7502_PolkCoCDLF_March2017_1stSemiAnnual_DIN28148_20170626

0Electronic Data -Email CD data loaded: Yes / No Doc/Event#:
Environmental Monitoring Division of Waste Management -Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off-site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures.on or nearby the
facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparer's name, telepho_ne number and E-mail address:
Name: Brain Gant Phone: [phone]
E -ma ii: [e-mail]
Facility name: Facility Address:
Polk County C & D Landfill/Polk Highways County MSW Landfill Mills Spring, North Carolina 28722
Environmental Status: (Check all that apply) D Initial/Background Monitoring � Detection Monitoring
e of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells Leachate monitoring data X Surface water monitorin data
Notification attached? D No. No groundwater or surface water standards were exceeded.
-------------------------
NC Landfill Rule: Actual sampling dates (e.g., October 20-24, 2006) Facility Permit# (.0500 or .1600) EJ .0500 and .1600
D Assessment Monitoring
D Methane gas monitoring data D Corrective action data (specify) D Other(specify)
March 8-9, 2017
D Corrective Action
� Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. D Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits.
· CertificationTo the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation; or certification including the possibility of a fine and Imprisonment.
Stuart A. Ryman, P.G.
Facility Representative Name (Print) Alec MacBeth
Signature
231 Haywood St. Asheville NC 28801
Facility Representative Address
P-1649
Project Geologist
Title Digttally signed by Alec MacBeth Date: 2017.06.30 09:43:31 -04'00'
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
828-281-3350
(Area Code) Telephone Number
June 26, 2017 Affix NC Licensed/ Professional Geologist Seal
Date

June 2017
Polk County Construction and Demolition Debris Landfill
And Municipal Solid Waste Landfill
Permit Number 75-02
Route 9, Polk County, North Carolina
Spring 2017
Semiannual Water Quality Monitoring Report
Prepared for Polk County, North Carolina

Project Number: C61476-01.01.02 A:\Projects\Polk County\Route 9 LF\Reports\2017\Spring\FINAL7502March2017 Water Quality Report mb.docx
June 2017
Polk County Construction and Demolition Debris Landfill
And Municipal Solid Waste Landfill
Permit Number 75-02
Route 9, Polk County, North Carolina
Spring 2017
Semiannual Water Quality Monitoring Report

Alec Macbeth, P.G.
Project Geologist
Prepared for
Polk County, North Carolina
Prepared by
Anchor QEA of North Carolina, PLLC 231 Haywood Street
Asheville, North Carolina

Spring 2017 Semiannual Water Quality Report 1 June 2017
TABLE OF CONTENTS
1 Introduction ................................................................................................................... 4
2 C&D Landfill ................................................................................................................... 5
2.1 Sampling and Analysis Methods ............................................................................................................. 5
2.2 Analytical Results ......................................................................................................................................... 6
2.2.1 Groundwater Samples ................................................................................................................. 7
2.2.2 Surface Water Samples ............................................................................................................... 8
3 MSW Landfill................................................................................................................. 10
3.1 Sampling and Analysis Methods ........................................................................................................... 10
3.2 Analytical Results ....................................................................................................................................... 11
3.2.1 Appendix I Metals ....................................................................................................................... 11
3.2.2 Appendix I VOCs ......................................................................................................................... 11
3.2.3 Field Parameters.......................................................................................................................... 11
4 Background Monitoring Well ...................................................................................... 13
4.1 Statistical Analysis Methodology .......................................................................................................... 13
4.2 Results of Statistical Analysis.................................................................................................................. 13
5 Summary .......................................................................................................................14
5.1 Future Activities .......................................................................................................................................... 14
6 References ..................................................................................................................... 16

TABLES
Table 1 Summary of Groundwater Elevation Data—March 2017
Table 2 Summary of Laboratory Analyses Performed on Samples
Table 3 Summary of Detected Constituents
Table 4 VOCs Background Well Comparison
Table 5 Metals Background Well Comparison
FIGURES
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Groundwater Elevation Map

Spring 2017 Semiannual Water Quality Report 2 June 2017
APPENDICES
Appendix A Sampling Logs and Equipment Documentation and Instrument Calibration Data
Sheets
Appendix B Report of Laboratory Analysis and Chain-of-Custody Documentation

Spring 2017 Semiannual Water Quality Report 3 June 2017
ABBREVIATIONS
µg/L micrograms per liter
µS/cm microsiemens per centimeter
1,2-DCA 1,1-dichloroethane
Altamont Altamont Environmental, Inc., which became Anchor QEA on December 29,
2016
Anchor QEA Anchor QEA of North Carolina, PLLC
C&D Construction and Demolition Debris
CFR Code of Federal Regulations
cis-1,2-DCE cis-1,2-dichloroethene
County Polk County Solid Waste Department
DENR North Carolina Department of Environment and Natural Resources, which is
now the DEQ
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
EDD Electronic Data Deliverable
EPA U.S. Environmental Protection Agency
GWP Groundwater Protection
IMAC interim maximum allowable concentrations
MDL method detection limit
mg/L milligrams per liter
MRL method reporting limit
MSW Municipal Solid Waste
mV millivolt
NCAC North Carolina Administrative Code
NTU Nephelometric turbidity units
ORP oxidation reduction potential
PVC polyvinyl chloride
RL Report Limit
Site Polk County Route 9 Landfill Facility
SU Standard Units
SWS Solid Waste Section
SWSL Solid Waste Section Limit
TCE trichloroethene
TestAmerica TestAmerica Laboratories, Inc.
VOC Volatile organic compound

Spring 2017 Semiannual Water Quality Report 4 June 2017
1 Introduction
The Polk County Solid Waste Department (County) maintains two landfills at the Polk County Route 9
Landfill Facility (Site), located on the west side of North Carolina Route 9, approximately 1.5 miles
northwest of the community of Mill Spring (Figure 1).
The northernmost landfill area is an inactive, closed, permitted Construction and Demolition
Debris (C&D) Landfill (Figure 2). The 3.5-acre C&D Landfill (formerly known as the “Operating
Landfill”) was capped during the summer of 2006, and a Closure Plan was submitted to Mr. James
Coffey at the North Carolina Department of Environment and Natural Resources (DENR), now known
as the Department of Environmental Quality (DEQ), on August 21, 2006.
The second landfill is a Municipal Solid Waste (MSW) Landfill composed of two discrete areas in the
west-central and southern parts of the Site (Figure 2). The MSW Landfill (formerly known as the
“Closed Landfill”) is inactive, closed, and maintained by the County. It was officially closed on April 9,
1994.
Both landfills are regulated by the DEQ, Division of Waste Management (DWM), under Permit No.
75-02 (Polk County C&D Landfill and MSW Landfill) as well as DEQ Solid Waste Management Rules
Title 15A, North Carolina Administrative Code (NCAC) Subchapter 13B, Section .0500 (C&D Landfill)
and Title 15A NCAC 13B.1600 (MSW Landfill). The permit requires semiannual monitoring of
groundwater and surface water quality. This report is being submitted by Anchor QEA of North
Carolina, PLLC (Anchor QEA) on behalf of the County, in accordance with the monitoring and
reporting requirements stated in the permit as well as the rules, and it provides an evaluation of
surface water and groundwater quality for the C&D Landfill and an evaluation of the groundwater
quality for the closed MSW Landfill.

Spring 2017 Semiannual Water Quality Report 5 June 2017
2 C&D Landfill
2.1 Sampling and Analysis Methods
Four monitoring wells (MW-01CD, MW-02CD, MW-03CD, and MW-04CD) and three surface water
locations (SS-1, SS-2, and SP-1) are monitored in association with the C&D Landfill. All of these
monitoring points, with the exception of MW-03CD, were sampled on March 8 and 9, 2017 by
Anchor QEA. Monitoring well MW-04CD was installed in January 2016 to be used as an alternative to
MW-03CD, per an approval letter from Ms. Elizabeth Werner of the DEQ dated September 8, 2015.
The approximate locations of the groundwater monitoring wells and surface water sampling points
are shown on Figure 2. Field sampling logs are included in Appendix A.
Monitoring wells MW-01CD, MW-02CD, and MW-04CD are constructed of 2-inch-diameter Schedule
40 polyvinyl chloride (PVC) well material. Well construction logs for MW-01CD and MW-02CD are
not available. The well construction log for MW-04CD is included in Appendix B of the Spring 2016
Semiannual Water Quality Report, produced by Altamont Environmental, Inc. (Altamont), which
became Anchor QEA on December 29, 2016 (Altamont 2016). Prior to sampling, water level
measurements were obtained. Table 1 and Figure 3 present the groundwater elevation data relative
to an assumed benchmark elevation.
Monitoring wells MW-01CD and MW-02CD were each purged and sampled using a new, disposable
polyethylene bailer. Due to poor well accessibility these wells are purged and sampled with a bailer,
as opposed to the low-flow sampling method discussed later in this report. These wells were purged
of three successive well volumes prior to sample collection. During purging, the pH, specific
conductivity, dissolved oxygen (DO), oxidation reduction potential (ORP), turbidity, and temperature
were measured and recorded at the start of purging and after each consecutive well volume was
purged. After the third consecutive well volume was purged, technicians collected a sample in
laboratory-supplied sample containers, while wearing a new pair of nitrile gloves.
Monitoring well MW-04CD was purged and sampled using a new, Teflon-constructed bailer to more
easily pass a slight bend in the well casing. Three separate samples were collected from this
monitoring well in order to further understand the concentration of metals in the groundwater. The
first sample collected was a “no-purge” sample [MW-04CD (No-Purge)], in which the bailer was
gently lowered into the water column in order to minimize sediment disturbance, and subsequently a
sample was collected with the initial purge water. Then the well followed the same sampling
procedures as monitoring wells MW-01CD and MW-02CD, and the second sample (MW-04CD) was
collected after purging three successive well volumes. The third sample [MW-04CD (Filtered)] was
then collected by filtering the groundwater through a 0.45-micron groundwater sampling filter in
order to reduce turbidity.

Spring 2017 Semiannual Water Quality Report 6 June 2017
The surface water sample collected at the SS-1 location is representative of surface water quality
upstream of the landfill. The surface water sample collected at the SS-2 location is representative of
surface water quality downstream of the landfill. The surface water sample collected from the SP-1
location is representative of surface water quality at a nearby spring that is situated at an elevation
lower than the landfill in an apparent downgradient direction (Figure 2). At each of these surface
water sampling locations, pH, specific conductivity, DO, ORP, turbidity, and temperature were
measured and a grab sample was collected by a technician wearing a new pair of nitrile gloves.
Collected groundwater and surface water samples were immediately placed on ice in sample coolers
for transport to the laboratory. Proper chain-of-custody documentation was maintained during the
collection and transport of each sample. A trip blank was also transported in the sample cooler and
analyzed for Appendix I volatile organic compounds (VOCs).
The groundwater and surface water samples were analyzed by TestAmerica Laboratories, Inc.
(TestAmerica), a laboratory certified in North Carolina, for Appendix I VOCs by United States
Environmental Protection Agency (EPA) Method 8260B and for Appendix I metals by EPA Methods
6010D, 6020B, and 7470A (Table 2). Appendix I parameters are referenced in the Code of Federal
Regulations (CFR), Title 40, Appendix I of Part 258. The samples MW-04CD (Filtered) and
MW-04CD (No-Purge) were analyzed for Appendix I metals by EPA Methods 6010D, 6020B, and
7470A. Additional observations and descriptions pertaining to individual wells are provided on the
sampling logs that are included in Appendix A. The report of laboratory analysis and chain-of-
custody forms are included in Appendix B.
2.2 Analytical Results
The laboratory analytical results for groundwater, surface water, and trip blank samples collected at
the C&D Landfill are provided in the report of laboratory analysis issued by TestAmerica
(Appendix B). In addition, all the laboratory analytical results are submitted to the DEQ DWM Solid
Waste Section (SWS) as a separate attachment in the Electronic Data Deliverable (EDD) format,
specified by the SWS on May 5, 2010.
As stipulated in the DWM document referenced above, all laboratory analytical results were reported
and appropriately qualified. Non-detections (non-detects), which are values reported by the
laboratory as below method detection limits (MDLs), are tabulated in Table 3 and the EDD, and are
qualified with the “U” qualifier. The MDL is the minimum concentration of a substance that can be
measured and reported by a laboratory with 99 percent confidence that the analyte concentration is
greater than zero. All detections (values above the MDL) were compared to analyte-specific SWSLs
established by the SWS. The SWSL is the lowest concentration of an analyte in a sample that can be
quantitatively determined with suitable precision and accuracy. If the reported concentration is
above the laboratory MDL and below the method reporting limit (MRL), the analytical result is

Spring 2017 Semiannual Water Quality Report 7 June 2017
qualified by the laboratory as estimated, and is flagged with a non-italicized “J” qualifier (J-flag). The
MRL is the minimum concentration of a target analyte that can be accurately determined by the
referenced method. If the reported concentration is above the laboratory MRL and below the SWSL,
the analytical result is qualified as estimated, and is flagged with an italicized “J” qualifier (italicized J-
flag) by Anchor QEA per DEQ requirements. The MRL is listed in the “Report Limit” (RL) column in the
report of laboratory analysis. Concentrations below the respective SWSLs are not discussed in the
text of this report unless they exceed their contaminant-specific water quality standards (as
described in the following paragraph).
Detected concentrations of analytes in groundwater samples were compared to current groundwater
quality standards specified in 15A NCAC 2L.0202, which are referred to as “2L standards”. Detected
concentrations of analytes in groundwater with no established 2L standards were compared either to
the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]) or Groundwater Protection (GWP) Standards, pursuant to
15A NCAC 13B.1634. Detections of analytes in surface-water samples were compared to 15A NCAC
2B surface-water quality standards (2B standards).
Table 3 presents the summary of laboratory analytical results for detected constituents only. Also
outlined in Table 3 are detections that were above their applicable SWSLs, as well as any analytes
that exceeded their respective 2L standards (including IMACs, if applicable), GWP Standards, or 2B
standards.
2.2.1 Groundwater Samples
2.2.1.1 Appendix I Metals
Thirteen metals were detected in one or more of the groundwater samples collected from the
monitoring wells at the C&D landfill. Eleven of the detected metals were reported at concentrations
above their respective SWSLs in monitoring well MW-04CD (Table 3). Six of these metals (barium,
beryllium, chromium, cobalt, lead, and vanadium) exceeded their respective 2L standards or IMACs in
MW-04CD (Table 3). In order to determine the source of the metals concentrations, the samples
MW-04CD (Filtered) and MW-04CD (No-Purge) were collected and analyzed for Appendix I metals.
Four metals were detected in MW-04CD (Filtered) and of these four metals, barium and zinc were
reported above their SWSLs and only vanadium exceeded its IMAC. Seven metals were detected in
MW-04CD (No-Purge) and only cobalt and vanadium exceeded their 2L standard or IMACs. These
results provide evidence that the metals exceedances associated with MW-04CD are related to
high-turbidity values.
No metals were detected above the SWSL in the sample collected from MW-01CD. Cobalt and
vanadium exceeded their 2L standards or IMACs in the sample collected from this monitoring well.

Spring 2017 Semiannual Water Quality Report 8 June 2017
The sample collected from MW-02CD had six metals detected above respective SWSLs (arsenic,
barium, beryllium, lead, vanadium, and zinc), while arsenic, cobalt, lead, and vanadium exceeded their
respective 2L standards or IMACs. This event was the first event where arsenic exceeded its 2L
standard in the sample collected from monitoring well MW-02CD. These results are consistent with
historical metals concentrations in these wells, and may be attributed to high turbidity values, as
noted below (Table 3).
2.2.1.2 Appendix I VOCs
No VOCs were detected from the groundwater samples collected from the C&D Landfill (Table 3).
2.2.1.3 Field Parameters
Groundwater pH readings were obtained from all monitoring wells sampled. The measured
groundwater pH values in MW-01CD, MW-02CD, and MW-04CD ranged from 5.90 Standard
Units (SU) to 6.20 SU, and were outside the 2L standard pH range of 6.5 to 8.5 SU (Table 3). These
results are consistent with historical data and are considered naturally occurring for groundwater in
this region.
Turbidity values for MW-01CD was 173 nephelometric turbidity units (NTUs); for both MW-02CD and
MW-04CD the measured turbidity was greater than 1,100 NTUs (out of the range of the
turbidimeter).
DO readings for MW-01CD, MW-02CD, and MW-04CD were recorded at 3.95 milligrams per
liter (mg/L), 9.25 mg/L, and 4.12 mg/L, respectively. Specific conductivity readings for these three
monitoring wells were recorded at 158 microsiemens per centimeter (µS/cm), 25 µS/cm, and 162
µS/cm, respectively. Recorded ORP values ranged between 165.0 millivolts (mV) in MW-01CD to
211.5 mV in MW-04CD. These field parameters do not have established groundwater standards.
2.2.2 Surface Water Samples
2.2.2.1 Appendix I Metals
Four metals (barium, cobalt, lead, and vanadium) were detected in one or more surface water
samples collected at the designated sampling locations (Table 3). Barium exceeded its SWSL in the
spring sample, SP-1. All other results were below their respective SWSLs and 2B surface water
standards.
2.2.2.2 Appendix I VOCs
No VOCs were detected in the collected surface water samples (Table 3).

Spring 2017 Semiannual Water Quality Report 9 June 2017
2.2.2.3 Field Parameters
The pH readings obtained from all sampled locations were within the 2B standard range of 6.00 to
9.00 SU (Table 3). Turbidity values measured in the surface water samples ranged from 1.94 NTUs
(SP-1) to 7.26 NTUs (SS-2) (Table 3). These values were all below the 2B surface water standard of 25
NTUs. DO values for the surface water samples ranged from 7.61 mg/L in SP-1 to 10.55 mg/L in SS-2.
All measured DO values were in compliance with the 2B surface water standard, which is defined as
“must be greater than or equal to 5.0 mg/L”.
Specific conductivity values ranged from 43 µS/cm (SS-2) to 136 µS/cm (SP-1). ORP values in the
surface water samples ranged from 166.4 mV in SS-1 to 259.2 mV in SS-2. Specific conductivity and
ORP do not have established 2B surface water standards. A full summary of field parameters is
provided in Table 3.

Spring 2017 Semiannual Water Quality Report 10 June 2017
3 MSW Landfill
3.1 Sampling and Analysis Methods
During the spring 2017 sampling event for the MSW Landfill, Anchor QEA sampled the applicable
monitoring wells, MW-2R, MW-3R, and MW-4, on March 8 and 9, 2017. Monitoring well MW-4 was
installed as an alternative to MW-1R, per an approval letter from Ms. Elizabeth Werner of the DEQ
dated September 8, 2015. The approximate locations of the groundwater monitoring wells are shown
on Figure 2. Field sampling logs are included in Appendix A.
Monitoring wells MW-2R and MW-4 were purged and sampled using low-flow techniques in
accordance with the procedures described in “Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures” (Groundwater Issues [EPA April 1996]). During purging, the pH, specific
conductivity, DO, ORP, turbidity, and temperature were measured and recorded approximately every
3 minutes. Well purging continued until these parameters stabilized, as determined by three
successive readings in which each parameter was within a range of values. Stabilization criteria was
determined by the US Region 4 EPA’s March 6, 2013 document Operating Procedure: Groundwater
Sampling. Parameters are considered “stable” as follows:
• pH +/- 0.1 unit
• Specific conductivity +/- 3 percent
• Temperature +/- 10 percent
• DO +/- 10 percent
• Turbidity +/- 10 percent
• ORP +/- 10 millivolts
Once all these parameters stabilized, a groundwater sample was collected in laboratory-supplied
sample containers by a technician wearing a new pair of nitrile gloves. A duplicate sample was taken
at MW-2R to ensure consistency with laboratory practices, and is listed as MW-2RDUP.
Monitoring well MW-3R was pumped dry using a Grundfos Redi-Flo2 Electrical Submersible Pump
on March 7, 2017 and the groundwater sample was collected following recharge the next day,
March 8, 2017.
Monitoring wells MW-2R and MW-4 are constructed of 2-inch-diameter Schedule 40 PVC well
material, while MW-3R is constructed of 6-inch-diameter Schedule 40 PVC well material. Well
construction logs for MW-2R are not available. The well construction record for the monitoring well
MW-3R is available and was included in Appendix D of the Fall 2012 Semiannual Water Quality
Monitoring Report. The well construction record for the recently installed monitoring well MW-4 is
included in Appendix B of the Spring 2016 Semiannual Water Quality Report (Altamont 2016).

Spring 2017 Semiannual Water Quality Report 11 June 2017
Prior to sampling the wells, field parameters and water level measurements were obtained. Table 1
and Figure 3 present the groundwater elevation data relative to an assumed benchmark elevation.
Field parameters are presented in the sampling logs (Appendix A).
Proper chain-of-custody documentation procedures were followed during collection and transport of
the samples. Analysis of the groundwater samples was performed by TestAmerica using the same
methods described in Section 2.1 (Table 2). Additional observations and descriptions pertaining to
individual wells are provided on the sampling logs included in Appendix A.
3.2 Analytical Results
The laboratory analytical results for groundwater and duplicate, and trip blank samples collected at
the MSW Landfill are provided in the report of laboratory analysis issued by TestAmerica
(Appendix B). In addition, all the laboratory analytical results are submitted to the DEQ DWM SWS as
a separate attachment in the EDD format, specified by the SWS on May 5, 2010.
The data for the MSW samples were compared to the SWSL and contaminant-specific water quality
standards as described in Section 2.2.
3.2.1 Appendix I Metals
Four metals were detected in one or more of the groundwater samples collected from the
monitoring wells. Of the detected metals, barium was present at concentrations above its respective
SWSL in one or more groundwater samples collected from the monitoring wells (Table 3). Vanadium
was the only metal detected at a concentration above its water quality standard (IMAC).
Exceedances of this metal (5.54 J micrograms per liter [µg/L] to 6.46 J µg/L) were identified in all of
the samples collected from monitoring wells associated with the MSW Landfill. Reported
concentrations of vanadium in the monitoring wells at the MSW landfill are consistent with historical
concentrations.
3.2.2 Appendix I VOCs
Three VOCs (1,1-dichloroethane [1,2-DCA], cis-1,2-dichloroethene [cis-1,2-DCE], and trichloroethene
[TCE]) were detected in one or more of the groundwater samples collected from the monitoring wells
(Table 3). Cis-1,2-DCE was the only VOC detected above the SWSL (Table 3). None of the VOCs were
detected at concentrations above the established 2L groundwater quality standards.
3.2.3 Field Parameters
The measured pH was outside the acceptable 2L standard range, established at 6.5 – 8.5 SU, in
monitoring wells MW-2R and MW-4 (Table 3). The recorded pH values for all MSW Landfill
monitoring wells are consistent with historical results.

