.035J NA NA 0.03 J 0.024 J 0.053 J 0.025 J 0.053 J 0.024 J Propionic Acid (mg/l)0.002 <0.002 NA NA 0.0024 J <0.002 0.004 J 0.031 J 0.0026 J <0.002 Butyric Aid (mg/l) 0.006 <0.006 NA NA <0.006 <0.006 0.006 J <0.006 <0.006 <0.006 Pyruvic Acid (mg/l) 0.002 <0.002 NA NA <0.002 <0.002 0.0023 J <0.002 <0.002 <0.002 Hexanoic Acid (mg/l)0.009 0.021 J NA NA 0.019 J <0.009 <0.009 <0.009 0.022 J <0.009 Methane (Max Dissolved) (ug/l)0.006 2.7 NA NA 3100 8200 6200 25 180 180 Ethane (ug/l)0.002 <0.002 NA NA 0.024 0.049 0.25 0.0031 J <0.002 0.037 Ethene (ug/l)0.006 <0.006 NA NA 0.079 0.4 0.055 0.0076 J 0.16 J 0.11 Hydrogen (nM)0.075 2.1 NA NA 1.6 1.9 1.8 1.6 NA 1.4 Note: J = Laboratory defined as between MDL and SWSL limit OR between the MDL and PQL (Practical Quantitation Limit). Non-detects are presented as <MDL value NA = Parameter Not Analyzed Lab data analysis by Environment 1, Inc. reports dated 5/22/2017 and 6/1/2017, Client ID #6000 and Microseeps/Pace Analytical Energy Services workorder #22394 H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\24. Scotland 4-17\4-17-scot_gw_tables.xlsx DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 6 Statistical Analysis Summary Scotland County Landfill April 18-19 , 2017 By: MG Date: 12/13/2016 Monitoring Well Parameter Result 2L/GWP* Test Unit %ND Test Statistically Significant? MW-4 Arsenic 10 10 ug/l 66.01 PPL N MW-4 Iron 33426 300 ug/l 0 Wilcoxon N MW-6 Iron 27552 300 ug/l 0 Wilcoxon N MW-7 Iron 87929 300 ug/l 0 Wilcoxon N MW-9 Iron 11163 300 ug/l 0 Wilcoxon N MW-12 Iron 35037 300 ug/l 0 Wilcoxon N MW-13 Iron 29610 300 ug/l 0 Wilcoxon N MW-12 Vanadium 27 0.3* ug/l 50.84 PPL N Notes: %ND Method chosen due to percent non-detects PPL Parametric Prediction Limit (Inter-Well) Wilcoxon Wilcoxon Rand Individual Well Test (Intra-well) Bold indicates statistical significance Lab analysis by Environment 1, Inc. reports dated 5/22/2017 & 6/1/2017, Client ID#6000. MW-1 and MW-8 are used as site background wells +?3URMHFWV?*URXQGZDWHU0RQLWRULQJ?*URXQGZDWHU0RQLWRULQJ5HSRUWV?6FRWODQG?6FRWODQG?VFRWBJZBWDEOHV[OV[ DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Table 7 Conductivity and Velocity Calculations Scotaland County Landfill April 18-19, 2017 By: MG Date: 6/22/2017 Well Groundwater Elevation (feet) Hydraulic Conductivity (ft/day) Porosity (%) Gradient Velocity (ft/day) MW-1 185.95 6.8 0.2 0.0177 0.603 MW-2 177.21 6.12 0.2 0.0173 0.529 MW-3 170.09 14.29 0.18 0.0128 1.016 MW-4 167.74 23.13 0.21 0.0047 0.521 MW-5 178.57 18.03 0.21 0.0168 1.444 MW-6 170.40 13.27 0.18 0.0114 0.843 MW-7 176.41 7.48 0.15 0.0137 0.682 MW-8 184.77 7.82 0.2 0.0091 0.354 Average Velocity (ft/day)0.749 Note:Velocity Calculated from V=K*I/n V = velocity K = Hydraulic Conductivity I = Gradient n = Porosity Hydraulic Conductivity values from 4/4/94 GAI Consultants Inc. report Estimated porosity values assumed from Groundwater and Wells (Driscoll) Water level data collected by Environment 1 personnel. H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\24. Scotland 4-17\4-17-scot_gw_tables.xlsx DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF APPENDIX A Monitoring Well Information April 2017 Groundwater Monitoring Report Scotland County Landfill Solid Waste Permit No. 83-01 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF FIELD BOREHOLE LOG BOREHOLE NUMBER PROJECT NAME: LOCATION: DRILLING CO: DRILLING METHOD: FIELD PARTY: GEOLOGIST: DATE BEGUN: COMPLETED: TOTAL DEPTH: TOP OF CASING ELEV.: Depth (ft) Time Date STATIC WATER LEVEL (BLS) DE P T H BL O W C O U N T SA M P L I N G M E T H O D RE C O V E R Y DR I L L M E T H O D DESCRIPTION LI T H O L O G Y WE L L IN S T A L L A T I O N 0.0 5.0 10.0 15.0 20.0 25.0 30.0 35.0 0.0 5.0 10.0 15.0 20.0 25.0 30.0 35.0 DE P T H Richardson Smith Gardner & Assoc 14 North Boylan Avenue, Raleigh NC 27603 (919) 828-0577 Page 1 of 1 GROUND ELEV.: NORTHING:EASTING:0 0 MW-12 HSA Scotland County Landfill Laurinburg, NC Zebra Environmental, Inc. Dan Ferrell J. Smyth 8/26/09 8/27/09 35 GRAB GRAB GRAB GRAB GRAB GRAB HSA SOIL: Dark brown dry topsoil SILTY SAND: Dry, brown to red silty F-M sand. CLAYEY SILTY SAND: Dry, tan brown clayey silty F-M sand. SILTY SAND: Dry, red brown to tan silty F-M sand. SILTY SAND: Moist, light tan silty F-M sand grading to silty F sand at 25 feet. SILTY SAND: Wet, Light tan, silty fF sand. B.T. at 35 feet. NA NA NA NA NA NA DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF FIELD BOREHOLE LOG BOREHOLE NUMBER PROJECT NAME: LOCATION: DRILLING CO: DRILLING METHOD: FIELD PARTY: GEOLOGIST: DATE BEGUN: COMPLETED: TOTAL DEPTH: TOP OF CASING ELEV.: Depth (ft) Time Date STATIC WATER LEVEL (BLS) DE P T H BL O W C O U N T SA M P L I N G M E T H O D RE C O V E R Y DR I L L M E T H O D DESCRIPTION LI T H O L O G Y WE L L IN S T A L L A T I O N 0.0 5.0 10.0 0.0 5.0 10.0 DE P T H Richardson Smith Gardner & Assoc 14 North Boylan Avenue, Raleigh NC 27603 (919) 828-0577 Page 1 of 1 GROUND ELEV.: NORTHING:EASTING:0 0 MW-13 HSA Scotland County Landfill Laurinburg, NC Zebra Environmental, Inc. Dan Ferrell J. Smyth 8/26/09 8/27/09 14.5 GRAB GRAB GRAB HSA SOIL: Dark brown dry topsoil SILTY SAND: Wet, black to gray silty F-M sand to sandy silt. SILTY SAND: Wet, Light tan silty F-C sand. B.T. @ 14.5 feet. NA NA NA NA NA NA DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF APPENDIX B Laboratory Analytical Report April 2017 Groundwater Monitoring Report Scotland County Landfill Solid Waste Permit No. 83-01 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. 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PO Box 7085 114 Oakmont Drive Greenville, NC 27835 April 28, 2017 RE: Pace Workorder: SCOTLAND CO. / 6000 Dear Steve Jones: 22394 Enclosed are the analytical results for sample(s) received by the laboratory on Friday, April 21, 2017. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Enclosures Ruth Welsh 04/28/2017 Ruth.Welsh@pacelabs.com Total Number of Pages ____ As a valued client we would appreciate your comments on our service. Please email PAESfeedback@pacelabs.com. Customer Service Representative 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. 26 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 2 of 24 LABORATORY ACCREDITATIONS & CERTIFICATIONS Pennsylvania Department of Environmental Protection, Bureau of Laboratories 02-00538 NELAP Non-Potable Water and Solid & Hazardous Waste Accreditor: Accreditation ID: Scope: West Virginia Department of Environmental Protection, Division of Water and Waste Management 395 Non-Potable Water Accreditor: Accreditation ID: Scope: South Carolina Department of Health and Environmental Control, Office of Environmental Laboratory Certification 89009003 Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA) Accreditor: Accreditation ID: Scope: NELAP: New Jersey, Department of Environmental Protection PA026 Non-Potable Water; Solid and Chemical Materials Accreditor: Accreditation ID: Scope: NELAP: New York, Department of Health Wadsworth Center 11815 Non-Potable Water; Solid and