8606_SurryCountyMSWLF_GWMR_DIN28077_20160614

Surry County Subtitle D Lined MSWLF
Mt. Airy, North Carolina
June 2016
Permit Number: 86-06
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G16025.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
MW-2 Area Investigations Page 2
MW-6R Area Investigations Page 2
MW-9S Area Investigations Page 2
Sampling Procedures Page 2
Field Parameter Data Page 3
Laboratory Results Page 3
Quality Control Samples Page 3
Groundwater Samples Page 3
Surface Water Samples Page 3
Leachate Samples Page 3
Groundwater and Surface Water Characterization Page 4
Findings Page 4
Closing Page 5
FIGURES
Topographic Map with Site Location Figure 1
Single Event Potentiometric Map of Uppermost Aquifer Figure 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, 2L, 2B, GWP or MCL (Appendix 1) Table 5
Detections Above MDL (Appendix II) Table 6
Detections in Leachate Samples above SWSL, 2L, 2B, GWP or MCL Table 7
Hydrologic Properties at Monitoring Well Locations Table 8
Total Metals Concentrations Evaluation Table Table 9
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
October 28, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US Highway 70
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Subtitle D Lined MSWLF, Phases 1 & 2
Permit No. 86-06
MESC0 Project No. G16025.0
Sampling Date(s). June 14-15, 2016
Dear Ms Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Monitoring Report for an event performed at the Surry County Subtitle D Lined
Municipal Solid Waste Landfill (MSWLF) in the Spring 2016. NCDEQ Solid Waste Rules 15A NCAC 13B.1632
requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents the quality
of the ground and surface waters during this monitoring event performed on June 14-15, 2016. Assessment
monitoring (full Appendix II monitoring) was initiated site-wide during this event in response to VOC(s) detected in
a few downgradient wells. The laboratory analytical results indicate that two downgradient wells contained vinyl
chloride above NC 2L Groundwater Standards. All detections remain below Federal “Drinking Water Standards”,
contaminants continue to be low in leachate samples and all the surface water samples continue to appear
unimpacted.
Background
The Surry County Subtitle D lined MSWLF, permit #86-06, is located at 237 Landfill Road, Mount Airy, Surry
County, North Carolina. The site location topographic map is depicted in the attached Figure 1. The lined MSWLF
is comprised of contiguous Phases 1 & 2 which are treated as a single unit in this report.
Water quality at this facility has been monitored at least semi-annually since 1998 with all historical data reviewed
in support of this report. This event was performed in accordance with the NC SWS rules/regulations as
promulgated in 15A NCAC 13B and as a condition of the permit to operate.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Well construction summary table, field observations table, field parameter data table, sampling
and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates table,
potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed herein.

MW-2 Area Investigations
During this event MESCO investigated the area around MW-2 in an attempt to identify the source of low “j”
qualified concentrations of VOCs detected in samples collected from MW-2. The double lined leachate lagoon
leak detection manhole was observed to be dry, indicating the lagoon has not leaked. Evidence has never been
found to suggest that the lagoon has ever overflowed. During this event no constituents were detected in MW-2
above SWSL or regulatory Standards. Supplemental surface water sample (SW-A), collected downgradient of MW-
2 continues to appear unimpaired.
MW-6R Area Investigations
During this event MESCO investigated the area around MW-6R in an attempt to identify the source of VOC
detections. MW-6R is located in a ditch that previously conveyed stormwater originating from the lined landfill.
During the construction of Phased 2 in 2009, stormwater originating near the landfill was rerouted so that it no
longer flows adjacent to MW-6R. Landfill gas (LFG) has been detected in migration monitoring probe MGP-5
located less than 75 feet away from MW-6R. Active LFG extraction has been initiated at Lined Phase 1 which
includes vacuum applied at the closest leachate collection system cleanout.. Surprisingly methane has been absent
from the adjacent cleanout during every reading MESCO has taken since it was tied into the active extraction
system. MW-6R contained vinyl chloride above the 2L Standard. There were no detections in a supplemental
surface water sample (SW-B) collected downgradient of MW-6R.
MW-9S Area Investigations
MESCO investigated the area around MW-9S in an attempt to identify the source of VOC detections during this
event. MW-9S is located about 180 feet downgradient of the Phase 2 sump near a previous drainage feature. Low
levels of chlorinated hydrocarbons have consistently been detected in samples collected from MW-9S since before
waste was deposited in Phase 2. MW-9S contained vinyl chloride above the 2L Standard. VOCs remain absent in
the adjacent deeper cluster well MW-9D. LFG has never been detected from head-space of MW-9S or from
adjacent migration probe MGP-12.
Sampling Procedure
MESCO personnel performed this sampling event using portable monitoring methodology in general accordance
with the site-specific SAP from the Phase 2 Design Hydrogeologic Study, approved June 13, 2008. Water samples
were collected from 14 downgradient groundwater monitoring wells (MW-2R, MW-3, MW-4S, MW-4D, MW-5,
MW-6R, MW-8, MW-9S, MW-9D, MW-10, MW-11S, MW-11D, MW-12 and MW-13), one background well
(MW-1), four downstream surface water locations (SW-4 , SWN-2, SW-A and SW-B), four upstream surface water
points (SWN-1, SW-1, SW-2 and SW-3) and a pre-treated leachate sample (LAGOON). Surface water points
SWN-3 and SWN-4 were not sampled because they were dry. Quality control measures included analysis of
equipment blanks (EB) field blanks (FB) and trip blanks (TB). Sampling locations are shown on the potentiometric
map (Figure 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of
three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney
Creek discharge feature at previously designated locations. During well purging and surface water sample
collection the required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-
preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported
to a NC-certified laboratory under proper C-O-C protocols within the specified hold times for each analysis.
2
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature,
total dissolved solids (TDS) and visual turbidity. A summary of the field parameter data is presented in Table 3 and
the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Services, Inc. (PACE) of Huntersville and Asheville NC performed the laboratory analysis of the
water and leachate samples. All groundwater samples were analyzed for the current 40 CFR 258 Appendix II list of
constituents as requested by the SWS. Surface waters were tested for the parameters listed in 40 CFR 258
Appendix I. Untreated leachate was tested for the specific parameters required by the SWS which includes VOCs,
total metals, phosphorous, BOD, COD, sulfide and nitrate. A sampling and analysis table summarizing the
locations, constituents and methods is presented as Table 4.
Water samples were analyzed to the laboratory specific Method Detection Limits (MDL), which are quantifiable at
or below the current Solid Waste Section detection limits (SWSL). Table 5 summarizes constituents detected in
groundwater and surface water samples that attain or were above the current SWSL, Groundwater Protection
Standards (GWP), North Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water
Standards (2B) for a class C waterbody, and Maximum Contaminant Levels (MCL) also known as “Federal Primary
Drinking Water Standards”. Table 6 summarizes the few Appendix II exclusive analytes , defined in this report as
not also listed on Appendix I, detected above the MDL. Table 7 summarizes constituents detected in the leachate
lagoon samples. Laboratory results and C-O-Cs are presented in Appendix A.
Quality Control Samples
No contaminants were detected in any of the quality control blanks, therefore the data set is believe to not be
significantly impacted by high bias or false positives.
Groundwater Samples
Total chromium was detected above the 2L Standard (10µg/L) in sample MW-5 (12.1 µg/L), MW-12 (10.4 µg/L)
and the highest in background well MW-1 (13.7 µg/L). Total cadmium was detected in samples MW-5 (2.3 µg/L),
and MW-9S (2.4 µg/L) above the 2L Standard (2 µg/L). Total vanadium was detected above the GWP Standard
but below the SWSL thus “j-qualified” in samples MW-5, MW-8, MW-10, MW-11D, MW-12, and background
well MW-1. Finally total cobalt was found in sample MW-9S (144 µg/L) which is above it's respective GWP
Standard (70 µg/L).
A sample collected from MW-6R contained levels of vinyl chloride (1.3 µg/L) above the 2L Standard (0.03 µg/L).
Sample MW-9S contained vinyl chloride at 0.72 µg/L which is above it's 2L Standard 0.03 µg/L but below the
SWSL (1 µg/L) therefore “j-qualified” .
The only Appendix II exclusive constituents, defined in this report as not also listed in Appendix I, detected above
MDL were low “j-qualified” constituents below established Standards.
Surface Water Samples
Contaminants were not detected above NC 2B Surface Water Standards in any of the surface water samples.
Leachate Samples
Contaminants in high concentrations have rarely been detected in leachate samples collected at this facility. During
this event vinyl chloride, the currently lone contaminant of concern, was detected in the leachate after being absent
the last 8 years and levels of total chromium were unprecedented (Table 7).
3
Groundwater and Surface Water Characterization
MESCO prepared a potentiometric map of the uppermost aquifer from groundwater elevation data recorded during
this monitoring event (Plate 2). Groundwater flow rates and directions were calculated and are included in the
hydrologic properties table (Table 8). Groundwater flow directions remain generally in a southerly direction
towards the Ararat River with groundwater velocities calculated by modified Darcy's equation varied considerably
due to the anisotropic geologic conditions. Streams located at the designated surface water sampling stations were
observed to be of moderate volume and flow with low turbidity.
Findings
The detections of total metals are not believed to have originated from anthropogenic source rather a product of
natural deposit erosion. All concentrations of metals that were above a Standard were lower than the highest
observed during their respective baseline period which was established during the first six months of operation,
below the all time highest obeserved levels in the background well and above the all time highest observed level in
the leachate after applying a 20:1 dilution mixing factor (Table 9).
Vinyl chloride has been detected above the 2L Standard in every sample collected from MW-6R over the past four
years but levels remain within it's own historically identified range. MW-6R is located approximately 100 feet
downgradient of the Phase 2 liner and within the compliance boundary. The portion of the aquifer impacted is
believed to be small as evidenced by lack of detections in MW-8 located along the downgradient flow path. The
active LFG extraction system is expected to operate indefinitely which may reduce levels of LFG migrating through
the vadose which may mitigate potential groundwater impacts.
Levels of PCE fell below the 2L Standard for the first time in over six years. MW-2 is located approximately 75
feet downgradient of the leachate lagoon and within the compliance boundary. Surface water point SW-A, collected
directly downgradient of MW-2 tested clean. Based upon all available evidence it is unlikely that the contaminants
detected in this area will migrate beyond the compliance boundary which extends beyond the large perennial
discharge feature. The discharge feature is expected to remain unimpacted as all levels of contaminants ever
detected in any downgradient groundwater sample are already below their respective 2B Surface Water Standard.
Vinyl chloride was detected in a sample collected from MW-9S above its 2L Standard for the fourth consecutive
event but was below the SWSL. MW-9S has consistently yielded results with low levels of chlorinated solvents
since the first Phase 2 pre-operation baseline event was performed more than five years ago.
Interpretation of results of surface water samples collected along Stoney Creek, including those newly instituted
directly downgradient of MW-2 and MW-6R, continue to indicate the local discharge feature remains unimpacted.
Although not applicable for regulatory compliance purposes it should be noted that no contaminants were detected
above Federally established “Drinking Water Standards”.
4
Figures
Tables
Surry County Subtitle D MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
June 14-15, 2016
Latitude Longitude
(inches)(ft)
MW-1 8/14/98 2 68.5 53.5 15 Rock 1127.02 1124.23 1064.98 62.04 36.434494 -80.577989
MW-2 8/16/98 2 23.5 8.5 15 Rock 936.68 933.91 923.47 13.21 36.430833 -80.571161
MW-3R 12/2/98 2 20 5 15 Rock 930.00 928.15 925.30 4.70 36.430714 -80.571575
MW-4S 8/11/98 2 20 5 15 943.23 940.31 934.00 9.23 36.430853 -80.572400
MW-4D 8/11/98 2 45 35 10 Rock 942.80 940.31 933.74 9.06 36.430853 -80.572400
MW-5 8/18/98 2 47.5 32.5 15 Rock 977.86 971.57 934.05 43.81 36.430356 -80.572961
MW-6R 3/22/99 2 79 64 15 Fractured Rock 1004.75 1001.81 939.10 65.65 36.429958 -80.573508
MW-8 9/1/09 2 70.75 55.75 15 Fractured Rock 971.03 968.35 909.71 61.32 36.429283 -80.573453
MW-9S 6/16/06 2 42.28 27.28 15 Fractured Rock 952.83 949.75 920.59 32.24 36.429314 -80.574464
MW-9D 6/16/06 2 65.54 55.54 10 Competent Rock 952.47 949.49 917.72 34.75 36.429314 -80.574464
MW-10 6/16/06 2 47.13 27.13 20 Fractured Rock 970.24 967.35 938.83 31.41 36.429519 -80.575486
MW-11S 9/3/09 2 46.05 31.05 15 Competent Rock 969.09 965.95 937.88 31.21 36.430197 -80.577131
MW-11D 9/3/09 2 65.31 55.31 10 Competent Rock 965.38 962.38 933.77 31.61 36.430197 -80.577131
MW-12 9/4/09 2 65 50 15 Competent Rock 996.66 993.71 945.74 50.92 36.429831 -80.576750
MW-13 9/3/09 2 36.31 21.31 15 Fractured Rock 983.13 979.83 956.75 26.38 36.430625 -80.578531
MLW-A 8/19/98 2 84 69 15 Competent Rock 1095.51 1092.51 1012.50 83.01 36.432881 -80.573539
P2-6S 6/7/06 2 66.38 51.38 15 Fractured Rock 1040.27 1037.36 983.99 56.28 36.431019 -80.578025
P2-6D 6/7/06 2 93.98 83.98 10 Competent Rock 1040.65 1037.56 975.67 64.98 36.431019 -80.578025
P2-11S 6/16/06 2 50.13 40.13 10 Competent Rock 1021.53 1018.40 972.32 49.21 36.430197 -80.577131
P2-11D 6/16/06 2 65.45 60.45 5 Competent Rock 1021.13 1018.73 971.45 49.68 36.430197 -80.577131
P2-12 6/16/06 2 59.56 44.56 15 Competent Rock 986.61 983.54 934.12 52.49 36.429831 -80.576750
NOTE:
1. Ground, datum and TOR elevations are in units of feet, well diameter are in units of inches.
Monitoring
Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length Geology of
Screened Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
Saprolite
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
June 15, 2016
Comments
MW-1 Yes Yes Yes Yes Yes Yes Background Well
MW-2 Yes Yes Yes Yes Yes ?
MW-3R Yes Yes Yes Yes Yes ?Pad covered by soil
MW-4S Yes Yes Yes Yes Yes ?Pad covered by soil
MW-4D Yes Yes Yes Yes Yes ?Pad covered by soil
MW-5 Yes Yes Yes Yes Yes Yes Repaired by Co. in Sept. 2013 Datum may have changed
MW-6R Yes Yes Yes Yes Yes Yes County improved surface seal in September 2013
MW-8 Yes Yes Yes Yes Yes Yes Path recently mowed
MW-9S Yes Yes Yes Yes Yes Yes
MW-9D Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes
MW-11S Yes Yes Yes Yes Yes Yes
MW-11D Yes Yes Yes Yes Yes Yes Slight hydrogen sulfide smell, very slow recharge
MW-12 Yes Yes Yes Yes Yes Yes Slow recharge
MW-13 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----
SW-2 Yes -----
SW-3 Yes -----
SWN-1 Yes -----
SWN-2 Yes -----
SWN-3 No -----Dry
SWN-4 No -----Dry. Always has been
SW-A Yes -----Supplemental sample per SWS verbal request
SW-B Yes -----Supplemental sample per SWS verbal request
LAGOON Yes Yes Yes Yes Yes Yes
MLW-A Yes Yes Yes Yes Yes ?Pad covered by soil
P2-6S Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-6D Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-11S Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-11D Yes Yes Yes Yes Yes Yes Depth to groundwater only
P2-12 Yes Yes Yes Yes Yes Yes Depth to groundwater only
Any unusual field conditions, observations, or events:
Phase 2 has an earthen berm built w/in liner limits which may reduce any potential for overland flow from Phase 2.
Paths leading to wells and around entire facility have been improved by County recently. All are 4X4 accessible.
Fourth consecutive event that surface water samples collected from points SW-A and SW-B per the SWS verbal request.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Low gage height & flow
Low gage height & flow
Low gage height & flow
Low gage height & flow
Low gage height & flow
Dual lined leachate lagoon leak detection manhole observed to be dry.
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
June 14-15, 2016
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L (%/Vol)Visual
MW-1 62.04 1064.98 1127.02 17.5 NR NR 6.31 116 NR Slight
MW-2 13.21 923.47 936.68 14.6 NR NR 5.3 77 NR Clear
MW-3R 4.70 925.30 930.00 15.9 NR NR 5.6 304 NR Clear
MW-4S 9.23 934.00 943.23 15.0 NR NR 5.3 104 NR Clear
MW-4D 9.06 933.74 942.80 15.0 NR NR 5.7 128 NR NR Clear
MW-5 43.81 934.05 977.86 14.4 NR NR 5.3 110 NR Clear
MW-6R 65.65 939.10 1004.75 18.1 NR NR 6.45 310 NR Clear
MW-8 61.32 909.71 971.03 17.5 NR NR 6.31 160 NR Slight
MW-9S 32.24 920.59 952.83 14.8 NR NR 5.6 237 NR Clear
MW-9D 34.75 917.72 952.47 15.9 NR NR 6.7 491 NR Clear
MW-10 31.41 938.83 970.24 15.1 NR NR 6.73 103 NR Clear
MW-11S 31.21 937.88 969.09 14.9 NR NR 5.99 97 NR Clear
MW-11D 31.61 933.77 965.38 14.5 NR NR 6.89 134 NR NR Clear
MW-12 50.92 945.74 996.66 14.3 NR NR 6.81 191 NR NR Clear
MW-13 26.38 956.75 983.13 16.1 NR NR 6.88 103 NR NR Clear
MLW-A 83.01 1012.50 1095.51 NR NR NR NR NR NR NR NR
P2-6S 56.28 983.99 1040.27 NR NR NR NR NR NR NR NR
P2-6D 64.98 975.67 1040.65 NR NR NR NR NR NR NR NR
P2-11S 49.21 972.32 1021.53 NR NR NR NR NR NR NR NR
P2-11D 49.68 971.45 1021.13 NR NR NR NR NR NR NR NR
P2-12 52.49 934.12 986.61 NR NR NR NR NR NR NR NR
Minimum 4.70 909.71 930.00 14.3 NR NR 5.30 77 NR Clear
Average 41.10 950.75 991.85 15.6 NR NR 6.12 178 NR Clear
Maximum 83.01 1064.98 1127.02 18.1 NR NR 6.89 491 NR Slight
SW-1 ---19.2 NR NR 7.03 80 NR -Clear
SW-2 ---20.1 NR NR 6.99 110 NR -Clear
SW-3 ---20.8 NR NR 7.17 120 NR -Clear
SW-4 ---20.7 NR NR 7.21 90 NR -Clear
SWN-1 ---21.5 NR NR 7.7 69 NR -Clear
SWN-2 ---19.9 NR NR 7.03 80 NR -Clear
SW-A ---19.3 NR NR 7.03 80 NR -Clear
SW-B ---20.1 NR NR 7.04 80 NR -Clear
Minimum ---19.2 NR NR 6.99 69 NR -Clear
Average ---20.2 NR NR 7.15 89 NR -Clear
Maximum ---21.5 NR NR 7.7 120 NR -Clear
NR = No reading attempted
btoc = Below top of casing
amsl = Above mean sea level
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane
Gas in
Headspace
Turbidity of
Metals
Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
June 14-15, 2016
App. I App. II Field Parameter
T o t a l M e t a l s
T o t a l M e t a l s (A p p I I )
H e r b i c i d e s -C h l o r i n a t e d A p p I I
P e s t i c i d e s A p p I I
T o t a l C y a n i d e
S u l f i d e
T e m p e r a t u r e
C o n d u c t i v i t y
T o t a l D i s s o l v e d S o l i d s (T D S )
p H T u r b i d i t y
S u l f a t e
p H P h o s p h o r u s
B O D , 5 d a y
C O D
N i t r a t e
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
L a b S W 8 1 5 1 A
L a b E P A 8 2 7 0 D
L a b E P A 8 0 8 1 B
L a b E P A 9 0 1 4
L a b S M 1 8 4 5 0 0 -S D
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d V i s u a l
L a b E P A 3 0 0 .0
L a b E P A 9 0 4 0
L a b E P A 3 6 5 .1
L a b S M 5 2 1 0 B
L a b S M 5 2 2 0 D
L a b E P A 3 5 3 .2
MW-1 x x x x x x x x x x x x
MW-2 x x x x x x x x x x x x
MW-3R x x x x x x x x x x x x
MW-4S x x x x x x x x x x x x
MW-4D x x x x x x x x x x x x
MW-5 x x x x x x x x x x x x
MW-6R x x x x x x x x x x x x
MW-8 x x x x x x x x x x x x
MW-9S x x x x x x x x x x x x
MW-9D x x x x x x x x x x x x
MW-10 x x x x x x x x x x x x
MW-11S x x x x x x x x x x x x
MW-11D x x x x x x x x x x x x
MW-12 x x x x x x x x x x x x
MW-13 x x x x x x x x x x x x
SWN-1 x x x x x x x
SWN-2 x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
SW-3 x x x x x x x
SW-4 x x x x x x x
SWN-3 Not sampled since dry which is typical
SWN-4 Not sampled since dry which is typical
SW-A x x x x x x x
SW-B x x x x x x x
LAGOON x x x x x x x x x
EB x x x
FB x x
TB x
Appendix I & II = Lists from current 40 CFR 258
Leachate
V O C s
V O C s (A p p I I )
S e m i v o l a t i l e O r g a n i c s (S V O C s ) A p p I I
Surry County Subtitle D Lined Landfill Page 1 of 2
Table 5
June 15, 2016
Result Unit
MW-1 Chromium, total 6/15/16 13.7 2.5 10 10 100 N (Is BG)
MW-1 Cobalt, total 6/15/16 12 2.5 10 NE 1 NE N (Is BG)
MW-1 Copper, total 6/15/16 15.9 2.5 10 1000 NE
MW-1 Vanadium, total 6/15/16 9.8j 2.5 25 NE 3.5 NE N (Is BG)
MW-1 Zinc, total 6/15/16 55.9 5 10 1000 NE
MW-4D Cadmium, total 6/15/16 1.1 0.5 1 2 5
MW-4D Zinc, total 6/15/16 10.7 5 10 1000 NE
MW-5 Barium, total 6/15/16 156 2.5 100 700 1300
MW-5 Cadmium, total 6/15/16 2.3 0.5 1 2 5 N (<BL, <BG, >L)
MW-5 Chromium, total 6/15/16 12.1 2.5 10 10 100 N (<BL, <BG, >L)
MW-5 Copper, total 6/15/16 10.7 2.5 10 1000 NE
MW-5 Vanadium, total 6/15/16 18.5j 2.5 25 NE 3.5 NE N (<BL, <BG, >L)
MW-5 Zinc, total 6/15/16 36.7 5 10 1000 NE
MW-6R 6/15/16 1.2 0.97 1 4.6 5
MW-6R Vinyl chloride 6/15/16 1.3 0.62 1 0.03 2 L &/or LFG
MW-8 Barium, total 6/15/16 137 2.5 100 700 1300
MW-8 Vanadium, total 6/15/16 9.4j 2.5 25 NE 3.5 NE N (<BL, <BG, >L)
MW-8 Zinc, total 6/15/16 35.4 5 10 1000 NE
MW-9S Barium, total 6/15/16 125 2.5 100 700 1300
MW-9S Cadmium, total 6/15/16 2.4 0.5 1 2 5 N (<BL, <BG, >L)
MW-9S Cobalt, total 6/15/16 144 2.5 10 NE 1 NE N (<BL, <BG, >L)
MW-9S Copper, total 6/15/16 12.2 2.5 10 1000 NE
MW-9S Vinyl chloride 6/15/16 0.72J 0.62 1 0.03 2 L &/or LFG
MW-9S Zinc, total 6/15/16 18 5 10 1000 NE
MW-10 6/15/16 1 0.97 1 4.6 5
MW-10 Vanadium, total 6/15/16 10.8j 2.5 25 NE 3.5 NE N (<BL, <BG, >L)
MW-10 Zinc, total 6/15/16 20.5 5 10 1000 NE
MW-11D Vanadium, total 6/15/16 8.3j 2.5 25 NE 3.5 NE N (<BL, <BG, >L)
MW-12 Chromium, total 6/15/16 10.4 2.5 10 10 100 N (<BL, <BG, >L)
MW-12 Copper, total 6/15/16 11.3 2.5 10 1000 NE
MW-12 Vanadium, total 6/15/16 13.6j 2.5 25 NE 3.5 NE N (<BL, <BG, >L)
MW-12 Zinc, total 6/15/16 28.4 5 10 1000 NE
SWN-1 Cadmium, total 6/15/16 1.3 0.5 1 2 5
SWN-1 Zinc, total 6/15/16 13.8 5 10 1000 NE
Detections in Water Samples above SWSL, 2L, 2B, GWP or MCL
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause
8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Methylene Chloride ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Methylene Chloride ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surry County Subtitle D Lined Landfill Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause
8
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
<BG = Below the highest level ever observed in the background well (MW-A).