Spring 2017 Semiannual Water Quality Report 12 June 2017
Turbidity values at the time of sampling monitoring wells MW-2R, MW-3R, and MW-4 ranged from
0.65 NTUs to 2.05 NTUs (Table 3). DO values for these monitoring wells ranged from 1.52 mg/L in
MW-4 to 5.94 mg/L in MW-3R. ORP values ranged from 141.1 mV in MW-3R to 308.8 in MW-2R.
Groundwater standards are not established for turbidity, DO, or ORP. Reported field parameter
values are generally consistent with historical data.

Spring 2017 Semiannual Water Quality Report 13 June 2017
4 Background Monitoring Well
4.1 Statistical Analysis Methodology
In 2012, background monitoring well MW-3R was installed upgradient of the other two MSW
monitoring wells and three C&D monitoring wells. MW-3R was installed to establish background
concentrations of Appendix I VOCs and metals upgradient of the MSW Landfill and C&D Landfill.
MW-3R, consistent with the other five monitoring wells, is sampled on a semiannual basis. MW-3R
has been sampled ten times from October 2012 to March 2017.
A brief statistical analysis presented herein compares background concentrations in MW-3R to
downgradient monitoring wells, and applicable groundwater standards. As part of the statistical
analysis, historical data since September 2012 (as applicable) has been summarized for the wells
sampled during this spring 2017 sampling event: MW-01CD, MW-02CD, MW-04CD, MW-2R, and
MW-4. Tables 4 and 5 list the constituents detected in each well for the subject monitoring period,
minimum concentration, maximum concentration, and average concentration of each detected
constituent, as well as the frequency of detection in each well. Results below the MDL were assumed
to equal half of the MDL.
4.2 Results of Statistical Analysis
A comparison of VOCs is presented in Table 4. No VOCs have been detected in the background well
(MW-3R) during the subject statistical analysis period. Three VOCs (1,1-dichloroethane, cis-1,2-
dichloroethene, and trichloroethene) have been detected in one or more of the downgradient
monitoring wells during the subject monitoring period. However, all of these detections were at
concentrations below the respective 2L standards. A comparison of the average concentrations of
VOCs in downgradient wells with the average concentrations of VOCs in the background well shows
that the majority of average concentrations in downgradient wells exceed those of the background
well.
A comparison of metals is presented in Table 5. During the subject monitoring period, barium,
cobalt, lead, and vanadium were detected in MW-3R at various concentrations. Vanadium was
detected above the IMAC standard in MW-3R during the subject monitoring period. Vanadium
concentrations have ranged from non-detect (below MDL) to concentrations above its IMAC
standard in MW-3R. Thirteen metals have been detected in one or more of the downgradient
monitoring wells during the subject monitoring period (Table 5). Eight of the average concentrations
of these metals exceeded groundwater quality standards in one or more downgradient monitoring
wells. Average concentrations for the majority of metals in downgradient monitoring wells exceeded
the average concentrations of those metals in the background well.

Spring 2017 Semiannual Water Quality Report 14 June 2017
5 Summary
Anchor QEA completed the first semiannual water quality monitoring event of 2017 at the Polk
County Landfills on March 7, 8, and 9, 2017.
Table 3 of this report and the TestAmerica report of laboratory analysis (Appendix B) provide
detailed analytical results and field data demonstrating the groundwater and surface water quality at
the Polk County Landfills. Six metals (barium, beryllium, chromium, cobalt, lead, and vanadium) were
detected at concentrations that exceeded their respective groundwater standards in the samples
collected from the C&D Landfill. Vanadium was the only metal detected at a concentration that
exceeded its IMAC groundwater standard in the samples collected during the subject monitoring
event. No VOCs were detected at concentrations above groundwater or surface water standards
from any of the samples collected during this water quality monitoring event. All pH values
measured in the samples collected from the MSW Landfill and C&D Landfill were outside of the
established 2L groundwater standard range, with the exception of the background monitoring well
(MW-3R). The recorded pH values are consistent with historical data.
Results for the newly installed replacement monitoring wells (MW-04CD and MW-4) are somewhat
mixed. Monitoring well MW-4 produces adequate water and exhibits lower turbidity levels than
those typically measured in the monitoring well that it replaced—MW-1R. As a result, metals
concentrations in the sample collected from MW-4 were lower than the average metals
concentrations historically measured in monitoring well MW-1R. In contrast, MW-04CD compares
closely to the monitoring well that it replaced (MW-03CD) in terms of water production.
Consequently, this monitoring well has been difficult to fully develop, resulting in highly turbid
samples that yield metals concentrations similar to those historically measured in MW-03CD. Due to
these conditions, Anchor QEA collected two extra samples from MW-04CD – one “no-purge” sample,
in which the initial purge water was sampled with little disturbance to the water column, and one
filtered sample, in which the sampled water was filtered through a 0.45-micron groundwater
sampling filter. The results from these samples provide evidence that the high metals concentrations
measured in MW-04CD are affected by the highly turbid water that the well produces.
Based on the number of detects, minimum, maximum, and average concentrations of site
constituents, monitoring well MW-3R appears to be effective in its use as a background monitoring
well. The average concentrations of both VOCs and metals in the majority of the downgradient wells
exceed those of the background well.
5.1 Future Activities
Anchor QEA recommends that Polk County continue to monitor VOCs and metals concentrations in
groundwater and surface water at the closed C&D and MSW landfills. Based on the data trends and

Spring 2017 Semiannual Water Quality Report 15 June 2017
evaluation presented in this report, Anchor QEA has discussed with Polk County options for
addressing the water quality impacts identified at the Site. Based on these discussions, Anchor QEA
proposes to continue collecting an additional metals sample, filtered through a 0.45-micron
groundwater filter, from MW-04CD.
Anchor QEA will continue to monitor the groundwater and surface water on a semiannual basis at
the Polk County C&D and MSW Landfills. The next sampling event is scheduled for September 2017.

Spring 2017 Semiannual Water Quality Report 16 June 2017
6 References
Altamont (Altamont Environmental, Inc.), 2011. Fall 2011 Semiannual Water Quality Monitoring
Report. February 7, 2013.
Altamont, 2016. Spring 2016 Semiannual Water Quality Monitoring Report. July 11, 2016.
DENR (North Carolina Department of Environment and Natural Resources), 2015. Relocation of MW-
03CD and MW-1R Approval – Polk County C&D and MSW Landfill, Route 9, Permit No. 75-02, Doc ID
No. 24963. September 8, 2015.
EPA (U.S. Environmental Protection Agency), revised 2013. SESD Operating Procedure: Groundwater
Sampling. March 6, 2013.
Puls, R.W., and M. J. Barcelona, 1996. Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures, United States Environmental Protection Agency, OSWER, EPA/540/S-95/504.

Tables
Table 1
Summary of Groundwater Elevation Data - March 2017
Spring 2017 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
June 2017
(feet)(feet TOC)(feet)
MW-01CD 2,955.50 110.73 2,844.77
MW-02CD 2,951.90 118.58 2,833.32
MW-03CD 2,969.60 118.90 2,850.70
MW-04CD NM 134.46 NA
MW-1R 2,867.70 29.63 2,838.07
MW-2R 2,837.20 34.21 2,802.99
MW-3R 2,962.00 78.57 2,883.43
MW-4 NM 11.63 NA
Notes:
C&D
MSW
Elevation Datum
Well Survey
MW-4 & MW-04CD
Depth to Water
NM Not measured
NA Not available
Monitoring wells MW-1R and MW-2R were surveyed on November 13, 2010. MW-3R was
surveyed on November 8, 2012. Remaining wells were surveyed on December 9, 2006. All
wells were surveyed by Wes Cole Land Surveying, PA.
All elevations were based on an assumed datum of 3,000 feet.
Installed in January 2016. These wells have not yet been surveyed.
Measured on March 7, 8 or 9, 2017.
Construction and Demolition
Municipal Solid Waste
Well ID
Depth
to
Water
Groundwater Elevation
C&D Landfill
MSW Landfill
Top of Casting
Elevation (From
Assumed Datum)
Table 2
Summary of Laboratory Analyses Performed on Samples
Spring 2017 Semiannual Water Quality Monitoring Report
Polk county Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
June 2017
GROUNDWATER SAMPLES
VOCs
EPA 8260B EPA 60101D EPA 6020B EPA 7470A
75-02 MW-01CD 3/8/2017 X X X X
75-02 MW-02CD 3/8/2017 X X X X
75-02 MW-04CD 3/8/2017 X X X X
75-02 MW-04CD (Filtered)3/8/2017 X X X
75-02 MW-04CD (No-Purge)3/8/2017 X X X
75-02 MW-2R 3/9/2017 X X X X
75-02 MW-2RDUP 3/9/2017 X X X X
75-02 MW-3R 3/8/2017 X X X X
75-02 MW-4 3/8/2017 X X X X
SURFACE WATER SAMPLES
VOCs
EPA 8260B EPA 60101D EPA 6020B EPA 7470A
75-02 SP-1 3/9/2017 X X X X
75-02 SS-1 3/9/2017 X X X X
75-02 SS-2 3/9/2017 X X X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
75-02 TRIP BLANK 3/9/2017 X
Notes:
VOCs
Analyses
MW-04CD and
MW-4
MSW Landfill
Facility
Permit Well ID Collect Date
Metals
C&D Landfill
Facility
Permit Well ID Collect Date
Metals
C&D Landfill
Well ID Collect Date
Volatile organic compounds
VOCs and metals analyses include Appendix I constituents per 40 CFR Part 258.
Installed in January 2016. These wells each replaced monitoring wells MW-03CD and MW-1R, respectively.
Facility
Permit
Table 3
Summary of Detected Constituents
Spring 2017 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
June 2017
Laboratory Certification 5445 (pH only)
Laboratory Methods
Parameter Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Mercury Nickel Selenium Vanadium Zinc
1,1-Dichloro-
ethane Acetone
cis-1,2-
Dichloro-
ethene
Trichloro-
ethene pH Turbidity
Dissolved
Oxygen Temperature
Specific
Conductivity
Oxidation
Reduction
Potential
CAS Number 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-97-6 7440-02-0 7782-49-2 7440-62-2 7440-66-6 75-34-3 67-64-1 156-59-2 79-01-6 SW320 SW330 7782-44-7 SW325 SW323 SW336
SWS ID 14 15 23 34 51 53 54 131 132 152 183 209 213 75 100 78 201 320 330 356 325 323 336
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU mg/L °C µS/cm mV
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Groundwater Samples
C&D Landfill
MW-01CD 3/8/2017 8.60 U 96.6 J 0.467 J 0.500 U 3.00 U 2.89 J 5.8 J 9.2 J 0.100 U 3.00 U 5.00 U 11.8 J 9.23 J 0.240 U 2.66 U 0.210 U 0.200 U 6.20 173 3.95 15.49 158 165.0
MW-02CD 3/8/2017 13.2 500 1.36 J 0.500 U 4.5 J 6.96 J 5.1 J 28.2 0.113 J 3.6 J 5.00 U 26.0 33.5 0.240 U 2.66 U 0.210 U 0.200 U 6.10 >1100 9.25 14.33 25 181.1
MW-04CD 3/8/2017 8.60 U 1,410 4.34 1.1 168 51.5 95.7 62.4 0.335 48.3 5.3 J 152 253 0.240 U 2.66 U 0.210 U 0.200 U 5.90 >1100 4.12 14.44 162 211.5
MW-04CD (Filtered)3/8/2017 8.60 U 182 0.100 U 0.500 U 3.00 U 0.453 J 5.00 U 2.00 U 0.100 U 3.00 U 5.00 U 1.23 J, B 19.7 J, B NA NA NA NA NA NA NA NA NA NA
MW-04CD (No-Purge)3/8/2017 8.60 U 232 0.190 J 0.500 U 7.6 J 2.39 J 5.00 U 6.1 J 0.100 U 3.00 U 5.00 U 13.9 J 23.9 J NA NA NA NA NA NA NA NA NA NA
MSW Landfill
MW-2R 3/9/2017 8.60 U 215 0.100 U 0.500 U 3.00 U 0.100 U 5.00 U 2.8 J 0.100 U 3.00 U 5.00 U 6.20 J 5.20 U 0.440 J 2.66 U 15.7 0.807 J 5.94 0.65 3.86 14.12 207 308.8
MW-2RDUP 3/9/2017 8.60 U 212 0.100 U 0.500 U 3.00 U 0.100 U 5.00 U 3.0 J 0.100 U 3.00 U 5.00 U 6.46 J 5.20 U 0.456 J 2.66 U 15.5 0.761 J 5.94 0.65 3.86 14.12 207 308.8
MW-3R 3/8/2017 8.60 U 8.1 J 0.100 U 0.500 U 3.00 U 0.124 J 5.00 U 2.0 J 0.100 U 3.00 U 5.00 U 5.54 J 5.20 U 0.240 U 2.66 U 0.210 U 0.200 U 6.66 0.65 5.94 20.01 75 141.1
MW-4 3/8/2017 8.60 U 310 0.100 U 0.500 U 3.00 U 0.328 J 5.00 U 3.0 J 0.100 U 3.00 U 5.00 U 6.18 J 5.20 U 0.240 U 2.66 U 0.941 J 0.200 U 5.70 2.05 1.52 15.94 184 188.8
Surface Water Samples
SP-1 3/9/2017 8.60 U 144 0.100 U 0.500 U 3.00 U 0.536 J 5.00 U 2.00 U 0.100 U 3.00 U 5.00 U 5.61 J 5.20 U 0.240 U 2.66 U 0.210 U 0.200 U 6.70 1.94 7.61 15.41 136 223.0
SS-1 3/9/2017 8.60 U 37.6 J 0.100 U 0.500 U 3.00 U 0.243 J 5.00 U 2.00 U 0.100 U 3.00 U 5.00 U 6.10 J 5.20 U 0.240 U 2.66 U 0.210 U 0.200 U 6.90 5.51 9.82 11.12 45 166.4
SS-2 3/9/2017 8.60 U 40.8 J 0.100 U 0.500 U 3.00 U 0.553 J 5.00 U 2.9 J 0.100 U 3.00 U 5.00 U 7.84 J 5.20 U 0.240 U 2.66 U 0.210 U 0.200 U 6.93 7.26 10.55 9.49 43 259.2
Quality Control Samples
TripBlank 3/9/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA 0.240 U 3.51 J 0.210 U 0.200 U NA NA NA NA NA NA
MDL 8.60 5.00 0.100 0.500 3.00 0.100 5.00 2.00 0.100 3.00 5.00 0.700 5.20 0.240 2.66 0.210 0.200 NA NA NA NA NA NA
MRL 10 10 2.0 1.0 5.0 2.0 10 5.0 0.20 10 10 2.0 25 1.0 25 1.0 1.0 NA NA NA NA NA NA
SWSL 10 100 1 1 10 10 10 10 0.2 50 10 25 10 5 100 5 1 NE NE NE NE NE NE
2L 10 700 NE 2 10 NE 1,000 15 1 100 20 NE 1,000 6 6,000 70 3 6.5-8.5 NE NE NE NE NE
IMAC NE NE 4 NE NE 1 NE NE NE NE NE 0.3 NE NE NE NE NE NE NE NE NE NE NE
GWP NE NE 4 NE NE 1 NE NE NE NE NE 0.3 NE NE NE NE NE NE NE NE NE NE NE
2B 10 200,000 6.5 0.15 35 4 2.7 0.54 0.012 16 5 NE 36 100 2,000 720 3 6.0-9.0 25 > 5.0 NE NE NE
Notes:
Parameters Only detected constituents are listed on this table. Please refer to TestAmerica Report of Laboratory Analysis (Appendix B) for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Anchor QEA.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for a compound that was found in both the laboratory blank and the sample.
2L
IMAC Interim maximum allowable concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
GWP
2B
NE Not Established
NA Not Applicable
500 Indicates a result in exceedance of the SWSL.
13.2 Indicates a result in exceedance of the 2L, IMAC, GWP, or 2B standard.
>1100 Indicates the turbidity readings was above the range of the turbidity meter.
MW-04CD (Filtered)One field-filtered sample was collected from MW-04CD and analyzed for Appendix I Metals to determine concentrations of dissolved metals.
MW-04CD (No-Purge)A no-purge sample was collected from MW-04CD by gently lowering a disposable bailer through the water column in order to minimize sediment disturbance.
EPA 6010D, EPA 6020B, EPA 7470A
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ (Amended April 1, 2013).
Groundwater Protection standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-section/environmental-monitoring/environmental-monitoring-list (last updated June, 2011). GWP
standard is used only if 2L or IMAC standards are not established for specific constituent.
Surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards," (last amended March, 2016) or standard obtained from National Criteria per EPA table (current as of May 15, 2013).
VOCs (Appendix I)
387
EPA 8260B
Field ParametersMetals (Appendix I)
387
Table 4
VOCs Background Well Comparison
Spring 2017 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 1
June 2017
Min.Max.Avg.
1/10 Acetone 1.41 U 10 U 2.88 6,000
8/10 Trichlorofluoromethane 0.21 U 0.65 J 0.36 2,000
1/6 Acetone 2.53 J 2.66 U 1.57 6,000
3/6 Trichlorofluoromethane 0.210 U 0.42 J 0.24 2,000
1/6 Xylene (Total)0.38 U 0.58 U 0.30 500
1/7 1,2-Dichlorobenzene 0.12 U 0.30 U 0.14 20
2/7 1,4-Dichlorobenzene 0.288 J 0.463 U 0.22 6
2/7 Acetone 2.66 U 10 U 4.12 6,000
2/6 Tetrahydrofuran 2.53 J 7.04 J 2.63 NE
7/7 Trichlorofluoromethane 0.301 J 0.52 J 0.39 2,000
1/7 Xylene (Total)0.38 U 0.66 U 0.34 500
2/3 Tetrahydrofuran 1.46 J 2.91 J 1.59 NE
1/3 Trichlorofluoromethane 0.21 U 0.496 J 0.27 2,000
1/7 1,4-Dichlorobenzene 0.17 J 0.33 U 0.14 6
2/7 cis-1,2-Dichloroethene 0.19 U 2.0 J 0.62 70
1/7 Tetrahydrofuran 0.82 U 3.1 U 1.39 NE
15/19 1,1-Dichloroethane 0.24 U 1.06 J 0.54 6
18/19 cis-1,2-Dichloroethene 5.2 15.7 11.16 70
3/19 Tetrachloroethene 0.14 U 0.46 U 0.15 0.7
18/19 Trichloroethene 0.47 U 1.56 0.92 3
1/19 Vinyl chloride 0.1 J 0.62 U 0.17 0.03
0/10 1,1-Dichloroethane 0.215 U 0.32 U 0.13 6
0/10 1,2-Dichlorobenzene 0.19 U 2.5 U 0.23 20
0/10 1,4-Dichlorobenzene 0.17 U 0.463 U 0.13 6
0/10 cis-1,2-Dichloroethene 0.19 U 0.299 U 0.11 70
0/10 Acetone 1.41 U 10 U 2.74 6,000
0/10 Tetrachloroethene 0.14 U 0.46 U 0.14 0.7
0/10 Tetrahydrofuran 0.82 U 3.1 U 0.92 NE
0/10 Trichloroethene 0.2 U 0.47 U 0.16 3
0/10 Trichlorofluoromethane 0.139 U 0.48 U 0.11 2,000
0/10 Vinyl chloride 0.18 U 0.62 U 0.18 0.03
0/10 Xylene (Total)0.298 U 0.66 U 0.28 500
2/3 1,4-Dichlorobenzene 0.17 U 0.530 J 0.31 6
3/3 cis-1,2-Dichloroethene 0.941 J 1.71 J 1.31 70
2/3 Chlorobenzene 0.18 U 0.347 J 0.23 50
1/3 Tetrahydrofuran 0.82 U 1.50 J 0.77 NE
Notes:
µg/L micrograms per liter
Min.minimum concentration (µg/L)
Max.maximum concentration (µg/L)
Avg.
2L
IMAC The IMAC concentrations listed in Appendix #1 of Subchapter 2L.
U A laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit (MDL).
J A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method reporting limit (MRL).
NA not applicable
# Detections
MW-02CD Only sampled six times due to a lack of well recharge during other sampling events.
MW-2R
MW-3R The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September 2012.
MW-4 and
MW-04CD Installed in January 2016 and were sampled for the first time during the March 2016 event.
MW-1R and
MW-03CD Not sampled after the installation of MW-4 and MW-04CD.
MW-2R (and
MW-2RDUP)
MW-3R
MW-2R had duplicate samples collected during 9 of the 10 sampling events, thus there are 19 total samples representing MW-2R.
Number of times the constituent was detected during the sample collection period.
MW-4
Average concentration (µg/L). Average concentrations were calculated by summing the constituent detections and dividing by the number of samples. When the sample
was below the MDL, half of the MDL value was used as the result. Results flagged with a "J" are estimated average concentrations.
Groundwater standard from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2L - Groundwater
Classifications and Standards," DENR (Amended April 1, 2013).
MW-1R
September 2012 to March 2017
Well # Detections Detected Constituents Concentration (µg/L)2L Standard or
IMAC
MW-01CD
MW-04CD
MW-03CD
MW-02CD
Table 5
Metals Background Well Comparison

Spring 2017 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 1 of 3
June 2017
Min.Max.Avg.
10/10 Barium 12.5 J 104 51.6 700
3/10 Beryllium 0.34 J 1.0 U 0.65 4
1/10 Cadmium 0.3 J 1.0 U 0.30 2
1/10 Chromium 2.5 U 5.0 U 3.66 10
3/10 Cobalt 0.5 U 5.0 U 3.4 1
4/10 Copper 2.5 U 8.30 J 5.52 1,000
5/10 Lead 2.0 U 9.2 J 10.9 15
1/10 Silver 2.5 U 5.02 J 4.99 20
2/10 Thallium 0.019 U 0.8 U 0.64 0.2
5/10 Vanadium 1.8 J 12.8 J 1.60 0.3
6/10 Zinc 9.23 J 105 15.6 1,000
1/6 Arsenic 3.69 U 13.2 5.26 10
6/6 Barium 41.0 J 627 306.9 700
3/6 Beryllium 0.5 U 1.58 J 0.83 4
2/6 Cadmium 0.3 J 1.5 0.47 2
4/6 Chromium 3.0 U 4.5 J 3.09 10
4/6 Cobalt 1.31 J 6.96 J 3.75 1
3/6 Copper 5.0 U 5.52 J 3.85 1,000
1/5 Mercury 0.1 U 0.15 U 0.07 1
5/6 Lead 2.0 U 30.7 15.9 15
3/6 Nickel 3.0 U 3.9 J 2.64 100
1/6 Silver 2.5 U 4.99 J 2.04 20
1/6 Thallium 0.2 U 0.8 U 0.35 0.2
5/6 Vanadium 1.6 J 43.6 18.4 0.3
5/6 Zinc 10 U 38.8 20.0 1,000
1/7 Arsenic 4.9 J 10 U 3.52 10
7/7 Barium 184 768 362.7 700
2/7 Beryllium 0.570 J 1.7 0.62 4
1/7 Cadmium 0.155 U 1.0 U 0.37 2
4/7 Chromium 3.0 U 20.3 6.89 10
3/7 Cobalt 1.43 J 10.1 3.79 1
4/7 Copper 5.0 U 21.8 8.80 1,000
4/7 Lead 5.0 U 18.6 7.42 15
4/7 Nickel 3.0 U 10.9 J 5.85 100
1/7 Silver 2.5 U 5.97 J 2.50 20
6/7 Thallium 0.026 J 0.644 J 0.23 0.2
7/7 Vanadium 4.0 J 54 16.3 0.3
7/7 Zinc 13.1 J 223 52.3 1,000
September 2012 to March 2017
Well # Detections
Detected
Constituents
Concentration (µg/L)2L Standard or
IMAC
MW-01CD
MW-03CD
MW-02CD
Table 5
Metals Background Well Comparison

