8301_ScotlandCDoverMSW_WQMonitoring_April2017_DIN28108_20170630

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April 2017 Groundwater Monitoring Report
Scotland County Landfill
Laurinburg, North Carolina
NC Solid Waste Permit # 83-01
Prepared for:
Scotland County Public Works Department
507 W. Covington Street
Laurinburg, North Carolina 28352
June 2017
Prepared by:
© 2017 Smith Gardner, Inc.
This document is intended for the sole use of the client for which it was prepared and
for the purpose agreed on by the client and Smith Gardner, Inc.
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April 2017 Groundwater Monitoring Report

Scotland County Landfill
NC Solid Waste Permit #83-01

Prepared For:
Scotland County Public Works Department
Laurinburg, North Carolina 28352

S+G Project No. SCOT-2

Madeline German, P.G.
Project Geologist

Joan Smyth, P.G.
Senior Hydrogeologist

June 2017

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Scotland County Landfill April 2017 Groundwater Monitoring Report
June 2017 Table of Contents Page i
Scotland County Landfill
Solid Waste Permit No. 83-01

April 2017 Water Quality Monitoring Report

Table of Contents
Page

1.0INTRODUCTION ......................................................................................................... 2
2.0SITE GEOLOGY ........................................................................................................... 2
3.0SAMPLING LOCATIONS ............................................................................................. 2
4.0SAMPLING PROCEDURES ......................................................................................... 3
5.0FIELD & LABORATORY RESULTS .............................................................................. 3
5.1Laboratory Analysis ................................................................................................... 3
5.2Field Results .............................................................................................................. 4
5.3Inorganic Constituent Laboratory Results ............................................................... 4
5.4Organic Constituent Laboratory Results .................................................................. 5
5.5Surface Water Analytical Results ............................................................................. 5
6.0CORRECTIVE MEASURES UPDATE ............................................................................ 5
7.0STATISTICAL ANALYSIS AND RESULTS .................................................................... 6
7.1Statistical Analysis .................................................................................................... 6
7.2Statistical Results ..................................................................................................... 6
8.0GROUNDWATER CHARACTERIZATION ...................................................................... 6
9.0CONCLUSIONS .......................................................................................................... 7

FIGURES
Figure 1 Groundwater Potentiometric Surface Map
Figure 2 Total VOC Isoconcentration Map

TABLES
Table 1 Groundwater Elevations
Table 2 Field Parameter Results
Table 3 Detected Inorganic Constituents
Table 4 Detected Organic Constituents
Table 5 Indicator Parameters
Table 6 Statistical Analysis Summary
Table 7 Conductivity and Velocity Calculations

APPENDICES
Appendix A Monitoring Well Information
Appendix B Laboratory Analytical Report
Appendix C Biochlor Models
Appendix D Time vs. Concentration Graphs
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Scotland County Landfill April 2017 Groundwater Monitoring Report
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1.0INTRODUCTION
The Scotland County Landfill, operating under Solid Waste Permit #83-01, is required to submit
semi-annual groundwater monitoring reports (15A NCAC 13B.0544) for assessment monitoring.
This report presents the results from the sampling conducted on April 18-19, 2017.

The Scotland County Landfill contains two disposal areas. Phase I is located north of Old
Maxton Road. Phases II and III are located south of Old Maxton Road. C&D waste is currently
accepted over the closed Phases II and III. Municipal Solid Waste (MSW) is presently
transferred off-site to a lined landfill in another county. The MSW landfill was closed per Solid
Waste Regulations and the certification report1 was submitted to the Solid Waste Section (SWS)
in August 1999. In 2007 the Scotland County Landfill was assessed to determine if groundwater
issues would require a remediation plan. The Corrective Action Plan2 was approved on
February 3, 2009. SSection 8.0 of this report is an update regarding the current corrective action
situation for this facility.

This report includes a field procedure summary, laboratory and statistical analyses,
groundwater characterization, summary tables, graphs and laboratory analytical reports.
2.0SITE GEOLOGY
According to the 1985 Geologic Map of North Carolina, the Scotland County Landfill is located in
an area underlain by the Middendorf Formation. The Geology of the Carolinas3 describes the
Middendorf Formation as deeply weathered at its type locality which has caused considerable
difficulty in identification. In North Carolina the Middendorf is described as interbedded sands
and clays with laterally discontinuous beds and common cross-bedding. Sandstone is the
dominant lithology with the basal portion being conglomeritic with quartz and white kaolin clay
clasts; believed to have been deposited in a fluvial upper delta plain environment.
3.0SAMPLING LOCATIONS
The groundwater monitoring network consists of twelve wells (MW-1 through MW-9 and MW-11
through MW-13) positioned around the landfill perimeter (FFigure 1). MW-2 and MW-11 are only
sampled during the spring event as approved in the March 2012 Revised Corrective Action
Update4. MW-1 and MW-8 serve as the background wells for this site. Two surface water
sampling points are located up and downstream of the landfill on Shoe Heel Creek. An

1 Construction Quality Assurance Report, Scotland County Landfill Phase III Closure, G.N. Richardson & Associates,
Inc. August 1999.
2 Corrective Action Plan, Scotland County Landfill, Richardson Smith Gardner and Associates, Approved
February 2009.
3 Horton, J. Wright, and Zullo, Victor, A., The Geology of the Carolinas, University of Tennessee Press, 1991.
4 Revised Corrective Action Update, Scotland County Landfill. Richardson Smith Gardner and Associates.
March 26, 2012.
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equipment blank (EB) and trip blank (TB) were also analyzed for quality control purposes. Well
depths range from 14.5 to 40 feet below grade. Available boring logs, presented in AAppendix A,
indicate wells were installed in varying amounts of sand, silt and clay. Well construction details
are provided in TTable 1.
4.0SAMPLING PROCEDURES
Sampling procedures followed the protocols set forth in the site’s approved Water Quality
Monitoring Plan2 and the North Carolina Water Quality Monitoring Guidance Document for Solid
Waste Facilities (North Carolina Department of Environment and Natural Resources, Division of
Waste Management). Each well was gauged to determine groundwater depth and then purged
three to five well volumes or until dry. Water table elevations and are included in TTable 1.

Samples were collected in laboratory prepared containers for the specified analytical
procedures. Sampling equipment, was brought to the site in sterile condition from the
manufacturer or was cleaned in the laboratory and transported to the site in a condition to avoid
potential contamination. Groundwater samples were properly preserved, placed on ice and
transported to the laboratory facility within the specified hold times for analysis.
5.0FIELD & LABORATORY RESULTS
Analytical results were compared to the NC DWM Solid Waste Section Quantitation Limits
(SWSLs), 15A NCAC 2L.0200 (2LStandard) and Federal Maximum Contaminant Limits (MCL).
Surface water results were compared with the NCAC 2B Standard for Class C waters (2B
Standard).

