7803_RobesonCoMSW_Nov2016_2ndSemiAnnual_DIN28078_20170131

Robeson County Landfill
Water Quality Monitoring Report

November 2016 Semi-Annual Event

Prepared on Behalf of:

Robeson County Landfill
246 Landfill Rd
Lumberton, North Carolina 28360

Facility Permit No. 78-03

Dated:

January 31, 2017

Prepared by:

1730 Rennert Rd.
Lumberton NC, 28360

TRANSMITTAL LETTER

January 26, 2017

Mrs. Elizabeth Werner
Hydrogeologist
North Carolina Department of Environment and Natural Resources
Division of Waste Management - Solid Waste Section
217 W Jones St, Raleigh, North Carolina 27603

Subject: Robeson County Landfill Water Quality Monitoring Report
November 2016 Semi-Annual Event
Robeson County Landfill
St. Pauls, Robeson County, North Carolina

To: Mrs. Werner

Hunt Environmental Associates, PLLC has prepared this November 2016 Semi-Annual Water
Quality Monitoring Report for the Robeson County Landfill. This report summarizes the
findings of sampling data gathered at the site. The scope of work at the site was executed in
order to fulfill the NCDENR Solid Waste Section reporting requirements for environmental
monitoring

We appreciate your consideration and review following the submission of this report. If you
have- any questions concerning this report, please don’t hesitate to contact us at [phone].

Respectfully Submitted,

______________________
Michael Cody Hunt, P.G., M.S.
Project Geologist

Table of Contents
1.0 INTRODUCTION ............................................................................................................... 1
2.0 SITE BACKGROUND AND MONITORING NETWORK .............................................. 1
3.0 SITE HYDROGEOLOGY ................................................................................................... 1
4.0 FIELD ACTIVITIES ........................................................................................................... 2
5.0 ANALYTICAL RESULTS ................................................................................................. 2
5.1 Groundwater ..................................................................................................................... 2
5.2 Surface Water ................................................................................................................... 5
5.3 Leachate ........................................................................................................................... 5
6.0 STATISTICAL PROCEDURES ......................................................................................... 5
6.1 STATISTICAL RESULTS SUMMARY......................................................................... 6
7.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................. 6

Figures

Figure 1: Groundwater Potentiometric Map

Tables

Table 1: Groundwater Monitoring Program
Table 2: Ground Water Elevations & Flow Velocities
Table 3: Analytical Results
Table 4: Statistical Analysis Summary

Appendices

Appendix A: Laboratory Analytical Results
Appendix B: Time Series Graphs
Appendix C: Non-Parametric Prediction Interval Inter-Well Comparisons

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1.0 INTRODUCTION

The Robeson County Landfill, operating under North Carolina Department of Environment and
Natural Resources (NCDENR) Solid Waste Permit #78-03, is required to submit semi-annual
groundwater monitoring reports for detection monitoring of the Phase 2, Phase 3, and Phase 4
lined landfills and assessment monitoring of the Phase 1 unlined landfill. This report presents
the results of the first semi-annual monitoring event for 2016, conducted in March of 2016. Also
included in this report are the results of the surface water and leachate monitoring that was
performed in conjunction with the groundwater monitoring event.

The Robeson County Landfill is currently accepting construction and demolition debris (C&D)
waste over the closed Phase 1 Municipal Solid Waste (MSW) unlined landfill. Currently, all
MSW is being disposed in the Phase 4 lined landfill. The Phase 1 unlined landfill has been
closed per NCDENR Solid Waste Regulations, and the C&D disposal will bring the landfill to
final closure contours.
2.0 SITE BACKGROUND AND MONITORING NETWORK

Currently twenty-nine groundwater monitoring wells are located around the perimeter of the
Phase 1, Phase 2, Phase 3, Phase 4 and C&D landfill cells (Figure 1). Table 1 lists the currently
monitored wells associated with each Phase of the landfill. Twenty-two groundwater monitoring
wells were monitored during this sampling event. Seven monitoring wells have been damaged
and were approved for closure by NCDENR Solid Waste Section correspondence from Ms.
Werner on March 22 of 2011, three wells were approved for closure and replacement on January
3, 2013 and therefore, none of them were sampled for this event.

Two surface water samples (SW-1 & SW-2) were collected as shown in Figure 1. Leachate
samples were also collected during this monitoring event for Phases 2, 3, and 4. Phase 2 and 3
leachate samples were collected from the respective line valves linked to the generator. The
Phase 4 leachate sample was collected from the line pump station.

This report includes summaries of the field procedures, and field, laboratory, and statistical
results from the November 2016 semi-annual groundwater sampling event. Field and laboratory
results of the surface water and leachate sampling are also presented. Summary tables of the
monitoring network, groundwater characteristics, field measurements, laboratory and statistical
analysis results, as well as graphs of groundwater analytical data over time are included at the
end of the report.
3.0 SITE HYDROGEOLOGY

The site is located in the Coastal Plain Physiographic province within the Cretaceous-age Black
Creek Formation. In general, the lithology of the site is composed of sandy soils with clay. As a
result, the direction of groundwater flow should be largely controlled by site topography.

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Figure 1 provides potentiometric surface maps and groundwater flow calculations for the
shallow aquifer utilizing groundwater level data from the Second Semi-Annual 2016 event.
Groundwater flow direction for the Second Semi-Annual 2016 event was to the southeast
towards the Big Marsh Swamp, consistent with past events. Groundwater velocity for the Second
Semi-Annual 2016 event was calculated utilizing Darcy’s law: V = Ki/n, where K = hydraulic
conductivity, i = groundwater gradient, n = porosity. Based on the fall dataset, groundwater
velocities are estimated to range from 0.18 feet/year (MW-24) to 91.39 feet/year (MW-9a).
4.0 FIELD ACTIVITIES

Groundwater, surface water, and leachate samples from the Robeson County Landfill were
collected on November 30 and December 1, 2016. Twenty two (22) groundwater samples were
collected by use of a disposable, laboratory decontaminated polyethylene bailer. Sampling
locations are presented on Figure 1. Groundwater elevations were measured at each well prior to
sampling and are presented in Table 2. These groundwater elevations were used to construct the
potentiometric contours for this sampling event as shown on Figure 1. The groundwater
elevations and potentiometric contours were used to estimate groundwater velocities at each well
presented in Table 2. After depth to groundwater was measured, water was purged from each
well to provide fresh formation water within the well water column prior to sampling. All
samples were collected in clean laboratory prepared containers for the specified analytical
methods. Groundwater samples were properly preserved, placed on ice, and transported to the
laboratory via overnight delivery. The samples were transported to ESC Lab Sciences Inc., a
North Carolina certified laboratory (NC DW #21704). Laboratory analyses consisted of those
noted in Table 1 and were reported according to the laboratory’s Method Detection Limits
(MDLs). The laboratory analytical reports are included in Appendix A.

Trip and equipment blanks were used for quality assurance/quality control (QA/QC). Trip blanks
were prepared by the laboratory and accompanied the coolers during the sampling event. One
equipment blank was prepared by pouring distilled water over a bailer and collecting the water in
containers provided by the laboratory. Sampling methods followed the protocol outlined in
NCDENR’s Guidelines for Groundwater, Soil, and Surface Water Sampling (NCDENR 2008)
and in accordance with the approved Sampling and Analysis Plan (Water Quality Monitoring
Plan, David Garrett and Associates, Raleigh, NC, 2009).
5.0 ANALYTICAL RESULTS
5.1 Groundwater

ESC Lab Sciences, Inc. located in Lebanon, Tennessee analyzed samples for the North Carolina
Appendix I volatile organic compounds (VOCs) and metals. In accordance with SWS guidelines
the analytical results were reported to the laboratory specific method detection limit (MDL) and
are quantifiable at or below Solid Waste Section Limits (SWSLs). The following list indicates
which analytes were detected above the SWSL at each sampling location. Underlined analytes
exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the
North Carolina Surface Water Standards for Class C Waters. A complete summary of all

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detected and estimated concentrations for this sampling event is presented in Table 3. Copies of
the laboratory analytical data reports are provided in Appendix A.

MW-3R
Volatile Organic Compounds: None Detected
Metals: Chromium, Vanadium, Selenium

MW-5
Volatile Organic Compounds: 1,4-Dichlorobenzene
Metals: None Detected

MW-6
Volatile Organic Compounds: None Detected
Metals: None Detected

MW-8
Volatile Organic Compounds: 1,4-Dichlorobenzene,
Metals: None Detected

MW-9A
Volatile Organic Compounds: 1,4-Dichlorobenzene, 1,1-Dichloroethane, Benzene
Metals: None Detected
MW-10
Volatile Organic Compounds: None Detected
Metals: Chromium, Zinc

MW-11
Volatile Organic Compounds: None Detected
Metals: Zinc

MW-12
Volatile Organic Compounds: None Detected
Metals: None Detected

MW-13R
Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene
Metals: Barium

MW-14
Volatile Organic Compounds: None Detected
Metals: Barium

MW-15
Volatile Organic Compounds: Acetone, Benzene, 1,4-Dichlorobenzene,
Metals: None Detected

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MW-16
Volatile Organic Compounds: Benzene, Chloroethane, 1,4-Dichlorobenzene
Metals: Barium, Arsenic

MW-17R
Volatile Organic Compounds: Tetrachloroethene, Trichloroethene
Metals: Barium, Chromium, Cobalt

MW-18
Volatile Organic Compounds: None Detected
Metals: Barium

MW-19
Volatile Organic Compounds: None Detected
Metals: Barium, Chromium, Vanadium, Copper, Lead, Zinc,
Arsenic

MW-20
Volatile Organic Compounds: None Detected
Metals: Barium, Lead

MW-21R
Volatile Organic Compounds: None Detected
Metals: Cobalt

MW-22
Volatile Organic Compounds: None Detected
Metals: None Detected

MW-23
Volatile Organic Compounds: None Detected
Metals: None Detected

MW-24R
Volatile Organic Compounds: None Detected
Metals: None Detected

MW-25R
Volatile Organic Compounds: None Detected
Metals: None Detected

MW-26
Volatile Organic Compounds: None Detected
Metals: None Detected

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5.2 Surface Water

HEA personnel sampled two surface water bodies in the vicinity of the Phase 1, 2, 3 and Phase 4
landfills (Figure 1). Surface water sampling point SW-1 is located below the outflow from the
existing sediment basin southwest of the Phase 1 cell. Surface water sampling point SW-2 is
located in a drainage ditch, southeast of the Phase 2 cell. The following list indicates which
analytes were detected above the SWSL at each sampling location. Underlined analytes
exceeded the North Carolina 2L Standard (NC 2L), the Groundwater Protection Standard, or the
North Carolina Surface Water Standards for Class C Waters.

SW-1
Volatile Organic Compounds: None Detected
Metals: Barium

SW-2
During the Second Semi-Annual sampling event this pond was dry therefore we did not
conduct a sampling.
5.3 Leachate

HEA personnel sampled three leachate drainage lines in the vicinity of the Phase 2, 3 and 4
landfill cells. Two leachate sampling locations are east of the Phase 2 and 3 cells; one is located
east of the Phase 4 cell. Analytical results are presented in Table 3.
6.0 STATISTICAL PROCEDURES

The laboratory data from the sampling event were reviewed and analyzed by HEA in order to
evaluate trends and changes in the results and to identify statistically significant differences
between compliance and background wells. Data entry and analysis were performed using the
Chemstat statistical software package developed by Starpoint Software, Cincinnati, OH.
Chemstat follows the EPA document, Statistical Analysis of Ground-Water Monitoring Data at
RCRA Facilities – Unified Guidance (March 2009), as well as NCDENR guidelines.

The data were reviewed to evaluate the most appropriate analysis methods. Initial analysis
consisted of a basic review of the data and of the time vs. concentration graphs (included in
Appendix B) to determine any major changes or trends in the data. Individual compliance well
historical means were compared to the pooled background historical means for MW-6 and MW-
12 to determine if detected constituents were statistically significantly different from general
background groundwater quality.

The statistical analysis results are summarized in Table 4 and provided in Appendix C.

6 | P a g e
6.1 STATISTICAL RESULTS SUMMARY

For the Second Semi-Annual 2016 event, statistically significant differences from background
concentrations and above SWSLs, shown in Table 4, were found for VOCs and Metals as
detailed below:

VOCs

 1,4-Dichlorobenzene – MW-9A, MW-15
 1,1-Dichloroethane – MW-9A
 Acetone – MW-15
 Chloroethane – MW-16

Metals

 Arsenic – MW-16
 Chromium – MW-3R MW-10, MW -17R
 Cobalt – MW-17R, MW-21R
 Selenium – MW-3R,
7.0 CONCLUSIONS AND RECOMMENDATIONS

For the Second Semi-Annual 2016 groundwater monitoring event, concentrations that were
detected above an NC SWSL and NC GWPS/NC 2L were also determined to statistically exceed
the background concentrations. Based on the statistical evaluations:

No groundwater detections were identified as statistically significant increases for the Second
Semi-Annual 2016 event.

The following groundwater detections were identified appearing to decrease site wide:

 Acetone
 Cadmium

The following groundwater detections were identified appearing to remain relatively constant
site wide:

 1,4-Dichlorobenzene
 1,1-Dichloroethane
 Arsenic
 Chromium
 Zinc
 Cobalt
 Selenium
 Benzene

7 | P a g e
During the Second Semi-Annual 2016 event, one Appendix I VOCs and two Appendix I
inorganic constituents were detected in surface water samples at quantified concentrations above
their respective NC SWSLs at SW-2: Acetone, Barium, and Zinc. These constituents do not have
a NC 2B Surface Water Standard established for swamp waters (status of discharge locations).

The site will continue monitoring in accordance with the requirements for Detection Monitoring
as outlined in Title 15A NCAC 13B .1633. The next semi-annual event is tentatively scheduled
for 2017.

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FIGURES

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TABLES

Location Phase Gradient Current Use Zone
Monitored
Laboratory
Analysis
MW-1 Phase 1 Up Background Shallow N/A
MW-2 Phase 1 Down Compliance Shallow N/A
MW-3r Phase 1 Down Compliance Shallow Appendix I +
MW-4a Phase 1 Up Background Shallow N/A
MW-5 Phase 1 Down Compliance Shallow Appendix I +
MW-5a Phase 1 Down Compliance Deep N/A
MW-6 Phase 1 Up Background Shallow Appendix I +
MW-7 Phase 1 Cross Compliance Shallow N/A
MW-8 Phase 1 Down Compliance Shallow Appendix I +
MW-9 Phase 1 Down Compliance Shallow N/A
MW-9a Phase 1 Down Compliance Shallow Appendix I +
MW-9b Phase 1 Down Compliance Deep N/A
MW-10 Phase 1 Down Compliance Shallow Appendix I
MW-11 Phase 1 Down Compliance Shallow Appendix I
MW-12 Phase 2 Up Background Shallow Appendix I
MW-13r Phase 2 Down Compliance Shallow Appendix I
MW-14 Phase 2 Down Compliance Shallow Appendix I
MW-15 Phase 2 Down Compliance Shallow Appendix I
MW-16 Phase 2 Down Compliance Shallow Appendix I
MW-17r Phase 2 Down Compliance Shallow Appendix I
MW-18 Phase 2 Down Compliance Shallow Appendix I
MW-19 C & D Down Not used Shallow Metals & VOC
MW-20 C & D Down Not used Shallow Metals & VOC
MW-21 Phase 3 Down Compliance Shallow Appendix I
MW-22 Phase 3 Down Compliance Shallow Appendix I
MW-23 Phase 3 Cross Compliance Shallow Appendix I
MW-24R Phase 4 Cross Compliance Shallow Appendix I
MW-25R Phase 4 Down Compliance Shallow Appendix I
MW-26 Phase 4 Up Compliance Shallow Appendix I
Notes:
Appendix 1 = Appendix I constituents were analyzed.
N/A = Not Analyzed
Table 1
Groundwater Monitoring Program
Monitoring wells MW-1, MW-2, MW-4a, MW-5a, MW-7, MW-9, and MW-9b
were not analyzed per GNRA's request approved by NCDENR on July 14, 2000.
Appendix 1 + = Appendix I plus previously detected Appendix II constituents
were analyzed.
Well TOC Elevation
(ft)
DTW
(ft)
WTE
(ft)
Hyd
Cond*
Porosity**
(%)
Gradient**
* (ft/ft)
Velocity****
(ft/day)(ft/year)
MW-1 151.14 nm NA 0.877 0.18 0.005 NA NA
MW-2 136.53 nm NA 0.822 0.16 0.005 NA NA
MW-4a 153.02 nm NA 0.959 0.18 0.005 NA NA
MW-7 155.89 nm NA 0.493 0.16 0.005 NA NA
MW-9 131.18 nm NA 0.466 0.20 0.005 NA NA
MW-9a 131.60 4.31 127.29 9.589 0.18 0.005 0.250 91.39
MW-16 149.64 15.80 133.84 8.506 0.18 0.005 0.222 81.07
MW-20 139.88 8.37 131.51 7.140 0.18 0.005 0.186 68.05
MW-8 131.01 4.81 126.20 5.479 0.20 0.005 0.129 47.00
MW-6 150.73 9.15 141.58 2.000 0.15 0.005 0.063 22.87
MW-12 157.79 16.45 141.34 2.041 0.18 0.005 0.053 19.45
MW-11 135.30 6.55 128.75 0.874 0.16 0.005 0.026 9.37
MW-10 133.33 5.25 128.08 0.603 0.18 0.005 0.016 5.75
MW-17r 150.31 12.35 137.96 0.257 0.15 0.005 0.008 2.94
MW-14 156.11 19.16 136.95 0.271 0.18 0.005 0.007 2.58
MW-18 151.17 13.55 137.62 0.246 0.18 0.005 0.006 2.34
MW-13r 154.98 18.74 136.24 0.237 0.18 0.005 0.006 2.26
MW-15a 151.91 16.00 135.91 0.183 0.16 0.005 0.005 1.96
MW-3r 137.38 9.85 127.53 0.142 0.20 0.005 0.0033 1.22
MW-21 150.88 14.00 136.88 0.065 0.18 0.005 0.002 0.62
MW-22 152.28 15.62 136.66 0.057 0.18 0.005 0.001 0.54
MW-26 154.59 13.61 140.98 0.05 0.18 0.005 0.00131 0.48
MW-5 130.50 3.48 127.02 0.036 0.18 0.005 0.0009 0.34
MW-23 151.75 12.31 139.44 0.028 0.18 0.005 0.001 0.27
MW- 154.25 15.85 138.40 0.025 0.18 0.005 0.00065 0.24
MW-19 146.95 14.88 132.07 0.020 0.18 0.005 0.001 0.19
MW-24 154.58 13.58 141.00 0.019 0.18 0.005 0.00049 0.18

Notes TOC = Top of casing elevation NA = not available
DTW = Depth to Water from TOC nm = not measured
WTE = Water Table Elevation ft = feet
Hyd Cond = Hydraulic Conductivity % = percent
* Hydraulic Conductivity values from previous slug tests
** Effective Porosity from Groundwater & Wells (Driscoll, 1986)
***Average gradient for the October 2011 sampling event
****Velocity calculated by HEA using V=KI/n where
V = Ground water velocity
K = Hydraulic conductivity
I = Ground water gradient
n = Effective porosity
Table 2
Ground Water Elevations & Flow Velocities
M
W
-
3
R
M
W
-
5
M
W
-
6
M
W
-
8
M
W
-
9
A
M
W
-
1
0
M
W
-
1
1
M
W
-
1
2
M
W
-
1
3
R
M
W
-
1
4
M
W
-
1
5
M
W
-
1
6
M
W
-
1
7
R
M
W
-
1
8
M
W
-
1
9
M
W
-
2
0
M
W
-
2
1
R
M
W
-
2
2
M
W
-
2
3
M
W
-
2
4
R
M
W
-
2
5
R
M
W
-
2
6
S
W
-
1
S
W
-
2
L
E
A
C
H
A
T
E

P
H
A
S
E

2
L
E
A
C
H
A
T
E

P
H
A
S
E

3
L
E
A
C
H
A
T
E

P
H
A
S
E

4
Analyte Solid Waste
Selection Limits
Alkalinity BDL BDL NM
Dissolved Solids 570 61 NM
Phosphorus,Total NM 0.332 0.824 1.3
Cod NM 418 634 1420
Bod NM 15 17.9 69
Barium 0.1 0.0849 0.015 0.012 0.0621 0.0868 0.0532 0.0439 0.0927 0.159 0.181 0.0669 0.144 0.137 0.122 0.512 0.105 0.029 0.0612 0.0115 0.0362 0.0219 0.0401 0.109 NM 0.32 0.218 0.147
Chromium 0.01 0.0101 BDL BDL BDL BDL 0.0122 BDL BDL BDL BDL BDL BDL 0.0116 BDL 0.0962 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0149 0.0194 BDL
Cobalt 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.017 BDL BDL BDL 0.0112 BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Nickel 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0262 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0187 0.0574 0.132
Silver 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Vanadium 0.025 0.0253 BDL BDL BDL BDL 0.0215 BDL 0.0228 BDL BDL BDL BDL 0.0237 BDL 0.154 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0233 0.0401 BDL
Antimony 0.006 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Arsenic 0.01 0.0021 BDL BDL 0.0028 BDL BDL 0.0024 BDL BDL BDL 0.0025 0.0141 BDL BDL 0.0138 BDL 0.0034 BDL BDL BDL 0.0026 BDL 0.0027 NM 0.0196 0.0366 0.125
Beryllium 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Cadmium 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Copper 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0261 BDL 0.0065 BDL BDL BDL BDL BDL BDL NM 0.0597 1.49 BDL
Lead 0.01 0.0046 BDL BDL 0.0085 BDL 0.0076 0.0029 0.004 0.0034 BDL BDL BDL 0.0086 0.0034 0.0878 0.0102 0.0025 BDL BDL BDL BDL BDL BDL NM 0.0061 0.212 BDL
Selenium 0.01 0.0463 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0073 BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Thallium 0.0055 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Zinc 0.01 BDL BDL BDL BDL BDL 0.0274 0.0347 BDL BDL BDL BDL BDL BDL BDL 0.114 BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0401 0.369 BDL
Acetone 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.104 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Acrylonitrile 0.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Benzene 0.001 BDL BDL BDL BDL 0.0014 BDL BDL BDL 0.0019 BDL 0.0017 0.00145 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0069 0.0051 0.0096
Bromochloromethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Bromodichloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Bromoform 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Bromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Carbon Disulfide 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Carbon Tetrachloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Chlorobenzene 0.003 BDL 0.0018 BDL BDL 0.002 BDL BDL BDL BDL BDL 0.0029 0.00162 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.0023 0.0027 BDL
Chlorodibromomethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Chloroethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0105 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Chloroform 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Chloromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Dibromomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,2-Dichlorobenzene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,4-Dichlorobenzene 0.001 BDL 0.0050 BDL 0.0029 0.0095 BDL BDL BDL 0.0025 BDL 0.0081 0.002 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.016 0.0101 0.0038
Trans-1,4-Dichloro-2-Butene 0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Project Sample ID
Table 3
Analytical Results
1,1-Dichloroethane 0.005 0.0022 0.0036 BDL 0.0042 0.0104 BDL BDL BDL BDL BDL 0.003 0.00115 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,2-Dichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,1-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Cis-1,2-Dichloroethene 0.005 BDL 0.0017 BDL BDL 0.0016 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Trans-1,2-Dichloroethene 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,2-Dichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Cis-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Trans-1,3-Dichloropropene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Ethylbenzene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL 0.0061 0.009
2-Hexanone 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Iodomethane 0.01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
2-Butanone (Mek)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Methylene Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
4-Methyl-2-Pentanone (Mibk)0.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Styrene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,1,1,2-Tetrachloroethane 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,1,2,2-Tetrachloroethane 0.003 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Tetrachloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0012 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Toluene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,1,1-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,1,2-Trichloroethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Trichloroethene 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Trichlorofluoromethane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
1,2,3-Trichloropropane 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Vinyl Acetate 0.05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Vinyl Chloride 0.001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM BDL BDL BDL
Xylenes, Total 0.005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM 0.02 0.0381 0.0217
Chloride 9.61 5.23 NM
Nitrate 10 NM BDL 0.151 BDL
Sulfate 250 BDL 7.35 NM BDL 62.1 16.4
Notes:BDL = Below Detection Limit
* All units mg/L
NM - Not Measured / Well Dry at Time of Sampling
Location Parameter Detected
Concentration
Detection
Limit
Units %ND Test Statistically
Significant?
Above
2L/MCL
MW-3R Chromium 0.010 <0.0100 mg/L 0%NPPL Y Y
MW-3R Vanadium 0.025 <0.0200 mg/L 49.09%NPPL N Y
MW-3R Selenium 0.046 <0.00200 mg/L 56.20%NPPL Y Y
MW-5 1,4-Dichlorobenzene 0.0050 <0.00100 mg/L 58.86%NPPL N N
MW-8 1,4-Dichlorobenzene 0.003 <0.00100 mg/L 58.86%NPPL N N
MW-9A Benzene 0.001 <0.00100 mg/L 61.43%NPPL N Y
MW-9A 1,4-Dichlorobenzene 0.0095 <0.00100 mg/L 58.86%NPPL Y Y
MW-9A 1,1-Dichloroethane 0.010 <0.00100 mg/L 40.10%NPPL Y Y
MW-10 Chromium 0.012 <0.0100 mg/L 0%NPPL Y Y
MW-10 Zinc 0.027 <0.0250 mg/L 42.86%NPPL N N
MW-11 Zinc 0.035 <0.0250 mg/L 42.86%NPPL N N
MW-12 Barium 0.11 <0.00500 mg/L 49.61%NPPL N N
MW-13R Barium 0.159 <0.00500 mg/L 49.61%NPPL N N
MW-13R Benzene 0.00189 <0.00100 mg/L 61.43%NPPL N Y
MW-13R 1,4-Dichlorobenzene 0.002 <0.00100 mg/L 58.86%NPPL N N
MW-14 Barium 0.181 <0.00500 mg/L 49.61%NPPL N N
MW-15 Benzene 0.002 <0.00100 mg/L 61.43%NPPL N Y
MW-15 Acetone 0.104 <0.05 mg/L 67.02%NPPL Y N
MW-15 1,4-Dichlorobenzene 0.008 <0.00100 mg/L 58.86%NPPL Y Y
MW-16 Barium 0.144 <0.00500 mg/L 49.61%NPPL N N
MW-16 Benzene 0.001 <0.0100 mg/L 61.43%NPPL N Y
MW-16 Arsenic 0.014 <0.002 mg/L 52.26%NPPL Y Y
MW-16 Chloroethane 0.011 <0.005 mg/L 54.07%NPPL Y N
MW-16 1,4-Dichlorobenzene 0.002 <0.00100 mg/L 58.86%NPPL N N
MW-17R Barium 0.137 <0.00500 mg/L 49.61%NPPL N N
MW-17R Chromium 0.012 <0.0100 mg/L 0%NPPL Y Y
MW-17R Cobalt 0.017 <0.0100 mg/L 52.84%NPPL Y Y
MW-17R Tetrachloroethene 0.001 <0.00100 mg/L 43.13%NPPL N N
MW-17R Trichloroethene 0.001 <0.00100 mg/L 66.08%NPPL N N
MW-18 Barium 0.122 <0.00500 mg/L 49.61%NPPL N N
MW-19 Barium 0.512 <0.00500 mg/L 49.61%NPPL N N
MW-19 Chromium 0.096 <0.0100 mg/L 0%NPPL N Y
MW-19 Vanadium 0.154 <0.0200 mg/L 49.09%NPPL N Y
MW-19 Arsenic 0.014 <0.002 mg/L 52.26%NPPL N Y
MW-19 Copper 0.026 <0.005 mg/L 52.34%NPPL N N
MW-19 Lead 0.088 <0.00200 mg/L 46.04%NPPL N Y
MW-19 Zinc 0.114 <0.0250 mg/L 42.86%NPPL N N
MW-20 Barium 0.105 <0.00500 mg/L 49.61%NPPL N N
MW-20 Lead 0.010 <0.00200 mg/L 46.04%NPPL N N
MW-21R Cobalt 0.011 <0.0100 mg/L 52.84%NPPL Y Y
Notes:
MW-1 (historical data only), MW-6 and MW-12 were used as background wells. Wells not listed did not have any detected constituents.
% ND = percent non-detect
NPPL = Non-Parametric Prediction Limit (Inter-Well)
mg/L = milligrams per Liter
NA = Not available
Table 4
Statistical Analysis Summary