Spring 2017 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 2 of 3
June 2017
Min.Max.Avg.
September 2012 to March 2017
Well # Detections
Detected
Constituents
Concentration (µg/L)2L Standard or
IMAC
3/3 Barium 645 3,130 1728 700
3/3 Beryllium 1.73 J 10.3 5.46 4
3/3 Cadmium 0.70 J 21 7.60 2
3/3 Chromium 58.8 417 214.6 10
3/3 Cobalt 23.9 125 66.8 1
3/3 Copper 35.2 278 136.3 1,000
1/3 Mercury 0.1 U 0.335 0.15 1
3/3 Lead 28.6 102 64.3 15
3/3 Nickel 25.9 114 62.7 100
1/3 Selenium 5 U 50 U 10.9 20
1/3 Thallium 0.5 U 1.44 J 0.70 0.2
3/3 Vanadium 74.5 532 252.8 0.3
3/3 Zinc 90.0 784.0 375.7 1,000
1/7 Arsenic 2.5 U 25.6 5.94 10
7/7 Barium 41.4 J 2,270 350.7 700
3/7 Beryllium 0.50 U 13.3 2.33 4
3/7 Cadmium 0.3 J 5.8 1.36 2
3/7 Chromium 2.5 U 51.5 9.57 10
3/7 Copper 2.5 U 122 21.4 1,000
3/7 Lead 2.0 U 64.7 12.0 15
3/7 Nickel 2.5 U 29.1 J 6.81 100
1/7 Silver 2.5 U 5.0 U 2.36 20
3/7 Thallium 0.025 U 1.2 J 0.28 0.2
4/7 Vanadium 1.74 J 407 64.5 0.3
6/7 Zinc 10 U 428 12.2 1,000
19/19 Barium 63.3 J 217 161.8 700
1/19 Cadmium 0.155 U 1.0 U 0.31 2
2/19 Chromium 2.5 U 5.0 U 1.95 10
2/19 Copper 2.5 U 7.01 J 2.84 1,000
4/19 Lead 2.0 U 5.41 U 2.20 15
1/19 Nickel 2.5 U 5.0 U 1.86 100
2/19 Silver 2.5 U 5.88 J 2.11 20
1/19 Thallium 0.019 U 0.8 U 0.17 0.2
8/19 Vanadium 0.2 U 8.87 J 2.88 0.3
8/19 Zinc 5.2 U 25.1 9.54 1,000
MW-2R (and MW-
2RDUP)
MW-1R
MW-04CD
Table 5
Metals Background Well Comparison

Spring 2017 Semiannual Water Quality Monitoring Report
Polk County Construction and Demolition Debris Landfill and Municipal Solid Waste Landfill
Page 3 of 3
June 2017
Min.Max.Avg.
September 2012 to March 2017
Well # Detections
Detected
Constituents
Concentration (µg/L)2L Standard or
IMAC
0/10 Arsenic 2.5 U 10.0 U 3.39 10
9/10 Barium 3.25 J 12.3 J 7.13 700
0/10 Beryllium 0.1 U 1.0 U 0.29 4
1/10 Cadmium 0.04 J 1.0 U 0.30 2
1/10 Chromium 2.02 J 5.0 U 1.83 10
1/10 Cobalt 0.124 J 5.0 U 1.61 1
0/10 Copper 0.672 U 5.0 U 2.16 1,000
2/10 Lead 2.0 U 5.41 U 2.02 15
0/10 Nickel 2.5 U 5.0 U 1.78 100
0/10 Silver 1.05 U 5.0 U 1.63 20
0/10 Thallium 0.019 U 0.8 U 0.16 0.2
4/10 Vanadium 0.2 U 8.27 J 2.70 0.3
0/10 Zinc 2.26 U 10.0 U 3.36 1,000
3/3 Barium 297 318 308 700
3/3 Cobalt 0.328 J 2.38 J 1.18 1
1/3 Lead 2.0 U 3.0 J 1.67 15
3/3 Vanadium 3.3 J 11.5 J 6.99 0.3
Notes:
µg/L micrograms per liter
Min.Minimum concentration (µg/L)
Max.Maximum concentration (ug/L)
Avg.
2L
IMAC Interim maximum allowable concentration. Concentrations are listed in Appendix #1 of the 2L.
U
J
NA not applicable
# Detections
1.85 Indicates result above 2L Standard or IMAC.
MW-02CD
MW-3R
MW-4 and MW-04CD
MW-1R and MW-03CD Monitoring wells MW-1R and MW-03CD are not sampled after the installation of MW-4 and MW-04CD.
Number of times the constituent was detected during the sample collection period. MW-2R had duplicate samples
collected during 9 of the 10 sampling events, thus there are 19 total samples representing MW-2R.
MW-02CD has only been sampled six times due to a lack of well recharge during subsequent sampling events.
The first sample collected from MW-3R during the sample collection period was collected in October 2012, not September
2012.
Monitoring wells MW-4 and MW-04CD were installed in January 2016 and were sampled for the first time during the March
2016 event.
MW-3R
MW-4
Average concentration (µg/L). Average concentrations were calculated by summing the constituent detections and dividing
by the number of samples. When the sample was below the MDL, half of the MDL value was used as the result. Results
flagged with a "J" are estimated averages.
Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environment and Natural
Resources, Subchapter 2L - Groundwater Classifications and Standards," DENR (Amended April 1, 2013).
A laboratory data qualifier used for parameters not detected at concentrations above the laboratory method detection limit
(MDL).
A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the method
reporting limit (MRL).

Figures
[0 2,0001,000
Feet
LEGEND:
Landfill Site Boundary
Publish Date: 2017/03/13, 9:15 AM | User: alesueurFilepath: P:\Projects\Polk County\Route 9 LF\Figures\GIS\MXD\2017\7502March2017 Figure 1-Site Location Map AQ.mxd
Figure 1Site Location Map
Polk County Route 9 Landfill Water Quality ReportPolk County C&D and MSW Landfills, Permit #75-02, Polk County, NC
SOURCE(S):Basemap: USGS 1:24,000 Scale Topo Maps, Mill Spring,North Carolina Quadrangle, 1990.Parcels: Polk County GIS
Anchor QEA of North Carolina, PLLC
@A@A
@A
@A
@A
@A
@A
@A #*
#*
#*
Transfer Station
Scale Station
Inactive C & D Landfill
Inactive ClosedMSW Landfill Cell
Inactive ClosedMSW Landfill Cell
LittleLittleWhiteoakWhiteoakCreekCreek
L i t t l e W h i t e o a k C r e e k
L i t t l e W h i t e o a k C r e e k
I n t e r m i t t e n t S t r e a m
I n t e r m i t t e n t S t r e a m
I n t e r m i t t e n t S t r e a m
I n t e r m i t t e n t S t r e a m
1 0 2 0
1 0 6 0
9 4 0
1
0
4
0
1 0 6 0
1060
1 0 8 0
1100
1 0 4 0
1 0 4 0
1100
1
0
2
0
1
0
2
0
1 0 6 0
1 0 6 0 1060
1060
1 1 4 0
10 2 0
1100
1080
1 0 8 0
1040
9
4
0
1060
1
0
8
0
1 0 4 0
1
0
4
0
1120
1080
1 0 4 0
1100
1120
1040
9 6 0
1 1 20
1 020
1 0 6 0
1 0 0 0
1 0 2 0
1 0 2 0
1
0
2
0
1060
1080
1100
1 0 4 0
1000
1080
1060
9 6 0
1 0 0 0
9 8 0
1040
NC 9 HWY
GREEN HILLS RD
L A K E
A D G E R
P K W Y
L I T T L E
F A R M L N
G A R R E T T R D
KELSEY LN
LANDFILL RD
MART IN WALKER RD
B
U
R
T

B
L
A
C
K
W
E
L
L

R
D
MW-01CD
MW-02CD
MW-03CD
MW-1R
MW-2R
MW-3R
MW-4
MW-04CD SP-01
SS-1
SS-2
[0 700350
Feet
NOTE(S):-Background monitoring well MW-3Rwas installed on September 25, 2012.-Monitoring wells MW-04CD andMW-4 were installed January 4 toJanuary 11, 2016.-Locations of MW-04CD and MW-4are approximate.
LEGEND:
#*Surface Water Sample Locations
@A Monitoring Well Locations
Landfill Site Boundary
Creeks and Streams
20-Foot Interval Contours
Polk County Roads
Publish Date: 2017/05/22, 9:40 AM | User: alesueurFilepath: P:\Polk County\Route 9 LF\Figures\GIS\MXD\2017\7502March2017 Figure 2-Site Layout Map AQ.mxd
Figure 2Site Layout Map
Polk County Route 9 Landfill Water Quality ReportPolk County C&D and MSW Landfills, Permit #75-02, Polk County, NC
SOURCE(S):Basemap: NC OneMap 2015Elevation Contours: NCDOT Lidar 2007Streams: NCDEQ Division of Water Quality DatabaseParcels: Polk County GIS
Anchor QEA of North Carolina, PLLC
%
%
%
#
I
#
I
#
I
@A@A
@A
@A
@A
@A
@A
@A
Transfer Station
Scale Station
Inactive C & D Landfill
Inactive ClosedMSW Landfill Cell
Inactive ClosedMSW Landfill Cell
KELSE
Y

L
N
N NC
9

H
W
Y
GARR
E
T
T

R
D
G
R
E
E
N

H
I
L
L
S

R
D
LANDFILL RD
B
U
R
T

B
L
A
C
K
W
E
L
L

R
D
IN
T
E
R
M
I
T
T
E
N
T

S
T
R
E
A
M
IN
T
E
R
M
I
T
T
E
N
T

S
T
R
E
A
M
LITTLELITTLEWHITEOAKWHITEOAKCREEKCREEK
MW-01CD
(2,844.77 ft)
MW-02CD
(2,833.32 ft)
MW-03CD
(2,850.70 ft)
MW-1R
(2,838.07 ft)
MW-2R
(2,802.99 ft)MW-3R
(2,883.43 ft)
MW-4
MW-04CD
SP-01
SS-1
SS-2
[0 600300
Feet
NOTE(S):-All water level elevations based onassumed datum of 3,000 feet.Groundwater elevation is calculated fromdepth to water measurements collectedMarch 7, 8, and 9, 2017.-Monitoring wells MW-04CD and MW-4were installed January 2016 and have notyet been surveyed.
LEGEND:
Landfill Parcel Boundary
@A Monitoring Well Location
#
I
Surface Water Sample Location
Groundwater Flow Direction
Elevation Contours (20-ft Interval)
Streams
Roads
Publish Date: 2017/05/22, 9:49 AM | User: alesueurFilepath: P:\Polk County\Route 9 LF\Figures\GIS\MXD\2017\7502March2017 Figure 3-GW Contour Map AQ.mxd
Figure 3Groundwater Elevation Map
Polk County Route 9 Landfill Water Quality ReportPolk County C&D and MSW Landfills, Permit #75-02, Polk County, NC
SOURCE(S):Basemap: NC OneMap 2015Elevation Contours: NCDOT Lidar 2007Streams: NCDEQ Division of Water Quality Database.Parcels: Polk County GIS
Anchor QEA of North Carolina, PLLC

Appendix A
Sampling Logs and Equipment
Documentation and Instrument
Calibration Data Sheets

