Loading...
HomeMy WebLinkAbout19025_AMI_VIR_20160421MINERAL SPRINGS ENVIRONMENTAL, P.C. 4600 MINERAL SPRINGS LANE RALEIGH, NORTH CAROLINA, 27616 919.261.8186 INDOOR AIR QUALITY AND GROUNDWATER SAMPLING REPORT FORMER AMERICAN MULTIMEDIA SITE 2609 TUCKER STREET EXTENSION BURLINGTON, ALAMANCE COUNTY, NORTH CAROLINA APRIL 21, 2016 MSE JOB NO. 849 Prepared For: MR. MILT PETTY CAROLINA HOSIERY MILLS INC. 710 KOURY DRIVE BURLINGTON, NORTH CAROLINA, 27215 DRAWINGS DRAWING NO. 1 TOPOGRAPHIC SITE MAP FORMER AMI SITE 2609 TUCKER STREET BURLINGTON, NORTH CAROLINA Date: February 2015 Job No.: MSE 849 File: 849/Drawing 1 By: KP SITE TABLES TA B L E 1 CO N C E N T R A T I O N O F S E L E C T E D C O N S T I T U E N T S I N I N D O O R A I R FO R M E R A M E R I C A N M U L T I M E D I A P R O P E R T Y BU R L I N G T O N , N O R T H C A R O L I N A MS E J O B N O . 8 4 9 An a l y t i c a l R e s u l t ( m i c r o g r a m s p e r c u b i c m e t e r ) IA - 1 I A - 2 I A - 3 I A - 4 I A - 5 I A - 6 I A - 7 I A - 8 I A - 9 I A - 1 0 I A - 1 1 No n - R e s i d e n t i a l S c r e e n i n g V a l u e 2 P r o p a n o l ND 1. 9 J 2. 1 J 1. 9 J 1. 9 J 2. 1 J 1. 9 J 2. 5 J 1. 8 J 2. 6 J ND NE 2 B u t a n o n e ND ND ND 3. 3 J ND 3. 3 J 2. 5 J ND ND 2. 6 J ND 4,380 Ac e t o n e 11 10 13 9. 7 11 13 13 12 11 12 6. 7 27,200 Ca r b o n D i s u l f i d e 3. 8 J ND ND ND ND ND ND ND ND ND ND 613 Ch l o r o f o r m ND ND ND ND ND ND ND 1. 6 J ND 1. 6 J ND 0.53 Ch l o r o m e t h a n e 1. 6 J 1. 5 J 1. 2 J 1. 2 J 1. 2 J 1. 3 J 1. 2 J 0. 9 8 J 1. 1 J 1. 2 J 1. 1 J 78 Di c h l o r o d i f l u o r o m e t h a n e 2. 2 J 1. 7 J 1. 6 J ND ND ND ND ND 1. 5 J 1. 5 J 1. 6 87 T e t r a c h l o r o e t h e n e 3. 3 J ND ND ND ND ND ND ND ND ND ND 35 Tr i c h l o r o f l u o r o m e t h a n e 1. 4 J 1. 3 J ND ND ND ND ND ND ND ND ND NE No t e s : NS - N o S t a n d a r d NE - N o t E s t a b l i s h e d ND - n o t d e t e c t e d Co n s t i t u e n t SA M P L E DA T E PC E Tr a n s 1 , 2 DC E T C E Vi n y l Ch l o r i d e Ci s 1 , 2 DC E ID CO L L E C T E D (µ g / L ) (µ g / L ) (µ g / L ) (µ g / L ) (µ g / L ) MW - 1 04 / 0 1 / 1 6 19 0 26 86 0 1 8 0 7 3 0 MW - 7 04 / 0 1 / 1 6 B Q L B Q L B Q L B Q L B Q L MW - 8 04 / 0 1 / 1 6 16 BQ L 3. 6 BQ L 3 . 1 MW - 9 04 / 0 1 / 1 6 4, 1 0 0 BQ L 26 0 BQ L 4 1 J MW - 1 0 04 / 0 1 / 1 6 4, 9 0 0 BQ L 2, 1 0 0 BQ L 27 0 MW - 1 3 04 / 0 1 / 1 6 21 , 0 0 0 BQ L 66 0 BQ L 65 0 NC G r o u n d w a t e r St a n d a r d 0. 7 1 0 0 2 . 8 0 . 0 3 7 0 No t e s : ug / l = m i c r o g r a m s p e r l i t e r MS E J o b 8 4 9 TA B L E 2 GR O U N D W A T E R S A M P L E A N A L Y T I C A L R E S U L T S FO R M E R A M E R I C A N M U L T I M E D I A P R O P E R T Y BU R L I N G T O N , N O R T H C A R O L I N A TC E - T r i c h l o r o e t h e n e Ci s 1 , 2 D C E - C i s 1 , 2 D i c h l o r o e t h e n e PC E - T e t r a c h l o r o e t h e n e Tr a n s 1 , 2 D C E - T r a n s 1 , 2 D i c h l o r o e t h e n e APPENDICES APPENDIX A PHOTOGRAPHS APPENDIX B INDOOR AND OUTSIDE AIR QUALITY AND GROUNDWATER ANALYTICAL RESULTS 4810 Executive Park Court, Suite 111 Jacksonville FL, 32216-6069 904.296.3007 904.296.6210Phone:FAX: ENCO Workorder(s): BZ01154 Raleigh, NC 27616 Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Enclosure(s) Project Number: [none], Project Name/Desc: AMI Attn: Kirk Pollard Mineral Springs Environmental (MI017) 4600 Mineral Springs Lane Chris Tompkins Project Manager Tuesday, April 12, 2016 RE: Laboratory Results for Dear Kirk Pollard, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, April 5, 2016. Enclosure(s) Page 1 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE IA-1 BZ01154-01RE1 Sampled:04/01/16 16:22 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 01:08 IA-2 BZ01154-02RE1 Sampled:04/01/16 16:11 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 01:48 IA-3 BZ01154-03RE1 Sampled:04/01/16 16:30 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 02:28 IA-4 BZ01154-04RE1 Sampled:04/01/16 16:33 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 03:07 IA-5 BZ01154-05RE2 Sampled:04/01/16 16:24 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/12/16 11:08 04/12/16 11:08 IA-6 BZ01154-06RE1 Sampled:04/01/16 16:29 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 10:12 IA-7 BZ01154-07RE1 Sampled:04/01/16 16:32 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 10:51 IA-8 BZ01154-08RE1 Sampled:04/01/16 16:33 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 11:31 IA-9 BZ01154-09RE1 Sampled:04/01/16 16:16 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 12:11 IA-10 BZ01154-10RE1 Sampled:04/01/16 16:18 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 12:52 IA-11 BZ01154-11RE1 Sampled:04/01/16 16:06 Received:04/05/16 10:00Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) TO-15 04/15/16 04/06/16 15:13 04/07/16 13:32 Page 2 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com SAMPLE DETECTION SUMMARY Lab ID:Client ID:IA-1 BZ01154-01RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 11 7.8 ug/m³ Air TO-15D Acetone 4.8 3.8 10 ug/m³ Air TO-15JD Carbon disulfide 0.94 1.6 6.8 ug/m³ Air TO-15JD Chloromethane 0.78 2.2 16 ug/m³ Air TO-15JD Dichlorodifluoromethane 1.6 3.3 22 ug/m³ Air TO-15JD Tetrachloroethene 1.7 1.4 18 ug/m³ Air TO-15JD Trichlorofluoromethane 1.3 Lab ID:Client ID:IA-2 BZ01154-02RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 1.9 7.9 ug/m³ Air TO-15JD 2-Propanol 1.8 10 7.7 ug/m³ Air TO-15D Acetone 4.7 1.5 6.7 ug/m³ Air TO-15JD Chloromethane 0.77 1.7 16 ug/m³ Air TO-15JD Dichlorodifluoromethane 1.5 1.3 18 ug/m³ Air TO-15JD Trichlorofluoromethane 1.2 Lab ID:Client ID:IA-3 BZ01154-03RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 2.1 7.9 ug/m³ Air TO-15JD 2-Propanol 1.8 13 7.7 ug/m³ Air TO-15D Acetone 4.7 1.2 6.7 ug/m³ Air TO-15JD Chloromethane 0.77 1.6 16 ug/m³ Air TO-15JD Dichlorodifluoromethane 1.5 Lab ID:Client ID:IA-4 BZ01154-04RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 1.9 8.0 ug/m³ Air TO-15JD 2-Propanol 1.9 9.7 7.7 ug/m³ Air TO-15D Acetone 4.8 1.2 6.7 ug/m³ Air TO-15JD Chloromethane 0.78 Lab ID:Client ID:IA-5 BZ01154-05RE2 Analyte MethodUnitsPQLResultsFlag NotesMDL 1.9 8.0 ug/m³ Air TO-15JD 2-Propanol 1.9 11 7.7 ug/m³ Air TO-15D Acetone 4.8 1.2 6.7 ug/m³ Air TO-15JD Chloromethane 0.78 Lab ID:Client ID:IA-6 BZ01154-06RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 3.3 9.5 ug/m³ Air TO-15JD 2-Butanone 2.5 2.1 7.9 ug/m³ Air TO-15JD 2-Propanol 1.8 13 7.7 ug/m³ Air TO-15D Acetone 4.7 1.3 6.7 ug/m³ Air TO-15JD Chloromethane 0.77 Lab ID:Client ID:IA-7 BZ01154-07RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 2.5 9.6 ug/m³ Air TO-15JD 2-Butanone 2.5 1.9 8.0 ug/m³ Air TO-15JD 2-Propanol 1.9 13 7.7 ug/m³ Air TO-15D Acetone 4.8 1.2 6.7 ug/m³ Air TO-15JD Chloromethane 0.78 Lab ID:Client ID:IA-8 BZ01154-08RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 2.5 7.9 ug/m³ Air TO-15JD 2-Propanol 1.8 12 7.6 ug/m³ Air TO-15D Acetone 4.7 1.6 16 ug/m³ Air TO-15JD Chloroform 1.2 0.98 6.6 ug/m³ Air TO-15JD Chloromethane 0.77 Lab ID:Client ID:IA-9 BZ01154-09RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 1.8 7.8 ug/m³ Air TO-15JD 2-Propanol 1.8 11 7.5 ug/m³ Air TO-15D Acetone 4.6 1.1 6.6 ug/m³ Air TO-15JD Chloromethane 0.76 1.5 16 ug/m³ Air TO-15JD Dichlorodifluoromethane 1.5 Page 3 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com SAMPLE DETECTION SUMMARY Lab ID:Client ID:IA-10 BZ01154-10RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 2.6 9.4 ug/m³ Air TO-15JD 2-Butanone 2.5 2.6 7.9 ug/m³ Air TO-15JD 2-Propanol 1.8 12 7.6 ug/m³ Air TO-15D Acetone 4.7 1.6 16 ug/m³ Air TO-15JD Chloroform 1.2 1.2 6.6 ug/m³ Air TO-15JD Chloromethane 0.77 1.5 16 ug/m³ Air TO-15JD Dichlorodifluoromethane 1.5 Lab ID:Client ID:IA-11 BZ01154-11RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 6.7 7.8 ug/m³ Air TO-15JD Acetone 4.8 1.1 6.8 ug/m³ Air TO-15JD Chloromethane 0.79 1.6 16 ug/m³ Air TO-15JD Dichlorodifluoromethane 1.6 Page 4 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-1Description:Lab Sample ID:BZ01154-01 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:22Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 01:081,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007181.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007181.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,1-Dichloroethene [75-35-4]0.94 LTS6D06007130.94 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,2,4-Trichlorobenzene [120-82-1]7.3 LTS6D06007247.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,2,4-Trimethylbenzene [95-63-6]1.9 LTS6D06007161.9 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007203.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,2-Dichloroethane [107-06-2]0.80 LTS6D06007130.80 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,3-Butadiene [106-99-0]0.75 LTS6D060077.20.75 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,3-Dichlorobenzene [541-73-1]3.2 LTS6D06007203.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007203.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:081,4-Dioxane [123-91-1]3.0 LTS6D06007123.0 UD 1.31 ug/m³ Air TO-15 04/07/16 01:082,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.31 ug/m³ Air TO-15 04/07/16 01:082-Butanone [78-93-3]2.5 LTS6D060079.72.5 UD 1.31 ug/m³ Air TO-15 04/07/16 01:082-Hexanone [591-78-6]2.1 LTS6D06007132.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:082-Propanol [67-63-0]1.9 LTS6D060078.01.9 UD 1.31 ug/m³ Air TO-15 04/07/16 01:083-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.31 ug/m³ Air TO-15 04/07/16 01:084-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.31 ug/m³ Air TO-15 04/07/16 01:084-Methyl-2-pentanone [108-10-1]1.8 LTS6D06007131.8 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Acetone [67-64-1]4.8 LTS6D060077.811D 1.31 ug/m³ Air TO-15 04/07/16 01:08Benzene [71-43-2]0.96 LTS6D06007100.96 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Bromoethene [593-60-2]1.3 LTS6D06007141.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Bromoform [75-25-2]2.7 LTS6D06007342.7 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Carbon disulfide [75-15-0]0.94 LTS6D06007103.8 JD 1.31 ug/m³ Air TO-15 04/07/16 01:08Carbon tetrachloride [56-23-5]1.4 LTS6D06007211.4 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Chloroethane [75-00-3]0.97 LTS6D060078.60.97 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Chloromethane [74-87-3]0.78 LTS6D060076.81.6 JD 1.31 ug/m³ Air TO-15 04/07/16 01:08cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Dibromochloromethane [124-48-1]1.6 LTS6D06007281.6 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Dichlorodifluoromethane [75-71-8]1.6 LTS6D06007162.2 JD 1.31 ug/m³ Air TO-15 04/07/16 01:08Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Hexachlorobutadiene [87-68-3]8.0 LTS6D06007358.0 UD 1.31 Page 5 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-1Description:Lab Sample ID:BZ01154-01 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:22Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 01:08Methylene chloride [75-09-2]1.4 LTS6D06007111.4 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Methyl-tert-butyl ether [1634-04-4]0.85 LTS6D06007120.85 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08n-Hexane [110-54-3]1.5 LTS6D06007121.5 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Propene [115-07-1]0.77 LTS6D060075.60.77 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Tetrachloroethene [127-18-4]1.7 LTS6D06007223.3 JD 1.31 ug/m³ Air TO-15 04/07/16 01:08Tetrahydrofuran [109-99-9]1.1 LTS6D060079.71.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Toluene [108-88-3]0.99 LTS6D06007120.99 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.31 ug/m³ Air TO-15 04/07/16 01:08trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08trans-1,3-Dichloropropene [10061-02-6]0.95 LTS6D06007150.95 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Trichloroethene [79-01-6]1.6 LTS6D06007181.6 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Trichlorofluoromethane [75-69-4]1.3 LTS6D06007181.4 JD 1.31 ug/m³ Air TO-15 04/07/16 01:08Vinyl acetate [108-05-4]1.1 LTS6D06007121.1 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Vinyl chloride [75-01-4]1.0 LTS6D060078.41.0 UD 1.31 ug/m³ Air TO-15 04/07/16 01:08Xylenes (Total) [1330-20-7]2.6 LTS6D06007142.6 UD 1.31 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13094 %LTSTO-15 04/07/16 01:086D060072931.2 1 Page 6 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-2Description:Lab Sample ID:BZ01154-02 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:11Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 01:481,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007181.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007181.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,1-Dichloroethene [75-35-4]0.92 LTS6D06007130.92 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,2,4-Trichlorobenzene [120-82-1]7.2 LTS6D06007247.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,2,4-Trimethylbenzene [95-63-6]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007193.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,2-Dichloroethane [107-06-2]0.78 LTS6D06007130.78 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,3-Butadiene [106-99-0]0.74 LTS6D060077.10.74 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007193.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007193.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:481,4-Dioxane [123-91-1]2.9 LTS6D06007122.9 UD 1.29 ug/m³ Air TO-15 04/07/16 01:482,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.29 ug/m³ Air TO-15 04/07/16 01:482-Butanone [78-93-3]2.5 LTS6D060079.52.5 UD 1.29 ug/m³ Air TO-15 04/07/16 01:482-Hexanone [591-78-6]2.1 LTS6D06007132.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:482-Propanol [67-63-0]1.8 LTS6D060077.91.9 JD 1.29 ug/m³ Air TO-15 04/07/16 01:483-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.29 ug/m³ Air TO-15 04/07/16 01:484-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 01:484-Methyl-2-pentanone [108-10-1]1.7 LTS6D06007131.7 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Acetone [67-64-1]4.7 LTS6D060077.710D 1.29 ug/m³ Air TO-15 04/07/16 01:48Benzene [71-43-2]0.95 LTS6D06007100.95 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Bromoethene [593-60-2]1.2 LTS6D06007141.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Bromoform [75-25-2]2.7 LTS6D06007332.7 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Carbon disulfide [75-15-0]0.92 LTS6D06007100.92 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Chloroethane [75-00-3]0.95 LTS6D060078.50.95 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Chloromethane [74-87-3]0.77 LTS6D060076.71.5 JD 1.29 ug/m³ Air TO-15 04/07/16 01:48cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Dibromochloromethane [124-48-1]1.5 LTS6D06007271.5 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.7 JD 1.29 ug/m³ Air TO-15 04/07/16 01:48Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Hexachlorobutadiene [87-68-3]7.8 LTS6D06007347.8 UD 1.29 Page 7 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-2Description:Lab Sample ID:BZ01154-02 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:11Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 01:48Methylene chloride [75-09-2]1.3 LTS6D06007111.3 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Methyl-tert-butyl ether [1634-04-4]0.84 LTS6D06007120.84 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48n-Hexane [110-54-3]1.5 LTS6D06007111.5 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Propene [115-07-1]0.75 LTS6D060075.60.75 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Tetrachloroethene [127-18-4]1.7 LTS6D06007221.7 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Tetrahydrofuran [109-99-9]1.1 LTS6D060079.51.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Toluene [108-88-3]0.97 LTS6D06007120.97 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.29 ug/m³ Air TO-15 04/07/16 01:48trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48trans-1,3-Dichloropropene [10061-02-6]0.94 LTS6D06007150.94 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.3 JD 1.29 ug/m³ Air TO-15 04/07/16 01:48Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Vinyl chloride [75-01-4]0.99 LTS6D060078.20.99 UD 1.29 ug/m³ Air TO-15 04/07/16 01:48Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.29 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13096 %LTSTO-15 04/07/16 01:486D060073031.2 1 Page 8 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-3Description:Lab Sample ID:BZ01154-03 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:30Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 02:281,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007181.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007181.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,1-Dichloroethene [75-35-4]0.92 LTS6D06007130.92 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,2,4-Trichlorobenzene [120-82-1]7.2 LTS6D06007247.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,2,4-Trimethylbenzene [95-63-6]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007193.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,2-Dichloroethane [107-06-2]0.78 LTS6D06007130.78 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,3-Butadiene [106-99-0]0.74 LTS6D060077.10.74 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007193.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007193.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:281,4-Dioxane [123-91-1]2.9 LTS6D06007122.9 UD 1.29 ug/m³ Air TO-15 04/07/16 02:282,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.29 ug/m³ Air TO-15 04/07/16 02:282-Butanone [78-93-3]2.5 LTS6D060079.52.5 UD 1.29 ug/m³ Air TO-15 04/07/16 02:282-Hexanone [591-78-6]2.1 LTS6D06007132.