APPENDIX A: LABORATORY ANALYTIC
RESULTS
ANALYTICAL REPORT
December 09, 2016
Hunt Environmental Associates
Sample Delivery Group:L875822
Samples Received:12/02/2016
Project Number:14-011550
Description:Robeson Co Solid Waste Semi-Annual Env Monitoring
Report To:Cody Hunt
1730 Rennert Road
Lumberton, NC 28360
Entire Report Reviewed By:
December 09, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
December 12, 2016
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 4
⁴Cn: Case Narrative 10
⁵Sr: Sample Results 11
MW-3R L875822-01 11
MW-5 L875822-02 13
MW-8 L875822-03 15
MW-9A L875822-04 17
MW-12 L875822-05 19
MW-13R L875822-06 21
MW-14 L875822-07 23
MW-15 L875822-08 25
MW-16 L875822-09 27
MW-17R L875822-10 29
MW-18 L875822-11 31
MW-19 L875822-12 33
MW-21R L875822-13 35
MW-22 L875822-14 37
MW-23 L875822-15 39
MW-24R L875822-16 41
MW-25R L875822-17 43
SW-1 L875822-18 45
TRIP BLANK L875822-19 47
LEACHATE PHASE 2 L875822-20 48
LEACHATE PHASE 3 L875822-21 50
LEACHATE PHASE 4 L875822-22 52
MW-10 L875822-23 54
MW-11 L875822-24 56
MW-20 L875822-25 58
MW-26 L875822-26 60
TRIP BLANK L875822-27 62
MW-6 L875822-28 63
⁶Qc: Quality Control Summary 65
Gravimetric Analysis by Method 2540 C-2011 65
Wet Chemistry by Method 2320 B-2011 67
Wet Chemistry by Method 365.4 69
Wet Chemistry by Method 410.4 70
Wet Chemistry by Method 5210 B-2011 71
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Wet Chemistry by Method 9056A 73
Metals (ICP) by Method 6010C 78
Metals (ICPMS) by Method 6020 81
Volatile Organic Compounds (GC/MS) by Method 8260B 86
⁷Gl: Glossary of Terms 102
⁸Al: Accreditations & Locations 103
⁹Sc: Chain of Custody 104
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-3R L875822-01 GW 12/01/16 09:56 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 06:57 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:24 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 18:21 12/04/16 18:21 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:04 12/07/16 23:04 LRL
Collected by Collected date/time Received date/time
MW-5 L875822-02 GW 12/01/16 15:40 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:00 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:28 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 18:44 12/04/16 18:44 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:17 12/07/16 23:17 LRL
Collected by Collected date/time Received date/time
MW-8 L875822-03 GW 12/01/16 11:38 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:03 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:31 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 19:07 12/04/16 19:07 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:29 12/07/16 23:29 LRL
Collected by Collected date/time Received date/time
MW-9A L875822-04 GW 12/01/16 10:38 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 06:47 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:43 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:02 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 19:30 12/04/16 19:30 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:42 12/07/16 23:42 LRL
Collected by Collected date/time Received date/time
MW-12 L875822-05 GW 11/30/16 11:53 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:11 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:47 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:18 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 19:53 12/04/16 19:53 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 23:55 12/07/16 23:55 LRL
Collected by Collected date/time Received date/time
MW-13R L875822-06 GW 11/30/16 15:50 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:13 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:10 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 20:16 12/04/16 20:16 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:07 12/08/16 00:07 LRL
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-14 L875822-07 GW 11/30/16 16:44 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:16 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:50 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:05 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 20:39 12/04/16 20:39 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:20 12/08/16 00:20 LRL
Collected by Collected date/time Received date/time
MW-15 L875822-08 GW 11/30/16 17:09 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:19 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:54 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:25 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 21:02 12/04/16 21:02 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:32 12/08/16 00:32 LRL
Collected by Collected date/time Received date/time
MW-16 L875822-09 GW 12/01/16 08:27 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:22 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 11:57 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:09 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 21:25 12/04/16 21:25 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:45 12/08/16 00:45 LRL
Collected by Collected date/time Received date/time
MW-17R L875822-10 GW 12/01/16 08:52 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:24 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:01 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:32 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 21:48 12/04/16 21:48 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 00:58 12/08/16 00:58 LRL
Collected by Collected date/time Received date/time
MW-18 L875822-11 GW 12/01/16 09:24 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:27 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:04 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:12 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 22:11 12/04/16 22:11 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:10 12/08/16 01:10 LRL
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-19 L875822-12 GW 11/30/16 14:00 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG931570 1 12/02/16 21:42 12/03/16 01:42 JM
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:30 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:08 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:43 LAT
Metals (ICPMS) by Method 6020 WG931509 5 12/03/16 20:55 12/05/16 15:50 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 22:35 12/04/16 22:35 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:22 12/08/16 01:22 LRL
Wet Chemistry by Method 2320 B-2011 WG931590 1 12/05/16 08:08 12/05/16 08:08 AMC
Wet Chemistry by Method 9056A WG931818 1 12/05/16 14:07 12/05/16 14:07 SAM
Collected by Collected date/time Received date/time
MW-21R L875822-13 GW 11/30/16 13:55 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:33 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:11 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:47 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 22:58 12/04/16 22:58 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:35 12/08/16 01:35 LRL
Collected by Collected date/time Received date/time
MW-22 L875822-14 GW 11/30/16 15:22 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:35 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 12:15 LAT
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 14:50 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 23:21 12/04/16 23:21 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 01:47 12/08/16 01:47 LRL
Collected by Collected date/time Received date/time
MW-23 L875822-15 GW 11/30/16 13:20 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:44 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:16 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 23:44 12/04/16 23:44 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:00 12/08/16 02:00 LRL
Collected by Collected date/time Received date/time
MW-24R L875822-16 GW 11/30/16 11:06 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:46 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:19 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 00:07 12/05/16 00:07 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:12 12/08/16 02:12 LRL
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-25R L875822-17 GW 11/30/16 10:30 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:49 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:23 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 00:30 12/05/16 00:30 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:25 12/08/16 02:25 LRL
Collected by Collected date/time Received date/time
SW-1 L875822-18 GW 12/01/16 13:17 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:52 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:26 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 00:53 12/05/16 00:53 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:37 12/08/16 02:37 LRL
Collected by Collected date/time Received date/time
TRIP BLANK L875822-19 GW 12/01/16 00:00 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/04/16 17:58 12/04/16 17:58 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/07/16 22:39 12/07/16 22:39 LRL
Collected by Collected date/time Received date/time
LEACHATE PHASE 2 L875822-20 GW 12/01/16 14:30 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:55 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:30 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/05/16 01:16 12/05/16 01:16 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG931552 1 12/08/16 02:49 12/08/16 02:49 LRL
Wet Chemistry by Method 365.4 WG932178 1 12/06/16 11:35 12/07/16 14:25 JER
Wet Chemistry by Method 410.4 WG931630 1 12/02/16 17:59 12/02/16 20:28 MZ
Wet Chemistry by Method 5210 B-2011 WG931445 1 12/02/16 15:20 12/07/16 10:31 ARM
Wet Chemistry by Method 9056A WG931491 1 12/03/16 01:35 12/03/16 01:35 SAM
Collected by Collected date/time Received date/time
LEACHATE PHASE 3 L875822-21 GW 12/01/16 14:40 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931506 1 12/03/16 20:53 12/06/16 07:57 LTB
Metals (ICPMS) by Method 6020 WG931509 1 12/03/16 20:55 12/05/16 15:33 LAT
Metals (ICPMS) by Method 6020 WG931509 5 12/03/16 20:55 12/05/16 15:54 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG931684 1 12/04/16 17:48 12/04/16 17:48 JAH
Wet Chemistry by Method 365.4 WG932178 1 12/06/16 11:35 12/07/16 14:26 JER
Wet Chemistry by Method 410.4 WG931630 1 12/02/16 17:59 12/02/16 20:28 MZ
Wet Chemistry by Method 5210 B-2011 WG931445 1 12/02/16 15:24 12/07/16 10:34 ARM
Wet Chemistry by Method 9056A WG931491 1 12/03/16 01:50 12/03/16 01:50 SAM
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
LEACHATE PHASE 4 L875822-22 GW 12/01/16 14:52 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG931720 9 12/03/16 08:33 12/05/16 08:56 LTB
Metals (ICPMS) by Method 6020 WG931723 9 12/05/16 17:50 12/06/16 11:05 LAT
Metals (ICPMS) by Method 6020 WG932463 9 12/06/16 13:39 12/06/16 19:59 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG931684 1 12/04/16 19:13 12/04/16 19:13 JAH
Wet Chemistry by Method 365.4 WG932178 1 12/06/16 11:35 12/07/16 14:28 JER
Wet Chemistry by Method 410.4 WG931630 25 12/02/16 17:59 12/02/16 20:29 MZ
Wet Chemistry by Method 5210 B-2011 WG931445 10 12/02/16 15:28 12/07/16 10:37 ARM
Wet Chemistry by Method 9056A WG931491 1 12/03/16 02:04 12/03/16 02:04 SAM
Collected by Collected date/time Received date/time
MW-10 L875822-23 GW 12/02/16 09:46 12/03/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:09 CCE
Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:42 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 01:54 12/08/16 01:54 DAH
Collected by Collected date/time Received date/time
MW-11 L875822-24 GW 12/02/16 09:20 12/03/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:16 CCE
Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:46 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 02:25 12/08/16 02:25 DAH
Collected by Collected date/time Received date/time
MW-20 L875822-25 GW 12/02/16 08:45 12/03/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Gravimetric Analysis by Method 2540 C-2011 WG932797 1 12/08/16 09:45 12/08/16 10:32 MMF
Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:19 CCE
Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:49 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/09/16 17:32 12/09/16 17:32 DN
Wet Chemistry by Method 2320 B-2011 WG932588 1 12/07/16 11:57 12/07/16 11:57 AMC
Wet Chemistry by Method 9056A WG932605 1 12/07/16 10:38 12/07/16 10:38 SAM
Collected by Collected date/time Received date/time
MW-26 L875822-26 GW 12/02/16 08:15 12/03/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 15:22 CCE
Metals (ICPMS) by Method 6020 WG932285 1 12/06/16 09:07 12/07/16 01:53 LAT
Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 02:57 12/08/16 02:57 ACG
Collected by Collected date/time Received date/time
TRIP BLANK L875822-27 GW 12/01/16 00:00 12/02/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG932369 1 12/08/16 13:39 12/08/16 13:39 DAH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-6 L875822-28 GW 12/05/16 14:21 12/06/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG932146 1 12/07/16 14:22 12/07/16 16:22 CCE
Metals (ICPMS) by Method 6020 WG932780 1 12/07/16 15:39 12/07/16 18:25 VSS
Volatile Organic Compounds (GC/MS) by Method 8260B WG933189 1 12/09/16 13:28 12/09/16 13:28 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG933189 1 12/09/16 16:09 12/09/16 16:09 DWR
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
ESC Sample ID Project Sample ID Method
L875822-22 LEACHATE PHASE 4 6010C, 6020
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jimmy Hunt
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L875822
MW-3R
Collected date/time: 12/01/16 09:56
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0849 0.00500 1 12/06/2016 06:57 WG931506
Chromium 0.0101 0.0100 1 12/06/2016 06:57 WG931506
Cobalt ND 0.0100 1 12/06/2016 06:57 WG931506
Nickel ND 0.0100 1 12/06/2016 06:57 WG931506
Silver ND 0.00500 1 12/06/2016 06:57 WG931506
Vanadium 0.0253 0.0200 1 12/06/2016 06:57 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:24 WG931509
Arsenic 0.00214 0.00200 1 12/05/2016 11:24 WG931509
Beryllium ND 0.00200 1 12/05/2016 11:24 WG931509
Cadmium ND 0.00100 1 12/05/2016 11:24 WG931509
Copper ND 0.00500 1 12/05/2016 11:24 WG931509
Lead 0.00459 0.00200 1 12/05/2016 11:24 WG931509
Selenium 0.0463 0.00200 1 12/05/2016 11:24 WG931509
Thallium ND 0.00200 1 12/05/2016 11:24 WG931509
Zinc ND 0.0250 1 12/05/2016 11:24 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 18:21 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 18:21 WG931552
Benzene ND 0.00100 1 12/04/2016 18:21 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 18:21 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 18:21 WG931552
Bromoform ND 0.00100 1 12/04/2016 18:21 WG931552
Bromomethane ND 0.00500 1 12/04/2016 18:21 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 18:21 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 18:21 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 18:21 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 18:21 WG931552
Chloroethane ND 0.00500 1 12/04/2016 18:21 WG931552
Chloroform ND 0.00500 1 12/04/2016 18:21 WG931552
Chloromethane ND 0.00250 1 12/04/2016 18:21 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 18:21 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 18:21 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 18:21 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 18:21 WG931552
1,1-Dichloroethane 0.00217 0.00100 1 12/04/2016 18:21 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 18:21 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 18:21 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:21 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:21 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 18:21 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 18:21 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 18:21 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 18:21 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 18:21 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 18:21 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L875822
MW-3R
Collected date/time: 12/01/16 09:56
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 18:21 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:21 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:21 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 18:21 WG931552
Toluene ND 0.00500 1 12/04/2016 18:21 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 18:21 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 18:21 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 18:21 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 18:21 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 18:21 WG931552
Vinyl acetate ND 0.0100 1 12/07/2016 23:04 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 18:21 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 18:21 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 18:21 WG931552
(S) Toluene-d8 100 90.0-115 12/07/2016 23:04 WG931552
(S) Dibromofluoromethane 87.5 79.0-121 12/07/2016 23:04 WG931552
(S) Dibromofluoromethane 100 79.0-121 12/04/2016 18:21 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 18:21 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/07/2016 23:04 WG931552
(S) 4-Bromofluorobenzene 99.7 80.1-120 12/07/2016 23:04 WG931552
(S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 18:21 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L875822
MW-5
Collected date/time: 12/01/16 15:40
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0154 0.00500 1 12/06/2016 07:00 WG931506
Chromium ND 0.0100 1 12/06/2016 07:00 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:00 WG931506
Nickel ND 0.0100 1 12/06/2016 07:00 WG931506
Silver ND 0.00500 1 12/06/2016 07:00 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:00 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:28 WG931509
Arsenic ND 0.00200 1 12/05/2016 11:28 WG931509
Beryllium ND 0.00200 1 12/05/2016 11:28 WG931509
Cadmium ND 0.00100 1 12/05/2016 11:28 WG931509
Copper ND 0.00500 1 12/05/2016 11:28 WG931509
Lead ND 0.00200 1 12/05/2016 11:28 WG931509
Selenium ND 0.00200 1 12/05/2016 11:28 WG931509
Thallium ND 0.00200 1 12/05/2016 11:28 WG931509
Zinc ND 0.0250 1 12/05/2016 11:28 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 18:44 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 18:44 WG931552
Benzene ND 0.00100 1 12/04/2016 18:44 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 18:44 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 18:44 WG931552
Bromoform ND 0.00100 1 12/04/2016 18:44 WG931552
Bromomethane ND 0.00500 1 12/04/2016 18:44 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 18:44 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 18:44 WG931552
Chlorobenzene 0.00184 0.00100 1 12/04/2016 18:44 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 18:44 WG931552
Chloroethane ND 0.00500 1 12/04/2016 18:44 WG931552
Chloroform ND 0.00500 1 12/04/2016 18:44 WG931552
Chloromethane ND 0.00250 1 12/04/2016 18:44 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 18:44 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 18:44 WG931552
1,4-Dichlorobenzene 0.00499 0.00100 1 12/04/2016 18:44 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 18:44 WG931552
1,1-Dichloroethane 0.00359 0.00100 1 12/04/2016 18:44 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 18:44 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 18:44 WG931552
cis-1,2-Dichloroethene 0.00174 0.00100 1 12/04/2016 18:44 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 18:44 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 18:44 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:44 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 18:44 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 18:44 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 18:44 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 18:44 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 18:44 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 18:44 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 18:44 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L875822
MW-5
Collected date/time: 12/01/16 15:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 18:44 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:44 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 18:44 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 18:44 WG931552
Toluene ND 0.00500 1 12/04/2016 18:44 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 18:44 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 18:44 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 18:44 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 18:44 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 18:44 WG931552
Vinyl acetate ND 0.0100 1 12/07/2016 23:17 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 18:44 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 18:44 WG931552
(S) Toluene-d8 102 90.0-115 12/04/2016 18:44 WG931552
(S) Toluene-d8 100 90.0-115 12/07/2016 23:17 WG931552
(S) Dibromofluoromethane 88.5 79.0-121 12/07/2016 23:17 WG931552
(S) Dibromofluoromethane 99.8 79.0-121 12/04/2016 18:44 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 18:44 WG931552
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/07/2016 23:17 WG931552
(S) 4-Bromofluorobenzene 99.7 80.1-120 12/07/2016 23:17 WG931552
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 18:44 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L875822
MW-8
Collected date/time: 12/01/16 11:38
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0621 0.00500 1 12/06/2016 07:03 WG931506
Chromium ND 0.0100 1 12/06/2016 07:03 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:03 WG931506
Nickel ND 0.0100 1 12/06/2016 07:03 WG931506
Silver ND 0.00500 1 12/06/2016 07:03 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:03 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:31 WG931509
Arsenic 0.00278 0.00200 1 12/05/2016 11:31 WG931509
Beryllium ND 0.00200 1 12/05/2016 11:31 WG931509
Cadmium ND 0.00100 1 12/05/2016 11:31 WG931509
Copper ND 0.00500 1 12/05/2016 11:31 WG931509
Lead 0.00846 0.00200 1 12/05/2016 11:31 WG931509
Selenium ND 0.00200 1 12/05/2016 11:31 WG931509
Thallium ND 0.00200 1 12/05/2016 11:31 WG931509
Zinc ND 0.0250 1 12/05/2016 11:31 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 19:07 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 19:07 WG931552
Benzene ND 0.00100 1 12/04/2016 19:07 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 19:07 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 19:07 WG931552
Bromoform ND 0.00100 1 12/04/2016 19:07 WG931552
Bromomethane ND 0.00500 1 12/04/2016 19:07 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 19:07 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 19:07 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 19:07 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 19:07 WG931552
Chloroethane ND 0.00500 1 12/04/2016 19:07 WG931552
Chloroform ND 0.00500 1 12/04/2016 19:07 WG931552
Chloromethane ND 0.00250 1 12/04/2016 19:07 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 19:07 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:07 WG931552
1,4-Dichlorobenzene 0.00291 0.00100 1 12/04/2016 19:07 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:07 WG931552
1,1-Dichloroethane 0.00417 0.00100 1 12/04/2016 19:07 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:07 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:07 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:07 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:07 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 19:07 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 19:07 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 19:07 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:07 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 19:07 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:07 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 15 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L875822
MW-8
Collected date/time: 12/01/16 11:38
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 19:07 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:07 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:07 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 19:07 WG931552
Toluene ND 0.00500 1 12/04/2016 19:07 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:07 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:07 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 19:07 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:07 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:07 WG931552
Vinyl acetate ND 0.0100 1 12/07/2016 23:29 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 19:07 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 19:07 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 19:07 WG931552
(S) Toluene-d8 99.3 90.0-115 12/07/2016 23:29 WG931552
(S) Dibromofluoromethane 84.4 79.0-121 12/07/2016 23:29 WG931552
(S) Dibromofluoromethane 97.9 79.0-121 12/04/2016 19:07 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 19:07 WG931552
(S) a,a,a-Trifluorotoluene 99.0 90.4-116 12/07/2016 23:29 WG931552
(S) 4-Bromofluorobenzene 99.2 80.1-120 12/07/2016 23:29 WG931552
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 19:07 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L875822
MW-9A
Collected date/time: 12/01/16 10:38
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0868 0.00500 1 12/06/2016 06:47 WG931506
Chromium ND 0.0100 1 12/06/2016 06:47 WG931506
Cobalt ND 0.0100 1 12/06/2016 06:47 WG931506
Nickel ND 0.0100 1 12/06/2016 06:47 WG931506
Silver ND 0.00500 1 12/06/2016 06:47 WG931506
Vanadium ND 0.0200 1 12/06/2016 06:47 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:43 WG931509
Arsenic ND 0.00200 1 12/05/2016 11:43 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:02 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:02 WG931509
Copper ND 0.00500 1 12/05/2016 11:43 WG931509
Lead ND 0.00200 1 12/05/2016 11:43 WG931509
Selenium ND 0.00200 1 12/05/2016 11:43 WG931509
Thallium ND 0.00200 1 12/05/2016 11:43 WG931509
Zinc ND 0.0250 1 12/05/2016 11:43 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 19:30 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 19:30 WG931552
Benzene 0.00144 0.00100 1 12/04/2016 19:30 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 19:30 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 19:30 WG931552
Bromoform ND 0.00100 1 12/04/2016 19:30 WG931552
Bromomethane ND 0.00500 1 12/04/2016 19:30 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 19:30 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 19:30 WG931552
Chlorobenzene 0.00199 0.00100 1 12/04/2016 19:30 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 19:30 WG931552
Chloroethane ND 0.00500 1 12/04/2016 19:30 WG931552
Chloroform ND 0.00500 1 12/04/2016 19:30 WG931552
Chloromethane ND 0.00250 1 12/04/2016 19:30 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 19:30 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:30 WG931552
1,4-Dichlorobenzene 0.00951 0.00100 1 12/04/2016 19:30 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:30 WG931552
1,1-Dichloroethane 0.0104 0.00100 1 12/04/2016 19:30 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:30 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:30 WG931552
cis-1,2-Dichloroethene 0.00155 0.00100 1 12/04/2016 19:30 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:30 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:30 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:30 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:30 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 19:30 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 19:30 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 19:30 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:30 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 19:30 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:30 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 17 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L875822
MW-9A
Collected date/time: 12/01/16 10:38
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 19:30 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:30 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:30 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 19:30 WG931552