Appendix B
Report of Laboratory Analysis and
Chain-of-Custody Documentation
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-123577-1
Client Project/Site: Polk County Route 9 Landfill
For:
Anchor QEA of North Carolina PLLC
231 W Haywood Street
Asheville, North Carolina 28801
Attn: Brian Gant
Authorized for release by:
3/31/2017 7:31:07 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
TestAmerica Job ID: 490-123577-1
Page 2 of 68 TestAmerica Nashville3/31/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68
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Sample Summary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-123577-1 MW-01CD Water 03/08/17 11:54 03/11/17 10:05
490-123577-2 MW-04CD Water 03/08/17 09:51 03/11/17 10:05
490-123577-3 MW-4 Water 03/08/17 13:27 03/11/17 10:05
490-123577-4 MW-2R Water 03/09/17 10:26 03/11/17 10:05
490-123577-5 MW-2RDUP Water 03/09/17 10:26 03/11/17 10:05
490-123577-6 MW-3R Water 03/08/17 14:00 03/11/17 10:05
490-123577-7 SP-1 Water 03/09/17 11:30 03/11/17 10:05
490-123577-8 SS-1 Water 03/09/17 10:55 03/11/17 10:05
490-123577-9 SS-2 Water 03/09/17 11:10 03/11/17 10:05
490-123577-10 Trip Blank Water 03/09/17 00:01 03/11/17 10:05
490-123577-11 MW-02CD Water 03/08/17 10:49 03/11/17 10:05
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Case Narrative
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-1
Project/Site: Polk County Route 9 Landfill
Job ID: 490-123577-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-123577-1
Comments
No additional comments.
Receipt
The samples were received on 3/11/2017 10:05 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 0.3º C.
GC/MS VOA
Method 8260B: Samples were received in unpreserved vials. MW-01CD (490-123577-1), MW-04CD (490-123577-2), MW-4
(490-123577-3), MW-2R (490-123577-4), MW-2RDUP (490-123577-5), MW-3R (490-123577-6), SP-1 (490-123577-7), SS-1
(490-123577-8), SS-2 (490-123577-9), Trip Blank (490-123577-10), and MW-02CD (490-123577-11)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 3005A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-417947.
Method 6010D: The continuing calibration verification (CCV) associated with batch 490-416586 recovered above the upper control limit for
Chromium and Cadmium. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have
been reported. The following samples are impacted: (LCS 490-416007/2-A), (LCSD 490-416007/3-A), (MB 490-416007/1-A),
(490-123702-H-1-A), (490-123702-H-1-B MS), (490-123702-H-1-C MSD), (490-123702-H-1-A PDS) and (490-123702-H-1-A SD).
Method 6010D: The low level check standard recovery associated with batch <490-418310> is outside the acceptance criteria for the
following analyte(s): Lead. Sample result was greater than 10x the RL therefore the data has been qualified and reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Field Service / Mobile Lab
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 03/08/17 11:54
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 18:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/20/17 18:39 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/20/17 18:39 1Benzene<0.200
1.00 0.150 ug/L 03/20/17 18:39 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/20/17 18:39 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/20/17 18:39 1Bromoform<0.290
1.00 0.350 ug/L 03/20/17 18:39 1Bromomethane<0.350
50.0 2.64 ug/L 03/20/17 18:39 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/20/17 18:39 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/20/17 18:39 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/20/17 18:39 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/20/17 18:39 1Chloroethane<0.360
1.00 0.230 ug/L 03/20/17 18:39 1Chloroform<0.230
1.00 0.360 ug/L 03/20/17 18:39 1Chloromethane<0.360
1.00 0.210 ug/L 03/20/17 18:39 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/20/17 18:39 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/20/17 18:39 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/20/17 18:39 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/20/17 18:39 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/20/17 18:39 1Dibromomethane<0.450
1.00 0.190 ug/L 03/20/17 18:39 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/20/17 18:39 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/20/17 18:39 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/20/17 18:39 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/20/17 18:39 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/20/17 18:39 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/20/17 18:39 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/20/17 18:39 12-Hexanone <1.28
10.0 1.50 ug/L 03/20/17 18:39 1Iodomethane<1.50
5.00 1.00 ug/L 03/20/17 18:39 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/20/17 18:39 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/20/17 18:39 1Styrene<0.280
1.00 0.150 ug/L 03/20/17 18:39 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/20/17 18:39 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/20/17 18:39 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/20/17 18:39 1Toluene<0.170
5.00 0.460 ug/L 03/20/17 18:39 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/20/17 18:39 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/20/17 18:39 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/20/17 18:39 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/20/17 18:39 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/20/17 18:39 1Trichloroethene<0.200
1.00 0.210 ug/L 03/20/17 18:39 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/20/17 18:39 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/20/17 18:39 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/20/17 18:39 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/20/17 18:39 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-1Client Sample ID: MW-01CD
Matrix: WaterDate Collected: 03/08/17 11:54
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)98 70-130 03/20/17 18:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)104 03/20/17 18:39 170-130
1,2-Dichloroethane-d4 (Surr)97 03/20/17 18:39 170-130
Toluene-d8 (Surr)101 03/20/17 18:39 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:31 1Barium0.0966
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 18:31 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:31 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:31 1Copper0.00580 J
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 18:31 1Lead0.00920
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 18:31 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:31 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:31 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 05:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 05:48 1Beryllium0.467 J
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 05:48 1Cobalt2.89
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 05:48 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 05:48 1Vanadium11.8
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 05:48 1Zinc9.23 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-2Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 03/08/17 09:51
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 19:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/20/17 19:07 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/20/17 19:07 1Benzene<0.200
1.00 0.150 ug/L 03/20/17 19:07 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/20/17 19:07 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/20/17 19:07 1Bromoform<0.290
1.00 0.350 ug/L 03/20/17 19:07 1Bromomethane<0.350
50.0 2.64 ug/L 03/20/17 19:07 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/20/17 19:07 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/20/17 19:07 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/20/17 19:07 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/20/17 19:07 1Chloroethane<0.360
1.00 0.230 ug/L 03/20/17 19:07 1Chloroform<0.230
1.00 0.360 ug/L 03/20/17 19:07 1Chloromethane<0.360
1.00 0.210 ug/L 03/20/17 19:07 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/20/17 19:07 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/20/17 19:07 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/20/17 19:07 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/20/17 19:07 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/20/17 19:07 1Dibromomethane<0.450
1.00 0.190 ug/L 03/20/17 19:07 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/20/17 19:07 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/20/17 19:07 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/20/17 19:07 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/20/17 19:07 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/20/17 19:07 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/20/17 19:07 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/20/17 19:07 12-Hexanone <1.28
10.0 1.50 ug/L 03/20/17 19:07 1Iodomethane<1.50
5.00 1.00 ug/L 03/20/17 19:07 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/20/17 19:07 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/20/17 19:07 1Styrene<0.280
1.00 0.150 ug/L 03/20/17 19:07 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/20/17 19:07 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/20/17 19:07 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/20/17 19:07 1Toluene<0.170
5.00 0.460 ug/L 03/20/17 19:07 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/20/17 19:07 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/20/17 19:07 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/20/17 19:07 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/20/17 19:07 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/20/17 19:07 1Trichloroethene<0.200
1.00 0.210 ug/L 03/20/17 19:07 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/20/17 19:07 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/20/17 19:07 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/20/17 19:07 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/20/17 19:07 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-2Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 03/08/17 09:51
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)98 70-130 03/20/17 19:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 03/20/17 19:07 170-130
1,2-Dichloroethane-d4 (Surr)97 03/20/17 19:07 170-130
Toluene-d8 (Surr)99 03/20/17 19:07 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 18:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:36 1Barium1.41
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 18:36 1Cadmium0.00110
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:36 1Chromium0.168
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:36 1Copper0.0957
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 18:36 1Lead0.0624
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 18:36 1Nickel0.0483
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:36 1Selenium0.00530 J
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:36 1Silver<0.00300
Method: 6010D - Metals (ICP) - Dissolved
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/28/17 22:54 03/29/17 12:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/28/17 22:54 03/29/17 12:05 1Barium0.182
0.00100 0.000500 mg/L 03/28/17 22:54 03/29/17 12:05 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/28/17 22:54 03/29/17 12:05 1Chromium<0.00300
0.0100 0.00500 mg/L 03/28/17 22:54 03/29/17 12:05 1Copper<0.00500
0.00500 0.00200 mg/L 03/28/17 22:54 03/29/17 12:05 1Lead<0.00200
0.0100 0.00300 mg/L 03/28/17 22:54 03/29/17 12:05 1Nickel<0.00300
0.0100 0.00500 mg/L 03/28/17 22:54 03/29/17 12:05 1Selenium<0.00500
0.00500 0.00300 mg/L 03/28/17 22:54 03/29/17 12:05 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:05 1Beryllium4.34
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:05 1Cobalt51.5
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:05 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:05 1Vanadium152
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:05 1Zinc253
Method: 6020B - Metals (ICP/MS) - Dissolved
RL MDL
Antimony <0.000800 0.00200 0.000800 mg/L 03/28/17 22:56 03/31/17 16:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00200 0.000100 mg/L 03/28/17 22:56 03/31/17 16:24 1Beryllium<0.000100
0.00200 0.000100 mg/L 03/28/17 22:56 03/31/17 16:24 1Cobalt0.000453 J
0.00200 0.000800 mg/L 03/28/17 22:56 03/31/17 16:24 1Thallium<0.000800
0.00200 0.000700 mg/L 03/28/17 22:56 03/31/17 16:24 1Vanadium0.00123 J B
0.0250 0.00520 mg/L 03/28/17 22:56 03/31/17 16:24 1Zinc0.0197 J B
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury 0.335 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-2Client Sample ID: MW-04CD
Matrix: WaterDate Collected: 03/08/17 09:51
Date Received: 03/11/17 10:05
Method: 7470A - Mercury (CVAA) - Dissolved
RL MDL
Mercury <0.000100 0.000200 0.000100 mg/L 03/29/17 08:06 03/29/17 12:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-3Client Sample ID: MW-4
Matrix: WaterDate Collected: 03/08/17 13:27
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 19:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/20/17 19:36 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/20/17 19:36 1Benzene<0.200
1.00 0.150 ug/L 03/20/17 19:36 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/20/17 19:36 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/20/17 19:36 1Bromoform<0.290
1.00 0.350 ug/L 03/20/17 19:36 1Bromomethane<0.350
50.0 2.64 ug/L 03/20/17 19:36 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/20/17 19:36 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/20/17 19:36 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/20/17 19:36 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/20/17 19:36 1Chloroethane<0.360
1.00 0.230 ug/L 03/20/17 19:36 1Chloroform<0.230
1.00 0.360 ug/L 03/20/17 19:36 1Chloromethane<0.360
1.00 0.210 ug/L 03/20/17 19:36 1cis-1,2-Dichloroethene 0.941 J
1.00 0.170 ug/L 03/20/17 19:36 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/20/17 19:36 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/20/17 19:36 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/20/17 19:36 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/20/17 19:36 1Dibromomethane<0.450
1.00 0.190 ug/L 03/20/17 19:36 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/20/17 19:36 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/20/17 19:36 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/20/17 19:36 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/20/17 19:36 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/20/17 19:36 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/20/17 19:36 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/20/17 19:36 12-Hexanone <1.28
10.0 1.50 ug/L 03/20/17 19:36 1Iodomethane<1.50
5.00 1.00 ug/L 03/20/17 19:36 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/20/17 19:36 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/20/17 19:36 1Styrene<0.280
1.00 0.150 ug/L 03/20/17 19:36 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/20/17 19:36 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/20/17 19:36 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/20/17 19:36 1Toluene<0.170
5.00 0.460 ug/L 03/20/17 19:36 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/20/17 19:36 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/20/17 19:36 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/20/17 19:36 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/20/17 19:36 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/20/17 19:36 1Trichloroethene<0.200
1.00 0.210 ug/L 03/20/17 19:36 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/20/17 19:36 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/20/17 19:36 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/20/17 19:36 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/20/17 19:36 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-3Client Sample ID: MW-4
Matrix: WaterDate Collected: 03/08/17 13:27
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)98 70-130 03/20/17 19:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/20/17 19:36 170-130
1,2-Dichloroethane-d4 (Surr)92 03/20/17 19:36 170-130
Toluene-d8 (Surr)100 03/20/17 19:36 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:41 1Barium0.310
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 18:41 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:41 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:41 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 18:41 1Lead0.00300 J
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 18:41 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:41 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:41 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:10 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:10 1Cobalt0.328 J
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:10 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:10 1Vanadium6.18
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:10 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 03/09/17 10:26
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 20:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/20/17 20:04 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/20/17 20:04 1Benzene<0.200
1.00 0.150 ug/L 03/20/17 20:04 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/20/17 20:04 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/20/17 20:04 1Bromoform<0.290
1.00 0.350 ug/L 03/20/17 20:04 1Bromomethane<0.350
50.0 2.64 ug/L 03/20/17 20:04 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/20/17 20:04 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/20/17 20:04 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/20/17 20:04 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/20/17 20:04 1Chloroethane<0.360
1.00 0.230 ug/L 03/20/17 20:04 1Chloroform<0.230
1.00 0.360 ug/L 03/20/17 20:04 1Chloromethane<0.360
1.00 0.210 ug/L 03/20/17 20:04 1cis-1,2-Dichloroethene 15.7
1.00 0.170 ug/L 03/20/17 20:04 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/20/17 20:04 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/20/17 20:04 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/20/17 20:04 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/20/17 20:04 1Dibromomethane<0.450
1.00 0.190 ug/L 03/20/17 20:04 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/20/17 20:04 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/20/17 20:04 11,1-Dichloroethane 0.440 J
1.00 0.200 ug/L 03/20/17 20:04 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/20/17 20:04 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/20/17 20:04 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/20/17 20:04 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/20/17 20:04 12-Hexanone <1.28
10.0 1.50 ug/L 03/20/17 20:04 1Iodomethane<1.50
5.00 1.00 ug/L 03/20/17 20:04 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/20/17 20:04 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/20/17 20:04 1Styrene<0.280
1.00 0.150 ug/L 03/20/17 20:04 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/20/17 20:04 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/20/17 20:04 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/20/17 20:04 1Toluene<0.170
5.00 0.460 ug/L 03/20/17 20:04 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/20/17 20:04 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/20/17 20:04 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/20/17 20:04 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/20/17 20:04 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/20/17 20:04 1Trichloroethene0.807 J
1.00 0.210 ug/L 03/20/17 20:04 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/20/17 20:04 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/20/17 20:04 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/20/17 20:04 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/20/17 20:04 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-4Client Sample ID: MW-2R
Matrix: WaterDate Collected: 03/09/17 10:26
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)98 70-130 03/20/17 20:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/20/17 20:04 170-130
1,2-Dichloroethane-d4 (Surr)94 03/20/17 20:04 170-130
Toluene-d8 (Surr)101 03/20/17 20:04 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 18:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:46 1Barium0.215
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 18:46 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:46 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:46 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 18:46 1Lead0.00280 J
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 18:46 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:46 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:46 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:16 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:16 1Cobalt<0.100
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:16 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:16 1Vanadium6.20
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:16 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 03/09/17 10:26
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 20:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/20/17 20:32 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/20/17 20:32 1Benzene<0.200
1.00 0.150 ug/L 03/20/17 20:32 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/20/17 20:32 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/20/17 20:32 1Bromoform<0.290
1.00 0.350 ug/L 03/20/17 20:32 1Bromomethane<0.350
50.0 2.64 ug/L 03/20/17 20:32 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/20/17 20:32 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/20/17 20:32 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/20/17 20:32 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/20/17 20:32 1Chloroethane<0.360
1.00 0.230 ug/L 03/20/17 20:32 1Chloroform<0.230
1.00 0.360 ug/L 03/20/17 20:32 1Chloromethane<0.360
1.00 0.210 ug/L 03/20/17 20:32 1cis-1,2-Dichloroethene 15.5
1.00 0.170 ug/L 03/20/17 20:32 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/20/17 20:32 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/20/17 20:32 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/20/17 20:32 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/20/17 20:32 1Dibromomethane<0.450
1.00 0.190 ug/L 03/20/17 20:32 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/20/17 20:32 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/20/17 20:32 11,1-Dichloroethane 0.456 J
1.00 0.200 ug/L 03/20/17 20:32 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/20/17 20:32 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/20/17 20:32 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/20/17 20:32 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/20/17 20:32 12-Hexanone <1.28
10.0 1.50 ug/L 03/20/17 20:32 1Iodomethane<1.50
5.00 1.00 ug/L 03/20/17 20:32 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/20/17 20:32 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/20/17 20:32 1Styrene<0.280
1.00 0.150 ug/L 03/20/17 20:32 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/20/17 20:32 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/20/17 20:32 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/20/17 20:32 1Toluene<0.170
5.00 0.460 ug/L 03/20/17 20:32 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/20/17 20:32 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/20/17 20:32 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/20/17 20:32 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/20/17 20:32 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/20/17 20:32 1Trichloroethene0.761 J
1.00 0.210 ug/L 03/20/17 20:32 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/20/17 20:32 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/20/17 20:32 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/20/17 20:32 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/20/17 20:32 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-5Client Sample ID: MW-2RDUP
Matrix: WaterDate Collected: 03/09/17 10:26
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)99 70-130 03/20/17 20:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/20/17 20:32 170-130
1,2-Dichloroethane-d4 (Surr)93 03/20/17 20:32 170-130
Toluene-d8 (Surr)100 03/20/17 20:32 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 18:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:52 1Barium0.212
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 18:52 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:52 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:52 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 18:52 1Lead0.00300 J
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 18:52 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:52 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:52 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:21 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:21 1Cobalt<0.100
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:21 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:21 1Vanadium6.46
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:21 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 03/08/17 14:00
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/21/17 15:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/21/17 15:53 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/21/17 15:53 1Benzene<0.200