Hazardous Waste Accreditor: Accreditation ID: Scope: State of Connecticut, Department of Public Health, Division of Environmental Health PH-0263 Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA) Accreditor: Accreditation ID: Scope: NELAP: Texas, Commission on Environmental Quality T104704453-09-TX Non-Potable Water Accreditor: Accreditation ID: Scope: State of New Hampshire 299409 Non-potable water Accreditor: Accreditation ID: Scope: State of Georgia Chapter 391-3-26 As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is accredited by the Pennsylvania Department of Environmental Protection Bureau of Laboratories under the National Environmental Laboratory Approval Program (NELAC). Accreditor: Accreditation ID: Scope: 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 3 of 24 SAMPLE SUMMARY Workorder: 22394 SCOTLAND CO. / 6000 Lab ID Sample ID Matrix Date Collected Date Received 223940001 MW1 Water 4/19/2017 13:55 4/21/2017 11:15 223940002 MW1 Bubble Strip 4/19/2017 13:55 4/21/2017 11:15 223940003 MW4 Water 4/19/2017 10:50 4/21/2017 11:15 223940004 MW4 Bubble Strip 4/19/2017 10:50 4/21/2017 11:15 223940005 MW6 Water 4/19/2017 09:50 4/21/2017 11:15 223940006 MW6 Bubble Strip 4/19/2017 09:50 4/21/2017 11:15 223940007 MW7 Water 4/19/2017 08:50 4/21/2017 11:15 223940008 MW7 Bubble Strip 4/19/2017 08:50 4/21/2017 11:15 223940009 MW9 Water 4/19/2017 12:30 4/21/2017 11:15 223940010 MW9 Bubble Strip 4/19/2017 12:30 4/21/2017 11:15 223940011 MW12 Water 4/19/2017 12:55 4/21/2017 11:15 223940012 MW13 Water 4/19/2017 11:55 4/21/2017 11:15 223940013 MW13 Bubble Strip 4/19/2017 11:55 4/21/2017 11:15 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 4 of 24 PROJECT SUMMARY Workorder: 22394 SCOTLAND CO. / 6000 Batch Comments Batch:EDON/3315 - Low Level Volatile Fatty Acids The percent recovery for the calibration verification was above laboratory control limits. Analytes Pyruvic and iso-Hexanoic acid. Results associated to samples may be biased high. 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 5 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW1 Matrix:Water Parameters Lab ID: Sample ID: 223940001 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 13:55 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.020J mg/l 0.20 1 4/25/2017 22:44 KB B0.0060 Acetic Acid 0.035J mg/l 0.10 1 4/25/2017 22:44 KB B0.0050 Propionic Acid 0.0020U mg/l 0.10 1 4/25/2017 22:44 KB0.0020 Butyric Acid 0.0060U mg/l 0.10 1 4/25/2017 22:44 KB0.0060 Pyruvic Acid 0.0020U mg/l 0.10 1 4/25/2017 22:44 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/25/2017 22:44 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/25/2017 22:44 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/25/2017 22:44 KB M10.0070 Hexanoic Acid 0.021J mg/l 0.20 1 4/25/2017 22:44 KB0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 6 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW1 Matrix:Bubble Strip Parameters Lab ID: Sample ID: 223940002 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 13:55 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 2.7 ug/l 0.050 1 4/27/2017 15:18 MM n0.0060 Ethane 0.0020U ug/l 0.010 1 4/27/2017 15:18 MM n0.0020 Ethene 0.0060U ug/l 0.010 1 4/27/2017 15:18 MM n0.0060 Hydrogen 2.1 nM 0.60 1 4/27/2017 15:18 MM n0.075 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 7 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW4 Matrix:Water Parameters Lab ID: Sample ID: 223940003 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 10:50 