Toluene ND 0.00500 1 12/04/2016 19:30 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:30 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:30 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 19:30 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:30 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:30 WG931552
Vinyl acetate ND 0.0100 1 12/07/2016 23:42 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 19:30 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 19:30 WG931552
(S) Toluene-d8 102 90.0-115 12/04/2016 19:30 WG931552
(S) Toluene-d8 101 90.0-115 12/07/2016 23:42 WG931552
(S) Dibromofluoromethane 87.8 79.0-121 12/07/2016 23:42 WG931552
(S) Dibromofluoromethane 99.2 79.0-121 12/04/2016 19:30 WG931552
(S) a,a,a-Trifluorotoluene 103 90.4-116 12/04/2016 19:30 WG931552
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/07/2016 23:42 WG931552
(S) 4-Bromofluorobenzene 99.7 80.1-120 12/07/2016 23:42 WG931552
(S) 4-Bromofluorobenzene 106 80.1-120 12/04/2016 19:30 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 18 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L875822
MW-12
Collected date/time: 11/30/16 11:53
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0927 0.00500 1 12/06/2016 07:11 WG931506
Chromium ND 0.0100 1 12/06/2016 07:11 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:11 WG931506
Nickel ND 0.0100 1 12/06/2016 07:11 WG931506
Silver ND 0.00500 1 12/06/2016 07:11 WG931506
Vanadium 0.0228 0.0200 1 12/06/2016 07:11 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:47 WG931509
Arsenic ND 0.00200 1 12/05/2016 11:47 WG931509
Beryllium ND 0.00200 1 12/05/2016 14:18 WG931509
Cadmium ND 0.00100 1 12/05/2016 14:18 WG931509
Copper ND 0.00500 1 12/05/2016 11:47 WG931509
Lead 0.00399 0.00200 1 12/05/2016 11:47 WG931509
Selenium ND 0.00200 1 12/05/2016 11:47 WG931509
Thallium ND 0.00200 1 12/05/2016 11:47 WG931509
Zinc ND 0.0250 1 12/05/2016 11:47 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 19:53 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 19:53 WG931552
Benzene ND 0.00100 1 12/04/2016 19:53 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 19:53 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 19:53 WG931552
Bromoform ND 0.00100 1 12/04/2016 19:53 WG931552
Bromomethane ND 0.00500 1 12/04/2016 19:53 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 19:53 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 19:53 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 19:53 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 19:53 WG931552
Chloroethane ND 0.00500 1 12/04/2016 19:53 WG931552
Chloroform ND 0.00500 1 12/04/2016 19:53 WG931552
Chloromethane ND 0.00250 1 12/04/2016 19:53 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 19:53 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:53 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 19:53 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:53 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:53 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:53 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:53 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 19:53 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 19:53 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 19:53 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:53 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 19:53 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:53 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 19 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L875822
MW-12
Collected date/time: 11/30/16 11:53
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 19:53 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:53 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:53 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 19:53 WG931552
Toluene ND 0.00500 1 12/04/2016 19:53 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:53 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 19:53 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:53 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:53 WG931552
Vinyl acetate ND 0.0100 1 12/07/2016 23:55 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 19:53 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 19:53 WG931552
(S) Toluene-d8 102 90.0-115 12/04/2016 19:53 WG931552
(S) Toluene-d8 101 90.0-115 12/07/2016 23:55 WG931552
(S) Dibromofluoromethane 88.7 79.0-121 12/07/2016 23:55 WG931552
(S) Dibromofluoromethane 98.9 79.0-121 12/04/2016 19:53 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 19:53 WG931552
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/07/2016 23:55 WG931552
(S) 4-Bromofluorobenzene 101 80.1-120 12/07/2016 23:55 WG931552
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 19:53 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 20 of 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 20 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L875822
MW-13R
Collected date/time: 11/30/16 15:50
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.159 0.00500 1 12/06/2016 07:13 WG931506
Chromium ND 0.0100 1 12/06/2016 07:13 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:13 WG931506
Nickel ND 0.0100 1 12/06/2016 07:13 WG931506
Silver ND 0.00500 1 12/06/2016 07:13 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:13 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:10 WG931509
Arsenic ND 0.00200 1 12/05/2016 11:10 WG931509
Beryllium ND 0.00200 1 12/05/2016 11:10 WG931509
Cadmium ND 0.00100 1 12/05/2016 11:10 WG931509
Copper ND 0.00500 1 12/05/2016 11:10 WG931509
Lead 0.00335 0.00200 1 12/05/2016 11:10 WG931509
Selenium ND 0.00200 1 12/05/2016 11:10 WG931509
Thallium ND 0.00200 1 12/05/2016 11:10 WG931509
Zinc ND 0.0250 1 12/05/2016 11:10 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 20:16 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 20:16 WG931552
Benzene 0.00189 0.00100 1 12/04/2016 20:16 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 20:16 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 20:16 WG931552
Bromoform ND 0.00100 1 12/04/2016 20:16 WG931552
Bromomethane ND 0.00500 1 12/04/2016 20:16 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 20:16 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 20:16 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 20:16 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 20:16 WG931552
Chloroethane ND 0.00500 1 12/04/2016 20:16 WG931552
Chloroform ND 0.00500 1 12/04/2016 20:16 WG931552
Chloromethane ND 0.00250 1 12/04/2016 20:16 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 20:16 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 20:16 WG931552
1,4-Dichlorobenzene 0.00249 0.00100 1 12/04/2016 20:16 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 20:16 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 20:16 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:16 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:16 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 20:16 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 20:16 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 20:16 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 20:16 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 20:16 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 20:16 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L875822
MW-13R
Collected date/time: 11/30/16 15:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 20:16 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:16 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:16 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 20:16 WG931552
Toluene ND 0.00500 1 12/04/2016 20:16 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 20:16 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 20:16 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 20:16 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 20:16 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 00:07 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 20:16 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 20:16 WG931552
(S) Toluene-d8 102 90.0-115 12/04/2016 20:16 WG931552
(S) Toluene-d8 102 90.0-115 12/08/2016 00:07 WG931552
(S) Dibromofluoromethane 88.8 79.0-121 12/08/2016 00:07 WG931552
(S) Dibromofluoromethane 101 79.0-121 12/04/2016 20:16 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 20:16 WG931552
(S) a,a,a-Trifluorotoluene 103 90.4-116 12/08/2016 00:07 WG931552
(S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 00:07 WG931552
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 20:16 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L875822
MW-14
Collected date/time: 11/30/16 16:44
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.181 0.00500 1 12/06/2016 07:16 WG931506
Chromium ND 0.0100 1 12/06/2016 07:16 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:16 WG931506
Nickel ND 0.0100 1 12/06/2016 07:16 WG931506
Silver ND 0.00500 1 12/06/2016 07:16 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:16 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:50 WG931509
Arsenic ND 0.00200 1 12/05/2016 11:50 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:05 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:05 WG931509
Copper ND 0.00500 1 12/05/2016 11:50 WG931509
Lead ND 0.00200 1 12/05/2016 11:50 WG931509
Selenium ND 0.00200 1 12/05/2016 11:50 WG931509
Thallium ND 0.00200 1 12/05/2016 11:50 WG931509
Zinc ND 0.0250 1 12/05/2016 11:50 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 20:39 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 20:39 WG931552
Benzene ND 0.00100 1 12/04/2016 20:39 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 20:39 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 20:39 WG931552
Bromoform ND 0.00100 1 12/04/2016 20:39 WG931552
Bromomethane ND 0.00500 1 12/04/2016 20:39 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 20:39 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 20:39 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 20:39 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 20:39 WG931552
Chloroethane ND 0.00500 1 12/04/2016 20:39 WG931552
Chloroform ND 0.00500 1 12/04/2016 20:39 WG931552
Chloromethane ND 0.00250 1 12/04/2016 20:39 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 20:39 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 20:39 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 20:39 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 20:39 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 20:39 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:39 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 20:39 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 20:39 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 20:39 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 20:39 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 20:39 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 20:39 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 20:39 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L875822
MW-14
Collected date/time: 11/30/16 16:44
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 20:39 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:39 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 20:39 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 20:39 WG931552
Toluene ND 0.00500 1 12/04/2016 20:39 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 20:39 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 20:39 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 20:39 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 20:39 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 00:20 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 20:39 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 20:39 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 20:39 WG931552
(S) Toluene-d8 101 90.0-115 12/08/2016 00:20 WG931552
(S) Dibromofluoromethane 89.9 79.0-121 12/08/2016 00:20 WG931552
(S) Dibromofluoromethane 100 79.0-121 12/04/2016 20:39 WG931552
(S) a,a,a-Trifluorotoluene 106 90.4-116 12/04/2016 20:39 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 00:20 WG931552
(S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 00:20 WG931552
(S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 20:39 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 24 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L875822
MW-15
Collected date/time: 11/30/16 17:09
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0669 0.00500 1 12/06/2016 07:19 WG931506
Chromium ND 0.0100 1 12/06/2016 07:19 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:19 WG931506
Nickel ND 0.0100 1 12/06/2016 07:19 WG931506
Silver ND 0.00500 1 12/06/2016 07:19 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:19 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:54 WG931509
Arsenic 0.00251 0.00200 1 12/05/2016 11:54 WG931509
Beryllium ND 0.00200 1 12/05/2016 14:25 WG931509
Cadmium ND 0.00100 1 12/05/2016 14:25 WG931509
Copper ND 0.00500 1 12/05/2016 11:54 WG931509
Lead ND 0.00200 1 12/05/2016 11:54 WG931509
Selenium ND 0.00200 1 12/05/2016 11:54 WG931509
Thallium ND 0.00200 1 12/05/2016 11:54 WG931509
Zinc ND 0.0250 1 12/05/2016 11:54 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone 0.104 0.0500 1 12/04/2016 21:02 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 21:02 WG931552
Benzene 0.00174 0.00100 1 12/04/2016 21:02 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 21:02 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 21:02 WG931552
Bromoform ND 0.00100 1 12/04/2016 21:02 WG931552
Bromomethane ND 0.00500 1 12/04/2016 21:02 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 21:02 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 21:02 WG931552
Chlorobenzene 0.00286 0.00100 1 12/04/2016 21:02 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 21:02 WG931552
Chloroethane ND 0.00500 1 12/04/2016 21:02 WG931552
Chloroform ND 0.00500 1 12/04/2016 21:02 WG931552
Chloromethane ND 0.00250 1 12/04/2016 21:02 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 21:02 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 21:02 WG931552
1,4-Dichlorobenzene 0.00813 0.00100 1 12/04/2016 21:02 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 21:02 WG931552
1,1-Dichloroethane 0.00303 0.00100 1 12/04/2016 21:02 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 21:02 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 21:02 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:02 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:02 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 21:02 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 21:02 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 21:02 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 21:02 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 21:02 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 21:02 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 25 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L875822
MW-15
Collected date/time: 11/30/16 17:09
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 21:02 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:02 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:02 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 21:02 WG931552
Toluene ND 0.00500 1 12/04/2016 21:02 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 21:02 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 21:02 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 21:02 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 21:02 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 21:02 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 00:32 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 21:02 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 21:02 WG931552
(S) Toluene-d8 102 90.0-115 12/04/2016 21:02 WG931552
(S) Toluene-d8 101 90.0-115 12/08/2016 00:32 WG931552
(S) Dibromofluoromethane 87.9 79.0-121 12/08/2016 00:32 WG931552
(S) Dibromofluoromethane 99.0 79.0-121 12/04/2016 21:02 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 21:02 WG931552
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/08/2016 00:32 WG931552
(S) 4-Bromofluorobenzene 99.3 80.1-120 12/08/2016 00:32 WG931552
(S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 21:02 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 26 of 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 26 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L875822
MW-16
Collected date/time: 12/01/16 08:27
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.144 0.00500 1 12/06/2016 07:22 WG931506
Chromium ND 0.0100 1 12/06/2016 07:22 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:22 WG931506
Nickel ND 0.0100 1 12/06/2016 07:22 WG931506
Silver ND 0.00500 1 12/06/2016 07:22 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:22 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 11:57 WG931509
Arsenic 0.0141 0.00200 1 12/05/2016 11:57 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:09 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:09 WG931509
Copper ND 0.00500 1 12/05/2016 11:57 WG931509
Lead ND 0.00200 1 12/05/2016 11:57 WG931509
Selenium ND 0.00200 1 12/05/2016 11:57 WG931509
Thallium ND 0.00200 1 12/05/2016 11:57 WG931509
Zinc ND 0.0250 1 12/05/2016 11:57 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 21:25 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 21:25 WG931552
Benzene 0.00145 0.00100 1 12/04/2016 21:25 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 21:25 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 21:25 WG931552
Bromoform ND 0.00100 1 12/04/2016 21:25 WG931552
Bromomethane ND 0.00500 1 12/04/2016 21:25 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 21:25 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 21:25 WG931552
Chlorobenzene 0.00162 0.00100 1 12/04/2016 21:25 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 21:25 WG931552
Chloroethane 0.0105 0.00500 1 12/04/2016 21:25 WG931552
Chloroform ND 0.00500 1 12/04/2016 21:25 WG931552
Chloromethane ND 0.00250 1 12/04/2016 21:25 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 21:25 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 21:25 WG931552
1,4-Dichlorobenzene 0.00200 0.00100 1 12/04/2016 21:25 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 21:25 WG931552
1,1-Dichloroethane 0.00115 0.00100 1 12/04/2016 21:25 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 21:25 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 21:25 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:25 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:25 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 21:25 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 21:25 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 21:25 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 21:25 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 21:25 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 21:25 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L875822
MW-16
Collected date/time: 12/01/16 08:27
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 21:25 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:25 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:25 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 21:25 WG931552
Toluene ND 0.00500 1 12/04/2016 21:25 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 21:25 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 21:25 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 21:25 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 21:25 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 21:25 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 00:45 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 21:25 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 21:25 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 21:25 WG931552
(S) Toluene-d8 100 90.0-115 12/08/2016 00:45 WG931552
(S) Dibromofluoromethane 88.7 79.0-121 12/08/2016 00:45 WG931552
(S) Dibromofluoromethane 99.8 79.0-121 12/04/2016 21:25 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 21:25 WG931552
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/08/2016 00:45 WG931552
(S) 4-Bromofluorobenzene 101 80.1-120 12/08/2016 00:45 WG931552
(S) 4-Bromofluorobenzene 102 80.1-120 12/04/2016 21:25 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L875822
MW-17R
Collected date/time: 12/01/16 08:52
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.137 0.00500 1 12/06/2016 07:24 WG931506
Chromium 0.0116 0.0100 1 12/06/2016 07:24 WG931506
Cobalt 0.0170 0.0100 1 12/06/2016 07:24 WG931506
Nickel ND 0.0100 1 12/06/2016 07:24 WG931506
Silver ND 0.00500 1 12/06/2016 07:24 WG931506
Vanadium 0.0237 0.0200 1 12/06/2016 07:24 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 12:01 WG931509
Arsenic ND 0.00200 1 12/05/2016 12:01 WG931509
Beryllium ND 0.00200 1 12/05/2016 14:32 WG931509
Cadmium ND 0.00100 1 12/05/2016 14:32 WG931509
Copper ND 0.00500 1 12/05/2016 12:01 WG931509
Lead 0.00858 0.00200 1 12/05/2016 12:01 WG931509
Selenium ND 0.00200 1 12/05/2016 12:01 WG931509
Thallium ND 0.00200 1 12/05/2016 12:01 WG931509
Zinc ND 0.0250 1 12/05/2016 12:01 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 21:48 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 21:48 WG931552
Benzene ND 0.00100 1 12/04/2016 21:48 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 21:48 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 21:48 WG931552
Bromoform ND 0.00100 1 12/04/2016 21:48 WG931552
Bromomethane ND 0.00500 1 12/04/2016 21:48 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 21:48 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 21:48 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 21:48 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 21:48 WG931552
Chloroethane ND 0.00500 1 12/04/2016 21:48 WG931552
Chloroform ND 0.00500 1 12/04/2016 21:48 WG931552
Chloromethane ND 0.00250 1 12/04/2016 21:48 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 21:48 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 21:48 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 21:48 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 21:48 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 21:48 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:48 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 21:48 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 21:48 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:48 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 21:48 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 21:48 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 21:48 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 21:48 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 21:48 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 21:48 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 21:48 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L875822
MW-17R
Collected date/time: 12/01/16 08:52
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 21:48 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:48 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 21:48 WG931552
Tetrachloroethene 0.00121 0.00100 1 12/04/2016 21:48 WG931552
Toluene ND 0.00500 1 12/04/2016 21:48 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 21:48 WG931552
Trichloroethene 0.00102 0.00100 1 12/04/2016 21:48 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 21:48 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 21:48 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 00:58 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 21:48 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 21:48 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 21:48 WG931552
(S) Toluene-d8 99.4 90.0-115 12/08/2016 00:58 WG931552
(S) Dibromofluoromethane 87.7 79.0-121 12/08/2016 00:58 WG931552
(S) Dibromofluoromethane 99.8 79.0-121 12/04/2016 21:48 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 21:48 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 00:58 WG931552
(S) 4-Bromofluorobenzene 99.7 80.1-120 12/08/2016 00:58 WG931552
(S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 21:48 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L875822
MW-18
Collected date/time: 12/01/16 09:24
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.122 0.00500 1 12/06/2016 07:27 WG931506
Chromium ND 0.0100 1 12/06/2016 07:27 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:27 WG931506
Nickel ND 0.0100 1 12/06/2016 07:27 WG931506
Silver ND 0.00500 1 12/06/2016 07:27 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:27 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 12:04 WG931509
Arsenic ND 0.00200 1 12/05/2016 12:04 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:12 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:12 WG931509
Copper ND 0.00500 1 12/05/2016 12:04 WG931509
Lead 0.00338 0.00200 1 12/05/2016 12:04 WG931509
Selenium ND 0.00200 1 12/05/2016 12:04 WG931509
Thallium ND 0.00200 1 12/05/2016 12:04 WG931509
Zinc ND 0.0250 1 12/05/2016 12:04 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 22:11 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 22:11 WG931552
Benzene ND 0.00100 1 12/04/2016 22:11 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 22:11 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 22:11 WG931552
Bromoform ND 0.00100 1 12/04/2016 22:11 WG931552
Bromomethane ND 0.00500 1 12/04/2016 22:11 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 22:11 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 22:11 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 22:11 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 22:11 WG931552
Chloroethane ND 0.00500 1 12/04/2016 22:11 WG931552
Chloroform ND 0.00500 1 12/04/2016 22:11 WG931552
Chloromethane ND 0.00250 1 12/04/2016 22:11 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 22:11 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 22:11 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 22:11 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 22:11 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 22:11 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:11 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:11 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 22:11 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 22:11 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 22:11 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 22:11 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 22:11 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 22:11 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L875822
MW-18
Collected date/time: 12/01/16 09:24
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 22:11 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:11 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:11 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 22:11 WG931552
Toluene ND 0.00500 1 12/04/2016 22:11 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 22:11 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 22:11 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 22:11 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 22:11 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 01:10 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 22:11 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 22:11 WG931552
(S) Toluene-d8 102 90.0-115 12/04/2016 22:11 WG931552
(S) Toluene-d8 99.9 90.0-115 12/08/2016 01:10 WG931552
(S) Dibromofluoromethane 87.4 79.0-121 12/08/2016 01:10 WG931552
(S) Dibromofluoromethane 98.1 79.0-121 12/04/2016 22:11 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 22:11 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 01:10 WG931552
(S) 4-Bromofluorobenzene 99.9 80.1-120 12/08/2016 01:10 WG931552
(S) 4-Bromofluorobenzene 103 80.1-120 12/04/2016 22:11 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L875822
MW-19
Collected date/time: 11/30/16 14:00
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 570 10.0 1 12/03/2016 01:42 WG931570
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity ND 20.0 1 12/05/2016 08:08 WG931590
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 9.61 1.00 1 12/05/2016 14:07 WG931818
Sulfate ND 5.00 1 12/05/2016 14:07 WG931818