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:282-Propanol [67-63-0]1.8 LTS6D060077.92.1 JD 1.29 ug/m³ Air TO-15 04/07/16 02:283-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.29 ug/m³ Air TO-15 04/07/16 02:284-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 02:284-Methyl-2-pentanone [108-10-1]1.7 LTS6D06007131.7 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Acetone [67-64-1]4.7 LTS6D060077.713D 1.29 ug/m³ Air TO-15 04/07/16 02:28Benzene [71-43-2]0.95 LTS6D06007100.95 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Bromoethene [593-60-2]1.2 LTS6D06007141.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Bromoform [75-25-2]2.7 LTS6D06007332.7 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Carbon disulfide [75-15-0]0.92 LTS6D06007100.92 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Chloroethane [75-00-3]0.95 LTS6D060078.50.95 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Chloromethane [74-87-3]0.77 LTS6D060076.71.2 JD 1.29 ug/m³ Air TO-15 04/07/16 02:28cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Dibromochloromethane [124-48-1]1.5 LTS6D06007271.5 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.6 JD 1.29 ug/m³ Air TO-15 04/07/16 02:28Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Hexachlorobutadiene [87-68-3]7.8 LTS6D06007347.8 UD 1.29 Page 9 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-3Description:Lab Sample ID:BZ01154-03 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:30Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 02:28Methylene chloride [75-09-2]1.3 LTS6D06007111.3 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Methyl-tert-butyl ether [1634-04-4]0.84 LTS6D06007120.84 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28n-Hexane [110-54-3]1.5 LTS6D06007111.5 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Propene [115-07-1]0.75 LTS6D060075.60.75 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Tetrachloroethene [127-18-4]1.7 LTS6D06007221.7 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Tetrahydrofuran [109-99-9]1.1 LTS6D060079.51.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Toluene [108-88-3]0.97 LTS6D06007120.97 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.29 ug/m³ Air TO-15 04/07/16 02:28trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28trans-1,3-Dichloropropene [10061-02-6]0.94 LTS6D06007150.94 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Vinyl chloride [75-01-4]0.99 LTS6D060078.20.99 UD 1.29 ug/m³ Air TO-15 04/07/16 02:28Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.29 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13095 %LTSTO-15 04/07/16 02:286D060073031.2 1 Page 10 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-4Description:Lab Sample ID:BZ01154-04 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:33Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 03:071,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007181.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007181.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,1-Dichloroethene [75-35-4]0.93 LTS6D06007130.93 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,2,4-Trichlorobenzene [120-82-1]7.2 LTS6D06007247.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,2,4-Trimethylbenzene [95-63-6]1.9 LTS6D06007161.9 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007203.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,2-Dichloroethane [107-06-2]0.79 LTS6D06007130.79 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,3-Butadiene [106-99-0]0.75 LTS6D060077.20.75 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007203.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007203.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:071,4-Dioxane [123-91-1]3.0 LTS6D06007123.0 UD 1.3 ug/m³ Air TO-15 04/07/16 03:072,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.3 ug/m³ Air TO-15 04/07/16 03:072-Butanone [78-93-3]2.5 LTS6D060079.62.5 UD 1.3 ug/m³ Air TO-15 04/07/16 03:072-Hexanone [591-78-6]2.1 LTS6D06007132.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:072-Propanol [67-63-0]1.9 LTS6D060078.01.9 JD 1.3 ug/m³ Air TO-15 04/07/16 03:073-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.3 ug/m³ Air TO-15 04/07/16 03:074-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.3 ug/m³ Air TO-15 04/07/16 03:074-Methyl-2-pentanone [108-10-1]1.8 LTS6D06007131.8 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Acetone [67-64-1]4.8 LTS6D060077.79.7 D 1.3 ug/m³ Air TO-15 04/07/16 03:07Benzene [71-43-2]0.96 LTS6D06007100.96 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Bromoethene [593-60-2]1.3 LTS6D06007141.3 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Bromoform [75-25-2]2.7 LTS6D06007342.7 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Carbon disulfide [75-15-0]0.93 LTS6D06007100.93 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Chloroethane [75-00-3]0.96 LTS6D060078.60.96 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Chloromethane [74-87-3]0.78 LTS6D060076.71.2 JD 1.3 ug/m³ Air TO-15 04/07/16 03:07cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Dibromochloromethane [124-48-1]1.6 LTS6D06007281.6 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.5 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Hexachlorobutadiene [87-68-3]7.9 LTS6D06007357.9 UD 1.3 Page 11 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-4Description:Lab Sample ID:BZ01154-04 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:33Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 03:07Methylene chloride [75-09-2]1.4 LTS6D06007111.4 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Methyl-tert-butyl ether [1634-04-4]0.84 LTS6D06007120.84 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07n-Hexane [110-54-3]1.5 LTS6D06007111.5 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Propene [115-07-1]0.76 LTS6D060075.60.76 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Tetrachloroethene [127-18-4]1.7 LTS6D06007221.7 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Tetrahydrofuran [109-99-9]1.1 LTS6D060079.61.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Toluene [108-88-3]0.98 LTS6D06007120.98 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.3 ug/m³ Air TO-15 04/07/16 03:07trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07trans-1,3-Dichloropropene [10061-02-6]0.94 LTS6D06007150.94 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Vinyl chloride [75-01-4]1.0 LTS6D060078.31.0 UD 1.3 ug/m³ Air TO-15 04/07/16 03:07Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.3 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13090 %LTSTO-15 04/07/16 03:076D060072831.2 1 Page 12 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-5Description:Lab Sample ID:BZ01154-05 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:24Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/12/16 11:081,1,1-Trichloroethane [71-55-6]1.1 LTS6D12006181.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D12006222.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,1,2-Trichloroethane [79-00-5]1.1 LTS6D12006181.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,1-Dichloroethane [75-34-3]1.1 LTS6D12006131.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,1-Dichloroethene [75-35-4]0.93 LTS6D12006130.93 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,2,4-Trichlorobenzene [120-82-1]7.2 LTS6D12006247.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,2,4-Trimethylbenzene [95-63-6]1.9 LTS6D12006161.9 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,2-Dibromoethane [106-93-4]1.8 LTS6D12006251.8 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,2-Dichlorobenzene [95-50-1]3.2 LTS6D12006203.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,2-Dichloroethane [107-06-2]0.79 LTS6D12006130.79 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,2-Dichloropropane [78-87-5]1.3 LTS6D12006151.3 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D12006161.8 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,3-Butadiene [106-99-0]0.75 LTS6D120067.20.75 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,3-Dichlorobenzene [541-73-1]3.1 LTS6D12006203.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,4-Dichlorobenzene [106-46-7]3.2 LTS6D12006203.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:081,4-Dioxane [123-91-1]3.0 LTS6D12006123.0 UD 1.3 ug/m³ Air TO-15 04/12/16 11:082,2,4-Trimethylpentane [540-84-1]1.6 LTS6D12006151.6 UD 1.3 ug/m³ Air TO-15 04/12/16 11:082-Butanone [78-93-3]2.5 LTS6D120069.62.5 UD 1.3 ug/m³ Air TO-15 04/12/16 11:082-Hexanone [591-78-6]2.1 LTS6D12006132.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:082-Propanol [67-63-0]1.9 LTS6D120068.01.9 JD 1.3 ug/m³ Air TO-15 04/12/16 11:083-Chloropropene [107-05-1]1.0 LTS6D12006101.0 UD 1.3 ug/m³ Air TO-15 04/12/16 11:084-Ethyltoluene [622-96-8]1.8 LTS6D12006161.8 UD 1.3 ug/m³ Air TO-15 04/12/16 11:084-Methyl-2-pentanone [108-10-1]1.8 LTS6D12006131.8 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Acetone [67-64-1]4.8 LTS6D120067.711D 1.3 ug/m³ Air TO-15 04/12/16 11:08Benzene [71-43-2]0.96 LTS6D12006100.96 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Benzyl chloride [100-44-7]2.1 LTS6D12006172.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Bromodichloromethane [75-27-4]1.3 LTS6D12006221.3 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Bromoethene [593-60-2]1.3 LTS6D12006141.3 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Bromoform [75-25-2]2.7 LTS6D12006342.7 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Bromomethane [74-83-9]1.1 LTS6D12006131.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Carbon disulfide [75-15-0]0.93 LTS6D12006100.93 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Carbon tetrachloride [56-23-5]1.4 LTS6D12006201.4 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Chlorobenzene [108-90-7]1.4 LTS6D12006151.4 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Chloroethane [75-00-3]0.96 LTS6D120068.60.96 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Chloroform [67-66-3]1.2 LTS6D12006161.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Chloromethane [74-87-3]0.78 LTS6D120066.71.2 JD 1.3 ug/m³ Air TO-15 04/12/16 11:08cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D12006131.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D12006151.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Cyclohexane [110-82-7]1.2 LTS6D12006111.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Dibromochloromethane [124-48-1]1.6 LTS6D12006281.6 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Dichlorodifluoromethane [75-71-8]1.5 LTS6D12006161.5 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Ethyl Acetate [141-78-6]1.1 LTS6D12006121.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Ethylbenzene [100-41-4]1.3 LTS6D12006141.3 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Freon 113 [76-13-1]2.3 LTS6D12006252.3 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Freon 114 [76-14-2]3.1 LTS6D12006233.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Heptane [142-82-5]1.5 LTS6D12006131.5 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Hexachlorobutadiene [87-68-3]7.9 LTS6D12006357.9 UD 1.3 Page 13 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-5Description:Lab Sample ID:BZ01154-05 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:24Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/12/16 11:08Methylene chloride [75-09-2]1.4 LTS6D12006111.4 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Methyl-tert-butyl ether [1634-04-4]0.84 LTS6D12006120.84 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08n-Hexane [110-54-3]1.5 LTS6D12006111.5 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Propene [115-07-1]0.76 LTS6D120065.60.76 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Styrene [100-42-5]1.3 LTS6D12006141.3 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Tetrachloroethene [127-18-4]1.7 LTS6D12006221.7 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Tetrahydrofuran [109-99-9]1.1 LTS6D120069.61.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Toluene [108-88-3]0.98 LTS6D12006120.98 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Total Light Petroleum Hydrocarbons 1200 LTS6D1200612001200UD 1.3 ug/m³ Air TO-15 04/12/16 11:08trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D12006131.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08trans-1,3-Dichloropropene [10061-02-6]0.94 LTS6D12006150.94 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Trichloroethene [79-01-6]1.6 LTS6D12006171.6 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Trichlorofluoromethane [75-69-4]1.2 LTS6D12006181.2 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Vinyl acetate [108-05-4]1.1 LTS6D12006111.1 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Vinyl chloride [75-01-4]1.0 LTS6D120068.31.0 UD 1.3 ug/m³ Air TO-15 04/12/16 11:08Xylenes (Total) [1330-20-7]2.5 LTS6D12006142.5 UD 1.3 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13088 %LTSTO-15 04/12/16 11:086D120062831.2 1 Page 14 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-6Description:Lab Sample ID:BZ01154-06 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:29Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 10:121,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007181.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007181.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,1-Dichloroethene [75-35-4]0.92 LTS6D06007130.92 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,2,4-Trichlorobenzene [120-82-1]7.2 LTS6D06007247.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,2,4-Trimethylbenzene [95-63-6]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007193.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,2-Dichloroethane [107-06-2]0.78 LTS6D06007130.78 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,3-Butadiene [106-99-0]0.74 LTS6D060077.10.74 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007193.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007193.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:121,4-Dioxane [123-91-1]2.9 LTS6D06007122.9 UD 1.29 ug/m³ Air TO-15 04/07/16 10:122,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.29 ug/m³ Air TO-15 04/07/16 10:122-Butanone [78-93-3]2.5 LTS6D060079.53.3 JD 1.29 ug/m³ Air TO-15 04/07/16 10:122-Hexanone [591-78-6]2.1 LTS6D06007132.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:122-Propanol [67-63-0]1.8 LTS6D060077.92.1 JD 1.29 ug/m³ Air TO-15 04/07/16 10:123-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.29 ug/m³ Air TO-15 04/07/16 10:124-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.29 ug/m³ Air TO-15 04/07/16 10:124-Methyl-2-pentanone [108-10-1]1.7 LTS6D06007131.7 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Acetone [67-64-1]4.7 LTS6D060077.713D 1.29 ug/m³ Air TO-15 04/07/16 10:12Benzene [71-43-2]0.95 LTS6D06007100.95 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Bromoethene [593-60-2]1.2 LTS6D06007141.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Bromoform [75-25-2]2.7 LTS6D06007332.7 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Carbon disulfide [75-15-0]0.92 LTS6D06007100.92 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Chloroethane [75-00-3]0.95 LTS6D060078.50.95 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Chloromethane [74-87-3]0.77 LTS6D060076.71.3 JD 1.29 ug/m³ Air TO-15 04/07/16 10:12cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Dibromochloromethane [124-48-1]1.5 LTS6D06007271.5 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.5 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Hexachlorobutadiene [87-68-3]7.8 LTS6D06007347.8 UD 1.29 Page 15 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-6Description:Lab Sample ID:BZ01154-06 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:29Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 10:12Methylene chloride [75-09-2]1.3 LTS6D06007111.3 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Methyl-tert-butyl ether [1634-04-4]0.84 LTS6D06007120.84 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12n-Hexane [110-54-3]1.5 LTS6D06007111.5 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Propene [115-07-1]0.75 LTS6D060075.60.75 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Tetrachloroethene [127-18-4]1.7 LTS6D06007221.7 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Tetrahydrofuran [109-99-9]1.1 LTS6D060079.51.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Toluene [108-88-3]0.97 LTS6D06007120.97 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.29 ug/m³ Air TO-15 04/07/16 10:12trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12trans-1,3-Dichloropropene [10061-02-6]0.94 LTS6D06007150.94 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Vinyl chloride [75-01-4]0.99 LTS6D060078.20.99 UD 1.29 ug/m³ Air TO-15 04/07/16 10:12Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.29 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13090 %LTSTO-15 04/07/16 10:126D060072831.2 1 Page 16 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-7Description:Lab Sample ID:BZ01154-07 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:32Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 10:511,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007181.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007181.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,1-Dichloroethene [75-35-4]0.93 LTS6D06007130.93 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,2,4-Trichlorobenzene [120-82-1]7.2 LTS6D06007247.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,2,4-Trimethylbenzene [95-63-6]1.9 LTS6D06007161.9 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007203.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,2-Dichloroethane [107-06-2]0.79 LTS6D06007130.79 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,3-Butadiene [106-99-0]0.75 LTS6D060077.20.75 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007203.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007203.