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.019J mg/l 0.20 1 4/26/2017 01:24 KB B0.0060 Acetic Acid 0.030J mg/l 0.10 1 4/26/2017 01:24 KB B0.0050 Propionic Acid 0.0024J mg/l 0.10 1 4/26/2017 01:24 KB0.0020 Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 01:24 KB0.0060 Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 01:24 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 01:24 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 01:24 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 01:24 KB M10.0070 Hexanoic Acid 0.019J mg/l 0.20 1 4/26/2017 01:24 KB0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 8 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW4 Matrix:Bubble Strip Parameters Lab ID: Sample ID: 223940004 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 10:50 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 3100 ug/l 0.050 1 4/27/2017 15:30 MM n0.0060 Ethane 0.024 ug/l 0.010 1 4/27/2017 15:30 MM n0.0020 Ethene 0.079 ug/l 0.010 1 4/27/2017 15:30 MM n0.0060 Hydrogen 1.6 nM 0.60 1 4/27/2017 15:30 MM n0.075 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 9 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW6 Matrix:Water Parameters Lab ID: Sample ID: 223940005 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 09:50 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.026J mg/l 0.20 1 4/26/2017 02:17 KB B0.0060 Acetic Acid 0.024J mg/l 0.10 1 4/26/2017 02:17 KB B0.0050 Propionic Acid 0.0020U mg/l 0.10 1 4/26/2017 02:17 KB0.0020 Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 02:17 KB0.0060 Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 02:17 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 02:17 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 02:17 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 02:17 KB M10.0070 Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 02:17 KB0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 10 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW6 Matrix:Bubble Strip Parameters Lab ID: Sample ID: 223940006 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 09:50 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 8200 ug/l 0.050 1 4/27/2017 15:43 MM n0.0060 Ethane 0.049 ug/l 0.010 1 4/27/2017 15:43 MM n0.0020 Ethene 0.40 ug/l 0.010 1 4/27/2017 15:43 MM n0.0060 Hydrogen 1.9 nM 0.60 1 4/27/2017 15:43 MM n0.075 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 11 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW7 Matrix:Water Parameters Lab ID: Sample ID: 223940007 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 08:50 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.035J mg/l 0.20 1 4/26/2017 03:10 KB B0.0060 Acetic Acid 0.053J mg/l 0.10 1 4/26/2017 03:10 KB B0.0050 Propionic Acid 0.0040J mg/l 0.10 1 4/26/2017 03:10 KB0.0020 Butyric Acid 0.0060J mg/l 0.10 1 4/26/2017 03:10 KB0.0060 Pyruvic Acid 0.0023J mg/l 0.10 1 4/26/2017 03:10 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 03:10 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 03:10 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 03:10 KB M10.0070 Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 03:10 KB0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 12 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW7 Matrix:Bubble Strip Parameters Lab ID: Sample ID: 223940008 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 08:50 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 6200 ug/l 0.050 1 4/27/2017 15:55 MM n0.0060 