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.512 0.00500 1 12/06/2016 07:30 WG931506
Chromium 0.0962 0.0100 1 12/06/2016 07:30 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:30 WG931506
Nickel 0.0262 0.0100 1 12/06/2016 07:30 WG931506
Silver ND 0.00500 1 12/06/2016 07:30 WG931506
Vanadium 0.154 0.0200 1 12/06/2016 07:30 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 12:08 WG931509
Arsenic 0.0138 0.00200 1 12/05/2016 12:08 WG931509
Beryllium ND 0.0100 5 12/05/2016 15:50 WG931509
Cadmium ND 0.00100 1 12/05/2016 14:43 WG931509
Copper 0.0261 0.00500 1 12/05/2016 12:08 WG931509
Lead 0.0878 0.00200 1 12/05/2016 12:08 WG931509
Selenium 0.00726 0.00200 1 12/05/2016 12:08 WG931509
Thallium ND 0.00200 1 12/05/2016 12:08 WG931509
Zinc 0.114 0.0250 1 12/05/2016 12:08 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 22:35 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 22:35 WG931552
Benzene ND 0.00100 1 12/04/2016 22:35 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 22:35 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 22:35 WG931552
Bromoform ND 0.00100 1 12/04/2016 22:35 WG931552
Bromomethane ND 0.00500 1 12/04/2016 22:35 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 22:35 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 22:35 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 22:35 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 22:35 WG931552
Chloroethane ND 0.00500 1 12/04/2016 22:35 WG931552
Chloroform ND 0.00500 1 12/04/2016 22:35 WG931552
Chloromethane ND 0.00250 1 12/04/2016 22:35 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L875822
MW-19
Collected date/time: 11/30/16 14:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dibromomethane ND 0.00100 1 12/04/2016 22:35 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 22:35 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 22:35 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 22:35 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 22:35 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:35 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:35 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 22:35 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 22:35 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 22:35 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 22:35 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 22:35 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 22:35 WG931552
Styrene ND 0.00100 1 12/04/2016 22:35 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:35 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:35 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 22:35 WG931552
Toluene ND 0.00500 1 12/04/2016 22:35 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 22:35 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 22:35 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 22:35 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 22:35 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 01:22 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 22:35 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 22:35 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 22:35 WG931552
(S) Toluene-d8 99.5 90.0-115 12/08/2016 01:22 WG931552
(S) Dibromofluoromethane 86.7 79.0-121 12/08/2016 01:22 WG931552
(S) Dibromofluoromethane 100 79.0-121 12/04/2016 22:35 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 22:35 WG931552
(S) a,a,a-Trifluorotoluene 99.9 90.4-116 12/08/2016 01:22 WG931552
(S) 4-Bromofluorobenzene 98.5 80.1-120 12/08/2016 01:22 WG931552
(S) 4-Bromofluorobenzene 102 80.1-120 12/04/2016 22:35 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L875822
MW-21R
Collected date/time: 11/30/16 13:55
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0290 0.00500 1 12/06/2016 07:33 WG931506
Chromium ND 0.0100 1 12/06/2016 07:33 WG931506
Cobalt 0.0112 0.0100 1 12/06/2016 07:33 WG931506
Nickel ND 0.0100 1 12/06/2016 07:33 WG931506
Silver ND 0.00500 1 12/06/2016 07:33 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:33 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 12:11 WG931509
Arsenic 0.00339 0.00200 1 12/05/2016 12:11 WG931509
Beryllium ND 0.00200 1 12/05/2016 14:47 WG931509
Cadmium ND 0.00100 1 12/05/2016 14:47 WG931509
Copper 0.00648 0.00500 1 12/05/2016 12:11 WG931509
Lead 0.00249 0.00200 1 12/05/2016 12:11 WG931509
Selenium ND 0.00200 1 12/05/2016 12:11 WG931509
Thallium ND 0.00200 1 12/05/2016 12:11 WG931509
Zinc ND 0.0250 1 12/05/2016 12:11 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 22:58 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 22:58 WG931552
Benzene ND 0.00100 1 12/04/2016 22:58 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 22:58 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 22:58 WG931552
Bromoform ND 0.00100 1 12/04/2016 22:58 WG931552
Bromomethane ND 0.00500 1 12/04/2016 22:58 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 22:58 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 22:58 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 22:58 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 22:58 WG931552
Chloroethane ND 0.00500 1 12/04/2016 22:58 WG931552
Chloroform ND 0.00500 1 12/04/2016 22:58 WG931552
Chloromethane ND 0.00250 1 12/04/2016 22:58 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 22:58 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 22:58 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 22:58 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 22:58 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 22:58 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:58 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 22:58 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 22:58 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 22:58 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 22:58 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 22:58 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 22:58 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 22:58 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 35 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L875822
MW-21R
Collected date/time: 11/30/16 13:55
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 22:58 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:58 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 22:58 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 22:58 WG931552
Toluene ND 0.00500 1 12/04/2016 22:58 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 22:58 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 22:58 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 22:58 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 22:58 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 01:35 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 22:58 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 22:58 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 22:58 WG931552
(S) Toluene-d8 101 90.0-115 12/08/2016 01:35 WG931552
(S) Dibromofluoromethane 88.1 79.0-121 12/08/2016 01:35 WG931552
(S) Dibromofluoromethane 98.9 79.0-121 12/04/2016 22:58 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 22:58 WG931552
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/08/2016 01:35 WG931552
(S) 4-Bromofluorobenzene 99.6 80.1-120 12/08/2016 01:35 WG931552
(S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 22:58 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L875822
MW-22
Collected date/time: 11/30/16 15:22
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0612 0.00500 1 12/06/2016 07:35 WG931506
Chromium ND 0.0100 1 12/06/2016 07:35 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:35 WG931506
Nickel ND 0.0100 1 12/06/2016 07:35 WG931506
Silver ND 0.00500 1 12/06/2016 07:35 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:35 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 12:15 WG931509
Arsenic ND 0.00200 1 12/05/2016 12:15 WG931509
Beryllium ND 0.00200 1 12/05/2016 14:50 WG931509
Cadmium ND 0.00100 1 12/05/2016 14:50 WG931509
Copper ND 0.00500 1 12/05/2016 12:15 WG931509
Lead ND 0.00200 1 12/05/2016 12:15 WG931509
Selenium ND 0.00200 1 12/05/2016 12:15 WG931509
Thallium ND 0.00200 1 12/05/2016 12:15 WG931509
Zinc ND 0.0250 1 12/05/2016 12:15 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 23:21 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 23:21 WG931552
Benzene ND 0.00100 1 12/04/2016 23:21 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 23:21 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 23:21 WG931552
Bromoform ND 0.00100 1 12/04/2016 23:21 WG931552
Bromomethane ND 0.00500 1 12/04/2016 23:21 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 23:21 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 23:21 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 23:21 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 23:21 WG931552
Chloroethane ND 0.00500 1 12/04/2016 23:21 WG931552
Chloroform ND 0.00500 1 12/04/2016 23:21 WG931552
Chloromethane ND 0.00250 1 12/04/2016 23:21 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 23:21 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 23:21 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 23:21 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 23:21 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 23:21 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:21 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:21 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 23:21 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 23:21 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 23:21 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 23:21 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 23:21 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 23:21 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 37 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L875822
MW-22
Collected date/time: 11/30/16 15:22
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 23:21 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:21 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:21 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 23:21 WG931552
Toluene ND 0.00500 1 12/04/2016 23:21 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 23:21 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 23:21 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 23:21 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 23:21 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 01:47 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 23:21 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 23:21 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 23:21 WG931552
(S) Toluene-d8 101 90.0-115 12/08/2016 01:47 WG931552
(S) Dibromofluoromethane 89.4 79.0-121 12/08/2016 01:47 WG931552
(S) Dibromofluoromethane 99.9 79.0-121 12/04/2016 23:21 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/04/2016 23:21 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/08/2016 01:47 WG931552
(S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 01:47 WG931552
(S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 23:21 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 38 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L875822
MW-23
Collected date/time: 11/30/16 13:20
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0115 0.00500 1 12/06/2016 07:44 WG931506
Chromium ND 0.0100 1 12/06/2016 07:44 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:44 WG931506
Nickel ND 0.0100 1 12/06/2016 07:44 WG931506
Silver ND 0.00500 1 12/06/2016 07:44 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:44 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 15:16 WG931509
Arsenic ND 0.00200 1 12/05/2016 15:16 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:16 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:16 WG931509
Copper ND 0.00500 1 12/05/2016 15:16 WG931509
Lead ND 0.00200 1 12/05/2016 15:16 WG931509
Selenium ND 0.00200 1 12/05/2016 15:16 WG931509
Thallium ND 0.00200 1 12/05/2016 15:16 WG931509
Zinc ND 0.0250 1 12/05/2016 15:16 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 23:44 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 23:44 WG931552
Benzene ND 0.00100 1 12/04/2016 23:44 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 23:44 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 23:44 WG931552
Bromoform ND 0.00100 1 12/04/2016 23:44 WG931552
Bromomethane ND 0.00500 1 12/04/2016 23:44 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 23:44 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 23:44 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 23:44 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 23:44 WG931552
Chloroethane ND 0.00500 1 12/04/2016 23:44 WG931552
Chloroform ND 0.00500 1 12/04/2016 23:44 WG931552
Chloromethane ND 0.00250 1 12/04/2016 23:44 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 23:44 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 23:44 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 23:44 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 23:44 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 23:44 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:44 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 23:44 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 23:44 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 23:44 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 23:44 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 23:44 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 23:44 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 23:44 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 39 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L875822
MW-23
Collected date/time: 11/30/16 13:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/04/2016 23:44 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:44 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 23:44 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 23:44 WG931552
Toluene ND 0.00500 1 12/04/2016 23:44 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 23:44 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 23:44 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 23:44 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 23:44 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 02:00 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 23:44 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 23:44 WG931552
(S) Toluene-d8 103 90.0-115 12/04/2016 23:44 WG931552
(S) Toluene-d8 99.5 90.0-115 12/08/2016 02:00 WG931552
(S) Dibromofluoromethane 86.5 79.0-121 12/08/2016 02:00 WG931552
(S) Dibromofluoromethane 97.9 79.0-121 12/04/2016 23:44 WG931552
(S) a,a,a-Trifluorotoluene 106 90.4-116 12/04/2016 23:44 WG931552
(S) a,a,a-Trifluorotoluene 99.7 90.4-116 12/08/2016 02:00 WG931552
(S) 4-Bromofluorobenzene 98.0 80.1-120 12/08/2016 02:00 WG931552
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 23:44 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/09/16 19:12 40 of 110
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Hunt Environmental Associates 14-011550 L875822 12/12/16 11:33 40 of 110
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L875822
MW-24R
Collected date/time: 11/30/16 11:06
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0362 0.00500 1 12/06/2016 07:46 WG931506
Chromium ND 0.0100 1 12/06/2016 07:46 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:46 WG931506
Nickel ND 0.0100 1 12/06/2016 07:46 WG931506
Silver ND 0.00500 1 12/06/2016 07:46 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:46 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 15:19 WG931509
Arsenic ND 0.00200 1 12/05/2016 15:19 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:19 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:19 WG931509
Copper ND 0.00500 1 12/05/2016 15:19 WG931509
Lead ND 0.00200 1 12/05/2016 15:19 WG931509
Selenium ND 0.00200 1 12/05/2016 15:19 WG931509
Thallium ND 0.00200 1 12/05/2016 15:19 WG931509
Zinc ND 0.0250 1 12/05/2016 15:19 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/05/2016 00:07 WG931552
Acrylonitrile ND 0.0100 1 12/05/2016 00:07 WG931552
Benzene ND 0.00100 1 12/05/2016 00:07 WG931552
Bromochloromethane ND 0.00100 1 12/05/2016 00:07 WG931552
Bromodichloromethane ND 0.00100 1 12/05/2016 00:07 WG931552
Bromoform ND 0.00100 1 12/05/2016 00:07 WG931552
Bromomethane ND 0.00500 1 12/05/2016 00:07 WG931552
Carbon disulfide ND 0.00100 1 12/05/2016 00:07 WG931552
Carbon tetrachloride ND 0.00100 1 12/05/2016 00:07 WG931552
Chlorobenzene ND 0.00100 1 12/05/2016 00:07 WG931552
Chlorodibromomethane ND 0.00100 1 12/05/2016 00:07 WG931552
Chloroethane ND 0.00500 1 12/05/2016 00:07 WG931552
Chloroform ND 0.00500 1 12/05/2016 00:07 WG931552
Chloromethane ND 0.00250 1 12/05/2016 00:07 WG931552
Dibromomethane ND 0.00100 1 12/05/2016 00:07 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 00:07 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/05/2016 00:07 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 00:07 WG931552
1,1-Dichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552
1,2-Dichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552
1,1-Dichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552
1,2-Dichloropropane ND 0.00100 1 12/05/2016 00:07 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:07 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:07 WG931552
Ethylbenzene ND 0.00100 1 12/05/2016 00:07 WG931552
2-Hexanone ND 0.0100 1 12/05/2016 00:07 WG931552
Iodomethane ND J4 0.0100 1 12/05/2016 00:07 WG931552
2-Butanone (MEK)ND 0.0100 1 12/05/2016 00:07 WG931552
Methylene Chloride ND 0.00500 1 12/05/2016 00:07 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 00:07 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L875822
MW-24R
Collected date/time: 11/30/16 11:06
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/05/2016 00:07 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:07 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:07 WG931552
Tetrachloroethene ND 0.00100 1 12/05/2016 00:07 WG931552
Toluene ND 0.00500 1 12/05/2016 00:07 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 00:07 WG931552
Trichloroethene ND 0.00100 1 12/05/2016 00:07 WG931552
Trichlorofluoromethane ND 0.00500 1 12/05/2016 00:07 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 00:07 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 02:12 WG931552
Vinyl chloride ND 0.00100 1 12/05/2016 00:07 WG931552
Xylenes, Total ND 0.00300 1 12/05/2016 00:07 WG931552
(S) Toluene-d8 103 90.0-115 12/05/2016 00:07 WG931552
(S) Toluene-d8 100 90.0-115 12/08/2016 02:12 WG931552
(S) Dibromofluoromethane 89.1 79.0-121 12/08/2016 02:12 WG931552
(S) Dibromofluoromethane 98.7 79.0-121 12/05/2016 00:07 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/05/2016 00:07 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 02:12 WG931552
(S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 02:12 WG931552
(S) 4-Bromofluorobenzene 103 80.1-120 12/05/2016 00:07 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L875822
MW-25R
Collected date/time: 11/30/16 10:30
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0219 0.00500 1 12/06/2016 07:49 WG931506
Chromium ND 0.0100 1 12/06/2016 07:49 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:49 WG931506
Nickel ND 0.0100 1 12/06/2016 07:49 WG931506
Silver ND 0.00500 1 12/06/2016 07:49 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:49 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 15:23 WG931509
Arsenic 0.00264 0.00200 1 12/05/2016 15:23 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:23 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:23 WG931509
Copper ND 0.00500 1 12/05/2016 15:23 WG931509
Lead ND 0.00200 1 12/05/2016 15:23 WG931509
Selenium ND 0.00200 1 12/05/2016 15:23 WG931509
Thallium ND 0.00200 1 12/05/2016 15:23 WG931509
Zinc ND 0.0250 1 12/05/2016 15:23 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/05/2016 00:30 WG931552
Acrylonitrile ND 0.0100 1 12/05/2016 00:30 WG931552
Benzene ND 0.00100 1 12/05/2016 00:30 WG931552
Bromochloromethane ND 0.00100 1 12/05/2016 00:30 WG931552
Bromodichloromethane ND 0.00100 1 12/05/2016 00:30 WG931552
Bromoform ND 0.00100 1 12/05/2016 00:30 WG931552
Bromomethane ND 0.00500 1 12/05/2016 00:30 WG931552
Carbon disulfide ND 0.00100 1 12/05/2016 00:30 WG931552
Carbon tetrachloride ND 0.00100 1 12/05/2016 00:30 WG931552
Chlorobenzene ND 0.00100 1 12/05/2016 00:30 WG931552
Chlorodibromomethane ND 0.00100 1 12/05/2016 00:30 WG931552
Chloroethane ND 0.00500 1 12/05/2016 00:30 WG931552
Chloroform ND 0.00500 1 12/05/2016 00:30 WG931552
Chloromethane ND 0.00250 1 12/05/2016 00:30 WG931552
Dibromomethane ND 0.00100 1 12/05/2016 00:30 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 00:30 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/05/2016 00:30 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 00:30 WG931552
1,1-Dichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552
1,2-Dichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552
1,1-Dichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552
1,2-Dichloropropane ND 0.00100 1 12/05/2016 00:30 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:30 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:30 WG931552
Ethylbenzene ND 0.00100 1 12/05/2016 00:30 WG931552
2-Hexanone ND 0.0100 1 12/05/2016 00:30 WG931552
Iodomethane ND J4 0.0100 1 12/05/2016 00:30 WG931552
2-Butanone (MEK)ND 0.0100 1 12/05/2016 00:30 WG931552
Methylene Chloride ND 0.00500 1 12/05/2016 00:30 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 00:30 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L875822
MW-25R
Collected date/time: 11/30/16 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/05/2016 00:30 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:30 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:30 WG931552
Tetrachloroethene ND 0.00100 1 12/05/2016 00:30 WG931552
Toluene ND 0.00500 1 12/05/2016 00:30 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 00:30 WG931552
Trichloroethene ND 0.00100 1 12/05/2016 00:30 WG931552
Trichlorofluoromethane ND 0.00500 1 12/05/2016 00:30 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 00:30 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 02:25 WG931552
Vinyl chloride ND 0.00100 1 12/05/2016 00:30 WG931552
Xylenes, Total ND 0.00300 1 12/05/2016 00:30 WG931552
(S) Toluene-d8 103 90.0-115 12/05/2016 00:30 WG931552
(S) Toluene-d8 100 90.0-115 12/08/2016 02:25 WG931552
(S) Dibromofluoromethane 88.2 79.0-121 12/08/2016 02:25 WG931552
(S) Dibromofluoromethane 99.0 79.0-121 12/05/2016 00:30 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/05/2016 00:30 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 02:25 WG931552
(S) 4-Bromofluorobenzene 99.0 80.1-120 12/08/2016 02:25 WG931552
(S) 4-Bromofluorobenzene 104 80.1-120 12/05/2016 00:30 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L875822
SW-1
Collected date/time: 12/01/16 13:17
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.109 0.00500 1 12/06/2016 07:52 WG931506
Chromium ND 0.0100 1 12/06/2016 07:52 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:52 WG931506
Nickel ND 0.0100 1 12/06/2016 07:52 WG931506
Silver ND 0.00500 1 12/06/2016 07:52 WG931506
Vanadium ND 0.0200 1 12/06/2016 07:52 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 15:26 WG931509
Arsenic 0.00267 0.00200 1 12/05/2016 15:26 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:26 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:26 WG931509
Copper ND 0.00500 1 12/05/2016 15:26 WG931509
Lead ND 0.00200 1 12/05/2016 15:26 WG931509
Selenium ND 0.00200 1 12/05/2016 15:26 WG931509
Thallium ND 0.00200 1 12/05/2016 15:26 WG931509
Zinc ND 0.0250 1 12/05/2016 15:26 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/05/2016 00:53 WG931552
Acrylonitrile ND 0.0100 1 12/05/2016 00:53 WG931552
Benzene ND 0.00100 1 12/05/2016 00:53 WG931552
Bromochloromethane ND 0.00100 1 12/05/2016 00:53 WG931552
Bromodichloromethane ND 0.00100 1 12/05/2016 00:53 WG931552
Bromoform ND 0.00100 1 12/05/2016 00:53 WG931552
Bromomethane ND 0.00500 1 12/05/2016 00:53 WG931552
Carbon disulfide ND 0.00100 1 12/05/2016 00:53 WG931552
Carbon tetrachloride ND 0.00100 1 12/05/2016 00:53 WG931552
Chlorobenzene ND 0.00100 1 12/05/2016 00:53 WG931552
Chlorodibromomethane ND 0.00100 1 12/05/2016 00:53 WG931552
Chloroethane ND 0.00500 1 12/05/2016 00:53 WG931552
Chloroform ND 0.00500 1 12/05/2016 00:53 WG931552
Chloromethane ND 0.00250 1 12/05/2016 00:53 WG931552
Dibromomethane ND 0.00100 1 12/05/2016 00:53 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 00:53 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/05/2016 00:53 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 00:53 WG931552
1,1-Dichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552
1,2-Dichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552
1,1-Dichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552
1,2-Dichloropropane ND 0.00100 1 12/05/2016 00:53 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:53 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 00:53 WG931552
Ethylbenzene ND 0.00100 1 12/05/2016 00:53 WG931552
2-Hexanone ND 0.0100 1 12/05/2016 00:53 WG931552
Iodomethane ND J4 0.0100 1 12/05/2016 00:53 WG931552
2-Butanone (MEK)ND 0.0100 1 12/05/2016 00:53 WG931552
Methylene Chloride ND 0.00500 1 12/05/2016 00:53 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 00:53 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L875822
SW-1
Collected date/time: 12/01/16 13:17
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/05/2016 00:53 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:53 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 00:53 WG931552
Tetrachloroethene ND 0.00100 1 12/05/2016 00:53 WG931552
Toluene ND 0.00500 1 12/05/2016 00:53 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 00:53 WG931552
Trichloroethene ND 0.00100 1 12/05/2016 00:53 WG931552
Trichlorofluoromethane ND 0.00500 1 12/05/2016 00:53 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 00:53 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 02:37 WG931552
Vinyl chloride ND 0.00100 1 12/05/2016 00:53 WG931552
Xylenes, Total ND 0.00300 1 12/05/2016 00:53 WG931552
(S) Toluene-d8 102 90.0-115 12/05/2016 00:53 WG931552
(S) Toluene-d8 100 90.0-115 12/08/2016 02:37 WG931552
(S) Dibromofluoromethane 86.8 79.0-121 12/08/2016 02:37 WG931552
(S) Dibromofluoromethane 99.2 79.0-121 12/05/2016 00:53 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/05/2016 00:53 WG931552
(S) a,a,a-Trifluorotoluene 101 90.4-116 12/08/2016 02:37 WG931552
(S) 4-Bromofluorobenzene 97.5 80.1-120 12/08/2016 02:37 WG931552
(S) 4-Bromofluorobenzene 104 80.1-120 12/05/2016 00:53 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L875822
TRIP BLANK
Collected date/time: 12/01/16 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 17:58 WG931552
Acrylonitrile ND 0.0100 1 12/04/2016 17:58 WG931552
Benzene ND 0.00100 1 12/04/2016 17:58 WG931552
Bromochloromethane ND 0.00100 1 12/04/2016 17:58 WG931552
Bromodichloromethane ND 0.00100 1 12/04/2016 17:58 WG931552
Bromoform ND 0.00100 1 12/04/2016 17:58 WG931552
Bromomethane ND 0.00500 1 12/04/2016 17:58 WG931552
Carbon disulfide ND 0.00100 1 12/04/2016 17:58 WG931552
Carbon tetrachloride ND 0.00100 1 12/04/2016 17:58 WG931552
Chlorobenzene ND 0.00100 1 12/04/2016 17:58 WG931552
Chlorodibromomethane ND 0.00100 1 12/04/2016 17:58 WG931552
Chloroethane ND 0.00500 1 12/04/2016 17:58 WG931552
Chloroform ND 0.00500 1 12/04/2016 17:58 WG931552
Chloromethane ND 0.00250 1 12/04/2016 17:58 WG931552
Dibromomethane ND 0.00100 1 12/04/2016 17:58 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 17:58 WG931552
1,4-Dichlorobenzene ND 0.00100 1 12/04/2016 17:58 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 17:58 WG931552
1,1-Dichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552
1,2-Dichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552
1,1-Dichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552
1,2-Dichloropropane ND 0.00100 1 12/04/2016 17:58 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:58 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:58 WG931552
Ethylbenzene ND 0.00100 1 12/04/2016 17:58 WG931552
2-Hexanone ND 0.0100 1 12/04/2016 17:58 WG931552
Iodomethane ND J4 0.0100 1 12/04/2016 17:58 WG931552
2-Butanone (MEK)ND 0.0100 1 12/04/2016 17:58 WG931552
