6708_CampLejeuneActiveMSW_June2016_1stSemiAnnual_DIN27466_20170213

MARINE CORPS BASE CAMP LEJEUNE
JACKSONVILLE, NORTH CAROLINA
Final Report
CY-2016 1st SEMIANNUAL DETECTION
MONITORING REPORT
SUBTITLE D LANDFILL
November 2016
CONTRACT: N62470-14-D-9022
DELIVERY ORDER:WE23
MID-ATLANTIC
1
Werner, Elizabeth
From:Marshall-Zank CIV James M <[e-mail]>
Sent:Monday, February 13, 2017 11:10 AM
To:Werner, Elizabeth
Cc:Acosta CIV Lauren D
Subject:Camp Lejeune Semi-Annual Landfill Groundwater Monitoring Reports for June 2016 Sampling; Active
Subtitle D and Closed Landfills
Attachments:EDD CZ09890 Landfill 13 Jul 16 0832.xls; EDD CZ09641 Landfill 14 Jul 16 0811.xls; EDD CZ09642
Landfill 13 Jul 16 0815.xls; Closed_Landfill_Env_Mon_Form Jun 2016 Sampling.pdf; Active_SubtitleD_
Env_Mon_Form_Jun 2016 Sampling.pdf
 Hello Elizabeth, 

Per subject, attached and below. 

In accordance with North Carolina Solid Waste Management requirements, this 
correspondence forwards results from the first semiannual assessment 
groundwater monitoring event for year 2016 conducted at the Marine Corps 
Base Camp Lejeune (MCB CAMLEJ) Closed Landfill and detection monitoring 
conducted at the MCB CAMLEJ's Subtitle D Active Landfill.  These reports 
were finalized in November 2016 for sampling performed in June 2016 and are 
attached in a separate emails due to file sizes. 

Please note that arsenic (wells MW‐B, MW‐ J and MW‐K) and benzene (well 
MW‐I) were detected just above the 15A NCAC 2L groundwater standard at 
the Closed Landfill.  These monitoring wells are situated adjacent to one 
another near the south and southwest end of the landfill.  Historically, 
these wells had occurrences of low levels of arsenic and benzene detections 
and/or exceedances.  In addition, well MW‐G, indicated a statistically 
significant increase (SSI) for barium and a value above the Solid Waste 
Section Limit (SWSL), however, well below the 2L standard.  It will be 
watched 
In future sampling events.  A complete data summary of all the detections 
can 
be found in Table 5‐1 of the report. 

There were no 15A NCAC 2L  exceedances detected at the Subtitle D Active 
Landfill. 

MCB CAMLEJ continues to sample active raw drinking water supply wells semi‐ 
annually and the wells nearest to the Closed Landfill are No.s 606 and 661. 
In mid‐March 2016, well 606 had a value of 0.67J ppb for arsenic, "J" 
indicating an estimated result less than a lab reporting limit but greater 
than or equal to the method detection limit.  Well 661 was not operating due 
to maintenance and no sampling was done.  Both wells were not operating or 
sampled at the next sampling event in late August 2016 due to maintenance. 

Electronic Data Deliverables (EDD) files for both landfills are attached to 
this email along with the NCDEQ Solid Waste Section Environmental Monitoring 
2
Reporting Forms.  As previously requested by your office, all future semi‐ 
Annual groundwater monitoring reports for both the Closed and Subtitle D 
Landfills will continue to be submitted electronically to you. 

If you have any questions, please contact Mr. James Marshall‐Zank, 
Environmental Quality Branch, Environmental Management Division, G‐F, at 
910‐451‐9122. 

Regards, James Marshall‐Zank 

James Marshall‐Zank 
Water Quality Section 
Environmental Quality Branch 
Environmental Management Division 
G‐F, MCB CAMLEJ 
Phone 910‐451‐9122 
Email:  [e-mail] 

Privacy Act ‐ 1974 As amended applies, this E‐Mail may contain information 
which must be protected IAW DoD 5400.11R, and is For Official Use Only 
(FOUO).  This email and any files transmitted with it are intended solely 
for the use of the individual or agency to which they are addressed.  If you 

have received this email in error, please notify me immediately. 

For Official Use Only ‐ Privacy Sensitive:  Any misuse or unauthorized 
disclosure may result in both civil and criminal penalties. 

CY-2016 1st SEMIANNUAL DETECTION
MONITORING REPORT
SUBTITLE D LANDFILL
MARINE CORPS BASE CAMP LEJEUNE

Prepared For:

NAVAL FACILITIES ENGINEERING COMMAND
MID-ATLANTIC (ENVIRONMENTAL)
NORFOLK, VA 23511

Contracting Officer’s Representative: Dialis B. Figueroa-Arriaga

Contract: N62470-14-D-9022
Delivery Order: WE23

November 2016

AH/BC Navy JV, LLC
11837 Rock Landing Drive, Suite 300
Newport News, VA 23606
[phone]

DETECTION MONITORING SEMIANNUAL REPORT
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC TABLE OF CONTENTS
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 i
ACRONYMS & ABBREVIATIONS................................................................... iii
1. INTRODUCTION ................................................................................... 1-1
2. GENERAL PHYSIOGRAPHY ............................................................... 2-1
2.1 SITE TOPOGRAPHY ................................................................................... 2-1
2.2 SITE GEOLOGY ........................................................................................ 2-1
2.3 SITE HYDROLOGY .................................................................................... 2-2
2.4 GROUNDWATER TABLE ............................................................................. 2-2
2.5 HYDRAULIC GRADIENT & GROUNDWATER FLOW VELOCITY CALCULATIONS.. 2-3
2.6 SURFACE WATER ..................................................................................... 2-4
3. SAMPING AND ANALYSIS PROGRAM ............................................... 3-1
3.1 MONITORING WELL SAMPLING PROTOCOL ................................................. 3-1
3.2 SURFACE WATER SAMPLING PROTOCOL ................................................... 3-2
3.3 LEACHATE SAMPLING PROTOCOL .............................................................. 3-2
3.4 SAMPLE HANDLING, TRANSPORTATION, AND ANALYSES .............................. 3-2
4. QUALITY CONTROL SAMPLES .......................................................... 4-1
5. ANALYTICAL RESULTS ...................................................................... 5-1
5.1 GROUNDWATER SAMPLES ........................................................................ 5-1
5.2 SURFACE WATER SAMPLES ...................................................................... 5-2
5.3 LEACHATE SAMPLES................................................................................. 5-2
6. STATISTICAL ANALYSIS ..................................................................... 6-1
6.1 METHODS ................................................................................................ 6-1
6.2 DATA PREPARATION ................................................................................. 6-2
6.2.1 Normality ..................................................................................... 6-2
6.2.2 Variance...................................................................................... 6-3
6.2.3 Dependence ............................................................................... 6-4
6.3 METHOD OF STATISTICAL EVALUATION ...................................................... 6-4
6.4 RESULTS ................................................................................................. 6-5
6.4.1 Inter-well Statistical Evaluation .................................................... 6-5
6.4.2 Intra-well Statistical Evaluation .................................................... 6-5
6.4.3 NCAC 2L/2B Exceedances ......................................................... 6-5
6.5 DISCUSSION OF STATISTICAL FINDINGS ..................................................... 6-6
7. SUMMARY ............................................................................................ 7-1
7.1 GROUNDWATER SAMPLES ........................................................................ 7-1
7.2 SURFACE WATER SAMPLES ...................................................................... 7-2
7.3 LEACHATE SAMPLE .................................................................................. 7-2
7.4 CONCLUSION ........................................................................................... 7-2

DETECTION MONITORING SEMIANNUAL REPORT
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC TABLE OF CONTENTS
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 ii
APPENDICES

A. Field Notes – Active Landfill
B. Laboratory Analysis (Provided Electronically)
C. 15A NCAC Solid Waste Reporting Limits / SWSL Limits
D. Chemstat Output (Provided Electronically)

TABLES
TABLE FOLLOWING PAGE
Table 2-1 Groundwater Field Data Summary ....................................................... 2-2
Table 5-1 Analytical Results Summary of Compounds Detected
Above SWSL ....................................................................................... 5-1
Table 6-1 Data Preparation Summary ................................................................. 6-2
Table 6-2 Summary of Inter-well Evaluations ....................................................... 6-5
Table 6-3 Summary of Intra-well Evaluations ....................................................... 6-5

FIGURES
FIGURE FOLLOWING PAGE
Figure 1-1 Groundwater Elevation Map ................................................................ 1-1
Figure 2-1 Potentiometric Surface Map ................................................................ 2-2

DETECTION MONITORING SEMIANNUAL REPORT
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC ACRONYMS AND ABBREVIATIONS
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 iii
ACRONYMS & ABBREVIATIONS

AH AH/BC Navy JV, LLC.
bgs below ground surface
CFR Code of Federal Regulations
COC chain of custody
CY calendar year
DMR Detection Monitoring Report
DO dissolved oxygen
EPA Environmental Protection Agency
FD field duplicate
GIS geographic information systems
i hydraulic gradient
K hydraulic conductivity
MCB CAMLEJ Marine Corps Base Camp Lejeune
MDL method detection limit
MSL mean sea level
MSWLF Municipal Solid Waste Landfill
MW monitoring wells
n effective porosity
NAVFAC Naval Facilities Engineering Command
NC North Carolina
NCAC North Carolina Administrative Code
NCDEQ North Carolina Department of Environmental Quality
PVC polyvinyl chloride
RCRA Resource Conservation and Recovery Act
RL reporting limit
SC specific conductivity
SSC statistically significant concentration
SSI statistically significant increase
SU standard units

DETECTION MONITORING SEMIANNUAL REPORT
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC ACRONYMS AND ABBREVIATIONS
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 iv
SW surface water
SWL static water level
SWMR Solid Waste Management Rules
SWSL Solid Waste Section Limits
VOC volatile organic compound
µg/L micrograms per liter

DETECTION MONITORING SEMIANNUAL REPORT SECTION 1
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC INTRODUCTION
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 1-1
1. INTRODUCTION
AH/BC Navy JV, LLC (AH) provided groundwater, surface water, and leachate
sampling services at the Subtitle D Municipal Solid Waste Landfill (MSWLF) facility at
Marine Corps Base Camp Lejeune (MCB CAMLEJ). This project was completed
under Naval Facilities Engineering Command (NAVFAC) Contract N62470-14-D-
9022, Delivery Order WE23. The closed landfill facility is located on Piney Green
Road, and a general layout of the facility is provided in Figure 1-1.
This report presents the results for the first biannual detection monitoring event for
calendar year (CY) 2016. The North Carolina (NC) Solid Waste Management Rules
(SWMR) require the MSWLF to monitor the groundwater using two types of
monitoring wells (MW); background and compliance wells. Wells installed
hydraulically up-gradient from the MSWLF are called background wells and wells
installed hydraulically down-gradient from the background wells are referred to as
compliance wells. Currently, there are three (3) background wells and thirteen1 (13)
compliance wells in the monitoring program at the MSWLF.
Historically, chloroform had been detected at chronic concentrations in monitoring
well MW-4 during earlier sampling events. For this reason, the MSWLF had begun
assessment monitoring in accordance with 15A North Carolina Administrative Code
(NCAC) 13B.1634 rules as directed by the North Carolina Department of
Environmental Quality (NCDEQ). MCB CAMLEJ had then conducted a limited
investigation for chloroform around MW-4. Upon completion of that investigation,
NCDEQ had allowed the MSWLF to return to a detection monitoring regime.
Samples are typically collected from three background monitoring wells (MW-1, MW-
11 and MW-12) and thirteen compliance wells (MW-2 through MW-10 and MW-14
through MW-17), and two surface water sampling points (SW-1 and SW-2) during
each sampling event. During the June 2016 sampling event (completed June 29th

1 Compliance well MW-13 was removed from service on 5 December 2014.
Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
GROUNDWATER ELEVATION MAP Figure 1-1

DETECTION MONITORING SEMIANNUAL REPORT SECTION 1
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC INTRODUCTION
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 1-2
through July 1st) samples were collected from all sampling locations including the
leachate collection system. As required in the Detection Monitoring Program, all
recovered monitoring well samples were analyzed for constituents listed in 40 Code
of Federal Regulations (CFR) 258 Appendix I Constituents for Detection Monitoring
(hereafter referred to as Appendix I).
There are currently three cells at the MSWLF: both Phase I and Phase II cells are
closed and the Phase III cell is currently receiving waste. The facility is expected to
open a new waste receiving unit in the near future which then will be known as the
Phase IV cell.

DETECTION MONITORING SEMIANNUAL REPORT SECTION 2
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC GENERAL PHYSIOGRAPHY
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 2-1
2. GENERAL PHYSIOGRAPHY
The general background information presented in this section was originally
presented in the June 2001 Detection Monitoring Report (DMR) prepared by S&ME
(S&ME, 2001). This information has been modified for brevity and updated where
necessary to reflect current conditions.
2.1 SITE TOPOGRAPHY
The naturally occurring topographic relief of the local area surrounding the MSWLF is
approximately 10 feet. The highest natural ground surface elevations, at 30 to 35 feet
above Mean Sea Level (MSL) Datum, occur within the central portion of the site. In
the vicinity of the Phase I and the Phase II cells, the ground surface slopes gently to
the south, to an approximate elevation of 25 feet at the intersection of Shell Rock and
Piney Green Roads. In the vicinity of the Phase III cell, the ground surface generally
slopes to the north towards Wallace Creek.
2.2 SITE GEOLOGY
Cretaceous-age sediments immediately overlying the basement rocks are divided into
undifferentiated units identified as the Cape Fear, Middendorf (formerly Tuscaloosa),
Black Creek, and Peedee Formations. Tertiary-age sediments deposited above the
Cretaceous units include the Beaufort, Castle Hayne, and Belgrade Formations.
Quaternary age surficial sediments consisting of sand, clay, gravel, and peat
deposited in marine, fluvial, aeolian and lacustrine environments overlie the Tertiary
units. Prior to commissioning new monitoring wells, soil borings were advanced into
the Quaternary deposits to a depth of approximately 30 feet within the area of the
MSWLF for the purposes of developing a stratigraphic profile.

DETECTION MONITORING SEMIANNUAL REPORT SECTION 2
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC GENERAL PHYSIOGRAPHY
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 2-2
2.3 SITE HYDROLOGY
Surficial groundwater flow patterns in the vicinity of the MSWLF have been evaluated
through a series of shallow monitoring wells finished at depths of about 30 feet (or
less) below ground surface (bgs). The depth to groundwater varies from less than two
feet bgs in the vicinity of Bearhead Creek to approximately 16 to 18 feet bgs in better-
drained portions of the site. The highest groundwater elevations may normally be
observed within the central portions of the MSWLF site, notably within the vicinity of
MW-1, MW-11 and MW-12. This area appears to indicate a groundwater divide
between the Phase III cell and the more southern oriented Phase I and Phase II cells.
2.4 GROUNDWATER TABLE
The depth to the groundwater table was measured in three background wells (MW-1,
MW-11 and MW-12) and thirteen compliance wells (MW-2 through MW-10 and MW-
14 through MW-17) during the June 2016 sampling event. At that time, each well was
examined for its general integrity, including protection from surface water inflow, well
identification tag, vented cap, lock, and general well security. Each well was opened
and the depth to the water table was measured from the top of the polyvinyl chloride
(PVC) well casing pipe using an electronic water level/slope indicator. The water table
elevation at each well was calculated by subtracting the depth to groundwater
measurement from the surveyed elevation of the top of the casing. Table 2-1 provides
groundwater measurements and groundwater elevation calculations for each of the
monitoring wells measured during the June 2016 sampling event, as well as, the
previous sampling event conducted in October 2015.
A water table contour map was constructed using a geographic information systems
(GIS) base map and plotting the groundwater elevations calculated for each
monitoring well location. Groundwater potentiometric surface contours which were
determined from the static groundwater measurements collected during the June
2016 sampling event are shown on Figure 2-1. As seen in previous monitoring
reports, within the vicinity of the MSWLF, groundwater flow appears to be split along
a drainage divide that approximately bifurcates the Phase II cell from the Phase III
Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
GROUNDWATER FIELD DATA SUMMARY Table 2-1
Phase 1
Background Well Compliance Wells Surface Water Samples
Sampling Date Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15
Water Table Data
Top of Casing Elevation (ft.)38.78 38.78 32.11 32.11 29.57 29.57 34.22 34.22 30.49 30.49 33.36 33.36 ****
Depth to Water from TOC (ft.)6.01 3.42 8.10 6.61 6.04 4.67 10.69 8.95 7.01 4.88 9.65 7.11 ****
Groundwater Elevation (ft.)32.77 35.36 24.01 25.50 23.53 24.90 23.53 25.27 23.48 25.61 23.71 26.25 ****
Field Parameters
pH 4.77 4.34 4.87 5.26 6.28 6.18 4.82 5.62 5.65 5.46 4.51 4.74 NR NR NR NR
Specific Conductance (mS/cm)0.05 0.07 0.04 0.07 0.20 0.35 0.07 0.14 0.14 0.21 0.02 0.02 NR NR NR NR
Temperature (o C)25.28 18.73 21.26 19.87 25.15 20.04 20.94 19.97 23.66 17.54 19.27 19.30 NR NR NR NR
Aquifer Parameters
Porosity (ne) 1 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 ****
Hydraulic Conductivity (K)2 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 ****
Hydraulic Gradient (i) 3 0.0000 0.0000 0.0060 0.0067 0.0054 0.0062 0.0052 0.0056 0.0053 0.0056 0.0052 0.0053 ****
Avg. Linear Velocity (v) 4 0.0 0.0 99.7 112.2 90.4 102.4 85.6 93.5 88.2 92.6 86.8 87.3 ****
Phase 2
Sampling Date Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15
Water Table Data
Top of Casing Elevation (ft.)34.25 34.25 34.46 34.46 38.77 38.77 38.75 38.75 43.94 43.94 42.87 42.87
Depth to Water from TOC (ft.)9.44 7.04 5.52 8.04 5.52 6.69 9.21 6.97 12.34 11.08 11.43 10.52
Groundwater Elevation (ft.)24.81 27.21 28.94 26.42 33.25 32.08 29.54 31.78 31.60 32.86 31.44 32.35
Field Parameters
pH 4.15 5.02 5.70 6.34 4.56 6.45 4.46 5.60 6.50 6.96 5.41 6.29
Specific Conductance (mS/cm)0.24 0.13 0.07 0.11 0.03 0.17 0.02 0.04 0.79 0.84 0.26 0.29
Temperature (o C)23.01 20.99 21.92 20.52 21.20 20.29 19.71 20.18 24.85 18.79 20.60 21.43
Aquifer Parameters
Porosity (ne) 1 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15
Hydraulic Conductivity (K)2 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241
Hydraulic Gradient (i) 3 0.0053 0.0041 0.0023 0.0054 -0.0023 0.0003 0.0023 0.0007 0.0000 0.0000 0.0000 0.0000
Avg. Linear Velocity (v) 4 88.6 68.7 38.0 90.1 -38.0 5.7 38.1 11.4 0.0 0.0 0.0 0.0
Phase 3 Notes:
~ The low pH values are within the historical range observed on-site.
* Surface water samples; no water table data nor aquifer parameters calculated
Sampling Date Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 Jul-16 Oct-15 ** Water levels resulted in a "dry well" condition during the sampling event. No water samples could be recovered.
Water Table Data *** Well MW-16R recently replaced MW-16
Top of Casing Elevation (ft.)34.39 34.39 34.17 34.17 41.99 41.99 33.05 33.05
Depth to Water from TOC (ft.)18.99 13.47 9.62 7.30 14.56 6.99 4.83 NS No surface water sample collected due to hunters and military exercises.
Groundwater Elevation (ft.)15.40 20.92 24.55 26.87 27.43 41.99 26.06 28.22 NR Not recorded during sampling
Field Parameters WD Well destroyed
pH 3.78 4.11 4.24 4.60 3.73 4.62 4.44 1 15% is an assumed average effective porosity value (ne) based on published data (Freeze and Cherry, 1979)
Specific Conductance (mS/cm)0.04 0.07 0.03 0.05 0.65 0.14 0.20 2 Hydraulic Conductivity (K) calculated during previous sampling events; reported in cm/sec.
Temperature (o C)19.20 19.07 21.91 20.92 20.17 22.97 19.75 3 Hydraulic Gradient (i) calculated by dividing the difference between two selected contour elevations (dh) by the horizontal
Aquifer Parameters distance (dl) measured between the two elevations (dh/dl); reported in ft/ft.
Porosity (ne) 1 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 4 Average Linear Velocity (v) is calculated as shown below; reported in ft/yr. 1.035E06K is conversion from cm/sec to feet/yr.
Hydraulic Conductivity (K)2 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 0.00241 v = -(1.035E06)K*i
Hydraulic Gradient (i) 3 0.0130 0.0096 0.0057 0.0048 0.0033 -0.0073 0.0044 0.0037 ne
Avg. Linear Velocity (v) 4 216.4 159.5 94.2 80.0 55.7 -121.9 74.0 62.0
MW-15 MW-16R***
MW-12
SW-1MW-3MW-2 MW-6 SW-2Monitor Well Number MW-1 MW-4 MW-5
MW-7R MW-10
Monitor Well Number MW-14
Monitor Well Number MW-11
Compliance Wells Background Wells
MW-8 MW9
MW-17
Compliance Wells
Sample Event:
6-29-16 Through 7-1-16
Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
POTENTIOMETRIC SURFACE MAP Figure 2-1

DETECTION MONITORING SEMIANNUAL REPORT SECTION 2
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC GENERAL PHYSIOGRAPHY
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 2-3
cell. Groundwater, generally, flows to the south-southwest towards Bearhead Creek
and to the north-northeast towards Wallace Creek.
2.5 HYDRAULIC GRADIENT & GROUNDWATER FLOW VELOCITY CALCULATIONS
The hydraulic gradients (i) between the background wells and each of the compliance
wells were determined by calculating the vertical difference between the groundwater
elevations observed at the background wells and each of the compliance wells and
then dividing that result by the measured distance from the background wells to each
corresponding compliance well. The following background wells were used for these
calculations: MW-1 for Phase I wells, MW-12 for Phases II wells, and MW-11 for
Phase III wells. Hydraulic gradients within the vicinity of the MSWLF are typically flat.
Positive gradients during the June 2016 event ranged from 0.00002 to 0.0130 feet per
foot.
Groundwater velocities were then calculated by multiplying the hydraulic gradient (i)
determined above by a previously determined hydraulic conductivity (k) constant and
then dividing that result by the estimated effective porosity (n) of the aquifer.
Calculated groundwater flow velocities are summarized in Table 2-1.
Based on the calculations, groundwater flow velocities during the June 2016 sampling
event in the Phase I cell ranged from approximately 85.6 feet per year between MW-1
and MW-4 to approximately 99.7 feet per year between MW-1 and MW-2.
Groundwater flow velocities in the Phase II cell ranged from approximately -38.0 feet
per year between MW-93 and MW-12 to approximately 88.6 feet per year between
MW-7R and MW-12. Groundwater flow velocities in the Phase III cell ranged from
approximately 55.7 feet per year between MW-11 and MW-16R to approximately
216.4 feet per year between MW-11 and MW-14.
On average, water levels during the June 2016 sampling event were approximately
1.7 feet lower than measured during the October 2015 sampling event.

2 A negative gradient of -0.0023 was calculated between well pairs MW-9 and MW-12. The observed
water level in MW-9 is currently anomalous in that it exceeds that of any background well.
3 The corresponding gradient and velocity of the MW-9/MW-12 well set should be regarded as ‘flat’.

DETECTION MONITORING SEMIANNUAL REPORT SECTION 2
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC GENERAL PHYSIOGRAPHY
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 2-4
2.6 SURFACE WATER
The MSWLF is located within the drainage basin of Bearhead Creek, a tributary of
Wallace Creek. Bearhead Creek is located west of the site and is the only surface
water body to directly receive drainage from the facility. Wallace Creek then flows
westward into the New River. According to MCB CAMLEJ’s 2001 Discharge
Monitoring Report (DMR), the central portion of the site (near MW-1) is poorly drained
and was classified as a wetland area. Phase I and Phase II of the MSWLF drain to
the south into Bearhead Creek. Phase III appears to drain towards the north (within
the Wallace Creek basin). There are two surface water sample collection points
located due south of the Phase I cell. These locations are indicated on Figures 1-1
and 2-1.

DETECTION MONITORING SEMIANNUAL REPORT SECTION 3
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC SAMPING AND ANALYSIS PROGRAM
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 3-1
3. SAMPING AND ANALYSIS PROGRAM
This section describes the procedures used for collecting the groundwater and
surface water samples. In accordance with 15A NCAC 13B.1633, MCB CAMLEJ has
conducted semiannual detection monitoring for Appendix I constituents at the
MSWLF.
During the June 2016 sampling event, all active monitoring wells were sampled and
analyzed for all Appendix I constituents. All methods used for sampling are compliant
with the NCDEQ Solid Waste Section Guidelines for Groundwater, Soil, and Surface
Water Sampling manual.
3.1 MONITORING WELL SAMPLING PROTOCOL
Prior to collecting groundwater samples, the static water level (SWL) was measured
using an electronic water level meter at each location. The height of the water column
was then used to calculate the well volume for each well.
Once the well volume was calculated, each well was purged using low-flow sampling
techniques, which minimize hydraulic stresses on the aquifer during purging and
sampling events. This technique also ensures the recovery of a representative water
sample directly from the aquifer formation as opposed to the water column. A
peristaltic pump was then attached to dedicated Teflon® tubing which had been
previously installed in each of the monitoring wells. The pump was then activated to
induce a low-flow condition in which groundwater begins to flow from the aquifer into
the screened zone of the monitoring well. The pump was then adjusted such that the
rate of discharge was balanced by the well’s rate of recovery. This rate of discharge
subsequently results in a minimal drawdown of water levels within each monitoring
well.
Temperature, pH, specific conductivity (SC), dissolved oxygen (DO), and turbidity
were field measured at five-minute intervals during well purging until temperature, pH,

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and SC stabilized, while turbidity and DO were within ±10% of the previous reading.
Stabilization is defined by NCDEQ as a variance of no more than ±0.2 standard units
(SU) pH, ±0.2° temperature, and ± 5.0% SC. Groundwater samples were collected as
soon as the water quality parameters met the stabilized condition criteria. The above
field measured parameters are discussed in the following sections and are
summarized in Table 2-1. Additional field notes are provided in Appendix A of this
report.
3.2 SURFACE WATER SAMPLING PROTOCOL
Surface water samples were collected from two surface water collection points
located along the banks of Bearhead Creek. The sample locations are shown in
Figures 1-1 and 2-1. Surface water samples were collected with the NCDEQ
approved “surface grab sample” technique4.
3.3 LEACHATE SAMPLING PROTOCOL
Leachate samples are collected from the leachate collection system when possible.
Samples are generally collected directly from a dedicated sample tap located on the
side-slope of the Phase 1 Cell near well MW-6. During the June 2016 sampling event,
a sample set was drawn from this tap. Leachate samples were collected with the
NCDEQ approved grab sample technique.
3.4 SAMPLE HANDLING, TRANSPORTATION, AND ANALYSES
After each sample was collected, the samples were labeled and placed in a shipping
cooler containing ice. Once sampling was complete, the samples were repackaged
with new/additional ice and prepared for shipment to Environmental Conservation
Laboratories, Inc., of Cary, North Carolina for analyses. All samples were properly
logged on a Chain-of-Custody (COC) form which was included with the sample
coolers. Once prepared, a COC seal was placed on the exterior of each shipping

4 As detailed in Appendix E of the Solid Waste Section Guidelines for Groundwater, Soil, and Surface
Water Sampling manual.

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cooler’s lid and secured with clear packing tape. All groundwater and surface water
samples were submitted for analyses for the constituents listed on the COC (the COC
is included in Appendix B).

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4. QUALITY CONTROL SAMPLES
Quality control samples are often used to demonstrate the adequacy of field
decontamination procedures (equipment rinsate blanks), assess the potential for
cross contamination during shipment of the sample containers from the laboratory to
the field or back to the laboratory (trip blanks), and to evaluate the consistency of
laboratory analytical processes (field duplicate samples).
During the sampling event, laboratory-prepared trip blanks accompanied the samples
and were analyzed for Appendix I volatile organic compounds (VOCs). No equipment
was reused in the field or decontaminated; therefore, no equipment rinsate blanks
were collected. In order to verify the laboratory’s level of precision, a field duplicate
(FD or “Dup”) sample was collected during the June 2016 sampling event. The
analytical results of the blind duplicate sample agreed closely with its corresponding
matched sample collected from well MW-17. The MW-17/”Dup” duplicate sample set
had an absolute average relative percent difference of 0.03% for all parameters. The
analytical results of the duplicate sample (“Dup”) are provided within Appendix B of
this report.

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5. ANALYTICAL RESULTS
The laboratory analytical reports and COC forms are included in Appendix B. The
analytical results for the organic and inorganic compounds that were detected above
the North Carolina Solid Waste Section Limit5 (SWSL) during the June 2016 sampling
event are summarized in Table 5-1. Also included in Table 5-1 are results that were
detected above the lab’s internal Method Detection Limit (MDL) but below the SWSL
Reporting Limit (RL) if the constituent was detected above the SWSL in at least one
other well. These values are typically associated with a “J” ‘flag’ to indicate that the
data was estimated by the laboratory. However, in some instances, a “J” flag was not
assigned to the result as the value was detected above the lab’s internal RL. Results
of estimated values (“J” flagged) and results above the lab’s internal RL, but below
the SWSL, were not included in the following sections as they do not exceed the
SWSL. These types of results are not to be included in statistical evaluations as
directed by NCDEQ.
5.1 GROUNDWATER SAMPLES
During the June 2016 sampling event, no Appendix I organic compounds were
detected above the SWSL.
Three Appendix I inorganic compounds, barium, vanadium and zinc, were detected
above the SWSL in four compliance wells and within one background well. Barium
was detected above the SWSL of 100 µg/L in well MW-16R and MW-17 at
concentrations of 157.0 µg/L 165.0 µg/L, respectively. These concentrations are
below the 15A NCAC 2L groundwater protection standard of 700 µg/L for barium.
Barium was also detected in all remaining wells; however, those values were below
the SWSL.

5 A complete list of SWSL concentrations managed by the NC Division of Waste Management is provid-
ed through the following web address: http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-
list. Additionally, a complete list of SWSLs has been included in this report as Appendix C.

Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
ANALYTICAL RESULTS SUMMARY OF COMPOUNDS
DETECTED ABOVE SWSL Table 5-1
Sample Event:
6-29-16 Through 7-1-16
MW1 MW11 MW12 MW2 MW3 MW4 MW5 MW6 MW7R MW8 MW9 MW10 SWSL 2L
None Detected
MW1 MW11 MW12 MW2 MW3 MW4 MW5 MW6 MW7R MW8 MW9 MW10 SWSL 2L
Barium 43.5 J 79.4 J 14.1 J 12.4 J 7.77 J 39.6 J 54.7 J 28.5 J 72.6 J 6.10 J 11.2 J 10.5 J 100 700
Vanadium 3.34 J 2.81 J ND 2.21 J ND ND ND ND 4.01 J 3.06 J ND 1.87 J 25 NE
Zinc ND 77.8 ND ND ND ND ND ND ND 13.3 ND 44.8 10 1000
Legend
MW14 MW15 MW16R MW17 SWSL 2L
None Detected XXX - Values are above 15A NCAC 2L Groundwater Protection Standards
XXX - Values are above NC SWSL Quantification Limits
Compliance - Units are in µg/l
MW14 MW15 MW16R MW17 SWSL 2L - B = Analyte is found in the assoicated blank at >1/2 RL
Barium 32.7 J 32.6 J 157.0 165.0 100 700 - J = result below reporting limit
Vanadium ND 1.67 J 42.4 2.87 J 25 NE - ND = Not detected
Zinc ND ND 30.0 ND 10 1000 - NA = Not applicable, well abandoned, not sampled
- NE = Not established
NCAC
NCAC
Compliance
Compliance
NCAC
Organic
NCAC
Inorganic
Organic
Inorganic
Background
Background
Compliance

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Vanadium was detected above the SWSL of 25 µg/L in compliance well MW-16R at a
concentration of 42.4 µg/L. Vanadium was also detected below the SWSL in
background wells MW-1 and MW-11 as well as compliance wells MW-2, MW-7R,
MW-8, MW-10, MW-15 and MW-17. There is no established 15A NCAC 2L standard
value for vanadium in groundwater.
Zinc was detected above the SWSL of 10 µg/L in three compliance wells and within
one background well. Compliance wells MW-8, MW-10 and MW-16R had zinc
concentrations of 13.3 µg/L, 44.8 µg/L and 30.0 µg/L, respectively. Zinc was also
detected above the SWSL in background well MW-11 at a concentration of 77.8 µg/L.
These zinc concentrations are below the 15A NCAC 2L standard of 1,000 µg/L for
zinc in groundwater. Zinc was not detected in any additional wells.
5.2 SURFACE WATER SAMPLES
Surface water samples SW-1 and SW-2 were analyzed for Appendix I constituents.
There were no Appendix I constituents detected above the 15A NCAC 2B surface
water quality standards during the June 2016 sampling event.
5.3 LEACHATE SAMPLES
Leachate samples were collected during the June 2016 event. Barium and zinc were
each detected above their corresponding SWSL values (but not above their
corresponding 15A NCAC 2L groundwater protection standards). Biochemical oxygen
demand, Chemical oxygen demand and turbidity were also detected; however, these
constituents do not have corresponding SWSL values. No Appendix I constituents
were detected above their corresponding SWSL and 15A NCAC 2L groundwater
protection standard values. A summary of analytical results is located in Appendix B
of this report.

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6. STATISTICAL ANALYSIS
This section describes the statistical methods used to evaluate qualified analytical
data. Qualified analytical data are classified as values that are free of Data Reporting
Qualifiers (such as “J” or “L”) which are also above the North Carolina Solid Waste
Section Limit (SWSL) quantitation limit for each analyte of interest. According to the
Division of Waste Management:
“…laboratory analytical results with estimated concentrations (J-flagged)
should not be included in statistical analysis.” 6
Statistical analyses were performed on all qualified data which have been collected at
the facility since December 1997. The objective of this statistical evaluation is to
determine whether indications of pollutants in compliance wells have or have not
significantly increased over that of the background well (inter-well changes) or
increased relative to their own water qualities (intra-well changes).
6.1 METHODS
AH has evaluated the historical data using statistical procedures outlined in Statistical
Analyses of Groundwater Monitoring Data at RCRA Facilities, Unified Final Guidance
(March 2009). Statistical analyses were performed only on qualified data where
analytic concentrations were detected above their corresponding SWSL quantitation
limits. This section provides a brief discussion of the general steps followed in the
statistical analysis.
The objective of this statistical evaluation is to determine whether indications of
pollutants in compliance wells have or have not significantly increased over that of the
background well (inter-well changes) or increased relative to their own historical water
qualities (intra-well changes). Statistical evaluations were conducted using ChemStat

6 As confirmed by Ervin Lane, Compliance Hydrogeologist, NC Department of Environment and Natural
Resources on November 22, 2010.