Constituents detected between the Method Detection Limit (MDL) and SWSL are a non-
quantifiable value defined by the laboratory as “J” values. Values reported below the MDL are
considered non-detect.

The laboratory analytical report is included as AAppendix B.
5.1Laboratory Analysis
Samples were collected and analyzed by Environment 1, Inc., Greenville, NC, a North
Carolina certified laboratory (NC Wastewater ID #10). Laboratory analysis for sampled
locations included:

xmetals plus mercury
xAppendix II volatile organic compounds (VOCs)
xtetrahydrofuran.

Select wells were also analyzed for:
xPesticides & PCBs
xsemi-volatile organics
xacid fraction compounds
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Monitored Natural Attenuation (MNA) sampling locations were also analyzed for:

xbiochemical oxygen demand
(BOD)
xchemical oxygen demand
(COD)
xnitrate nitrogen
xtotal organic carbon (TOC)
xtotal alkalinity
xiron
xchloride
xsulfate
xsulfide
xcarbon dioxide

MNA compounds analyzed by Pace Analytical Energy Services, LLC. (220 William Pitt
Way, Pittsburg, PA 15238) included:
xdissolved methane
xhydrogen
xethane
xethane
xvolatile fatty acids

Analysis for these constituents was performed via the EPA approved methods identified
in the laboratory report.
5.2Field Results
Field parameters pH, conductivity, temperature, turbidity, dissolved oxygen and oxygen
reduction potential (ORP) were collected by Environment 1; data is presented in TTable 2.
April 2017 data is generally consistent with previously recorded field measurements at
the site. Turbidity concentrations in MW-2, MW-7 and MW-12 were reported at levels
over 100 NTUs.
5.3Inorganic Constituent Laboratory Results
The inorganic constituent Arsenic was detected at its 2L Standard in the sample
collected from MW-4 this event.

Iron was detected above its 2L Standard in samples (MW-1, MW-6, MW-7, MW-9, MW-12
and MW-13) collected during this event.

Vanadium (MW-12) was the only inorganic constituent detected above its GWP Standard
for this event.

Elevated turbidity values likely contributed to the elevated inorganic detections this
event. The influence of turbidity on inorganic results in general, and these constituents
in particular, at this site was characterized in the Inorganic Constituent Alternate Source
Demonstration Report5. This report summarized the results of both total and dissolved
analysis samples collected during the fall 2016 monitoring event. In particular, the

5 Smith Gardner, Inc., Inorganic Constituent Alternate Source Demonstration Report, Scotland County Landfill Facility, April 2017.
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constituents detected above the groundwater standards were found to be naturally
occurring with total concentrations that were biased high by turbidity in the samples.

Most inorganic constituents were non-quantifiable “J-values” or reported below the
MDL. Inorganic detections are presented on TTable 3.
5.4Organic Constituent Laboratory Results
Five organic constituents were detected above their 2L Standards:

x1,1-Dichloroethane (MW-6),
x1,4-Dichorobenzene (Mw-2, MW-6),
xBenzene(MW-2, MW-3, MW-6,MW-7 and MW-13),
xDieldrin (MW-7)
xVinyl chloride (MW-3, MW-4, MW-6 and MW-13).

Tetrahydrofuran was detected in the samples collected from MW-2 and MW-13 this
event however; standards have not been established for this parameter.

Organic detections are presented on TTable 4. Additionally, a total volatile organic
compound (VOC) isopach map is presented as FFigure 2. This map shows where VOC
concentrations have been detected around the site for this sampling event.
5.5Surface Water Analytical Results
No inorganic or organic constituents were reported above the 2B Standard in samples
collected this event.
6.0CORRECTIVE MEASURES UPDATE
Scotland County is currently operating under a Corrective Action Plan (CAP)6 approved February
3, 2009, and a Revised Corrective Action Update letter7 to Brian Wootton at NCDENR SWS
submitted on March 26, 2012. Adjustments to the MNA parameters were implemented starting
with the spring 2012 sampling event based on verbal approval from NCDENR, including reduced
sampling parameters, frequency and locations.

This event is a third year event therefore samples from select locations were analyzed for the
full suite of MNA indicator parameters. Laboratory results indicate methanogenic processes
continue to be present on site, and natural attenuation is occurring. Results are summarized in
Table 5.

6 Corrective Action Plan, Scotland County Landfill, Richardson Smith Gardner and Associates, Inc. January 2009,
approved February 2009.
7 Letter from Joan Smyth of RSG to Brian Wootton of NCDENR dated March 26, 2012.
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Scotland County Landfill April 2017 Groundwater Monitoring Report
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Biochlor is an EPA screening tool, designed to simulate natural attenuation of chlorinated
solvents. For this event biochlor was run on wells MW-4, MW-6, MW-12 and MW-13. Models
indicate a slight decrease in parent compounds as the chlorinated solvents attenuate. Results
are presented in AAppendix C.
7.0STATISTICAL ANALYSIS AND RESULTS
7.1Statistical Analysis
Smith Gardner, Inc. (S+G) reviewed the laboratory data from this event to evaluate
trends, examine major site changes and establish statistical significance while
considering differences between up and down gradient wells. Data entry and analysis
was performed using the Chempoint and Chemstat statistical software package
developed specifically for RCRA Subtitle D sites (Starpoint Software, Cincinnati, OH).
Chemstat follows EPA and DWM protocols for approved statistical analysis methods for
groundwater data.

The data from this event was added to our existing site database, reviewed to evaluate
the most appropriate analysis methods and checked for outliers and erroneous results.
Initial analysis to determine noteworthy changes or data trends involved basic data
review and construction of a time-concentration graph for specific parameters (included
in AAppendix D). A statistical analysis summary is presented as TTable 6.
7.2Statistical Results
Statistical analysis was performed for arsenic, iron and vanadium for reported total
metals concentrations at or above their 2L or GWP Standards this event. Statistical
analysis was not performed on constituents detected in background wells. Wilcoxon
Rand Individual Well Test (Intra-well) was completed for iron. Parametric Prediction
Limit Test (Inter-well) was completed for arsenic and vanadium. No concentrations
were determined to be statistically significant this event.
8.0GROUNDWATER CHARACTERIZATION
A potentiometric surface map was prepared from groundwater elevations for this sampling
event. In general, groundwater is flowing east toward Shoe Heel Creek Swamp. This is
consistent with groundwater flow patterns previously reported for the site. The potentiometric
surface map is attached as FFigure 1.