Ethane 0.25 ug/l 0.010 1 4/27/2017 15:55 MM n0.0020 Ethene 0.055 ug/l 0.010 1 4/27/2017 15:55 MM n0.0060 Hydrogen 1.8 nM 0.60 1 4/27/2017 15:55 MM n0.075 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 13 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW9 Matrix:Water Parameters Lab ID: Sample ID: 223940009 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 12:30 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.037J mg/l 0.20 1 4/26/2017 04:04 KB B0.0060 Acetic Acid 0.025J mg/l 0.10 1 4/26/2017 04:04 KB B0.0050 Propionic Acid 0.0031J mg/l 0.10 1 4/26/2017 04:04 KB0.0020 Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 04:04 KB0.0060 Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 04:04 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 04:04 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 04:04 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 04:04 KB M10.0070 Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 04:04 KB0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 14 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW9 Matrix:Bubble Strip Parameters Lab ID: Sample ID: 223940010 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 12:30 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 25 ug/l 0.050 1 4/27/2017 16:08 MM n0.0060 Ethane 0.0031J ug/l 0.010 1 4/27/2017 16:08 MM n0.0020 Ethene 0.0076J ug/l 0.010 1 4/27/2017 16:08 MM n0.0060 Hydrogen 1.6 nM 0.60 1 4/27/2017 16:08 MM n0.075 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 15 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW12 Matrix:Water Parameters Lab ID: Sample ID: 223940011 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 12:55 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.090J mg/l 0.20 1 4/26/2017 04:57 KB B0.0060 Acetic Acid 0.053J mg/l 0.10 1 4/26/2017 04:57 KB B0.0050 Propionic Acid 0.0026J mg/l 0.10 1 4/26/2017 04:57 KB0.0020 Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 04:57 KB0.0060 Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 04:57 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 04:57 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 04:57 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 04:57 KB M10.0070 Hexanoic Acid 0.022J mg/l 0.20 1 4/26/2017 04:57 KB0.0090 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 180 ug/l 0.50 1 4/28/2017 08:11 TD n0.027 Ethane 0.0070U ug/l 0.10 1 4/28/2017 08:11 TD n0.0070 Ethene 0.016J ug/l 0.10 1 4/28/2017 08:11 TD n0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 16 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW13 Matrix:Water Parameters Lab ID: Sample ID: 223940012 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 11:55 EDonors - PAES Analysis Desc: AM23G Analytical Method: AM23G Lactic Acid 0.041J mg/l 0.20 1 4/26/2017 05:50 KB B0.0060 Acetic Acid 0.024J mg/l 0.10 1 4/26/2017 05:50 KB B0.0050 Propionic Acid 0.0020U mg/l 0.10 1 4/26/2017 05:50 KB0.0020 Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 05:50 KB0.0060 Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 05:50 KB M10.0020 i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 05:50 KB0.015 Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 05:50 KB0.0030 i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 05:50 KB M10.0070 Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 05:50 KB0.0090 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 17 of 24 ANALYTICAL RESULTS Workorder: 22394 SCOTLAND CO. / 6000 4/21/2017 11:15 MW13 