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version 6.2.1 (Starpoint Software, Inc, 2008), and the resultant output is located in
Appendix D.
6.2 DATA PREPARATION
Initially, general statistical parameters were computed for any parameter detected
above the SWSL standard. These statistical parameters include the sample minimum,
maximum, mean, and standard deviation. Additionally, the percentage of non-detects
was computed, and statistical outliers (for normal or transformed data sets) were
identified.
Conditions of each data set’s numerical distribution were evaluated in order to deter-
mine which statistical method was most appropriate. Three conditions were
considered in order to determine the appropriate method: normality, variance, and
independence. The percentage of non-detects is also taken into consideration. As
concentration data inherently belong to a one-tailed distribution system, contaminant
parameters tend to be positively skewed from zero-concentration towards a higher
concentration. Most groundwater quality data follow normal or log-normal distribution
patterns. Data sets that are normally distributed are analyzed using parametric
statistical procedures. Data sets that are non-normal or un-transformable require non-
parametric analysis procedures. Additionally, data sets with a high percentage of non-
detects also require non-parametric analysis methods.
A summary of the data preparation results is provided in Table 6-1.
6.2.1 Normality
The quality of results from statistical tests (based on the assumption of normality) be-
comes questionable when data does not follow the normal model of distribution. The
first level of method assessment is to determine if each data set follows the normal
(Gaussian) model of distribution. Data sets with greater than 50 samples utilize the
Shapiro-Francia test to determine normality (this method was used for this report).
For data sets with less than 50 samples, the Shapiro-Wilks test is used.
Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
DATA PREPARATION SUMMARY Table 6-1
Sample Event:
6-29-16 Through 7-1-16
Organic
None Detected
Inorganic
Barium Non-Equal Non-Normal Non-Transformable 91.41%Poisson Prediction Yes
Vanadium Non-Equal Non-Normal Non-Transformable 96.53%Poisson Prediction Yes
Zinc Non-Equal Non-Normal Non-Transformable 88.67%Non-Parametric Prediction
Limit Yes
Required Bulk Analysis
Method
Levene's Equal
Variance Test
Shapiro-Francia
Normality Test Transformable Percent Non-
Detects
Evaluation
Required

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These methods are suitable for groundwater data in that they substantially weigh the
tails of data sets distribution. This is critical as the tails of a data set’s distribution
often depart from a normal distribution. When normality tests initially reveal the
condition of non-normality, a redistribution-transformation of the data set is attempted.
Transformed data sets are reevaluated for normality. If the condition of normality is
met, the data set will remain transformed. If the condition of non-normality is present
after transformation, the data set is returned to its original form and the condition of
non-normality is considered valid. All data generated from this sampling event as well
as every preceding sampling event (from both the up-gradient and down-gradient
wells) were used in the evaluation of normality.
6.2.2 Variance
Many statistical tests are based on the assumption of equal variance among data
sets. Each data set’s “spread” or “variance” is assessed in order to determine if the
condition of equal variance between each data set exists. The power of parametric
testing decreases with an increase in data variance. Therefore, non-parametric tests
are utilized when the calculated variance of a data set exceeds a tabulated and
acceptable level of variance. Variance of a data set may be evaluated graphically or
through computation. The graphic method is qualitative and is only used for an initial
approximation of variance or where the variance is assumed to be so small that
further quantitative measurements are not required.
The facilities data sets are evaluated quantitatively with ChemStat. The test of equal
variance (homogeneity) compares the measured spread of a group to a tabulated
spread at a specified significance level. Where the measured spread exceeds the
accepted spread, the assumption that data are of equal variance is rejected and the
choice of test type used in statistical analyses should reflect this finding. Where data
is found to be normally distributed, the Bartlett’s test for equal variance may be used.
Where data is found to have a non-normal distribution, the Levene’s test for equal
variance is used.

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6.2.3 Dependence
The condition of data set dependence is critical. Most statistical procedures are
based on the assumption of data independence. The location of each well assures
that the collected samples are physically independent in that the data generated, and
ultimately the evaluation, will be independent as well. No formal test for dependence
is required.
6.3 METHOD OF STATISTICAL EVALUATION
The Environmental Protection Agency (EPA) issued a procedural manual called the
Statistical Analysis of Ground-Water Monitoring Data at RCRA Facilities, Unified Final
Guidance (March 2009). Within the Unified Final Guidance manual, in "Appendix B. -
Historical Notes", a reference was made to the EPA's "Addendum to Interim Final
Guidance" document stating that the "test of proportions" method was no longer
recommended for data sets which have greater than 90% "non-detect" data. The
EPA's updated guidance now recommends utilizing the "Poisson
Prediction/Tolerance limit" method when working with data sets with greater than
90% "non-detect" results.
Methods of statistical evaluation were chosen based on results from the data
preparation procedure (refer to Section 6.2). During data preparation, it was revealed
that the data could not be transformed and normalized. Also, the non-detect rate for
this facility generally averages approximately 95% for constituents detected above
the SWSL standard. The Poisson Prediction Limit method was utilized for bulk
analysis where whole sample populations were identified to have “non-detect” rates
of greater than 90% during the data preparation phase. Otherwise, the Non-
Parametric Prediction limit test was used for inter-well comparisons/analysis.
Supplemental intra-well prediction limit comparisons were utilized in the event that
inter-well tests indicated that a statistically significant value was identified. Depending
on each well’s single parameter non-detect rate, either the Poisson or the Non-
Parametric Prediction limit method was used.

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Statistically significant concentrations (SSCs), and potential statistically significant
increases (SSIs), were identified when the current data collected during the June
2015 sampling event exceeded its corresponding background prediction limit.
6.4 RESULTS
The following subsections describe the results of the statistical evaluations.
6.4.1 Inter-well Statistical Evaluation
Inter-well evaluations were performed if any constituent in any compliance well had a
concentration above the NC SWSL standard. Three inorganic constituents required
analysis as indicated in Table 5-1. Inter-well analyses were performed for each of the
following constituents: barium, vanadium and zinc. Inter-well evaluations of the down-
gradient locations identified three potential inorganic SSCs: barium concentrations in
wells MW-16R and MW-17, and the vanadium concentration in well MW-16R. Current
zinc concentrations were not found to be significant. See Table 6-2 for a summary of
inter-well testing results.
6.4.2 Intra-well Statistical Evaluation
Intra-well evaluations were performed on constituents that were identified as potential
SSCs during inter-well bulk analysis. With respect to inorganic constituents, the
potential inter-well SSC identified for the barium concentration in MW-17 was
confirmed as a SSC through intra-well analysis. Additionally, the current vanadium
concentration in well MW-16R was also confirmed to be a SSC through intra-well
analysis. See Table 6-3 for a summary of intra-well testing results.
6.4.3 NCAC 2L/2B Exceedances
No 15A NCAC 2L groundwater water protection standard exceedances were
encountered during the June 2016 sampling event.
Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
SUMMARY OF INTER-WELL EVALUATIONS Table 6-2
Sample Event:
6-29-16 Through 7-1-16
MW-1 MW-11 MW-12 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7R MW-8 MW-9 MW-10 SWSL 2L
None Detected
MW-1 MW-11 MW-12 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7R MW-8 MW-9 MW-10 SWSL 2L
Barium 100 700
Vandadium 25 NE
Zinc X XNP XNP 10 1000
MW-14 MW-15 MW-16R MW-17 SWSL 2L
None Detected
MW-14 MW-15 MW-16R MW-17 SWSL 2L
Barium X X 100 700
Vanadium X 25 NE
Zinc XNP 10 1000
Legend
X
XPP - Poisson Prediction Limit Method - Current concentrations are evaluated as not statistically significant compared to background at a 95% confidence level
XNP - Non-Parametric Prediciton Limit Method - Current concentrations are evaluated as not statistically significant compared to background at a 92.5% confidence level
X
X - Background concentration over 2L standard
Organic NCAC
Inorganic Background Compliance NCAC
Background Compliance
- Background concentration over SWSL standard
NCAC
- All Methods - Current concentrations are evaluated as statistically significant compared to background
Inorganic
Organic Compliance
Compliance
NCAC
Detection Monitoring Semiannual Report, Subtitle D Landfill
MCB Camp Lejeune, NC
SUMMARY OF INTRA-WELL EVALUATIONS Table 6-3
Sample Event:
6-29-16 Through 7-1-16
MW-1 MW-11 MW-12 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7R MW-8 MW-9 MW-10 SWSL 2L
None Detected
MW-1 MW-11 MW-12 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7R MW-8 MW-9 MW-10 SWSL 2L
Barium 100 700
Vanadium 25 NE
Zinc X 10 1000
MW-14 MW-15 MW-16R MW-17 SWSL 2L
None Detected
MW-14 MW-15 MW-16R MW-17 SWSL 2L
Barium XNP XNP 100 700
Vanadium XNP 25 NE
Zinc 10 1000
Legend
XPP - Poisson Prediction Limit Method - Current concentration evaluated as statistically significant compared to background
XNP - Non-Parametric Prediction Limit Method - Current concentration evaluated as statistically significant compared to background
XPP - Poisson Prediction Limit Method - Current concentration evaluated as not statistically significant compared to background at a 95% confidence level
XNP - Non-Parametric Prediciton Limit Method - Current concentration evaluated as not statistically significant compared to its background, confidence level = >90%
X
X
- Background concentration over SWSL standard
- Background concentration over 2L standard
Organic
Inorganic
Compliance NCAC
Compliance NCAC
Organic Background Compliance NCAC
Inorganic Background Compliance NCAC

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6.5 DISCUSSION OF STATISTICAL FINDINGS
The whole data set for the Subtitle D landfill is limited by a relatively small sample
population of target constituents that subsequently have a high percentage of non-
detects. Statistical evaluations can also be subject to additional non-numeric
interpretations. Constituents that may be identified as potential SSCs may not be
relevant in the context of the regulations if the detected value is below published
quantification limits. In this regard, qualifying any concentration that is detected below
the SWSL concentration as a SSC would be erroneous, as the validity of the result is
in question (i.e., the detected parameter would be below the quantification threshold
established by the State of North Carolina). At times a laboratory may have the ability
to reliably detect concentrations below the SWSL. However, the state established the
SWSL values to eliminate uncertainty with respect to data validation. Although a
concern, this type of evaluation is no longer required as statistical evaluations are
only performed on values that are detected above the SWSL.
A SSI may be identified if two SSCs are identified in series from one sampling event
to another indicating an increasing trend. As none of the current intra-well SSCs were
preceded by a SSC from the previous sampling event, no SSIs were identified as a
result of the June 2016 sampling event.

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7. SUMMARY
Samples were collected from three background wells, thirteen compliance wells and
two surface water collection points during the June 2016 sampling event. Samples
were also collected from the facility’s leachate collection system. Groundwater and
surface water samples were analyzed for all Appendix I constituents. Statistical
evaluations were then completed for constituents reported above the SWSL
quantification standard.
7.1 GROUNDWATER SAMPLES
Three inorganic SSC were initially identified through inter-well analysis based on data
collected during the June 2016 sampling event. Intra-well evaluation of the three
inter-well SSCs resulted in the identification of two intra-well SSCs.
Based on the results of the statistical evaluations, the following observations can be
made:
 The current concentration of barium in wells MW-16 and MW-17 (157 µg/L
and 165 µg/L, respectively) is significantly lower than the 15A NCAC 2L
groundwater protection standard of 700 µg/L. The current concentration of
barium in well MW-16 was not confirmed to be a SSC. However, the
concentration in MW-17 was confirmed to be a SSC through both inter and
intra-well analyses.
 The current concentration of vanadium in MW-16R (42.4 µg/L) was also
confirmed to be a SSC through both inter and intra-well analyses. Vanadium
does not have an established 15A NCAC 2L groundwater protection standard.
 The current zinc concentrations in wells MW-8 (13.3 µg/L), MW-10 (44.8 µg/L)
and MW-16R (30.0 µg/L) were not found to be SSCs through inter-well
analysis. In addition, the current concentrations are significantly lower than the
15A NCAC 2L groundwater protection standard of 1,000 µg/L for zinc in
groundwater.

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7.2 SURFACE WATER SAMPLES
Surface water samples SW-1 and SW-2 were analyzed for Appendix I constituents.
There were no Appendix I constituents detected above the 15A NCAC 2B surface
water quality standards during the June 2016 sampling event.
7.3 LEACHATE SAMPLE
Leachate samples were collected during the June 2016 event. Barium and zinc were
each detected above their corresponding SWSL values (but not above their
corresponding 15A NCAC 2L groundwater protection standards). Biochemical oxygen
demand, Chemical oxygen demand and turbidity were also detected; however, these
constituents do not have corresponding SWSL values. No Appendix I constituents
were detected above their corresponding SWSL and 15A NCAC 2L groundwater
protection standard values. A summary of analytical results is located in Appendix B
of this report.
7.4 CONCLUSION
Three inorganic Appendix I constituents were detected above the SWSL during the
June 2016 sampling event. No Appendix I constituents were detected above their
corresponding 15A NCAC 2L groundwater protection standards. Constituents that
were detected above the corresponding SWSL are summarized below:
Well MW-8
Zinc was detected above the SWSL at a concentration of 13.3 µg/L. This
concentration was not determined to be a SSC or SSI through inter-well analysis.
Additionally, the current concentration is well below the 15A NCAC 2L protection
standard of 1,000 µg/L.

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Well MW-10
Zinc was detected above the SWSL at a concentration of 44.8 µg/L. This
concentration was not determined to be a SSC or SSI through inter-well analysis.
Additionally, the current concentration is well below the 15A NCAC 2L protection
standard of 1,000 µg/L.
Well MW-11
Zinc was detected above the SWSL at a concentration of 77.8 µg/L. This
concentration did not require statistical analysis as it is a background well.
Additionally, the current concentration is well below the 15A NCAC 2L protection
standard of 1,000 µg/L.
Well MW-16R
Barium was detected above the SWSL at a concentration of 157.0 µg/L. The current
concentration was not confirmed as a SSC/SSI through both inter and intra-well
analyses. Additionally, the current concentration is well below the 15A NCAC 2L
protection standard of 700 µg/L.
Vanadium was detected above the SWSL at a concentration of 42.4 µg/L. The current
concentration was confirmed as a SSC through inter and intra-well analyses. The
current concentration does not exceed any 15A NCAC 2L protection standard as one
has not been established for vanadium.
Zinc was detected above the SWSL at a concentration of 30.0 µg/L. The current
concentration was not confirmed as a SSC through inter-well analyses. Additionally,
the current concentration is well below the 15A NCAC 2L protection standard of 1,000
µg/L.
Well MW-17
Barium was detected above the SWSL at a concentration of 165.0 µg/L. The current
concentration was confirmed as a SSC/SSI through both inter and intra-well

DETECTION MONITORING SEMIANNUAL REPORT SECTION 7
SUBTITLE D LANDFILL, MCB CAMP LEJEUNE, NC SUMMARY
AH/BC Navy JV, LLC. Final, November 2016
119-WE23 7-4
analyses. However, the current concentration is well below the 15A NCAC 2L
protection standard of 700 µg/L.
General Guidance
The facility is required to declare all Appendix I SSIs and 15A NCAC 2L exceedances
when they are encountered. During the June 2016 sampling event, no SSIs or 2L
exceedances were identified. Currently there are no statistical or historical indications
that any current concentrations are of concern.