Groundwater flow velocities were calculated for monitoring wells MW-1 through MW-8 using
the equation:
V = Ki/n
Where: K = hydraulic conductivity
i = groundwater gradient
n = porosity

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Groundwater flow velocities ranged from 0.354 ft/day (MW-8) to 1.444 ft/day (MW-5), and
averaged 0.749 ft/day. Calculated flow velocities are presented in TTable 7.
9.0CONCLUSIONS
Laboratory results indicate that water quality at the Scotland County Landfill is generally
consistent with reported historical detections. Groundwater analysis indicates that inorganic
parameter concentrations were likely influenced by high turbidity of naturally occurring metals
in samples collected this event. Flow direction and gradient remain consistent with reported
historical observations. Natural attenuation continues to degrade chlorinated solvents on site.
Overall total VOC concentrations have decreased since the last biochlor model. All four
modeled locations have adequate to strong evidence for anaerobic biodegradation according to
the Natural Attenuation Screening Protocol. The facility will continue semi-annual monitoring
with the next event that will include full MNA analysis, scheduled for October 2017.

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FIGURES

April 2017 Groundwater Monitoring Report
Scotland County Landfill
Solid Waste Permit No. 83-01
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TABLES

April 2017 Groundwater Monitoring Report
Scotland County Landfill
Solid Waste Permit No. 83-01
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Table 1
Groundwater Elevations
Scotland County Landfill
April 18-19, 2017
By:MG
Date: 6/12/2017
Well
Well
Installation
Date
Latitude Longitude
Well
Diameter
(inches)
Total
Well
Depth
(ft bgs)
Ground
Surface
Elevation
(ft amsl)
TOC
Elevation
(ft amsl)
Depth to
Water (ft
bgs)
Water
Table
Elevation
(ft bgs)
Screen
Interval
(feet bgs)
Screen
Geology
MW-1 11/15/1993 34.72284 79.38451 2.0 21.0 190.35 192.83 6.88 185.95 5-20 sand with clay
MW-2 11/18/1993 34.72577 79.38255 2.0 30.0 195.85 197.62 20.41 177.21 14-29 sand
MW-3 11/19/1993 34.72696 79.37951 2.0 30.0 190.41 192.92 22.83 170.09 14-29 clayey sand
MW-4 11/22/1993 34.72575 79.37836 2.0 34.0 190.12 191.11 23.37 167.74 18-33 clayey sand
MW-5 11/17/1993 34.72290 79.38181 2.0 28.0 190.29 193.69 15.12 178.57 12-27 clayey sand
MW-6 11/22/1993 34.72599 79.37951 2.0 40.0 180.27 186.44 16.04 170.40 19-39 sand and clay
MW-7 11/23/1993 34.72821 79.38067 2.0 30.0 191.99 194.53 18.12 176.41 14-29 sandy clay
MW-8 11/23/1993 34.72479 79.38627 2.0 21.0 193.75 196.05 11.28 184.77 5-20 sand
MW-9 9/17/1990 34.72625 79.37735 4.0 22.0 169.83 171.22 7.27 163.95 NA clay
MW-10 NA 34.72227 79.38415 NA NA 192.00 193.31 7.70 185.61 NA NA
MW-11 4/24/1981 34.72857 79.37891 4.0 40.0 177.13 179.82 17.18 162.64 30-40 sand
MW-12* 8/27/2009 34.72760 79.37871 2.0 35.0 187.17 187.00 27.55 159.45 25-35 silty sand
MW-13* 8/27/2009 34.72644 79.37724 2.0 14.5 162.00 162.00 3.30 158.70 4.5-14.5 silty sand
Note:
NA = not available
bgs = below ground surface
amsl = above mean sea level
Water level data collected by Environment 1 personnel.
Available well logs provided in AAppendix A
*GSE and TOC are approximate for MW-12 and MW-13
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Table 2
Field Parameter Results
Scotland County Landfill
April 18-19, 2017
By:MG
Date: 6/12/2017
Well pH (Std
Units)
Specific
Conductivity
(umhos/cm)
Temperature
(Celsius)
Turbidity
(NTU)
DO
(mg/l)
ORP
(mV)
MW-1 5.5 114 19 16 6140 63
MW-2 5.8 538 19 320 200 84
MW-3 5.8 251 19 17 180 113
MW-4 5.8 188 18 70 410 58
MW-5 6.4 498 16 8.2 2860 86
MW-6 5.5 335 17 5.6 120 77
MW-7 6.2 1013 17 400 1100 35
MW-8 4.6 103 19 13 5940 101
MW-9 5.4 250 17 55 2190 95
MW-11 4.8 144 18 8.1 3620 180
MW-12 6.0 948 20 290 670 27
MW-13 5.6 366 17 55 170 70
Upstream 5.8 62 19 NA NA NA
Downstream 6.3 123 20 NA NA NA
Note:
NA = Not Analyzed
Field measurements collected by Environment 1, Inc.
personnel; from reports dated: 5/22/2017 & 6/1/2017, Client
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Table 3
Detected Inorganic Constituents
Scotland County Landfill
April 18-19, 2017
By: MG
Date: 6/13/2017
Parameter MDL SWSL
2L /
GWP*MCL 2B MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-11 MW-12 MW-13 Upstream Downstream
Antimony 0.06 6 1 *6 640 0.07 J 0.13 J 0.06 J <0.06 0.11 J <0.06 <0.06 <0.06 0.07 J <0.06 0.1 J <0.06 <0.06 <0.06
Arsenic 0.07 10 10 10 10 0.2 J 6.4 J 1.9 J 110 1.1 J 3.1 J 4.4 J <0.07 0.24 J 0.09 J 6.6 J 1.3 J 0.64 J 0.32 J
Barium 0.07 100 700 2000 200000 12.4 J 30.1 J 36.1 J 18.6 J 25.4 J 30.6 J 66.6 J 53.2 J 17 J 27.3 J 12.7 J 40.8 J 16.6 J 13.3 J
Beryllium 0.07 1 4 *4 6.5 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 0.14 J 0.18 J <0.07 <0.07 <0.07
Cadmium 0.08 1 2 5 2 0.08 J 0.16 J 0.28 J 0.12 J 0.13 J 0.09 J 0.13 J 0.59 J 0.25 J <0.08 0.52 J 0.12 J <0.08 <0.08
Cobalt 0.24 10 1 *NE 4 0.38 J 1.7 J 0.65 J <0.24 1.3 J <0.24 0.31 J 1.6 J <0.24 3.5 J <0.24 0.81 J 0.95 J 0.51 J
Total Chromium 0.08 10 10 100 50 1 J 0.69 J 0.28 J 0.54 J 0.18 J <0.08 <0.08 0.15 J <0.08 4 J 9.6 J 0.41 J 0.78 J 0.31 J
Copper 0.09 10 1000 1300 7 0.55 J 3.1 J 4.4 J 0.83 J 5.8 J 0.29 J 11 1.6 J 0.69 J 2.2 J 2.9 J 1.5 J 0.65 J 0.94 J
Iron 13.27 300 300 300 1000 9972 NA NA 333426 NA 227552 87929 NA 111163 NA 335037 29610 NA NA
Iron (dissolved) 13.27 300 300 300 1000 NA NA NA NA NA NA NA NA 186 J NA 228358 20637 NA NA
Lead 0.08 10 15 15 25 1.3 J 1.7 J 1.6 J 0.97 J 1.1 J 0.13 J 0.85 J 1.8 J 0.89 J 7.3 J 4.5 J 1.6 J 0.79 J 1.1 J
Mercury 0.07 0.2 1 2 0.012 <0.07 0.16 J <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 <0.07 0.41 <0.07 2.34 NA NA
Nickel 0.08 50 100 NE 88 0.69 J 1.2 J 1.4 J 0.42 J 1.7 J 0.54 J 1 J 1.7 J 0.68 J 1.2 J 0.84 J 0.61 J 1.5 J 0.98 J
Selenium 0.51 10 20 50 5 <0.51 0.63 J <0.51 <0.51 0.69 J <0.51 0.52 J <0.51 <0.51 <0.51 1.9 J 0.53 J <0.51 <0.51
Thallium 0.08 6 0.28* 2 0.47 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 0.12 J <0.08 <0.08 0.09 J <0.08 <0.08
Tin 0.13 100 2000* NE 800 NA 0.26 J 1.6 J <0.13 NA <0.13 0.21 J NA <0.13 0.44 J <0.13 0.29 J NA NA
Vanadium 0.24 25 0.3 *NE NE 2.9 J 4.6 J 1 J 6.2 J 1.4 J 3.1 J 0.62 J 0.53 J 0.91 J 0.28 J 227 3.3 J 0.57 J 0.49 J
Zinc 0.66 10 1000 5000 50 1.7 J 102 14 2.7 J 4.4 J 2.9 J 8.8 J 66 1.3 J 9 J 6.6 J 0.72 J 6 J 8.9 J
Note:
MDL -Method Detection Limit Table units are presented in ug/l.
SWSL -Solid Waste Section Quantitation Limits Lab analysis by Environment 1, Inc. reports dated 5/22/2017 & 6/1/2017, Client ID#6000.
2L -Groundwater Standards (15A NCAC 2L 0200)
GWP -Groundwater Protection Standards (noted by *)