Matrix:Bubble Strip Parameters Lab ID: Sample ID: 223940013 Results Units PQL DF ByAnalyzedMDL Qualifiers Date Collected: Date Received: 4/19/2017 11:55 RISK - PAES Analysis Desc: AM20GAX Analytical Method: AM20GAX Methane 180 ug/l 0.050 1 4/27/2017 16:20 MM n0.0060 Ethane 0.037 ug/l 0.010 1 4/27/2017 16:20 MM n0.0020 Ethene 0.11 ug/l 0.010 1 4/27/2017 16:20 MM n0.0060 Hydrogen 1.4 nM 0.60 1 4/27/2017 16:20 MM n0.075 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 18 of 24 ANALYTICAL RESULTS QUALIFIERS Workorder: 22394 SCOTLAND CO. / 6000 DEFINITIONS/QUALIFIERS U J Indicates the compound was analyzed for, but not detected at or above the noted concentration. Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL). MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection. PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation. ND Not detected at or above reporting limit. DF Dilution Factor. S Surrogate. RPD Relative Percent Difference. % Rec Percent Recovery. The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n The analyte was detected in the associated blank.B The continuing calibration verification recovery was outside laboratory control limits.M1 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 19 of 24 QUALITY CONTROL DATA Workorder: 22394 SCOTLAND CO. / 6000 QC Batch: QC Batch Method: EDON/3315 AM23G Analysis Method:AM23G Associated Lab Samples:223940001, 223940003, 223940005, 223940007, 223940009, 223940011, 223940012 METHOD BLANK: 48399 Parameter Units Result Blank Limit Reporting Qualifiers EDonors Lactic Acid 0.010Jmg/l 0.0060 B Acetic Acid 0.0089Jmg/l 0.0050 B Propionic Acid 0.0020Umg/l 0.0020 Butyric Acid 0.0060Umg/l 0.0060 Pyruvic Acid 0.0020Umg/l 0.0020 M1 i-Pentanoic Acid 0.015Umg/l 0.015 Pentanoic Acid 0.0030Umg/l 0.0030 i-Hexanoic Acid 0.0070Umg/l 0.0070 M1 Hexanoic Acid 0.0090Umg/l 0.0090 LABORATORY CONTROL SAMPLE: Parameter Units Conc. Spike Result LCS Qualifiers LCS % Rec % Rec Limits 48400 EDonors Lactic Acid 2mg/l 2.0 B103 70-130 Acetic Acid 2mg/l 2.1 B107 70-130 Propionic Acid 2mg/l 2.1 107 70-130 Butyric Acid 2mg/l 2.1 105 70-130 Pyruvic Acid 2mg/l 2.3 M1115 70-130 i-Pentanoic Acid 2mg/l 2.1 105 70-130 Pentanoic Acid 2mg/l 2.0 101 70-130 i-Hexanoic Acid 2mg/l 2.0 M1100 70-130 Hexanoic Acid 2mg/l 1.8 90 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Units Conc. Spike Result MS 48401 48402 MSD Result % Rec MS MSD % Rec % Rec Limit RPD RPD Max QualifiersResult Original 223940001Original: EDonors Lactic Acid mg/l 2 2.1 103 70-130 B2.0 102 0.98 300.02 Acetic Acid mg/l 2 2.1 105 70-130 B2.1 106 0.95 300.035 Propionic Acid mg/l 2 2.1 106 70-1302.1 106 0 300 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 20 of 24 QUALITY CONTROL DATA Workorder: 22394 SCOTLAND CO. / 6000 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter Units Conc. Spike Result MS 48401 48402 MSD Result % Rec MS MSD % Rec % Rec Limit RPD RPD Max QualifiersResult Original 223940001Original: Butyric Acid mg/l 2 2.1 104 70-1302.1 105 0.96 300.0029 Pyruvic Acid mg/l 2 2.2 112 70-130 M12.2 112 0 300 i-Pentanoic Acid mg/l 2 2.1 105 70-1302.1 106 0.95 300 Pentanoic Acid mg/l 2 2.0 103 70-1302.1 104 0.97 300 i-Hexanoic Acid mg/l 2 2.3 115 70-130 M12.2 111 3.5 300 Hexanoic Acid mg/l 2 2.1 102 70-1302.1 104 1.9 300.021 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 21 of 24 QUALITY CONTROL DATA Workorder: 22394 SCOTLAND CO. / 6000 QC Batch: QC Batch Method: DISG/6073 AM20GAX Analysis Method:AM20GAX Associated Lab Samples:223940002, 