AH/BC Navy JV, LLC.
APPENDIX A
Field Notes – Subtitle D Landfill

(18 PAGES)
AH/BC Navy JV, LLC.
APPENDIX B
Laboratory Analysis and EDD

(98 PAGES – PROVIDED ELECTRONICALLY; EDD
PROVIDED ELECTRONICALLY)
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CZ09641
Newport News, VA 23606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Subtitle-D Landfill
Attn: Matt Reed
AH Environmental Consultants (AH001)
11837 Rock Landing Drive, Suite 300
Bill Scott
Project Manager
Thursday, July 14, 2016
RE: Laboratory Results for
Dear Matt Reed,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Saturday, July 2, 2016.
The total number of pages in this report, including this page is 78.
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SAMPLE SUMMARY/LABORATORY CHRONICLE
6708-MW1 CZ09641-01 Sampled:07/01/16 13:35 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 12:42
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 13:21
EPA 8260B 07/15/16 07/07/16 14:45 7/8/2016 11:16
6708-MW2 CZ09641-02 Sampled:06/30/16 18:22 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:13 7/11/2016 12:45
EPA 6020B 12/27/16 07/07/16 10:04 7/11/2016 13:51
EPA 8260B 07/14/16 07/07/16 14:45 7/8/2016 11:47
6708-MW3 CZ09641-03 Sampled:06/30/16 18:22 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:13 7/11/2016 12:47
EPA 6020B 12/27/16 07/07/16 10:04 7/11/2016 13:55
EPA 8260B 07/14/16 07/07/16 14:45 7/8/2016 12:18
6708-MW4 CZ09641-04 Sampled:06/30/16 19:10 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:13 7/11/2016 12:50
EPA 6020B 12/27/16 07/07/16 10:04 7/11/2016 13:58
EPA 8260B 07/14/16 07/07/16 14:45 7/8/2016 12:51
6708-MW5 CZ09641-05 Sampled:06/30/16 19:22 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:13 7/11/2016 12:20
EPA 6020B 12/27/16 07/07/16 10:04 7/11/2016 14:02
EPA 8260B 07/14/16 07/07/16 14:45 7/8/2016 13:22
6708-MW6 CZ09641-06 Sampled:06/30/16 20:08 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:13 7/11/2016 12:52
EPA 6020B 12/27/16 07/07/16 10:04 7/11/2016 14:05
EPA 8260B 07/14/16 07/07/16 14:45 7/8/2016 13:53
6708-MW7 CZ09641-07 Sampled:06/30/16 20:46 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:13 7/11/2016 12:55
EPA 6020B 12/27/16 07/07/16 10:04 7/11/2016 14:09
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6708-MW7 CZ09641-07RE1 Sampled:06/30/16 20:46 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 07/14/16 07/11/16 08:29 7/11/2016 17:05
6708-MW8 CZ09641-08 Sampled:07/01/16 07:04 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:10
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:13
6708-MW8 CZ09641-08RE1 Sampled:07/01/16 07:04 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 07/15/16 07/11/16 08:29 7/11/2016 17:35
6708-MW9 CZ09641-09 Sampled:07/01/16 08:30 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:12
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:28
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 14:48
6708-MW10 CZ09641-10 Sampled:07/01/16 09:00 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:15
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:32
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 15:18
6708-MW11 CZ09641-11 Sampled:07/01/16 12:26 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:17
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:35
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 15:49
6708-MW12 CZ09641-12 Sampled:07/01/16 11:50 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:20
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:39
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 16:19
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6708-MW14 CZ09641-13 Sampled:07/01/16 10:55 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:22
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:42
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 16:49
6708-MW15 CZ09641-14 Sampled:07/01/16 10:05 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:25
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:46
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 17:19
6708-MW16 CZ09641-15 Sampled:07/01/16 12:35 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:27
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:49
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 17:49
6708-MW17 CZ09641-16 Sampled:07/01/16 10:42 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:29
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:53
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 18:19
6708-SW1 CZ09641-17 Sampled:07/01/16 06:40 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:32
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 14:57
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 18:50
6708-SW2 CZ09641-18 Sampled:07/01/16 06:18 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:39
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 15:00
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 19:20
6708-Dup CZ09641-19 Sampled:07/01/16 10:42 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/28/16 07/08/16 09:13 7/11/2016 13:42
EPA 6020B 12/28/16 07/07/16 10:04 7/11/2016 15:11
EPA 8260B 07/15/16 07/08/16 16:19 7/11/2016 19:50
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6708-TripBlank CZ09641-20 Sampled:06/30/16 18:22 Received:07/02/16 12:15Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 07/14/16 07/08/16 16:19 7/11/2016 14:18
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW1 CZ09641-01
Flag NotesMDLNC SWSLMRLDF
43.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
3.34 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW2 CZ09641-02
Flag NotesMDLNC SWSLMRLDF
12.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.80 ug/L EPA 6010DJ 1010.01.401Chromium - Total
0.112 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
2.21 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW3 CZ09641-03
Flag NotesMDLNC SWSLMRLDF
7.77 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW4 CZ09641-04
Flag NotesMDLNC SWSLMRLDF
39.6 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.6 ug/L EPA 8260BJ 51.00.181Chloroform
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW5 CZ09641-05
Flag NotesMDLNC SWSLMRLDF
54.7 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW6 CZ09641-06
Flag NotesMDLNC SWSLMRLDF
28.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW7 CZ09641-07
Flag NotesMDLNC SWSLMRLDF
72.6 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.69 ug/L EPA 6010DJ 1010.01.401Chromium - Total
1.88 ug/L EPA 6020BJ 103.000.9101Selenium - Total
4.01 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW8 CZ09641-08
Flag NotesMDLNC SWSLMRLDF
7.18 ug/L EPA 6010DJ 1010.06.801Arsenic - Total
6.10 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.33 ug/L EPA 6010DJ 1010.01.401Chromium - Total
3.06 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
13.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW9 CZ09641-09
Flag NotesMDLNC SWSLMRLDF
11.2 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.122 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW10 CZ09641-10
Flag NotesMDLNC SWSLMRLDF
10.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.87 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
44.8 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW11 CZ09641-11
Flag NotesMDLNC SWSLMRLDF
0.436 ug/L EPA 6020BJ 62.000.2201Antimony - Total
79.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.128 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
2.81 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
77.8 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW12 CZ09641-12
Flag NotesMDLNC SWSLMRLDF
14.1 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW14 CZ09641-13
Flag NotesMDLNC SWSLMRLDF
32.7 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW15 CZ09641-14
Flag NotesMDLNC SWSLMRLDF
32.6 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.116 ug/L EPA 6010DJ 11.000.1001Beryllium - Total
1.67 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW16 CZ09641-15
Flag NotesMDLNC SWSLMRLDF
8.10 ug/L EPA 6010DJ 1010.06.801Arsenic - Total
157 ug/L EPA 6010D 10010.01.001Barium - Total
0.389 ug/L EPA 6010DJ 11.000.1001Beryllium - Total
2.47 ug/L EPA 6010DJ 1010.01.401Chromium - Total
2.97 ug/L EPA 6010DJ 5010.02.201Nickel - Total
2.11 ug/L EPA 6020BJ 103.000.9101Selenium - Total
42.4 ug/L EPA 6010D 2510.01.401Vanadium - Total
30.0 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-MW17 CZ09641-16
Flag NotesMDLNC SWSLMRLDF
165 ug/L EPA 6010D 10010.01.001Barium - Total
0.132 ug/L EPA 6010DJ 11.000.1001Beryllium - Total
0.139 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
2.87 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-SW1 CZ09641-17
Flag NotesMDLNC SWSLMRLDF
25.8 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-SW2 CZ09641-18
Flag NotesMDLNC SWSLMRLDF
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Analyte MethodUnitsResults
Lab ID:Client ID:6708-SW2 CZ09641-18
Flag NotesMDLNC SWSLMRLDF
26.0 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:6708-Dup CZ09641-19
Flag NotesMDLNC SWSLMRLDF
159 ug/L EPA 6010D 10010.01.001Barium - Total
0.140 ug/L EPA 6010DJ 11.000.1001Beryllium - Total
0.145 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
2.74 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
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ANALYTICAL RESULTS
6708-MW1Description:Lab Sample ID:CZ09641-01 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 13:35 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 11:161,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/08/16 11:161,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/08/16 11:161,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/08/16 11:161,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 11:161,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/08/16 11:161,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 11:161,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 11:161,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/08/16 11:161,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/08/16 11:161,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/08/16 11:161,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/08/16 11:161,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/08/16 11:161,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/08/16 11:162-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/08/16 11:162-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/08/16 11:164-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/08/16 11:16Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/08/16 11:16Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/08/16 11:16Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 11:16Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/08/16 11:16Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 11:16Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/08/16 11:16Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/08/16 11:16Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/08/16 11:16Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 11:16Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 11:16Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/08/16 11:16Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/08/16 11:16Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 11:16cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/08/16 11:16cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/08/16 11:16Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 11:16Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/08/16 11:16Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 11:16Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/08/16 11:16m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/08/16 11:16Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 11:16o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/08/16 11:16Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/08/16 11:16Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 11:16Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 11:16trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 11:16trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 11:16trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/08/16 11:16Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 11:16Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/08/16 11:16Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/08/16 11:16Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
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6708-MW1Description:Lab Sample ID:CZ09641-01 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 13:35 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 11:16Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13697 %refEPA 8260B 07/08/16 11:166G070434950.0 1
Dibromofluoromethane 67-129106 %refEPA 8260B 07/08/16 11:166G070435350.0 1
Toluene-d8 59-13492 %refEPA 8260B 07/08/16 11:166G070434650.0 1
Page 10 of 78
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6708-MW1Description:Lab Sample ID:CZ09641-01 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 13:35 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 13:21Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:42Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:42Barium [7440-39-3] ^1.00 VLO10.043.5 J 1001
ug/L EPA 6010D 07/11/16 12:42Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:42Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:42Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 12:42Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:42Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:42Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:42Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 13:21Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 12:42Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 13:21Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 12:42Vanadium [7440-62-2] ^1.40 VLO10.03.34 J 251
ug/L EPA 6010D 07/11/16 12:42Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW2Description:Lab Sample ID:CZ09641-02 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 11:471,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/08/16 11:471,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/08/16 11:471,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/08/16 11:471,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 11:471,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/08/16 11:471,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 11:471,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 11:471,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/08/16 11:471,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/08/16 11:471,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/08/16 11:471,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/08/16 11:471,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/08/16 11:471,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/08/16 11:472-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/08/16 11:472-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/08/16 11:474-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/08/16 11:47Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/08/16 11:47Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/08/16 11:47Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 11:47Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/08/16 11:47Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 11:47Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/08/16 11:47Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/08/16 11:47Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/08/16 11:47Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 11:47Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 11:47Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/08/16 11:47Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/08/16 11:47Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 11:47cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/08/16 11:47cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/08/16 11:47Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 11:47Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/08/16 11:47Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 11:47Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/08/16 11:47m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/08/16 11:47Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 11:47o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/08/16 11:47Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/08/16 11:47Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 11:47Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 11:47trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 11:47trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 11:47trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/08/16 11:47Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 11:47Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/08/16 11:47Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/08/16 11:47Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/08/16 11:47Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW2Description:Lab Sample ID:CZ09641-02 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13696 %refEPA 8260B 07/08/16 11:476G070434850.0 1
Dibromofluoromethane 67-129104 %refEPA 8260B 07/08/16 11:476G070435250.0 1
Toluene-d8 59-13492 %refEPA 8260B 07/08/16 11:476G070434650.0 1
Page 13 of 78
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6708-MW2Description:Lab Sample ID:CZ09641-02 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 13:51Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:45Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:45Barium [7440-39-3] ^1.00 VLO10.012.4 J 1001
ug/L EPA 6010D 07/11/16 12:45Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:45Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:45Chromium [7440-47-3] ^1.40 VLO10.01.80 J 101
ug/L EPA 6010D 07/11/16 12:45Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:45Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:45Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:45Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 13:51Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 12:45Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 13:51Thallium [7440-28-0] ^0.110 VLO1.000.112 J 5.51
ug/L EPA 6010D 07/11/16 12:45Vanadium [7440-62-2] ^1.40 VLO10.02.21 J 251
ug/L EPA 6010D 07/11/16 12:45Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW3Description:Lab Sample ID:CZ09641-03 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 12:181,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/08/16 12:181,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/08/16 12:181,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/08/16 12:181,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 12:181,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/08/16 12:181,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 12:181,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 12:181,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/08/16 12:181,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/08/16 12:181,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/08/16 12:181,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/08/16 12:181,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/08/16 12:181,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/08/16 12:182-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/08/16 12:182-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/08/16 12:184-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/08/16 12:18Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/08/16 12:18Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/08/16 12:18Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 12:18Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/08/16 12:18Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 12:18Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/08/16 12:18Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/08/16 12:18Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/08/16 12:18Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 12:18Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 12:18Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/08/16 12:18Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/08/16 12:18Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 12:18cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/08/16 12:18cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/08/16 12:18Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 12:18Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/08/16 12:18Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 12:18Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/08/16 12:18m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/08/16 12:18Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 12:18o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/08/16 12:18Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/08/16 12:18Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 12:18Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 12:18trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 12:18trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 12:18trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/08/16 12:18Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 12:18Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/08/16 12:18Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/08/16 12:18Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/08/16 12:18Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW3Description:Lab Sample ID:CZ09641-03 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13698 %refEPA 8260B 07/08/16 12:186G070434950.0 1
Dibromofluoromethane 67-129106 %refEPA 8260B 07/08/16 12:186G070435350.0 1
Toluene-d8 59-13492 %refEPA 8260B 07/08/16 12:186G070434650.0 1
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6708-MW3Description:Lab Sample ID:CZ09641-03 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 13:55Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:47Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:47Barium [7440-39-3] ^1.00 VLO10.07.77 J 1001
ug/L EPA 6010D 07/11/16 12:47Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:47Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:47Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 12:47Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:47Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:47Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:47Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 13:55Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 12:47Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 13:55Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 12:47Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 12:47Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW4Description:Lab Sample ID:CZ09641-04 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 19:10 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 12:511,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/08/16 12:511,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/08/16 12:511,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/08/16 12:511,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 12:511,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/08/16 12:511,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 12:511,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 12:511,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/08/16 12:511,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/08/16 12:511,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/08/16 12:511,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/08/16 12:511,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/08/16 12:511,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/08/16 12:512-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/08/16 12:512-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/08/16 12:514-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/08/16 12:51Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/08/16 12:51Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/08/16 12:51Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 12:51Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/08/16 12:51Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 12:51Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/08/16 12:51Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/08/16 12:51Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/08/16 12:51Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 12:51Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 12:51Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/08/16 12:51Chloroform [67-66-3] ^0.18 ref1.01.6 J 51
ug/L EPA 8260B 07/08/16 12:51Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 12:51cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/08/16 12:51cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/08/16 12:51Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 12:51Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/08/16 12:51Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 12:51Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/08/16 12:51m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/08/16 12:51Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 12:51o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/08/16 12:51Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/08/16 12:51Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 12:51Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 12:51trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 12:51trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 12:51trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/08/16 12:51Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 12:51Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/08/16 12:51Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/08/16 12:51Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/08/16 12:51Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW4Description:Lab Sample ID:CZ09641-04 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 19:10 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13696 %refEPA 8260B 07/08/16 12:516G070434850.0 1
Dibromofluoromethane 67-129105 %refEPA 8260B 07/08/16 12:516G070435350.0 1
Toluene-d8 59-13493 %refEPA 8260B 07/08/16 12:516G070434650.0 1
Page 19 of 78
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www.encolabs.com
6708-MW4Description:Lab Sample ID:CZ09641-04 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 19:10 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 13:58Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:50Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:50Barium [7440-39-3] ^1.00 VLO10.039.6 J 1001
ug/L EPA 6010D 07/11/16 12:50Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:50Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:50Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 12:50Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:50Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:50Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:50Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 13:58Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 12:50Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 13:58Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 12:50Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 12:50Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW5Description:Lab Sample ID:CZ09641-05 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 19:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 13:221,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/08/16 13:221,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/08/16 13:221,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/08/16 13:221,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 13:221,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/08/16 13:221,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 13:221,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 13:221,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/08/16 13:221,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/08/16 13:221,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/08/16 13:221,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/08/16 13:221,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/08/16 13:221,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/08/16 13:222-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/08/16 13:222-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/08/16 13:224-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/08/16 13:22Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/08/16 13:22Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/08/16 13:22Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 13:22Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/08/16 13:22Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 13:22Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/08/16 13:22Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/08/16 13:22Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/08/16 13:22Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 13:22Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 13:22Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/08/16 13:22Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/08/16 13:22Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 13:22cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/08/16 13:22cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/08/16 13:22Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 13:22Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/08/16 13:22Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 13:22Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/08/16 13:22m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/08/16 13:22Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 13:22o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/08/16 13:22Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/08/16 13:22Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 13:22Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 13:22trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 13:22trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 13:22trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/08/16 13:22Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 13:22Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/08/16 13:22Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/08/16 13:22Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/08/16 13:22Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW5Description:Lab Sample ID:CZ09641-05 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 19:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13697 %refEPA 8260B 07/08/16 13:226G070434950.0 1
Dibromofluoromethane 67-129107 %refEPA 8260B 07/08/16 13:226G070435450.0 1
Toluene-d8 59-13492 %refEPA 8260B 07/08/16 13:226G070434650.0 1
Page 22 of 78
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6708-MW5Description:Lab Sample ID:CZ09641-05 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 19:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:02Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:20Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:20Barium [7440-39-3] ^1.00 VLO10.054.7 J 1001
ug/L EPA 6010D 07/11/16 12:20Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:20Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:20Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 12:20Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:20Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:20Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:20Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:02Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 12:20Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:02Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 12:20Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 12:20Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW6Description:Lab Sample ID:CZ09641-06 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 20:08 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/08/16 13:531,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/08/16 13:531,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/08/16 13:531,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/08/16 13:531,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 13:531,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/08/16 13:531,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 13:531,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 13:531,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/08/16 13:531,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/08/16 13:531,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/08/16 13:531,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/08/16 13:531,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/08/16 13:531,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/08/16 13:532-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/08/16 13:532-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/08/16 13:534-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/08/16 13:53Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/08/16 13:53Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/08/16 13:53Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 13:53Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/08/16 13:53Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 13:53Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/08/16 13:53Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/08/16 13:53Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/08/16 13:53Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 13:53Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 13:53Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/08/16 13:53Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/08/16 13:53Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 13:53cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/08/16 13:53cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/08/16 13:53Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/08/16 13:53Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/08/16 13:53Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/08/16 13:53Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/08/16 13:53m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/08/16 13:53Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/08/16 13:53o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/08/16 13:53Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/08/16 13:53Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/08/16 13:53Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/08/16 13:53trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/08/16 13:53trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 13:53trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/08/16 13:53Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/08/16 13:53Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/08/16 13:53Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/08/16 13:53Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/08/16 13:53Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Page 24 of 78
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6708-MW6Description:Lab Sample ID:CZ09641-06 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 20:08 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13696 %refEPA 8260B 07/08/16 13:536G070434850.0 1
Dibromofluoromethane 67-129107 %refEPA 8260B 07/08/16 13:536G070435450.0 1
Toluene-d8 59-13495 %refEPA 8260B 07/08/16 13:536G070434750.0 1
Page 25 of 78
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www.encolabs.com
6708-MW6Description:Lab Sample ID:CZ09641-06 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 20:08 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:05Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:52Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:52Barium [7440-39-3] ^1.00 VLO10.028.5 J 1001
ug/L EPA 6010D 07/11/16 12:52Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:52Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:52Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 12:52Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:52Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:52Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:52Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:05Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 12:52Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:05Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 12:52Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 12:52Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 26 of 78
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6708-MW7Description:Lab Sample ID:CZ09641-07 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 20:46 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 17:051,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/11/16 17:051,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/11/16 17:051,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/11/16 17:051,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:051,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/11/16 17:051,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:051,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:051,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/11/16 17:051,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/11/16 17:051,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/11/16 17:051,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/11/16 17:051,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/11/16 17:051,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/11/16 17:052-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/11/16 17:052-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/11/16 17:054-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/11/16 17:05Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/11/16 17:05Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/11/16 17:05Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:05Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/11/16 17:05Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:05Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/11/16 17:05Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/11/16 17:05Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/11/16 17:05Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:05Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:05Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/11/16 17:05Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/11/16 17:05Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:05cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/11/16 17:05cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/11/16 17:05Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:05Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/11/16 17:05Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:05Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/11/16 17:05m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/11/16 17:05Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:05o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/11/16 17:05Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/11/16 17:05Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:05Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:05trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:05trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:05trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/11/16 17:05Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:05Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/11/16 17:05Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/11/16 17:05Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/11/16 17:05Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW7Description:Lab Sample ID:CZ09641-07 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 20:46 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13694 %refEPA 8260B 07/11/16 17:056G110214750.0 1
Dibromofluoromethane 67-12993 %refEPA 8260B 07/11/16 17:056G110214650.0 1
Toluene-d8 59-13495 %refEPA 8260B 07/11/16 17:056G110214850.0 1
Page 28 of 78
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www.encolabs.com
6708-MW7Description:Lab Sample ID:CZ09641-07 07/02/16 12:15Received:
Matrix:Ground Water Sampled:06/30/16 20:46 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:09Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 12:55Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 12:55Barium [7440-39-3] ^1.00 VLO10.072.6 J 1001
ug/L EPA 6010D 07/11/16 12:55Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 12:55Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 12:55Chromium [7440-47-3] ^1.40 VLO10.01.69 J 101
ug/L EPA 6010D 07/11/16 12:55Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 12:55Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 12:55Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 12:55Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:09Selenium [7782-49-2] ^0.910 VLO3.001.88 J 101
ug/L EPA 6010D 07/11/16 12:55Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:09Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 12:55Vanadium [7440-62-2] ^1.40 VLO10.04.01 J 251
ug/L EPA 6010D 07/11/16 12:55Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW8Description:Lab Sample ID:CZ09641-08 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 07:04 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 17:351,1,1,2-Tetrachloroethane [630-20-6] ^0.17 ref1.00.17 U 51
ug/L EPA 8260B 07/11/16 17:351,1,1-Trichloroethane [71-55-6] ^0.12 ref1.00.12 U 11
ug/L EPA 8260B 07/11/16 17:351,1,2,2-Tetrachloroethane [79-34-5] ^0.28 ref1.00.28 U 31
ug/L EPA 8260B 07/11/16 17:351,1,2-Trichloroethane [79-00-5] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:351,1-Dichloroethane [75-34-3] ^0.13 ref1.00.13 U 51
ug/L EPA 8260B 07/11/16 17:351,1-Dichloroethene [75-35-4] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:351,2,3-Trichloropropane [96-18-4] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:351,2-Dibromo-3-chloropropane [96-12-8] ^0.48 ref1.00.48 U 131
ug/L EPA 8260B 07/11/16 17:351,2-Dibromoethane [106-93-4] ^0.66 ref1.00.66 U 11
ug/L EPA 8260B 07/11/16 17:351,2-Dichlorobenzene [95-50-1] ^0.19 ref1.00.19 U 51
ug/L EPA 8260B 07/11/16 17:351,2-Dichloroethane [107-06-2] ^0.21 ref1.00.21 U 11
ug/L EPA 8260B 07/11/16 17:351,2-Dichloropropane [78-87-5] ^0.10 ref1.00.10 U 11
ug/L EPA 8260B 07/11/16 17:351,4-Dichlorobenzene [106-46-7] ^0.19 ref1.00.19 U 11
ug/L EPA 8260B 07/11/16 17:352-Butanone [78-93-3] ^1.3 ref5.01.3 U 1001
ug/L EPA 8260B 07/11/16 17:352-Hexanone [591-78-6] ^0.88 ref5.00.88 U 501
ug/L EPA 8260B 07/11/16 17:354-Methyl-2-pentanone [108-10-1] ^1.1 ref5.01.1 U 1001
ug/L EPA 8260B 07/11/16 17:35Acetone [67-64-1] ^10 ref2010U 1001
ug/L EPA 8260B 07/11/16 17:35Acrylonitrile [107-13-1] ^3.5 ref103.5 U 2001
ug/L EPA 8260B 07/11/16 17:35Benzene [71-43-2] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:35Bromochloromethane [74-97-5] ^0.48 ref1.00.48 U 31
ug/L EPA 8260B 07/11/16 17:35Bromodichloromethane [75-27-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:35Bromoform [75-25-2] ^0.22 ref1.00.22 U 31
ug/L EPA 8260B 07/11/16 17:35Bromomethane [74-83-9] ^0.14 ref1.00.14 U 101
ug/L EPA 8260B 07/11/16 17:35Carbon disulfide [75-15-0] ^1.5 ref5.01.5 U 1001
ug/L EPA 8260B 07/11/16 17:35Carbon tetrachloride [56-23-5] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:35Chlorobenzene [108-90-7] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:35Chloroethane [75-00-3] ^0.23 ref1.00.23 U 101
ug/L EPA 8260B 07/11/16 17:35Chloroform [67-66-3] ^0.18 ref1.00.18 U 51
ug/L EPA 8260B 07/11/16 17:35Chloromethane [74-87-3] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:35cis-1,2-Dichloroethene [156-59-2] ^0.15 ref1.00.15 U 51
ug/L EPA 8260B 07/11/16 17:35cis-1,3-Dichloropropene [10061-01-5] ^0.20 ref1.00.20 U 11
ug/L EPA 8260B 07/11/16 17:35Dibromochloromethane [124-48-1] ^0.17 ref1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:35Dibromomethane [74-95-3] ^0.27 ref1.00.27 U 101
ug/L EPA 8260B 07/11/16 17:35Ethylbenzene [100-41-4] ^0.13 ref1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:35Iodomethane [74-88-4] ^1.7 ref5.01.7 U 101
ug/L EPA 8260B 07/11/16 17:35m,p-Xylenes [108-38-3/106-42-3] ^0.17 ref2.00.17 U NE1
ug/L EPA 8260B 07/11/16 17:35Methylene chloride [75-09-2] ^0.23 ref1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:35o-Xylene [95-47-6] ^0.065 ref1.00.065 U NE1
ug/L EPA 8260B 07/11/16 17:35Styrene [100-42-5] ^0.11 ref1.00.11 U 11
ug/L EPA 8260B 07/11/16 17:35Tetrachloroethene [127-18-4] ^0.17 ref1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:35Toluene [108-88-3] ^0.14 ref1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:35trans-1,2-Dichloroethene [156-60-5] ^0.21 ref1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:35trans-1,3-Dichloropropene [10061-02-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:35trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 ref1.00.70 U 1001
ug/L EPA 8260B 07/11/16 17:35Trichloroethene [79-01-6] ^0.15 ref1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:35Trichlorofluoromethane [75-69-4] ^0.24 ref1.00.24 U 11
ug/L EPA 8260B 07/11/16 17:35Vinyl acetate [108-05-4] ^0.95 ref5.00.95 U 501
ug/L EPA 8260B 07/11/16 17:35Vinyl chloride [75-01-4] ^0.32 ref1.00.32 U 11
ug/L EPA 8260B 07/11/16 17:35Xylenes (Total) [1330-20-7] ^0.45 ref3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW8Description:Lab Sample ID:CZ09641-08 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 07:04 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13694 %refEPA 8260B 07/11/16 17:356G110214750.0 1
Dibromofluoromethane 67-12992 %refEPA 8260B 07/11/16 17:356G110214650.0 1
Toluene-d8 59-13495 %refEPA 8260B 07/11/16 17:356G110214750.0 1
Page 31 of 78
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6708-MW8Description:Lab Sample ID:CZ09641-08 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 07:04 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:13Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:10Arsenic [7440-38-2] ^6.80 VLO10.07.18 J 101
ug/L EPA 6010D 07/11/16 13:10Barium [7440-39-3] ^1.00 VLO10.06.10 J 1001
ug/L EPA 6010D 07/11/16 13:10Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:10Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:10Chromium [7440-47-3] ^1.40 VLO10.02.33 J 101
ug/L EPA 6010D 07/11/16 13:10Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:10Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:10Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:10Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:13Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:10Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:13Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:10Vanadium [7440-62-2] ^1.40 VLO10.03.06 J 251
ug/L EPA 6010D 07/11/16 13:10Zinc [7440-66-6] ^4.40 VLO10.013.3 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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www.encolabs.com
6708-MW9Description:Lab Sample ID:CZ09641-09 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 08:30 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 14:481,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 14:481,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 14:481,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 14:481,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 14:481,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 14:481,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 14:481,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 14:481,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 14:481,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 14:481,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 14:481,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 14:481,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 14:481,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 14:482-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 14:482-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 14:484-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 14:48Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 14:48Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 14:48Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 14:48Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 14:48Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 14:48Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 14:48Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 14:48Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 14:48Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 14:48Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 14:48Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 14:48Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 14:48Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 14:48cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 14:48cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 14:48Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 14:48Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 14:48Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 14:48Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 14:48m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 14:48Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 14:48o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 14:48Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 14:48Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 14:48Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 14:48trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 14:48trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 14:48trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 14:48Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 14:48Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 14:48Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 14:48Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 14:48Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW9Description:Lab Sample ID:CZ09641-09 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 08:30 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %REFEPA 8260B 07/11/16 14:486G080314650.0 1
Dibromofluoromethane 67-129110 %REFEPA 8260B 07/11/16 14:486G080315550.0 1
Toluene-d8 59-134103 %REFEPA 8260B 07/11/16 14:486G080315150.0 1
Page 34 of 78
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www.encolabs.com
6708-MW9Description:Lab Sample ID:CZ09641-09 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 08:30 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:28Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:12Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:12Barium [7440-39-3] ^1.00 VLO10.011.2 J 1001
ug/L EPA 6010D 07/11/16 13:12Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:12Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:12Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:12Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:12Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:12Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:12Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:28Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:12Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:28Thallium [7440-28-0] ^0.110 VLO1.000.122 J 5.51
ug/L EPA 6010D 07/11/16 13:12Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 13:12Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 35 of 78
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www.encolabs.com
6708-MW10Description:Lab Sample ID:CZ09641-10 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 09:00 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 15:181,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 15:181,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 15:181,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 15:181,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 15:181,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 15:181,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 15:181,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 15:181,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 15:181,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 15:181,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 15:181,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 15:181,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 15:181,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 15:182-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 15:182-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 15:184-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 15:18Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 15:18Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 15:18Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 15:18Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 15:18Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 15:18Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 15:18Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 15:18Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 15:18Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 15:18Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 15:18Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 15:18Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 15:18Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 15:18cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 15:18cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 15:18Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 15:18Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 15:18Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 15:18Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 15:18m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 15:18Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 15:18o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 15:18Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 15:18Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 15:18Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 15:18trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 15:18trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 15:18trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 15:18Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 15:18Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 15:18Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 15:18Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 15:18Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW10Description:Lab Sample ID:CZ09641-10 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 09:00 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13693 %REFEPA 8260B 07/11/16 15:186G080314750.0 1
Dibromofluoromethane 67-129107 %REFEPA 8260B 07/11/16 15:186G080315350.0 1
Toluene-d8 59-134101 %REFEPA 8260B 07/11/16 15:186G080315150.0 1
Page 37 of 78
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www.encolabs.com
6708-MW10Description:Lab Sample ID:CZ09641-10 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 09:00 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:32Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:15Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:15Barium [7440-39-3] ^1.00 VLO10.010.5 J 1001
ug/L EPA 6010D 07/11/16 13:15Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:15Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:15Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:15Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:15Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:15Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:15Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:32Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:15Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:32Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:15Vanadium [7440-62-2] ^1.40 VLO10.01.87 J 251
ug/L EPA 6010D 07/11/16 13:15Zinc [7440-66-6] ^4.40 VLO10.044.8 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW11Description:Lab Sample ID:CZ09641-11 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 12:26 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 15:491,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 15:491,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 15:491,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 15:491,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 15:491,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 15:491,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 15:491,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 15:491,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 15:491,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 15:491,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 15:491,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 15:491,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 15:491,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 15:492-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 15:492-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 15:494-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 15:49Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 15:49Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 15:49Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 15:49Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 15:49Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 15:49Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 15:49Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 15:49Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 15:49Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 15:49Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 15:49Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 15:49Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 15:49Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 15:49cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 15:49cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 15:49Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 15:49Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 15:49Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 15:49Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 15:49m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 15:49Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 15:49o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 15:49Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 15:49Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 15:49Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 15:49trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 15:49trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 15:49trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 15:49Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 15:49Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 15:49Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 15:49Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 15:49Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW11Description:Lab Sample ID:CZ09641-11 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 12:26 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13688 %REFEPA 8260B 07/11/16 15:496G080314450.0 1
Dibromofluoromethane 67-129109 %REFEPA 8260B 07/11/16 15:496G080315550.0 1
Toluene-d8 59-134100 %REFEPA 8260B 07/11/16 15:496G080315050.0 1
Page 40 of 78
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www.encolabs.com
6708-MW11Description:Lab Sample ID:CZ09641-11 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 12:26 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:35Antimony [7440-36-0] ^0.220 VLO2.000.436 J 61
ug/L EPA 6010D 07/11/16 13:17Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:17Barium [7440-39-3] ^1.00 VLO10.079.4 J 1001
ug/L EPA 6010D 07/11/16 13:17Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:17Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:17Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:17Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:17Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:17Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:17Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:35Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:17Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:35Thallium [7440-28-0] ^0.110 VLO1.000.128 J 5.51
ug/L EPA 6010D 07/11/16 13:17Vanadium [7440-62-2] ^1.40 VLO10.02.81 J 251
ug/L EPA 6010D 07/11/16 13:17Zinc [7440-66-6] ^4.40 VLO10.077.8 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW12Description:Lab Sample ID:CZ09641-12 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 11:50 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 16:191,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 16:191,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 16:191,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 16:191,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 16:191,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 16:191,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 16:191,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 16:191,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 16:191,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 16:191,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 16:191,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 16:191,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 16:191,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 16:192-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 16:192-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 16:194-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 16:19Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 16:19Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 16:19Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 16:19Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 16:19Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 16:19Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 16:19Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 16:19Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 16:19Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 16:19Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 16:19Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 16:19Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 16:19Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 16:19cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 16:19cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 16:19Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 16:19Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 16:19Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 16:19Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 16:19m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 16:19Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 16:19o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 16:19Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 16:19Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 16:19Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 16:19trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 16:19trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 16:19trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 16:19Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 16:19Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 16:19Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 16:19Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 16:19Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW12Description:Lab Sample ID:CZ09641-12 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 11:50 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13690 %REFEPA 8260B 07/11/16 16:196G080314550.0 1
Dibromofluoromethane 67-129109 %REFEPA 8260B 07/11/16 16:196G080315450.0 1