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
1 Table contains constituents detected at or above SWSL, 2L, 2B, GWP or MCL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
<BL = Below it's own BaseLine level established by the highest of the first 4 initial events within the first six months of operation.
>L = Above the highest ever observed in leachate after a 20:1 dilution factor.
L = Leachate
Surry County Lined MSWLF, Mt. Airy Page 1 of 1
Table 6
June 15, 2016
Sample ID Result Unit
MW-1 Cyanide, total 6/15/16 4.9j 4 10 70 200
MW-4S 6/15/16 1j 0.77 10 NE NE NE
MW-9S Cyanide, total 6/15/16 5.1j 4 10 70 NE
EB Tin, total 6/17/16 2.8j 2.5 100 NE NE NE NE
FB Tin, total 6/17/16 2.9j 2.5 100 NE NE NE NE
MW-8 Tin, total 6/15/16 8.4 2.5 100 NE NE NE NE
A definitive source of the detection was not determined as part of this report.
NE = Not Established
Detections in Water Samples above MDL (Appendix II Exclusive)
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7
ug/L
7,12-Dimethylbenz(a)anthracene ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains App II exclusive constituents detected over MDL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 GWP = Groundwater Protection Standard
7 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
j = The reported value is estimated & between the laboratory MDL & the SWSL, adjusted for actual sample preparation data and moisture content
* = 2L Standard is assigned to “free cyanide” not total cyanide so not considered a regulatory exceedance
BOLD = Concentration >applicable 2L Standard
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 7
June 15, 2016
Result Unit
LAGOON 6/15/16 4.6 0.24 1 0.4 5
LAGOON 6/15/16 1.1 0.27 1 0.6 5
LAGOON 6/15/16 3.6 0.33 1 6 75
LAGOON Benzene 6/15/16 3.5 0.25 1 1 5
LAGOON 6/15/16 6.7 0.19 5 70 70
LAGOON 6/15/16 2 0.3 1 550 700
LAGOON Vinyl chloride 6/15/16 4 0.62 1 0.03 2
LAGOON Chromium, total 6/15/16 13.3 2.5 10 10 100
LAGOON Thallium, total 6/15/16 8.9 5 5.5 NE 0.28 2
LAGOON Barium, total 6/15/16 189 2.5 100 700 1300
LAGOON BOD, 5 day 6/15/16 36000 2000 2000
LAGOON COD 6/15/16 114000 25000 50000
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
Detections in Leachate Samples above SWSL, 2L, 2B, GWP or MCL
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7
1,2-Dichloroethane ug/L
1,2-Dichloropropane ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Ethylbenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, 2L, 2B, GWP or MCL
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 8
June 16, 2016
Flow Rate
(cm/second)(%)(feet/feet)(feet/year)
MW-1 2.45E-04 3 0.165 1,394 N49E 62.04 1064.98 Rock
MW-2 3.20E-04 3 0.034 372 S27E 13.21 923.47 Rock
MW-3R 3.20E-04 3 0.039 425 S29E 4.70 925.3 Rock
MW-4S 1.50E-04 3 0.109 564 S24E 9.23 934.00 Sandy Silt & Fractured Rock
MW-4D 1.59E-04 3 --S23E 9.06 933.74 Rock
MW-5 3.20E-04 3 0.131 1,442 S60E 43.70 934.05 Rock
MW-6R 3.20E-04 3 0.075 830 S20E 65.65 939.10 Fractured Rock
MW-8 1.08E-03 3 0.064 2,366 S15E 61.32 909.71 Fractured Rock
MW-9S 7.45E-04 3 0.056 1,434 S23E 32.24 920.59 Fractured Rock
MW-9D 1.07E-05 3 --S23E 34.75 917.72 Competent Rock
MW-10 1.43E-04 3 0.084 415 S03E 31.41 938.83 Fractured Rock
MW-11S 6.19E-05 3 0.089 190 S02W 31.21 937.88 Competent Rock
MW-11D 3 ---37.35 915.7 Competent Rock
MW-12 1.91E-06 3 0.216 14 S28W 50.92 945.74 Competent Rock
MW-13 2.71E-03 3 0.140 13,117 S32W 26.38 956.75 Fractured Rock
P2-12 5.91E-07 3 0.057 1 S24W 52.49 934.12 Competent Rock
MLW-A 3 0.167 -N82E 83.01 1012.5 Competent Rock
Minimum 5.91E-07 3 0.034 1 -4.70 909.71 -
Average 4.39E-04 3 0.102 787 -38.16 943.78 -
Maximum 2.71E-03 3 0.216 2,366 -83.01 1064.98 -
NOTE: Hydraulic conductivity and effective porosity values derived from slug tests performed by MESCO.
where
Hydrogeologic Properties at Monitoring Well Locations
Monitoring
Location
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity
Hydraulic
Gradient
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation
Screened Interval
Lithology(feet btoc)(feet amsl)
na
na
Hydrologic gradient from water levels recorded on June 16, 2016.
Flow rate for MW-13 was considered an outlier; therefore not included in the average or maximum.
Flow rate (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e

Table 9
Total Metal Concentrations Evaluation Table
Surry Co. Subtitle D Lined MSWLF, Phases 1&2
Total Metal An
t
i
m
o
n
y
Ar
s
e
n
i
c
Ba
r
i
u
m
Be
r
y
l
l
i
u
m
Ca
d
m
i
u
m
Ch
r
o
m
i
u
m
Co
b
a
l
t
Co
p
p
e
r
Le
a
d
Ni
c
k
e
l
Se
l
e
n
i
u
m
Si
l
v
e
r
Th
a
l
l
i
u
m
Va
n
a
d
i
u
m
Zin
c
SWSL 6 10 100 1 1 10 10 10 10 50 10 10 5.5 25 10
2L/GWP STANDARD
SAMPLE ID
Screened
Lithology Data Period
MW-1 (BG Well)Bedrock ALL TIME HIGH 12.5 18.6 655 8.6 53.4 222 73.9 262 48.3 98.17.8 ND 10.5 147 806.
MW-2 Bedrock Max Baseline <30 <10 <500 2 1 <10 14 <200 <10 <50 <20 <10 <10 <40 <50
MW-3/MW-3R Bedrock Max Baseline <30 <10 <500 2 <1 <10 <10 <200 22 <50 <20 <10 <10 <40 <50
MW-4S Bedrock Max Baseline <30 <10 1860.26 9 146 164 <200 110 80.<20 <10 <10 <40 615.
MW-4D Bedrock Max Baseline <30 <10 <500 <2 13 12 <10 <200 <10 159 <20 <10 <10 <40 175.
MW-5 Bedrock Max Baseline <30 <10 <500 <2 4 29 15.<200 <10 99.<20 <10 <10 <40 107.
MW-6/MW-6R Bedrock Max Baseline <30 <10 <500 <2 2.16 18.<200 17 <50 <20 <10 <10 <40 93.
MW-8 Bedrock Max Baseline <5 15 2000 9.8 <1 154 87.5 108 44.5 99.5 <10 <5 5.4 256 720
MW-9S Bedrock Max Baseline <5 4.7 313 1.4 <1 39.7 10.4 19.2 12.2 21 <10 0.46 4.4 57.9 105
MW-9D Bedrock Max Baseline <5 <5 116 0.46 <1 21.9 7.3 10.1 <5 27.4 <10 0.41 <5.5 20.3 45.9
MW-10 Bedrock Max Baseline <5 <5 150 0.97 <1 25.2 8.8 18.9 7.3 22.4 <10 <5 <5.5 34.6 92.2
MW-11S Bedrock Max Baseline <5 5.6 182 2.4 <1 27.5 23 26.3 17.6 21.4 <10 0.12 <5.5 40.5 67.7
MW-11D Bedrock Max Baseline <5 6.3 119 0.79 <1 26.9 14.6 21.9 8 20.8 <10 0.24 <5.5 35.3 69.7
MW-12 Bedrock Max Baseline <5 <5 155 0.77 2.5 22.4 13.3 25.2 8.2 19.5 <10 <5 <5.5 31.2 47.6
MW-13 Bedrock Max Baseline <5 4.4 114 3.3 <1 16.1 19 20.8 10.5 14.8 <10 <5 <5.5 22.7 59.7
MW-14 Bedrock Max Baseline 6.4 <5 37.5 <1 <1 <5 <5 <5 <5 <5 <10 <5 6.6 <5 <10
MW-15 Bedrock Max Baseline 5.6 <5 60.1 1.5 6.9 42.7 5.7 6.5 6.9 7 <10 <5 7.7 38.3 46.8
MW-16 Bedrock Max Baseline 5.9 <5 80.2 <1 <1 <5 <5 <5 <5 <5 <10 <5 <5.5 <5 <10
LAGOON -ALL TIME HIGH 10 ND 847 ND ND 13.3 137 ND ND 8.9 13.4 2.4 57 9.5 31.1
Table contains concentrations of Appendix I metals
All Time High = Highest ever recorded at either the upgradient backgound well or untreated leachate sample. Samples consistantly collected on a semi-annual basis. This value will be kept current.
When two wells shown together indicates wells that have been replaced so data used for both wells
RED BOLD = Concentration Exceeded 2L or GWP Standard
Max Baseline = Maximum concentration detected during the first four events performed within 6 months of commencement of landfill operations including at least 1 before opening. Considered natural
intrawell background levels.
< = Not Detected with Detection Limit Indicated
SWSL = Solid Waste Section Reporting Limit
2L = North Carolina 15A NCAC 2L Groundwater Quality Standard (Current as of 10/6/16)
GWP = Groundwater Protection Standard (Current as of 10/6/16)
(BG Well) = Background Well Located hydraulically upgradient of Waste Unit
0.28 3.5 1000
BACKGROUND WELL PHASES 1-2
PHASES 1&2 CONTIGUOUS (PHASE 1 BASELINE 1998) (PHASE 2 BASELINE 2012)
UNTREATED LEACHATE (EFFECTIVELY A COMPOSITE OF PHASES 1&2) RESULTS FROM 1996 - 2016
70 1000 15 100 20 201.4 10 700 4 2 10
Iredell Co. Subtitle D Landfill, Phase 4 Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
July 01, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92301747
92301747
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CO. LINED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 16, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 139
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 2 of 139
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92301747001 MW-1 Water 06/15/16 16:45 06/16/16 08:06
92301747002 MW-2 Water 06/15/16 11:30 06/16/16 08:06
92301747003 MW-3R Water 06/15/16 11:20 06/16/16 08:06
92301747004 MW-4S Water 06/15/16 10:50 06/16/16 08:06
92301747005 MW-4D Water 06/15/16 10:45 06/16/16 08:06
92301747006 MW-5 Water 06/15/16 14:14 06/16/16 08:06
92301747007 MW-6R Water 06/15/16 14:35 06/16/16 08:06
92301747008 MW-8 Water 06/15/16 10:55 06/16/16 08:06
92301747009 MW-9S Water 06/15/16 09:00 06/16/16 08:06
92301747010 MW-9D Water 06/15/16 09:05 06/16/16 08:06
92301747011 MW-10 Water 06/15/16 10:06 06/16/16 08:06
92301747012 MW-11S Water 06/15/16 09:15 06/16/16 08:06
92301747013 MW-11D Water 06/15/16 09:19 06/16/16 08:06
92301747014 MW-12 Water 06/15/16 12:15 06/16/16 08:06
92301747015 MW-13 Water 06/15/16 12:10 06/16/16 08:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 139
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92301747001 MW-1 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747002 MW-2 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747003 MW-3R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747004 MW-4S EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747005 MW-4D EPA 8081 21 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 139
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747006 MW-5 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747007 MW-6R EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747008 MW-8 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747009 MW-9S EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 139
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747010 MW-9D EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747011 MW-10 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747012 MW-11S EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747013 MW-11D EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 139
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747014 MW-12 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
92301747015 MW-13 EPA 8081 21 PASI-CSWB
EPA 8082 8 PASI-CSWB
EPA 8151 6 PASI-OLJM
EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CNB
SM 4500-S2D 1 PASI-AWRC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92301747001 Collected:06/15/16 16:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/17/16 19:15 309-00-206/17/16 09:000.050 0.050 1
alpha-BHC ND ug/L 06/17/16 19:15 319-84-606/17/16 09:000.050 0.050 1
beta-BHC ND ug/L 06/17/16 19:15 319-85-706/17/16 09:000.050 0.050 1
delta-BHC ND ug/L 06/17/16 19:15 319-86-806/17/16 09:000.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/17/16 19:15 58-89-906/17/16 09:000.050 0.050 1
Chlordane (Technical)ND ug/L 06/17/16 19:15 57-74-906/17/16 09:000.50 0.20 1
4,4'-DDD ND ug/L 06/17/16 19:15 72-54-806/17/16 09:000.10 0.050 1
4,4'-DDE ND ug/L 06/17/16 19:15 72-55-906/17/16 09:000.10 0.050 1
4,4'-DDT ND ug/L 06/17/16 19:15 50-29-306/17/16 09:000.10 0.050 1
Dieldrin ND ug/L 06/17/16 19:15 60-57-106/17/16 09:000.075 0.050 1
Endosulfan I ND ug/L 06/17/16 19:15 959-98-806/17/16 09:000.10 0.050 1
Endosulfan II ND ug/L 06/17/16 19:15 33213-65-906/17/16 09:000.10 0.050 1
Endosulfan sulfate ND ug/L 06/17/16 19:15 1031-07-806/17/16 09:000.10 0.050 1
Endrin ND ug/L 06/17/16 19:15 72-20-806/17/16 09:000.10 0.050 1
Endrin aldehyde ND ug/L 06/17/16 19:15 7421-93-406/17/16 09:000.10 0.050 1
Heptachlor ND ug/L 06/17/16 19:15 76-44-806/17/16 09:000.050 0.050 1
Heptachlor epoxide ND ug/L 06/17/16 19:15 1024-57-306/17/16 09:000.075 0.050 1
Methoxychlor ND ug/L 06/17/16 19:15 72-43-506/17/16 09:001.0 0.15 1
Toxaphene ND ug/L 06/17/16 19:15 8001-35-206/17/16 09:001.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)85 %06/17/16 19:15 877-09-806/17/16 09:0020-130 1
Decachlorobiphenyl (S)62 %06/17/16 19:15 2051-24-306/17/16 09:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 02:32 12674-11-206/17/16 09:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 02:32 11104-28-206/17/16 09:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 02:32 11141-16-506/17/16 09:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 02:32 53469-21-906/17/16 09:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 02:32 12672-29-606/17/16 09:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 02:32 11097-69-106/17/16 09:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 02:32 11096-82-506/17/16 09:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)58 %06/18/16 02:32 2051-24-306/17/16 09:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 12:12 94-75-706/20/16 17:300.97 0.23 1
Dinoseb ND ug/L 06/22/16 12:12 88-85-7 CH06/20/16 17:300.19 0.059 1
Pentachlorophenol ND ug/L 06/22/16 12:12 87-86-506/20/16 17:300.029 0.018 1
2,4,5-T ND ug/L 06/22/16 12:12 93-76-506/20/16 17:300.20 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 12:12 93-72-106/20/16 17:300.20 0.051 1
Surrogates
2,4-DCAA (S)95 %06/22/16 12:12 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 17:09 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:25 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92301747001 Collected:06/15/16 16:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 66.7J ug/L 06/20/16 21:25 7440-39-306/17/16 21:051002.5 1
Beryllium 0.63J ug/L 06/20/16 21:25 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:25 7440-43-906/17/16 21:051.0 0.50 1
Chromium 13.7 ug/L 06/24/16 14:56 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt 12.0 ug/L 06/20/16 21:25 7440-48-406/17/16 21:0510.0 2.5 1
Copper 15.9 ug/L 06/20/16 21:25 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:25 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 20.8J ug/L 06/20/16 21:25 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:25 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:25 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:25 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 21:25 7440-31-506/17/16 21:051002.5 1
Vanadium 9.8J ug/L 06/20/16 21:25 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 55.9 ug/L 06/20/16 21:25 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:17 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/22/16 22:16 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/22/16 22:16 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/22/16 22:16 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/22/16 22:16 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/22/16 22:16 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/22/16 22:16 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/22/16 22:16 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/22/16 22:16 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/22/16 22:16 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/22/16 22:16 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/22/16 22:16 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/22/16 22:16 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/22/16 22:16 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/22/16 22:16 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/22/16 22:16 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/22/16 22:16 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/22/16 22:16 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/22/16 22:16 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/22/16 22:16 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/22/16 22:16 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/22/16 22:16 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/22/16 22:16 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/22/16 22:16 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/22/16 22:16 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/22/16 22:16 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/22/16 22:16 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/22/16 22:16 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92301747001 Collected:06/15/16 16:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/22/16 22:16 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/22/16 22:16 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/22/16 22:16 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/22/16 22:16 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/22/16 22:16 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/22/16 22:16 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/22/16 22:16 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/22/16 22:16 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/22/16 22:16 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/22/16 22:16 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/22/16 22:16 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/22/16 22:16 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/22/16 22:16 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/22/16 22:16 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/22/16 22:16 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/22/16 22:16 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/22/16 22:16 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/22/16 22:16 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/22/16 22:16 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/22/16 22:16 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/22/16 22:16 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/22/16 22:16 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/22/16 22:16 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/22/16 22:16 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/22/16 22:16 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/22/16 22:16 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/22/16 22:16 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/22/16 22:16 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/22/16 22:16 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/22/16 22:16 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/22/16 22:16 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/22/16 22:16 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/22/16 22:16 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/22/16 22:16 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/22/16 22:16 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/22/16 22:16 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/22/16 22:16 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/22/16 22:16 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/22/16 22:1606/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/22/16 22:16 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/22/16 22:16 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/22/16 22:16 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/22/16 22:16 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/22/16 22:16 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/22/16 22:16 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/22/16 22:16 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92301747001 Collected:06/15/16 16:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/22/16 22:16 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/22/16 22:16 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/22/16 22:16 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/22/16 22:16 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/22/16 22:16 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/22/16 22:16 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/22/16 22:16 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/22/16 22:16 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/22/16 22:16 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/22/16 22:16 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/22/16 22:16 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/22/16 22:16 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/22/16 22:16 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/22/16 22:16 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/22/16 22:16 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/22/16 22:16 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/22/16 22:16 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/22/16 22:16 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/22/16 22:16 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/22/16 22:1606/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/22/16 22:16 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/22/16 22:16 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/22/16 22:16 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/22/16 22:16 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/22/16 22:16 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/22/16 22:16 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/22/16 22:16 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/22/16 22:16 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/22/16 22:16 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/22/16 22:16 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/22/16 22:16 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/22/16 22:16 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)80 %06/22/16 22:16 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)82 %06/22/16 22:16 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)101 %06/22/16 22:16 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)29 %06/22/16 22:16 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)43 %06/22/16 22:16 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)97 %06/22/16 22:16 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 16:38 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 16:38 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 16:38 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 16:38 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 16:38 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92301747001 Collected:06/15/16 16:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 16:38 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 16:38 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 16:38 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 16:38 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 16:38 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 16:38 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 16:38 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 16:38 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 16:38 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 16:38 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 16:38 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 16:38 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 16:38 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 16:38 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 16:38 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 16:38 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 16:38 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 16:38 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 16:38 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 16:38 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 16:38 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 16:38 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 16:38 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 16:38 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 16:38 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 16:38 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 16:38 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 16:38 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 16:38 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 16:38 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 16:38 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 16:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 16:38 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 16:38 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 16:38 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 16:38 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 16:38 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 16:38 74-88-4 M110.0 0.32 1
Isobutanol ND ug/L 06/17/16 16:38 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 16:38 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 16:38 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 16:38 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 16:38 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 16:38 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 16:38 107-12-01503.6 1
Styrene ND ug/L 06/17/16 16:38 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 12 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92301747001 Collected:06/15/16 16:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 16:38 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 16:38 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 16:38 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 16:38 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 16:38 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 16:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 16:38 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 16:38 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 16:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 16:38 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 16:38 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 16:38 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 16:38 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 16:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 16:38 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 16:38 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.9J ug/L 06/17/16 15:11 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92301747002 Collected:06/15/16 11:30 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/17/16 19:33 309-00-206/17/16 09:000.050 0.050 1
alpha-BHC ND ug/L 06/17/16 19:33 319-84-606/17/16 09:000.050 0.050 1
beta-BHC ND ug/L 06/17/16 19:33 319-85-706/17/16 09:000.050 0.050 1
delta-BHC ND ug/L 06/17/16 19:33 319-86-806/17/16 09:000.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/17/16 19:33 58-89-906/17/16 09:000.050 0.050 1
Chlordane (Technical)ND ug/L 06/17/16 19:33 57-74-906/17/16 09:000.50 0.20 1
4,4'-DDD ND ug/L 06/17/16 19:33 72-54-806/17/16 09:000.10 0.050 1
4,4'-DDE ND ug/L 06/17/16 19:33 72-55-906/17/16 09:000.10 0.050 1
4,4'-DDT ND ug/L 06/17/16 19:33 50-29-306/17/16 09:000.10 0.050 1
Dieldrin ND ug/L 06/17/16 19:33 60-57-106/17/16 09:000.075 0.050 1
Endosulfan I ND ug/L 06/17/16 19:33 959-98-806/17/16 09:000.10 0.050 1
Endosulfan II ND ug/L 06/17/16 19:33 33213-65-906/17/16 09:000.10 0.050 1
Endosulfan sulfate ND ug/L 06/17/16 19:33 1031-07-806/17/16 09:000.10 0.050 1
Endrin ND ug/L 06/17/16 19:33 72-20-806/17/16 09:000.10 0.050 1
Endrin aldehyde ND ug/L 06/17/16 19:33 7421-93-406/17/16 09:000.10 0.050 1
Heptachlor ND ug/L 06/17/16 19:33 76-44-806/17/16 09:000.050 0.050 1
Heptachlor epoxide ND ug/L 06/17/16 19:33 1024-57-306/17/16 09:000.075 0.050 1
Methoxychlor ND ug/L 06/17/16 19:33 72-43-506/17/16 09:001.0 0.15 1
Toxaphene ND ug/L 06/17/16 19:33 8001-35-206/17/16 09:001.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)78 %06/17/16 19:33 877-09-806/17/16 09:0020-130 1
Decachlorobiphenyl (S)65 %06/17/16 19:33 2051-24-306/17/16 09:0020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 02:53 12674-11-206/17/16 09:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 02:53 11104-28-206/17/16 09:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 02:53 11141-16-506/17/16 09:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 02:53 53469-21-906/17/16 09:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 02:53 12672-29-606/17/16 09:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 02:53 11097-69-106/17/16 09:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 02:53 11096-82-506/17/16 09:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)60 %06/18/16 02:53 2051-24-306/17/16 09:0010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 12:42 94-75-706/20/16 17:300.95 0.23 1
Dinoseb ND ug/L 06/22/16 12:42 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 12:42 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 12:42 93-76-506/20/16 17:300.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 12:42 93-72-106/20/16 17:300.19 0.049 1
Surrogates
2,4-DCAA (S)93 %06/22/16 12:42 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 17:22 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:28 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92301747002 Collected:06/15/16 11:30 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 38.8J ug/L 06/20/16 21:28 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:28 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:28 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:28 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:28 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:28 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:28 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:28 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:28 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:28 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:28 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 21:28 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 21:28 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:28 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:24 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/22/16 22:45 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/22/16 22:45 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/22/16 22:45 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/22/16 22:45 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/22/16 22:45 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/22/16 22:45 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/22/16 22:45 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/22/16 22:45 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/22/16 22:45 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/22/16 22:45 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/22/16 22:45 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/22/16 22:45 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/22/16 22:45 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/22/16 22:45 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/22/16 22:45 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/22/16 22:45 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/22/16 22:45 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/22/16 22:45 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/22/16 22:45 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/22/16 22:45 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/22/16 22:45 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/22/16 22:45 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/22/16 22:45 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/22/16 22:45 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/22/16 22:45 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/22/16 22:45 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/22/16 22:45 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92301747002 Collected:06/15/16 11:30 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/22/16 22:45 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/22/16 22:45 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/22/16 22:45 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/22/16 22:45 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/22/16 22:45 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/22/16 22:45 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/22/16 22:45 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/22/16 22:45 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/22/16 22:45 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/22/16 22:45 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/22/16 22:45 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/22/16 22:45 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/22/16 22:45 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/22/16 22:45 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/22/16 22:45 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/22/16 22:45 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/22/16 22:45 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/22/16 22:45 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/22/16 22:45 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/22/16 22:45 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/22/16 22:45 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/22/16 22:45 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/22/16 22:45 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/22/16 22:45 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/22/16 22:45 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/22/16 22:45 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/22/16 22:45 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/22/16 22:45 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/22/16 22:45 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/22/16 22:45 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/22/16 22:45 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/22/16 22:45 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/22/16 22:45 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/22/16 22:45 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/22/16 22:45 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/22/16 22:45 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/22/16 22:45 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/22/16 22:45 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/22/16 22:4506/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/22/16 22:45 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/22/16 22:45 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/22/16 22:45 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/22/16 22:45 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/22/16 22:45 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/22/16 22:45 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/22/16 22:45 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92301747002 Collected:06/15/16 11:30 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/22/16 22:45 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/22/16 22:45 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/22/16 22:45 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/22/16 22:45 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/22/16 22:45 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/22/16 22:45 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/22/16 22:45 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/22/16 22:45 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/22/16 22:45 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/22/16 22:45 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/22/16 22:45 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/22/16 22:45 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/22/16 22:45 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/22/16 22:45 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/22/16 22:45 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/22/16 22:45 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/22/16 22:45 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/22/16 22:45 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/22/16 22:45 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/22/16 22:4506/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/22/16 22:45 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/22/16 22:45 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/22/16 22:45 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/22/16 22:45 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/22/16 22:45 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/22/16 22:45 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/22/16 22:45 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/22/16 22:45 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/22/16 22:45 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/22/16 22:45 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/22/16 22:45 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/22/16 22:45 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)70 %06/22/16 22:45 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)74 %06/22/16 22:45 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)97 %06/22/16 22:45 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)24 %06/22/16 22:45 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)36 %06/22/16 22:45 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)84 %06/22/16 22:45 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 16:56 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 16:56 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 16:56 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 16:56 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 16:56 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Page 17 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92301747002 Collected:06/15/16 11:30 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 16:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 16:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 16:56 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 16:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 16:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 16:56 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 16:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 16:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 16:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 16:56 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 16:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 16:56 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 16:56 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 16:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 16:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 16:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 16:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 16:56 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 16:56 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 16:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 16:56 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 16:56 75-71-85.0 0.21 1
1,1-Dichloroethane 2.7J ug/L 06/17/16 16:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 16:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 16:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.7J ug/L 06/17/16 16:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 16:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 16:56 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 16:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 16:56 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 16:56 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 16:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 16:56 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 16:56 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 16:56 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 16:56 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 16:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 16:56 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 16:56 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 16:56 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 16:56 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 16:56 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 16:56 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 16:56 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 16:56 107-12-01503.6 1
Styrene ND ug/L 06/17/16 16:56 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92301747002 Collected:06/15/16 11:30 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 16:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 16:56 79-34-53.0 0.40 1