Methylene Chloride ND 0.00500 1 12/04/2016 17:58 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 17:58 WG931552
Styrene ND 0.00100 1 12/04/2016 17:58 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:58 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:58 WG931552
Tetrachloroethene ND 0.00100 1 12/04/2016 17:58 WG931552
Toluene ND 0.00500 1 12/04/2016 17:58 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 17:58 WG931552
Trichloroethene ND 0.00100 1 12/04/2016 17:58 WG931552
Trichlorofluoromethane ND 0.00500 1 12/04/2016 17:58 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 17:58 WG931552
Vinyl acetate ND 0.0100 1 12/07/2016 22:39 WG931552
Vinyl chloride ND 0.00100 1 12/04/2016 17:58 WG931552
Xylenes, Total ND 0.00300 1 12/04/2016 17:58 WG931552
(S) Toluene-d8 104 90.0-115 12/04/2016 17:58 WG931552
(S) Toluene-d8 99.3 90.0-115 12/07/2016 22:39 WG931552
(S) Dibromofluoromethane 85.8 79.0-121 12/07/2016 22:39 WG931552
(S) Dibromofluoromethane 98.3 79.0-121 12/04/2016 17:58 WG931552
(S) a,a,a-Trifluorotoluene 105 90.4-116 12/04/2016 17:58 WG931552
(S) a,a,a-Trifluorotoluene 99.7 90.4-116 12/07/2016 22:39 WG931552
(S) 4-Bromofluorobenzene 100 80.1-120 12/07/2016 22:39 WG931552
(S) 4-Bromofluorobenzene 104 80.1-120 12/04/2016 17:58 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L875822
LEACHATE PHASE 2
Collected date/time: 12/01/16 14:30
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Phosphorus,Total 0.332 B 0.100 1 12/07/2016 14:25 WG932178
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 418 10.0 1 12/02/2016 20:28 WG931630
Wet Chemistry by Method 5210 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
BOD 15.0 10.0 1 12/07/2016 10:31 WG931445
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Nitrate as (N)ND 0.100 1 12/03/2016 01:35 WG931491
Sulfate ND 5.00 1 12/03/2016 01:35 WG931491
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.320 0.00500 1 12/06/2016 07:55 WG931506
Chromium 0.0149 0.0100 1 12/06/2016 07:55 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:55 WG931506
Nickel 0.0187 0.0100 1 12/06/2016 07:55 WG931506
Silver ND 0.00500 1 12/06/2016 07:55 WG931506
Vanadium 0.0233 0.0200 1 12/06/2016 07:55 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/05/2016 15:30 WG931509
Arsenic 0.0196 0.00200 1 12/05/2016 15:30 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:30 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:30 WG931509
Copper 0.0597 0.00500 1 12/05/2016 15:30 WG931509
Lead 0.00614 0.00200 1 12/05/2016 15:30 WG931509
Selenium ND 0.00200 1 12/05/2016 15:30 WG931509
Thallium ND 0.00200 1 12/05/2016 15:30 WG931509
Zinc 0.0401 0.0250 1 12/05/2016 15:30 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/05/2016 01:16 WG931552
Acrylonitrile ND 0.0100 1 12/05/2016 01:16 WG931552
Benzene 0.00694 0.00100 1 12/05/2016 01:16 WG931552
Bromochloromethane ND 0.00100 1 12/05/2016 01:16 WG931552
Bromodichloromethane ND 0.00100 1 12/05/2016 01:16 WG931552
Bromoform ND 0.00100 1 12/05/2016 01:16 WG931552
Bromomethane ND 0.00500 1 12/05/2016 01:16 WG931552
Carbon disulfide ND 0.00100 1 12/05/2016 01:16 WG931552
Carbon tetrachloride ND 0.00100 1 12/05/2016 01:16 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L875822
LEACHATE PHASE 2
Collected date/time: 12/01/16 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chlorobenzene 0.00233 0.00100 1 12/05/2016 01:16 WG931552
Chlorodibromomethane ND 0.00100 1 12/05/2016 01:16 WG931552
Chloroethane ND 0.00500 1 12/05/2016 01:16 WG931552
Chloroform ND 0.00500 1 12/05/2016 01:16 WG931552
Chloromethane ND 0.00250 1 12/05/2016 01:16 WG931552
Dibromomethane ND 0.00100 1 12/05/2016 01:16 WG931552
1,2-Dichlorobenzene ND 0.00100 1 12/05/2016 01:16 WG931552
1,4-Dichlorobenzene 0.0160 0.00100 1 12/05/2016 01:16 WG931552
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/05/2016 01:16 WG931552
1,1-Dichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552
1,2-Dichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552
1,1-Dichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552
cis-1,2-Dichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552
trans-1,2-Dichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552
1,2-Dichloropropane ND 0.00100 1 12/05/2016 01:16 WG931552
cis-1,3-Dichloropropene ND 0.00100 1 12/05/2016 01:16 WG931552
trans-1,3-Dichloropropene ND 0.00100 1 12/05/2016 01:16 WG931552
Ethylbenzene ND 0.00100 1 12/05/2016 01:16 WG931552
2-Hexanone ND 0.0100 1 12/05/2016 01:16 WG931552
Iodomethane ND J4 0.0100 1 12/05/2016 01:16 WG931552
2-Butanone (MEK)ND 0.0100 1 12/05/2016 01:16 WG931552
Methylene Chloride ND 0.00500 1 12/05/2016 01:16 WG931552
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/05/2016 01:16 WG931552
Styrene ND 0.00100 1 12/05/2016 01:16 WG931552
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/05/2016 01:16 WG931552
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/05/2016 01:16 WG931552
Tetrachloroethene ND 0.00100 1 12/05/2016 01:16 WG931552
Toluene ND 0.00500 1 12/05/2016 01:16 WG931552
1,1,1-Trichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552
1,1,2-Trichloroethane ND 0.00100 1 12/05/2016 01:16 WG931552
Trichloroethene ND 0.00100 1 12/05/2016 01:16 WG931552
Trichlorofluoromethane ND 0.00500 1 12/05/2016 01:16 WG931552
1,2,3-Trichloropropane ND 0.00250 1 12/05/2016 01:16 WG931552
Vinyl acetate ND 0.0100 1 12/08/2016 02:49 WG931552
Vinyl chloride ND 0.00100 1 12/05/2016 01:16 WG931552
Xylenes, Total 0.0200 0.00300 1 12/05/2016 01:16 WG931552
(S) Toluene-d8 102 90.0-115 12/05/2016 01:16 WG931552
(S) Toluene-d8 101 90.0-115 12/08/2016 02:49 WG931552
(S) Dibromofluoromethane 86.1 79.0-121 12/08/2016 02:49 WG931552
(S) Dibromofluoromethane 99.1 79.0-121 12/05/2016 01:16 WG931552
(S) a,a,a-Trifluorotoluene 104 90.4-116 12/05/2016 01:16 WG931552
(S) a,a,a-Trifluorotoluene 103 90.4-116 12/08/2016 02:49 WG931552
(S) 4-Bromofluorobenzene 100 80.1-120 12/08/2016 02:49 WG931552
(S) 4-Bromofluorobenzene 105 80.1-120 12/05/2016 01:16 WG931552
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L875822
LEACHATE PHASE 3
Collected date/time: 12/01/16 14:40
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Phosphorus,Total 0.824 0.100 1 12/07/2016 14:26 WG932178
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 634 10.0 1 12/02/2016 20:28 WG931630
Wet Chemistry by Method 5210 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
BOD 17.9 10.0 1 12/07/2016 10:34 WG931445
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Nitrate as (N)0.151 0.100 1 12/03/2016 01:50 WG931491
Sulfate 62.1 5.00 1 12/03/2016 01:50 WG931491
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.218 0.00500 1 12/06/2016 07:57 WG931506
Chromium 0.0194 0.0100 1 12/06/2016 07:57 WG931506
Cobalt ND 0.0100 1 12/06/2016 07:57 WG931506
Nickel 0.0574 0.0100 1 12/06/2016 07:57 WG931506
Silver ND 0.00500 1 12/06/2016 07:57 WG931506
Vanadium 0.0401 0.0200 1 12/06/2016 07:57 WG931506
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0100 5 12/05/2016 15:54 WG931509
Arsenic 0.0366 0.0100 5 12/05/2016 15:54 WG931509
Beryllium ND 0.00200 1 12/05/2016 15:33 WG931509
Cadmium ND 0.00100 1 12/05/2016 15:33 WG931509
Copper 1.49 0.0250 5 12/05/2016 15:54 WG931509
Lead 0.212 0.00200 1 12/05/2016 15:33 WG931509
Selenium ND 0.00200 1 12/05/2016 15:33 WG931509
Thallium ND 0.00200 1 12/05/2016 15:33 WG931509
Zinc 0.369 0.125 5 12/05/2016 15:54 WG931509
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 17:48 WG931684
Acrylonitrile ND 0.0100 1 12/04/2016 17:48 WG931684
Benzene 0.00507 0.00100 1 12/04/2016 17:48 WG931684
Bromochloromethane ND 0.00100 1 12/04/2016 17:48 WG931684
Bromodichloromethane ND 0.00100 1 12/04/2016 17:48 WG931684
Bromoform ND 0.00100 1 12/04/2016 17:48 WG931684
Bromomethane ND 0.00500 1 12/04/2016 17:48 WG931684
Carbon disulfide ND 0.00100 1 12/04/2016 17:48 WG931684
Carbon tetrachloride ND 0.00100 1 12/04/2016 17:48 WG931684
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L875822
LEACHATE PHASE 3
Collected date/time: 12/01/16 14:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chlorobenzene 0.00271 0.00100 1 12/04/2016 17:48 WG931684
Chlorodibromomethane ND 0.00100 1 12/04/2016 17:48 WG931684
Chloroethane ND 0.00500 1 12/04/2016 17:48 WG931684
Chloroform ND 0.00500 1 12/04/2016 17:48 WG931684
Chloromethane ND 0.00250 1 12/04/2016 17:48 WG931684
Dibromomethane ND 0.00100 1 12/04/2016 17:48 WG931684
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 17:48 WG931684
1,4-Dichlorobenzene 0.0101 0.00100 1 12/04/2016 17:48 WG931684
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 17:48 WG931684
1,1-Dichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684
1,2-Dichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684
1,1-Dichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684
1,2-Dichloropropane ND 0.00100 1 12/04/2016 17:48 WG931684
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:48 WG931684
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 17:48 WG931684
Ethylbenzene 0.00611 0.00100 1 12/04/2016 17:48 WG931684
2-Hexanone ND 0.0100 1 12/04/2016 17:48 WG931684
Iodomethane ND 0.0100 1 12/04/2016 17:48 WG931684
2-Butanone (MEK)ND 0.0100 1 12/04/2016 17:48 WG931684
Methylene Chloride ND 0.00500 1 12/04/2016 17:48 WG931684
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 17:48 WG931684
Styrene ND 0.00100 1 12/04/2016 17:48 WG931684
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:48 WG931684
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 17:48 WG931684
Tetrachloroethene ND 0.00100 1 12/04/2016 17:48 WG931684
Toluene ND 0.00500 1 12/04/2016 17:48 WG931684
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 17:48 WG931684
Trichloroethene ND 0.00100 1 12/04/2016 17:48 WG931684
Trichlorofluoromethane ND 0.00500 1 12/04/2016 17:48 WG931684
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 17:48 WG931684
Vinyl acetate ND 0.0100 1 12/04/2016 17:48 WG931684
Vinyl chloride ND 0.00100 1 12/04/2016 17:48 WG931684
Xylenes, Total 0.0381 0.00300 1 12/04/2016 17:48 WG931684
(S) Toluene-d8 105 90.0-115 12/04/2016 17:48 WG931684
(S) Dibromofluoromethane 97.2 79.0-121 12/04/2016 17:48 WG931684
(S) a,a,a-Trifluorotoluene 107 90.4-116 12/04/2016 17:48 WG931684
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 17:48 WG931684
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22
L875822
LEACHATE PHASE 4
Collected date/time: 12/01/16 14:52
Wet Chemistry by Method 365.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Phosphorus,Total 1.30 0.100 1 12/07/2016 14:28 WG932178
Wet Chemistry by Method 410.4
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
COD 1420 250 25 12/02/2016 20:29 WG931630
Wet Chemistry by Method 5210 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
BOD 69.0 33.3 10 12/07/2016 10:37 WG931445
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Nitrate as (N)ND 0.100 1 12/03/2016 02:04 WG931491
Sulfate 16.4 5.00 1 12/03/2016 02:04 WG931491
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.147 0.0450 9 12/05/2016 08:56 WG931720
Chromium ND 0.0900 9 12/05/2016 08:56 WG931720
Cobalt ND 0.0900 9 12/05/2016 08:56 WG931720
Nickel 0.132 0.0900 9 12/05/2016 08:56 WG931720
Silver ND 0.0450 9 12/05/2016 08:56 WG931720
Vanadium ND 0.180 9 12/05/2016 08:56 WG931720
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.0180 9 12/06/2016 11:05 WG931723
Arsenic 0.125 0.0180 9 12/06/2016 11:05 WG931723
Beryllium ND 0.0180 9 12/06/2016 11:05 WG931723
Cadmium ND 0.00900 9 12/06/2016 11:05 WG931723
Copper ND 0.0450 9 12/06/2016 19:59 WG932463
Lead ND 0.0180 9 12/06/2016 11:05 WG931723
Selenium ND 0.0180 9 12/06/2016 11:05 WG931723
Thallium ND 0.0180 9 12/06/2016 11:05 WG931723
Zinc ND 0.225 9 12/06/2016 11:05 WG931723
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/04/2016 19:13 WG931684
Acrylonitrile ND 0.0100 1 12/04/2016 19:13 WG931684
Benzene 0.00959 0.00100 1 12/04/2016 19:13 WG931684
Bromochloromethane ND 0.00100 1 12/04/2016 19:13 WG931684
Bromodichloromethane ND 0.00100 1 12/04/2016 19:13 WG931684
Bromoform ND 0.00100 1 12/04/2016 19:13 WG931684
Bromomethane ND 0.00500 1 12/04/2016 19:13 WG931684
Carbon disulfide ND 0.00100 1 12/04/2016 19:13 WG931684
Carbon tetrachloride ND 0.00100 1 12/04/2016 19:13 WG931684
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22
L875822
LEACHATE PHASE 4
Collected date/time: 12/01/16 14:52
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chlorobenzene ND 0.00100 1 12/04/2016 19:13 WG931684
Chlorodibromomethane ND 0.00100 1 12/04/2016 19:13 WG931684
Chloroethane ND 0.00500 1 12/04/2016 19:13 WG931684
Chloroform ND 0.00500 1 12/04/2016 19:13 WG931684
Chloromethane ND 0.00250 1 12/04/2016 19:13 WG931684
Dibromomethane ND 0.00100 1 12/04/2016 19:13 WG931684
1,2-Dichlorobenzene ND 0.00100 1 12/04/2016 19:13 WG931684
1,4-Dichlorobenzene 0.00379 0.00100 1 12/04/2016 19:13 WG931684
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/04/2016 19:13 WG931684
1,1-Dichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684
1,2-Dichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684
1,1-Dichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684
cis-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684
trans-1,2-Dichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684
1,2-Dichloropropane ND 0.00100 1 12/04/2016 19:13 WG931684
cis-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:13 WG931684
trans-1,3-Dichloropropene ND 0.00100 1 12/04/2016 19:13 WG931684
Ethylbenzene 0.00899 0.00100 1 12/04/2016 19:13 WG931684
2-Hexanone ND 0.0100 1 12/04/2016 19:13 WG931684
Iodomethane ND 0.0100 1 12/04/2016 19:13 WG931684
2-Butanone (MEK)ND 0.0100 1 12/04/2016 19:13 WG931684
Methylene Chloride ND 0.00500 1 12/04/2016 19:13 WG931684
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/04/2016 19:13 WG931684
Styrene ND 0.00100 1 12/04/2016 19:13 WG931684
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:13 WG931684
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/04/2016 19:13 WG931684
Tetrachloroethene ND 0.00100 1 12/04/2016 19:13 WG931684
Toluene ND 0.00500 1 12/04/2016 19:13 WG931684
1,1,1-Trichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684
1,1,2-Trichloroethane ND 0.00100 1 12/04/2016 19:13 WG931684
Trichloroethene ND 0.00100 1 12/04/2016 19:13 WG931684
Trichlorofluoromethane ND 0.00500 1 12/04/2016 19:13 WG931684
1,2,3-Trichloropropane ND 0.00250 1 12/04/2016 19:13 WG931684
Vinyl acetate ND 0.0100 1 12/04/2016 19:13 WG931684
Vinyl chloride ND 0.00100 1 12/04/2016 19:13 WG931684
Xylenes, Total 0.0217 0.00300 1 12/04/2016 19:13 WG931684
(S) Toluene-d8 105 90.0-115 12/04/2016 19:13 WG931684
(S) Dibromofluoromethane 91.9 79.0-121 12/04/2016 19:13 WG931684
(S) a,a,a-Trifluorotoluene 111 90.4-116 12/04/2016 19:13 WG931684
(S) 4-Bromofluorobenzene 105 80.1-120 12/04/2016 19:13 WG931684
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23
L875822
MW-10
Collected date/time: 12/02/16 09:46
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0532 0.00500 1 12/07/2016 16:09 WG932146
Chromium 0.0122 B 0.0100 1 12/07/2016 16:09 WG932146
Cobalt ND 0.0100 1 12/07/2016 16:09 WG932146
Nickel ND 0.0100 1 12/07/2016 16:09 WG932146
Silver ND 0.00500 1 12/07/2016 16:09 WG932146
Vanadium 0.0215 0.0200 1 12/07/2016 16:09 WG932146
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/07/2016 01:42 WG932285
Arsenic ND 0.00200 1 12/07/2016 01:42 WG932285
Beryllium ND 0.00200 1 12/07/2016 01:42 WG932285
Cadmium ND 0.00100 1 12/07/2016 01:42 WG932285
Copper ND 0.00500 1 12/07/2016 01:42 WG932285
Lead 0.00760 0.00200 1 12/07/2016 01:42 WG932285
Selenium ND 0.00200 1 12/07/2016 01:42 WG932285
Thallium ND 0.00200 1 12/07/2016 01:42 WG932285
Zinc 0.0274 B 0.0250 1 12/07/2016 01:42 WG932285
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 J4 0.0500 1 12/08/2016 01:54 WG932369
Acrylonitrile ND 0.0100 1 12/08/2016 01:54 WG932369
Benzene ND 0.00100 1 12/08/2016 01:54 WG932369
Bromochloromethane ND 0.00100 1 12/08/2016 01:54 WG932369
Bromodichloromethane ND 0.00100 1 12/08/2016 01:54 WG932369
Bromoform ND 0.00100 1 12/08/2016 01:54 WG932369
Bromomethane ND 0.00500 1 12/08/2016 01:54 WG932369
Carbon disulfide ND J3 0.00100 1 12/08/2016 01:54 WG932369
Carbon tetrachloride ND 0.00100 1 12/08/2016 01:54 WG932369
Chlorobenzene ND 0.00100 1 12/08/2016 01:54 WG932369
Chlorodibromomethane ND 0.00100 1 12/08/2016 01:54 WG932369
Chloroethane ND 0.00500 1 12/08/2016 01:54 WG932369
Chloroform ND 0.00500 1 12/08/2016 01:54 WG932369
Chloromethane ND 0.00250 1 12/08/2016 01:54 WG932369
Dibromomethane ND 0.00100 1 12/08/2016 01:54 WG932369
1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 01:54 WG932369
1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 01:54 WG932369
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 01:54 WG932369
1,1-Dichloroethane ND 0.00100 1 12/08/2016 01:54 WG932369
1,2-Dichloroethane ND 0.00100 1 12/08/2016 01:54 WG932369
1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 01:54 WG932369
cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 01:54 WG932369
trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 01:54 WG932369
1,2-Dichloropropane ND 0.00100 1 12/08/2016 01:54 WG932369
cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 01:54 WG932369
trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 01:54 WG932369
Ethylbenzene ND 0.00100 1 12/08/2016 01:54 WG932369
2-Hexanone ND 0.0100 1 12/08/2016 01:54 WG932369
Iodomethane ND 0.0100 1 12/08/2016 01:54 WG932369
2-Butanone (MEK)ND 0.0100 1 12/08/2016 01:54 WG932369
Methylene Chloride ND 0.00500 1 12/08/2016 01:54 WG932369
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 01:54 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23
L875822
MW-10
Collected date/time: 12/02/16 09:46
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/08/2016 01:54 WG932369
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 01:54 WG932369
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 01:54 WG932369
Tetrachloroethene ND J3 0.00100 1 12/08/2016 01:54 WG932369
Toluene ND 0.00500 1 12/08/2016 01:54 WG932369
1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 01:54 WG932369
1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 01:54 WG932369
Trichloroethene ND 0.00100 1 12/08/2016 01:54 WG932369
Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 01:54 WG932369
1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 01:54 WG932369
Vinyl acetate ND 0.0100 1 12/08/2016 01:54 WG932369
Vinyl chloride ND J3 0.00100 1 12/08/2016 01:54 WG932369
Xylenes, Total ND J3 0.00300 1 12/08/2016 01:54 WG932369
(S) Toluene-d8 100 90.0-115 12/08/2016 01:54 WG932369
(S) Dibromofluoromethane 104 79.0-121 12/08/2016 01:54 WG932369
(S) a,a,a-Trifluorotoluene 100 90.4-116 12/08/2016 01:54 WG932369
(S) 4-Bromofluorobenzene 96.5 80.1-120 12/08/2016 01:54 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24
L875822
MW-11
Collected date/time: 12/02/16 09:20
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0439 0.00500 1 12/07/2016 16:16 WG932146
Chromium ND 0.0100 1 12/07/2016 16:16 WG932146
Cobalt ND 0.0100 1 12/07/2016 16:16 WG932146
Nickel ND 0.0100 1 12/07/2016 16:16 WG932146
Silver ND 0.00500 1 12/07/2016 16:16 WG932146
Vanadium ND 0.0200 1 12/07/2016 16:16 WG932146
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/07/2016 01:46 WG932285
Arsenic 0.00242 0.00200 1 12/07/2016 01:46 WG932285
Beryllium ND 0.00200 1 12/07/2016 01:46 WG932285
Cadmium ND 0.00100 1 12/07/2016 01:46 WG932285
Copper ND 0.00500 1 12/07/2016 01:46 WG932285
Lead 0.00293 0.00200 1 12/07/2016 01:46 WG932285
Selenium ND 0.00200 1 12/07/2016 01:46 WG932285
Thallium ND 0.00200 1 12/07/2016 01:46 WG932285
Zinc 0.0347 B 0.0250 1 12/07/2016 01:46 WG932285
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 J4 0.0500 1 12/08/2016 02:25 WG932369
Acrylonitrile ND 0.0100 1 12/08/2016 02:25 WG932369
Benzene ND 0.00100 1 12/08/2016 02:25 WG932369
Bromochloromethane ND 0.00100 1 12/08/2016 02:25 WG932369
Bromodichloromethane ND 0.00100 1 12/08/2016 02:25 WG932369
Bromoform ND 0.00100 1 12/08/2016 02:25 WG932369
Bromomethane ND 0.00500 1 12/08/2016 02:25 WG932369
Carbon disulfide ND J3 0.00100 1 12/08/2016 02:25 WG932369
Carbon tetrachloride ND 0.00100 1 12/08/2016 02:25 WG932369
Chlorobenzene ND 0.00100 1 12/08/2016 02:25 WG932369
Chlorodibromomethane ND 0.00100 1 12/08/2016 02:25 WG932369
Chloroethane ND 0.00500 1 12/08/2016 02:25 WG932369
Chloroform ND 0.00500 1 12/08/2016 02:25 WG932369
Chloromethane ND 0.00250 1 12/08/2016 02:25 WG932369
Dibromomethane ND 0.00100 1 12/08/2016 02:25 WG932369
1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 02:25 WG932369
1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 02:25 WG932369
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 02:25 WG932369
1,1-Dichloroethane ND 0.00100 1 12/08/2016 02:25 WG932369
1,2-Dichloroethane ND 0.00100 1 12/08/2016 02:25 WG932369
1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 02:25 WG932369
cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 02:25 WG932369
trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 02:25 WG932369
1,2-Dichloropropane ND 0.00100 1 12/08/2016 02:25 WG932369
cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:25 WG932369
trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:25 WG932369
Ethylbenzene ND 0.00100 1 12/08/2016 02:25 WG932369
2-Hexanone ND 0.0100 1 12/08/2016 02:25 WG932369
Iodomethane ND 0.0100 1 12/08/2016 02:25 WG932369
2-Butanone (MEK)ND 0.0100 1 12/08/2016 02:25 WG932369
Methylene Chloride ND 0.00500 1 12/08/2016 02:25 WG932369
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 02:25 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24
L875822
MW-11
Collected date/time: 12/02/16 09:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/08/2016 02:25 WG932369
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:25 WG932369
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:25 WG932369
Tetrachloroethene ND J3 0.00100 1 12/08/2016 02:25 WG932369
Toluene ND 0.00500 1 12/08/2016 02:25 WG932369
1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 02:25 WG932369
1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 02:25 WG932369
Trichloroethene ND 0.00100 1 12/08/2016 02:25 WG932369
Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 02:25 WG932369
1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 02:25 WG932369
Vinyl acetate ND 0.0100 1 12/08/2016 02:25 WG932369
Vinyl chloride ND J3 0.00100 1 12/08/2016 02:25 WG932369
Xylenes, Total ND J3 0.00300 1 12/08/2016 02:25 WG932369
(S) Toluene-d8 101 90.0-115 12/08/2016 02:25 WG932369
(S) Dibromofluoromethane 106 79.0-121 12/08/2016 02:25 WG932369
(S) a,a,a-Trifluorotoluene 99.6 90.4-116 12/08/2016 02:25 WG932369
(S) 4-Bromofluorobenzene 93.1 80.1-120 12/08/2016 02:25 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25
L875822
MW-20
Collected date/time: 12/02/16 08:45
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dissolved Solids 61.0 10.0 1 12/08/2016 10:32 WG932797
Wet Chemistry by Method 2320 B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Alkalinity ND 20.0 1 12/07/2016 11:57 WG932588
Wet Chemistry by Method 9056A
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Chloride 5.23 1.00 1 12/07/2016 10:38 WG932605
Sulfate 7.35 5.00 1 12/07/2016 10:38 WG932605
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.105 0.00500 1 12/07/2016 16:19 WG932146
Chromium ND 0.0100 1 12/07/2016 16:19 WG932146
Cobalt ND 0.0100 1 12/07/2016 16:19 WG932146
Nickel ND 0.0100 1 12/07/2016 16:19 WG932146
Silver ND 0.00500 1 12/07/2016 16:19 WG932146
Vanadium ND 0.0200 1 12/07/2016 16:19 WG932146
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/07/2016 01:49 WG932285
Arsenic ND 0.00200 1 12/07/2016 01:49 WG932285
Beryllium ND 0.00200 1 12/07/2016 01:49 WG932285
Cadmium ND 0.00100 1 12/07/2016 01:49 WG932285
Copper ND 0.00500 1 12/07/2016 01:49 WG932285
Lead 0.0102 0.00200 1 12/07/2016 01:49 WG932285
Selenium ND 0.00200 1 12/07/2016 01:49 WG932285
Thallium ND 0.00200 1 12/07/2016 01:49 WG932285
Zinc ND 0.0250 1 12/07/2016 01:49 WG932285
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 J4 0.0500 1 12/09/2016 17:32 WG932369
Acrylonitrile ND 0.0100 1 12/09/2016 17:32 WG932369
Benzene ND 0.00100 1 12/09/2016 17:32 WG932369
Bromochloromethane ND 0.00100 1 12/09/2016 17:32 WG932369
Bromodichloromethane ND 0.00100 1 12/09/2016 17:32 WG932369
Bromoform ND 0.00100 1 12/09/2016 17:32 WG932369
Bromomethane ND 0.00500 1 12/09/2016 17:32 WG932369
Carbon disulfide ND J3 0.00100 1 12/09/2016 17:32 WG932369
Carbon tetrachloride ND 0.00100 1 12/09/2016 17:32 WG932369
Chlorobenzene ND 0.00100 1 12/09/2016 17:32 WG932369
Chlorodibromomethane ND 0.00100 1 12/09/2016 17:32 WG932369
Chloroethane ND 0.00500 1 12/09/2016 17:32 WG932369
Chloroform ND 0.00500 1 12/09/2016 17:32 WG932369
Chloromethane ND 0.00250 1 12/09/2016 17:32 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25
L875822
MW-20
Collected date/time: 12/02/16 08:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dibromomethane ND 0.00100 1 12/09/2016 17:32 WG932369
1,2-Dichlorobenzene ND 0.00100 1 12/09/2016 17:32 WG932369
1,4-Dichlorobenzene ND 0.00100 1 12/09/2016 17:32 WG932369
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/09/2016 17:32 WG932369
1,1-Dichloroethane ND 0.00100 1 12/09/2016 17:32 WG932369
1,2-Dichloroethane ND 0.00100 1 12/09/2016 17:32 WG932369
1,1-Dichloroethene ND J3 0.00100 1 12/09/2016 17:32 WG932369
cis-1,2-Dichloroethene ND 0.00100 1 12/09/2016 17:32 WG932369
trans-1,2-Dichloroethene ND J3 0.00100 1 12/09/2016 17:32 WG932369
1,2-Dichloropropane ND 0.00100 1 12/09/2016 17:32 WG932369
cis-1,3-Dichloropropene ND 0.00100 1 12/09/2016 17:32 WG932369
trans-1,3-Dichloropropene ND 0.00100 1 12/09/2016 17:32 WG932369
Ethylbenzene ND 0.00100 1 12/09/2016 17:32 WG932369
2-Hexanone ND 0.0100 1 12/09/2016 17:32 WG932369
Iodomethane ND 0.0100 1 12/09/2016 17:32 WG932369
2-Butanone (MEK)ND 0.0100 1 12/09/2016 17:32 WG932369
Methylene Chloride ND 0.00500 1 12/09/2016 17:32 WG932369
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/09/2016 17:32 WG932369
Styrene ND 0.00100 1 12/09/2016 17:32 WG932369
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/09/2016 17:32 WG932369
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/09/2016 17:32 WG932369
Tetrachloroethene ND J3 0.00100 1 12/09/2016 17:32 WG932369
Toluene ND 0.00500 1 12/09/2016 17:32 WG932369
1,1,1-Trichloroethane ND J3 0.00100 1 12/09/2016 17:32 WG932369
1,1,2-Trichloroethane ND 0.00100 1 12/09/2016 17:32 WG932369
Trichloroethene ND 0.00100 1 12/09/2016 17:32 WG932369
Trichlorofluoromethane ND J3 0.00500 1 12/09/2016 17:32 WG932369
1,2,3-Trichloropropane ND 0.00250 1 12/09/2016 17:32 WG932369
Vinyl acetate ND 0.0100 1 12/09/2016 17:32 WG932369
Vinyl chloride ND J3 0.00100 1 12/09/2016 17:32 WG932369
Xylenes, Total ND J3 0.00300 1 12/09/2016 17:32 WG932369
(S) Toluene-d8 106 90.0-115 12/09/2016 17:32 WG932369
(S) Dibromofluoromethane 104 79.0-121 12/09/2016 17:32 WG932369
(S) a,a,a-Trifluorotoluene 103 90.4-116 12/09/2016 17:32 WG932369
(S) 4-Bromofluorobenzene 96.7 80.1-120 12/09/2016 17:32 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26
L875822
MW-26
Collected date/time: 12/02/16 08:15
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0401 0.00500 1 12/07/2016 15:22 WG932146
Chromium ND 0.0100 1 12/07/2016 15:22 WG932146
Cobalt ND 0.0100 1 12/07/2016 15:22 WG932146
Nickel ND 0.0100 1 12/07/2016 15:22 WG932146
Silver ND 0.00500 1 12/07/2016 15:22 WG932146
Vanadium ND 0.0200 1 12/07/2016 15:22 WG932146
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/07/2016 01:53 WG932285
Arsenic ND 0.00200 1 12/07/2016 01:53 WG932285
Beryllium ND 0.00200 1 12/07/2016 01:53 WG932285
Cadmium ND 0.00100 1 12/07/2016 01:53 WG932285
Copper ND 0.00500 1 12/07/2016 01:53 WG932285
Lead ND 0.00200 1 12/07/2016 01:53 WG932285
Selenium ND 0.00200 1 12/07/2016 01:53 WG932285
Thallium ND 0.00200 1 12/07/2016 01:53 WG932285
Zinc ND 0.0250 1 12/07/2016 01:53 WG932285
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 J4 0.0500 1 12/08/2016 02:57 WG932369
Acrylonitrile ND 0.0100 1 12/08/2016 02:57 WG932369
Benzene ND 0.00100 1 12/08/2016 02:57 WG932369
Bromochloromethane ND 0.00100 1 12/08/2016 02:57 WG932369
Bromodichloromethane ND 0.00100 1 12/08/2016 02:57 WG932369
Bromoform ND 0.00100 1 12/08/2016 02:57 WG932369
Bromomethane ND 0.00500 1 12/08/2016 02:57 WG932369
Carbon disulfide ND J3 0.00100 1 12/08/2016 02:57 WG932369
Carbon tetrachloride ND 0.00100 1 12/08/2016 02:57 WG932369
Chlorobenzene ND 0.00100 1 12/08/2016 02:57 WG932369
Chlorodibromomethane ND 0.00100 1 12/08/2016 02:57 WG932369
Chloroethane ND 0.00500 1 12/08/2016 02:57 WG932369
Chloroform ND 0.00500 1 12/08/2016 02:57 WG932369
Chloromethane ND 0.00250 1 12/08/2016 02:57 WG932369