Toluene-d8 59-134104 %REFEPA 8260B 07/11/16 16:196G080315250.0 1
Page 43 of 78
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www.encolabs.com
6708-MW12Description:Lab Sample ID:CZ09641-12 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 11:50 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:39Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:20Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:20Barium [7440-39-3] ^1.00 VLO10.014.1 J 1001
ug/L EPA 6010D 07/11/16 13:20Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:20Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:20Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:20Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:20Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:20Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:20Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:39Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:20Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:39Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:20Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 13:20Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW14Description:Lab Sample ID:CZ09641-13 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:55 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 16:491,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 16:491,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 16:491,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 16:491,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 16:491,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 16:491,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 16:491,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 16:491,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 16:491,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 16:491,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 16:491,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 16:491,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 16:491,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 16:492-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 16:492-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 16:494-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 16:49Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 16:49Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 16:49Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 16:49Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 16:49Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 16:49Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 16:49Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 16:49Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 16:49Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 16:49Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 16:49Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 16:49Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 16:49Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 16:49cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 16:49cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 16:49Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 16:49Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 16:49Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 16:49Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 16:49m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 16:49Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 16:49o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 16:49Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 16:49Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 16:49Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 16:49trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 16:49trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 16:49trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 16:49Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 16:49Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 16:49Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 16:49Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 16:49Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW14Description:Lab Sample ID:CZ09641-13 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:55 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13692 %REFEPA 8260B 07/11/16 16:496G080314650.0 1
Dibromofluoromethane 67-129113 %REFEPA 8260B 07/11/16 16:496G080315750.0 1
Toluene-d8 59-134104 %REFEPA 8260B 07/11/16 16:496G080315250.0 1
Page 46 of 78
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www.encolabs.com
6708-MW14Description:Lab Sample ID:CZ09641-13 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:55 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:42Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:22Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:22Barium [7440-39-3] ^1.00 VLO10.032.7 J 1001
ug/L EPA 6010D 07/11/16 13:22Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:22Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:22Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:22Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:22Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:22Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:22Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:42Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:22Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:42Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:22Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 13:22Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 47 of 78
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6708-MW15Description:Lab Sample ID:CZ09641-14 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:05 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 17:191,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 17:191,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 17:191,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 17:191,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:191,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 17:191,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:191,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:191,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 17:191,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 17:191,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 17:191,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 17:191,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 17:191,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 17:192-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 17:192-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 17:194-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 17:19Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 17:19Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 17:19Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:19Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 17:19Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:19Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 17:19Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 17:19Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 17:19Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:19Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:19Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 17:19Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 17:19Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:19cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 17:19cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 17:19Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:19Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 17:19Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:19Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 17:19m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 17:19Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:19o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 17:19Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 17:19Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:19Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:19trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:19trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:19trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 17:19Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:19Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 17:19Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 17:19Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 17:19Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW15Description:Lab Sample ID:CZ09641-14 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:05 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13695 %REFEPA 8260B 07/11/16 17:196G080314850.0 1
Dibromofluoromethane 67-129114 %REFEPA 8260B 07/11/16 17:196G080315750.0 1
Toluene-d8 59-134108 %REFEPA 8260B 07/11/16 17:196G080315450.0 1
Page 49 of 78
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www.encolabs.com
6708-MW15Description:Lab Sample ID:CZ09641-14 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:05 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:46Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:25Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:25Barium [7440-39-3] ^1.00 VLO10.032.6 J 1001
ug/L EPA 6010D 07/11/16 13:25Beryllium [7440-41-7] ^0.100 VLO1.000.116 J 11
ug/L EPA 6010D 07/11/16 13:25Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:25Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:25Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:25Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:25Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:25Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:46Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:25Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:46Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:25Vanadium [7440-62-2] ^1.40 VLO10.01.67 J 251
ug/L EPA 6010D 07/11/16 13:25Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW16Description:Lab Sample ID:CZ09641-15 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 12:35 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 17:491,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 17:491,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 17:491,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 17:491,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:491,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 17:491,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:491,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:491,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 17:491,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 17:491,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 17:491,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 17:491,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 17:491,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 17:492-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 17:492-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 17:494-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 17:49Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 17:49Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 17:49Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:49Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 17:49Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:49Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 17:49Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 17:49Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 17:49Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:49Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:49Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 17:49Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 17:49Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:49cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 17:49cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 17:49Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 17:49Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 17:49Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 17:49Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 17:49m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 17:49Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 17:49o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 17:49Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 17:49Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 17:49Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 17:49trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 17:49trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:49trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 17:49Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 17:49Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 17:49Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 17:49Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 17:49Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW16Description:Lab Sample ID:CZ09641-15 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 12:35 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13693 %REFEPA 8260B 07/11/16 17:496G080314750.0 1
Dibromofluoromethane 67-129112 %REFEPA 8260B 07/11/16 17:496G080315650.0 1
Toluene-d8 59-134104 %REFEPA 8260B 07/11/16 17:496G080315250.0 1
Page 52 of 78
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www.encolabs.com
6708-MW16Description:Lab Sample ID:CZ09641-15 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 12:35 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:49Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:27Arsenic [7440-38-2] ^6.80 VLO10.08.10 J 101
ug/L EPA 6010D 07/11/16 13:27Barium [7440-39-3] ^1.00 VLO10.0157 1001
ug/L EPA 6010D 07/11/16 13:27Beryllium [7440-41-7] ^0.100 VLO1.000.389 J 11
ug/L EPA 6010D 07/11/16 13:27Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:27Chromium [7440-47-3] ^1.40 VLO10.02.47 J 101
ug/L EPA 6010D 07/11/16 13:27Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:27Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:27Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:27Nickel [7440-02-0] ^2.20 VLO10.02.97 J 501
ug/L EPA 6020B 07/11/16 14:49Selenium [7782-49-2] ^0.910 VLO3.002.11 J 101
ug/L EPA 6010D 07/11/16 13:27Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:49Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:27Vanadium [7440-62-2] ^1.40 VLO10.042.4 251
ug/L EPA 6010D 07/11/16 13:27Zinc [7440-66-6] ^4.40 VLO10.030.0 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-MW17Description:Lab Sample ID:CZ09641-16 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:42 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 18:191,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 18:191,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 18:191,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 18:191,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 18:191,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 18:191,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 18:191,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 18:191,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 18:191,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 18:191,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 18:191,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 18:191,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 18:191,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 18:192-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 18:192-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 18:194-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 18:19Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 18:19Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 18:19Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 18:19Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 18:19Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 18:19Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 18:19Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 18:19Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 18:19Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 18:19Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 18:19Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 18:19Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 18:19Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 18:19cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 18:19cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 18:19Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 18:19Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 18:19Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 18:19Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 18:19m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 18:19Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 18:19o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 18:19Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 18:19Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 18:19Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 18:19trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 18:19trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 18:19trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 18:19Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 18:19Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 18:19Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 18:19Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 18:19Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-MW17Description:Lab Sample ID:CZ09641-16 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:42 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13693 %REFEPA 8260B 07/11/16 18:196G080314650.0 1
Dibromofluoromethane 67-129116 %REFEPA 8260B 07/11/16 18:196G080315850.0 1
Toluene-d8 59-134106 %REFEPA 8260B 07/11/16 18:196G080315350.0 1
Page 55 of 78
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6708-MW17Description:Lab Sample ID:CZ09641-16 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:42 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:53Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:29Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:29Barium [7440-39-3] ^1.00 VLO10.0165 1001
ug/L EPA 6010D 07/11/16 13:29Beryllium [7440-41-7] ^0.100 VLO1.000.132 J 11
ug/L EPA 6010D 07/11/16 13:29Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:29Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:29Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:29Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:29Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:29Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:53Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:29Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:53Thallium [7440-28-0] ^0.110 VLO1.000.139 J 5.51
ug/L EPA 6010D 07/11/16 13:29Vanadium [7440-62-2] ^1.40 VLO10.02.87 J 251
ug/L EPA 6010D 07/11/16 13:29Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-SW1Description:Lab Sample ID:CZ09641-17 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 06:40 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 18:501,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 18:501,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 18:501,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 18:501,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 18:501,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 18:501,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 18:501,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 18:501,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 18:501,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 18:501,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 18:501,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 18:501,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 18:501,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 18:502-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 18:502-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 18:504-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 18:50Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 18:50Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 18:50Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 18:50Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 18:50Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 18:50Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 18:50Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 18:50Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 18:50Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 18:50Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 18:50Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 18:50Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 18:50Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 18:50cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 18:50cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 18:50Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 18:50Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 18:50Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 18:50Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 18:50m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 18:50Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 18:50o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 18:50Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 18:50Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 18:50Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 18:50trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 18:50trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 18:50trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 18:50Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 18:50Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 18:50Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 18:50Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 18:50Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-SW1Description:Lab Sample ID:CZ09641-17 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 06:40 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13697 %REFEPA 8260B 07/11/16 18:506G080314850.0 1
Dibromofluoromethane 67-129114 %REFEPA 8260B 07/11/16 18:506G080315750.0 1
Toluene-d8 59-134105 %REFEPA 8260B 07/11/16 18:506G080315350.0 1
Page 58 of 78
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6708-SW1Description:Lab Sample ID:CZ09641-17 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 06:40 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 14:57Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:32Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:32Barium [7440-39-3] ^1.00 VLO10.025.8 J 1001
ug/L EPA 6010D 07/11/16 13:32Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:32Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:32Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:32Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:32Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:32Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:32Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 14:57Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:32Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 14:57Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:32Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 13:32Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-SW2Description:Lab Sample ID:CZ09641-18 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 06:18 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 19:201,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 19:201,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 19:201,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 19:201,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 19:201,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 19:201,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 19:201,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 19:201,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 19:201,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 19:201,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 19:201,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 19:201,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 19:201,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 19:202-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 19:202-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 19:204-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 19:20Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 19:20Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 19:20Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 19:20Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 19:20Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 19:20Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 19:20Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 19:20Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 19:20Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 19:20Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 19:20Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 19:20Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 19:20Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 19:20cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 19:20cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 19:20Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 19:20Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 19:20Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 19:20Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 19:20m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 19:20Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 19:20o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 19:20Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 19:20Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 19:20Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 19:20trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 19:20trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 19:20trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 19:20Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 19:20Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 19:20Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 19:20Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 19:20Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-SW2Description:Lab Sample ID:CZ09641-18 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 06:18 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13696 %REFEPA 8260B 07/11/16 19:206G080314850.0 1
Dibromofluoromethane 67-129117 %REFEPA 8260B 07/11/16 19:206G080315950.0 1
Toluene-d8 59-134109 %REFEPA 8260B 07/11/16 19:206G080315550.0 1
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6708-SW2Description:Lab Sample ID:CZ09641-18 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 06:18 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 15:00Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:39Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:39Barium [7440-39-3] ^1.00 VLO10.026.0 J 1001
ug/L EPA 6010D 07/11/16 13:39Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 13:39Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:39Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:39Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:39Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:39Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:39Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 15:00Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:39Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 15:00Thallium [7440-28-0] ^0.110 VLO1.000.110 U 5.51
ug/L EPA 6010D 07/11/16 13:39Vanadium [7440-62-2] ^1.40 VLO10.01.40 U 251
ug/L EPA 6010D 07/11/16 13:39Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-DupDescription:Lab Sample ID:CZ09641-19 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:42 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 19:501,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 19:501,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 19:501,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 19:501,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 19:501,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 19:501,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 19:501,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 19:501,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 19:501,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 19:501,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 19:501,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 19:501,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 19:501,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 19:502-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 19:502-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 19:504-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 19:50Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 19:50Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 19:50Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 19:50Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 19:50Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 19:50Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 19:50Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 19:50Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 19:50Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 19:50Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 19:50Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 19:50Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 19:50Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 19:50cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 19:50cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 19:50Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 19:50Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 19:50Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 19:50Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 19:50m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 19:50Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 19:50o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 19:50Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 19:50Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 19:50Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 19:50trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 19:50trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 19:50trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 19:50Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 19:50Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 19:50Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 19:50Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 19:50Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-DupDescription:Lab Sample ID:CZ09641-19 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:42 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13694 %REFEPA 8260B 07/11/16 19:506G080314750.0 1
Dibromofluoromethane 67-129115 %REFEPA 8260B 07/11/16 19:506G080315750.0 1
Toluene-d8 59-134107 %REFEPA 8260B 07/11/16 19:506G080315350.0 1
Page 64 of 78
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6708-DupDescription:Lab Sample ID:CZ09641-19 07/02/16 12:15Received:
Matrix:Ground Water Sampled:07/01/16 10:42 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 15:11Antimony [7440-36-0] ^0.220 VLO2.000.220 U 61
ug/L EPA 6010D 07/11/16 13:42Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 13:42Barium [7440-39-3] ^1.00 VLO10.0159 1001
ug/L EPA 6010D 07/11/16 13:42Beryllium [7440-41-7] ^0.100 VLO1.000.140 J 11
ug/L EPA 6010D 07/11/16 13:42Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 13:42Chromium [7440-47-3] ^1.40 VLO10.01.40 U 101
ug/L EPA 6010D 07/11/16 13:42Cobalt [7440-48-4] ^1.10 VLO10.01.10 U 101
ug/L EPA 6010D 07/11/16 13:42Copper [7440-50-8] ^1.60 VLO10.01.60 U 101
ug/L EPA 6010D 07/11/16 13:42Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 13:42Nickel [7440-02-0] ^2.20 VLO10.02.20 U 501
ug/L EPA 6020B 07/11/16 15:11Selenium [7782-49-2] ^0.910 VLO3.000.910 U 101
ug/L EPA 6010D 07/11/16 13:42Silver [7440-22-4] ^1.90 VLO10.01.90 U 101
ug/L EPA 6020B 07/11/16 15:11Thallium [7440-28-0] ^0.110 VLO1.000.145 J 5.51
ug/L EPA 6010D 07/11/16 13:42Vanadium [7440-62-2] ^1.40 VLO10.02.74 J 251
ug/L EPA 6010D 07/11/16 13:42Zinc [7440-66-6] ^4.40 VLO10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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6708-TripBlankDescription:Lab Sample ID:CZ09641-20 07/02/16 12:15Received:
Matrix:Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/11/16 14:181,1,1,2-Tetrachloroethane [630-20-6] ^0.17 REF1.00.17 U 51
ug/L EPA 8260B 07/11/16 14:181,1,1-Trichloroethane [71-55-6] ^0.12 REF1.00.12 U 11
ug/L EPA 8260B 07/11/16 14:181,1,2,2-Tetrachloroethane [79-34-5] ^0.28 REF1.00.28 U 31
ug/L EPA 8260B 07/11/16 14:181,1,2-Trichloroethane [79-00-5] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 14:181,1-Dichloroethane [75-34-3] ^0.13 REF1.00.13 U 51
ug/L EPA 8260B 07/11/16 14:181,1-Dichloroethene [75-35-4] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 14:181,2,3-Trichloropropane [96-18-4] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 14:181,2-Dibromo-3-chloropropane [96-12-8] ^0.48 REF1.00.48 U 131
ug/L EPA 8260B 07/11/16 14:181,2-Dibromoethane [106-93-4] ^0.66 REF1.00.66 U 11
ug/L EPA 8260B 07/11/16 14:181,2-Dichlorobenzene [95-50-1] ^0.19 REF1.00.19 U 51
ug/L EPA 8260B 07/11/16 14:181,2-Dichloroethane [107-06-2] ^0.21 REF1.00.21 U 11
ug/L EPA 8260B 07/11/16 14:181,2-Dichloropropane [78-87-5] ^0.10 REF1.00.10 U 11
ug/L EPA 8260B 07/11/16 14:181,4-Dichlorobenzene [106-46-7] ^0.19 REF1.00.19 U 11
ug/L EPA 8260B 07/11/16 14:182-Butanone [78-93-3] ^1.3 REF5.01.3 U 1001
ug/L EPA 8260B 07/11/16 14:182-Hexanone [591-78-6] ^0.88 REF5.00.88 U 501
ug/L EPA 8260B 07/11/16 14:184-Methyl-2-pentanone [108-10-1] ^1.1 REF5.01.1 U 1001
ug/L EPA 8260B 07/11/16 14:18Acetone [67-64-1] ^10 REF2010U 1001
ug/L EPA 8260B 07/11/16 14:18Acrylonitrile [107-13-1] ^3.5 REF103.5 U 2001
ug/L EPA 8260B 07/11/16 14:18Benzene [71-43-2] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 14:18Bromochloromethane [74-97-5] ^0.48 REF1.00.48 U 31
ug/L EPA 8260B 07/11/16 14:18Bromodichloromethane [75-27-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 14:18Bromoform [75-25-2] ^0.22 REF1.00.22 U 31
ug/L EPA 8260B 07/11/16 14:18Bromomethane [74-83-9] ^0.14 REF1.00.14 U 101
ug/L EPA 8260B 07/11/16 14:18Carbon disulfide [75-15-0] ^1.5 REF5.01.5 U 1001
ug/L EPA 8260B 07/11/16 14:18Carbon tetrachloride [56-23-5] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 14:18Chlorobenzene [108-90-7] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 14:18Chloroethane [75-00-3] ^0.23 REF1.00.23 U 101
ug/L EPA 8260B 07/11/16 14:18Chloroform [67-66-3] ^0.18 REF1.00.18 U 51
ug/L EPA 8260B 07/11/16 14:18Chloromethane [74-87-3] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 14:18cis-1,2-Dichloroethene [156-59-2] ^0.15 REF1.00.15 U 51
ug/L EPA 8260B 07/11/16 14:18cis-1,3-Dichloropropene [10061-01-5] ^0.20 REF1.00.20 U 11
ug/L EPA 8260B 07/11/16 14:18Dibromochloromethane [124-48-1] ^0.17 REF1.00.17 U 31
ug/L EPA 8260B 07/11/16 14:18Dibromomethane [74-95-3] ^0.27 REF1.00.27 U 101
ug/L EPA 8260B 07/11/16 14:18Ethylbenzene [100-41-4] ^0.13 REF1.00.13 U 11
ug/L EPA 8260B 07/11/16 14:18Iodomethane [74-88-4] ^1.7 REF5.01.7 U 101
ug/L EPA 8260B 07/11/16 14:18m,p-Xylenes [108-38-3/106-42-3] ^0.17 REF2.00.17 U NE1
ug/L EPA 8260B 07/11/16 14:18Methylene chloride [75-09-2] ^0.23 REF1.00.23 U 11
ug/L EPA 8260B 07/11/16 14:18o-Xylene [95-47-6] ^0.065 REF1.00.065 U NE1
ug/L EPA 8260B 07/11/16 14:18Styrene [100-42-5] ^0.11 REF1.00.11 U 11
ug/L EPA 8260B 07/11/16 14:18Tetrachloroethene [127-18-4] ^0.17 REF1.00.17 U 11
ug/L EPA 8260B 07/11/16 14:18Toluene [108-88-3] ^0.14 REF1.00.14 U 11
ug/L EPA 8260B 07/11/16 14:18trans-1,2-Dichloroethene [156-60-5] ^0.21 REF1.00.21 U 51
ug/L EPA 8260B 07/11/16 14:18trans-1,3-Dichloropropene [10061-02-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 14:18trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 REF1.00.70 U 1001
ug/L EPA 8260B 07/11/16 14:18Trichloroethene [79-01-6] ^0.15 REF1.00.15 U 11
ug/L EPA 8260B 07/11/16 14:18Trichlorofluoromethane [75-69-4] ^0.24 REF1.00.24 U 11
ug/L EPA 8260B 07/11/16 14:18Vinyl acetate [108-05-4] ^0.95 REF5.00.95 U 501
ug/L EPA 8260B 07/11/16 14:18Vinyl chloride [75-01-4] ^0.32 REF1.00.32 U 11
ug/L EPA 8260B 07/11/16 14:18Xylenes (Total) [1330-20-7] ^0.45 REF3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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6708-TripBlankDescription:Lab Sample ID:CZ09641-20 07/02/16 12:15Received:
Matrix:Water Sampled:06/30/16 18:22 Work Order:CZ09641
Subtitle-D LandfillProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13695 %REFEPA 8260B 07/11/16 14:186G080314850.0 1
Dibromofluoromethane 67-129108 %REFEPA 8260B 07/11/16 14:186G080315450.0 1
Toluene-d8 59-134101 %REFEPA 8260B 07/11/16 14:186G080315150.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6G07043 - EPA 5030B_MS
Prepared: 07/07/2016 14:45 Analyzed: 07/08/2016 06:33Blank (6G07043-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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Volatile Organic Compounds by GCMS - Quality Control
Batch 6G07043 - EPA 5030B_MS
Prepared: 07/07/2016 14:45 Analyzed: 07/08/2016 06:33Blank (6G07043-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9648
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10352
ug/L 50.0 59-134Surrogate: Toluene-d8 9346
Prepared: 07/07/2016 14:45 Analyzed: 07/08/2016 03:23LCS (6G07043-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1339419 1,1-Dichloroethene
ug/L1.0 20.0 81-1349118 Benzene
ug/L1.0 20.0 83-1179319 Chlorobenzene
ug/L1.0 20.0 71-1188717 Toluene
ug/L1.0 20.0 74-11910020 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10050
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 07/07/2016 14:45 Analyzed: 07/08/2016 03:55Matrix Spike (6G07043-MS1)
Source: CZ10009-07
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133980.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 81-134910.15 U18 Benzene
ug/L1.0 20.0 83-117940.17 U19 Chlorobenzene
ug/L1.0 20.0 71-118900.14 U18 Toluene
ug/L1.0 20.0 74-1191010.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9547
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9950
ug/L 50.0 59-134Surrogate: Toluene-d8 9347
Prepared: 07/07/2016 14:45 Analyzed: 07/08/2016 04:27Matrix Spike Dup (6G07043-MSD1)
Source: CZ10009-07
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13392 60.21 U18 1,1-Dichloroethene
ug/L1.0 20.0 1781-13489 20.15 U18 Benzene
ug/L1.0 20.0 1683-11791 30.17 U18 Chlorobenzene
ug/L1.0 20.0 1771-11886 40.14 U17 Toluene
ug/L1.0 20.0 2274-11998 40.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9547
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9949
ug/L 50.0 59-134Surrogate: Toluene-d8 9246
Batch 6G08031 - EPA 5030B_MS
Prepared: 07/08/2016 16:19 Analyzed: 07/11/2016 11:47Blank (6G08031-BLK1)
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Batch 6G08031 - EPA 5030B_MS
Prepared: 07/08/2016 16:19 Analyzed: 07/11/2016 11:47Blank (6G08031-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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Volatile Organic Compounds by GCMS - Quality Control
Batch 6G08031 - EPA 5030B_MS
Prepared: 07/08/2016 16:19 Analyzed: 07/11/2016 11:47Blank (6G08031-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9547
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11055
ug/L 50.0 59-134Surrogate: Toluene-d8 10352
Prepared: 07/08/2016 16:19 Analyzed: 07/11/2016 12:17LCS (6G08031-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310621 1,1-Dichloroethene
ug/L1.0 20.0 81-13410321 Benzene
ug/L1.0 20.0 83-1179820 Chlorobenzene
ug/L1.0 20.0 71-1189619 Toluene
ug/L1.0 20.0 74-11910220 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9548
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11155
ug/L 50.0 59-134Surrogate: Toluene-d8 10251
Prepared: 07/08/2016 16:19 Analyzed: 07/11/2016 12:47Matrix Spike (6G08031-MS1)
Source: CZ10009-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331120.21 U22 1,1-Dichloroethene
ug/L1.0 20.0 81-1341120.15 U22 Benzene
ug/L1.0 20.0 83-1171050.17 U21 Chlorobenzene
ug/L1.0 20.0 71-1181030.14 U21 Toluene
ug/L1.0 20.0 74-1191100.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10753
ug/L 50.0 59-134Surrogate: Toluene-d8 10150
Prepared: 07/08/2016 16:19 Analyzed: 07/11/2016 13:17Matrix Spike Dup (6G08031-MSD1)
Source: CZ10009-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133109 20.21 U22 1,1-Dichloroethene
ug/L1.0 20.0 1781-134104 80.15 U21 Benzene
ug/L1.0 20.0 1683-117100 50.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-11896 80.14 U19 Toluene
ug/L1.0 20.0 2274-119100 90.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9547
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10955
ug/L 50.0 59-134Surrogate: Toluene-d8 10251
Batch 6G11021 - EPA 5030B_MS
Prepared: 07/11/2016 08:29 Analyzed: 07/11/2016 14:10Blank (6G11021-BLK1)
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Volatile Organic Compounds by GCMS - Quality Control
Batch 6G11021 - EPA 5030B_MS
Prepared: 07/11/2016 08:29 Analyzed: 07/11/2016 14:10Blank (6G11021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6G11021 - EPA 5030B_MS
Prepared: 07/11/2016 08:29 Analyzed: 07/11/2016 14:10Blank (6G11021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9346
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9347
ug/L 50.0 59-134Surrogate: Toluene-d8 9547
Prepared: 07/11/2016 08:29 Analyzed: 07/11/2016 10:45LCS (6G11021-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1338216 1,1-Dichloroethene
ug/L1.0 20.0 81-1349218 Benzene
ug/L1.0 20.0 83-1179218 Chlorobenzene
ug/L1.0 20.0 71-1189018 Toluene
ug/L1.0 20.0 74-1199519 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9346
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8944
ug/L 50.0 59-134Surrogate: Toluene-d8 9849
Prepared: 07/11/2016 08:29 Analyzed: 07/11/2016 11:14Matrix Spike (6G11021-MS1)
Source: CZ10026-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133810.21 U16 1,1-Dichloroethene
ug/L1.0 20.0 81-134930.15 U19 Benzene
ug/L1.0 20.0 83-117910.17 U18 Chlorobenzene
ug/L1.0 20.0 71-118900.14 U18 Toluene
ug/L1.0 20.0 74-119930.15 U19 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9146
ug/L 50.0 59-134Surrogate: Toluene-d8 9548
Prepared: 07/11/2016 08:29 Analyzed: 07/11/2016 11:44Matrix Spike Dup (6G11021-MSD1)
Source: CZ10026-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13379 30.21 U16 1,1-Dichloroethene
ug/L1.0 20.0 1781-13491 20.15 U18 Benzene
ug/L1.0 20.0 1683-11791 0.80.17 U18 Chlorobenzene
ug/L1.0 20.0 1771-11888 30.14 U18 Toluene
ug/L1.0 20.0 2274-11994 0.10.15 U19 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9548
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9246
ug/L 50.0 59-134Surrogate: Toluene-d8 9749
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G07021 - EPA 3005A
Prepared: 07/07/2016 10:04 Analyzed: 07/11/2016 13:14Blank (6G07021-BLK1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G07021 - EPA 3005A
Prepared: 07/07/2016 10:04 Analyzed: 07/11/2016 13:14Blank (6G07021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.220 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 07/07/2016 10:04 Analyzed: 07/11/2016 13:17LCS (6G07021-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120103206 Antimony
ug/L3.00 200 80-120109218 Selenium
ug/L1.00 200 80-120110221 Thallium
Prepared: 07/07/2016 10:04 Analyzed: 07/11/2016 13:24Matrix Spike (6G07021-MS1)
Source: CZ09641-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251080.220 U216 Antimony
ug/L3.00 200 75-1251090.910 U218 Selenium
ug/L1.00 200 75-1251090.110 U218 Thallium
Prepared: 07/07/2016 10:04 Analyzed: 07/11/2016 13:40Matrix Spike Dup (6G07021-MSD1)
Source: CZ09641-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125105 20.220 U211 Antimony
ug/L3.00 200 2075-125111 20.910 U221 Selenium
ug/L1.00 200 2075-125109 0.20.110 U218 Thallium
Prepared: 07/07/2016 10:04 Analyzed: 07/11/2016 13:44Post Spike (6G07021-PS1)
Source: CZ09641-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201070.0837214 Antimony
ug/L3.00 200 80-1201120.163224 Selenium
ug/L1.00 200 80-1201080.108216 Thallium
Batch 6G08013 - EPA 3005A
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:14Blank (6G08013-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G08013 - EPA 3005A
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:14Blank (6G08013-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:18LCS (6G08013-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-120102204 Arsenic
ug/L10.0 200 80-12098196 Barium
ug/L1.00 20.0 80-1209819.6 Beryllium
ug/L1.00 20.0 80-12010019.9 Cadmium
ug/L10.0 200 80-12098195 Chromium
ug/L10.0 200 80-12099198 Cobalt
ug/L10.0 200 80-12094189 Copper
ug/L10.0 200 80-120100200 Lead
ug/L10.0 200 80-120100199 Nickel
ug/L10.0 200 80-120100200 Silver
ug/L10.0 200 80-12099198 Vanadium
ug/L10.0 200 80-12098196 Zinc
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:23Matrix Spike (6G08013-MS1)
Source: CZ09641-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251096.80 U218 Arsenic
ug/L10.0 200 75-12510154.7257 Barium
ug/L1.00 20.0 75-1251040.100 U20.8 Beryllium
ug/L1.00 20.0 75-1251050.360 U21.0 Cadmium
ug/L10.0 200 75-1251031.40 U206 Chromium
ug/L10.0 200 75-1251041.10 U209 Cobalt
ug/L10.0 200 75-1251001.60 U201 Copper
ug/L10.0 200 75-1251053.10 U209 Lead
ug/L10.0 200 75-1251042.20 U209 Nickel
ug/L10.0 200 75-1251051.90 U210 Silver
ug/L10.0 200 75-1251061.40 U211 Vanadium
ug/L10.0 200 75-1251034.40 U206 Zinc
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:33Matrix Spike Dup (6G08013-MSD1)
Source: CZ09641-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125110 0.96.80 U220 Arsenic
ug/L10.0 200 2075-125104 254.7263 Barium
ug/L1.00 20.0 2075-125107 30.100 U21.4 Beryllium
ug/L1.00 20.0 2075-125107 20.360 U21.5 Cadmium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G08013 - EPA 3005A
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:33Matrix Spike Dup (6G08013-MSD1) Continued
Source: CZ09641-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125106 21.40 U211 Chromium
ug/L10.0 200 2075-125107 21.10 U214 Cobalt
ug/L10.0 200 2075-125103 31.60 U206 Copper
ug/L10.0 200 2075-125108 33.10 U215 Lead
ug/L10.0 200 2075-125106 22.20 U213 Nickel
ug/L10.0 200 2075-125108 31.90 U216 Silver
ug/L10.0 200 2075-125108 21.40 U217 Vanadium
ug/L10.0 200 2075-125106 24.40 U211 Zinc
Prepared: 07/08/2016 09:13 Analyzed: 07/11/2016 12:35Post Spike (6G08013-PS1)
Source: CZ09641-05
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120105-0.001160.211 Arsenic
mg/L0.0100 0.200 80-120980.05470.251 Barium
mg/L0.00100 0.0200 80-1201005.49E-50.0201 Beryllium
mg/L0.00100 0.0200 80-120100-8.59E-50.0201 Cadmium
mg/L0.0100 0.200 80-120100-0.0004640.199 Chromium
mg/L0.0100 0.200 80-120100-0.0009040.201 Cobalt
mg/L0.0100 0.200 80-120970.0003690.194 Copper
mg/L0.0100 0.200 80-120100-0.003820.201 Lead
mg/L0.0100 0.200 80-1201000.0005420.201 Nickel
mg/L0.0100 0.200 80-1201010.001300.204 Silver
mg/L0.0100 0.200 80-1201020.0005510.204 Vanadium
mg/L0.0100 0.200 80-1201020.0009850.204 Zinc
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
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919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CZ09642
Newport News, VA 23606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Subtitle-D Landfill Leachate
Attn: Matt Reed
AH Environmental Consultants (AH001)
11837 Rock Landing Drive, Suite 300
Bill Scott
Project Manager
Wednesday, July 13, 2016
RE: Laboratory Results for
Dear Matt Reed,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, July 1, 2016.
The total number of pages in this report, including this page is 15.
Page 1 of 16
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SAMPLE SUMMARY/LABORATORY CHRONICLE
6708-Leachate CZ09642-01 Sampled:06/30/16 15:50 Received:07/01/16 10:46Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 12/27/16 07/08/16 09:04 7/11/2016 11:25
EPA 6020B 12/27/16 07/07/16 09:55 7/11/2016 12:14
EPA 8260B 07/14/16 07/07/16 10:49 7/7/2016 20:01
SM 2130B-2001 07/02/16 15:50 07/01/16 13:45 7/1/2016 13:45
SM 5210B-2001 07/02/16 15:50 07/01/16 14:06 7/1/2016 14:06
SM 5220D-1997 07/28/16 07/07/16 15:02 7/8/2016 11:30
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:6708-Leachate CZ09642-01
Flag NotesMDLNC SWSLMRLDF
927 ug/L EPA 6010D 10010.01.001Barium - Total
4400 ug/L SM 5210B-2001 NE200020001Biochemical Oxygen Demand
220000 ug/L SM 5220D-1997 NE10000100001Chemical Oxygen Demand
2.8 ug/L EPA 8260BJD R-0435.00.855Chlorobenzene
1.42 ug/L EPA 6010DJ 1010.01.401Chromium - Total
2.62 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
2.68 ug/L EPA 6010DJ 1010.01.601Copper - Total
19.0 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1.93 ug/L EPA 6010DJ 1010.01.901Silver - Total
2.58 ug/L EPA 6020BJD 5.510.01.1010Thallium - Total
130 NTU SM 2130B-2001D NE201020Turbidity
4.95 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
33.9 ug/L EPA 6010D 1010.04.401Zinc - Total
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ANALYTICAL RESULTS
6708-LeachateDescription:Lab Sample ID:CZ09642-01 07/01/16 10:46Received:
Matrix:Water Sampled:06/30/16 15:50 Work Order:CZ09642
Subtitle-D Landfill LeachateProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/07/16 20:011,1,1,2-Tetrachloroethane [630-20-6] ^0.85 ref5.00.85 UD R-0455
ug/L EPA 8260B 07/07/16 20:011,1,1-Trichloroethane [71-55-6] ^0.60 ref5.00.60 UD R-0415
ug/L EPA 8260B 07/07/16 20:011,1,2,2-Tetrachloroethane [79-34-5] ^1.4 ref5.01.4 UD R-0435
ug/L EPA 8260B 07/07/16 20:011,1,2-Trichloroethane [79-00-5] ^0.70 ref5.00.70 UD R-0415
ug/L EPA 8260B 07/07/16 20:011,1-Dichloroethane [75-34-3] ^0.65 ref5.00.65 UD R-0455
ug/L EPA 8260B 07/07/16 20:011,1-Dichloroethene [75-35-4] ^1.0 ref5.01.0 UD R-0455
ug/L EPA 8260B 07/07/16 20:011,2,3-Trichloropropane [96-18-4] ^1.2 ref5.01.2 UD R-0415
ug/L EPA 8260B 07/07/16 20:011,2-Dibromo-3-chloropropane [96-12-8] ^2.4 ref5.02.4 UD R-04135
ug/L EPA 8260B 07/07/16 20:011,2-Dibromoethane [106-93-4] ^3.3 ref5.03.3 UD R-0415
ug/L EPA 8260B 07/07/16 20:011,2-Dichlorobenzene [95-50-1] ^0.95 ref5.00.95 UD R-0455
ug/L EPA 8260B 07/07/16 20:011,2-Dichloroethane [107-06-2] ^1.0 ref5.01.0 UD R-0415
ug/L EPA 8260B 07/07/16 20:011,2-Dichloropropane [78-87-5] ^0.50 ref5.00.50 UD R-0415
ug/L EPA 8260B 07/07/16 20:011,4-Dichlorobenzene [106-46-7] ^0.95 ref5.00.95 UD R-0415
ug/L EPA 8260B 07/07/16 20:012-Butanone [78-93-3] ^6.5 ref256.5 UD R-041005
ug/L EPA 8260B 07/07/16 20:012-Hexanone [591-78-6] ^4.4 ref254.4 UD R-04505
ug/L EPA 8260B 07/07/16 20:014-Methyl-2-pentanone [108-10-1] ^5.5 ref255.5 UD R-041005
ug/L EPA 8260B 07/07/16 20:01Acetone [67-64-1] ^50 ref10050UD R-041005
ug/L EPA 8260B 07/07/16 20:01Acrylonitrile [107-13-1] ^18 ref5018UD R-042005
ug/L EPA 8260B 07/07/16 20:01Benzene [71-43-2] ^0.75 ref5.00.75 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Bromochloromethane [74-97-5] ^2.4 ref5.02.4 UD R-0435
ug/L EPA 8260B 07/07/16 20:01Bromodichloromethane [75-27-4] ^0.85 ref5.00.85 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Bromoform [75-25-2] ^1.1 ref5.01.1 UD R-0435
ug/L EPA 8260B 07/07/16 20:01Bromomethane [74-83-9] ^0.70 ref5.00.70 UD R-04105
ug/L EPA 8260B 07/07/16 20:01Carbon disulfide [75-15-0] ^7.5 ref257.5 UD R-041005
ug/L EPA 8260B 07/07/16 20:01Carbon tetrachloride [56-23-5] ^0.85 ref5.00.85 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Chlorobenzene [108-90-7] ^0.85 ref5.02.8 JD R-0435
ug/L EPA 8260B 07/07/16 20:01Chloroethane [75-00-3] ^1.2 ref5.01.2 UD R-04105
ug/L EPA 8260B 07/07/16 20:01Chloroform [67-66-3] ^0.90 ref5.00.90 UD R-0455
ug/L EPA 8260B 07/07/16 20:01Chloromethane [74-87-3] ^0.65 ref5.00.65 UD R-0415
ug/L EPA 8260B 07/07/16 20:01cis-1,2-Dichloroethene [156-59-2] ^0.75 ref5.00.75 UD R-0455
ug/L EPA 8260B 07/07/16 20:01cis-1,3-Dichloropropene [10061-01-5] ^1.0 ref5.01.0 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Dibromochloromethane [124-48-1] ^0.85 ref5.00.85 UD R-0435
ug/L EPA 8260B 07/07/16 20:01Dibromomethane [74-95-3] ^1.4 ref5.01.4 UD R-04105
ug/L EPA 8260B 07/07/16 20:01Ethylbenzene [100-41-4] ^0.65 ref5.00.65 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Iodomethane [74-88-4] ^8.5 ref258.5 UD R-04105
ug/L EPA 8260B 07/07/16 20:01m,p-Xylenes [108-38-3/106-42-3] ^0.85 ref100.85 UD R-04NE5
ug/L EPA 8260B 07/07/16 20:01Methylene chloride [75-09-2] ^1.2 ref5.01.2 UD R-0415
ug/L EPA 8260B 07/07/16 20:01o-Xylene [95-47-6] ^0.32 ref5.00.32 UD R-04NE5
ug/L EPA 8260B 07/07/16 20:01Styrene [100-42-5] ^0.55 ref5.00.55 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Tetrachloroethene [127-18-4] ^0.85 ref5.00.85 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Toluene [108-88-3] ^0.70 ref5.00.70 UD R-0415
ug/L EPA 8260B 07/07/16 20:01trans-1,2-Dichloroethene [156-60-5] ^1.0 ref5.01.0 UD R-0455
ug/L EPA 8260B 07/07/16 20:01trans-1,3-Dichloropropene [10061-02-6] ^0.75 ref5.00.75 UD R-0415
ug/L EPA 8260B 07/07/16 20:01trans-1,4-Dichloro-2-butene [110-57-6] ^3.5 ref5.03.5 UD R-041005
ug/L EPA 8260B 07/07/16 20:01Trichloroethene [79-01-6] ^0.75 ref5.00.75 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Trichlorofluoromethane [75-69-4] ^1.2 ref5.01.2 UD R-0415
ug/L EPA 8260B 07/07/16 20:01Vinyl acetate [108-05-4] ^4.8 ref254.8 UD R-04505
ug/L EPA 8260B 07/07/16 20:01Vinyl chloride [75-01-4] ^1.6 ref5.01.6 UD R-0415
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6708-LeachateDescription:Lab Sample ID:CZ09642-01 07/01/16 10:46Received:
Matrix:Water Sampled:06/30/16 15:50 Work Order:CZ09642
Subtitle-D Landfill LeachateProject:Sampled By:Jacob Carpenter
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 07/07/16 20:01Xylenes (Total) [1330-20-7] ^2.2 ref152.2 UD R-0455
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13694 %refEPA 8260B 07/07/16 20:016G070194750.0 R-041
Dibromofluoromethane 67-129103 %refEPA 8260B 07/07/16 20:016G070195150.0 R-041
Toluene-d8 59-13494 %refEPA 8260B 07/07/16 20:016G070194750.0 R-041
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6708-LeachateDescription:Lab Sample ID:CZ09642-01 07/01/16 10:46Received:
Matrix:Water Sampled:06/30/16 15:50 Work Order:CZ09642
Subtitle-D Landfill LeachateProject:Sampled By:Jacob Carpenter
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 07/11/16 12:14Antimony [7440-36-0] ^2.20 VLO20.02.20 UD 610
ug/L EPA 6010D 07/11/16 11:25Arsenic [7440-38-2] ^6.80 VLO10.06.80 U 101
ug/L EPA 6010D 07/11/16 11:25Barium [7440-39-3] ^1.00 VLO10.0927 1001
ug/L EPA 6010D 07/11/16 11:25Beryllium [7440-41-7] ^0.100 VLO1.000.100 U 11
ug/L EPA 6010D 07/11/16 11:25Cadmium [7440-43-9] ^0.360 VLO1.000.360 U 11
ug/L EPA 6010D 07/11/16 11:25Chromium [7440-47-3] ^1.40 VLO10.01.42 J 101
ug/L EPA 6010D 07/11/16 11:25Cobalt [7440-48-4] ^1.10 VLO10.02.62 J 101
ug/L EPA 6010D 07/11/16 11:25Copper [7440-50-8] ^1.60 VLO10.02.68 J 101
ug/L EPA 6010D 07/11/16 11:25Lead [7439-92-1] ^3.10 VLO10.03.10 U 101
ug/L EPA 6010D 07/11/16 11:25Nickel [7440-02-0] ^2.20 VLO10.019.0 J 501
ug/L EPA 6020B 07/11/16 12:14Selenium [7782-49-2] ^9.10 VLO30.09.10 UD 1010
ug/L EPA 6010D 07/11/16 11:25Silver [7440-22-4] ^1.90 VLO10.01.93 J 101
ug/L EPA 6020B 07/11/16 12:14Thallium [7440-28-0] ^1.10 VLO10.02.58 JD 5.510
ug/L EPA 6010D 07/11/16 11:25Vanadium [7440-62-2] ^1.40 VLO10.04.95 J 251
ug/L EPA 6010D 07/11/16 11:25Zinc [7440-66-6] ^4.40 VLO10.033.9 101
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6708-LeachateDescription:Lab Sample ID:CZ09642-01 07/01/16 10:46Received:
Matrix:Water Sampled:06/30/16 15:50 Work Order:CZ09642
Subtitle-D Landfill LeachateProject:Sampled By:Jacob Carpenter
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5210B-2001 07/01/16 14:06Biochemical Oxygen Demand^2000 JOC20004400 NE1
ug/L SM 5220D-1997 07/08/16 11:30Chemical Oxygen Demand^10000 JOC10000220000 NE1
NTU SM 2130B-2001 07/01/16 13:45Turbidity^10 MMR20130D NE20
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6G07019 - EPA 5030B_MS
Prepared: 07/07/2016 10:49 Analyzed: 07/07/2016 18:26Blank (6G07019-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 6G07019 - EPA 5030B_MS
Prepared: 07/07/2016 10:49 Analyzed: 07/07/2016 18:26Blank (6G07019-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9548
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10050
ug/L 50.0 59-134Surrogate: Toluene-d8 9146
Prepared: 07/07/2016 10:49 Analyzed: 07/07/2016 13:53LCS (6G07019-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1339218 1,1-Dichloroethene
ug/L1.0 20.0 81-1349419 Benzene
ug/L1.0 20.0 83-1179619 Chlorobenzene
ug/L1.0 20.0 71-1189319 Toluene
ug/L1.0 20.0 74-11910220 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9748
ug/L 50.0 59-134Surrogate: Toluene-d8 9346
Prepared: 07/07/2016 10:49 Analyzed: 07/07/2016 14:22Matrix Spike (6G07019-MS1)
Source: CZ10009-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 40.0 75-133900.21 U36 1,1-Dichloroethene
ug/L1.0 40.0 81-134920.15 U37 Benzene
ug/L1.0 40.0 83-117950.17 U38 Chlorobenzene
ug/L1.0 40.0 71-118910.14 U36 Toluene
ug/L1.0 40.0 74-1191000.15 U40 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9648
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9648
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 07/07/2016 10:49 Analyzed: 07/07/2016 14:52Matrix Spike Dup (6G07019-MSD1)
Source: CZ10009-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 40.0 2075-13385 60.21 U34 1,1-Dichloroethene
ug/L1.0 40.0 1781-13489 30.15 U36 Benzene
ug/L1.0 40.0 1683-11795 0.70.17 U38 Chlorobenzene
ug/L1.0 40.0 1771-11892 0.90.14 U37 Toluene
ug/L1.0 40.0 2274-11996 40.15 U39 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9447
ug/L 50.0 59-134Surrogate: Toluene-d8 9346
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G07018 - EPA 3005A
Prepared: 07/07/2016 09:55 Analyzed: 07/11/2016 11:34Blank (6G07018-BLK1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G07018 - EPA 3005A
Prepared: 07/07/2016 09:55 Analyzed: 07/11/2016 11:34Blank (6G07018-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.220 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 07/07/2016 09:55 Analyzed: 07/11/2016 11:37LCS (6G07018-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120108216 Antimony
ug/L3.00 200 80-120113227 Selenium
ug/L1.00 200 80-120119239 Thallium
Prepared: 07/07/2016 09:55 Analyzed: 07/11/2016 11:44Matrix Spike (6G07018-MS1)
Source: CZ09890-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251070.259214 Antimony
ug/L3.00 200 75-125900.910 U179 Selenium
ug/L1.00 200 75-1251140.110 U228 Thallium
Prepared: 07/07/2016 09:55 Analyzed: 07/11/2016 11:48Matrix Spike Dup (6G07018-MSD1)
Source: CZ09890-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125108 10.259217 Antimony
ug/L3.00 200 2075-12589 0.60.910 U178 Selenium
ug/L1.00 200 2075-125113 0.90.110 U226 Thallium
Prepared: 07/07/2016 09:55 Analyzed: 07/11/2016 11:52Post Spike (6G07018-PS1)
Source: CZ09890-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201070.259214 Antimony
ug/L3.00 200 80-1201110.0979221 Selenium
ug/L1.00 200 80-1201110.100223 Thallium
Batch 6G08010 - EPA 3005A
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:40Blank (6G08010-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.100 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G08010 - EPA 3005A
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:40Blank (6G08010-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:46LCS (6G08010-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12098197 Arsenic
ug/L10.0 200 80-12098195 Barium
ug/L1.00 20.0 80-1209819.6 Beryllium
ug/L1.00 20.0 80-1209919.8 Cadmium
ug/L10.0 200 80-12097195 Chromium
ug/L10.0 200 80-12098196 Cobalt
ug/L10.0 200 80-12098196 Copper
ug/L10.0 200 80-12098197 Lead
ug/L10.0 200 80-12099198 Nickel
ug/L10.0 200 80-120100200 Silver
ug/L10.0 200 80-12099197 Vanadium
ug/L10.0 200 80-120100199 Zinc
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:53Matrix Spike (6G08010-MS1)
Source: CZ09890-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-1251026.80 U203 Arsenic
ug/L10.0 200 75-1259822.8218 Barium
ug/L1.00 20.0 75-125990.100 U19.7 Beryllium
ug/L1.00 20.0 75-125970.360 U19.5 Cadmium
ug/L10.0 200 75-125981.40 U195 Chromium
ug/L10.0 200 75-125981.10 U196 Cobalt
ug/L10.0 200 75-125951.60 U191 Copper
ug/L10.0 200 75-125983.10 U196 Lead
ug/L10.0 200 75-1251002.20 U199 Nickel
ug/L10.0 200 75-1251001.90 U200 Silver
ug/L10.0 200 75-1251001.40 U200 Vanadium
ug/L10.0 200 75-125984.40 U197 Zinc
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:55Matrix Spike Dup (6G08010-MSD1)
Source: CZ09890-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125102 0.26.80 U204 Arsenic
ug/L10.0 200 2075-12599 122.8221 Barium
ug/L1.00 20.0 2075-125100 10.100 U19.9 Beryllium
ug/L1.00 20.0 2075-125100 30.360 U20.0 Cadmium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 6G08010 - EPA 3005A
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:55Matrix Spike Dup (6G08010-MSD1) Continued
Source: CZ09890-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-12599 11.40 U198 Chromium
ug/L10.0 200 2075-125101 31.10 U202 Cobalt
ug/L10.0 200 2075-12596 11.60 U193 Copper
ug/L10.0 200 2075-125101 33.10 U202 Lead
ug/L10.0 200 2075-125101 12.20 U202 Nickel
ug/L10.0 200 2075-125101 0.91.90 U202 Silver
ug/L10.0 200 2075-125101 11.40 U202 Vanadium
ug/L10.0 200 2075-12599 0.84.40 U199 Zinc
Prepared: 07/08/2016 09:04 Analyzed: 07/11/2016 10:57Post Spike (6G08010-PS1)
Source: CZ09890-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-1201000.0008910.201 Arsenic
mg/L0.0100 0.200 80-120960.02280.215 Barium
mg/L0.00100 0.0200 80-120973.21E-50.0194 Beryllium
mg/L0.00100 0.0200 80-12097-0.0002750.0194 Cadmium
mg/L0.0100 0.200 80-12096-0.0004830.193 Chromium
mg/L0.0100 0.200 80-12098-0.0009100.196 Cobalt
mg/L0.0100 0.200 80-12094-0.0003050.187 Copper
mg/L0.0100 0.200 80-12098-0.004680.196 Lead
mg/L0.0100 0.200 80-12099-3.51E-50.197 Nickel
mg/L0.0100 0.200 80-12099-0.0003730.198 Silver
mg/L0.0100 0.200 80-120980.001100.197 Vanadium
mg/L0.0100 0.200 80-12099-0.0005450.198 Zinc
Classical Chemistry Parameters - Quality Control
Batch 6G01024 - NO PREP
Prepared & Analyzed: 07/01/2016 14:06Blank (6G01024-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L20002000U Biochemical Oxygen Demand
Prepared & Analyzed: 07/01/2016 14:06LCS (6G01024-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2000 198000 85-115104210000 Biochemical Oxygen Demand
Prepared & Analyzed: 07/01/2016 14:06Duplicate (6G01024-DUP1)
Source: CZ08551-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2000 304240000240000 Biochemical Oxygen Demand
Page 12 of 15
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www.encolabs.com
QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 6G01026 - NO PREP
Prepared & Analyzed: 07/01/2016 13:45Blank (6G01026-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.00.50 U Turbidity
Prepared & Analyzed: 07/01/2016 13:45LCS (6G01026-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU1.0 20.0 90-1109920 Turbidity
Prepared & Analyzed: 07/01/2016 13:45Duplicate (6G01026-DUP1)
Source: CZ09642-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
NTU20 250.5130130D Turbidity
Batch 6G07036 - Same
Prepared: 07/07/2016 15:02 Analyzed: 07/08/2016 11:30Blank (6G07036-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000010000U Chemical Oxygen Demand
Prepared: 07/07/2016 15:02 Analyzed: 07/08/2016 11:30LCS (6G07036-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 90-110100500000 Chemical Oxygen Demand
Prepared: 07/07/2016 15:02 Analyzed: 07/08/2016 11:30Matrix Spike (6G07036-MS1)
Source: CZ05789-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L40000 2000000 90-1101037200002800000 Chemical Oxygen Demand
Prepared: 07/07/2016 15:02 Analyzed: 07/08/2016 11:30Matrix Spike Dup (6G07036-MSD1)
Source: CZ05789-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L40000 2000000 1090-110104 0.97200002800000 Chemical Oxygen Demand
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
The Reporting Limits for this analysis are elevated due to sample foaming.R-04
Page 14 of 15
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AH/BC Navy JV, LLC.
APPENDIX C
15A NCAC Solid Waste Reporting Limits /
SWSL Limits

