9601_WayneCounty_GWMR_DIN28166_20160901

Wayne County Active C&D and Closed MSWLF
Dudley, North Carolina
September 2016
MESCO Project Number: G16016.0
Semi-Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
P.O. Box 97
Garner, NC 27529
License No. C-0281

Permit Number: 96-01
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 3
Groundwater Samples Detected Above Standards Page 3
Surface Water Samples Detected Above Standards Page 3
Corrective Action Update Page 3
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 4
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer w/ VOC Detection Above 2L Standard Figure 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections in Water Samples Above SWSL, 2L, 2B, GWP or MCL (Appendix I) Table 5
Detections in Water Samples Above MDL (Appendix II Exclusive) Table 6
MNA Parameter Data Summary Table 7
Hydrologic Properties at Monitoring Well Locations Table 8
APPENDICIES
Laboratory Analysis Reports and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
December 26, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update
Wayne County Active C&D and Closed MSWLF (Dudley)
Permit No. 96-01
MESCO Project No. G16016.0
Event Date(s): September 1, 2016
Dear Ms. Drummond,
Introduction
The Wayne County Landfill (Permit #96-01) is located at 460 S Landfill Road (SR 1129), Dudley, Wayne County,
North Carolina. A topographic map showing the location of the site is included as Figure 1.
The Wayne County unlined closed Municipal Solid Waste Landfill (MSWLF) and active Construction and Demolition
(C&D) Landfill located in Dudley NC, currently operating under Permit #96-01 is required to submit semi-annual
compliance reports as a condition of 15A NCAC 13B.1630. This report documents the quality of the ground and
surface waters during this monitoring event performed on September 1, 2016. Laboratory analytical results, which
consisted of targeting Appendix II constituents, indicate that levels of one or two metals were detected above
applicable regulatory groundwater Standards in samples collected from four wells including the background well. No
contaminants were detected in any surface water sample sample during this event. Corrective action via monitored
natural attenuation (MNA) is planned to continue.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, corrective action update,
ground/surface water characterization, and findings. Well construction summary table, field observations table, field
parameter data table, sampling and analysis summary table, detections compared to Standards tables, MNA parameter
summary table, a groundwater flow directions/rates table, potentiometric map, quality assurance/quality control data,
and laboratory analytical data results are enclosed herein.
Background
Prior to operating as a C&D landfill the site operated as a Municipal Solid Waste (MSW) unlined sanitary landfill that
consisted of two units. The first unit (Unit 1) was closed prior to October 1991 with a 24 inch final soil cover. The
second unit (Unit 2) was closed with a low permeability cohesive cap and erosive layer prior to December 31, 1998 in
accordance with the Transition Plan. The C&D landfill is operating on top of the Unit 2 MSW landfill. The separate
active Subtitle D Lined MSWLF (permit #96-06), located adjacent to the C&D landfill across an unnamed tributary of
Edward's Branch, was monitored in conjunction with this site but reported separately.

Water quality at this landfill has been monitored at least semi-annually since 1991. Current data was compared to data
compiled since 1994 in support of this report. Municipal Engineering Services Company, P.A. (MESCO) submitted an
Assessment and Corrective Action (ACM) [DIN8821] report dated August 30, 2007 which was approved by the NC Solid
Waste Section (SWS) on November 1, 2007 [DIN3328]. MESCO then developed a Corrective Action Plan (CAP)
[DIN8821] on October 22, 2009 which was approved by the SWS on October 23, 2009 [DIN8822].
Groundwater remediation using Monitored Natural Attenuation (MNA) was initiated on August 6, 2009 and has
continued on a semi-annual basis.
Following establishment of the two year MNA baseline, MESCO completed a Corrective Action Evaluation Report
(CAER) [DIN 13923] on May 10, 2011. The CAER was reviewed and the proposed modifications of MNA parameters
and frequency were approved by the SWS [DIN 16967]. Background well MW-1 was abandoned and replaced by MW-
1R as pre-authorized by SWS [DIN 19050] on June 4, 2013. MESCO submitted a Request for Appendix II Groundwater
Monitoring Modification dated April 24, 2014 which was approved by the SWS. The Water Quality Sampling and
Analysis Plan (SAP) which provides for a subset of wells to decrease Appendix II monitoring frequency was revised and
submitted on December 15, 2014 as requested by the SWS. Groundwater remediation through MNA per the CAP is
scheduled to continue provided there is no change directed by the SWS.
Sampling Procedure
MESCO performed this sampling event utilizing portable monitoring methodology in accordance with the approved SAP
based on the Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008.
The new site-specific SAP entails continued semi-annual water quality monitoring which includes annual corrective
action monitoring and targeting of specific Appendix II constituents at a subset of wells once every three years.
Keeping with the established schedule this event consists of assessment monitoring (Appendix II) at all groundwater
locations. Water samples were collected from monitoring locations designated in the SAP with the exception of SW-2
and SW-3 which are chronically dry. Water quality monitoring was performed on ten wells (MW-2, MW-3, MW-4,
MW-5, MW-6, MW-7, MW-8, MW-9, MW-10 and MW-11), background well (MW-1R) and two surface water points
(SW-1, SW-2). Quality control measures implemented during this event included quantification of an equipment blank
(EB), field blank (FB) and travel blank (TB). A supplemental surface water sample (SW-By_MW-2) was collected from
the western tributary of Edward's Branch directly downgradient of MW-2. Data from a surface water location from the
Subtitle D Lined SAP SW-6 (shared) is presented because this local discharge feature is shared by both permits.
Monitoring locations are depicted on the potentiometric map, included as Figure 2.
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and integrity
of all monitoring locations were visually evaluated and deficiencies rectified as documented on Table 2. The depth to
water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low-flow
pumping methodology or bailing was utilized to adequately purge the wells a minimum of three times the volume of
standing water in the well or until dry. Surface water samples were dipped from the surface of the creeks at previously
designated locations. Samples were then placed into laboratory-prepared, pre-preserved containers. Samples were kept
on ice and transported to a NC-certified laboratory under proper chain of custody (C-O-C) protocol and analyzed within
the required hold times.
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature,
dissolved oxygen (DO), oxidation reduction potential (ORP) and visual turbidity. A summary of the field parameter data
is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratories (PACE) performed the laboratory analysis. All groundwater samples were analyzed for
Appendix II constituents and surface water samples were tested for parameters listed in Appendix I of 40 CFR 258. All
water samples were tested for tetrahydrofuran. Additionally MNA monitoring consisting of field parameters was
performed on MW-2, MW-8 and MW-1R. A sampling and analysis table summarizing the locations, targeted
constituents and methods is presented as Table 4. Laboratory results and C-O-Cs are contained in Appendix A.
2
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below the
current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and surface water
samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a Class C
waterbody and Federal Maximum Contaminant Levels (MCL) also known as “Primary Drinking Water Standards”.
Table 6 shows the Appendix II exclusive (defined in this report as not also listed in Appendix I) constituents detected
above the MDL.
Quality Control Samples
Total tin (Appendix II constituent) and tetrahydrofuran (CDLF specific analyte) were detected in the quality control
blank(s) (FB and EB). Since the tetrahydrofuran was also only detected in MW-2 and MW-11 at a very low “j-qualified”
concentration any potential artifact contamination is largely non-consequential.
Groundwater Samples Detected Above Standards
Total arsenic was detected in samples MW-2 (43 µg/L) and MW-11 (10.4 µg/L) above the 2L Standard (10.0 µg/L).
Total vanadium was detected in samples MW-2 (11 µg/L), MW-3 (17.6 µg/L) and background well MW-1R (28.4 µg/L)
above the GWP Standard (3.5 µg/L).
Surface Water Samples Detected Above Standards
Constituents were not detected in any surface water sample in concentrations above the established 2B Standards.
Supplemental surface water sample SW-By_MW-2 collected at the property line approximately 166 feet hydraulically
downgradient of MW-2 continues to lack contaminants.
Corrective Action Update
Groundwater remediation measures through MNA continues to be implemented at the facility. Semi-annual MNA
monitoring of MW-2, MW-8 and background well MW-1 was initiated on August 6, 2009 and was consistently
performed for the full suite of SWS recommended parameters for seven consecutive semi-annual events. The SAP
prescribes MNA monitoring for specific constituents to be performed annually or bi-annually. Keeping with established
SAP select MNA parameters were analyzed during this event as presented on Table 7.
The active Landfill Gas Collection and Control System (GCCS) continues operations. The GCCS extracts LFG for
energy production therefore is closely maintained for optimum efficiency which may have a collateral remediation effect
on groundwater.
Groundwater and Surface Water Characterization
A potentiometric map of the uppermost aquifer created from groundwater elevation data collected during this event is
included as Figure 2. Groundwater flow rates and directions were calculated based on collected data and are included in
Table 8. Groundwater generally generally flows southwesterly towards Edward's Branch ranging from approximately 3
foot/year (MW-5) to 328 feet/year (MW-3) with an average rate of 72 feet/year The calculated flow directions and
gradients are consistent with historical observations. Streams located within the facility boundaries were visually
observed at low seasonal flow, low volume and low turbidity.
Findings
The preliminary source of total vanadium is not believed to be anthropogenic but rather originating from erosion of
natural deposits as evidenced by higher levels observed in samples collected from the background well MW-1R. The
source of the elevated concentrations of arsenic detected in samples MW-2 and MW-11 is either natural or a product of
LFG.
3
Benzene at MW-2, the only VOC detected in excess of regulatory compliance Standards since 2007, was below the 2L
Standard. Conditions near MW-2 appear to improve as levels of benzene at MW-2 have been below the 2L Standard
three out of the last four events. The horizontal extent of the plume downgradient of MW-2 appears to have not impacted
the adjacent local discharge feature as evidenced by the lack of detections in surface water samples SW-By_MW-2 and
SW-1.
Groundwater quality monitored by MW-8, located hydraulically upgradient of waste, has improved significantly since the
ACM was drafted as evidenced by the lack of contaminant detections in levels exceeding the 2L Standard during the past
9 years. The single contaminant of concern detected above 2L in MW-8 since ACM (1,4-dichlorobenzene) has not been
detected at a concentration above its current 2L Standard since August 2007.
Constituents listed in 40 CFR 258 Appendix II that are not also listed in Appendix I consisted of only total cyanide well
below the SWSL and 2L Standard.
The lack of detections in surface water samples indicate the discharge features remain unimpacted.
Closing
Water quality monitoring which will include targeting the full suite of MNA constituents is planned for February 2017. If
you have any questions or comments, please contact us at [phone] or by email at [e-mail] .
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
Jonathan Pfohl Steven R. Gandy, Ph.D., P.E.Environmental Specialist Senior Project Manager

Enclosures
cc: Mr. Tim Rogers
Wayne County
Ms. Christine Ritter
Solid Waste Section

4
Figures
Topographic Map with Site Location
01 1 MILE
FIGURE 1
Wayne County Landfill North Carolina (Dudley)
CLOSED MSW FACILITY
SUBTITLE D MSW
LANDFILL FACILITY
460 B South Landfill Rd
Dudley, NC 28333
Lat:35-17-19.1338
Long:-78-04-17.2971
Northing:561283.19
Easting:2277068.62
N
Tables
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
September 1, 2016
Latitude Longitude
(inches)(ft)
MW-1R 6/4/13 2 27.32 12.32 15 Soil Sand 169.64 166.64 148.05 21.59 35.292408 -78.064431
MW-2 8/28/90 2 15 10 5 Soil Sand 134.52 132.78 128.50 6.02 35.290714 -78.076225
MW-3 8/27/90 2 18 12 6 Soil Sand 134.81 133.03 134.81 0.00 35.293192 -78.072156
MW-4 8/28/90 2 15 10 5 Soil Sand 150.20 148.17 142.72 7.48 35.293003 -78.066253
MW-5 8/31/94 2 18 3 15 Soil Sand 124.78 120.56 121.77 3.01 35.292597 -78.075936
MW-6 8/31/94 2 18.14 3.14 15 Soil Sand 145.53 143.62 138.28 7.25 35.293439 -78.068656
MW-7 8/31/94 2 19 4 15 Soil Sand 143.59 140.74 134.31 9.28 35.288761 -78.074700
MW-8 8/30/94 2 29 14 15 Soil Sand 161.88 160.88 143.13 18.75 35.290178 -78.068706
MW-9 7/9/09 2 25 10 15 Soil Sand 162.96 159.78 144.23 18.73 35.290025 -78.068242
MW-10 7/9/09 2 25 10 15 Soil Sand 162.90 160.01 147.06 15.84 35.289869 -78.069167
MW-11 7/9/09 2 15 5 10 Soil Sand 127.23 124.50 124.17 3.06 35.291844 -78.076250
NOTE:
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
na = not available
bgs = below ground surface
amsl= above mean sea level
btoc = below top of PVC well casing
Wayne County Active C&D and Closed MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
September 1, 2016
Locked Comments
MW-1R Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes
MW-3 Yes Yes Yes repaired Yes Yes
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Yes
MW-6 Yes Yes Yes Yes Yes Yes Hear water cascade into well
MW-7 Yes Yes Yes Yes Yes Yes
MW-8 Yes Yes Yes Yes Yes Yes
MW-9 Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes covered
SW-1 Yes -----Shared Downstream of SW-3
SW-2 No -----Dry Upstream nearest MW-7.
SW-3 No -----Dry-Shared Upstream nearest MW-4
SW-6 Yes -----Shared nearest MW-5
SW-By _MW-2 Yes -----Not required but supplemental sample
Any unusual field conditions, observations, or events:
SW-2 (Closed) upstream nearest MW-7 was dry which is typical.
SW-3 (Closed) upstream nearest MW-4 was dry which is typical
MW-3 well case lid and lock replaced by county.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Effective
Flowing artesian, lid & lock replaced
Flowing artesian, hinge rusting
Flowing artesian, lock rusting
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 3
Field Parameter Data Summary
September 1, 2016
Parameter Temp.ORP DO pH TDS Turbidity
Units C mg/L SU mg/L NTU or Visual
MW-1R 21.59 148.04 169.63 17.8 283 5.5 4.7 18 NR Moderate
MW-2 6.02 128.50 134.52 22.1 -51 0.6 6.0 1532 NR Clear
MW-3 0.00 134.81 134.81 18.0 242 2.2 5.7 44 NR Clear
MW-4 7.48 142.72 150.20 19.1 238 2.1 4.8 263 NR Clear
MW-5 3.01 121.77 124.78 20.4 189 2.3 4.4 68 NR Slight
MW-6 7.25 138.28 145.53 18.9 118 2.1 5.2 495 NR Clear
MW-7 9.28 134.31 143.59 21.1 281 2.3 4.2 71 NR Slight
MW-8 18.75 143.13 161.88 18.2 303 2.5 4.2 56 NR Clear
MW-9 18.73 144.23 162.96 NR NR NR NR NR NR NR
MW-10 15.84 147.06 162.90 NR NR NR NR NR NR NR
MW-11 3.06 124.17 127.23 20.7 132 4.3 5.5 1493 NR Slight
Minimum 0.00 121.77 124.78 17.8 -51 0.6 4.2 18 NR Clear
Average 10.09 137.00 147.09 19.6 193 2.7 5.0 449 NR Slight
Maximum 21.59 148.04 169.63 22.1 303 5.5 6.0 1532 NR Moderate
SW-1 ---22.1 NR NR 6.9 998 NR Slight
SW-2 Dry ---------
---22.7 193 5.9 6.4 242 NR Clear
SW-3 Dry ---------
SW-6 ---23.2 NR NR 6.9 883 NR Slight
Minimum ---22.1 NR NR 6.4 242 NR Clear
Average ---22.7 NR NR 6.7 708 NR Clear
Maximum ---23.2 NR NR 6.9 998 NR Slight
NR = No reading attempted
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
SW-ByMW-2
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 4
Sampling and Analysis Summary
September 1, 2016
App. I CDLF Field Parameter App. II
T o t a l M e t a l s
D i s s o l v e d O x y g e n (D O )
O x i d a t i o n R e d u c t i o n P o t e n t i a l (O R P )
T e m p e r a t u r e
C o n d u c t i v i t y
T o t a l D i s s o l v e d S o l i d s (T D S )
p H T u r b i d i t y
T o t a l M e t a l s
D i s s o l v e d M e t a l s
P e s t i c i d e s
H e r b i c i d e s -C h l o r i n a t e d
T o t a l C y a n i d e
S u l f i d e
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 8 2 6 0 B
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
V i s u a l
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 8 0 8 1 B
L a b S W 8 1 5 1 A
L a b E P A 8 0 8 2 A
L a b E P A 8 2 7 0 D
L a b E P A 9 0 1 4
L a b S M 1 8 4 5 0 0 -S D
MW-1 x x x x x x x x x x x x x x x
MW-2 x x x x x x x x x x x x x x x
MW-3 x x x x x x x x x x x x x x x
MW-4 x x x x x x x x x x x x x x x
MW-5 x x x x x x x x x x x x x x x
MW-6 x x x x x x x x x x x x x x x
MW-7 x x x x x x x x x x x x x x x
MW-8 x x x x x x x x x x x x x x x
MW-9 x x x x x x x x x x x x x x x
MW-10 x x x x x x x x x x x x x x x
MW-11 x x x x x x x x x x x x x x x
SW-1 x x x x x x x x x
SW-2 Dry so not sampled
x x x x x x x x
SW-3 Dry so not sampled
SW-6 x x x x x x x
EB x x x
FB x x x
TB x x
App I & II = Appendix I & II List from current 40 CFR 258
V O C s
T e t r a h y d r o f u r a n
V O C s
P o l y c h l o r i n a t e d b i p h e n y l (P C B )
S e m i v o l a t i l e O r g a n i c s (S V O C s )
SW-ByMW-2
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 5
September 1, 2016
Result Unit
MW-1R Chromium,Total 9/1/16 20.1 2.5 10 10 100 N (is Background)
MW-1R Vanadium,Total 9/1/16 28.4 2.5 25 NE 3.5 NE N (is Background)
MW-2 9/1/16 2.9 0.33 1 6 75
MW-2 Arsenic,Total 9/1/16 43 2.5 10 10 10 N or LFG
MW-2 Barium,Total 9/1/16 170 2.5 100 700 2000
MW-2 9/1/16 10.8 0.23 3 50 100
MW-2 9/1/16 4.5J 3.1 NE NE NE
MW-2 Vanadium,Total 9/1/16 11J 2.5 25 NE 3.5 NE N
MW-3 Selenium,Total 9/1/16 5J 5 10 20 50
MW-3 Vanadium,Total 9/1/16 17.6J 2.5 25 NE 3.5 NE N
MW-5 Zinc,Total 9/1/16 10.7 5 10 1000 NE
MW-6 Barium,Total 9/1/16 130 2.5 100 700 2000
MW-7 Cadmium,Total 9/1/16 1.5 0.5 1 2 5
MW-11 Arsenic,Total 9/1/16 10.4 2.5 10 10 10 N or LFG
MW-11 Barium,Total 9/1/16 200 2.5 100 700 2000
MW-11 9/1/16 4J 3.1 NE NE NE
SW-1 Barium,Total 9/1/16 175 2.5 100 200000 2000
SW-6 Barium,Total 9/1/16 166 2.5 100 200000 2000
FB 9/1/16 3.1J 10 NE NE NE
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to EMRF instructions.
J=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
Detections in Water Samples above SWSL, 2L, 2B, GWP or MCL
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
Chlorobenzene ug/L
Tetrahydrofuran ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Tetrahydrofuran ug/L
ug/L
ug/L
Tetrahydrofuran ug/L
1 Table contains constituents listed in 40CFR Appendix I detected at or above SWSL, GWP, 2L, 2B or MCL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 6
September 1, 2016
Sample ID Result Unit
MW-2 Cyanide 9/1/2016 5.3j 4 10 70 200
MW-8 Cyanide 9/1/2016 4.3j 4 10 70 200
MW-11 Cyanide 9/1/2016 4.2j 4 10 70 200
EB Tin, total 9/1/2016 2.9j 2.5 100 NE NE NE
FB Tin, total 9/1/2016 3.6j 2.5 100 NE NE NE
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
Detections in Water Samples Above MDL (Appendix II Exclusive)
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains Appendix II exclusive constituents (not also listed on Appendix I) detected at or above MDL.