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:511,4-Dioxane [123-91-1]3.0 LTS6D06007123.0 UD 1.3 ug/m³ Air TO-15 04/07/16 10:512,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.3 ug/m³ Air TO-15 04/07/16 10:512-Butanone [78-93-3]2.5 LTS6D060079.62.5 JD 1.3 ug/m³ Air TO-15 04/07/16 10:512-Hexanone [591-78-6]2.1 LTS6D06007132.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:512-Propanol [67-63-0]1.9 LTS6D060078.01.9 JD 1.3 ug/m³ Air TO-15 04/07/16 10:513-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.3 ug/m³ Air TO-15 04/07/16 10:514-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.3 ug/m³ Air TO-15 04/07/16 10:514-Methyl-2-pentanone [108-10-1]1.8 LTS6D06007131.8 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Acetone [67-64-1]4.8 LTS6D060077.713D 1.3 ug/m³ Air TO-15 04/07/16 10:51Benzene [71-43-2]0.96 LTS6D06007100.96 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Bromoethene [593-60-2]1.3 LTS6D06007141.3 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Bromoform [75-25-2]2.7 LTS6D06007342.7 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Carbon disulfide [75-15-0]0.93 LTS6D06007100.93 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Chloroethane [75-00-3]0.96 LTS6D060078.60.96 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Chloromethane [74-87-3]0.78 LTS6D060076.71.2 JD 1.3 ug/m³ Air TO-15 04/07/16 10:51cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Dibromochloromethane [124-48-1]1.6 LTS6D06007281.6 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.5 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Hexachlorobutadiene [87-68-3]7.9 LTS6D06007357.9 UD 1.3 Page 17 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-7Description:Lab Sample ID:BZ01154-07 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:32Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 10:51Methylene chloride [75-09-2]1.4 LTS6D06007111.4 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Methyl-tert-butyl ether [1634-04-4]0.84 LTS6D06007120.84 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51n-Hexane [110-54-3]1.5 LTS6D06007111.5 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Propene [115-07-1]0.76 LTS6D060075.60.76 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Tetrachloroethene [127-18-4]1.7 LTS6D06007221.7 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Tetrahydrofuran [109-99-9]1.1 LTS6D060079.61.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Toluene [108-88-3]0.98 LTS6D06007120.98 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.3 ug/m³ Air TO-15 04/07/16 10:51trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51trans-1,3-Dichloropropene [10061-02-6]0.94 LTS6D06007150.94 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Vinyl chloride [75-01-4]1.0 LTS6D060078.31.0 UD 1.3 ug/m³ Air TO-15 04/07/16 10:51Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.3 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13089 %LTSTO-15 04/07/16 10:516D060072831.2 1 Page 18 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-8Description:Lab Sample ID:BZ01154-08 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:33Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 11:311,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007171.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007171.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,1-Dichloroethene [75-35-4]0.91 LTS6D06007130.91 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,2,4-Trichlorobenzene [120-82-1]7.1 LTS6D06007247.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,2,4-Trimethylbenzene [95-63-6]1.8 LTS6D06007161.8 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007193.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,2-Dichloroethane [107-06-2]0.78 LTS6D06007130.78 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,3-Butadiene [106-99-0]0.74 LTS6D060077.10.74 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007193.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007193.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:311,4-Dioxane [123-91-1]2.9 LTS6D06007122.9 UD 1.28 ug/m³ Air TO-15 04/07/16 11:312,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.28 ug/m³ Air TO-15 04/07/16 11:312-Butanone [78-93-3]2.5 LTS6D060079.42.5 UD 1.28 ug/m³ Air TO-15 04/07/16 11:312-Hexanone [591-78-6]2.0 LTS6D06007132.0 UD 1.28 ug/m³ Air TO-15 04/07/16 11:312-Propanol [67-63-0]1.8 LTS6D060077.92.5 JD 1.28 ug/m³ Air TO-15 04/07/16 11:313-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.28 ug/m³ Air TO-15 04/07/16 11:314-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.28 ug/m³ Air TO-15 04/07/16 11:314-Methyl-2-pentanone [108-10-1]1.7 LTS6D06007131.7 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Acetone [67-64-1]4.7 LTS6D060077.612D 1.28 ug/m³ Air TO-15 04/07/16 11:31Benzene [71-43-2]0.94 LTS6D06007100.94 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Bromodichloromethane [75-27-4]1.3 LTS6D06007211.3 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Bromoethene [593-60-2]1.2 LTS6D06007141.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Bromoform [75-25-2]2.6 LTS6D06007332.6 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Bromomethane [74-83-9]1.1 LTS6D06007121.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Carbon disulfide [75-15-0]0.92 LTS6D06007100.92 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Chloroethane [75-00-3]0.95 LTS6D060078.40.95 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Chloroform [67-66-3]1.2 LTS6D06007161.6 JD 1.28 ug/m³ Air TO-15 04/07/16 11:31Chloromethane [74-87-3]0.77 LTS6D060076.60.98 JD 1.28 ug/m³ Air TO-15 04/07/16 11:31cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Dibromochloromethane [124-48-1]1.5 LTS6D06007271.5 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.5 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Freon 114 [76-14-2]3.0 LTS6D06007223.0 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Hexachlorobutadiene [87-68-3]7.8 LTS6D06007347.8 UD 1.28 Page 19 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-8Description:Lab Sample ID:BZ01154-08 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:33Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 11:31Methylene chloride [75-09-2]1.3 LTS6D06007111.3 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Methyl-tert-butyl ether [1634-04-4]0.83 LTS6D06007120.83 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31n-Hexane [110-54-3]1.4 LTS6D06007111.4 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Propene [115-07-1]0.75 LTS6D060075.50.75 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Tetrachloroethene [127-18-4]1.6 LTS6D06007221.6 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Tetrahydrofuran [109-99-9]1.1 LTS6D060079.41.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Toluene [108-88-3]0.96 LTS6D06007120.96 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.28 ug/m³ Air TO-15 04/07/16 11:31trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31trans-1,3-Dichloropropene [10061-02-6]0.93 LTS6D06007150.93 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Vinyl chloride [75-01-4]0.98 LTS6D060078.20.98 UD 1.28 ug/m³ Air TO-15 04/07/16 11:31Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.28 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13089 %LTSTO-15 04/07/16 11:316D060072831.2 1 Page 20 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-9Description:Lab Sample ID:BZ01154-09 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:16Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 12:111,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007171.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007171.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,1-Dichloroethene [75-35-4]0.91 LTS6D06007130.91 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,2,4-Trichlorobenzene [120-82-1]7.1 LTS6D06007247.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,2,4-Trimethylbenzene [95-63-6]1.8 LTS6D06007161.8 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,2-Dibromoethane [106-93-4]1.8 LTS6D06007241.8 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,2-Dichlorobenzene [95-50-1]3.1 LTS6D06007193.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,2-Dichloroethane [107-06-2]0.77 LTS6D06007130.77 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,3,5-Trimethylbenzene [108-67-8]1.7 LTS6D06007161.7 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,3-Butadiene [106-99-0]0.73 LTS6D060077.00.73 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007193.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,4-Dichlorobenzene [106-46-7]3.1 LTS6D06007193.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:111,4-Dioxane [123-91-1]2.9 LTS6D06007112.9 UD 1.27 ug/m³ Air TO-15 04/07/16 12:112,2,4-Trimethylpentane [540-84-1]1.5 LTS6D06007151.5 UD 1.27 ug/m³ Air TO-15 04/07/16 12:112-Butanone [78-93-3]2.4 LTS6D060079.42.4 UD 1.27 ug/m³ Air TO-15 04/07/16 12:112-Hexanone [591-78-6]2.0 LTS6D06007132.0 UD 1.27 ug/m³ Air TO-15 04/07/16 12:112-Propanol [67-63-0]1.8 LTS6D060077.81.8 JD 1.27 ug/m³ Air TO-15 04/07/16 12:113-Chloropropene [107-05-1]0.99 LTS6D060079.90.99 UD 1.27 ug/m³ Air TO-15 04/07/16 12:114-Ethyltoluene [622-96-8]1.7 LTS6D06007161.7 UD 1.27 ug/m³ Air TO-15 04/07/16 12:114-Methyl-2-pentanone [108-10-1]1.7 LTS6D06007131.7 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Acetone [67-64-1]4.6 LTS6D060077.511D 1.27 ug/m³ Air TO-15 04/07/16 12:11Benzene [71-43-2]0.93 LTS6D06007100.93 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Benzyl chloride [100-44-7]2.0 LTS6D06007162.0 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Bromodichloromethane [75-27-4]1.3 LTS6D06007211.3 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Bromoethene [593-60-2]1.2 LTS6D06007141.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Bromoform [75-25-2]2.6 LTS6D06007332.6 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Bromomethane [74-83-9]1.1 LTS6D06007121.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Carbon disulfide [75-15-0]0.91 LTS6D060079.90.91 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Chlorobenzene [108-90-7]1.3 LTS6D06007151.3 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Chloroethane [75-00-3]0.94 LTS6D060078.40.94 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Chloromethane [74-87-3]0.76 LTS6D060076.61.1 JD 1.27 ug/m³ Air TO-15 04/07/16 12:11cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007141.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Dibromochloromethane [124-48-1]1.5 LTS6D06007271.5 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.5 JD 1.27 ug/m³ Air TO-15 04/07/16 12:11Ethyl Acetate [141-78-6]1.1 LTS6D06007111.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Freon 113 [76-13-1]2.2 LTS6D06007242.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Freon 114 [76-14-2]3.0 LTS6D06007223.0 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Hexachlorobutadiene [87-68-3]7.7 LTS6D06007347.7 UD 1.27 Page 21 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-9Description:Lab Sample ID:BZ01154-09 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:16Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 12:11Methylene chloride [75-09-2]1.3 LTS6D06007111.3 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Methyl-tert-butyl ether [1634-04-4]0.82 LTS6D06007110.82 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11n-Hexane [110-54-3]1.4 LTS6D06007111.4 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Propene [115-07-1]0.74 LTS6D060075.50.74 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Styrene [100-42-5]1.2 LTS6D06007141.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Tetrachloroethene [127-18-4]1.6 LTS6D06007221.6 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Tetrahydrofuran [109-99-9]1.0 LTS6D060079.41.0 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Toluene [108-88-3]0.96 LTS6D06007120.96 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.27 ug/m³ Air TO-15 04/07/16 12:11trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11trans-1,3-Dichloropropene [10061-02-6]0.92 LTS6D06007140.92 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Vinyl chloride [75-01-4]0.97 LTS6D060078.10.97 UD 1.27 ug/m³ Air TO-15 04/07/16 12:11Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.27 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13092 %LTSTO-15 04/07/16 12:116D060072931.2 1 Page 22 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-10Description:Lab Sample ID:BZ01154-10 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:18Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 12:521,1,1-Trichloroethane [71-55-6]1.1 LTS6D06007171.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,1,2,2-Tetrachloroethane [79-34-5]2.2 LTS6D06007222.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,1,2-Trichloroethane [79-00-5]1.1 LTS6D06007171.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,1-Dichloroethene [75-35-4]0.91 LTS6D06007130.91 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,2,4-Trichlorobenzene [120-82-1]7.1 LTS6D06007247.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,2,4-Trimethylbenzene [95-63-6]1.8 LTS6D06007161.8 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,2-Dichlorobenzene [95-50-1]3.2 LTS6D06007193.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,2-Dichloroethane [107-06-2]0.78 LTS6D06007130.78 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,3-Butadiene [106-99-0]0.74 LTS6D060077.10.74 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,3-Dichlorobenzene [541-73-1]3.1 LTS6D06007193.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,4-Dichlorobenzene [106-46-7]3.2 LTS6D06007193.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:521,4-Dioxane [123-91-1]2.9 LTS6D06007122.9 UD 1.28 ug/m³ Air TO-15 04/07/16 12:522,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.28 ug/m³ Air TO-15 04/07/16 12:522-Butanone [78-93-3]2.5 LTS6D060079.42.6 JD 1.28 ug/m³ Air TO-15 04/07/16 12:522-Hexanone [591-78-6]2.0 LTS6D06007132.0 UD 1.28 ug/m³ Air TO-15 04/07/16 12:522-Propanol [67-63-0]1.8 LTS6D060077.92.6 JD 1.28 ug/m³ Air TO-15 04/07/16 12:523-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.28 ug/m³ Air TO-15 04/07/16 12:524-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.28 ug/m³ Air TO-15 04/07/16 12:524-Methyl-2-pentanone [108-10-1]1.7 LTS6D06007131.7 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Acetone [67-64-1]4.7 LTS6D060077.612D 1.28 ug/m³ Air TO-15 04/07/16 12:52Benzene [71-43-2]0.94 LTS6D06007100.94 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Bromodichloromethane [75-27-4]1.3 LTS6D06007211.3 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Bromoethene [593-60-2]1.2 LTS6D06007141.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Bromoform [75-25-2]2.6 LTS6D06007332.6 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Bromomethane [74-83-9]1.1 LTS6D06007121.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Carbon disulfide [75-15-0]0.92 LTS6D06007100.92 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Carbon tetrachloride [56-23-5]1.4 LTS6D06007201.4 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Chloroethane [75-00-3]0.95 LTS6D060078.40.95 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Chloroform [67-66-3]1.2 LTS6D06007161.6 JD 1.28 ug/m³ Air TO-15 04/07/16 12:52Chloromethane [74-87-3]0.77 LTS6D060076.61.2 JD 1.28 ug/m³ Air TO-15 04/07/16 12:52cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Dibromochloromethane [124-48-1]1.5 LTS6D06007271.5 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Dichlorodifluoromethane [75-71-8]1.5 LTS6D06007161.5 JD 1.28 ug/m³ Air TO-15 04/07/16 12:52Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Freon 114 [76-14-2]3.0 LTS6D06007223.0 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Heptane [142-82-5]1.5 LTS6D06007131.5 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Hexachlorobutadiene [87-68-3]7.8 LTS6D06007347.8 UD 1.28 Page 23 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-10Description:Lab Sample ID:BZ01154-10 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:18Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 12:52Methylene chloride [75-09-2]1.3 LTS6D06007111.3 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Methyl-tert-butyl ether [1634-04-4]0.83 LTS6D06007120.83 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52n-Hexane [110-54-3]1.4 LTS6D06007111.4 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Propene [115-07-1]0.75 LTS6D060075.50.75 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Tetrachloroethene [127-18-4]1.6 LTS6D06007221.6 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Tetrahydrofuran [109-99-9]1.1 LTS6D060079.41.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Toluene [108-88-3]0.96 LTS6D06007120.96 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.28 ug/m³ Air TO-15 04/07/16 12:52trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52trans-1,3-Dichloropropene [10061-02-6]0.93 LTS6D06007150.93 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Trichloroethene [79-01-6]1.6 LTS6D06007171.6 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Trichlorofluoromethane [75-69-4]1.2 LTS6D06007181.2 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Vinyl acetate [108-05-4]1.1 LTS6D06007111.1 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Vinyl chloride [75-01-4]0.98 LTS6D060078.20.98 UD 1.28 ug/m³ Air TO-15 04/07/16 12:52Xylenes (Total) [1330-20-7]2.5 LTS6D06007142.5 UD 1.28 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13086 %LTSTO-15 04/07/16 12:526D060072731.2 1 Page 24 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-11Description:Lab Sample ID:BZ01154-11 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:06Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 13:321,1,1-Trichloroethane [71-55-6]1.2 LTS6D06007181.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,1,2,2-Tetrachloroethane [79-34-5]2.3 LTS6D06007232.