223940004, 223940006, 223940008, 223940010, 223940013 METHOD BLANK: 48447 Parameter Units Result Blank Limit Reporting Qualifiers RISK Methane 0.0060Uug/l 0.0060 n Ethane 0.0020Uug/l 0.0020 n Ethene 0.0060Uug/l 0.0060 n METHOD BLANK: 48448 Parameter Units Result Blank Limit Reporting Qualifiers RISK Hydrogen 0.075UnM 0.075 n LABORATORY CONTROL SAMPLE & LCSD: Parameter Units Conc. Spike Result LCS 48449 48451 LCSD Result % Rec LCS LCSD % Rec % Rec Limit RPD RPD Max Qualifiers RISK Methane ug/l 8.1 8.4 104 80-120 n8.4 104 0 20 Ethane ug/l 6.4 6.4 101 80-120 n6.4 100 1 20 Ethene ug/l 16 16 100 80-120 n16 99 1 20 LABORATORY CONTROL SAMPLE & LCSD: Parameter Units Conc. Spike Result LCS 48450 48452 LCSD Result % Rec LCS LCSD % Rec % Rec Limit RPD RPD Max Qualifiers RISK Hydrogen nM 24 24 98 80-120 n23 96 2.1 20 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 22 of 24 QUALITY CONTROL DATA Workorder: 22394 SCOTLAND CO. / 6000 QC Batch: QC Batch Method: DISG/6074 AM20GAX Analysis Method:AM20GAX Associated Lab Samples:223940011 METHOD BLANK: 48453 Parameter Units Result Blank Limit Reporting Qualifiers RISK Methane 0.027Uug/l 0.027 n Ethane 0.0070Uug/l 0.0070 n Ethene 0.0090Uug/l 0.0090 n LABORATORY CONTROL SAMPLE & LCSD: Parameter Units Conc. Spike Result LCS 48455 48457 LCSD Result % Rec LCS LCSD % Rec % Rec Limit RPD RPD Max Qualifiers RISK Methane ug/l 750 830 111 80-120 n890 119 7 20 Ethane ug/l 38 40 104 80-120 n40 106 1.9 20 Ethene ug/l 35 37 105 80-120 n38 107 1.9 20 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 23 of 24 QUALITY CONTROL DATA QUALIFIERS Workorder: 22394 SCOTLAND CO. / 6000 QUALITY CONTROL PARAMETER QUALIFIERS The analyte was detected in the associated blank.B The continuing calibration verification recovery was outside laboratory control limits.M1 The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Pace Analytical Energy Services LLC CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, Report ID: 22394 - 918073 Page 24 of 24 QUALITY CONTROL DATA CROSS REFERENCE TABLE Workorder: 22394 SCOTLAND CO. / 6000 Lab ID Sample ID Prep Method Analysis MethodPrep Batch Batch Analysis 223940001 MW1 EDON/3315AM23G 223940003 MW4 EDON/3315AM23G 223940005 MW6 EDON/3315AM23G 223940007 MW7 EDON/3315AM23G 223940009 MW9 EDON/3315AM23G 223940011 MW12 EDON/3315AM23G 223940012 MW13 EDON/3315AM23G 223940002 MW1 DISG/6073AM20GAX 223940004 MW4 DISG/6073AM20GAX 223940006 MW6 DISG/6073AM20GAX 223940008 MW7 DISG/6073AM20GAX 223940010 MW9 DISG/6073AM20GAX 223940013 MW13 DISG/6073AM20GAX 223940011 MW12 DISG/6074AM20GAX 220 William Pitt Way Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 without the written consent of Pace Analytical Energy Services LLC. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF APPENDIX C Biochlor Models April 2017 Groundwater Monitoring Report Scotland County Landfill Solid Waste Permit No. 83-01 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. 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RATE 'LVSOD\HG&RPSRXQG PJGD\7LPH \U 7DUJHW/HYHOPJ/ 'LVSOD\HG0RGHO1R'HJUDGDWLRQ '&( 3OXPH0DVV2UGHURI0DJQLWXGH$FFXUDF\ 3OXPH0DVV,I1R'HJUDGDWLRQ (Kg) 3OXPH0DVV,I%LRWUDQVIRUPDWLRQ3URGXFWLRQ(Kg) 0DVV5HPRYHG(Kg) %LRWUDQVIRUPHG &KDQJHLQ0DVV5DWH &XUUHQW9ROXPHRI*URXQG:DWHULQ3OXPH &DQ W&DOFMGal )ORZ5DWHRI:DWHU7KURXJK6RXUFH$UHD MGD 3XPSLQJ5DWH (gpm) 3RUH9ROXPHV5HPRYHG3HU<U 3RUH9ROXPHVWR&OHDQ8S &OHDQ8S7LPH (yr) 5HWXUQWR,QSXW3ORW$OO'DWD 3ORW'DWD!7DUJHW 0DVV+(/3 6HH*DOORQ 6KRZ1R 6KRZ 7R&HQWHUOLQH ,I&DQ W&DOFPDNHPRGHODUHD ORQJHU IW &R