Tetrachloroethene 0.64J ug/L 06/17/16 16:56 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 16:56 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 16:56 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 16:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 16:56 79-00-51.0 0.29 1
Trichloroethene 0.49J ug/L 06/17/16 16:56 79-01-61.0 0.47 1
Trichlorofluoromethane 0.22J ug/L 06/17/16 16:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 16:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 16:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 16:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 16:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 16:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 16:56 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 16:56 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:12 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92301747003 Collected:06/15/16 11:20 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/20/16 22:47 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/20/16 22:47 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/20/16 22:47 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/20/16 22:47 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/20/16 22:47 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/20/16 22:47 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/20/16 22:47 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/20/16 22:47 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/20/16 22:47 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/20/16 22:47 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/20/16 22:47 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/20/16 22:47 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/20/16 22:47 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/20/16 22:47 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/20/16 22:47 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/20/16 22:47 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/20/16 22:47 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/20/16 22:47 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/20/16 22:47 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)76 %06/20/16 22:47 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)81 %06/20/16 22:47 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 04:16 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 04:16 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 04:16 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 04:16 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 04:16 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 04:16 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 04:16 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)56 %06/18/16 04:16 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 13:12 94-75-706/20/16 17:300.97 0.23 1
Dinoseb ND ug/L 06/22/16 13:12 88-85-7 CH06/20/16 17:300.20 0.059 1
Pentachlorophenol ND ug/L 06/22/16 13:12 87-86-506/20/16 17:300.029 0.018 1
2,4,5-T ND ug/L 06/22/16 13:12 93-76-506/20/16 17:300.20 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 13:12 93-72-106/20/16 17:300.20 0.051 1
Surrogates
2,4-DCAA (S)89 %06/22/16 13:12 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 17:25 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:31 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92301747003 Collected:06/15/16 11:20 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 84.1J ug/L 06/20/16 21:31 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:31 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:31 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:31 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:31 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:31 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:31 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 2.8J ug/L 06/20/16 21:31 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:31 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:31 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:31 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 21:31 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 21:31 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 6.1J ug/L 06/20/16 21:31 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:27 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/22/16 23:14 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/22/16 23:14 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/22/16 23:14 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/22/16 23:14 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/22/16 23:14 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/22/16 23:14 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/22/16 23:14 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/22/16 23:14 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/22/16 23:14 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/22/16 23:14 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/22/16 23:14 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/22/16 23:14 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/22/16 23:14 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/22/16 23:14 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/22/16 23:14 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/22/16 23:14 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/22/16 23:14 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/22/16 23:14 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/22/16 23:14 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/22/16 23:14 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/22/16 23:14 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/22/16 23:14 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/22/16 23:14 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/22/16 23:14 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/22/16 23:14 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/22/16 23:14 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/22/16 23:14 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92301747003 Collected:06/15/16 11:20 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/22/16 23:14 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/22/16 23:14 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/22/16 23:14 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/22/16 23:14 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/22/16 23:14 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/22/16 23:14 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/22/16 23:14 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/22/16 23:14 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/22/16 23:14 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/22/16 23:14 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/22/16 23:14 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/22/16 23:14 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/22/16 23:14 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/22/16 23:14 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/22/16 23:14 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/22/16 23:14 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/22/16 23:14 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/22/16 23:14 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/22/16 23:14 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/22/16 23:14 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/22/16 23:14 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/22/16 23:14 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/22/16 23:14 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/22/16 23:14 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/22/16 23:14 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/22/16 23:14 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/22/16 23:14 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/22/16 23:14 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/22/16 23:14 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/22/16 23:14 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/22/16 23:14 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/22/16 23:14 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/22/16 23:14 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/22/16 23:14 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/22/16 23:14 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/22/16 23:14 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/22/16 23:14 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/22/16 23:14 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/22/16 23:1406/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/22/16 23:14 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/22/16 23:14 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/22/16 23:14 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/22/16 23:14 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/22/16 23:14 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/22/16 23:14 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/22/16 23:14 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 22 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92301747003 Collected:06/15/16 11:20 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/22/16 23:14 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/22/16 23:14 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/22/16 23:14 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/22/16 23:14 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/22/16 23:14 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/22/16 23:14 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/22/16 23:14 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/22/16 23:14 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/22/16 23:14 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/22/16 23:14 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/22/16 23:14 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/22/16 23:14 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/22/16 23:14 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/22/16 23:14 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/22/16 23:14 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/22/16 23:14 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/22/16 23:14 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/22/16 23:14 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/22/16 23:14 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/22/16 23:1406/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/22/16 23:14 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/22/16 23:14 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/22/16 23:14 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/22/16 23:14 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/22/16 23:14 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/22/16 23:14 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/22/16 23:14 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/22/16 23:14 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/22/16 23:14 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/22/16 23:14 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/22/16 23:14 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/22/16 23:14 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)53 %06/22/16 23:14 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)56 %06/22/16 23:14 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)74 %06/22/16 23:14 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)19 %06/22/16 23:14 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)27 %06/22/16 23:14 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)78 %06/22/16 23:14 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 17:30 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 17:30 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 17:30 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 17:30 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 17:30 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92301747003 Collected:06/15/16 11:20 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 17:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 17:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 17:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 17:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 17:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 17:30 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 17:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 17:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 17:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 17:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 17:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 17:30 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 17:30 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 17:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 17:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 17:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 17:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 17:30 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 17:30 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 17:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 17:30 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 17:30 75-71-85.0 0.21 1
1,1-Dichloroethane 2.4J ug/L 06/17/16 17:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 17:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 17:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.8J ug/L 06/17/16 17:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 17:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 17:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 17:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 17:30 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 17:30 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 17:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 17:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 17:30 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 17:30 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 17:30 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 17:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 17:30 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 17:30 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 17:30 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 17:30 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 17:30 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 17:30 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 17:30 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 17:30 107-12-01503.6 1
Styrene ND ug/L 06/17/16 17:30 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92301747003 Collected:06/15/16 11:20 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 17:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 17:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 17:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 17:30 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 17:30 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 17:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 17:30 79-00-51.0 0.29 1
Trichloroethene 0.49J ug/L 06/17/16 17:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 17:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 17:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 17:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 17:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 17:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 17:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 17:30 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 17:30 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:13 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92301747004 Collected:06/15/16 10:50 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/20/16 23:04 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/20/16 23:04 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/20/16 23:04 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/20/16 23:04 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/20/16 23:04 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/20/16 23:04 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/20/16 23:04 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/20/16 23:04 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/20/16 23:04 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/20/16 23:04 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/20/16 23:04 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/20/16 23:04 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/20/16 23:04 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/20/16 23:04 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/20/16 23:04 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/20/16 23:04 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/20/16 23:04 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/20/16 23:04 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/20/16 23:04 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)82 %06/20/16 23:04 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)50 %06/20/16 23:04 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 04:37 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 04:37 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 04:37 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 04:37 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 04:37 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 04:37 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 04:37 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)43 %06/18/16 04:37 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 13:42 94-75-706/20/16 17:300.96 0.23 1
Dinoseb ND ug/L 06/22/16 13:42 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 13:42 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 13:42 93-76-506/20/16 17:300.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 13:42 93-72-106/20/16 17:300.19 0.050 1
Surrogates
2,4-DCAA (S)87 %06/22/16 13:42 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 04:38 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:49 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92301747004 Collected:06/15/16 10:50 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 51.7J ug/L 06/20/16 21:49 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:49 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:49 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:49 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:49 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:49 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:49 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:49 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:49 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:49 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:49 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 21:49 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 21:49 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:49 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:29 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/28/16 13:15 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/28/16 13:15 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/28/16 13:15 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/28/16 13:15 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/28/16 13:15 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/28/16 13:15 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/28/16 13:15 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/28/16 13:15 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/28/16 13:15 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/28/16 13:15 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/28/16 13:15 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/28/16 13:15 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/28/16 13:15 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/28/16 13:15 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/28/16 13:15 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/28/16 13:15 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/28/16 13:15 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/16 13:15 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/28/16 13:15 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/28/16 13:15 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/28/16 13:15 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/28/16 13:15 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/28/16 13:15 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/28/16 13:15 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/28/16 13:15 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/28/16 13:15 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/28/16 13:15 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92301747004 Collected:06/15/16 10:50 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/28/16 13:15 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/28/16 13:15 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/28/16 13:15 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/28/16 13:15 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/28/16 13:15 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene 1.0J ug/L 06/28/16 13:15 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/28/16 13:15 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/28/16 13:15 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/28/16 13:15 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/28/16 13:15 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/16 13:15 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/28/16 13:15 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/28/16 13:15 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/28/16 13:15 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/28/16 13:15 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/16 13:15 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/28/16 13:15 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/28/16 13:15 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/16 13:15 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/28/16 13:15 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/28/16 13:15 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/28/16 13:15 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/28/16 13:15 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/28/16 13:15 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/28/16 13:15 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/28/16 13:15 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/28/16 13:15 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/16 13:15 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/28/16 13:15 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/28/16 13:15 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/28/16 13:15 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/28/16 13:15 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/28/16 13:15 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/28/16 13:15 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/28/16 13:15 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/28/16 13:15 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/28/16 13:15 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/16 13:15 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/16 13:1506/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/28/16 13:15 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/28/16 13:15 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/28/16 13:15 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/28/16 13:15 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/28/16 13:15 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/28/16 13:15 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/28/16 13:15 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92301747004 Collected:06/15/16 10:50 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/28/16 13:15 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/28/16 13:15 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/28/16 13:15 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/28/16 13:15 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/28/16 13:15 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/28/16 13:15 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/16 13:15 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/28/16 13:15 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/28/16 13:15 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/28/16 13:15 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/28/16 13:15 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/28/16 13:15 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/16 13:15 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/28/16 13:15 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/28/16 13:15 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/28/16 13:15 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/28/16 13:15 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/28/16 13:15 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/28/16 13:15 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/28/16 13:1506/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/28/16 13:15 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/28/16 13:15 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/28/16 13:15 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/28/16 13:15 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/28/16 13:15 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/28/16 13:15 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/28/16 13:15 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/28/16 13:15 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/28/16 13:15 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/16 13:15 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/28/16 13:15 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/28/16 13:15 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)72 %06/28/16 13:15 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)76 %06/28/16 13:15 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)98 %06/28/16 13:15 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)33 %06/28/16 13:15 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)40 %06/28/16 13:15 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)76 %06/28/16 13:15 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 17:47 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 17:47 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 17:47 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 17:47 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 17:47 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92301747004 Collected:06/15/16 10:50 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 17:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 17:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 17:47 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 17:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 17:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 17:47 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 17:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 17:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 17:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 17:47 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 17:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 17:47 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 17:47 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 17:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 17:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 17:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 17:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 17:47 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 17:47 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 17:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 17:47 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 17:47 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 17:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 17:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 17:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 17:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 17:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 17:47 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 17:47 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 17:47 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 17:47 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 17:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 17:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 17:47 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 17:47 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 17:47 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 17:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 17:47 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 17:47 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 17:47 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 17:47 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 17:47 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 17:47 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 17:47 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 17:47 107-12-01503.6 1
Styrene ND ug/L 06/17/16 17:47 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92301747004 Collected:06/15/16 10:50 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 17:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 17:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 17:47 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 17:47 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 17:47 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 17:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 17:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 17:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 17:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 17:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 17:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 17:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 17:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 17:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 17:47 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 17:47 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:13 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 31 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92301747005 Collected:06/15/16 10:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/20/16 23:22 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/20/16 23:22 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/20/16 23:22 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/20/16 23:22 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/20/16 23:22 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/20/16 23:22 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/20/16 23:22 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/20/16 23:22 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/20/16 23:22 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/20/16 23:22 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/20/16 23:22 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/20/16 23:22 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/20/16 23:22 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/20/16 23:22 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/20/16 23:22 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/20/16 23:22 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/20/16 23:22 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/20/16 23:22 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/20/16 23:22 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)93 %06/20/16 23:22 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)61 %06/20/16 23:22 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 04:58 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 04:58 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 04:58 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 04:58 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 04:58 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 04:58 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 04:58 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)56 %06/18/16 04:58 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 14:12 94-75-706/20/16 17:300.99 0.24 1
Dinoseb ND ug/L 06/22/16 14:12 88-85-7 CH06/20/16 17:300.20 0.060 1
Pentachlorophenol ND ug/L 06/22/16 14:12 87-86-506/20/16 17:300.030 0.018 1
2,4,5-T ND ug/L 06/22/16 14:12 93-76-506/20/16 17:300.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 14:12 93-72-106/20/16 17:300.20 0.052 1
Surrogates
2,4-DCAA (S)80 %06/22/16 14:12 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 04:57 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:58 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92301747005 Collected:06/15/16 10:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 52.4J ug/L 06/20/16 21:58 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:58 7440-41-706/17/16 21:051.0 0.50 1
Cadmium 1.1 ug/L 06/20/16 21:58 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:58 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:58 7440-48-406/17/16 21:0510.0 2.5 1
Copper 2.6J ug/L 06/20/16 21:58 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:58 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:58 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:58 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:58 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:58 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 21:58 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 21:58 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 10.7 ug/L 06/20/16 21:58 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:32 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/28/16 11:20 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/28/16 11:20 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/28/16 11:20 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/28/16 11:20 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/28/16 11:20 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/28/16 11:20 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/28/16 11:20 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/28/16 11:20 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/28/16 11:20 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/28/16 11:20 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/28/16 11:20 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/28/16 11:20 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/28/16 11:20 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/28/16 11:20 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/28/16 11:20 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/28/16 11:20 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/28/16 11:20 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/16 11:20 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/28/16 11:20 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/28/16 11:20 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/28/16 11:20 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/28/16 11:20 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/28/16 11:20 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/28/16 11:20 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/28/16 11:20 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/28/16 11:20 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/28/16 11:20 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92301747005 Collected:06/15/16 10:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/28/16 11:20 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/28/16 11:20 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/28/16 11:20 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/28/16 11:20 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/28/16 11:20 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/28/16 11:20 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/28/16 11:20 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/28/16 11:20 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/28/16 11:20 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/28/16 11:20 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/16 11:20 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/28/16 11:20 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/28/16 11:20 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/28/16 11:20 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/28/16 11:20 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/16 11:20 117-84-0 M106/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/28/16 11:20 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/28/16 11:20 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/16 11:20 117-81-7 M106/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/28/16 11:20 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/28/16 11:20 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/28/16 11:20 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/28/16 11:20 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/28/16 11:20 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/28/16 11:20 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/28/16 11:20 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/28/16 11:20 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/16 11:20 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/28/16 11:20 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/28/16 11:20 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/28/16 11:20 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/28/16 11:20 143-50-0 M106/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/28/16 11:20 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/28/16 11:20 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/28/16 11:20 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/28/16 11:20 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/28/16 11:20 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/16 11:20 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/16 11:2006/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/28/16 11:20 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/28/16 11:20 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/28/16 11:20 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/28/16 11:20 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/28/16 11:20 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/28/16 11:20 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/28/16 11:20 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92301747005 Collected:06/15/16 10:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/28/16 11:20 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/28/16 11:20 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/28/16 11:20 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/28/16 11:20 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/28/16 11:20 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/28/16 11:20 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/16 11:20 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/28/16 11:20 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/28/16 11:20 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/28/16 11:20 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/28/16 11:20 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/28/16 11:20 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/16 11:20 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/28/16 11:20 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/28/16 11:20 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/28/16 11:20 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/28/16 11:20 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/28/16 11:20 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/28/16 11:20 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/28/16 11:2006/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/28/16 11:20 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/28/16 11:20 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/28/16 11:20 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/28/16 11:20 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/28/16 11:20 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/28/16 11:20 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/28/16 11:20 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/28/16 11:20 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/28/16 11:20 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/16 11:20 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/28/16 11:20 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/28/16 11:20 99-35-4 L3,M006/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)70 %06/28/16 11:20 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)68 %06/28/16 11:20 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)93 %06/28/16 11:20 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)29 %06/28/16 11:20 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)38 %06/28/16 11:20 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)74 %06/28/16 11:20 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 18:04 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 18:04 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 18:04 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 18:04 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 18:04 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92301747005 Collected:06/15/16 10:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 18:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 18:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 18:04 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 18:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 18:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 18:04 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 18:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 18:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 18:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 18:04 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 18:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 18:04 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 18:04 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 18:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 18:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 18:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 18:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 18:04 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 18:04 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 18:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 18:04 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 18:04 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 18:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 18:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 18:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 18:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 18:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 18:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 18:04 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 18:04 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 18:04 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 18:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 18:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 18:04 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 18:04 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 18:04 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 18:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 18:04 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 18:04 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 18:04 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 18:04 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 18:04 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 18:04 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 18:04 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 18:04 107-12-01503.6 1