MCL - Federal Maximum Contaminant Level
2B -NCAC 2B Standard for Class C waters
BOLD -Detection above 2L or GWP Standard
J-Laboratory defined concentration, between MDL and SWSL
< MDL -Not detected at or above MDL
NE -Standard Not Established
NA -Parameter Not Analyzed
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Table 4
Detected Organic Constituents
Scotland County Landfill
April 18-19, 2017
By: MG
Date: 6/12/2017
Parameter MDL SWSL 2L/GWP* MCL 2B MW-2 MW-3 MW-4 MW-6 MW-7 MW-9 MW-13 Upstream
1,1-Dichloroethane 0.20 5 6 NE 100 6.4 1.7 J <0.2 77.9 0.3 J 0.7 J 4.2 J <0.2
1,1-Dichloroethene 0.17 5 7 100 1500 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 0.2 J <0.17
1,2-Dichloropropane 0.21 1 0.6 5 15 0.6 J <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
1,4-Dichlorobenzene 0.39 1 6 75 100 110.4 1 <0.39 113.1 1 <0.39 2.7 <0.39
Benzene 0.24 1 1 5 51 44.6 1 <0.24 55.1 3.5 <0.24 11.3 <0.24
Chlorobenzene 0.30 3 50 100 140 2.4 J <0.3 <0.3 0.6 J 3.1 <0.3 1.1 J <0.3
Chloroethane 0.48 10 3000 NE NE <0.48 <0.48 <0.48 0.6 J <0.48 <0.48 <0.48 <0.48
Cis-1,2-Dichloroethene 0.25 5 70 70 720 10.5 <0.25 <0.25 0.3 J <0.25 <0.25 4.2 J <0.25
Dichlorodifluoromethane 0.51 5 1000 NE NE <0.51 <0.51 <0.51 1.3 J <0.51 <0.51 <0.51 NA
Dieldrin 0.04 0.075 0.002 NE NE <0.042 <0.042 <0.042 <0.042 00.0927 <0.042 <0.042 NA
Ethylbenzene 0.21 1 600 700 97 3.2 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21
Tetrachloroethene 0.17 1 0.7 5 3.3 0.5 J <0.17 <0.17 <0.17 <0.17 <0.17 <0.17 <0.17
Tetrahydrofuran 0.39 NE NE NE NE 6.4 <0.39 <0.39 <0.39 0.7 J <0.39 1.7 NA
Toluene 0.23 1 600 1000 11 0.3 J 0.3 J <0.23 <0.23 <0.23 <0.23 <0.23 0.8 J
Trichloroethene 0.23 1 3 5 30 1.3 <0.23 <0.23 <0.23 <0.23 <0.23 0.7 J <0.23
Vinyl Chloride 0.630 1 0.03 2 2.4 110.7 2.6 1.4 16.5 <0.63 <0.63 44.8 <0.63
Xylenes 0.68 5 500 10000 670 1.3 J <0.68 <0.68 <0.68 <0.68 <0.68 <0.68 <0.68
Note:
MDL - Method Detection Limit Table units are presented in ug/l.
SWSL - Solid Waste Section Quantitation Limits
2L - Groundwater Standards (15A NCAC 2L 0200)
GWP -Groundwater Protection Standards (noted by *)
MCL - Federal Maximum Contaminant Level
BOLD - Detection above 2L or GWP Standard
J - Laboratory defined concentration between MDL and SWSL
< MDL - Not detected at or above MDL
NE - Standard Not Established
NA - Parameter Not Analyzed
Lab data analysis by Environment 1, Inc.
reports dated 5/22/2017 & 6/1/2017, Client
H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\24. Scotland 4-17\4-17-scot_gw_tables.xlsx
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Table 5
Indicator Parameters
Scotland County Landfill
April 18-19, 2017
By: MG
Date: 6/13/2017
Parameter (units)MDL MW-1 MW-2 MW-3 MW-4 MW-6 MW-7 MW-9 MW-12 MW-13
BOD (mg/l)2 <2 NA NA <2 <2 6.2 <2 5.8 <2
COD (mg/l)0.84 22 NA NA 25 28 43 27 43 26
Nitrate Nitrogen (mg/l)0.003 1.95 J NA NA <0.003 <0.003 <0.003 0.32 J <0.84 <0.84
Total Organic Carbon (mg/l)0.12 1.06 NA NA 1.78 4.04 5.95 2.62 4.64 2.88
Total Alkalinity (mg CaCO3/l)1 3 NA NA 55 99 391 6 228 55
Chloride (mg/l)5 16 NA NA 8 18 6 13 23 32
Sulfate (mg/l)5 18.3 J NA NA 13.8 J 23.8 J 9.6 J 70.2 J 128 J 58.7 J
Sulfide (ug/l)100 <100 154 J 220 J <100 105 J <100 <100 <100 <100
Dissolved Oxygen (mg/l)0.1 6.14 0.2 0.18 0.41 0.12 1.1 2.19 0.67 0.17
Carbon Dioxide (mg/l)1 19 NA NA 212 365 484 85 380 197
ORP (MV)NE 63 84 113 58 77 35 95 27 70
Lactic Acid (mg/l)0.006 0.02 J NA NA 0.019 J 0.026 J 0.035 J 0.037 J 0.09 J 0.041 J
Acetic Acid (mg/l)0.005 0.035J NA NA 0.03 J 0.024 J 0.053 J 0.025 J 0.053 J 0.024 J
Propionic Acid (mg/l)0.002 <0.002 NA NA 0.0024 J <0.002 0.004 J 0.031 J 0.0026 J <0.002
Butyric Aid (mg/l) 0.006 <0.006 NA NA <0.006 <0.006 0.006 J <0.006 <0.006 <0.006
Pyruvic Acid (mg/l) 0.002 <0.002 NA NA <0.002 <0.002 0.0023 J <0.002 <0.002 <0.002
Hexanoic Acid (mg/l)0.009 0.021 J NA NA 0.019 J <0.009 <0.009 <0.009 0.022 J <0.009
Methane (Max Dissolved) (ug/l)0.006 2.7 NA NA 3100 8200 6200 25 180 180
Ethane (ug/l)0.002 <0.002 NA NA 0.024 0.049 0.25 0.0031 J <0.002 0.037
Ethene (ug/l)0.006 <0.006 NA NA 0.079 0.4 0.055 0.0076 J 0.16 J 0.11
Hydrogen (nM)0.075 2.1 NA NA 1.6 1.9 1.8 1.6 NA 1.4
Note:
J = Laboratory defined as between MDL and SWSL limit OR between the MDL and PQL (Practical Quantitation Limit).
Non-detects are presented as <MDL value
NA = Parameter Not Analyzed
Lab data analysis by Environment 1, Inc. reports dated 5/22/2017 and 6/1/2017, Client ID #6000 and
Microseeps/Pace Analytical Energy Services workorder #22394
H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\24. Scotland 4-17\4-17-scot_gw_tables.xlsx
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Table 6
Statistical Analysis Summary
Scotland County Landfill
April 18-19 , 2017
By: MG
Date: 12/13/2016
Monitoring Well Parameter Result 2L/GWP* Test Unit %ND Test
Statistically
Significant?
MW-4 Arsenic 10 10 ug/l 66.01 PPL N
MW-4 Iron 33426 300 ug/l 0 Wilcoxon N
MW-6 Iron 27552 300 ug/l 0 Wilcoxon N
MW-7 Iron 87929 300 ug/l 0 Wilcoxon N
MW-9 Iron 11163 300 ug/l 0 Wilcoxon N
MW-12 Iron 35037 300 ug/l 0 Wilcoxon N
MW-13 Iron 29610 300 ug/l 0 Wilcoxon N
MW-12 Vanadium
27 0.3* ug/l 50.84 PPL N
Notes:
%ND Method chosen due to percent non-detects
PPL Parametric Prediction Limit (Inter-Well)
Wilcoxon Wilcoxon Rand Individual Well Test (Intra-well)
Bold indicates statistical significance
Lab analysis by Environment 1, Inc. reports dated 5/22/2017 & 6/1/2017, Client ID#6000.
MW-1 and MW-8 are used as site background wells
+?3URMHFWV?*URXQGZDWHU0RQLWRULQJ?*URXQGZDWHU0RQLWRULQJ5HSRUWV?6FRWODQG?6FRWODQG?VFRWBJZBWDEOHV[OV[
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Table 7
Conductivity and Velocity Calculations
Scotaland County Landfill
April 18-19, 2017
By: MG
Date: 6/22/2017
Well
Groundwater
Elevation
(feet)
Hydraulic
Conductivity
(ft/day)
Porosity (%) Gradient
Velocity
(ft/day)
MW-1 185.95 6.8 0.2 0.0177 0.603
MW-2 177.21 6.12 0.2 0.0173 0.529
MW-3 170.09 14.29 0.18 0.0128 1.016
MW-4 167.74 23.13 0.21 0.0047 0.521
MW-5 178.57 18.03 0.21 0.0168 1.444
MW-6 170.40 13.27 0.18 0.0114 0.843
MW-7 176.41 7.48 0.15 0.0137 0.682
MW-8 184.77 7.82 0.2 0.0091 0.354
Average Velocity (ft/day)0.749
Note:Velocity Calculated from V=K*I/n
V = velocity
K = Hydraulic Conductivity
I = Gradient
n = Porosity
Hydraulic Conductivity values from 4/4/94 GAI Consultants Inc. report
Estimated porosity values assumed from Groundwater and Wells (Driscoll)
Water level data collected by Environment 1 personnel.
H:\Projects\Groundwater Monitoring\2. Groundwater Monitoring Reports\Scotland\24. Scotland 4-17\4-17-scot_gw_tables.xlsx
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APPENDIX A
Monitoring Well Information