(12 PAGES)

Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
CAS Number Name Other Names 2L Std.GWP* Std.SWSL**SW ID App I
* GWP = Groundwater Protection
** SWSL = Solid Waste Last updated: 6/13/2011 8:19:15 AM
630-20-6 1,1,1,2-Tetrachloroethane Ethane, 1,1,1,2-tetrachloro-NE 1 5 190 I
71-55-6 1,1,1-Trichloroethane;Ethane, 1,1,1-trichloro-200 --1 200 I
79-34-5 1,1,2,2-Tetrachloroethane Ethane, 1,1,2,2-tetrachloro-0.2 0.18 3 191 I
79-00-5 1,1,2-Trichloroethane Ethane, 1,1,2-trichloro-NE 0.6 1 202 I
76-13-1 1,1,2-Trichlorotrifluoroethane CFC-113 200000 NE NE 398
92-52-4 1,1-biphenyl 1,1-biphenyl 400 --10 421
75-34-3 1,1-Dichloroethane; Ethyldidene Ethane, 1,1-dichloro-6 --5 75 I
75-35-4 1,1-Dichloroethylene; 1,1-Ethene, 1,1-dichloro-7 --5 77 I
563-58-6 1,1-Dichloropropene 1-Propene, 1,1-dichloro-NE NE 5 85
96-18-4 1,2,3-Trichloropropane Propane, 1,2,3-trichloro-0.005 --1 206 I
95-94-3 1,2,4,5-Tetrachlorobenzene Benzene, 1,2,4,5-tetrachloro-NE 2 10 189
120-82-1 1,2,4-Trichlorobenzene Benzene, 1,2,4-trichloro-70 70 10 199
95-63-6 1,2,4-Trimethylbenzene Pseudocumene 400 NE NE 372
226-36-8 1,2,5,6-Dibenzacridine NE NE NE 385
96-12-8 1,2-Dibromo-3-chloropropane; DBCP Propane, 1,2-dibromo-3-chloro-0.04 --13 67 I
106-93-4 1,2-Dibromoethane; Ethylene dibromide;Ethane, 1,2-dibromo-0.02 --1 68 I
107-06-2 1,2-Dichloroethane; Ethylene Ethane, 1,2-dichloro-0.4 --1 76 I
540-59-0 1,2-Dichloroethylene mixed isomers Mixed Isomers NE 60 NE 481
78-87-5 1,2-Dichloropropane Propane, 1,2-dichloro-0.6 --1 82 I
122-66-7 1,2-Diphenylhydrazine NE NE NE 394
108-67-8 1,3,5-Trimethylbenzene)Mesitylene 400 NE NE 373
142-28-9 1,3-Dichloropropane; Trimethylene Propane, 1,3-dichloro-NE NE 1 83
106-37-6 1,4-Dibromobenzene p-Dibromobenzene, p-Bromobenzene 70 471
123-91-1 1,4-dioxane 1,4-dioxane 3 --10 422
130-15-4 1,4-Naphthoquinone 1,4-Naphthalenedione NE NE 10 149
87-61-6 1-2-3-Trichlorobenzene NE NE NE 371
90-12-0 1-Methylnaphthalene α-methylnaphthalene NE 1 NE 503
134-32-7 1-Naphthylamine 1-Naphthalenamine NE NE 10 150
120-36-5 2-(2-4-dichlorophenoxy)propionic NE NE NE 352
594-20-7 2,2-Dichloropropane; Isopropylidene Propane, 2,2-dichloro-NE NE 15 84
1
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
58-90-2 2,3,4,6-Tetrachlorophenol Phenol, 2,3,4,6-tetrachloro-200 --10 193
93-76-5 2,4,5-T; 2,4,5-Trichlorophenoxyacetic Acetic acid, (2,4,5-trichlorophenoxy)-NE NE 2 188
93-72-1 2,4,5-TP Acid Silvex 50 NE NE 452
95-95-4 2,4,5-Trichlorophenol Phenol, 2,4,5-trichloro-NE 63 10 204
88-06-2 2,4,6-Trichlorophenol Phenol, 2,4,6-trichloro-NE 4 10 205
94-75-7 2,4-D; 2,4-Dichlorophenoxyacetic Acetic acid, (2,4-dichlorophenoxy)-70 --2 59
120-83-2 2,4-Dichlorophenol Phenol, 2,4-dichloro-NE 0.98 10 80
105-67-9 2,4-Dimethylphenol; m-Xylenol Phenol, 2,4-dimethyl-100 --10 95
51-28-5 2,4-Dinitrophenol Phenol, 2,4-dinitro-NE NE 50 99
121-14-2 2,4-Dinitrotoluene Benzene, 1-methyl-2,4-dinitro-NE 0.1 10 100
87-65-0 2,6-Dichlorophenol Phenol, 2,6-dichloro-NE NE 10 81
606-20-2 2,6-Dinitrotoluene Benzene, 2-methyl-1,3-dinitro-NE NE 10 101
94-82-6 2-4 DB NE NE NE 350
53-96-3 2-Acetylaminofluorene; 2-AAF Acetamide, N-9H-fluoren-2-yl-NE NE 20 6
110-75-8 2-Chloroethylvinyl ether NE NE NE 358
91-58-7 2-Chloronaphthalene Naphthalene, 2-chloro-NE NE 10 47
95-57-8 2-Chlorophenol Phenol, 2-chloro-0.4 --10 48
591-78-6 2-Hexanone; Methyl butyl ketone 2-Hexanone NE 40 50 124 I
91-57-6 2-Methylnaphthalene Naphthalene, 2-methyl-30 --10 145
91-59-8 2-Naphthylamine 2-Naphthalenamine NE NE 10 151
109-06-8 2-Picoline NE NE NE 390
91-94-1 3,3'-Dichlorobenzidine [1,1'-Biphenyl]-4,4'-diamine,3,3'-NE NE 20 72
119-93-7 3,3'-Dimethylbenzidine [1,1'-Biphenyl]-4,4'-diamine,3,3'-NE NE 10 94
56-49-5 3-Methylcholanthrene Benz[j]aceanthrylene,1,2-dihydro-3-NE NE 10 138
72-54-8 4,4'-DDD Benzene 1,1'-(2,2-0.1 --0.1 60
72-55-9 4,4'-DDE Benzene, 1,1'-NE NE 0.1 61
50-29-3 4,4'-DDT Benzene, 1,1'-(2,2,2-0.1 --0.1 62
534-52-1 4,6-Dinitro-o-cresol; 4,6-Dinitro-2-Phenol, 2-methyl-4,6-dinitro-NE NE 50 98
92-67-1 4-Aminobiphenyl [1,1'-Biphenyl]-4-amine NE NE 20 11
460-00-4 4-Bromofluorobenzene NE NE NE 463
101-55-3 4-Bromophenyl phenyl ether Benzene, 1-bromo-4-phenoxy-NE NE 10 31
7005-72-3 4-Chlorophenyl phenyl ether Benzene, 1-chloro-4-phenoxy-NE NE 10 49
108-10-1 4-Methyl-2-pentanone; Methyl isobutyl 2-Pentanone, 4-methyl-NE 560 100 147 I
56-57-5 4-nitroquinoline-1-oxide NE NE NE 388
2
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
99-55-8 5-Nitro-o-toluidine Benzenamine, 2-methyl-5-nitro-NE NE 10 157
57-97-6 7,12-Dimethylbenz[a]anthracene Benz[a]anthracene, 7,12-dimethyl-NE NE 10 93
83-32-9 Acenaphthene Acenaphthylene, 1,2-dihydro-80 --10 1
208-96-8 Acenaphthylene Acenaphthylene 200 --10 2
SW416 Acetic Acid Acetic Acid NE NE NE 416
34256-82-1 Acetochlor 100 490
187022-11-3 Acetochlor ESA 1000 491
184992-44-4 Acetochlor OXA 1000 492
67-64-1 Acetone 2-Propanone 6000 --100 3 I
75-05-8 Acetonitrile; Methyl cyanide Acetonitrile NE 42 55 4
98-86-2 Acetophenone Ethanone, 1-phenyl-NE 700 10 5
50594-66-6 Acifluorofen Acifluorofen 453
107-02-8 Acrolein 2-Propenal NE 4 53 7
79-06-1 Acrylamide Acrylamide 0.008 --NE 429
107-13-1 Acrylonitrile 2-Propenenitrile NE NE 200 8 I
15972-60-8 Alachlor 0.4 469
309-00-2 Aldrin 1,4:5,8-NE 0.002 0.05 9
SW337 Alkalinity NE NE NE 337
107-05-1 Allyl chloride 1-Propene, 3-chloro-NE NE 10 10
319-84-6 alpha-BHC Cyclohexane,1,2,3,4,5,6-hexachloro-NE 0.006 0.05 24
319-84-6 alpha-Hexachlorocyclohexane α-Benzenehexachloride NE 0.006 NE 501
--Aluminum Aluminum NE 3500 NE 454
7429-90-5 Aluminum NE 3500 NE 438
7664-41-7 Ammonia Ammonia NE 1500 NE 435
62-53-3 Aniline NE NE NE 381
120-12-7 Anthracene Anthracene 2000 --10 12
7440-36-0 Antimony Antimony NE 1 6 13 I
140-57-8 Aramite NE NE NE 382
12674-11-2 Aroclor 1016 congener of PCB; see (1336-36-3)NE NE NE 401
11104-28-2 Aroclor 1221 congener of PCB; see (1336-36-3)NE NE NE 402
11141-16-5 Aroclor 1232 congener of PCB; see (1336-36-3)NE NE NE 403
53469-21-9 Aroclor 1242 congener of PCB; see (1336-36-3)NE NE NE 404
12672-29-6 Aroclor 1248 congener of PCB; see (1336-36-3)NE NE NE 405
11097-69-1 Aroclor 1254 congener of PCB; see (1336-36-3)NE NE NE 406
3
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
11096-82-5 Aroclor 1260 congener of PCB; see (1336-36-3)NE NE NE 407
7440-38-2 Arsenic Arsenic 10 --10 14 I
7440-39-3 Barium Barium 700 --100 15 I
25057-89-0 Bentazon NE NE NE 462
100-52-7 Benzaldehyde Phenylmethanal,NE 700 NE 496
71-43-2 Benzene Benzene 1 --1 16 I
122-09-8 Benzeneethanamine, alpha,alpha- NE NE NE 386
92-87-5 Benzidine NE NE NE 383
56-55-3 Benzo[a]anthracene;Benz[a]anthracene 0.05 --10 17
50-32-8 Benzo[a]pyrene Benzo[a]pyrene 0.005 --10 21
205-99-2 Benzo[b]fluoranthene Benz[e]acephenanthrylene 0.05 --10 18
191-24-2 Benzo[ghi]perylene Benzo[ghi]perylene 200 --10 20
207-08-9 Benzo[k]fluoranthene Benzo[k]fluoranthene 0.5 --10 19
65-85-0 Benzoic Acid 30000 28000 NE 395
100-51-6 Benzyl alcohol Benzenemethanol NE 700 20 22
7440-41-7 Beryllium Beryllium NE 4 1 23 I
319-85-7 beta-BHC Cyclohexane,1,2,3,4,5,6-hexachloro-NE 0.019 0.05 25
319-85-7 beta-Hexachlorocyclohexane β-Benzenehexachloride NE 0.02 NE 502
SW347 Bicarbonate (as CaCO3) NE NE NE 347
SW316 Biological Oxygen Demand BOD NE NE NE 316
101-84-8 biphenyl ether biphenyl ether NE NE 10 423
108-60-1 Bis(2-chloro-1-methylethyl) ether; 2,2'-Propane, 2,2'-oxybis[1-chloro-NE NE 10 46
111-91-1 Bis(2-chloroethoxy)methane Ethane, 1,1'-[methylenebis(oxy)]bis [2-NE NE 10 42
111-44-4 Bis(2-chloroethyl)ether; Dichloroethyl Ethane, 1,1'-oxybis[2-chloro-NE 0.031 10 43
39638-32-9 Bis(2-chloroisopropyl) ether 0.03 NE NE 384
117-81-7 Bis(2-ethylhexyl) phthalate 1,2-Benzenedicarboxylic acid, bis(2-3 NE 15 111
7440-42-8 Boron Boron 700 --NE 428
108-86-1 Bromobenzene NE NE NE 360
74-97-5 Bromochloromethane;Methane, bromochloro-NE 0.6 3 28 I
75-27-4 Bromodichloromethane;Methane, bromodichloro-0.6 --1 29 I
75-25-2 Bromoform; Tribromomethane Methane, tribromo-4 --3 30 I
71-36-3 Butanol n n-Butyl Alcohol NE 700 470
78-92-2 Butanol sec sec-Butyl Alcohol NE 10000 483
85-68-7 Butyl benzyl phthalate; Benzyl butyl 1,2-Benzenedicarboxylicacid, butyl 1000 --10 32
4
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
SW418 Butyric Acid Butyric Acid NE NE NE 418
7440-43-9 Cadmium Cadmium 2 --1 34 I
7440-70-2 Calcium NE NE NE 375
471-34-1 Calcium carbonate NE NE NE 464
105-60-2 Caprolactam 4000 NE NE 440
86-74-8 Carbazole dibenzopyrrole, diphenylenimine,NE 2 NE 497
1563-66-2 Carbofuran Carbofuran 40 NE NE 430
124-38-9 Carbon Dioxide NE NE NE 459
SW413 Carbon Dioxide (CO2)CO2 Gas NE NE NE 413
75-15-0 Carbon disulfide Carbon disulfide 700 --100 35 I
56-23-5 Carbon tetrachloride Methane, tetrachloro-0.3 --1 36 I
SW348 Carbonate (as CaCO3) NE NE NE 348
7440-44-0 Charcoal NE NE NE 466
SW317 Chemical Oxygen Demand COD NE NE NE 317
57-74-9 Chlordane 4,7-Methano-1H-indene,1,2,4,5,6,7,8,8-0.1 --0.5 339
12789-03-6 Chlordane (constituents) NE NE NE 400
5103-71-9 Chlordane, alpha cis-Chlordane NE NE NE 379
5103-74-2 Chlordane, beta trans-Chlordane NE NE NE 378
5566-34-7 Chlordane, gamma NE NE NE 399
16887-00-6 Chloride Chloride 455
SW301 Chloride 250000 --NE 301
108-90-7 Chlorobenzene Benzene, chloro-50 --3 39 I
510-15-6 Chlorobenzilate Benzeneacetic acid, 4-chloro-(4-NE NE 10 40
75-00-3 Chloroethane; Ethyl chloride Ethane, chloro-3000 --10 41 I
67-66-3 Chloroform; Trichloromethane Methane, trichloro-70 --5 44 I
126-99-8 Chloroprene 1,3-Butadiene, 2-chloro-NE NE 20 50
7440-47-3 Chromium Chromium 10 --10 51 I
218-01-9 Chrysene Chrysene 5 --10 52
156-59-2 cis-1,2-Dichloroethylene; cis-1,2-Ethene, 1,2-dichloro-,(Z)-70 --5 78 I
10061-01-5 cis-1,3-Dichloropropene 1-Propene, 1,3-dichloro-, (Z)-0.4 --1 86 I
7440-48-4 Cobalt Cobalt NE 1 10 53 I
SW309 Coliform (total) 1 NE NE 309
SW310 Color (color units) 15 NE NE 310
7440-50-8 Copper Copper 1000 --10 54 I
5
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
57-12-5 Cyanide Cyanide 70 --10 58
75-99-0 Dalapon NE 200 NE 355
3424-82-6 DDE o,p-DDE 0.1 472
319-86-8 delta-BHC Cyclohexane,1,2,3,4,5,6-hexachloro-NE 0.019 0.05 26
SW318 Depth To Water (ft)DTW NE NE NE 318
117-81-7 Di(2-ethylhexyl)phthalate Di(2-ethylhexyl)phthalate, DEHP 2.5 --NE 431
2303-16-4 Diallate Carbamothioic acid,bis(1-methylethyl)-,NE NE 10 63
53-70-3 Dibenz[a,h]anthracene Dibenz[a,h]anthracene 0.005 --10 64
132-64-9 Dibenzofuran Dibenzofuran NE 28 10 65
124-48-1 Dibromochloromethane;Methane, dibromochloro-0.4 0.41 3 66 I
1918-00-9 Dicamba NE NE NE 353
79-43-6 Dichloroacetic Acid NE 0.7 NE 480
75-71-8 Dichlorodifluoromethane; CFC 12 Methane,dichlorodifluoro-1000 --5 74
60-57-1 Dieldrin 2,7:3,6-Dimethanonaphth[2,3-0.002 --0.075 88
84-66-2 Diethyl phthalate 1,2-Benzenedicarboxylicacid, diethyl 6000 --10 90
60-51-5 Dimethoate Phosphorodithioic acid,O,O-dimethyl S-NE NE 20 91
131-11-3 Dimethyl phthalate 1,2-Benzenedicarboxylicacid, dimethyl NE NE 10 96
84-74-2 Di-n-butyl phthalate 1,2-Benzenedicarboxylic acid, dibutyl 700 --10 33
117-84-0 Di-n-octyl phthalate 1,2-Benzenedicarboxylicacid, dioctyl 100 --10 168
88-85-7 Dinoseb; DNBP; 2-sec-Butyl-4,6-Phenol, 2-(1-methylpropyl)-4,6-dinitro-NE 7 1 102
1746-01-6 Dioxin 2,3,7,8-TCDD 0.2 NE NE 441
101-84-8 Diphenyl ether Diphenyl oxide; 1,1'-Oxybisbenzene;NE 100 NE 498
122-39-4 Diphenylamine Benzenamine, N-phenyl-NE NE 10 103
85-00-7 Diquat 20 473
74-82-8 Dissolved Methane Dissolved Methane 456
7782-44-7 Dissolved Oxygen NE NE NE 356
298-04-4 Disulfoton Phosphorodithioic acid,O,O-diethyl S-[2-0.3 --10 104
3648-20-2 Diundecyl phthalate Santicizer 711 100 NE NE 442
959-98-8 Endosulfan I 6,9-Methano-2,4,3-benzodiox-40 NE 0.1 105
33213-65-9 Endosulfan II 6,9-Methano-2,4,3---42 0.1 106
1031-07-8 Endosulfan sulfate 6,9-Methano-2,4,3-NE 40 0.1 107
145-73-3 Endothall 100 474
72-20-8 Endrin 2,7:3,6-Dimethanonaphth[2,3-b]oxirene,2 --0.1 108
7421-93-4 Endrin aldehyde 1,2,4-Methenocyclo-penta[cd]pentalene-2 --0.1 109
6
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
106-89-8 Epichlorohydrin 4 NE NE 443
74-84-0 Ethane- Dissolved NE NE NE 331
64-17-5 Ethanol Ethyl alcohol, Ethyl hydrate,NE 4000 NE 499
74-85-1 Ethene- Dissolved NE NE NE 332
141-78-6 Ethyl acetate 3000 NE NE 444
97-63-2 Ethyl methacrylate 2-Propenoic acid, 2-methyl-, ethyl NE NE 10 112
62-50-0 Ethyl methanesulfonate Methanesulfonic acid,ethyl ester NE NE 20 113
637-92-3 Ethyl tert-butyl ether ETBE, Ethyl tertiary butyl ether NE 47 NE 500
100-41-4 Ethylbenzene Benzene, ethyl-600 --1 110 I
107-21-1 ethylene glycol ethylene glycol 10000 --10,000 424
52-85-7 Famphur Phosphorothioic acid, O-[4-NE NE 20 114
SW334 Ferrous Iron- Dissolved NE NE NE 334
206-44-0 Fluoranthene Fluoranthene 300 --10 115
86-73-7 Fluorene 9H-Fluorene 300 --10 116
16984-48-8 Fluoride 2000 --2000 312
SW313 Foaming Agents 500 --NE 313
50-00-0 Formaldehyde 600 NE NE 445
59-89-9 gamma-BHC (Lindane)gamma-BHC (Lindane) 457
58-89-9 gamma-BHC; Lindane Cyclohexane,1,2,3,4,5,6-hexachloro-0.03 --0.05 27
SW314 Gross Alpha 15 NE NE 314
SW427 Groundwater Elevation (feet)GW Elevation (feet)NE NE NE 427
SW319 Head (ft mean sea level) NE NE NE 319
76-44-8 Heptachlor 4,7-Methano-1H-indene,1,4,5,6,7,8,8-0.008 --0.05 117
1024-57-3 Heptachlor epoxide 2,5-Methano-2H-indeno[1,2-0.004 --0.075 118
142-82-5 Heptane Heptane 400 --NE 432
118-74-1 Hexachlorobenzene Benzene, hexachloro-0.02 --10 119
87-68-3 Hexachlorobutadiene 1,3-Butadiene,1,1,2,3,4,4-hexachloro-0.4 0.44 10 120
608-73-1 Hexachlorocyclohexane isomers 0.02 NE NE 446
77-47-4 Hexachlorocyclopentadiene 1,3-Cyclopentadiene,1,2,3,4,5,5-NE 50 10 121
67-72-1 Hexachloroethane Ethane, hexachloro-NE 2.5 10 122
70-30-4 Hexachlorophene NE NE NE 387
1888-71-7 Hexachloropropene 1-Propene, 1,1,2,3,3,3-hexachloro-NE NE 10 123
142-62-1 Hexanoic Acid NE NE NE 485
133-74-0 Hydrogen Gas Dissolved Hydrogen Gas NE NE NE 420
7
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
SW338 Hydrogen Sulfide NE NE NE 338
646-07-1 i-Hexonic Acid NE NE NE 486
193-39-5 Indeno(1,2,3-cd)pyrene Indeno[1,2,3-cd]pyrene 0.05 --10 125
503-74-2 i-Pentanoic Acid NE NE NE 488
7439-89-6 Iron 300 --300 340
78-83-1 Isobutyl alcohol 1-Propanol, 2-methyl-NE NE 100 126
465-73-6 Isodrin 1,4,5,8-Dimethanonaphthalene,1,2,3,4,1 NE NE 20 127
78-59-1 Isophorone 2-Cyclohexen-1-one,3,5,5-trimethyl-40 --10 128
108-20-3 Isopropyl ether 70 --NE 366
98-82-8 Isopropylbenzene 70 --NE 367
120-58-1 Isosafrole 1,3-Benzodioxole, 5-(1-propenyl)-NE NE 10 129
143-50-0 Kepone 1,3,4-Metheno-2H-cyclobuta-NE NE 20 130
SW415 Lactic Acid Lactic Acid NE NE NE 415
SW329 Landfill Gas LFG NE NE NE 329
7439-92-1 Lead Lead 15 --10 131 I
SW374 m-&p-Cresol (combined) NE NE NE 374
SW359 m-&p-Xylene (combined) NE NE NE 359
7439-95-4 Magnesium NE NE NE 376
7439-96-5 Manganese 50 --50 342
SW335 Manganese- Dissolved 50 --50 335
94-74-6 MCPA NE NE NE 351
108-39-4 m-Cresol; 3-Methylphenol Phenol, 3-methyl-400 --10 345
541-73-1 m-Dichlorobenzene; 1,3-Benzene, 1,3-dichloro-200 --5 70
99-65-0 m-Dinitrobenzene Benzene, 1,3-dinitro-NE NE 20 97
93-65-2 Mecopop, MCPP NE NE NE 354
7439-97-6 Mercury Mercury 1 --0.2 132
126-98-7 Methacrylonitrile 2-Propenenitrile, 2-methyl-NE NE 100 133
SW333 Methane- Dissolved NE NE NE 333
67-56-1 Methanol 4000 NE NE 448
91-80-5 Methapyrilene 1,2,Ethanediamine, N,N-dimethyl-N'-2-NE NE 100 134
72-43-5 Methoxychlor Benzene, 1,1'-40 --1 135
72-43-5 Methoxychlor 40 NE NE 449
74-83-9 Methyl bromide; Bromomethane Methane, bromo-NE 10 10 136 I
74-87-3 Methyl chloride; Chloromethane Methane, chloro-3 --1 137 I
8
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
78-93-3 Methyl ethyl ketone; MEK; 2-2-Butanone 4000 --100 141 I
74-88-4 Methyl iodide; Iodomethane Methane, iodo-NE NE 10 142 I
108-10-1 Methyl Isobutyl Ketone 100 493
80-62-6 Methyl methacrylate 2-Propenoic acid, 2-methyl-, methyl NE 25 30 143
66-27-3 Methyl methanesulfonate Methanesulfonic acid,methyl ester NE NE 10 144
298-00-0 Methyl parathion; Parathion methyl Phosphorothioic acid,O,O-dimethyl NE NE 10 146
2037-26-5 Methylbenzene NE NE NE 461
74-95-3 Methylene bromide;Methane, dibromo-NE 70 10 139 I
75-09-2 Methylene chloride;Methane, dichloro-5 --1 140 I
1634-04-4 Methyl-tert-butyl ether (MTBE) 20 --NE 369
99-09-2 m-Nitroaniline; 3-Nitroaniline Benzenamine, 3-nitro-NE NE 50 153
7439-98-7 Molybdenum NE NE NE 397
108-38-3 m-Xylene NE NE NE 409
91-20-3 Naphthalene Naphthalene 6 --10 148
104-51-8 n-Butylbenzene 70 --NE 361
110-54-3 n-Hexane 400 NE NE 447
7440-02-0 Nickel Nickel 100 --50 152 I
14797-55-8 Nitrate (as N) 10000 --10000 303
14797-65-0 Nitrite (as N) 1000 --1000 304
98-95-3 Nitrobenzene Benzene, nitro-NE NE 10 156
7727-37-9 Nitrogen NE NE NE 467
55-18-5 N-Nitrosodiethylamine Ethanamine, N-ethyl-N-nitroso-NE NE 20 160
62-75-9 N-Nitrosodimethylamine Methanamine, N-methyl-N-nitroso-0.0007 --10 161
924-16-3 N-Nitrosodi-n-butylamine 1-Butanamine, N-butyl-N-nitroso-NE NE 10 162
86-30-6 N-Nitrosodiphenylamine Benzenamine, N-nitroso-N-phenyl-NE NE 10 163
SW426 N-N-NE NE 10 426
SW439 N- NE NE NE 439
621-64-7 N-Nitrosodipropylamine; N-Nitroso-N-1-Propanamine, N-nitroso-N-propyl-NE NE 10 164
10595-95-6 N-Nitrosomethylethalamine Ethanamine, N-methyl-N-nitroso-NE NE 10 165
59-89-2 N-Nitrosomorpholine NE NE NE 389
100-75-4 N-Nitrosopiperidine Piperidine, 1-nitroso-NE NE 20 166
930-55-2 N-Nitrosopyrrolidine Pyrrolidine, 1-nitroso-NE NE 10 167
SW419 No2/No3 (nitrate & nitrite reported NOX NE NE NE 419
103-65-1 n-Propylbenzene 70 NE NE 370
9
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
126-68-1 O,O,O-Triethyl phosphorothioate Phosphorothioic acid,O,O,O-triethyl NE NE 10 207
297-97-2 O,O-Diethyl O-2-pyrazinyl Phosphorothioic acid,O,O-diethyl O-NE NE 20 89
136777-61-2 o,p-Xylene NE NE NE 460
95-49-8 o-Chlorotoluene 2-chlorotoluene 100 NE NE 364
95-48-7 o-Cresol; 2-Methylphenol Phenol, 2-methyl-NE 400 10 56
95-50-1 o-Dichlorobenzene; 1,2-Benzene, 1,2-dichloro-20 --5 69 I
88-74-4 o-Nitroaniline; 2-Nitroaniline Benzenamine, 2-nitro-NE NE 50 154
88-75-5 o-Nitrophenol; 2-Nitrophenol Phenol, 2-nitro-NE NE 10 158
SW437 Orthophosphate Phosphorus NE NE NE 437
95-53-4 o-Toluidine Benzenamine, 2-methyl-NE NE 10 197
23135-22-0 Oxamyl 200 NE NE 450
SW336 Oxygen Reduction Potential (mV)ORP NE NE NE 336
96-47-6 o-Xylene NE NE NE 408
60-11-7 p-(Dimethylamino)azobenzene Benzenamine, N,N-dimethyl-4-NE NE 10 92
56-38-2 Parathion Phosphorothioic acid,O,O-diethyl-O-(4-NE NE 10 169
106-47-8 p-Chloroaniline Benzenamine, 4-chloro-NE NE 20 38
59-50-7 p-Chloro-m-cresol; 4-Chloro-3-Phenol, 4-chloro-3-methyl-NE NE 20 45
106-43-4 p-Chlorotoluene NE 24 NE 365
106-44-5 p-Cresol; 4-Methylphenol Phenol, 4-methyl-40 NE--10 344
99-87-6 p-Cymene NE 25 NE 368
106-46-7 p-Dichlorobenzene; 1,4-Benzene, 1,4-dichloro-6 --1 71 I
608-93-5 Pentachlorobenzene Benzene, pentachloro-NE NE 10 171
76-01-7 Pentachloroethane NE NE NE 380
82-68-8 Pentachloronitrobenzene Benzene,pentachloronitro-NE NE 20 172
87-86-5 Pentachlorophenol Phenol, pentachloro-0.3 --25 173
109-52-4 Pentanoic Acid NE NE NE 487
7790-98-9 Perchlorate and Perchlorate Salts 2 494
335-67-1 Perfluorooctanoic acid PFOA, C8 2 484
SW307 petroleum aliphatic carbon fraction class 10000 --NE 307
SW305 petroleum aliphatic carbon fraction class 400 --NE 305
SW306 petroleum aliphatic carbon fraction class 700 --NE 306
SW308 petroleum aromatics carbon fraction 200 --NE 308
SW320 pH (field) NE NE NE 320
SW321 pH (lab) NE NE NE 321
10
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
62-44-2 Phenacetin Acetamide, N-(4-ethoxyphenyl)NE NE 20 174
85-01-8 Phenanthrene Phenanthrene 200 --10 175
108-95-2 Phenol Phenol 30 --10 177
298-02-2 Phorate Phosphorodithioic acid,O,O-diethyl S-1 --10 178
96-91-3 Picramic Acid 2-amino-4,6-dinitiphenol NE 0.7 NE 482
100-01-6 p-Nitroaniline; 4-Nitroaniline Benzenamine, 4-nitro-NE NE 20 155
100-02-7 p-Nitrophenol; 4-Nitrophenol Phenol, 4-nitro-NE NE 50 159
1336-36-3 Polychlorinated biphenyls; PCBs 1,1'-Biphenyl,chloro derivatives Method NE 0.09 2 434
9/7/7440 Potassium NE NE NE 377
106-50-3 p-Phenylenediamine 1,4-Benzenediamine NE NE 10 176
23950-58-5 Pronamide Benzamide, 3,5-dichloro-N-(1,1-NE NE 10 179
SW417 Propionic Acid Propionic Acid NE NE NE 417
107-12-0 Propionitrile; Ethyl cyanide Propanenitrile NE NE 150 180
57-55-6 Propylene Glycol NE 140,000 NE 507
106-42-3 p-Xylene NE NE NE 410
129-00-0 Pyrene Pyrene 200 --10 181

110-86-1 Pyridine NE 7 NE 391
SW414 Pyruvic Acid Pyruvic Acid NE NE NE 414
94-59-7 Safrole 1,3-Benzodioxole, 5-(2-propenyl)-NE NE 10 182
135-98-8 sec-Butylbenzene 70 --NE 362
7782-49-2 Selenium Selenium 20 --10 183 I
7440-22-4 Silver Silver 20 --10 184 I
93-72-1 Silvex; 2,4,5-TP Propanoic acid, 2-(2,4,5-50 --2 185
122-34-9 Simazine 4 NE NE 451
7440-23-5 Sodium NE 20000 NE 322
SW323 SpecCond (field) NE NE NE 323
SW324 SpecCond (lab) NE NE NE 324
7440-24-6 Strontium NE NE NE 465
100-42-5 Styrene Benzene, ethenyl-70 --1 186 I
14808-79-8 Sulfate 250000 --250000 315
18496-25-8 Sulfide Sulfide NE NE 1000 187
3689-24-5 Sulfotep NE NE NE 392
99-35-4 sym-Trinitrobenzene Benzene, 1,3,5-trinitro-NE NE 10 208
11
Appendix C Solid Waste Environmental Monitoring Reporting Limits and Standards
15A NCAC 2L and SWSL Limits
SW325 Temp (oC) NE NE NE 325
994-05-8 tert-Amyl methyl ether TAME, 2-methoxy-2-methylbutane NE 128 NE 504
98-06-6 tert-Butylbenzene 70 --NE 363
75-65-0 Tertiary Butyl Alcohol tert-butanol NE 10 NE 505
127-18-4 Tetrachloroethylene; Tetrachloroethene;Ethene, tetrachloro-0.7 --1 192 I
109-99-9 Tetrahydrofuran NE NE NE 458
7440-28-0 Thallium Thallium NE 0.28 5.5 194 I
7440-31-5 Tin Tin NE 2000 100 195
108-88-3 Toluene Benzene, methyl-600 --1 196 I
SW328 Top Of Casing (ft mean sea level)TOC NE NE NE 328
SW425 Total BHC NE 0.019 NE 425
SW311 Total Dissolved Solids TDS 500000 --NE 311
SW436 Total Fatty Acids Total Fatty Acids NE NE NE 436
E-10195 Total Organic Carbon NE NE NE 357
SW396 Total Organic Halides NE NE NE 396
7723-14-0 Total Phosphorus Total Phosphorus NE NE NE 412
SW343 Total Suspended Solids NE NE NE 343
SW411 Total Well Depth (ft)TD NE NE NE 411
8001-35-2 Toxaphene Toxaphene 0.03 --1.5 198
156-60-5 trans-1,2-Dichloroethylene; trans-1,2-Ethene, 1,2-dichloro-,(E)-100 --5 79 I
10061-02-6 trans-1,3-Dichloropropene 1-Propene, 1,3-dichloro-, (E)-0.4 --1 87 I
110-57-6 trans-1,4-Dichloro-2-butene 2-Butene, 1,4-dichloro-, (E)-NE NE 100 73 I
79-01-6 Trichloroethylene; Trichloroethene Ethene, trichloro-3 --1 201 I
75-69-4 Trichlorofluoromethane; CFC-11 Methane,trichlorofluoro-2000 --1 203 I
SW330 Turbidity NE NE NE 330
7440-62-2 Vanadium Vanadium NE 0.3 25 209 I
108-05-4 Vinyl acetate Acetic acid, ethenylester NE 88 50 210 I
75-01-4 Vinyl chloride; Chloroethene Ethene, chloro-0.03 --1 211 I
1330-20-7 Xylene (total)(o-,m-,and p-, Benzene, dimethyl 500 --5 346 I
7440-66-6 Zinc Zinc 1000 --10 213 I
12
AH/BC Navy JV, LLC.
APPENDIX D
Chemstat Output

(112 PAGES – PROVIDED ELECTRONICALLY)