Styrene ND ug/L 06/17/16 18:04 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92301747005 Collected:06/15/16 10:45 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 18:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 18:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 18:04 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 18:04 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 18:04 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 18:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 18:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 18:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 18:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 18:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 18:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 18:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 18:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 18:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 18:04 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 18:04 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:14 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92301747006 Collected:06/15/16 14:14 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/20/16 23:39 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/20/16 23:39 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/20/16 23:39 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/20/16 23:39 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/20/16 23:39 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/20/16 23:39 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/20/16 23:39 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/20/16 23:39 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/20/16 23:39 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/20/16 23:39 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/20/16 23:39 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/20/16 23:39 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/20/16 23:39 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/20/16 23:39 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/20/16 23:39 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/20/16 23:39 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/20/16 23:39 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/20/16 23:39 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/20/16 23:39 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)76 %06/20/16 23:39 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)55 %06/20/16 23:39 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 05:39 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 05:39 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 05:39 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 05:39 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 05:39 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 05:39 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 05:39 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)49 %06/18/16 05:39 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 14:42 94-75-706/20/16 17:300.96 0.23 1
Dinoseb ND ug/L 06/22/16 14:42 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 14:42 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 14:42 93-76-506/20/16 17:300.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 14:42 93-72-106/20/16 17:300.19 0.050 1
Surrogates
2,4-DCAA (S)86 %06/22/16 14:42 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:00 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:02 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92301747006 Collected:06/15/16 14:14 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 156 ug/L 06/20/16 22:02 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:02 7440-41-706/17/16 21:051.0 0.50 1
Cadmium 2.3 ug/L 06/20/16 22:02 7440-43-906/17/16 21:051.0 0.50 1
Chromium 12.1 ug/L 06/20/16 22:02 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt 5.8J ug/L 06/20/16 22:02 7440-48-406/17/16 21:0510.0 2.5 1
Copper 10.7 ug/L 06/20/16 22:02 7440-50-806/17/16 21:0510.0 2.5 1
Lead 4.8J ug/L 06/20/16 22:02 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 7.0J ug/L 06/20/16 22:02 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:02 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:02 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:02 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:02 7440-31-506/17/16 21:051002.5 1
Vanadium 18.5J ug/L 06/20/16 22:02 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 36.7 ug/L 06/20/16 22:02 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:34 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/28/16 11:49 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/28/16 11:49 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/28/16 11:49 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/28/16 11:49 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/28/16 11:49 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/28/16 11:49 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/28/16 11:49 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/28/16 11:49 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/28/16 11:49 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/28/16 11:49 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/28/16 11:49 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/28/16 11:49 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/28/16 11:49 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/28/16 11:49 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/28/16 11:49 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/28/16 11:49 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/28/16 11:49 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/16 11:49 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/28/16 11:49 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/28/16 11:49 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/28/16 11:49 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/28/16 11:49 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/28/16 11:49 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/28/16 11:49 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/28/16 11:49 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/28/16 11:49 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/28/16 11:49 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92301747006 Collected:06/15/16 14:14 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/28/16 11:49 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/28/16 11:49 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/28/16 11:49 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/28/16 11:49 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/28/16 11:49 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/28/16 11:49 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/28/16 11:49 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/28/16 11:49 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/28/16 11:49 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/28/16 11:49 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/16 11:49 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/28/16 11:49 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/28/16 11:49 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/28/16 11:49 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/28/16 11:49 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/16 11:49 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/28/16 11:49 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/28/16 11:49 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/16 11:49 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/28/16 11:49 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/28/16 11:49 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/28/16 11:49 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/28/16 11:49 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/28/16 11:49 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/28/16 11:49 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/28/16 11:49 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/28/16 11:49 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/16 11:49 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/28/16 11:49 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/28/16 11:49 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/28/16 11:49 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/28/16 11:49 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/28/16 11:49 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/28/16 11:49 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/28/16 11:49 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/28/16 11:49 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/28/16 11:49 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/16 11:49 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/16 11:4906/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/28/16 11:49 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/28/16 11:49 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/28/16 11:49 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/28/16 11:49 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/28/16 11:49 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/28/16 11:49 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/28/16 11:49 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92301747006 Collected:06/15/16 14:14 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/28/16 11:49 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/28/16 11:49 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/28/16 11:49 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/28/16 11:49 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/28/16 11:49 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/28/16 11:49 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/16 11:49 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/28/16 11:49 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/28/16 11:49 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/28/16 11:49 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/28/16 11:49 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/28/16 11:49 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/16 11:49 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/28/16 11:49 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/28/16 11:49 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/28/16 11:49 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/28/16 11:49 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/28/16 11:49 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/28/16 11:49 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/28/16 11:4906/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/28/16 11:49 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/28/16 11:49 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/28/16 11:49 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/28/16 11:49 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/28/16 11:49 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/28/16 11:49 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/28/16 11:49 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/28/16 11:49 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/28/16 11:49 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/16 11:49 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/28/16 11:49 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/28/16 11:49 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)84 %06/28/16 11:49 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)83 %06/28/16 11:49 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)104 %06/28/16 11:49 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)36 %06/28/16 11:49 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)44 %06/28/16 11:49 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)86 %06/28/16 11:49 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 18:21 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 18:21 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 18:21 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 18:21 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 18:21 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 41 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92301747006 Collected:06/15/16 14:14 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 18:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 18:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 18:21 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 18:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 18:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 18:21 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 18:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 18:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 18:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 18:21 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 18:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 18:21 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 18:21 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 18:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 18:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 18:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 18:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 18:21 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 18:21 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 18:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 18:21 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 18:21 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 18:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 18:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 18:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.52J ug/L 06/17/16 18:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 18:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 18:21 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 18:21 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 18:21 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 18:21 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 18:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 18:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 18:21 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 18:21 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 18:21 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 18:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 18:21 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 18:21 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 18:21 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 18:21 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 18:21 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 18:21 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 18:21 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 18:21 107-12-01503.6 1
Styrene ND ug/L 06/17/16 18:21 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92301747006 Collected:06/15/16 14:14 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 18:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 18:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 18:21 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 18:21 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 18:21 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 18:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 18:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 18:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 18:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 18:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 18:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 18:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 18:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %06/17/16 18:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %06/17/16 18:21 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 18:21 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:15 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92301747007 Collected:06/15/16 14:35 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/20/16 23:57 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/20/16 23:57 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/20/16 23:57 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/20/16 23:57 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/20/16 23:57 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/20/16 23:57 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/20/16 23:57 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/20/16 23:57 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/20/16 23:57 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/20/16 23:57 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/20/16 23:57 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/20/16 23:57 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/20/16 23:57 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/20/16 23:57 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/20/16 23:57 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/20/16 23:57 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/20/16 23:57 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/20/16 23:57 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/20/16 23:57 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)66 %06/20/16 23:57 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)65 %06/20/16 23:57 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 06:00 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 06:00 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 06:00 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 06:00 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 06:00 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 06:00 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 06:00 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)60 %06/18/16 06:00 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 15:12 94-75-706/20/16 17:300.95 0.23 1
Dinoseb ND ug/L 06/22/16 15:12 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 15:12 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 15:12 93-76-506/20/16 17:300.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 15:12 93-72-106/20/16 17:300.19 0.050 1
Surrogates
2,4-DCAA (S)82 %06/22/16 15:12 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:03 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:05 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92301747007 Collected:06/15/16 14:35 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 67.0J ug/L 06/20/16 22:05 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:05 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:05 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 22:05 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:05 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 22:05 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:05 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 22:05 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:05 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:05 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:05 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:05 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 22:05 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 22:05 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:36 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 15:17 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 15:17 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 15:17 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 15:17 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 15:17 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 15:17 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 15:17 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 15:17 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 15:17 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 15:17 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 15:17 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 15:17 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 15:17 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 15:17 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 15:17 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 15:17 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 15:17 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 15:17 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 15:17 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 15:17 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 15:17 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 15:17 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 15:17 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 15:17 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 15:17 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 15:17 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 15:17 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92301747007 Collected:06/15/16 14:35 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 15:17 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 15:17 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 15:17 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 15:17 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 15:17 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 15:17 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 15:17 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 15:17 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 15:17 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 15:17 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 15:17 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 15:17 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 15:17 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 15:17 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 15:17 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 15:17 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 15:17 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 15:17 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 15:17 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 15:17 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 15:17 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 15:17 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 15:17 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 15:17 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 15:17 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 15:17 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 15:17 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 15:17 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 15:17 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 15:17 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 15:17 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 15:17 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 15:17 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 15:17 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 15:17 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 15:17 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 15:17 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 15:17 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 15:1706/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 15:17 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 15:17 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 15:17 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 15:17 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 15:17 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 15:17 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 15:17 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 46 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92301747007 Collected:06/15/16 14:35 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 15:17 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 15:17 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 15:17 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 15:17 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 15:17 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 15:17 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 15:17 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 15:17 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 15:17 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 15:17 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 15:17 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 15:17 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 15:17 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 15:17 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 15:17 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 15:17 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 15:17 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 15:17 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 15:17 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 15:1706/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 15:17 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 15:17 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 15:17 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 15:17 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 15:17 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 15:17 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 15:17 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 15:17 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 15:17 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 15:17 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 15:17 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 15:17 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)60 %06/23/16 15:17 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)63 %06/23/16 15:17 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)80 %06/23/16 15:17 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)22 %06/23/16 15:17 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)33 %06/23/16 15:17 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)90 %06/23/16 15:17 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 18:38 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 18:38 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 18:38 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 18:38 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 18:38 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92301747007 Collected:06/15/16 14:35 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene 0.37J ug/L 06/17/16 18:38 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 18:38 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 18:38 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 18:38 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 18:38 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 18:38 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 18:38 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 18:38 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 18:38 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 18:38 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 18:38 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 18:38 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 18:38 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 18:38 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 18:38 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 18:38 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 18:38 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 18:38 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 18:38 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 18:38 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 18:38 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 18:38 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 18:38 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 18:38 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 18:38 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.2J ug/L 06/17/16 18:38 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 18:38 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 18:38 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 18:38 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 18:38 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 18:38 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 18:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 18:38 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 18:38 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 18:38 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 18:38 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 18:38 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 18:38 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 18:38 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 18:38 126-98-71000.93 1
Methylene Chloride 1.2 ug/L 06/17/16 18:38 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 18:38 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 18:38 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 18:38 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 18:38 107-12-01503.6 1
Styrene ND ug/L 06/17/16 18:38 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92301747007 Collected:06/15/16 14:35 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 18:38 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 18:38 79-34-53.0 0.40 1
Tetrachloroethene 0.57J ug/L 06/17/16 18:38 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 18:38 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 18:38 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 18:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 18:38 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 18:38 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 18:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 18:38 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 18:38 108-05-450.0 0.35 1
Vinyl chloride 1.3 ug/L 06/17/16 18:38 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 18:38 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %06/17/16 18:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 18:38 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 18:38 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:16 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92301747008 Collected:06/15/16 10:55 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 00:14 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 00:14 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 00:14 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 00:14 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 00:14 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 00:14 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 00:14 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 00:14 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 00:14 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 00:14 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 00:14 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 00:14 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 00:14 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 00:14 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 00:14 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 00:14 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 00:14 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 00:14 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 00:14 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %06/21/16 00:14 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)51 %06/21/16 00:14 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 06:42 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 06:42 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 06:42 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 06:42 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 06:42 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 06:42 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 06:42 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)49 %06/18/16 06:42 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 15:42 94-75-706/20/16 17:300.95 0.23 1
Dinoseb ND ug/L 06/22/16 15:42 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 15:42 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 15:42 93-76-506/20/16 17:300.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 15:42 93-72-106/20/16 17:300.19 0.050 1
Surrogates
2,4-DCAA (S)90 %06/22/16 15:42 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:06 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:08 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92301747008 Collected:06/15/16 10:55 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 137 ug/L 06/20/16 22:08 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:08 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:08 7440-43-906/17/16 21:051.0 0.50 1
Chromium 6.3J ug/L 06/20/16 22:08 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:08 7440-48-406/17/16 21:0510.0 2.5 1
Copper 5.7J ug/L 06/20/16 22:08 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:08 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 4.5J ug/L 06/20/16 22:08 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:08 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:08 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:08 7440-28-006/17/16 21:055.5 5.0 1
Tin 8.4J ug/L 06/20/16 22:08 7440-31-506/17/16 21:051002.5 1