April 2017 Groundwater Monitoring Report
Scotland County Landfill
Solid Waste Permit No. 83-01
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FIELD BOREHOLE LOG
BOREHOLE NUMBER
PROJECT NAME:
LOCATION:
DRILLING CO:
DRILLING METHOD:
FIELD PARTY:
GEOLOGIST:
DATE BEGUN: COMPLETED:
TOTAL DEPTH:
TOP OF CASING ELEV.:
Depth (ft)
Time
Date
STATIC WATER LEVEL (BLS)
DE
P
T
H
BL
O
W

C
O
U
N
T
SA
M
P
L
I
N
G

M
E
T
H
O
D
RE
C
O
V
E
R
Y
DR
I
L
L

M
E
T
H
O
D
DESCRIPTION LI
T
H
O
L
O
G
Y
WE
L
L
IN
S
T
A
L
L
A
T
I
O
N
0.0
5.0
10.0
15.0
20.0
25.0
30.0
35.0
0.0
5.0
10.0
15.0
20.0
25.0
30.0
35.0
DE
P
T
H
Richardson Smith Gardner & Assoc
14 North Boylan Avenue, Raleigh NC 27603
[phone] Page 1 of 1
GROUND ELEV.:
NORTHING:EASTING:0 0
MW-12
HSA
Scotland County Landfill
Laurinburg, NC
Zebra Environmental, Inc.
Dan Ferrell
J. Smyth
8/26/09 8/27/09
35
GRAB
GRAB
GRAB
GRAB
GRAB
GRAB
HSA SOIL: Dark brown dry topsoil
SILTY SAND: Dry, brown to red silty F-M sand.
CLAYEY SILTY SAND: Dry, tan brown clayey silty
F-M sand.
SILTY SAND: Dry, red brown to tan silty F-M sand.
SILTY SAND: Moist, light tan silty F-M sand grading
to silty F sand at 25 feet.
SILTY SAND: Wet, Light tan, silty fF sand. B.T. at
35 feet.
NA
NA
NA
NA
NA
NA
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FIELD BOREHOLE LOG
BOREHOLE NUMBER
PROJECT NAME:
LOCATION:
DRILLING CO:
DRILLING METHOD:
FIELD PARTY:
GEOLOGIST:
DATE BEGUN: COMPLETED:
TOTAL DEPTH:
TOP OF CASING ELEV.:
Depth (ft)
Time
Date
STATIC WATER LEVEL (BLS)
DE
P
T
H
BL
O
W