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Maximum Contaminant Level aka Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 7
MNA Parameter Data Summary
September 1, 2016
Parameters Method MDL*Units
MW-1R MW-2 MW-8
09/01/16 09/01/16 09/01/16
VFA – Acetic Acid AM23G NS NS NS NS
AM23G NS NS NS NS
AM23G NS NS NS NS
AM23G NS NS NS NS
AM23G NS NS NS NS
VFA – Lactic Acid AM23G NS NS NS NS
AM23G NS NS NS NS
AM23G NS NS NS NS
AM23G NS NS NS NS
Hydrogen AM20GAX NS NS NS NS
Methane AM20GAX NS NS NS NS
AM20GAX NS NS NS NS
Ethane AM20GAX NS NS NS NS
CO2-Dissolved 0 mg/L NS NS NS
Alkalinity SM 2320B 1000 NS NS NS
Sulfate EPA 300.0 1000 NS NS NS
Sulfide SM 4500-S2D 100 <100 <100 <100
Chloride SM 4500-Cl-E 500 NS NS NS
TOC SM 5310B 500 NS NS NS
COD SM 5220D 12500 NS NS NS
BOD SM 5210B NS NS NS NS
Iron, ferrous SM 3500-Fe B 0.5 NS NS NS
Nitrate EPA 353.2 10 NS NS NS
Temperature Field Instrument 0 Degrees C 17.8 22.1 18.2
ORP Field Instrument -900 283 -51 303
DO Field Instrument 0 5.5 0.6 2.5
pH Field Instrument 0.00 SU 4.7 6.0 4.20
Specific Conductance Field Instrument 0 18 1532 56
Turbidity Field Instrument 1.00 NTU NS NS NS
Notes:
VFA = Volatile Fatty Acids
MDL* = Lowest Method Detection Limit for Lab Parameters or Lowest Field Measurement Possible
>100 = CO2 Concentration Exceeds Maximum capability of Method Used
NS = Not Sampled as not required during this specific event.
ug/L
VFA – Butyric Acid ug/L
VFA – Hexanoic Acid ug/L
VFA – i-Hexanoic Acid ug/L
VFA – i-Pentanoic Acid ug/L
ug/L
VFA – Pentaonic Acid ug/L
VFA – Propionic Acid ug/L
VFA – Pyruvic Acid ug/L
nM
ug/L
Ethene ug/L
ug/L
Field Hach Kit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mV
ug/L
uMhos
Constituents Below Quantization Limit are shown as <MDL value
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 8
September 1, 2016
Linear Velocity
(cm/sec)(%)(ft/ft)(ft/yr)
MW-1R 20 0.034 N47W 21.59 148.05
MW-2 3.00E-04 20 0.016 25 N51W 6.02 128.50
MW-3 6.40E-03 20 0.0099 328 N58W 0.00 134.81
MW-4 9.90E-04 20 0.007 34 N52W 7.48 142.72
MW-5 3.10E-05 20 0.020 3 N46W 3.01 121.77
MW-6 1.60E-04 20 0.006 5 N40W 7.25 138.28
MW-7 7.30E-05 20 0.007 3 N38W 9.28 134.31
MW-8 3.40E-04 20 0.058 102 N19E 18.75 143.13
Minimum 3.10E-05 20 0.006 3 -0.00 121.77
Average 1.18E-03 20 0.020 72 -9.17 136.45
Maximum 6.40E-03 20 0.058 328 -21.59 148.05
NOTE:
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation
(ft btoc)(ft amsl)
na na
Data for conductivities and effective porosity obtained from GAI Consultants' Water Sampling Report (January, 1995).
Hydrologic Gradient from groundwater elevations recorded on September 1, 2016.
Linear Velocity (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e

Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
September 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311078
92311078
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE CLOSED LF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 84
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 2 of 84
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Lab ID Sample ID Matrix Date Collected Date Received
92311078001 MW-1R Water 09/01/16 08:30 09/02/16 08:50
92311078002 MW-2 Water 09/01/16 14:30 09/02/16 08:50
92311078003 MW-4 Water 09/01/16 13:10 09/02/16 08:50
92311078004 MW-6 Water 09/01/16 12:00 09/02/16 08:50
92311078005 MW-8 Water 09/01/16 15:30 09/02/16 08:50
92311078006 MW-11 Water 09/01/16 10:30 09/02/16 08:50
92311078007 MW-3 Water 09/01/16 13:35 09/02/16 08:50
92311078008 MW-5 Water 09/01/16 09:50 09/02/16 08:50
92311078009 MW-7 Water 09/01/16 11:15 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 3 of 84
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311078001 MW-1R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92311078002 MW-2 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92311078003 MW-4 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92311078004 MW-6 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92311078005 MW-8 EPA 8081 21 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 84
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92311078006 MW-11 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 12 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 68 PASI-CGAW
SM 4500-S2D 1 PASI-AMDW
SM 4500-CN-E 1 PASI-ASER
92311078007 MW-3 EPA 6010 15 PASI-ASH1
EPA 8260 68 PASI-CGAW
92311078008 MW-5 EPA 6010 15 PASI-ASH1
EPA 8260 68 PASI-CGAW
92311078009 MW-7 EPA 6010 15 PASI-ASH1
EPA 8260 68 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-1R Lab ID:92311078001 Collected:09/01/16 08:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 19:45 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 19:45 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 19:45 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 19:45 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 19:45 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 19:45 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 19:45 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 19:45 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 19:45 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 19:45 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 19:45 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 19:45 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 19:45 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 19:45 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 19:45 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 19:45 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 19:45 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 19:45 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 19:45 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)71 %09/07/16 19:45 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)63 %09/07/16 19:45 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 16:51 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 16:51 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 16:51 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 16:51 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 16:51 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 16:51 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 16:51 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)62 %09/07/16 16:51 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 13:58 25057-89-009/06/16 09:200.095 0.047 1
2,4-D ND ug/L 09/08/16 13:58 94-75-709/06/16 09:200.94 0.22 1
Dalapon ND ug/L 09/08/16 13:58 75-99-0 L309/06/16 09:200.91 0.43 1
2,4-DB ND ug/L 09/08/16 13:58 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 13:58 1918-00-909/06/16 09:200.094 0.030 1
Dichlorprop ND ug/L 09/08/16 13:58 120-36-509/06/16 09:200.65 0.19 1
Dinoseb ND ug/L 09/08/16 13:58 88-85-709/06/16 09:200.19 0.057 1
Pentachlorophenol ND ug/L 09/08/16 13:58 87-86-509/06/16 09:200.028 0.017 1
Picloram ND ug/L 09/08/16 13:58 1918-02-109/06/16 09:200.095 0.019 1
2,4,5-T ND ug/L 09/08/16 13:58 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 13:58 93-72-109/06/16 09:200.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-1R Lab ID:92311078001 Collected:09/01/16 08:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)88 %09/08/16 13:58 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 22:57 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 5.8J ug/L 09/07/16 22:57 7440-38-209/06/16 21:0010.0 2.5 1
Barium 20.2J ug/L 09/07/16 22:57 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 22:57 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 22:57 7440-43-909/06/16 21:001.0 0.50 1
Chromium 20.1 ug/L 09/07/16 22:57 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 22:57 7440-48-409/06/16 21:0010.0 2.5 1
Copper 3.1J ug/L 09/07/16 22:57 7440-50-809/06/16 21:0010.0 2.5 1
Lead 4.4J ug/L 09/07/16 22:57 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 22:57 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 22:57 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 22:57 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 22:57 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 22:57 7440-31-509/06/16 21:001002.5 1
Vanadium 28.4 ug/L 09/07/16 22:57 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 22:57 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 12:50 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 13:12 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 13:12 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 13:12 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 13:12 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 13:12 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 13:12 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 13:12 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 13:12 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 13:12 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 13:12 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 13:12 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 13:12 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 13:12 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 13:12 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 13:12 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 13:12 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 13:12 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 13:12 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 13:12 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 13:12 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 13:12 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-1R Lab ID:92311078001 Collected:09/01/16 08:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 13:12 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 13:12 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 13:12 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 13:12 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 13:12 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 13:12 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 13:12 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 13:12 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 13:12 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 13:12 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 13:12 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 13:12 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 13:12 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 13:12 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 13:12 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 13:12 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 13:12 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 13:12 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 13:12 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 13:12 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 13:12 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 13:12 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 13:12 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 13:12 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 13:12 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 13:12 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 13:12 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 13:12 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 13:12 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 13:12 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 13:12 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 13:12 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 13:12 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 13:12 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 13:12 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 13:12 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 13:12 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 13:12 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 13:12 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 13:12 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 13:12 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 13:12 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 13:12 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 13:12 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 13:1209/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 13:12 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 8 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-1R Lab ID:92311078001 Collected:09/01/16 08:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 13:12 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 13:12 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 13:12 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 13:12 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 13:12 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 13:12 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 13:12 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 13:12 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 13:12 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 13:12 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 13:12 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 13:12 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 13:12 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 13:12 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 13:12 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 13:12 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 13:12 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 13:12 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 13:12 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 13:12 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 13:12 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 13:12 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 13:12 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 13:12 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 13:12 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 13:1209/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 13:12 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 13:12 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 13:12 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 13:12 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 13:12 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 13:12 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 13:12 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 13:12 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 13:12 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 13:12 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 13:12 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 13:12 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)66 %09/19/16 13:12 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)66 %09/19/16 13:12 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)92 %09/19/16 13:12 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)35 %09/19/16 13:12 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)38 %09/19/16 13:12 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)74 %09/19/16 13:12 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 9 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-1R Lab ID:92311078001 Collected:09/01/16 08:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 04:19 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 04:19 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 04:19 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 04:19 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 04:19 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 04:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 04:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 04:19 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 04:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 04:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 04:19 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 04:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 04:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 04:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 04:19 75-00-310.0 0.54 1
Chloroform 0.60J ug/L 09/08/16 04:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 04:19 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 04:19 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 04:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 04:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 04:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 04:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 04:19 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 04:19 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 04:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 04:19 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 04:19 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 04:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 04:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 04:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 04:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 04:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 04:19 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 04:19 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 04:19 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 04:19 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 04:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 04:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 04:19 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 04:19 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 04:19 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 04:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 04:19 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 04:19 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 04:19 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 04:19 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-1R Lab ID:92311078001 Collected:09/01/16 08:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 04:19 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 04:19 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 04:19 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 04:19 107-12-01503.6 1
Styrene ND ug/L 09/08/16 04:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 04:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 04:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 04:19 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 04:19 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 04:19 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 04:19 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 04:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 04:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 04:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 04:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 04:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 04:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 04:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 04:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %09/08/16 04:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 04:19 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 04:19 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/07/16 00:10 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:34 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-2 Lab ID:92311078002 Collected:09/01/16 14:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 20:03 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 20:03 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 20:03 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 20:03 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 20:03 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 20:03 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 20:03 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 20:03 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 20:03 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 20:03 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 20:03 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 20:03 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 20:03 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 20:03 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 20:03 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 20:03 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 20:03 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 20:03 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 20:03 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)40 %09/07/16 20:03 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)66 %09/07/16 20:03 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 17:11 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 17:11 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 17:11 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 17:11 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 17:11 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 17:11 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 17:11 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)72 %09/07/16 17:11 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 14:28 25057-89-009/06/16 09:200.095 0.047 1
2,4-D ND ug/L 09/08/16 14:28 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 14:28 75-99-0 L309/06/16 09:200.92 0.43 1
2,4-DB ND ug/L 09/08/16 14:28 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 14:28 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 14:28 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 14:28 88-85-709/06/16 09:200.19 0.057 1
Pentachlorophenol ND ug/L 09/08/16 14:28 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 14:28 1918-02-109/06/16 09:200.095 0.019 1
2,4,5-T ND ug/L 09/08/16 14:28 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 14:28 93-72-109/06/16 09:200.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-2 Lab ID:92311078002 Collected:09/01/16 14:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)97 %09/08/16 14:28 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:06 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 43.0 ug/L 09/07/16 23:06 7440-38-209/06/16 21:0010.0 2.5 1
Barium 170 ug/L 09/07/16 23:06 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:06 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:06 7440-43-909/06/16 21:001.0 0.50 1
Chromium 4.1J ug/L 09/07/16 23:06 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:06 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:06 7440-50-809/06/16 21:0010.0 2.5 1
Lead 3.9J ug/L 09/07/16 23:06 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:06 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:06 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:06 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:06 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:06 7440-31-509/06/16 21:001002.5 1
Vanadium 11.0J ug/L 09/07/16 23:06 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:06 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 12:53 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 13:40 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 13:40 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 13:40 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 13:40 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 13:40 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 13:40 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 13:40 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 13:40 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 13:40 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 13:40 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 13:40 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 13:40 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 13:40 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 13:40 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 13:40 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 13:40 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 13:40 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 13:40 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 13:40 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 13:40 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 13:40 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-2 Lab ID:92311078002 Collected:09/01/16 14:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 13:40 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 13:40 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 13:40 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 13:40 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 13:40 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 13:40 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 13:40 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 13:40 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 13:40 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 13:40 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 13:40 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 13:40 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 13:40 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 13:40 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 13:40 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 13:40 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 13:40 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 13:40 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 13:40 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 13:40 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 13:40 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 13:40 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 13:40 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 13:40 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 13:40 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 13:40 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 13:40 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 13:40 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 13:40 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 13:40 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 13:40 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 13:40 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 13:40 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 13:40 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 13:40 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 13:40 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 13:40 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 13:40 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 13:40 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 13:40 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 13:40 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 13:40 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 13:40 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 13:40 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 13:4009/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 13:40 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-2 Lab ID:92311078002 Collected:09/01/16 14:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 13:40 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 13:40 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 13:40 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 13:40 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 13:40 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 13:40 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 13:40 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 13:40 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 13:40 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 13:40 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 13:40 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 13:40 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 13:40 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 13:40 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 13:40 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 13:40 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 13:40 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 13:40 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 13:40 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 13:40 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 13:40 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 13:40 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 13:40 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 13:40 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 13:40 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 13:4009/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 13:40 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 13:40 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 13:40 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 13:40 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 13:40 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 13:40 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 13:40 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 13:40 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 13:40 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 13:40 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 13:40 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 13:40 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)69 %09/19/16 13:40 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)71 %09/19/16 13:40 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)67 %09/19/16 13:40 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)31 %09/19/16 13:40 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)41 %09/19/16 13:40 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)86 %09/19/16 13:40 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-2 Lab ID:92311078002 Collected:09/01/16 14:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 04:36 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 04:36 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 04:36 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 04:36 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 04:36 107-05-110.0 1.5 1
Benzene 0.94J ug/L 09/08/16 04:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 04:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 04:36 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 04:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 04:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 04:36 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 04:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 04:36 56-23-51.0 0.25 1