Vanadium 9.4J ug/L 06/20/16 22:08 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 35.4 ug/L 06/20/16 22:08 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:43 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 16:17 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 16:17 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 16:17 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 16:17 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 16:17 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 16:17 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 16:17 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 16:17 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 16:17 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 16:17 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 16:17 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 16:17 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 16:17 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 16:17 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 16:17 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 16:17 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 16:17 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 16:17 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 16:17 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 16:17 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 16:17 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 16:17 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 16:17 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 16:17 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 16:17 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 16:17 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 16:17 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92301747008 Collected:06/15/16 10:55 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 16:17 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 16:17 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 16:17 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 16:17 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 16:17 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 16:17 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 16:17 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 16:17 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 16:17 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 16:17 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 16:17 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 16:17 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 16:17 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 16:17 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 16:17 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 16:17 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 16:17 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 16:17 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 16:17 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 16:17 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 16:17 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 16:17 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 16:17 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 16:17 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 16:17 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 16:17 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 16:17 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 16:17 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 16:17 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 16:17 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 16:17 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 16:17 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 16:17 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 16:17 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 16:17 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 16:17 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 16:17 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 16:17 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 16:1706/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 16:17 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 16:17 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 16:17 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 16:17 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 16:17 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 16:17 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 16:17 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92301747008 Collected:06/15/16 10:55 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 16:17 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 16:17 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 16:17 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 16:17 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 16:17 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 16:17 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 16:17 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 16:17 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 16:17 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 16:17 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 16:17 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 16:17 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 16:17 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 16:17 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 16:17 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 16:17 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 16:17 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 16:17 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 16:17 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 16:1706/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 16:17 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 16:17 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 16:17 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 16:17 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 16:17 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 16:17 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 16:17 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 16:17 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 16:17 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 16:17 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 16:17 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 16:17 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)76 %06/23/16 16:17 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)79 %06/23/16 16:17 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)86 %06/23/16 16:17 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)27 %06/23/16 16:17 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)42 %06/23/16 16:17 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)88 %06/23/16 16:17 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 18:55 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 18:55 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 18:55 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 18:55 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 18:55 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92301747008 Collected:06/15/16 10:55 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 18:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 18:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 18:55 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 18:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 18:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 18:55 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 18:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 18:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 18:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 18:55 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 18:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 18:55 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 18:55 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 18:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 18:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 18:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 18:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 18:55 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 18:55 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 18:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 18:55 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 18:55 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 18:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 18:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 18:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 18:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 18:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 18:55 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 18:55 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 18:55 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 18:55 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 18:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 18:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 18:55 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 18:55 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 18:55 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 18:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 18:55 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 18:55 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 18:55 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 18:55 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 18:55 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 18:55 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 18:55 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 18:55 107-12-01503.6 1
Styrene ND ug/L 06/17/16 18:55 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92301747008 Collected:06/15/16 10:55 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 18:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 18:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 18:55 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 18:55 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 18:55 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 18:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 18:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 18:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 18:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 18:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 18:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 18:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 18:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 18:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 18:55 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 18:55 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:19 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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[phone]
Page 55 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92301747009 Collected:06/15/16 09:00 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 00:32 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 00:32 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 00:32 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 00:32 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 00:32 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 00:32 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 00:32 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 00:32 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 00:32 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 00:32 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 00:32 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 00:32 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 00:32 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 00:32 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 00:32 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 00:32 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 00:32 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 00:32 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 00:32 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)77 %06/21/16 00:32 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)71 %06/21/16 00:32 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 07:02 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 07:02 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 07:02 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 07:02 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 07:02 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 07:02 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 07:02 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)64 %06/18/16 07:02 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 16:12 94-75-706/20/16 17:300.96 0.23 1
Dinoseb ND ug/L 06/22/16 16:12 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 16:12 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 16:12 93-76-506/20/16 17:300.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 16:12 93-72-106/20/16 17:300.19 0.050 1
Surrogates
2,4-DCAA (S)81 %06/22/16 16:12 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:09 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:11 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92301747009 Collected:06/15/16 09:00 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 125 ug/L 06/20/16 22:11 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:11 7440-41-706/17/16 21:051.0 0.50 1
Cadmium 2.4 ug/L 06/20/16 22:11 7440-43-906/17/16 21:051.0 0.50 1
Chromium 8.7J ug/L 06/20/16 22:11 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt 144 ug/L 06/20/16 22:11 7440-48-406/17/16 21:0510.0 2.5 1
Copper 12.2 ug/L 06/20/16 22:11 7440-50-806/17/16 21:0510.0 2.5 1
Lead 4.0J ug/L 06/20/16 22:11 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 10.7J ug/L 06/20/16 22:11 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:11 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:11 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:11 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:11 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 22:11 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 18.0 ug/L 06/20/16 22:11 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:46 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 16:46 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 16:46 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 16:46 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 16:46 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 16:46 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 16:46 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 16:46 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 16:46 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 16:46 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 16:46 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 16:46 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 16:46 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 16:46 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 16:46 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 16:46 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 16:46 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 16:46 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 16:46 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 16:46 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 16:46 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 16:46 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 16:46 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 16:46 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 16:46 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 16:46 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 16:46 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 16:46 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92301747009 Collected:06/15/16 09:00 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 16:46 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 16:46 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 16:46 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 16:46 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 16:46 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 16:46 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 16:46 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 16:46 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 16:46 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 16:46 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 16:46 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 16:46 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 16:46 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 16:46 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 16:46 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 16:46 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 16:46 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 16:46 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 16:46 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 16:46 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 16:46 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 16:46 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 16:46 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 16:46 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 16:46 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 16:46 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 16:46 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 16:46 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 16:46 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 16:46 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 16:46 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 16:46 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 16:46 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 16:46 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 16:46 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 16:46 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 16:46 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 16:46 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 16:4606/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 16:46 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 16:46 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 16:46 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 16:46 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 16:46 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 16:46 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 16:46 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92301747009 Collected:06/15/16 09:00 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 16:46 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 16:46 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 16:46 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 16:46 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 16:46 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 16:46 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 16:46 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 16:46 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 16:46 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 16:46 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 16:46 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 16:46 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 16:46 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 16:46 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 16:46 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 16:46 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 16:46 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 16:46 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 16:46 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 16:4606/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 16:46 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 16:46 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 16:46 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 16:46 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 16:46 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 16:46 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 16:46 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 16:46 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 16:46 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 16:46 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 16:46 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 16:46 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)76 %06/23/16 16:46 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)77 %06/23/16 16:46 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)96 %06/23/16 16:46 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)29 %06/23/16 16:46 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)44 %06/23/16 16:46 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)90 %06/23/16 16:46 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 19:12 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 19:12 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 19:12 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 19:12 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 19:12 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92301747009 Collected:06/15/16 09:00 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene 0.39J ug/L 06/17/16 19:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 19:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 19:12 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 19:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 19:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 19:12 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 19:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 19:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 19:12 108-90-73.0 0.23 1
Chloroethane 0.87J ug/L 06/17/16 19:12 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 19:12 67-66-35.0 0.14 1
Chloromethane 0.20J ug/L 06/17/16 19:12 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 19:12 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 19:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 19:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 19:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 19:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 19:12 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 19:12 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 19:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 19:12 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 19:12 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 19:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 19:12 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 19:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 3.6J ug/L 06/17/16 19:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene 0.79J ug/L 06/17/16 19:12 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 19:12 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 19:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 19:12 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 19:12 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 19:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 19:12 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 19:12 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 19:12 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 19:12 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 19:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 19:12 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 19:12 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 19:12 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 19:12 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 19:12 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 19:12 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 19:12 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 19:12 107-12-01503.6 1
Styrene ND ug/L 06/17/16 19:12 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Page 60 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92301747009 Collected:06/15/16 09:00 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 19:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 19:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 19:12 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 19:12 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 19:12 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 19:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 19:12 79-00-51.0 0.29 1
Trichloroethene 0.67J ug/L 06/17/16 19:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 19:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 19:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 19:12 108-05-450.0 0.35 1
Vinyl chloride 0.72J ug/L 06/17/16 19:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 19:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %06/17/16 19:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 19:12 17060-07-070-130 1
Toluene-d8 (S)101 %06/17/16 19:12 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.1J ug/L 06/17/16 15:21 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92301747010 Collected:06/15/16 09:05 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 00:50 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 00:50 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 00:50 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 00:50 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 00:50 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 00:50 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 00:50 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 00:50 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 00:50 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 00:50 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 00:50 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 00:50 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 00:50 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 00:50 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 00:50 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 00:50 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 00:50 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 00:50 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 00:50 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)84 %06/21/16 00:50 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)89 %06/21/16 00:50 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 07:23 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 07:23 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 07:23 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 07:23 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 07:23 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 07:23 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 07:23 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)78 %06/18/16 07:23 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 16:42 94-75-706/20/16 17:300.95 0.23 1
Dinoseb ND ug/L 06/22/16 16:42 88-85-7 CH06/20/16 17:300.19 0.057 1
Pentachlorophenol ND ug/L 06/22/16 16:42 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 16:42 93-76-506/20/16 17:300.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 16:42 93-72-106/20/16 17:300.19 0.049 1
Surrogates
2,4-DCAA (S)86 %06/22/16 16:42 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:12 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:23 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92301747010 Collected:06/15/16 09:05 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 50.4J ug/L 06/20/16 22:23 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:23 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:23 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 22:23 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:23 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 22:23 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:23 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 3.6J ug/L 06/20/16 22:23 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:23 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:23 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:23 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:23 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 22:23 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 7.6J ug/L 06/20/16 22:23 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:48 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 17:17 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 17:17 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 17:17 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 17:17 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 17:17 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 17:17 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 17:17 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 17:17 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 17:17 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 17:17 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 17:17 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 17:17 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 17:17 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 17:17 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 17:17 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 17:17 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 17:17 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 17:17 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 17:17 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 17:17 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 17:17 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 17:17 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 17:17 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 17:17 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 17:17 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 17:17 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 17:17 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92301747010 Collected:06/15/16 09:05 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 17:17 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 17:17 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 17:17 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 17:17 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 17:17 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 17:17 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 17:17 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 17:17 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 17:17 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 17:17 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 17:17 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 17:17 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 17:17 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 17:17 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 17:17 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 17:17 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 17:17 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 17:17 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 17:17 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 17:17 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 17:17 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 17:17 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 17:17 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 17:17 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 17:17 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 17:17 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 17:17 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 17:17 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 17:17 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 17:17 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 17:17 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 17:17 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 17:17 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 17:17 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 17:17 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 17:17 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 17:17 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 17:17 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 17:1706/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 17:17 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 17:17 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 17:17 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 17:17 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 17:17 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 17:17 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 17:17 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92301747010 Collected:06/15/16 09:05 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 17:17 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 17:17 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 17:17 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 17:17 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 17:17 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 17:17 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 17:17 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 17:17 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 17:17 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 17:17 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 17:17 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 17:17 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 17:17 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 17:17 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 17:17 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 17:17 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 17:17 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 17:17 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 17:17 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 17:1706/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 17:17 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 17:17 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 17:17 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 17:17 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 17:17 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 17:17 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 17:17 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 17:17 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 17:17 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 17:17 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 17:17 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 17:17 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)68 %06/23/16 17:17 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)73 %06/23/16 17:17 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)90 %06/23/16 17:17 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)25 %06/23/16 17:17 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)38 %06/23/16 17:17 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)87 %06/23/16 17:17 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 19:29 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 19:29 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 19:29 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 19:29 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 19:29 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 65 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92301747010 Collected:06/15/16 09:05 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 19:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 19:29 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 19:29 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 19:29 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 19:29 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 19:29 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 19:29 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 19:29 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 19:29 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 19:29 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 19:29 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 19:29 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 19:29 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 19:29 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 19:29 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 19:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 19:29 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 19:29 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 19:29 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 19:29 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 19:29 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 19:29 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 19:29 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 19:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 19:29 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.0J ug/L 06/17/16 19:29 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 19:29 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 19:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 19:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 19:29 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 19:29 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 19:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 19:29 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 19:29 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 19:29 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 19:29 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 19:29 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 19:29 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 19:29 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 19:29 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 19:29 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 19:29 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 19:29 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 19:29 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 19:29 107-12-01503.6 1
Styrene ND ug/L 06/17/16 19:29 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92301747010 Collected:06/15/16 09:05 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 19:29 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 19:29 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 19:29 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 19:29 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 19:29 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 19:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 19:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 19:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 19:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 19:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 19:29 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 19:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 19:29 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 19:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 19:29 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 19:29 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-8 M310001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:22 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92301747011 Collected:06/15/16 10:06 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 01:07 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 01:07 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 01:07 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 01:07 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 01:07 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 01:07 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 01:07 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 01:07 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 01:07 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 01:07 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 01:07 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 01:07 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 01:07 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 01:07 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 01:07 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 01:07 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 01:07 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 01:07 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 01:07 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)88 %06/21/16 01:07 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)72 %06/21/16 01:07 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 07:44 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 07:44 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 07:44 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 07:44 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 07:44 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 07:44 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 07:44 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)65 %06/18/16 07:44 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/22/16 17:12 94-75-706/20/16 17:300.96 0.23 1