Page 1
Concentrations (ppb)
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 547
Total Non-Detect: 500
Percent Non-Detects: 91.4077%
Total Background Measurements: 117
There are 3 background locations
Loc.Meas.ND Date Conc.Original
MW-1 39 36 (92.3077%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 2100 2100
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 2.4 2.4
5/13/2010 23 23
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-11 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
Page 2
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 32 32
5/13/2010 44 44
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-12 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
Page 3
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 24 24
5/13/2010 18 18
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
There are 14 compliance locations
Loc.Meas.ND Date Conc.Original
MW-10 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 13 13
5/13/2010 76 76
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
Page 4
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-2 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 33 33
5/13/2010 14 14
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-3 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
Page 5
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 16 16
5/13/2010 9.2 9.2
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-4 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 65 65
5/13/2010 41 41
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
Page 6
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-5 39 36 (92.3077%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 67 67
5/13/2010 68 68
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 105 105
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-6 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
Page 7
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 41 41
5/13/2010 58 58
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-7 53 47 (88.6792%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
Page 8
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 0.01 0.01
10/19/2009 47 47
5/13/2010 ND<0.01 ND<0.01
5/13/2010 73 73
10/7/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
5/19/2011 142 142
10/6/2011 ND<0.01 ND<0.01
10/6/2011 129 129
5/16/2012 ND<0.01 ND<0.01
5/16/2012 153 153
10/3/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-8 39 36 (92.3077%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 5.9 5.9
Page 9
5/13/2010 70 70
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 109 109
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-9 39 35 (89.7436%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 100 100
5/13/2010 26 26
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 113 113
10/3/2012 ND<0.01 ND<0.01
9/4/2013 115 115
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-13 13 12 (92.3077%)5/13/2010 21 21
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
Page 10
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-14 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-15 13 12 (92.3077%)5/13/2010 61 61
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-16 13 8 (61.5385%)5/13/2010 68 68
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 102 102
10/3/2012 176 176
9/4/2013 117 117
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 157 157
MW-17 13 6 (46.1538%)5/13/2010 65 65
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
Page 11
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 116 116
5/28/2014 139 139
11/5/2014 120 120
6/8/2015 120 120
10/27/2015 150 150
6/29/2016 165 165
There are 0 unused locations
Loc.Meas.ND Date Conc.Original
Page 12
Basic Statistics
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements 547
Total Non-Detects 500 (91.4077%)
Pooled Mean 11.3781
Pooled Std Dev 92.9237
Compliance Meas.430
Compliance Mean 8.85923
Compliance Std Dev 27.9685
Background Meas.117
Background Mean 20.6353
Background Std Dev 194.011
Background Locations
There are 3 background location
Location Meas.Non-Detects % ND Total
MW-1 39 36 92.3077 2175.71
MW-11 39 37 94.8718 136.31
MW-12 39 37 94.8718 102.31
Location Mean Std Dev Std Err Rank Sum Rank Mean
MW-1 55.7874 335.985 0 10577 271.205
MW-11 3.49513 9.00816 0 10298.5 264.064
MW-12 2.62333 5.69305 0 10287.5 263.782
Compliance Locations
There are 14 compliance location
Location Obs.Non-Detects % ND Total
MW-10 39 37 94.8718 149.31
MW-2 39 37 94.8718 107.31
MW-3 39 37 94.8718 85.51
MW-4 39 37 94.8718 166.31
MW-5 39 36 92.3077 300.3
MW-6 39 37 94.8718 159.31
MW-7 53 47 88.6792 604.42
MW-8 39 36 92.3077 245.2
MW-9 39 35 89.7436 414.29
MW-13 13 12 92.3077 21.12
MW-14 13 13 100 0.13
MW-15 13 12 92.3077 61.12
MW-16 13 8 61.5385 620.08
MW-17 13 6 46.1538 875.06
Location Mean Std Dev Dif From Bkg Std Err Rank Sum Rank Mean
MW-10 3.82846 12.5377 -16.8068 17.1449 10301.5 264.141
MW-2 2.75154 6.46801 -17.8838 17.1449 10288.5 263.808
MW-3 2.19256 4.45196 -18.4427 17.1449 10279.5 263.577
MW-4 4.26436 12.351 -16.3709 17.1449 10304.5 264.218
MW-5 7.7 22.0201 -12.9353 17.1449 10596 271.692
MW-6 4.08487 11.4642 -16.5504 17.1449 10303.5 264.192
Page 13
MW-7 11.4042 34.3789 -9.23115 15.353 14942.5 281.934
MW-8 6.28718 20.4387 -14.3481 17.1449 10579 271.256
MW-9 10.6228 29.4105 -10.0125 17.1449 10875.5 278.859
MW-13 1.62462 5.82158 -19.0107 27.1085 3515 270.385
MW-14 0.01 1.80556e-018 -20.6253 27.1085 3256.5 250.5
MW-15 4.70154 16.9156 -15.9338 27.1085 3526 271.231
MW-16 47.6985 67.5556 27.0632 27.1085 4685 360.385
MW-17 67.3123 68.693 46.677 27.1085 5262 404.769
Analysis of Variance Statistics
SS Wells 157670
SS Total 4.71461e+006
Kruskal-Wallis Statistics
Non-Detect Rank 250.5
Background Rank Sum 31163
Background Rank Mean 266.35
H Statistic 14.329
H Adjusted for Ties 60.6503
Page 14
Shapiro-Francia Test of Normality
Parameter: Barium
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Number of Measurements = 547
i x(i)m(i)sum(m^2)sum(mx)
1 0.01 0 0 0
2 0.01 -2.74777 7.55021 -0.0274777
3 0.01 -2.57583 14.1851 -0.053236
4 0.01 -2.45727 20.2233 -0.0778087
5 0.01 -2.36561 25.8195 -0.101465
6 0.01 -2.32634 31.2313 -0.124728
7 0.01 -2.25713 36.326 -0.1473
8 0.01 -2.19728 41.154 -0.169272
9 0.01 -2.14441 45.7525 -0.190716
10 0.01 -2.09693 50.1496 -0.211686
11 0.01 -2.05375 54.3675 -0.232223
12 0.01 -2.03352 58.5027 -0.252558
13 0.01 -1.99539 62.4843 -0.272512
14 0.01 -1.95996 66.3258 -0.292112
15 0.01 -1.92684 70.0385 -0.31138
16 0.01 -1.8957 73.6321 -0.330337
17 0.01 -1.86629 77.1152 -0.349
18 0.01 -1.85218 80.5457 -0.367522
19 0.01 -1.82501 83.8764 -0.385772
20 0.01 -1.79912 87.1132 -0.403763
21 0.01 -1.77438 90.2616 -0.421507
22 0.01 -1.75069 93.3265 -0.439014
23 0.01 -1.7392 96.3513 -0.456406
24 0.01 -1.71688 99.299 -0.473575
25 0.01 -1.6954 102.173 -0.490529
26 0.01 -1.67466 104.978 -0.507275
27 0.01 -1.65463 107.716 -0.523822
28 0.01 -1.63524 110.39 -0.540174
29 0.01 -1.62576 113.033 -0.556432
30 0.01 -1.60725 115.616 -0.572504
31 0.01 -1.58927 118.142 -0.588397
32 0.01 -1.57179 120.612 -0.604115
33 0.01 -1.55477 123.03 -0.619662
34 0.01 -1.5382 125.396 -0.635044
35 0.01 -1.53007 127.737 -0.650345
36 0.01 -1.5141 130.029 -0.665486
37 0.01 -1.49852 132.275 -0.680471
38 0.01 -1.48328 134.475 -0.695304
39 0.01 -1.46838 136.631 -0.709988
40 0.01 -1.46106 138.766 -0.724599
41 0.01 -1.44663 140.859 -0.739065
42 0.01 -1.4325 142.911 -0.75339
43 0.01 -1.41865 144.923 -0.767576
44 0.01 -1.40507 146.897 -0.781627
45 0.01 -1.39175 148.834 -0.795545
46 0.01 -1.38517 150.753 -0.809396
47 0.01 -1.3722 152.636 -0.823118
Page 15
48 0.01 -1.35946 154.484 -0.836713
49 0.01 -1.34694 156.298 -0.850182
50 0.01 -1.33462 158.08 -0.863529
51 0.01 -1.32251 159.829 -0.876754
52 0.01 -1.31652 161.562 -0.889919
53 0.01 -1.30469 163.264 -0.902966
54 0.01 -1.29303 164.936 -0.915896
55 0.01 -1.28155 166.578 -0.928712
56 0.01 -1.27024 168.192 -0.941414
57 0.01 -1.25908 169.777 -0.954005
58 0.01 -1.25357 171.349 -0.96654
59 0.01 -1.24264 172.893 -0.978967
60 0.01 -1.23187 174.41 -0.991286
61 0.01 -1.22123 175.902 -1.0035
62 0.01 -1.21073 177.368 -1.01561
63 0.01 -1.20553 178.821 -1.02766
64 0.01 -1.19522 180.249 -1.03961
65 0.01 -1.18504 181.654 -1.05146
66 0.01 -1.17499 183.034 -1.06321
67 0.01 -1.16505 184.392 -1.07486
68 0.01 -1.15522 185.726 -1.08642
69 0.01 -1.15035 187.05 -1.09792
70 0.01 -1.14069 188.351 -1.10933
71 0.01 -1.13113 189.63 -1.12064
72 0.01 -1.12168 190.888 -1.13185
73 0.01 -1.11232 192.126 -1.14298
74 0.01 -1.10306 193.342 -1.15401
75 0.01 -1.09847 194.549 -1.16499
76 0.01 -1.08935 195.736 -1.17589
77 0.01 -1.08032 196.903 -1.18669
78 0.01 -1.07138 198.051 -1.1974
79 0.01 -1.06252 199.18 -1.20803
80 0.01 -1.05812 200.299 -1.21861
81 0.01 -1.04939 201.4 -1.2291
82 0.01 -1.04073 202.483 -1.23951
83 0.01 -1.03215 203.549 -1.24983
84 0.01 -1.02365 204.597 -1.26007
85 0.01 -1.01522 205.627 -1.27022
86 0.01 -1.01104 206.65 -1.28033
87 0.01 -1.00271 207.655 -1.29036
88 0.01 -0.994457 208.644 -1.3003
89 0.01 -0.986272 209.617 -1.31017
90 0.01 -0.97815 210.573 -1.31995
91 0.01 -0.970094 211.515 -1.32965
92 0.01 -0.966088 212.448 -1.33931
93 0.01 -0.958125 213.366 -1.34889
94 0.01 -0.950222 214.269 -1.35839
95 0.01 -0.942375 215.157 -1.36782
96 0.01 -0.93459 216.03 -1.37716
97 0.01 -0.926859 216.889 -1.38643
98 0.01 -0.923014 217.741 -1.39566
99 0.01 -0.915365 218.579 -1.40481
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Page 16
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Page 17
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Page 18
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Page 19
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Page 20
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Page 21
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Page 22
447 10 0.900227 304.242 132.568
448 10 0.907769 305.066 141.646
449 10 0.915365 305.904 150.8
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484 10 1.19522 344.824 518.8
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498 10 1.33462 367.347 696.278
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501 10 1.3722 372.892 737.064
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Page 23
504 10 1.40507 378.722 778.884
505 13 1.41865 380.735 797.327
506 14 1.4325 382.787 817.382
507 16 1.44663 384.879 840.528
508 18 1.46106 387.014 866.827
509 21 1.46838 389.17 897.663
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511 24 1.49852 393.616 967.743
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520 61 1.63524 415.93 1574.53
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522 65 1.67466 421.472 1790.94
523 67 1.6954 424.346 1904.53
524 68 1.71688 427.294 2021.28
525 68 1.7392 430.319 2139.54
526 70 1.75069 433.384 2262.09
527 73 1.77438 436.532 2391.62
528 76 1.79912 439.769 2528.35
529 100 1.82501 443.1 2710.85
530 102 1.85218 446.53 2899.78
531 105 1.86629 450.013 3095.74
532 109 1.8957 453.607 3302.37
533 113 1.92684 457.319 3520.1
534 115 1.95996 461.161 3745.5
535 116 1.99539 465.143 3976.96
536 117 2.03352 469.278 4214.88
537 120 2.05375 473.496 4461.33
538 120 2.09693 477.893 4712.96
539 129 2.14441 482.491 4989.59
540 139 2.19728 487.319 5295.02
541 142 2.25713 492.414 5615.53
542 150 2.32634 497.826 5964.48
543 153 2.36561 503.422 6326.42
544 157 2.45727 509.46 6712.21
545 165 2.57583 516.095 7137.22
546 176 2.74777 523.645 7620.83
547 2100 0 523.645 7620.83
Data Set Standard Deviation = 92.9237
Numerator = 5.8077e+007
Denominator = 2.46878e+009
W Statistic = 0.0235246 = 5.8077e+007 / 2.46878e+009
5% Critical value of 0.976 exceeds 0.0235246
Evidence of non-normality at 95% level of significance
1% Critical value of 0.967 exceeds 0.0235246
Evidence of non-normality at 99% level of significance
Page 24
Levene's Test for Equal of Variance
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Overall Mean = 17.71
Overall Std Dev = 89.6204
Overall Total = 9687.38
SS Groups = 398557
SS Total = 4.38537e+006
ANOVA Table
Source of Sum of Degrees of Mean
Variation Squares Freedom Squares F
Between Groups 398557 16 24909.8 3.31146
Error (within groups)3.98682e+006 530 7522.3
Totals 4.38537e+006 546
95% F-Statistic = 1.57
3.31146 exceeds 1.57; assumption of equal variance should be rejected
Group: MW-1 Sample Residual
12/9/1997 45.7874
1/27/1998 45.7874
3/25/1998 45.7874
4/8/1998 45.7874
11/6/1998 45.7874
8/5/1999 2044.21
11/9/1999 55.7774
9/26/2000 55.7774
1/30/2001 55.7774
9/26/2001 55.7774
5/30/2002 55.7774
10/9/2002 55.7774
5/16/2003 55.7774
10/21/2003 55.7774
5/27/2004 55.7774
10/7/2004 55.7774
5/19/2005 55.7774
10/18/2005 55.7774
5/9/2006 55.7774
10/17/2006 55.7774
5/16/2007 55.7774
10/23/2007 55.7774
6/11/2008 55.7774
11/23/2008 55.7774
5/7/2009 55.7774
10/19/2009 53.3874
5/13/2010 32.7874
10/7/2010 55.7774
5/19/2011 55.7774
10/6/2011 55.7774
Page 25
5/16/2012 55.7774
10/3/2012 55.7774
9/4/2013 55.7774
12/4/2013 55.7774
5/28/2014 55.7774
11/5/2014 55.7774
6/8/2015 55.7774
10/27/2015 55.7774
6/29/2016 55.7774
Group: MW-11 Sample Residual
12/9/1997 6.50487
1/27/1998 6.50487
3/25/1998 6.50487
4/8/1998 6.50487
11/6/1998 6.50487
8/5/1999 6.50487
11/9/1999 3.48513
9/26/2000 3.48513
1/30/2001 3.48513
9/26/2001 3.48513
5/30/2002 3.48513
10/9/2002 3.48513
5/16/2003 3.48513
10/21/2003 3.48513
5/27/2004 3.48513
10/7/2004 3.48513
5/19/2005 3.48513
10/18/2005 3.48513
5/9/2006 3.48513
10/17/2006 3.48513
5/16/2007 3.48513
10/23/2007 3.48513
6/11/2008 3.48513
11/23/2008 3.48513
5/7/2009 3.48513
10/19/2009 28.5049
5/13/2010 40.5049
10/7/2010 3.48513
5/19/2011 3.48513
10/6/2011 3.48513
5/16/2012 3.48513
10/3/2012 3.48513
9/4/2013 3.48513
12/4/2013 3.48513
5/28/2014 3.48513
11/5/2014 3.48513
6/8/2015 3.48513
10/27/2015 3.48513
6/29/2016 3.48513
Group: MW-12 Sample Residual
12/9/1997 7.37667
1/27/1998 7.37667
3/25/1998 7.37667
4/8/1998 7.37667
11/6/1998 7.37667
Page 26
8/5/1999 7.37667
11/9/1999 2.61333
9/26/2000 2.61333
1/30/2001 2.61333
9/26/2001 2.61333
5/30/2002 2.61333
10/9/2002 2.61333
5/16/2003 2.61333
10/21/2003 2.61333
5/27/2004 2.61333
10/7/2004 2.61333
5/19/2005 2.61333
10/18/2005 2.61333
5/9/2006 2.61333
10/17/2006 2.61333
5/16/2007 2.61333
10/23/2007 2.61333
6/11/2008 2.61333
11/23/2008 2.61333
5/7/2009 2.61333
10/19/2009 21.3767
5/13/2010 15.3767
10/7/2010 2.61333
5/19/2011 2.61333
10/6/2011 2.61333
5/16/2012 2.61333
10/3/2012 2.61333
9/4/2013 2.61333
12/4/2013 2.61333
5/28/2014 2.61333
11/5/2014 2.61333
6/8/2015 2.61333
10/27/2015 2.61333
6/29/2016 2.61333
Group: MW-10 Date Residual
12/9/1997 6.17154
1/27/1998 6.17154
3/25/1998 6.17154
4/8/1998 6.17154
11/6/1998 6.17154
8/5/1999 6.17154
11/9/1999 3.81846
9/26/2000 3.81846
1/30/2001 3.81846
9/26/2001 3.81846
5/30/2002 3.81846
10/9/2002 3.81846
5/16/2003 3.81846
10/21/2003 3.81846
5/27/2004 3.81846
10/7/2004 3.81846
5/19/2005 3.81846
10/18/2005 3.81846
5/9/2006 3.81846
10/17/2006 3.81846
5/16/2007 3.81846
Page 27
10/23/2007 3.81846
6/11/2008 3.81846
11/23/2008 3.81846
5/7/2009 3.81846
10/19/2009 9.17154
5/13/2010 72.1715
10/7/2010 3.81846
5/19/2011 3.81846
10/6/2011 3.81846
5/16/2012 3.81846
10/3/2012 3.81846
9/4/2013 3.81846
12/4/2013 3.81846
5/28/2014 3.81846
11/5/2014 3.81846
6/8/2015 3.81846
10/27/2015 3.81846
6/29/2016 3.81846
Group: MW-2 Date Residual
12/9/1997 7.24846
1/27/1998 7.24846
3/25/1998 7.24846
4/8/1998 7.24846
11/6/1998 7.24846
8/5/1999 7.24846
11/9/1999 2.74154
9/26/2000 2.74154
1/30/2001 2.74154
9/26/2001 2.74154
5/30/2002 2.74154
10/9/2002 2.74154
5/16/2003 2.74154
10/21/2003 2.74154
5/27/2004 2.74154
10/7/2004 2.74154
5/19/2005 2.74154
10/18/2005 2.74154
5/9/2006 2.74154
10/17/2006 2.74154
5/16/2007 2.74154
10/23/2007 2.74154
6/11/2008 2.74154
11/23/2008 2.74154
5/7/2009 2.74154
10/19/2009 30.2485
5/13/2010 11.2485
10/7/2010 2.74154
5/19/2011 2.74154
10/6/2011 2.74154
5/16/2012 2.74154
10/3/2012 2.74154
9/4/2013 2.74154
12/4/2013 2.74154
5/28/2014 2.74154
11/5/2014 2.74154
6/8/2015 2.74154
Page 28
10/27/2015 2.74154
6/29/2016 2.74154
Group: MW-3 Date Residual
12/9/1997 7.80744
1/27/1998 7.80744
3/25/1998 7.80744
4/8/1998 7.80744
11/6/1998 7.80744
8/5/1999 7.80744
11/9/1999 2.18256
9/26/2000 2.18256
1/30/2001 2.18256
9/26/2001 2.18256
5/30/2002 2.18256
10/9/2002 2.18256
5/16/2003 2.18256
10/21/2003 2.18256
5/27/2004 2.18256
10/7/2004 2.18256
5/19/2005 2.18256
10/18/2005 2.18256
5/9/2006 2.18256
10/17/2006 2.18256
5/16/2007 2.18256
10/23/2007 2.18256
6/11/2008 2.18256
11/23/2008 2.18256
5/7/2009 2.18256
10/19/2009 13.8074
5/13/2010 7.00744
10/7/2010 2.18256
5/19/2011 2.18256
10/6/2011 2.18256
5/16/2012 2.18256
10/3/2012 2.18256
9/4/2013 2.18256
12/4/2013 2.18256
5/28/2014 2.18256
11/5/2014 2.18256
6/8/2015 2.18256
10/27/2015 2.18256
6/29/2016 2.18256
Group: MW-4 Date Residual
12/9/1997 5.73564
1/27/1998 5.73564
3/25/1998 5.73564
4/8/1998 5.73564
11/6/1998 5.73564
8/5/1999 5.73564
11/9/1999 4.25436
9/26/2000 4.25436
1/30/2001 4.25436
9/26/2001 4.25436
5/30/2002 4.25436
10/9/2002 4.25436
Page 29
5/16/2003 4.25436
10/21/2003 4.25436
5/27/2004 4.25436
10/7/2004 4.25436
5/19/2005 4.25436
10/18/2005 4.25436
5/9/2006 4.25436
10/17/2006 4.25436
5/16/2007 4.25436
10/23/2007 4.25436
6/11/2008 4.25436
11/23/2008 4.25436
5/7/2009 4.25436
10/19/2009 60.7356
5/13/2010 36.7356
10/7/2010 4.25436
5/19/2011 4.25436
10/6/2011 4.25436
5/16/2012 4.25436
10/3/2012 4.25436
9/4/2013 4.25436
12/4/2013 4.25436
5/28/2014 4.25436
11/5/2014 4.25436
6/8/2015 4.25436
10/27/2015 4.25436
6/29/2016 4.25436
Group: MW-5 Date Residual
12/9/1997 2.3
1/27/1998 2.3
3/25/1998 2.3
4/8/1998 2.3
11/6/1998 2.3
8/5/1999 2.3
11/9/1999 7.69
9/26/2000 7.69
1/30/2001 7.69
9/26/2001 7.69
5/30/2002 7.69
10/9/2002 7.69
5/16/2003 7.69
10/21/2003 7.69
5/27/2004 7.69
10/7/2004 7.69
5/19/2005 7.69
10/18/2005 7.69
5/9/2006 7.69
10/17/2006 7.69
5/16/2007 7.69
10/23/2007 7.69
6/11/2008 7.69
11/23/2008 7.69
5/7/2009 7.69
10/19/2009 59.3
5/13/2010 60.3
10/7/2010 7.69
Page 30
5/19/2011 7.69
10/6/2011 7.69
5/16/2012 7.69
10/3/2012 7.69
9/4/2013 97.3
12/4/2013 7.69
5/28/2014 7.69
11/5/2014 7.69
6/8/2015 7.69
10/27/2015 7.69
6/29/2016 7.69
Group: MW-6 Date Residual
12/9/1997 5.91513
1/27/1998 5.91513
3/25/1998 5.91513
4/8/1998 5.91513
11/6/1998 5.91513
8/5/1999 5.91513
11/9/1999 4.07487
9/26/2000 4.07487
1/30/2001 4.07487
9/26/2001 4.07487
5/30/2002 4.07487
10/9/2002 4.07487
5/16/2003 4.07487
10/21/2003 4.07487
5/27/2004 4.07487
10/7/2004 4.07487
5/19/2005 4.07487
10/18/2005 4.07487
5/9/2006 4.07487
10/17/2006 4.07487
5/16/2007 4.07487
10/23/2007 4.07487
6/11/2008 4.07487
11/23/2008 4.07487
5/7/2009 4.07487
10/19/2009 36.9151
5/13/2010 53.9151
10/7/2010 4.07487
5/19/2011 4.07487
10/6/2011 4.07487
5/16/2012 4.07487
10/3/2012 4.07487
9/4/2013 4.07487
12/4/2013 4.07487
5/28/2014 4.07487
11/5/2014 4.07487
6/8/2015 4.07487
10/27/2015 4.07487
6/29/2016 4.07487
Group: MW-7 Date Residual
12/9/1997 1.40415
1/27/1998 1.40415
3/25/1998 1.40415
Page 31
4/8/1998 1.40415
11/6/1998 1.40415
8/5/1999 1.40415
11/9/1999 11.3942
9/26/2000 11.3942
1/30/2001 11.3942
9/26/2001 11.3942
5/30/2002 11.3942
10/9/2002 11.3942
5/16/2003 11.3942
10/21/2003 11.3942
5/27/2004 11.3942
10/7/2004 11.3942
5/19/2005 11.3942
10/18/2005 11.3942
5/9/2006 11.3942
10/17/2006 11.3942
5/16/2007 11.3942
10/23/2007 11.3942
6/11/2008 11.3942
11/23/2008 11.3942
5/7/2009 11.3942
10/19/2009 11.3942
10/19/2009 35.5958
5/13/2010 11.3942
5/13/2010 61.5958
10/7/2010 11.3942
10/7/2010 11.3942
5/19/2011 11.3942
5/19/2011 130.596
10/6/2011 11.3942
10/6/2011 117.596
5/16/2012 11.3942
5/16/2012 141.596
10/3/2012 11.3942
10/3/2012 11.3942
9/4/2013 11.3942
9/4/2013 11.3942
12/4/2013 11.3942
12/4/2013 11.3942
5/28/2014 11.3942
5/28/2014 11.3942
11/5/2014 11.3942
11/5/2014 11.3942
6/8/2015 11.3942
6/8/2015 11.3942
10/27/2015 11.3942
10/27/2015 11.3942
6/29/2016 11.3942
6/29/2016 11.3942
Group: MW-8 Date Residual
12/9/1997 3.71282
1/27/1998 3.71282
3/25/1998 3.71282
4/8/1998 3.71282
11/6/1998 3.71282
Page 32
8/5/1999 3.71282
11/9/1999 6.27718
9/26/2000 6.27718
1/30/2001 6.27718
9/26/2001 6.27718
5/30/2002 6.27718
10/9/2002 6.27718
5/16/2003 6.27718
10/21/2003 6.27718
5/27/2004 6.27718
10/7/2004 6.27718
5/19/2005 6.27718
10/18/2005 6.27718
5/9/2006 6.27718
10/17/2006 6.27718
5/16/2007 6.27718
10/23/2007 6.27718
6/11/2008 6.27718
11/23/2008 6.27718
5/7/2009 6.27718
10/19/2009 0.387179
5/13/2010 63.7128
10/7/2010 6.27718
5/19/2011 6.27718
10/6/2011 6.27718
5/16/2012 102.713
10/3/2012 6.27718
9/4/2013 6.27718
12/4/2013 6.27718
5/28/2014 6.27718
11/5/2014 6.27718
6/8/2015 6.27718
10/27/2015 6.27718
6/29/2016 6.27718
Group: MW-9 Date Residual
12/9/1997 0.622821
1/27/1998 0.622821
3/25/1998 0.622821
4/8/1998 0.622821
11/6/1998 0.622821
8/5/1999 0.622821
11/9/1999 10.6128
9/26/2000 10.6128
1/30/2001 10.6128
9/26/2001 10.6128
5/30/2002 10.6128
10/9/2002 10.6128
5/16/2003 10.6128
10/21/2003 10.6128
5/27/2004 10.6128
10/7/2004 10.6128
5/19/2005 10.6128
10/18/2005 10.6128
5/9/2006 10.6128
10/17/2006 10.6128
5/16/2007 10.6128
Page 33
10/23/2007 10.6128
6/11/2008 10.6128
11/23/2008 10.6128
5/7/2009 10.6128
10/19/2009 89.3772
5/13/2010 15.3772
10/7/2010 10.6128
5/19/2011 10.6128
10/6/2011 10.6128
5/16/2012 102.377
10/3/2012 10.6128
9/4/2013 104.377
12/4/2013 10.6128
5/28/2014 10.6128
11/5/2014 10.6128
6/8/2015 10.6128
10/27/2015 10.6128
6/29/2016 10.6128
Group: MW-13 Date Residual
5/13/2010 19.3754
10/7/2010 1.61462
5/19/2011 1.61462
10/6/2011 1.61462
5/16/2012 1.61462
10/3/2012 1.61462
9/4/2013 1.61462
12/4/2013 1.61462
5/28/2014 1.61462
11/5/2014 1.61462
6/8/2015 1.61462
10/27/2015 1.61462
6/29/2016 1.61462
Group: MW-14 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Group: MW-15 Date Residual
5/13/2010 56.2985
10/7/2010 4.69154
5/19/2011 4.69154
10/6/2011 4.69154
5/16/2012 4.69154
10/3/2012 4.69154
9/4/2013 4.69154
Page 34
12/4/2013 4.69154
5/28/2014 4.69154
11/5/2014 4.69154
6/8/2015 4.69154
10/27/2015 4.69154
6/29/2016 4.69154
Group: MW-16 Date Residual
5/13/2010 20.3015
10/7/2010 47.6885
5/19/2011 47.6885
10/6/2011 47.6885
5/16/2012 54.3015
10/3/2012 128.302
9/4/2013 69.3015
12/4/2013 47.6885
5/28/2014 47.6885
11/5/2014 47.6885
6/8/2015 47.6885
10/27/2015 47.6885
6/29/2016 109.302
Group: MW-17 Date Residual
5/13/2010 2.31231
10/7/2010 67.3023
5/19/2011 67.3023
10/6/2011 67.3023
5/16/2012 67.3023
10/3/2012 67.3023
9/4/2013 67.3023
12/4/2013 48.6877
5/28/2014 71.6877
11/5/2014 52.6877
6/8/2015 52.6877
10/27/2015 82.6877
6/29/2016 97.6877
Page 35
Poisson Prediction Limit (Inter-Well)
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Recent Dates = 1
Poisson Count of 117 background Samples = 2414.33
99% t-test = 2.35892
95% t-test = 1.6581
Well: MW-10
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-2
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-3
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-4
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-5
Page 36
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-6
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-7
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
2 0.01 FALSE FALSE
Well: MW-8
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-9
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-13
Number of comparisons = 1
Page 37
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-14
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-15
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-16
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 157 TRUE TRUE
Well: MW-17
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 31.4205
95% Prediction Limit (Tk) = 28.2113
Samples Sum 95 %tile 99 %tile
1 165 TRUE TRUE
Page 38
Non-Parametric Prediction Interval
Intra-Well Comparison for MW-16
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 66.6667%
Future Samples (k) = 1
Recent Dates = 1
Baseline Measurements (n) = 12
Maximum Baseline Concentration = 176
Confidence Level = 92.3%
False Positive Rate = 7.7%
Baseline Measurements Date Value
5/13/2010 68
10/7/2010 ND<0.01
5/19/2011 ND<0.01
10/6/2011 ND<0.01
5/16/2012 102
10/3/2012 176
9/4/2013 117
12/4/2013 ND<0.01
5/28/2014 ND<0.01
11/5/2014 ND<0.01
6/8/2015 ND<0.01
10/27/2015 ND<0.01
Date Count Mean Significant
6/29/2016 1 157 FALSE
Page 39
Non-Parametric Prediction Interval
Intra-Well Comparison for MW-17
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 50%
Future Samples (k) = 1
Recent Dates = 1
Baseline Measurements (n) = 12
Maximum Baseline Concentration = 150
Confidence Level = 92.3%
False Positive Rate = 7.7%
Baseline Measurements Date Value
5/13/2010 65
10/7/2010 ND<0.01
5/19/2011 ND<0.01
10/6/2011 ND<0.01
5/16/2012 ND<0.01
10/3/2012 ND<0.01
9/4/2013 ND<0.01
12/4/2013 116
5/28/2014 139
11/5/2014 120
6/8/2015 120
10/27/2015 150
Date Count Mean Significant
6/29/2016 1 165 TRUE
Page 40
Concentrations (ppb)
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 547
Total Non-Detect: 528
Percent Non-Detects: 96.5265%
Total Background Measurements: 117
There are 3 background locations
Loc.Meas.ND Date Conc.Original
MW-1 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 3.9 3.9
5/13/2010 3.4 3.4
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-11 39 36 (92.3077%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
Page 41
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 19 19
5/13/2010 10 10
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 40.5 40.5
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-12 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
Page 42
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 8.8 8.8
5/13/2010 4.5 4.5
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
There are 14 compliance locations
Loc.Meas.ND Date Conc.Original
MW-10 39 38 (97.4359%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 71 71
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
Page 43
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-2 39 38 (97.4359%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 3.6 3.6
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-3 39 39 (100%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
Page 44
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-4 39 38 (97.4359%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 25 25
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
Page 45
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-5 39 39 (100%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-6 39 39 (100%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
Page 46
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-7 53 52 (98.1132%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
Page 47
11/23/2008 62 62
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-8 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 4 4
Page 48
5/13/2010 10 10
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-9 39 37 (94.8718%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 5 5
5/13/2010 9.1 9.1
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-13 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
Page 49
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-14 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-15 13 12 (92.3077%)5/13/2010 3.7 3.7
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-16 13 11 (84.6154%)5/13/2010 3.8 3.8
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 42.4 42.4
MW-17 13 12 (92.3077%)5/13/2010 3.8 3.8
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
Page 50
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
There are 0 unused locations
Loc.Meas.ND Date Conc.Original
Page 51
Basic Statistics
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements 547
Total Non-Detects 528 (96.5265%)
Pooled Mean 1.9343
Pooled Std Dev 5.89379
Compliance Meas.430
Compliance Mean 1.83033
Compliance Std Dev 6.0199
Background Meas.117
Background Mean 2.31641
Background Std Dev 5.41225
Background Locations
There are 3 background location
Location Meas.Non-Detects % ND Total
MW-1 39 37 94.8718 67.61
MW-11 39 36 92.3077 129.8