Chlorobenzene 10.8 ug/L 09/08/16 04:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 04:36 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 04:36 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 04:36 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 04:36 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 04:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 04:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 04:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 04:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 04:36 95-50-15.0 0.30 1
1,3-Dichlorobenzene 0.30J ug/L 09/08/16 04:36 541-73-15.0 0.24 1
1,4-Dichlorobenzene 2.9 ug/L 09/08/16 04:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 04:36 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 04:36 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 04:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 04:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 04:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 04:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 04:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 04:36 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 04:36 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 04:36 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 04:36 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 04:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 04:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 04:36 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 04:36 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 04:36 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 04:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 04:36 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 04:36 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 04:36 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 04:36 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-2 Lab ID:92311078002 Collected:09/01/16 14:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 04:36 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 04:36 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 04:36 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 04:36 107-12-01503.6 1
Styrene ND ug/L 09/08/16 04:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 04:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 04:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 04:36 127-18-41.0 0.46 1
Tetrahydrofuran 4.5J ug/L 09/08/16 04:36 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 04:36 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 04:36 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 04:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 04:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 04:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 04:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 04:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 04:36 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 04:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 04:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %09/08/16 04:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 04:36 17060-07-070-130 1
Toluene-d8 (S)102 %09/08/16 04:36 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/07/16 00:10 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.3J ug/L 09/13/16 03:35 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-4 Lab ID:92311078003 Collected:09/01/16 13:10 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 20:20 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 20:20 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 20:20 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 20:20 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 20:20 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 20:20 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 20:20 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 20:20 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 20:20 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 20:20 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 20:20 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 20:20 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 20:20 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 20:20 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 20:20 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 20:20 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 20:20 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 20:20 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 20:20 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)40 %09/07/16 20:20 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)54 %09/07/16 20:20 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 17:31 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 17:31 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 17:31 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 17:31 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 17:31 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 17:31 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 17:31 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)58 %09/07/16 17:31 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 14:58 25057-89-009/06/16 09:200.096 0.048 1
2,4-D ND ug/L 09/08/16 14:58 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 14:58 75-99-0 L309/06/16 09:200.92 0.44 1
2,4-DB ND ug/L 09/08/16 14:58 94-82-609/06/16 09:201.9 0.52 1
Dicamba ND ug/L 09/08/16 14:58 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 14:58 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 14:58 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 14:58 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 14:58 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 14:58 93-76-509/06/16 09:200.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 14:58 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 18 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-4 Lab ID:92311078003 Collected:09/01/16 13:10 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)83 %09/08/16 14:58 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:09 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:09 7440-38-209/06/16 21:0010.0 2.5 1
Barium 55.3J ug/L 09/07/16 23:09 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:09 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:09 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:09 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:09 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:09 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:09 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:09 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:09 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:09 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:09 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:09 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:09 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:09 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:00 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 14:09 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 14:09 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 14:09 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 14:09 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 14:09 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 14:09 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 14:09 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 14:09 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 14:09 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 14:09 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 14:09 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 14:09 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 14:09 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 14:09 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 14:09 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 14:09 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 14:09 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 14:09 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 14:09 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 14:09 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 14:09 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-4 Lab ID:92311078003 Collected:09/01/16 13:10 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 14:09 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 14:09 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 14:09 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 14:09 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 14:09 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 14:09 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 14:09 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 14:09 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 14:09 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 14:09 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 14:09 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 14:09 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 14:09 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 14:09 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 14:09 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 14:09 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 14:09 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 14:09 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 14:09 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 14:09 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 14:09 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 14:09 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 14:09 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 14:09 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 14:09 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 14:09 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 14:09 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 14:09 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 14:09 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 14:09 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 14:09 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 14:09 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 14:09 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 14:09 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 14:09 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 14:09 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 14:09 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 14:09 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 14:09 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 14:09 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 14:09 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 14:09 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 14:09 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 14:09 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 14:0909/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 14:09 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-4 Lab ID:92311078003 Collected:09/01/16 13:10 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 14:09 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 14:09 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 14:09 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 14:09 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 14:09 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 14:09 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 14:09 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 14:09 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 14:09 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 14:09 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 14:09 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 14:09 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 14:09 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 14:09 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 14:09 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 14:09 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 14:09 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 14:09 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 14:09 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 14:09 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 14:09 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 14:09 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 14:09 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 14:09 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 14:09 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 14:0909/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 14:09 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 14:09 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 14:09 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 14:09 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 14:09 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 14:09 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 14:09 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 14:09 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 14:09 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 14:09 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 14:09 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 14:09 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)14 %09/19/16 14:09 4165-60-0 S009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)36 %09/19/16 14:09 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)68 %09/19/16 14:09 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)11 %09/19/16 14:09 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)8 %09/19/16 14:09 367-12-4 S009/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)71 %09/19/16 14:09 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-4 Lab ID:92311078003 Collected:09/01/16 13:10 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 04:53 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 04:53 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 04:53 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 04:53 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 04:53 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 04:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 04:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 04:53 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 04:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 04:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 04:53 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 04:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 04:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 04:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 04:53 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 04:53 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 04:53 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 04:53 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 04:53 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 04:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 04:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 04:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 04:53 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 04:53 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 04:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 04:53 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 04:53 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 04:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 04:53 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 04:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 04:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 04:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 04:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 04:53 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 04:53 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 04:53 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 04:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 04:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 04:53 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 04:53 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 04:53 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 04:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 04:53 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 04:53 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 04:53 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 04:53 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-4 Lab ID:92311078003 Collected:09/01/16 13:10 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 04:53 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 04:53 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 04:53 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 04:53 107-12-01503.6 1
Styrene ND ug/L 09/08/16 04:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 04:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 04:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 04:53 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 04:53 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 04:53 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 04:53 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 04:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 04:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 04:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 04:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 04:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 04:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 04:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 04:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %09/08/16 04:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 04:53 17060-07-070-130 1
Toluene-d8 (S)101 %09/08/16 04:53 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/07/16 00:10 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:36 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-6 Lab ID:92311078004 Collected:09/01/16 12:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 20:38 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 20:38 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 20:38 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 20:38 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 20:38 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 20:38 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 20:38 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 20:38 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 20:38 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 20:38 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 20:38 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 20:38 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 20:38 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 20:38 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 20:38 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 20:38 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 20:38 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 20:38 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 20:38 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)51 %09/07/16 20:38 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)55 %09/07/16 20:38 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 17:51 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 17:51 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 17:51 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 17:51 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 17:51 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 17:51 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 17:51 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)57 %09/07/16 17:51 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 15:28 25057-89-009/06/16 09:200.096 0.048 1
2,4-D ND ug/L 09/08/16 15:28 94-75-709/06/16 09:200.96 0.23 1
Dalapon ND ug/L 09/08/16 15:28 75-99-0 L309/06/16 09:200.93 0.44 1
2,4-DB ND ug/L 09/08/16 15:28 94-82-609/06/16 09:201.9 0.52 1
Dicamba ND ug/L 09/08/16 15:28 1918-00-909/06/16 09:200.096 0.030 1
Dichlorprop ND ug/L 09/08/16 15:28 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 15:28 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 15:28 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 15:28 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 15:28 93-76-509/06/16 09:200.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 15:28 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-6 Lab ID:92311078004 Collected:09/01/16 12:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)95 %09/08/16 15:28 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:12 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 4.5J ug/L 09/07/16 23:12 7440-38-209/06/16 21:0010.0 2.5 1
Barium 130 ug/L 09/07/16 23:12 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:12 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:12 7440-43-909/06/16 21:001.0 0.50 1
Chromium 2.7J ug/L 09/07/16 23:12 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:12 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:12 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:12 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:12 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:12 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:12 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:12 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:12 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:12 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:12 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:02 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 14:37 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 14:37 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 14:37 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 14:37 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 14:37 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 14:37 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 14:37 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 14:37 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 14:37 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 14:37 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 14:37 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 14:37 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 14:37 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 14:37 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 14:37 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 14:37 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 14:37 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 14:37 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 14:37 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 14:37 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 14:37 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-6 Lab ID:92311078004 Collected:09/01/16 12:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 14:37 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 14:37 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 14:37 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 14:37 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 14:37 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 14:37 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 14:37 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 14:37 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 14:37 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 14:37 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 14:37 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 14:37 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 14:37 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 14:37 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 14:37 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 14:37 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 14:37 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 14:37 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 14:37 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 14:37 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 14:37 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 14:37 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 14:37 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 14:37 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 14:37 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 14:37 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 14:37 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 14:37 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 14:37 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 14:37 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 14:37 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 14:37 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 14:37 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 14:37 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 14:37 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 14:37 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 14:37 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 14:37 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 14:37 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 14:37 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 14:37 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 14:37 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 14:37 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 14:37 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 14:3709/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 14:37 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-6 Lab ID:92311078004 Collected:09/01/16 12:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 14:37 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 14:37 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 14:37 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 14:37 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 14:37 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 14:37 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 14:37 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 14:37 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 14:37 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 14:37 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 14:37 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 14:37 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 14:37 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 14:37 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 14:37 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 14:37 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 14:37 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 14:37 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 14:37 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 14:37 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 14:37 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 14:37 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 14:37 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 14:37 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 14:37 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 14:3709/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 14:37 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 14:37 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 14:37 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 14:37 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 14:37 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 14:37 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 14:37 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 14:37 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 14:37 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 14:37 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 14:37 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 14:37 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)79 %09/19/16 14:37 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)82 %09/19/16 14:37 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)71 %09/19/16 14:37 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)33 %09/19/16 14:37 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)45 %09/19/16 14:37 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)92 %09/19/16 14:37 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
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Page 27 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-6 Lab ID:92311078004 Collected:09/01/16 12:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 05:11 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 05:11 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 05:11 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 05:11 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 05:11 107-05-110.0 1.5 1
Benzene 0.36J ug/L 09/08/16 05:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 05:11 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 05:11 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 05:11 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 05:11 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 05:11 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 05:11 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 05:11 56-23-51.0 0.25 1
Chlorobenzene 1.5J ug/L 09/08/16 05:11 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 05:11 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 05:11 67-66-35.0 0.14 1
Chloromethane 0.18J ug/L 09/08/16 05:11 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 05:11 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 05:11 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 05:11 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 05:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 05:11 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.53J ug/L 09/08/16 05:11 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 05:11 541-73-15.0 0.24 1
1,4-Dichlorobenzene 0.71J ug/L 09/08/16 05:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 05:11 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 05:11 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 05:11 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 05:11 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 05:11 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.42J ug/L 09/08/16 05:11 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 05:11 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 05:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 05:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 05:11 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 05:11 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 05:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 05:11 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 05:11 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 05:11 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 05:11 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 05:11 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 05:11 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 05:11 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 05:11 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 05:11 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-6 Lab ID:92311078004 Collected:09/01/16 12:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 05:11 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 05:11 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 05:11 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 05:11 107-12-01503.6 1
Styrene ND ug/L 09/08/16 05:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 05:11 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 05:11 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 05:11 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 05:11 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 05:11 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 05:11 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 05:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 05:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 05:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 05:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 05:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 05:11 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 05:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 05:11 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %09/08/16 05:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 05:11 17060-07-070-130 1
Toluene-d8 (S)103 %09/08/16 05:11 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/07/16 00:10 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 09/13/16 03:36 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-8 Lab ID:92311078005 Collected:09/01/16 15:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 20:56 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 20:56 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 20:56 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 20:56 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 20:56 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 20:56 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 20:56 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 20:56 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 20:56 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 20:56 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 20:56 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 20:56 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 20:56 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 20:56 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 20:56 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 20:56 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 20:56 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 20:56 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 20:56 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)52 %09/07/16 20:56 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)48 %09/07/16 20:56 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 18:11 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 18:11 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 18:11 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 18:11 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 18:11 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 18:11 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 18:11 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)48 %09/07/16 18:11 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 15:58 25057-89-009/06/16 09:200.095 0.047 1
2,4-D ND ug/L 09/08/16 15:58 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 15:58 75-99-0 L309/06/16 09:200.92 0.43 1
2,4-DB ND ug/L 09/08/16 15:58 94-82-609/06/16 09:201.9 0.51 1
Dicamba ND ug/L 09/08/16 15:58 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 15:58 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 15:58 88-85-709/06/16 09:200.19 0.057 1
Pentachlorophenol ND ug/L 09/08/16 15:58 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 15:58 1918-02-109/06/16 09:200.095 0.019 1
2,4,5-T ND ug/L 09/08/16 15:58 93-76-509/06/16 09:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 15:58 93-72-109/06/16 09:200.19 0.049 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-8 Lab ID:92311078005 Collected:09/01/16 15:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)75 %09/08/16 15:58 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:16 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:16 7440-38-209/06/16 21:0010.0 2.5 1
Barium 54.8J ug/L 09/07/16 23:16 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:16 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:16 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:16 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:16 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:16 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:16 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:16 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:16 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:16 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:16 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:16 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:16 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:16 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:04 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 15:05 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 15:05 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 15:05 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 15:05 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 15:05 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 15:05 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 15:05 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 15:05 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 15:05 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 15:05 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 15:05 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 15:05 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 15:05 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 15:05 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 15:05 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 15:05 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 15:05 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 15:05 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 15:05 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 15:05 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 15:05 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-8 Lab ID:92311078005 Collected:09/01/16 15:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 15:05 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 15:05 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 15:05 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 15:05 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 15:05 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 15:05 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 15:05 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 15:05 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 15:05 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 15:05 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 15:05 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 15:05 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 15:05 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 15:05 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 15:05 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 15:05 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 15:05 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 15:05 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 15:05 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 15:05 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 15:05 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 15:05 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 15:05 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 15:05 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 15:05 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 15:05 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 15:05 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 15:05 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 15:05 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 15:05 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 15:05 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 15:05 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 15:05 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 15:05 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 15:05 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 15:05 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 15:05 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 15:05 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 15:05 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 15:05 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 15:05 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 15:05 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 15:05 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 15:05 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 15:0509/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 15:05 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 32 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-8 Lab ID:92311078005 Collected:09/01/16 15:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 15:05 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 15:05 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 15:05 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 15:05 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 15:05 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 15:05 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 15:05 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 15:05 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 15:05 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 15:05 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 15:05 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 15:05 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 15:05 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 15:05 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 15:05 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 15:05 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 15:05 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 15:05 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 15:05 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 15:05 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 15:05 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 15:05 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 15:05 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 15:05 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 15:05 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 15:0509/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 15:05 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 15:05 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 15:05 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 15:05 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 15:05 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 15:05 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 15:05 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 15:05 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 15:05 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 15:05 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 15:05 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 15:05 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)82 %09/19/16 15:05 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)83 %09/19/16 15:05 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)86 %09/19/16 15:05 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)37 %09/19/16 15:05 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)47 %09/19/16 15:05 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)95 %09/19/16 15:05 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-8 Lab ID:92311078005 Collected:09/01/16 15:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 05:28 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 05:28 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 05:28 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 05:28 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 05:28 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 05:28 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 05:28 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 05:28 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 05:28 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 05:28 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 05:28 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 05:28 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 05:28 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 05:28 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 05:28 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 05:28 67-66-35.0 0.14 1
Chloromethane 0.32J ug/L 09/08/16 05:28 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 05:28 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 05:28 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 05:28 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 05:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 05:28 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 05:28 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 05:28 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 05:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 05:28 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 05:28 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 05:28 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 05:28 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 05:28 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 05:28 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 05:28 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 05:28 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 05:28 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 05:28 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 05:28 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 05:28 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 05:28 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 05:28 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 05:28 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 05:28 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 05:28 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 05:28 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 05:28 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 05:28 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 05:28 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-8 Lab ID:92311078005 Collected:09/01/16 15:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 05:28 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 05:28 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 05:28 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 05:28 107-12-01503.6 1
Styrene ND ug/L 09/08/16 05:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 05:28 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 05:28 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 05:28 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 05:28 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 05:28 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 05:28 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 05:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 05:28 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 05:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 05:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 05:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 05:28 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 05:28 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 05:28 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 05:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 05:28 17060-07-070-130 1
Toluene-d8 (S)103 %09/08/16 05:28 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/07/16 00:10 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.3J ug/L 09/13/16 03:39 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-11 Lab ID:92311078006 Collected:09/01/16 10:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 09/07/16 21:13 309-00-209/07/16 09:200.050 0.050 1
alpha-BHC ND ug/L 09/07/16 21:13 319-84-609/07/16 09:200.050 0.050 1
beta-BHC ND ug/L 09/07/16 21:13 319-85-709/07/16 09:200.050 0.050 1
delta-BHC ND ug/L 09/07/16 21:13 319-86-809/07/16 09:200.050 0.050 1
gamma-BHC (Lindane)ND ug/L 09/07/16 21:13 58-89-909/07/16 09:200.050 0.050 1
Chlordane (Technical)ND ug/L 09/07/16 21:13 57-74-909/07/16 09:200.50 0.20 1
4,4'-DDD ND ug/L 09/07/16 21:13 72-54-809/07/16 09:200.10 0.050 1
4,4'-DDE ND ug/L 09/07/16 21:13 72-55-909/07/16 09:200.10 0.050 1
4,4'-DDT ND ug/L 09/07/16 21:13 50-29-309/07/16 09:200.10 0.050 1
Dieldrin ND ug/L 09/07/16 21:13 60-57-109/07/16 09:200.075 0.050 1
Endosulfan I ND ug/L 09/07/16 21:13 959-98-809/07/16 09:200.10 0.050 1
Endosulfan II ND ug/L 09/07/16 21:13 33213-65-909/07/16 09:200.10 0.050 1
Endosulfan sulfate ND ug/L 09/07/16 21:13 1031-07-809/07/16 09:200.10 0.050 1
Endrin ND ug/L 09/07/16 21:13 72-20-809/07/16 09:200.10 0.050 1
Endrin aldehyde ND ug/L 09/07/16 21:13 7421-93-409/07/16 09:200.10 0.050 1
Heptachlor ND ug/L 09/07/16 21:13 76-44-809/07/16 09:200.050 0.050 1
Heptachlor epoxide ND ug/L 09/07/16 21:13 1024-57-309/07/16 09:200.075 0.050 1
Methoxychlor ND ug/L 09/07/16 21:13 72-43-509/07/16 09:201.0 0.15 1
Toxaphene ND ug/L 09/07/16 21:13 8001-35-209/07/16 09:201.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)48 %09/07/16 21:13 877-09-809/07/16 09:2020-130 1
Decachlorobiphenyl (S)54 %09/07/16 21:13 2051-24-309/07/16 09:2020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 09/07/16 18:30 12674-11-209/07/16 09:200.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 09/07/16 18:30 11104-28-209/07/16 09:200.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 09/07/16 18:30 11141-16-509/07/16 09:200.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 09/07/16 18:30 53469-21-909/07/16 09:200.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 09/07/16 18:30 12672-29-609/07/16 09:200.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 09/07/16 18:30 11097-69-109/07/16 09:200.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 09/07/16 18:30 11096-82-509/07/16 09:200.50 0.50 1
Surrogates
Decachlorobiphenyl (S)54 %09/07/16 18:30 2051-24-309/07/16 09:2010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Bentazon ND ug/L 09/08/16 16:28 25057-89-009/06/16 09:200.096 0.048 1
2,4-D ND ug/L 09/08/16 16:28 94-75-709/06/16 09:200.95 0.23 1
Dalapon ND ug/L 09/08/16 16:28 75-99-0 L309/06/16 09:200.92 0.44 1
2,4-DB ND ug/L 09/08/16 16:28 94-82-609/06/16 09:201.9 0.52 1
Dicamba ND ug/L 09/08/16 16:28 1918-00-909/06/16 09:200.095 0.030 1
Dichlorprop ND ug/L 09/08/16 16:28 120-36-509/06/16 09:200.66 0.19 1
Dinoseb ND ug/L 09/08/16 16:28 88-85-709/06/16 09:200.19 0.058 1
Pentachlorophenol ND ug/L 09/08/16 16:28 87-86-509/06/16 09:200.029 0.017 1
Picloram ND ug/L 09/08/16 16:28 1918-02-109/06/16 09:200.096 0.019 1
2,4,5-T ND ug/L 09/08/16 16:28 93-76-509/06/16 09:200.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 09/08/16 16:28 93-72-109/06/16 09:200.19 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-11 Lab ID:92311078006 Collected:09/01/16 10:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
Surrogates
2,4-DCAA (S)86 %09/08/16 16:28 19719-28-909/06/16 09:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:28 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 10.4 ug/L 09/07/16 23:28 7440-38-209/06/16 21:0010.0 2.5 1
Barium 200 ug/L 09/07/16 23:28 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:28 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:28 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:28 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt 4.7J ug/L 09/07/16 23:28 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:28 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:28 7439-92-109/06/16 21:0010.0 2.5 1
Nickel 5.2J ug/L 09/07/16 23:28 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:28 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:28 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:28 7440-28-009/06/16 21:005.5 5.0 1
Tin ND ug/L 09/07/16 23:28 7440-31-509/06/16 21:001002.5 1
Vanadium ND ug/L 09/07/16 23:28 7440-62-209/06/16 21:0025.0 2.5 1
Zinc 7.9J ug/L 09/07/16 23:28 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/08/16 13:07 7439-97-609/03/16 06:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 09/19/16 15:33 83-32-909/06/16 13:4010.0 0.25 1
Acenaphthylene ND ug/L 09/19/16 15:33 208-96-809/06/16 13:4010.0 0.21 1
Acetophenone ND ug/L 09/19/16 15:33 98-86-209/06/16 13:4010.0 2.0 1
2-Acetylaminofluorene ND ug/L 09/19/16 15:33 53-96-309/06/16 13:4020.0 0.84 1
4-Aminobiphenyl ND ug/L 09/19/16 15:33 92-67-109/06/16 13:4020.0 0.92 1
Anthracene ND ug/L 09/19/16 15:33 120-12-709/06/16 13:4010.0 0.14 1
Benzo(a)anthracene ND ug/L 09/19/16 15:33 56-55-309/06/16 13:4010.0 0.33 1
Benzo(a)pyrene ND ug/L 09/19/16 15:33 50-32-809/06/16 13:4010.0 0.30 1
Benzo(b)fluoranthene ND ug/L 09/19/16 15:33 205-99-209/06/16 13:4010.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 09/19/16 15:33 191-24-209/06/16 13:4010.0 0.38 1
Benzo(k)fluoranthene ND ug/L 09/19/16 15:33 207-08-909/06/16 13:4010.0 0.43 1
Benzyl alcohol ND ug/L 09/19/16 15:33 100-51-609/06/16 13:4020.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 09/19/16 15:33 101-55-309/06/16 13:4010.0 1.3 1
Butylbenzylphthalate ND ug/L 09/19/16 15:33 85-68-709/06/16 13:4010.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 09/19/16 15:33 59-50-709/06/16 13:4020.0 4.2 1
4-Chloroaniline ND ug/L 09/19/16 15:33 106-47-809/06/16 13:4020.0 3.4 1
Chlorobenzilate ND ug/L 09/19/16 15:33 510-15-609/06/16 13:4010.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 09/19/16 15:33 111-91-109/06/16 13:4010.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 09/19/16 15:33 111-44-409/06/16 13:4010.0 1.5 1
2-Chloronaphthalene ND ug/L 09/19/16 15:33 91-58-709/06/16 13:4010.0 2.2 1
2-Chlorophenol ND ug/L 09/19/16 15:33 95-57-809/06/16 13:4010.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-11 Lab ID:92311078006 Collected:09/01/16 10:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Chlorophenylphenyl ether ND ug/L 09/19/16 15:33 7005-72-309/06/16 13:4010.0 2.1 1
Chrysene ND ug/L 09/19/16 15:33 218-01-909/06/16 13:4010.0 0.21 1
Diallate ND ug/L 09/19/16 15:33 2303-16-409/06/16 13:4010.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 09/19/16 15:33 53-70-309/06/16 13:4010.0 0.55 1
Dibenzofuran ND ug/L 09/19/16 15:33 132-64-909/06/16 13:4010.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 09/19/16 15:33 91-94-109/06/16 13:4020.0 1.4 1
2,4-Dichlorophenol ND ug/L 09/19/16 15:33 120-83-209/06/16 13:4010.0 1.7 1
2,6-Dichlorophenol ND ug/L 09/19/16 15:33 87-65-009/06/16 13:4010.0 1.8 1
Diethylphthalate ND ug/L 09/19/16 15:33 84-66-209/06/16 13:4060001.3 1
Dimethoate ND ug/L 09/19/16 15:33 60-51-509/06/16 13:4020.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 09/19/16 15:33 60-11-709/06/16 13:4010.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 09/19/16 15:33 57-97-609/06/16 13:4010.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 09/19/16 15:33 119-93-709/06/16 13:4010.0 2.1 1
2,4-Dimethylphenol ND ug/L 09/19/16 15:33 105-67-909/06/16 13:4010.0 2.2 1
Dimethylphthalate ND ug/L 09/19/16 15:33 131-11-309/06/16 13:4010.0 1.5 1
Di-n-butylphthalate ND ug/L 09/19/16 15:33 84-74-209/06/16 13:4010.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 09/19/16 15:33 534-52-109/06/16 13:4050.0 1.7 1
1,3-Dinitrobenzene ND ug/L 09/19/16 15:33 99-65-009/06/16 13:4020.0 1.5 1
2,4-Dinitrophenol ND ug/L 09/19/16 15:33 51-28-509/06/16 13:4050.0 6.5 1
2,4-Dinitrotoluene ND ug/L 09/19/16 15:33 121-14-209/06/16 13:4010.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/19/16 15:33 606-20-209/06/16 13:4010.0 1.7 1
Di-n-octylphthalate ND ug/L 09/19/16 15:33 117-84-009/06/16 13:4010.0 0.86 1
Diphenylamine ND ug/L 09/19/16 15:33 122-39-409/06/16 13:4010.0 1.3 1
Disulfoton ND ug/L 09/19/16 15:33 298-04-409/06/16 13:4010.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/19/16 15:33 117-81-709/06/16 13:4015.0 0.85 1
Ethyl methanesulfonate ND ug/L 09/19/16 15:33 62-50-009/06/16 13:4020.0 1.8 1
Famphur ND ug/L 09/19/16 15:33 52-85-709/06/16 13:4020.0 1.7 1
Fluoranthene ND ug/L 09/19/16 15:33 206-44-009/06/16 13:4010.0 0.21 1
Fluorene ND ug/L 09/19/16 15:33 86-73-709/06/16 13:4010.0 0.21 1
Hexachlorobenzene ND ug/L 09/19/16 15:33 118-74-109/06/16 13:4010.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 09/19/16 15:33 77-47-409/06/16 13:4010.0 1.8 1
Hexachloroethane ND ug/L 09/19/16 15:33 67-72-109/06/16 13:4010.0 1.5 1
Hexachloropropene ND ug/L 09/19/16 15:33 1888-71-709/06/16 13:4010.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/19/16 15:33 193-39-509/06/16 13:4010.0 0.29 1
Isodrin ND ug/L 09/19/16 15:33 465-73-609/06/16 13:4020.0 2.0 1
Isophorone ND ug/L 09/19/16 15:33 78-59-109/06/16 13:4010.0 1.8 1
Isosafrole ND ug/L 09/19/16 15:33 120-58-109/06/16 13:4010.0 1.8 1
Kepone ND ug/L 09/19/16 15:33 143-50-009/06/16 13:4020.0 3.1 1
Methapyrilene ND ug/L 09/19/16 15:33 91-80-509/06/16 13:401002.7 1
3-Methylcholanthrene ND ug/L 09/19/16 15:33 56-49-509/06/16 13:4010.0 0.82 1
Methyl methanesulfonate ND ug/L 09/19/16 15:33 66-27-309/06/16 13:4010.0 1.3 1
2-Methylnaphthalene ND ug/L 09/19/16 15:33 91-57-609/06/16 13:4010.0 0.28 1
Methyl parathion ND ug/L 09/19/16 15:33 298-00-009/06/16 13:4010.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 09/19/16 15:33 95-48-709/06/16 13:4010.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/19/16 15:3309/06/16 13:4010.0 1.7 1
1-Naphthalenamine ND ug/L 09/19/16 15:33 134-32-709/06/16 13:4010.0 0.96 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-11 Lab ID:92311078006 Collected:09/01/16 10:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Naphthalenamine ND ug/L 09/19/16 15:33 91-59-809/06/16 13:4010.0 0.98 1
1,4-Naphthoquinone ND ug/L 09/19/16 15:33 130-15-409/06/16 13:4010.0 1.8 1
2-Nitroaniline ND ug/L 09/19/16 15:33 88-74-409/06/16 13:4050.0 2.8 1
3-Nitroaniline ND ug/L 09/19/16 15:33 99-09-209/06/16 13:4050.0 2.4 1
4-Nitroaniline ND ug/L 09/19/16 15:33 100-01-609/06/16 13:4020.0 2.5 1
Nitrobenzene ND ug/L 09/19/16 15:33 98-95-309/06/16 13:4010.0 1.7 1
2-Nitrophenol ND ug/L 09/19/16 15:33 88-75-509/06/16 13:4010.0 1.7 1
4-Nitrophenol ND ug/L 09/19/16 15:33 100-02-709/06/16 13:4050.0 5.8 1
5-Nitro-o-toluidine ND ug/L 09/19/16 15:33 99-55-809/06/16 13:4010.0 1.2 1
N-Nitrosodiethylamine ND ug/L 09/19/16 15:33 55-18-509/06/16 13:4020.0 1.8 1
N-Nitrosodimethylamine ND ug/L 09/19/16 15:33 62-75-909/06/16 13:4010.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 09/19/16 15:33 924-16-309/06/16 13:4010.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/19/16 15:33 621-64-709/06/16 13:4010.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 09/19/16 15:33 86-30-609/06/16 13:4010.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 09/19/16 15:33 10595-95-609/06/16 13:4010.0 1.8 1
N-Nitrosopiperidine ND ug/L 09/19/16 15:33 100-75-409/06/16 13:4020.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 09/19/16 15:33 930-55-2 L309/06/16 13:4010.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 09/19/16 15:33 126-68-109/06/16 13:4010.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/19/16 15:33 108-60-109/06/16 13:4010.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 09/19/16 15:33 56-38-209/06/16 13:4010.0 1.1 1
Pentachlorobenzene ND ug/L 09/19/16 15:33 608-93-509/06/16 13:4010.0 2.0 1
Pentachloronitrobenzene ND ug/L 09/19/16 15:33 82-68-809/06/16 13:4020.0 1.0 1
Pentachlorophenol ND ug/L 09/19/16 15:33 87-86-509/06/16 13:4025.0 2.3 1
Phenacetin ND ug/L 09/19/16 15:33 62-44-209/06/16 13:4020.0 0.97 1
Phenanthrene ND ug/L 09/19/16 15:33 85-01-809/06/16 13:4010.0 0.22 1
Phenol ND ug/L 09/19/16 15:3309/06/16 13:4010.0 1.7 1
p-Phenylenediamine ND ug/L 09/19/16 15:33 106-50-309/06/16 13:4010.0 0.96 1
Phorate ND ug/L 09/19/16 15:33 298-02-209/06/16 13:4010.0 1.1 1
Pronamide ND ug/L 09/19/16 15:33 23950-58-509/06/16 13:4010.0 0.97 1
Pyrene ND ug/L 09/19/16 15:33 129-00-009/06/16 13:4010.0 0.19 1
Safrole ND ug/L 09/19/16 15:33 94-59-709/06/16 13:4010.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 09/19/16 15:33 95-94-309/06/16 13:4010.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 09/19/16 15:33 58-90-209/06/16 13:4010.0 2.3 1
Thionazin ND ug/L 09/19/16 15:33 297-97-209/06/16 13:4020.0 1.2 1
O-Toluidine ND ug/L 09/19/16 15:33 95-53-4 L309/06/16 13:4010.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 09/19/16 15:33 95-95-409/06/16 13:4010.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 09/19/16 15:33 88-06-209/06/16 13:4010.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 09/19/16 15:33 99-35-409/06/16 13:4010.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)79 %09/19/16 15:33 4165-60-009/06/16 13:4021-110 1
2-Fluorobiphenyl (S)82 %09/19/16 15:33 321-60-809/06/16 13:4027-110 1
Terphenyl-d14 (S)91 %09/19/16 15:33 1718-51-009/06/16 13:4031-107 1
Phenol-d6 (S)32 %09/19/16 15:33 13127-88-309/06/16 13:4010-110 1
2-Fluorophenol (S)45 %09/19/16 15:33 367-12-409/06/16 13:4012-110 1
2,4,6-Tribromophenol (S)91 %09/19/16 15:33 118-79-609/06/16 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-11 Lab ID:92311078006 Collected:09/01/16 10:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 05:45 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 05:45 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 05:45 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 05:45 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 05:45 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 05:45 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 05:45 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 05:45 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 05:45 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 05:45 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 05:45 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 05:45 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 05:45 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 05:45 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 05:45 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 05:45 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 05:45 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 05:45 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 05:45 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 05:45 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 05:45 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 05:45 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 05:45 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 05:45 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 05:45 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 05:45 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 05:45 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 05:45 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 05:45 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 05:45 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.34J ug/L 09/08/16 05:45 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 05:45 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 05:45 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 05:45 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 05:45 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 05:45 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 05:45 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 05:45 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 05:45 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 05:45 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 05:45 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 05:45 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 05:45 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 05:45 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 05:45 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 05:45 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-11 Lab ID:92311078006 Collected:09/01/16 10:30 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 05:45 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 05:45 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 05:45 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 05:45 107-12-01503.6 1
Styrene ND ug/L 09/08/16 05:45 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 05:45 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 05:45 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 05:45 127-18-41.0 0.46 1
Tetrahydrofuran 4.0J ug/L 09/08/16 05:45 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 05:45 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 05:45 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 05:45 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 05:45 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 05:45 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 05:45 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 05:45 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 05:45 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 05:45 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 05:45 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 05:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 05:45 17060-07-070-130 1
Toluene-d8 (S)103 %09/08/16 05:45 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 09/07/16 00:10 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.2J ug/L 09/13/16 03:43 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-3 Lab ID:92311078007 Collected:09/01/16 13:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:31 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 5.8J ug/L 09/07/16 23:31 7440-38-209/06/16 21:0010.0 2.5 1
Barium 18.8J ug/L 09/07/16 23:31 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:31 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:31 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:31 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:31 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:31 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:31 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:31 7440-02-009/06/16 21:0050.0 2.5 1
Selenium 5.0J ug/L 09/07/16 23:31 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:31 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:31 7440-28-009/06/16 21:005.5 5.0 1
Vanadium 17.6J ug/L 09/07/16 23:31 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:31 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 06:02 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 06:02 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 06:02 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 06:02 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 06:02 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 06:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 06:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 06:02 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 06:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 06:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 06:02 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 06:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 06:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 06:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 06:02 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 06:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 06:02 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 06:02 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 06:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 06:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 06:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 06:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 06:02 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 06:02 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 06:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 06:02 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 06:02 75-71-8 M15.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 06:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 06:02 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-3 Lab ID:92311078007 Collected:09/01/16 13:35 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 09/08/16 06:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 06:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 06:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 06:02 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 06:02 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 06:02 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 06:02 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 06:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 06:02 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 06:02 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 06:02 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 06:02 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 06:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 06:02 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 06:02 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 06:02 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 06:02 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 06:02 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 06:02 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 06:02 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 06:02 107-12-01503.6 1
Styrene ND ug/L 09/08/16 06:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 06:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 06:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 06:02 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 06:02 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 06:02 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 06:02 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 06:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 06:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 06:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 06:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 06:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 06:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 06:02 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 06:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %09/08/16 06:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/08/16 06:02 17060-07-070-130 1
Toluene-d8 (S)106 %09/08/16 06:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-5 Lab ID:92311078008 Collected:09/01/16 09:50 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:38 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:38 7440-38-209/06/16 21:0010.0 2.5 1
Barium 48.5J ug/L 09/07/16 23:38 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:38 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:38 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:38 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:38 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:38 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:38 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:38 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:38 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:38 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:38 7440-28-009/06/16 21:005.5 5.0 1
Vanadium 3.4J ug/L 09/07/16 23:38 7440-62-209/06/16 21:0025.0 2.5 1
Zinc 10.7 ug/L 09/07/16 23:38 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 07:28 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 07:28 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 07:28 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 07:28 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 07:28 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 07:28 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 07:28 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 07:28 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 07:28 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 07:28 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 07:28 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 07:28 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 07:28 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 07:28 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 07:28 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 07:28 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 07:28 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 07:28 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 07:28 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 07:28 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 07:28 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 07:28 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 07:28 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 07:28 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 07:28 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 07:28 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 07:28 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 07:28 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 07:28 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-5 Lab ID:92311078008 Collected:09/01/16 09:50 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 09/08/16 07:28 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 07:28 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 07:28 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 07:28 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 07:28 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 07:28 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 07:28 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 07:28 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 07:28 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 07:28 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 07:28 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 07:28 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 07:28 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 07:28 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 07:28 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 07:28 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 07:28 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 07:28 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 07:28 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 07:28 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 07:28 107-12-01503.6 1
Styrene ND ug/L 09/08/16 07:28 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 07:28 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 07:28 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 07:28 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 07:28 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 07:28 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 07:28 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 07:28 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 07:28 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 07:28 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 07:28 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 07:28 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 07:28 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 07:28 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 07:28 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 07:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/08/16 07:28 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 07:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-7 Lab ID:92311078009 Collected:09/01/16 11:15 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:44 7440-36-009/06/16 21:006.0 3.8 1
Arsenic 4.5J ug/L 09/07/16 23:44 7440-38-209/06/16 21:0010.0 2.5 1
Barium 34.3J ug/L 09/07/16 23:44 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:44 7440-41-709/06/16 21:001.0 0.50 1
Cadmium 1.5 ug/L 09/07/16 23:44 7440-43-909/06/16 21:001.0 0.50 1
Chromium ND ug/L 09/07/16 23:44 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:44 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:44 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:44 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:44 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:44 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:44 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:44 7440-28-009/06/16 21:005.5 5.0 1
Vanadium ND ug/L 09/07/16 23:44 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:44 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 07:46 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 07:46 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 07:46 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 07:46 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 07:46 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 07:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 07:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 07:46 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 07:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 07:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 07:46 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 07:46 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 07:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 07:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 07:46 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 07:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 07:46 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 07:46 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 07:46 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 07:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 07:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 07:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 07:46 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 07:46 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 07:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 07:46 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 07:46 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 07:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 07:46 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 46 of 84
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Sample:MW-7 Lab ID:92311078009 Collected:09/01/16 11:15 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 09/08/16 07:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 07:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 07:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 07:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 07:46 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 07:46 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 07:46 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 07:46 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 07:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 07:46 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 07:46 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 07:46 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 07:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 07:46 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 07:46 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 07:46 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 07:46 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 07:46 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 07:46 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 07:46 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 07:46 107-12-01503.6 1
Styrene ND ug/L 09/08/16 07:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 07:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 07:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 07:46 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 07:46 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 07:46 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 07:46 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 07:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 07:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 07:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 07:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 07:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 07:46 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 07:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 07:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %09/08/16 07:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/08/16 07:46 17060-07-070-130 1
Toluene-d8 (S)106 %09/08/16 07:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Huntersville, NC 28078
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Page 47 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327371
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814119
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 09/08/16 12:340.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814120LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814121MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311072001
1814122
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-125104 3 252.5ND 2.5 2.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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[phone]
Page 48 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327495
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006, 92311078007,
92311078008, 92311078009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814776
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006, 92311078007,
92311078008, 92311078009
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/07/16 22:513.8
Arsenic ug/L ND 10.0 09/07/16 22:512.5
Barium ug/L ND 100 09/07/16 22:512.5
Beryllium ug/L ND 1.0 09/07/16 22:510.50
Cadmium ug/L ND 1.0 09/07/16 22:510.50
Chromium ug/L ND 10.0 09/07/16 22:512.5
Cobalt ug/L ND 10.0 09/07/16 22:512.5
Copper ug/L ND 10.0 09/07/16 22:512.5
Lead ug/L ND 10.0 09/07/16 22:512.5
Nickel ug/L ND 50.0 09/07/16 22:512.5
Selenium ug/L ND 10.0 09/07/16 22:515.0
Silver ug/L ND 10.0 09/07/16 22:512.5
Thallium ug/L ND 5.5 09/07/16 22:515.0
Tin ug/L ND 100 09/07/16 22:512.5
Vanadium ug/L ND 25.0 09/07/16 22:512.5
Zinc ug/L ND 10.0 09/07/16 22:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814777LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 463500 93 80-120
Arsenic ug/L 449500 90 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 502500 100 80-120
Lead ug/L 471500 94 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 478500 96 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 460500 92 80-120
Tin ug/L 476500 95 80-120
Vanadium ug/L 490500 98 80-120
Zinc ug/L 474500 95 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814778MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311078001
1814779
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 85 75-12586 0 25500ND428430
Arsenic ug/L 500 87 75-12588 1 255005.8J 443 446
Barium ug/L 500 104 75-125104 1 2550020.2J 539 542
Beryllium ug/L 500 100 75-125101 1 25500ND499503
Cadmium ug/L 500 97 75-12597 0 25500ND484485
Chromium ug/L 500 104 75-125106 2 2550020.1 541 550
Cobalt ug/L 500 95 75-12595 0 25500ND475475
Copper ug/L 500 102 75-125103 0 255003.1J 514 516
Lead ug/L 500 93 75-12593 0 255004.4J 469 469
Nickel ug/L 500 95 75-12596 1 25500ND476481
Selenium ug/L 500 92 75-12592 1 25500ND462466
Silver ug/L 250 98 75-12598 0 25250ND245245
Thallium ug/L 500 90 75-12591 1 25500ND451456
Tin ug/L 500 94 75-12594 0 25500ND471471
Vanadium ug/L 500 99 75-125100 1 2550028.4 524 527
Zinc ug/L 500 96 75-12596 0 25500ND482485
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327683
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006, 92311078007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815879
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006, 92311078007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/07/16 23:440.33
1,1,1-Trichloroethane ug/L ND 1.0 09/07/16 23:440.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/07/16 23:440.40
1,1,2-Trichloroethane ug/L ND 1.0 09/07/16 23:440.29
1,1-Dichloroethane ug/L ND 5.0 09/07/16 23:440.32
1,1-Dichloroethene ug/L ND 5.0 09/07/16 23:440.56
1,1-Dichloropropene ug/L ND 5.0 09/07/16 23:440.49
1,2,3-Trichloropropane ug/L ND 1.0 09/07/16 23:440.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/07/16 23:440.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/07/16 23:442.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/07/16 23:440.27
1,2-Dichlorobenzene ug/L ND 5.0 09/07/16 23:440.30
1,2-Dichloroethane ug/L ND 1.0 09/07/16 23:440.24
1,2-Dichloropropane ug/L ND 1.0 09/07/16 23:440.27
1,3-Dichlorobenzene ug/L ND 5.0 09/07/16 23:440.24
1,3-Dichloropropane ug/L ND 1.0 09/07/16 23:440.28
1,4-Dichlorobenzene ug/L ND 1.0 09/07/16 23:440.33
2,2-Dichloropropane ug/L ND 15.0 09/07/16 23:440.13
2-Butanone (MEK)ug/L ND 100 09/07/16 23:440.96
2-Hexanone ug/L ND 50.0 09/07/16 23:440.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/07/16 23:440.33
Acetone ug/L ND 100 09/07/16 23:4410.0
Acetonitrile ug/L ND 55.0 09/07/16 23:442.2
Acrolein ug/L ND 53.0 09/07/16 23:441.6
Acrylonitrile ug/L ND 200 09/07/16 23:441.9
Allyl chloride ug/L ND 10.0 09/07/16 23:441.5
Benzene ug/L ND 1.0 09/07/16 23:440.25
Bromochloromethane ug/L ND 3.0 09/07/16 23:440.17
Bromodichloromethane ug/L ND 1.0 09/07/16 23:440.18
Bromoform ug/L ND 3.0 09/07/16 23:440.26
Bromomethane ug/L ND 10.0 09/07/16 23:440.29
Carbon disulfide ug/L ND 100 09/07/16 23:441.2
Carbon tetrachloride ug/L ND 1.0 09/07/16 23:440.25
Chlorobenzene ug/L ND 3.0 09/07/16 23:440.23
Chloroethane ug/L ND 10.0 09/07/16 23:440.54
Chloroform ug/L ND 5.0 09/07/16 23:440.14
Chloromethane ug/L ND 1.0 09/07/16 23:440.11
Chloroprene ug/L ND 20.0 09/07/16 23:440.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/07/16 23:440.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/07/16 23:440.13
Dibromochloromethane ug/L ND 3.0 09/07/16 23:440.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 51 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815879
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006, 92311078007
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 09/07/16 23:440.21
Dichlorodifluoromethane ug/L ND 5.0 09/07/16 23:440.21
Ethyl methacrylate ug/L ND 10.0 09/07/16 23:440.20
Ethylbenzene ug/L ND 1.0 09/07/16 23:440.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/07/16 23:440.71
Iodomethane ug/L ND 10.0 09/07/16 23:440.32
Isobutanol ug/L ND 100 09/07/16 23:4435.0
Methacrylonitrile ug/L ND 100 09/07/16 23:440.93
Methyl methacrylate ug/L ND 30.0 09/07/16 23:442.0
Methylene Chloride ug/L ND 1.0 09/07/16 23:440.97
Naphthalene ug/L ND 10.0 09/07/16 23:440.24
Propionitrile ug/L ND 150 09/07/16 23:443.6
Styrene ug/L ND 1.0 09/07/16 23:440.26
Tetrachloroethene ug/L ND 1.0 09/07/16 23:440.46
Tetrahydrofuran ug/L ND 10.0 09/07/16 23:443.1
Toluene ug/L ND 1.0 09/07/16 23:440.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/07/16 23:440.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/07/16 23:440.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/07/16 23:441.0
Trichloroethene ug/L ND 1.0 09/07/16 23:440.47
Trichlorofluoromethane ug/L ND 1.0 09/07/16 23:440.20
Vinyl acetate ug/L ND 50.0 09/07/16 23:440.35
Vinyl chloride ug/L ND 1.0 09/07/16 23:440.62
Xylene (Total)ug/L ND 5.0 09/07/16 23:440.66
1,2-Dichloroethane-d4 (S)%105 70-130 09/07/16 23:44
4-Bromofluorobenzene (S)%101 70-130 09/07/16 23:44
Toluene-d8 (S)%101 70-130 09/07/16 23:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815880LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.050 110 80-125
1,1,1-Trichloroethane ug/L 51.850 104 71-129
1,1,2,2-Tetrachloroethane ug/L 56.350 113 79-124
1,1,2-Trichloroethane ug/L 52.150 104 85-125
1,1-Dichloroethane ug/L 50.850 102 73-126
1,1-Dichloroethene ug/L 54.350 109 66-135
1,1-Dichloropropene ug/L 52.350 105 74-135
1,2,3-Trichloropropane ug/L 53.550 107 75-130
1,2,4-Trichlorobenzene ug/L 56.350 113 75-134
1,2-Dibromo-3-chloropropane ug/L 52.850 106 71-133
1,2-Dibromoethane (EDB)ug/L 60.450 121 83-124
1,2-Dichlorobenzene ug/L 56.350 113 80-133
1,2-Dichloroethane ug/L 50.450 101 67-128
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815880LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 51.350 103 75-132
1,3-Dichlorobenzene ug/L 56.650 113 77-130
1,3-Dichloropropane ug/L 54.150 108 76-131
1,4-Dichlorobenzene ug/L 54.550 109 78-130
2,2-Dichloropropane ug/L 49.050 98 40-160
2-Butanone (MEK)ug/L 127100 127 61-144
2-Hexanone ug/L 125100 125 68-143
4-Methyl-2-pentanone (MIBK)ug/L 115100 115 72-135
Acetone ug/L 155 L010015548-146
Acetonitrile ug/L 593500 119 62-150
Acrolein ug/L 289 F325011624-160
Acrylonitrile ug/L 288250 115 40-160
Allyl chloride ug/L 51.650 103 66-137
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 54.250 108 71-125
Bromodichloromethane ug/L 53.150 106 78-124
Bromoform ug/L 47.550 95 71-128
Bromomethane ug/L 49.7 F3509940-160
Carbon disulfide ug/L 67.7J F35013550-160
Carbon tetrachloride ug/L 52.750 105 69-131
Chlorobenzene ug/L 53.550 107 81-122
Chloroethane ug/L 49.950 100 39-148
Chloroform ug/L 49.350 99 73-127
Chloromethane ug/L 47.250 94 44-146
Chloroprene ug/L 53.850 108 75-145
cis-1,2-Dichloroethene ug/L 51.350 103 74-124
cis-1,3-Dichloropropene ug/L 54.750 109 72-132
Dibromochloromethane ug/L 57.350 115 78-125
Dibromomethane ug/L 51.150 102 82-120
Dichlorodifluoromethane ug/L 47.050 94 34-157
Ethyl methacrylate ug/L 56.150 112 82-121
Ethylbenzene ug/L 52.250 104 79-121
Hexachloro-1,3-butadiene ug/L 52.550 105 72-131
Iodomethane ug/L 113100 113 39-154
Isobutanol ug/L 15601000 156 34-160
Methacrylonitrile ug/L 595500 119 74-134
Methyl methacrylate ug/L 57.150 114 84-124
Methylene Chloride ug/L 54.950 110 64-133
Naphthalene ug/L 54.650 109 73-133
Propionitrile ug/L 616500 123 73-140
Styrene ug/L 54.250 108 84-126
Tetrachloroethene ug/L 52.350 105 78-122
Tetrahydrofuran ug/L 611500 122 69-148
Toluene ug/L 51.650 103 80-121
trans-1,2-Dichloroethene ug/L 51.150 102 71-127
trans-1,3-Dichloropropene ug/L 53.050 106 69-141
trans-1,4-Dichloro-2-butene ug/L 92.4J F3,L05018540-160
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815880LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 52.250 104 78-122
Trichlorofluoromethane ug/L 49.750 99 53-137
Vinyl acetate ug/L 119100 119 40-160
Vinyl chloride ug/L 46.850 94 58-137
Xylene (Total)ug/L 155150 103 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815882MATRIX SPIKE SAMPLE:
MSSpike
Result
92311078007
1,1,1,2-Tetrachloroethane ug/L 21.320 107 70-130ND
1,1,1-Trichloroethane ug/L 23.520 118 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.220 101 70-130ND
1,1,2-Trichloroethane ug/L 20.920 104 70-130ND
1,1-Dichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethene ug/L 23.120 115 70-166ND
1,1-Dichloropropene ug/L 22.920 115 70-130ND
1,2,3-Trichloropropane ug/L 21.820 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.720 114 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.020 105 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.620 118 70-130ND
1,2-Dichlorobenzene ug/L 23.020 115 70-130ND
1,2-Dichloroethane ug/L 21.320 106 70-130ND
1,2-Dichloropropane ug/L 22.520 112 70-130ND
1,3-Dichlorobenzene ug/L 22.820 114 70-130ND
1,3-Dichloropropane ug/L 22.320 111 70-130ND
1,4-Dichlorobenzene ug/L 21.620 108 70-130ND
2,2-Dichloropropane ug/L 24.320 122 70-130ND
2-Butanone (MEK)ug/L 39.2J40 98 70-130ND
2-Hexanone ug/L 40.5J40 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.2J40 98 70-130ND
Acetone ug/L 34.5J40 86 70-130ND
Acetonitrile ug/L 180200 90 70-130ND
Acrolein ug/L 114100 114 70-130ND
Acrylonitrile ug/L 104J100 104 70-130ND
Allyl chloride ug/L 21.320 106 70-130ND
Benzene ug/L 22.520 113 70-148ND
Bromochloromethane ug/L 23.020 115 70-130ND
Bromodichloromethane ug/L 22.620 113 70-130ND
Bromoform ug/L 20.720 103 70-130ND
Bromomethane ug/L 20.220 101 70-130ND
Carbon disulfide ug/L 23.1J20 116 70-130ND
Carbon tetrachloride ug/L 22.920 114 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815882MATRIX SPIKE SAMPLE:
MSSpike
Result
92311078007
Chlorobenzene ug/L 23.520 118 70-146ND
Chloroethane ug/L 21.020 105 70-130ND
Chloroform ug/L 22.120 110 70-130ND
Chloromethane ug/L 18.220 91 70-130ND
Chloroprene ug/L 23.320 117 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 22.820 114 70-130ND
Dibromochloromethane ug/L 21.120 105 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Dichlorodifluoromethane ug/L 13.3 M1206670-130ND
Ethyl methacrylate ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 22.820 114 70-130ND
Hexachloro-1,3-butadiene ug/L 24.620 123 70-130ND
Iodomethane ug/L 43.440 108 70-130ND
Isobutanol ug/L 366400 91 70-130ND
Methacrylonitrile ug/L 216200 108 70-130ND
Methyl methacrylate ug/L 21.1J20 105 70-130ND
Methylene Chloride ug/L 19.820 99 70-130ND
Naphthalene ug/L 20.420 102 70-130ND
Propionitrile ug/L 200200 100 70-130ND
Styrene ug/L 25.020 125 70-130ND
Tetrachloroethene ug/L 21.820 109 70-130ND
Tetrahydrofuran ug/L 200200 100 70-130ND
Toluene ug/L 21.920 109 70-155ND
trans-1,2-Dichloroethene ug/L 23.320 116 70-130ND
trans-1,3-Dichloropropene ug/L 21.720 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.6J20 98 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 22.320 111 70-130ND
Vinyl acetate ug/L 42.8J40 107 70-130ND
Vinyl chloride ug/L 19.420 97 70-130ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078006
1815881SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078006
1815881SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.24J 300.34J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L 0.28J 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311078006
1815881SAMPLE DUPLICATE:
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 304.0J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 4102
4-Bromofluorobenzene (S)%103 2101
Toluene-d8 (S)%109 5103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311078008, 92311078009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311078008, 92311078009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/08/16 00:010.33
1,1,1-Trichloroethane ug/L ND 1.0 09/08/16 00:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/08/16 00:010.40
1,1,2-Trichloroethane ug/L ND 1.0 09/08/16 00:010.29
1,1-Dichloroethane ug/L ND 5.0 09/08/16 00:010.32
1,1-Dichloroethene ug/L ND 5.0 09/08/16 00:010.56
1,1-Dichloropropene ug/L ND 5.0 09/08/16 00:010.49
1,2,3-Trichloropropane ug/L ND 1.0 09/08/16 00:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/08/16 00:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/08/16 00:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/16 00:010.27
1,2-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.30
1,2-Dichloroethane ug/L ND 1.0 09/08/16 00:010.24
1,2-Dichloropropane ug/L ND 1.0 09/08/16 00:010.27
1,3-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.24
1,3-Dichloropropane ug/L ND 1.0 09/08/16 00:010.28
1,4-Dichlorobenzene ug/L ND 1.0 09/08/16 00:010.33
2,2-Dichloropropane ug/L ND 15.0 09/08/16 00:010.13
2-Butanone (MEK)ug/L ND 100 09/08/16 00:010.96
2-Hexanone ug/L ND 50.0 09/08/16 00:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/08/16 00:010.33
Acetone ug/L ND 100 09/08/16 00:0110.0
Acetonitrile ug/L ND 55.0 09/08/16 00:012.2
Acrolein ug/L ND 53.0 09/08/16 00:011.6
Acrylonitrile ug/L ND 200 09/08/16 00:011.9
Allyl chloride ug/L ND 10.0 09/08/16 00:011.5
Benzene ug/L ND 1.0 09/08/16 00:010.25
Bromochloromethane ug/L ND 3.0 09/08/16 00:010.17
Bromodichloromethane ug/L ND 1.0 09/08/16 00:010.18
Bromoform ug/L ND 3.0 09/08/16 00:010.26
Bromomethane ug/L ND 10.0 09/08/16 00:010.29
Carbon disulfide ug/L ND 100 09/08/16 00:011.2
Carbon tetrachloride ug/L ND 1.0 09/08/16 00:010.25
Chlorobenzene ug/L ND 3.0 09/08/16 00:010.23
Chloroethane ug/L ND 10.0 09/08/16 00:010.54
Chloroform ug/L ND 5.0 09/08/16 00:010.14
Chloromethane ug/L ND 1.0 09/08/16 00:010.11
Chloroprene ug/L ND 20.0 09/08/16 00:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.13
Dibromochloromethane ug/L ND 3.0 09/08/16 00:010.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311078008, 92311078009
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 09/08/16 00:010.21
Dichlorodifluoromethane ug/L ND 5.0 09/08/16 00:010.21
Ethyl methacrylate ug/L ND 10.0 09/08/16 00:010.20
Ethylbenzene ug/L ND 1.0 09/08/16 00:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/08/16 00:010.71
Iodomethane ug/L ND 10.0 09/08/16 00:010.32
Isobutanol ug/L ND 100 09/08/16 00:0135.0
Methacrylonitrile ug/L ND 100 09/08/16 00:010.93
Methyl methacrylate ug/L ND 30.0 09/08/16 00:012.0
Methylene Chloride ug/L ND 1.0 09/08/16 00:010.97
Naphthalene ug/L ND 10.0 09/08/16 00:010.24
Propionitrile ug/L ND 150 09/08/16 00:013.6
Styrene ug/L ND 1.0 09/08/16 00:010.26
Tetrachloroethene ug/L ND 1.0 09/08/16 00:010.46
Tetrahydrofuran ug/L ND 10.0 09/08/16 00:013.1
Toluene ug/L ND 1.0 09/08/16 00:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/08/16 00:011.0
Trichloroethene ug/L ND 1.0 09/08/16 00:010.47
Trichlorofluoromethane ug/L ND 1.0 09/08/16 00:010.20
Vinyl acetate ug/L ND 50.0 09/08/16 00:010.35
Vinyl chloride ug/L ND 1.0 09/08/16 00:010.62
Xylene (Total)ug/L ND 5.0 09/08/16 00:010.66
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/16 00:01
4-Bromofluorobenzene (S)%101 70-130 09/08/16 00:01
Toluene-d8 (S)%103 70-130 09/08/16 00:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 80-125
1,1,1-Trichloroethane ug/L 54.750 109 71-129
1,1,2,2-Tetrachloroethane ug/L 53.850 108 79-124
1,1,2-Trichloroethane ug/L 53.150 106 85-125
1,1-Dichloroethane ug/L 54.750 109 73-126
1,1-Dichloroethene ug/L 59.450 119 66-135
1,1-Dichloropropene ug/L 56.350 113 74-135
1,2,3-Trichloropropane ug/L 54.150 108 75-130
1,2,4-Trichlorobenzene ug/L 56.550 113 75-134
1,2-Dibromo-3-chloropropane ug/L 52.050 104 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 57.850 116 80-133
1,2-Dichloroethane ug/L 54.050 108 67-128
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 53.150 106 75-132
1,3-Dichlorobenzene ug/L 57.650 115 77-130
1,3-Dichloropropane ug/L 54.250 108 76-131
1,4-Dichlorobenzene ug/L 55.150 110 78-130
2,2-Dichloropropane ug/L 53.350 107 40-160
2-Butanone (MEK)ug/L 133100 133 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 158 L010015848-146
Acetonitrile ug/L 623500 125 62-150
Acrolein ug/L 307 F325012324-160
Acrylonitrile ug/L 297250 119 40-160
Allyl chloride ug/L 55.550 111 66-137
Benzene ug/L 55.650 111 80-125
Bromochloromethane ug/L 59.350 119 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 53.7 F35010740-160
Carbon disulfide ug/L 74.3J F35014950-160
Carbon tetrachloride ug/L 58.250 116 69-131
Chlorobenzene ug/L 55.950 112 81-122
Chloroethane ug/L 55.850 112 39-148
Chloroform ug/L 53.150 106 73-127
Chloromethane ug/L 52.150 104 44-146
Chloroprene ug/L 57.250 114 75-145
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
cis-1,3-Dichloropropene ug/L 57.450 115 72-132
Dibromochloromethane ug/L 57.550 115 78-125
Dibromomethane ug/L 52.150 104 82-120
Dichlorodifluoromethane ug/L 51.750 103 34-157
Ethyl methacrylate ug/L 56.750 113 82-121
Ethylbenzene ug/L 54.250 108 79-121
Hexachloro-1,3-butadiene ug/L 57.750 115 72-131
Iodomethane ug/L 124100 124 39-154
Isobutanol ug/L 15401000 154 34-160
Methacrylonitrile ug/L 606500 121 74-134
Methyl methacrylate ug/L 57.650 115 84-124
Methylene Chloride ug/L 58.550 117 64-133
Naphthalene ug/L 55.150 110 73-133
Propionitrile ug/L 620500 124 73-140
Styrene ug/L 56.350 113 84-126
Tetrachloroethene ug/L 54.450 109 78-122
Tetrahydrofuran ug/L 609500 122 69-148
Toluene ug/L 54.550 109 80-121
trans-1,2-Dichloroethene ug/L 55.850 112 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
trans-1,4-Dichloro-2-butene ug/L 92.9J F3,L05018640-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 55.550 111 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 123100 123 40-160
Vinyl chloride ug/L 52.350 105 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,1-Dichloropropene ug/L 21.620 108 70-130ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.820 114 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 19.720 99 70-130ND
1,2-Dichloropropane ug/L 21.120 106 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,3-Dichloropropane ug/L 20.320 101 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2,2-Dichloropropane ug/L 22.820 114 70-130ND
2-Butanone (MEK)ug/L 39.8J40 99 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.1J40 98 70-130ND
Acetone ug/L 37.7J40 73 70-130ND
Acetonitrile ug/L 186200 93 70-130ND
Acrolein ug/L 115100 115 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 20.720 104 70-130ND
Benzene ug/L 21.920 109 70-148ND
Bromochloromethane ug/L 21.120 105 70-130ND
Bromodichloromethane ug/L 20.920 104 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
Chloroprene ug/L 22.020 110 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 108 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 20.320 101 70-130ND
Dichlorodifluoromethane ug/L 13.5 M1206870-130ND
Ethyl methacrylate ug/L 20.620 103 70-130ND
Ethylbenzene ug/L 21.120 106 70-130ND
Hexachloro-1,3-butadiene ug/L 24.220 121 70-130ND
Iodomethane ug/L 40.040 100 70-130ND
Isobutanol ug/L 423400 106 70-130ND
Methacrylonitrile ug/L 205200 102 70-130ND
Methyl methacrylate ug/L 21.0J20 105 70-130ND
Methylene Chloride ug/L 18.620 93 70-130ND
Naphthalene ug/L 20.620 103 70-130ND
Propionitrile ug/L 205200 103 70-130ND
Styrene ug/L 21.820 109 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Tetrahydrofuran ug/L 205200 101 70-130ND
Toluene ug/L 21.420 103 70-1550.76J
trans-1,2-Dichloroethene ug/L 21.520 107 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 22.620 113 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 39.8J40 100 70-130ND
Vinyl chloride ug/L 18.220 91 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L 0.66J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 7105
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%108 6102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327585
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815055
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 09/07/16 21:310.050
4,4'-DDE ug/L ND 0.10 09/07/16 21:310.050
4,4'-DDT ug/L ND 0.10 09/07/16 21:310.050
Aldrin ug/L ND 0.050 09/07/16 21:310.050
alpha-BHC ug/L ND 0.050 09/07/16 21:310.050
beta-BHC ug/L ND 0.050 09/07/16 21:310.050
Chlordane (Technical)ug/L ND 0.50 09/07/16 21:310.20
delta-BHC ug/L ND 0.050 09/07/16 21:310.050
Dieldrin ug/L ND 0.075 09/07/16 21:310.050
Endosulfan I ug/L ND 0.10 09/07/16 21:310.050
Endosulfan II ug/L ND 0.10 09/07/16 21:310.050
Endosulfan sulfate ug/L ND 0.10 09/07/16 21:310.050
Endrin ug/L ND 0.10 09/07/16 21:310.050
Endrin aldehyde ug/L ND 0.10 09/07/16 21:310.050
gamma-BHC (Lindane)ug/L ND 0.050 09/07/16 21:310.050
Heptachlor ug/L ND 0.050 09/07/16 21:310.050
Heptachlor epoxide ug/L ND 0.075 09/07/16 21:310.050
Methoxychlor ug/L ND 1.0 09/07/16 21:310.15
Toxaphene ug/L ND 1.5 09/07/16 21:310.20
Decachlorobiphenyl (S)%67 20-130 09/07/16 21:31
Tetrachloro-m-xylene (S)%63 20-130 09/07/16 21:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815056LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.19.25 77 20-150
4,4'-DDE ug/L 0.18.25 72 20-150
4,4'-DDT ug/L 0.20.25 80 20-150
Aldrin ug/L 0.14.25 55 20-150
alpha-BHC ug/L 0.17.25 70 20-150
beta-BHC ug/L 0.18.25 74 20-150
delta-BHC ug/L 0.18.25 75 20-150
Dieldrin ug/L 0.17.25 69 20-150
Endosulfan I ug/L 0.18.25 75 20-150
Endosulfan II ug/L 0.20.25 81 20-150
Endosulfan sulfate ug/L 0.20.25 82 20-150
Endrin ug/L 0.18.25 72 20-150
Endrin aldehyde ug/L 0.18.25 74 20-150
gamma-BHC (Lindane)ug/L 0.18.25 72 20-150
Heptachlor ug/L 0.16.25 66 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815056LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.18.25 72 20-150
Methoxychlor ug/L 0.73J.74 98 20-150
Decachlorobiphenyl (S)%61 20-130
Tetrachloro-m-xylene (S)%68 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815057MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738010
4,4'-DDD ug/L 0.15.25 59 20-150ND
4,4'-DDE ug/L 0.15.25 61 20-150ND
4,4'-DDT ug/L 0.15.25 60 20-150ND
Aldrin ug/L 0.14.25 57 20-150ND
alpha-BHC ug/L 0.17.25 68 20-150ND
beta-BHC ug/L 0.18.25 71 20-150ND
delta-BHC ug/L 0.18.25 73 20-150ND
Dieldrin ug/L 0.16.25 63 20-150ND
Endosulfan I ug/L 0.17.25 70 20-150ND
Endosulfan II ug/L 0.17.25 69 20-150ND
Endosulfan sulfate ug/L 0.17.25 68 20-150ND
Endrin ug/L 0.18.25 73 20-150ND
Endrin aldehyde ug/L 0.15.25 61 20-150ND
gamma-BHC (Lindane)ug/L 0.18.25 71 20-150ND
Heptachlor ug/L 0.18.25 73 20-150ND
Heptachlor epoxide ug/L 0.18.25 74 20-150ND
Methoxychlor ug/L 0.57J.74 77 20-150ND
Decachlorobiphenyl (S)%37 20-130
Tetrachloro-m-xylene (S)%69 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738011
1815058SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738011
1815058SAMPLE DUPLICATE:
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%62 261
Tetrachloro-m-xylene (S)%70 675
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327587
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815061
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 09/07/16 22:500.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 09/07/16 22:500.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 09/07/16 22:500.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 09/07/16 22:500.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 09/07/16 22:500.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 09/07/16 22:500.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 09/07/16 22:500.50
Decachlorobiphenyl (S)%64 10-132 09/07/16 22:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815062LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 4.55 89 50-150
PCB-1260 (Aroclor 1260)ug/L 5.15 102 50-150
Decachlorobiphenyl (S)%65 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815063MATRIX SPIKE SAMPLE:
MSSpike
Result
92310738016
PCB-1016 (Aroclor 1016)ug/L 5.05 99 50-150ND
PCB-1260 (Aroclor 1260)ug/L 4.85 95 50-150ND
Decachlorobiphenyl (S)%84 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92310738017
1815064SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%71 568
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
318978
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1695159
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 09/08/16 06:570.042
2,4,5-TP (Silvex)ug/L ND 0.19 09/08/16 06:570.049
2,4-D ug/L ND 0.94 09/08/16 06:570.22
2,4-DB ug/L ND 1.9 09/08/16 06:570.51
Bentazon ug/L ND 0.094 09/08/16 06:570.047
Dalapon ug/L ND 0.91 09/08/16 06:570.43
Dicamba ug/L ND 0.094 09/08/16 06:570.030
Dichlorprop ug/L ND 0.65 09/08/16 06:570.19
Dinoseb ug/L ND 0.19 09/08/16 06:570.057
Pentachlorophenol ug/L ND 0.028 09/08/16 06:570.017
Picloram ug/L ND 0.094 09/08/16 06:570.019
2,4-DCAA (S)%79 39-139 09/08/16 06:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1695160LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.21.2 103 37-133
2,4,5-TP (Silvex)ug/L 1.11.2 94 53-134
2,4-D ug/L 5.46 91 35-124
2,4-DB ug/L 13.512 112 31-132
Bentazon ug/L 0.50.6 83 51-125
Dalapon ug/L 7.7 L0612910-122
Dicamba ug/L 0.55.6 92 44-125
Dichlorprop ug/L 4.04.2 96 70-130
Dinoseb ug/L 0.871.2 73 13-116
Pentachlorophenol ug/L 0.18.18 101 39-170
Picloram ug/L 0.60.6 100 10-127
2,4-DCAA (S)%89 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1695291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738010
1695292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 2.4 106 37-13399 6 402.4ND 2.5 2.4
2,4,5-TP (Silvex)ug/L 2.4 97 53-13492 5 402.4ND 2.3 2.2
2,4-D ug/L 12 93 35-12489 4 4012ND11.2 10.7
2,4-DB ug/L 24 104 31-13296 8 4024ND25.0 23.0
Bentazon ug/L 1.2 82 51-12579 3 401.2ND 0.98 0.95
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1695291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738010
1695292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dalapon ug/L M01212310-122129 4 4012ND14.8 15.4
Dicamba ug/L 1.2 93 44-12589 4 401.2ND 1.1 1.1
Dichlorprop ug/L 8.4 95 70-13092 3 408.4ND 8.0 7.7
Dinoseb ug/L 2.4 53 13-11672 30 402.4ND 1.3 1.7
Pentachlorophenol ug/L .36 96 39-17096 0 40.36ND 0.34 0.34
Picloram ug/L 1.2 105 10-12793 12 401.2ND 1.3 1.1
2,4-DCAA (S)%93 39-13987 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327459
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814546
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 09/14/16 16:261.7
1,3,5-Trinitrobenzene ug/L ND 10.0 09/14/16 16:261.1
1,3-Dinitrobenzene ug/L ND 20.0 09/14/16 16:261.5
1,4-Naphthoquinone ug/L ND 10.0 09/14/16 16:261.8
1-Naphthalenamine ug/L ND 10.0 09/14/16 16:260.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/14/16 16:261.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 09/14/16 16:262.3
2,4,5-Trichlorophenol ug/L ND 10.0 09/14/16 16:262.2
2,4,6-Trichlorophenol ug/L ND 10.0 09/14/16 16:261.9
2,4-Dichlorophenol ug/L ND 10.0 09/14/16 16:261.7
2,4-Dimethylphenol ug/L ND 10.0 09/14/16 16:262.2
2,4-Dinitrophenol ug/L ND 50.0 09/14/16 16:266.5
2,4-Dinitrotoluene ug/L ND 10.0 09/14/16 16:261.2
2,6-Dichlorophenol ug/L ND 10.0 09/14/16 16:261.8
2,6-Dinitrotoluene ug/L ND 10.0 09/14/16 16:261.7
2-Acetylaminofluorene ug/L 7.1J 20.0 09/14/16 16:260.84
2-Chloronaphthalene ug/L ND 10.0 09/14/16 16:262.2
2-Chlorophenol ug/L ND 10.0 09/14/16 16:261.5
2-Methylnaphthalene ug/L ND 10.0 09/14/16 16:260.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/14/16 16:261.7
2-Naphthalenamine ug/L ND 10.0 09/14/16 16:260.98
2-Nitroaniline ug/L ND 50.0 09/14/16 16:262.8
2-Nitrophenol ug/L ND 10.0 09/14/16 16:261.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/14/16 16:261.7
3,3'-Dichlorobenzidine ug/L ND 20.0 09/14/16 16:261.4
3,3'-Dimethylbenzidine ug/L ND 10.0 09/14/16 16:262.1
3-Methylcholanthrene ug/L ND 10.0 09/14/16 16:260.82
3-Nitroaniline ug/L ND 50.0 09/14/16 16:262.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 09/14/16 16:261.7
4-Aminobiphenyl ug/L ND 20.0 09/14/16 16:260.92
4-Bromophenylphenyl ether ug/L ND 10.0 09/14/16 16:261.3
4-Chloro-3-methylphenol ug/L ND 20.0 09/14/16 16:264.2
4-Chloroaniline ug/L ND 20.0 09/14/16 16:263.4
4-Chlorophenylphenyl ether ug/L ND 10.0 09/14/16 16:262.1
4-Nitroaniline ug/L ND 20.0 09/14/16 16:262.5
4-Nitrophenol ug/L ND 50.0 09/14/16 16:265.8
5-Nitro-o-toluidine ug/L ND 10.0 09/14/16 16:261.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 09/14/16 16:260.77
Acenaphthene ug/L ND 10.0 09/14/16 16:260.25
Acenaphthylene ug/L ND 10.0 09/14/16 16:260.21
Acetophenone ug/L ND 10.0 09/14/16 16:262.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 71 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814546
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 09/14/16 16:260.14
Benzo(a)anthracene ug/L ND 10.0 09/14/16 16:260.33
Benzo(a)pyrene ug/L ND 10.0 09/14/16 16:260.30
Benzo(b)fluoranthene ug/L ND 10.0 09/14/16 16:260.28
Benzo(g,h,i)perylene ug/L ND 10.0 09/14/16 16:260.38
Benzo(k)fluoranthene ug/L ND 10.0 09/14/16 16:260.43
Benzyl alcohol ug/L ND 20.0 09/14/16 16:263.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/14/16 16:261.7
bis(2-Chloroethyl) ether ug/L ND 10.0 09/14/16 16:261.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 09/14/16 16:260.85
Butylbenzylphthalate ug/L ND 10.0 09/14/16 16:260.75
Chlorobenzilate ug/L ND 10.0 09/14/16 16:260.72
Chrysene ug/L ND 10.0 09/14/16 16:260.21
Di-n-butylphthalate ug/L ND 10.0 09/14/16 16:261.1
Di-n-octylphthalate ug/L ND 10.0 09/14/16 16:260.86
Diallate ug/L ND 10.0 09/14/16 16:261.3
Dibenz(a,h)anthracene ug/L ND 10.0 09/14/16 16:260.55
Dibenzofuran ug/L ND 10.0 09/14/16 16:261.8
Diethylphthalate ug/L ND 6000 09/14/16 16:261.3
Dimethoate ug/L ND 20.0 09/14/16 16:260.92
Dimethylphthalate ug/L ND 10.0 09/14/16 16:261.5
Diphenylamine ug/L ND 10.0 09/14/16 16:261.3
Disulfoton ug/L ND 10.0 09/14/16 16:261.4
Ethyl methanesulfonate ug/L ND 20.0 09/14/16 16:261.8
Famphur ug/L ND 20.0 09/14/16 16:261.7
Fluoranthene ug/L ND 10.0 09/14/16 16:260.21
Fluorene ug/L ND 10.0 09/14/16 16:260.21
Hexachlorobenzene ug/L ND 10.0 09/14/16 16:261.1
Hexachlorocyclopentadiene ug/L ND 10.0 09/14/16 16:261.8
Hexachloroethane ug/L ND 10.0 09/14/16 16:261.5
Hexachloropropene ug/L ND 10.0 09/14/16 16:261.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/14/16 16:260.29
Isodrin ug/L ND 20.0 09/14/16 16:262.0
Isophorone ug/L ND 10.0 09/14/16 16:261.8
Isosafrole ug/L ND 10.0 09/14/16 16:261.8
Kepone ug/L ND 20.0 09/14/16 16:263.1
Methapyrilene ug/L ND 100 09/14/16 16:262.7
Methyl methanesulfonate ug/L ND 10.0 09/14/16 16:261.3
Methyl parathion ug/L ND 10.0 09/14/16 16:261.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 09/14/16 16:262.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/14/16 16:262.1
N-Nitrosodiethylamine ug/L ND 20.0 09/14/16 16:261.8
N-Nitrosodimethylamine ug/L ND 10.0 09/14/16 16:261.3
N-Nitrosodiphenylamine ug/L ND 10.0 09/14/16 16:261.3
N-Nitrosomethylethylamine ug/L ND 10.0 09/14/16 16:261.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 72 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814546
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 09/14/16 16:261.9
N-Nitrosopyrrolidine ug/L ND 10.0 09/14/16 16:262.5
Nitrobenzene ug/L ND 10.0 09/14/16 16:261.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 09/14/16 16:261.8
O-Toluidine ug/L ND 10.0 09/14/16 16:261.6
P-Dimethylaminoazobenzene ug/L ND 10.0 09/14/16 16:260.35
p-Phenylenediamine ug/L ND 10.0 09/14/16 16:260.96
Parathion (Ethyl parathion)ug/L ND 10.0 09/14/16 16:261.1
Pentachlorobenzene ug/L ND 10.0 09/14/16 16:262.0
Pentachloronitrobenzene ug/L ND 20.0 09/14/16 16:261.0
Pentachlorophenol ug/L ND 25.0 09/14/16 16:262.3
Phenacetin ug/L ND 20.0 09/14/16 16:260.97
Phenanthrene ug/L ND 10.0 09/14/16 16:260.22
Phenol ug/L ND 10.0 09/14/16 16:261.7
Phorate ug/L ND 10.0 09/14/16 16:261.1
Pronamide ug/L ND 10.0 09/14/16 16:260.97
Pyrene ug/L ND 10.0 09/14/16 16:260.19
Safrole ug/L ND 10.0 09/14/16 16:261.5
Thionazin ug/L ND 20.0 09/14/16 16:261.2
2,4,6-Tribromophenol (S)%88 27-110 09/14/16 16:26
2-Fluorobiphenyl (S)%70 27-110 09/14/16 16:26
2-Fluorophenol (S)%45 12-110 09/14/16 16:26
Nitrobenzene-d5 (S)%77 21-110 09/14/16 16:26
Phenol-d6 (S)%33 10-110 09/14/16 16:26
Terphenyl-d14 (S)%89 31-107 09/14/16 16:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 38.650 77 16-129
1,3,5-Trinitrobenzene ug/L 53.950 108 55-125
1,3-Dinitrobenzene ug/L 54.250 108 30-122
1,4-Naphthoquinone ug/L 49.050 98 31-120
1-Naphthalenamine ug/L 43.450 87 37-126
2,2'-Oxybis(1-chloropropane)ug/L 38.450 77 18-120
2,3,4,6-Tetrachlorophenol ug/L 11850 237 54-276
2,4,5-Trichlorophenol ug/L 47.950 96 43-113
2,4,6-Trichlorophenol ug/L 48.450 97 42-120
2,4-Dichlorophenol ug/L 48.850 98 30-120
2,4-Dimethylphenol ug/L 44.550 89 29-111
2,4-Dinitrophenol ug/L 193250 77 19-132
2,4-Dinitrotoluene ug/L 59.750 119 58-128
2,6-Dichlorophenol ug/L 44.950 90 54-128
2,6-Dinitrotoluene ug/L 60.550 121 54-129
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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[phone]
Page 73 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 61.850 124 81-160
2-Chloronaphthalene ug/L 50.150 100 43-117
2-Chlorophenol ug/L 38.450 77 37-120
2-Methylnaphthalene ug/L 46.750 93 33-120
2-Methylphenol(o-Cresol)ug/L 34.650 69 31-120
2-Naphthalenamine ug/L 55.350 111 41-136
2-Nitroaniline ug/L 73.1100 73 48-121
2-Nitrophenol ug/L 47.950 96 25-116
3&4-Methylphenol(m&p Cresol)ug/L 30.050 60 23-120
3,3'-Dichlorobenzidine ug/L 97.0250 39 10-154
3,3'-Dimethylbenzidine ug/L 96.6100 97 10-157
3-Methylcholanthrene ug/L 52.450 105 65-130
3-Nitroaniline ug/L 89.3100 89 43-115
4,6-Dinitro-2-methylphenol ug/L 96.1100 96 44-124
4-Aminobiphenyl ug/L 49.350 99 21-125
4-Bromophenylphenyl ether ug/L 49.050 98 34-113
4-Chloro-3-methylphenol ug/L 98.8100 99 31-110
4-Chloroaniline ug/L 91.2100 91 20-120
4-Chlorophenylphenyl ether ug/L 53.750 107 34-116
4-Nitroaniline ug/L 94.0100 94 46-128
4-Nitrophenol ug/L 108250 43 11-120
5-Nitro-o-toluidine ug/L 65.550 131 78-160
7,12-Dimethylbenz(a)anthracene ug/L 46.550 93 47-124
Acenaphthene ug/L 42.150 84 48-114
Acenaphthylene ug/L 44.050 88 48-112
Acetophenone ug/L 39.950 80 24-120
Anthracene ug/L 43.450 87 57-118
Benzo(a)anthracene ug/L 48.150 96 56-121
Benzo(a)pyrene ug/L 48.450 97 55-127
Benzo(b)fluoranthene ug/L 51.850 104 53-128
Benzo(g,h,i)perylene ug/L 54.250 108 54-125
Benzo(k)fluoranthene ug/L 50.450 101 51-123
Benzyl alcohol ug/L 66.7100 67 27-120
bis(2-Chloroethoxy)methane ug/L 43.850 88 32-120
bis(2-Chloroethyl) ether ug/L 39.950 80 33-111
bis(2-Ethylhexyl)phthalate ug/L 40.850 82 50-145
Butylbenzylphthalate ug/L 42.450 85 54-138
Chlorobenzilate ug/L 49.050 98 65-132
Chrysene ug/L 48.450 97 58-127
Di-n-butylphthalate ug/L 43.050 86 56-125
Di-n-octylphthalate ug/L 37.550 75 50-134
Diallate ug/L 48.850 98 47-123
Dibenz(a,h)anthracene ug/L 54.350 109 53-129
Dibenzofuran ug/L 44.150 88 45-120
Diethylphthalate ug/L 50.8J50 102 53-120
Dimethoate ug/L 52.750 105 57-139
Dimethylphthalate ug/L 49.050 98 55-116
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Huntersville, NC 28078
[phone]
Page 74 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 37.750 75 42-120
Disulfoton ug/L 46.650 93 49-156
Ethyl methanesulfonate ug/L 51.950 104 43-120
Famphur ug/L 87.6100 88 40-160
Fluoranthene ug/L 49.350 99 57-125
Fluorene ug/L 49.850 100 53-118
Hexachlorobenzene ug/L 52.650 105 49-116
Hexachlorocyclopentadiene ug/L 31.350 63 26-158
Hexachloroethane ug/L 27.250 54 30-114
Hexachloropropene ug/L 26.750 53 13-137
Indeno(1,2,3-cd)pyrene ug/L 51.650 103 55-128
Isodrin ug/L 47.250 94 68-129
Isophorone ug/L 46.050 92 31-118
Isosafrole ug/L 42.650 85 48-107
Kepone ug/L 91.5100 92 10-124
Methapyrilene ug/L 58.1J50 116 40-160
Methyl methanesulfonate ug/L 34.050 68 25-114
Methyl parathion ug/L 53.850 108 58-137
N-Nitroso-di-n-butylamine ug/L 53.050 106 36-115
N-Nitroso-di-n-propylamine ug/L 35.650 71 32-119
N-Nitrosodiethylamine ug/L 56.550 113 47-115
N-Nitrosodimethylamine ug/L 22.650 45 13-120
N-Nitrosodiphenylamine ug/L 37.750 75 43-120
N-Nitrosomethylethylamine ug/L 46.750 93 39-120
N-Nitrosopiperidine ug/L 54.550 109 43-113
N-Nitrosopyrrolidine ug/L 79.2 L05015832-110
Nitrobenzene ug/L 42.850 86 33-110
O,O,O-Triethylphosphorothioate ug/L 43.350 87 51-127
O-Toluidine ug/L 61.3 L05012327-120
P-Dimethylaminoazobenzene ug/L 25.2100 25 10-120
p-Phenylenediamine ug/L 63.450 127 72-143
Parathion (Ethyl parathion)ug/L 52.450 105 56-140
Pentachlorobenzene ug/L 43.050 86 30-137
Pentachloronitrobenzene ug/L 53.250 106 70-124
Pentachlorophenol ug/L 105250 42 10-137
Phenacetin ug/L 55.050 110 60-130
Phenanthrene ug/L 44.150 88 57-117
Phenol ug/L 19.850 40 10-120
Phorate ug/L 49.150 98 55-126
Pronamide ug/L 47.550 95 75-124
Pyrene ug/L 45.050 90 55-122
Safrole ug/L 44.250 88 41-120
Thionazin ug/L 52.050 104 63-137
2,4,6-Tribromophenol (S)%106 27-110
2-Fluorobiphenyl (S)%76 27-110
2-Fluorophenol (S)%47 12-110
Nitrobenzene-d5 (S)%78 21-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814547LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%32 10-110
Terphenyl-d14 (S)%96 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 76 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327528
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814893
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004, 92311078005, 92311078006
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 09/07/16 00:10100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814894LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 536J500 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814895MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310972002
1814896
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 95 80-12095 1 10500ND482J485J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814897MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310972012
1814898
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 89 80-12089 0 10500ND450J450J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328197
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1818832
Associated Lab Samples:92311078001, 92311078002, 92311078003, 92311078004
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 09/13/16 03:114.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1818833LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 98.4100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818834MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738009
1818835
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L R11007975-12590 13 10100ND81.9 93.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818836MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311268001
1818837
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 106 75-125108 2 10100ND110112
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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[phone]
Page 78 of 84
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
328198
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92311078005, 92311078006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1818838
Associated Lab Samples:92311078005, 92311078006
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 09/13/16 03:374.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1818839LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 109100 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818840MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311078005
1818841
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 105 75-125102 3 101004.3J 109 107
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1818842MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311478001
1818843
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1100075-1251 10100ND5.3J 7.1J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Huntersville, NC 28078
[phone]
Page 79 of 84
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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[phone]
Page 80 of 84
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311078001 327585 327743MW-1R EPA 3510 EPA 8081
92311078002 327585 327743MW-2 EPA 3510 EPA 8081
92311078003 327585 327743MW-4 EPA 3510 EPA 8081
92311078004 327585 327743MW-6 EPA 3510 EPA 8081
92311078005 327585 327743MW-8 EPA 3510 EPA 8081
92311078006 327585 327743MW-11 EPA 3510 EPA 8081
92311078001 327587 327745MW-1R EPA 3510 EPA 8082
92311078002 327587 327745MW-2 EPA 3510 EPA 8082
92311078003 327587 327745MW-4 EPA 3510 EPA 8082
92311078004 327587 327745MW-6 EPA 3510 EPA 8082
92311078005 327587 327745MW-8 EPA 3510 EPA 8082
92311078006 327587 327745MW-11 EPA 3510 EPA 8082
92311078001 318978 319386MW-1R EPA 8151 EPA 8151
92311078002 318978 319386MW-2 EPA 8151 EPA 8151
92311078003 318978 319386MW-4 EPA 8151 EPA 8151
92311078004 318978 319386MW-6 EPA 8151 EPA 8151
92311078005 318978 319386MW-8 EPA 8151 EPA 8151
92311078006 318978 319386MW-11 EPA 8151 EPA 8151
92311078001 327495 327550MW-1R EPA 3010A EPA 6010
92311078002 327495 327550MW-2 EPA 3010A EPA 6010
92311078003 327495 327550MW-4 EPA 3010A EPA 6010
92311078004 327495 327550MW-6 EPA 3010A EPA 6010
92311078005 327495 327550MW-8 EPA 3010A EPA 6010
92311078006 327495 327550MW-11 EPA 3010A EPA 6010
92311078007 327495 327550MW-3 EPA 3010A EPA 6010
92311078008 327495 327550MW-5 EPA 3010A EPA 6010
92311078009 327495 327550MW-7 EPA 3010A EPA 6010
92311078001 327371 327378MW-1R EPA 7470 EPA 7470
92311078002 327371 327378MW-2 EPA 7470 EPA 7470
92311078003 327371 327378MW-4 EPA 7470 EPA 7470
92311078004 327371 327378MW-6 EPA 7470 EPA 7470
92311078005 327371 327378MW-8 EPA 7470 EPA 7470
92311078006 327371 327378MW-11 EPA 7470 EPA 7470
92311078001 327459 327627MW-1R EPA 3510 EPA 8270
92311078002 327459 327627MW-2 EPA 3510 EPA 8270
92311078003 327459 327627MW-4 EPA 3510 EPA 8270
92311078004 327459 327627MW-6 EPA 3510 EPA 8270
92311078005 327459 327627MW-8 EPA 3510 EPA 8270
92311078006 327459 327627MW-11 EPA 3510 EPA 8270
92311078001 327683MW-1R EPA 8260
92311078002 327683MW-2 EPA 8260
92311078003 327683MW-4 EPA 8260
92311078004 327683MW-6 EPA 8260
92311078005 327683MW-8 EPA 8260
92311078006 327683MW-11 EPA 8260
92311078007 327683MW-3 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 81 of 84
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311078
WAYNE CLOSED LF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311078008 327693MW-5 EPA 8260
92311078009 327693MW-7 EPA 8260
92311078001 327528MW-1R SM 4500-S2D
92311078002 327528MW-2 SM 4500-S2D
92311078003 327528MW-4 SM 4500-S2D
92311078004 327528MW-6 SM 4500-S2D
92311078005 327528MW-8 SM 4500-S2D
92311078006 327528MW-11 SM 4500-S2D
92311078001 328197MW-1R SM 4500-CN-E
92311078002 328197MW-2 SM 4500-CN-E
92311078003 328197MW-4 SM 4500-CN-E
92311078004 328197MW-6 SM 4500-CN-E
92311078005 328198MW-8 SM 4500-CN-E
92311078006 328198MW-11 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/19/2016 04:38 PM
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Page 82 of 84
Page 83 of 84
Page 84 of 84
#=CL#
September 13, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311096
92311096
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
WAYNE MSWLF BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92311096001 EB Water 09/01/16 17:00 09/02/16 08:50
92311096002 FB Water 09/01/16 17:15 09/02/16 08:50
92311096003 TB Water 09/01/16 00:00 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311096001 EB EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AWAB
EPA 8260 68 PASI-CGAW
92311096002 FB EPA 6010 16 PASI-AJMW
EPA 7470 1 PASI-AWAB
EPA 8260 68 PASI-CGAW
92311096003 TB EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:EB Lab ID:92311096001 Collected:09/01/16 17:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/11/16 00:31 7440-36-009/09/16 19:206.0 3.8 1
Arsenic ND ug/L 09/11/16 00:31 7440-38-209/09/16 19:2010.0 2.5 1
Barium ND ug/L 09/11/16 00:31 7440-39-309/09/16 19:201002.5 1
Beryllium ND ug/L 09/11/16 00:31 7440-41-709/09/16 19:201.0 0.50 1
Cadmium ND ug/L 09/11/16 00:31 7440-43-909/09/16 19:201.0 0.50 1
Chromium ND ug/L 09/11/16 00:31 7440-47-309/09/16 19:2010.0 2.5 1
Cobalt ND ug/L 09/11/16 00:31 7440-48-409/09/16 19:2010.0 2.5 1
Copper ND ug/L 09/11/16 00:31 7440-50-809/09/16 19:2010.0 2.5 1
Lead ND ug/L 09/11/16 00:31 7439-92-109/09/16 19:2010.0 2.5 1
Nickel ND ug/L 09/11/16 00:31 7440-02-009/09/16 19:2050.0 2.5 1
Selenium ND ug/L 09/11/16 00:31 7782-49-209/09/16 19:2010.0 5.0 1
Silver ND ug/L 09/11/16 00:31 7440-22-409/09/16 19:2010.0 2.5 1
Thallium ND ug/L 09/11/16 00:31 7440-28-009/09/16 19:205.5 5.0 1
Tin 2.9J ug/L 09/11/16 00:31 7440-31-509/09/16 19:201002.5 1
Vanadium ND ug/L 09/11/16 00:31 7440-62-209/09/16 19:2025.0 2.5 1
Zinc 6.1J ug/L 09/11/16 00:31 7440-66-6 B09/09/16 19:2010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/09/16 12:49 7439-97-609/09/16 02:450.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 06:37 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 06:37 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 06:37 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 06:37 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 06:37 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 06:37 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 06:37 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 06:37 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 06:37 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 06:37 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 06:37 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 06:37 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 06:37 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 06:37 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 06:37 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 06:37 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 06:37 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 06:37 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 06:37 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 06:37 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 06:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 06:37 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 06:37 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 06:37 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 06:37 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:EB Lab ID:92311096001 Collected:09/01/16 17:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 06:37 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 06:37 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 06:37 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 06:37 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 06:37 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 06:37 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 06:37 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 06:37 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 06:37 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 06:37 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 06:37 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 06:37 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 06:37 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 06:37 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 06:37 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 06:37 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 06:37 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 06:37 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 06:37 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 06:37 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 06:37 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 06:37 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 06:37 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 06:37 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 06:37 107-12-01503.6 1
Styrene ND ug/L 09/08/16 06:37 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 06:37 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 06:37 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 06:37 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 06:37 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 06:37 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 06:37 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 06:37 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 06:37 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 06:37 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 06:37 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 06:37 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 06:37 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 06:37 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 06:37 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 06:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 06:37 17060-07-070-130 1
Toluene-d8 (S)101 %09/08/16 06:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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[phone]
Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:FB Lab ID:92311096002 Collected:09/01/16 17:15 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/11/16 00:34 7440-36-009/09/16 19:206.0 3.8 1
Arsenic ND ug/L 09/11/16 00:34 7440-38-209/09/16 19:2010.0 2.5 1
Barium ND ug/L 09/11/16 00:34 7440-39-309/09/16 19:201002.5 1
Beryllium ND ug/L 09/11/16 00:34 7440-41-709/09/16 19:201.0 0.50 1
Cadmium ND ug/L 09/11/16 00:34 7440-43-909/09/16 19:201.0 0.50 1
Chromium ND ug/L 09/11/16 00:34 7440-47-309/09/16 19:2010.0 2.5 1
Cobalt ND ug/L 09/11/16 00:34 7440-48-409/09/16 19:2010.0 2.5 1
Copper ND ug/L 09/11/16 00:34 7440-50-809/09/16 19:2010.0 2.5 1
Lead ND ug/L 09/11/16 00:34 7439-92-109/09/16 19:2010.0 2.5 1
Nickel ND ug/L 09/11/16 00:34 7440-02-009/09/16 19:2050.0 2.5 1
Selenium ND ug/L 09/11/16 00:34 7782-49-209/09/16 19:2010.0 5.0 1
Silver ND ug/L 09/11/16 00:34 7440-22-409/09/16 19:2010.0 2.5 1
Thallium ND ug/L 09/11/16 00:34 7440-28-009/09/16 19:205.5 5.0 1
Tin 3.6J ug/L 09/11/16 00:34 7440-31-509/09/16 19:201002.5 1
Vanadium ND ug/L 09/11/16 00:34 7440-62-209/09/16 19:2025.0 2.5 1
Zinc 7.3J ug/L 09/11/16 00:34 7440-66-6 B09/09/16 19:2010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 09/09/16 13:01 7439-97-609/09/16 02:450.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 06:54 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 06:54 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 06:54 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 06:54 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 06:54 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 06:54 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 06:54 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 06:54 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 06:54 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 06:54 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 06:54 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 06:54 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 06:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 06:54 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 06:54 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 06:54 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 06:54 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 06:54 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 06:54 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 06:54 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 06:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 06:54 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 06:54 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 06:54 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 06:54 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:FB Lab ID:92311096002 Collected:09/01/16 17:15 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 06:54 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 06:54 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 06:54 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 06:54 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 06:54 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 06:54 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 06:54 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 06:54 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 06:54 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 06:54 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 06:54 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 06:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 06:54 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 06:54 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 06:54 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 06:54 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 06:54 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 06:54 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 06:54 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 06:54 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 06:54 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 09/08/16 06:54 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 06:54 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 06:54 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 06:54 107-12-01503.6 1
Styrene ND ug/L 09/08/16 06:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 06:54 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 06:54 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 06:54 127-18-41.0 0.46 1
Tetrahydrofuran 3.7J ug/L 09/08/16 06:54 109-99-910.0 3.1 1
Toluene ND ug/L 09/08/16 06:54 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 06:54 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 06:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 06:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 06:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 06:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 06:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 06:54 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 06:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 06:54 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 06:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %09/08/16 06:54 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 06:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:TB Lab ID:92311096003 Collected:09/01/16 00:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 07:11 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 07:11 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 07:11 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 07:11 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 07:11 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 07:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 07:11 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 07:11 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 07:11 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 07:11 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 07:11 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 07:11 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 07:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 07:11 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 07:11 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 07:11 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 07:11 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 07:11 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 07:11 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 07:11 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 07:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 07:11 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 07:11 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 07:11 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 07:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 07:11 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 07:11 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 07:11 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 07:11 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 07:11 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 07:11 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 07:11 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 07:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 07:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 07:11 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 07:11 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 07:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 07:11 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 07:11 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 07:11 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 07:11 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 07:11 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 07:11 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 07:11 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 07:11 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 07:11 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Sample:TB Lab ID:92311096003 Collected:09/01/16 00:00 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 07:11 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 07:11 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 07:11 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 07:11 107-12-01503.6 1
Styrene ND ug/L 09/08/16 07:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 07:11 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 07:11 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 07:11 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 07:11 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 07:11 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 07:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 07:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 07:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 07:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 07:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 07:11 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 07:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 07:11 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 07:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 07:11 17060-07-070-130 1
Toluene-d8 (S)105 %09/08/16 07:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327540
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92311096001, 92311096002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814951
Associated Lab Samples:92311096001, 92311096002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 09/09/16 12:280.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814952LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814953MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311075001
1814954
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 48 75-12596 66 252.5ND 1.2 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327945
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92311096001, 92311096002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1817217
Associated Lab Samples:92311096001, 92311096002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/11/16 00:033.8
Arsenic ug/L 6.5J 10.0 09/11/16 00:032.5
Barium ug/L ND 100 09/11/16 00:032.5
Beryllium ug/L ND 1.0 09/11/16 00:030.50
Cadmium ug/L ND 1.0 09/11/16 00:030.50
Chromium ug/L ND 10.0 09/11/16 00:032.5
Cobalt ug/L ND 10.0 09/11/16 00:032.5
Copper ug/L ND 10.0 09/11/16 00:032.5
Lead ug/L ND 10.0 09/11/16 00:032.5
Nickel ug/L ND 50.0 09/11/16 00:032.5
Selenium ug/L ND 10.0 09/11/16 00:035.0
Silver ug/L ND 10.0 09/11/16 00:032.5
Thallium ug/L ND 5.5 09/11/16 00:035.0
Tin ug/L ND 100 09/11/16 00:032.5
Vanadium ug/L ND 25.0 09/11/16 00:032.5
Zinc ug/L 6.2J 10.0 09/11/16 00:035.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1817218LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 502500 100 80-120
Arsenic ug/L 497500 99 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 520500 104 80-120
Cadmium ug/L 508500 102 80-120
Chromium ug/L 519500 104 80-120
Cobalt ug/L 518500 104 80-120
Copper ug/L 522500 104 80-120
Lead ug/L 510500 102 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 255250 102 80-120
Thallium ug/L 512500 102 80-120
Tin ug/L 513500 103 80-120
Vanadium ug/L 510500 102 80-120
Zinc ug/L 530500 106 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1817219MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92310738018
1817220
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12597 0 25500ND486484
Arsenic ug/L 500 98 75-12598 0 25500ND491492
Barium ug/L 500 97 75-12598 1 25500415899905
Beryllium ug/L 500 100 75-125101 0 25500ND502504
Cadmium ug/L 500 98 75-12598 0 255002.3 493 494
Chromium ug/L 500 99 75-125100 0 25500ND497498
Cobalt ug/L 500 99 75-12599 0 25500ND499499
Copper ug/L 500 101 75-125101 0 25500ND509510
Lead ug/L 500 98 75-12597 0 25500ND490489
Nickel ug/L 500 97 75-12597 0 25500ND486486
Selenium ug/L 500 100 75-125100 0 25500ND500502
Silver ug/L 250 98 75-12599 1 25250ND246247
Thallium ug/L 500 97 75-12597 0 25500ND487487
Tin ug/L 500 98 75-12598 0 25500ND494494
Vanadium ug/L 500 99 75-12599 0 25500ND495497
Zinc ug/L 500 101 75-125101 0 2550018.5 524 524
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311096001, 92311096002, 92311096003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311096001, 92311096002, 92311096003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/08/16 00:010.33
1,1,1-Trichloroethane ug/L ND 1.0 09/08/16 00:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/08/16 00:010.40
1,1,2-Trichloroethane ug/L ND 1.0 09/08/16 00:010.29
1,1-Dichloroethane ug/L ND 5.0 09/08/16 00:010.32
1,1-Dichloroethene ug/L ND 5.0 09/08/16 00:010.56
1,1-Dichloropropene ug/L ND 5.0 09/08/16 00:010.49
1,2,3-Trichloropropane ug/L ND 1.0 09/08/16 00:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/08/16 00:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/08/16 00:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/16 00:010.27
1,2-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.30
1,2-Dichloroethane ug/L ND 1.0 09/08/16 00:010.24
1,2-Dichloropropane ug/L ND 1.0 09/08/16 00:010.27
1,3-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.24
1,3-Dichloropropane ug/L ND 1.0 09/08/16 00:010.28
1,4-Dichlorobenzene ug/L ND 1.0 09/08/16 00:010.33
2,2-Dichloropropane ug/L ND 15.0 09/08/16 00:010.13
2-Butanone (MEK)ug/L ND 100 09/08/16 00:010.96
2-Hexanone ug/L ND 50.0 09/08/16 00:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/08/16 00:010.33
Acetone ug/L ND 100 09/08/16 00:0110.0
Acetonitrile ug/L ND 55.0 09/08/16 00:012.2
Acrolein ug/L ND 53.0 09/08/16 00:011.6
Acrylonitrile ug/L ND 200 09/08/16 00:011.9
Allyl chloride ug/L ND 10.0 09/08/16 00:011.5
Benzene ug/L ND 1.0 09/08/16 00:010.25
Bromochloromethane ug/L ND 3.0 09/08/16 00:010.17
Bromodichloromethane ug/L ND 1.0 09/08/16 00:010.18
Bromoform ug/L ND 3.0 09/08/16 00:010.26
Bromomethane ug/L ND 10.0 09/08/16 00:010.29
Carbon disulfide ug/L ND 100 09/08/16 00:011.2
Carbon tetrachloride ug/L ND 1.0 09/08/16 00:010.25
Chlorobenzene ug/L ND 3.0 09/08/16 00:010.23
Chloroethane ug/L ND 10.0 09/08/16 00:010.54
Chloroform ug/L ND 5.0 09/08/16 00:010.14
Chloromethane ug/L ND 1.0 09/08/16 00:010.11
Chloroprene ug/L ND 20.0 09/08/16 00:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.13
Dibromochloromethane ug/L ND 3.0 09/08/16 00:010.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311096001, 92311096002, 92311096003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 09/08/16 00:010.21
Dichlorodifluoromethane ug/L ND 5.0 09/08/16 00:010.21
Ethyl methacrylate ug/L ND 10.0 09/08/16 00:010.20
Ethylbenzene ug/L ND 1.0 09/08/16 00:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/08/16 00:010.71
Iodomethane ug/L ND 10.0 09/08/16 00:010.32
Isobutanol ug/L ND 100 09/08/16 00:0135.0
Methacrylonitrile ug/L ND 100 09/08/16 00:010.93
Methyl methacrylate ug/L ND 30.0 09/08/16 00:012.0
Methylene Chloride ug/L ND 1.0 09/08/16 00:010.97
Naphthalene ug/L ND 10.0 09/08/16 00:010.24
Propionitrile ug/L ND 150 09/08/16 00:013.6
Styrene ug/L ND 1.0 09/08/16 00:010.26
Tetrachloroethene ug/L ND 1.0 09/08/16 00:010.46
Tetrahydrofuran ug/L ND 10.0 09/08/16 00:013.1
Toluene ug/L ND 1.0 09/08/16 00:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/08/16 00:011.0
Trichloroethene ug/L ND 1.0 09/08/16 00:010.47
Trichlorofluoromethane ug/L ND 1.0 09/08/16 00:010.20
Vinyl acetate ug/L ND 50.0 09/08/16 00:010.35
Vinyl chloride ug/L ND 1.0 09/08/16 00:010.62
Xylene (Total)ug/L ND 5.0 09/08/16 00:010.66
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/16 00:01
4-Bromofluorobenzene (S)%101 70-130 09/08/16 00:01
Toluene-d8 (S)%103 70-130 09/08/16 00:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 80-125
1,1,1-Trichloroethane ug/L 54.750 109 71-129
1,1,2,2-Tetrachloroethane ug/L 53.850 108 79-124
1,1,2-Trichloroethane ug/L 53.150 106 85-125
1,1-Dichloroethane ug/L 54.750 109 73-126
1,1-Dichloroethene ug/L 59.450 119 66-135
1,1-Dichloropropene ug/L 56.350 113 74-135
1,2,3-Trichloropropane ug/L 54.150 108 75-130
1,2,4-Trichlorobenzene ug/L 56.550 113 75-134
1,2-Dibromo-3-chloropropane ug/L 52.050 104 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 57.850 116 80-133
1,2-Dichloroethane ug/L 54.050 108 67-128
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 53.150 106 75-132
1,3-Dichlorobenzene ug/L 57.650 115 77-130
1,3-Dichloropropane ug/L 54.250 108 76-131
1,4-Dichlorobenzene ug/L 55.150 110 78-130
2,2-Dichloropropane ug/L 53.350 107 40-160
2-Butanone (MEK)ug/L 133100 133 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 158 L010015848-146
Acetonitrile ug/L 623500 125 62-150
Acrolein ug/L 307 F325012324-160
Acrylonitrile ug/L 297250 119 40-160
Allyl chloride ug/L 55.550 111 66-137
Benzene ug/L 55.650 111 80-125
Bromochloromethane ug/L 59.350 119 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 53.7 F35010740-160
Carbon disulfide ug/L 74.3J F35014950-160
Carbon tetrachloride ug/L 58.250 116 69-131
Chlorobenzene ug/L 55.950 112 81-122
Chloroethane ug/L 55.850 112 39-148
Chloroform ug/L 53.150 106 73-127
Chloromethane ug/L 52.150 104 44-146
Chloroprene ug/L 57.250 114 75-145
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
cis-1,3-Dichloropropene ug/L 57.450 115 72-132
Dibromochloromethane ug/L 57.550 115 78-125
Dibromomethane ug/L 52.150 104 82-120
Dichlorodifluoromethane ug/L 51.750 103 34-157
Ethyl methacrylate ug/L 56.750 113 82-121
Ethylbenzene ug/L 54.250 108 79-121
Hexachloro-1,3-butadiene ug/L 57.750 115 72-131
Iodomethane ug/L 124100 124 39-154
Isobutanol ug/L 15401000 154 34-160
Methacrylonitrile ug/L 606500 121 74-134
Methyl methacrylate ug/L 57.650 115 84-124
Methylene Chloride ug/L 58.550 117 64-133
Naphthalene ug/L 55.150 110 73-133
Propionitrile ug/L 620500 124 73-140
Styrene ug/L 56.350 113 84-126
Tetrachloroethene ug/L 54.450 109 78-122
Tetrahydrofuran ug/L 609500 122 69-148
Toluene ug/L 54.550 109 80-121
trans-1,2-Dichloroethene ug/L 55.850 112 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
trans-1,4-Dichloro-2-butene ug/L 92.9J F3,L05018640-160
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 55.550 111 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 123100 123 40-160
Vinyl chloride ug/L 52.350 105 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,1-Dichloropropene ug/L 21.620 108 70-130ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.820 114 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 19.720 99 70-130ND
1,2-Dichloropropane ug/L 21.120 106 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,3-Dichloropropane ug/L 20.320 101 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2,2-Dichloropropane ug/L 22.820 114 70-130ND
2-Butanone (MEK)ug/L 39.8J40 99 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.1J40 98 70-130ND
Acetone ug/L 37.7J40 73 70-130ND
Acetonitrile ug/L 186200 93 70-130ND
Acrolein ug/L 115100 115 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 20.720 104 70-130ND
Benzene ug/L 21.920 109 70-148ND
Bromochloromethane ug/L 21.120 105 70-130ND
Bromodichloromethane ug/L 20.920 104 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
Chloroprene ug/L 22.020 110 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 108 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 20.320 101 70-130ND
Dichlorodifluoromethane ug/L 13.5 M1206870-130ND
Ethyl methacrylate ug/L 20.620 103 70-130ND
Ethylbenzene ug/L 21.120 106 70-130ND
Hexachloro-1,3-butadiene ug/L 24.220 121 70-130ND
Iodomethane ug/L 40.040 100 70-130ND
Isobutanol ug/L 423400 106 70-130ND
Methacrylonitrile ug/L 205200 102 70-130ND
Methyl methacrylate ug/L 21.0J20 105 70-130ND
Methylene Chloride ug/L 18.620 93 70-130ND
Naphthalene ug/L 20.620 103 70-130ND
Propionitrile ug/L 205200 103 70-130ND
Styrene ug/L 21.820 109 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Tetrahydrofuran ug/L 205200 101 70-130ND
Toluene ug/L 21.420 103 70-1550.76J
trans-1,2-Dichloroethene ug/L 21.520 107 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 22.620 113 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 39.8J40 100 70-130ND
Vinyl chloride ug/L 18.220 91 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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[phone]
Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L 0.66J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 7105
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%108 6102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
Pace Analytical Services, Inc.
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[phone]
Page 20 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311096
WAYNE MSWLF BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311096001 327945 328067EBEPA 3010A EPA 6010
92311096002 327945 328067FBEPA 3010A EPA 6010
92311096001 327540 327557EBEPA 7470 EPA 7470
92311096002 327540 327557FBEPA 7470 EPA 7470
92311096001 327693EBEPA 8260
92311096002 327693FBEPA 8260
92311096003 327693TBEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/13/2016 05:02 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 24
Page 23 of 24
Page 24 of 24
#=CL#
September 09, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311098
92311098
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Wayne Closed MSWLF SW-ByMW-2
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Huntersville, NC 28078
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 17
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Lab ID Sample ID Matrix Date Collected Date Received
92311098001 SW-ByMW-2 Water 09/01/16 14:40 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
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Page 3 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311098001 SW-ByMW-2 EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Sample:SW-ByMW-2 Lab ID:92311098001 Collected:09/01/16 14:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 08:37 67-64-1 L310010.0 1
Acetonitrile ND ug/L 09/08/16 08:37 75-05-855.0 2.2 1
Acrolein ND ug/L 09/08/16 08:37 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 09/08/16 08:37 107-13-12001.9 1
Allyl chloride ND ug/L 09/08/16 08:37 107-05-110.0 1.5 1