1.00 0.150 ug/L 03/21/17 15:53 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/21/17 15:53 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/21/17 15:53 1Bromoform<0.290
1.00 0.350 ug/L 03/21/17 15:53 1Bromomethane<0.350
50.0 2.64 ug/L 03/21/17 15:53 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/21/17 15:53 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/21/17 15:53 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/21/17 15:53 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/21/17 15:53 1Chloroethane<0.360
1.00 0.230 ug/L 03/21/17 15:53 1Chloroform<0.230
1.00 0.360 ug/L 03/21/17 15:53 1Chloromethane<0.360
1.00 0.210 ug/L 03/21/17 15:53 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/21/17 15:53 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/21/17 15:53 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/21/17 15:53 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/21/17 15:53 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/21/17 15:53 1Dibromomethane<0.450
1.00 0.190 ug/L 03/21/17 15:53 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/21/17 15:53 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/21/17 15:53 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/21/17 15:53 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/21/17 15:53 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/21/17 15:53 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/21/17 15:53 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/21/17 15:53 12-Hexanone <1.28
10.0 1.50 ug/L 03/21/17 15:53 1Iodomethane<1.50
5.00 1.00 ug/L 03/21/17 15:53 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/21/17 15:53 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/21/17 15:53 1Styrene<0.280
1.00 0.150 ug/L 03/21/17 15:53 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/21/17 15:53 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/21/17 15:53 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/21/17 15:53 1Toluene<0.170
5.00 0.460 ug/L 03/21/17 15:53 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/21/17 15:53 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/21/17 15:53 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/21/17 15:53 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/21/17 15:53 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/21/17 15:53 1Trichloroethene<0.200
1.00 0.210 ug/L 03/21/17 15:53 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/21/17 15:53 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/21/17 15:53 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/21/17 15:53 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/21/17 15:53 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-6Client Sample ID: MW-3R
Matrix: WaterDate Collected: 03/08/17 14:00
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)97 70-130 03/21/17 15:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/21/17 15:53 170-130
1,2-Dichloroethane-d4 (Surr)97 03/21/17 15:53 170-130
Toluene-d8 (Surr)101 03/21/17 15:53 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 18:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:57 1Barium0.00810 J
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 18:57 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:57 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:57 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 18:57 1Lead0.00200 J
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 18:57 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 18:57 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 18:57 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:27 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:27 1Cobalt0.124 J
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:27 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:27 1Vanadium5.54
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:27 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 03/09/17 11:30
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/21/17 16:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/21/17 16:21 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/21/17 16:21 1Benzene<0.200
1.00 0.150 ug/L 03/21/17 16:21 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/21/17 16:21 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/21/17 16:21 1Bromoform<0.290
1.00 0.350 ug/L 03/21/17 16:21 1Bromomethane<0.350
50.0 2.64 ug/L 03/21/17 16:21 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/21/17 16:21 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/21/17 16:21 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/21/17 16:21 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/21/17 16:21 1Chloroethane<0.360
1.00 0.230 ug/L 03/21/17 16:21 1Chloroform<0.230
1.00 0.360 ug/L 03/21/17 16:21 1Chloromethane<0.360
1.00 0.210 ug/L 03/21/17 16:21 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/21/17 16:21 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/21/17 16:21 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/21/17 16:21 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/21/17 16:21 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/21/17 16:21 1Dibromomethane<0.450
1.00 0.190 ug/L 03/21/17 16:21 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/21/17 16:21 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/21/17 16:21 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/21/17 16:21 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/21/17 16:21 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/21/17 16:21 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/21/17 16:21 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/21/17 16:21 12-Hexanone <1.28
10.0 1.50 ug/L 03/21/17 16:21 1Iodomethane<1.50
5.00 1.00 ug/L 03/21/17 16:21 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/21/17 16:21 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/21/17 16:21 1Styrene<0.280
1.00 0.150 ug/L 03/21/17 16:21 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/21/17 16:21 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/21/17 16:21 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/21/17 16:21 1Toluene<0.170
5.00 0.460 ug/L 03/21/17 16:21 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/21/17 16:21 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/21/17 16:21 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/21/17 16:21 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/21/17 16:21 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/21/17 16:21 1Trichloroethene<0.200
1.00 0.210 ug/L 03/21/17 16:21 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/21/17 16:21 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/21/17 16:21 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/21/17 16:21 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/21/17 16:21 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-7Client Sample ID: SP-1
Matrix: WaterDate Collected: 03/09/17 11:30
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)95 70-130 03/21/17 16:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 03/21/17 16:21 170-130
1,2-Dichloroethane-d4 (Surr)93 03/21/17 16:21 170-130
Toluene-d8 (Surr)101 03/21/17 16:21 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 19:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:02 1Barium0.144
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 19:02 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:02 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:02 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 19:02 1Lead<0.00200
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 19:02 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:02 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:02 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:32 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:32 1Cobalt0.536 J
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:32 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:32 1Vanadium5.61
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:32 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 03/09/17 10:55
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/21/17 16:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/21/17 16:49 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/21/17 16:49 1Benzene<0.200
1.00 0.150 ug/L 03/21/17 16:49 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/21/17 16:49 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/21/17 16:49 1Bromoform<0.290
1.00 0.350 ug/L 03/21/17 16:49 1Bromomethane<0.350
50.0 2.64 ug/L 03/21/17 16:49 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/21/17 16:49 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/21/17 16:49 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/21/17 16:49 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/21/17 16:49 1Chloroethane<0.360
1.00 0.230 ug/L 03/21/17 16:49 1Chloroform<0.230
1.00 0.360 ug/L 03/21/17 16:49 1Chloromethane<0.360
1.00 0.210 ug/L 03/21/17 16:49 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/21/17 16:49 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/21/17 16:49 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/21/17 16:49 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/21/17 16:49 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/21/17 16:49 1Dibromomethane<0.450
1.00 0.190 ug/L 03/21/17 16:49 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/21/17 16:49 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/21/17 16:49 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/21/17 16:49 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/21/17 16:49 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/21/17 16:49 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/21/17 16:49 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/21/17 16:49 12-Hexanone <1.28
10.0 1.50 ug/L 03/21/17 16:49 1Iodomethane<1.50
5.00 1.00 ug/L 03/21/17 16:49 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/21/17 16:49 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/21/17 16:49 1Styrene<0.280
1.00 0.150 ug/L 03/21/17 16:49 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/21/17 16:49 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/21/17 16:49 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/21/17 16:49 1Toluene<0.170
5.00 0.460 ug/L 03/21/17 16:49 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/21/17 16:49 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/21/17 16:49 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/21/17 16:49 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/21/17 16:49 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/21/17 16:49 1Trichloroethene<0.200
1.00 0.210 ug/L 03/21/17 16:49 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/21/17 16:49 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/21/17 16:49 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/21/17 16:49 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/21/17 16:49 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-8Client Sample ID: SS-1
Matrix: WaterDate Collected: 03/09/17 10:55
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)98 70-130 03/21/17 16:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 03/21/17 16:49 170-130
1,2-Dichloroethane-d4 (Surr)96 03/21/17 16:49 170-130
Toluene-d8 (Surr)100 03/21/17 16:49 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 19:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:07 1Barium0.0376
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 19:07 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:07 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:07 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 19:07 1Lead<0.00200
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 19:07 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:07 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:07 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:38 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:38 1Cobalt0.243 J
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:38 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:38 1Vanadium6.10
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:38 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 03/09/17 11:10
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 21:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/20/17 21:00 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/20/17 21:00 1Benzene<0.200
1.00 0.150 ug/L 03/20/17 21:00 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/20/17 21:00 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/20/17 21:00 1Bromoform<0.290
1.00 0.350 ug/L 03/20/17 21:00 1Bromomethane<0.350
50.0 2.64 ug/L 03/20/17 21:00 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/20/17 21:00 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/20/17 21:00 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/20/17 21:00 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/20/17 21:00 1Chloroethane<0.360
1.00 0.230 ug/L 03/20/17 21:00 1Chloroform<0.230
1.00 0.360 ug/L 03/20/17 21:00 1Chloromethane<0.360
1.00 0.210 ug/L 03/20/17 21:00 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/20/17 21:00 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/20/17 21:00 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/20/17 21:00 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/20/17 21:00 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/20/17 21:00 1Dibromomethane<0.450
1.00 0.190 ug/L 03/20/17 21:00 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/20/17 21:00 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/20/17 21:00 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/20/17 21:00 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/20/17 21:00 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/20/17 21:00 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/20/17 21:00 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/20/17 21:00 12-Hexanone <1.28
10.0 1.50 ug/L 03/20/17 21:00 1Iodomethane<1.50
5.00 1.00 ug/L 03/20/17 21:00 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/20/17 21:00 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/20/17 21:00 1Styrene<0.280
1.00 0.150 ug/L 03/20/17 21:00 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/20/17 21:00 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/20/17 21:00 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/20/17 21:00 1Toluene<0.170
5.00 0.460 ug/L 03/20/17 21:00 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/20/17 21:00 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/20/17 21:00 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/20/17 21:00 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/20/17 21:00 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/20/17 21:00 1Trichloroethene<0.200
1.00 0.210 ug/L 03/20/17 21:00 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/20/17 21:00 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/20/17 21:00 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/20/17 21:00 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/20/17 21:00 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-9Client Sample ID: SS-2
Matrix: WaterDate Collected: 03/09/17 11:10
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)98 70-130 03/20/17 21:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)103 03/20/17 21:00 170-130
1,2-Dichloroethane-d4 (Surr)93 03/20/17 21:00 170-130
Toluene-d8 (Surr)100 03/20/17 21:00 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 19:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:13 1Barium0.0408
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 19:13 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:13 1Chromium<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:13 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 19:13 1Lead0.00290 J
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 19:13 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:13 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:13 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:43 1Beryllium<0.100
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:43 1Cobalt0.553 J
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:43 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:43 1Vanadium7.84
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:43 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/09/17 00:01
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 3.51 J 25.0 2.66 ug/L 03/21/17 02:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/21/17 02:12 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/21/17 02:12 1Benzene<0.200
1.00 0.150 ug/L 03/21/17 02:12 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/21/17 02:12 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/21/17 02:12 1Bromoform<0.290
1.00 0.350 ug/L 03/21/17 02:12 1Bromomethane<0.350
50.0 2.64 ug/L 03/21/17 02:12 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/21/17 02:12 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/21/17 02:12 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/21/17 02:12 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/21/17 02:12 1Chloroethane<0.360
1.00 0.230 ug/L 03/21/17 02:12 1Chloroform<0.230
1.00 0.360 ug/L 03/21/17 02:12 1Chloromethane<0.360
1.00 0.210 ug/L 03/21/17 02:12 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/21/17 02:12 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/21/17 02:12 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/21/17 02:12 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/21/17 02:12 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/21/17 02:12 1Dibromomethane<0.450
1.00 0.190 ug/L 03/21/17 02:12 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/21/17 02:12 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/21/17 02:12 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/21/17 02:12 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/21/17 02:12 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/21/17 02:12 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/21/17 02:12 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/21/17 02:12 12-Hexanone <1.28
10.0 1.50 ug/L 03/21/17 02:12 1Iodomethane<1.50
5.00 1.00 ug/L 03/21/17 02:12 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/21/17 02:12 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/21/17 02:12 1Styrene<0.280
1.00 0.150 ug/L 03/21/17 02:12 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/21/17 02:12 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/21/17 02:12 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/21/17 02:12 1Toluene<0.170
5.00 0.460 ug/L 03/21/17 02:12 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/21/17 02:12 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/21/17 02:12 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/21/17 02:12 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/21/17 02:12 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/21/17 02:12 1Trichloroethene<0.200
1.00 0.210 ug/L 03/21/17 02:12 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/21/17 02:12 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/21/17 02:12 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/21/17 02:12 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/21/17 02:12 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/09/17 00:01
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)99 70-130 03/21/17 02:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 03/21/17 02:12 170-130
1,2-Dichloroethane-d4 (Surr)96 03/21/17 02:12 170-130
Toluene-d8 (Surr)101 03/21/17 02:12 170-130
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-11Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 03/08/17 10:49
Date Received: 03/11/17 10:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/21/17 17:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 03/21/17 17:18 1Acrylonitrile<0.500
1.00 0.200 ug/L 03/21/17 17:18 1Benzene<0.200
1.00 0.150 ug/L 03/21/17 17:18 1Bromochloromethane<0.150
1.00 0.170 ug/L 03/21/17 17:18 1Bromodichloromethane<0.170
1.00 0.290 ug/L 03/21/17 17:18 1Bromoform<0.290
1.00 0.350 ug/L 03/21/17 17:18 1Bromomethane<0.350
50.0 2.64 ug/L 03/21/17 17:18 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 03/21/17 17:18 1Carbon disulfide <0.220
1.00 0.180 ug/L 03/21/17 17:18 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 03/21/17 17:18 1Chlorobenzene<0.180
1.00 0.360 ug/L 03/21/17 17:18 1Chloroethane<0.360
1.00 0.230 ug/L 03/21/17 17:18 1Chloroform<0.230
1.00 0.360 ug/L 03/21/17 17:18 1Chloromethane<0.360
1.00 0.210 ug/L 03/21/17 17:18 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 03/21/17 17:18 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 03/21/17 17:18 1Dibromochloromethane<0.250
10.0 0.940 ug/L 03/21/17 17:18 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 03/21/17 17:18 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 03/21/17 17:18 1Dibromomethane<0.450
1.00 0.190 ug/L 03/21/17 17:18 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 03/21/17 17:18 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 03/21/17 17:18 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 03/21/17 17:18 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 03/21/17 17:18 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 03/21/17 17:18 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 03/21/17 17:18 1Ethylbenzene<0.190
10.0 1.28 ug/L 03/21/17 17:18 12-Hexanone <1.28
10.0 1.50 ug/L 03/21/17 17:18 1Iodomethane<1.50
5.00 1.00 ug/L 03/21/17 17:18 1Methylene Chloride <1.00
10.0 0.810 ug/L 03/21/17 17:18 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 03/21/17 17:18 1Styrene<0.280
1.00 0.150 ug/L 03/21/17 17:18 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 03/21/17 17:18 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 03/21/17 17:18 1Tetrachloroethene<0.140
1.00 0.170 ug/L 03/21/17 17:18 1Toluene<0.170
5.00 0.460 ug/L 03/21/17 17:18 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 03/21/17 17:18 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 03/21/17 17:18 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 03/21/17 17:18 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 03/21/17 17:18 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 03/21/17 17:18 1Trichloroethene<0.200
1.00 0.210 ug/L 03/21/17 17:18 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 03/21/17 17:18 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 03/21/17 17:18 1Vinyl acetate <1.71
1.00 0.180 ug/L 03/21/17 17:18 1Vinyl chloride <0.180
3.00 0.580 ug/L 03/21/17 17:18 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-11Client Sample ID: MW-02CD
Matrix: WaterDate Collected: 03/08/17 10:49
Date Received: 03/11/17 10:05
4-Bromofluorobenzene (Surr)97 70-130 03/21/17 17:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 03/21/17 17:18 170-130
1,2-Dichloroethane-d4 (Surr)92 03/21/17 17:18 170-130
Toluene-d8 (Surr)100 03/21/17 17:18 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 0.0132 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 19:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:28 1Barium0.500
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 19:28 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:28 1Chromium0.00450 J
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:28 1Copper0.00510 J
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 19:28 1Lead0.0282
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 19:28 1Nickel0.00360 J
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:28 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:28 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:49 1Beryllium1.36 J
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:49 1Cobalt6.96
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:49 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:49 1Vanadium26.0
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:49 1Zinc33.5
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury 0.113 J 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-415705/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/20/17 13:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 03/20/17 13:56 1Acrylonitrile
<0.200 0.2001.00 ug/L 03/20/17 13:56 1Benzene
<0.150 0.1501.00 ug/L 03/20/17 13:56 1Bromochloromethane
<0.170 0.1701.00 ug/L 03/20/17 13:56 1Bromodichloromethane
<0.290 0.2901.00 ug/L 03/20/17 13:56 1Bromoform
<0.350 0.3501.00 ug/L 03/20/17 13:56 1Bromomethane
<2.64 2.6450.0 ug/L 03/20/17 13:56 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 03/20/17 13:56 1Carbon disulfide
<0.180 0.1801.00 ug/L 03/20/17 13:56 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 03/20/17 13:56 1Chlorobenzene
<0.360 0.3601.00 ug/L 03/20/17 13:56 1Chloroethane
<0.230 0.2301.00 ug/L 03/20/17 13:56 1Chloroform
<0.360 0.3601.00 ug/L 03/20/17 13:56 1Chloromethane
<0.210 0.2101.00 ug/L 03/20/17 13:56 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/20/17 13:56 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 03/20/17 13:56 1Dibromochloromethane
<0.940 0.94010.0 ug/L 03/20/17 13:56 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 03/20/17 13:56 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 03/20/17 13:56 1Dibromomethane
<0.190 0.1901.00 ug/L 03/20/17 13:56 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 03/20/17 13:56 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 03/20/17 13:56 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 03/20/17 13:56 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 03/20/17 13:56 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 03/20/17 13:56 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 03/20/17 13:56 1Ethylbenzene