Dibromomethane ND 0.00100 1 12/08/2016 02:57 WG932369
1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 02:57 WG932369
1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 02:57 WG932369
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 02:57 WG932369
1,1-Dichloroethane ND 0.00100 1 12/08/2016 02:57 WG932369
1,2-Dichloroethane ND 0.00100 1 12/08/2016 02:57 WG932369
1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 02:57 WG932369
cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 02:57 WG932369
trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 02:57 WG932369
1,2-Dichloropropane ND 0.00100 1 12/08/2016 02:57 WG932369
cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:57 WG932369
trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 02:57 WG932369
Ethylbenzene ND 0.00100 1 12/08/2016 02:57 WG932369
2-Hexanone ND 0.0100 1 12/08/2016 02:57 WG932369
Iodomethane ND 0.0100 1 12/08/2016 02:57 WG932369
2-Butanone (MEK)ND 0.0100 1 12/08/2016 02:57 WG932369
Methylene Chloride ND 0.00500 1 12/08/2016 02:57 WG932369
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 02:57 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26
L875822
MW-26
Collected date/time: 12/02/16 08:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/08/2016 02:57 WG932369
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:57 WG932369
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 02:57 WG932369
Tetrachloroethene ND J3 0.00100 1 12/08/2016 02:57 WG932369
Toluene ND 0.00500 1 12/08/2016 02:57 WG932369
1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 02:57 WG932369
1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 02:57 WG932369
Trichloroethene ND 0.00100 1 12/08/2016 02:57 WG932369
Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 02:57 WG932369
1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 02:57 WG932369
Vinyl acetate ND 0.0100 1 12/08/2016 02:57 WG932369
Vinyl chloride ND J3 0.00100 1 12/08/2016 02:57 WG932369
Xylenes, Total ND J3 0.00300 1 12/08/2016 02:57 WG932369
(S) Toluene-d8 99.9 90.0-115 12/08/2016 02:57 WG932369
(S) Dibromofluoromethane 106 79.0-121 12/08/2016 02:57 WG932369
(S) a,a,a-Trifluorotoluene 99.7 90.4-116 12/08/2016 02:57 WG932369
(S) 4-Bromofluorobenzene 94.5 80.1-120 12/08/2016 02:57 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27
L875822
TRIP BLANK
Collected date/time: 12/01/16 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND J3 J4 0.0500 1 12/08/2016 13:39 WG932369
Acrylonitrile ND 0.0100 1 12/08/2016 13:39 WG932369
Benzene ND 0.00100 1 12/08/2016 13:39 WG932369
Bromochloromethane ND 0.00100 1 12/08/2016 13:39 WG932369
Bromodichloromethane ND 0.00100 1 12/08/2016 13:39 WG932369
Bromoform ND 0.00100 1 12/08/2016 13:39 WG932369
Bromomethane ND 0.00500 1 12/08/2016 13:39 WG932369
Carbon disulfide ND J3 0.00100 1 12/08/2016 13:39 WG932369
Carbon tetrachloride ND 0.00100 1 12/08/2016 13:39 WG932369
Chlorobenzene ND 0.00100 1 12/08/2016 13:39 WG932369
Chlorodibromomethane ND 0.00100 1 12/08/2016 13:39 WG932369
Chloroethane ND 0.00500 1 12/08/2016 13:39 WG932369
Chloroform ND 0.00500 1 12/08/2016 13:39 WG932369
Chloromethane ND 0.00250 1 12/08/2016 13:39 WG932369
Dibromomethane ND 0.00100 1 12/08/2016 13:39 WG932369
1,2-Dichlorobenzene ND 0.00100 1 12/08/2016 13:39 WG932369
1,4-Dichlorobenzene ND 0.00100 1 12/08/2016 13:39 WG932369
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/08/2016 13:39 WG932369
1,1-Dichloroethane ND 0.00100 1 12/08/2016 13:39 WG932369
1,2-Dichloroethane ND 0.00100 1 12/08/2016 13:39 WG932369
1,1-Dichloroethene ND J3 0.00100 1 12/08/2016 13:39 WG932369
cis-1,2-Dichloroethene ND 0.00100 1 12/08/2016 13:39 WG932369
trans-1,2-Dichloroethene ND J3 0.00100 1 12/08/2016 13:39 WG932369
1,2-Dichloropropane ND 0.00100 1 12/08/2016 13:39 WG932369
cis-1,3-Dichloropropene ND 0.00100 1 12/08/2016 13:39 WG932369
trans-1,3-Dichloropropene ND 0.00100 1 12/08/2016 13:39 WG932369
Ethylbenzene ND 0.00100 1 12/08/2016 13:39 WG932369
2-Hexanone ND 0.0100 1 12/08/2016 13:39 WG932369
Iodomethane ND 0.0100 1 12/08/2016 13:39 WG932369
2-Butanone (MEK)ND 0.0100 1 12/08/2016 13:39 WG932369
Methylene Chloride ND 0.00500 1 12/08/2016 13:39 WG932369
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/08/2016 13:39 WG932369
Styrene ND 0.00100 1 12/08/2016 13:39 WG932369
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/08/2016 13:39 WG932369
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/08/2016 13:39 WG932369
Tetrachloroethene ND J3 0.00100 1 12/08/2016 13:39 WG932369
Toluene ND 0.00500 1 12/08/2016 13:39 WG932369
1,1,1-Trichloroethane ND J3 0.00100 1 12/08/2016 13:39 WG932369
1,1,2-Trichloroethane ND 0.00100 1 12/08/2016 13:39 WG932369
Trichloroethene ND 0.00100 1 12/08/2016 13:39 WG932369
Trichlorofluoromethane ND J3 0.00500 1 12/08/2016 13:39 WG932369
1,2,3-Trichloropropane ND 0.00250 1 12/08/2016 13:39 WG932369
Vinyl acetate ND 0.0100 1 12/08/2016 13:39 WG932369
Vinyl chloride ND J3 0.00100 1 12/08/2016 13:39 WG932369
Xylenes, Total ND J3 0.00300 1 12/08/2016 13:39 WG932369
(S) Toluene-d8 100 90.0-115 12/08/2016 13:39 WG932369
(S) Dibromofluoromethane 108 79.0-121 12/08/2016 13:39 WG932369
(S) a,a,a-Trifluorotoluene 98.6 90.4-116 12/08/2016 13:39 WG932369
(S) 4-Bromofluorobenzene 91.9 80.1-120 12/08/2016 13:39 WG932369
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28
L875822
MW-6
Collected date/time: 12/05/16 14:21
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Barium 0.0120 0.00500 1 12/07/2016 16:22 WG932146
Chromium ND 0.0100 1 12/07/2016 16:22 WG932146
Cobalt ND 0.0100 1 12/07/2016 16:22 WG932146
Nickel ND 0.0100 1 12/07/2016 16:22 WG932146
Silver ND 0.00500 1 12/07/2016 16:22 WG932146
Vanadium ND 0.0200 1 12/07/2016 16:22 WG932146
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Antimony ND 0.00200 1 12/07/2016 18:25 WG932780
Arsenic ND 0.00200 1 12/07/2016 18:25 WG932780
Beryllium ND 0.00200 1 12/07/2016 18:25 WG932780
Cadmium ND 0.00100 1 12/07/2016 18:25 WG932780
Copper ND 0.00500 1 12/07/2016 18:25 WG932780
Lead ND 0.00200 1 12/07/2016 18:25 WG932780
Selenium ND 0.00200 1 12/07/2016 18:25 WG932780
Thallium ND 0.00200 1 12/07/2016 18:25 WG932780
Zinc ND 0.0250 1 12/07/2016 18:25 WG932780
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acetone ND 0.0500 1 12/09/2016 16:09 WG933189
Acrylonitrile ND 0.0100 1 12/09/2016 16:09 WG933189
Benzene ND 0.00100 1 12/09/2016 16:09 WG933189
Bromochloromethane ND 0.00100 1 12/09/2016 16:09 WG933189
Bromodichloromethane ND 0.00100 1 12/09/2016 16:09 WG933189
Bromoform ND 0.00100 1 12/09/2016 16:09 WG933189
Bromomethane ND J3 0.00500 1 12/09/2016 13:28 WG933189
Carbon disulfide ND 0.00100 1 12/09/2016 16:09 WG933189
Carbon tetrachloride ND 0.00100 1 12/09/2016 16:09 WG933189
Chlorobenzene ND 0.00100 1 12/09/2016 16:09 WG933189
Chlorodibromomethane ND 0.00100 1 12/09/2016 16:09 WG933189
Chloroethane ND 0.00500 1 12/09/2016 16:09 WG933189
Chloroform ND 0.00500 1 12/09/2016 16:09 WG933189
Chloromethane ND 0.00250 1 12/09/2016 16:09 WG933189
Dibromomethane ND 0.00100 1 12/09/2016 16:09 WG933189
1,2-Dichlorobenzene ND 0.00100 1 12/09/2016 16:09 WG933189
1,4-Dichlorobenzene ND 0.00100 1 12/09/2016 16:09 WG933189
trans-1,4-Dichloro-2-butene ND 0.00250 1 12/09/2016 16:09 WG933189
1,1-Dichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189
1,2-Dichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189
1,1-Dichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189
cis-1,2-Dichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189
trans-1,2-Dichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189
1,2-Dichloropropane ND 0.00100 1 12/09/2016 16:09 WG933189
cis-1,3-Dichloropropene ND 0.00100 1 12/09/2016 16:09 WG933189
trans-1,3-Dichloropropene ND 0.00100 1 12/09/2016 16:09 WG933189
Ethylbenzene ND 0.00100 1 12/09/2016 16:09 WG933189
2-Hexanone ND 0.0100 1 12/09/2016 16:09 WG933189
Iodomethane ND J4 0.0100 1 12/09/2016 16:09 WG933189
2-Butanone (MEK)ND 0.0100 1 12/09/2016 16:09 WG933189
Methylene Chloride ND 0.00500 1 12/09/2016 16:09 WG933189
4-Methyl-2-pentanone (MIBK)ND 0.0100 1 12/09/2016 16:09 WG933189
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28
L875822
MW-6
Collected date/time: 12/05/16 14:21
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Styrene ND 0.00100 1 12/09/2016 16:09 WG933189
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/09/2016 16:09 WG933189
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/09/2016 16:09 WG933189
Tetrachloroethene ND 0.00100 1 12/09/2016 16:09 WG933189
Toluene ND 0.00500 1 12/09/2016 16:09 WG933189
1,1,1-Trichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189
1,1,2-Trichloroethane ND 0.00100 1 12/09/2016 16:09 WG933189
Trichloroethene ND 0.00100 1 12/09/2016 16:09 WG933189
Trichlorofluoromethane ND 0.00500 1 12/09/2016 16:09 WG933189
1,2,3-Trichloropropane ND 0.00250 1 12/09/2016 16:09 WG933189
Vinyl acetate ND 0.0100 1 12/09/2016 16:09 WG933189
Vinyl chloride ND 0.00100 1 12/09/2016 16:09 WG933189
Xylenes, Total ND 0.00300 1 12/09/2016 16:09 WG933189
(S) Toluene-d8 104 90.0-115 12/09/2016 16:09 WG933189
(S) Toluene-d8 107 90.0-115 12/09/2016 13:28 WG933189
(S) Dibromofluoromethane 108 79.0-121 12/09/2016 13:28 WG933189
(S) Dibromofluoromethane 104 79.0-121 12/09/2016 16:09 WG933189
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/09/2016 16:09 WG933189
(S) a,a,a-Trifluorotoluene 102 90.4-116 12/09/2016 13:28 WG933189
(S) 4-Bromofluorobenzene 102 80.1-120 12/09/2016 13:28 WG933189
(S) 4-Bromofluorobenzene 101 80.1-120 12/09/2016 16:09 WG933189
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931570
Gravimetric Analysis by Method 2540 C-2011 L875822-12
Method Blank (MB)
(MB) R3182284-1 12/03/16 01:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U 2.82 10.0
L875591-03 Original Sample (OS) • Duplicate (DUP)
(OS) L875591-03 12/03/16 01:42 • (DUP) R3182284-4 12/03/16 01:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Dissolved Solids 743 711 1 4.40 5
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182284-2 12/03/16 01:42 • (LCSD) R3182284-3 12/03/16 01:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Dissolved Solids 8800 8420 8640 95.7 98.2 85.0-115 2.58 5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932797
Gravimetric Analysis by Method 2540 C-2011 L875822-25
Method Blank (MB)
(MB) R3183725-1 12/08/16 10:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Dissolved Solids U 2.82 10.0
L876439-02 Original Sample (OS) • Duplicate (DUP)
(OS) L876439-02 12/08/16 10:32 • (DUP) R3183725-4 12/08/16 10:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Dissolved Solids 5560 5480 1 1.45 5
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183725-2 12/08/16 10:32 • (LCSD) R3183725-3 12/08/16 10:32
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Dissolved Solids 8800 8550 8790 97.2 99.9 85.0-115 2.77 5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931590
Wet Chemistry by Method 2320 B-2011 L875822-12
Method Blank (MB)
(MB) R3182429-1 12/05/16 07:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Alkalinity U 2.71 20.0
L876120-01 Original Sample (OS) • Duplicate (DUP)
(OS) L876120-01 12/05/16 07:34 • (DUP) R3182429-3 12/05/16 07:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Alkalinity 63.2 64.3 1 2.00 20
L875837-18 Original Sample (OS) • Duplicate (DUP)
(OS) L875837-18 12/05/16 10:31 • (DUP) R3182429-8 12/05/16 10:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Alkalinity 671 654 1 3.00 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182429-4 12/05/16 08:37 • (LCSD) R3182429-5 12/05/16 10:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Alkalinity 100 92.8 96.2 93.0 96.0 85.0-115 4.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932588
Wet Chemistry by Method 2320 B-2011 L875822-25
Method Blank (MB)
(MB) R3183099-1 12/07/16 11:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Alkalinity 4.19 J 2.71 20.0
L876441-01 Original Sample (OS) • Duplicate (DUP)
(OS) L876441-01 12/07/16 11:42 • (DUP) R3183099-3 12/07/16 11:50
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Alkalinity 132 134 1 2.00 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183099-4 12/07/16 12:40 • (LCSD) R3183099-8 12/07/16 16:06
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Alkalinity 100 99.5 85.8 99.0 86.0 85.0-115 15.0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932178
Wet Chemistry by Method 365.4 L875822-20,21,22
Method Blank (MB)
(MB) R3183300-1 12/07/16 14:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Phosphorus,Total 0.0398 J 0.0350 0.100
L875763-01 Original Sample (OS) • Duplicate (DUP)
(OS) L875763-01 12/07/16 14:21 • (DUP) R3183300-4 12/07/16 14:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Phosphorus,Total 1.21 1.27 1 5.00 20
L876134-01 Original Sample (OS) • Duplicate (DUP)
(OS) L876134-01 12/07/16 14:36 • (DUP) R3183300-5 12/07/16 14:38
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Phosphorus,Total 0.427 0.420 1 2.00 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183300-2 12/07/16 14:17 • (LCSD) R3183300-3 12/07/16 14:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Phosphorus,Total 1.00 1.03 0.999 103 100 90.0-110 3.00 20
L876151-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876151-01 12/07/16 14:45 • (MS) R3183300-6 12/07/16 14:47 • (MSD) R3183300-7 12/07/16 14:48
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Phosphorus,Total 2.50 ND 2.37 2.29 91.0 88.0 1 90.0-110 J6 3.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931630
Wet Chemistry by Method 410.4 L875822-20,21,22
Method Blank (MB)
(MB) R3182204-1 12/02/16 20:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
COD U 3.00 10.0
L875790-01 Original Sample (OS) • Duplicate (DUP)
(OS) L875790-01 12/02/16 20:27 • (DUP) R3182204-4 12/02/16 20:27
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
COD 22.8 22.5 1 1.00 20
L875836-09 Original Sample (OS) • Duplicate (DUP)
(OS) L875836-09 12/02/16 20:30 • (DUP) R3182204-7 12/02/16 20:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
COD 10.4 ND 1 12.0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182204-2 12/02/16 20:26 • (LCSD) R3182204-3 12/02/16 20:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
COD 242 244 241 101 99.0 90.0-110 1.00 20
L875836-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875836-03 12/02/16 20:29 • (MS) R3182204-5 12/02/16 20:29 • (MSD) R3182204-6 12/02/16 20:29
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
COD 400 21.7 435 424 103 101 1 80.0-120 3.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931445
Wet Chemistry by Method 5210 B-2011 L875822-20,21,22
Method Blank (MB)
(MB) R3182990-1 12/07/16 11:27
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
BOD U 1 1.00
L875804-02 Original Sample (OS) • Duplicate (DUP)
(OS) L875804-02 12/07/16 09:59 • (DUP) R3182990-5 12/07/16 10:02
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
BOD ND 0.000 1 0 30
L875836-09 Original Sample (OS) • Duplicate (DUP)
(OS) L875836-09 12/07/16 10:25 • (DUP) R3182990-6 12/07/16 10:27
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
BOD ND 0.000 1 0 30
L875834-01 Original Sample (OS) • Duplicate (DUP)
(OS) L875834-01 12/07/16 10:47 • (DUP) R3182990-7 12/07/16 10:48
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
BOD 7.20 8.50 1 17 30
Laboratory Control Sample (LCS)
(LCS) R3182990-2 12/07/16 09:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 197 99.7 84.6-115
Laboratory Control Sample (LCS)
(LCS) R3182990-3 12/07/16 10:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 201 102 84.6-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931445
Wet Chemistry by Method 5210 B-2011 L875822-20,21,22
Laboratory Control Sample (LCS)
(LCS) R3182990-4 12/07/16 11:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
BOD 198 176 88.7 84.6-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931491
Wet Chemistry by Method 9056A L875822-20,21,22
Method Blank (MB)
(MB) R3182241-1 12/02/16 19:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Nitrate U 0.0227 0.100
Sulfate U 0.0774 5.00
L875818-07 Original Sample (OS) • Duplicate (DUP)
(OS) L875818-07 12/02/16 23:35 • (DUP) R3182241-5 12/02/16 23:50
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Nitrate ND 0.000 1 0 15
Sulfate 5.18 11.5 1 76 P1 15
L875837-15 Original Sample (OS) • Duplicate (DUP)
(OS) L875837-15 12/03/16 02:19 • (DUP) R3182241-6 12/03/16 02:34
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Nitrate U 0.000 1 0 15
Sulfate 3.17 3.19 1 1 J 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182241-2 12/02/16 20:06 • (LCSD) R3182241-3 12/02/16 20:21
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Nitrate 8.00 7.90 7.92 99 99 80-120 0 15
Sulfate 40.0 39.1 39.1 98 98 80-120 0 15
L875837-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875837-17 12/03/16 03:04 • (MS) R3182241-7 12/03/16 03:19 • (MSD) R3182241-8 12/03/16 03:34
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Nitrate 5.00 U 4.85 4.81 97 96 1 80-120 1 15
Sulfate 50.0 26.2 74.7 74.8 97 97 1 80-120 0 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931491
Wet Chemistry by Method 9056A L875822-20,21,22
L875809-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L875809-04 12/02/16 22:06 • (MS) R3182241-4 12/02/16 23:05
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Sulfate 50.0 31.3 75.3 88 1 80-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931818
Wet Chemistry by Method 9056A L875822-12
Method Blank (MB)
(MB) R3182594-1 12/05/16 10:04
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Chloride 0.125 J 0.0519 1.00
Sulfate 0.118 J 0.0774 5.00
L875818-01 Original Sample (OS) • Duplicate (DUP)
(OS) L875818-01 12/05/16 11:24 • (DUP) R3182594-4 12/05/16 11:38
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Chloride 209 208 10 0 15
Sulfate 591 588 10 1 15
L875829-31 Original Sample (OS) • Duplicate (DUP)
(OS) L875829-31 12/05/16 14:52 • (DUP) R3182594-6 12/05/16 15:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Chloride 28.0 30.1 1 7 15
Sulfate U 0.000 1 0 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182594-2 12/05/16 10:19 • (LCSD) R3182594-3 12/05/16 10:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Chloride 40.0 40.0 39.5 100 99 80-120 1 15
Sulfate 40.0 39.9 39.7 100 99 80-120 0 15
L875818-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L875818-02 12/05/16 11:53 • (MS) R3182594-5 12/05/16 12:08
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Sulfate 50.0 14.0 64.4 101 1 80-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932605
Wet Chemistry by Method 9056A L875822-25
Method Blank (MB)
(MB) R3183265-1 12/07/16 07:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Chloride U 0.0519 1.00
Sulfate U 0.0774 5.00
L875924-01 Original Sample (OS) • Duplicate (DUP)
(OS) L875924-01 12/07/16 11:08 • (DUP) R3183265-5 12/07/16 11:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Chloride 19.3 19.3 1 0 15
Sulfate 65.5 65.5 1 0 15
L876290-01 Original Sample (OS) • Duplicate (DUP)
(OS) L876290-01 12/07/16 15:06 • (DUP) R3183265-6 12/07/16 15:21
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/l mg/l %%
Sulfate 8.58 8.61 1 0 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183265-2 12/07/16 07:15 • (LCSD) R3183265-3 12/07/16 07:30
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Chloride 40.0 38.7 38.8 97 97 80-120 0 15
Sulfate 40.0 39.4 39.4 98 99 80-120 0 15
L875822-25 Original Sample (OS) • Matrix Spike (MS)
(OS) L875822-25 12/07/16 10:38 • (MS) R3183265-4 12/07/16 10:53
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Chloride 50.0 5.23 54.8 99 1 80-120
Sulfate 50.0 7.35 57.9 101 1 80-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932605
Wet Chemistry by Method 9056A L875822-25
L876290-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876290-02 12/07/16 15:36 • (MS) R3183265-7 12/07/16 15:51 • (MSD) R3183265-8 12/07/16 16:06
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Sulfate 50.0 ND 49.5 49.5 99 99 1 80-120 0 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931506
Metals (ICP) by Method 6010C L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
Method Blank (MB)
(MB) R3182600-1 12/06/16 06:39
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Barium U 0.0017 0.00500
Chromium U 0.0014 0.0100
Cobalt U 0.0023 0.0100
Nickel U 0.0049 0.0100
Silver U 0.0028 0.00500
Vanadium U 0.0024 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182600-2 12/06/16 06:42 • (LCSD) R3182600-3 12/06/16 06:44
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Barium 1.00 1.03 1.04 103 104 80-120 1 20
Chromium 1.00 0.973 0.977 97 98 80-120 0 20
Cobalt 1.00 1.00 1.01 100 101 80-120 1 20
Nickel 1.00 0.955 0.958 95 96 80-120 0 20
Silver 0.200 0.173 0.173 86 87 80-120 0 20
Vanadium 1.00 0.954 0.961 95 96 80-120 1 20
L875822-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875822-04 12/06/16 06:47 • (MS) R3182600-5 12/06/16 06:52 • (MSD) R3182600-6 12/06/16 06:55
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Barium 1.00 0.0868 1.12 1.12 103 103 1 75-125 0 20
Chromium 1.00 ND 0.952 0.954 95 95 1 75-125 0 20
Cobalt 1.00 ND 1.01 1.00 101 100 1 75-125 0 20
Nickel 1.00 ND 0.954 0.949 95 95 1 75-125 1 20
Silver 0.200 ND 0.172 0.172 86 86 1 75-125 0 20
Vanadium 1.00 ND 0.956 0.957 96 96 1 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931720
Metals (ICP) by Method 6010C L875822-22
Method Blank (MB)
(MB) R3182402-1 12/05/16 08:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Barium U 0.0017 0.00500
Chromium U 0.0014 0.0100
Cobalt U 0.0023 0.0100
Nickel U 0.0049 0.0100
Silver U 0.0028 0.00500
Vanadium U 0.0024 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182402-2 12/05/16 08:20 • (LCSD) R3182402-3 12/05/16 08:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Barium 1.00 1.01 1.03 101 103 80-120 2 20
Chromium 1.00 0.961 0.977 96 98 80-120 2 20
Cobalt 1.00 0.984 1.00 98 100 80-120 2 20
Nickel 1.00 0.978 0.996 98 100 80-120 2 20
Silver 0.200 0.177 0.181 89 90 80-120 2 20
Vanadium 1.00 0.994 1.03 99 103 80-120 4 20
L876003-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876003-05 12/05/16 08:25 • (MS) R3182402-5 12/05/16 08:31 • (MSD) R3182402-6 12/05/16 08:33
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Barium 1.00 ND 1.03 1.02 103 102 1 75-125 0 20
Chromium 1.00 ND 0.967 0.975 97 98 1 75-125 1 20
Cobalt 1.00 ND 1.00 1.00 100 100 1 75-125 0 20
Nickel 1.00 ND 0.989 0.991 99 99 1 75-125 0 20
Silver 0.200 ND 0.177 0.177 89 88 1 75-125 0 20
Vanadium 1.00 ND 1.00 0.989 100 99 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932146
Metals (ICP) by Method 6010C L875822-23,24,25,26,28
Method Blank (MB)
(MB) R3183085-1 12/07/16 15:14
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Barium U 0.0017 0.00500
Chromium 0.00189 J 0.0014 0.0100
Cobalt U 0.0023 0.0100
Nickel U 0.0049 0.0100
Silver U 0.0028 0.00500
Vanadium U 0.0024 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183085-2 12/07/16 15:17 • (LCSD) R3183085-3 12/07/16 15:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Barium 1.00 1.04 1.04 104 104 80-120 1 20
Chromium 1.00 0.941 0.950 94 95 80-120 1 20
Cobalt 1.00 1.01 1.02 101 102 80-120 1 20
Nickel 1.00 0.999 1.01 100 101 80-120 1 20
Silver 0.200 0.182 0.183 91 91 80-120 1 20
Vanadium 1.00 0.985 0.987 99 99 80-120 0 20
L875822-26 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875822-26 12/07/16 15:22 • (MS) R3183085-5 12/07/16 15:33 • (MSD) R3183085-6 12/07/16 15:36
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Barium 1.00 0.0401 1.07 1.07 103 103 1 75-125 0 20
Chromium 1.00 ND 0.947 0.943 95 94 1 75-125 0 20
Cobalt 1.00 ND 1.01 1.01 101 101 1 75-125 1 20
Nickel 1.00 ND 1.00 0.998 100 100 1 75-125 0 20
Silver 0.200 ND 0.182 0.181 91 91 1 75-125 0 20
Vanadium 1.00 ND 0.984 0.980 98 98 1 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931509
Metals (ICPMS) by Method 6020 L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
Method Blank (MB)
(MB) R3182477-1 12/05/16 11:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00200
Arsenic U 0.00025 0.00200
Beryllium U 0.00012 0.00200
Cadmium U 0.00016 0.00100
Copper U 0.00052 0.00500
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc U 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182477-2 12/05/16 11:03 • (LCSD) R3182477-3 12/05/16 11:07
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0579 0.0489 0.0486 84 84 80-120 1 20
Arsenic 0.0500 0.0481 0.0477 96 95 80-120 1 20
Beryllium 0.0500 0.0442 0.0428 88 86 80-120 3 20
Cadmium 0.0500 0.0507 0.0519 101 104 80-120 2 20
Copper 0.0500 0.0550 0.0541 110 108 80-120 2 20
Lead 0.0500 0.0494 0.0490 99 98 80-120 1 20
Selenium 0.0500 0.0541 0.0519 108 104 80-120 4 20
Thallium 0.0500 0.0468 0.0459 94 92 80-120 2 20
Zinc 0.0500 0.0511 0.0498 102 100 80-120 3 20
L875822-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875822-06 12/05/16 11:10 • (MS) R3182477-5 12/05/16 11:17 • (MSD) R3182477-6 12/05/16 11:21
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0579 ND 0.0498 0.0502 86 87 1 75-125 1 20
Arsenic 0.0500 ND 0.0472 0.0478 93 94 1 75-125 1 20
Beryllium 0.0500 ND 0.0424 0.0425 84 85 1 75-125 0 20
Cadmium 0.0500 ND 0.0525 0.0526 105 105 1 75-125 0 20
Copper 0.0500 ND 0.0553 0.0551 108 107 1 75-125 0 20
Lead 0.0500 0.00335 0.0534 0.0541 100 101 1 75-125 1 20
Selenium 0.0500 ND 0.0540 0.0547 106 107 1 75-125 1 20
Thallium 0.0500 ND 0.0470 0.0477 94 95 1 75-125 2 20
Zinc 0.0500 ND 0.0628 0.0603 102 97 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931723
Metals (ICPMS) by Method 6020 L875822-22
Method Blank (MB)
(MB) R3182667-1 12/06/16 10:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00200
Arsenic U 0.00025 0.00200
Beryllium U 0.00012 0.00200
Cadmium U 0.00016 0.00100
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc U 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182667-2 12/06/16 10:40 • (LCSD) R3182667-3 12/06/16 10:44
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0579 0.0504 0.0503 87 87 80-120 0 20
Arsenic 0.0500 0.0482 0.0480 96 96 80-120 1 20
Beryllium 0.0500 0.0455 0.0458 91 92 80-120 1 20
Cadmium 0.0500 0.0520 0.0520 104 104 80-120 0 20
Lead 0.0500 0.0480 0.0482 96 96 80-120 0 20
Selenium 0.0500 0.0543 0.0526 109 105 80-120 3 20
Thallium 0.0500 0.0480 0.0481 96 96 80-120 0 20
Zinc 0.0500 0.0494 0.0480 99 96 80-120 3 20
L875797-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875797-02 12/06/16 10:47 • (MS) R3182667-5 12/06/16 10:55 • (MSD) R3182667-6 12/06/16 10:58
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0579 U 0.0517 0.0517 89 89 1 75-125 0 20
Arsenic 0.0500 0.000331 0.0464 0.0469 92 93 1 75-125 1 20
Beryllium 0.0500 U 0.0452 0.0449 90 90 1 75-125 1 20
Cadmium 0.0500 U 0.0504 0.0507 101 101 1 75-125 1 20
Lead 0.0500 U 0.0480 0.0482 96 96 1 75-125 0 20
Selenium 0.0500 0.00872 0.0598 0.0609 102 104 1 75-125 2 20
Thallium 0.0500 U 0.0476 0.0480 95 96 1 75-125 1 20
Zinc 0.0500 0.00315 0.0461 0.0637 86 121 1 75-125 J3 32 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932285
Metals (ICPMS) by Method 6020 L875822-23,24,25,26
Method Blank (MB)
(MB) R3182868-1 12/07/16 01:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00200
Arsenic U 0.00025 0.00200
Beryllium U 0.00012 0.00200
Cadmium U 0.00016 0.00100
Copper U 0.00052 0.00500
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc 0.00363 J 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182868-2 12/07/16 01:14 • (LCSD) R3182868-3 12/07/16 01:18
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0579 0.0539 0.0514 93 89 80-120 5 20
Arsenic 0.0500 0.0489 0.0478 98 96 80-120 2 20
Beryllium 0.0500 0.0469 0.0455 94 91 80-120 3 20
Cadmium 0.0500 0.0488 0.0472 98 94 80-120 3 20
Copper 0.0500 0.0528 0.0499 106 100 80-120 6 20
Lead 0.0500 0.0470 0.0460 94 92 80-120 2 20
Selenium 0.0500 0.0502 0.0479 100 96 80-120 5 20
Thallium 0.0500 0.0469 0.0456 94 91 80-120 3 20
Zinc 0.0500 0.0550 0.0505 110 101 80-120 8 20
L876291-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876291-13 12/07/16 01:21 • (MS) R3182868-5 12/07/16 01:28 • (MSD) R3182868-6 12/07/16 01:32
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0579 U 0.0532 0.0537 92 93 1 75-125 1 20
Arsenic 0.0500 0.0739 0.120 0.120 93 92 1 75-125 0 20
Beryllium 0.0500 U 0.0449 0.0451 90 90 1 75-125 0 20
Cadmium 0.0500 U 0.0472 0.0495 94 99 1 75-125 5 20
Copper 0.0500 0.000946 0.0465 0.0479 91 94 1 75-125 3 20
Lead 0.0500 U 0.0461 0.0463 92 93 1 75-125 1 20
Selenium 0.0500 U 0.0504 0.0484 101 97 1 75-125 4 20
Thallium 0.0500 U 0.0461 0.0465 92 93 1 75-125 1 20
Zinc 0.0500 0.00626 0.0498 0.0507 87 89 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932463
Metals (ICPMS) by Method 6020 L875822-22
Method Blank (MB)
(MB) R3182825-1 12/06/16 19:10