Dinoseb ND ug/L 06/22/16 17:12 88-85-7 CH06/20/16 17:300.19 0.058 1
Pentachlorophenol ND ug/L 06/22/16 17:12 87-86-506/20/16 17:300.029 0.017 1
2,4,5-T ND ug/L 06/22/16 17:12 93-76-506/20/16 17:300.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/22/16 17:12 93-72-106/20/16 17:300.20 0.050 1
Surrogates
2,4-DCAA (S)74 %06/22/16 17:12 19719-28-906/20/16 17:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:15 7440-36-006/17/16 21:056.0 3.8 1
Arsenic 3.4J ug/L 06/20/16 22:26 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92301747011 Collected:06/15/16 10:06 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 77.6J ug/L 06/20/16 22:26 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:26 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:26 7440-43-906/17/16 21:051.0 0.50 1
Chromium 8.4J ug/L 06/20/16 22:26 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:26 7440-48-406/17/16 21:0510.0 2.5 1
Copper 4.3J ug/L 06/20/16 22:26 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:26 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 4.4J ug/L 06/20/16 22:26 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:26 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:26 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:26 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:26 7440-31-506/17/16 21:051002.5 1
Vanadium 10.8J ug/L 06/20/16 22:26 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 20.5 ug/L 06/20/16 22:26 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:50 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 17:47 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 17:47 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 17:47 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 17:47 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 17:47 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 17:47 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 17:47 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 17:47 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 17:47 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 17:47 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 17:47 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 17:47 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 17:47 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 17:47 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 17:47 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 17:47 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 17:47 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 17:47 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 17:47 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 17:47 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 17:47 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 17:47 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 17:47 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 17:47 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 17:47 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 17:47 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 17:47 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92301747011 Collected:06/15/16 10:06 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 17:47 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 17:47 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 17:47 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 17:47 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 17:47 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 17:47 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 17:47 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 17:47 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 17:47 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 17:47 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 17:47 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 17:47 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 17:47 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 17:47 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 17:47 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 17:47 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 17:47 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 17:47 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 17:47 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 17:47 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 17:47 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 17:47 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 17:47 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 17:47 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 17:47 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 17:47 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 17:47 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 17:47 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 17:47 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 17:47 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 17:47 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 17:47 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 17:47 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 17:47 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 17:47 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 17:47 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 17:47 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 17:47 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 17:4706/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 17:47 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 17:47 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 17:47 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 17:47 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 17:47 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 17:47 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 17:47 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 70 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92301747011 Collected:06/15/16 10:06 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 17:47 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 17:47 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 17:47 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 17:47 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 17:47 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 17:47 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 17:47 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 17:47 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 17:47 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 17:47 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 17:47 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 17:47 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 17:47 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 17:47 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 17:47 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 17:47 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 17:47 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 17:47 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 17:47 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 17:4706/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 17:47 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 17:47 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 17:47 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 17:47 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 17:47 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 17:47 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 17:47 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 17:47 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 17:47 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 17:47 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 17:47 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 17:47 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)71 %06/23/16 17:47 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)74 %06/23/16 17:47 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)98 %06/23/16 17:47 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)26 %06/23/16 17:47 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)39 %06/23/16 17:47 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)86 %06/23/16 17:47 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 19:47 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 19:47 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 19:47 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 19:47 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 19:47 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 71 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92301747011 Collected:06/15/16 10:06 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene 0.47J ug/L 06/17/16 19:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 19:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 19:47 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 19:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 19:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 19:47 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 19:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 19:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 19:47 108-90-73.0 0.23 1
Chloroethane 0.62J ug/L 06/17/16 19:47 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 19:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 19:47 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 19:47 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 19:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 19:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 19:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 19:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 19:47 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 19:47 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 19:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 19:47 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 19:47 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 19:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 19:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 19:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.62J ug/L 06/17/16 19:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene 0.57J ug/L 06/17/16 19:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 19:47 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 19:47 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 19:47 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 19:47 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 19:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 19:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 19:47 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 19:47 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 19:47 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 19:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 19:47 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 19:47 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 19:47 126-98-71000.93 1
Methylene Chloride 1.0 ug/L 06/17/16 19:47 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 19:47 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 19:47 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 19:47 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 19:47 107-12-01503.6 1
Styrene ND ug/L 06/17/16 19:47 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92301747011 Collected:06/15/16 10:06 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 19:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 19:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 19:47 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 19:47 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 19:47 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 19:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 19:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 19:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 19:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 19:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 19:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 19:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 19:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 19:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 19:47 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 19:47 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:23 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 73 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92301747012 Collected:06/15/16 09:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 01:25 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 01:25 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 01:25 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 01:25 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 01:25 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 01:25 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 01:25 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 01:25 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 01:25 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 01:25 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 01:25 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 01:25 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 01:25 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 01:25 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 01:25 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 01:25 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 01:25 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 01:25 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 01:25 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)88 %06/21/16 01:25 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)71 %06/21/16 01:25 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 08:05 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 08:05 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 08:05 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 08:05 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 08:05 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 08:05 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 08:05 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)64 %06/18/16 08:05 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/24/16 06:37 94-75-706/22/16 17:200.97 0.23 1
Dinoseb ND ug/L 06/24/16 06:37 88-85-706/22/16 17:200.20 0.059 1
Pentachlorophenol ND ug/L 06/24/16 06:37 87-86-506/22/16 17:200.029 0.018 1
2,4,5-T ND ug/L 06/24/16 06:37 93-76-506/22/16 17:200.20 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/24/16 06:37 93-72-106/22/16 17:200.20 0.051 1
Surrogates
2,4-DCAA (S)87 %06/24/16 06:37 19719-28-906/22/16 17:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:18 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:29 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92301747012 Collected:06/15/16 09:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 12.4J ug/L 06/20/16 22:29 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:29 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:29 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 22:29 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:29 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 22:29 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:29 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 22:29 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:29 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:29 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:29 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:29 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 22:29 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 22:29 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:53 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 18:17 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 18:17 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 18:17 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 18:17 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 18:17 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 18:17 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 18:17 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 18:17 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 18:17 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 18:17 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 18:17 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 18:17 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 18:17 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 18:17 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 18:17 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 18:17 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 18:17 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 18:17 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 18:17 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 18:17 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 18:17 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 18:17 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 18:17 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 18:17 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 18:17 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 18:17 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 18:17 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92301747012 Collected:06/15/16 09:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 18:17 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 18:17 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 18:17 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 18:17 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 18:17 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 18:17 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 18:17 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 18:17 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 18:17 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 18:17 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 18:17 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 18:17 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 18:17 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 18:17 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 18:17 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 18:17 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 18:17 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 18:17 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 18:17 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 18:17 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 18:17 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 18:17 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 18:17 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 18:17 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 18:17 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 18:17 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 18:17 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 18:17 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 18:17 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 18:17 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 18:17 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 18:17 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 18:17 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 18:17 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 18:17 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 18:17 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 18:17 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 18:17 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 18:1706/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 18:17 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 18:17 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 18:17 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 18:17 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 18:17 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 18:17 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 18:17 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92301747012 Collected:06/15/16 09:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 18:17 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 18:17 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 18:17 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 18:17 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 18:17 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 18:17 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 18:17 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 18:17 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 18:17 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 18:17 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 18:17 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 18:17 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 18:17 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 18:17 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 18:17 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 18:17 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 18:17 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 18:17 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 18:17 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 18:1706/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 18:17 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 18:17 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 18:17 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 18:17 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 18:17 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 18:17 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 18:17 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 18:17 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 18:17 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 18:17 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 18:17 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 18:17 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)54 %06/23/16 18:17 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)61 %06/23/16 18:17 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)87 %06/23/16 18:17 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)24 %06/23/16 18:17 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)32 %06/23/16 18:17 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)75 %06/23/16 18:17 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 20:04 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 20:04 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 20:04 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 20:04 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 20:04 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92301747012 Collected:06/15/16 09:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 20:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 20:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 20:04 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 20:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 20:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 20:04 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 20:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 20:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 20:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 20:04 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 20:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 20:04 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 20:04 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 20:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 20:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 20:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 20:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 20:04 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 20:04 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 20:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 20:04 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 20:04 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 20:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 20:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 20:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 20:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 20:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 20:04 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 20:04 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 20:04 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 20:04 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 20:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 20:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 20:04 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 20:04 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 20:04 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 20:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 20:04 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 20:04 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 20:04 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 20:04 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 20:04 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 20:04 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 20:04 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 20:04 107-12-01503.6 1
Styrene ND ug/L 06/17/16 20:04 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92301747012 Collected:06/15/16 09:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 20:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 20:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 20:04 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 20:04 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 20:04 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 20:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 20:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 20:04 79-01-61.0 0.47 1
Trichlorofluoromethane 0.29J ug/L 06/17/16 20:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 20:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 20:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 20:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 20:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 20:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 20:04 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 20:04 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:24 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 79 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92301747013 Collected:06/15/16 09:19 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 01:42 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 01:42 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 01:42 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 01:42 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 01:42 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 01:42 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 01:42 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 01:42 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 01:42 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 01:42 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 01:42 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 01:42 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 01:42 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 01:42 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 01:42 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 01:42 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 01:42 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 01:42 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 01:42 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)72 %06/21/16 01:42 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)77 %06/21/16 01:42 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 08:25 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 08:25 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 08:25 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 08:25 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 08:25 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 08:25 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 08:25 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)72 %06/18/16 08:25 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/24/16 07:07 94-75-706/22/16 17:200.94 0.22 1
Dinoseb ND ug/L 06/24/16 07:07 88-85-706/22/16 17:200.19 0.057 1
Pentachlorophenol ND ug/L 06/24/16 07:07 87-86-506/22/16 17:200.028 0.017 1
2,4,5-T ND ug/L 06/24/16 07:07 93-76-506/22/16 17:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 06/24/16 07:07 93-72-106/22/16 17:200.19 0.049 1
Surrogates
2,4-DCAA (S)76 %06/24/16 07:07 19719-28-906/22/16 17:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 4.6J ug/L 06/20/16 05:22 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:33 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92301747013 Collected:06/15/16 09:19 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium ND ug/L 06/20/16 22:33 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:33 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:33 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 22:33 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:33 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 22:33 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:33 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 22:33 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:33 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:33 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:33 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:33 7440-31-506/17/16 21:051002.5 1
Vanadium 8.3J ug/L 06/20/16 22:33 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 22:33 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:55 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/28/16 12:18 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/28/16 12:18 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/28/16 12:18 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/28/16 12:18 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/28/16 12:18 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/28/16 12:18 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/28/16 12:18 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/28/16 12:18 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/28/16 12:18 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/28/16 12:18 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/28/16 12:18 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/28/16 12:18 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/28/16 12:18 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/28/16 12:18 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/28/16 12:18 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/28/16 12:18 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/28/16 12:18 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/16 12:18 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/28/16 12:18 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/28/16 12:18 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/28/16 12:18 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/28/16 12:18 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/28/16 12:18 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/28/16 12:18 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/28/16 12:18 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/28/16 12:18 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/28/16 12:18 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92301747013 Collected:06/15/16 09:19 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/28/16 12:18 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/28/16 12:18 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/28/16 12:18 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/28/16 12:18 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/28/16 12:18 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/28/16 12:18 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/28/16 12:18 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/28/16 12:18 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/28/16 12:18 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/28/16 12:18 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/16 12:18 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/28/16 12:18 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/28/16 12:18 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/28/16 12:18 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/28/16 12:18 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/16 12:18 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/28/16 12:18 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/28/16 12:18 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/16 12:18 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/28/16 12:18 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/28/16 12:18 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/28/16 12:18 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/28/16 12:18 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/28/16 12:18 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/28/16 12:18 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/28/16 12:18 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/28/16 12:18 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/16 12:18 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/28/16 12:18 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/28/16 12:18 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/28/16 12:18 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/28/16 12:18 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/28/16 12:18 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/28/16 12:18 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/28/16 12:18 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/28/16 12:18 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/28/16 12:18 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/16 12:18 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/16 12:1806/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/28/16 12:18 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/28/16 12:18 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/28/16 12:18 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/28/16 12:18 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/28/16 12:18 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/28/16 12:18 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/28/16 12:18 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92301747013 Collected:06/15/16 09:19 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/28/16 12:18 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/28/16 12:18 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/28/16 12:18 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/28/16 12:18 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/28/16 12:18 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/28/16 12:18 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/16 12:18 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/28/16 12:18 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/28/16 12:18 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/28/16 12:18 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/28/16 12:18 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/28/16 12:18 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/16 12:18 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/28/16 12:18 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/28/16 12:18 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/28/16 12:18 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/28/16 12:18 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/28/16 12:18 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/28/16 12:18 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/28/16 12:1806/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/28/16 12:18 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/28/16 12:18 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/28/16 12:18 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/28/16 12:18 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/28/16 12:18 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/28/16 12:18 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/28/16 12:18 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/28/16 12:18 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/28/16 12:18 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/16 12:18 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/28/16 12:18 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/28/16 12:18 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)76 %06/28/16 12:18 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)80 %06/28/16 12:18 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)69 %06/28/16 12:18 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)31 %06/28/16 12:18 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)39 %06/28/16 12:18 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)81 %06/28/16 12:18 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 20:21 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 20:21 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 20:21 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 20:21 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 20:21 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92301747013 Collected:06/15/16 09:19 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 20:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 20:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 20:21 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 20:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 20:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 20:21 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 20:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 20:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 20:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 20:21 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 20:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 20:21 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 20:21 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 20:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 20:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 20:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 20:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 20:21 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 20:21 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 20:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 20:21 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 20:21 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 20:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 20:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 20:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 20:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 20:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 20:21 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 20:21 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 20:21 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 20:21 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 20:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 20:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 20:21 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 20:21 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 20:21 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 20:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 20:21 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 20:21 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 20:21 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 20:21 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 20:21 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 20:21 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 20:21 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 20:21 107-12-01503.6 1