<1.28 1.2810.0 ug/L 03/20/17 13:56 12-Hexanone
<1.50 1.5010.0 ug/L 03/20/17 13:56 1Iodomethane
<1.00 1.005.00 ug/L 03/20/17 13:56 1Methylene Chloride
<0.810 0.81010.0 ug/L 03/20/17 13:56 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 03/20/17 13:56 1Styrene
<0.150 0.1501.00 ug/L 03/20/17 13:56 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 03/20/17 13:56 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 03/20/17 13:56 1Tetrachloroethene
<0.170 0.1701.00 ug/L 03/20/17 13:56 1Toluene
<0.460 0.4605.00 ug/L 03/20/17 13:56 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 03/20/17 13:56 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/20/17 13:56 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 03/20/17 13:56 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 03/20/17 13:56 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 03/20/17 13:56 1Trichloroethene
<0.210 0.2101.00 ug/L 03/20/17 13:56 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 03/20/17 13:56 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 03/20/17 13:56 1Vinyl acetate
<0.180 0.1801.00 ug/L 03/20/17 13:56 1Vinyl chloride
<0.580 0.5803.00 ug/L 03/20/17 13:56 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-415705/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
4-Bromofluorobenzene (Surr)99 70-130 03/20/17 13:56 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 03/20/17 13:56 1Dibromofluoromethane (Surr)70-130
96 03/20/17 13:56 11,2-Dichloroethane-d4 (Surr)70-130
101 03/20/17 13:56 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415705/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
Acetone 100 105.0 ug/L 105 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 199.7 ug/L 100 63-135
Benzene 20.0 19.23 ug/L 96 70-130
Bromochloromethane 20.0 17.71 ug/L 89 70-130
Bromodichloromethane 20.0 18.49 ug/L 92 70-130
Bromoform 20.0 20.05 ug/L 100 70-137
Bromomethane 20.0 20.48 ug/L 102 53-150
2-Butanone (MEK)100 91.16 ug/L 91 55-143
Carbon disulfide 20.0 19.18 ug/L 96 64-135
Carbon tetrachloride 20.0 18.20 ug/L 91 70-147
Chlorobenzene 20.0 19.50 ug/L 97 70-130
Chloroethane 20.0 21.86 ug/L 109 60-138
Chloroform 20.0 17.74 ug/L 89 70-130
Chloromethane 20.0 23.74 ug/L 119 33-150
cis-1,2-Dichloroethene 20.0 18.77 ug/L 94 70-130
cis-1,3-Dichloropropene 20.0 20.15 ug/L 101 70-133
Dibromochloromethane 20.0 20.19 ug/L 101 70-133
1,2-Dibromo-3-Chloropropane 20.0 19.55 ug/L 98 45-138
1,2-Dibromoethane (EDB)20.0 18.99 ug/L 95 70-130
Dibromomethane 20.0 18.88 ug/L 94 70-130
1,2-Dichlorobenzene 20.0 19.74 ug/L 99 70-130
1,4-Dichlorobenzene 20.0 19.54 ug/L 98 70-130
1,1-Dichloroethane 20.0 18.59 ug/L 93 70-130
1,2-Dichloroethane 20.0 16.84 ug/L 84 70-130
1,1-Dichloroethene 20.0 19.43 ug/L 97 70-132
1,2-Dichloropropane 20.0 19.73 ug/L 99 70-130
Ethylbenzene 20.0 19.36 ug/L 97 70-130
2-Hexanone 100 100.0 ug/L 100 54-142
Iodomethane 20.0 20.86 ug/L 104 40-150
Methylene Chloride 20.0 19.16 ug/L 96 70-130
4-Methyl-2-pentanone (MIBK)100 98.61 ug/L 99 60-137
Styrene 20.0 19.20 ug/L 96 70-130
1,1,1,2-Tetrachloroethane 20.0 18.74 ug/L 94 70-130
1,1,2,2-Tetrachloroethane 20.0 20.90 ug/L 105 69-131
Tetrachloroethene 20.0 19.25 ug/L 96 70-130
Toluene 20.0 20.00 ug/L 100 70-130
trans-1,4-Dichloro-2-butene 20.0 17.50 ug/L 87 41-150
trans-1,2-Dichloroethene 20.0 19.15 ug/L 96 70-130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415705/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
trans-1,3-Dichloropropene 20.0 18.64 ug/L 93 63-142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 20.0 16.93 ug/L 85 70-135
1,1,2-Trichloroethane 20.0 19.46 ug/L 97 70-130
Trichloroethene 20.0 19.49 ug/L 97 70-130
Trichlorofluoromethane 20.0 18.05 ug/L 90 59-150
1,2,3-Trichloropropane 20.0 17.65 ug/L 88 70-131
Vinyl acetate 40.0 40.29 ug/L 101 54-146
Vinyl chloride 20.0 23.35 ug/L 117 57-137
Xylenes, Total 40.0 37.67 ug/L 94 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
94Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-415705/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
Acetone 100 94.69 ug/L 95 39-150 10 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 194.2 ug/L 97 63-135 3 16
Benzene 20.0 19.76 ug/L 99 70-130 3 12
Bromochloromethane 20.0 17.35 ug/L 87 70-130 2 16
Bromodichloromethane 20.0 18.23 ug/L 91 70-130 1 14
Bromoform 20.0 19.60 ug/L 98 70-137 2 14
Bromomethane 20.0 19.60 ug/L 98 53-150 4 19
2-Butanone (MEK)100 88.87 ug/L 89 55-143 3 19
Carbon disulfide 20.0 18.98 ug/L 95 64-135 1 16
Carbon tetrachloride 20.0 18.39 ug/L 92 70-147 1 16
Chlorobenzene 20.0 19.23 ug/L 96 70-130 1 12
Chloroethane 20.0 21.73 ug/L 109 60-138 1 15
Chloroform 20.0 17.62 ug/L 88 70-130 1 14
Chloromethane 20.0 22.39 ug/L 112 33-150 6 20
cis-1,2-Dichloroethene 20.0 18.83 ug/L 94 70-130 0 15
cis-1,3-Dichloropropene 20.0 19.57 ug/L 98 70-133 3 15
Dibromochloromethane 20.0 19.78 ug/L 99 70-133 2 13
1,2-Dibromo-3-Chloropropane 20.0 18.48 ug/L 92 45-138 6 19
1,2-Dibromoethane (EDB)20.0 18.99 ug/L 95 70-130 0 13
Dibromomethane 20.0 17.98 ug/L 90 70-130 5 14
1,2-Dichlorobenzene 20.0 19.37 ug/L 97 70-130 2 12
1,4-Dichlorobenzene 20.0 18.92 ug/L 95 70-130 3 12
1,1-Dichloroethane 20.0 18.53 ug/L 93 70-130 0 17
1,2-Dichloroethane 20.0 16.65 ug/L 83 70-130 1 13
1,1-Dichloroethene 20.0 18.83 ug/L 94 70-132 3 20
1,2-Dichloropropane 20.0 19.64 ug/L 98 70-130 0 15
Ethylbenzene 20.0 18.97 ug/L 95 70-130 2 12
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-415705/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
2-Hexanone 100 93.21 ug/L 93 54-142 7 17
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Iodomethane 20.0 19.68 ug/L 98 40-150 6 20
Methylene Chloride 20.0 18.67 ug/L 93 70-130 3 15
4-Methyl-2-pentanone (MIBK)100 94.34 ug/L 94 60-137 4 21
Styrene 20.0 18.75 ug/L 94 70-130 2 12
1,1,1,2-Tetrachloroethane 20.0 18.89 ug/L 94 70-130 1 13
1,1,2,2-Tetrachloroethane 20.0 20.74 ug/L 104 69-131 1 15
Tetrachloroethene 20.0 19.33 ug/L 97 70-130 0 17
Toluene 20.0 19.68 ug/L 98 70-130 2 13
trans-1,4-Dichloro-2-butene 20.0 16.68 ug/L 83 41-150 5 20
trans-1,2-Dichloroethene 20.0 19.03 ug/L 95 70-130 1 15
trans-1,3-Dichloropropene 20.0 18.72 ug/L 94 63-142 0 13
1,1,1-Trichloroethane 20.0 17.10 ug/L 86 70-135 1 15
1,1,2-Trichloroethane 20.0 19.46 ug/L 97 70-130 0 13
Trichloroethene 20.0 19.28 ug/L 96 70-130 1 14
Trichlorofluoromethane 20.0 17.40 ug/L 87 59-150 4 22
1,2,3-Trichloropropane 20.0 17.32 ug/L 87 70-131 2 14
Vinyl acetate 40.0 40.22 ug/L 101 54-146 0 20
Vinyl chloride 20.0 22.76 ug/L 114 57-137 3 15
Xylenes, Total 40.0 36.81 ug/L 92 70-132 2 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-124065-E-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
Acetone 6.47 J 100 104.4 ug/L 98 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 219.5 ug/L 110 50-135
Benzene <0.200 20.0 22.46 ug/L 112 55-147
Bromochloromethane <0.150 20.0 20.12 ug/L 101 59-132
Bromodichloromethane <0.170 20.0 21.04 ug/L 105 70-140
Bromoform <0.290 20.0 21.55 ug/L 108 53-150
Bromomethane <0.350 20.0 21.21 ug/L 106 30-150
2-Butanone (MEK)<2.64 100 98.10 ug/L 98 50-143
Carbon disulfide <0.220 20.0 21.67 ug/L 108 35-150
Carbon tetrachloride <0.180 20.0 21.60 ug/L 108 56-150
Chlorobenzene <0.180 20.0 22.00 ug/L 110 70-130
Chloroethane <0.360 20.0 25.11 ug/L 126 58-141
Chloroform <0.230 20.0 21.12 ug/L 106 66-138
Chloromethane <0.360 20.0 27.07 ug/L 135 10-150
cis-1,2-Dichloroethene <0.210 20.0 22.01 ug/L 110 68-131
cis-1,3-Dichloropropene <0.170 20.0 21.65 ug/L 108 70-133
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-124065-E-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
Dibromochloromethane <0.250 20.0 22.19 ug/L 111 66-140
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane <0.940 20.0 20.39 ug/L 102 38-138
1,2-Dibromoethane (EDB)<0.210 20.0 20.89 ug/L 104 65-137
Dibromomethane <0.450 20.0 21.12 ug/L 106 70-130
1,2-Dichlorobenzene <0.190 20.0 21.33 ug/L 107 70-130
1,4-Dichlorobenzene <0.170 20.0 21.19 ug/L 106 70-130
1,1-Dichloroethane <0.240 20.0 21.90 ug/L 110 61-139
1,2-Dichloroethane <0.200 20.0 19.24 ug/L 96 64-136
1,1-Dichloroethene <0.250 20.0 22.83 ug/L 114 54-150
1,2-Dichloropropane <0.250 20.0 22.04 ug/L 110 67-130
Ethylbenzene <0.190 20.0 21.78 ug/L 109 65-139
2-Hexanone <1.28 100 102.1 ug/L 102 44-150
Iodomethane <1.50 20.0 19.80 ug/L 99 34-150
Methylene Chloride <1.00 20.0 21.89 ug/L 109 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 102.9 ug/L 103 50-140
Styrene <0.280 20.0 21.44 ug/L 107 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 21.62 ug/L 108 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 22.98 ug/L 115 56-145
Tetrachloroethene <0.140 20.0 21.97 ug/L 110 57-138
Toluene <0.170 20.0 22.56 ug/L 113 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 18.54 ug/L 93 39-150
trans-1,2-Dichloroethene <0.230 20.0 22.27 ug/L 111 59-143
trans-1,3-Dichloropropene <0.170 20.0 20.20 ug/L 101 63-142
1,1,1-Trichloroethane <0.190 20.0 20.07 ug/L 100 68-144
1,1,2-Trichloroethane <0.190 20.0 21.71 ug/L 109 70-130
Trichloroethene <0.200 20.0 22.45 ug/L 112 63-135
Trichlorofluoromethane <0.210 20.0 20.30 ug/L 102 44-150
1,2,3-Trichloropropane <0.230 20.0 19.79 ug/L 99 65-131
Vinyl acetate <1.71 40.0 41.62 ug/L 104 43-146
Vinyl chloride <0.180 20.0 27.21 ug/L 136 57-150
Xylenes, Total <0.580 40.0 41.55 ug/L 104 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MS MS
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
871,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-124065-F-3 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
Acetone 6.47 J 100 97.54 ug/L 91 39-150 7 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 205.8 ug/L 103 50-135 6 23
Benzene <0.200 20.0 21.73 ug/L 109 55-147 3 22
Bromochloromethane <0.150 20.0 19.14 ug/L 96 59-132 5 21
Bromodichloromethane <0.170 20.0 19.91 ug/L 100 70-140 6 196
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-124065-F-3 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415705
Bromoform <0.290 20.0 20.43 ug/L 102 53-150 5 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromomethane <0.350 20.0 20.72 ug/L 104 30-150 2 44
2-Butanone (MEK)<2.64 100 90.00 ug/L 90 50-143 9 28
Carbon disulfide <0.220 20.0 21.22 ug/L 106 35-150 2 34
Carbon tetrachloride <0.180 20.0 20.55 ug/L 103 56-150 5 18
Chlorobenzene <0.180 20.0 20.87 ug/L 104 70-130 5 15
Chloroethane <0.360 20.0 24.48 ug/L 122 58-141 3 31
Chloroform <0.230 20.0 20.15 ug/L 101 66-138 5 21
Chloromethane <0.360 20.0 25.35 ug/L 127 10-150 7 43
cis-1,2-Dichloroethene <0.210 20.0 20.70 ug/L 103 68-131 6 21
cis-1,3-Dichloropropene <0.170 20.0 20.47 ug/L 102 70-133 6 19
Dibromochloromethane <0.250 20.0 20.84 ug/L 104 66-140 6 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 18.47 ug/L 92 38-138 10 26
1,2-Dibromoethane (EDB)<0.210 20.0 19.23 ug/L 96 65-137 8 21
Dibromomethane <0.450 20.0 19.67 ug/L 98 70-130 7 19
1,2-Dichlorobenzene <0.190 20.0 20.00 ug/L 100 70-130 6 15
1,4-Dichlorobenzene <0.170 20.0 19.68 ug/L 98 70-130 7 14
1,1-Dichloroethane <0.240 20.0 20.48 ug/L 102 61-139 7 23
1,2-Dichloroethane <0.200 20.0 17.94 ug/L 90 64-136 7 22
1,1-Dichloroethene <0.250 20.0 21.72 ug/L 109 54-150 5 24
1,2-Dichloropropane <0.250 20.0 21.45 ug/L 107 67-130 3 19
Ethylbenzene <0.190 20.0 20.67 ug/L 103 65-139 5 18
2-Hexanone <1.28 100 95.40 ug/L 95 44-150 7 21
Iodomethane <1.50 20.0 19.66 ug/L 98 34-150 1 37
Methylene Chloride <1.00 20.0 20.52 ug/L 103 64-130 6 22
4-Methyl-2-pentanone (MIBK)<0.810 100 97.22 ug/L 97 50-140 6 24
Styrene <0.280 20.0 20.17 ug/L 101 70-130 6 16
1,1,1,2-Tetrachloroethane <0.150 20.0 20.23 ug/L 101 70-131 7 16
1,1,2,2-Tetrachloroethane <0.190 20.0 21.09 ug/L 105 56-145 9 19
Tetrachloroethene <0.140 20.0 20.85 ug/L 104 57-138 5 17
Toluene <0.170 20.0 21.39 ug/L 107 64-136 5 18
trans-1,4-Dichloro-2-butene <0.460 20.0 17.34 ug/L 87 39-150 7 28
trans-1,2-Dichloroethene <0.230 20.0 20.95 ug/L 105 59-143 6 25
trans-1,3-Dichloropropene <0.170 20.0 19.03 ug/L 95 63-142 6 18
1,1,1-Trichloroethane <0.190 20.0 19.45 ug/L 97 68-144 3 17
1,1,2-Trichloroethane <0.190 20.0 20.57 ug/L 103 70-130 5 18
Trichloroethene <0.200 20.0 21.65 ug/L 108 63-135 4 17
Trichlorofluoromethane <0.210 20.0 20.28 ug/L 101 44-150 0 32
1,2,3-Trichloropropane <0.230 20.0 18.05 ug/L 90 65-131 9 19
Vinyl acetate <1.71 40.0 36.94 ug/L 92 43-146 12 20
Vinyl chloride <0.180 20.0 25.93 ug/L 130 57-150 5 37
Xylenes, Total <0.580 40.0 39.39 ug/L 98 69-132 5 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MSD MSD
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
981,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Client Sample ID: Method BlankLab Sample ID: MB 490-415793/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/21/17 01:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 03/21/17 01:43 1Acrylonitrile
<0.200 0.2001.00 ug/L 03/21/17 01:43 1Benzene
<0.150 0.1501.00 ug/L 03/21/17 01:43 1Bromochloromethane
<0.170 0.1701.00 ug/L 03/21/17 01:43 1Bromodichloromethane
<0.290 0.2901.00 ug/L 03/21/17 01:43 1Bromoform
<0.350 0.3501.00 ug/L 03/21/17 01:43 1Bromomethane
<2.64 2.6450.0 ug/L 03/21/17 01:43 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 03/21/17 01:43 1Carbon disulfide
<0.180 0.1801.00 ug/L 03/21/17 01:43 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 03/21/17 01:43 1Chlorobenzene
<0.360 0.3601.00 ug/L 03/21/17 01:43 1Chloroethane
<0.230 0.2301.00 ug/L 03/21/17 01:43 1Chloroform
<0.360 0.3601.00 ug/L 03/21/17 01:43 1Chloromethane
<0.210 0.2101.00 ug/L 03/21/17 01:43 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/21/17 01:43 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 03/21/17 01:43 1Dibromochloromethane
<0.940 0.94010.0 ug/L 03/21/17 01:43 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 03/21/17 01:43 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 03/21/17 01:43 1Dibromomethane
<0.190 0.1901.00 ug/L 03/21/17 01:43 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 03/21/17 01:43 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 03/21/17 01:43 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 03/21/17 01:43 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 03/21/17 01:43 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 03/21/17 01:43 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 03/21/17 01:43 1Ethylbenzene
<1.28 1.2810.0 ug/L 03/21/17 01:43 12-Hexanone
<1.50 1.5010.0 ug/L 03/21/17 01:43 1Iodomethane
<1.00 1.005.00 ug/L 03/21/17 01:43 1Methylene Chloride
<0.810 0.81010.0 ug/L 03/21/17 01:43 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 03/21/17 01:43 1Styrene
<0.150 0.1501.00 ug/L 03/21/17 01:43 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 03/21/17 01:43 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 03/21/17 01:43 1Tetrachloroethene
<0.170 0.1701.00 ug/L 03/21/17 01:43 1Toluene
<0.460 0.4605.00 ug/L 03/21/17 01:43 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 03/21/17 01:43 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/21/17 01:43 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 03/21/17 01:43 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 03/21/17 01:43 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 03/21/17 01:43 1Trichloroethene
<0.210 0.2101.00 ug/L 03/21/17 01:43 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 03/21/17 01:43 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 03/21/17 01:43 1Vinyl acetate
<0.180 0.1801.00 ug/L 03/21/17 01:43 1Vinyl chloride
<0.580 0.5803.00 ug/L 03/21/17 01:43 1Xylenes, Total
4-Bromofluorobenzene (Surr)98 70-130 03/21/17 01:43 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-415793/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Dibromofluoromethane (Surr)100 70-130 03/21/17 01:43 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 03/21/17 01:43 11,2-Dichloroethane-d4 (Surr)70-130
100 03/21/17 01:43 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415793/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Acetone 100 93.01 ug/L 93 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 194.2 ug/L 97 63-135
Benzene 20.0 19.48 ug/L 97 70-130
Bromochloromethane 20.0 17.09 ug/L 85 70-130
Bromodichloromethane 20.0 17.84 ug/L 89 70-130
Bromoform 20.0 18.91 ug/L 95 70-137
Bromomethane 20.0 18.48 ug/L 92 53-150
2-Butanone (MEK)100 89.68 ug/L 90 55-143
Carbon disulfide 20.0 18.61 ug/L 93 64-135
Carbon tetrachloride 20.0 17.33 ug/L 87 70-147
Chlorobenzene 20.0 18.88 ug/L 94 70-130
Chloroethane 20.0 21.85 ug/L 109 60-138
Chloroform 20.0 17.61 ug/L 88 70-130
Chloromethane 20.0 22.73 ug/L 114 33-150
cis-1,2-Dichloroethene 20.0 18.87 ug/L 94 70-130
cis-1,3-Dichloropropene 20.0 18.36 ug/L 92 70-133
Dibromochloromethane 20.0 18.64 ug/L 93 70-133
1,2-Dibromo-3-Chloropropane 20.0 17.81 ug/L 89 45-138
1,2-Dibromoethane (EDB)20.0 18.23 ug/L 91 70-130
Dibromomethane 20.0 18.02 ug/L 90 70-130
1,2-Dichlorobenzene 20.0 18.69 ug/L 93 70-130
1,4-Dichlorobenzene 20.0 18.73 ug/L 94 70-130
1,1-Dichloroethane 20.0 18.37 ug/L 92 70-130
1,2-Dichloroethane 20.0 16.58 ug/L 83 70-130
1,1-Dichloroethene 20.0 18.50 ug/L 92 70-132
1,2-Dichloropropane 20.0 19.28 ug/L 96 70-130
Ethylbenzene 20.0 18.67 ug/L 93 70-130
2-Hexanone 100 91.78 ug/L 92 54-142
Iodomethane 20.0 17.93 ug/L 90 40-150
Methylene Chloride 20.0 18.57 ug/L 93 70-130
4-Methyl-2-pentanone (MIBK)100 92.66 ug/L 93 60-137
Styrene 20.0 18.37 ug/L 92 70-130
1,1,1,2-Tetrachloroethane 20.0 18.58 ug/L 93 70-130
1,1,2,2-Tetrachloroethane 20.0 19.88 ug/L 99 69-131
Tetrachloroethene 20.0 18.78 ug/L 94 70-130
Toluene 20.0 19.26 ug/L 96 70-130
trans-1,4-Dichloro-2-butene 20.0 15.36 ug/L 77 41-150
trans-1,2-Dichloroethene 20.0 18.62 ug/L 93 70-130
trans-1,3-Dichloropropene 20.0 17.29 ug/L 86 63-142
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415793/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
1,1,1-Trichloroethane 20.0 16.70 ug/L 84 70-135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2-Trichloroethane 20.0 18.89 ug/L 94 70-130
Trichloroethene 20.0 19.39 ug/L 97 70-130
Trichlorofluoromethane 20.0 17.21 ug/L 86 59-150
1,2,3-Trichloropropane 20.0 16.98 ug/L 85 70-131
Vinyl acetate 40.0 34.94 ug/L 87 54-146
Vinyl chloride 20.0 22.56 ug/L 113 57-137
Xylenes, Total 40.0 35.64 ug/L 89 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-415793/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Acetone 100 95.79 ug/L 96 39-150 3 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 193.9 ug/L 97 63-135 0 16
Benzene 20.0 19.87 ug/L 99 70-130 2 12
Bromochloromethane 20.0 18.06 ug/L 90 70-130 5 16
Bromodichloromethane 20.0 18.32 ug/L 92 70-130 3 14
Bromoform 20.0 19.47 ug/L 97 70-137 3 14
Bromomethane 20.0 20.08 ug/L 100 53-150 8 19
2-Butanone (MEK)100 88.36 ug/L 88 55-143 1 19
Carbon disulfide 20.0 20.17 ug/L 101 64-135 8 16
Carbon tetrachloride 20.0 18.17 ug/L 91 70-147 5 16
Chlorobenzene 20.0 19.71 ug/L 99 70-130 4 12
Chloroethane 20.0 22.17 ug/L 111 60-138 1 15
Chloroform 20.0 18.27 ug/L 91 70-130 4 14
Chloromethane 20.0 23.58 ug/L 118 33-150 4 20
cis-1,2-Dichloroethene 20.0 19.21 ug/L 96 70-130 2 15
cis-1,3-Dichloropropene 20.0 19.03 ug/L 95 70-133 4 15
Dibromochloromethane 20.0 19.67 ug/L 98 70-133 5 13
1,2-Dibromo-3-Chloropropane 20.0 17.86 ug/L 89 45-138 0 19
1,2-Dibromoethane (EDB)20.0 18.32 ug/L 92 70-130 1 13
Dibromomethane 20.0 18.43 ug/L 92 70-130 2 14
1,2-Dichlorobenzene 20.0 19.35 ug/L 97 70-130 4 12
1,4-Dichlorobenzene 20.0 19.34 ug/L 97 70-130 3 12
1,1-Dichloroethane 20.0 19.02 ug/L 95 70-130 3 17
1,2-Dichloroethane 20.0 16.68 ug/L 83 70-130 1 13
1,1-Dichloroethene 20.0 19.32 ug/L 97 70-132 4 20
1,2-Dichloropropane 20.0 19.98 ug/L 100 70-130 4 15
Ethylbenzene 20.0 19.41 ug/L 97 70-130 4 12
2-Hexanone 100 91.61 ug/L 92 54-142 0 17
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-415793/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Iodomethane 20.0 19.61 ug/L 98 40-150 9 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 20.0 19.24 ug/L 96 70-130 4 15
4-Methyl-2-pentanone (MIBK)100 95.32 ug/L 95 60-137 3 21
Styrene 20.0 19.28 ug/L 96 70-130 5 12
1,1,1,2-Tetrachloroethane 20.0 19.17 ug/L 96 70-130 3 13
1,1,2,2-Tetrachloroethane 20.0 20.34 ug/L 102 69-131 2 15
Tetrachloroethene 20.0 19.52 ug/L 98 70-130 4 17
Toluene 20.0 19.98 ug/L 100 70-130 4 13
trans-1,4-Dichloro-2-butene 20.0 15.85 ug/L 79 41-150 3 20
trans-1,2-Dichloroethene 20.0 19.43 ug/L 97 70-130 4 15
trans-1,3-Dichloropropene 20.0 17.87 ug/L 89 63-142 3 13
1,1,1-Trichloroethane 20.0 17.42 ug/L 87 70-135 4 15
1,1,2-Trichloroethane 20.0 19.44 ug/L 97 70-130 3 13
Trichloroethene 20.0 19.85 ug/L 99 70-130 2 14
Trichlorofluoromethane 20.0 17.42 ug/L 87 59-150 1 22
1,2,3-Trichloropropane 20.0 17.21 ug/L 86 70-131 1 14
Vinyl acetate 40.0 33.93 ug/L 85 54-146 3 20
Vinyl chloride 20.0 23.65 ug/L 118 57-137 5 15
Xylenes, Total 40.0 37.34 ug/L 93 70-132 5 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 720-78166-A-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Acetone <2.66 100 98.81 ug/L 99 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 206.1 ug/L 103 50-135
Benzene <0.200 20.0 20.96 ug/L 105 55-147
Bromochloromethane <0.150 20.0 18.89 ug/L 94 59-132
Bromodichloromethane <0.170 20.0 19.66 ug/L 98 70-140
Bromoform <0.290 20.0 20.20 ug/L 101 53-150
Bromomethane <0.350 20.0 19.69 ug/L 98 30-150
2-Butanone (MEK)<2.64 100 92.83 ug/L 93 50-143
Carbon disulfide <0.220 20.0 20.05 ug/L 100 35-150
Carbon tetrachloride <0.180 20.0 19.98 ug/L 100 56-150
Chlorobenzene <0.180 20.0 20.41 ug/L 102 70-130
Chloroethane <0.360 20.0 23.55 ug/L 118 58-141
Chloroform <0.230 20.0 19.38 ug/L 97 66-138
Chloromethane <0.360 20.0 25.00 ug/L 125 10-150
cis-1,2-Dichloroethene 6.30 20.0 27.37 ug/L 105 68-131
cis-1,3-Dichloropropene <0.170 20.0 19.15 ug/L 96 70-133
Dibromochloromethane <0.250 20.0 20.46 ug/L 102 66-140
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 720-78166-A-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
1,2-Dibromo-3-Chloropropane <0.940 20.0 18.95 ug/L 95 38-138
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromoethane (EDB)<0.210 20.0 18.96 ug/L 95 65-137
Dibromomethane <0.450 20.0 19.71 ug/L 99 70-130
1,2-Dichlorobenzene <0.190 20.0 20.31 ug/L 102 70-130
1,4-Dichlorobenzene <0.170 20.0 20.26 ug/L 101 70-130
1,1-Dichloroethane <0.240 20.0 20.48 ug/L 102 61-139
1,2-Dichloroethane <0.200 20.0 18.39 ug/L 92 64-136
1,1-Dichloroethene <0.250 20.0 21.51 ug/L 108 54-150
1,2-Dichloropropane <0.250 20.0 20.70 ug/L 104 67-130
Ethylbenzene <0.190 20.0 20.17 ug/L 101 65-139
2-Hexanone <1.28 100 91.00 ug/L 91 44-150
Iodomethane <1.50 20.0 19.59 ug/L 98 34-150
Methylene Chloride <1.00 20.0 20.04 ug/L 100 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 94.02 ug/L 94 50-140
Styrene <0.280 20.0 19.75 ug/L 99 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 19.68 ug/L 98 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 21.37 ug/L 107 56-145
Tetrachloroethene <0.140 20.0 20.64 ug/L 103 57-138
Toluene <0.170 20.0 20.65 ug/L 103 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 16.55 ug/L 83 39-150
trans-1,2-Dichloroethene <0.230 20.0 20.52 ug/L 103 59-143
trans-1,3-Dichloropropene <0.170 20.0 18.07 ug/L 90 63-142
1,1,1-Trichloroethane <0.190 20.0 18.63 ug/L 93 68-144
1,1,2-Trichloroethane <0.190 20.0 20.01 ug/L 100 70-130
Trichloroethene 40.1 20.0 56.75 ug/L 83 63-135
Trichlorofluoromethane <0.210 20.0 19.55 ug/L 98 44-150
1,2,3-Trichloropropane <0.230 20.0 18.43 ug/L 92 65-131
Vinyl acetate <1.71 40.0 36.13 ug/L 90 43-146
Vinyl chloride 1.23 20.0 26.54 ug/L 127 57-150
Xylenes, Total <0.580 40.0 38.06 ug/L 95 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MS MS
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 720-78166-A-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Acetone <2.66 100 101.2 ug/L 101 39-150 2 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 200.2 ug/L 100 50-135 3 23
Benzene <0.200 20.0 20.25 ug/L 101 55-147 3 22
Bromochloromethane <0.150 20.0 18.41 ug/L 92 59-132 3 21
Bromodichloromethane <0.170 20.0 18.93 ug/L 95 70-140 4 196
Bromoform <0.290 20.0 19.22 ug/L 96 53-150 5 20
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 720-78166-A-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415793
Bromomethane <0.350 20.0 20.09 ug/L 100 30-150 2 44
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2-Butanone (MEK)<2.64 100 88.49 ug/L 88 50-143 5 28
Carbon disulfide <0.220 20.0 19.34 ug/L 97 35-150 4 34
Carbon tetrachloride <0.180 20.0 19.29 ug/L 96 56-150 4 18
Chlorobenzene <0.180 20.0 19.67 ug/L 98 70-130 4 15
Chloroethane <0.360 20.0 22.91 ug/L 115 58-141 3 31
Chloroform <0.230 20.0 18.61 ug/L 93 66-138 4 21
Chloromethane <0.360 20.0 24.27 ug/L 121 10-150 3 43
cis-1,2-Dichloroethene 6.30 20.0 26.62 ug/L 102 68-131 3 21
cis-1,3-Dichloropropene <0.170 20.0 18.30 ug/L 91 70-133 5 19
Dibromochloromethane <0.250 20.0 19.25 ug/L 96 66-140 6 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 17.71 ug/L 89 38-138 7 26
1,2-Dibromoethane (EDB)<0.210 20.0 18.08 ug/L 90 65-137 5 21
Dibromomethane <0.450 20.0 18.87 ug/L 94 70-130 4 19
1,2-Dichlorobenzene <0.190 20.0 19.10 ug/L 95 70-130 6 15
1,4-Dichlorobenzene <0.170 20.0 19.03 ug/L 95 70-130 6 14
1,1-Dichloroethane <0.240 20.0 20.13 ug/L 101 61-139 2 23
1,2-Dichloroethane <0.200 20.0 17.68 ug/L 88 64-136 4 22
1,1-Dichloroethene <0.250 20.0 21.23 ug/L 106 54-150 1 24
1,2-Dichloropropane <0.250 20.0 20.12 ug/L 101 67-130 3 19
Ethylbenzene <0.190 20.0 19.38 ug/L 97 65-139 4 18
2-Hexanone <1.28 100 90.72 ug/L 91 44-150 0 21
Iodomethane <1.50 20.0 19.62 ug/L 98 34-150 0 37
Methylene Chloride <1.00 20.0 19.52 ug/L 98 64-130 3 22
4-Methyl-2-pentanone (MIBK)<0.810 100 90.26 ug/L 90 50-140 4 24
Styrene <0.280 20.0 18.90 ug/L 95 70-130 4 16
1,1,1,2-Tetrachloroethane <0.150 20.0 19.34 ug/L 97 70-131 2 16
1,1,2,2-Tetrachloroethane <0.190 20.0 19.90 ug/L 99 56-145 7 19
Tetrachloroethene <0.140 20.0 19.80 ug/L 99 57-138 4 17
Toluene <0.170 20.0 19.97 ug/L 100 64-136 3 18