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,1,2-Trichloroethane [79-00-5]1.2 LTS6D06007181.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,1-Dichloroethane [75-34-3]1.1 LTS6D06007131.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,1-Dichloroethene [75-35-4]0.94 LTS6D06007130.94 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,2,4-Trichlorobenzene [120-82-1]7.3 LTS6D06007247.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,2,4-Trimethylbenzene [95-63-6]1.9 LTS6D06007161.9 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,2-Dibromoethane [106-93-4]1.8 LTS6D06007251.8 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,2-Dichlorobenzene [95-50-1]3.3 LTS6D06007203.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,2-Dichloroethane [107-06-2]0.80 LTS6D06007130.80 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,2-Dichloropropane [78-87-5]1.3 LTS6D06007151.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,3,5-Trimethylbenzene [108-67-8]1.8 LTS6D06007161.8 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,3-Butadiene [106-99-0]0.76 LTS6D060077.30.76 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,3-Dichlorobenzene [541-73-1]3.2 LTS6D06007203.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,4-Dichlorobenzene [106-46-7]3.3 LTS6D06007203.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:321,4-Dioxane [123-91-1]3.0 LTS6D06007123.0 UD 1.32 ug/m³ Air TO-15 04/07/16 13:322,2,4-Trimethylpentane [540-84-1]1.6 LTS6D06007151.6 UD 1.32 ug/m³ Air TO-15 04/07/16 13:322-Butanone [78-93-3]2.5 LTS6D060079.72.5 UD 1.32 ug/m³ Air TO-15 04/07/16 13:322-Hexanone [591-78-6]2.1 LTS6D06007142.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:322-Propanol [67-63-0]1.9 LTS6D060078.11.9 UD 1.32 ug/m³ Air TO-15 04/07/16 13:323-Chloropropene [107-05-1]1.0 LTS6D06007101.0 UD 1.32 ug/m³ Air TO-15 04/07/16 13:324-Ethyltoluene [622-96-8]1.8 LTS6D06007161.8 UD 1.32 ug/m³ Air TO-15 04/07/16 13:324-Methyl-2-pentanone [108-10-1]1.8 LTS6D06007141.8 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Acetone [67-64-1]4.8 LTS6D060077.86.7 JD 1.32 ug/m³ Air TO-15 04/07/16 13:32Benzene [71-43-2]0.97 LTS6D06007110.97 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Benzyl chloride [100-44-7]2.1 LTS6D06007172.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Bromodichloromethane [75-27-4]1.3 LTS6D06007221.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Bromoethene [593-60-2]1.3 LTS6D06007141.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Bromoform [75-25-2]2.7 LTS6D06007342.7 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Bromomethane [74-83-9]1.1 LTS6D06007131.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Carbon disulfide [75-15-0]0.95 LTS6D06007100.95 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Carbon tetrachloride [56-23-5]1.4 LTS6D06007211.4 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Chlorobenzene [108-90-7]1.4 LTS6D06007151.4 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Chloroethane [75-00-3]0.98 LTS6D060078.70.98 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Chloroform [67-66-3]1.2 LTS6D06007161.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Chloromethane [74-87-3]0.79 LTS6D060076.81.1 JD 1.32 ug/m³ Air TO-15 04/07/16 13:32cis-1,2-Dichloroethene [156-59-2]1.2 LTS6D06007131.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32cis-1,3-Dichloropropene [10061-01-5]1.2 LTS6D06007151.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Cyclohexane [110-82-7]1.2 LTS6D06007111.2 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Dibromochloromethane [124-48-1]1.6 LTS6D06007281.6 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Dichlorodifluoromethane [75-71-8]1.6 LTS6D06007161.6 JD 1.32 ug/m³ Air TO-15 04/07/16 13:32Ethyl Acetate [141-78-6]1.1 LTS6D06007121.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Ethylbenzene [100-41-4]1.3 LTS6D06007141.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Freon 113 [76-13-1]2.3 LTS6D06007252.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Freon 114 [76-14-2]3.1 LTS6D06007233.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Heptane [142-82-5]1.5 LTS6D06007141.5 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Hexachlorobutadiene [87-68-3]8.0 LTS6D06007358.0 UD 1.32 Page 25 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com ANALYTICAL RESULTS IA-11Description:Lab Sample ID:BZ01154-11 04/05/16 10:00Received: BZ01154Work Order:04/01/16 16:06Sampled:AirMatrix: % Solids:Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/m³ Air TO-15 04/07/16 13:32Methylene chloride [75-09-2]1.4 LTS6D06007111.4 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Methyl-tert-butyl ether [1634-04-4]0.86 LTS6D06007120.86 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32n-Hexane [110-54-3]1.5 LTS6D06007121.5 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Propene [115-07-1]0.77 LTS6D060075.70.77 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Styrene [100-42-5]1.3 LTS6D06007141.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Tetrachloroethene [127-18-4]1.7 LTS6D06007221.7 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Tetrahydrofuran [109-99-9]1.1 LTS6D060079.71.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Toluene [108-88-3]0.99 LTS6D06007120.99 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Total Light Petroleum Hydrocarbons 1200 LTS6D0600712001200UD 1.32 ug/m³ Air TO-15 04/07/16 13:32trans-1,2-Dichloroethene [156-60-5]1.1 LTS6D06007131.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32trans-1,3-Dichloropropene [10061-02-6]0.96 LTS6D06007150.96 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Trichloroethene [79-01-6]1.6 LTS6D06007181.6 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Trichlorofluoromethane [75-69-4]1.3 LTS6D06007191.3 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Vinyl acetate [108-05-4]1.1 LTS6D06007121.1 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Vinyl chloride [75-01-4]1.0 LTS6D060078.41.0 UD 1.32 ug/m³ Air TO-15 04/07/16 13:32Xylenes (Total) [1330-20-7]2.6 LTS6D06007142.6 UD 1.32 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 64-13086 %LTSTO-15 04/07/16 13:326D060072731.2 1 Page 26 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06007 - Same Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 16:07Blank (6D06007-BLK1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air140.87 U 1,1,1-Trichloroethane ug/m³ Air171.7 U 1,1,2,2-Tetrachloroethane ug/m³ Air140.87 U 1,1,2-Trichloroethane ug/m³ Air100.85 U 1,1-Dichloroethane ug/m³ Air9.90.71 U 1,1-Dichloroethene ug/m³ Air195.6 U 1,2,4-Trichlorobenzene ug/m³ Air121.4 U 1,2,4-Trimethylbenzene ug/m³ Air191.4 U 1,2-Dibromoethane ug/m³ Air152.5 U 1,2-Dichlorobenzene ug/m³ Air100.61 U 1,2-Dichloroethane ug/m³ Air121.0 U 1,2-Dichloropropane ug/m³ Air121.4 U 1,3,5-Trimethylbenzene ug/m³ Air5.50.58 U 1,3-Butadiene ug/m³ Air152.4 U 1,3-Dichlorobenzene ug/m³ Air152.5 U 1,4-Dichlorobenzene ug/m³ Air9.02.3 U 1,4-Dioxane ug/m³ Air121.2 U 2,2,4-Trimethylpentane ug/m³ Air7.41.9 U 2-Butanone ug/m³ Air101.6 U 2-Hexanone ug/m³ Air6.11.4 U 2-Propanol ug/m³ Air7.80.78 U 3-Chloropropene ug/m³ Air121.4 U 4-Ethyltoluene ug/m³ Air101.4 U 4-Methyl-2-pentanone ug/m³ Air5.93.7 U Acetone ug/m³ Air8.00.73 U Benzene ug/m³ Air131.6 U Benzyl chloride ug/m³ Air171.0 U Bromodichloromethane ug/m³ Air110.96 U Bromoethene ug/m³ Air262.1 U Bromoform ug/m³ Air9.70.85 U Bromomethane ug/m³ Air7.80.72 U Carbon disulfide ug/m³ Air161.1 U Carbon tetrachloride ug/m³ Air121.1 U Chlorobenzene ug/m³ Air6.60.74 U Chloroethane ug/m³ Air120.93 U Chloroform ug/m³ Air5.20.60 U Chloromethane ug/m³ Air9.90.91 U cis-1,2-Dichloroethene ug/m³ Air110.91 U cis-1,3-Dichloropropene ug/m³ Air8.60.93 U Cyclohexane ug/m³ Air211.2 U Dibromochloromethane ug/m³ Air121.2 U Dichlorodifluoromethane ug/m³ Air9.00.86 U Ethyl Acetate ug/m³ Air111.0 U Ethylbenzene ug/m³ Air191.8 U Freon 113 ug/m³ Air172.4 U Freon 114 ug/m³ Air101.1 U Heptane ug/m³ Air276.1 U Hexachlorobutadiene ug/m³ Air8.71.0 U Methylene chloride ug/m³ Air9.00.65 U Methyl-tert-butyl ether Page 27 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06007 - Same - Continued Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 16:07Blank (6D06007-BLK1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air8.81.1 U n-Hexane ug/m³ Air4.30.59 U Propene ug/m³ Air110.98 U Styrene ug/m³ Air171.3 U Tetrachloroethene ug/m³ Air7.40.83 U Tetrahydrofuran ug/m³ Air9.40.75 U Toluene ug/m³ Air920920U Total Light Petroleum Hydrocarbons ug/m³ Air9.90.83 U trans-1,2-Dichloroethene ug/m³ Air110.73 U trans-1,3-Dichloropropene ug/m³ Air131.2 U Trichloroethene ug/m³ Air140.96 U Trichlorofluoromethane ug/m³ Air8.80.85 U Vinyl acetate ug/m³ Air6.40.77 U Vinyl chloride ug/m³ Air112.0 U Xylenes (Total) ppbv 31.2 64-1304-Bromofluorobenzene 9329 Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 15:28LCS (6D06007-BS1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air14 54.6 69-1308949 1,1,1-Trichloroethane ug/m³ Air17 68.7 70-13710572 1,1,2,2-Tetrachloroethane ug/m³ Air14 54.6 70-13610457 1,1,2-Trichloroethane ug/m³ Air10 40.5 70-1309639 1,1-Dichloroethane ug/m³ Air9.9 39.7 70-1309236 1,1-Dichloroethene ug/m³ Air19 74.2 14-1879973 1,2,4-Trichlorobenzene ug/m³ Air12 49.2 70-14610552 1,2,4-Trimethylbenzene ug/m³ Air19 76.8 70-13010682 1,2-Dibromoethane ug/m³ Air15 60.1 52-1609759 1,2-Dichlorobenzene ug/m³ Air10 40.5 56-1338635 1,2-Dichloroethane ug/m³ Air12 46.2 70-13710046 1,2-Dichloropropane ug/m³ Air12 49.2 70-14110250 1,3,5-Trimethylbenzene ug/m³ Air5.5 22.1 56-1457717 1,3-Butadiene ug/m³ Air15 60.1 57-1559255 1,3-Dichlorobenzene ug/m³ Air15 60.1 52-1639758 1,4-Dichlorobenzene ug/m³ Air9.0 36.0 34-16410638 1,4-Dioxane ug/m³ Air12 46.7 70-1489846 2,2,4-Trimethylpentane ug/m³ Air7.4 29.5 52-1469428 2-Butanone ug/m³ Air10 41.0 54-14311045 2-Hexanone ug/m³ Air6.1 24.6 10-1839323 2-Propanol ug/m³ Air7.8 31.3 52-1399329 3-Chloropropene ug/m³ Air12 49.2 70-14410451 4-Ethyltoluene ug/m³ Air10 41.0 61-14010543 4-Methyl-2-pentanone ug/m³ Air5.9 23.8 47-1468220 Acetone ug/m³ Air8.0 32.0 68-14910032 Benzene ug/m³ Air13 51.8 57-14910655 Benzyl chloride ug/m³ Air17 67.0 70-1309362 Bromodichloromethane ug/m³ Air11 43.7 70-1369140 Bromoethene ug/m³ Air26 103 70-135105110 Bromoform ug/m³ Air9.7 38.8 70-1337931 Bromomethane Page 28 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06007 - Same - Continued Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 15:28LCS (6D06007-BS1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air7.8 31.1 61-1559730 Carbon disulfide ug/m³ Air16 62.9 60-1328855 Carbon tetrachloride ug/m³ Air12 46.0 70-13910347 Chlorobenzene ug/m³ Air6.6 26.4 70-1358823 Chloroethane ug/m³ Air12 48.8 70-1309345 Chloroform ug/m³ Air5.2 20.7 70-1408618 Chloromethane ug/m³ Air9.9 39.6 70-14510341 cis-1,2-Dichloroethene ug/m³ Air11 45.4 70-13110447 cis-1,3-Dichloropropene ug/m³ Air8.6 34.4 70-1419834 Cyclohexane ug/m³ Air21 85.2 60-1419984 Dibromochloromethane ug/m³ Air12 49.5 42-1597437 Dichlorodifluoromethane ug/m³ Air9.0 36.0 57-1449534 Ethyl Acetate ug/m³ Air11 43.4 70-14410043 Ethylbenzene ug/m³ Air19 76.6 70-1339472 Freon 113 ug/m³ Air17 69.9 47-1647653 Freon 114 ug/m³ Air10 41.0 51-1569439 Heptane ug/m³ Air27 107 58-1578995 Hexachlorobutadiene ug/m³ Air8.7 34.7 70-1488128 Methylene chloride ug/m³ Air9.0 36.1 70-1309635 Methyl-tert-butyl ether ug/m³ Air8.8 35.2 68-1439032 n-Hexane ug/m³ Air4.3 17.2 62-1438515 Propene ug/m³ Air11 42.6 70-14311348 Styrene ug/m³ Air17 67.8 70-14210470 Tetrachloroethene ug/m³ Air7.4 29.5 52-1529628 Tetrahydrofuran ug/m³ Air9.4 37.7 70-14410640 Toluene ug/m³ Air9.9 39.6 70-1309738 trans-1,2-Dichloroethene ug/m³ Air11 45.4 70-13010548 trans-1,3-Dichloropropene ug/m³ Air13 53.7 70-1319953 Trichloroethene ug/m³ Air14 56.2 53-1358447 Trichlorofluoromethane ug/m³ Air8.8 35.2 62-14210035 Vinyl acetate ug/m³ Air6.4 25.6 70-1378622 Vinyl chloride ppbv 31.2 64-1304-Bromofluorobenzene 8928 Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 23:15Matrix Spike (6D06007-MS1) Source: BZ01154-11 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air720 2880 69-13010246 U2900 1,1,1-Trichloroethane ug/m³ Air910 3620 70-13710291 U3700 1,1,2,2-Tetrachloroethane ug/m³ Air720 2880 70-1369646 U2800 1,1,2-Trichloroethane ug/m³ Air530 2140 70-1309245 U2000 1,1-Dichloroethane ug/m³ Air520 2090 70-1309638 U2000 1,1-Dichloroethene ug/m³ Air980 3920 14-187109290 U4300 1,2,4-Trichlorobenzene ug/m³ Air650 2590 70-14612175 U3100 1,2,4-Trimethylbenzene ug/m³ Air1000 4060 70-13010373 U4200 1,2-Dibromoethane ug/m³ Air790 3170 52-160107130 U3400 1,2-Dichlorobenzene ug/m³ Air530 2140 56-13310032 U2100 1,2-Dichloroethane ug/m³ Air610 2440 70-1378554 U2100 1,2-Dichloropropane ug/m³ Air650 2590 70-14112073 U3100 1,3,5-Trimethylbenzene ug/m³ Air290 1170 56-1459530 U1100 1,3-Butadiene Page 29 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06007 - Same - Continued Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 23:15Matrix Spike (6D06007-MS1) Continued Source: BZ01154-11 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air790 3170 57-155104130 U3300 1,3-Dichlorobenzene ug/m³ Air790 3170 52-163109130 U3500 1,4-Dichlorobenzene ug/m³ Air480 1900 34-16490120 U1700 1,4-Dioxane ug/m³ Air620 2470 70-1489164 U2200 2,2,4-Trimethylpentane ug/m³ Air390 1560 52-14689100 U1400 2-Butanone ug/m³ Air540 2160 54-14310084 U2200 2-Hexanone ug/m³ Air320 1300 10-1838775 U1100 2-Propanol ug/m³ Air410 1650 52-1398941 U1500 3-Chloropropene ug/m³ Air650 2590 70-14412173 U3100 4-Ethyltoluene ug/m³ Air540 2160 61-1409271 U2000 4-Methyl-2-pentanone ug/m³ Air310 1250 47-14685190 U1100 Acetone ug/m³ Air420 1690 68-1499339 U1600 Benzene ug/m³ Air680 2730 57-14911385 U3100 Benzyl chloride ug/m³ Air880 3540 70-1309453 U3300 Bromodichloromethane ug/m³ Air580 2310 70-13610751 U2500 Bromoethene ug/m³ Air1400 5450 70-135105110 U5700 Bromoform ug/m³ Air510 2050 70-13310345 U2100 Bromomethane ug/m³ Air410 1640 61-1559738 U1600 Carbon disulfide ug/m³ Air830 3320 60-13210456 U3500 Carbon tetrachloride ug/m³ Air610 2430 70-1399656 U2300 Chlorobenzene ug/m³ Air350 1390 70-1359639 U1300 Chloroethane ug/m³ Air640 2580 70-1309949 U2500 Chloroform ug/m³ Air270 1090 70-1409932 U1100 Chloromethane ug/m³ Air520 2090 70-1459648 U2000 cis-1,2-Dichloroethene ug/m³ Air600 2400 70-1319448 U2200 cis-1,3-Dichloropropene ug/m³ Air450 1820 70-1418849 U1600 Cyclohexane ug/m³ Air1100 4500 60-14110063 U4500 Dibromochloromethane ug/m³ Air650 2610 42-15911063 U2900 Dichlorodifluoromethane ug/m³ Air480 1900 57-1448746 U1700 Ethyl Acetate ug/m³ Air570 2290 70-1449853 U2200 Ethylbenzene ug/m³ Air1000 4040 70-1339793 U3900 Freon 113 ug/m³ Air920 3690 47-164108130 U4000 Freon 114 ug/m³ Air540 2160 51-1568761 U1900 Heptane ug/m³ Air1400 5630 58-15796320 U5400 Hexachlorobutadiene ug/m³ Air460 1830 70-1487855 U1400 Methylene chloride ug/m³ Air480 1900 70-1309334 U1800 Methyl-tert-butyl ether ug/m³ Air460 1860 68-1438160 U1500 n-Hexane ug/m³ Air230 908 62-1439231 U840 Propene ug/m³ Air560 2250 70-14310552 U2400 Styrene ug/m³ Air890 3580 70-1429368 U3300 Tetrachloroethene ug/m³ Air390 1560 52-1528544 U1300 Tetrahydrofuran ug/m³ Air500 1990 70-1449440 U1900 Toluene ug/m³ Air520 2090 70-1309744 U2000 trans-1,2-Dichloroethene ug/m³ Air600 2400 70-13010238 U2400 trans-1,3-Dichloropropene ug/m³ Air710 2830 70-1319665 U2700 Trichloroethene ug/m³ Air740 2970 53-13510550 U3100 Trichlorofluoromethane ug/m³ Air460 1860 62-1429245 U1700 Vinyl acetate ug/m³ Air340 1350 70-13710240 U1400 Vinyl chloride ppbv 31.2 64-1304-Bromofluorobenzene 10332 Page 30 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06007 - Same - Continued Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 23:52Matrix Spike Dup (6D06007-MSD1) Source: BZ01154-11 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air720 2880 2569-13098 446 U2800 1,1,1-Trichloroethane ug/m³ Air910 3620 3670-137122 1891 U4400 1,1,2,2-Tetrachloroethane ug/m³ Air720 2880 2270-136102 646 U2900 1,1,2-Trichloroethane ug/m³ Air530 2140 2770-13095 345 U2000 1,1-Dichloroethane ug/m³ Air520 2090 2070-13094 238 U2000 1,1-Dichloroethene ug/m³ Air980 3920 5914-187104 5290 U4100 1,2,4-Trichlorobenzene ug/m³ Air650 2590 4270-146118 275 U3100 1,2,4-Trimethylbenzene ug/m³ Air1000 4060 2070-130107 473 U4300 1,2-Dibromoethane ug/m³ Air790 3170 5052-160100 7130 U3200 1,2-Dichlorobenzene ug/m³ Air530 2140 2956-13396 432 U2000 1,2-Dichloroethane ug/m³ Air610 2440 1970-13792 854 U2200 1,2-Dichloropropane ug/m³ Air650 2590 3670-141118 273 U3100 1,3,5-Trimethylbenzene ug/m³ Air290 1170 5956-14581 1630 U950 1,3-Butadiene ug/m³ Air790 3170 4457-15597 7130 U3100 1,3-Dichlorobenzene ug/m³ Air790 3170 4752-163103 6130 U3300 1,4-Dichlorobenzene ug/m³ Air480 1900 4934-16497 8120 U1800 1,4-Dioxane ug/m³ Air620 2470 2970-14894 364 U2300 2,2,4-Trimethylpentane ug/m³ Air390 1560 4352-14691 2100 U1400 2-Butanone ug/m³ Air540 2160 4854-143105 584 U2300 2-Hexanone ug/m³ Air320 1300 5610-18391 475 U1200 2-Propanol ug/m³ Air410 1650 2952-13991 341 U1500 3-Chloropropene ug/m³ Air650 2590 3370-144119 273 U3100 4-Ethyltoluene ug/m³ Air540 2160 3761-14096 471 U2100 4-Methyl-2-pentanone ug/m³ Air310 1250 7647-14685 0.5190 U1100 Acetone ug/m³ Air420 1690 2668-14996 439 U1600 Benzene ug/m³ Air680 2730 5657-149105 785 U2900 Benzyl chloride ug/m³ Air880 3540 1670-13095 153 U3400 Bromodichloromethane ug/m³ Air580 2310 1770-136102 551 U2400 Bromoethene ug/m³ Air1400 5450 2070-135105 0.3110 U5700 Bromoform ug/m³ Air510 2050 2170-13392 1245 U1900 Bromomethane ug/m³ Air410 1640 4161-15597 0.00938 U1600 Carbon disulfide ug/m³ Air830 3320 2560-13298 656 U3300 Carbon tetrachloride ug/m³ Air610 2430 1170-13999 356 U2400 Chlorobenzene ug/m³ Air350 1390 2070-13596 0.139 U1300 Chloroethane ug/m³ Air640 2580 2170-13097 249 U2500 Chloroform ug/m³ Air270 1090 2770-14092 832 U1000 Chloromethane ug/m³ Air520 2090 2070-145101 548 U2100 cis-1,2-Dichloroethene ug/m³ Air600 2400 1870-13197 448 U2300 cis-1,3-Dichloropropene ug/m³ Air450 1820 6370-14191 349 U1700 Cyclohexane ug/m³ Air1100 4500 2160-141104 463 U4700 Dibromochloromethane ug/m³ Air650 2610 3242-15981 3063 U2100 Dichlorodifluoromethane ug/m³ Air480 1900 5657-14489 246 U1700 Ethyl Acetate ug/m³ Air570 2290 1070-14499 153 U2300 Ethylbenzene ug/m³ Air1000 4040 1670-13398 0.993 U3900 Freon 113 ug/m³ Air920 3690 4247-16486 23130 U3200 Freon 114 ug/m³ Air540 2160 5951-15689 261 U1900 Heptane ug/m³ Air1400 5630 5358-15791 5320 U5100 Hexachlorobutadiene ug/m³ Air460 1830 7170-14881 455 U1500 Methylene chloride ug/m³ Air480 1900 2070-13098 534 U1900 Methyl-tert-butyl ether Page 31 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06007 - Same - Continued Prepared: 04/06/2016 15:13 Analyzed: 04/06/2016 23:52Matrix Spike Dup (6D06007-MSD1) Continued Source: BZ01154-11 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air460 1860 3168-14384 460 U1600 n-Hexane ug/m³ Air230 908 4062-14387 631 U790 Propene ug/m³ Air560 2250 1970-143108 352 U2400 Styrene ug/m³ Air890 3580 2770-14299 668 U3600 Tetrachloroethene ug/m³ Air390 1560 2852-15289 444 U1400 Tetrahydrofuran ug/m³ Air500 1990 2470-144100 740 U2000 Toluene ug/m³ Air520 2090 1970-13097 0.844 U2000 trans-1,2-Dichloroethene ug/m³ Air600 2400 2170-130105 338 U2500 trans-1,3-Dichloropropene ug/m³ Air710 2830 2870-13198 265 U2800 Trichloroethene ug/m³ Air740 2970 3553-13594 1150 U2800 Trichlorofluoromethane ug/m³ Air460 1860 2262-14296 545 U1800 Vinyl acetate ug/m³ Air340 1350 2670-13793 940 U1300 Vinyl chloride ppbv 31.2 64-1304-Bromofluorobenzene 10432 Batch 6D12006 - Same Prepared & Analyzed: 04/11/2016 18:48Blank (6D12006-BLK1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air140.87 U 1,1,1-Trichloroethane ug/m³ Air171.7 U 1,1,2,2-Tetrachloroethane ug/m³ Air140.87 U 1,1,2-Trichloroethane ug/m³ Air100.85 U 1,1-Dichloroethane ug/m³ Air9.90.71 U 1,1-Dichloroethene ug/m³ Air195.6 U 1,2,4-Trichlorobenzene ug/m³ Air121.4 U 1,2,4-Trimethylbenzene ug/m³ Air191.4 U 1,2-Dibromoethane ug/m³ Air152.5 U 1,2-Dichlorobenzene ug/m³ Air100.61 U 1,2-Dichloroethane ug/m³ Air121.0 U 1,2-Dichloropropane ug/m³ Air121.4 U 1,3,5-Trimethylbenzene ug/m³ Air5.50.58 U 1,3-Butadiene ug/m³ Air152.4 U 1,3-Dichlorobenzene ug/m³ Air152.5 U 1,4-Dichlorobenzene ug/m³ Air9.02.3 U 1,4-Dioxane ug/m³ Air121.2 U 2,2,4-Trimethylpentane ug/m³ Air7.41.9 U 2-Butanone ug/m³ Air101.6 U 2-Hexanone ug/m³ Air6.11.4 U 2-Propanol ug/m³ Air7.80.78 U 3-Chloropropene ug/m³ Air121.4 U 4-Ethyltoluene ug/m³ Air101.4 U 4-Methyl-2-pentanone ug/m³ Air5.93.7 U Acetone ug/m³ Air8.00.73 U Benzene ug/m³ Air131.6 U Benzyl chloride ug/m³ Air171.0 U Bromodichloromethane ug/m³ Air110.96 U Bromoethene ug/m³ Air262.1 U Bromoform ug/m³ Air9.70.85 U Bromomethane Page 32 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D12006 - Same - Continued Prepared & Analyzed: 04/11/2016 18:48Blank (6D12006-BLK1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air7.80.72 U Carbon disulfide ug/m³ Air161.1 U Carbon tetrachloride ug/m³ Air121.1 U Chlorobenzene ug/m³ Air6.60.74 U Chloroethane ug/m³ Air120.93 U Chloroform ug/m³ Air5.20.60 U Chloromethane ug/m³ Air9.90.91 U cis-1,2-Dichloroethene ug/m³ Air110.91 U cis-1,3-Dichloropropene ug/m³ Air8.60.93 U Cyclohexane ug/m³ Air211.2 U Dibromochloromethane ug/m³ Air121.2 U Dichlorodifluoromethane ug/m³ Air9.00.86 U Ethyl Acetate ug/m³ Air111.0 U Ethylbenzene ug/m³ Air191.8 U Freon 113 ug/m³ Air172.4 U Freon 114 ug/m³ Air101.1 U Heptane ug/m³ Air276.1 U Hexachlorobutadiene ug/m³ Air8.71.0 U Methylene chloride ug/m³ Air9.00.65 U Methyl-tert-butyl ether ug/m³ Air8.81.1 U n-Hexane ug/m³ Air4.30.59 U Propene ug/m³ Air110.98 U Styrene ug/m³ Air171.3 U Tetrachloroethene ug/m³ Air7.40.83 U Tetrahydrofuran ug/m³ Air9.40.75 U Toluene ug/m³ Air920920U Total Light Petroleum Hydrocarbons ug/m³ Air9.90.83 U trans-1,2-Dichloroethene ug/m³ Air110.73 U trans-1,3-Dichloropropene ug/m³ Air131.2 U Trichloroethene ug/m³ Air140.96 U Trichlorofluoromethane ug/m³ Air8.80.85 U Vinyl acetate ug/m³ Air6.40.77 U Vinyl chloride ug/m³ Air112.0 U Xylenes (Total) ppbv 31.2 64-1304-Bromofluorobenzene 9128 Prepared & Analyzed: 04/12/2016 01:15LCS (6D12006-BS1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air14 54.6 69-13010256 1,1,1-Trichloroethane ug/m³ Air17 68.7 70-13711680 1,1,2,2-Tetrachloroethane ug/m³ Air14 54.6 70-13611261 1,1,2-Trichloroethane ug/m³ Air10 40.5 70-13010844 1,1-Dichloroethane ug/m³ Air9.9 39.7 70-13010843 1,1-Dichloroethene ug/m³ Air19 74.2 14-187157120 1,2,4-Trichlorobenzene ug/m³ Air12 49.2 70-14612260 1,2,4-Trimethylbenzene ug/m³ Air19 76.8 70-13011387 1,2-Dibromoethane ug/m³ Air15 60.1 52-16012173 1,2-Dichlorobenzene ug/m³ Air10 40.5 56-13310643 1,2-Dichloroethane ug/m³ Air12 46.2 70-13711051 1,2-Dichloropropane Page 33 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D12006 - Same - Continued Prepared & Analyzed: 04/12/2016 01:15LCS (6D12006-BS1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air12 49.2 70-14111758 1,3,5-Trimethylbenzene ug/m³ Air5.5 22.1 56-14510824 1,3-Butadiene ug/m³ Air15 60.1 57-15511368 1,3-Dichlorobenzene ug/m³ Air15 60.1 52-16311972 1,4-Dichlorobenzene ug/m³ Air9.0 36.0 34-16410939 1,4-Dioxane ug/m³ Air12 46.7 70-14811152 2,2,4-Trimethylpentane ug/m³ Air7.4 29.5 52-14610732 2-Butanone ug/m³ Air10 41.0 54-14312451 2-Hexanone ug/m³ Air6.1 24.6 10-18311729 2-Propanol ug/m³ Air7.8 31.3 52-13910734 3-Chloropropene ug/m³ Air12 49.2 70-14411154 4-Ethyltoluene ug/m³ Air10 41.0 61-14011748 4-Methyl-2-pentanone ug/m³ Air5.9 23.8 47-1469723 Acetone ug/m³ Air8.0 32.0 68-14911136 Benzene ug/m³ Air13 51.8 57-14911861 Benzyl chloride ug/m³ Air17 67.0 70-13010268 Bromodichloromethane ug/m³ Air11 43.7 70-13610445 Bromoethene ug/m³ Air26 103 70-135109110 Bromoform ug/m³ Air9.7 38.8 70-13310039 Bromomethane ug/m³ Air7.8 31.1 61-15510031 Carbon disulfide ug/m³ Air16 62.9 60-13210164 Carbon tetrachloride ug/m³ Air12 46.0 70-13910549 Chlorobenzene ug/m³ Air6.6 26.4 70-13510227 Chloroethane ug/m³ Air12 48.8 70-13010752 Chloroform ug/m³ Air5.2 20.7 70-14011524 Chloromethane ug/m³ Air9.9 39.6 70-14510943 cis-1,2-Dichloroethene ug/m³ Air11 45.4 70-13111351 cis-1,3-Dichloropropene ug/m³ Air8.6 34.4 70-14111038 Cyclohexane ug/m³ Air21 85.2 60-14110488 Dibromochloromethane ug/m³ Air12 49.5 42-15912160 Dichlorodifluoromethane ug/m³ Air9.0 36.0 57-14411040 Ethyl Acetate ug/m³ Air11 43.4 70-14410445 Ethylbenzene ug/m³ Air19 76.6 70-13310379 Freon 113 ug/m³ Air17 69.9 47-16411278 Freon 114 ug/m³ Air10 41.0 51-15611145 Heptane ug/m³ Air27 107 58-157130140 Hexachlorobutadiene ug/m³ Air8.7 34.7 70-14810336 Methylene chloride ug/m³ Air9.0 36.1 70-13010739 Methyl-tert-butyl ether ug/m³ Air8.8 35.2 68-14311340 n-Hexane ug/m³ Air4.3 17.2 62-14311019 Propene ug/m³ Air11 42.6 70-14312051 Styrene ug/m³ Air17 67.8 70-14210269 Tetrachloroethene ug/m³ Air7.4 29.5 52-15210932 Tetrahydrofuran ug/m³ Air9.4 37.7 70-14410841 Toluene ug/m³ Air9.9 39.6 70-13010843 trans-1,2-Dichloroethene ug/m³ Air11 45.4 70-13011854 trans-1,3-Dichloropropene ug/m³ Air13 53.7 70-1319953 Trichloroethene ug/m³ Air14 56.2 53-13510559 Trichlorofluoromethane ug/m³ Air8.8 35.2 62-14211942 Vinyl acetate Page 34 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D12006 - Same - Continued Prepared & Analyzed: 04/12/2016 01:15LCS (6D12006-BS1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air6.4 25.6 70-13711529 Vinyl chloride ppbv 31.2 64-1304-Bromofluorobenzene 9931 Prepared & Analyzed: 04/12/2016 12:51LCS Dup (6D12006-BSD1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air14 54.6 2569-130104 257 1,1,1-Trichloroethane ug/m³ Air17 68.7 3670-137116 0.00880 1,1,2,2-Tetrachloroethane ug/m³ Air14 54.6 2270-136112 0.561 1,1,2-Trichloroethane ug/m³ Air10 40.5 2770-130107 0.343 1,1-Dichloroethane ug/m³ Air9.9 39.7 2070-130109 143 1,1-Dichloroethene ug/m³ Air19 74.2 5914-187152 3110 1,2,4-Trichlorobenzene ug/m³ Air12 49.2 4270-146121 0.560 1,2,4-Trimethylbenzene ug/m³ Air19 76.8 2070-130115 288 1,2-Dibromoethane ug/m³ Air15 60.1 5052-160120 172 1,2-Dichlorobenzene ug/m³ Air10 40.5 2956-133108 144 1,2-Dichloroethane ug/m³ Air12 46.2 1970-137111 151 1,2-Dichloropropane ug/m³ Air12 49.2 3670-141119 158 1,3,5-Trimethylbenzene ug/m³ Air5.5 22.1 5956-145106 223 1,3-Butadiene ug/m³ Air15 60.1 4457-155112 167 1,3-Dichlorobenzene ug/m³ Air15 60.1 4752-163118 171 1,4-Dichlorobenzene ug/m³ Air9.0 36.0 4934-164113 341 1,4-Dioxane ug/m³ Air12 46.7 2970-148112 153 2,2,4-Trimethylpentane ug/m³ Air7.4 29.5 4352-146113 533 2-Butanone ug/m³ Air10 41.0 4854-143128 352 2-Hexanone ug/m³ Air6.1 24.6 5610-183119 129 2-Propanol ug/m³ Air7.8 31.3 2952-139110 335 3-Chloropropene ug/m³ Air12 49.2 3370-144109 254 4-Ethyltoluene ug/m³ Air10 41.0 3761-140119 249 4-Methyl-2-pentanone ug/m³ Air5.9 23.8 7647-146100 324 Acetone ug/m³ Air8.0 32.0 2668-149111 0.136 Benzene ug/m³ Air13 51.8 5657-149115 260 Benzyl chloride ug/m³ Air17 67.0 1670-130105 370 Bromodichloromethane ug/m³ Air11 43.7 1770-136105 0.646 Bromoethene ug/m³ Air26 103 2070-135112 3120 Bromoform ug/m³ Air9.7 38.8 2170-133102 240 Bromomethane ug/m³ Air7.8 31.1 4161-155102 232 Carbon disulfide ug/m³ Air16 62.9 2560-132101 0.563 Carbon tetrachloride ug/m³ Air12 46.0 1170-139107 249 Chlorobenzene ug/m³ Air6.6 26.4 2070-135105 328 Chloroethane ug/m³ Air12 48.8 2170-130107 0.452 Chloroform ug/m³ Air5.2 20.7 2770-140112 223 Chloromethane ug/m³ Air9.9 39.6 2070-145112 344 cis-1,2-Dichloroethene ug/m³ Air11 45.4 1870-131116 253 cis-1,3-Dichloropropene ug/m³ Air8.6 34.4 6370-141111 0.638 Cyclohexane ug/m³ Air21 85.2 2160-141108 492 Dibromochloromethane ug/m³ Air12 49.5 3242-159115 557 Dichlorodifluoromethane ug/m³ Air9.0 36.0 5657-144111 0.140 Ethyl Acetate ug/m³ Air11 43.4 1070-144105 0.645 Ethylbenzene Page 35 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D12006 - Same - Continued Prepared & Analyzed: 04/12/2016 12:51LCS Dup (6D12006-BSD1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/m³ Air19 76.6 1670-133105 280 Freon 113 ug/m³ Air17 69.9 4247-164104 873 Freon 114 ug/m³ Air10 41.0 5951-156113 246 Heptane ug/m³ Air27 107 5358-157130 0.01140 Hexachlorobutadiene ug/m³ Air8.7 34.7 7170-148104 0.836 Methylene chloride ug/m³ Air9.0 36.1 2070-130110 340 Methyl-tert-butyl ether ug/m³ Air8.8 35.2 3168-143114 140 n-Hexane ug/m³ Air4.3 17.2 4062-143110 0.0619 Propene ug/m³ Air11 42.6 1970-143126 554 Styrene ug/m³ Air17 67.8 2770-142104 271 Tetrachloroethene ug/m³ Air7.4 29.5 2852-152112 233 Tetrahydrofuran ug/m³ Air9.4 37.7 2470-144109 141 Toluene ug/m³ Air9.9 39.6 1970-130108 0.143 trans-1,2-Dichloroethene ug/m³ Air11 45.4 2170-130120 255 trans-1,3-Dichloropropene ug/m³ Air13 53.7 2870-131104 456 Trichloroethene ug/m³ Air14 56.2 3553-135103 258 Trichlorofluoromethane ug/m³ Air8.8 35.2 2262-142122 243 Vinyl acetate ug/m³ Air6.4 25.6 2670-137112 229 Vinyl chloride ppbv 31.2 64-1304-Bromofluorobenzene 9730 Page 36 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com FLAGS/NOTES AND DEFINITIONS The analyte was detected in the associated method blank. The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. MRL E U J D B N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a “tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Page 37 of 38This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL 102-A Woodwinds Industrial Court Cary NC, 27511 919.467.3090 919.467.3515Phone:FAX: ENCO Workorder(s): CZ04159 Raleigh, NC 27616 Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Enclosure(s) Project Number: [none], Project Name/Desc: AMI Attn: Kirk Pollard Mineral Springs Environmental (MI017) 4600 Mineral Springs Lane Bill Scott Project Manager Wednesday, April 13, 2016 RE: Laboratory Results for Dear Kirk Pollard, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, April 4, 2016. Enclosure(s) Page 1 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 1 of 26 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE MW-1 CZ04159-01RE1 Sampled:04/01/16 09:21 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/07/16 11:06 04/07/16 15:45 MW-7 CZ04159-02RE1 Sampled:04/01/16 10:30 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/07/16 11:06 04/07/16 15:16 MW-8 CZ04159-03 Sampled:04/01/16 10:15 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/06/16 12:15 04/06/16 21:18 MW-9 CZ04159-04RE1 Sampled:04/01/16 09:45 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/07/16 11:06 04/07/16 16:15 MW-10 CZ04159-05RE1 Sampled:04/01/16 09:30 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/07/16 11:06 04/07/16 16:44 MW-13 CZ04159-06RE1 Sampled:04/01/16 10:00 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/07/16 11:06 04/07/16 17:13 Trip Blank CZ04159-07 Sampled:04/01/16 09:21 Received:04/04/16 09:45Client ID:Lab ID: Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s) EPA 8260B 04/15/16 04/07/16 11:06 04/08/16 14:21 Page 2 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 2 of 26 www.encolabs.com SAMPLE DETECTION SUMMARY Lab ID:Client ID:MW-1 CZ04159-01RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 730 20 ug/L EPA 8260BD cis-1,2-Dichloroethene 3.0 190 20 ug/L EPA 8260BD Tetrachloroethene 3.4 26 20 ug/L EPA 8260BD trans-1,2-Dichloroethene 4.2 860 20 ug/L EPA 8260BD Trichloroethene 3.0 180 20 ug/L EPA 8260BD Vinyl chloride 6.4 Lab ID:Client ID:MW-8 CZ04159-03 Analyte MethodUnitsPQLResultsFlag NotesMDL 3.1 1.0 ug/L EPA 8260B cis-1,2-Dichloroethene 0.15 16 1.0 ug/L EPA 8260B Tetrachloroethene 0.17 3.6 1.0 ug/L EPA 8260B Trichloroethene 0.15 Lab ID:Client ID:MW-9 CZ04159-04RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 41 100 ug/L EPA 8260BJD cis-1,2-Dichloroethene 15 4100 100 ug/L EPA 8260BD Tetrachloroethene 17 260 100 ug/L EPA 8260BD Trichloroethene 15 Lab ID:Client ID:MW-10 CZ04159-05RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 270 100 ug/L EPA 8260BD cis-1,2-Dichloroethene 15 4900 100 ug/L EPA 8260BD Tetrachloroethene 17 2100 100 ug/L EPA 8260BD Trichloroethene 15 Lab ID:Client ID:MW-13 CZ04159-06RE1 Analyte MethodUnitsPQLResultsFlag NotesMDL 650 500 ug/L EPA 8260BD cis-1,2-Dichloroethene 75 21000 500 ug/L EPA 8260BD Tetrachloroethene 85 660 500 ug/L EPA 8260BD Trichloroethene 75 Page 3 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 3 of 26 www.encolabs.com ANALYTICAL RESULTS MW-1Description:Lab Sample ID:CZ04159-01 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:21Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 15:451,1,1,2-Tetrachloroethane [630-20-6]^3.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,1,1-Trichloroethane [71-55-6]^2.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,1,2,2-Tetrachloroethane [79-34-5]^5.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,1,2-Trichloroethane [79-00-5]^2.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,1-Dichloroethane [75-34-3]^2.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,1-Dichloroethene [75-35-4]^4.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,1-Dichloropropene [563-58-6]^3.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2,3-Trichlorobenzene [87-61-6]^0.24 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2,3-Trichloropropane [96-18-4]^4.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2,4-Trichlorobenzene [120-82-1]^2.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2,4-Trimethylbenzene [95-63-6]^2.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2-Dibromo-3-chloropropane [96-12-8]^9.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2-Dibromoethane [106-93-4]^13 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2-Dichlorobenzene [95-50-1]^3.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2-Dichloroethane [107-06-2]^4.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,2-Dichloropropane [78-87-5]^2.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,3,5-Trimethylbenzene [108-67-8]^6.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,3-Dichlorobenzene [541-73-1]^3.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,3-Dichloropropane [142-28-9]^3.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:451,4-Dichlorobenzene [106-46-7]^3.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:452,2-Dichloropropane [594-20-7]^5.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:452-Butanone [78-93-3]^26 MSZ6D07032100ND 20 ug/L EPA 8260B 04/07/16 15:452-Chloroethyl Vinyl Ether [110-75-8]^22 MSZ6D07032100ND 20 ug/L EPA 8260B 04/07/16 15:452-Chlorotoluene [95-49-8]^1.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:452-Hexanone [591-78-6]^18 MSZ6D07032100ND 20 ug/L EPA 8260B 04/07/16 15:454-Chlorotoluene [106-43-4]^1.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:454-Isopropyltoluene [99-87-6]^1.7 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:454-Methyl-2-pentanone [108-10-1]^22 MSZ6D07032100ND 20 ug/L EPA 8260B 04/07/16 15:45Benzene [71-43-2]^3.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Bromobenzene [108-86-1]^3.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Bromochloromethane [74-97-5]^9.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Bromodichloromethane [75-27-4]^3.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Bromoform [75-25-2]^4.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Bromomethane [74-83-9]^2.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Carbon disulfide [75-15-0]^30 MSZ6D07032100ND 20 ug/L EPA 8260B 04/07/16 15:45Carbon tetrachloride [56-23-5]^3.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Chlorobenzene [108-90-7]^3.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Chloroethane [75-00-3]^4.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Chloroform [67-66-3]^3.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Chloromethane [74-87-3]^2.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45cis-1,2-Dichloroethene [156-59-2]^3.0 MSZ6D0703220730D 20 ug/L EPA 8260B 04/07/16 15:45cis-1,3-Dichloropropene [10061-01-5]^4.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Dibromochloromethane [124-48-1]^3.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Dibromomethane [74-95-3]^5.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Dichlorodifluoromethane [75-71-8]^4.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Ethylbenzene [100-41-4]^2.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Hexachlorobutadiene [87-68-3]^4.4 MSZ6D0703220ND 20 Page 4 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 4 of 26 www.encolabs.com ANALYTICAL RESULTS MW-1Description:Lab Sample ID:CZ04159-01 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:21Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 15:45Isopropyl Ether [108-20-3]^1.1 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Isopropylbenzene [98-82-8]^2.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45m,p-Xylenes [108-38-3/106-42-3]^3.4 MSZ6D0703240ND 20 ug/L EPA 8260B 04/07/16 15:45Methylene chloride [75-09-2]^4.6 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Methyl-tert-Butyl Ether [1634-04-4]^3.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Naphthalene [91-20-3]^2.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45n-Butyl Benzene [104-51-8]^1.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45n-Propyl Benzene [103-65-1]^2.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45o-Xylene [95-47-6]^1.3 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45sec-Butylbenzene [135-98-8]^2.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Styrene [100-42-5]^2.2 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45tert-Butylbenzene [98-06-6]^3.4 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Tetrachloroethene [127-18-4]^3.4 MSZ6D0703220190D 20 ug/L EPA 8260B 04/07/16 15:45Toluene [108-88-3]^2.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45trans-1,2-Dichloroethene [156-60-5]^4.2 MSZ6D070322026D 20 ug/L EPA 8260B 04/07/16 15:45trans-1,3-Dichloropropene [10061-02-6]^3.0 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Trichloroethene [79-01-6]^3.0 MSZ6D0703220860D 20 ug/L EPA 8260B 04/07/16 15:45Trichlorofluoromethane [75-69-4]^4.8 MSZ6D0703220ND 20 ug/L EPA 8260B 04/07/16 15:45Vinyl chloride [75-01-4]^6.4 MSZ6D0703220180D 20 ug/L EPA 8260B 04/07/16 15:45Xylenes (Total) [1330-20-7]^9.0 MSZ6D0703260ND 20 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13696 %MSZEPA 8260B 04/07/16 15:456D070324850.0 1 Dibromofluoromethane 67-129106 %MSZEPA 8260B 04/07/16 15:456D070325350.0 1 Toluene-d8 59-13497 %MSZEPA 8260B 04/07/16 15:456D070324950.0 1 Page 5 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 5 of 26 www.encolabs.com ANALYTICAL RESULTS MW-7Description:Lab Sample ID:CZ04159-02 04/04/16 09:45Received: CZ04159Work Order:04/01/16 10:30Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 15:161,1,1,2-Tetrachloroethane [630-20-6]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,1,1-Trichloroethane [71-55-6]^0.12 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,1,2,2-Tetrachloroethane [79-34-5]^0.28 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,1,2-Trichloroethane [79-00-5]^0.14 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,1-Dichloroethane [75-34-3]^0.13 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,1-Dichloroethene [75-35-4]^0.21 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,1-Dichloropropene [563-58-6]^0.15 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2,3-Trichlorobenzene [87-61-6]^0.012 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2,3-Trichloropropane [96-18-4]^0.23 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2,4-Trichlorobenzene [120-82-1]^0.14 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2,4-Trimethylbenzene [95-63-6]^0.10 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2-Dibromo-3-chloropropane [96-12-8]^0.48 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2-Dibromoethane [106-93-4]^0.66 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2-Dichlorobenzene [95-50-1]^0.19 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2-Dichloroethane [107-06-2]^0.21 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,2-Dichloropropane [78-87-5]^0.10 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,3,5-Trimethylbenzene [108-67-8]^0.30 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,3-Dichlorobenzene [541-73-1]^0.15 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,3-Dichloropropane [142-28-9]^0.16 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:161,4-Dichlorobenzene [106-46-7]^0.19 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:162,2-Dichloropropane [594-20-7]^0.28 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:162-Butanone [78-93-3]^1.3 MSZ6D070325.0ND 1 ug/L EPA 8260B 04/07/16 15:162-Chloroethyl Vinyl Ether [110-75-8]^1.1 MSZ6D070325.0ND 1 ug/L EPA 8260B 04/07/16 15:162-Chlorotoluene [95-49-8]^0.081 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:162-Hexanone [591-78-6]^0.88 MSZ6D070325.0ND 1 ug/L EPA 8260B 04/07/16 15:164-Chlorotoluene [106-43-4]^0.068 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:164-Isopropyltoluene [99-87-6]^0.085 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:164-Methyl-2-pentanone [108-10-1]^1.1 MSZ6D070325.0ND 1 ug/L EPA 8260B 04/07/16 15:16Benzene [71-43-2]^0.15 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Bromobenzene [108-86-1]^0.16 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Bromochloromethane [74-97-5]^0.48 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Bromodichloromethane [75-27-4]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Bromoform [75-25-2]^0.22 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Bromomethane [74-83-9]^0.14 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Carbon disulfide [75-15-0]^1.5 MSZ6D070325.0ND 1 ug/L EPA 8260B 04/07/16 15:16Carbon tetrachloride [56-23-5]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Chlorobenzene [108-90-7]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Chloroethane [75-00-3]^0.23 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Chloroform [67-66-3]^0.18 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Chloromethane [74-87-3]^0.13 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16cis-1,2-Dichloroethene [156-59-2]^0.15 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16cis-1,3-Dichloropropene [10061-01-5]^0.20 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Dibromochloromethane [124-48-1]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Dibromomethane [74-95-3]^0.27 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Dichlorodifluoromethane [75-71-8]^0.20 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Ethylbenzene [100-41-4]^0.13 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Hexachlorobutadiene [87-68-3]^0.22 MSZ6D070321.0ND 1 Page 6 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 6 of 26 www.encolabs.com ANALYTICAL RESULTS MW-7Description:Lab Sample ID:CZ04159-02 04/04/16 09:45Received: CZ04159Work Order:04/01/16 10:30Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 15:16Isopropyl Ether [108-20-3]^0.054 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Isopropylbenzene [98-82-8]^0.14 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16m,p-Xylenes [108-38-3/106-42-3]^0.17 MSZ6D070322.0ND 1 ug/L EPA 8260B 04/07/16 15:16Methylene chloride [75-09-2]^0.23 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Methyl-tert-Butyl Ether [1634-04-4]^0.16 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Naphthalene [91-20-3]^0.11 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16n-Butyl Benzene [104-51-8]^0.058 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16n-Propyl Benzene [103-65-1]^0.12 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16o-Xylene [95-47-6]^0.065 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16sec-Butylbenzene [135-98-8]^0.10 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Styrene [100-42-5]^0.11 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16tert-Butylbenzene [98-06-6]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Tetrachloroethene [127-18-4]^0.17 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Toluene [108-88-3]^0.14 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16trans-1,2-Dichloroethene [156-60-5]^0.21 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16trans-1,3-Dichloropropene [10061-02-6]^0.15 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Trichloroethene [79-01-6]^0.15 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Trichlorofluoromethane [75-69-4]^0.24 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Vinyl chloride [75-01-4]^0.32 MSZ6D070321.0ND 1 ug/L EPA 8260B 04/07/16 15:16Xylenes (Total) [1330-20-7]^0.45 MSZ6D070323.0ND 1 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13694 %MSZEPA 8260B 04/07/16 15:166D070324750.0 1 Dibromofluoromethane 67-129104 %MSZEPA 8260B 04/07/16 15:166D070325250.0 1 Toluene-d8 59-13497 %MSZEPA 8260B 04/07/16 15:166D070324950.0 1 Page 7 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 7 of 26 www.encolabs.com ANALYTICAL RESULTS MW-8Description:Lab Sample ID:CZ04159-03 04/04/16 09:45Received: CZ04159Work Order:04/01/16 10:15Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/06/16 21:181,1,1,2-Tetrachloroethane [630-20-6]^0.17 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,1,1-Trichloroethane [71-55-6]^0.12 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,1,2,2-Tetrachloroethane [79-34-5]^0.28 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,1,2-Trichloroethane [79-00-5]^0.14 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,1-Dichloroethane [75-34-3]^0.13 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,1-Dichloroethene [75-35-4]^0.21 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,1-Dichloropropene [563-58-6]^0.15 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2,3-Trichlorobenzene [87-61-6]^0.012 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2,3-Trichloropropane [96-18-4]^0.23 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2,4-Trichlorobenzene [120-82-1]^0.14 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2,4-Trimethylbenzene [95-63-6]^0.10 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2-Dibromo-3-chloropropane [96-12-8]^0.48 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2-Dibromoethane [106-93-4]^0.66 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2-Dichlorobenzene [95-50-1]^0.19 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2-Dichloroethane [107-06-2]^0.21 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,2-Dichloropropane [78-87-5]^0.10 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,3,5-Trimethylbenzene [108-67-8]^0.30 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,3-Dichlorobenzene [541-73-1]^0.15 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,3-Dichloropropane [142-28-9]^0.16 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:181,4-Dichlorobenzene [106-46-7]^0.19 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:182,2-Dichloropropane [594-20-7]^0.28 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:182-Butanone [78-93-3]^1.3 MSZ6D060235.0ND 1 ug/L EPA 8260B 04/06/16 21:182-Chloroethyl Vinyl Ether [110-75-8]^1.1 MSZ6D060235.0ND 1 ug/L EPA 8260B 04/06/16 21:182-Chlorotoluene [95-49-8]^0.081 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:182-Hexanone [591-78-6]^0.88 MSZ6D060235.0ND 1 ug/L EPA 8260B 04/06/16 21:184-Chlorotoluene [106-43-4]^0.068 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:184-Isopropyltoluene [99-87-6]^0.085 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:184-Methyl-2-pentanone [108-10-1]^1.1 MSZ6D060235.0ND 1 ug/L EPA 8260B 04/06/16 21:18Benzene [71-43-2]^0.15 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Bromobenzene [108-86-1]^0.16 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Bromochloromethane [74-97-5]^0.48 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Bromodichloromethane [75-27-4]^0.17 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Bromoform [75-25-2]^0.22 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Bromomethane [74-83-9]^0.14 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Carbon disulfide [75-15-0]^1.5 MSZ6D060235.0ND 1 ug/L EPA 8260B 04/06/16 21:18Carbon tetrachloride [56-23-5]^0.17 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Chlorobenzene [108-90-7]^0.17 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Chloroethane [75-00-3]^0.23 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Chloroform [67-66-3]^0.18 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Chloromethane [74-87-3]^0.13 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18cis-1,2-Dichloroethene [156-59-2]^0.15 MSZ6D060231.03.1 1 ug/L EPA 8260B 04/06/16 21:18cis-1,3-Dichloropropene [10061-01-5]^0.20 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Dibromochloromethane [124-48-1]^0.17 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Dibromomethane [74-95-3]^0.27 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Dichlorodifluoromethane [75-71-8]^0.20 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Ethylbenzene [100-41-4]^0.13 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Hexachlorobutadiene [87-68-3]^0.22 MSZ6D060231.0ND 1 Page 8 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 8 of 26 www.encolabs.com ANALYTICAL RESULTS MW-8Description:Lab Sample ID:CZ04159-03 04/04/16 09:45Received: CZ04159Work Order:04/01/16 10:15Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/06/16 21:18Isopropyl Ether [108-20-3]^0.054 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Isopropylbenzene [98-82-8]^0.14 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18m,p-Xylenes [108-38-3/106-42-3]^0.17 MSZ6D060232.0ND 1 ug/L EPA 8260B 04/06/16 21:18Methylene chloride [75-09-2]^0.23 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Methyl-tert-Butyl Ether [1634-04-4]^0.16 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Naphthalene [91-20-3]^0.11 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18n-Butyl Benzene [104-51-8]^0.058 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18n-Propyl Benzene [103-65-1]^0.12 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18o-Xylene [95-47-6]^0.065 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18sec-Butylbenzene [135-98-8]^0.10 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Styrene [100-42-5]^0.11 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18tert-Butylbenzene [98-06-6]^0.17 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Tetrachloroethene [127-18-4]^0.17 MSZ6D060231.016 1 ug/L EPA 8260B 04/06/16 21:18Toluene [108-88-3]^0.14 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18trans-1,2-Dichloroethene [156-60-5]^0.21 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18trans-1,3-Dichloropropene [10061-02-6]^0.15 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Trichloroethene [79-01-6]^0.15 MSZ6D060231.03.6 1 ug/L EPA 8260B 04/06/16 21:18Trichlorofluoromethane [75-69-4]^0.24 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Vinyl chloride [75-01-4]^0.32 MSZ6D060231.0ND 1 ug/L EPA 8260B 04/06/16 21:18Xylenes (Total) [1330-20-7]^0.45 MSZ6D060233.0ND 1 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13693 %MSZEPA 8260B 04/06/16 21:186D060234750.0 1 Dibromofluoromethane 67-129106 %MSZEPA 8260B 04/06/16 21:186D060235350.0 1 Toluene-d8 59-13495 %MSZEPA 8260B 04/06/16 21:186D060234850.0 1 Page 9 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 9 of 26 www.encolabs.com ANALYTICAL RESULTS MW-9Description:Lab Sample ID:CZ04159-04 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:45Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 16:151,1,1,2-Tetrachloroethane [630-20-6]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,1,1-Trichloroethane [71-55-6]^12 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,1,2,2-Tetrachloroethane [79-34-5]^28 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,1,2-Trichloroethane [79-00-5]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,1-Dichloroethane [75-34-3]^13 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,1-Dichloroethene [75-35-4]^21 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,1-Dichloropropene [563-58-6]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2,3-Trichlorobenzene [87-61-6]^1.2 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2,3-Trichloropropane [96-18-4]^23 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2,4-Trichlorobenzene [120-82-1]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2,4-Trimethylbenzene [95-63-6]^10 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2-Dibromo-3-chloropropane [96-12-8]^48 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2-Dibromoethane [106-93-4]^66 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2-Dichlorobenzene [95-50-1]^19 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2-Dichloroethane [107-06-2]^21 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,2-Dichloropropane [78-87-5]^10 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,3,5-Trimethylbenzene [108-67-8]^30 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,3-Dichlorobenzene [541-73-1]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,3-Dichloropropane [142-28-9]^16 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:151,4-Dichlorobenzene [106-46-7]^19 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:152,2-Dichloropropane [594-20-7]^28 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:152-Butanone [78-93-3]^130 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:152-Chloroethyl Vinyl Ether [110-75-8]^110 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:152-Chlorotoluene [95-49-8]^8.1 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:152-Hexanone [591-78-6]^88 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:154-Chlorotoluene [106-43-4]^6.8 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:154-Isopropyltoluene [99-87-6]^8.5 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:154-Methyl-2-pentanone [108-10-1]^110 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:15Benzene [71-43-2]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Bromobenzene [108-86-1]^16 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Bromochloromethane [74-97-5]^48 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Bromodichloromethane [75-27-4]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Bromoform [75-25-2]^22 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Bromomethane [74-83-9]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Carbon disulfide [75-15-0]^150 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:15Carbon tetrachloride [56-23-5]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Chlorobenzene [108-90-7]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Chloroethane [75-00-3]^23 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Chloroform [67-66-3]^18 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Chloromethane [74-87-3]^13 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15cis-1,2-Dichloroethene [156-59-2]^15 MSZ6D0703210041JD 100 ug/L EPA 8260B 04/07/16 16:15cis-1,3-Dichloropropene [10061-01-5]^20 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Dibromochloromethane [124-48-1]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Dibromomethane [74-95-3]^27 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Dichlorodifluoromethane [75-71-8]^20 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Ethylbenzene [100-41-4]^13 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Hexachlorobutadiene [87-68-3]^22 MSZ6D07032100ND 100 Page 10 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 10 of 26 www.encolabs.com ANALYTICAL RESULTS MW-9Description:Lab Sample ID:CZ04159-04 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:45Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 16:15Isopropyl Ether [108-20-3]^5.4 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Isopropylbenzene [98-82-8]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15m,p-Xylenes [108-38-3/106-42-3]^17 MSZ6D07032200ND 100 ug/L EPA 8260B 04/07/16 16:15Methylene chloride [75-09-2]^23 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Methyl-tert-Butyl Ether [1634-04-4]^16 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Naphthalene [91-20-3]^11 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15n-Butyl Benzene [104-51-8]^5.8 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15n-Propyl Benzene [103-65-1]^12 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15o-Xylene [95-47-6]^6.5 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15sec-Butylbenzene [135-98-8]^10 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Styrene [100-42-5]^11 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15tert-Butylbenzene [98-06-6]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Tetrachloroethene [127-18-4]^17 MSZ6D070321004100D 100 ug/L EPA 8260B 04/07/16 16:15Toluene [108-88-3]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15trans-1,2-Dichloroethene [156-60-5]^21 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15trans-1,3-Dichloropropene [10061-02-6]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Trichloroethene [79-01-6]^15 MSZ6D07032100260D 100 ug/L EPA 8260B 04/07/16 16:15Trichlorofluoromethane [75-69-4]^24 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Vinyl chloride [75-01-4]^32 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:15Xylenes (Total) [1330-20-7]^45 MSZ6D07032300ND 100 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13694 %MSZEPA 8260B 04/07/16 16:156D070324750.0 1 Dibromofluoromethane 67-129105 %MSZEPA 8260B 04/07/16 16:156D070325250.0 1 Toluene-d8 59-13498 %MSZEPA 8260B 04/07/16 16:156D070324950.0 1 Page 11 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 11 of 26 www.encolabs.com ANALYTICAL RESULTS MW-10Description:Lab Sample ID:CZ04159-05 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:30Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 16:441,1,1,2-Tetrachloroethane [630-20-6]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,1,1-Trichloroethane [71-55-6]^12 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,1,2,2-Tetrachloroethane [79-34-5]^28 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,1,2-Trichloroethane [79-00-5]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,1-Dichloroethane [75-34-3]^13 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,1-Dichloroethene [75-35-4]^21 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,1-Dichloropropene [563-58-6]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2,3-Trichlorobenzene [87-61-6]^1.2 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2,3-Trichloropropane [96-18-4]^23 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2,4-Trichlorobenzene [120-82-1]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2,4-Trimethylbenzene [95-63-6]^10 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2-Dibromo-3-chloropropane [96-12-8]^48 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2-Dibromoethane [106-93-4]^66 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2-Dichlorobenzene [95-50-1]^19 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2-Dichloroethane [107-06-2]^21 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,2-Dichloropropane [78-87-5]^10 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,3,5-Trimethylbenzene [108-67-8]^30 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,3-Dichlorobenzene [541-73-1]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,3-Dichloropropane [142-28-9]^16 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:441,4-Dichlorobenzene [106-46-7]^19 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:442,2-Dichloropropane [594-20-7]^28 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:442-Butanone [78-93-3]^130 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:442-Chloroethyl Vinyl Ether [110-75-8]^110 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:442-Chlorotoluene [95-49-8]^8.1 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:442-Hexanone [591-78-6]^88 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:444-Chlorotoluene [106-43-4]^6.8 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:444-Isopropyltoluene [99-87-6]^8.5 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:444-Methyl-2-pentanone [108-10-1]^110 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:44Benzene [71-43-2]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Bromobenzene [108-86-1]^16 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Bromochloromethane [74-97-5]^48 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Bromodichloromethane [75-27-4]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Bromoform [75-25-2]^22 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Bromomethane [74-83-9]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Carbon disulfide [75-15-0]^150 MSZ6D07032500ND 100 ug/L EPA 8260B 04/07/16 16:44Carbon tetrachloride [56-23-5]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Chlorobenzene [108-90-7]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Chloroethane [75-00-3]^23 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Chloroform [67-66-3]^18 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Chloromethane [74-87-3]^13 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44cis-1,2-Dichloroethene [156-59-2]^15 MSZ6D07032100270D 100 ug/L EPA 8260B 04/07/16 16:44cis-1,3-Dichloropropene [10061-01-5]^20 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Dibromochloromethane [124-48-1]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Dibromomethane [74-95-3]^27 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Dichlorodifluoromethane [75-71-8]^20 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Ethylbenzene [100-41-4]^13 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Hexachlorobutadiene [87-68-3]^22 MSZ6D07032100ND 100 Page 12 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 12 of 26 www.encolabs.com ANALYTICAL RESULTS MW-10Description:Lab Sample ID:CZ04159-05 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:30Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 16:44Isopropyl Ether [108-20-3]^5.4 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Isopropylbenzene [98-82-8]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44m,p-Xylenes [108-38-3/106-42-3]^17 MSZ6D07032200ND 100 ug/L EPA 8260B 04/07/16 16:44Methylene chloride [75-09-2]^23 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Methyl-tert-Butyl Ether [1634-04-4]^16 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Naphthalene [91-20-3]^11 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44n-Butyl Benzene [104-51-8]^5.8 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44n-Propyl Benzene [103-65-1]^12 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44o-Xylene [95-47-6]^6.5 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44sec-Butylbenzene [135-98-8]^10 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Styrene [100-42-5]^11 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44tert-Butylbenzene [98-06-6]^17 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Tetrachloroethene [127-18-4]^17 MSZ6D070321004900D 100 ug/L EPA 8260B 04/07/16 16:44Toluene [108-88-3]^14 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44trans-1,2-Dichloroethene [156-60-5]^21 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44trans-1,3-Dichloropropene [10061-02-6]^15 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Trichloroethene [79-01-6]^15 MSZ6D070321002100D 100 ug/L EPA 8260B 04/07/16 16:44Trichlorofluoromethane [75-69-4]^24 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Vinyl chloride [75-01-4]^32 MSZ6D07032100ND 100 ug/L EPA 8260B 04/07/16 16:44Xylenes (Total) [1330-20-7]^45 MSZ6D07032300ND 100 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13696 %MSZEPA 8260B 04/07/16 16:446D070324850.0 1 Dibromofluoromethane 67-129106 %MSZEPA 8260B 04/07/16 16:446D070325350.0 1 Toluene-d8 59-13496 %MSZEPA 8260B 04/07/16 16:446D070324850.0 1 Page 13 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 13 of 26 www.encolabs.com ANALYTICAL RESULTS MW-13Description:Lab Sample ID:CZ04159-06 04/04/16 09:45Received: CZ04159Work Order:04/01/16 10:00Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 17:131,1,1,2-Tetrachloroethane [630-20-6]^85 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,1,1-Trichloroethane [71-55-6]^60 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,1,2,2-Tetrachloroethane [79-34-5]^140 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,1,2-Trichloroethane [79-00-5]^70 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,1-Dichloroethane [75-34-3]^65 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,1-Dichloroethene [75-35-4]^100 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,1-Dichloropropene [563-58-6]^75 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2,3-Trichlorobenzene [87-61-6]^6.0 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2,3-Trichloropropane [96-18-4]^120 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2,4-Trichlorobenzene [120-82-1]^70 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2,4-Trimethylbenzene [95-63-6]^50 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2-Dibromo-3-chloropropane [96-12-8]^240 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2-Dibromoethane [106-93-4]^330 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2-Dichlorobenzene [95-50-1]^95 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2-Dichloroethane [107-06-2]^100 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,2-Dichloropropane [78-87-5]^50 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,3,5-Trimethylbenzene [108-67-8]^150 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,3-Dichlorobenzene [541-73-1]^75 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,3-Dichloropropane [142-28-9]^80 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:131,4-Dichlorobenzene [106-46-7]^95 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:132,2-Dichloropropane [594-20-7]^140 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:132-Butanone [78-93-3]^650 MSZ6D070322500ND 500 ug/L EPA 8260B 04/07/16 17:132-Chloroethyl Vinyl Ether [110-75-8]^550 MSZ6D070322500ND 500 ug/L EPA 8260B 04/07/16 17:132-Chlorotoluene [95-49-8]^40 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:132-Hexanone [591-78-6]^440 MSZ6D070322500ND 500 ug/L EPA 8260B 04/07/16 17:134-Chlorotoluene [106-43-4]^34 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:134-Isopropyltoluene [99-87-6]^42 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:134-Methyl-2-pentanone [108-10-1]^550 MSZ6D070322500ND 500 ug/L EPA 8260B 04/07/16 17:13Benzene [71-43-2]^75 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Bromobenzene [108-86-1]^80 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Bromochloromethane [74-97-5]^240 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Bromodichloromethane [75-27-4]^85 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Bromoform [75-25-2]^110 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Bromomethane [74-83-9]^70 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Carbon disulfide [75-15-0]^750 MSZ6D070322500ND 500 ug/L EPA 8260B 04/07/16 17:13Carbon tetrachloride [56-23-5]^85 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Chlorobenzene [108-90-7]^85 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Chloroethane [75-00-3]^120 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Chloroform [67-66-3]^90 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Chloromethane [74-87-3]^65 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13cis-1,2-Dichloroethene [156-59-2]^75 MSZ6D07032500650D 500 ug/L EPA 8260B 04/07/16 17:13cis-1,3-Dichloropropene [10061-01-5]^100 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Dibromochloromethane [124-48-1]^85 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Dibromomethane [74-95-3]^140 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Dichlorodifluoromethane [75-71-8]^100 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Ethylbenzene [100-41-4]^65 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Hexachlorobutadiene [87-68-3]^110 MSZ6D07032500ND 500 Page 14 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 14 of 26 www.encolabs.com ANALYTICAL RESULTS MW-13Description:Lab Sample ID:CZ04159-06 04/04/16 09:45Received: CZ04159Work Order:04/01/16 10:00Sampled:WaterMatrix: Jimmy HairSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/07/16 17:13Isopropyl Ether [108-20-3]^27 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Isopropylbenzene [98-82-8]^70 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13m,p-Xylenes [108-38-3/106-42-3]^85 MSZ6D070321000ND 500 ug/L EPA 8260B 04/07/16 17:13Methylene chloride [75-09-2]^120 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Methyl-tert-Butyl Ether [1634-04-4]^80 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Naphthalene [91-20-3]^55 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13n-Butyl Benzene [104-51-8]^29 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13n-Propyl Benzene [103-65-1]^60 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13o-Xylene [95-47-6]^32 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13sec-Butylbenzene [135-98-8]^50 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Styrene [100-42-5]^55 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13tert-Butylbenzene [98-06-6]^85 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Tetrachloroethene [127-18-4]^85 MSZ6D0703250021000D 500 ug/L EPA 8260B 04/07/16 17:13Toluene [108-88-3]^70 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13trans-1,2-Dichloroethene [156-60-5]^100 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13trans-1,3-Dichloropropene [10061-02-6]^75 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Trichloroethene [79-01-6]^75 MSZ6D07032500660D 500 ug/L EPA 8260B 04/07/16 17:13Trichlorofluoromethane [75-69-4]^120 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Vinyl chloride [75-01-4]^160 MSZ6D07032500ND 500 ug/L EPA 8260B 04/07/16 17:13Xylenes (Total) [1330-20-7]^220 MSZ6D070321500ND 500 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13697 %MSZEPA 8260B 04/07/16 17:136D070324850.0 1 Dibromofluoromethane 67-129107 %MSZEPA 8260B 04/07/16 17:136D070325450.0 1 Toluene-d8 59-13498 %MSZEPA 8260B 04/07/16 17:136D070324950.0 1 Page 15 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 15 of 26 www.encolabs.com ANALYTICAL RESULTS Trip BlankDescription:Lab Sample ID:CZ04159-07 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:21Sampled:WaterMatrix: ENCOSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/08/16 14:211,1,1,2-Tetrachloroethane [630-20-6]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,1,1-Trichloroethane [71-55-6]^0.12 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,1,2,2-Tetrachloroethane [79-34-5]^0.28 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,1,2-Trichloroethane [79-00-5]^0.14 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,1-Dichloroethane [75-34-3]^0.13 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,1-Dichloroethene [75-35-4]^0.21 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,1-Dichloropropene [563-58-6]^0.15 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2,3-Trichlorobenzene [87-61-6]^0.012 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2,3-Trichloropropane [96-18-4]^0.23 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2,4-Trichlorobenzene [120-82-1]^0.14 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2,4-Trimethylbenzene [95-63-6]^0.10 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2-Dibromo-3-chloropropane [96-12-8]^0.48 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2-Dibromoethane [106-93-4]^0.66 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2-Dichlorobenzene [95-50-1]^0.19 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2-Dichloroethane [107-06-2]^0.21 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,2-Dichloropropane [78-87-5]^0.10 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,3,5-Trimethylbenzene [108-67-8]^0.30 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,3-Dichlorobenzene [541-73-1]^0.15 