Q F H Q W U D W L R Q P J / 'LVWDQFHIURP6RXUFHIW &RPSDUHWR3XPSDQG7UHDW VRXUFHWRHGJH 6HHDFUHIW DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF 6WDUW+HUH 3&( ',662/9('62/9(17&21&(175$7,216,13/80(7&( Transverse '&( Distance (ft) Distance from Source (ft)9& (7+ MASS ( ( ( ( ( ( ( ( ( ( ( RATE 'LVSOD\HG&RPSRXQG PJGD\7LPH \U 7DUJHW/HYHOPJ/ 'LVSOD\HG0RGHO1R'HJUDGDWLRQ 9& 3OXPH0DVV2UGHURI0DJQLWXGH$FFXUDF\ 3OXPH0DVV,I1R'HJUDGDWLRQ (Kg) 3OXPH0DVV,I%LRWUDQVIRUPDWLRQ3URGXFWLRQ(Kg) 0DVV5HPRYHG(Kg) %LRWUDQVIRUPHG &KDQJHLQ0DVV5DWH &XUUHQW9ROXPHRI*URXQG:DWHULQ3OXPH &DQ W&DOFMGal )ORZ5DWHRI:DWHU7KURXJK6RXUFH$UHD MGD 3XPSLQJ5DWH (gpm) 3RUH9ROXPHV5HPRYHG3HU<U 3RUH9ROXPHVWR&OHDQ8S &OHDQ8S7LPH (yr) 5HWXUQWR,QSXW3ORW$OO'DWD 3ORW'DWD!7DUJHW 0DVV+(/3 6HH*DOORQ 6KRZ1R 6KRZ 7R&HQWHUOLQH ,I&DQ W&DOFPDNHPRGHODUHD ORQJHU IW &R Q F H Q W U D W L R Q P J / 'LVWDQFHIURP6RXUFHIW &RPSDUHWR3XPSDQG7UHDW VRXUFHWRHGJH 6HHDFUHIW DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF 6WDUW+HUH 3&( ',662/9('62/9(17&21&(175$7,216,13/80(7&( Transverse '&( Distance (ft) Distance from Source (ft)9& (7+ MASS ( ( ( ( ( ( ( ( ( ( ( RATE 'LVSOD\HG&RPSRXQG PJGD\7LPH \U 7DUJHW/HYHO PJ/ 'LVSOD\HG0RGHO1R'HJUDGDWLRQ (7+ 3OXPH0DVV2UGHURI0DJQLWXGH$FFXUDF\ 3OXPH0DVV,I1R'HJUDGDWLRQ (Kg) 3OXPH0DVV,I%LRWUDQVIRUPDWLRQ3URGXFWLRQ(Kg) 0DVV5HPRYHG(Kg) %LRWUDQVIRUPHG &KDQJHLQ0DVV5DWH &XUUHQW9ROXPHRI*URXQG:DWHULQ3OXPH MGal )ORZ5DWHRI:DWHU7KURXJK6RXUFH$UHD MGD 3XPSLQJ5DWH (gpm) 3RUH9ROXPHV5HPRYHG3HU<U ',9 3RUH9ROXPHVWR&OHDQ8S &OHDQ8S7LPH (yr) 5HWXUQWR,QSXW3ORW$OO'DWD 3ORW'DWD!7DUJHW 0DVV+(/3 6HH*DOORQ 6KRZ1R 6KRZ 7R&HQWHUOLQH ,I&DQ W&DOFPDNHPRGHODUHD ORQJHU IW &R Q F H Q W U D W L R Q P J / 'LVWDQFHIURP6RXUFHIW &RPSDUHWR3XPSDQG7UHDW VRXUFHWRHGJH 6HHDFUHIW DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF APPENDIX D Time vs. Concentration Graphs April 2017 Groundwater Monitoring Reports Scotland County Landfill Solid Waste Permit No. 83-01 DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF This page intentionally left blank. DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ ϱ ϭϬ ϭϱ ϮϬ Ϯϱ ϯϬ ϯϱ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ ϭ͕ϭͲŝĐŚůŽƌŽĞƚŚĂŶĞ DtͲϲ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ Ϯ ϰ ϲ ϴ ϭϬ ϭϮ ϭϰ ϭϲ ϭϴ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ ϭ͕ϰͲŝĐŚůŽƌŽďĞŶǌĞŶĞ DtͲϮ DtͲϲ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ ϱ ϭϬ ϭϱ ϮϬ Ϯϱ ϯϬ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ ƌƐĞŶŝĐ DtͲϰ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ ϭ Ϯ ϯ ϰ ϱ ϲ ϳ ϴ ϵ ϭϬ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ ĞŶǌĞŶĞ DtͲϭϯ DtͲϮ DtͲϯ DtͲϲ DtͲϳ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ͘ϬϬ Ϭ͘Ϭϱ Ϭ͘ϭϬ Ϭ͘ϭϱ Ϭ͘ϮϬ Ϭ͘Ϯϱ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ ŝĞůĚƌŝŶ DtͲϳ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ ϱϬ͕ϬϬϬ ϭϬϬ͕ϬϬϬ ϭϱϬ͕ϬϬϬ ϮϬϬ͕ϬϬϬ ϮϱϬ͕ϬϬϬ ϯϬϬ͕ϬϬϬ ϯϱϬ͕ϬϬϬ ϰϬϬ͕ϬϬϬ ϰϱϬ͕ϬϬϬ ϱϬϬ͕ϬϬϬ ϳͬϲͬϮϬϬϵ ϭϭͬϭϴͬϮϬϭϬ ϰͬϭͬϮϬϭϮ ϴͬϭϰͬϮϬϭϯ ϭϮͬϮϳͬϮϬϭϰ ϱͬϭϬͬϮϬϭϲ ϵͬϮϮͬϮϬϭϳ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ /ƌŽŶ DtͲϭ DtͲϭϮ DtͲϭϯ DtͲϰ DtͲϲ DtͲϳ DtͲϵ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ ϮϬ ϰϬ ϲϬ ϴϬ ϭϬϬ ϭϮϬ ϭϰϬ ϭϲϬ ϭϴϬ ϮϬϬ ϮͬϮϮͬϮϬϬϴ ϳͬϲͬϮϬϬϵ ϭϭͬϭϴͬϮϬϭϬ ϰͬϭͬϮϬϭϮ ϴͬϭϰͬϮϬϭϯ ϭϮͬϮϳͬϮϬϭϰ ϱͬϭϬͬϮϬϭϲ ϵͬϮϮͬϮϬϭϳ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ sĂŶĂĚŝƵŵ DtͲϭϮ 'tW DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF Ϭ ϭϬ ϮϬ ϯϬ ϰϬ ϱϬ ϲϬ ϳϬ Ž Ŷ Đ Ğ Ŷ ƚ ƌ Ă ƚ ŝ Ž Ŷ ; Ƶ Ő ͬ ů Ϳ ĂƚĞ sŝŶǇůŚůŽƌŝĚĞ DtͲϭϯ DtͲϮ DtͲϯ DtͲϰ DtͲϲ Ϯ> DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF