9601_WayneCounty_GWMR_DIN28164_20160211

Wayne County Active C&D and Closed MSWLF
Dudley, North Carolina
February 2015
MESCO Project Number: G15016.0
Semi-Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Municipal Engineering Services Company, P.A.
Garner and Boone, North Carolina
P.O. Box 97
Garner, NC 27529
License No. C-0281

Permit Number: 96-01
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 2
Field Parameter Data Page 2
Laboratory Results Page 3
Quality Control Samples Page 3
Groundwater Samples Page 3
Surface Water Samples Page 3
Corrective Action Update Page 3
Groundwater and Surface Water Characterization Page 4
Findings Page 4
Closing Page 4
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer w/ VOC Detection Above 2L Standard Figure 2
Time-Series Graphs of Select Constituents Figure 3
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, or 2B (Appendix 1) Table 5
MNA Parameter Data Summary Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
APPENDIX
Laboratory Analysis Reports and Chains of Custody Appendix A
August 4, 2016
Ms. Jaclynne Drummond
Solid Waste Section
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update
Wayne County Active C&D and Closed MSWLF (Dudley)
Permit No. 96-01
MESCO Project No. G15016.0
Event Date(s): February 11-12, 2015
Dear Ms. Drummond,
Introduction
The Wayne County landfill (Permit #96-01) is located at 460 S Landfill Road (SR 1129), Dudley, Wayne County,
North Carolina. A topographic map showing the location of the site is included as Figure 1.
The Wayne County unlined closed Municipal Solid Waste Landfill (MSWLF) and active Construction and Demolition
(C&D) Landfill located in Dudley NC, currently operating under Permit #96-01 is required to submit semi-annual
compliance reports as a condition of 15A NCAC 13B.1630. This report documents the quality of the ground and
surface waters during this monitoring event performed on February 11-12, 2015. Laboratory analytical results indicate
that no constituents attributed to anthropogenic sources were detected in concentrations exceeding regulatory
Standards for the first time since August 2007. Corrective action via monitored natural attenuation (MNA) is planned
to continue.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and a recent SWS
memorandum this report contains sampling procedures, field and laboratory results, corrective action update,
ground/surface water characterization, and findings. Well construction summary table, field observations table, field
parameter data table, sampling and analysis summary table, detections compared to Standards tables, a groundwater
flow directions/rates table, potentiometric map, time-series graph, quality assurance/quality control data, and
laboratory analytical data results are enclosed herein.
Background
Prior to operating as a C&D landfill the site operated as a Municipal Solid Waste (MSW) unlined sanitary landfill that
consisted of two units. The first unit (Unit 1) was closed prior to October 1991 with a 24 inch final soil cover. The
second unit (Unit 2) was closed with a low permeability cohesive cap and erosive layer prior to December 31, 1998 in
accordance with the Transition Plan. The C&D landfill is operating on top of the Unit 2 MSW landfill. The separate
active Subtitle D Lined MSWLF (permit #96-06), located adjacent to the C&D landfill across the unnamed tributary of
Edward's Branch, was monitored in conjunction with this site but reported separately.

Water quality at this landfill has been monitored at least semi-annually since 1991. Current data was compared to data
compiled since 1994 in support of this report. Municipal Engineering Services Company, P.A. (MESCO) submitted an
Assessment and Corrective Action (ACM) [DIN8821] report dated August 30, 2007 which was approved by the NC Solid
Waste Section (SWS) on November 1, 2007 [DIN3328]. MESCO then developed a Corrective Action Plan (CAP)
[DIN8821] on October 22, 2009 which was approved by the SWS on October 23, 2009 [DIN8822]. Groundwater
remediation using Monitored Natural Attenuation (MNA) was initiated on August 6, 2009 and has continued on a semi-
annual basis. Following establishment of the two year MNA baseline, MESCO completed a Corrective Action
Evaluation Report (CAER) [DIN 13923] on May 10, 2011. The CAER was reviewed and the proposed modifications of
MNA parameters and frequency were approved by the SWS [DIN 16967].
Background well MW-1 was abandoned and replaced by MW-1R as pre-authorized by SWS [DIN 19050] on June 4,
2013. MESCO submitted a Request for Appendix II Groundwater Monitoring Modification dated April 24, 2014 which
was approved by the SWS. The Water Quality Sampling and Analysis Plan (SAP) which provides for a subset of wells to
decrease Appendix II monitoring frequency was revised and submitted on December 15, 2014 as requested by Ms.
Christine Ritter of the SWS. Groundwater remediation through MNA per the CAP is scheduled to continue provided
there is no change directed by the SWS.
Sampling Procedure
MESCO performed this sampling event utilizing portable monitoring methodology in accordance with the approved SAP
based on the NCDENR SWS guidance document Solid Waste Section Guidelines for Groundwater, Soil, and Surface
Water Sampling revised April 2008. The new site-specific SAP entails continued semi-annual water quality monitoring
which includes annual corrective action monitoring and targeting of specific Appendix II constituents at a subset of wells
once every three years. Keeping with the historical schedule this event consists of detection monitoring (Appendix I) at
all locations and corrective action monitoring via select MNA performance parameters at MW-2, MW-8 and background
well MW-1R. Water samples were collected from monitoring locations designated in the SAP with the exception of SW-
2 and SW-3, which were dry. Water quality monitoring was performed on ten wells (MW-2, MW-3, MW-4, MW-5,
MW-6, MW-7, MW-8, MW-9, MW-10 and MW-11), one background well (MW-1R) and one surface water point (SW-
1). Quality control measures implemented during this event included quantification of an equipment blank (EB), field
blank (FB) and travel blank (TB). A supplemental surface water sample (SW-By_MW-2) was collected from the western
tributary of Edward's Branch directly downgradient of MW-2. Data from two surface water locations from the Subtitle D
Lined SAP SW-2 (shared) and SW-3 (shared) are presented because this local discharge feature is shared by both permits.
Monitoring locations are depicted on the potentiometric map, included as Figure 2.
This semi-annual event consisted of targeting constituents listed in 40 CFR Appendix I and full SWS recommended
MNA performance parameters. Water samples were collected from monitoring locations designated in the SAP with the
exception of SW-2 and SW-3, which were dry. Water quality monitoring was performed on ten wells (MW-2, MW-3,
MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-10 and MW-11), one background well (MW-1R) and one surface
water point (SW-1). Quality control measures implemented during this event included quantification of an equipment
blank (EB), field blank (FB) and travel blank (TB). A supplemental surface water sample (SW-By_MW-2) was collected
from the western tributary of Edward's Branch directly downgradient of MW-2. Data from two surface water locations
from the Subtitle D Lined SAP SW-2 (shared) and SW-3 (shared) are presented because this local discharge feature is
shared by both permits. Monitoring locations are depicted on the potentiometric map, included as Figure 2.
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and integrity
of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table 2. The depth
to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low-flow
pumping methodology or bailing was utilized to adequately purge the wells a minimum of three times the volume of
standing water in the well or until dry. Surface water samples were dipped from the surface of the creeks at previously
designated locations. Samples were then placed into laboratory-prepared, pre-preserved containers. Samples were kept
on ice and transported to a NC-certified laboratory under proper chain of custody (C-O-C) protocol and analyzed within
the required hold times.
2
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature,
dissolved oxygen (DO), oxidation reduction potential (ORP), dissolved carbon dioxide (CO2), total dissolved solids
(TDS) and turbidity. A summary of the field parameter data is presented in Table 3.
Laboratory Results
Pace Analytical Laboratories (PACE) performed the laboratory analysis. All samples were analyzed for Appendix I
constituents listed in 40 CFR 258. Additionally, the prescribed MNA performance parameters were quantified from
samples collected from MW-2, MW-8 and background well MW-1R. A sampling and analysis table summarizing the
locations, targeted constituents and methods is presented as Table 4. Laboratory results and C-O-Cs are contained in
Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below the
current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and surface water
samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North Carolina
Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a Class C waterbody and
Maximum Contaminant Levels (MCL) also known as “Federal Primary Drinking Water Standards”.
Quality Control Samples
Cis-1,2-dichlroethene was detected in non-quantifiable (“j-qualified”) levels in all blanks (EB, FB, TB). Since cis-1,2-
dichroloethene was not detected in any ground or surface water samples above regulatory Standards, any potential
field/lab induced artifact contamination is non-consequential.
Groundwater Samples
Total metals detected in excess of their respective 2L Standards were cadmium in MW-11 [2.8 µg/L / (2L Standard of 2.0
µg/L)] and chromium in hydraulically upgradient background well MW-1R [(27.3 µg/L / (2L Standard of 10 µg/L)].
Total vanadium was detected in MW-2 (9.3j µg/L), MW-5 (10j µg/L), MW-9 (6.2j µg/L), MW-11 (3.6j µg/L) and
hydraulically upgradient background well MW-1R (38.8 µg/L) which were above the GWP (3.5 µg/L).
During this event benzene was detected in sample MW-2 at 0.31j µg/L which is below the SWSL and 2L Standard (1.0
µg/L) after being consistently reported in excess of the 2L Standard the past seven years.
Surface Water Samples
Constituents were not detected in any surface water sample in concentrations above the established 2B Standards.
Supplemental surface water sample SW-By_MW-2 collected at the property line approximately 166 feet hydraulically
downgradient of MW-2 continues to lack Appendix II VOCs.
Corrective Action Update
Groundwater remediation measures through MNA continues to be implemented at the facility. Semi-annual MNA
monitoring of MW-2, MW-8 and background well MW-1 was initiated on August 6, 2009 and was consistently
performed for the full suite of SWS recommended parameters for six consecutive semi-annual events. The SAP
prescribes MNA monitoring to be performed annually or bi-annually depending upon specific constituents. Keeping with
established schedule the full suite of MNA parameters were analyzed during this event as presented on Table 6.
Interpretation of current MNA data continues to support previous assertions that groundwater geochemical conditions
exist that may be considered favorable for continued natural attenuation.
The active Landfill Gas Collection and Control System (GCCS) continues operations. The GCCS extracts LFG for
energy production therefore is closely maintained for optimum efficiency which may have a collateral remediation effect
on groundwater.
3
Figures
Topographic Map with Site Location
01 1 MILE
FIGURE 1
Wayne County Landfill North Carolina (Dudley)
CLOSED MSW FACILITY
SUBTITLE D MSW
LANDFILL FACILITY
460 B South Landfill Rd
Dudley, NC 28333
Lat:35-17-19.1338
Long:-78-04-17.2971
Northing:561283.19
Easting:2277068.62
N
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Figure 3
Time-Series Graphs of Select Constituents
September 8, 1994 - February 12, 2015
Non-Detects Shown at Method Detection Level.
2L
2L
2L
2L
2L NC Groundwater Standard
MCLMCL “Drinking Water Standard”
Tables
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
February 12, 2015
Latitude Longitude
(inches)(ft)
MW-1R 6/4/13 2 27.32 12.32 15 Soil Sand 169.64 166.64 150.21 19.43 35.292408 -78.064431
MW-2 8/28/90 2 15 10 5 Soil Sand 134.52 132.78 130.18 4.34 35.290714 -78.076225
MW-3 8/27/90 2 18 12 6 Soil Sand 134.81 133.03 134.81 0.00 35.293192 -78.072156
MW-4 8/28/90 2 15 10 5 Soil Sand 150.20 148.17 143.61 6.59 35.293003 -78.066253
MW-5 8/31/94 2 18 3 15 Soil Sand 124.78 120.56 122.13 2.65 35.292597 -78.075936
MW-6 8/31/94 2 18.14 3.14 15 Soil Sand 145.53 143.62 140.52 5.01 35.293439 -78.068656
MW-7 8/31/94 2 19 4 15 Soil Sand 143.59 140.74 138.68 4.91 35.288761 -78.074700
MW-8 8/30/94 2 29 14 15 Soil Sand 161.88 160.88 142.53 19.35 35.290178 -78.068706
MW-9 7/9/09 2 25 10 15 Soil Sand 162.96 159.78 144.79 18.17 35.290025 -78.068242
MW-10 7/9/09 2 25 10 15 Soil Sand 162.90 160.01 147.65 15.25 35.289869 -78.069167
MW-11 7/9/09 2 15 5 10 Soil Sand 127.23 124.50 125.26 1.97 35.291844 -78.076250
NOTE:
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
na = not available
bgs = below ground surface
amsl= above mean sea level
btoc = below top of PVC well casing
Wayne County Active C&D and Closed MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
February 12, 2015
Locked Comments
MW-1R Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes
MW-3 Yes Yes Yes Yes Yes Yes Flowing artesian
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Yes
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes
MW-8 Yes Yes Yes Yes Yes Yes
MW-9 Yes Yes No Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes Yes Artesian
SW-1 Yes -----Shared Downstream of SW-3
SW-2 No -----Dry-Upstream nearest MW-7
SW-2 Yes -----Shared nearest lined MW-2
SW-3 Yes -----Shared downstream of SW-2
SW-3 No -----Dry-Shared Upstream nearest MW-4
SW-By _MW-2 Yes -----Not required but supplemental sample
Any unusual field conditions, observations, or events:
All wells with the exception of MW-1R and MW-4 have been painted blue by the County since August 2013.
Wells have had sediment removed from concrete pads surrounding wells by County since August 2013.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Effective
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 3
Field Parameter Data Summary
February 12, 2015
Parameter Temp.ORP DO pH TDS Turbidity
Units C mg/L SU mg/L NTU or Visual
MW-1R 19.43 150.20 169.63 16.1 319 6.3 6.17 0 0 297
MW-2 4.34 130.18 134.52 14.2 -37 0.8 6.83 1410 760 210
MW-3 0.00 134.81 134.81 13.1 223 NR 5.38 0 0 Slight
MW-4 6.59 143.61 150.20 16.1 257 NR 5.91 0 0 Clear
MW-5 2.65 122.13 124.78 15.7 223 NR 5.53 100 40 Slight
MW-6 5.01 140.52 145.53 14.9 132 NR 5.31 90 40 Clear
MW-7 4.91 138.68 143.59 14.7 338 NR 5.11 10 0 Clear
MW-8 19.35 142.53 161.88 14.9 327 3.2 5.17 10 0 81
MW-9 18.17 144.79 162.96 16.2 342 NR 5.14 50 20 Moderate
MW-10 15.25 147.65 162.90 14.7 310 NR 5.21 70 30 Moderate
MW-11 1.97 125.26 127.23 10.7 127 NR 5.88 1220 610 Moderate
Minimum 0.00 122.13 124.78 10.7 -37 0.8 5.11 0 0 Clear
Average 8.88 138.21 147.09 14.7 233 3.4 5.60 269 136 Slight
Maximum 19.43 150.20 169.63 16.2 342 6.3 6.83 1410 760 Moderate
SW-1 ---8.1 NR NR 6.97 60 20 Clear
SW-2 ---7.7 NR NR 6.93 60 20 Clear
---7.5 NR NR 6.91 60 20 Clear
SW-3 ---7.9 NR NR 6.98 60 20 Clear
Minimum ---7.5 NR NR 6.91 60 20 Clear
Average ---7.8 NR NR 6.95 60 20 Clear
Maximum ---8.1 NR NR 6.98 60 20 Clear
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
SW-ByMW-2
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 4
Sampling and Analysis Summary
February 12, 2015
Field Parameter MNA
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4
MW-1R x x x x x x x x x x x x x x x x x x x x x x
MW-2 x x x x x x x x x x x x x x x x x x x x x x
MW-3 x x x x x x x
MW-4 x x x x x x x
MW-5 x x x x x x x
MW-6 x x x x x x x
MW-7 x x x x x x x
MW-8 x x x x x x x x x x x x x x x x x x x x x x x
MW-9 x x x x x x x
MW-10 x x x x x x x
MW-11 x x x x x x x
SW-1 x x x x x x
SW-2 Dry
SW-2 (shared)x x x x x x
x x x x x
SW-3 (shared)x x x x x x
SW-3 Dry
EB x x
FB x x
TB x
App. I App II
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SW-ByMW-2
App I & II = Appendix I & II List from current 40 CFR 258
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 5
Detections in Water Samples above SWSL, GWP, 2L or 2B (Appendix I)
February 11-12, 2015
Sample ID Result Unit
MW-1R Chromium, total 2/12/15 27.3 2.5 10 10 100 N & B
MW-1R Vanadium, total 2/12/15 38.8 2.5 25 3.5 NE
MW-2 Vanadium, total 2/12/15 9.3,j 2.5 25 3.5 NE
MW-2 2/12/15 5 0.23 3 50 100
MW-2 Barium, total 2/12/15 160 2.5 100 700 2000
MW-2 2/12/15 1.4 0.33 1 6 75
MW-3 Cadmium, total 2/12/15 1 0.5 1 2 5
MW-5 Vanadium, total 2/12/15 10,j 2.5 25 3.5 NE
MW-5 Zinc, total 2/12/15 11.5 5 10 1000 5000
MW-9 Cadmium, total 2/12/15 1.8 0.5 1 2 5
MW-9 Zinc, total 2/12/15 11.1 5 10 1000 5000
MW-9 Vanadium, total 2/12/15 6.2,j 2.5 25 3.5 NE
MW-10 Zinc, total 2/12/15 25.6 5 10 1000 5000
MW-10 Barium, total 2/12/15 409 2.5 100 700 2000
MW-11 Cadmium, total 2/12/15 2.8 0.5 1 2 5 N
MW-11 Vanadium, total 2/12/15 3.6,j 2.5 25 3.5 NE
MW-11 Barium, total 2/12/15 142 2.5 100 700 2000
SW-4 Zinc, total 2/11/15 15 5 10 50 5000
SW-5 Barium, total 2/11/15 320 2.5 100 200000 2000
SW-5 Zinc, total 2/11/15 18 5 10 50 5000
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
B = Background as detected hydraulically upgradient/upstream of facility
BOLD = Concentration > 2L, 2B or MCL Standard
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
Chlorobenzene ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 6
MNA Parameter Data Summary
February 12, 2015
Parameters Method MDL*Units MW-1R MW-2 MW-8
02/12/15 02/12/15 02/12/15
VFA – Acetic Acid AM23G 8 74 120 60 j
AM23G 7 <7 <7 <7
AM23G NS NS NS NS
AM23G NS NS NS NS
AM23G NS NS NS NS
VFA – Lactic Acid AM23G 12 300 590 240
AM23G NS NS NS NS
AM23G 11 <11 <11 <11
AM23G 9 <9 <9 <9
Hydrogen AM20GAX 0.13 0.82 1.3 1.8
Methane AM20GAX 0.01 1 2000 5.6
AM20GAX 0.01 <0.008 <0.008 0.1
Ethane AM20GAX 0 0.0045 j 1.2 0.05
CO2-Dissolved 0 mg/L 30 >100 >100
Alkalinity SM 2320B 1000 <1000 586000 <1000
Sulfate EPA 300.0 1000 1460 j 23700 j 2990 j
Sulfide SM 4500-S2D 100 <100 <100 <100
Chloride SM 4500-Cl-E 500 8650 60800 2590
TOC SM 5310B 500 3310 31000 1910
COD SM 5220D 12500 <12500 82000 <12500
BOD SM 5210B 2000 <2000 <2000 <2000
Iron EPA 6010 25 20900 37800 2870
Nitrate EPA 353.2 10 880 j <10 20.5 j
Temperature Field Instrument 0 Degrees C 16.1 14.2 14.9
ORP Field Instrument -900 319 -37 327
DO Field Instrument 0 6.3 0.8 3.2
pH Field Instrument 0.00 SU 6.17 6.83 5.17
Specific Conductance Field Instrument 0 0 1410 10
Turbidity Field Instrument 1.00 NTU 297 210 81
Notes:
VFA = Volatile Fatty Acids
MDL* = Lowest Method Detection Limit for Lab Parameters or Lowest Field Measurement Possible
>100 = CO2 Concentration Exceeds Maximum capability of Method Used
Constituents Below Quantization Limit are shown as <MDL value
NS = Not Sampled as not required during this specific event.
ug/L
VFA – Butyric Acid ug/L
VFA – Hexanoic Acid ug/L
VFA – i-Hexanoic Acid ug/L
VFA – i-Pentanoic Acid ug/L
ug/L
VFA – Pentaonic Acid ug/L
VFA – Propionic Acid ug/L
VFA – Pyruvic Acid ug/L
nM
ug/L
Ethene ug/L
ug/L
Field Hach Kit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mV
ug/L
uMhos
5X Chloride in MW-2 analyzed under 5x dilution (mdl = 2,500)
Wayne County Active C&D and Closed MSWLF (Dudley)Page 1 of 1
Table 7
February 12, 2015
MW-1R 20 0.006 N76W 19.43 150.21
MW-2 3.00E-04 20 0.009 14 N46W 4.34 130.18
MW-3 6.40E-03 20 0.015 506 N49W 0.00 134.81
MW-4 9.90E-04 20 0.008 39 N21W 6.59 143.61
MW-5 3.10E-05 20 0.021 3 N42W 2.65 122.13
MW-6 1.60E-04 20 0.019 16 N27W 5.01 140.52
MW-7 7.30E-05 20 0.017 7 N55W 4.91 138.68
MW-8 3.40E-04 20 0.047 83 N13E 19.35 142.53
Minimum 3.10E-05 20 0.006 3 -0.00 122.13
Average 1.18E-03 20 0.018 95 -7.79 137.83
Maximum 6.40E-03 20 0.047 506 -19.43 150.21
NOTE: Data for conductivities and effective porosity obtained from GAI Consultants' Water Sampling Report (January, 1995).
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity (%)
Hydraulic
Gradient (ft/ft)
Linear Velocity
(ft/yr)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation
(ft amsl)
na na
Hydrologic Gradient from groundwater elevations recorded on February 12, 2015.
Linear Velocity (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e
-=
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
March 04, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237750
92237750
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne Closed MSWLF (Dudley)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Report revised 3/4/15 to remove false positive 1,2-Dichloroethane detection from Method Blank #
30436.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 37
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Lab ID Sample ID Matrix Date Collected Date Received
92237750001 MW-1 Water 02/12/15 13:55 02/13/15 15:45
92237750002 MW-2 Water 02/12/15 15:35 02/13/15 15:45
92237750003 MW-3 Water 02/12/15 16:30 02/13/15 15:45
92237750004 MW-4 Water 02/12/15 13:30 02/13/15 15:45
92237750005 MW-5 Water 02/12/15 12:05 02/13/15 15:45
92237750006 MW-6 Water 02/12/15 10:10 02/13/15 15:45
92237750007 MW-7 Water 02/12/15 10:40 02/13/15 15:45
92237750008 MW-8 Water 02/12/15 14:50 02/13/15 15:45
92237750009 MW-9 Water 02/12/15 11:00 02/13/15 15:45
92237750010 MW-10 Water 02/12/15 11:20 02/13/15 15:45
92237750011 MW-11 Water 02/12/15 11:50 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 3 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237750001 MW-1 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750002 MW-2 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750003 MW-3 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750004 MW-4 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750005 MW-5 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750006 MW-6 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750007 MW-7 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750008 MW-8 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AHVK
EPA 8260 51 PASI-CGAW
92237750009 MW-9 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750010 MW-10 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237750011 MW-11 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-1 Lab ID:92237750001 Collected:02/12/15 13:55 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/18/15 23:54 7440-36-002/16/15 16:106.0 3.8 1
Arsenic 3.9J ug/L 02/18/15 23:54 7440-38-202/16/15 16:1010.0 2.5 1
Barium 23.4J ug/L 02/18/15 23:54 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/18/15 23:54 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.73J ug/L 02/18/15 23:54 7440-43-902/16/15 16:101.0 0.50 1
Chromium 27.3 ug/L 02/18/15 23:54 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/18/15 23:54 7440-48-402/16/15 16:1010.0 2.5 1
Copper 4.7J ug/L 02/18/15 23:54 7440-50-802/16/15 16:1010.0 2.5 1
Lead 7.3J ug/L 02/18/15 23:54 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/18/15 23:54 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/18/15 23:54 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/18/15 23:54 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/18/15 23:54 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 38.8 ug/L 02/18/15 23:54 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 8.1J ug/L 02/18/15 23:54 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 15:14 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 15:14 107-13-12001.9 1
Benzene ND ug/L 02/22/15 15:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 15:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 15:14 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 15:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 15:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 15:14 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 15:14 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 15:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 15:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 15:14 75-00-310.0 0.54 1
Chloroform 0.73J ug/L 02/22/15 15:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 15:14 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 15:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 15:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 15:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 15:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 15:14 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 15:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 15:14 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 15:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 15:14 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 15:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.24J ug/L 02/22/15 15:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 15:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 15:14 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 15:14 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 15:14 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-1 Lab ID:92237750001 Collected:02/12/15 13:55 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 15:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 15:14 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 15:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 15:14 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 15:14 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 15:14 108-10-11000.33 1
Styrene ND ug/L 02/22/15 15:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 15:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 15:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 15:14 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 15:14 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 15:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 15:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 15:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 15:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 15:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 15:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 15:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 15:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 15:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %02/22/15 15:14 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 15:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-2 Lab ID:92237750002 Collected:02/12/15 15:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/18/15 23:57 7440-36-002/16/15 16:106.0 3.8 1
Arsenic 6.7J ug/L 02/18/15 23:57 7440-38-202/16/15 16:1010.0 2.5 1
Barium 160 ug/L 02/18/15 23:57 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/18/15 23:57 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/18/15 23:57 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/18/15 23:57 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/18/15 23:57 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/18/15 23:57 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/18/15 23:57 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/18/15 23:57 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/18/15 23:57 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/18/15 23:57 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/18/15 23:57 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 9.3J ug/L 02/18/15 23:57 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 7.7J ug/L 02/18/15 23:57 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 18.0J ug/L 02/22/15 15:31 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 15:31 107-13-12001.9 1
Benzene 0.31J ug/L 02/22/15 15:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 15:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 15:31 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 15:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 15:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 15:31 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 15:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 15:31 56-23-51.0 0.25 1
Chlorobenzene 5.0 ug/L 02/22/15 15:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 15:31 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 15:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 15:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 15:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 15:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 15:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 15:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 15:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.4 ug/L 02/22/15 15:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 15:31 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 15:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 15:31 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 15:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 15:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 15:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 15:31 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 15:31 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 15:31 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-2 Lab ID:92237750002 Collected:02/12/15 15:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 15:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 15:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 15:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 15:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 15:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 15:31 108-10-11000.33 1
Styrene ND ug/L 02/22/15 15:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 15:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 15:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 15:31 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 15:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 15:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 15:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 15:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 15:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 15:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 15:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 15:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 15:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 15:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 15:31 17060-07-070-130 1
Toluene-d8 (S)100 %02/22/15 15:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-3 Lab ID:92237750003 Collected:02/12/15 16:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:00 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:00 7440-38-202/16/15 16:1010.0 2.5 1
Barium 17.0J ug/L 02/19/15 00:00 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:00 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.0 ug/L 02/19/15 00:00 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:00 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:00 7440-48-402/16/15 16:1010.0 2.5 1
Copper 3.3J ug/L 02/19/15 00:00 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:00 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:00 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:00 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:00 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:00 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:00 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 9.3J ug/L 02/19/15 00:00 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 15:48 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 15:48 107-13-12001.9 1
Benzene ND ug/L 02/22/15 15:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 15:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 15:48 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 15:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 15:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 15:48 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 15:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 15:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 15:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 15:48 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 15:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 15:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 15:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 15:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 15:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 15:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 15:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 15:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 15:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 15:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 15:48 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 15:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 15:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 15:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 15:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 15:48 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 15:48 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-3 Lab ID:92237750003 Collected:02/12/15 16:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 15:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 15:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 15:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 15:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 15:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 15:48 108-10-11000.33 1
Styrene ND ug/L 02/22/15 15:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 15:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 15:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 15:48 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 15:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 15:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 15:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 15:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 15:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 15:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 15:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 15:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 15:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 15:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 15:48 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 15:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-4 Lab ID:92237750004 Collected:02/12/15 13:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:03 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:03 7440-38-202/16/15 16:1010.0 2.5 1
Barium 22.6J ug/L 02/19/15 00:03 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:03 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:03 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:03 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:03 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:03 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:03 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:03 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:03 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:03 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:03 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:03 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/19/15 00:03 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 16:05 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 16:05 107-13-12001.9 1
Benzene ND ug/L 02/22/15 16:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 16:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 16:05 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 16:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 16:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 16:05 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 16:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 16:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 16:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 16:05 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 16:05 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 16:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 16:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 16:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 16:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 16:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 16:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 16:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 16:05 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 16:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 16:05 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 16:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 16:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 16:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 16:05 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 16:05 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 16:05 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-4 Lab ID:92237750004 Collected:02/12/15 13:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 16:05 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 16:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 16:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 16:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 16:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 16:05 108-10-11000.33 1
Styrene ND ug/L 02/22/15 16:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 16:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 16:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 16:05 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 16:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 16:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 16:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 16:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 16:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 16:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 16:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 16:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 16:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %02/22/15 16:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %02/22/15 16:05 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 16:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-5 Lab ID:92237750005 Collected:02/12/15 12:05 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:06 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:06 7440-38-202/16/15 16:1010.0 2.5 1
Barium 38.9J ug/L 02/19/15 00:06 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:06 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.2 ug/L 02/19/15 00:06 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:06 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:06 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:06 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:06 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:06 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:06 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:06 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:06 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 10J ug/L 02/19/15 00:06 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 11.5 ug/L 02/19/15 00:06 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 16:22 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 16:22 107-13-12001.9 1
Benzene ND ug/L 02/22/15 16:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 16:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 16:22 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 16:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 16:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 16:22 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 16:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 16:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 16:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 16:22 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 16:22 67-66-35.0 0.14 1
Chloromethane 0.22J ug/L 02/22/15 16:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 16:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 16:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 16:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 16:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 16:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 16:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 16:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 16:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 16:22 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 16:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 16:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 16:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 16:22 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 16:22 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 16:22 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-5 Lab ID:92237750005 Collected:02/12/15 12:05 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 16:22 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 16:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 16:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 16:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 16:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 16:22 108-10-11000.33 1
Styrene ND ug/L 02/22/15 16:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 16:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 16:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 16:22 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 16:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 16:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 16:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 16:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 16:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 16:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 16:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 16:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 16:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %02/22/15 16:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %02/22/15 16:22 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 16:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-6 Lab ID:92237750006 Collected:02/12/15 10:10 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:09 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:09 7440-38-202/16/15 16:1010.0 2.5 1
Barium 85.3J ug/L 02/19/15 00:09 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:09 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:09 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:09 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:09 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:09 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:09 7439-92-102/16/15 16:1010.0 2.5 1
Nickel 2.7J ug/L 02/19/15 00:09 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:09 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:09 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:09 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:09 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 6.2J ug/L 02/19/15 00:09 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 16:39 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 16:39 107-13-12001.9 1
Benzene ND ug/L 02/22/15 16:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 16:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 16:39 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 16:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 16:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 16:39 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 16:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 16:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 16:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 16:39 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 16:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 16:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 16:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 16:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 16:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 16:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 16:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 16:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 16:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 16:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 16:39 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 16:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 16:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 16:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 16:39 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 16:39 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 16:39 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-6 Lab ID:92237750006 Collected:02/12/15 10:10 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 16:39 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 16:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 16:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 16:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 16:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 16:39 108-10-11000.33 1
Styrene ND ug/L 02/22/15 16:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 16:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 16:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 16:39 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 16:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 16:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 16:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 16:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 16:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 16:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 16:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 16:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 16:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/22/15 16:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %02/22/15 16:39 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 16:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-7 Lab ID:92237750007 Collected:02/12/15 10:40 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:12 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:12 7440-38-202/16/15 16:1010.0 2.5 1
Barium 35.6J ug/L 02/19/15 00:12 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:12 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:12 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:12 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:12 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:12 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:12 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:12 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:12 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:12 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:12 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:12 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 6.9J ug/L 02/19/15 00:12 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 16:55 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 16:55 107-13-12001.9 1
Benzene ND ug/L 02/22/15 16:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 16:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 16:55 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 16:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 16:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 16:55 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 16:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 16:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 16:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 16:55 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 16:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 16:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 16:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 16:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 16:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 16:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 16:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 16:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 16:55 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 16:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 16:55 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 16:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 16:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 16:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 16:55 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 16:55 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 16:55 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-7 Lab ID:92237750007 Collected:02/12/15 10:40 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 16:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 16:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 16:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 16:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 16:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 16:55 108-10-11000.33 1
Styrene ND ug/L 02/22/15 16:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 16:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 16:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 16:55 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 16:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 16:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 16:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 16:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 16:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 16:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 16:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 16:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 16:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %02/22/15 16:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %02/22/15 16:55 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 16:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-8 Lab ID:92237750008 Collected:02/12/15 14:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:15 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:15 7440-38-202/16/15 16:1010.0 2.5 1
Barium 99.9J ug/L 02/19/15 00:15 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:15 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:15 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:15 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:15 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:15 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:15 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:15 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:15 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:15 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:15 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:15 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/19/15 00:15 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 02/19/15 13:35 7439-97-602/14/15 18:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 17:12 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 17:12 107-13-12001.9 1
Benzene ND ug/L 02/22/15 17:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 17:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 17:12 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 17:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 17:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 17:12 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 17:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 17:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 17:12 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 17:12 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 17:12 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 17:12 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 17:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 17:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 17:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 17:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 17:12 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 17:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 17:12 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 17:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 17:12 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 17:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 17:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 17:12 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-8 Lab ID:92237750008 Collected:02/12/15 14:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 02/22/15 17:12 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 17:12 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 17:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/22/15 17:12 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 17:12 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 17:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 17:12 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 17:12 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 17:12 108-10-11000.33 1
Styrene ND ug/L 02/22/15 17:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 17:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 17:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 17:12 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 17:12 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 17:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 17:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 17:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 17:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 17:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 17:12 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 17:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 17:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %02/22/15 17:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 17:12 17060-07-070-130 1
Toluene-d8 (S)100 %02/22/15 17:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-9 Lab ID:92237750009 Collected:02/12/15 11:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:28 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:28 7440-38-202/16/15 16:1010.0 2.5 1
Barium 29.9J ug/L 02/19/15 00:28 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:28 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.8 ug/L 02/19/15 00:28 7440-43-902/16/15 16:101.0 0.50 1
Chromium 5.5J ug/L 02/19/15 00:28 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:28 7440-48-402/16/15 16:1010.0 2.5 1
Copper 2.6J ug/L 02/19/15 00:28 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:28 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:28 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:28 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:28 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:28 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 6.2J ug/L 02/19/15 00:28 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 11.1 ug/L 02/19/15 00:28 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 17:29 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 17:29 107-13-12001.9 1
Benzene ND ug/L 02/22/15 17:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 17:29 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 17:29 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 17:29 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 17:29 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 17:29 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 17:29 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 17:29 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 17:29 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 17:29 75-00-310.0 0.54 1
Chloroform 0.88J ug/L 02/22/15 17:29 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 17:29 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 17:29 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 17:29 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 17:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 17:29 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 17:29 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 17:29 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 17:29 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 17:29 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 17:29 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 17:29 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 17:29 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 17:29 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 17:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 17:29 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 17:29 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
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Page 21 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-9 Lab ID:92237750009 Collected:02/12/15 11:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 17:29 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 17:29 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 17:29 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 17:29 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 17:29 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 17:29 108-10-11000.33 1
Styrene ND ug/L 02/22/15 17:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 17:29 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 17:29 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 17:29 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 17:29 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 17:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 17:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 17:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 17:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 17:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 17:29 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 17:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 17:29 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %02/22/15 17:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 17:29 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 17:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
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Page 22 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-10 Lab ID:92237750010 Collected:02/12/15 11:20 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:31 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:31 7440-38-202/16/15 16:1010.0 2.5 1
Barium 409 ug/L 02/19/15 00:31 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:31 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.80J ug/L 02/19/15 00:31 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:31 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt 2.8J ug/L 02/19/15 00:31 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:31 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:31 7439-92-102/16/15 16:1010.0 2.5 1
Nickel 3.6J ug/L 02/19/15 00:31 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:31 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:31 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:31 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:31 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 25.6 ug/L 02/19/15 00:31 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 24.1J ug/L 02/22/15 17:46 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 17:46 107-13-12001.9 1
Benzene ND ug/L 02/22/15 17:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 17:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 17:46 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 17:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 17:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 17:46 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 17:46 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 17:46 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 17:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 17:46 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 17:46 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 17:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 17:46 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 17:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 17:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 17:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 17:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 17:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 17:46 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 17:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 17:46 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 17:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/22/15 17:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 17:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 17:46 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 17:46 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 17:46 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
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Huntersville, NC 28078
[phone]
Page 23 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-10 Lab ID:92237750010 Collected:02/12/15 11:20 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 17:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 17:46 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 17:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 17:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 17:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 17:46 108-10-11000.33 1
Styrene ND ug/L 02/22/15 17:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 17:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 17:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 17:46 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 17:46 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 17:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 17:46 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 17:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 17:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 17:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 17:46 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 17:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 17:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 17:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %02/22/15 17:46 17060-07-070-130 1
Toluene-d8 (S)98 %02/22/15 17:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-11 Lab ID:92237750011 Collected:02/12/15 11:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:34 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:34 7440-38-202/16/15 16:1010.0 2.5 1
Barium 142 ug/L 02/19/15 00:34 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:34 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 2.8 ug/L 02/19/15 00:34 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:34 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:34 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:34 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:34 7439-92-102/16/15 16:1010.0 2.5 1
Nickel 4.8J ug/L 02/19/15 00:34 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:34 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:34 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:34 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 3.6J ug/L 02/19/15 00:34 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.4J ug/L 02/19/15 00:34 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 18:03 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 18:03 107-13-12001.9 1
Benzene ND ug/L 02/22/15 18:03 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 18:03 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 18:03 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 18:03 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 18:03 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 18:03 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 18:03 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 18:03 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 18:03 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 18:03 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 18:03 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 18:03 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 18:03 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 18:03 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 18:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 18:03 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 18:03 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 18:03 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 18:03 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 18:03 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 18:03 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 18:03 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.25J ug/L 02/22/15 18:03 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 18:03 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 18:03 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 18:03 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 18:03 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Sample:MW-11 Lab ID:92237750011 Collected:02/12/15 11:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 18:03 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 18:03 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 18:03 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 18:03 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 18:03 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 18:03 108-10-11000.33 1
Styrene ND ug/L 02/22/15 18:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 18:03 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 18:03 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 18:03 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 18:03 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 18:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 18:03 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 18:03 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 18:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 18:03 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 18:03 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 18:03 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 18:03 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %02/22/15 18:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 18:03 17060-07-070-130 1
Toluene-d8 (S)100 %02/22/15 18:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/7580
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92237750008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392337
Associated Lab Samples:92237750008
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 02/19/15 12:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392338LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392339MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1392340
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 101 75-125106 5 252.5ND 2.5 2.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237750001, 92237750002, 92237750003, 92237750004, 92237750005, 92237750006, 92237750007,
92237750008, 92237750009, 92237750010, 92237750011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237750001, 92237750002, 92237750003, 92237750004, 92237750005, 92237750006, 92237750007,
92237750008, 92237750009, 92237750010, 92237750011
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/18/15 23:26
Arsenic ug/L ND 10.0 02/18/15 23:26
Barium ug/L ND 100 02/18/15 23:26
Beryllium ug/L ND 1.0 02/18/15 23:26
Cadmium ug/L ND 1.0 02/18/15 23:26
Chromium ug/L ND 10.0 02/18/15 23:26
Cobalt ug/L ND 10.0 02/18/15 23:26
Copper ug/L ND 10.0 02/18/15 23:26
Lead ug/L ND 10.0 02/18/15 23:26
Nickel ug/L ND 50.0 02/18/15 23:26
Selenium ug/L ND 10.0 02/18/15 23:26
Silver ug/L ND 10.0 02/18/15 23:26
Thallium ug/L ND 5.5 02/18/15 23:26
Vanadium ug/L ND 25.0 02/18/15 23:26
Zinc ug/L ND 10.0 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 483500 97 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 465500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 440500 88 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 466500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 05:05 PM
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Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 2 25500ND479490
Arsenic ug/L 500 92 75-12595 3 25500ND462474
Barium ug/L 500 99 75-125101 3 25500ND493507
Beryllium ug/L 500 98 75-125101 3 25500ND490505
Cadmium ug/L 500 98 75-125100 3 25500ND488501
Chromium ug/L 500 102 75-125105 3 25500ND510525
Cobalt ug/L 500 99 75-125102 3 25500ND497511
Copper ug/L 500 98 75-125101 3 25500ND493507
Lead ug/L 500 99 75-125102 2 25500ND496509
Nickel ug/L 500 97 75-125100 3 25500ND486499
Selenium ug/L 500 92 75-12594 2 25500ND462470
Silver ug/L 250 99 75-125101 2 25250ND248254
Thallium ug/L 500 89 75-12592 4 25500ND448465
Vanadium ug/L 500 97 75-125100 3 25500ND486500
Zinc ug/L 500 93 75-12595 2 25500ND469479
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30436
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237750001, 92237750002, 92237750003, 92237750004, 92237750005, 92237750006, 92237750007,
92237750008, 92237750009, 92237750010, 92237750011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1395932
Associated Lab Samples:92237750001, 92237750002, 92237750003, 92237750004, 92237750005, 92237750006, 92237750007,
92237750008, 92237750009, 92237750010, 92237750011
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/22/15 12:24
1,1,1-Trichloroethane ug/L ND 1.0 02/22/15 12:24
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/22/15 12:24
1,1,2-Trichloroethane ug/L ND 1.0 02/22/15 12:24
1,1-Dichloroethane ug/L ND 5.0 02/22/15 12:24
1,1-Dichloroethene ug/L ND 5.0 02/22/15 12:24
1,2,3-Trichloropropane ug/L ND 1.0 02/22/15 12:24
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/22/15 12:24
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/22/15 12:24
1,2-Dichlorobenzene ug/L ND 5.0 02/22/15 12:24
1,2-Dichloroethane ug/L ND 1.0 02/22/15 12:24
1,2-Dichloropropane ug/L ND 1.0 02/22/15 12:24
1,3-Dichloropropane ug/L ND 1.0 02/22/15 12:24
1,4-Dichlorobenzene ug/L ND 1.0 02/22/15 12:24
2-Butanone (MEK)ug/L ND 100 02/22/15 12:24
2-Hexanone ug/L ND 50.0 02/22/15 12:24
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/22/15 12:24
Acetone ug/L ND 100 02/22/15 12:24
Acrylonitrile ug/L ND 200 02/22/15 12:24
Benzene ug/L ND 1.0 02/22/15 12:24
Bromochloromethane ug/L ND 3.0 02/22/15 12:24
Bromodichloromethane ug/L ND 1.0 02/22/15 12:24
Bromoform ug/L ND 3.0 02/22/15 12:24
Bromomethane ug/L ND 10.0 02/22/15 12:24
Carbon disulfide ug/L ND 100 02/22/15 12:24
Carbon tetrachloride ug/L ND 1.0 02/22/15 12:24
Chlorobenzene ug/L ND 3.0 02/22/15 12:24
Chloroethane ug/L ND 10.0 02/22/15 12:24
Chloroform ug/L ND 5.0 02/22/15 12:24
Chloromethane ug/L ND 1.0 02/22/15 12:24
cis-1,2-Dichloroethene ug/L ND 5.0 02/22/15 12:24
cis-1,3-Dichloropropene ug/L ND 1.0 02/22/15 12:24
Dibromochloromethane ug/L ND 3.0 02/22/15 12:24
Dibromomethane ug/L ND 10.0 02/22/15 12:24
Ethylbenzene ug/L ND 1.0 02/22/15 12:24
Iodomethane ug/L ND 10.0 02/22/15 12:24
Methylene Chloride ug/L ND 1.0 02/22/15 12:24
Styrene ug/L ND 1.0 02/22/15 12:24
Tetrachloroethene ug/L ND 1.0 02/22/15 12:24
Toluene ug/L ND 1.0 02/22/15 12:24
REPORT OF LABORATORY ANALYSIS
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Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1395932
Associated Lab Samples:92237750001, 92237750002, 92237750003, 92237750004, 92237750005, 92237750006, 92237750007,
92237750008, 92237750009, 92237750010, 92237750011
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 02/22/15 12:24
trans-1,3-Dichloropropene ug/L ND 1.0 02/22/15 12:24
trans-1,4-Dichloro-2-butene ug/L ND 100 02/22/15 12:24
Trichloroethene ug/L ND 1.0 02/22/15 12:24
Trichlorofluoromethane ug/L ND 1.0 02/22/15 12:24
Vinyl acetate ug/L ND 50.0 02/22/15 12:24
Vinyl chloride ug/L ND 1.0 02/22/15 12:24
Xylene (Total)ug/L ND 5.0 02/22/15 12:24
1,2-Dichloroethane-d4 (S)%103 70-130 02/22/15 12:24
4-Bromofluorobenzene (S)%98 70-130 02/22/15 12:24
Toluene-d8 (S)%99 70-130 02/22/15 12:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1395933LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.250 104 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 48.050 96 66-135
1,2,3-Trichloropropane ug/L 49.450 99 75-130
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 51.550 103 83-124
1,2-Dichlorobenzene ug/L 49.750 99 80-133
1,2-Dichloroethane ug/L 48.250 96 67-128
1,2-Dichloropropane ug/L 51.450 103 75-132
1,3-Dichloropropane ug/L 50.750 101 76-131
1,4-Dichlorobenzene ug/L 49.850 100 78-130
2-Butanone (MEK)ug/L 94.8J100 95 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 102100 102 48-146
Acrylonitrile ug/L 263250 105 40-160
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 52.350 105 71-125
Bromodichloromethane ug/L 47.950 96 78-124
Bromoform ug/L 42.650 85 71-128
Bromomethane ug/L 44.250 88 40-160
Carbon disulfide ug/L 44.2J50 88 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 50.150 100 81-122
Chloroethane ug/L 52.950 106 39-148
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 31 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1395933LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 45.950 92 73-127
Chloromethane ug/L 51.650 103 44-146
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 52.650 105 72-132
Dibromochloromethane ug/L 43.050 86 78-125
Dibromomethane ug/L 52.450 105 82-120
Ethylbenzene ug/L 50.650 101 79-121
Iodomethane ug/L 95.6100 96 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 53.750 107 84-126
Tetrachloroethene ug/L 48.650 97 78-122
Toluene ug/L 51.450 103 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 47.850 96 69-141
trans-1,4-Dichloro-2-butene ug/L 50.7J50 101 40-160
Trichloroethene ug/L 50.350 101 78-122
Trichlorofluoromethane ug/L 52.950 106 53-137
Vinyl acetate ug/L 98.3100 98 40-160
Vinyl chloride ug/L 50.050 100 58-137
Xylene (Total)ug/L 151150 101 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1400344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1400345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 3 3021.4 20.9
1,1,1-Trichloroethane ug/L 2 3024.1 23.7
1,1,2,2-Tetrachloroethane ug/L 2 3021.0 20.6
1,1,2-Trichloroethane ug/L 6 3021.9 20.7
1,1-Dichloroethane ug/L 20 114 70-130110 3 30201.3 24.1 23.4
1,1-Dichloroethene ug/L 20 112 70-166107 5 30200.84J 23.3 22.2
1,2,3-Trichloropropane ug/L 2 3021.3 20.9
1,2-Dibromo-3-
chloropropane ug/L 1 3019.5 19.7
1,2-Dibromoethane (EDB)ug/L 1 3021.4 21.2
1,2-Dichlorobenzene ug/L 3 3021.1 20.4
1,2-Dichloroethane ug/L 20 113 70-130108 4 3020ND22.6 21.7
1,2-Dichloropropane ug/L 4 3021.9 21.0
1,3-Dichloropropane ug/L 2 3021.5 21.0
1,4-Dichlorobenzene ug/L 4 3021.5 20.6
2-Butanone (MEK)ug/L 1 3040.8J 41.4J
2-Hexanone ug/L 1 3041.1J 41.6J
REPORT OF LABORATORY ANALYSIS
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Page 32 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1400344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1400345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Methyl-2-pentanone
(MIBK)ug/L 3 3043.6J 42.3J
Acetone ug/L 1 3045.6J 45.8J
Acrylonitrile ug/L 0 30113J113J
Benzene ug/L 3 3023.2 22.4
Bromochloromethane ug/L 2 3022.7 22.2
Bromodichloromethane ug/L 4 3019.9 19.2
Bromoform ug/L 1 3017.8 17.7
Bromomethane ug/L 13 3020.7 18.2
Carbon disulfide ug/L 4 3019.1J 18.3J
Carbon tetrachloride ug/L 2 3022.6 22.1
Chlorobenzene ug/L 3 3021.6 21.0
Chloroethane ug/L 6 3026.3 24.7
Chloroform ug/L 1 3020.3 20.6
Chloromethane ug/L 4 3023.2 22.4
cis-1,2-Dichloroethene ug/L 20 106 70-13097 2 302084.1 105 104
cis-1,3-Dichloropropene ug/L 3 3020.2 19.6
Dibromochloromethane ug/L 1 3018.1 17.9
Dibromomethane ug/L 2 3021.5 21.0
Ethylbenzene ug/L 3 3022.4 21.8
Iodomethane ug/L 20 3034.7 42.6
Methylene Chloride ug/L 2 3022.5 22.1
Styrene ug/L 4 3022.2 21.2
Tetrachloroethene ug/L 4 3021.7 20.8
Toluene ug/L 3 3022.4 21.7
trans-1,2-Dichloroethene ug/L 20 113 70-130110 3 30201.3 24.0 23.3
trans-1,3-Dichloropropene ug/L 2 3019.3 18.9
trans-1,4-Dichloro-2-butene ug/L 2 3019.1J 19.5J
Trichloroethene ug/L 20 105 69-15191 3 302077.6 98.6 95.8
Trichlorofluoromethane ug/L 4 3026.6 25.4
Vinyl acetate ug/L 2 3030.6J 30.0J
Vinyl chloride ug/L 20 113 70-130109 4 3020ND22.7 21.7
1,2-Dichloroethane-d4 (S)%104 70-130102
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
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Page 33 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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Page 34 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237750
Wayne Closed MSWLF (Dudley)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237750001 MPRP/17907 ICP/16106MW-1 EPA 3010 EPA 6010
92237750002 MPRP/17907 ICP/16106MW-2 EPA 3010 EPA 6010
92237750003 MPRP/17907 ICP/16106MW-3 EPA 3010 EPA 6010
92237750004 MPRP/17907 ICP/16106MW-4 EPA 3010 EPA 6010
92237750005 MPRP/17907 ICP/16106MW-5 EPA 3010 EPA 6010
92237750006 MPRP/17907 ICP/16106MW-6 EPA 3010 EPA 6010
92237750007 MPRP/17907 ICP/16106MW-7 EPA 3010 EPA 6010
92237750008 MPRP/17907 ICP/16106MW-8 EPA 3010 EPA 6010
92237750009 MPRP/17907 ICP/16106MW-9 EPA 3010 EPA 6010
92237750010 MPRP/17907 ICP/16106MW-10 EPA 3010 EPA 6010
92237750011 MPRP/17907 ICP/16106MW-11 EPA 3010 EPA 6010
92237750008 MERP/7580 MERC/7275MW-8 EPA 7470 EPA 7470
92237750001 MSV/30436MW-1 EPA 8260
92237750002 MSV/30436MW-2 EPA 8260
92237750003 MSV/30436MW-3 EPA 8260
92237750004 MSV/30436MW-4 EPA 8260
92237750005 MSV/30436MW-5 EPA 8260
92237750006 MSV/30436MW-6 EPA 8260
92237750007 MSV/30436MW-7 EPA 8260
92237750008 MSV/30436MW-8 EPA 8260
92237750009 MSV/30436MW-9 EPA 8260
92237750010 MSV/30436MW-10 EPA 8260
92237750011 MSV/30436MW-11 EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 35 of 37
Page 36 of 37
Page 37 of 37
#=CL#
February 27, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237753
92237753
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne MSWLF-SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Lab ID Sample ID Matrix Date Collected Date Received
92237753001 SW-2 Water 02/11/15 17:15 02/13/15 15:45
92237753002 SW-3 Water 02/11/15 17:25 02/13/15 15:45
92237753003 SW-1 Water 02/11/15 17:35 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
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Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237753001 SW-2 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237753002 SW-3 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237753003 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-2 Lab ID:92237753001 Collected:02/11/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:37 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:37 7440-38-202/16/15 16:1010.0 2.5 1
Barium 27.1J ug/L 02/19/15 00:37 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:37 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:37 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:37 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:37 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:37 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:37 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:37 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:37 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:37 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:37 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:37 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 7.6J ug/L 02/19/15 00:37 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:08 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:08 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:08 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:08 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:08 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:08 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:08 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:08 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-2 Lab ID:92237753001 Collected:02/11/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:08 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:08 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 18:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/25/15 18:08 17060-07-070-130 1
Toluene-d8 (S)95 %02/25/15 18:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-3 Lab ID:92237753002 Collected:02/11/15 17:25 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:40 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:40 7440-38-202/16/15 16:1010.0 2.5 1
Barium 60.1J ug/L 02/19/15 00:40 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:40 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:40 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:40 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:40 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:40 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:40 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:40 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:40 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:40 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:40 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:40 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 7.1J ug/L 02/19/15 00:40 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:25 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:25 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:25 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:25 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:25 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:25 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:25 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:25 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:25 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-3 Lab ID:92237753002 Collected:02/11/15 17:25 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:25 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:25 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 18:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/25/15 18:25 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 18:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92237753003 Collected:02/11/15 17:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:43 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:43 7440-38-202/16/15 16:1010.0 2.5 1
Barium 63.3J ug/L 02/19/15 00:43 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:43 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:43 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:43 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:43 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:43 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:43 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:43 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:43 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:43 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:43 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:43 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.8J ug/L 02/19/15 00:43 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:42 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:42 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:42 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:42 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:42 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:42 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:42 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:42 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:42 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92237753003 Collected:02/11/15 17:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:42 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:42 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 18:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/25/15 18:42 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 18:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237753001, 92237753002, 92237753003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237753001, 92237753002, 92237753003
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/18/15 23:26
Arsenic ug/L ND 10.0 02/18/15 23:26
Barium ug/L ND 100 02/18/15 23:26
Beryllium ug/L ND 1.0 02/18/15 23:26
Cadmium ug/L ND 1.0 02/18/15 23:26
Chromium ug/L ND 10.0 02/18/15 23:26
Cobalt ug/L ND 10.0 02/18/15 23:26
Copper ug/L ND 10.0 02/18/15 23:26
Lead ug/L ND 10.0 02/18/15 23:26
Nickel ug/L ND 50.0 02/18/15 23:26
Selenium ug/L ND 10.0 02/18/15 23:26
Silver ug/L ND 10.0 02/18/15 23:26
Thallium ug/L ND 5.5 02/18/15 23:26
Vanadium ug/L ND 25.0 02/18/15 23:26
Zinc ug/L ND 10.0 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 483500 97 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 465500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 440500 88 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 466500 93 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 2 25500ND479490
Arsenic ug/L 500 92 75-12595 3 25500ND462474
Barium ug/L 500 99 75-125101 3 25500ND493507
Beryllium ug/L 500 98 75-125101 3 25500ND490505
Cadmium ug/L 500 98 75-125100 3 25500ND488501
Chromium ug/L 500 102 75-125105 3 25500ND510525
Cobalt ug/L 500 99 75-125102 3 25500ND497511
Copper ug/L 500 98 75-125101 3 25500ND493507
Lead ug/L 500 99 75-125102 2 25500ND496509
Nickel ug/L 500 97 75-125100 3 25500ND486499
Selenium ug/L 500 92 75-12594 2 25500ND462470
Silver ug/L 250 99 75-125101 2 25250ND248254
Thallium ug/L 500 89 75-12592 4 25500ND448465
Vanadium ug/L 500 97 75-125100 3 25500ND486500
Zinc ug/L 500 93 75-12595 2 25500ND469479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30489
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237753001, 92237753002, 92237753003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397928
Associated Lab Samples:92237753001, 92237753002, 92237753003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/25/15 17:18
1,1,1-Trichloroethane ug/L ND 1.0 02/25/15 17:18
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/25/15 17:18
1,1,2-Trichloroethane ug/L ND 1.0 02/25/15 17:18
1,1-Dichloroethane ug/L ND 5.0 02/25/15 17:18
1,1-Dichloroethene ug/L ND 5.0 02/25/15 17:18
1,2,3-Trichloropropane ug/L ND 1.0 02/25/15 17:18
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/25/15 17:18
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/25/15 17:18
1,2-Dichlorobenzene ug/L ND 5.0 02/25/15 17:18
1,2-Dichloroethane ug/L ND 1.0 02/25/15 17:18
1,2-Dichloropropane ug/L ND 1.0 02/25/15 17:18
1,3-Dichloropropane ug/L ND 1.0 02/25/15 17:18
1,4-Dichlorobenzene ug/L ND 1.0 02/25/15 17:18
2-Butanone (MEK)ug/L ND 100 02/25/15 17:18
2-Hexanone ug/L ND 50.0 02/25/15 17:18
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/25/15 17:18
Acetone ug/L ND 100 02/25/15 17:18
Acrylonitrile ug/L ND 200 02/25/15 17:18
Benzene ug/L ND 1.0 02/25/15 17:18
Bromochloromethane ug/L ND 3.0 02/25/15 17:18
Bromodichloromethane ug/L ND 1.0 02/25/15 17:18
Bromoform ug/L ND 3.0 02/25/15 17:18
Bromomethane ug/L ND 10.0 02/25/15 17:18
Carbon disulfide ug/L ND 100 02/25/15 17:18
Carbon tetrachloride ug/L ND 1.0 02/25/15 17:18
Chlorobenzene ug/L ND 3.0 02/25/15 17:18
Chloroethane ug/L ND 10.0 02/25/15 17:18
Chloroform ug/L ND 5.0 02/25/15 17:18
Chloromethane ug/L ND 1.0 02/25/15 17:18
cis-1,2-Dichloroethene ug/L ND 5.0 02/25/15 17:18
cis-1,3-Dichloropropene ug/L ND 1.0 02/25/15 17:18
Dibromochloromethane ug/L ND 3.0 02/25/15 17:18
Dibromomethane ug/L ND 10.0 02/25/15 17:18
Ethylbenzene ug/L ND 1.0 02/25/15 17:18
Iodomethane ug/L ND 10.0 02/25/15 17:18
Methylene Chloride ug/L ND 1.0 02/25/15 17:18
Styrene ug/L ND 1.0 02/25/15 17:18
Tetrachloroethene ug/L ND 1.0 02/25/15 17:18
Toluene ug/L ND 1.0 02/25/15 17:18
trans-1,2-Dichloroethene ug/L ND 5.0 02/25/15 17:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397928
Associated Lab Samples:92237753001, 92237753002, 92237753003
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 02/25/15 17:18
trans-1,4-Dichloro-2-butene ug/L ND 100 02/25/15 17:18
Trichloroethene ug/L ND 1.0 02/25/15 17:18
Trichlorofluoromethane ug/L ND 1.0 02/25/15 17:18
Vinyl acetate ug/L ND 50.0 02/25/15 17:18
Vinyl chloride ug/L ND 1.0 02/25/15 17:18
Xylene (Total)ug/L ND 5.0 02/25/15 17:18
1,2-Dichloroethane-d4 (S)%99 70-130 02/25/15 17:18
4-Bromofluorobenzene (S)%99 70-130 02/25/15 17:18
Toluene-d8 (S)%95 70-130 02/25/15 17:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397929LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.050 94 80-125
1,1,1-Trichloroethane ug/L 48.350 97 71-129
1,1,2,2-Tetrachloroethane ug/L 46.450 93 79-124
1,1,2-Trichloroethane ug/L 48.350 97 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 46.450 93 66-135
1,2,3-Trichloropropane ug/L 48.150 96 75-130
1,2-Dibromo-3-chloropropane ug/L 46.550 93 71-133
1,2-Dibromoethane (EDB)ug/L 50.150 100 83-124
1,2-Dichlorobenzene ug/L 49.150 98 80-133
1,2-Dichloroethane ug/L 49.250 98 67-128
1,2-Dichloropropane ug/L 48.750 97 75-132
1,3-Dichloropropane ug/L 47.850 96 76-131
1,4-Dichlorobenzene ug/L 48.650 97 78-130
2-Butanone (MEK)ug/L 104100 104 61-144
2-Hexanone ug/L 93.8100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.0J100 98 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 258250 103 40-160
Benzene ug/L 49.850 100 80-125
Bromochloromethane ug/L 46.650 93 71-125
Bromodichloromethane ug/L 44.650 89 78-124
Bromoform ug/L 42.750 85 71-128
Bromomethane ug/L 44.450 89 40-160
Carbon disulfide ug/L 40.4J50 81 50-160
Carbon tetrachloride ug/L 48.450 97 69-131
Chlorobenzene ug/L 47.250 94 81-122
Chloroethane ug/L 36.850 74 39-148
Chloroform ug/L 44.250 88 73-127
Chloromethane ug/L 48.150 96 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397929LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 49.350 99 74-124
cis-1,3-Dichloropropene ug/L 47.450 95 72-132
Dibromochloromethane ug/L 43.850 88 78-125
Dibromomethane ug/L 48.450 97 82-120
Ethylbenzene ug/L 47.650 95 79-121
Iodomethane ug/L 100100 100 39-154
Methylene Chloride ug/L 53.050 106 64-133
Styrene ug/L 48.550 97 84-126
Tetrachloroethene ug/L 47.550 95 78-122
Toluene ug/L 48.550 97 80-121
trans-1,2-Dichloroethene ug/L 48.650 97 71-127
trans-1,3-Dichloropropene ug/L 47.350 95 69-141
trans-1,4-Dichloro-2-butene ug/L 49.5J50 99 40-160
Trichloroethene ug/L 48.850 98 78-122
Trichlorofluoromethane ug/L 54.850 110 53-137
Vinyl acetate ug/L 108100 108 40-160
Vinyl chloride ug/L 42.650 85 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1398024MATRIX SPIKE SAMPLE:
MSSpike
Result
92238381004
1,1,1,2-Tetrachloroethane ug/L 42.640 107 70-130ND
1,1,1-Trichloroethane ug/L 45.740 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 39.940 100 70-130ND
1,1,2-Trichloroethane ug/L 42.540 106 70-130ND
1,1-Dichloroethane ug/L 43.140 108 70-130ND
1,1-Dichloroethene ug/L 45.140 113 70-166ND
1,2,3-Trichloropropane ug/L 41.440 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 38.440 96 70-130ND
1,2-Dibromoethane (EDB)ug/L 43.640 109 70-130ND
1,2-Dichlorobenzene ug/L 43.040 107 70-130ND
1,2-Dichloroethane ug/L 44.340 111 70-130ND
1,2-Dichloropropane ug/L 41.740 104 70-130ND
1,3-Dichloropropane ug/L 42.140 105 70-130ND
1,4-Dichlorobenzene ug/L 43.140 108 70-130ND
2-Butanone (MEK)ug/L 86.6J80 108 70-130ND
2-Hexanone ug/L 79.980 100 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 82.5J80 103 70-130ND
Acetone ug/L 86.6J80 104 70-130ND
Acrylonitrile ug/L 227200 113 70-130ND
Benzene ug/L 44.840 112 70-148ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1398024MATRIX SPIKE SAMPLE:
MSSpike
Result
92238381004
Bromochloromethane ug/L 43.240 108 70-130ND
Bromodichloromethane ug/L 39.340 98 70-130ND
Bromoform ug/L 36.240 90 70-130ND
Bromomethane ug/L 36.440 91 70-130ND
Carbon disulfide ug/L 36.6J40 92 70-130ND
Carbon tetrachloride ug/L 45.740 114 70-130ND
Chlorobenzene ug/L 42.140 105 70-146ND
Chloroethane ug/L 35.140 88 70-130ND
Chloroform ug/L 40.140 100 70-130ND
Chloromethane ug/L 41.740 104 70-130ND
cis-1,2-Dichloroethene ug/L 44.240 111 70-130ND
cis-1,3-Dichloropropene ug/L 38.840 97 70-130ND
Dibromochloromethane ug/L 38.440 96 70-130ND
Dibromomethane ug/L 41.840 104 70-130ND
Ethylbenzene ug/L 42.840 107 70-130ND
Iodomethane ug/L 85.080 106 70-130ND
Methylene Chloride ug/L 47.840 120 70-130ND
Styrene ug/L 42.740 107 70-130ND
Tetrachloroethene ug/L 42.040 105 70-130ND
Toluene ug/L 42.940 107 70-155ND
trans-1,2-Dichloroethene ug/L 44.840 112 70-130ND
trans-1,3-Dichloropropene ug/L 40.040 100 70-130ND
trans-1,4-Dichloro-2-butene ug/L 39.4J40 99 70-130ND
Trichloroethene ug/L 43.740 109 69-151ND
Trichlorofluoromethane ug/L 52.040 130 70-130ND
Vinyl acetate ug/L 70.680 88 70-130ND
Vinyl chloride ug/L 37.940 95 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1398900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1398901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 103 70-130103 0 3020ND20.6 20.5
1,1,1-Trichloroethane ug/L 20 109 70-130111 1 3020ND21.9 22.1
1,1,2,2-Tetrachloroethane ug/L 20 98 70-13098 1 3020ND19.6 19.5
1,1,2-Trichloroethane ug/L 20 103 70-130103 0 3020ND20.5 20.6
1,1-Dichloroethane ug/L 20 104 70-130106 2 3020ND20.8 21.2
1,1-Dichloroethene ug/L 20 105 70-166111 6 3020ND20.9 22.1
1,2,3-Trichloropropane ug/L 20 106 70-130107 0 3020ND21.2 21.3
1,2-Dibromo-3-
chloropropane ug/L 20 95 70-13093 2 3020ND18.9 18.6
1,2-Dibromoethane (EDB)ug/L 20 102 70-130104 2 3020ND20.4 20.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1398900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1398901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 106 70-130105 1 3020ND21.2 21.0
1,2-Dichloroethane ug/L 20 105 70-130105 0 3020ND20.9 20.9
1,2-Dichloropropane ug/L 20 100 70-130101 1 3020ND19.9 20.1
1,3-Dichloropropane ug/L 20 100 70-130101 0 3020ND20.1 20.1
1,4-Dichlorobenzene ug/L 20 106 70-130107 1 3020ND21.2 21.4
2-Butanone (MEK)ug/L 40 104 70-130100 4 3040ND41.4J 40.0J
2-Hexanone ug/L 40 103 70-130101 2 3040ND41.3J 40.5J
4-Methyl-2-pentanone
(MIBK)ug/L 40 103 70-130103 0 3040ND41.1J 41.1J
Acetone ug/L 40 115 70-130109 5 3040ND45.9J 43.5J
Acrylonitrile ug/L 100 114 70-130113 1 30100ND114J113J
Benzene ug/L 20 110 70-148112 2 3020ND22.0 22.4
Bromochloromethane ug/L 20 100 70-130106 6 3020ND20.1 21.3
Bromodichloromethane ug/L 20 93 70-13094 0 3020ND18.6 18.7
Bromoform ug/L 20 88 70-13087 1 3020ND17.6 17.4
Bromomethane ug/L 20 75 70-13087 15 3020ND15.0 17.4
Carbon disulfide ug/L 20 88 70-13089 1 3020ND17.6J 17.9J
Carbon tetrachloride ug/L 20 115 70-130114 1 3020ND23.1 22.8
Chlorobenzene ug/L 20 104 70-146103 1 3020ND20.8 20.6
Chloroethane ug/L 20 89 70-13094 5 3020ND17.9 18.7
Chloroform ug/L 20 93 70-13097 4 3020ND18.7 19.4
Chloromethane ug/L 20 105 70-130104 1 3020ND21.1 20.8
cis-1,2-Dichloroethene ug/L 20 105 70-130106 1 3020ND21.0 21.2
cis-1,3-Dichloropropene ug/L 20 88 70-13089 1 3020ND17.6 17.8
Dibromochloromethane ug/L 20 90 70-13090 0 3020ND17.9 18.0
Dibromomethane ug/L 20 99 70-13099 1 3020ND19.7 19.9
Ethylbenzene ug/L 20 105 70-130107 1 3020ND21.1 21.4
Iodomethane ug/L 40 90 70-13098 8 3040ND35.9 39.1
Methylene Chloride ug/L 20 115 70-130115 0 3020ND22.9 23.0
Styrene ug/L 20 99 70-13099 0 3020ND19.8 19.8
Tetrachloroethene ug/L 20 101 70-130101 0 3020ND20.2 20.2
Toluene ug/L 20 105 70-155106 1 3020ND21.0 21.2
trans-1,2-Dichloroethene ug/L 20 106 70-130104 1 3020ND21.1 20.9
trans-1,3-Dichloropropene ug/L 20 92 70-13091 1 3020ND18.4 18.3
trans-1,4-Dichloro-2-butene ug/L 20 104 70-13099 5 3020ND20.9J 19.8J
Trichloroethene ug/L 20 109 69-151109 1 3020ND21.9 21.7
Trichlorofluoromethane ug/L M02013570-130130 4 3020ND27.1 25.9
Vinyl acetate ug/L 40 80 70-13082 3 3040ND31.9J 32.8J
Vinyl chloride ug/L 20 91 70-13093 2 3020ND18.2 18.5
1,2-Dichloroethane-d4 (S)%97 70-13099
4-Bromofluorobenzene (S)%H59370-13092
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92238381003
1398023SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92238381003
1398023SAMPLE DUPLICATE:
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101 3104
4-Bromofluorobenzene (S)%100 298
Toluene-d8 (S)%94 194
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Page 19 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Page 20 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237753001 MPRP/17907 ICP/16106SW-2 EPA 3010 EPA 6010
92237753002 MPRP/17907 ICP/16106SW-3 EPA 3010 EPA 6010
92237753003 MPRP/17907 ICP/16106SW-1 EPA 3010 EPA 6010
92237753001 MSV/30489SW-2 EPA 8260
92237753002 MSV/30489SW-3 EPA 8260
92237753003 MSV/30489SW-1 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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[phone]
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
February 27, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237754
92237754
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne Closed MWSLF SW by MW2
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 14
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 14
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Lab ID Sample ID Matrix Date Collected Date Received
92237754001 SW-ByMW-2 Water 02/12/15 15:40 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 3 of 14
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237754001 SW-ByMW-2 EPA 8260 67 PASI-CSNP
REPORT OF LABORATORY ANALYSIS
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Page 4 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Sample:SW-ByMW-2 Lab ID:92237754001 Collected:02/12/15 15:40 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 22:30 67-64-110010.0 1
Acetonitrile ND ug/L 02/25/15 22:30 75-05-855.0 2.2 1
Acrolein ND ug/L 02/25/15 22:30 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 02/25/15 22:30 107-13-12001.9 1
Allyl chloride ND ug/L 02/25/15 22:30 107-05-110.0 1.5 1
Benzene ND ug/L 02/25/15 22:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 22:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 22:30 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 22:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 22:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 22:30 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 22:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 22:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 22:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 22:30 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 22:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 22:30 74-87-31.0 0.11 1
Chloroprene ND ug/L 02/25/15 22:30 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 22:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 22:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 22:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 22:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 22:30 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 02/25/15 22:30 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 02/25/15 22:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 22:30 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 02/25/15 22:30 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 02/25/15 22:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 22:30 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 22:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 22:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 22:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 22:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 22:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 02/25/15 22:30 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 02/25/15 22:30 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 22:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/25/15 22:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 22:30 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 02/25/15 22:30 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 02/25/15 22:30 87-68-310.0 0.71 1
2-Hexanone ND ug/L 02/25/15 22:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 22:30 74-88-410.0 0.32 1
Isobutanol ND ug/L 02/25/15 22:30 78-83-110035.0 1
Methacrylonitrile ND ug/L 02/25/15 22:30 126-98-71000.93 1
Methylene Chloride ND ug/L 02/25/15 22:30 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Sample:SW-ByMW-2 Lab ID:92237754001 Collected:02/12/15 15:40 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 02/25/15 22:30 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 22:30 108-10-11000.33 1
Naphthalene ND ug/L 02/25/15 22:30 91-20-310.0 0.24 1
Propionitrile ND ug/L 02/25/15 22:30 107-12-01503.6 1
Styrene ND ug/L 02/25/15 22:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 22:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 22:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 22:30 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 22:30 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 02/25/15 22:30 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 02/25/15 22:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 22:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 22:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 22:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 22:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 22:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 22:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 22:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %02/25/15 22:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %02/25/15 22:30 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 22:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30492
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397974
Associated Lab Samples:92237754001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/25/15 16:01
1,1,1-Trichloroethane ug/L ND 1.0 02/25/15 16:01
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/25/15 16:01
1,1,2-Trichloroethane ug/L ND 1.0 02/25/15 16:01
1,1-Dichloroethane ug/L ND 5.0 02/25/15 16:01
1,1-Dichloroethene ug/L ND 5.0 02/25/15 16:01
1,1-Dichloropropene ug/L ND 5.0 02/25/15 16:01
1,2,3-Trichloropropane ug/L ND 1.0 02/25/15 16:01
1,2,4-Trichlorobenzene ug/L ND 10.0 02/25/15 16:01
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/25/15 16:01
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/25/15 16:01
1,2-Dichlorobenzene ug/L ND 5.0 02/25/15 16:01
1,2-Dichloroethane ug/L ND 1.0 02/25/15 16:01
1,2-Dichloropropane ug/L ND 1.0 02/25/15 16:01
1,3-Dichlorobenzene ug/L ND 5.0 02/25/15 16:01
1,3-Dichloropropane ug/L ND 1.0 02/25/15 16:01
1,4-Dichlorobenzene ug/L ND 1.0 02/25/15 16:01
2,2-Dichloropropane ug/L ND 15.0 02/25/15 16:01
2-Butanone (MEK)ug/L ND 100 02/25/15 16:01
2-Hexanone ug/L ND 50.0 02/25/15 16:01
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/25/15 16:01
Acetone ug/L ND 100 02/25/15 16:01
Acetonitrile ug/L ND 55.0 02/25/15 16:01
Acrolein ug/L ND 53.0 02/25/15 16:01
Acrylonitrile ug/L ND 200 02/25/15 16:01
Allyl chloride ug/L ND 10.0 02/25/15 16:01
Benzene ug/L ND 1.0 02/25/15 16:01
Bromochloromethane ug/L ND 3.0 02/25/15 16:01
Bromodichloromethane ug/L ND 1.0 02/25/15 16:01
Bromoform ug/L ND 3.0 02/25/15 16:01
Bromomethane ug/L ND 10.0 02/25/15 16:01
Carbon disulfide ug/L ND 100 02/25/15 16:01
Carbon tetrachloride ug/L ND 1.0 02/25/15 16:01
Chlorobenzene ug/L ND 3.0 02/25/15 16:01
Chloroethane ug/L ND 10.0 02/25/15 16:01
Chloroform ug/L ND 5.0 02/25/15 16:01
Chloromethane ug/L ND 1.0 02/25/15 16:01
Chloroprene ug/L ND 20.0 02/25/15 16:01
cis-1,2-Dichloroethene ug/L ND 5.0 02/25/15 16:01
cis-1,3-Dichloropropene ug/L ND 1.0 02/25/15 16:01
Dibromochloromethane ug/L ND 3.0 02/25/15 16:01
REPORT OF LABORATORY ANALYSIS
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Page 7 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397974
Associated Lab Samples:92237754001
Matrix:Water
Analyzed
Dibromomethane ug/L ND 10.0 02/25/15 16:01
Dichlorodifluoromethane ug/L ND 5.0 02/25/15 16:01
Ethyl methacrylate ug/L ND 10.0 02/25/15 16:01
Ethylbenzene ug/L ND 1.0 02/25/15 16:01
Hexachloro-1,3-butadiene ug/L ND 10.0 02/25/15 16:01
Iodomethane ug/L ND 10.0 02/25/15 16:01
Isobutanol ug/L ND 100 02/25/15 16:01
Methacrylonitrile ug/L ND 100 02/25/15 16:01
Methyl methacrylate ug/L ND 30.0 02/25/15 16:01
Methylene Chloride ug/L ND 1.0 02/25/15 16:01
Naphthalene ug/L ND 10.0 02/25/15 16:01
Propionitrile ug/L ND 150 02/25/15 16:01
Styrene ug/L ND 1.0 02/25/15 16:01
Tetrachloroethene ug/L ND 1.0 02/25/15 16:01
Toluene ug/L ND 1.0 02/25/15 16:01
trans-1,2-Dichloroethene ug/L ND 5.0 02/25/15 16:01
trans-1,3-Dichloropropene ug/L ND 1.0 02/25/15 16:01
trans-1,4-Dichloro-2-butene ug/L ND 100 02/25/15 16:01
Trichloroethene ug/L ND 1.0 02/25/15 16:01
Trichlorofluoromethane ug/L ND 1.0 02/25/15 16:01
Vinyl acetate ug/L ND 50.0 02/25/15 16:01
Vinyl chloride ug/L ND 1.0 02/25/15 16:01
Xylene (Total)ug/L ND 5.0 02/25/15 16:01
1,2-Dichloroethane-d4 (S)%98 70-130 02/25/15 16:01
4-Bromofluorobenzene (S)%108 70-130 02/25/15 16:01
Toluene-d8 (S)%99 70-130 02/25/15 16:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397975LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.450 99 80-125
1,1,1-Trichloroethane ug/L 47.550 95 71-129
1,1,2,2-Tetrachloroethane ug/L 46.450 93 79-124
1,1,2-Trichloroethane ug/L 47.950 96 85-125
1,1-Dichloroethane ug/L 44.350 89 73-126
1,1-Dichloroethene ug/L 43.150 86 66-135
1,1-Dichloropropene ug/L 47.550 95 74-135
1,2,3-Trichloropropane ug/L 46.950 94 75-130
1,2,4-Trichlorobenzene ug/L 51.250 102 75-134
1,2-Dibromo-3-chloropropane ug/L 44.450 89 71-133
1,2-Dibromoethane (EDB)ug/L 47.350 95 83-124
1,2-Dichlorobenzene ug/L 45.350 91 80-133
1,2-Dichloroethane ug/L 44.350 89 67-128
1,2-Dichloropropane ug/L 46.750 93 75-132
REPORT OF LABORATORY ANALYSIS
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Page 8 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397975LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 45.650 91 77-130
1,3-Dichloropropane ug/L 45.350 91 76-131
1,4-Dichlorobenzene ug/L 45.950 92 78-130
2,2-Dichloropropane ug/L 47.950 96 40-160
2-Butanone (MEK)ug/L 89.2J100 89 61-144
2-Hexanone ug/L 97.6100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 99.6J100 100 72-135
Acetone ug/L 95.6J100 96 48-146
Acetonitrile ug/L 436500 87 62-150
Acrolein ug/L 280250 112 24-160
Acrylonitrile ug/L 238250 95 40-160
Allyl chloride ug/L 37.850 76 66-137
Benzene ug/L 48.950 98 80-125
Bromochloromethane ug/L 47.250 94 71-125
Bromodichloromethane ug/L 44.850 90 78-124
Bromoform ug/L 40.950 82 71-128
Bromomethane ug/L 30.750 61 40-160
Carbon disulfide ug/L 39.0J50 78 50-160
Carbon tetrachloride ug/L 51.050 102 69-131
Chlorobenzene ug/L 46.750 93 81-122
Chloroethane ug/L 47.250 94 39-148
Chloroform ug/L 42.150 84 73-127
Chloromethane ug/L 40.850 82 44-146
Chloroprene ug/L 43.550 87 75-145
cis-1,2-Dichloroethene ug/L 45.150 90 74-124
cis-1,3-Dichloropropene ug/L 50.850 102 72-132
Dibromochloromethane ug/L 40.150 80 78-125
Dibromomethane ug/L 52.750 105 82-120
Dichlorodifluoromethane ug/L 48.850 98 34-157
Ethyl methacrylate ug/L 46.250 92 82-121
Ethylbenzene ug/L 47.950 96 79-121
Hexachloro-1,3-butadiene ug/L 51.650 103 72-131
Iodomethane ug/L 80.6100 81 39-154
Isobutanol ug/L 10401000 104 34-160
Methacrylonitrile ug/L 453500 91 74-134
Methyl methacrylate ug/L 48.950 98 84-124
Methylene Chloride ug/L 46.050 92 64-133
Naphthalene ug/L 46.950 94 73-133
Propionitrile ug/L 487500 97 73-140
Styrene ug/L 50.050 100 84-126
Tetrachloroethene ug/L 48.250 96 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 44.750 89 71-127
trans-1,3-Dichloropropene ug/L 47.150 94 69-141
trans-1,4-Dichloro-2-butene ug/L 50.0J50 100 40-160
Trichloroethene ug/L 48.050 96 78-122
Trichlorofluoromethane ug/L 49.550 99 53-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 12:50 PM
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[phone]
Page 9 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397975LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 97.0100 97 40-160
Vinyl chloride ug/L 41.850 84 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%110 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 12:50 PM
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Page 10 of 14
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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Page 11 of 14
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237754
Wayne Closed MWSLF SW by MW2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237754001 MSV/30492SW-ByMW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 12 of 14
Page 13 of 14
Page 14 of 14
#=CL#
February 28, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237756
92237756
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne Closed MNA
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 35
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Lab ID Sample ID Matrix Date Collected Date Received
92237756001 MW-1R Water 02/12/15 13:55 02/13/15 15:45
92237756002 MW-2 Water 02/12/15 15:35 02/13/15 15:45
92237756003 MW-8 Water 02/12/15 14:50 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
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Page 3 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237756001 MW-1R EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AMAB
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-ASER
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
92237756002 MW-2 EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AMAB
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-ASER
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
92237756003 MW-8 EPA 6010 1 PASI-ASH1
SM 2320B 1 PASI-AMAB
SM 4500-S2D 1 PASI-AMAB
SM 5210B 1 PASI-ASER
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-ADMN
SM 4500-Cl-E 1 PASI-ASER
SM 5220D 1 PASI-AMAB
SM 5310B 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
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Page 4 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Sample:MW-1R Lab ID:92237756001 Collected:02/12/15 13:55 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Iron 20900 ug/L 02/19/15 00:46 7439-89-602/16/15 16:1030025.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 ND ug/L 02/19/15 19:01500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 02/18/15 11:00 18496-25-810001001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 02/19/15 05:40 L202/14/15 06:00200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1460J ug/L 02/20/15 11:47 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 880J ug/L 02/13/15 23:011000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 8650 ug/L 02/16/15 21:27 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 02/19/15 10:2525000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 3310 ug/L 02/19/15 15:52 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Sample:MW-2 Lab ID:92237756002 Collected:02/12/15 15:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Iron 37800 ug/L 02/19/15 00:49 7439-89-602/16/15 16:1030025.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 586000 ug/L 02/19/15 19:09500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 02/18/15 11:00 18496-25-810001001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 02/19/15 05:40 L202/14/15 06:00200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 23700J ug/L 02/20/15 12:01 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 02/13/15 23:071000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 60800 ug/L 02/16/15 21:30 16887-00-6500025005
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 82000 ug/L 02/19/15 10:2525000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 31000 ug/L 02/19/15 16:05 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Sample:MW-8 Lab ID:92237756003 Collected:02/12/15 14:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Iron 2870 ug/L 02/19/15 00:52 7439-89-602/16/15 16:1030025.0 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 ND ug/L 02/19/15 19:19500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 02/18/15 11:00 18496-25-810001001
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day ND ug/L 02/19/15 05:40 L202/14/15 06:00200020001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2990J ug/L 02/20/15 12:41 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 20.5J ug/L 02/13/15 23:061000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2590 ug/L 02/16/15 21:31 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 02/19/15 10:2525000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1910 ug/L 02/19/15 16:19 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 7 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Iron ug/L ND 300 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Iron ug/L 48205000 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron ug/L 5000 98 75-125101 3 255000ND49205080
REPORT OF LABORATORY ANALYSIS
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Page 8 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/35785
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1394319
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 ug/L ND 5000 02/19/15 15:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1394320LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4520050000 90 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1394321MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237125001
1394322
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500006190-11063 1 45000039.3 mg/L 69700 70600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1394323MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237449009
1394324
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M15000071990-110736 2 45000046.0 mg/L 405000 414000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 9 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/35759
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1393331
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Sulfide ug/L ND 1000 02/18/15 11:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1393332LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 498J500 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647004
1393334
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15005890-11058 1 10500ND290J288J
REPORT OF LABORATORY ANALYSIS
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Page 10 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/35720
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392148
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
BOD, 5 day ug/L ND 2000 02/19/15 05:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392149LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 136000 L01980006984.5-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92237707001
1392150SAMPLE DUPLICATE:
BOD, 5 day ug/L ND 10<2.0 mg/L
REPORT OF LABORATORY ANALYSIS
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Page 11 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21952
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1393460
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Sulfate ug/L ND 250000 02/19/15 12:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1393461LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 18900J20000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237633002
1393463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M1200008990-11089 0 1020000ND19300J19400J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393464MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1393465
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 104 90-110101 1 102000015.6 mg/L 36400J 35900J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 12 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21921
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392134
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Nitrogen, Nitrate ug/L ND 20.0 02/13/15 22:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392135LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24802500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392136MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237756001
1392137
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 93 90-11093 0 102500880J32203200
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 13 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21922
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392138
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Chloride ug/L ND 1000 02/16/15 21:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392139LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2100020000 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392140MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237088001
1392141
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 200000 100 90-11099 0 1020000084.1 mg/L 284000 283000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392142MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237151006
1392143
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000008790-11086 0 1010000021.4 mg/L 108000 107000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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[phone]
Page 14 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21950
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1393350
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Chemical Oxygen Demand ug/L ND 25000 02/19/15 10:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1393351LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 770000750000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393352MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237491001
1393353
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M17500007990-11077 1 3750000974 mg/L 1560000 1550000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393354MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237535006
1393355
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 108 90-110107 1 3750000ND809000804000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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Page 15 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21964
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92237756001, 92237756002, 92237756003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1394359
Associated Lab Samples:92237756001, 92237756002, 92237756003
Matrix:Water
Analyzed
Total Organic Carbon ug/L ND 1000 02/19/15 14:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1394360LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2450025000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1394361MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237464001
1394362
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M6250007790-11085 1 525000197 mg/L 216000 218000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237756
Wayne Closed MNA
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237756
Wayne Closed MNA
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237756001 MPRP/17907 ICP/16106MW-1R EPA 3010 EPA 6010
92237756002 MPRP/17907 ICP/16106MW-2 EPA 3010 EPA 6010
92237756003 MPRP/17907 ICP/16106MW-8 EPA 3010 EPA 6010
92237756001 WET/35785MW-1R SM 2320B
92237756002 WET/35785MW-2 SM 2320B
92237756003 WET/35785MW-8 SM 2320B
92237756001 WET/35759MW-1R SM 4500-S2D
92237756002 WET/35759MW-2 SM 4500-S2D
92237756003 WET/35759MW-8 SM 4500-S2D
92237756001 WET/35720 WET/35722MW-1R SM 5210B SM 5210B
92237756002 WET/35720 WET/35722MW-2 SM 5210B SM 5210B
92237756003 WET/35720 WET/35722MW-8 SM 5210B SM 5210B
92237756001 WETA/21952MW-1R EPA 300.0
92237756002 WETA/21952MW-2 EPA 300.0
92237756003 WETA/21952MW-8 EPA 300.0
92237756001 WETA/21921MW-1R EPA 353.2
92237756002 WETA/21921MW-2 EPA 353.2
92237756003 WETA/21921MW-8 EPA 353.2
92237756001 WETA/21922MW-1R SM 4500-Cl-E
92237756002 WETA/21922MW-2 SM 4500-Cl-E
92237756003 WETA/21922MW-8 SM 4500-Cl-E
92237756001 WETA/21950MW-1R SM 5220D
92237756002 WETA/21950MW-2 SM 5220D
92237756003 WETA/21950MW-8 SM 5220D
92237756001 WETA/21964MW-1R SM 5310B
92237756002 WETA/21964MW-2 SM 5310B
92237756003 WETA/21964MW-8 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/28/2015 08:22 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 35
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#=CL#
March 04, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237748
92237748
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne MSWLF Blanks
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Report revised 3/4/15 to remove false positive 1,2-Dichloroethane detection from Method Blank
#30436.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 20
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Lab ID Sample ID Matrix Date Collected Date Received
92237748001 EB Water 02/12/15 17:15 02/13/15 15:45
92237748002 FB Water 02/12/15 17:30 02/13/15 15:45
92237748003 TB Water 02/12/15 00:00 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237748001 EB EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237748002 FB EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237748003 TB EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:EB Lab ID:92237748001 Collected:02/12/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/18/15 23:32 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/18/15 23:32 7440-38-202/16/15 16:1010.0 2.5 1
Barium ND ug/L 02/18/15 23:32 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/18/15 23:32 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/18/15 23:32 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/18/15 23:32 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/18/15 23:32 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/18/15 23:32 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/18/15 23:32 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/18/15 23:32 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/18/15 23:32 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/18/15 23:32 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/18/15 23:32 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/18/15 23:32 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/18/15 23:32 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 14:23 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 14:23 107-13-12001.9 1
Benzene ND ug/L 02/22/15 14:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 14:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 14:23 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 14:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 14:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 14:23 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 14:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 14:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 14:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 14:23 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 14:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 14:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 14:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 14:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 14:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 14:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 14:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 14:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 14:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 14:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 14:23 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 14:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.47J ug/L 02/22/15 14:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 14:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 14:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 14:23 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 14:23 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:EB Lab ID:92237748001 Collected:02/12/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 14:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 14:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 14:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 14:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 14:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 14:23 108-10-11000.33 1
Styrene ND ug/L 02/22/15 14:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 14:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 14:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 14:23 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 14:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 14:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 14:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 14:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 14:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 14:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 14:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 14:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 14:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 14:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %02/22/15 14:23 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 14:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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Huntersville, NC 28078
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Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:FB Lab ID:92237748002 Collected:02/12/15 17:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/18/15 23:51 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/18/15 23:51 7440-38-202/16/15 16:1010.0 2.5 1
Barium ND ug/L 02/18/15 23:51 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/18/15 23:51 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/18/15 23:51 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/18/15 23:51 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/18/15 23:51 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/18/15 23:51 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/18/15 23:51 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/18/15 23:51 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/18/15 23:51 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/18/15 23:51 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/18/15 23:51 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/18/15 23:51 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/18/15 23:51 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 14:40 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 14:40 107-13-12001.9 1
Benzene ND ug/L 02/22/15 14:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 14:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 14:40 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 14:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 14:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 14:40 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 14:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 14:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 14:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 14:40 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 14:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 14:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 14:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 14:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 14:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 14:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 14:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 14:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 14:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 14:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 14:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 14:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.37J ug/L 02/22/15 14:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 14:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 14:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 14:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 14:40 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:FB Lab ID:92237748002 Collected:02/12/15 17:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 14:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 14:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 14:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 14:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 14:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 14:40 108-10-11000.33 1
Styrene ND ug/L 02/22/15 14:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 14:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 14:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 14:40 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 14:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 14:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 14:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 14:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 14:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 14:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 14:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 14:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 14:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 14:40 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 14:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:TB Lab ID:92237748003 Collected:02/12/15 00:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 14:57 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 14:57 107-13-12001.9 1
Benzene ND ug/L 02/22/15 14:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 14:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 14:57 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 14:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 14:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 14:57 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 14:57 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 14:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 14:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 14:57 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 14:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 14:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 14:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 14:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 14:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 14:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 14:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 14:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 14:57 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 14:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 14:57 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 14:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.31J ug/L 02/22/15 14:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 14:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 14:57 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 14:57 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 14:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/22/15 14:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 14:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 14:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 14:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 14:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 14:57 108-10-11000.33 1
Styrene ND ug/L 02/22/15 14:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 14:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 14:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 14:57 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 14:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 14:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 14:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 14:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 14:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 14:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 14:57 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:TB Lab ID:92237748003 Collected:02/12/15 00:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 02/22/15 14:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 14:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %02/22/15 14:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %02/22/15 14:57 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 14:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237748001, 92237748002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237748001, 92237748002
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/18/15 23:26
Arsenic ug/L ND 10.0 02/18/15 23:26
Barium ug/L ND 100 02/18/15 23:26
Beryllium ug/L ND 1.0 02/18/15 23:26
Cadmium ug/L ND 1.0 02/18/15 23:26
Chromium ug/L ND 10.0 02/18/15 23:26
Cobalt ug/L ND 10.0 02/18/15 23:26
Copper ug/L ND 10.0 02/18/15 23:26
Lead ug/L ND 10.0 02/18/15 23:26
Nickel ug/L ND 50.0 02/18/15 23:26
Selenium ug/L ND 10.0 02/18/15 23:26
Silver ug/L ND 10.0 02/18/15 23:26
Thallium ug/L ND 5.5 02/18/15 23:26
Vanadium ug/L ND 25.0 02/18/15 23:26
Zinc ug/L ND 10.0 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 483500 97 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 465500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 440500 88 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 466500 93 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 2 25500ND479490
Arsenic ug/L 500 92 75-12595 3 25500ND462474
Barium ug/L 500 99 75-125101 3 25500ND493507
Beryllium ug/L 500 98 75-125101 3 25500ND490505
Cadmium ug/L 500 98 75-125100 3 25500ND488501
Chromium ug/L 500 102 75-125105 3 25500ND510525
Cobalt ug/L 500 99 75-125102 3 25500ND497511
Copper ug/L 500 98 75-125101 3 25500ND493507
Lead ug/L 500 99 75-125102 2 25500ND496509
Nickel ug/L 500 97 75-125100 3 25500ND486499
Selenium ug/L 500 92 75-12594 2 25500ND462470
Silver ug/L 250 99 75-125101 2 25250ND248254
Thallium ug/L 500 89 75-12592 4 25500ND448465
Vanadium ug/L 500 97 75-125100 3 25500ND486500
Zinc ug/L 500 93 75-12595 2 25500ND469479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30436
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237748001, 92237748002, 92237748003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1395932
Associated Lab Samples:92237748001, 92237748002, 92237748003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/22/15 12:24
1,1,1-Trichloroethane ug/L ND 1.0 02/22/15 12:24
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/22/15 12:24
1,1,2-Trichloroethane ug/L ND 1.0 02/22/15 12:24
1,1-Dichloroethane ug/L ND 5.0 02/22/15 12:24
1,1-Dichloroethene ug/L ND 5.0 02/22/15 12:24
1,2,3-Trichloropropane ug/L ND 1.0 02/22/15 12:24
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/22/15 12:24
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/22/15 12:24
1,2-Dichlorobenzene ug/L ND 5.0 02/22/15 12:24
1,2-Dichloroethane ug/L ND 1.0 02/22/15 12:24
1,2-Dichloropropane ug/L ND 1.0 02/22/15 12:24
1,3-Dichloropropane ug/L ND 1.0 02/22/15 12:24
1,4-Dichlorobenzene ug/L ND 1.0 02/22/15 12:24
2-Butanone (MEK)ug/L ND 100 02/22/15 12:24
2-Hexanone ug/L ND 50.0 02/22/15 12:24
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/22/15 12:24
Acetone ug/L ND 100 02/22/15 12:24
Acrylonitrile ug/L ND 200 02/22/15 12:24
Benzene ug/L ND 1.0 02/22/15 12:24
Bromochloromethane ug/L ND 3.0 02/22/15 12:24
Bromodichloromethane ug/L ND 1.0 02/22/15 12:24
Bromoform ug/L ND 3.0 02/22/15 12:24
Bromomethane ug/L ND 10.0 02/22/15 12:24
Carbon disulfide ug/L ND 100 02/22/15 12:24
Carbon tetrachloride ug/L ND 1.0 02/22/15 12:24
Chlorobenzene ug/L ND 3.0 02/22/15 12:24
Chloroethane ug/L ND 10.0 02/22/15 12:24
Chloroform ug/L ND 5.0 02/22/15 12:24
Chloromethane ug/L ND 1.0 02/22/15 12:24
cis-1,2-Dichloroethene ug/L ND 5.0 02/22/15 12:24
cis-1,3-Dichloropropene ug/L ND 1.0 02/22/15 12:24
Dibromochloromethane ug/L ND 3.0 02/22/15 12:24
Dibromomethane ug/L ND 10.0 02/22/15 12:24
Ethylbenzene ug/L ND 1.0 02/22/15 12:24
Iodomethane ug/L ND 10.0 02/22/15 12:24
Methylene Chloride ug/L ND 1.0 02/22/15 12:24
Styrene ug/L ND 1.0 02/22/15 12:24
Tetrachloroethene ug/L ND 1.0 02/22/15 12:24
Toluene ug/L ND 1.0 02/22/15 12:24
trans-1,2-Dichloroethene ug/L ND 5.0 02/22/15 12:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1395932
Associated Lab Samples:92237748001, 92237748002, 92237748003
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 02/22/15 12:24
trans-1,4-Dichloro-2-butene ug/L ND 100 02/22/15 12:24
Trichloroethene ug/L ND 1.0 02/22/15 12:24
Trichlorofluoromethane ug/L ND 1.0 02/22/15 12:24
Vinyl acetate ug/L ND 50.0 02/22/15 12:24
Vinyl chloride ug/L ND 1.0 02/22/15 12:24
Xylene (Total)ug/L ND 5.0 02/22/15 12:24
1,2-Dichloroethane-d4 (S)%103 70-130 02/22/15 12:24
4-Bromofluorobenzene (S)%98 70-130 02/22/15 12:24
Toluene-d8 (S)%99 70-130 02/22/15 12:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1395933LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.250 104 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 48.050 96 66-135
1,2,3-Trichloropropane ug/L 49.450 99 75-130
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 51.550 103 83-124
1,2-Dichlorobenzene ug/L 49.750 99 80-133
1,2-Dichloroethane ug/L 48.250 96 67-128
1,2-Dichloropropane ug/L 51.450 103 75-132
1,3-Dichloropropane ug/L 50.750 101 76-131
1,4-Dichlorobenzene ug/L 49.850 100 78-130
2-Butanone (MEK)ug/L 94.8J100 95 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 102100 102 48-146
Acrylonitrile ug/L 263250 105 40-160
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 52.350 105 71-125
Bromodichloromethane ug/L 47.950 96 78-124
Bromoform ug/L 42.650 85 71-128
Bromomethane ug/L 44.250 88 40-160
Carbon disulfide ug/L 44.2J50 88 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 50.150 100 81-122
Chloroethane ug/L 52.950 106 39-148
Chloroform ug/L 45.950 92 73-127
Chloromethane ug/L 51.650 103 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1395933LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 52.650 105 72-132
Dibromochloromethane ug/L 43.050 86 78-125
Dibromomethane ug/L 52.450 105 82-120
Ethylbenzene ug/L 50.650 101 79-121
Iodomethane ug/L 95.6100 96 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 53.750 107 84-126
Tetrachloroethene ug/L 48.650 97 78-122
Toluene ug/L 51.450 103 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 47.850 96 69-141
trans-1,4-Dichloro-2-butene ug/L 50.7J50 101 40-160
Trichloroethene ug/L 50.350 101 78-122
Trichlorofluoromethane ug/L 52.950 106 53-137
Vinyl acetate ug/L 98.3100 98 40-160
Vinyl chloride ug/L 50.050 100 58-137
Xylene (Total)ug/L 151150 101 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1400344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1400345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 3 3021.4 20.9
1,1,1-Trichloroethane ug/L 2 3024.1 23.7
1,1,2,2-Tetrachloroethane ug/L 2 3021.0 20.6
1,1,2-Trichloroethane ug/L 6 3021.9 20.7
1,1-Dichloroethane ug/L 20 114 70-130110 3 30201.3 24.1 23.4
1,1-Dichloroethene ug/L 20 112 70-166107 5 30200.84J 23.3 22.2
1,2,3-Trichloropropane ug/L 2 3021.3 20.9
1,2-Dibromo-3-
chloropropane ug/L 1 3019.5 19.7
1,2-Dibromoethane (EDB)ug/L 1 3021.4 21.2
1,2-Dichlorobenzene ug/L 3 3021.1 20.4
1,2-Dichloroethane ug/L 20 113 70-130108 4 3020ND22.6 21.7
1,2-Dichloropropane ug/L 4 3021.9 21.0
1,3-Dichloropropane ug/L 2 3021.5 21.0
1,4-Dichlorobenzene ug/L 4 3021.5 20.6
2-Butanone (MEK)ug/L 1 3040.8J 41.4J
2-Hexanone ug/L 1 3041.1J 41.6J
4-Methyl-2-pentanone
(MIBK)ug/L 3 3043.6J 42.3J
Acetone ug/L 1 3045.6J 45.8J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1400344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1400345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acrylonitrile ug/L 0 30113J113J
Benzene ug/L 3 3023.2 22.4
Bromochloromethane ug/L 2 3022.7 22.2
Bromodichloromethane ug/L 4 3019.9 19.2
Bromoform ug/L 1 3017.8 17.7
Bromomethane ug/L 13 3020.7 18.2
Carbon disulfide ug/L 4 3019.1J 18.3J
Carbon tetrachloride ug/L 2 3022.6 22.1
Chlorobenzene ug/L 3 3021.6 21.0
Chloroethane ug/L 6 3026.3 24.7
Chloroform ug/L 1 3020.3 20.6
Chloromethane ug/L 4 3023.2 22.4
cis-1,2-Dichloroethene ug/L 20 106 70-13097 2 302084.1 105 104
cis-1,3-Dichloropropene ug/L 3 3020.2 19.6
Dibromochloromethane ug/L 1 3018.1 17.9
Dibromomethane ug/L 2 3021.5 21.0
Ethylbenzene ug/L 3 3022.4 21.8
Iodomethane ug/L 20 3034.7 42.6
Methylene Chloride ug/L 2 3022.5 22.1
Styrene ug/L 4 3022.2 21.2
Tetrachloroethene ug/L 4 3021.7 20.8
Toluene ug/L 3 3022.4 21.7
trans-1,2-Dichloroethene ug/L 20 113 70-130110 3 30201.3 24.0 23.3
trans-1,3-Dichloropropene ug/L 2 3019.3 18.9
trans-1,4-Dichloro-2-butene ug/L 2 3019.1J 19.5J
Trichloroethene ug/L 20 105 69-15191 3 302077.6 98.6 95.8
Trichlorofluoromethane ug/L 4 3026.6 25.4
Vinyl acetate ug/L 2 3030.6J 30.0J
Vinyl chloride ug/L 20 113 70-130109 4 3020ND22.7 21.7
1,2-Dichloroethane-d4 (S)%104 70-130102
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 20
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237748001 MPRP/17907 ICP/16106EBEPA 3010 EPA 6010
92237748002 MPRP/17907 ICP/16106FBEPA 3010 EPA 6010
92237748001 MSV/30436EBEPA 8260
92237748002 MSV/30436FBEPA 8260
92237748003 MSV/30436TBEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 20
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