trans-1,4-Dichloro-2-butene <0.460 20.0 14.73 ug/L 74 39-150 12 28
trans-1,2-Dichloroethene <0.230 20.0 19.89 ug/L 99 59-143 3 25
trans-1,3-Dichloropropene <0.170 20.0 17.00 ug/L 85 63-142 6 18
1,1,1-Trichloroethane <0.190 20.0 18.14 ug/L 91 68-144 3 17
1,1,2-Trichloroethane <0.190 20.0 19.45 ug/L 97 70-130 3 18
Trichloroethene 40.1 20.0 55.35 ug/L 76 63-135 3 17
Trichlorofluoromethane <0.210 20.0 18.29 ug/L 91 44-150 7 32
1,2,3-Trichloropropane <0.230 20.0 16.84 ug/L 84 65-131 9 19
Vinyl acetate <1.71 40.0 36.82 ug/L 92 43-146 2 20
Vinyl chloride 1.23 20.0 26.56 ug/L 127 57-150 0 37
Xylenes, Total <0.580 40.0 36.75 ug/L 92 69-132 4 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
MSD MSD
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
991,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-415957/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
RL MDL
Acetone <2.66 25.0 2.66 ug/L 03/21/17 15:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 03/21/17 15:24 1Acrylonitrile
<0.200 0.2001.00 ug/L 03/21/17 15:24 1Benzene
<0.150 0.1501.00 ug/L 03/21/17 15:24 1Bromochloromethane
<0.170 0.1701.00 ug/L 03/21/17 15:24 1Bromodichloromethane
<0.290 0.2901.00 ug/L 03/21/17 15:24 1Bromoform
<0.350 0.3501.00 ug/L 03/21/17 15:24 1Bromomethane
<2.64 2.6450.0 ug/L 03/21/17 15:24 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 03/21/17 15:24 1Carbon disulfide
<0.180 0.1801.00 ug/L 03/21/17 15:24 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 03/21/17 15:24 1Chlorobenzene
<0.360 0.3601.00 ug/L 03/21/17 15:24 1Chloroethane
<0.230 0.2301.00 ug/L 03/21/17 15:24 1Chloroform
<0.360 0.3601.00 ug/L 03/21/17 15:24 1Chloromethane
<0.210 0.2101.00 ug/L 03/21/17 15:24 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/21/17 15:24 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 03/21/17 15:24 1Dibromochloromethane
<0.940 0.94010.0 ug/L 03/21/17 15:24 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 03/21/17 15:24 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 03/21/17 15:24 1Dibromomethane
<0.190 0.1901.00 ug/L 03/21/17 15:24 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 03/21/17 15:24 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 03/21/17 15:24 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 03/21/17 15:24 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 03/21/17 15:24 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 03/21/17 15:24 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 03/21/17 15:24 1Ethylbenzene
<1.28 1.2810.0 ug/L 03/21/17 15:24 12-Hexanone
<1.50 1.5010.0 ug/L 03/21/17 15:24 1Iodomethane
<1.00 1.005.00 ug/L 03/21/17 15:24 1Methylene Chloride
<0.810 0.81010.0 ug/L 03/21/17 15:24 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 03/21/17 15:24 1Styrene
<0.150 0.1501.00 ug/L 03/21/17 15:24 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 03/21/17 15:24 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 03/21/17 15:24 1Tetrachloroethene
<0.170 0.1701.00 ug/L 03/21/17 15:24 1Toluene
<0.460 0.4605.00 ug/L 03/21/17 15:24 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 03/21/17 15:24 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 03/21/17 15:24 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 03/21/17 15:24 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 03/21/17 15:24 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 03/21/17 15:24 1Trichloroethene
<0.210 0.2101.00 ug/L 03/21/17 15:24 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 03/21/17 15:24 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 03/21/17 15:24 1Vinyl acetate
<0.180 0.1801.00 ug/L 03/21/17 15:24 1Vinyl chloride
<0.580 0.5803.00 ug/L 03/21/17 15:24 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-415957/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
4-Bromofluorobenzene (Surr)97 70-130 03/21/17 15:24 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 03/21/17 15:24 1Dibromofluoromethane (Surr)70-130
94 03/21/17 15:24 11,2-Dichloroethane-d4 (Surr)70-130
101 03/21/17 15:24 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415957/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
Acetone 100 102.0 ug/L 102 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 199.5 ug/L 100 63-135
Benzene 20.0 19.01 ug/L 95 70-130
Bromochloromethane 20.0 17.57 ug/L 88 70-130
Bromodichloromethane 20.0 17.99 ug/L 90 70-130
Bromoform 20.0 18.98 ug/L 95 70-137
Bromomethane 20.0 19.41 ug/L 97 53-150
2-Butanone (MEK)100 91.90 ug/L 92 55-143
Carbon disulfide 20.0 18.68 ug/L 93 64-135
Carbon tetrachloride 20.0 17.76 ug/L 89 70-147
Chlorobenzene 20.0 18.92 ug/L 95 70-130
Chloroethane 20.0 21.49 ug/L 107 60-138
Chloroform 20.0 17.58 ug/L 88 70-130
Chloromethane 20.0 22.80 ug/L 114 33-150
cis-1,2-Dichloroethene 20.0 18.44 ug/L 92 70-130
cis-1,3-Dichloropropene 20.0 18.61 ug/L 93 70-133
Dibromochloromethane 20.0 19.15 ug/L 96 70-133
1,2-Dibromo-3-Chloropropane 20.0 18.58 ug/L 93 45-138
1,2-Dibromoethane (EDB)20.0 18.12 ug/L 91 70-130
Dibromomethane 20.0 18.12 ug/L 91 70-130
1,2-Dichlorobenzene 20.0 19.15 ug/L 96 70-130
1,4-Dichlorobenzene 20.0 18.54 ug/L 93 70-130
1,1-Dichloroethane 20.0 18.40 ug/L 92 70-130
1,2-Dichloroethane 20.0 16.47 ug/L 82 70-130
1,1-Dichloroethene 20.0 19.28 ug/L 96 70-132
1,2-Dichloropropane 20.0 19.37 ug/L 97 70-130
Ethylbenzene 20.0 18.65 ug/L 93 70-130
2-Hexanone 100 93.93 ug/L 94 54-142
Iodomethane 20.0 18.56 ug/L 93 40-150
Methylene Chloride 20.0 19.45 ug/L 97 70-130
4-Methyl-2-pentanone (MIBK)100 93.61 ug/L 94 60-137
Styrene 20.0 18.53 ug/L 93 70-130
1,1,1,2-Tetrachloroethane 20.0 18.38 ug/L 92 70-130
1,1,2,2-Tetrachloroethane 20.0 20.04 ug/L 100 69-131
Tetrachloroethene 20.0 18.85 ug/L 94 70-130
Toluene 20.0 19.02 ug/L 95 70-130
trans-1,4-Dichloro-2-butene 20.0 16.46 ug/L 82 41-150
trans-1,2-Dichloroethene 20.0 18.51 ug/L 93 70-130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415957/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
trans-1,3-Dichloropropene 20.0 17.66 ug/L 88 63-142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 20.0 16.60 ug/L 83 70-135
1,1,2-Trichloroethane 20.0 18.95 ug/L 95 70-130
Trichloroethene 20.0 18.85 ug/L 94 70-130
Trichlorofluoromethane 20.0 17.58 ug/L 88 59-150
1,2,3-Trichloropropane 20.0 17.59 ug/L 88 70-131
Vinyl acetate 40.0 36.95 ug/L 92 54-146
Vinyl chloride 20.0 23.06 ug/L 115 57-137
Xylenes, Total 40.0 35.42 ug/L 89 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-415957/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
Acetone 100 105.9 ug/L 106 39-150 4 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 201.5 ug/L 101 63-135 1 16
Benzene 20.0 20.06 ug/L 100 70-130 5 12
Bromochloromethane 20.0 18.17 ug/L 91 70-130 3 16
Bromodichloromethane 20.0 18.69 ug/L 93 70-130 4 14
Bromoform 20.0 18.74 ug/L 94 70-137 1 14
Bromomethane 20.0 20.60 ug/L 103 53-150 6 19
2-Butanone (MEK)100 89.57 ug/L 90 55-143 3 19
Carbon disulfide 20.0 19.87 ug/L 99 64-135 6 16
Carbon tetrachloride 20.0 18.65 ug/L 93 70-147 5 16
Chlorobenzene 20.0 19.18 ug/L 96 70-130 1 12
Chloroethane 20.0 22.98 ug/L 115 60-138 7 15
Chloroform 20.0 18.43 ug/L 92 70-130 5 14
Chloromethane 20.0 24.16 ug/L 121 33-150 6 20
cis-1,2-Dichloroethene 20.0 19.71 ug/L 99 70-130 7 15
cis-1,3-Dichloropropene 20.0 18.78 ug/L 94 70-133 1 15
Dibromochloromethane 20.0 18.57 ug/L 93 70-133 3 13
1,2-Dibromo-3-Chloropropane 20.0 18.02 ug/L 90 45-138 3 19
1,2-Dibromoethane (EDB)20.0 17.96 ug/L 90 70-130 1 13
Dibromomethane 20.0 18.60 ug/L 93 70-130 3 14
1,2-Dichlorobenzene 20.0 18.52 ug/L 93 70-130 3 12
1,4-Dichlorobenzene 20.0 18.39 ug/L 92 70-130 1 12
1,1-Dichloroethane 20.0 19.23 ug/L 96 70-130 4 17
1,2-Dichloroethane 20.0 16.83 ug/L 84 70-130 2 13
1,1-Dichloroethene 20.0 20.49 ug/L 102 70-132 6 20
1,2-Dichloropropane 20.0 19.89 ug/L 99 70-130 3 15
Ethylbenzene 20.0 19.11 ug/L 96 70-130 2 12
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-415957/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
2-Hexanone 100 91.04 ug/L 91 54-142 3 17
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Iodomethane 20.0 20.71 ug/L 104 40-150 11 20
Methylene Chloride 20.0 20.01 ug/L 100 70-130 3 15
4-Methyl-2-pentanone (MIBK)100 91.73 ug/L 92 60-137 2 21
Styrene 20.0 18.72 ug/L 94 70-130 1 12
1,1,1,2-Tetrachloroethane 20.0 18.66 ug/L 93 70-130 1 13
1,1,2,2-Tetrachloroethane 20.0 19.67 ug/L 98 69-131 2 15
Tetrachloroethene 20.0 19.40 ug/L 97 70-130 3 17
Toluene 20.0 19.70 ug/L 98 70-130 4 13
trans-1,4-Dichloro-2-butene 20.0 16.16 ug/L 81 41-150 2 20
trans-1,2-Dichloroethene 20.0 19.41 ug/L 97 70-130 5 15
trans-1,3-Dichloropropene 20.0 17.50 ug/L 87 63-142 1 13
1,1,1-Trichloroethane 20.0 17.61 ug/L 88 70-135 6 15
1,1,2-Trichloroethane 20.0 18.74 ug/L 94 70-130 1 13
Trichloroethene 20.0 20.09 ug/L 100 70-130 6 14
Trichlorofluoromethane 20.0 18.50 ug/L 93 59-150 5 22
1,2,3-Trichloropropane 20.0 16.89 ug/L 84 70-131 4 14
Vinyl acetate 40.0 40.00 ug/L 100 54-146 8 20
Vinyl chloride 20.0 24.23 ug/L 121 57-137 5 15
Xylenes, Total 40.0 36.49 ug/L 91 70-132 3 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
871,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: MW-3RLab Sample ID: 490-123577-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
Acetone <2.66 250 218.4 ug/L 87 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 428.5 ug/L 86 50-135
Benzene <0.200 50.0 44.65 ug/L 89 55-147
Bromochloromethane <0.150 50.0 39.89 ug/L 80 59-132
Bromodichloromethane <0.170 50.0 43.65 ug/L 87 70-140
Bromoform <0.290 50.0 44.52 ug/L 89 53-150
Bromomethane <0.350 50.0 43.94 ug/L 88 30-150
2-Butanone (MEK)<2.64 250 193.9 ug/L 78 50-143
Carbon disulfide <0.220 50.0 35.95 ug/L 72 35-150
Carbon tetrachloride <0.180 50.0 41.91 ug/L 84 56-150
Chlorobenzene <0.180 50.0 44.15 ug/L 88 70-130
Chloroethane <0.360 50.0 48.80 ug/L 98 58-141
Chloroform <0.230 50.0 41.63 ug/L 83 66-138
Chloromethane <0.360 50.0 49.41 ug/L 99 10-150
cis-1,2-Dichloroethene <0.210 50.0 43.31 ug/L 87 68-131
cis-1,3-Dichloropropene <0.170 50.0 44.81 ug/L 90 70-133
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-3RLab Sample ID: 490-123577-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
Dibromochloromethane <0.250 50.0 45.13 ug/L 90 66-140
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane <0.940 50.0 42.44 ug/L 85 38-138
1,2-Dibromoethane (EDB)<0.210 50.0 42.09 ug/L 84 65-137
Dibromomethane <0.450 50.0 42.68 ug/L 85 70-130
1,2-Dichlorobenzene <0.190 50.0 43.88 ug/L 88 70-130
1,4-Dichlorobenzene <0.170 50.0 43.58 ug/L 87 70-130
1,1-Dichloroethane <0.240 50.0 42.96 ug/L 86 61-139
1,2-Dichloroethane <0.200 50.0 37.73 ug/L 75 64-136
1,1-Dichloroethene <0.250 50.0 43.81 ug/L 88 54-150
1,2-Dichloropropane <0.250 50.0 46.09 ug/L 92 67-130
Ethylbenzene <0.190 50.0 43.78 ug/L 88 65-139
2-Hexanone <1.28 250 207.0 ug/L 83 44-150
Iodomethane <1.50 50.0 47.00 ug/L 94 34-150
Methylene Chloride <1.00 50.0 42.80 ug/L 86 64-130
4-Methyl-2-pentanone (MIBK)<0.810 250 212.1 ug/L 85 50-140
Styrene <0.280 50.0 42.99 ug/L 86 70-130
1,1,1,2-Tetrachloroethane <0.150 50.0 43.84 ug/L 88 70-131
1,1,2,2-Tetrachloroethane <0.190 50.0 45.73 ug/L 91 56-145
Tetrachloroethene <0.140 50.0 43.63 ug/L 87 57-138
Toluene <0.170 50.0 44.84 ug/L 90 64-136
trans-1,4-Dichloro-2-butene <0.460 50.0 36.74 ug/L 73 39-150
trans-1,2-Dichloroethene <0.230 50.0 41.94 ug/L 84 59-143
trans-1,3-Dichloropropene <0.170 50.0 42.19 ug/L 84 63-142
1,1,1-Trichloroethane <0.190 50.0 40.68 ug/L 81 68-144
1,1,2-Trichloroethane <0.190 50.0 43.81 ug/L 88 70-130
Trichloroethene <0.200 50.0 46.23 ug/L 92 63-135
Trichlorofluoromethane <0.210 50.0 40.82 ug/L 82 44-150
1,2,3-Trichloropropane <0.230 50.0 38.58 ug/L 77 65-131
Vinyl acetate <1.71 100 81.50 ug/L 82 43-146
Vinyl chloride <0.180 50.0 50.61 ug/L 101 57-150
Xylenes, Total <0.580 100 84.07 ug/L 84 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
MS MS
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
861,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: MW-3RLab Sample ID: 490-123577-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
Acetone <2.66 250 219.5 ug/L 88 39-150 1 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 422.6 ug/L 85 50-135 1 23
Benzene <0.200 50.0 43.37 ug/L 87 55-147 3 22
Bromochloromethane <0.150 50.0 38.66 ug/L 77 59-132 3 21
Bromodichloromethane <0.170 50.0 42.25 ug/L 85 70-140 3 196
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-3RLab Sample ID: 490-123577-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 415957
Bromoform <0.290 50.0 44.67 ug/L 89 53-150 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromomethane <0.350 50.0 43.50 ug/L 87 30-150 1 44
2-Butanone (MEK)<2.64 250 189.1 ug/L 76 50-143 3 28
Carbon disulfide <0.220 50.0 35.50 ug/L 71 35-150 1 34
Carbon tetrachloride <0.180 50.0 41.11 ug/L 82 56-150 2 18
Chlorobenzene <0.180 50.0 43.74 ug/L 87 70-130 1 15
Chloroethane <0.360 50.0 47.26 ug/L 95 58-141 3 31
Chloroform <0.230 50.0 40.50 ug/L 81 66-138 3 21
Chloromethane <0.360 50.0 49.25 ug/L 98 10-150 0 43
cis-1,2-Dichloroethene <0.210 50.0 42.17 ug/L 84 68-131 3 21
cis-1,3-Dichloropropene <0.170 50.0 44.61 ug/L 89 70-133 0 19
Dibromochloromethane <0.250 50.0 45.05 ug/L 90 66-140 0 19
1,2-Dibromo-3-Chloropropane <0.940 50.0 43.13 ug/L 86 38-138 2 26
1,2-Dibromoethane (EDB)<0.210 50.0 42.38 ug/L 85 65-137 1 21
Dibromomethane <0.450 50.0 41.85 ug/L 84 70-130 2 19
1,2-Dichlorobenzene <0.190 50.0 43.39 ug/L 87 70-130 1 15
1,4-Dichlorobenzene <0.170 50.0 42.75 ug/L 85 70-130 2 14
1,1-Dichloroethane <0.240 50.0 41.94 ug/L 84 61-139 2 23
1,2-Dichloroethane <0.200 50.0 36.67 ug/L 73 64-136 3 22
1,1-Dichloroethene <0.250 50.0 41.07 ug/L 82 54-150 6 24
1,2-Dichloropropane <0.250 50.0 45.89 ug/L 92 67-130 0 19
Ethylbenzene <0.190 50.0 43.38 ug/L 87 65-139 1 18
2-Hexanone <1.28 250 208.0 ug/L 83 44-150 0 21
Iodomethane <1.50 50.0 44.96 ug/L 90 34-150 4 37
Methylene Chloride <1.00 50.0 41.52 ug/L 83 64-130 3 22
4-Methyl-2-pentanone (MIBK)<0.810 250 211.8 ug/L 85 50-140 0 24
Styrene <0.280 50.0 42.90 ug/L 86 70-130 0 16
1,1,1,2-Tetrachloroethane <0.150 50.0 43.03 ug/L 86 70-131 2 16
1,1,2,2-Tetrachloroethane <0.190 50.0 46.28 ug/L 93 56-145 1 19
Tetrachloroethene <0.140 50.0 43.32 ug/L 87 57-138 1 17
Toluene <0.170 50.0 44.41 ug/L 89 64-136 1 18
trans-1,4-Dichloro-2-butene <0.460 50.0 37.13 ug/L 74 39-150 1 28
trans-1,2-Dichloroethene <0.230 50.0 41.31 ug/L 83 59-143 2 25
trans-1,3-Dichloropropene <0.170 50.0 42.15 ug/L 84 63-142 0 18
1,1,1-Trichloroethane <0.190 50.0 39.20 ug/L 78 68-144 4 17
1,1,2-Trichloroethane <0.190 50.0 44.45 ug/L 89 70-130 1 18
Trichloroethene <0.200 50.0 44.75 ug/L 90 63-135 3 17
Trichlorofluoromethane <0.210 50.0 41.58 ug/L 83 44-150 2 32
1,2,3-Trichloropropane <0.230 50.0 38.12 ug/L 76 65-131 1 19
Vinyl acetate <1.71 100 86.32 ug/L 86 43-146 6 20
Vinyl chloride <0.180 50.0 49.75 ug/L 99 57-150 2 37
Xylenes, Total <0.580 100 83.24 ug/L 83 69-132 1 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
104
MSD MSD
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
861,2-Dichloroethane-d4 (Surr)70 -130
104Toluene-d8 (Surr)70 -130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-416007/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416586 Prep Batch: 416007
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 17:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00500 0.005000.0100 mg/L 03/21/17 12:46 03/22/17 17:22 1Barium
<0.000500 ^0.0005000.00100 mg/L 03/21/17 12:46 03/22/17 17:22 1Cadmium
<0.00300 ^0.003000.00500 mg/L 03/21/17 12:46 03/22/17 17:22 1Chromium
<0.00500 0.005000.0100 mg/L 03/21/17 12:46 03/22/17 17:22 1Copper
<0.00200 0.002000.00500 mg/L 03/21/17 12:46 03/22/17 17:22 1Lead
<0.00300 0.003000.0100 mg/L 03/21/17 12:46 03/22/17 17:22 1Nickel
<0.00500 0.005000.0100 mg/L 03/21/17 12:46 03/22/17 17:22 1Selenium
<0.00300 0.003000.00500 mg/L 03/21/17 12:46 03/22/17 17:22 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-416007/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416586 Prep Batch: 416007
Arsenic 0.100 0.09170 mg/L 92 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 0.100 0.1051 mg/L 105 80-120
Cadmium 0.100 0.1043 ^mg/L 104 80-120
Chromium 0.100 0.1095 ^mg/L 110 80-120
Copper 0.100 0.1038 mg/L 104 80-120
Lead 0.100 0.1013 mg/L 101 80-120
Nickel 0.100 0.09910 mg/L 99 80-120
Selenium 0.100 0.09540 mg/L 95 80-120
Silver 0.100 0.09280 mg/L 93 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-416007/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416586 Prep Batch: 416007
Arsenic 0.100 0.09750 mg/L 98 80-120 6 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Barium 0.100 0.1058 mg/L 106 80-120 1 20
Cadmium 0.100 0.1054 ^mg/L 105 80-120 1 20
Chromium 0.100 0.1091 ^mg/L 109 80-120 0 20
Copper 0.100 0.1030 mg/L 103 80-120 1 20
Lead 0.100 0.1023 mg/L 102 80-120 1 20
Nickel 0.100 0.1000 mg/L 100 80-120 1 20
Selenium 0.100 0.09550 mg/L 96 80-120 0 20
Silver 0.100 0.09300 mg/L 93 80-120 0 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-123702-H-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416586 Prep Batch: 416007
Arsenic <0.00860 0.100 0.09900 mg/L 99 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0291 0.100 0.1341 mg/L 105 75-125
Cadmium <0.000500 ^0.100 0.1039 ^mg/L 104 75-125
Chromium <0.00300 ^0.100 0.1079 ^mg/L 108 75-125
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-123702-H-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416586 Prep Batch: 416007
Copper <0.00500 0.100 0.1041 mg/L 104 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Lead <0.00200 0.100 0.1022 mg/L 102 75-125
Nickel <0.00300 0.100 0.09570 mg/L 96 75-125
Selenium <0.00500 0.100 0.09880 mg/L 99 75-125
Silver <0.00300 0.100 0.09210 mg/L 92 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-123702-H-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416586 Prep Batch: 416007
Arsenic <0.00860 0.100 0.1019 mg/L 102 75-125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0291 0.100 0.1347 mg/L 106 75-125 0 20
Cadmium <0.000500 ^0.100 0.1042 ^mg/L 104 75-125 0 20
Chromium <0.00300 ^0.100 0.1088 ^mg/L 109 75-125 1 20
Copper <0.00500 0.100 0.1050 mg/L 105 75-125 1 20
Lead <0.00200 0.100 0.1011 mg/L 101 75-125 1 20
Nickel <0.00300 0.100 0.09640 mg/L 96 75-125 1 20
Selenium <0.00500 0.100 0.09580 mg/L 96 75-125 3 20
Silver <0.00300 0.100 0.09430 mg/L 94 75-125 2 20
Client Sample ID: Method BlankLab Sample ID: MB 490-417946/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 418310 Prep Batch: 417946
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/28/17 22:54 03/29/17 11:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00860 0.008600.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Arsenic
<0.00500 0.005000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Barium
<0.00500 0.005000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Barium
<0.000500 0.0005000.00100 mg/L 03/28/17 22:54 03/29/17 11:49 1Cadmium
<0.000500 0.0005000.00100 mg/L 03/28/17 22:54 03/29/17 11:49 1Cadmium
<0.00300 0.003000.00500 mg/L 03/28/17 22:54 03/29/17 11:49 1Chromium
<0.00300 0.003000.00500 mg/L 03/28/17 22:54 03/29/17 11:49 1Chromium
<0.00500 0.005000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Copper
<0.00500 0.005000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Copper
<0.00200 0.002000.00500 mg/L 03/28/17 22:54 03/29/17 11:49 1Lead
<0.00200 0.002000.00500 mg/L 03/28/17 22:54 03/29/17 11:49 1Lead
<0.00300 0.003000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Nickel
<0.00300 0.003000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Nickel
<0.00500 0.005000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Selenium
<0.00500 0.005000.0100 mg/L 03/28/17 22:54 03/29/17 11:49 1Selenium
<0.00300 0.003000.00500 mg/L 03/28/17 22:54 03/29/17 11:49 1Silver
<0.00300 0.003000.00500 mg/L 03/28/17 22:54 03/29/17 11:49 1Silver
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-417946/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 418310 Prep Batch: 417946
Arsenic 0.100 0.09990 mg/L 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 0.100 0.09990 mg/L 100 80-120
Barium 0.100 0.1006 mg/L 101 80-120
Barium 0.100 0.1006 mg/L 101 80-120
Cadmium 0.100 0.09670 mg/L 97 80-120
Cadmium 0.100 0.09670 mg/L 97 80-120
Chromium 0.100 0.09630 mg/L 96 80-120
Chromium 0.100 0.09630 mg/L 96 80-120
Copper 0.100 0.09810 mg/L 98 80-120
Copper 0.100 0.09810 mg/L 98 80-120
Lead 0.100 0.09750 mg/L 98 80-120
Lead 0.100 0.09750 mg/L 98 80-120
Nickel 0.100 0.09850 mg/L 99 80-120
Nickel 0.100 0.09850 mg/L 99 80-120
Selenium 0.100 0.09670 mg/L 97 80-120
Selenium 0.100 0.09670 mg/L 97 80-120
Silver 0.100 0.1005 mg/L 101 80-120
Silver 0.100 0.1005 mg/L 101 80-120
Client Sample ID: MW-04CDLab Sample ID: 490-123577-2 MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 418310 Prep Batch: 417946
Arsenic <0.00860 0.100 0.09610 mg/L 96 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic <0.00860 0.100 0.09610 mg/L 96 75-125
Barium 0.182 0.100 0.2748 mg/L 93 75-125
Barium 0.182 0.100 0.2748 mg/L 93 75-125
Cadmium <0.000500 0.100 0.09280 mg/L 93 75-125
Cadmium <0.000500 0.100 0.09280 mg/L 93 75-125
Chromium <0.00300 0.100 0.09290 mg/L 93 75-125
Chromium <0.00300 0.100 0.09290 mg/L 93 75-125
Copper <0.00500 0.100 0.09630 mg/L 96 75-125
Copper <0.00500 0.100 0.09630 mg/L 96 75-125
Lead <0.00200 0.100 0.09210 mg/L 92 75-125
Lead <0.00200 0.100 0.09210 mg/L 92 75-125
Nickel <0.00300 0.100 0.09320 mg/L 93 75-125
Nickel <0.00300 0.100 0.09320 mg/L 93 75-125
Selenium <0.00500 0.100 0.09550 mg/L 96 75-125
Selenium <0.00500 0.100 0.09550 mg/L 96 75-125
Silver <0.00300 0.100 0.09640 mg/L 96 75-125
Silver <0.00300 0.100 0.09640 mg/L 96 75-125
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: MW-04CDLab Sample ID: 490-123577-2 MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 418310 Prep Batch: 417946
Arsenic <0.00860 0.100 0.09650 mg/L 97 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic <0.00860 0.100 0.09650 mg/L 97 75-125 0 20
Barium 0.182 0.100 0.2786 mg/L 97 75-125 1 20
Barium 0.182 0.100 0.2786 mg/L 97 75-125 1 20
Cadmium <0.000500 0.100 0.09390 mg/L 94 75-125 1 20
Cadmium <0.000500 0.100 0.09390 mg/L 94 75-125 1 20
Chromium <0.00300 0.100 0.09460 mg/L 95 75-125 2 20
Chromium <0.00300 0.100 0.09460 mg/L 95 75-125 2 20
Copper <0.00500 0.100 0.09700 mg/L 97 75-125 1 20
Copper <0.00500 0.100 0.09700 mg/L 97 75-125 1 20
Lead <0.00200 0.100 0.09300 mg/L 93 75-125 1 20
Lead <0.00200 0.100 0.09300 mg/L 93 75-125 1 20
Nickel <0.00300 0.100 0.09480 mg/L 95 75-125 2 20
Nickel <0.00300 0.100 0.09480 mg/L 95 75-125 2 20
Selenium <0.00500 0.100 0.09580 mg/L 96 75-125 0 20
Selenium <0.00500 0.100 0.09580 mg/L 96 75-125 0 20
Silver <0.00300 0.100 0.09710 mg/L 97 75-125 1 20
Silver <0.00300 0.100 0.09710 mg/L 97 75-125 1 20
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-416010/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 04:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.100 0.1002.00 ug/L 03/21/17 12:51 03/30/17 04:59 1Beryllium
<0.100 0.1002.00 ug/L 03/21/17 12:51 03/30/17 04:59 1Cobalt
<0.800 0.8002.00 ug/L 03/21/17 12:51 03/30/17 04:59 1Thallium
<5.20 5.2025.0 ug/L 03/21/17 12:51 03/30/17 04:59 1Zinc
Client Sample ID: Method BlankLab Sample ID: MB 490-416010/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418845 Prep Batch: 416010
RL MDL
Vanadium <0.700 2.00 0.700 ug/L 03/21/17 12:51 03/30/17 21:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-416010/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony 100 92.44 ug/L 92 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 102.2 ug/L 102 80-120
Cobalt 100 101.9 ug/L 102 80-120
Thallium 100 99.41 ug/L 99 80-120
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-416010/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Vanadium 100 101.8 ug/L 102 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Zinc 100 87.99 ug/L 88 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-416010/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony 100 90.49 ug/L 90 80-120 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Beryllium 100 100.4 ug/L 100 80-120 2 20
Cobalt 100 98.42 ug/L 98 80-120 3 20
Thallium 100 97.53 ug/L 98 80-120 2 20
Vanadium 100 98.30 ug/L 98 80-120 3 20
Zinc 100 86.89 ug/L 87 80-120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-123717-H-1-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony <0.800 100 91.68 ug/L 92 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <0.100 100 101.6 ug/L 102 75-125
Cobalt 0.101 J 100 100.2 ug/L 100 75-125
Thallium <0.800 100 95.86 ug/L 96 75-125
Vanadium 5.46 100 101.9 ug/L 96 75-125
Zinc 19.4 J 100 103.7 ug/L 84 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-123717-H-1-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony <0.800 100 91.89 ug/L 92 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.100 100 102.4 ug/L 102 75-125 1 20
Cobalt 0.101 J 100 97.76 ug/L 98 75-125 2 20
Thallium <0.800 100 96.79 ug/L 97 75-125 1 20
Vanadium 5.46 100 97.69 ug/L 92 75-125 4 20
Zinc 19.4 J 100 101.9 ug/L 83 75-125 2 20
Client Sample ID: Method BlankLab Sample ID: MB 490-417947/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 418994 Prep Batch: 417947
RL MDL
Antimony <0.000800 0.00200 0.000800 mg/L 03/28/17 22:56 03/31/17 16:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000100 0.0001000.00200 mg/L 03/28/17 22:56 03/31/17 16:13 1Beryllium
<0.000100 0.0001000.00200 mg/L 03/28/17 22:56 03/31/17 16:13 1Cobalt
<0.000800 0.0008000.00200 mg/L 03/28/17 22:56 03/31/17 16:13 1Thallium
0.0007444 J 0.0007000.00200 mg/L 03/28/17 22:56 03/31/17 16:13 1Vanadium
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-417947/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 418994 Prep Batch: 417947
RL MDL
Zinc 0.02232 J 0.0250 0.00520 mg/L 03/28/17 22:56 03/31/17 16:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-417947/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 418994 Prep Batch: 417947