Benzene ND ug/L 09/08/16 08:37 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 08:37 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 08:37 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 08:37 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 08:37 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 08:37 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 08:37 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 08:37 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 08:37 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 08:37 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 08:37 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 08:37 74-87-31.0 0.11 1
Chloroprene ND ug/L 09/08/16 08:37 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 08:37 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 08:37 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 08:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 08:37 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 08:37 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 09/08/16 08:37 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 09/08/16 08:37 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 08:37 110-57-6 L31001.0 1
Dichlorodifluoromethane ND ug/L 09/08/16 08:37 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 09/08/16 08:37 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 08:37 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 08:37 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 08:37 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 08:37 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 08:37 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 09/08/16 08:37 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 09/08/16 08:37 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 09/08/16 08:37 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 08:37 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 08:37 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 09/08/16 08:37 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 09/08/16 08:37 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 09/08/16 08:37 87-68-310.0 0.71 1
2-Hexanone ND ug/L 09/08/16 08:37 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 08:37 74-88-410.0 0.32 1
Isobutanol ND ug/L 09/08/16 08:37 78-83-110035.0 1
Methacrylonitrile ND ug/L 09/08/16 08:37 126-98-71000.93 1
Methylene Chloride ND ug/L 09/08/16 08:37 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
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Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Sample:SW-ByMW-2 Lab ID:92311098001 Collected:09/01/16 14:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 09/08/16 08:37 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 08:37 108-10-11000.33 1
Naphthalene ND ug/L 09/08/16 08:37 91-20-310.0 0.24 1
Propionitrile ND ug/L 09/08/16 08:37 107-12-01503.6 1
Styrene ND ug/L 09/08/16 08:37 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 08:37 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 08:37 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 08:37 127-18-41.0 0.46 1
Toluene ND ug/L 09/08/16 08:37 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 09/08/16 08:37 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 09/08/16 08:37 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 08:37 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 08:37 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 08:37 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 08:37 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 08:37 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 08:37 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 08:37 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %09/08/16 08:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %09/08/16 08:37 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 08:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 6 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311098001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311098001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/08/16 00:010.33
1,1,1-Trichloroethane ug/L ND 1.0 09/08/16 00:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/08/16 00:010.40
1,1,2-Trichloroethane ug/L ND 1.0 09/08/16 00:010.29
1,1-Dichloroethane ug/L ND 5.0 09/08/16 00:010.32
1,1-Dichloroethene ug/L ND 5.0 09/08/16 00:010.56
1,1-Dichloropropene ug/L ND 5.0 09/08/16 00:010.49
1,2,3-Trichloropropane ug/L ND 1.0 09/08/16 00:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 09/08/16 00:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/08/16 00:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/16 00:010.27
1,2-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.30
1,2-Dichloroethane ug/L ND 1.0 09/08/16 00:010.24
1,2-Dichloropropane ug/L ND 1.0 09/08/16 00:010.27
1,3-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.24
1,3-Dichloropropane ug/L ND 1.0 09/08/16 00:010.28
1,4-Dichlorobenzene ug/L ND 1.0 09/08/16 00:010.33
2,2-Dichloropropane ug/L ND 15.0 09/08/16 00:010.13
2-Butanone (MEK)ug/L ND 100 09/08/16 00:010.96
2-Hexanone ug/L ND 50.0 09/08/16 00:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/08/16 00:010.33
Acetone ug/L ND 100 09/08/16 00:0110.0
Acetonitrile ug/L ND 55.0 09/08/16 00:012.2
Acrolein ug/L ND 53.0 09/08/16 00:011.6
Acrylonitrile ug/L ND 200 09/08/16 00:011.9
Allyl chloride ug/L ND 10.0 09/08/16 00:011.5
Benzene ug/L ND 1.0 09/08/16 00:010.25
Bromochloromethane ug/L ND 3.0 09/08/16 00:010.17
Bromodichloromethane ug/L ND 1.0 09/08/16 00:010.18
Bromoform ug/L ND 3.0 09/08/16 00:010.26
Bromomethane ug/L ND 10.0 09/08/16 00:010.29
Carbon disulfide ug/L ND 100 09/08/16 00:011.2
Carbon tetrachloride ug/L ND 1.0 09/08/16 00:010.25
Chlorobenzene ug/L ND 3.0 09/08/16 00:010.23
Chloroethane ug/L ND 10.0 09/08/16 00:010.54
Chloroform ug/L ND 5.0 09/08/16 00:010.14
Chloromethane ug/L ND 1.0 09/08/16 00:010.11
Chloroprene ug/L ND 20.0 09/08/16 00:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.13
Dibromochloromethane ug/L ND 3.0 09/08/16 00:010.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
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Page 7 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311098001
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 09/08/16 00:010.21
Dichlorodifluoromethane ug/L ND 5.0 09/08/16 00:010.21
Ethyl methacrylate ug/L ND 10.0 09/08/16 00:010.20
Ethylbenzene ug/L ND 1.0 09/08/16 00:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 09/08/16 00:010.71
Iodomethane ug/L ND 10.0 09/08/16 00:010.32
Isobutanol ug/L ND 100 09/08/16 00:0135.0
Methacrylonitrile ug/L ND 100 09/08/16 00:010.93
Methyl methacrylate ug/L ND 30.0 09/08/16 00:012.0
Methylene Chloride ug/L ND 1.0 09/08/16 00:010.97
Naphthalene ug/L ND 10.0 09/08/16 00:010.24
Propionitrile ug/L ND 150 09/08/16 00:013.6
Styrene ug/L ND 1.0 09/08/16 00:010.26
Tetrachloroethene ug/L ND 1.0 09/08/16 00:010.46
Toluene ug/L ND 1.0 09/08/16 00:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/08/16 00:011.0
Trichloroethene ug/L ND 1.0 09/08/16 00:010.47
Trichlorofluoromethane ug/L ND 1.0 09/08/16 00:010.20
Vinyl acetate ug/L ND 50.0 09/08/16 00:010.35
Vinyl chloride ug/L ND 1.0 09/08/16 00:010.62
Xylene (Total)ug/L ND 5.0 09/08/16 00:010.66
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/16 00:01
4-Bromofluorobenzene (S)%101 70-130 09/08/16 00:01
Toluene-d8 (S)%103 70-130 09/08/16 00:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 80-125
1,1,1-Trichloroethane ug/L 54.750 109 71-129
1,1,2,2-Tetrachloroethane ug/L 53.850 108 79-124
1,1,2-Trichloroethane ug/L 53.150 106 85-125
1,1-Dichloroethane ug/L 54.750 109 73-126
1,1-Dichloroethene ug/L 59.450 119 66-135
1,1-Dichloropropene ug/L 56.350 113 74-135
1,2,3-Trichloropropane ug/L 54.150 108 75-130
1,2,4-Trichlorobenzene ug/L 56.550 113 75-134
1,2-Dibromo-3-chloropropane ug/L 52.050 104 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 57.850 116 80-133
1,2-Dichloroethane ug/L 54.050 108 67-128
1,2-Dichloropropane ug/L 53.150 106 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 57.650 115 77-130
1,3-Dichloropropane ug/L 54.250 108 76-131
1,4-Dichlorobenzene ug/L 55.150 110 78-130
2,2-Dichloropropane ug/L 53.350 107 40-160
2-Butanone (MEK)ug/L 133100 133 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 158 L010015848-146
Acetonitrile ug/L 623500 125 62-150
Acrolein ug/L 307 F325012324-160
Acrylonitrile ug/L 297250 119 40-160
Allyl chloride ug/L 55.550 111 66-137
Benzene ug/L 55.650 111 80-125
Bromochloromethane ug/L 59.350 119 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 53.7 F35010740-160
Carbon disulfide ug/L 74.3J F35014950-160
Carbon tetrachloride ug/L 58.250 116 69-131
Chlorobenzene ug/L 55.950 112 81-122
Chloroethane ug/L 55.850 112 39-148
Chloroform ug/L 53.150 106 73-127
Chloromethane ug/L 52.150 104 44-146
Chloroprene ug/L 57.250 114 75-145
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
cis-1,3-Dichloropropene ug/L 57.450 115 72-132
Dibromochloromethane ug/L 57.550 115 78-125
Dibromomethane ug/L 52.150 104 82-120
Dichlorodifluoromethane ug/L 51.750 103 34-157
Ethyl methacrylate ug/L 56.750 113 82-121
Ethylbenzene ug/L 54.250 108 79-121
Hexachloro-1,3-butadiene ug/L 57.750 115 72-131
Iodomethane ug/L 124100 124 39-154
Isobutanol ug/L 15401000 154 34-160
Methacrylonitrile ug/L 606500 121 74-134
Methyl methacrylate ug/L 57.650 115 84-124
Methylene Chloride ug/L 58.550 117 64-133
Naphthalene ug/L 55.150 110 73-133
Propionitrile ug/L 620500 124 73-140
Styrene ug/L 56.350 113 84-126
Tetrachloroethene ug/L 54.450 109 78-122
Toluene ug/L 54.550 109 80-121
trans-1,2-Dichloroethene ug/L 55.850 112 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
trans-1,4-Dichloro-2-butene ug/L 92.9J F3,L05018640-160
Trichloroethene ug/L 55.550 111 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 123100 123 40-160
Vinyl chloride ug/L 52.350 105 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,1-Dichloropropene ug/L 21.620 108 70-130ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.820 114 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 19.720 99 70-130ND
1,2-Dichloropropane ug/L 21.120 106 70-130ND
1,3-Dichlorobenzene ug/L 21.420 107 70-130ND
1,3-Dichloropropane ug/L 20.320 101 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2,2-Dichloropropane ug/L 22.820 114 70-130ND
2-Butanone (MEK)ug/L 39.8J40 99 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.1J40 98 70-130ND
Acetone ug/L 37.7J40 73 70-130ND
Acetonitrile ug/L 186200 93 70-130ND
Acrolein ug/L 115100 115 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 20.720 104 70-130ND
Benzene ug/L 21.920 109 70-148ND
Bromochloromethane ug/L 21.120 105 70-130ND
Bromodichloromethane ug/L 20.920 104 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
Chloroprene ug/L 22.020 110 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 108 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 20.320 101 70-130ND
Dichlorodifluoromethane ug/L 13.5 M1206870-130ND
Ethyl methacrylate ug/L 20.620 103 70-130ND
Ethylbenzene ug/L 21.120 106 70-130ND
Hexachloro-1,3-butadiene ug/L 24.220 121 70-130ND
Iodomethane ug/L 40.040 100 70-130ND
Isobutanol ug/L 423400 106 70-130ND
Methacrylonitrile ug/L 205200 102 70-130ND
Methyl methacrylate ug/L 21.0J20 105 70-130ND
Methylene Chloride ug/L 18.620 93 70-130ND
Naphthalene ug/L 20.620 103 70-130ND
Propionitrile ug/L 205200 103 70-130ND
Styrene ug/L 21.820 109 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Toluene ug/L 21.420 103 70-1550.76J
trans-1,2-Dichloroethene ug/L 21.520 107 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 22.620 113 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 39.8J40 100 70-130ND
Vinyl chloride ug/L 18.220 91 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.66J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 12 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 7105
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%108 6102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 13 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 14 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311098
Wayne Closed MSWLF SW-ByMW-2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311098001 327693SW-ByMW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:39 PM
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[phone]
Page 15 of 17
Page 16 of 17
Page 17 of 17
#=CL#
September 09, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92311079
92311079
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Wayne MSWLF-SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Lab ID Sample ID Matrix Date Collected Date Received
92311079001 SW-1 Water 09/01/16 16:40 09/02/16 08:50
92311079002 SW-6 Water 09/01/16 16:55 09/02/16 08:50
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92311079001 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92311079002 SW-6 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92311079001 Collected:09/01/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:34 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:34 7440-38-209/06/16 21:0010.0 2.5 1
Barium 175 ug/L 09/07/16 23:34 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:34 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:34 7440-43-909/06/16 21:001.0 0.50 1
Chromium 3.5J ug/L 09/07/16 23:34 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:34 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:34 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:34 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:34 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:34 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:34 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:34 7440-28-009/06/16 21:005.5 5.0 1
Vanadium ND ug/L 09/07/16 23:34 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:34 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 08:03 67-64-1 L310010.0 1
Acrylonitrile ND ug/L 09/08/16 08:03 107-13-12001.9 1
Benzene ND ug/L 09/08/16 08:03 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 08:03 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 08:03 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 08:03 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 08:03 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 08:03 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 08:03 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 08:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 08:03 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 08:03 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 08:03 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 08:03 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 08:03 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 08:03 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 08:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 08:03 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 08:03 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/08/16 08:03 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 08:03 110-57-6 L31001.0 1
1,1-Dichloroethane ND ug/L 09/08/16 08:03 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 08:03 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 08:03 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 08:03 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 08:03 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 08:03 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 08:03 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 08:03 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92311079001 Collected:09/01/16 16:40 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/08/16 08:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/08/16 08:03 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 08:03 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 09/08/16 08:03 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 08:03 108-10-11000.33 1
Styrene ND ug/L 09/08/16 08:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 08:03 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 08:03 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 08:03 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 08:03 109-99-910.0 3.1 1
Toluene 0.42J ug/L 09/08/16 08:03 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/08/16 08:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 08:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 08:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 08:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 08:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 08:03 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 08:03 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 08:03 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %09/08/16 08:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/08/16 08:03 17060-07-070-130 1
Toluene-d8 (S)102 %09/08/16 08:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-6 Lab ID:92311079002 Collected:09/01/16 16:55 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 09/07/16 23:41 7440-36-009/06/16 21:006.0 3.8 1
Arsenic ND ug/L 09/07/16 23:41 7440-38-209/06/16 21:0010.0 2.5 1
Barium 166 ug/L 09/07/16 23:41 7440-39-309/06/16 21:001002.5 1
Beryllium ND ug/L 09/07/16 23:41 7440-41-709/06/16 21:001.0 0.50 1
Cadmium ND ug/L 09/07/16 23:41 7440-43-909/06/16 21:001.0 0.50 1
Chromium 3.0J ug/L 09/07/16 23:41 7440-47-309/06/16 21:0010.0 2.5 1
Cobalt ND ug/L 09/07/16 23:41 7440-48-409/06/16 21:0010.0 2.5 1
Copper ND ug/L 09/07/16 23:41 7440-50-809/06/16 21:0010.0 2.5 1
Lead ND ug/L 09/07/16 23:41 7439-92-109/06/16 21:0010.0 2.5 1
Nickel ND ug/L 09/07/16 23:41 7440-02-009/06/16 21:0050.0 2.5 1
Selenium ND ug/L 09/07/16 23:41 7782-49-209/06/16 21:0010.0 5.0 1
Silver ND ug/L 09/07/16 23:41 7440-22-409/06/16 21:0010.0 2.5 1
Thallium ND ug/L 09/07/16 23:41 7440-28-009/06/16 21:005.5 5.0 1
Vanadium ND ug/L 09/07/16 23:41 7440-62-209/06/16 21:0025.0 2.5 1
Zinc ND ug/L 09/07/16 23:41 7440-66-609/06/16 21:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 09/08/16 08:20 67-64-1 L310010.0 1
Acrylonitrile ND ug/L 09/08/16 08:20 107-13-12001.9 1
Benzene ND ug/L 09/08/16 08:20 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 09/08/16 08:20 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 09/08/16 08:20 75-27-41.0 0.18 1
Bromoform ND ug/L 09/08/16 08:20 75-25-23.0 0.26 1
Bromomethane ND ug/L 09/08/16 08:20 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 09/08/16 08:20 78-93-31000.96 1
Carbon disulfide ND ug/L 09/08/16 08:20 75-15-01001.2 1
Carbon tetrachloride ND ug/L 09/08/16 08:20 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 09/08/16 08:20 108-90-73.0 0.23 1
Chloroethane ND ug/L 09/08/16 08:20 75-00-310.0 0.54 1
Chloroform ND ug/L 09/08/16 08:20 67-66-35.0 0.14 1
Chloromethane ND ug/L 09/08/16 08:20 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/16 08:20 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 09/08/16 08:20 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/16 08:20 106-93-41.0 0.27 1
Dibromomethane ND ug/L 09/08/16 08:20 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 09/08/16 08:20 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 09/08/16 08:20 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 09/08/16 08:20 110-57-6 L31001.0 1
1,1-Dichloroethane ND ug/L 09/08/16 08:20 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 09/08/16 08:20 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 09/08/16 08:20 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 09/08/16 08:20 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 09/08/16 08:20 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 09/08/16 08:20 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 09/08/16 08:20 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 09/08/16 08:20 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Sample:SW-6 Lab ID:92311079002 Collected:09/01/16 16:55 Received:09/02/16 08:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 09/08/16 08:20 100-41-41.0 0.30 1
2-Hexanone ND ug/L 09/08/16 08:20 591-78-650.0 0.46 1
Iodomethane ND ug/L 09/08/16 08:20 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 09/08/16 08:20 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/16 08:20 108-10-11000.33 1
Styrene ND ug/L 09/08/16 08:20 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/16 08:20 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/16 08:20 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 09/08/16 08:20 127-18-41.0 0.46 1
Tetrahydrofuran ND ug/L 09/08/16 08:20 109-99-910.0 3.1 1
Toluene 0.76J ug/L 09/08/16 08:20 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 09/08/16 08:20 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 09/08/16 08:20 79-00-51.0 0.29 1
Trichloroethene ND ug/L 09/08/16 08:20 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 09/08/16 08:20 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 09/08/16 08:20 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 09/08/16 08:20 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 09/08/16 08:20 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 09/08/16 08:20 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %09/08/16 08:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/08/16 08:20 17060-07-070-130 1
Toluene-d8 (S)104 %09/08/16 08:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327495
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92311079001, 92311079002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1814776
Associated Lab Samples:92311079001, 92311079002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 09/07/16 22:513.8
Arsenic ug/L ND 10.0 09/07/16 22:512.5
Barium ug/L ND 100 09/07/16 22:512.5
Beryllium ug/L ND 1.0 09/07/16 22:510.50
Cadmium ug/L ND 1.0 09/07/16 22:510.50
Chromium ug/L ND 10.0 09/07/16 22:512.5
Cobalt ug/L ND 10.0 09/07/16 22:512.5
Copper ug/L ND 10.0 09/07/16 22:512.5
Lead ug/L ND 10.0 09/07/16 22:512.5
Nickel ug/L ND 50.0 09/07/16 22:512.5
Selenium ug/L ND 10.0 09/07/16 22:515.0
Silver ug/L ND 10.0 09/07/16 22:512.5
Thallium ug/L ND 5.5 09/07/16 22:515.0
Vanadium ug/L ND 25.0 09/07/16 22:512.5
Zinc ug/L ND 10.0 09/07/16 22:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1814777LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 463500 93 80-120
Arsenic ug/L 449500 90 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 478500 96 80-120
Copper ug/L 502500 100 80-120
Lead ug/L 471500 94 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 478500 96 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 460500 92 80-120
Vanadium ug/L 490500 98 80-120
Zinc ug/L 474500 95 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1814778MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92311078001
1814779
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 85 75-12586 0 25500ND428430
Arsenic ug/L 500 87 75-12588 1 255005.8J 443 446
Barium ug/L 500 104 75-125104 1 2550020.2J 539 542
Beryllium ug/L 500 100 75-125101 1 25500ND499503
Cadmium ug/L 500 97 75-12597 0 25500ND484485
Chromium ug/L 500 104 75-125106 2 2550020.1 541 550
Cobalt ug/L 500 95 75-12595 0 25500ND475475
Copper ug/L 500 102 75-125103 0 255003.1J 514 516
Lead ug/L 500 93 75-12593 0 255004.4J 469 469
Nickel ug/L 500 95 75-12596 1 25500ND476481
Selenium ug/L 500 92 75-12592 1 25500ND462466
Silver ug/L 250 98 75-12598 0 25250ND245245
Thallium ug/L 500 90 75-12591 1 25500ND451456
Vanadium ug/L 500 99 75-125100 1 2550028.4 524 527
Zinc ug/L 500 96 75-12596 0 25500ND482485
REPORT OF LABORATORY ANALYSIS
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Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
327693
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92311079001, 92311079002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311079001, 92311079002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/08/16 00:010.33
1,1,1-Trichloroethane ug/L ND 1.0 09/08/16 00:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 09/08/16 00:010.40
1,1,2-Trichloroethane ug/L ND 1.0 09/08/16 00:010.29
1,1-Dichloroethane ug/L ND 5.0 09/08/16 00:010.32
1,1-Dichloroethene ug/L ND 5.0 09/08/16 00:010.56
1,2,3-Trichloropropane ug/L ND 1.0 09/08/16 00:010.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 09/08/16 00:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/16 00:010.27
1,2-Dichlorobenzene ug/L ND 5.0 09/08/16 00:010.30
1,2-Dichloroethane ug/L ND 1.0 09/08/16 00:010.24
1,2-Dichloropropane ug/L ND 1.0 09/08/16 00:010.27
1,4-Dichlorobenzene ug/L ND 1.0 09/08/16 00:010.33
2-Butanone (MEK)ug/L ND 100 09/08/16 00:010.96
2-Hexanone ug/L ND 50.0 09/08/16 00:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 09/08/16 00:010.33
Acetone ug/L ND 100 09/08/16 00:0110.0
Acrylonitrile ug/L ND 200 09/08/16 00:011.9
Benzene ug/L ND 1.0 09/08/16 00:010.25
Bromochloromethane ug/L ND 3.0 09/08/16 00:010.17
Bromodichloromethane ug/L ND 1.0 09/08/16 00:010.18
Bromoform ug/L ND 3.0 09/08/16 00:010.26
Bromomethane ug/L ND 10.0 09/08/16 00:010.29
Carbon disulfide ug/L ND 100 09/08/16 00:011.2
Carbon tetrachloride ug/L ND 1.0 09/08/16 00:010.25
Chlorobenzene ug/L ND 3.0 09/08/16 00:010.23
Chloroethane ug/L ND 10.0 09/08/16 00:010.54
Chloroform ug/L ND 5.0 09/08/16 00:010.14
Chloromethane ug/L ND 1.0 09/08/16 00:010.11
cis-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.13
Dibromochloromethane ug/L ND 3.0 09/08/16 00:010.21
Dibromomethane ug/L ND 10.0 09/08/16 00:010.21
Ethylbenzene ug/L ND 1.0 09/08/16 00:010.30
Iodomethane ug/L ND 10.0 09/08/16 00:010.32
Methylene Chloride ug/L ND 1.0 09/08/16 00:010.97
Styrene ug/L ND 1.0 09/08/16 00:010.26
Tetrachloroethene ug/L ND 1.0 09/08/16 00:010.46
Tetrahydrofuran ug/L ND 10.0 09/08/16 00:013.1
Toluene ug/L ND 1.0 09/08/16 00:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 09/08/16 00:010.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1815920
Associated Lab Samples:92311079001, 92311079002
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/16 00:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 09/08/16 00:011.0
Trichloroethene ug/L ND 1.0 09/08/16 00:010.47
Trichlorofluoromethane ug/L ND 1.0 09/08/16 00:010.20
Vinyl acetate ug/L ND 50.0 09/08/16 00:010.35
Vinyl chloride ug/L ND 1.0 09/08/16 00:010.62
Xylene (Total)ug/L ND 5.0 09/08/16 00:010.66
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/16 00:01
4-Bromofluorobenzene (S)%101 70-130 09/08/16 00:01
Toluene-d8 (S)%103 70-130 09/08/16 00:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 80-125
1,1,1-Trichloroethane ug/L 54.750 109 71-129
1,1,2,2-Tetrachloroethane ug/L 53.850 108 79-124
1,1,2-Trichloroethane ug/L 53.150 106 85-125
1,1-Dichloroethane ug/L 54.750 109 73-126
1,1-Dichloroethene ug/L 59.450 119 66-135
1,2,3-Trichloropropane ug/L 54.150 108 75-130
1,2-Dibromo-3-chloropropane ug/L 52.050 104 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 57.850 116 80-133
1,2-Dichloroethane ug/L 54.050 108 67-128
1,2-Dichloropropane ug/L 53.150 106 75-132
1,4-Dichlorobenzene ug/L 55.150 110 78-130
2-Butanone (MEK)ug/L 133100 133 61-144
2-Hexanone ug/L 122100 122 68-143
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 158 L010015848-146
Acrylonitrile ug/L 297250 119 40-160
Benzene ug/L 55.650 111 80-125
Bromochloromethane ug/L 59.350 119 71-125
Bromodichloromethane ug/L 53.450 107 78-124
Bromoform ug/L 49.550 99 71-128
Bromomethane ug/L 53.7 F35010740-160
Carbon disulfide ug/L 74.3J F35014950-160
Carbon tetrachloride ug/L 58.250 116 69-131
Chlorobenzene ug/L 55.950 112 81-122
Chloroethane ug/L 55.850 112 39-148
Chloroform ug/L 53.150 106 73-127
Chloromethane ug/L 52.150 104 44-146
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1815921LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,3-Dichloropropene ug/L 57.450 115 72-132
Dibromochloromethane ug/L 57.550 115 78-125
Dibromomethane ug/L 52.150 104 82-120
Ethylbenzene ug/L 54.250 108 79-121
Iodomethane ug/L 124100 124 39-154
Methylene Chloride ug/L 58.550 117 64-133
Styrene ug/L 56.350 113 84-126
Tetrachloroethene ug/L 54.450 109 78-122
Tetrahydrofuran ug/L 609500 122 69-148
Toluene ug/L 54.550 109 80-121
trans-1,2-Dichloroethene ug/L 55.850 112 71-127
trans-1,3-Dichloropropene ug/L 54.650 109 69-141
trans-1,4-Dichloro-2-butene ug/L 92.9J F3,L05018640-160
Trichloroethene ug/L 55.550 111 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 123100 123 40-160
Vinyl chloride ug/L 52.350 105 58-137
Xylene (Total)ug/L 161150 107 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
1,1,1,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 21.720 109 70-166ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.720 114 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 19.720 99 70-130ND
1,2-Dichloropropane ug/L 21.120 106 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2-Butanone (MEK)ug/L 39.8J40 99 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.1J40 98 70-130ND
Acetone ug/L 37.7J40 73 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Benzene ug/L 21.920 109 70-148ND
Bromochloromethane ug/L 21.120 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1815923MATRIX SPIKE SAMPLE:
MSSpike
Result
92311079002
Bromodichloromethane ug/L 20.920 104 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 21.720 108 70-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 22.720 114 70-130ND
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 18.020 90 70-130ND
cis-1,2-Dichloroethene ug/L 21.220 106 70-130ND
cis-1,3-Dichloropropene ug/L 21.520 108 70-130ND
Dibromochloromethane ug/L 19.420 97 70-130ND
Dibromomethane ug/L 20.320 101 70-130ND
Ethylbenzene ug/L 21.120 106 70-130ND
Iodomethane ug/L 40.040 100 70-130ND
Methylene Chloride ug/L 18.620 93 70-130ND
Styrene ug/L 21.820 109 70-130ND
Tetrachloroethene ug/L 20.320 102 70-130ND
Tetrahydrofuran ug/L 205200 101 70-130ND
Toluene ug/L 21.420 103 70-1550.76J
trans-1,2-Dichloroethene ug/L 21.520 107 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 20.1J20 101 70-130ND
Trichloroethene ug/L 22.620 113 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 39.8J40 100 70-130ND
Vinyl chloride ug/L 18.220 91 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92311079001
1815922SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Tetrahydrofuran ug/L ND 30ND
Toluene ug/L 0.66J 300.42J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%98 7105
4-Bromofluorobenzene (S)%99 2101
Toluene-d8 (S)%108 6102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92311079
Wayne MSWLF-SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92311079001 327495 327550SW-1 EPA 3010A EPA 6010
92311079002 327495 327550SW-6 EPA 3010A EPA 6010
92311079001 327693SW-1 EPA 8260
92311079002 327693SW-6 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/09/2016 02:38 PM
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[phone]
Page 17 of 19
Page 18 of 19
Page 19 of 19
Appendix B
Field Sampling Parameter Data Sheet(s)