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Copper U 0.00052 0.00500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3182825-2 12/06/16 19:13 • (LCSD) R3182825-3 12/06/16 19:17
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Copper 0.0500 0.0475 0.0499 95 100 80-120 5 20
L876441-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876441-05 12/06/16 19:20 • (MS) R3182825-5 12/06/16 19:28 • (MSD) R3182825-6 12/06/16 19:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Copper 0.0500 U 0.0434 0.0441 87 88 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932780
Metals (ICPMS) by Method 6020 L875822-28
Method Blank (MB)
(MB) R3183132-1 12/07/16 17:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Antimony U 0.000754 0.00200
Arsenic U 0.00025 0.00200
Beryllium U 0.00012 0.00200
Cadmium U 0.00016 0.00100
Copper U 0.00052 0.00500
Lead U 0.00024 0.00200
Selenium U 0.00038 0.00200
Thallium U 0.00019 0.00200
Zinc U 0.00256 0.0250
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183132-2 12/07/16 17:35 • (LCSD) R3183132-3 12/07/16 17:38
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Antimony 0.0579 0.0520 0.0514 90 89 80-120 1 20
Arsenic 0.0500 0.0472 0.0459 94 92 80-120 3 20
Beryllium 0.0500 0.0444 0.0438 89 88 80-120 1 20
Cadmium 0.0500 0.0519 0.0507 104 101 80-120 2 20
Copper 0.0500 0.0509 0.0496 102 99 80-120 3 20
Lead 0.0500 0.0478 0.0470 96 94 80-120 2 20
Selenium 0.0500 0.0502 0.0480 100 96 80-120 4 20
Thallium 0.0500 0.0473 0.0470 95 94 80-120 1 20
Zinc 0.0500 0.0471 0.0450 94 90 80-120 5 20
L876653-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876653-08 12/07/16 17:42 • (MS) R3183132-5 12/07/16 17:49 • (MSD) R3183132-6 12/07/16 17:52
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Antimony 0.0579 ND 0.0502 0.0504 87 87 1 75-125 0 20
Arsenic 0.0500 ND 0.0481 0.0461 96 92 1 75-125 4 20
Beryllium 0.0500 ND 0.0440 0.0434 88 87 1 75-125 1 20
Cadmium 0.0500 ND 0.0529 0.0523 106 105 1 75-125 1 20
Copper 0.0500 ND 0.0530 0.0517 103 100 1 75-125 2 20
Lead 0.0500 ND 0.0477 0.0477 95 95 1 75-125 0 20
Selenium 0.0500 ND 0.0489 0.0468 98 94 1 75-125 4 20
Thallium 0.0500 ND 0.0472 0.0473 94 95 1 75-125 0 20
Zinc 0.0500 ND 0.0488 0.0469 98 94 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931552
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3183096-3 12/04/16 17:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromochloromethane U 0.000520 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene U 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Toluene U 0.000780 0.00500
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931552
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3183096-3 12/04/16 17:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Trichlorofluoromethane U 0.00120 0.00500
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl chloride U 0.000259 0.00100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 102 90.0-115
(S) Dibromofluoromethane 98.6 79.0-121
(S) a,a,a-Trifluorotoluene 105 90.4-116
(S) 4-Bromofluorobenzene 104 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183096-1 12/04/16 15:58 • (LCSD) R3183096-2 12/04/16 16:21
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.112 0.114 89.3 91.4 28.7-175 2.31 20.9
Acrylonitrile 0.125 0.134 0.127 107 102 58.2-145 5.40 20
Benzene 0.0250 0.0262 0.0258 105 103 73.0-122 1.45 20
Bromodichloromethane 0.0250 0.0277 0.0277 111 111 75.5-121 0.200 20
Bromochloromethane 0.0250 0.0299 0.0285 120 114 78.9-123 4.63 20
Bromoform 0.0250 0.0276 0.0269 110 108 71.5-131 2.49 20
Bromomethane 0.0250 0.0189 0.0198 75.5 79.1 22.4-187 4.74 20
Carbon disulfide 0.0250 0.0233 0.0230 93.2 92.1 53.0-134 1.12 20
Carbon tetrachloride 0.0250 0.0261 0.0264 104 106 70.9-129 1.37 20
Chlorobenzene 0.0250 0.0286 0.0286 114 115 79.7-122 0.200 20
Chlorodibromomethane 0.0250 0.0284 0.0286 114 114 78.2-124 0.850 20
Chloroethane 0.0250 0.0285 0.0294 114 117 41.2-153 2.87 20
Chloroform 0.0250 0.0283 0.0277 113 111 73.2-125 1.96 20
Chloromethane 0.0250 0.0173 0.0180 69.4 71.9 55.8-134 3.57 20
Dibromomethane 0.0250 0.0266 0.0266 106 107 79.5-118 0.230 20
1,2-Dichlorobenzene 0.0250 0.0286 0.0286 115 114 84.7-118 0.150 20
1,4-Dichlorobenzene 0.0250 0.0263 0.0268 105 107 82.2-114 2.02 20
trans-1,4-Dichloro-2-butene 0.0250 0.0273 0.0272 109 109 58.3-129 0.510 20
1,1-Dichloroethane 0.0250 0.0273 0.0273 109 109 71.7-127 0.210 20
1,2-Dichloroethane 0.0250 0.0263 0.0263 105 105 65.3-126 0.190 20
1,1-Dichloroethene 0.0250 0.0256 0.0253 102 101 59.9-137 0.960 20
cis-1,2-Dichloroethene 0.0250 0.0284 0.0282 113 113 77.3-122 0.460 20
trans-1,2-Dichloroethene 0.0250 0.0278 0.0278 111 111 72.6-125 0.110 20
1,2-Dichloropropane 0.0250 0.0277 0.0280 111 112 77.4-125 0.990 20
cis-1,3-Dichloropropene 0.0250 0.0289 0.0289 115 115 77.7-124 0.0400 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931552
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183096-1 12/04/16 15:58 • (LCSD) R3183096-2 12/04/16 16:21
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
trans-1,3-Dichloropropene 0.0250 0.0300 0.0300 120 120 73.5-127 0.100 20
Ethylbenzene 0.0250 0.0278 0.0281 111 112 80.9-121 1.00 20
2-Hexanone 0.125 0.138 0.134 111 107 59.4-151 2.85 20
Iodomethane 0.125 0.0734 0.0777 58.7 62.2 64.6-137 J4 J4 5.69 20
2-Butanone (MEK)0.125 0.130 0.124 104 99.2 46.4-155 4.66 20
Methylene Chloride 0.0250 0.0249 0.0245 99.7 97.9 69.5-120 1.85 20
4-Methyl-2-pentanone (MIBK)0.125 0.127 0.127 102 101 63.3-138 0.620 20
Styrene 0.0250 0.0283 0.0294 113 118 79.9-124 3.67 20
1,1,1,2-Tetrachloroethane 0.0250 0.0276 0.0281 111 112 78.5-125 1.66 20
1,1,2,2-Tetrachloroethane 0.0250 0.0258 0.0260 103 104 79.3-123 0.990 20
Tetrachloroethene 0.0250 0.0274 0.0279 110 112 73.5-130 2.01 20
Toluene 0.0250 0.0277 0.0280 111 112 77.9-116 1.34 20
1,1,1-Trichloroethane 0.0250 0.0271 0.0276 109 110 71.1-129 1.56 20
1,1,2-Trichloroethane 0.0250 0.0269 0.0266 107 106 81.6-120 1.07 20
Trichloroethene 0.0250 0.0276 0.0283 110 113 79.5-121 2.54 20
Trichlorofluoromethane 0.0250 0.0284 0.0282 113 113 49.1-157 0.690 20
1,2,3-Trichloropropane 0.0250 0.0275 0.0274 110 110 74.9-124 0.300 20
Vinyl chloride 0.0250 0.0276 0.0272 110 109 61.5-134 1.57 20
Xylenes, Total 0.0750 0.0832 0.0835 111 111 79.2-122 0.430 20
(S) Toluene-d8 104 103 90.0-115
(S) Dibromofluoromethane 102 98.4 79.0-121
(S) a,a,a-Trifluorotoluene 104 105 90.4-116
(S) 4-Bromofluorobenzene 102 102 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183281-4 12/07/16 22:01 • (LCSD) R3183281-6 12/08/16 03:02
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Vinyl acetate 0.125 0.111 0.107 89.0 85.6 41.7-159 3.91 20
(S) Toluene-d8 100 101 90.0-115
(S) Dibromofluoromethane 88.2 89.6 79.0-121
(S) a,a,a-Trifluorotoluene 100 101 90.4-116
(S) 4-Bromofluorobenzene 97.5 96.5 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22
Method Blank (MB)
(MB) R3183112-4 12/04/16 14:27
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromochloromethane U 0.000520 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene U 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Toluene U 0.000780 0.00500
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22
Method Blank (MB)
(MB) R3183112-4 12/04/16 14:27
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Trichlorofluoromethane U 0.00120 0.00500
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl acetate U 0.00163 0.0100
Vinyl chloride U 0.000259 0.00100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 105 90.0-115
(S) Dibromofluoromethane 104 79.0-121
(S) a,a,a-Trifluorotoluene 107 90.4-116
(S) 4-Bromofluorobenzene 104 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183112-1 12/04/16 11:08 • (LCSD) R3183112-2 12/04/16 11:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.174 0.170 139 136 28.7-175 2.29 20.9
Acrylonitrile 0.125 0.141 0.143 113 115 58.2-145 1.51 20
Benzene 0.0250 0.0250 0.0247 100 98.8 73.0-122 1.37 20
Bromodichloromethane 0.0250 0.0237 0.0232 94.9 92.7 75.5-121 2.33 20
Bromochloromethane 0.0250 0.0256 0.0255 102 102 78.9-123 0.260 20
Bromoform 0.0250 0.0255 0.0256 102 103 71.5-131 0.670 20
Bromomethane 0.0250 0.0258 0.0233 103 93.4 22.4-187 10.0 20
Carbon disulfide 0.0250 0.0216 0.0212 86.5 84.7 53.0-134 2.01 20
Carbon tetrachloride 0.0250 0.0240 0.0236 96.2 94.5 70.9-129 1.72 20
Chlorobenzene 0.0250 0.0261 0.0255 104 102 79.7-122 2.20 20
Chlorodibromomethane 0.0250 0.0259 0.0257 104 103 78.2-124 0.760 20
Chloroethane 0.0250 0.0253 0.0245 101 98.2 41.2-153 3.07 20
Chloroform 0.0250 0.0248 0.0243 99.3 97.1 73.2-125 2.26 20
Chloromethane 0.0250 0.0246 0.0236 98.4 94.3 55.8-134 4.19 20
Dibromomethane 0.0250 0.0246 0.0245 98.5 98.1 79.5-118 0.320 20
1,2-Dichlorobenzene 0.0250 0.0265 0.0262 106 105 84.7-118 1.09 20
1,4-Dichlorobenzene 0.0250 0.0249 0.0249 99.5 99.4 82.2-114 0.0300 20
trans-1,4-Dichloro-2-butene 0.0250 0.0257 0.0255 103 102 58.3-129 0.480 20
1,1-Dichloroethane 0.0250 0.0258 0.0257 103 103 71.7-127 0.150 20
1,2-Dichloroethane 0.0250 0.0234 0.0230 93.6 92.1 65.3-126 1.56 20
1,1-Dichloroethene 0.0250 0.0216 0.0212 86.2 84.9 59.9-137 1.56 20
cis-1,2-Dichloroethene 0.0250 0.0256 0.0255 102 102 77.3-122 0.280 20
trans-1,2-Dichloroethene 0.0250 0.0259 0.0253 103 101 72.6-125 2.00 20
1,2-Dichloropropane 0.0250 0.0252 0.0248 101 99.1 77.4-125 1.54 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183112-1 12/04/16 11:08 • (LCSD) R3183112-2 12/04/16 11:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
cis-1,3-Dichloropropene 0.0250 0.0262 0.0262 105 105 77.7-124 0.0400 20
trans-1,3-Dichloropropene 0.0250 0.0247 0.0248 98.6 99.1 73.5-127 0.510 20
Ethylbenzene 0.0250 0.0260 0.0254 104 102 80.9-121 2.40 20
2-Hexanone 0.125 0.128 0.127 102 102 59.4-151 0.190 20
Iodomethane 0.125 0.114 0.113 91.2 90.1 64.6-137 1.22 20
2-Butanone (MEK)0.125 0.131 0.133 105 107 46.4-155 1.79 20
Methylene Chloride 0.0250 0.0233 0.0229 93.2 91.4 69.5-120 1.90 20
4-Methyl-2-pentanone (MIBK)0.125 0.126 0.125 100 99.8 63.3-138 0.670 20
Styrene 0.0250 0.0263 0.0256 105 102 79.9-124 2.62 20
1,1,1,2-Tetrachloroethane 0.0250 0.0266 0.0255 106 102 78.5-125 4.37 20
1,1,2,2-Tetrachloroethane 0.0250 0.0246 0.0245 98.5 98.2 79.3-123 0.310 20
Tetrachloroethene 0.0250 0.0264 0.0255 106 102 73.5-130 3.33 20
Toluene 0.0250 0.0243 0.0238 97.2 95.3 77.9-116 2.01 20
1,1,1-Trichloroethane 0.0250 0.0250 0.0240 100 96.0 71.1-129 4.21 20
1,1,2-Trichloroethane 0.0250 0.0247 0.0247 98.8 98.7 81.6-120 0.140 20
Trichloroethene 0.0250 0.0256 0.0252 102 101 79.5-121 1.65 20
Trichlorofluoromethane 0.0250 0.0220 0.0219 88.0 87.7 49.1-157 0.410 20
1,2,3-Trichloropropane 0.0250 0.0254 0.0251 102 100 74.9-124 1.32 20
Vinyl acetate 0.125 0.128 0.127 103 102 41.7-159 0.720 20
Vinyl chloride 0.0250 0.0271 0.0263 108 105 61.5-134 2.84 20
Xylenes, Total 0.0750 0.0779 0.0765 104 102 79.2-122 1.77 20
(S) Toluene-d8 105 104 90.0-115
(S) Dibromofluoromethane 107 107 79.0-121
(S) a,a,a-Trifluorotoluene 105 105 90.4-116
(S) 4-Bromofluorobenzene 103 101 80.1-120
L875828-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875828-05 12/04/16 20:56 • (MS) R3183112-5 12/04/16 21:16 • (MSD) R3183112-6 12/04/16 21:36
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Acetone 0.125 31.2 87.8 85.3 90.6 86.6 500 25.0-156 2.88 21.5
Acrylonitrile 0.125 ND 76.3 71.0 122 114 500 55.9-161 7.19 20
Benzene 0.0250 0.409 13.1 12.6 101 97.6 500 58.6-133 3.80 20
Bromodichloromethane 0.0250 ND 12.5 12.1 100 96.6 500 69.2-127 3.53 20
Bromochloromethane 0.0250 ND 13.3 12.7 106 102 500 74.4-128 4.25 20
Bromoform 0.0250 ND 14.1 14.0 113 112 500 66.3-140 1.26 20
Bromomethane 0.0250 ND 11.9 11.1 94.9 88.9 500 16.6-183 6.51 20.5
Carbon disulfide 0.0250 ND 10.2 10.2 81.3 81.2 500 34.9-138 0.0700 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22
L875828-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875828-05 12/04/16 20:56 • (MS) R3183112-5 12/04/16 21:16 • (MSD) R3183112-6 12/04/16 21:36
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Carbon tetrachloride 0.0250 ND 12.2 11.9 97.8 95.5 500 60.6-139 2.36 20
Chlorobenzene 0.0250 ND 13.9 13.4 111 107 500 70.1-130 3.21 20
Chlorodibromomethane 0.0250 ND 14.1 14.0 113 112 500 71.6-132 0.690 20
Chloroethane 0.0250 ND 12.2 11.9 97.6 95.5 500 33.3-155 2.22 20
Chloroform 0.0250 0.467 13.1 12.4 101 95.6 500 66.1-133 5.07 20
Chloromethane 0.0250 ND 10.9 10.4 87.0 83.2 500 40.7-139 4.48 20
Dibromomethane 0.0250 ND 12.9 12.5 103 99.8 500 72.8-127 3.31 20
1,2-Dichlorobenzene 0.0250 ND 13.7 13.5 109 108 500 77.4-127 1.03 20
1,4-Dichlorobenzene 0.0250 ND 12.9 12.6 103 101 500 74.4-123 2.34 20
trans-1,4-Dichloro-2-butene 0.0250 ND 12.7 12.5 102 100 500 57.6-136 1.77 20
1,1-Dichloroethane 0.0250 ND 13.5 12.8 108 102 500 64.0-134 5.23 20
1,2-Dichloroethane 0.0250 ND 12.3 11.9 98.0 94.8 500 60.7-132 3.30 20
1,1-Dichloroethene 0.0250 ND 11.6 10.9 92.8 87.5 500 48.8-144 5.96 20
cis-1,2-Dichloroethene 0.0250 ND 13.3 12.4 106 99.1 500 60.6-136 7.05 20
trans-1,2-Dichloroethene 0.0250 ND 12.8 12.1 103 96.5 500 61.0-132 6.09 20
1,2-Dichloropropane 0.0250 ND 13.1 12.7 105 102 500 69.7-130 3.42 20
cis-1,3-Dichloropropene 0.0250 ND 13.6 13.2 108 106 500 71.1-129 2.59 20
trans-1,3-Dichloropropene 0.0250 ND 12.8 12.5 102 99.9 500 66.3-136 2.47 20
Ethylbenzene 0.0250 1.66 15.2 14.8 108 105 500 62.7-136 2.98 20
2-Hexanone 0.125 ND 66.1 64.9 106 104 500 59.4-154 1.92 20.1
Iodomethane 0.125 ND 61.8 59.4 98.9 95.0 500 55.2-140 3.95 20
2-Butanone (MEK)0.125 26.6 76.9 72.6 80.5 73.6 500 45.0-156 5.74 20.8
Methylene Chloride 0.0250 ND 12.3 11.9 98.4 95.1 500 61.5-125 3.37 20
4-Methyl-2-pentanone (MIBK)0.125 47.9 117 113 110 104 500 60.7-150 3.36 20
Styrene 0.0250 ND 13.9 13.6 112 108 500 68.2-133 2.87 20
1,1,1,2-Tetrachloroethane 0.0250 ND 14.3 13.9 114 111 500 70.5-132 2.74 20
1,1,2,2-Tetrachloroethane 0.0250 ND 13.4 13.2 107 106 500 64.9-145 1.51 20
Tetrachloroethene 0.0250 ND 13.4 13.2 107 105 500 57.4-141 1.78 20
Toluene 0.0250 89.4 100 99.5 88.0 80.4 500 67.8-124 0.950 20
1,1,1-Trichloroethane 0.0250 ND 13.0 12.5 104 99.7 500 58.7-134 4.23 20
1,1,2-Trichloroethane 0.0250 ND 13.6 13.3 109 107 500 74.1-130 2.18 20
Trichloroethene 0.0250 ND 13.1 12.7 105 102 500 48.9-148 3.24 20
Trichlorofluoromethane 0.0250 ND 11.3 10.9 90.3 87.5 500 39.9-165 3.20 20
1,2,3-Trichloropropane 0.0250 ND 14.2 13.6 113 109 500 71.5-134 4.22 20
Vinyl acetate 0.125 ND 70.9 68.0 113 109 500 42.8-181 4.23 20
Vinyl chloride 0.0250 ND 12.6 11.9 101 95.5 500 44.3-143 5.26 20
Xylenes, Total 0.0750 8.64 49.7 48.3 109 106 500 65.6-133 2.72 20
(S) Toluene-d8 104 104 90.0-115
(S) Dibromofluoromethane 105 103 79.0-121
(S) a,a,a-Trifluorotoluene 106 107 90.4-116
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG931684
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-21,22
L875828-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L875828-05 12/04/16 20:56 • (MS) R3183112-5 12/04/16 21:16 • (MSD) R3183112-6 12/04/16 21:36
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
(S) 4-Bromofluorobenzene 104 103 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27
Method Blank (MB)
(MB) R3183408-3 12/07/16 22:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone 0.0254 J 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromochloromethane U 0.000520 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene U 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Toluene U 0.000780 0.00500
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27
Method Blank (MB)
(MB) R3183408-3 12/07/16 22:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Trichlorofluoromethane U 0.00120 0.00500
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl acetate U 0.00163 0.0100
Vinyl chloride U 0.000259 0.00100
Xylenes, Total U 0.00106 0.00300
(S) a,a,a-Trifluorotoluene 101 90.4-116
(S) Toluene-d8 101 89.0-112
(S) Dibromofluoromethane 105 80.0-119
(S) 4-Bromofluorobenzene 94.8 85.0-114
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183408-1 12/07/16 21:00 • (LCSD) R3183408-2 12/07/16 21:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Bromochloromethane 0.0250 0.0292 0.0248 117 99.2 78.9-123 16.3 20
Acetone 0.125 0.226 0.170 181 136 28.7-175 J4 J3 28.3 20.9
Acrylonitrile 0.125 0.170 0.140 136 112 58.2-145 19.4 20
Benzene 0.0250 0.0283 0.0234 113 93.6 73.0-122 19.2 20
Carbon disulfide 0.0250 0.0302 0.0244 121 97.6 53.0-134 J3 21.2 20
Bromodichloromethane 0.0250 0.0261 0.0219 104 87.8 75.5-121 17.2 20
Bromoform 0.0250 0.0272 0.0231 109 92.4 71.5-131 16.5 20
Bromomethane 0.0250 0.0308 0.0261 123 104 22.4-187 16.5 20
Carbon tetrachloride 0.0250 0.0262 0.0215 105 85.9 70.9-129 19.9 20
Chlorobenzene 0.0250 0.0267 0.0221 107 88.3 79.7-122 18.8 20
Chlorodibromomethane 0.0250 0.0278 0.0233 111 93.1 78.2-124 17.7 20
Chloroethane 0.0250 0.0288 0.0239 115 95.5 41.2-153 18.6 20
Chloroform 0.0250 0.0277 0.0231 111 92.4 73.2-125 18.0 20
Chloromethane 0.0250 0.0283 0.0232 113 92.9 55.8-134 19.7 20
trans-1,4-Dichloro-2-butene 0.0250 0.0183 0.0156 73.3 62.4 58.3-129 16.0 20
Dibromomethane 0.0250 0.0284 0.0240 114 96.0 79.5-118 16.9 20
1,2-Dichlorobenzene 0.0250 0.0276 0.0233 110 93.4 84.7-118 16.6 20
1,4-Dichlorobenzene 0.0250 0.0259 0.0219 104 87.7 82.2-114 16.6 20
1,1-Dichloroethane 0.0250 0.0304 0.0249 122 99.7 71.7-127 19.8 20
1,2-Dichloroethane 0.0250 0.0285 0.0242 114 96.7 65.3-126 16.5 20
1,1-Dichloroethene 0.0250 0.0296 0.0237 118 94.6 59.9-137 J3 22.3 20
cis-1,2-Dichloroethene 0.0250 0.0287 0.0237 115 94.9 77.3-122 19.0 20
trans-1,2-Dichloroethene 0.0250 0.0291 0.0234 116 93.7 72.6-125 J3 21.5 20
1,2-Dichloropropane 0.0250 0.0293 0.0247 117 98.8 77.4-125 17.2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183408-1 12/07/16 21:00 • (LCSD) R3183408-2 12/07/16 21:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
cis-1,3-Dichloropropene 0.0250 0.0289 0.0243 115 97.0 77.7-124 17.3 20
2-Hexanone 0.125 0.130 0.112 104 90.0 59.4-151 14.9 20
trans-1,3-Dichloropropene 0.0250 0.0277 0.0234 111 93.7 73.5-127 16.9 20
Iodomethane 0.125 0.153 0.127 122 102 64.6-137 18.5 20
Ethylbenzene 0.0250 0.0256 0.0209 102 83.7 80.9-121 20.0 20
2-Butanone (MEK)0.125 0.149 0.125 119 100 46.4-155 16.9 20
Methylene Chloride 0.0250 0.0281 0.0233 112 93.2 69.5-120 18.7 20
4-Methyl-2-pentanone (MIBK)0.125 0.158 0.137 126 110 63.3-138 14.2 20
Styrene 0.0250 0.0261 0.0217 105 86.7 79.9-124 18.7 20
1,1,1,2-Tetrachloroethane 0.0250 0.0273 0.0225 109 89.9 78.5-125 19.4 20
1,1,2,2-Tetrachloroethane 0.0250 0.0280 0.0233 112 93.2 79.3-123 18.2 20
Tetrachloroethene 0.0250 0.0254 0.0205 102 81.9 73.5-130 J3 21.6 20
Toluene 0.0250 0.0263 0.0216 105 86.5 77.9-116 19.5 20
1,1,1-Trichloroethane 0.0250 0.0262 0.0214 105 85.6 71.1-129 J3 20.1 20
1,1,2-Trichloroethane 0.0250 0.0266 0.0224 107 89.7 81.6-120 17.2 20
Vinyl acetate 0.125 0.170 0.141 136 113 41.7-159 18.9 20
Trichloroethene 0.0250 0.0272 0.0225 109 90.0 79.5-121 18.9 20
Trichlorofluoromethane 0.0250 0.0320 0.0252 128 101 49.1-157 J3 23.7 20
1,2,3-Trichloropropane 0.0250 0.0262 0.0221 105 88.2 74.9-124 17.1 20
Vinyl chloride 0.0250 0.0300 0.0240 120 96.1 61.5-134 J3 22.0 20
Xylenes, Total 0.0750 0.0771 0.0627 103 83.6 79.2-122 J3 20.6 20
(S) a,a,a-Trifluorotoluene 100 99.4 90.4-116
(S) Toluene-d8 100 100 89.0-112
(S) Dibromofluoromethane 106 107 80.0-119
(S) 4-Bromofluorobenzene 94.5 93.6 85.0-114
L876258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876258-01 12/08/16 06:01 • (MS) R3183408-4 12/08/16 00:31 • (MSD) R3183408-5 12/08/16 01:00
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Bromochloromethane 0.0250 ND 0.244 0.244 97.5 97.4 10 74.4-128 0.0900 20
Acetone 0.125 ND 1.85 1.78 137 131 10 25.0-156 4.21 21.5
Acrylonitrile 0.125 ND 1.42 1.36 113 109 10 55.9-161 3.69 20
Benzene 0.0250 0.417 0.603 0.606 74.6 75.8 10 58.6-133 0.510 20
Carbon disulfide 0.0250 ND 0.205 0.199 82.0 79.6 10 34.9-138 2.95 20
Bromodichloromethane 0.0250 ND 0.229 0.223 91.5 89.1 10 69.2-127 2.68 20
Bromoform 0.0250 ND 0.238 0.235 95.1 93.9 10 66.3-140 1.31 20
Bromomethane 0.0250 ND 0.258 0.252 103 101 10 16.6-183 2.33 20.5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27
L876258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876258-01 12/08/16 06:01 • (MS) R3183408-4 12/08/16 00:31 • (MSD) R3183408-5 12/08/16 01:00
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Carbon tetrachloride 0.0250 ND 0.230 0.226 92.1 90.3 10 60.6-139 1.89 20
Chlorobenzene 0.0250 ND 0.234 0.227 93.8 90.8 10 70.1-130 3.20 20
Chlorodibromomethane 0.0250 ND 0.241 0.234 96.6 93.6 10 71.6-132 3.10 20
Chloroethane 0.0250 ND 0.247 0.241 99.0 96.5 10 33.3-155 2.56 20
Chloroform 0.0250 ND 0.242 0.239 96.8 95.4 10 66.1-133 1.43 20
Chloromethane 0.0250 ND 0.236 0.229 94.5 91.6 10 40.7-139 3.15 20
trans-1,4-Dichloro-2-butene 0.0250 ND 0.175 0.171 69.8 68.3 10 57.6-136 2.25 20
Dibromomethane 0.0250 ND 0.240 0.236 95.9 94.4 10 72.8-127 1.52 20
1,2-Dichlorobenzene 0.0250 ND 0.244 0.239 97.7 95.6 10 77.4-127 2.21 20
1,4-Dichlorobenzene 0.0250 ND 0.232 0.223 92.8 89.3 10 74.4-123 3.87 20
1,1-Dichloroethane 0.0250 ND 0.258 0.257 103 103 10 64.0-134 0.490 20
1,2-Dichloroethane 0.0250 ND 0.243 0.240 97.1 95.9 10 60.7-132 1.31 20
1,1-Dichloroethene 0.0250 ND 0.244 0.233 97.6 93.3 10 48.8-144 4.43 20
cis-1,2-Dichloroethene 0.0250 ND 0.247 0.243 97.7 96.0 10 60.6-136 1.83 20
trans-1,2-Dichloroethene 0.0250 ND 0.241 0.236 96.4 94.6 10 61.0-132 1.95 20
1,2-Dichloropropane 0.0250 0.0119 0.255 0.251 97.3 95.8 10 69.7-130 1.58 20
cis-1,3-Dichloropropene 0.0250 ND 0.248 0.242 99.3 96.9 10 71.1-129 2.44 20
2-Hexanone 0.125 ND 1.16 1.13 92.6 90.2 10 59.4-154 2.59 20.1
trans-1,3-Dichloropropene 0.0250 ND 0.239 0.232 93.3 90.6 10 66.3-136 2.88 20
Iodomethane 0.125 ND 1.16 1.13 92.5 90.7 10 55.2-140 1.94 20
Ethylbenzene 0.0250 0.200 0.408 0.405 83.1 81.9 10 62.7-136 0.740 20
2-Butanone (MEK)0.125 0.109 1.23 1.20 89.7 86.9 10 45.0-156 2.89 20.8
Methylene Chloride 0.0250 ND 0.233 0.229 93.3 91.5 10 61.5-125 1.89 20
4-Methyl-2-pentanone (MIBK)0.125 ND 1.32 1.29 105 103 10 60.7-150 1.99 20
Styrene 0.0250 ND 0.234 0.229 91.7 89.7 10 68.2-133 2.12 20
1,1,1,2-Tetrachloroethane 0.0250 ND 0.240 0.227 96.0 90.9 10 70.5-132 5.44 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.241 0.235 96.6 94.0 10 64.9-145 2.66 20
Tetrachloroethene 0.0250 ND 0.221 0.218 88.5 87.4 10 57.4-141 1.28 20
Toluene 0.0250 0.321 0.518 0.513 78.8 76.9 10 67.8-124 0.930 20
1,1,1-Trichloroethane 0.0250 ND 0.228 0.225 91.1 89.8 10 58.7-134 1.43 20
1,1,2-Trichloroethane 0.0250 ND 0.232 0.225 92.8 90.0 10 74.1-130 3.11 20
Vinyl acetate 0.125 ND 1.45 1.42 116 113 10 42.8-181 2.19 20
Trichloroethene 0.0250 ND 0.241 0.232 96.3 92.9 10 48.9-148 3.57 20
Trichlorofluoromethane 0.0250 ND 0.295 0.286 118 114 10 39.9-165 3.23 20
1,2,3-Trichloropropane 0.0250 ND 0.226 0.220 90.6 87.8 10 71.5-134 3.12 20
Vinyl chloride 0.0250 ND 0.261 0.253 104 101 10 44.3-143 2.99 20
Xylenes, Total 0.0750 0.466 1.10 1.08 84.5 81.8 10 65.6-133 1.87 20
(S) a,a,a-Trifluorotoluene 100 97.8 90.4-116
(S) Toluene-d8 102 101 89.0-112
(S) Dibromofluoromethane 105 106 80.0-119
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG932369
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-23,24,25,26,27
L876258-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L876258-01 12/08/16 06:01 • (MS) R3183408-4 12/08/16 00:31 • (MSD) R3183408-5 12/08/16 01:00
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
(S) 4-Bromofluorobenzene 96.0 94.7 85.0-114
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG933189
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-28
Method Blank (MB)
(MB) R3183710-1 12/09/16 09:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acetone 0.0329 J 0.0100 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromochloromethane U 0.000520 0.00100
Bromoform U 0.000469 0.00100
Carbon disulfide U 0.000275 0.00100
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
Chloroform U 0.000324 0.00500
Chloromethane 0.000853 J 0.000276 0.00250
Dibromomethane U 0.000346 0.00100
1,2-Dichlorobenzene U 0.000349 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
trans-1,4-Dichloro-2-butene U 0.000866 0.00250
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
cis-1,2-Dichloroethene U 0.000260 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
2-Hexanone U 0.00382 0.0100
Iodomethane U 0.00171 0.0100
2-Butanone (MEK)U 0.00393 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00214 0.0100
Styrene U 0.000307 0.00100
1,1,1,2-Tetrachloroethane U 0.000385 0.00100
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Toluene U 0.000780 0.00500
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
Trichlorofluoromethane U 0.00120 0.00500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG933189
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-28
Method Blank (MB)
(MB) R3183710-1 12/09/16 09:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
1,2,3-Trichloropropane U 0.000807 0.00250
Vinyl acetate U 0.00163 0.0100
Vinyl chloride U 0.000259 0.00100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 105 90.0-115
(S) Dibromofluoromethane 101 79.0-121
(S) a,a,a-Trifluorotoluene 101 90.4-116
(S) 4-Bromofluorobenzene 102 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183710-2 12/09/16 11:11 • (LCSD) R3183710-3 12/09/16 11:32
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acetone 0.125 0.137 0.146 109 117 28.7-175 6.40 20.9
Acrylonitrile 0.125 0.0950 0.108 76.0 86.5 58.2-145 12.9 20
Benzene 0.0250 0.0211 0.0227 84.3 90.9 73.0-122 7.58 20
Bromodichloromethane 0.0250 0.0223 0.0237 89.4 94.8 75.5-121 5.87 20
Bromochloromethane 0.0250 0.0219 0.0231 87.5 92.4 78.9-123 5.43 20
Bromoform 0.0250 0.0211 0.0233 84.4 93.3 71.5-131 10.0 20
Bromomethane 0.0250 0.0218 0.0176 87.3 70.4 22.4-187 J3 21.5 20
Carbon disulfide 0.0250 0.0197 0.0205 78.8 82.0 53.0-134 3.95 20
Carbon tetrachloride 0.0250 0.0220 0.0203 87.9 81.2 70.9-129 7.91 20
Chlorobenzene 0.0250 0.0236 0.0251 94.4 100 79.7-122 6.01 20
Chlorodibromomethane 0.0250 0.0240 0.0256 96.0 103 78.2-124 6.62 20
Chloroethane 0.0250 0.0262 0.0279 105 112 41.2-153 6.32 20
Chloroform 0.0250 0.0225 0.0240 90.2 96.1 73.2-125 6.36 20
Chloromethane 0.0250 0.0284 0.0306 114 122 55.8-134 7.41 20
Dibromomethane 0.0250 0.0234 0.0255 93.5 102 79.5-118 8.58 20
1,2-Dichlorobenzene 0.0250 0.0221 0.0240 88.4 96.0 84.7-118 8.24 20
1,4-Dichlorobenzene 0.0250 0.0218 0.0239 87.2 95.7 82.2-114 9.30 20
trans-1,4-Dichloro-2-butene 0.0250 0.0187 0.0200 74.8 80.1 58.3-129 6.85 20
1,1-Dichloroethane 0.0250 0.0210 0.0225 84.2 90.1 71.7-127 6.79 20
1,2-Dichloroethane 0.0250 0.0231 0.0248 92.5 99.4 65.3-126 7.09 20
1,1-Dichloroethene 0.0250 0.0214 0.0230 85.5 92.0 59.9-137 7.35 20
cis-1,2-Dichloroethene 0.0250 0.0209 0.0231 83.5 92.5 77.3-122 10.2 20
trans-1,2-Dichloroethene 0.0250 0.0216 0.0230 86.4 92.0 72.6-125 6.29 20
1,2-Dichloropropane 0.0250 0.0217 0.0234 86.8 93.6 77.4-125 7.48 20
cis-1,3-Dichloropropene 0.0250 0.0225 0.0247 90.2 98.7 77.7-124 9.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG933189
Volatile Organic Compounds (GC/MS) by Method 8260B L875822-28
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3183710-2 12/09/16 11:11 • (LCSD) R3183710-3 12/09/16 11:32
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
trans-1,3-Dichloropropene 0.0250 0.0221 0.0244 88.5 97.6 73.5-127 9.84 20
Ethylbenzene 0.0250 0.0233 0.0251 93.2 100 80.9-121 7.52 20
2-Hexanone 0.125 0.104 0.115 82.9 92.3 59.4-151 10.8 20
Iodomethane 0.125 0.0682 0.0787 54.6 62.9 64.6-137 J4 J4 14.3 20
2-Butanone (MEK)0.125 0.0797 0.0899 63.8 72.0 46.4-155 12.1 20
Methylene Chloride 0.0250 0.0208 0.0213 83.3 85.4 69.5-120 2.42 20
4-Methyl-2-pentanone (MIBK)0.125 0.0998 0.115 79.8 92.1 63.3-138 14.3 20
Styrene 0.0250 0.0235 0.0252 94.0 101 79.9-124 7.17 20
1,1,1,2-Tetrachloroethane 0.0250 0.0224 0.0244 89.4 97.6 78.5-125 8.80 20
1,1,2,2-Tetrachloroethane 0.0250 0.0203 0.0226 81.1 90.4 79.3-123 10.9 20
Tetrachloroethene 0.0250 0.0241 0.0247 96.4 98.7 73.5-130 2.38 20
Toluene 0.0250 0.0221 0.0237 88.6 94.9 77.9-116 6.90 20
1,1,1-Trichloroethane 0.0250 0.0225 0.0244 90.1 97.7 71.1-129 8.06 20
1,1,2-Trichloroethane 0.0250 0.0228 0.0242 91.1 96.7 81.6-120 5.98 20
Trichloroethene 0.0250 0.0228 0.0257 91.0 103 79.5-121 12.3 20
Trichlorofluoromethane 0.0250 0.0223 0.0240 89.1 96.2 49.1-157 7.62 20
1,2,3-Trichloropropane 0.0250 0.0216 0.0244 86.5 97.6 74.9-124 12.1 20
Vinyl acetate 0.125 0.106 0.116 84.5 93.1 41.7-159 9.71 20
Vinyl chloride 0.0250 0.0178 0.0191 71.0 76.4 61.5-134 7.31 20
Xylenes, Total 0.0750 0.0700 0.0753 93.3 100 79.2-122 7.31 20
(S) Toluene-d8 105 105 90.0-115
(S) Dibromofluoromethane 103 100 79.0-121
(S) a,a,a-Trifluorotoluene 104 103 90.4-116
(S) 4-Bromofluorobenzene 103 101 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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10 | P a g e