Antimony 0.100 0.1006 mg/L 101 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 0.100 0.09956 mg/L 100 80-120
Cobalt 0.100 0.1029 mg/L 103 80-120
Thallium 0.100 0.09225 mg/L 92 80-120
Vanadium 0.100 0.09906 mg/L 99 80-120
Zinc 0.100 0.1043 mg/L 104 80-120
Client Sample ID: MW-04CDLab Sample ID: 490-123577-2 MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 418994 Prep Batch: 417947
Antimony <0.000800 0.100 0.1006 mg/L 101 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <0.000100 0.100 0.09767 mg/L 98 75-125
Cobalt 0.000453 J 0.100 0.1024 mg/L 102 75-125
Thallium <0.000800 0.100 0.09253 mg/L 93 75-125
Vanadium 0.00123 J B 0.100 0.09860 mg/L 97 75-125
Zinc 0.0197 J B 0.100 0.1182 mg/L 98 75-125
Client Sample ID: MW-04CDLab Sample ID: 490-123577-2 MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 418994 Prep Batch: 417947
Antimony <0.000800 0.100 0.1010 mg/L 101 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.000100 0.100 0.09613 mg/L 96 75-125 2 20
Cobalt 0.000453 J 0.100 0.1050 mg/L 105 75-125 3 20
Thallium <0.000800 0.100 0.09281 mg/L 93 75-125 0 20
Vanadium 0.00123 J B 0.100 0.09936 mg/L 98 75-125 1 20
Zinc 0.0197 J B 0.100 0.1240 mg/L 104 75-125 5 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-415182/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 06:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415182/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
Mercury 1.00 0.9638 ug/L 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-123570-B-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
Mercury <0.100 1.00 1.138 ug/L 114 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-123570-B-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
Mercury <0.100 1.00 1.028 ug/L 103 75-125 10 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-417962/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418661 Prep Batch: 417962
RL MDL
Mercury <0.000100 0.000200 0.000100 mg/L 03/29/17 08:06 03/29/17 11:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-417962/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418661 Prep Batch: 417962
Mercury 0.00100 0.0008923 mg/L 89 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-417962/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418661 Prep Batch: 417962
Mercury 0.00100 0.0008852 mg/L 89 80-120 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-124516-D-1-H MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418661 Prep Batch: 417962
Mercury <0.000100 0.00100 0.0008766 mg/L 88 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-124516-D-1-I MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418661 Prep Batch: 417962
Mercury <0.000100 0.00100 0.0007847 mg/L 78 75-125 11 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
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QC Association Summary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
GC/MS VOA
Analysis Batch: 415705
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-123577-1 MW-01CD Total/NA
Water 8260B490-123577-2 MW-04CD Total/NA
Water 8260B490-123577-3 MW-4 Total/NA
Water 8260B490-123577-4 MW-2R Total/NA
Water 8260B490-123577-5 MW-2RDUP Total/NA
Water 8260B490-123577-9 SS-2 Total/NA
Water 8260BMB 490-415705/9 Method Blank Total/NA
Water 8260BLCS 490-415705/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-415705/4 Lab Control Sample Dup Total/NA
Water 8260B490-124065-E-3 MS Matrix Spike Total/NA
Water 8260B490-124065-F-3 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 415793
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-123577-10 Trip Blank Total/NA
Water 8260BMB 490-415793/7 Method Blank Total/NA
Water 8260BLCS 490-415793/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-415793/4 Lab Control Sample Dup Total/NA
Water 8260B720-78166-A-4 MS Matrix Spike Total/NA
Water 8260B720-78166-A-4 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 415957
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-123577-6 MW-3R Total/NA
Water 8260B490-123577-7 SP-1 Total/NA
Water 8260B490-123577-8 SS-1 Total/NA
Water 8260B490-123577-11 MW-02CD Total/NA
Water 8260BMB 490-415957/10 Method Blank Total/NA
Water 8260BLCS 490-415957/4 Lab Control Sample Total/NA
Water 8260BLCSD 490-415957/5 Lab Control Sample Dup Total/NA
Water 8260B490-123577-6 MS MW-3R Total/NA
Water 8260B490-123577-6 MSD MW-3R Total/NA
Metals
Prep Batch: 415182
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-123577-1 MW-01CD Total/NA
Water 7470A490-123577-2 MW-04CD Total/NA
Water 7470A490-123577-3 MW-4 Total/NA
Water 7470A490-123577-4 MW-2R Total/NA
Water 7470A490-123577-5 MW-2RDUP Total/NA
Water 7470A490-123577-6 MW-3R Total/NA
Water 7470A490-123577-7 SP-1 Total/NA
Water 7470A490-123577-8 SS-1 Total/NA
Water 7470A490-123577-9 SS-2 Total/NA
Water 7470A490-123577-11 MW-02CD Total/NA
Water 7470AMB 490-415182/1-A Method Blank Total/NA
Water 7470ALCS 490-415182/2-A Lab Control Sample Total/NA
Water 7470A490-123570-B-1-B MS Matrix Spike Total/NA
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QC Association Summary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Prep Batch: 415182 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-123570-B-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 416007
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-123577-1 MW-01CD Total/NA
Water 3010A490-123577-2 MW-04CD Total/NA
Water 3010A490-123577-3 MW-4 Total/NA
Water 3010A490-123577-4 MW-2R Total/NA
Water 3010A490-123577-5 MW-2RDUP Total/NA
Water 3010A490-123577-6 MW-3R Total/NA
Water 3010A490-123577-7 SP-1 Total/NA
Water 3010A490-123577-8 SS-1 Total/NA
Water 3010A490-123577-9 SS-2 Total/NA
Water 3010A490-123577-11 MW-02CD Total/NA
Water 3010AMB 490-416007/1-A Method Blank Total/NA
Water 3010ALCS 490-416007/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-416007/3-A Lab Control Sample Dup Total/NA
Water 3010A490-123702-H-1-B MS Matrix Spike Total/NA
Water 3010A490-123702-H-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 416010
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-123577-1 MW-01CD Total/NA
Water 3010A490-123577-2 MW-04CD Total/NA
Water 3010A490-123577-3 MW-4 Total/NA
Water 3010A490-123577-4 MW-2R Total/NA
Water 3010A490-123577-5 MW-2RDUP Total/NA
Water 3010A490-123577-6 MW-3R Total/NA
Water 3010A490-123577-7 SP-1 Total/NA
Water 3010A490-123577-8 SS-1 Total/NA
Water 3010A490-123577-9 SS-2 Total/NA
Water 3010A490-123577-11 MW-02CD Total/NA
Water 3010AMB 490-416010/1-A Method Blank Total/NA
Water 3010ALCS 490-416010/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-416010/3-A Lab Control Sample Dup Total/NA
Water 3010A490-123717-H-1-C MS Matrix Spike Total/NA
Water 3010A490-123717-H-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 416586
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 416007490-123577-1 MW-01CD Total/NA
Water 6010D 416007490-123577-2 MW-04CD Total/NA
Water 6010D 416007490-123577-3 MW-4 Total/NA
Water 6010D 416007490-123577-4 MW-2R Total/NA
Water 6010D 416007490-123577-5 MW-2RDUP Total/NA
Water 6010D 416007490-123577-6 MW-3R Total/NA
Water 6010D 416007490-123577-7 SP-1 Total/NA
Water 6010D 416007490-123577-8 SS-1 Total/NA
Water 6010D 416007490-123577-9 SS-2 Total/NA
Water 6010D 416007490-123577-11 MW-02CD Total/NA
Water 6010D 416007MB 490-416007/1-A Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Analysis Batch: 416586 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 416007LCS 490-416007/2-A Lab Control Sample Total/NA
Water 6010D 416007LCSD 490-416007/3-A Lab Control Sample Dup Total/NA
Water 6010D 416007490-123702-H-1-B MS Matrix Spike Total/NA
Water 6010D 416007490-123702-H-1-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 416854
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 415182490-123577-1 MW-01CD Total/NA
Water 7470A 415182490-123577-2 MW-04CD Total/NA
Water 7470A 415182490-123577-3 MW-4 Total/NA
Water 7470A 415182490-123577-4 MW-2R Total/NA
Water 7470A 415182490-123577-5 MW-2RDUP Total/NA
Water 7470A 415182490-123577-6 MW-3R Total/NA
Water 7470A 415182490-123577-7 SP-1 Total/NA
Water 7470A 415182490-123577-8 SS-1 Total/NA
Water 7470A 415182490-123577-9 SS-2 Total/NA
Water 7470A 415182490-123577-11 MW-02CD Total/NA
Water 7470A 415182MB 490-415182/1-A Method Blank Total/NA
Water 7470A 415182LCS 490-415182/2-A Lab Control Sample Total/NA
Water 7470A 415182490-123570-B-1-B MS Matrix Spike Total/NA
Water 7470A 415182490-123570-B-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 417946
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A490-123577-2 MW-04CD Dissolved
Water 3005AMB 490-417946/1-A Method Blank Total Recoverable
Water 3005ALCS 490-417946/2-A Lab Control Sample Total Recoverable
Water 3005A490-123577-2 MS MW-04CD Dissolved
Water 3005A490-123577-2 MSD MW-04CD Dissolved
Prep Batch: 417947
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A490-123577-2 MW-04CD Dissolved
Water 3005AMB 490-417947/1-A Method Blank Total Recoverable
Water 3005ALCS 490-417947/2-A Lab Control Sample Total Recoverable
Water 3005A490-123577-2 MS MW-04CD Dissolved
Water 3005A490-123577-2 MSD MW-04CD Dissolved
Prep Batch: 417962
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-123577-2 MW-04CD Dissolved
Water 7470AMB 490-417962/1-A Method Blank Total/NA
Water 7470ALCS 490-417962/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-417962/3-A Lab Control Sample Dup Total/NA
Water 7470A490-124516-D-1-H MS Matrix Spike Total/NA
Water 7470A490-124516-D-1-I MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 418310
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 417946490-123577-2 MW-04CD Dissolved
Water 6010D 417946MB 490-417946/1-A Method Blank Total Recoverable
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QC Association Summary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Metals (Continued)
Analysis Batch: 418310 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 417946LCS 490-417946/2-A Lab Control Sample Total Recoverable
Water 6010D 417946490-123577-2 MS MW-04CD Dissolved
Water 6010D 417946490-123577-2 MSD MW-04CD Dissolved
Analysis Batch: 418502
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 416010490-123577-1 MW-01CD Total/NA
Water 6020B 416010490-123577-2 MW-04CD Total/NA
Water 6020B 416010490-123577-3 MW-4 Total/NA
Water 6020B 416010490-123577-4 MW-2R Total/NA
Water 6020B 416010490-123577-5 MW-2RDUP Total/NA
Water 6020B 416010490-123577-6 MW-3R Total/NA
Water 6020B 416010490-123577-7 SP-1 Total/NA
Water 6020B 416010490-123577-8 SS-1 Total/NA
Water 6020B 416010490-123577-9 SS-2 Total/NA
Water 6020B 416010490-123577-11 MW-02CD Total/NA
Water 6020B 416010MB 490-416010/1-A Method Blank Total/NA
Water 6020B 416010LCS 490-416010/2-A Lab Control Sample Total/NA
Water 6020B 416010LCSD 490-416010/3-A Lab Control Sample Dup Total/NA
Water 6020B 416010490-123717-H-1-C MS Matrix Spike Total/NA
Water 6020B 416010490-123717-H-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 418661
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 417962490-123577-2 MW-04CD Dissolved
Water 7470A 417962MB 490-417962/1-A Method Blank Total/NA
Water 7470A 417962LCS 490-417962/2-A Lab Control Sample Total/NA
Water 7470A 417962LCSD 490-417962/3-A Lab Control Sample Dup Total/NA
Water 7470A 417962490-124516-D-1-H MS Matrix Spike Total/NA
Water 7470A 417962490-124516-D-1-I MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 418845
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 416010MB 490-416010/1-A Method Blank Total/NA
Analysis Batch: 418994
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 417947490-123577-2 MW-04CD Dissolved
Water 6020B 417947MB 490-417947/1-A Method Blank Total Recoverable
Water 6020B 417947LCS 490-417947/2-A Lab Control Sample Total Recoverable
Water 6020B 417947490-123577-2 MS MW-04CD Dissolved
Water 6020B 417947490-123577-2 MSD MW-04CD Dissolved
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-01CD Lab Sample ID: 490-123577-1
Matrix: WaterDate Collected: 03/08/17 11:54
Date Received: 03/11/17 10:05
Analysis 8260B RP03/20/17 18:391 TAL NSH415705
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 18:31 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 05:48 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:19 CAH TAL NSHTotal/NA
Client Sample ID: MW-04CD Lab Sample ID: 490-123577-2
Matrix: WaterDate Collected: 03/08/17 09:51
Date Received: 03/11/17 10:05
Analysis 8260B RP03/20/17 19:071 TAL NSH415705
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3005A 417946 03/28/17 22:54 JSF TAL NSHDissolved50 mL 50 mL
Analysis 6010D 1 418310 03/29/17 12:05 LCS TAL NSHDissolved
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 18:36 LCS TAL NSHTotal/NA
Prep 3005A 417947 03/28/17 22:56 JSF TAL NSHDissolved50 mL 50 mL
Analysis 6020B 1 418994 03/31/17 16:24 BLG TAL NSHDissolved
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:05 CME TAL NSHTotal/NA
Prep 7470A 417962 03/29/17 08:06 CAH TAL NSHDissolved30 mL 30 mL
Analysis 7470A 1 418661 03/29/17 12:39 CME TAL NSHDissolved
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:21 CAH TAL NSHTotal/NA
Client Sample ID: MW-4 Lab Sample ID: 490-123577-3
Matrix: WaterDate Collected: 03/08/17 13:27
Date Received: 03/11/17 10:05
Analysis 8260B RP03/20/17 19:361 TAL NSH415705
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 18:41 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:10 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:24 CAH TAL NSHTotal/NA
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-2R Lab Sample ID: 490-123577-4
Matrix: WaterDate Collected: 03/09/17 10:26
Date Received: 03/11/17 10:05
Analysis 8260B RP03/20/17 20:041 TAL NSH415705
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 18:46 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:16 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:27 CAH TAL NSHTotal/NA
Client Sample ID: MW-2RDUP Lab Sample ID: 490-123577-5
Matrix: WaterDate Collected: 03/09/17 10:26
Date Received: 03/11/17 10:05
Analysis 8260B RP03/20/17 20:321 TAL NSH415705
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 18:52 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:21 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:30 CAH TAL NSHTotal/NA
Client Sample ID: MW-3R Lab Sample ID: 490-123577-6
Matrix: WaterDate Collected: 03/08/17 14:00
Date Received: 03/11/17 10:05
Analysis 8260B RP03/21/17 15:531 TAL NSH415957
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 18:57 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:27 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:32 CAH TAL NSHTotal/NA
Client Sample ID: SP-1 Lab Sample ID: 490-123577-7
Matrix: WaterDate Collected: 03/09/17 11:30
Date Received: 03/11/17 10:05
Analysis 8260B RP03/21/17 16:211 TAL NSH415957
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 19:02 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: SP-1 Lab Sample ID: 490-123577-7
Matrix: WaterDate Collected: 03/09/17 11:30
Date Received: 03/11/17 10:05
Analysis 6020B CME03/30/17 06:321 TAL NSH418502
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:35 CAH TAL NSHTotal/NA
Client Sample ID: SS-1 Lab Sample ID: 490-123577-8
Matrix: WaterDate Collected: 03/09/17 10:55
Date Received: 03/11/17 10:05
Analysis 8260B RP03/21/17 16:491 TAL NSH415957
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 19:07 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:38 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:38 CAH TAL NSHTotal/NA
Client Sample ID: SS-2 Lab Sample ID: 490-123577-9
Matrix: WaterDate Collected: 03/09/17 11:10
Date Received: 03/11/17 10:05
Analysis 8260B RP03/20/17 21:001 TAL NSH415705
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 19:13 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:43 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:46 CAH TAL NSHTotal/NA
Client Sample ID: Trip Blank Lab Sample ID: 490-123577-10
Matrix: WaterDate Collected: 03/09/17 00:01
Date Received: 03/11/17 10:05
Analysis 8260B NC03/21/17 02:121 TAL NSH415793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-1
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-02CD Lab Sample ID: 490-123577-11
Matrix: WaterDate Collected: 03/08/17 10:49
Date Received: 03/11/17 10:05
Analysis 8260B RP03/21/17 17:181 TAL NSH415957
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 416007 03/21/17 12:46 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 19:28 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:49 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:49 CAH TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-123577-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-1
Project/Site: Polk County Route 9 Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Anchor QEA of North Carolina PLLC Job Number: 490-123577-1
SDG Number:
Login Number: 123577
Question Answer Comment
Creator: West, Derrick D
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-123577-2
Client Project/Site: Polk County Route 9 Landfill
For:
Anchor QEA of North Carolina PLLC
231 W Haywood Street
Asheville, North Carolina 28801
Attn: Brian Gant
Authorized for release by:
3/31/2017 3:31:14 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
TestAmerica Job ID: 490-123577-2
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
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Sample Summary
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-123577-12 MW-04CD-No Purge Water 03/08/17 09:18 03/11/17 10:05
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Case Narrative
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-2
Project/Site: Polk County Route 9 Landfill
Job ID: 490-123577-2
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-123577-2
Comments
No additional comments.
Receipt
The samples were received on 3/11/2017 10:05 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 0.3º C.
Metals
Method 6010D: The continuing calibration verification (CCV) associated with batch 490-416586 recovered above the upper control limit for
Chromium and Cadmium. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have
been reported. The following samples are impacted: (LCS 490-416007/2-A), (LCSD 490-416007/3-A), (MB 490-416007/1-A),
(490-123702-H-1-A), (490-123702-H-1-B MS), (490-123702-H-1-C MSD), (490-123702-H-1-A PDS) and (490-123702-H-1-A SD).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Qualifiers
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Lab Sample ID: 490-123577-12Client Sample ID: MW-04CD-No Purge
Matrix: WaterDate Collected: 03/08/17 09:18
Date Received: 03/11/17 10:05
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 03/21/17 12:46 03/22/17 19:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:33 1Barium0.232
0.00100 0.000500 mg/L 03/21/17 12:46 03/22/17 19:33 1Cadmium<0.000500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:33 1Chromium0.00760
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:33 1Copper<0.00500
0.00500 0.00200 mg/L 03/21/17 12:46 03/22/17 19:33 1Lead0.00610
0.0100 0.00300 mg/L 03/21/17 12:46 03/22/17 19:33 1Nickel<0.00300
0.0100 0.00500 mg/L 03/21/17 12:46 03/22/17 19:33 1Selenium<0.00500
0.00500 0.00300 mg/L 03/21/17 12:46 03/22/17 19:33 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:54 1Beryllium0.190 J
2.00 0.100 ug/L 03/21/17 12:51 03/30/17 06:54 1Cobalt2.39
2.00 0.800 ug/L 03/21/17 12:51 03/30/17 06:54 1Thallium<0.800
2.00 0.700 ug/L 03/21/17 12:51 03/30/17 06:54 1Vanadium13.9
25.0 5.20 ug/L 03/21/17 12:51 03/30/17 06:54 1Zinc23.9 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 07:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-416010/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
RL MDL
Antimony <0.800 2.00 0.800 ug/L 03/21/17 12:51 03/30/17 04:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.100 0.1002.00 ug/L 03/21/17 12:51 03/30/17 04:59 1Beryllium
<0.100 0.1002.00 ug/L 03/21/17 12:51 03/30/17 04:59 1Cobalt
<0.800 0.8002.00 ug/L 03/21/17 12:51 03/30/17 04:59 1Thallium
<5.20 5.2025.0 ug/L 03/21/17 12:51 03/30/17 04:59 1Zinc
Client Sample ID: Method BlankLab Sample ID: MB 490-416010/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418845 Prep Batch: 416010
RL MDL
Vanadium <0.700 2.00 0.700 ug/L 03/21/17 12:51 03/30/17 21:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-416010/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony 100 92.44 ug/L 92 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 102.2 ug/L 102 80-120
Cobalt 100 101.9 ug/L 102 80-120
Thallium 100 99.41 ug/L 99 80-120
Vanadium 100 101.8 ug/L 102 80-120
Zinc 100 87.99 ug/L 88 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-416010/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony 100 90.49 ug/L 90 80-120 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Beryllium 100 100.4 ug/L 100 80-120 2 20
Cobalt 100 98.42 ug/L 98 80-120 3 20
Thallium 100 97.53 ug/L 98 80-120 2 20
Vanadium 100 98.30 ug/L 98 80-120 3 20
Zinc 100 86.89 ug/L 87 80-120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-123717-H-1-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony <0.800 100 91.68 ug/L 92 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <0.100 100 101.6 ug/L 102 75-125
Cobalt 0.101 J 100 100.2 ug/L 100 75-125
Thallium <0.800 100 95.86 ug/L 96 75-125
Vanadium 5.46 100 101.9 ug/L 96 75-125
Zinc 19.4 J 100 103.7 ug/L 84 75-125
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QC Sample Results
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-123717-H-1-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 418502 Prep Batch: 416010
Antimony <0.800 100 91.89 ug/L 92 75-125 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.100 100 102.4 ug/L 102 75-125 1 20
Cobalt 0.101 J 100 97.76 ug/L 98 75-125 2 20
Thallium <0.800 100 96.79 ug/L 97 75-125 1 20
Vanadium 5.46 100 97.69 ug/L 92 75-125 4 20
Zinc 19.4 J 100 101.9 ug/L 83 75-125 2 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-415182/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
RL MDL
Mercury <0.100 0.200 0.100 ug/L 03/17/17 08:40 03/24/17 06:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-415182/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
Mercury 1.00 0.9638 ug/L 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-123570-B-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
Mercury <0.100 1.00 1.138 ug/L 114 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-123570-B-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 416854 Prep Batch: 415182
Mercury <0.100 1.00 1.028 ug/L 103 75-125 10 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Metals
Prep Batch: 415182
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-123577-12 MW-04CD-No Purge Total/NA
Water 7470AMB 490-415182/1-A Method Blank Total/NA
Water 7470ALCS 490-415182/2-A Lab Control Sample Total/NA
Water 7470A490-123570-B-1-B MS Matrix Spike Total/NA
Water 7470A490-123570-B-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 416007
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-123577-12 MW-04CD-No Purge Total/NA
Prep Batch: 416010
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-123577-12 MW-04CD-No Purge Total/NA
Water 3010AMB 490-416010/1-A Method Blank Total/NA
Water 3010ALCS 490-416010/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-416010/3-A Lab Control Sample Dup Total/NA
Water 3010A490-123717-H-1-C MS Matrix Spike Total/NA
Water 3010A490-123717-H-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 416586
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 416007490-123577-12 MW-04CD-No Purge Total/NA
Analysis Batch: 416854
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 415182490-123577-12 MW-04CD-No Purge Total/NA
Water 7470A 415182MB 490-415182/1-A Method Blank Total/NA
Water 7470A 415182LCS 490-415182/2-A Lab Control Sample Total/NA
Water 7470A 415182490-123570-B-1-B MS Matrix Spike Total/NA
Water 7470A 415182490-123570-B-1-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 418502
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 416010490-123577-12 MW-04CD-No Purge Total/NA
Water 6020B 416010MB 490-416010/1-A Method Blank Total/NA
Water 6020B 416010LCS 490-416010/2-A Lab Control Sample Total/NA
Water 6020B 416010LCSD 490-416010/3-A Lab Control Sample Dup Total/NA
Water 6020B 416010490-123717-H-1-C MS Matrix Spike Total/NA
Water 6020B 416010490-123717-H-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 418845
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 416010MB 490-416010/1-A Method Blank Total/NA
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-2
Project/Site: Polk County Route 9 Landfill
Client Sample ID: MW-04CD-No Purge Lab Sample ID: 490-123577-12
Matrix: WaterDate Collected: 03/08/17 09:18
Date Received: 03/11/17 10:05
Prep 3010A CAH03/21/17 12:46 TAL NSH416007
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis 6010D 1 416586 03/22/17 19:33 LCS TAL NSHTotal/NA
Prep 3010A 416010 03/21/17 12:51 CAH TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 418502 03/30/17 06:54 CME TAL NSHTotal/NA
Prep 7470A 415182 03/17/17 08:40 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 416854 03/24/17 07:51 CAH TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-123577-2Client: Anchor QEA of North Carolina PLLC
Project/Site: Polk County Route 9 Landfill
Method Method Description LaboratoryProtocol
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-123577-2
Project/Site: Polk County Route 9 Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
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Login Sample Receipt Checklist
Client: Anchor QEA of North Carolina PLLC Job Number: 490-123577-2
SDG Number:
Login Number: 123577
Question Answer Comment
Creator: West, Derrick D
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
Page 16 of 16 3/31/2017
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