C
O
U
N
T
SA
M
P
L
I
N
G

M
E
T
H
O
D
RE
C
O
V
E
R
Y
DR
I
L
L

M
E
T
H
O
D
DESCRIPTION LI
T
H
O
L
O
G
Y
WE
L
L
IN
S
T
A
L
L
A
T
I
O
N
0.0
5.0
10.0
0.0
5.0
10.0
DE
P
T
H
Richardson Smith Gardner & Assoc
14 North Boylan Avenue, Raleigh NC 27603
[phone] Page 1 of 1
GROUND ELEV.:
NORTHING:EASTING:0 0
MW-13
HSA
Scotland County Landfill
Laurinburg, NC
Zebra Environmental, Inc.
Dan Ferrell
J. Smyth
8/26/09 8/27/09
14.5
GRAB
GRAB
GRAB
HSA SOIL: Dark brown dry topsoil
SILTY SAND: Wet, black to gray silty F-M sand to
sandy silt.
SILTY SAND: Wet, Light tan silty F-C sand. B.T. @
14.5 feet.
NA
NA
NA
NA
NA
NA
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APPENDIX B
Laboratory Analytical Report

April 2017 Groundwater Monitoring Report
Scotland County Landfill
Solid Waste Permit No. 83-01
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Pace Analytical Energy Services LLC
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 22394 - 918073 Page 1 of 24
Steve Jones
Environment 1, Inc.
PO Box 7085
114 Oakmont Drive
Greenville, NC 27835
April 28, 2017
RE:
Pace Workorder:
SCOTLAND CO. / 6000
Dear Steve Jones:
22394
Enclosed are the analytical results for sample(s) received by the laboratory on Friday, April 21, 2017. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in
the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Enclosures
Ruth Welsh 04/28/2017
[e-mail]
Total Number of Pages ____
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
Customer Service Representative
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LABORATORY ACCREDITATIONS & CERTIFICATIONS
Pennsylvania Department of Environmental Protection, Bureau of Laboratories
02-00538
NELAP Non-Potable Water and Solid & Hazardous Waste
Accreditor:
Accreditation ID:
Scope:
West Virginia Department of Environmental Protection, Division of Water and Waste
Management
395
Non-Potable Water
Accreditor:
Accreditation ID:
Scope:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
89009003
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
Accreditation ID:
Scope:
NELAP: New Jersey, Department of Environmental Protection
PA026
Non-Potable Water; Solid and Chemical Materials
Accreditor:
Accreditation ID:
Scope:
NELAP: New York, Department of Health Wadsworth Center
11815
Non-Potable Water; Solid and Hazardous Waste
Accreditor:
Accreditation ID:
Scope:
State of Connecticut, Department of Public Health, Division of Environmental Health
PH-0263
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
Accreditation ID:
Scope:
NELAP: Texas, Commission on Environmental Quality
T104704453-09-TX
Non-Potable Water
Accreditor:
Accreditation ID:
Scope:
State of New Hampshire
299409
Non-potable water
Accreditor:
Accreditation ID:
Scope:
State of Georgia
Chapter 391-3-26
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Accreditor:
Accreditation ID:
Scope:
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SAMPLE SUMMARY
Workorder: 22394 SCOTLAND CO. / 6000
Lab ID Sample ID Matrix Date Collected Date Received
223940001 MW1 Water 4/19/2017 13:55 4/21/2017 11:15
223940002 MW1 Bubble Strip 4/19/2017 13:55 4/21/2017 11:15
223940003 MW4 Water 4/19/2017 10:50 4/21/2017 11:15
223940004 MW4 Bubble Strip 4/19/2017 10:50 4/21/2017 11:15
223940005 MW6 Water 4/19/2017 09:50 4/21/2017 11:15
223940006 MW6 Bubble Strip 4/19/2017 09:50 4/21/2017 11:15
223940007 MW7 Water 4/19/2017 08:50 4/21/2017 11:15
223940008 MW7 Bubble Strip 4/19/2017 08:50 4/21/2017 11:15
223940009 MW9 Water 4/19/2017 12:30 4/21/2017 11:15
223940010 MW9 Bubble Strip 4/19/2017 12:30 4/21/2017 11:15
223940011 MW12 Water 4/19/2017 12:55 4/21/2017 11:15
223940012 MW13 Water 4/19/2017 11:55 4/21/2017 11:15
223940013 MW13 Bubble Strip 4/19/2017 11:55 4/21/2017 11:15
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PROJECT SUMMARY
Workorder: 22394 SCOTLAND CO. / 6000
Batch Comments
Batch:EDON/3315 - Low Level Volatile Fatty Acids
The percent recovery for the calibration verification was above laboratory control limits. Analytes Pyruvic and iso-Hexanoic acid.
Results associated to samples may be biased high.
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ANALYTICAL RESULTS
Workorder: 22394 SCOTLAND CO. / 6000
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MW1
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940001
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 13:55
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.020J mg/l 0.20 1 4/25/2017 22:44 KB B0.0060
Acetic Acid 0.035J mg/l 0.10 1 4/25/2017 22:44 KB B0.0050
Propionic Acid 0.0020U mg/l 0.10 1 4/25/2017 22:44 KB0.0020
Butyric Acid 0.0060U mg/l 0.10 1 4/25/2017 22:44 KB0.0060
Pyruvic Acid 0.0020U mg/l 0.10 1 4/25/2017 22:44 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/25/2017 22:44 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/25/2017 22:44 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/25/2017 22:44 KB M10.0070
Hexanoic Acid 0.021J mg/l 0.20 1 4/25/2017 22:44 KB0.0090
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ANALYTICAL RESULTS
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MW1
Matrix:Bubble Strip
Parameters
Lab ID:
Sample ID:
223940002
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 13:55
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 2.7 ug/l 0.050 1 4/27/2017 15:18 MM n0.0060
Ethane 0.0020U ug/l 0.010 1 4/27/2017 15:18 MM n0.0020
Ethene 0.0060U ug/l 0.010 1 4/27/2017 15:18 MM n0.0060
Hydrogen 2.1 nM 0.60 1 4/27/2017 15:18 MM n0.075
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ANALYTICAL RESULTS
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MW4
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940003
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 10:50
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.019J mg/l 0.20 1 4/26/2017 01:24 KB B0.0060
Acetic Acid 0.030J mg/l 0.10 1 4/26/2017 01:24 KB B0.0050
Propionic Acid 0.0024J mg/l 0.10 1 4/26/2017 01:24 KB0.0020
Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 01:24 KB0.0060
Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 01:24 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 01:24 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 01:24 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 01:24 KB M10.0070
Hexanoic Acid 0.019J mg/l 0.20 1 4/26/2017 01:24 KB0.0090
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ANALYTICAL RESULTS
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MW4
Matrix:Bubble Strip
Parameters
Lab ID:
Sample ID:
223940004
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 10:50
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 3100 ug/l 0.050 1 4/27/2017 15:30 MM n0.0060
Ethane 0.024 ug/l 0.010 1 4/27/2017 15:30 MM n0.0020
Ethene 0.079 ug/l 0.010 1 4/27/2017 15:30 MM n0.0060
Hydrogen 1.6 nM 0.60 1 4/27/2017 15:30 MM n0.075
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ANALYTICAL RESULTS
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MW6
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940005
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 09:50
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.026J mg/l 0.20 1 4/26/2017 02:17 KB B0.0060
Acetic Acid 0.024J mg/l 0.10 1 4/26/2017 02:17 KB B0.0050
Propionic Acid 0.0020U mg/l 0.10 1 4/26/2017 02:17 KB0.0020
Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 02:17 KB0.0060
Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 02:17 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 02:17 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 02:17 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 02:17 KB M10.0070
Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 02:17 KB0.0090
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ANALYTICAL RESULTS
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MW6
Matrix:Bubble Strip
Parameters
Lab ID:
Sample ID:
223940006
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 09:50
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 8200 ug/l 0.050 1 4/27/2017 15:43 MM n0.0060
Ethane 0.049 ug/l 0.010 1 4/27/2017 15:43 MM n0.0020
Ethene 0.40 ug/l 0.010 1 4/27/2017 15:43 MM n0.0060
Hydrogen 1.9 nM 0.60 1 4/27/2017 15:43 MM n0.075
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ANALYTICAL RESULTS
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MW7
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940007
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 08:50
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.035J mg/l 0.20 1 4/26/2017 03:10 KB B0.0060
Acetic Acid 0.053J mg/l 0.10 1 4/26/2017 03:10 KB B0.0050
Propionic Acid 0.0040J mg/l 0.10 1 4/26/2017 03:10 KB0.0020
Butyric Acid 0.0060J mg/l 0.10 1 4/26/2017 03:10 KB0.0060
Pyruvic Acid 0.0023J mg/l 0.10 1 4/26/2017 03:10 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 03:10 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 03:10 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 03:10 KB M10.0070
Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 03:10 KB0.0090
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ANALYTICAL RESULTS
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MW7
Matrix:Bubble Strip
Parameters
Lab ID:
Sample ID:
223940008
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 08:50
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 6200 ug/l 0.050 1 4/27/2017 15:55 MM n0.0060
Ethane 0.25 ug/l 0.010 1 4/27/2017 15:55 MM n0.0020
Ethene 0.055 ug/l 0.010 1 4/27/2017 15:55 MM n0.0060
Hydrogen 1.8 nM 0.60 1 4/27/2017 15:55 MM n0.075
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ANALYTICAL RESULTS
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MW9
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940009
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 12:30
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.037J mg/l 0.20 1 4/26/2017 04:04 KB B0.0060
Acetic Acid 0.025J mg/l 0.10 1 4/26/2017 04:04 KB B0.0050
Propionic Acid 0.0031J mg/l 0.10 1 4/26/2017 04:04 KB0.0020
Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 04:04 KB0.0060
Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 04:04 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 04:04 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 04:04 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 04:04 KB M10.0070
Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 04:04 KB0.0090
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ANALYTICAL RESULTS
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MW9
Matrix:Bubble Strip
Parameters
Lab ID:
Sample ID:
223940010
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 12:30
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 25 ug/l 0.050 1 4/27/2017 16:08 MM n0.0060
Ethane 0.0031J ug/l 0.010 1 4/27/2017 16:08 MM n0.0020
Ethene 0.0076J ug/l 0.010 1 4/27/2017 16:08 MM n0.0060
Hydrogen 1.6 nM 0.60 1 4/27/2017 16:08 MM n0.075
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ANALYTICAL RESULTS
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MW12
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940011
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 12:55
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.090J mg/l 0.20 1 4/26/2017 04:57 KB B0.0060
Acetic Acid 0.053J mg/l 0.10 1 4/26/2017 04:57 KB B0.0050
Propionic Acid 0.0026J mg/l 0.10 1 4/26/2017 04:57 KB0.0020
Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 04:57 KB0.0060
Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 04:57 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 04:57 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 04:57 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 04:57 KB M10.0070
Hexanoic Acid 0.022J mg/l 0.20 1 4/26/2017 04:57 KB0.0090
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 180 ug/l 0.50 1 4/28/2017 08:11 TD n0.027
Ethane 0.0070U ug/l 0.10 1 4/28/2017 08:11 TD n0.0070
Ethene 0.016J ug/l 0.10 1 4/28/2017 08:11 TD n0.0090
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ANALYTICAL RESULTS
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MW13
Matrix:Water
Parameters
Lab ID:
Sample ID:
223940012
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 11:55
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.041J mg/l 0.20 1 4/26/2017 05:50 KB B0.0060
Acetic Acid 0.024J mg/l 0.10 1 4/26/2017 05:50 KB B0.0050
Propionic Acid 0.0020U mg/l 0.10 1 4/26/2017 05:50 KB0.0020
Butyric Acid 0.0060U mg/l 0.10 1 4/26/2017 05:50 KB0.0060
Pyruvic Acid 0.0020U mg/l 0.10 1 4/26/2017 05:50 KB M10.0020
i-Pentanoic Acid 0.015U mg/l 0.10 1 4/26/2017 05:50 KB0.015
Pentanoic Acid 0.0030U mg/l 0.10 1 4/26/2017 05:50 KB0.0030
i-Hexanoic Acid 0.0070U mg/l 0.20 1 4/26/2017 05:50 KB M10.0070
Hexanoic Acid 0.0090U mg/l 0.20 1 4/26/2017 05:50 KB0.0090
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ANALYTICAL RESULTS
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MW13
Matrix:Bubble Strip
Parameters
Lab ID:
Sample ID:
223940013
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/19/2017 11:55