MW-12 39 37 94.8718 73.61
Location Mean Std Dev Std Err Rank Sum Rank Mean
MW-1 1.73359 3.66191 0 10849.5 278.192
MW-11 3.32821 7.72769 0 11148 285.846
MW-12 1.88744 3.8346 0 10860.5 278.474
Compliance Locations
There are 14 compliance location
Location Obs.Non-Detects % ND Total
MW-10 39 38 97.4359 131.32
MW-2 39 38 97.4359 63.92
MW-3 39 39 100 60.33
MW-4 39 38 97.4359 85.32
MW-5 39 39 100 60.33
MW-6 39 39 100 60.33
MW-7 53 52 98.1132 122.46
MW-8 39 37 94.8718 74.31
MW-9 39 37 94.8718 74.41
MW-13 13 13 100 0.13
MW-14 13 13 100 0.13
MW-15 13 12 92.3077 3.82
MW-16 13 11 84.6154 46.31
MW-17 13 12 92.3077 3.92
Location Mean Std Dev Dif From Bkg Std Err Rank Sum Rank Mean
MW-10 3.36718 11.6966 1.05077 1.09469 10598 271.744
MW-2 1.63897 3.657 -0.677436 1.09469 10581 271.308
MW-3 1.54692 3.65152 -0.769487 1.09469 10315.5 264.5
MW-4 2.18769 5.22733 -0.128718 1.09469 10594 271.641
MW-5 1.54692 3.65152 -0.769487 1.09469 10315.5 264.5
MW-6 1.54692 3.65152 -0.769487 1.09469 10315.5 264.5
Page 52
MW-7 2.31057 8.9454 -0.00584422 0.980274 14300 269.811
MW-8 1.90538 3.88795 -0.411026 1.09469 10862.5 278.526
MW-9 1.90795 3.85883 -0.408462 1.09469 10862.5 278.526
MW-13 0.01 1.80556e-018 -2.30641 1.73086 3438.5 264.5
MW-14 0.01 1.80556e-018 -2.30641 1.73086 3438.5 264.5
MW-15 0.293846 1.02342 -2.02256 1.73086 3705 285
MW-16 3.56231 11.7162 1.2459 1.73086 3986.5 306.654
MW-17 0.301538 1.05116 -2.01487 1.73086 3707 285.154
Analysis of Variance Statistics
SS Wells 388.904
SS Total 18966.3
Kruskal-Wallis Statistics
Non-Detect Rank 264.5
Background Rank Sum 32858
Background Rank Mean 280.838
H Statistic 1.5474
H Adjusted for Ties 15.3775
Page 53
Shapiro-Francia Test of Normality
Parameter: Vanadium
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Number of Measurements = 547
i x(i)m(i)sum(m^2)sum(mx)
1 0.01 0 0 0
2 0.01 -2.74777 7.55021 -0.0274777
3 0.01 -2.57583 14.1851 -0.053236
4 0.01 -2.45727 20.2233 -0.0778087
5 0.01 -2.36561 25.8195 -0.101465
6 0.01 -2.32634 31.2313 -0.124728
7 0.01 -2.25713 36.326 -0.1473
8 0.01 -2.19728 41.154 -0.169272
9 0.01 -2.14441 45.7525 -0.190716
10 0.01 -2.09693 50.1496 -0.211686
11 0.01 -2.05375 54.3675 -0.232223
12 0.01 -2.03352 58.5027 -0.252558
13 0.01 -1.99539 62.4843 -0.272512
14 0.01 -1.95996 66.3258 -0.292112
15 0.01 -1.92684 70.0385 -0.31138
16 0.01 -1.8957 73.6321 -0.330337
17 0.01 -1.86629 77.1152 -0.349
18 0.01 -1.85218 80.5457 -0.367522
19 0.01 -1.82501 83.8764 -0.385772
20 0.01 -1.79912 87.1132 -0.403763
21 0.01 -1.77438 90.2616 -0.421507
22 0.01 -1.75069 93.3265 -0.439014
23 0.01 -1.7392 96.3513 -0.456406
24 0.01 -1.71688 99.299 -0.473575
25 0.01 -1.6954 102.173 -0.490529
26 0.01 -1.67466 104.978 -0.507275
27 0.01 -1.65463 107.716 -0.523822
28 0.01 -1.63524 110.39 -0.540174
29 0.01 -1.62576 113.033 -0.556432
30 0.01 -1.60725 115.616 -0.572504
31 0.01 -1.58927 118.142 -0.588397
32 0.01 -1.57179 120.612 -0.604115
33 0.01 -1.55477 123.03 -0.619662
34 0.01 -1.5382 125.396 -0.635044
35 0.01 -1.53007 127.737 -0.650345
36 0.01 -1.5141 130.029 -0.665486
37 0.01 -1.49852 132.275 -0.680471
38 0.01 -1.48328 134.475 -0.695304
39 0.01 -1.46838 136.631 -0.709988
40 0.01 -1.46106 138.766 -0.724599
41 0.01 -1.44663 140.859 -0.739065
42 0.01 -1.4325 142.911 -0.75339
43 0.01 -1.41865 144.923 -0.767576
44 0.01 -1.40507 146.897 -0.781627
45 0.01 -1.39175 148.834 -0.795545
46 0.01 -1.38517 150.753 -0.809396
47 0.01 -1.3722 152.636 -0.823118
Page 54
48 0.01 -1.35946 154.484 -0.836713
49 0.01 -1.34694 156.298 -0.850182
50 0.01 -1.33462 158.08 -0.863529
51 0.01 -1.32251 159.829 -0.876754
52 0.01 -1.31652 161.562 -0.889919
53 0.01 -1.30469 163.264 -0.902966
54 0.01 -1.29303 164.936 -0.915896
55 0.01 -1.28155 166.578 -0.928712
56 0.01 -1.27024 168.192 -0.941414
57 0.01 -1.25908 169.777 -0.954005
58 0.01 -1.25357 171.349 -0.96654
59 0.01 -1.24264 172.893 -0.978967
60 0.01 -1.23187 174.41 -0.991286
61 0.01 -1.22123 175.902 -1.0035
62 0.01 -1.21073 177.368 -1.01561
63 0.01 -1.20553 178.821 -1.02766
64 0.01 -1.19522 180.249 -1.03961
65 0.01 -1.18504 181.654 -1.05146
66 0.01 -1.17499 183.034 -1.06321
67 0.01 -1.16505 184.392 -1.07486
68 0.01 -1.15522 185.726 -1.08642
69 0.01 -1.15035 187.05 -1.09792
70 0.01 -1.14069 188.351 -1.10933
71 0.01 -1.13113 189.63 -1.12064
72 0.01 -1.12168 190.888 -1.13185
73 0.01 -1.11232 192.126 -1.14298
74 0.01 -1.10306 193.342 -1.15401
75 0.01 -1.09847 194.549 -1.16499
76 0.01 -1.08935 195.736 -1.17589
77 0.01 -1.08032 196.903 -1.18669
78 0.01 -1.07138 198.051 -1.1974
79 0.01 -1.06252 199.18 -1.20803
80 0.01 -1.05812 200.299 -1.21861
81 0.01 -1.04939 201.4 -1.2291
82 0.01 -1.04073 202.483 -1.23951
83 0.01 -1.03215 203.549 -1.24983
84 0.01 -1.02365 204.597 -1.26007
85 0.01 -1.01522 205.627 -1.27022
86 0.01 -1.01104 206.65 -1.28033
87 0.01 -1.00271 207.655 -1.29036
88 0.01 -0.994457 208.644 -1.3003
89 0.01 -0.986272 209.617 -1.31017
90 0.01 -0.97815 210.573 -1.31995
91 0.01 -0.970094 211.515 -1.32965
92 0.01 -0.966088 212.448 -1.33931
93 0.01 -0.958125 213.366 -1.34889
94 0.01 -0.950222 214.269 -1.35839
95 0.01 -0.942375 215.157 -1.36782
96 0.01 -0.93459 216.03 -1.37716
97 0.01 -0.926859 216.889 -1.38643
98 0.01 -0.923014 217.741 -1.39566
99 0.01 -0.915365 218.579 -1.40481
100 0.01 -0.907769 219.403 -1.41389
101 0.01 -0.900227 220.214 -1.42289
102 0.01 -0.892733 221.011 -1.43182
103 0.01 -0.889006 221.801 -1.44071
104 0.01 -0.881587 222.578 -1.44953
Page 55
105 0.01 -0.874218 223.342 -1.45827
106 0.01 -0.866894 224.094 -1.46694
107 0.01 -0.859618 224.833 -1.47554
108 0.01 -0.852385 225.559 -1.48406
109 0.01 -0.848786 226.28 -1.49255
110 0.01 -0.841621 226.988 -1.50096
111 0.01 -0.834498 227.685 -1.50931
112 0.01 -0.827417 228.369 -1.51758
113 0.01 -0.820379 229.042 -1.52579
114 0.01 -0.813379 229.704 -1.53392
115 0.01 -0.809896 230.36 -1.54202
116 0.01 -0.802956 231.004 -1.55005
117 0.01 -0.796056 231.638 -1.55801
118 0.01 -0.789191 232.261 -1.5659
119 0.01 -0.782366 232.873 -1.57372
120 0.01 -0.778966 233.48 -1.58151
121 0.01 -0.772193 234.076 -1.58924
122 0.01 -0.765456 234.662 -1.59689
123 0.01 -0.758753 235.238 -1.60448
124 0.01 -0.752084 235.803 -1.612
125 0.01 -0.745449 236.359 -1.61945
126 0.01 -0.742143 236.91 -1.62687
127 0.01 -0.735557 237.451 -1.63423
128 0.01 -0.729003 237.982 -1.64152
129 0.01 -0.722479 238.504 -1.64875
130 0.01 -0.715986 239.017 -1.65591
131 0.01 -0.709522 239.52 -1.663
132 0.01 -0.706302 240.019 -1.67006
133 0.01 -0.699883 240.509 -1.67706
134 0.01 -0.693493 240.99 -1.684
135 0.01 -0.687131 241.462 -1.69087
136 0.01 -0.680797 241.926 -1.69768
137 0.01 -0.67449 242.381 -1.70442
138 0.01 -0.671346 242.831 -1.71113
139 0.01 -0.665079 243.274 -1.71779
140 0.01 -0.658838 243.708 -1.72437
141 0.01 -0.652622 244.134 -1.7309
142 0.01 -0.646431 244.552 -1.73736
143 0.01 -0.643345 244.965 -1.7438
144 0.01 -0.637192 245.371 -1.75017
145 0.01 -0.631062 245.77 -1.75648
146 0.01 -0.624956 246.16 -1.76273
147 0.01 -0.618872 246.543 -1.76892
148 0.01 -0.612813 246.919 -1.77505
149 0.01 -0.609791 247.291 -1.78114
150 0.01 -0.603765 247.655 -1.78718
151 0.01 -0.597761 248.012 -1.79316
152 0.01 -0.591776 248.363 -1.79908
153 0.01 -0.585815 248.706 -1.80494
154 0.01 -0.579873 249.042 -1.81073
155 0.01 -0.576911 249.375 -1.8165
156 0.01 -0.570999 249.701 -1.82221
157 0.01 -0.565108 250.02 -1.82786
158 0.01 -0.559237 250.333 -1.83346
159 0.01 -0.553384 250.639 -1.83899
160 0.01 -0.550465 250.942 -1.8445
161 0.01 -0.544642 251.239 -1.84994
Page 56
162 0.01 -0.538836 251.529 -1.85533
163 0.01 -0.533048 251.813 -1.86066
164 0.01 -0.52728 252.091 -1.86593
165 0.01 -0.521527 252.363 -1.87115
166 0.01 -0.518658 252.632 -1.87634
167 0.01 -0.51293 252.896 -1.88146
168 0.01 -0.507221 253.153 -1.88654
169 0.01 -0.501527 253.404 -1.89155
170 0.01 -0.49585 253.65 -1.89651
171 0.01 -0.490189 253.89 -1.90141
172 0.01 -0.487364 254.128 -1.90629
173 0.01 -0.481728 254.36 -1.9111
174 0.01 -0.476105 254.587 -1.91586
175 0.01 -0.470498 254.808 -1.92057
176 0.01 -0.464904 255.024 -1.92522
177 0.01 -0.462114 255.238 -1.92984
178 0.01 -0.456542 255.446 -1.93441
179 0.01 -0.450985 255.65 -1.93892
180 0.01 -0.445443 255.848 -1.94337
181 0.01 -0.439913 256.042 -1.94777
182 0.01 -0.434397 256.23 -1.95211
183 0.01 -0.431644 256.417 -1.95643
184 0.01 -0.426148 256.598 -1.96069
185 0.01 -0.420664 256.775 -1.9649
186 0.01 -0.415193 256.948 -1.96905
187 0.01 -0.409735 257.115 -1.97315
188 0.01 -0.40429 257.279 -1.97719
189 0.01 -0.401571 257.44 -1.98121
190 0.01 -0.396142 257.597 -1.98517
191 0.01 -0.390726 257.75 -1.98907
192 0.01 -0.385321 257.898 -1.99293
193 0.01 -0.379927 258.043 -1.99673
194 0.01 -0.374544 258.183 -2.00047
195 0.01 -0.371856 258.321 -2.00419
196 0.01 -0.36649 258.455 -2.00786
197 0.01 -0.361133 258.586 -2.01147
198 0.01 -0.355788 258.712 -2.01502
199 0.01 -0.350451 258.835 -2.01853
200 0.01 -0.347787 258.956 -2.02201
201 0.01 -0.342466 259.073 -2.02543
202 0.01 -0.337155 259.187 -2.0288
203 0.01 -0.331854 259.297 -2.03212
204 0.01 -0.326561 259.404 -2.03539
205 0.01 -0.321278 259.507 -2.0386
206 0.01 -0.318639 259.609 -2.04179
207 0.01 -0.31337 259.707 -2.04492
208 0.01 -0.308108 259.802 -2.048
209 0.01 -0.302855 259.894 -2.05103
210 0.01 -0.297612 259.982 -2.05401
211 0.01 -0.292375 260.068 -2.05693
212 0.01 -0.28976 260.152 -2.05983
213 0.01 -0.284535 260.232 -2.06267
214 0.01 -0.279319 260.311 -2.06547
215 0.01 -0.27411 260.386 -2.06821
216 0.01 -0.268908 260.458 -2.0709
217 0.01 -0.266311 260.529 -2.07356
218 0.01 -0.26112 260.597 -2.07617
Page 57
219 0.01 -0.255936 260.663 -2.07873
220 0.01 -0.250759 260.725 -2.08124
221 0.01 -0.24559 260.786 -2.08369
222 0.01 -0.240426 260.844 -2.0861
223 0.01 -0.237847 260.9 -2.08848
224 0.01 -0.232693 260.954 -2.0908
225 0.01 -0.227545 261.006 -2.09308
226 0.01 -0.222403 261.056 -2.0953
227 0.01 -0.217267 261.103 -2.09747
228 0.01 -0.212137 261.148 -2.0996
229 0.01 -0.209575 261.192 -2.10169
230 0.01 -0.204452 261.233 -2.10374
231 0.01 -0.199336 261.273 -2.10573
232 0.01 -0.194225 261.311 -2.10767
233 0.01 -0.189118 261.347 -2.10956
234 0.01 -0.184017 261.381 -2.1114
235 0.01 -0.181468 261.413 -2.11322
236 0.01 -0.176374 261.445 -2.11498
237 0.01 -0.171285 261.474 -2.11669
238 0.01 -0.166199 261.502 -2.11836
239 0.01 -0.161119 261.527 -2.11997
240 0.01 -0.158579 261.553 -2.12155
241 0.01 -0.153505 261.576 -2.12309
242 0.01 -0.148434 261.598 -2.12457
243 0.01 -0.143367 261.619 -2.12601
244 0.01 -0.138305 261.638 -2.12739
245 0.01 -0.133244 261.656 -2.12872
246 0.01 -0.130716 261.673 -2.13003
247 0.01 -0.125661 261.689 -2.13129
248 0.01 -0.12061 261.703 -2.13249
249 0.01 -0.115562 261.716 -2.13365
250 0.01 -0.110516 261.729 -2.13475
251 0.01 -0.105474 261.74 -2.13581
252 0.01 -0.102953 261.75 -2.13684
253 0.01 -0.0979139 261.76 -2.13782
254 0.01 -0.0928787 261.769 -2.13875
255 0.01 -0.0878447 261.776 -2.13962
256 0.01 -0.0828129 261.783 -2.14045
257 0.01 -0.0802981 261.79 -2.14125
258 0.01 -0.0752698 261.795 -2.14201
259 0.01 -0.0702426 261.8 -2.14271
260 0.01 -0.0652187 261.804 -2.14336
261 0.01 -0.0601949 261.808 -2.14396
262 0.01 -0.0551734 261.811 -2.14452
263 0.01 -0.0526632 261.814 -2.14504
264 0.01 -0.0476439 261.816 -2.14552
265 0.01 -0.0426257 261.818 -2.14594
266 0.01 -0.0376076 261.819 -2.14632
267 0.01 -0.0325917 261.82 -2.14665
268 0.01 -0.0275759 261.821 -2.14692
269 0.01 -0.0250691 261.822 -2.14717
270 0.01 -0.0200544 261.822 -2.14737
271 0.01 -0.0150408 261.822 -2.14752
272 0.01 -0.0100272 261.823 -2.14762
273 0.01 -0.00501359 261.823 -2.14767
274 0.01 0 261.823 -2.14767
275 0.01 0.00501359 261.823 -2.14762
Page 58
276 0.01 0.0100272 261.823 -2.14752
277 0.01 0.0150408 261.823 -2.14737
278 0.01 0.0200544 261.823 -2.14717
279 0.01 0.0250691 261.824 -2.14692
280 0.01 0.0275759 261.825 -2.14665
281 0.01 0.0325917 261.826 -2.14632
282 0.01 0.0376076 261.827 -2.14594
283 0.01 0.0426257 261.829 -2.14552
284 0.01 0.0476439 261.831 -2.14504
285 0.01 0.0526632 261.834 -2.14452
286 0.01 0.0551734 261.837 -2.14396
287 0.01 0.0601949 261.841 -2.14336
288 0.01 0.0652187 261.845 -2.14271
289 0.01 0.0702426 261.85 -2.14201
290 0.01 0.0752698 261.856 -2.14125
291 0.01 0.0802981 261.862 -2.14045
292 0.01 0.0828129 261.869 -2.13962
293 0.01 0.0878447 261.877 -2.13875
294 0.01 0.0928787 261.885 -2.13782
295 0.01 0.0979139 261.895 -2.13684
296 0.01 0.102953 261.905 -2.13581
297 0.01 0.105474 261.917 -2.13475
298 0.01 0.110516 261.929 -2.13365
299 0.01 0.115562 261.942 -2.13249
300 0.01 0.12061 261.957 -2.13129
301 0.01 0.125661 261.972 -2.13003
302 0.01 0.130716 261.99 -2.12872
303 0.01 0.133244 262.007 -2.12739
304 0.01 0.138305 262.026 -2.12601
305 0.01 0.143367 262.047 -2.12457
306 0.01 0.148434 262.069 -2.12309
307 0.01 0.153505 262.093 -2.12155
308 0.01 0.158579 262.118 -2.11997
309 0.01 0.161119 262.144 -2.11836
310 0.01 0.166199 262.171 -2.11669
311 0.01 0.171285 262.201 -2.11498
312 0.01 0.176374 262.232 -2.11322
313 0.01 0.181468 262.265 -2.1114
314 0.01 0.184017 262.299 -2.10956
315 0.01 0.189118 262.334 -2.10767
316 0.01 0.194225 262.372 -2.10573
317 0.01 0.199336 262.412 -2.10374
318 0.01 0.204452 262.454 -2.10169
319 0.01 0.209575 262.498 -2.0996
320 0.01 0.212137 262.543 -2.09747
321 0.01 0.217267 262.59 -2.0953
322 0.01 0.222403 262.639 -2.09308
323 0.01 0.227545 262.691 -2.0908
324 0.01 0.232693 262.745 -2.08848
325 0.01 0.237847 262.802 -2.0861
326 0.01 0.240426 262.859 -2.08369
327 0.01 0.24559 262.92 -2.08124
328 0.01 0.250759 262.983 -2.07873
329 0.01 0.255936 263.048 -2.07617
330 0.01 0.26112 263.116 -2.07356
331 0.01 0.266311 263.187 -2.0709
332 0.01 0.268908 263.26 -2.06821
Page 59
333 0.01 0.27411 263.335 -2.06547
334 0.01 0.279319 263.413 -2.06267
335 0.01 0.284535 263.494 -2.05983
336 0.01 0.28976 263.578 -2.05693
337 0.01 0.292375 263.663 -2.05401
338 0.01 0.297612 263.752 -2.05103
339 0.01 0.302855 263.843 -2.048
340 0.01 0.308108 263.938 -2.04492
341 0.01 0.31337 264.037 -2.04179
342 0.01 0.318639 264.138 -2.0386
343 0.01 0.321278 264.241 -2.03539
344 0.01 0.326561 264.348 -2.03212
345 0.01 0.331854 264.458 -2.0288
346 0.01 0.337155 264.572 -2.02543
347 0.01 0.342466 264.689 -2.02201
348 0.01 0.347787 264.81 -2.01853
349 0.01 0.350451 264.933 -2.01502
350 0.01 0.355788 265.059 -2.01147
351 0.01 0.361133 265.19 -2.00786
352 0.01 0.36649 265.324 -2.00419
353 0.01 0.371856 265.462 -2.00047
354 0.01 0.374544 265.603 -1.99673
355 0.01 0.379927 265.747 -1.99293
356 0.01 0.385321 265.896 -1.98907
357 0.01 0.390726 266.048 -1.98517
358 0.01 0.396142 266.205 -1.98121
359 0.01 0.401571 266.366 -1.97719
360 0.01 0.40429 266.53 -1.97315
361 0.01 0.409735 266.698 -1.96905
362 0.01 0.415193 266.87 -1.9649
363 0.01 0.420664 267.047 -1.96069
364 0.01 0.426148 267.229 -1.95643
365 0.01 0.431644 267.415 -1.95211
366 0.01 0.434397 267.604 -1.94777
367 0.01 0.439913 267.797 -1.94337
368 0.01 0.445443 267.996 -1.93892
369 0.01 0.450985 268.199 -1.93441
370 0.01 0.456542 268.407 -1.92984
371 0.01 0.462114 268.621 -1.92522
372 0.01 0.464904 268.837 -1.92057
373 0.01 0.470498 269.059 -1.91586
374 0.01 0.476105 269.285 -1.9111
375 0.01 0.481728 269.517 -1.90629
376 0.01 0.487364 269.755 -1.90141
377 0.01 0.490189 269.995 -1.89651
378 0.01 0.49585 270.241 -1.89155
379 0.01 0.501527 270.492 -1.88654
380 0.01 0.507221 270.75 -1.88146
381 0.01 0.51293 271.013 -1.87634
382 0.01 0.518658 271.282 -1.87115
383 0.01 0.521527 271.554 -1.86593
384 0.01 0.52728 271.832 -1.86066
385 0.01 0.533048 272.116 -1.85533
386 0.01 0.538836 272.406 -1.84994
387 0.01 0.544642 272.703 -1.8445
388 0.01 0.550465 273.006 -1.83899
389 0.01 0.553384 273.312 -1.83346
Page 60
390 0.01 0.559237 273.625 -1.82786
391 0.01 0.565108 273.944 -1.82221
392 0.01 0.570999 274.27 -1.8165
393 0.01 0.576911 274.603 -1.81073
394 0.01 0.579873 274.939 -1.80494
395 0.01 0.585815 275.283 -1.79908
396 0.01 0.591776 275.633 -1.79316
397 0.01 0.597761 275.99 -1.78718
398 0.01 0.603765 276.355 -1.78114
399 0.01 0.609791 276.726 -1.77505
400 0.01 0.612813 277.102 -1.76892
401 0.01 0.618872 277.485 -1.76273
402 0.01 0.624956 277.876 -1.75648
403 0.01 0.631062 278.274 -1.75017
404 0.01 0.637192 278.68 -1.7438
405 0.01 0.643345 279.094 -1.73736
406 0.01 0.646431 279.512 -1.7309
407 0.01 0.652622 279.938 -1.72437
408 0.01 0.658838 280.372 -1.71779
409 0.01 0.665079 280.814 -1.71113
410 0.01 0.671346 281.265 -1.70442
411 0.01 0.67449 281.72 -1.69768
412 0.01 0.680797 282.183 -1.69087
413 0.01 0.687131 282.655 -1.684
414 0.01 0.693493 283.136 -1.67706
415 0.01 0.699883 283.626 -1.67006
416 0.01 0.706302 284.125 -1.663
417 0.01 0.709522 284.628 -1.65591
418 0.01 0.715986 285.141 -1.64875
419 0.01 0.722479 285.663 -1.64152
420 0.01 0.729003 286.194 -1.63423
421 0.01 0.735557 286.735 -1.62687
422 0.01 0.742143 287.286 -1.61945
423 0.01 0.745449 287.842 -1.612
424 0.01 0.752084 288.407 -1.60448
425 0.01 0.758753 288.983 -1.59689
426 0.01 0.765456 289.569 -1.58924
427 0.01 0.772193 290.165 -1.58151
428 0.01 0.778966 290.772 -1.57372
429 0.01 0.782366 291.384 -1.5659
430 0.01 0.789191 292.007 -1.55801
431 0.01 0.796056 292.641 -1.55005
432 0.01 0.802956 293.286 -1.54202
433 0.01 0.809896 293.941 -1.53392
434 0.01 0.813379 294.603 -1.52579
435 0.01 0.820379 295.276 -1.51758
436 0.01 0.827417 295.961 -1.50931
437 0.01 0.834498 296.657 -1.50096
438 0.01 0.841621 297.365 -1.49255
439 0.01 0.848786 298.086 -1.48406
440 0.01 0.852385 298.812 -1.47554
441 0.01 0.859618 299.551 -1.46694
442 0.01 0.866894 300.303 -1.45827
443 0.01 0.874218 301.067 -1.44953
444 0.01 0.881587 301.844 -1.44071
445 0.01 0.889006 302.635 -1.43182
446 0.01 0.892733 303.432 -1.42289
Page 61
447 0.01 0.900227 304.242 -1.41389
448 0.01 0.907769 305.066 -1.40481
449 0.01 0.915365 305.904 -1.39566
450 0.01 0.923014 306.756 -1.38643
451 0.01 0.926859 307.615 -1.37716
452 0.01 0.93459 308.488 -1.36782
453 0.01 0.942375 309.376 -1.35839
454 0.01 0.950222 310.279 -1.34889
455 0.01 0.958125 311.197 -1.33931
456 0.01 0.966088 312.131 -1.32965
457 3.4 0.970094 313.072 1.96867
458 3.6 0.97815 314.029 5.49001
459 3.7 0.986272 315.001 9.13922
460 3.8 0.994457 315.99 12.9182
461 3.8 1.00271 316.996 16.7285
462 3.9 1.01104 318.018 20.6715
463 4 1.01522 319.049 24.7324
464 4.5 1.02365 320.096 29.3388
465 5 1.03215 321.162 34.4996
466 8.8 1.04073 322.245 43.658
467 9.1 1.04939 323.346 53.2074
468 10 1.05812 324.466 63.7887
469 10 1.06252 325.595 74.4139
470 10 1.07138 326.743 85.1276
471 10 1.08032 327.91 95.9308
472 10 1.08935 329.096 106.824
473 10 1.09847 330.303 117.809
474 10 1.10306 331.52 128.84
475 10 1.11232 332.757 139.963
476 10 1.12168 334.015 151.18
477 10 1.13113 335.295 162.491
478 10 1.14069 336.596 173.898
479 10 1.15035 337.919 185.401
480 10 1.15522 339.254 196.954
481 10 1.16505 340.611 208.604
482 10 1.17499 341.992 220.354
483 10 1.18504 343.396 232.204
484 10 1.19522 344.824 244.157
485 10 1.20553 346.278 256.212
486 10 1.21073 347.744 268.319
487 10 1.22123 349.235 280.531
488 10 1.23187 350.752 292.85
489 10 1.24264 352.297 305.276
490 10 1.25357 353.868 317.812
491 10 1.25908 355.453 330.403
492 10 1.27024 357.067 343.105
493 10 1.28155 358.709 355.921
494 10 1.29303 360.381 368.851
495 10 1.30469 362.083 381.898
496 10 1.31652 363.817 395.063
497 10 1.32251 365.566 408.288
498 10 1.33462 367.347 421.635
499 10 1.34694 369.161 435.104
500 10 1.35946 371.009 448.699
501 10 1.3722 372.892 462.421
502 10 1.38517 374.811 476.272
503 10 1.39175 376.748 490.19
Page 62
504 10 1.40507 378.722 504.241
505 10 1.41865 380.735 518.427
506 10 1.4325 382.787 532.752
507 10 1.44663 384.879 547.218
508 10 1.46106 387.014 561.829
509 10 1.46838 389.17 576.513
510 10 1.48328 391.37 591.346
511 10 1.49852 393.616 606.331
512 10 1.5141 395.908 621.472
513 10 1.53007 398.25 636.772
514 10 1.5382 400.616 652.155
515 10 1.55477 403.033 667.702
516 10 1.57179 405.503 683.42
517 10 1.58927 408.029 699.313
518 10 1.60725 410.612 715.385
519 10 1.62576 413.256 731.643
520 10 1.63524 415.93 747.995
521 10 1.65463 418.667 764.542
522 10 1.67466 421.472 781.288
523 10 1.6954 424.346 798.242
524 10 1.71688 427.294 815.411
525 10 1.7392 430.319 832.803
526 10 1.75069 433.384 850.31
527 10 1.77438 436.532 868.054
528 10 1.79912 439.769 886.045
529 10 1.82501 443.1 904.295
530 10 1.85218 446.53 922.817
531 10 1.86629 450.013 941.48
532 10 1.8957 453.607 960.437
533 10 1.92684 457.319 979.705
534 10 1.95996 461.161 999.304
535 10 1.99539 465.143 1019.26
536 10 2.03352 469.278 1039.59
537 10 2.05375 473.496 1060.13
538 10 2.09693 477.893 1081.1
539 10 2.14441 482.491 1102.54
540 10 2.19728 487.319 1124.52
541 10 2.25713 492.414 1147.09
542 19 2.32634 497.826 1191.29
543 25 2.36561 503.422 1250.43
544 40.5 2.45727 509.46 1349.95
545 42.4 2.57583 516.095 1459.16
546 62 2.74777 523.645 1629.53
547 71 0 523.645 1629.53
Data Set Standard Deviation = 5.89379
Numerator = 2.65535e+006
Denominator = 9.93159e+006
W Statistic = 0.267365 = 2.65535e+006 / 9.93159e+006
5% Critical value of 0.976 exceeds 0.267365
Evidence of non-normality at 95% level of significance
1% Critical value of 0.967 exceeds 0.267365
Evidence of non-normality at 99% level of significance
Page 63
Levene's Test for Equal of Variance
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Overall Mean = 3.15165
Overall Std Dev = 4.90646
Overall Total = 1723.95
SS Groups = 1006.76
SS Total = 13144.1
ANOVA Table
Source of Sum of Degrees of Mean
Variation Squares Freedom Squares F
Between Groups 1006.76 16 62.9223 2.74763
Error (within groups)12137.3 530 22.9006
Totals 13144.1 546
95% F-Statistic = 1.57
2.74763 exceeds 1.57; assumption of equal variance should be rejected
Group: MW-1 Sample Residual
12/9/1997 8.26641
1/27/1998 8.26641
3/25/1998 8.26641
4/8/1998 8.26641
11/6/1998 8.26641
8/5/1999 8.26641
11/9/1999 1.72359
9/26/2000 1.72359
1/30/2001 1.72359
9/26/2001 1.72359
5/30/2002 1.72359
10/9/2002 1.72359
5/16/2003 1.72359
10/21/2003 1.72359
5/27/2004 1.72359
10/7/2004 1.72359
5/19/2005 1.72359
10/18/2005 1.72359
5/9/2006 1.72359
10/17/2006 1.72359
5/16/2007 1.72359
10/23/2007 1.72359
6/11/2008 1.72359
11/23/2008 1.72359
5/7/2009 1.72359
10/19/2009 2.16641
5/13/2010 1.66641
10/7/2010 1.72359
5/19/2011 1.72359
10/6/2011 1.72359
Page 64
5/16/2012 1.72359
10/3/2012 1.72359
9/4/2013 1.72359
12/4/2013 1.72359
5/28/2014 1.72359
11/5/2014 1.72359
6/8/2015 1.72359
10/27/2015 1.72359
6/29/2016 1.72359
Group: MW-11 Sample Residual
12/9/1997 6.67179
1/27/1998 6.67179
3/25/1998 6.67179
4/8/1998 6.67179
11/6/1998 6.67179
8/5/1999 6.67179
11/9/1999 3.31821
9/26/2000 3.31821
1/30/2001 3.31821
9/26/2001 3.31821
5/30/2002 3.31821
10/9/2002 3.31821
5/16/2003 3.31821
10/21/2003 3.31821
5/27/2004 3.31821
10/7/2004 3.31821
5/19/2005 3.31821
10/18/2005 3.31821
5/9/2006 3.31821
10/17/2006 3.31821
5/16/2007 3.31821
10/23/2007 3.31821
6/11/2008 3.31821
11/23/2008 3.31821
5/7/2009 3.31821
10/19/2009 15.6718
5/13/2010 6.67179
10/7/2010 3.31821
5/19/2011 3.31821
10/6/2011 3.31821
5/16/2012 37.1718
10/3/2012 3.31821
9/4/2013 3.31821
12/4/2013 3.31821
5/28/2014 3.31821
11/5/2014 3.31821
6/8/2015 3.31821
10/27/2015 3.31821
6/29/2016 3.31821
Group: MW-12 Sample Residual
12/9/1997 8.11256
1/27/1998 8.11256
3/25/1998 8.11256
4/8/1998 8.11256
11/6/1998 8.11256
Page 65
8/5/1999 8.11256
11/9/1999 1.87744
9/26/2000 1.87744
1/30/2001 1.87744
9/26/2001 1.87744
5/30/2002 1.87744
10/9/2002 1.87744
5/16/2003 1.87744
10/21/2003 1.87744
5/27/2004 1.87744
10/7/2004 1.87744
5/19/2005 1.87744
10/18/2005 1.87744
5/9/2006 1.87744
10/17/2006 1.87744
5/16/2007 1.87744
10/23/2007 1.87744
6/11/2008 1.87744
11/23/2008 1.87744
5/7/2009 1.87744
10/19/2009 6.91256
5/13/2010 2.61256
10/7/2010 1.87744
5/19/2011 1.87744
10/6/2011 1.87744
5/16/2012 1.87744
10/3/2012 1.87744
9/4/2013 1.87744
12/4/2013 1.87744
5/28/2014 1.87744
11/5/2014 1.87744
6/8/2015 1.87744
10/27/2015 1.87744
6/29/2016 1.87744
Group: MW-10 Date Residual
12/9/1997 6.63282
1/27/1998 6.63282
3/25/1998 6.63282
4/8/1998 6.63282
11/6/1998 6.63282
8/5/1999 6.63282
11/9/1999 3.35718
9/26/2000 3.35718
1/30/2001 3.35718
9/26/2001 3.35718
5/30/2002 3.35718
10/9/2002 3.35718
5/16/2003 3.35718
10/21/2003 3.35718
5/27/2004 3.35718
10/7/2004 3.35718
5/19/2005 3.35718
10/18/2005 3.35718
5/9/2006 3.35718
10/17/2006 3.35718
5/16/2007 3.35718
Page 66
10/23/2007 3.35718
6/11/2008 3.35718
11/23/2008 3.35718
5/7/2009 3.35718
10/19/2009 3.35718
5/13/2010 67.6328
10/7/2010 3.35718
5/19/2011 3.35718
10/6/2011 3.35718
5/16/2012 3.35718
10/3/2012 3.35718
9/4/2013 3.35718
12/4/2013 3.35718
5/28/2014 3.35718
11/5/2014 3.35718
6/8/2015 3.35718
10/27/2015 3.35718
6/29/2016 3.35718
Group: MW-2 Date Residual
12/9/1997 8.36103
1/27/1998 8.36103
3/25/1998 8.36103
4/8/1998 8.36103
11/6/1998 8.36103
8/5/1999 8.36103
11/9/1999 1.62897
9/26/2000 1.62897
1/30/2001 1.62897
9/26/2001 1.62897
5/30/2002 1.62897
10/9/2002 1.62897
5/16/2003 1.62897
10/21/2003 1.62897
5/27/2004 1.62897
10/7/2004 1.62897
5/19/2005 1.62897
10/18/2005 1.62897
5/9/2006 1.62897
10/17/2006 1.62897
5/16/2007 1.62897
10/23/2007 1.62897
6/11/2008 1.62897
11/23/2008 1.62897
5/7/2009 1.62897
10/19/2009 1.96103
5/13/2010 1.62897
10/7/2010 1.62897
5/19/2011 1.62897
10/6/2011 1.62897
5/16/2012 1.62897
10/3/2012 1.62897
9/4/2013 1.62897
12/4/2013 1.62897
5/28/2014 1.62897
11/5/2014 1.62897
6/8/2015 1.62897
Page 67
10/27/2015 1.62897
6/29/2016 1.62897
Group: MW-3 Date Residual
12/9/1997 8.45308
1/27/1998 8.45308
3/25/1998 8.45308
4/8/1998 8.45308
11/6/1998 8.45308
8/5/1999 8.45308
11/9/1999 1.53692
9/26/2000 1.53692
1/30/2001 1.53692
9/26/2001 1.53692
5/30/2002 1.53692
10/9/2002 1.53692
5/16/2003 1.53692
10/21/2003 1.53692
5/27/2004 1.53692
10/7/2004 1.53692
5/19/2005 1.53692
10/18/2005 1.53692
5/9/2006 1.53692
10/17/2006 1.53692
5/16/2007 1.53692
10/23/2007 1.53692
6/11/2008 1.53692
11/23/2008 1.53692
5/7/2009 1.53692
10/19/2009 1.53692
5/13/2010 1.53692
10/7/2010 1.53692
5/19/2011 1.53692
10/6/2011 1.53692
5/16/2012 1.53692
10/3/2012 1.53692
9/4/2013 1.53692
12/4/2013 1.53692
5/28/2014 1.53692
11/5/2014 1.53692
6/8/2015 1.53692
10/27/2015 1.53692
6/29/2016 1.53692
Group: MW-4 Date Residual
12/9/1997 7.81231
1/27/1998 7.81231
3/25/1998 7.81231
4/8/1998 7.81231
11/6/1998 7.81231
8/5/1999 7.81231
11/9/1999 2.17769
9/26/2000 2.17769
1/30/2001 2.17769
9/26/2001 2.17769
5/30/2002 2.17769
10/9/2002 2.17769
Page 68
5/16/2003 2.17769
10/21/2003 2.17769
5/27/2004 2.17769
10/7/2004 2.17769
5/19/2005 2.17769
10/18/2005 2.17769
5/9/2006 2.17769
10/17/2006 2.17769
5/16/2007 2.17769
10/23/2007 2.17769
6/11/2008 2.17769
11/23/2008 2.17769
5/7/2009 2.17769
10/19/2009 22.8123
5/13/2010 2.17769
10/7/2010 2.17769
5/19/2011 2.17769
10/6/2011 2.17769
5/16/2012 2.17769
10/3/2012 2.17769
9/4/2013 2.17769
12/4/2013 2.17769
5/28/2014 2.17769
11/5/2014 2.17769
6/8/2015 2.17769
10/27/2015 2.17769
6/29/2016 2.17769
Group: MW-5 Date Residual
12/9/1997 8.45308
1/27/1998 8.45308
3/25/1998 8.45308
4/8/1998 8.45308
11/6/1998 8.45308
8/5/1999 8.45308
11/9/1999 1.53692
9/26/2000 1.53692
1/30/2001 1.53692
9/26/2001 1.53692
5/30/2002 1.53692
10/9/2002 1.53692
5/16/2003 1.53692
10/21/2003 1.53692
5/27/2004 1.53692
10/7/2004 1.53692
5/19/2005 1.53692
10/18/2005 1.53692
5/9/2006 1.53692
10/17/2006 1.53692
5/16/2007 1.53692
10/23/2007 1.53692
6/11/2008 1.53692
11/23/2008 1.53692
5/7/2009 1.53692
10/19/2009 1.53692
5/13/2010 1.53692
10/7/2010 1.53692
Page 69
5/19/2011 1.53692
10/6/2011 1.53692
5/16/2012 1.53692
10/3/2012 1.53692
9/4/2013 1.53692
12/4/2013 1.53692
5/28/2014 1.53692
11/5/2014 1.53692
6/8/2015 1.53692
10/27/2015 1.53692
6/29/2016 1.53692
Group: MW-6 Date Residual
12/9/1997 8.45308
1/27/1998 8.45308
3/25/1998 8.45308
4/8/1998 8.45308
11/6/1998 8.45308
8/5/1999 8.45308
11/9/1999 1.53692
9/26/2000 1.53692
1/30/2001 1.53692
9/26/2001 1.53692
5/30/2002 1.53692
10/9/2002 1.53692
5/16/2003 1.53692
10/21/2003 1.53692
5/27/2004 1.53692
10/7/2004 1.53692
5/19/2005 1.53692
10/18/2005 1.53692
5/9/2006 1.53692
10/17/2006 1.53692
5/16/2007 1.53692
10/23/2007 1.53692
6/11/2008 1.53692
11/23/2008 1.53692
5/7/2009 1.53692
10/19/2009 1.53692
5/13/2010 1.53692