Styrene ND ug/L 06/17/16 20:21 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 84 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92301747013 Collected:06/15/16 09:19 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 20:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 20:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 20:21 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 20:21 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 20:21 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 20:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 20:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 20:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 20:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 20:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 20:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 20:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 20:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 20:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 20:21 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 20:21 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:25 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92301747014 Collected:06/15/16 12:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 02:00 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 02:00 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 02:00 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 02:00 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 02:00 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 02:00 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 02:00 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 02:00 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 02:00 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 02:00 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 02:00 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 02:00 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 02:00 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 02:00 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 02:00 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 02:00 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 02:00 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 02:00 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 02:00 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %06/21/16 02:00 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)65 %06/21/16 02:00 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 08:46 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 08:46 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 08:46 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 08:46 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 08:46 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 08:46 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 08:46 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)57 %06/18/16 08:46 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/24/16 07:37 94-75-706/22/16 17:200.96 0.23 1
Dinoseb ND ug/L 06/24/16 07:37 88-85-706/22/16 17:200.19 0.058 1
Pentachlorophenol ND ug/L 06/24/16 07:37 87-86-506/22/16 17:200.029 0.017 1
2,4,5-T ND ug/L 06/24/16 07:37 93-76-506/22/16 17:200.19 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/24/16 07:37 93-72-106/22/16 17:200.19 0.050 1
Surrogates
2,4-DCAA (S)83 %06/24/16 07:37 19719-28-906/22/16 17:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:34 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:36 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92301747014 Collected:06/15/16 12:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 77.7J ug/L 06/20/16 22:36 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:36 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:36 7440-43-906/17/16 21:051.0 0.50 1
Chromium 10.4 ug/L 06/20/16 22:36 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt 2.7J ug/L 06/20/16 22:36 7440-48-406/17/16 21:0510.0 2.5 1
Copper 11.3 ug/L 06/20/16 22:36 7440-50-806/17/16 21:0510.0 2.5 1
Lead 4.3J ug/L 06/20/16 22:36 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 8.9J ug/L 06/20/16 22:36 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:36 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:36 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:36 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:36 7440-31-506/17/16 21:051002.5 1
Vanadium 13.6J ug/L 06/20/16 22:36 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 28.4 ug/L 06/20/16 22:36 7440-66-6 B06/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 13:58 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 19:18 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 19:18 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 19:18 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 19:18 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 19:18 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 19:18 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 19:18 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 19:18 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 19:18 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 19:18 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 19:18 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 19:18 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 19:18 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 19:18 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 19:18 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 19:18 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 19:18 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 19:18 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 19:18 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 19:18 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 19:18 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 19:18 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 19:18 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 19:18 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 19:18 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 19:18 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 19:18 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92301747014 Collected:06/15/16 12:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 19:18 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 19:18 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 19:18 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 19:18 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 19:18 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 19:18 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 19:18 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 19:18 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 19:18 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 19:18 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 19:18 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 19:18 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 19:18 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 19:18 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 19:18 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 19:18 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 19:18 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 19:18 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 19:18 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 19:18 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 19:18 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 19:18 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 19:18 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 19:18 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 19:18 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 19:18 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 19:18 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 19:18 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 19:18 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 19:18 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 19:18 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 19:18 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 19:18 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 19:18 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 19:18 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 19:18 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 19:18 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 19:18 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 19:1806/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 19:18 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 19:18 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 19:18 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 19:18 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 19:18 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 19:18 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 19:18 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92301747014 Collected:06/15/16 12:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 19:18 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 19:18 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 19:18 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 19:18 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 19:18 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 19:18 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 19:18 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 19:18 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 19:18 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 19:18 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 19:18 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 19:18 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 19:18 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 19:18 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 19:18 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 19:18 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 19:18 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 19:18 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 19:18 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 19:1806/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 19:18 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 19:18 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 19:18 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 19:18 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 19:18 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 19:18 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 19:18 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 19:18 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 19:18 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 19:18 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 19:18 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 19:18 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)72 %06/23/16 19:18 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)78 %06/23/16 19:18 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)70 %06/23/16 19:18 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)25 %06/23/16 19:18 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)40 %06/23/16 19:18 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)85 %06/23/16 19:18 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 20:38 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 20:38 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 20:38 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 20:38 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 20:38 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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[phone]
Page 89 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92301747014 Collected:06/15/16 12:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 20:38 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 20:38 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 20:38 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 20:38 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 20:38 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 20:38 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 20:38 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 20:38 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 20:38 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 20:38 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 20:38 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 20:38 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 20:38 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 20:38 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 20:38 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 20:38 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 20:38 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 20:38 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 20:38 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 20:38 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 20:38 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 20:38 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 20:38 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 20:38 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 20:38 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 20:38 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 20:38 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 20:38 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 20:38 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 20:38 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 20:38 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 20:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 20:38 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 20:38 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 20:38 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 20:38 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 20:38 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 20:38 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 20:38 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 20:38 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 20:38 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 20:38 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 20:38 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 20:38 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 20:38 107-12-01503.6 1
Styrene ND ug/L 06/17/16 20:38 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92301747014 Collected:06/15/16 12:15 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 20:38 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 20:38 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 20:38 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 20:38 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 20:38 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 20:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 20:38 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 20:38 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 20:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 20:38 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 20:38 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 20:38 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 20:38 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 20:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 20:38 17060-07-070-130 1
Toluene-d8 (S)101 %06/17/16 20:38 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:26 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92301747015 Collected:06/15/16 12:10 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/21/16 02:17 309-00-206/17/16 13:180.050 0.050 1
alpha-BHC ND ug/L 06/21/16 02:17 319-84-606/17/16 13:180.050 0.050 1
beta-BHC ND ug/L 06/21/16 02:17 319-85-706/17/16 13:180.050 0.050 1
delta-BHC ND ug/L 06/21/16 02:17 319-86-806/17/16 13:180.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/21/16 02:17 58-89-906/17/16 13:180.050 0.050 1
Chlordane (Technical)ND ug/L 06/21/16 02:17 57-74-906/17/16 13:180.50 0.20 1
4,4'-DDD ND ug/L 06/21/16 02:17 72-54-806/17/16 13:180.10 0.050 1
4,4'-DDE ND ug/L 06/21/16 02:17 72-55-906/17/16 13:180.10 0.050 1
4,4'-DDT ND ug/L 06/21/16 02:17 50-29-306/17/16 13:180.10 0.050 1
Dieldrin ND ug/L 06/21/16 02:17 60-57-106/17/16 13:180.075 0.050 1
Endosulfan I ND ug/L 06/21/16 02:17 959-98-806/17/16 13:180.10 0.050 1
Endosulfan II ND ug/L 06/21/16 02:17 33213-65-906/17/16 13:180.10 0.050 1
Endosulfan sulfate ND ug/L 06/21/16 02:17 1031-07-806/17/16 13:180.10 0.050 1
Endrin ND ug/L 06/21/16 02:17 72-20-806/17/16 13:180.10 0.050 1
Endrin aldehyde ND ug/L 06/21/16 02:17 7421-93-406/17/16 13:180.10 0.050 1
Heptachlor ND ug/L 06/21/16 02:17 76-44-806/17/16 13:180.050 0.050 1
Heptachlor epoxide ND ug/L 06/21/16 02:17 1024-57-306/17/16 13:180.075 0.050 1
Methoxychlor ND ug/L 06/21/16 02:17 72-43-506/17/16 13:181.0 0.15 1
Toxaphene ND ug/L 06/21/16 02:17 8001-35-206/17/16 13:181.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)97 %06/21/16 02:17 877-09-806/17/16 13:1820-130 1
Decachlorobiphenyl (S)89 %06/21/16 02:17 2051-24-306/17/16 13:1820-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/18/16 09:07 12674-11-206/17/16 13:180.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/18/16 09:07 11104-28-206/17/16 13:180.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/18/16 09:07 11141-16-506/17/16 13:180.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/18/16 09:07 53469-21-906/17/16 13:180.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/18/16 09:07 12672-29-606/17/16 13:180.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/18/16 09:07 11097-69-106/17/16 13:180.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/18/16 09:07 11096-82-506/17/16 13:180.50 0.50 1
Surrogates
Decachlorobiphenyl (S)75 %06/18/16 09:07 2051-24-306/17/16 13:1810-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/24/16 08:07 94-75-706/22/16 17:200.95 0.23 1
Dinoseb ND ug/L 06/24/16 08:07 88-85-706/22/16 17:200.19 0.057 1
Pentachlorophenol ND ug/L 06/24/16 08:07 87-86-506/22/16 17:200.029 0.017 1
2,4,5-T ND ug/L 06/24/16 08:07 93-76-506/22/16 17:200.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 06/24/16 08:07 93-72-106/22/16 17:200.19 0.049 1
Surrogates
2,4-DCAA (S)84 %06/24/16 08:07 19719-28-906/22/16 17:2039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/20/16 05:37 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:39 7440-38-206/17/16 21:0510.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92301747015 Collected:06/15/16 12:10 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Barium 21.7J ug/L 06/20/16 22:39 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:39 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:39 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 22:39 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 22:39 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 22:39 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 22:39 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 22:39 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:39 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:39 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 22:39 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:39 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 22:39 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 22:39 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/27/16 14:00 7439-97-606/20/16 18:080.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/23/16 19:48 83-32-906/20/16 11:4810.0 0.25 1
Acenaphthylene ND ug/L 06/23/16 19:48 208-96-806/20/16 11:4810.0 0.21 1
Acetophenone ND ug/L 06/23/16 19:48 98-86-206/20/16 11:4810.0 2.0 1
2-Acetylaminofluorene ND ug/L 06/23/16 19:48 53-96-306/20/16 11:4820.0 0.84 1
4-Aminobiphenyl ND ug/L 06/23/16 19:48 92-67-106/20/16 11:4820.0 0.92 1
Anthracene ND ug/L 06/23/16 19:48 120-12-706/20/16 11:4810.0 0.14 1
Benzo(a)anthracene ND ug/L 06/23/16 19:48 56-55-306/20/16 11:4810.0 0.33 1
Benzo(a)pyrene ND ug/L 06/23/16 19:48 50-32-806/20/16 11:4810.0 0.30 1
Benzo(b)fluoranthene ND ug/L 06/23/16 19:48 205-99-206/20/16 11:4810.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 06/23/16 19:48 191-24-206/20/16 11:4810.0 0.38 1
Benzo(k)fluoranthene ND ug/L 06/23/16 19:48 207-08-906/20/16 11:4810.0 0.43 1
Benzyl alcohol ND ug/L 06/23/16 19:48 100-51-606/20/16 11:4820.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 06/23/16 19:48 101-55-306/20/16 11:4810.0 1.3 1
Butylbenzylphthalate ND ug/L 06/23/16 19:48 85-68-706/20/16 11:4810.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 06/23/16 19:48 59-50-706/20/16 11:4820.0 4.2 1
4-Chloroaniline ND ug/L 06/23/16 19:48 106-47-806/20/16 11:4820.0 3.4 1
Chlorobenzilate ND ug/L 06/23/16 19:48 510-15-606/20/16 11:4810.0 0.72 1
bis(2-Chloroethoxy)methane ND ug/L 06/23/16 19:48 111-91-106/20/16 11:4810.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 06/23/16 19:48 111-44-406/20/16 11:4810.0 1.5 1
2-Chloronaphthalene ND ug/L 06/23/16 19:48 91-58-706/20/16 11:4810.0 2.2 1
2-Chlorophenol ND ug/L 06/23/16 19:48 95-57-806/20/16 11:4810.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/23/16 19:48 7005-72-306/20/16 11:4810.0 2.1 1
Chrysene ND ug/L 06/23/16 19:48 218-01-906/20/16 11:4810.0 0.21 1
Diallate ND ug/L 06/23/16 19:48 2303-16-406/20/16 11:4810.0 1.3 1
Dibenz(a,h)anthracene ND ug/L 06/23/16 19:48 53-70-306/20/16 11:4810.0 0.55 1
Dibenzofuran ND ug/L 06/23/16 19:48 132-64-906/20/16 11:4810.0 1.8 1
3,3'-Dichlorobenzidine ND ug/L 06/23/16 19:48 91-94-106/20/16 11:4820.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92301747015 Collected:06/15/16 12:10 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dichlorophenol ND ug/L 06/23/16 19:48 120-83-206/20/16 11:4810.0 1.7 1
2,6-Dichlorophenol ND ug/L 06/23/16 19:48 87-65-006/20/16 11:4810.0 1.8 1
Diethylphthalate ND ug/L 06/23/16 19:48 84-66-206/20/16 11:4860001.3 1
Dimethoate ND ug/L 06/23/16 19:48 60-51-506/20/16 11:4820.0 0.92 1
P-Dimethylaminoazobenzene ND ug/L 06/23/16 19:48 60-11-706/20/16 11:4810.0 0.35 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/23/16 19:48 57-97-606/20/16 11:4810.0 0.77 1
3,3'-Dimethylbenzidine ND ug/L 06/23/16 19:48 119-93-706/20/16 11:4810.0 2.1 1
2,4-Dimethylphenol ND ug/L 06/23/16 19:48 105-67-906/20/16 11:4810.0 2.2 1
Dimethylphthalate ND ug/L 06/23/16 19:48 131-11-306/20/16 11:4810.0 1.5 1
Di-n-butylphthalate ND ug/L 06/23/16 19:48 84-74-206/20/16 11:4810.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 06/23/16 19:48 534-52-106/20/16 11:4850.0 1.7 1
1,3-Dinitrobenzene ND ug/L 06/23/16 19:48 99-65-006/20/16 11:4820.0 1.5 1
2,4-Dinitrophenol ND ug/L 06/23/16 19:48 51-28-506/20/16 11:4850.0 6.5 1
2,4-Dinitrotoluene ND ug/L 06/23/16 19:48 121-14-206/20/16 11:4810.0 1.2 1
2,6-Dinitrotoluene ND ug/L 06/23/16 19:48 606-20-206/20/16 11:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/23/16 19:48 117-84-006/20/16 11:4810.0 0.86 1
Diphenylamine ND ug/L 06/23/16 19:48 122-39-406/20/16 11:4810.0 1.3 1
Disulfoton ND ug/L 06/23/16 19:48 298-04-406/20/16 11:4810.0 1.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/23/16 19:48 117-81-706/20/16 11:4815.0 0.85 1
Ethyl methanesulfonate ND ug/L 06/23/16 19:48 62-50-006/20/16 11:4820.0 1.8 1
Famphur ND ug/L 06/23/16 19:48 52-85-706/20/16 11:4820.0 1.7 1
Fluoranthene ND ug/L 06/23/16 19:48 206-44-006/20/16 11:4810.0 0.21 1
Fluorene ND ug/L 06/23/16 19:48 86-73-706/20/16 11:4810.0 0.21 1
Hexachlorobenzene ND ug/L 06/23/16 19:48 118-74-106/20/16 11:4810.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 06/23/16 19:48 77-47-406/20/16 11:4810.0 1.8 1
Hexachloroethane ND ug/L 06/23/16 19:48 67-72-106/20/16 11:4810.0 1.5 1
Hexachloropropene ND ug/L 06/23/16 19:48 1888-71-706/20/16 11:4810.0 1.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/23/16 19:48 193-39-506/20/16 11:4810.0 0.29 1
Isodrin ND ug/L 06/23/16 19:48 465-73-606/20/16 11:4820.0 2.0 1
Isophorone ND ug/L 06/23/16 19:48 78-59-106/20/16 11:4810.0 1.8 1
Isosafrole ND ug/L 06/23/16 19:48 120-58-106/20/16 11:4810.0 1.8 1
Kepone ND ug/L 06/23/16 19:48 143-50-006/20/16 11:4820.0 3.1 1
Methapyrilene ND ug/L 06/23/16 19:48 91-80-506/20/16 11:481002.7 1
3-Methylcholanthrene ND ug/L 06/23/16 19:48 56-49-506/20/16 11:4810.0 0.82 1
Methyl methanesulfonate ND ug/L 06/23/16 19:48 66-27-306/20/16 11:4810.0 1.3 1
2-Methylnaphthalene ND ug/L 06/23/16 19:48 91-57-606/20/16 11:4810.0 0.28 1
Methyl parathion ND ug/L 06/23/16 19:48 298-00-006/20/16 11:4810.0 1.1 1
2-Methylphenol(o-Cresol)ND ug/L 06/23/16 19:48 95-48-706/20/16 11:4810.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/23/16 19:4806/20/16 11:4810.0 1.7 1
1-Naphthalenamine ND ug/L 06/23/16 19:48 134-32-706/20/16 11:4810.0 0.96 1
2-Naphthalenamine ND ug/L 06/23/16 19:48 91-59-806/20/16 11:4810.0 0.98 1
1,4-Naphthoquinone ND ug/L 06/23/16 19:48 130-15-406/20/16 11:4810.0 1.8 1
2-Nitroaniline ND ug/L 06/23/16 19:48 88-74-406/20/16 11:4850.0 2.8 1
3-Nitroaniline ND ug/L 06/23/16 19:48 99-09-206/20/16 11:4850.0 2.4 1
4-Nitroaniline ND ug/L 06/23/16 19:48 100-01-606/20/16 11:4820.0 2.5 1
Nitrobenzene ND ug/L 06/23/16 19:48 98-95-306/20/16 11:4810.0 1.7 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92301747015 Collected:06/15/16 12:10 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Nitrophenol ND ug/L 06/23/16 19:48 88-75-506/20/16 11:4810.0 1.7 1
4-Nitrophenol ND ug/L 06/23/16 19:48 100-02-706/20/16 11:4850.0 5.8 1
5-Nitro-o-toluidine ND ug/L 06/23/16 19:48 99-55-806/20/16 11:4810.0 1.2 1
N-Nitrosodiethylamine ND ug/L 06/23/16 19:48 55-18-506/20/16 11:4820.0 1.8 1
N-Nitrosodimethylamine ND ug/L 06/23/16 19:48 62-75-906/20/16 11:4810.0 1.3 1
N-Nitroso-di-n-butylamine ND ug/L 06/23/16 19:48 924-16-306/20/16 11:4810.0 2.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/23/16 19:48 621-64-706/20/16 11:4810.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 06/23/16 19:48 86-30-606/20/16 11:4810.0 1.3 1
N-Nitrosomethylethylamine ND ug/L 06/23/16 19:48 10595-95-606/20/16 11:4810.0 1.8 1
N-Nitrosopiperidine ND ug/L 06/23/16 19:48 100-75-406/20/16 11:4820.0 1.9 1
N-Nitrosopyrrolidine ND ug/L 06/23/16 19:48 930-55-206/20/16 11:4810.0 2.5 1
O,O,O-Triethylphosphorothioate ND ug/L 06/23/16 19:48 126-68-106/20/16 11:4810.0 1.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/23/16 19:48 108-60-106/20/16 11:4810.0 1.6 1
Parathion (Ethyl parathion)ND ug/L 06/23/16 19:48 56-38-206/20/16 11:4810.0 1.1 1
Pentachlorobenzene ND ug/L 06/23/16 19:48 608-93-506/20/16 11:4810.0 2.0 1
Pentachloronitrobenzene ND ug/L 06/23/16 19:48 82-68-806/20/16 11:4820.0 1.0 1
Pentachlorophenol ND ug/L 06/23/16 19:48 87-86-506/20/16 11:4825.0 2.3 1
Phenacetin ND ug/L 06/23/16 19:48 62-44-206/20/16 11:4820.0 0.97 1
Phenanthrene ND ug/L 06/23/16 19:48 85-01-806/20/16 11:4810.0 0.22 1
Phenol ND ug/L 06/23/16 19:4806/20/16 11:4810.0 1.7 1
p-Phenylenediamine ND ug/L 06/23/16 19:48 106-50-306/20/16 11:4810.0 0.96 1
Phorate ND ug/L 06/23/16 19:48 298-02-206/20/16 11:4810.0 1.1 1
Pronamide ND ug/L 06/23/16 19:48 23950-58-506/20/16 11:4810.0 0.97 1
Pyrene ND ug/L 06/23/16 19:48 129-00-006/20/16 11:4810.0 0.19 1
Safrole ND ug/L 06/23/16 19:48 94-59-706/20/16 11:4810.0 1.5 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/23/16 19:48 95-94-306/20/16 11:4810.0 1.7 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/23/16 19:48 58-90-206/20/16 11:4810.0 2.3 1
Thionazin ND ug/L 06/23/16 19:48 297-97-206/20/16 11:4820.0 1.2 1
O-Toluidine ND ug/L 06/23/16 19:48 95-53-406/20/16 11:4810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/23/16 19:48 95-95-406/20/16 11:4810.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 06/23/16 19:48 88-06-206/20/16 11:4810.0 1.9 1
1,3,5-Trinitrobenzene ND ug/L 06/23/16 19:48 99-35-4 L306/20/16 11:4810.0 1.1 1
Surrogates
Nitrobenzene-d5 (S)75 %06/23/16 19:48 4165-60-006/20/16 11:4821-110 1
2-Fluorobiphenyl (S)77 %06/23/16 19:48 321-60-806/20/16 11:4827-110 1
Terphenyl-d14 (S)87 %06/23/16 19:48 1718-51-006/20/16 11:4831-107 1
Phenol-d6 (S)26 %06/23/16 19:48 13127-88-306/20/16 11:4810-110 1
2-Fluorophenol (S)41 %06/23/16 19:48 367-12-406/20/16 11:4812-110 1
2,4,6-Tribromophenol (S)88 %06/23/16 19:48 118-79-606/20/16 11:4827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 20:55 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 20:55 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 20:55 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 20:55 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 20:55 107-05-110.0 1.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 95 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92301747015 Collected:06/15/16 12:10 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Benzene ND ug/L 06/17/16 20:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 20:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 20:55 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 20:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 20:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 20:55 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 20:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 20:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 20:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 20:55 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 20:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 20:55 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 20:55 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 20:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 20:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 20:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 20:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 20:55 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 20:55 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/17/16 20:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 20:55 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 20:55 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/17/16 20:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 20:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 20:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 20:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 20:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 20:55 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 20:55 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 20:55 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 20:55 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 20:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 20:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/17/16 20:55 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 20:55 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 20:55 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 20:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 20:55 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 20:55 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 20:55 126-98-71000.93 1
Methylene Chloride ND ug/L 06/17/16 20:55 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 20:55 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 20:55 108-10-11000.33 1
Naphthalene ND ug/L 06/17/16 20:55 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 20:55 107-12-01503.6 1
Styrene ND ug/L 06/17/16 20:55 100-42-51.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 139
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92301747015 Collected:06/15/16 12:10 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 20:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 20:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 20:55 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 20:55 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 20:55 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 20:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 20:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 20:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 20:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 20:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 20:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 20:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 20:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 20:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 20:55 17060-07-070-130 1
Toluene-d8 (S)101 %06/17/16 20:55 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/20/16 20:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/17/16 15:27 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 97 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/9633
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1759234
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/27/16 13:050.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759235LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1759236MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301747001
1759237
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 102 75-12597 5 252.5ND 2.5 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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Page 98 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/22070
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92301747001, 92301747002, 92301747003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758278
Associated Lab Samples:92301747001, 92301747002, 92301747003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 06/21/16 16:043.8
Arsenic ug/L ND 10.0 06/20/16 20:012.5
Barium ug/L ND 100 06/20/16 20:012.5
Beryllium ug/L ND 1.0 06/20/16 20:010.50
Cadmium ug/L ND 1.0 06/20/16 20:010.50
Chromium ug/L ND 10.0 06/24/16 14:472.5
Cobalt ug/L ND 10.0 06/20/16 20:012.5
Copper ug/L ND 10.0 06/20/16 20:012.5
Lead ug/L ND 10.0 06/20/16 20:012.5
Nickel ug/L ND 50.0 06/20/16 20:012.5
Selenium ug/L ND 10.0 06/20/16 20:015.0
Silver ug/L ND 10.0 06/20/16 20:012.5
Thallium ug/L ND 5.5 06/20/16 20:015.0
Tin ug/L ND 100 06/20/16 20:012.5
Vanadium ug/L ND 25.0 06/20/16 20:012.5
Zinc ug/L ND 10.0 06/20/16 20:015.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758279LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 523500 105 80-120
Arsenic ug/L 513500 103 80-120
Barium ug/L 525500 105 80-120
Beryllium ug/L 503500 101 80-120
Cadmium ug/L 537500 107 80-120
Chromium ug/L 518500 104 80-120
Cobalt ug/L 533500 107 80-120
Copper ug/L 514500 103 80-120
Lead ug/L 526500 105 80-120
Nickel ug/L 520500 104 80-120
Selenium ug/L 524500 105 80-120
Silver ug/L 257250 103 80-120
Thallium ug/L 505500 101 80-120
Tin ug/L 539500 108 80-120
Vanadium ug/L 520500 104 80-120
Zinc ug/L 522500 104 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 99 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758280MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301640001
1758281
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125103 0 25500ND517516
Arsenic ug/L 500 111 75-125100 10 25500ND556504
Barium ug/L 500 111 75-125103 6 25500111666626
Beryllium ug/L 500 106 75-12599 6 25500ND530497
Cadmium ug/L 500 115 75-125105 10 25500ND575523
Chromium ug/L 500 103 75-125102 1 25500ND516513
Cobalt ug/L 500 115 75-125104 9 255004.7J 578 526
Copper ug/L 500 102 75-125101 1 25500ND509505
Lead ug/L 500 113 75-125103 10 25500ND568515
Nickel ug/L 500 112 75-125102 9 255003.8J 562 514
Selenium ug/L 500 111 75-125102 8 25500ND554510
Silver ug/L 250 101 75-125101 0 25250ND252252
Thallium ug/L 500 108 75-12598 9 25500ND541493
Tin ug/L 500 116 75-125106 10 25500ND582529
Vanadium ug/L 500 102 75-125102 0 255004.6J 514 517
Zinc ug/L 500 112 75-125102 9 2550012.1 573 522
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/22071
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92301747004, 92301747005, 92301747006, 92301747007, 92301747008, 92301747009, 92301747010,
92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758286
Associated Lab Samples:92301747004, 92301747005, 92301747006, 92301747007, 92301747008, 92301747009, 92301747010,
92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 06/20/16 04:323.8
Arsenic ug/L ND 10.0 06/20/16 21:432.5
Barium ug/L ND 100 06/20/16 21:432.5
Beryllium ug/L ND 1.0 06/20/16 21:430.50
Cadmium ug/L ND 1.0 06/20/16 21:430.50
Chromium ug/L ND 10.0 06/20/16 21:432.5
Cobalt ug/L ND 10.0 06/20/16 21:432.5
Copper ug/L ND 10.0 06/20/16 21:432.5
Lead ug/L ND 10.0 06/20/16 21:432.5
Nickel ug/L ND 50.0 06/20/16 21:432.5
Selenium ug/L ND 10.0 06/20/16 21:435.0
Silver ug/L ND 10.0 06/20/16 21:432.5
Thallium ug/L ND 5.5 06/20/16 21:435.0
Tin ug/L ND 100 06/20/16 21:432.5
Vanadium ug/L ND 25.0 06/20/16 21:432.5
Zinc ug/L 8.7J 10.0 06/20/16 21:435.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758287LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 542500 108 80-120
Arsenic ug/L 521500 104 80-120
Barium ug/L 530500 106 80-120
Beryllium ug/L 502500 100 80-120
Cadmium ug/L 545500 109 80-120
Chromium ug/L 525500 105 80-120
Cobalt ug/L 538500 108 80-120
Copper ug/L 519500 104 80-120
Lead ug/L 533500 107 80-120
Nickel ug/L 524500 105 80-120
Selenium ug/L 529500 106 80-120
Silver ug/L 255250 102 80-120
Thallium ug/L 509500 102 80-120
Tin ug/L 544500 109 80-120
Vanadium ug/L 514500 103 80-120
Zinc ug/L 531500 106 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758288MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301747004
1758289
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 106 75-125105 1 25500ND529523
Arsenic ug/L 500 102 75-125103 1 25500ND511516
Barium ug/L 500 105 75-125105 0 2550051.7J 579 578
Beryllium ug/L 500 101 75-125101 0 25500ND506505
Cadmium ug/L 500 107 75-125107 0 25500ND535535
Chromium ug/L 500 104 75-125105 1 25500ND522525
Cobalt ug/L 500 106 75-125106 0 25500ND529530
Copper ug/L 500 103 75-125104 1 25500ND517520
Lead ug/L 500 104 75-125105 0 25500ND522524
Nickel ug/L 500 104 75-125104 0 25500ND518520
Selenium ug/L 500 104 75-125104 0 25500ND520519
Silver ug/L 250 102 75-125103 1 25250ND255257
Thallium ug/L 500 99 75-125100 1 25500ND500505
Tin ug/L 500 107 75-125107 0 25500ND537537
Vanadium ug/L 500 104 75-125104 0 25500ND522523
Zinc ug/L 500 104 75-125104 0 25500ND522523
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/37336
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758547
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/17/16 13:300.33
1,1,1-Trichloroethane ug/L ND 1.0 06/17/16 13:300.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/17/16 13:300.40
1,1,2-Trichloroethane ug/L ND 1.0 06/17/16 13:300.29
1,1-Dichloroethane ug/L ND 5.0 06/17/16 13:300.32
1,1-Dichloroethene ug/L ND 5.0 06/17/16 13:300.56
1,1-Dichloropropene ug/L ND 5.0 06/17/16 13:300.49
1,2,3-Trichloropropane ug/L ND 1.0 06/17/16 13:300.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/17/16 13:300.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/17/16 13:302.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/17/16 13:300.27
1,2-Dichlorobenzene ug/L ND 5.0 06/17/16 13:300.30
1,2-Dichloroethane ug/L ND 1.0 06/17/16 13:300.24
1,2-Dichloropropane ug/L ND 1.0 06/17/16 13:300.27
1,3-Dichlorobenzene ug/L ND 5.0 06/17/16 13:300.24