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 180 ug/l 0.050 1 4/27/2017 16:20 MM n0.0060
Ethane 0.037 ug/l 0.010 1 4/27/2017 16:20 MM n0.0020
Ethene 0.11 ug/l 0.010 1 4/27/2017 16:20 MM n0.0060
Hydrogen 1.4 nM 0.60 1 4/27/2017 16:20 MM n0.075
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ANALYTICAL RESULTS QUALIFIERS
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DEFINITIONS/QUALIFIERS
U
J
Indicates the compound was analyzed for, but not detected at or above the noted concentration.
Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n
The analyte was detected in the associated blank.B
The continuing calibration verification recovery was outside laboratory control limits.M1
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QUALITY CONTROL DATA
Workorder: 22394 SCOTLAND CO. / 6000
QC Batch:
QC Batch Method:
EDON/3315
AM23G
Analysis Method:AM23G
Associated Lab Samples:223940001, 223940003, 223940005, 223940007, 223940009, 223940011, 223940012
METHOD BLANK: 48399
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
EDonors
Lactic Acid 0.010Jmg/l 0.0060 B
Acetic Acid 0.0089Jmg/l 0.0050 B
Propionic Acid 0.0020Umg/l 0.0020
Butyric Acid 0.0060Umg/l 0.0060
Pyruvic Acid 0.0020Umg/l 0.0020 M1
i-Pentanoic Acid 0.015Umg/l 0.015
Pentanoic Acid 0.0030Umg/l 0.0030
i-Hexanoic Acid 0.0070Umg/l 0.0070 M1
Hexanoic Acid 0.0090Umg/l 0.0090
LABORATORY CONTROL SAMPLE:
Parameter Units Conc.
Spike
Result
LCS
Qualifiers
LCS
% Rec
% Rec
Limits
48400
EDonors
Lactic Acid 2mg/l 2.0 B103 70-130
Acetic Acid 2mg/l 2.1 B107 70-130
Propionic Acid 2mg/l 2.1 107 70-130
Butyric Acid 2mg/l 2.1 105 70-130
Pyruvic Acid 2mg/l 2.3 M1115 70-130
i-Pentanoic Acid 2mg/l 2.1 105 70-130
Pentanoic Acid 2mg/l 2.0 101 70-130
i-Hexanoic Acid 2mg/l 2.0 M1100 70-130
Hexanoic Acid 2mg/l 1.8 90 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter Units Conc.
Spike
Result
MS
48401 48402
MSD
Result % Rec
MS MSD
% Rec
% Rec
Limit RPD RPD
Max
QualifiersResult
Original
223940001Original:
EDonors
Lactic Acid mg/l 2 2.1 103 70-130 B2.0 102 0.98 300.02
Acetic Acid mg/l 2 2.1 105 70-130 B2.1 106 0.95 300.035
Propionic Acid mg/l 2 2.1 106 70-1302.1 106 0 300
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QUALITY CONTROL DATA
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MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter Units Conc.
Spike
Result
MS
48401 48402
MSD
Result % Rec
MS MSD
% Rec
% Rec
Limit RPD RPD
Max
QualifiersResult
Original
223940001Original:
Butyric Acid mg/l 2 2.1 104 70-1302.1 105 0.96 300.0029
Pyruvic Acid mg/l 2 2.2 112 70-130 M12.2 112 0 300
i-Pentanoic Acid mg/l 2 2.1 105 70-1302.1 106 0.95 300
Pentanoic Acid mg/l 2 2.0 103 70-1302.1 104 0.97 300
i-Hexanoic Acid mg/l 2 2.3 115 70-130 M12.2 111 3.5 300
Hexanoic Acid mg/l 2 2.1 102 70-1302.1 104 1.9 300.021
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QUALITY CONTROL DATA
Workorder: 22394 SCOTLAND CO. / 6000
QC Batch:
QC Batch Method:
DISG/6073
AM20GAX
Analysis Method:AM20GAX
Associated Lab Samples:223940002, 223940004, 223940006, 223940008, 223940010, 223940013
METHOD BLANK: 48447
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Methane 0.0060Uug/l 0.0060 n
Ethane 0.0020Uug/l 0.0020 n
Ethene 0.0060Uug/l 0.0060 n
METHOD BLANK: 48448
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Hydrogen 0.075UnM 0.075 n
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
48449 48451
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Methane ug/l 8.1 8.4 104 80-120 n8.4 104 0 20
Ethane ug/l 6.4 6.4 101 80-120 n6.4 100 1 20
Ethene ug/l 16 16 100 80-120 n16 99 1 20
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
48450 48452
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Hydrogen nM 24 24 98 80-120 n23 96 2.1 20
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QUALITY CONTROL DATA
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QC Batch:
QC Batch Method:
DISG/6074
AM20GAX
Analysis Method:AM20GAX
Associated Lab Samples:223940011
METHOD BLANK: 48453
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Methane 0.027Uug/l 0.027 n
Ethane 0.0070Uug/l 0.0070 n
Ethene 0.0090Uug/l 0.0090 n
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
48455 48457
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Methane ug/l 750 830 111 80-120 n890 119 7 20
Ethane ug/l 38 40 104 80-120 n40 106 1.9 20
Ethene ug/l 35 37 105 80-120 n38 107 1.9 20
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
without the written consent of Pace Analytical Energy Services LLC.
DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF
Pace Analytical Energy Services LLC
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 22394 - 918073 Page 23 of 24
QUALITY CONTROL DATA QUALIFIERS
Workorder: 22394 SCOTLAND CO. / 6000
QUALITY CONTROL PARAMETER QUALIFIERS
The analyte was detected in the associated blank.B
The continuing calibration verification recovery was outside laboratory control limits.M1
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
without the written consent of Pace Analytical Energy Services LLC.
DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF
Pace Analytical Energy Services LLC
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 22394 - 918073 Page 24 of 24
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: 22394 SCOTLAND CO. / 6000
Lab ID Sample ID Prep Method Analysis MethodPrep Batch Batch
Analysis
223940001 MW1 EDON/3315AM23G
223940003 MW4 EDON/3315AM23G
223940005 MW6 EDON/3315AM23G
223940007 MW7 EDON/3315AM23G
223940009 MW9 EDON/3315AM23G
223940011 MW12 EDON/3315AM23G
223940012 MW13 EDON/3315AM23G
223940002 MW1 DISG/6073AM20GAX
223940004 MW4 DISG/6073AM20GAX
223940006 MW6 DISG/6073AM20GAX
223940008 MW7 DISG/6073AM20GAX
223940010 MW9 DISG/6073AM20GAX
223940013 MW13 DISG/6073AM20GAX
223940011 MW12 DISG/6074AM20GAX
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
without the written consent of Pace Analytical Energy Services LLC.
DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF
DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF
DocuSign Envelope ID: 13B3146B-95A0-4E4C-AB9E-B2B3308E56FF

APPENDIX C
Biochlor Models

April 2017 Groundwater Monitoring Report
Scotland County Landfill
Solid Waste Permit No. 83-01
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APPENDIX D
Time vs. Concentration Graphs

April 2017 Groundwater Monitoring Reports
Scotland County Landfill
Solid Waste Permit No. 83-01
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