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,3-Dichloropropane [142-28-9]^0.16 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:211,4-Dichlorobenzene [106-46-7]^0.19 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:212,2-Dichloropropane [594-20-7]^0.28 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:212-Butanone [78-93-3]^1.3 MSZ6D080155.0ND 1 ug/L EPA 8260B 04/08/16 14:212-Chloroethyl Vinyl Ether [110-75-8]^1.1 MSZ6D080155.0ND 1 ug/L EPA 8260B 04/08/16 14:212-Chlorotoluene [95-49-8]^0.081 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:212-Hexanone [591-78-6]^0.88 MSZ6D080155.0ND 1 ug/L EPA 8260B 04/08/16 14:214-Chlorotoluene [106-43-4]^0.068 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:214-Isopropyltoluene [99-87-6]^0.085 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:214-Methyl-2-pentanone [108-10-1]^1.1 MSZ6D080155.0ND 1 ug/L EPA 8260B 04/08/16 14:21Benzene [71-43-2]^0.15 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Bromobenzene [108-86-1]^0.16 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Bromochloromethane [74-97-5]^0.48 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Bromodichloromethane [75-27-4]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Bromoform [75-25-2]^0.22 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Bromomethane [74-83-9]^0.14 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Carbon disulfide [75-15-0]^1.5 MSZ6D080155.0ND 1 ug/L EPA 8260B 04/08/16 14:21Carbon tetrachloride [56-23-5]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Chlorobenzene [108-90-7]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Chloroethane [75-00-3]^0.23 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Chloroform [67-66-3]^0.18 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Chloromethane [74-87-3]^0.13 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21cis-1,2-Dichloroethene [156-59-2]^0.15 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21cis-1,3-Dichloropropene [10061-01-5]^0.20 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Dibromochloromethane [124-48-1]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Dibromomethane [74-95-3]^0.27 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Dichlorodifluoromethane [75-71-8]^0.20 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Ethylbenzene [100-41-4]^0.13 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Hexachlorobutadiene [87-68-3]^0.22 MSZ6D080151.0ND 1 Page 16 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 16 of 26 www.encolabs.com ANALYTICAL RESULTS Trip BlankDescription:Lab Sample ID:CZ04159-07 04/04/16 09:45Received: CZ04159Work Order:04/01/16 09:21Sampled:WaterMatrix: ENCOSampled By:Project:AMI Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number] ug/L EPA 8260B 04/08/16 14:21Isopropyl Ether [108-20-3]^0.054 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Isopropylbenzene [98-82-8]^0.14 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21m,p-Xylenes [108-38-3/106-42-3]^0.17 MSZ6D080152.0ND 1 ug/L EPA 8260B 04/08/16 14:21Methylene chloride [75-09-2]^0.23 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Methyl-tert-Butyl Ether [1634-04-4]^0.16 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Naphthalene [91-20-3]^0.11 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21n-Butyl Benzene [104-51-8]^0.058 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21n-Propyl Benzene [103-65-1]^0.12 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21o-Xylene [95-47-6]^0.065 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21sec-Butylbenzene [135-98-8]^0.10 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Styrene [100-42-5]^0.11 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21tert-Butylbenzene [98-06-6]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Tetrachloroethene [127-18-4]^0.17 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Toluene [108-88-3]^0.14 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21trans-1,2-Dichloroethene [156-60-5]^0.21 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21trans-1,3-Dichloropropene [10061-02-6]^0.15 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Trichloroethene [79-01-6]^0.15 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Trichlorofluoromethane [75-69-4]^0.24 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Vinyl chloride [75-01-4]^0.32 MSZ6D080151.0ND 1 ug/L EPA 8260B 04/08/16 14:21Xylenes (Total) [1330-20-7]^0.45 MSZ6D080153.0ND 1 Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF 4-Bromofluorobenzene 53-13692 %MSZEPA 8260B 04/08/16 14:216D080154650.0 1 Dibromofluoromethane 67-129119 %MSZEPA 8260B 04/08/16 14:216D080155950.0 1 Toluene-d8 59-134104 %MSZEPA 8260B 04/08/16 14:216D080155250.0 1 Page 17 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 17 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06023 - EPA 5030B_MS Prepared: 04/06/2016 12:15 Analyzed: 04/06/2016 13:01Blank (6D06023-BLK1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.00.17 U 1,1,1,2-Tetrachloroethane ug/L1.00.12 U 1,1,1-Trichloroethane ug/L1.00.28 U 1,1,2,2-Tetrachloroethane ug/L1.00.14 U 1,1,2-Trichloroethane ug/L1.00.13 U 1,1-Dichloroethane ug/L1.00.21 U 1,1-Dichloroethene ug/L1.00.15 U 1,1-Dichloropropene ug/L1.00.012 U 1,2,3-Trichlorobenzene ug/L1.00.23 U 1,2,3-Trichloropropane ug/L1.00.14 U 1,2,4-Trichlorobenzene ug/L1.00.10 U 1,2,4-Trimethylbenzene ug/L1.00.48 U 1,2-Dibromo-3-chloropropane ug/L1.00.66 U 1,2-Dibromoethane ug/L1.00.19 U 1,2-Dichlorobenzene ug/L1.00.21 U 1,2-Dichloroethane ug/L1.00.10 U 1,2-Dichloropropane ug/L1.00.30 U 1,3,5-Trimethylbenzene ug/L1.00.15 U 1,3-Dichlorobenzene ug/L1.00.16 U 1,3-Dichloropropane ug/L1.00.19 U 1,4-Dichlorobenzene ug/L1.00.28 U 2,2-Dichloropropane ug/L5.01.3 U 2-Butanone ug/L5.01.1 U 2-Chloroethyl Vinyl Ether ug/L1.00.081 U 2-Chlorotoluene ug/L5.00.88 U 2-Hexanone ug/L1.00.068 U 4-Chlorotoluene ug/L1.00.085 U 4-Isopropyltoluene ug/L5.01.1 U 4-Methyl-2-pentanone ug/L1.00.15 U Benzene ug/L1.00.16 U Bromobenzene ug/L1.00.48 U Bromochloromethane ug/L1.00.17 U Bromodichloromethane ug/L1.00.22 U Bromoform ug/L1.00.14 U Bromomethane ug/L5.01.5 U Carbon disulfide ug/L1.00.17 U Carbon tetrachloride ug/L1.00.17 U Chlorobenzene ug/L1.00.23 U Chloroethane ug/L1.00.18 U Chloroform ug/L1.00.13 U Chloromethane ug/L1.00.15 U cis-1,2-Dichloroethene ug/L1.00.20 U cis-1,3-Dichloropropene ug/L1.00.17 U Dibromochloromethane ug/L1.00.27 U Dibromomethane ug/L1.00.20 U Dichlorodifluoromethane ug/L1.00.13 U Ethylbenzene ug/L1.00.22 U Hexachlorobutadiene ug/L1.00.054 U Isopropyl Ether ug/L1.00.14 U Isopropylbenzene Page 18 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 18 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06023 - EPA 5030B_MS - Continued Prepared: 04/06/2016 12:15 Analyzed: 04/06/2016 13:01Blank (6D06023-BLK1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L2.00.17 U m,p-Xylenes ug/L1.00.23 U Methylene chloride ug/L1.00.16 U Methyl-tert-Butyl Ether ug/L1.00.11 U Naphthalene ug/L1.00.058 U n-Butyl Benzene ug/L1.00.12 U n-Propyl Benzene ug/L1.00.065 U o-Xylene ug/L1.00.10 U sec-Butylbenzene ug/L1.00.11 U Styrene ug/L1.00.17 U tert-Butylbenzene ug/L1.00.17 U Tetrachloroethene ug/L1.00.14 U Toluene ug/L1.00.21 U trans-1,2-Dichloroethene ug/L1.00.15 U trans-1,3-Dichloropropene ug/L1.00.15 U Trichloroethene ug/L1.00.24 U Trichlorofluoromethane ug/L1.00.32 U Vinyl chloride ug/L3.00.45 U Xylenes (Total) ug/L 50.0 53-1364-Bromofluorobenzene 9347 ug/L 50.0 67-129Dibromofluoromethane10553 ug/L 50.0 59-134Toluene-d8 9548 Prepared: 04/06/2016 12:15 Analyzed: 04/06/2016 13:31LCS (6D06023-BS1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 75-13311222 1,1-Dichloroethene ug/L1.0 20.0 81-13410120 Benzene ug/L1.0 20.0 83-1179920 Chlorobenzene ug/L1.0 20.0 71-1189820 Toluene ug/L1.0 20.0 74-11910721 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 10050 ug/L 50.0 67-129Dibromofluoromethane10753 ug/L 50.0 59-134Toluene-d8 9849 Prepared: 04/06/2016 12:15 Analyzed: 04/06/2016 14:00Matrix Spike (6D06023-MS1) Source: CZ04877-03 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 75-1331060.21 U21 1,1-Dichloroethene ug/L1.0 20.0 81-134980.15 U20 Benzene ug/L1.0 20.0 83-117970.17 U19 Chlorobenzene ug/L1.0 20.0 71-118940.14 U19 Toluene ug/L1.0 20.0 74-1191040.15 U21 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9748 ug/L 50.0 67-129Dibromofluoromethane10553 ug/L 50.0 59-134Toluene-d8 9749 Page 19 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 19 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D06023 - EPA 5030B_MS - Continued Prepared: 04/06/2016 12:15 Analyzed: 04/06/2016 14:29Matrix Spike Dup (6D06023-MSD1) Source: CZ04877-03 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 2075-133103 30.21 U21 1,1-Dichloroethene ug/L1.0 20.0 1781-13498 0.050.15 U20 Benzene ug/L1.0 20.0 1683-11796 0.90.17 U19 Chlorobenzene ug/L1.0 20.0 1771-11894 0.10.14 U19 Toluene ug/L1.0 20.0 2274-119102 20.15 U20 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9749 ug/L 50.0 67-129Dibromofluoromethane10452 ug/L 50.0 59-134Toluene-d8 9748 Batch 6D07032 - EPA 5030B_MS Prepared: 04/07/2016 11:06 Analyzed: 04/07/2016 11:41Blank (6D07032-BLK1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.00.17 U 1,1,1,2-Tetrachloroethane ug/L1.00.12 U 1,1,1-Trichloroethane ug/L1.00.28 U 1,1,2,2-Tetrachloroethane ug/L1.00.14 U 1,1,2-Trichloroethane ug/L1.00.13 U 1,1-Dichloroethane ug/L1.00.21 U 1,1-Dichloroethene ug/L1.00.15 U 1,1-Dichloropropene ug/L1.00.012 U 1,2,3-Trichlorobenzene ug/L1.00.23 U 1,2,3-Trichloropropane ug/L1.00.14 U 1,2,4-Trichlorobenzene ug/L1.00.10 U 1,2,4-Trimethylbenzene ug/L1.00.48 U 1,2-Dibromo-3-chloropropane ug/L1.00.66 U 1,2-Dibromoethane ug/L1.00.19 U 1,2-Dichlorobenzene ug/L1.00.21 U 1,2-Dichloroethane ug/L1.00.10 U 1,2-Dichloropropane ug/L1.00.30 U 1,3,5-Trimethylbenzene ug/L1.00.15 U 1,3-Dichlorobenzene ug/L1.00.16 U 1,3-Dichloropropane ug/L1.00.19 U 1,4-Dichlorobenzene ug/L1.00.28 U 2,2-Dichloropropane ug/L5.01.3 U 2-Butanone ug/L5.01.1 U 2-Chloroethyl Vinyl Ether ug/L1.00.081 U 2-Chlorotoluene ug/L5.00.88 U 2-Hexanone ug/L1.00.068 U 4-Chlorotoluene ug/L1.00.085 U 4-Isopropyltoluene ug/L5.01.1 U 4-Methyl-2-pentanone ug/L1.00.15 U Benzene ug/L1.00.16 U Bromobenzene ug/L1.00.48 U Bromochloromethane ug/L1.00.17 U Bromodichloromethane ug/L1.00.22 U Bromoform ug/L1.00.14 U Bromomethane ug/L5.01.5 U Carbon disulfide Page 20 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 20 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D07032 - EPA 5030B_MS - Continued Prepared: 04/07/2016 11:06 Analyzed: 04/07/2016 11:41Blank (6D07032-BLK1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.00.17 U Carbon tetrachloride ug/L1.00.17 U Chlorobenzene ug/L1.00.23 U Chloroethane ug/L1.00.18 U Chloroform ug/L1.00.13 U Chloromethane ug/L1.00.15 U cis-1,2-Dichloroethene ug/L1.00.20 U cis-1,3-Dichloropropene ug/L1.00.17 U Dibromochloromethane ug/L1.00.27 U Dibromomethane ug/L1.00.20 U Dichlorodifluoromethane ug/L1.00.13 U Ethylbenzene ug/L1.00.22 U Hexachlorobutadiene ug/L1.00.054 U Isopropyl Ether ug/L1.00.14 U Isopropylbenzene ug/L2.00.17 U m,p-Xylenes ug/L1.00.23 U Methylene chloride ug/L1.00.16 U Methyl-tert-Butyl Ether ug/L1.00.11 U Naphthalene ug/L1.00.058 U n-Butyl Benzene ug/L1.00.12 U n-Propyl Benzene ug/L1.00.065 U o-Xylene ug/L1.00.10 U sec-Butylbenzene ug/L1.00.11 U Styrene ug/L1.00.17 U tert-Butylbenzene ug/L1.00.17 U Tetrachloroethene ug/L1.00.14 U Toluene ug/L1.00.21 U trans-1,2-Dichloroethene ug/L1.00.15 U trans-1,3-Dichloropropene ug/L1.00.15 U Trichloroethene ug/L1.00.24 U Trichlorofluoromethane ug/L1.00.32 U Vinyl chloride ug/L3.00.45 U Xylenes (Total) ug/L 50.0 53-1364-Bromofluorobenzene 9547 ug/L 50.0 67-129Dibromofluoromethane10553 ug/L 50.0 59-134Toluene-d8 9748 Prepared: 04/07/2016 11:06 Analyzed: 04/07/2016 12:10LCS (6D07032-BS1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 75-13310621 1,1-Dichloroethene ug/L1.0 20.0 81-1349920 Benzene ug/L1.0 20.0 83-1179519 Chlorobenzene ug/L1.0 20.0 71-1189419 Toluene ug/L1.0 20.0 74-11910321 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9949 ug/L 50.0 67-129Dibromofluoromethane10553 ug/L 50.0 59-134Toluene-d8 9749 Page 21 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 21 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D07032 - EPA 5030B_MS - Continued Prepared: 04/07/2016 11:06 Analyzed: 04/07/2016 12:40Matrix Spike (6D07032-MS1) Source: CZ04877-08 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 75-1331070.21 U21 1,1-Dichloroethene ug/L1.0 20.0 81-134990.15 U20 Benzene ug/L1.0 20.0 83-117960.17 U19 Chlorobenzene ug/L1.0 20.0 71-118920.14 U18 Toluene ug/L1.0 20.0 74-1191040.15 U21 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9749 ug/L 50.0 67-129Dibromofluoromethane10553 ug/L 50.0 59-134Toluene-d8 9648 Prepared: 04/07/2016 11:06 Analyzed: 04/07/2016 13:09Matrix Spike Dup (6D07032-MSD1) Source: CZ04877-08 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 2075-133102 50.21 U20 1,1-Dichloroethene ug/L1.0 20.0 1781-13496 30.15 U19 Benzene ug/L1.0 20.0 1683-11792 40.17 U18 Chlorobenzene ug/L1.0 20.0 1771-11892 0.70.14 U18 Toluene ug/L1.0 20.0 2274-119102 20.15 U20 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9548 ug/L 50.0 67-129Dibromofluoromethane10452 ug/L 50.0 59-134Toluene-d8 9849 Batch 6D08015 - EPA 5030B_MS Prepared: 04/08/2016 10:30 Analyzed: 04/08/2016 13:23Blank (6D08015-BLK1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.00.17 U 1,1,1,2-Tetrachloroethane ug/L1.00.12 U 1,1,1-Trichloroethane ug/L1.00.28 U 1,1,2,2-Tetrachloroethane ug/L1.00.14 U 1,1,2-Trichloroethane ug/L1.00.13 U 1,1-Dichloroethane ug/L1.00.21 U 1,1-Dichloroethene ug/L1.00.15 U 1,1-Dichloropropene ug/L1.00.012 U 1,2,3-Trichlorobenzene ug/L1.00.23 U 1,2,3-Trichloropropane ug/L1.00.14 U 1,2,4-Trichlorobenzene ug/L1.00.10 U 1,2,4-Trimethylbenzene ug/L1.00.48 U 1,2-Dibromo-3-chloropropane ug/L1.00.66 U 1,2-Dibromoethane ug/L1.00.19 U 1,2-Dichlorobenzene ug/L1.00.21 U 1,2-Dichloroethane ug/L1.00.10 U 1,2-Dichloropropane ug/L1.00.30 U 1,3,5-Trimethylbenzene ug/L1.00.15 U 1,3-Dichlorobenzene ug/L1.00.16 U 1,3-Dichloropropane ug/L1.00.19 U 1,4-Dichlorobenzene ug/L1.00.28 U 2,2-Dichloropropane ug/L5.01.3 U 2-Butanone Page 22 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 22 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D08015 - EPA 5030B_MS - Continued Prepared: 04/08/2016 10:30 Analyzed: 04/08/2016 13:23Blank (6D08015-BLK1) Continued FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L5.01.1 U 2-Chloroethyl Vinyl Ether ug/L1.00.081 U 2-Chlorotoluene ug/L5.00.88 U 2-Hexanone ug/L1.00.068 U 4-Chlorotoluene ug/L1.00.085 U 4-Isopropyltoluene ug/L5.01.1 U 4-Methyl-2-pentanone ug/L1.00.15 U Benzene ug/L1.00.16 U Bromobenzene ug/L1.00.48 U Bromochloromethane ug/L1.00.17 U Bromodichloromethane ug/L1.00.22 U Bromoform ug/L1.00.14 U Bromomethane ug/L5.01.5 U Carbon disulfide ug/L1.00.17 U Carbon tetrachloride ug/L1.00.17 U Chlorobenzene ug/L1.00.23 U Chloroethane ug/L1.00.18 U Chloroform ug/L1.00.13 U Chloromethane ug/L1.00.15 U cis-1,2-Dichloroethene ug/L1.00.20 U cis-1,3-Dichloropropene ug/L1.00.17 U Dibromochloromethane ug/L1.00.27 U Dibromomethane ug/L1.00.20 U Dichlorodifluoromethane ug/L1.00.13 U Ethylbenzene ug/L1.00.22 U Hexachlorobutadiene ug/L1.00.054 U Isopropyl Ether ug/L1.00.14 U Isopropylbenzene ug/L2.00.17 U m,p-Xylenes ug/L1.00.23 U Methylene chloride ug/L1.00.16 U Methyl-tert-Butyl Ether ug/L1.00.11 U Naphthalene ug/L1.00.058 U n-Butyl Benzene ug/L1.00.12 U n-Propyl Benzene ug/L1.00.065 U o-Xylene ug/L1.00.10 U sec-Butylbenzene ug/L1.00.11 U Styrene ug/L1.00.17 U tert-Butylbenzene ug/L1.00.17 U Tetrachloroethene ug/L1.00.14 U Toluene ug/L1.00.21 U trans-1,2-Dichloroethene ug/L1.00.15 U trans-1,3-Dichloropropene ug/L1.00.15 U Trichloroethene ug/L1.00.24 U Trichlorofluoromethane ug/L1.00.32 U Vinyl chloride ug/L3.00.45 U Xylenes (Total) ug/L 50.0 53-1364-Bromofluorobenzene 9447 ug/L 50.0 67-129Dibromofluoromethane11357 ug/L 50.0 59-134Toluene-d8 10151 Page 23 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 23 of 26 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6D08015 - EPA 5030B_MS - Continued Prepared: 04/08/2016 10:30 Analyzed: 04/08/2016 11:56LCS (6D08015-BS1) FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 75-13311924 1,1-Dichloroethene ug/L1.0 20.0 81-13410621 Benzene ug/L1.0 20.0 83-1179419 Chlorobenzene ug/L1.0 20.0 71-1189619 Toluene ug/L1.0 20.0 74-1199920 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9045 ug/L 50.0 67-129Dibromofluoromethane10954 ug/L 50.0 59-134Toluene-d8 10251 Prepared: 04/08/2016 10:30 Analyzed: 04/08/2016 12:25Matrix Spike (6D08015-MS1) Source: CZ04877-09 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 75-1331190.21 U24 1,1-Dichloroethene ug/L1.0 20.0 81-1341040.15 U21 Benzene ug/L1.0 20.0 83-1171000.17 U20 Chlorobenzene ug/L1.0 20.0 71-1181040.14 U21 Toluene ug/L1.0 20.0 74-1191010.15 U20 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9447 ug/L 50.0 67-129Dibromofluoromethane11055 ug/L 50.0 59-134Toluene-d8 10251 Prepared: 04/08/2016 10:30 Analyzed: 04/08/2016 12:54Matrix Spike Dup (6D08015-MSD1) Source: CZ04877-09 FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL Spike Source %REC RPD ug/L1.0 20.0 2075-133116 20.21 U23 1,1-Dichloroethene ug/L1.0 20.0 1781-134105 20.15 U21 Benzene ug/L1.0 20.0 1683-117100 0.10.17 U20 Chlorobenzene ug/L1.0 20.0 1771-118102 20.14 U20 Toluene ug/L1.0 20.0 2274-11997 50.15 U19 Trichloroethene ug/L 50.0 53-1364-Bromofluorobenzene 9648 ug/L 50.0 67-129Dibromofluoromethane11256 ug/L 50.0 59-134Toluene-d8 10352 Page 24 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 24 of 26 www.encolabs.com FLAGS/NOTES AND DEFINITIONS The analyte was detected in the associated method blank. The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. MRL E U J D B ND The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a “tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Page 25 of 26This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 25 of 26 Page 26 of 26