APPENDIX B: TIME SERIES GRAPHS

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5/22/2016 11/30/2016
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11 | P a g e

APPENDIX C: NON-PARAMETRIC PREDICTION
INTERVAL INTER-WELL COMPARISONS
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: 1,1-Dichloroethane
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 40.1042%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 5
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.259 FALSE
MW-2 3/24/2000 1 7 TRUE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 12/1/2016 1 4.17 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 12/1/2016 1 10.4 TRUE
MW-11 12/2/2016 1 0.259 FALSE
MW-5 12/1/2016 1 3.59 FALSE
MW-15A 10/2/2013 1 4.6 FALSE
MW-16 12/1/2016 1 1.15 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 12/1/2016 1 0.259 FALSE
MW-14 11/30/2016 1 0.259 FALSE
MW-13R 11/30/2016 1 0.259 FALSE
MW-17R 12/1/2016 1 0.259 FALSE
MW-5A 10/21/2011 1 0.2 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.259 FALSE
MW-21 10/2/2013 1 0.3 FALSE
Page 2
MW-22 11/30/2016 1 0.259 FALSE
MW-23 11/30/2016 1 0.259 FALSE
MW-24 10/1/2013 1 0.2 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 12/2/2016 1 0.259 FALSE
MW-25R 11/30/2016 1 0.259 FALSE
MW-15 11/30/2016 1 3.03 FALSE
MW-24R 11/30/2016 1 0.259 FALSE
MW-21R 11/30/2016 1 0.259 FALSE
MW-3R 12/1/2016 1 2.17 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: 1,4-Dichlorobenzene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 58.8616%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 5
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.274 FALSE
MW-2 3/24/2000 1 5 FALSE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 12/1/2016 1 2.91 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 12/1/2016 1 9.51 TRUE
MW-11 12/2/2016 1 0.274 FALSE
MW-5 12/1/2016 1 4.99 FALSE
MW-15A 10/2/2013 1 8.9 TRUE
MW-16 12/1/2016 1 2 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 12/1/2016 1 0.274 FALSE
MW-14 11/30/2016 1 0.274 FALSE
MW-13R 11/30/2016 1 2.49 FALSE
MW-17R 12/1/2016 1 0.274 FALSE
MW-5A 10/21/2011 1 0.39 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.274 FALSE
MW-21 10/2/2013 1 0.6 FALSE
Page 2
MW-22 11/30/2016 1 0.274 FALSE
MW-23 11/30/2016 1 0.274 FALSE
MW-24 10/1/2013 1 0.39 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 12/2/2016 1 0.274 FALSE
MW-25R 11/30/2016 1 0.274 FALSE
MW-15 11/30/2016 1 8.13 TRUE
MW-24R 11/30/2016 1 0.274 FALSE
MW-21R 11/30/2016 1 0.274 FALSE
MW-3R 12/1/2016 1 0.274 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Acetone
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 67.0157%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 100
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 10 FALSE
MW-2 3/24/2000 1 100 FALSE
MW-3 9/11/2001 1 100 FALSE
MW-7 3/24/2000 1 100 FALSE
MW-8 12/1/2016 1 10 FALSE
MW-9 9/11/2001 1 100 FALSE
MW-9A 12/1/2016 1 10 FALSE
MW-11 12/2/2016 1 10 FALSE
MW-5 12/1/2016 1 10 FALSE
MW-15A 10/2/2013 1 52.7 FALSE
MW-16 12/1/2016 1 10 FALSE
MW-17 6/12/1997 1 100 FALSE
MW-18 12/1/2016 1 10 FALSE
MW-14 11/30/2016 1 10 FALSE
MW-13R 11/30/2016 1 10 FALSE
MW-17R 12/1/2016 1 10 FALSE
MW-5A 10/21/2011 1 9.06 FALSE
MW-9B 3/24/2000 1 100 FALSE
MW-9R 3/16/2016 1 10 FALSE
MW-21 10/2/2013 1 821 TRUE
Page 2
MW-22 11/30/2016 1 10 FALSE
MW-23 11/30/2016 1 10 FALSE
MW-24 10/1/2013 1 9.06 FALSE
MW-25 3/10/2010 1 65.1 FALSE
MW-26 12/2/2016 1 10 FALSE
MW-25R 11/30/2016 1 10 FALSE
MW-15 11/30/2016 1 104 TRUE
MW-24R 11/30/2016 1 10 FALSE
MW-21R 11/30/2016 1 10 FALSE
MW-3R 12/1/2016 1 10 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Arsenic
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 52.2639%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 10
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.25 FALSE
MW-2 3/24/2000 1 35 TRUE
MW-3 9/11/2001 1 10 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 12/1/2016 1 2.78 FALSE
MW-9 9/11/2001 1 10 FALSE
MW-9A 12/1/2016 1 0.25 FALSE
MW-11 12/2/2016 1 2.42 FALSE
MW-5 12/1/2016 1 0.25 FALSE
MW-15A 10/2/2013 1 6.2 FALSE
MW-16 12/1/2016 1 14.1 TRUE
MW-17 6/12/1997 1 10 FALSE
MW-18 12/1/2016 1 0.25 FALSE
MW-14 11/30/2016 1 0.25 FALSE
MW-13R 11/30/2016 1 0.25 FALSE
MW-17R 12/1/2016 1 0.25 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 0.25 FALSE
MW-21 10/2/2013 1 2.4 FALSE
Page 2
MW-22 11/30/2016 1 0.25 FALSE
MW-23 11/30/2016 1 0.25 FALSE
MW-24 10/1/2013 1 0.41 FALSE
MW-25 3/10/2010 1 3.3 FALSE
MW-26 12/2/2016 1 0.25 FALSE
MW-25R 11/30/2016 1 2.64 FALSE
MW-15 11/30/2016 1 2.51 FALSE
MW-24R 11/30/2016 1 0.25 FALSE
MW-21R 11/30/2016 1 3.39 FALSE
MW-3R 12/1/2016 1 2.14 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Barium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 49.6134%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 500
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 53.2 FALSE
MW-2 3/24/2000 1 500 FALSE
MW-3 9/11/2001 1 500 FALSE
MW-7 3/24/2000 1 500 FALSE
MW-8 12/1/2016 1 62.1 FALSE
MW-9 9/11/2001 1 500 FALSE
MW-9A 12/1/2016 1 86.8 FALSE
MW-11 12/2/2016 1 43.9 FALSE
MW-5 12/1/2016 1 15.4 FALSE
MW-15A 10/2/2013 1 58.6 FALSE
MW-16 12/1/2016 1 144 FALSE
MW-17 6/12/1997 1 500 FALSE
MW-18 12/1/2016 1 122 FALSE
MW-14 11/30/2016 1 181 FALSE
MW-13R 11/30/2016 1 159 FALSE
MW-17R 12/1/2016 1 137 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 66.6 FALSE
MW-21 10/2/2013 1 32.1 FALSE
Page 2
MW-22 11/30/2016 1 61.2 FALSE
MW-23 11/30/2016 1 11.5 FALSE
MW-24 10/1/2013 1 38.2 FALSE
MW-25 3/10/2010 1 13.7 FALSE
MW-26 12/2/2016 1 40.1 FALSE
MW-25R 11/30/2016 1 21.9 FALSE
MW-15 11/30/2016 1 66.9 FALSE
MW-24R 11/30/2016 1 36.2 FALSE
MW-21R 11/30/2016 1 29 FALSE
MW-3R 12/1/2016 1 84.9 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Benzene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 61.4286%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 5
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.331 FALSE
MW-2 3/24/2000 1 5 FALSE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 12/1/2016 1 0.331 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 12/1/2016 1 1.44 FALSE
MW-11 12/2/2016 1 0.331 FALSE
MW-5 12/1/2016 1 0.331 FALSE
MW-15A 10/2/2013 1 1.8 FALSE
MW-16 12/1/2016 1 1.45 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 12/1/2016 1 0.331 FALSE
MW-14 11/30/2016 1 0.331 FALSE
MW-13R 11/30/2016 1 1.89 FALSE
MW-17R 12/1/2016 1 0.331 FALSE
MW-5A 10/21/2011 1 0.24 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.331 FALSE
MW-21 10/2/2013 1 0.9 FALSE
Page 2
MW-22 11/30/2016 1 0.331 FALSE
MW-23 11/30/2016 1 0.331 FALSE
MW-24 10/1/2013 1 0.24 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 12/2/2016 1 0.331 FALSE
MW-25R 11/30/2016 1 0.331 FALSE
MW-15 11/30/2016 1 1.74 FALSE
MW-24R 11/30/2016 1 0.331 FALSE
MW-21R 11/30/2016 1 0.331 FALSE
MW-3R 12/1/2016 1 0.331 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Chloroethane
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 54.0682%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 103
Maximum Background Value = 10
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.453 FALSE
MW-2 3/24/2000 1 14 TRUE
MW-3 9/11/2001 1 10 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 12/1/2016 1 0.453 FALSE
MW-9 9/11/2001 1 43 TRUE
MW-9A 12/1/2016 1 0.453 FALSE
MW-11 12/2/2016 1 0.453 FALSE
MW-5 12/1/2016 1 0.453 FALSE
MW-15A 10/2/2013 1 2.6 FALSE
MW-16 12/1/2016 1 10.5 TRUE
MW-17 6/12/1997 1 10 FALSE
MW-18 12/1/2016 1 0.453 FALSE
MW-14 11/30/2016 1 0.453 FALSE
MW-13R 11/30/2016 1 0.453 FALSE
MW-17R 12/1/2016 1 0.453 FALSE
MW-5A 10/21/2011 1 0.48 FALSE
MW-9B 3/24/2000 1 10 FALSE
MW-9R 3/16/2016 1 0.453 FALSE
MW-21 10/2/2013 1 0.48 FALSE
Page 2
MW-22 11/30/2016 1 0.453 FALSE
MW-23 11/30/2016 1 0.453 FALSE
MW-24 10/1/2013 1 0.48 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 12/2/2016 1 0.453 FALSE
MW-25R 11/30/2016 1 0.453 FALSE
MW-15 11/30/2016 1 0.453 FALSE
MW-24R 11/30/2016 1 0.453 FALSE
MW-21R 11/30/2016 1 0.453 FALSE
MW-3R 12/1/2016 1 0.453 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Chromium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 0%
Number of comparisons = 19
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 8
Maximum Background Value = 8.35
Confidence Level = 50%
False Positive Rate = 50%
Location Date Count Mean Significant
MW-9R 3/16/2016 1 12.1 TRUE
MW-5 12/1/2016 1 1.4 FALSE
MW-8 12/1/2016 1 1.4 FALSE
MW-9A 12/1/2016 1 1.4 FALSE
MW-10 12/2/2016 1 12.2 TRUE
MW-11 12/2/2016 1 1.4 FALSE
MW-13R 11/30/2016 1 1.4 FALSE
MW-14 11/30/2016 1 1.4 FALSE
MW-15 11/30/2016 1 1.4 FALSE
MW-16 12/1/2016 1 1.4 FALSE
MW-17R 12/1/2016 1 11.6 TRUE
MW-18 12/1/2016 1 1.4 FALSE
MW-21R 11/30/2016 1 1.4 FALSE
MW-22 11/30/2016 1 1.4 FALSE
MW-23 11/30/2016 1 1.4 FALSE
MW-24R 11/30/2016 1 1.4 FALSE
MW-25R 11/30/2016 1 1.4 FALSE
MW-26 12/2/2016 1 1.4 FALSE
MW-3R 12/1/2016 1 10.1 TRUE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Cobalt
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 52.8424%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 10
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 2.3 FALSE
MW-2 3/24/2000 1 10 FALSE
MW-3 9/11/2001 1 10 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 12/1/2016 1 2.3 FALSE
MW-9 9/11/2001 1 10 FALSE
MW-9A 12/1/2016 1 2.3 FALSE
MW-11 12/2/2016 1 2.3 FALSE
MW-5 12/1/2016 1 2.3 FALSE
MW-15A 10/2/2013 1 3.3 FALSE
MW-16 12/1/2016 1 2.3 FALSE
MW-17 6/12/1997 1 11 TRUE
MW-18 12/1/2016 1 2.3 FALSE
MW-14 11/30/2016 1 2.3 FALSE
MW-13R 11/30/2016 1 2.3 FALSE
MW-17R 12/1/2016 1 17 TRUE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 2.3 FALSE
MW-21 10/2/2013 1 19 TRUE
Page 2
MW-22 11/30/2016 1 2.3 FALSE
MW-23 11/30/2016 1 2.3 FALSE
MW-24 10/1/2013 1 1.3 FALSE
MW-25 3/10/2010 1 1.6 FALSE
MW-26 12/2/2016 1 2.3 FALSE
MW-25R 11/30/2016 1 2.3 FALSE
MW-15 11/30/2016 1 2.3 FALSE
MW-24R 11/30/2016 1 2.3 FALSE
MW-21R 11/30/2016 1 11.2 TRUE
MW-3R 12/1/2016 1 2.3 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Copper
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 52.3447%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 108
Maximum Background Value = 200
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.52 FALSE
MW-2 3/24/2000 1 200 FALSE
MW-3 9/11/2001 1 200 FALSE
MW-7 3/24/2000 1 200 FALSE
MW-8 12/1/2016 1 0.52 FALSE
MW-9 9/11/2001 1 200 FALSE
MW-9A 12/1/2016 1 0.52 FALSE
MW-11 12/2/2016 1 0.52 FALSE
MW-5 12/1/2016 1 0.52 FALSE
MW-15A 10/2/2013 1 8.8 FALSE
MW-16 12/1/2016 1 0.52 FALSE
MW-17 6/12/1997 1 200 FALSE
MW-18 12/1/2016 1 0.52 FALSE
MW-14 11/30/2016 1 0.52 FALSE
MW-13R 11/30/2016 1 0.52 FALSE
MW-17R 12/1/2016 1 0.52 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 0.52 FALSE
MW-21 10/2/2013 1 4.4 FALSE
Page 2
MW-22 11/30/2016 1 0.52 FALSE
MW-23 11/30/2016 1 0.52 FALSE
MW-24 10/1/2013 1 4.5 FALSE
MW-25 3/10/2010 1 4.2 FALSE
MW-26 12/2/2016 1 0.52 FALSE
MW-25R 11/30/2016 1 0.52 FALSE
MW-15 11/30/2016 1 0.52 FALSE
MW-24R 11/30/2016 1 0.52 FALSE
MW-21R 11/30/2016 1 6.48 FALSE
MW-3R 12/1/2016 1 0.52 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Lead
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 46.0441%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 41
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 7.6 FALSE
MW-2 3/24/2000 1 20 FALSE
MW-3 9/11/2001 1 20 FALSE
MW-7 3/24/2000 1 10 FALSE
MW-8 12/1/2016 1 8.46 FALSE
MW-9 9/11/2001 1 18 FALSE
MW-9A 12/1/2016 1 0.24 FALSE
MW-11 12/2/2016 1 2.93 FALSE
MW-5 12/1/2016 1 0.24 FALSE
MW-15A 10/2/2013 1 0.74 FALSE
MW-16 12/1/2016 1 0.24 FALSE
MW-17 6/12/1997 1 10 FALSE
MW-18 12/1/2016 1 3.38 FALSE
MW-14 11/30/2016 1 0.24 FALSE
MW-13R 11/30/2016 1 3.35 FALSE
MW-17R 12/1/2016 1 8.58 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 4.26 FALSE
MW-21 10/2/2013 1 0.3 FALSE
Page 2
MW-22 11/30/2016 1 0.24 FALSE
MW-23 11/30/2016 1 0.24 FALSE
MW-24 10/1/2013 1 1.1 FALSE
MW-25 3/10/2010 1 6.7 FALSE
MW-26 12/2/2016 1 0.24 FALSE
MW-25R 11/30/2016 1 0.24 FALSE
MW-15 11/30/2016 1 0.24 FALSE
MW-24R 11/30/2016 1 0.24 FALSE
MW-21R 11/30/2016 1 2.49 FALSE
MW-3R 12/1/2016 1 4.59 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Selenium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 56.2016%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 20
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.38 FALSE
MW-2 3/24/2000 1 20 FALSE
MW-3 9/11/2001 1 39 TRUE
MW-7 3/24/2000 1 20 FALSE
MW-8 12/1/2016 1 0.38 FALSE
MW-9 9/11/2001 1 20 FALSE
MW-9A 12/1/2016 1 0.38 FALSE
MW-11 12/2/2016 1 0.38 FALSE
MW-5 12/1/2016 1 0.38 FALSE
MW-15A 10/2/2013 1 2.1 FALSE
MW-16 12/1/2016 1 0.38 FALSE
MW-17 6/12/1997 1 20 FALSE
MW-18 12/1/2016 1 0.38 FALSE
MW-14 11/30/2016 1 0.38 FALSE
MW-13R 11/30/2016 1 0.38 FALSE
MW-17R 12/1/2016 1 0.38 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 22.6 TRUE
MW-21 10/2/2013 1 1.2 FALSE
Page 2
MW-22 11/30/2016 1 0.38 FALSE
MW-23 11/30/2016 1 0.38 FALSE
MW-24 10/1/2013 1 0.18 FALSE
MW-25 3/10/2010 1 0.4 FALSE
MW-26 12/2/2016 1 0.38 FALSE
MW-25R 11/30/2016 1 0.38 FALSE
MW-15 11/30/2016 1 0.38 FALSE
MW-24R 11/30/2016 1 0.38 FALSE
MW-21R 11/30/2016 1 0.38 FALSE
MW-3R 12/1/2016 1 46.3 TRUE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Tetrachloroethene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 43.1267%
Number of comparisons = 24
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 37
Maximum Background Value = 5
Confidence Level = 82.2%
False Positive Rate = 17.8%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.372 FALSE
MW-11 12/2/2016 1 0.372 FALSE
MW-13R 11/30/2016 1 0.372 FALSE
MW-14 11/30/2016 1 0.372 FALSE
MW-15A 10/2/2013 1 0.17 FALSE
MW-16 12/1/2016 1 0.372 FALSE
MW-17R 12/1/2016 1 1.21 FALSE
MW-18 12/1/2016 1 0.372 FALSE
MW-21 10/2/2013 1 0.17 FALSE
MW-22 11/30/2016 1 0.372 FALSE
MW-23 11/30/2016 1 0.372 FALSE
MW-9R 3/16/2016 1 0.372 FALSE
MW-5 12/1/2016 1 0.372 FALSE
MW-8 12/1/2016 1 0.372 FALSE
MW-9A 12/1/2016 1 0.372 FALSE
MW-24 10/1/2013 1 0.17 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 12/2/2016 1 0.372 FALSE
MW-25R 11/30/2016 1 0.372 FALSE
MW-5A 10/21/2011 1 0.17 FALSE
Page 2
MW-15 11/30/2016 1 0.372 FALSE
MW-24R 11/30/2016 1 0.372 FALSE
MW-21R 11/30/2016 1 0.372 FALSE
MW-3R 12/1/2016 1 0.372 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Trichloroethene
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 66.0782%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 107
Maximum Background Value = 7
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 0.398 FALSE
MW-2 3/24/2000 1 5 FALSE
MW-3 9/11/2001 1 5 FALSE
MW-7 3/24/2000 1 5 FALSE
MW-8 12/1/2016 1 0.398 FALSE
MW-9 9/11/2001 1 5 FALSE
MW-9A 12/1/2016 1 0.398 FALSE
MW-11 12/2/2016 1 0.398 FALSE
MW-5 12/1/2016 1 0.398 FALSE
MW-15A 10/2/2013 1 0.23 FALSE
MW-16 12/1/2016 1 0.398 FALSE
MW-17 6/12/1997 1 5 FALSE
MW-18 12/1/2016 1 0.398 FALSE
MW-14 11/30/2016 1 0.398 FALSE
MW-13R 11/30/2016 1 0.398 FALSE
MW-17R 12/1/2016 1 1.02 FALSE
MW-5A 10/21/2011 1 0.23 FALSE
MW-9B 3/24/2000 1 5 FALSE
MW-9R 3/16/2016 1 0.398 FALSE
MW-21 10/2/2013 1 0.23 FALSE
Page 2
MW-22 11/30/2016 1 0.398 FALSE
MW-23 11/30/2016 1 0.398 FALSE
MW-24 10/1/2013 1 0.23 FALSE
MW-25 3/10/2010 1 0 FALSE
MW-26 12/2/2016 1 0.398 FALSE
MW-25R 11/30/2016 1 0.398 FALSE
MW-15 11/30/2016 1 0.398 FALSE
MW-24R 11/30/2016 1 0.398 FALSE
MW-21R 11/30/2016 1 0.398 FALSE
MW-3R 12/1/2016 1 0.398 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Vanadium
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 49.0933%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 105
Maximum Background Value = 210
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 21.5 FALSE
MW-2 3/24/2000 1 40 FALSE
MW-3 9/11/2001 1 40 FALSE
MW-7 3/24/2000 1 40 FALSE
MW-8 12/1/2016 1 2.4 FALSE
MW-9 9/11/2001 1 40 FALSE
MW-9A 12/1/2016 1 2.4 FALSE
MW-11 12/2/2016 1 2.4 FALSE
MW-5 12/1/2016 1 2.4 FALSE
MW-15A 10/2/2013 1 0.07 FALSE
MW-16 12/1/2016 1 2.4 FALSE
MW-17 6/12/1997 1 40 FALSE
MW-18 12/1/2016 1 2.4 FALSE
MW-14 11/30/2016 1 2.4 FALSE
MW-13R 11/30/2016 1 2.4 FALSE
MW-17R 12/1/2016 1 23.7 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 26.2 FALSE
MW-21 10/2/2013 1 0.07 FALSE
Page 2
MW-22 11/30/2016 1 2.4 FALSE
MW-23 11/30/2016 1 2.4 FALSE
MW-24 10/1/2013 1 0.91 FALSE
MW-25 3/10/2010 1 10.6 FALSE
MW-26 12/2/2016 1 2.4 FALSE
MW-25R 11/30/2016 1 2.4 FALSE
MW-15 11/30/2016 1 2.4 FALSE
MW-24R 11/30/2016 1 2.4 FALSE
MW-21R 11/30/2016 1 2.4 FALSE
MW-3R 12/1/2016 1 25.3 FALSE
Page 1
Non-Parametric Prediction Interval
Inter-Well Comparison
Parameter: Zinc
Original Data (Not Transformed)
Non-Detects Replaced with Detection Limit
Total Percent Non-Detects = 42.8571%
Number of comparisons = 30
Future Samples (k) = 8
Recent Dates = 1
Background Measurements (n) = 107
Maximum Background Value = 260
Confidence Level = 92.6%
False Positive Rate = 7.4%
Location Date Count Mean Significant
MW-10 12/2/2016 1 27.4 FALSE
MW-2 3/24/2000 1 50 FALSE
MW-3 9/11/2001 1 50 FALSE
MW-7 3/24/2000 1 50 FALSE
MW-8 12/1/2016 1 2.56 FALSE
MW-9 9/11/2001 1 50 FALSE
MW-9A 12/1/2016 1 2.56 FALSE
MW-11 12/2/2016 1 34.7 FALSE
MW-5 12/1/2016 1 2.56 FALSE
MW-15A 10/2/2013 1 5.4 FALSE
MW-16 12/1/2016 1 2.56 FALSE
MW-17 6/12/1997 1 50 FALSE
MW-18 12/1/2016 1 2.56 FALSE
MW-14 11/30/2016 1 2.56 FALSE
MW-13R 11/30/2016 1 2.56 FALSE
MW-17R 12/1/2016 1 2.56 FALSE
MW-5A 3/19/2012 1 0 FALSE
MW-9B 3/19/2012 1 0 FALSE
MW-9R 3/16/2016 1 2.56 FALSE
MW-21 10/2/2013 1 8.4 FALSE
Page 2
MW-22 11/30/2016 1 2.56 FALSE
MW-23 11/30/2016 1 2.56 FALSE
MW-24 10/1/2013 1 2.4 FALSE
MW-25 3/10/2010 1 26 FALSE
MW-26 12/2/2016 1 2.56 FALSE
MW-25R 11/30/2016 1 2.56 FALSE
MW-15 11/30/2016 1 2.56 FALSE
MW-24R 11/30/2016 1 2.56 FALSE
MW-21R 11/30/2016 1 2.56 FALSE
MW-3R 12/1/2016 1 2.56 FALSE