10/7/2010 1.53692
5/19/2011 1.53692
10/6/2011 1.53692
5/16/2012 1.53692
10/3/2012 1.53692
9/4/2013 1.53692
12/4/2013 1.53692
5/28/2014 1.53692
11/5/2014 1.53692
6/8/2015 1.53692
10/27/2015 1.53692
6/29/2016 1.53692
Group: MW-7 Date Residual
12/9/1997 7.68943
1/27/1998 7.68943
3/25/1998 7.68943
Page 70
4/8/1998 7.68943
11/6/1998 7.68943
8/5/1999 7.68943
11/9/1999 2.30057
9/26/2000 2.30057
1/30/2001 2.30057
9/26/2001 2.30057
5/30/2002 2.30057
10/9/2002 2.30057
5/16/2003 2.30057
10/21/2003 2.30057
5/27/2004 2.30057
10/7/2004 2.30057
5/19/2005 2.30057
10/18/2005 2.30057
5/9/2006 2.30057
10/17/2006 2.30057
5/16/2007 2.30057
10/23/2007 2.30057
6/11/2008 2.30057
11/23/2008 59.6894
5/7/2009 2.30057
10/19/2009 2.30057
10/19/2009 2.30057
5/13/2010 2.30057
5/13/2010 2.30057
10/7/2010 2.30057
10/7/2010 2.30057
5/19/2011 2.30057
5/19/2011 2.30057
10/6/2011 2.30057
10/6/2011 2.30057
5/16/2012 2.30057
5/16/2012 2.30057
10/3/2012 2.30057
10/3/2012 2.30057
9/4/2013 2.30057
9/4/2013 2.30057
12/4/2013 2.30057
12/4/2013 2.30057
5/28/2014 2.30057
5/28/2014 2.30057
11/5/2014 2.30057
11/5/2014 2.30057
6/8/2015 2.30057
6/8/2015 2.30057
10/27/2015 2.30057
10/27/2015 2.30057
6/29/2016 2.30057
6/29/2016 2.30057
Group: MW-8 Date Residual
12/9/1997 8.09462
1/27/1998 8.09462
3/25/1998 8.09462
4/8/1998 8.09462
11/6/1998 8.09462
Page 71
8/5/1999 8.09462
11/9/1999 1.89538
9/26/2000 1.89538
1/30/2001 1.89538
9/26/2001 1.89538
5/30/2002 1.89538
10/9/2002 1.89538
5/16/2003 1.89538
10/21/2003 1.89538
5/27/2004 1.89538
10/7/2004 1.89538
5/19/2005 1.89538
10/18/2005 1.89538
5/9/2006 1.89538
10/17/2006 1.89538
5/16/2007 1.89538
10/23/2007 1.89538
6/11/2008 1.89538
11/23/2008 1.89538
5/7/2009 1.89538
10/19/2009 2.09462
5/13/2010 8.09462
10/7/2010 1.89538
5/19/2011 1.89538
10/6/2011 1.89538
5/16/2012 1.89538
10/3/2012 1.89538
9/4/2013 1.89538
12/4/2013 1.89538
5/28/2014 1.89538
11/5/2014 1.89538
6/8/2015 1.89538
10/27/2015 1.89538
6/29/2016 1.89538
Group: MW-9 Date Residual
12/9/1997 8.09205
1/27/1998 8.09205
3/25/1998 8.09205
4/8/1998 8.09205
11/6/1998 8.09205
8/5/1999 8.09205
11/9/1999 1.89795
9/26/2000 1.89795
1/30/2001 1.89795
9/26/2001 1.89795
5/30/2002 1.89795
10/9/2002 1.89795
5/16/2003 1.89795
10/21/2003 1.89795
5/27/2004 1.89795
10/7/2004 1.89795
5/19/2005 1.89795
10/18/2005 1.89795
5/9/2006 1.89795
10/17/2006 1.89795
5/16/2007 1.89795
Page 72
10/23/2007 1.89795
6/11/2008 1.89795
11/23/2008 1.89795
5/7/2009 1.89795
10/19/2009 3.09205
5/13/2010 7.19205
10/7/2010 1.89795
5/19/2011 1.89795
10/6/2011 1.89795
5/16/2012 1.89795
10/3/2012 1.89795
9/4/2013 1.89795
12/4/2013 1.89795
5/28/2014 1.89795
11/5/2014 1.89795
6/8/2015 1.89795
10/27/2015 1.89795
6/29/2016 1.89795
Group: MW-13 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Group: MW-14 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Group: MW-15 Date Residual
5/13/2010 3.40615
10/7/2010 0.283846
5/19/2011 0.283846
10/6/2011 0.283846
5/16/2012 0.283846
10/3/2012 0.283846
9/4/2013 0.283846
Page 73
12/4/2013 0.283846
5/28/2014 0.283846
11/5/2014 0.283846
6/8/2015 0.283846
10/27/2015 0.283846
6/29/2016 0.283846
Group: MW-16 Date Residual
5/13/2010 0.237692
10/7/2010 3.55231
5/19/2011 3.55231
10/6/2011 3.55231
5/16/2012 3.55231
10/3/2012 3.55231
9/4/2013 3.55231
12/4/2013 3.55231
5/28/2014 3.55231
11/5/2014 3.55231
6/8/2015 3.55231
10/27/2015 3.55231
6/29/2016 38.8377
Group: MW-17 Date Residual
5/13/2010 3.49846
10/7/2010 0.291538
5/19/2011 0.291538
10/6/2011 0.291538
5/16/2012 0.291538
10/3/2012 0.291538
9/4/2013 0.291538
12/4/2013 0.291538
5/28/2014 0.291538
11/5/2014 0.291538
6/8/2015 0.291538
10/27/2015 0.291538
6/29/2016 0.291538
Page 74
Poisson Prediction Limit (Inter-Well)
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Recent Dates = 1
Poisson Count of 117 background Samples = 271.02
99% t-test = 2.35892
95% t-test = 1.6581
Well: MW-10
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-2
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-3
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-4
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-5
Page 75
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-6
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-7
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
2 0.01 FALSE FALSE
Well: MW-8
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-9
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-13
Number of comparisons = 1
Page 76
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-14
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-15
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Well: MW-16
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 42.4 TRUE TRUE
Well: MW-17
Number of comparisons = 1
Future Samples (k) = 1
c = 0.00854701
99% Prediction Limit (Tk) = 5.9458
95% Prediction Limit (Tk) = 4.86253
Samples Sum 95 %tile 99 %tile
1 0.01 FALSE FALSE
Page 77
Non-Parametric Prediction Interval
Intra-Well Comparison for MW-16
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 91.6667%
Future Samples (k) = 1
Recent Dates = 1
Baseline Measurements (n) = 12
Maximum Baseline Concentration = 3.8
Confidence Level = 92.3%
False Positive Rate = 7.7%
Baseline Measurements Date Value
5/13/2010 3.8
10/7/2010 ND<0.01
5/19/2011 ND<0.01
10/6/2011 ND<0.01
5/16/2012 ND<0.01
10/3/2012 ND<0.01
9/4/2013 ND<0.01
12/4/2013 ND<0.01
5/28/2014 ND<0.01
11/5/2014 ND<0.01
6/8/2015 ND<0.01
10/27/2015 ND<0.01
Date Count Mean Significant
6/29/2016 1 42.4 TRUE
Page 78
Concentrations (ppb)
Parameter: Zinc
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements: 547
Total Non-Detect: 485
Percent Non-Detects: 88.6654%
Total Background Measurements: 117
There are 3 background locations
Loc.Meas.ND Date Conc.Original
MW-1 39 38 (97.4359%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 78 78
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-11 39 28 (71.7949%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
Page 79
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 135 135
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 28 28
5/13/2010 13 13
10/7/2010 ND<0.01 ND<0.01
5/19/2011 13.7 13.7
10/6/2011 ND<0.01 ND<0.01
5/16/2012 394 394
10/3/2012 39.8 39.8
9/4/2013 10.6 10.6
12/4/2013 ND<0.01 ND<0.01
5/28/2014 17.7 17.7
11/5/2014 ND<0.01 ND<0.01
6/8/2015 57 57
10/27/2015 130 130
6/29/2016 77.8 77.8
MW-12 39 36 (92.3077%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
Page 80
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 50 50
10/19/2009 12 12
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 10.8 10.8
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
There are 14 compliance locations
Loc.Meas.ND Date Conc.Original
MW-10 39 26 (66.6667%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 10 10
5/13/2010 120 120
10/7/2010 260 260
5/19/2011 197 197
10/6/2011 138 138
5/16/2012 89.6 89.6
10/3/2012 44.6 44.6
9/4/2013 30 30
12/4/2013 24.4 24.4
5/28/2014 36.4 36.4
Page 81
11/5/2014 16 16
6/8/2015 ND<0.01 ND<0.01
10/27/2015 33 33
6/29/2016 44.8 44.8
MW-2 39 34 (87.1795%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 14 14
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 16.9 16.9
10/3/2012 20.2 20.2
9/4/2013 17.6 17.6
12/4/2013 15.3 15.3
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-3 39 39 (100%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
Page 82
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-4 39 38 (97.4359%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 13 13
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
Page 83
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-5 39 38 (97.4359%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 15.3 15.3
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-6 39 39 (100%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
Page 84
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-7 53 51 (96.2264%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 137 137
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
Page 85
11/23/2008 64 64
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-8 39 18 (46.1538%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 104 104
10/7/2004 121 121
5/19/2005 ND<0.01 ND<0.01
10/18/2005 158 158
5/9/2006 ND<0.01 ND<0.01
10/17/2006 146 146
5/16/2007 91 91
10/23/2007 130 130
6/11/2008 61 61
11/23/2008 ND<0.01 ND<0.01
5/7/2009 53 53
10/19/2009 2.5 2.5
Page 86
5/13/2010 110 110
10/7/2010 270 270
5/19/2011 47.9 47.9
10/6/2011 59.8 59.8
5/16/2012 133 133
10/3/2012 98.1 98.1
9/4/2013 42.7 42.7
12/4/2013 48.8 48.8
5/28/2014 ND<0.01 ND<0.01
11/5/2014 100 100
6/8/2015 110 110
10/27/2015 80 80
6/29/2016 13.3 13.3
MW-9 39 36 (92.3077%)12/9/1997 ND<10 ND<10
1/27/1998 ND<10 ND<10
3/25/1998 ND<10 ND<10
4/8/1998 ND<10 ND<10
11/6/1998 ND<10 ND<10
8/5/1999 ND<10 ND<10
11/9/1999 ND<0.01 ND<0.01
9/26/2000 ND<0.01 ND<0.01
1/30/2001 ND<0.01 ND<0.01
9/26/2001 ND<0.01 ND<0.01
5/30/2002 ND<0.01 ND<0.01
10/9/2002 ND<0.01 ND<0.01
5/16/2003 ND<0.01 ND<0.01
10/21/2003 ND<0.01 ND<0.01
5/27/2004 ND<0.01 ND<0.01
10/7/2004 ND<0.01 ND<0.01
5/19/2005 ND<0.01 ND<0.01
10/18/2005 ND<0.01 ND<0.01
5/9/2006 ND<0.01 ND<0.01
10/17/2006 ND<0.01 ND<0.01
5/16/2007 ND<0.01 ND<0.01
10/23/2007 ND<0.01 ND<0.01
6/11/2008 ND<0.01 ND<0.01
11/23/2008 ND<0.01 ND<0.01
5/7/2009 ND<0.01 ND<0.01
10/19/2009 ND<0.01 ND<0.01
5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 13.1 13.1
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 11.6 11.6
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 15 15
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-13 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
Page 87
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-14 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-15 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
MW-16 13 12 (92.3077%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 30 30
MW-17 13 13 (100%)5/13/2010 ND<0.01 ND<0.01
10/7/2010 ND<0.01 ND<0.01
5/19/2011 ND<0.01 ND<0.01
10/6/2011 ND<0.01 ND<0.01
Page 88
5/16/2012 ND<0.01 ND<0.01
10/3/2012 ND<0.01 ND<0.01
9/4/2013 ND<0.01 ND<0.01
12/4/2013 ND<0.01 ND<0.01
5/28/2014 ND<0.01 ND<0.01
11/5/2014 ND<0.01 ND<0.01
6/8/2015 ND<0.01 ND<0.01
10/27/2015 ND<0.01 ND<0.01
6/29/2016 ND<0.01 ND<0.01
There are 0 unused locations
Loc.Meas.ND Date Conc.Original
Page 89
Basic Statistics
Parameter: Zinc
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Measurements 547
Total Non-Detects 485 (88.6654%)
Pooled Mean 9.48527
Pooled Std Dev 33.3243
Compliance Meas.430
Compliance Mean 9.18649
Compliance Std Dev 30.7598
Background Meas.117
Background Mean 10.5833
Background Std Dev 41.549
Background Locations
There are 3 background location
Location Meas.Non-Detects % ND Total
MW-1 39 38 97.4359 128.33
MW-11 39 28 71.7949 976.82
MW-12 39 36 92.3077 133.1
Location Mean Std Dev Std Err Rank Sum Rank Mean
MW-1 3.29051 12.7338 0 9759 250.231
MW-11 25.0467 68.6231 0 12469 319.718
MW-12 3.41282 8.74552 0 10246 262.718
Compliance Locations
There are 14 compliance location
Location Obs.Non-Detects % ND Total
MW-10 39 26 66.6667 1104
MW-2 39 34 87.1795 144.28
MW-3 39 39 100 60.33
MW-4 39 38 97.4359 73.32
MW-5 39 38 97.4359 75.62
MW-6 39 39 100 60.33
MW-7 53 51 96.2264 261.45
MW-8 39 18 46.1538 2040.22
MW-9 39 36 92.3077 100
MW-13 13 13 100 0.13
MW-14 13 13 100 0.13
MW-15 13 13 100 0.13
MW-16 13 12 92.3077 30.12
MW-17 13 13 100 0.13
Location Mean Std Dev Dif From Bkg Std Err Rank Sum Rank Mean
MW-10 28.3077 57.4665 17.7244 5.61982 13061 334.897
MW-2 3.69949 6.28227 -6.88385 5.61982 10768 276.103
MW-3 1.54692 3.65152 -9.03641 5.61982 9477 243
MW-4 1.88 4.07548 -8.70333 5.61982 9727 249.41
MW-5 1.93897 4.25338 -8.64436 5.61982 9734 249.59
MW-6 1.54692 3.65152 -9.03641 5.61982 9477 243
Page 90
MW-7 4.93302 20.6506 -5.65031 5.03245 13456 253.887
MW-8 52.3133 62.4896 41.73 5.61982 15413 395.205
MW-9 2.5641 4.79792 -8.01923 5.61982 10230 262.308
MW-13 0.01 1.80556e-018 -10.5733 8.88572 3159 243
MW-14 0.01 1.80556e-018 -10.5733 8.88572 3159 243
MW-15 0.01 1.80556e-018 -10.5733 8.88572 3159 243
MW-16 2.31692 8.31773 -8.26641 8.88572 3425 263.462
MW-17 0.01 1.80556e-018 -10.5733 8.88572 3159 243
Analysis of Variance Statistics
SS Wells 116732
SS Total 606339
Kruskal-Wallis Statistics
Non-Detect Rank 243
Background Rank Sum 32474
Background Rank Mean 277.556
H Statistic 36.7974
H Adjusted for Ties 121.463
Page 91
Shapiro-Francia Test of Normality
Parameter: Zinc
All Locations
Normality Test of Parameter Concentrations
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Number of Measurements = 547
i x(i)m(i)sum(m^2)sum(mx)
1 0.01 0 0 0
2 0.01 -2.74777 7.55021 -0.0274777
3 0.01 -2.57583 14.1851 -0.053236
4 0.01 -2.45727 20.2233 -0.0778087
5 0.01 -2.36561 25.8195 -0.101465
6 0.01 -2.32634 31.2313 -0.124728
7 0.01 -2.25713 36.326 -0.1473
8 0.01 -2.19728 41.154 -0.169272
9 0.01 -2.14441 45.7525 -0.190716
10 0.01 -2.09693 50.1496 -0.211686
11 0.01 -2.05375 54.3675 -0.232223
12 0.01 -2.03352 58.5027 -0.252558
13 0.01 -1.99539 62.4843 -0.272512
14 0.01 -1.95996 66.3258 -0.292112
15 0.01 -1.92684 70.0385 -0.31138
16 0.01 -1.8957 73.6321 -0.330337
17 0.01 -1.86629 77.1152 -0.349
18 0.01 -1.85218 80.5457 -0.367522
19 0.01 -1.82501 83.8764 -0.385772
20 0.01 -1.79912 87.1132 -0.403763
21 0.01 -1.77438 90.2616 -0.421507
22 0.01 -1.75069 93.3265 -0.439014
23 0.01 -1.7392 96.3513 -0.456406
24 0.01 -1.71688 99.299 -0.473575
25 0.01 -1.6954 102.173 -0.490529
26 0.01 -1.67466 104.978 -0.507275
27 0.01 -1.65463 107.716 -0.523822
28 0.01 -1.63524 110.39 -0.540174
29 0.01 -1.62576 113.033 -0.556432
30 0.01 -1.60725 115.616 -0.572504
31 0.01 -1.58927 118.142 -0.588397
32 0.01 -1.57179 120.612 -0.604115
33 0.01 -1.55477 123.03 -0.619662
34 0.01 -1.5382 125.396 -0.635044
35 0.01 -1.53007 127.737 -0.650345
36 0.01 -1.5141 130.029 -0.665486
37 0.01 -1.49852 132.275 -0.680471
38 0.01 -1.48328 134.475 -0.695304
39 0.01 -1.46838 136.631 -0.709988
40 0.01 -1.46106 138.766 -0.724599
41 0.01 -1.44663 140.859 -0.739065
42 0.01 -1.4325 142.911 -0.75339
43 0.01 -1.41865 144.923 -0.767576
44 0.01 -1.40507 146.897 -0.781627
45 0.01 -1.39175 148.834 -0.795545
46 0.01 -1.38517 150.753 -0.809396
47 0.01 -1.3722 152.636 -0.823118
Page 92
48 0.01 -1.35946 154.484 -0.836713
49 0.01 -1.34694 156.298 -0.850182
50 0.01 -1.33462 158.08 -0.863529
51 0.01 -1.32251 159.829 -0.876754
52 0.01 -1.31652 161.562 -0.889919
53 0.01 -1.30469 163.264 -0.902966
54 0.01 -1.29303 164.936 -0.915896
55 0.01 -1.28155 166.578 -0.928712
56 0.01 -1.27024 168.192 -0.941414
57 0.01 -1.25908 169.777 -0.954005
58 0.01 -1.25357 171.349 -0.96654
59 0.01 -1.24264 172.893 -0.978967
60 0.01 -1.23187 174.41 -0.991286
61 0.01 -1.22123 175.902 -1.0035
62 0.01 -1.21073 177.368 -1.01561
63 0.01 -1.20553 178.821 -1.02766
64 0.01 -1.19522 180.249 -1.03961
65 0.01 -1.18504 181.654 -1.05146
66 0.01 -1.17499 183.034 -1.06321
67 0.01 -1.16505 184.392 -1.07486
68 0.01 -1.15522 185.726 -1.08642
69 0.01 -1.15035 187.05 -1.09792
70 0.01 -1.14069 188.351 -1.10933
71 0.01 -1.13113 189.63 -1.12064
72 0.01 -1.12168 190.888 -1.13185
73 0.01 -1.11232 192.126 -1.14298
74 0.01 -1.10306 193.342 -1.15401
75 0.01 -1.09847 194.549 -1.16499
76 0.01 -1.08935 195.736 -1.17589
77 0.01 -1.08032 196.903 -1.18669
78 0.01 -1.07138 198.051 -1.1974
79 0.01 -1.06252 199.18 -1.20803
80 0.01 -1.05812 200.299 -1.21861
81 0.01 -1.04939 201.4 -1.2291
82 0.01 -1.04073 202.483 -1.23951
83 0.01 -1.03215 203.549 -1.24983
84 0.01 -1.02365 204.597 -1.26007
85 0.01 -1.01522 205.627 -1.27022
86 0.01 -1.01104 206.65 -1.28033
87 0.01 -1.00271 207.655 -1.29036
88 0.01 -0.994457 208.644 -1.3003
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Page 97
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Page 98
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Page 99
447 10 0.900227 304.242 256.244
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Page 100
504 17.7 1.40507 378.722 995.151
505 20.2 1.41865 380.735 1023.81
506 24.4 1.4325 382.787 1058.76
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528 91 1.79912 439.769 3008.67
529 98.1 1.82501 443.1 3187.71
530 100 1.85218 446.53 3372.93
531 104 1.86629 450.013 3567.02
532 110 1.8957 453.607 3775.55
533 110 1.92684 457.319 3987.5
534 120 1.95996 461.161 4222.69
535 121 1.99539 465.143 4464.14
536 130 2.03352 469.278 4728.49
537 130 2.05375 473.496 4995.48
538 133 2.09693 477.893 5274.37
539 135 2.14441 482.491 5563.87
540 137 2.19728 487.319 5864.9
541 138 2.25713 492.414 6176.38
542 146 2.32634 497.826 6516.03
543 158 2.36561 503.422 6889.79
544 197 2.45727 509.46 7373.88
545 260 2.57583 516.095 8043.59
546 270 2.74777 523.645 8785.49
547 394 0 523.645 8785.49
Data Set Standard Deviation = 33.3243
Numerator = 7.71848e+007
Denominator = 3.17506e+008
W Statistic = 0.243097 = 7.71848e+007 / 3.17506e+008
5% Critical value of 0.976 exceeds 0.243097
Evidence of non-normality at 95% level of significance
1% Critical value of 0.967 exceeds 0.243097
Evidence of non-normality at 99% level of significance
Page 101
Levene's Test for Equal of Variance
Parameter: Zinc
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Overall Mean = 11.8719
Overall Std Dev = 27.4866
Overall Total = 6493.95
SS Groups = 132246
SS Total = 412511
ANOVA Table
Source of Sum of Degrees of Mean
Variation Squares Freedom Squares F
Between Groups 132246 16 8265.38 15.6304
Error (within groups)280265 530 528.801
Totals 412511 546
95% F-Statistic = 1.57
15.6304 exceeds 1.57; assumption of equal variance should be rejected
Group: MW-1 Sample Residual
12/9/1997 6.70949
1/27/1998 6.70949
3/25/1998 6.70949
4/8/1998 6.70949
11/6/1998 6.70949
8/5/1999 74.7095
11/9/1999 3.28051
9/26/2000 3.28051
1/30/2001 3.28051
9/26/2001 3.28051
5/30/2002 3.28051
10/9/2002 3.28051
5/16/2003 3.28051
10/21/2003 3.28051
5/27/2004 3.28051
10/7/2004 3.28051
5/19/2005 3.28051
10/18/2005 3.28051
5/9/2006 3.28051
10/17/2006 3.28051
5/16/2007 3.28051
10/23/2007 3.28051
6/11/2008 3.28051
11/23/2008 3.28051
5/7/2009 3.28051
10/19/2009 3.28051
5/13/2010 3.28051
10/7/2010 3.28051
5/19/2011 3.28051
10/6/2011 3.28051
Page 102
5/16/2012 3.28051
10/3/2012 3.28051
9/4/2013 3.28051
12/4/2013 3.28051
5/28/2014 3.28051
11/5/2014 3.28051
6/8/2015 3.28051
10/27/2015 3.28051
6/29/2016 3.28051
Group: MW-11 Sample Residual
12/9/1997 15.0467
1/27/1998 15.0467
3/25/1998 15.0467
4/8/1998 15.0467
11/6/1998 15.0467
8/5/1999 15.0467
11/9/1999 25.0367
9/26/2000 25.0367
1/30/2001 25.0367
9/26/2001 25.0367
5/30/2002 25.0367
10/9/2002 25.0367
5/16/2003 25.0367
10/21/2003 25.0367
5/27/2004 25.0367
10/7/2004 109.953
5/19/2005 25.0367
10/18/2005 25.0367
5/9/2006 25.0367
10/17/2006 25.0367
5/16/2007 25.0367
10/23/2007 25.0367
6/11/2008 25.0367
11/23/2008 25.0367
5/7/2009 25.0367
10/19/2009 2.95333
5/13/2010 12.0467
10/7/2010 25.0367
5/19/2011 11.3467
10/6/2011 25.0367
5/16/2012 368.953
10/3/2012 14.7533
9/4/2013 14.4467
12/4/2013 25.0367
5/28/2014 7.34667
11/5/2014 25.0367
6/8/2015 31.9533
10/27/2015 104.953
6/29/2016 52.7533
Group: MW-12 Sample Residual
12/9/1997 6.58718
1/27/1998 6.58718
3/25/1998 6.58718
4/8/1998 6.58718
11/6/1998 6.58718
Page 103
8/5/1999 6.58718
11/9/1999 3.40282
9/26/2000 3.40282
1/30/2001 3.40282
9/26/2001 3.40282
5/30/2002 3.40282
10/9/2002 3.40282
5/16/2003 3.40282
10/21/2003 3.40282
5/27/2004 3.40282
10/7/2004 3.40282
5/19/2005 3.40282
10/18/2005 3.40282
5/9/2006 3.40282
10/17/2006 3.40282
5/16/2007 3.40282
10/23/2007 3.40282
6/11/2008 3.40282
11/23/2008 3.40282
5/7/2009 46.5872
10/19/2009 8.58718
5/13/2010 3.40282
10/7/2010 3.40282
5/19/2011 3.40282
10/6/2011 3.40282
5/16/2012 3.40282
10/3/2012 3.40282
9/4/2013 3.40282
12/4/2013 7.38718
5/28/2014 3.40282
11/5/2014 3.40282
6/8/2015 3.40282
10/27/2015 3.40282
6/29/2016 3.40282
Group: MW-10 Date Residual
12/9/1997 18.3077
1/27/1998 18.3077
3/25/1998 18.3077
4/8/1998 18.3077
11/6/1998 18.3077
8/5/1999 18.3077
11/9/1999 28.2977
9/26/2000 28.2977
1/30/2001 28.2977
9/26/2001 28.2977
5/30/2002 28.2977
10/9/2002 28.2977
5/16/2003 28.2977
10/21/2003 28.2977
5/27/2004 28.2977
10/7/2004 28.2977
5/19/2005 28.2977
10/18/2005 28.2977
5/9/2006 28.2977
10/17/2006 28.2977
5/16/2007 28.2977
Page 104
10/23/2007 28.2977
6/11/2008 28.2977
11/23/2008 28.2977
5/7/2009 28.2977
10/19/2009 18.3077
5/13/2010 91.6923
10/7/2010 231.692
5/19/2011 168.692
10/6/2011 109.692
5/16/2012 61.2923
10/3/2012 16.2923
9/4/2013 1.69231
12/4/2013 3.90769
5/28/2014 8.09231
11/5/2014 12.3077
6/8/2015 28.2977
10/27/2015 4.69231
6/29/2016 16.4923
Group: MW-2 Date Residual
12/9/1997 6.30051
1/27/1998 6.30051
3/25/1998 6.30051
4/8/1998 6.30051
11/6/1998 6.30051
8/5/1999 6.30051
11/9/1999 3.68949
9/26/2000 3.68949
1/30/2001 3.68949
9/26/2001 3.68949
5/30/2002 3.68949
10/9/2002 3.68949
5/16/2003 3.68949
10/21/2003 3.68949
5/27/2004 3.68949
10/7/2004 3.68949
5/19/2005 3.68949
10/18/2005 3.68949
5/9/2006 3.68949
10/17/2006 3.68949
5/16/2007 3.68949
10/23/2007 3.68949
6/11/2008 3.68949
11/23/2008 3.68949
5/7/2009 3.68949
10/19/2009 10.3005
5/13/2010 3.68949
10/7/2010 3.68949
5/19/2011 3.68949
10/6/2011 3.68949
5/16/2012 13.2005
10/3/2012 16.5005
9/4/2013 13.9005
12/4/2013 11.6005
5/28/2014 3.68949
11/5/2014 3.68949
6/8/2015 3.68949
Page 105
10/27/2015 3.68949
6/29/2016 3.68949
Group: MW-3 Date Residual
12/9/1997 8.45308
1/27/1998 8.45308
3/25/1998 8.45308
4/8/1998 8.45308
11/6/1998 8.45308
8/5/1999 8.45308
11/9/1999 1.53692
9/26/2000 1.53692
1/30/2001 1.53692
9/26/2001 1.53692
5/30/2002 1.53692
10/9/2002 1.53692
5/16/2003 1.53692
10/21/2003 1.53692
5/27/2004 1.53692
10/7/2004 1.53692
5/19/2005 1.53692
10/18/2005 1.53692
5/9/2006 1.53692
10/17/2006 1.53692
5/16/2007 1.53692
10/23/2007 1.53692
6/11/2008 1.53692
11/23/2008 1.53692
5/7/2009 1.53692
10/19/2009 1.53692
5/13/2010 1.53692
10/7/2010 1.53692
5/19/2011 1.53692
10/6/2011 1.53692
5/16/2012 1.53692
10/3/2012 1.53692
9/4/2013 1.53692
12/4/2013 1.53692
5/28/2014 1.53692
11/5/2014 1.53692
6/8/2015 1.53692
10/27/2015 1.53692
6/29/2016 1.53692
Group: MW-4 Date Residual
12/9/1997 8.12
1/27/1998 8.12
3/25/1998 8.12
4/8/1998 8.12
11/6/1998 8.12
8/5/1999 8.12
11/9/1999 1.87
9/26/2000 1.87
1/30/2001 1.87
9/26/2001 1.87
5/30/2002 1.87
10/9/2002 1.87
Page 106
5/16/2003 1.87
10/21/2003 1.87
5/27/2004 1.87
10/7/2004 1.87
5/19/2005 1.87
10/18/2005 1.87
5/9/2006 1.87
10/17/2006 1.87
5/16/2007 1.87
10/23/2007 1.87
6/11/2008 1.87
11/23/2008 1.87
5/7/2009 1.87
10/19/2009 11.12
5/13/2010 1.87
10/7/2010 1.87
5/19/2011 1.87
10/6/2011 1.87
5/16/2012 1.87
10/3/2012 1.87
9/4/2013 1.87
12/4/2013 1.87
5/28/2014 1.87
11/5/2014 1.87
6/8/2015 1.87
10/27/2015 1.87
6/29/2016 1.87
Group: MW-5 Date Residual
12/9/1997 8.06103
1/27/1998 8.06103
3/25/1998 8.06103
4/8/1998 8.06103
11/6/1998 8.06103
8/5/1999 8.06103
11/9/1999 1.92897
9/26/2000 1.92897
1/30/2001 1.92897
9/26/2001 1.92897
5/30/2002 1.92897
10/9/2002 1.92897
5/16/2003 1.92897
10/21/2003 1.92897
5/27/2004 1.92897
10/7/2004 1.92897
5/19/2005 1.92897
10/18/2005 1.92897
5/9/2006 1.92897
10/17/2006 1.92897
5/16/2007 1.92897
10/23/2007 1.92897
6/11/2008 1.92897
11/23/2008 1.92897
5/7/2009 1.92897
10/19/2009 1.92897
5/13/2010 1.92897
10/7/2010 1.92897
Page 107
5/19/2011 1.92897
10/6/2011 13.361
5/16/2012 1.92897
10/3/2012 1.92897
9/4/2013 1.92897
12/4/2013 1.92897
5/28/2014 1.92897
11/5/2014 1.92897
6/8/2015 1.92897
10/27/2015 1.92897
6/29/2016 1.92897
Group: MW-6 Date Residual
12/9/1997 8.45308
1/27/1998 8.45308
3/25/1998 8.45308
4/8/1998 8.45308
11/6/1998 8.45308
8/5/1999 8.45308
11/9/1999 1.53692
9/26/2000 1.53692
1/30/2001 1.53692
9/26/2001 1.53692
5/30/2002 1.53692
10/9/2002 1.53692
5/16/2003 1.53692
10/21/2003 1.53692
5/27/2004 1.53692
10/7/2004 1.53692
5/19/2005 1.53692
10/18/2005 1.53692
5/9/2006 1.53692
10/17/2006 1.53692
5/16/2007 1.53692
10/23/2007 1.53692
6/11/2008 1.53692
11/23/2008 1.53692
5/7/2009 1.53692
10/19/2009 1.53692
5/13/2010 1.53692
10/7/2010 1.53692
5/19/2011 1.53692
10/6/2011 1.53692
5/16/2012 1.53692
10/3/2012 1.53692
9/4/2013 1.53692
12/4/2013 1.53692
5/28/2014 1.53692
11/5/2014 1.53692
6/8/2015 1.53692
10/27/2015 1.53692
6/29/2016 1.53692
Group: MW-7 Date Residual
12/9/1997 5.06698
1/27/1998 5.06698
3/25/1998 5.06698
Page 108
4/8/1998 5.06698
11/6/1998 5.06698
8/5/1999 5.06698
11/9/1999 4.92302
9/26/2000 4.92302
1/30/2001 4.92302
9/26/2001 4.92302
5/30/2002 4.92302
10/9/2002 4.92302
5/16/2003 4.92302
10/21/2003 4.92302
5/27/2004 4.92302
10/7/2004 4.92302
5/19/2005 4.92302
10/18/2005 132.067
5/9/2006 4.92302
10/17/2006 4.92302
5/16/2007 4.92302
10/23/2007 4.92302
6/11/2008 4.92302
11/23/2008 59.067
5/7/2009 4.92302
10/19/2009 4.92302
10/19/2009 4.92302
5/13/2010 4.92302
5/13/2010 4.92302
10/7/2010 4.92302
10/7/2010 4.92302
5/19/2011 4.92302
5/19/2011 4.92302
10/6/2011 4.92302
10/6/2011 4.92302
5/16/2012 4.92302
5/16/2012 4.92302
10/3/2012 4.92302
10/3/2012 4.92302
9/4/2013 4.92302
9/4/2013 4.92302
12/4/2013 4.92302
12/4/2013 4.92302
5/28/2014 4.92302
5/28/2014 4.92302
11/5/2014 4.92302
11/5/2014 4.92302
6/8/2015 4.92302
6/8/2015 4.92302
10/27/2015 4.92302
10/27/2015 4.92302
6/29/2016 4.92302
6/29/2016 4.92302
Group: MW-8 Date Residual
12/9/1997 42.3133
1/27/1998 42.3133
3/25/1998 42.3133
4/8/1998 42.3133
11/6/1998 42.3133
Page 109
8/5/1999 42.3133
11/9/1999 52.3033
9/26/2000 52.3033
1/30/2001 52.3033
9/26/2001 52.3033
5/30/2002 52.3033
10/9/2002 52.3033
5/16/2003 52.3033
10/21/2003 52.3033
5/27/2004 51.6867
10/7/2004 68.6867
5/19/2005 52.3033
10/18/2005 105.687
5/9/2006 52.3033
10/17/2006 93.6867
5/16/2007 38.6867
10/23/2007 77.6867
6/11/2008 8.68667
11/23/2008 52.3033
5/7/2009 0.686667
10/19/2009 49.8133
5/13/2010 57.6867
10/7/2010 217.687
5/19/2011 4.41333
10/6/2011 7.48667
5/16/2012 80.6867
10/3/2012 45.7867
9/4/2013 9.61333
12/4/2013 3.51333
5/28/2014 52.3033
11/5/2014 47.6867
6/8/2015 57.6867
10/27/2015 27.6867
6/29/2016 39.0133
Group: MW-9 Date Residual
12/9/1997 7.4359
1/27/1998 7.4359
3/25/1998 7.4359
4/8/1998 7.4359
11/6/1998 7.4359
8/5/1999 7.4359
11/9/1999 2.5541
9/26/2000 2.5541
1/30/2001 2.5541
9/26/2001 2.5541
5/30/2002 2.5541
10/9/2002 2.5541
5/16/2003 2.5541
10/21/2003 2.5541
5/27/2004 2.5541
10/7/2004 2.5541
5/19/2005 2.5541
10/18/2005 2.5541
5/9/2006 2.5541
10/17/2006 2.5541
5/16/2007 2.5541
Page 110
10/23/2007 2.5541
6/11/2008 2.5541
11/23/2008 2.5541
5/7/2009 2.5541
10/19/2009 2.5541
5/13/2010 2.5541
10/7/2010 2.5541
5/19/2011 10.5359
10/6/2011 2.5541
5/16/2012 2.5541
10/3/2012 2.5541
9/4/2013 9.0359
12/4/2013 2.5541
5/28/2014 2.5541
11/5/2014 2.5541
6/8/2015 12.4359
10/27/2015 2.5541
6/29/2016 2.5541
Group: MW-13 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Group: MW-14 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Group: MW-15 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
Page 111
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Group: MW-16 Date Residual
5/13/2010 2.30692
10/7/2010 2.30692
5/19/2011 2.30692
10/6/2011 2.30692
5/16/2012 2.30692
10/3/2012 2.30692
9/4/2013 2.30692
12/4/2013 2.30692
5/28/2014 2.30692
11/5/2014 2.30692
6/8/2015 2.30692
10/27/2015 2.30692
6/29/2016 27.6831
Group: MW-17 Date Residual
5/13/2010 1.73472e-018
10/7/2010 1.73472e-018
5/19/2011 1.73472e-018
10/6/2011 1.73472e-018
5/16/2012 1.73472e-018
10/3/2012 1.73472e-018
9/4/2013 1.73472e-018
12/4/2013 1.73472e-018
5/28/2014 1.73472e-018
11/5/2014 1.73472e-018
6/8/2015 1.73472e-018
10/27/2015 1.73472e-018
6/29/2016 1.73472e-018
Page 112
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Zinc
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 88.6654%
Number of comparisons = 14
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 117
Maximum Background Value = 394
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 6/29/2016 1 44.8 FALSE
MW-2 6/29/2016 1 0.01 FALSE
MW-3 6/29/2016 1 0.01 FALSE
MW-4 6/29/2016 1 0.01 FALSE
MW-5 6/29/2016 1 0.01 FALSE
MW-6 6/29/2016 1 0.01 FALSE
MW-7 6/29/2016 2 0.01 FALSE
MW-8 6/29/2016 1 13.3 FALSE
MW-9 6/29/2016 1 0.01 FALSE
MW-13 6/29/2016 1 0.01 FALSE
MW-14 6/29/2016 1 0.01 FALSE
MW-15 6/29/2016 1 0.01 FALSE
MW-16 6/29/2016 1 30 FALSE
MW-17 6/29/2016 1 0.01 FALSE