9209_NorthWakeCDLF_GWMR_DIN28101_20160901

North Wake C&D Landfill
Facility Permit No. 9209-CDLF
Semi-Annual Sampling Report
(September 2016 Sampling Event)
Wake County
Report
Prepared December 2016

5400 Glenwood Avenue, Suite 400
Raleigh, North Carolina 27612
tel: [phone]
fax: [phone]

December 16, 2016

Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778

Subject: September 2016 Semi-Annual Groundwater Monitoring Report
North Wake C&D Landfill
Facility Permit No. 9209-CDLF

Dear Ms. Drummond:
CDM Smith Inc. (CDM Smith), on behalf of Wake County, is submitting an electronic copy of the
September 2016 semi-annual sampling event report. This letter report presents the results of the
most recent semi-annual sampling event at the North Wake C&D Landfill and constitutes the second
sampling event for 2016. The approved groundwater monitoring network consists of the background
well (i.e. MW-1) and three downgradient compliance wells (i.e. CD-1, -2, and -3). Field activities and
results of the September 2016 sampling event are discussed below.
Field Activities
Groundwater samples from the North Wake C&D Landfill were collected on September 1, 2016, by
use of disposable, laboratory decontaminated bailers. Monitoring well locations for the North Wake
C&D Landfill are shown on Figure 1. Well construction details are provided in Table 1.
Groundwater elevations were measured at each well prior to sampling and are presented in Table 2.
These groundwater elevations were used to construct a potentiometric surface map for this sampling
event. The potentiometric contours are shown on Figure 1.
After depth to groundwater was measured, three well volumes of water were removed from each
well prior to sampling to provide fresh formation water within the well water column. Each well
volume was measured for pH, conductivity, temperature, turbidity, dissolved oxygen, and oxidation-
reduction potential using a YSI-556 multi-parameter water quality meter and a HANNA HI 98703
turbidity meter. Monitoring wells with elevated turbidity were allowed to stabilize prior to sample
collection. The water quality parameters at the time of sampling are presented in Table 2.

Ms. Jaclynne Drummond
December 16, 2016
Page 2
Sampling Results
Shealy Environmental Services, Inc. located in West Columbia, South Carolina, analyzed the
groundwater samples for North Carolina Appendix I volatile organic compounds (VOCs) and Resource
and Conservation Recovery Act metals (i.e. arsenic, barium, cadmium, chromium, lead, mercury,
selenium, and silver). In accordance with Solid Waste Section (SWS) guidelines the analytical results
were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or
below SWS Limits (SWSLs). All monitoring wells for the C&D Landfill had detections of analytes above
the MDL but below SWSLs. These detections were qualified as estimated or “J” flags.
Vinyl chloride and mercury were detected above their 15A NCAC 02L .0202 (NC 2L) Groundwater
Standard in samples collected from CD-3. Vinyl chloride has never been detected in this compliance
well. Mercury has historically been detected below the NC 2L Standard in the background monitoring
well MW-1 and CD-3. Future analytical results will be evaluated to determine if a trend appears.
Equipment and trip blanks were analyzed for quality control. A duplicate sample was also collected for
quality control. The equipment blank had estimated detections of acetone and 2-butanone below
their respective NC 2L Standard. There were no VOC detections in the trip blank. The duplicate sample
collected from CD-3 had similar analyte detections and concentrations compared to the parent
sample. A complete summary of all detected and estimated concentrations for the September 2016
and previous sampling events is presented in Table 3. The laboratory analytical data report is provided
in Appendix A.
The next semi-annual sampling event will be completed in the spring of 2017. If you have any
questions or require further explanation, do not hesitate to call me at [phone].
Very truly yours,

Mathew F. Colone, P.G.
CDM Smith Inc.

cc: John Roberson, WCSWM
Elliott Cornell, WCSWM
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December 2016
Table 3
Detected Groundwater Constituents - Metals and Volatile Organic Compounds
September 2016 Semi-Annual Sampling Event
North Wake C&D Landfill - Permit Number 9209-CDLF
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0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 6,000 7 70 5 0.03 2,000
0.01 0.1 0.001 0.01 0.01 0.0002 0.01 0.01 100 5 5 1 1 1
MW-1 14-Mar-11 0.0421J
MW-1 20-Oct-11 0.0444J 0.00619J
MW-1 11-Apr-12 0.0384J
MW-1 26-Oct-12 0.0431J 0.00387J
MW-1 11-Apr-13 0.040J
MW-1 2-Oct-13 0.050J 0.001J
MW-1 3-Apr-14 0.040J 0.016 8.1J
MW-1 12-Nov-14 0.040J 0.00006J
MW-1 8-Apr-15 0.040J 0.001J 0.00021
MW-1 7-Oct-15 0.060J 0.001J 0.003J 0.00009J
MW-1 24-Mar-16 0.002J 0.040J 0.00013J 8.6J 0.27JB
MW-1 1-Sep-16 0.053J 0.000061J 0.0012J 0.0023J 0.00014J 2.3J
CD-1 14-Mar-11 0.00312J 0.174 0.00978J 0.00434J
CD-1 20-Oct-11 0.0629J 0.00306J
CD-1 11-Apr-12 0.0731J 0.00372J
CD-1 26-Oct-12 0.227 0.00793J 0.00669J
CD-1 11-Apr-13 0.130 0.007J
CD-1 2-Oct-13 0.220 0.013
CD-1 3-Apr-14 0.130 0.009J
CD-1 12-Nov-14 0.120 0.006J
CD-1 8-Apr-15 0.090J 0.006J
CD-1 7-Oct-15 0.070J 0.004J 6.1J
CD-1 25-Mar-16 0.002J 0.060J 0.003J 0.27JB
CD-1 1-Sep-16 0.068J 0.000065J 0.0031J 0.00059J
CD-2 14-Mar-11 0.0569J 0.00174J 0.00274J 0.97J
CD-2 20-Oct-11 0.0532J 0.00378J 5.9J 1.8J
CD-2 11-Apr-12 0.340 0.0156 0.0142 0.00247J 0.80J
CD-2 26-Oct-12 0.102 0.00481J 0.00389J
CD-2 11-Apr-13 0.120 0.004J
CD-2 2-Oct-13 0.080J 0.005J
CD-2 3-Apr-14 0.060J 0.006J 0.61J
CD-2 12-Nov-14 0.040J 0.003J
CD-2 8-Apr-15 0.060J 0.002J 0.36J
CD-2 7-Oct-15 0.050J 0.0010J 0.003J
CD-2 25-Mar-16 0.002J 0.040J 0.001J
CD-2 1-Sep-16 0.066J 0.00023J 0.0032J 0.00094J
CD-3 14-Mar-11 0.0507J
CD-3 20-Oct-11 0.0453J
CD-3 11-Apr-12 0.0675J 0.00226J
CD-3 26-Oct-12 0.0731J 0.00361J
CD-3 11-Apr-13 0.050J
CD-3 1-Oct-13 0.030J 0.00003J
CD-3 3-Apr-14 0.040J 0.001J
CD-3 12-Nov-14 0.040J 0.00008J
CD-3 8-Apr-15 0.040J 0.0001J
CD-3 7-Oct-15 0.050J 0.00026 0.28J
CD-3 24-Mar-16 0.003J 0.050J 0.00060 0.28JB 0.24J
CD-3 1-Sep-16 0.082J 0.000078J 0.0026J 0.0014 0.51J 1.2

Notes:
1. Metal detections are in milligrams per liter (parts per million).
2. Volatile organic compound detections are in micrograms per liter (parts per billion).
4. B - Indicates the analyte was detected in the associated method blank.
- Concentration exceeds the 15A NCAC 02L .0202 (2L) Groundwater Standard.
- Indicates the result is below the detection limit.
North Carolina 2L Standard
Solid Waste Section Limit
Metals
3. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit.
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Volatile Organic Compounds
Page 1 of 1 December 2016
Figure 1: Potentiometric Surface Map
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GW Elev.244.51GW Elev.228.73GW Elev.221.91 GW Elev.220.51 GW Elev.233.12 GW Elev.243.07 GW Elev. 242.19 GW Elev.263.94 LEGEND Groundwater Monitoring Well Potentiometric Contour (dashed where inferred)
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Appendix A
Analytical Data
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
RI02013Lot Number:
North Wake C&D LandfillProject Name:
09/09/2016Date Completed:
Catherine S. Dover
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 40
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
CDM Smith
Lot Number: RI02013
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: North Wake C&D Landfill
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 40
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
CDM Smith
Lot Number: RI02013

Project Name: North Wake C&D Landfill
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/01/2016 1320MW-1 Aqueous 09/02/2016
002 09/01/2016 1355CD-1 Aqueous 09/02/2016
003 09/01/2016 1345CD-2 Aqueous 09/02/2016
004 09/01/2016 1335CD-3 Aqueous 09/02/2016
005 09/01/2016 0800DUPAqueous 09/02/2016
006 09/01/2016 1410EQ BLANK Aqueous 09/02/2016
007 09/01/2016TRIP BLANK Aqueous 09/02/2016
(7 samples)
Page: 3 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-1
RI02013-001
09/01/2016 1320
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0326 ECP 21411
2 5030B 8260B 1 09/08/2016 0326 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 2.3 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 4 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-1
RI02013-001
09/01/2016 1320
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0326 ECP 21411
2 5030B 8260B 1 09/08/2016 0326 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 93 70-130 99 70-130
1,2-Dichloroethane-d4 103 70-130 88 70-130
Toluene-d8 100 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 5 of 40
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Shealy Environmental Services, Inc.

Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-1
RI02013-001
09/01/2016 1320
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1400 BNW 09/07/2016 1253 21415
1 7470A 7470A 1 09/06/2016 1714 COH 09/06/2016 1234 21320
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 53 J 1ug/L0.53100
Cadmium 7440-43-9 6020A 0.061 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 1.2 J 1ug/L0.6310
Lead 7439-92-1 6020A 2.3 J 1ug/L0.1510
Mercury 7439-97-6 7470A 0.00014 J 1mg/L0.0000280.0010
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 6 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-1
RI02013-002
09/01/2016 1355
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0350 ECP 21411
2 5030B 8260B 1 09/08/2016 0349 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 7 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-1
RI02013-002
09/01/2016 1355
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0350 ECP 21411
2 5030B 8260B 1 09/08/2016 0349 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 96 70-130 102 70-130
1,2-Dichloroethane-d4 105 70-130 88 70-130
Toluene-d8 100 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 8 of 40
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Shealy Environmental Services, Inc.

Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-1
RI02013-002
09/01/2016 1355
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1439 BNW 09/07/2016 1253 21415
1 7470A 7470A 1 09/06/2016 1717 COH 09/06/2016 1234 21320
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 68 J 1ug/L0.53100
Cadmium 7440-43-9 6020A 0.065 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 3.1 J 1ug/L0.6310
Lead 7439-92-1 6020A 0.59 J 1ug/L0.1510
Mercury 7439-97-6 7470A 0.0010 U 1mg/L0.0000280.0010
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 9 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-2
RI02013-003
09/01/2016 1345
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0414 ECP 21411
2 5030B 8260B 1 09/08/2016 0412 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 10 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-2
RI02013-003
09/01/2016 1345
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0414 ECP 21411
2 5030B 8260B 1 09/08/2016 0412 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 99 70-130 100 70-130
1,2-Dichloroethane-d4 108 70-130 87 70-130
Toluene-d8 104 70-130 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 11 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-2
RI02013-003
09/01/2016 1345
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1444 BNW 09/07/2016 1253 21415
1 7470A 7470A 1 09/06/2016 1725 COH 09/06/2016 1234 21320
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 66 J 1ug/L0.53100
Cadmium 7440-43-9 6020A 0.23 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 3.2 J 1ug/L0.6310
Lead 7439-92-1 6020A 0.94 J 1ug/L0.1510
Mercury 7439-97-6 7470A 0.0010 U 1mg/L0.0000280.0010
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 12 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-3
RI02013-004
09/01/2016 1335
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0437 ECP 21411
2 5030B 8260B 1 09/08/2016 0435 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.51 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 13 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-3
RI02013-004
09/01/2016 1335
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0437 ECP 21411
2 5030B 8260B 1 09/08/2016 0435 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 1.2 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 97 70-130
1,2-Dichloroethane-d4 106 70-130 86 70-130
Toluene-d8 103 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 14 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-3
RI02013-004
09/01/2016 1335
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1450 BNW 09/07/2016 1253 21415
1 7470A 7470A 1 09/06/2016 1728 COH 09/06/2016 1234 21320
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 82 J 1ug/L0.53100
Cadmium 7440-43-9 6020A 0.078 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Lead 7439-92-1 6020A 2.6 J 1ug/L0.1510
Mercury 7439-97-6 7470A 0.0014 1mg/L0.0000280.0010
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 15 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02013-005
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0501 ECP 21411
2 5030B 8260B 1 09/08/2016 0458 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.54 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 16 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02013-005
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0501 ECP 21411
2 5030B 8260B 1 09/08/2016 0458 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 1.1 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 104 70-130 100 70-130
1,2-Dichloroethane-d4 105 70-130 90 70-130
Toluene-d8 102 70-130 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 17 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
RI02013-005
09/01/2016 0800
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1456 BNW 09/07/2016 1253 21415
1 7470A 7470A 1 09/06/2016 1731 COH 09/06/2016 1234 21320
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 80 J 1ug/L0.53100
Cadmium 7440-43-9 6020A 0.069 J 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Lead 7439-92-1 6020A 2.3 J 1ug/L0.1510
Mercury 7439-97-6 7470A 0.0013 1mg/L0.0000280.0010
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 18 of 40
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
RI02013-006
09/01/2016 1410
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0128 ECP 21411
2 5030B 8260B 1 09/08/2016 0521 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 5.1 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 6.4 J 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 19 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
RI02013-006
09/01/2016 1410
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0128 ECP 21411
2 5030B 8260B 1 09/08/2016 0521 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 97 70-130
1,2-Dichloroethane-d4 106 70-130 87 70-130
Toluene-d8 101 70-130 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 20 of 40
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Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
RI02013-006
09/01/2016 1410
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020A 1 09/08/2016 1501 BNW 09/07/2016 1253 21415
1 7470A 7470A 1 09/06/2016 1734 COH 09/06/2016 1234 21320
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020A 10 U 1ug/L0.2610
Barium 7440-39-3 6020A 100 U 1ug/L0.53100
Cadmium 7440-43-9 6020A 1.0 U 1ug/L0.0441.0
Chromium 7440-47-3 6020A 10 U 1ug/L0.6310
Lead 7439-92-1 6020A 10 U 1ug/L0.1510
Mercury 7439-97-6 7470A 0.0010 U 1mg/L0.0000280.0010
Selenium 7782-49-2 6020A 10 U 1ug/L0.9510
Silver 7440-22-4 6020A 10 U 1ug/L0.1710
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 21 of 40
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK
RI02013-007
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0152 ECP 21411
2 5030B 8260B 1 09/08/2016 0544 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 UH 2ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 22 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK
RI02013-007
09/01/2016
09/02/2016
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/07/2016 0152 ECP 21411
2 5030B 8260B 1 09/08/2016 0544 ECP 21511
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 97 70-130 H 101 70-130
1,2-Dichloroethane-d4 107 70-130 H 88 70-130
Toluene-d8 102 70-130 H 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 23 of 40
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QC Summary
Page: 24 of 40
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21411-001
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 09/06/2016 2159U102.0 ug/L1
Acrylonitrile 5.0 09/06/2016 2159U5.0 0.80 ug/L1
Benzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromochloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromodichloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromoform 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 09/06/2016 2159U0.50 0.40 ug/L1
2-Butanone (MEK)10 09/06/2016 2159U102.0 ug/L1
Carbon disulfide 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloroform 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dibromochloromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 09/06/2016 2159U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,4-Dichlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Ethylbenzene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
2-Hexanone 10 09/06/2016 2159U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 09/06/2016 2159U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 09/06/2016 2159U102.0 ug/L1
Methylene chloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Styrene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Tetrachloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Tetrahydrofuran 5.0 09/06/2016 2159U5.0 1.0 ug/L1
Toluene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Trichloroethene 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
1,2,3-Trichloropropane 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 40
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21411-001
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Vinyl acetate 5.0 09/06/2016 2159U5.0 1.2 ug/L1
Vinyl chloride 0.50 09/06/2016 2159U0.50 0.40 ug/L1
Xylenes (total)1.0 09/06/2016 2159U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 40
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21411-002
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 95 09/06/2016 20579510060-1401
Acrylonitrile 93 09/06/2016 20579310060-1401
Benzene 47 09/06/2016 2057935070-1301
Bromochloromethane 50 09/06/2016 20571005070-1301
Bromodichloromethane 49 09/06/2016 2057985070-1301
Bromoform 46 09/06/2016 2057925070-1301
Bromomethane (Methyl bromide)55 09/06/2016 20571115060-1401
2-Butanone (MEK)95 09/06/2016 20579510060-1401
Carbon disulfide 50 09/06/2016 20571005060-1401
Carbon tetrachloride 51 09/06/2016 20571025070-1301
Chlorobenzene 46 09/06/2016 2057925070-1301
Chloroethane 56 09/06/2016 20571135060-1401
Chloroform 47 09/06/2016 2057935070-1301
Chloromethane (Methyl chloride)51 09/06/2016 20571025050-1301
1,2-Dibromo-3-chloropropane (DBCP)46 09/06/2016 2057915070-1301
Dibromochloromethane 47 09/06/2016 2057945070-1301
1,2-Dibromoethane (EDB)45 09/06/2016 2057905070-1301
Dibromomethane (Methylene bromide)47 09/06/2016 2057945070-1301
1,4-Dichlorobenzene 44 09/06/2016 2057885070-1301
1,2-Dichlorobenzene 46 09/06/2016 2057925070-1301
1,2-Dichloroethane 47 09/06/2016 2057945070-1301
1,1-Dichloroethane 49 09/06/2016 2057985070-1301
cis-1,2-Dichloroethene 48 09/06/2016 2057975070-1301
1,1-Dichloroethene 50 09/06/2016 2057995070-1301
trans-1,2-Dichloroethene 51 09/06/2016 20571025070-1301
1,2-Dichloropropane 49 09/06/2016 2057975070-1301
cis-1,3-Dichloropropene 47 09/06/2016 2057945070-1301
trans-1,3-Dichloropropene 45 09/06/2016 2057895070-1301
Ethylbenzene 48 09/06/2016 2057965070-1301
2-Hexanone 96 09/06/2016 20579610060-1401
Methyl iodide (Iodomethane)49 09/06/2016 2057975070-1301
4-Methyl-2-pentanone 98 09/06/2016 20579810060-1401
Methylene chloride 45 09/06/2016 2057905070-1301
Styrene 49 09/06/2016 2057995070-1301
1,1,2,2-Tetrachloroethane 45 09/06/2016 2057915070-1301
1,1,1,2-Tetrachloroethane 48 09/06/2016 2057965070-1301
Tetrachloroethene 48 09/06/2016 2057965070-1301
Tetrahydrofuran 47 09/06/2016 2057935070-1301
Toluene 46 09/06/2016 2057925070-1301
1,1,2-Trichloroethane 46 09/06/2016 2057935070-1301
1,1,1-Trichloroethane 48 09/06/2016 2057965070-1301
Trichloroethene 49 09/06/2016 2057985070-1301
Trichlorofluoromethane 60 09/06/2016 20571195060-1401
1,2,3-Trichloropropane 46 09/06/2016 2057935070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 40
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21411-002
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Vinyl acetate 51 09/06/2016 20571025060-1401
Vinyl chloride 50 09/06/2016 20571015060-1401
Xylenes (total)97 09/06/2016 20579710070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 28 of 40
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21411-003
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Acetone 99 09/07/2016 06359910060-1404.5 201
Acrylonitrile 95 09/07/2016 06359510060-1402.0 401
Benzene 47 09/07/2016 0635945070-1301.3 201
Bromochloromethane 51 09/07/2016 06351025070-1301.8 201
Bromodichloromethane 50 09/07/2016 06351005070-1302.3 201
Bromoform 45 09/07/2016 0635905070-1302.3 201
Bromomethane (Methyl bromide)56 09/07/2016 06351135060-1402.0 201
2-Butanone (MEK)98 09/07/2016 06359810060-1403.5 201
Carbon disulfide 52 09/07/2016 06351045060-1404.3 201
Carbon tetrachloride 52 09/07/2016 06351045070-1302.5 201
Chlorobenzene 47 09/07/2016 0635945070-1302.3 201
Chloroethane 57 09/07/2016 06351145060-1401.3 201
Chloroform 48 09/07/2016 0635965070-1302.6 201
Chloromethane (Methyl chloride)55 09/07/2016 06351115050-1308.1 201
1,2-Dibromo-3-chloropropane (DBCP)43 09/07/2016 0635875070-1304.9 201
Dibromochloromethane 47 09/07/2016 0635945070-1300.26 201
1,2-Dibromoethane (EDB)46 09/07/2016 0635925070-1301.9 201
Dibromomethane (Methylene bromide)49 09/07/2016 0635985070-1304.3 201
1,4-Dichlorobenzene 43 09/07/2016 0635875070-1301.7 201
1,2-Dichlorobenzene 46 09/07/2016 0635935070-1300.62 201
1,2-Dichloroethane 49 09/07/2016 0635985070-1304.8 201
1,1-Dichloroethane 51 09/07/2016 06351015070-1302.8 201
cis-1,2-Dichloroethene 50 09/07/2016 0635995070-1302.4 201
1,1-Dichloroethene 51 09/07/2016 06351015070-1302.4 201
trans-1,2-Dichloroethene 52 09/07/2016 06351045070-1302.2 201
1,2-Dichloropropane 49 09/07/2016 0635985070-1300.69 201
cis-1,3-Dichloropropene 46 09/07/2016 0635925070-1302.2 201
trans-1,3-Dichloropropene 44 09/07/2016 0635875070-1302.0 201
Ethylbenzene 48 09/07/2016 0635975070-1301.1 201
2-Hexanone 97 09/07/2016 06359710060-1400.77 201
Methyl iodide (Iodomethane)51 09/07/2016 06351015070-1304.2 201
4-Methyl-2-pentanone 100 09/07/2016 063510210060-1403.8 201
Methylene chloride 48 09/07/2016 0635965070-1305.6 201
Styrene 50 09/07/2016 06351005070-1301.3 201
1,1,2,2-Tetrachloroethane 45 09/07/2016 0635905070-1300.50 201
1,1,1,2-Tetrachloroethane 49 09/07/2016 0635985070-1302.7 201
Tetrachloroethene 47 09/07/2016 0635945070-1302.0 201
Tetrahydrofuran 50 09/07/2016 06351015070-1307.9 201
Toluene 46 09/07/2016 0635915070-1300.54 201
1,1,2-Trichloroethane 47 09/07/2016 0635955070-1302.3 201
1,1,1-Trichloroethane 50 09/07/2016 0635995070-1303.1 201
Trichloroethene 50 09/07/2016 06351005070-1302.1 201
Trichlorofluoromethane 61 09/07/2016 06351225060-1402.0 201
1,2,3-Trichloropropane 46 09/07/2016 0635935070-1300.18 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 29 of 40
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:RQ21411-003
21411 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Vinyl acetate 48 09/07/2016 0635975060-1405.1 201
Vinyl chloride 52 09/07/2016 06351055060-1404.1 201
Xylenes (total)98 09/07/2016 06359810070-1300.82 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 101 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 30 of 40
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:RQ21511-001
21511 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
trans-1,4-Dichloro-2-butene 2.0 09/07/2016 2222U2.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 83 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 31 of 40
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:RQ21511-002
21511 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 47 09/07/2016 2131955034-1421
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 82 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 32 of 40
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Shealy Environmental Services, Inc.

Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21415-001
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Arsenic 10 09/08/2016 1218U100.26 ug/L1
Barium 100 09/08/2016 1218U1000.53 ug/L1
Cadmium 1.0 09/08/2016 1218U1.0 0.044 ug/L1
Chromium 10 09/08/2016 1218U100.63 ug/L1
Lead 10 09/08/2016 1218U100.15 ug/L1
Selenium 10 09/08/2016 1218U100.95 ug/L1
Silver 10 09/08/2016 1218U100.17 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 33 of 40
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Shealy Environmental Services, Inc.

Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21415-002
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Arsenic 94 09/08/2016 12249410080-1201
Barium 95 09/08/2016 12249510080-1201
Cadmium 94 09/08/2016 12249410080-1201
Chromium 100 09/08/2016 122410110080-1201
Lead 100 09/08/2016 122410310080-1201
Selenium 95 09/08/2016 12249510080-1201
Silver 100 09/08/2016 122410410080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 34 of 40
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Shealy Environmental Services, Inc.

Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:RI02013-001MS
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Arsenic 89 09/08/2016 14058910075-1300.0 1
Barium 150 09/08/2016 140510110075-125531
Cadmium 96 09/08/2016 14059610075-1250.061 1
Chromium 100 09/08/2016 140510210075-1251.2 1
Lead 110 09/08/2016 140510810075-1252.3 1
Selenium 85 09/08/2016 14058510075-1250.0 1
Silver 100 09/08/2016 140510210075-1250.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 35 of 40
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Shealy Environmental Services, Inc.

Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:RI02013-001MD
21415 3005A
09/07/2016 1253Analytical Method:6020A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Arsenic 89 09/08/2016 14118910075-1300.41 200.0 1
Barium 150 09/08/2016 141110010075-1251.1 20531
Cadmium 94 09/08/2016 14119410075-1251.5 200.061 1
Chromium 100 09/08/2016 141110110075-1250.59 201.2 1
Lead 110 09/08/2016 141110710075-1251.2 202.3 1
Selenium 86 09/08/2016 14118610075-1250.87 200.0 1
Silver 100 09/08/2016 141110210075-1250.59 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 36 of 40
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Shealy Environmental Services, Inc.

Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:RQ21320-001
21320 7470A
09/06/2016 1234Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Mercury 0.000047 09/06/2016 1624J0.0010 0.000028 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 37 of 40
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Shealy Environmental Services, Inc.

Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:RQ21320-002
21320 7470A
09/06/2016 1234Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Mercury 0.0022 09/06/2016 16261080.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 38 of 40
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Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
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SHEALY ENVIRONMENTAL SERVICES, INC.

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SHEALY ENVIRONMENTAL SERVICES, INC.

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cdmsmith.com