1,3-Dichloropropane ug/L ND 1.0 06/17/16 13:300.28
1,4-Dichlorobenzene ug/L ND 1.0 06/17/16 13:300.33
2,2-Dichloropropane ug/L ND 15.0 06/17/16 13:300.13
2-Butanone (MEK)ug/L ND 100 06/17/16 13:300.96
2-Hexanone ug/L ND 50.0 06/17/16 13:300.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/17/16 13:300.33
Acetone ug/L ND 100 06/17/16 13:3010.0
Acetonitrile ug/L ND 55.0 06/17/16 13:302.2
Acrolein ug/L ND 53.0 06/17/16 13:301.6
Acrylonitrile ug/L ND 200 06/17/16 13:301.9
Allyl chloride ug/L ND 10.0 06/17/16 13:301.5
Benzene ug/L ND 1.0 06/17/16 13:300.25
Bromochloromethane ug/L ND 3.0 06/17/16 13:300.17
Bromodichloromethane ug/L ND 1.0 06/17/16 13:300.18
Bromoform ug/L ND 3.0 06/17/16 13:300.26
Bromomethane ug/L ND 10.0 06/17/16 13:300.29
Carbon disulfide ug/L ND 100 06/17/16 13:301.2
Carbon tetrachloride ug/L ND 1.0 06/17/16 13:300.25
Chlorobenzene ug/L ND 3.0 06/17/16 13:300.23
Chloroethane ug/L ND 10.0 06/17/16 13:300.54
Chloroform ug/L ND 5.0 06/17/16 13:300.14
Chloromethane ug/L ND 1.0 06/17/16 13:300.11
Chloroprene ug/L ND 20.0 06/17/16 13:300.27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758547
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
cis-1,2-Dichloroethene ug/L ND 5.0 06/17/16 13:300.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/17/16 13:300.13
Dibromochloromethane ug/L ND 3.0 06/17/16 13:300.21
Dibromomethane ug/L ND 10.0 06/17/16 13:300.21
Dichlorodifluoromethane ug/L ND 5.0 06/17/16 13:300.21
Ethyl methacrylate ug/L ND 10.0 06/17/16 13:300.20
Ethylbenzene ug/L ND 1.0 06/17/16 13:300.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/17/16 13:300.71
Iodomethane ug/L ND 10.0 06/17/16 13:300.32
Isobutanol ug/L ND 100 06/17/16 13:3035.0
Methacrylonitrile ug/L ND 100 06/17/16 13:300.93
Methyl methacrylate ug/L ND 30.0 06/17/16 13:302.0
Methylene Chloride ug/L ND 1.0 06/17/16 13:300.97
Naphthalene ug/L ND 10.0 06/17/16 13:300.24
Propionitrile ug/L ND 150 06/17/16 13:303.6
Styrene ug/L ND 1.0 06/17/16 13:300.26
Tetrachloroethene ug/L ND 1.0 06/17/16 13:300.46
Toluene ug/L ND 1.0 06/17/16 13:300.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/17/16 13:300.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/17/16 13:300.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/17/16 13:301.0
Trichloroethene ug/L ND 1.0 06/17/16 13:300.47
Trichlorofluoromethane ug/L ND 1.0 06/17/16 13:300.20
Vinyl acetate ug/L ND 50.0 06/17/16 13:300.35
Vinyl chloride ug/L ND 1.0 06/17/16 13:300.62
Xylene (Total)ug/L ND 5.0 06/17/16 13:300.66
1,2-Dichloroethane-d4 (S)%95 70-130 06/17/16 13:30
4-Bromofluorobenzene (S)%96 70-130 06/17/16 13:30
Toluene-d8 (S)%99 70-130 06/17/16 13:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758548LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.750 93 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 47.650 95 85-125
1,1-Dichloroethane ug/L 47.750 95 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,1-Dichloropropene ug/L 46.450 93 74-135
1,2,3-Trichloropropane ug/L 45.450 91 75-130
1,2,4-Trichlorobenzene ug/L 52.150 104 75-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758548LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 51.450 103 83-124
1,2-Dichlorobenzene ug/L 51.050 102 80-133
1,2-Dichloroethane ug/L 42.450 85 67-128
1,2-Dichloropropane ug/L 46.050 92 75-132
1,3-Dichlorobenzene ug/L 48.850 98 77-130
1,3-Dichloropropane ug/L 44.950 90 76-131
1,4-Dichlorobenzene ug/L 48.050 96 78-130
2,2-Dichloropropane ug/L 50.350 101 40-160
2-Butanone (MEK)ug/L 90.7J100 91 61-144
2-Hexanone ug/L 95.2100 95 68-143
4-Methyl-2-pentanone (MIBK)ug/L 90.6J100 91 72-135
Acetone ug/L 87.3J100 87 48-146
Acetonitrile ug/L 447500 89 62-150
Acrolein ug/L 181250 72 24-160
Acrylonitrile ug/L 242250 97 40-160
Allyl chloride ug/L 48.950 98 66-137
Benzene ug/L 48.550 97 80-125
Bromochloromethane ug/L 50.950 102 71-125
Bromodichloromethane ug/L 51.950 104 78-124
Bromoform ug/L 45.850 92 71-128
Bromomethane ug/L 47.350 95 40-160
Carbon disulfide ug/L 51.4J50 103 50-160
Carbon tetrachloride ug/L 51.050 102 69-131
Chlorobenzene ug/L 47.650 95 81-122
Chloroethane ug/L 42.750 85 39-148
Chloroform ug/L 47.450 95 73-127
Chloromethane ug/L 49.150 98 44-146
Chloroprene ug/L 46.550 93 75-145
cis-1,2-Dichloroethene ug/L 47.950 96 74-124
cis-1,3-Dichloropropene ug/L 49.950 100 72-132
Dibromochloromethane ug/L 47.950 96 78-125
Dibromomethane ug/L 46.550 93 82-120
Dichlorodifluoromethane ug/L 39.550 79 34-157
Ethyl methacrylate ug/L 46.450 93 82-121
Ethylbenzene ug/L 47.550 95 79-121
Hexachloro-1,3-butadiene ug/L 53.250 106 72-131
Iodomethane ug/L 114100 114 39-154
Isobutanol ug/L 11601000 116 34-160
Methacrylonitrile ug/L 448500 90 74-134
Methyl methacrylate ug/L 48.650 97 84-124
Methylene Chloride ug/L 45.950 92 64-133
Naphthalene ug/L 48.950 98 73-133
Propionitrile ug/L 474500 95 73-140
Styrene ug/L 49.150 98 84-126
Tetrachloroethene ug/L 45.150 90 78-122
Toluene ug/L 48.350 97 80-121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758548LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,2-Dichloroethene ug/L 48.750 97 71-127
trans-1,3-Dichloropropene ug/L 48.050 96 69-141
trans-1,4-Dichloro-2-butene ug/L 59.7J50 119 40-160
Trichloroethene ug/L 46.450 93 78-122
Trichlorofluoromethane ug/L 45.050 90 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 46.050 92 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758549MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747001
1,1,1,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,1-Trichloroethane ug/L 23.120 116 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.520 103 70-130ND
1,1,2-Trichloroethane ug/L 20.120 101 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 23.220 116 70-166ND
1,1-Dichloropropene ug/L 21.720 109 70-130ND
1,2,3-Trichloropropane ug/L 19.820 99 70-130ND
1,2,4-Trichlorobenzene ug/L 21.320 106 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.420 112 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.520 112 70-130ND
1,2-Dichlorobenzene ug/L 22.120 111 70-130ND
1,2-Dichloroethane ug/L 19.220 95 70-130ND
1,2-Dichloropropane ug/L 20.320 102 70-130ND
1,3-Dichlorobenzene ug/L 21.620 108 70-130ND
1,3-Dichloropropane ug/L 20.120 101 70-130ND
1,4-Dichlorobenzene ug/L 20.820 104 70-130ND
2,2-Dichloropropane ug/L 21.120 106 70-130ND
2-Butanone (MEK)ug/L 38.4J40 96 70-130ND
2-Hexanone ug/L 39.8J40 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.0J40 93 70-130ND
Acetone ug/L 38.7J40 97 70-130ND
Acetonitrile ug/L 197200 99 70-130ND
Acrolein ug/L 91.3100 91 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 21.620 108 70-130ND
Benzene ug/L 21.620 108 70-148ND
Bromochloromethane ug/L 22.420 112 70-130ND
Bromodichloromethane ug/L 21.820 109 70-130ND
Bromoform ug/L 21.920 110 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758549MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747001
Bromomethane ug/L 25.920 129 70-130ND
Carbon disulfide ug/L 22.8J20 114 70-130ND
Carbon tetrachloride ug/L 24.820 124 70-130ND
Chlorobenzene ug/L 21.620 108 70-146ND
Chloroethane ug/L 20.520 103 70-130ND
Chloroform ug/L 21.120 105 70-130ND
Chloromethane ug/L 22.820 114 70-130ND
Chloroprene ug/L 21.120 106 70-130ND
cis-1,2-Dichloroethene ug/L 21.720 109 70-130ND
cis-1,3-Dichloropropene ug/L 20.320 101 70-130ND
Dibromochloromethane ug/L 21.920 109 70-130ND
Dibromomethane ug/L 20.120 101 70-130ND
Dichlorodifluoromethane ug/L 17.620 88 70-130ND
Ethyl methacrylate ug/L 21.220 106 70-130ND
Ethylbenzene ug/L 21.520 107 70-130ND
Hexachloro-1,3-butadiene ug/L 21.520 108 70-130ND
Iodomethane ug/L 55.4 M14013970-130ND
Isobutanol ug/L 470400 118 70-130ND
Methacrylonitrile ug/L 192200 96 70-130ND
Methyl methacrylate ug/L 21.1J20 105 70-130ND
Methylene Chloride ug/L 21.120 102 70-130ND
Naphthalene ug/L 20.120 101 70-130ND
Propionitrile ug/L 192200 96 70-130ND
Styrene ug/L 21.920 110 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 21.420 107 70-155ND
trans-1,2-Dichloroethene ug/L 22.420 112 70-130ND
trans-1,3-Dichloropropene ug/L 19.520 98 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.2J20 76 70-130ND
Trichloroethene ug/L 21.020 105 69-151ND
Trichlorofluoromethane ug/L 21.720 108 70-130ND
Vinyl acetate ug/L 40.1J40 100 70-130ND
Vinyl chloride ug/L 21.420 107 70-130ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747002
1758550SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 2.7J 0 302.7J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747002
1758550SAMPLE DUPLICATE:
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 1.7J 0 301.7J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Page 108 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747002
1758550SAMPLE DUPLICATE:
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 0.67J 300.64J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 0.48J 300.49J
Trichlorofluoromethane ug/L 0.21J 300.22J
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%93 497
4-Bromofluorobenzene (S)%97 298
Toluene-d8 (S)%99 1100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/43117
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92301747001, 92301747002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758035
Associated Lab Samples:92301747001, 92301747002
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/17/16 20:250.050
4,4'-DDE ug/L ND 0.10 06/17/16 20:250.050
4,4'-DDT ug/L ND 0.10 06/17/16 20:250.050
Aldrin ug/L ND 0.050 06/17/16 20:250.050
alpha-BHC ug/L ND 0.050 06/17/16 20:250.050
beta-BHC ug/L ND 0.050 06/17/16 20:250.050
Chlordane (Technical)ug/L ND 0.50 06/17/16 20:250.20
delta-BHC ug/L ND 0.050 06/17/16 20:250.050
Dieldrin ug/L ND 0.075 06/17/16 20:250.050
Endosulfan I ug/L ND 0.10 06/17/16 20:250.050
Endosulfan II ug/L ND 0.10 06/17/16 20:250.050
Endosulfan sulfate ug/L ND 0.10 06/17/16 20:250.050
Endrin ug/L ND 0.10 06/17/16 20:250.050
Endrin aldehyde ug/L ND 0.10 06/17/16 20:250.050
gamma-BHC (Lindane)ug/L ND 0.050 06/17/16 20:250.050
Heptachlor ug/L ND 0.050 06/17/16 20:250.050
Heptachlor epoxide ug/L ND 0.075 06/17/16 20:250.050
Methoxychlor ug/L ND 1.0 06/17/16 20:250.15
Toxaphene ug/L ND 1.5 06/17/16 20:250.20
Decachlorobiphenyl (S)%80 20-130 06/17/16 20:25
Tetrachloro-m-xylene (S)%91 20-130 06/17/16 20:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758036LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1758037
4,4'-DDD ug/L 0.24.25 97 20-150950.24 1 30
4,4'-DDE ug/L 0.23.25 92 20-150910.22 1 30
4,4'-DDT ug/L 0.24.25 95 20-150950.23 1 30
Aldrin ug/L 0.22.25 90 20-150900.22 0 30
alpha-BHC ug/L 0.22.25 89 20-150890.22 0 30
beta-BHC ug/L 0.23.25 93 20-150930.23 0 30
delta-BHC ug/L 0.23.25 94 20-150930.23 0 30
Dieldrin ug/L 0.22.25 90 20-150900.22 1 30
Endosulfan I ug/L 0.24.25 96 20-150970.24 1 30
Endosulfan II ug/L 0.26.25 103 20-1501020.25 1 30
Endosulfan sulfate ug/L 0.26.25 104 20-1501030.26 1 30
Endrin ug/L 0.24.25 97 20-150970.24 0 30
Endrin aldehyde ug/L 0.21.25 84 20-150840.21 0 30
gamma-BHC (Lindane)ug/L 0.22.25 90 20-150900.22 0 30
Heptachlor ug/L 0.22.25 90 20-150900.22 0 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Huntersville, NC 28078
[phone]
Page 110 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758036LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1758037
Heptachlor epoxide ug/L 0.23.25 93 20-150910.22 3 30
Methoxychlor ug/L 0.85J.74 114 20-1501140.84J 1 30
Decachlorobiphenyl (S)%81 20-13081
Tetrachloro-m-xylene (S)%86 20-13087
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/43123
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92301747003, 92301747004, 92301747005, 92301747006, 92301747007, 92301747008, 92301747009,
92301747010, 92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758438
Associated Lab Samples:92301747003, 92301747004, 92301747005, 92301747006, 92301747007, 92301747008, 92301747009,
92301747010, 92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/17/16 21:180.050
4,4'-DDE ug/L ND 0.10 06/17/16 21:180.050
4,4'-DDT ug/L ND 0.10 06/17/16 21:180.050
Aldrin ug/L ND 0.050 06/17/16 21:180.050
alpha-BHC ug/L ND 0.050 06/17/16 21:180.050
beta-BHC ug/L ND 0.050 06/17/16 21:180.050
Chlordane (Technical)ug/L ND 0.50 06/17/16 21:180.20
delta-BHC ug/L ND 0.050 06/17/16 21:180.050
Dieldrin ug/L ND 0.075 06/17/16 21:180.050
Endosulfan I ug/L ND 0.10 06/17/16 21:180.050
Endosulfan II ug/L ND 0.10 06/17/16 21:180.050
Endosulfan sulfate ug/L ND 0.10 06/17/16 21:180.050
Endrin ug/L ND 0.10 06/17/16 21:180.050
Endrin aldehyde ug/L ND 0.10 06/17/16 21:180.050
gamma-BHC (Lindane)ug/L ND 0.050 06/17/16 21:180.050
Heptachlor ug/L ND 0.050 06/17/16 21:180.050
Heptachlor epoxide ug/L ND 0.075 06/17/16 21:180.050
Methoxychlor ug/L ND 1.0 06/17/16 21:180.15
Toxaphene ug/L ND 1.5 06/17/16 21:180.20
Decachlorobiphenyl (S)%54 20-130 06/17/16 21:18
Tetrachloro-m-xylene (S)%84 20-130 06/17/16 21:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758439LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.24.25 95 20-150
4,4'-DDE ug/L 0.22.25 90 20-150
4,4'-DDT ug/L 0.23.25 95 20-150
Aldrin ug/L 0.22.25 87 20-150
alpha-BHC ug/L 0.22.25 88 20-150
beta-BHC ug/L 0.22.25 91 20-150
delta-BHC ug/L 0.23.25 92 20-150
Dieldrin ug/L 0.22.25 89 20-150
Endosulfan I ug/L 0.24.25 96 20-150
Endosulfan II ug/L 0.25.25 102 20-150
Endosulfan sulfate ug/L 0.26.25 104 20-150
Endrin ug/L 0.24.25 96 20-150
Endrin aldehyde ug/L 0.21.25 85 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758439LABORATORY CONTROL SAMPLE:
LCSSpike
gamma-BHC (Lindane)ug/L 0.21.25 87 20-150
Heptachlor ug/L 0.22.25 88 20-150
Heptachlor epoxide ug/L 0.22.25 90 20-150
Methoxychlor ug/L 0.85J.74 115 20-150
Decachlorobiphenyl (S)%53 20-130
Tetrachloro-m-xylene (S)%71 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758440MATRIX SPIKE SAMPLE:
MSSpike
Result
92301165020
4,4'-DDD ug/L 0.22.25 88 20-150ND
4,4'-DDE ug/L 0.20.25 81 20-150ND
4,4'-DDT ug/L 0.23.25 92 20-150ND
Aldrin ug/L 0.19.25 76 20-150ND
alpha-BHC ug/L 0.19.25 78 20-150ND
beta-BHC ug/L 0.19.25 78 20-150ND
delta-BHC ug/L 0.21.25 83 20-150ND
Dieldrin ug/L 0.20.25 81 20-150ND
Endosulfan I ug/L 0.22.25 87 20-150ND
Endosulfan II ug/L 0.23.25 91 20-150ND
Endosulfan sulfate ug/L 0.25.25 101 20-150ND
Endrin ug/L 0.23.25 94 20-150ND
Endrin aldehyde ug/L 0.18.25 74 20-150ND
gamma-BHC (Lindane)ug/L 0.19.25 76 20-150ND
Heptachlor ug/L 0.19.25 75 20-150ND
Heptachlor epoxide ug/L 0.20.25 80 20-150ND
Methoxychlor ug/L 0.83J.74 111 20-150ND
Decachlorobiphenyl (S)%67 20-130
Tetrachloro-m-xylene (S)%82 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301165021
1758441SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301165021
1758441SAMPLE DUPLICATE:
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%73 172
Tetrachloro-m-xylene (S)%68 1478
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/43116
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92301747001, 92301747002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758014
Associated Lab Samples:92301747001, 92301747002
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/17/16 13:300.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/17/16 13:300.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/17/16 13:300.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/17/16 13:300.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/17/16 13:300.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/17/16 13:300.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/17/16 13:300.50
Decachlorobiphenyl (S)%75 10-132 06/17/16 13:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758015LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 4.75 95 50-150
PCB-1260 (Aroclor 1260)ug/L 5.25 105 50-150
Decachlorobiphenyl (S)%72 10-132
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758016MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301165001
1758017
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)ug/L 5 93 50-15096 3 305ND4.6 4.8
PCB-1260 (Aroclor 1260)ug/L 5 94 50-15093 0 305ND4.7 4.7
Decachlorobiphenyl (S)%56 10-13250
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/43124
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92301747003, 92301747004, 92301747005, 92301747006, 92301747007, 92301747008, 92301747009,
92301747010, 92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758444
Associated Lab Samples:92301747003, 92301747004, 92301747005, 92301747006, 92301747007, 92301747008, 92301747009,
92301747010, 92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/18/16 09:280.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/18/16 09:280.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/18/16 09:280.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/18/16 09:280.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/18/16 09:280.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/18/16 09:280.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/18/16 09:280.50
Decachlorobiphenyl (S)%50 10-132 06/18/16 09:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758445LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 4.95 97 50-150
PCB-1260 (Aroclor 1260)ug/L 5.65 113 50-150
Decachlorobiphenyl (S)%57 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758511MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747005
PCB-1016 (Aroclor 1016)ug/L 4.75 94 50-150ND
PCB-1260 (Aroclor 1260)ug/L 4.45 88 50-150ND
Decachlorobiphenyl (S)%52 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747007
1758512SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%67 1260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28682
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1611321
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/22/16 05:130.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/22/16 05:130.049
2,4-D ug/L ND 0.94 06/22/16 05:130.22
Dinoseb ug/L ND 0.19 06/22/16 05:130.057
Pentachlorophenol ug/L ND 0.028 06/22/16 05:130.017
2,4-DCAA (S)%100 39-139 06/22/16 05:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1611322LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.61.2 130 37-133
2,4,5-TP (Silvex)ug/L 1.31.2 112 53-134
2,4-D ug/L 6.26 103 35-124
Dinoseb ug/L 0.911.2 76 13-116
Pentachlorophenol ug/L 0.24.18 135 39-170
2,4-DCAA (S)%101 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1612708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301165001
1612709
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 112 37-133118 4 401.2ND 1.4 1.4
2,4,5-TP (Silvex)ug/L 1.2 98 53-134124 22 401.2ND 1.2 1.5
2,4-D ug/L 6.1 89 35-124102 11 406.1ND 5.5 6.1
Dinoseb ug/L 1.2 81 13-11686 4 401.2ND 0.99 1.0
Pentachlorophenol ug/L .18 125 39-170146 14 40.18ND 0.23 0.26
2,4-DCAA (S)%89 39-13997 40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 117 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28725
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92301747012, 92301747013, 92301747014, 92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1614851
Associated Lab Samples:92301747012, 92301747013, 92301747014, 92301747015
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/24/16 05:070.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/24/16 05:070.049
2,4-D ug/L ND 0.94 06/24/16 05:070.22
Dinoseb ug/L ND 0.19 06/24/16 05:070.057
Pentachlorophenol ug/L ND 0.028 06/24/16 05:070.017
2,4-DCAA (S)%104 39-139 06/24/16 05:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1614852LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1615213
2,4,5-T ug/L 1.41.2 113 37-1331111.3 1 40
2,4,5-TP (Silvex)ug/L 1.31.2 110 53-1341031.2 6 40
2,4-D ug/L 5.76 96 35-124935.6 3 40
Dinoseb ug/L 1.11.2 88 13-116810.97 8 40
Pentachlorophenol ug/L 0.19.18 105 39-1701030.19 2 40
2,4-DCAA (S)%96 39-13991 40
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1616742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92302126002
1616743
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 88 37-133104 17 401.2ND 1.1 1.3
2,4,5-TP (Silvex)ug/L 1.2 82 53-134101 21 401.2ND 0.99 1.2
2,4-D ug/L 6 73 35-12487 18 406ND4.4 5.2
Dinoseb ug/L R11.2 50 13-116101 68 401.2ND 0.60 1.2
Pentachlorophenol ug/L .18 66 39-17082 23 40.18ND 0.12 0.15
2,4-DCAA (S)%75 39-13992 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/43142
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1759513
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/22/16 21:481.7
1,3,5-Trinitrobenzene ug/L ND 10.0 06/22/16 21:481.1
1,3-Dinitrobenzene ug/L ND 20.0 06/22/16 21:481.5
1,4-Naphthoquinone ug/L ND 10.0 06/22/16 21:481.8
1-Naphthalenamine ug/L ND 10.0 06/22/16 21:480.96
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/22/16 21:481.6
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/22/16 21:482.3
2,4,5-Trichlorophenol ug/L ND 10.0 06/22/16 21:482.2
2,4,6-Trichlorophenol ug/L ND 10.0 06/22/16 21:481.9
2,4-Dichlorophenol ug/L ND 10.0 06/22/16 21:481.7
2,4-Dimethylphenol ug/L ND 10.0 06/22/16 21:482.2
2,4-Dinitrophenol ug/L ND 50.0 06/22/16 21:486.5
2,4-Dinitrotoluene ug/L ND 10.0 06/22/16 21:481.2
2,6-Dichlorophenol ug/L ND 10.0 06/22/16 21:481.8
2,6-Dinitrotoluene ug/L ND 10.0 06/22/16 21:481.7
2-Acetylaminofluorene ug/L ND 20.0 06/22/16 21:480.84
2-Chloronaphthalene ug/L ND 10.0 06/22/16 21:482.2
2-Chlorophenol ug/L ND 10.0 06/22/16 21:481.5
2-Methylnaphthalene ug/L ND 10.0 06/22/16 21:480.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/22/16 21:481.7
2-Naphthalenamine ug/L ND 10.0 06/22/16 21:480.98
2-Nitroaniline ug/L ND 50.0 06/22/16 21:482.8
2-Nitrophenol ug/L ND 10.0 06/22/16 21:481.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/22/16 21:481.7
3,3'-Dichlorobenzidine ug/L ND 20.0 06/22/16 21:481.4
3,3'-Dimethylbenzidine ug/L ND 10.0 06/22/16 21:482.1
3-Methylcholanthrene ug/L ND 10.0 06/22/16 21:480.82
3-Nitroaniline ug/L ND 50.0 06/22/16 21:482.4
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/22/16 21:481.7
4-Aminobiphenyl ug/L ND 20.0 06/22/16 21:480.92
4-Bromophenylphenyl ether ug/L ND 10.0 06/22/16 21:481.3
4-Chloro-3-methylphenol ug/L ND 20.0 06/22/16 21:484.2
4-Chloroaniline ug/L ND 20.0 06/22/16 21:483.4
4-Chlorophenylphenyl ether ug/L ND 10.0 06/22/16 21:482.1
4-Nitroaniline ug/L ND 20.0 06/22/16 21:482.5
4-Nitrophenol ug/L ND 50.0 06/22/16 21:485.8
5-Nitro-o-toluidine ug/L ND 10.0 06/22/16 21:481.2
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/22/16 21:480.77
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1759513
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
Acenaphthene ug/L ND 10.0 06/22/16 21:480.25
Acenaphthylene ug/L ND 10.0 06/22/16 21:480.21
Acetophenone ug/L ND 10.0 06/22/16 21:482.0
Anthracene ug/L ND 10.0 06/22/16 21:480.14
Benzo(a)anthracene ug/L ND 10.0 06/22/16 21:480.33
Benzo(a)pyrene ug/L ND 10.0 06/22/16 21:480.30
Benzo(b)fluoranthene ug/L ND 10.0 06/22/16 21:480.28
Benzo(g,h,i)perylene ug/L ND 10.0 06/22/16 21:480.38
Benzo(k)fluoranthene ug/L ND 10.0 06/22/16 21:480.43
Benzyl alcohol ug/L ND 20.0 06/22/16 21:483.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/22/16 21:481.7
bis(2-Chloroethyl) ether ug/L ND 10.0 06/22/16 21:481.5
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/22/16 21:480.85
Butylbenzylphthalate ug/L ND 10.0 06/22/16 21:480.75
Chlorobenzilate ug/L ND 10.0 06/22/16 21:480.72
Chrysene ug/L ND 10.0 06/22/16 21:480.21
Di-n-butylphthalate ug/L ND 10.0 06/22/16 21:481.1
Di-n-octylphthalate ug/L ND 10.0 06/22/16 21:480.86
Diallate ug/L ND 10.0 06/22/16 21:481.3
Dibenz(a,h)anthracene ug/L ND 10.0 06/22/16 21:480.55
Dibenzofuran ug/L ND 10.0 06/22/16 21:481.8
Diethylphthalate ug/L ND 6000 06/22/16 21:481.3
Dimethoate ug/L ND 20.0 06/22/16 21:480.92
Dimethylphthalate ug/L ND 10.0 06/22/16 21:481.5
Diphenylamine ug/L ND 10.0 06/22/16 21:481.3
Disulfoton ug/L ND 10.0 06/22/16 21:481.4
Ethyl methanesulfonate ug/L ND 20.0 06/22/16 21:481.8
Famphur ug/L ND 20.0 06/22/16 21:481.7
Fluoranthene ug/L ND 10.0 06/22/16 21:480.21
Fluorene ug/L ND 10.0 06/22/16 21:480.21
Hexachlorobenzene ug/L ND 10.0 06/22/16 21:481.1
Hexachlorocyclopentadiene ug/L ND 10.0 06/22/16 21:481.8
Hexachloroethane ug/L ND 10.0 06/22/16 21:481.5
Hexachloropropene ug/L ND 10.0 06/22/16 21:481.6
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/22/16 21:480.29
Isodrin ug/L ND 20.0 06/22/16 21:482.0
Isophorone ug/L ND 10.0 06/22/16 21:481.8
Isosafrole ug/L ND 10.0 06/22/16 21:481.8
Kepone ug/L ND 20.0 06/22/16 21:483.1
Methapyrilene ug/L ND 100 06/22/16 21:482.7
Methyl methanesulfonate ug/L ND 10.0 06/22/16 21:481.3
Methyl parathion ug/L ND 10.0 06/22/16 21:481.1
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/22/16 21:482.2
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/22/16 21:482.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1759513
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
N-Nitrosodiethylamine ug/L ND 20.0 06/22/16 21:481.8
N-Nitrosodimethylamine ug/L ND 10.0 06/22/16 21:481.3
N-Nitrosodiphenylamine ug/L ND 10.0 06/22/16 21:481.3
N-Nitrosomethylethylamine ug/L ND 10.0 06/22/16 21:481.8
N-Nitrosopiperidine ug/L ND 20.0 06/22/16 21:481.9
N-Nitrosopyrrolidine ug/L ND 10.0 06/22/16 21:482.5
Nitrobenzene ug/L ND 10.0 06/22/16 21:481.7
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/22/16 21:481.8
O-Toluidine ug/L ND 10.0 06/22/16 21:481.6
P-Dimethylaminoazobenzene ug/L ND 10.0 06/22/16 21:480.35
p-Phenylenediamine ug/L ND 10.0 06/22/16 21:480.96
Parathion (Ethyl parathion)ug/L ND 10.0 06/22/16 21:481.1
Pentachlorobenzene ug/L ND 10.0 06/22/16 21:482.0
Pentachloronitrobenzene ug/L ND 20.0 06/22/16 21:481.0
Pentachlorophenol ug/L ND 25.0 06/22/16 21:482.3
Phenacetin ug/L ND 20.0 06/22/16 21:480.97
Phenanthrene ug/L ND 10.0 06/22/16 21:480.22
Phenol ug/L ND 10.0 06/22/16 21:481.7
Phorate ug/L ND 10.0 06/22/16 21:481.1
Pronamide ug/L ND 10.0 06/22/16 21:480.97
Pyrene ug/L ND 10.0 06/22/16 21:480.19
Safrole ug/L ND 10.0 06/22/16 21:481.5
Thionazin ug/L ND 20.0 06/22/16 21:481.2
2,4,6-Tribromophenol (S)%87 27-110 06/22/16 21:48
2-Fluorobiphenyl (S)%68 27-110 06/22/16 21:48
2-Fluorophenol (S)%35 12-110 06/22/16 21:48
Nitrobenzene-d5 (S)%70 21-110 06/22/16 21:48
Phenol-d6 (S)%24 10-110 06/22/16 21:48
Terphenyl-d14 (S)%102 31-107 06/22/16 21:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759514LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 30.850 62 16-129
1,3,5-Trinitrobenzene ug/L 190 L05037955-125
1,3-Dinitrobenzene ug/L 46.750 93 30-122
1,4-Naphthoquinone ug/L 38.050 76 31-120
1-Naphthalenamine ug/L 27.150 54 37-126
2,2'-Oxybis(1-chloropropane)ug/L 30.150 60 18-120
2,3,4,6-Tetrachlorophenol ug/L 96.350 193 54-276
2,4,5-Trichlorophenol ug/L 46.550 93 43-113
2,4,6-Trichlorophenol ug/L 50.450 101 42-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759514LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/L 42.250 84 30-120
2,4-Dimethylphenol ug/L 42.250 84 29-111
2,4-Dinitrophenol ug/L 187250 75 19-132
2,4-Dinitrotoluene ug/L 49.150 98 58-128
2,6-Dichlorophenol ug/L 43.050 86 54-128
2,6-Dinitrotoluene ug/L 49.950 100 54-129
2-Acetylaminofluorene ug/L 51.550 103 81-160
2-Chloronaphthalene ug/L 41.650 83 43-117
2-Chlorophenol ug/L 34.450 69 37-120
2-Methylnaphthalene ug/L 30.050 60 33-120
2-Methylphenol(o-Cresol)ug/L 28.350 57 31-120
2-Naphthalenamine ug/L 40.350 81 41-136
2-Nitroaniline ug/L 85.8100 86 48-121
2-Nitrophenol ug/L 42.750 85 25-116
3&4-Methylphenol(m&p Cresol)ug/L 57.650 115 23-120
3,3'-Dichlorobenzidine ug/L 93.4250 37 10-154
3,3'-Dimethylbenzidine ug/L 34.6100 35 10-157
3-Methylcholanthrene ug/L 51.150 102 65-130
3-Nitroaniline ug/L 84.2100 84 43-115
4,6-Dinitro-2-methylphenol ug/L 91.0100 91 44-124
4-Aminobiphenyl ug/L 20.550 41 21-125
4-Bromophenylphenyl ether ug/L 45.250 90 34-113
4-Chloro-3-methylphenol ug/L 78.9100 79 31-110
4-Chloroaniline ug/L 71.8100 72 20-120
4-Chlorophenylphenyl ether ug/L 45.050 90 34-116
4-Nitroaniline ug/L 87.0100 87 46-128
4-Nitrophenol ug/L 81.5250 33 11-120
5-Nitro-o-toluidine ug/L 56.750 113 78-160
7,12-Dimethylbenz(a)anthracene ug/L 47.950 96 47-124
Acenaphthene ug/L 38.250 76 48-114
Acenaphthylene ug/L 39.350 79 48-112
Acetophenone ug/L 35.350 71 24-120
Anthracene ug/L 40.550 81 57-118
Benzo(a)anthracene ug/L 44.050 88 56-121
Benzo(a)pyrene ug/L 43.350 87 55-127
Benzo(b)fluoranthene ug/L 48.750 97 53-128
Benzo(g,h,i)perylene ug/L 43.950 88 54-125
Benzo(k)fluoranthene ug/L 41.250 82 51-123
Benzyl alcohol ug/L 61.9100 62 27-120
bis(2-Chloroethoxy)methane ug/L 36.850 74 32-120
bis(2-Chloroethyl) ether ug/L 35.650 71 33-111
bis(2-Ethylhexyl)phthalate ug/L 50.750 101 50-145
Butylbenzylphthalate ug/L 52.050 104 54-138
Chlorobenzilate ug/L 52.850 106 65-132
Chrysene ug/L 42.550 85 58-127
Di-n-butylphthalate ug/L 48.050 96 56-125
Di-n-octylphthalate ug/L 51.850 104 50-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759514LABORATORY CONTROL SAMPLE:
LCSSpike
Diallate ug/L 42.850 86 47-123
Dibenz(a,h)anthracene ug/L 44.350 89 53-129
Dibenzofuran ug/L 43.850 88 45-120
Diethylphthalate ug/L 45.4J50 91 53-120
Dimethoate ug/L 42.450 85 57-139
Dimethylphthalate ug/L 45.750 91 55-116
Diphenylamine ug/L 39.950 80 42-120
Disulfoton ug/L 43.350 87 49-156
Ethyl methanesulfonate ug/L 34.250 68 43-120
Famphur ug/L 84.7100 85 40-160
Fluoranthene ug/L 41.050 82 57-125
Fluorene ug/L 42.950 86 53-118
Hexachlorobenzene ug/L 43.550 87 49-116
Hexachlorocyclopentadiene ug/L 27.550 55 26-158
Hexachloroethane ug/L 21.050 42 30-114
Hexachloropropene ug/L 19.050 38 13-137
Indeno(1,2,3-cd)pyrene ug/L 46.650 93 55-128
Isodrin ug/L 54.350 109 68-129
Isophorone ug/L 34.650 69 31-118
Isosafrole ug/L 42.150 84 48-107
Kepone ug/L 49.5100 50 10-124
Methapyrilene ug/L 33.8J50 68 40-160
Methyl methanesulfonate ug/L 25.950 52 25-114
Methyl parathion ug/L 46.550 93 58-137
N-Nitroso-di-n-butylamine ug/L 30.050 60 36-115
N-Nitroso-di-n-propylamine ug/L 32.150 64 32-119
N-Nitrosodiethylamine ug/L 37.450 75 47-115
N-Nitrosodimethylamine ug/L 19.350 39 13-120
N-Nitrosodiphenylamine ug/L 39.950 80 43-120
N-Nitrosomethylethylamine ug/L 33.450 67 39-120
N-Nitrosopiperidine ug/L 43.750 87 43-113
N-Nitrosopyrrolidine ug/L 38.150 76 32-110
Nitrobenzene ug/L 37.850 76 33-110
O,O,O-Triethylphosphorothioate ug/L 43.350 87 51-127
O-Toluidine ug/L 30.650 61 27-120
P-Dimethylaminoazobenzene ug/L 25.9100 26 10-120
p-Phenylenediamine ug/L 44.150 88 72-143
Parathion (Ethyl parathion)ug/L 46.750 93 56-140
Pentachlorobenzene ug/L 37.850 76 30-137
Pentachloronitrobenzene ug/L 56.250 112 70-124
Pentachlorophenol ug/L 93.1250 37 10-137
Phenacetin ug/L 47.550 95 60-130
Phenanthrene ug/L 40.250 80 57-117
Phenol ug/L 14.650 29 10-120
Phorate ug/L 59.750 119 55-126
Pronamide ug/L 51.150 102 75-124
Pyrene ug/L 43.350 87 55-122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759514LABORATORY CONTROL SAMPLE:
LCSSpike
Safrole ug/L 32.050 64 41-120
Thionazin ug/L 46.750 93 63-137
2,4,6-Tribromophenol (S)%110 27-110
2-Fluorobiphenyl (S)%81 27-110
2-Fluorophenol (S)%42 12-110
Nitrobenzene-d5 (S)%81 21-110
Phenol-d6 (S)%29 10-110
Terphenyl-d14 (S)%101 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1759515MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747005
1,2,4,5-Tetrachlorobenzene ug/L 17.625 71 50-150ND
1,3,5-Trinitrobenzene ug/L 93.9 M02537650-150ND
1,3-Dinitrobenzene ug/L 23.625 94 50-150ND
1,4-Naphthoquinone ug/L 18.725 75 50-150ND
1-Naphthalenamine ug/L 16.125 64 50-150ND
2,2'-Oxybis(1-chloropropane)ug/L 27.350 55 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 69.450 139 50-150ND
2,4,5-Trichlorophenol ug/L 46.250 92 19-105ND
2,4,6-Trichlorophenol ug/L 47.250 94 13-108ND
2,4-Dichlorophenol ug/L 39.250 78 29-111ND
2,4-Dimethylphenol ug/L 39.050 78 21-103ND
2,4-Dinitrophenol ug/L 168250 67 10-109ND
2,4-Dinitrotoluene ug/L 50.850 102 27-104ND
2,6-Dichlorophenol ug/L 20.425 82 50-150ND
2,6-Dinitrotoluene ug/L 50.150 100 28-101ND
2-Acetylaminofluorene ug/L 27.025 106 50-150ND
2-Chloronaphthalene ug/L 37.950 76 14-102ND
2-Chlorophenol ug/L 32.850 66 16-110ND
2-Methylnaphthalene ug/L 30.150 60 13-110ND
2-Methylphenol(o-Cresol)ug/L 27.850 56 19-110ND
2-Naphthalenamine ug/L 20.325 81 50-150ND
2-Nitroaniline ug/L 83.9100 84 26-103ND
2-Nitrophenol ug/L 40.250 80 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 41.150 82 20-110ND
3,3'-Dichlorobenzidine ug/L 99.3250 40 25-112ND
3,3'-Dimethylbenzidine ug/L 34.150 68 50-150ND
3-Methylcholanthrene ug/L 25.825 101 50-150ND
3-Nitroaniline ug/L 88.2100 88 29-110ND
4,6-Dinitro-2-methylphenol ug/L 97.3100 97 10-117ND
4-Aminobiphenyl ug/L 16.3J25 65 50-150ND
4-Bromophenylphenyl ether ug/L 44.850 90 20-105ND
4-Chloro-3-methylphenol ug/L 78.3100 78 22-110ND
4-Chloroaniline ug/L 69.6100 70 20-100ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Huntersville, NC 28078
[phone]
Page 124 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1759515MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747005
4-Chlorophenylphenyl ether ug/L 44.850 90 19-102ND
4-Nitroaniline ug/L 95.9100 96 29-110ND
4-Nitrophenol ug/L 103250 41 10-110ND
5-Nitro-o-toluidine ug/L 29.825 119 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 24.525 95 50-150ND
Acenaphthene ug/L 37.450 75 17-100ND
Acenaphthylene ug/L 38.450 77 21-100ND
Acetophenone ug/L 33.650 67 50-150ND
Anthracene ug/L 40.250 80 24-109ND
Benzo(a)anthracene ug/L 45.650 91 22-117ND
Benzo(a)pyrene ug/L 44.050 88 23-104ND
Benzo(b)fluoranthene ug/L 47.350 95 23-103ND
Benzo(g,h,i)perylene ug/L 44.050 88 18-111ND
Benzo(k)fluoranthene ug/L 41.350 83 22-113ND
Benzyl alcohol ug/L 60.9100 61 19-101ND
bis(2-Chloroethoxy)methane ug/L 33.550 67 22-110ND
bis(2-Chloroethyl) ether ug/L 32.950 66 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 52.2 M15010423-102ND
Butylbenzylphthalate ug/L 53.250 106 25-110ND
Chlorobenzilate ug/L 28.025 110 50-150ND
Chrysene ug/L 42.850 86 23-115ND
Di-n-butylphthalate ug/L 47.950 96 26-110ND
Di-n-octylphthalate ug/L 58.9 M15011822-110ND
Diallate ug/L 20.625 82 50-150ND
Dibenz(a,h)anthracene ug/L 45.550 91 21-112ND
Dibenzofuran ug/L 43.350 87 19-102ND
Diethylphthalate ug/L 46.3J50 93 29-110ND
Dimethoate ug/L 22.425 90 50-150ND
Dimethylphthalate ug/L 45.650 91 27-110ND
Diphenylamine ug/L 38.850 78 50-150ND
Disulfoton ug/L 21.825 87 50-150ND
Ethyl methanesulfonate ug/L 16.5J25 66 50-150ND
Famphur ug/L 31.750 63 50-150ND
Fluoranthene ug/L 43.850 88 23-112ND
Fluorene ug/L 42.650 85 22-104ND
Hexachlorobenzene ug/L 43.250 86 21-116ND
Hexachlorocyclopentadiene ug/L 33.650 67 10-110ND
Hexachloroethane ug/L 22.750 45 10-110ND
Hexachloropropene ug/L 16.225 65 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 47.550 95 20-113ND
Isodrin ug/L 26.525 106 50-150ND
Isophorone ug/L 32.550 65 50-150ND
Isosafrole ug/L 20.625 82 50-150ND
Kepone ug/L 18.1J M1503450-150ND
Methapyrilene ug/L 24.2J25 97 50-150ND
Methyl methanesulfonate ug/L 13.025 52 50-150ND
Methyl parathion ug/L 23.525 94 50-150ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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[phone]
Page 125 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1759515MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747005
N-Nitroso-di-n-butylamine ug/L 14.425 57 50-150ND
N-Nitroso-di-n-propylamine ug/L 30.250 60 21-105ND
N-Nitrosodiethylamine ug/L 17.9J25 72 50-150ND
N-Nitrosodimethylamine ug/L 20.350 41 10-110ND
N-Nitrosodiphenylamine ug/L 38.850 78 23-107ND
N-Nitrosomethylethylamine ug/L 16.125 64 50-150ND
N-Nitrosopiperidine ug/L 20.925 84 50-150ND
N-Nitrosopyrrolidine ug/L 19.125 76 50-150ND
Nitrobenzene ug/L 34.750 69 20-110ND
O,O,O-Triethylphosphorothioate ug/L 21.025 84 50-150ND
O-Toluidine ug/L 15.025 60 50-150ND
P-Dimethylaminoazobenzene ug/L 13.125 51 50-150ND
p-Phenylenediamine ug/L 25.325 101 50-150ND
Parathion (Ethyl parathion)ug/L 23.825 95 50-150ND
Pentachlorobenzene ug/L 19.025 76 50-150ND
Pentachloronitrobenzene ug/L 29.025 116 50-150ND
Pentachlorophenol ug/L 82.6250 33 10-118ND
Phenacetin ug/L 25.125 101 50-150ND
Phenanthrene ug/L 40.050 80 24-106ND
Phenol ug/L 15.450 31 12-110ND
Phorate ug/L 29.625 118 50-150ND
Pronamide ug/L 26.025 104 50-150ND
Pyrene ug/L 41.850 84 24-114ND
Safrole ug/L 16.725 67 50-150ND
Thionazin ug/L 23.825 95 50-150ND
2,4,6-Tribromophenol (S)%104 27-110
2-Fluorobiphenyl (S)%75 27-110
2-Fluorophenol (S)%42 12-110
Nitrobenzene-d5 (S)%73 21-110
Phenol-d6 (S)%30 10-110
Terphenyl-d14 (S)%90 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747007
1759516SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747007
1759516SAMPLE DUPLICATE:
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747007
1759516SAMPLE DUPLICATE:
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747007
1759516SAMPLE DUPLICATE:
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%90 190
2-Fluorobiphenyl (S)%78 2363
2-Fluorophenol (S)%42 2533
Nitrobenzene-d5 (S)%76 2460
Phenol-d6 (S)%27 1922
Terphenyl-d14 (S)%93 1480
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/45640
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1759825
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/20/16 20:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759826LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 528J500 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1759827MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301574001
1759828
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 93 90-11093 0 10500ND467J467J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1759829MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301717002
1759830
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 90-110105 0 10500ND527J527J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/45641
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92301747010, 92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1759831
Associated Lab Samples:92301747010, 92301747011, 92301747012, 92301747013, 92301747014, 92301747015
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/20/16 20:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1759832LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 528J500 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1759833MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301747010
1759834
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M35004190-11041 0 10500ND270J270J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1759835MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301760004
1759836
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M3500890-1108 10500NDNDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 131 of 139
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/27991
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758024
Associated Lab Samples:92301747001, 92301747002, 92301747003, 92301747004, 92301747005, 92301747006, 92301747007,
92301747008, 92301747009, 92301747010, 92301747011, 92301747012, 92301747013, 92301747014,
92301747015
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/17/16 15:344.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758025LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 106100 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758026MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301533003
1758027
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 81 75-12578 3 10100ND85.0 82.7
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758028MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301747008
1758029
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 100 75-125101 0 10100ND104104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 139
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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[phone]
Page 133 of 139
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92301747001 OEXT/43117 GCSV/25298MW-1 EPA 3510 EPA 8081
92301747002 OEXT/43117 GCSV/25298MW-2 EPA 3510 EPA 8081
92301747003 OEXT/43123 GCSV/25304MW-3R EPA 3510 EPA 8081
92301747004 OEXT/43123 GCSV/25304MW-4S EPA 3510 EPA 8081
92301747005 OEXT/43123 GCSV/25304MW-4D EPA 3510 EPA 8081
92301747006 OEXT/43123 GCSV/25304MW-5 EPA 3510 EPA 8081
92301747007 OEXT/43123 GCSV/25304MW-6R EPA 3510 EPA 8081
92301747008 OEXT/43123 GCSV/25304MW-8 EPA 3510 EPA 8081
92301747009 OEXT/43123 GCSV/25304MW-9S EPA 3510 EPA 8081
92301747010 OEXT/43123 GCSV/25304MW-9D EPA 3510 EPA 8081
92301747011 OEXT/43123 GCSV/25304MW-10 EPA 3510 EPA 8081
92301747012 OEXT/43123 GCSV/25304MW-11S EPA 3510 EPA 8081
92301747013 OEXT/43123 GCSV/25304MW-11D EPA 3510 EPA 8081
92301747014 OEXT/43123 GCSV/25304MW-12 EPA 3510 EPA 8081
92301747015 OEXT/43123 GCSV/25304MW-13 EPA 3510 EPA 8081
92301747001 OEXT/43116 GCSV/25297MW-1 EPA 3510 EPA 8082
92301747002 OEXT/43116 GCSV/25297MW-2 EPA 3510 EPA 8082
92301747003 OEXT/43124 GCSV/25307MW-3R EPA 3510 EPA 8082
92301747004 OEXT/43124 GCSV/25307MW-4S EPA 3510 EPA 8082
92301747005 OEXT/43124 GCSV/25307MW-4D EPA 3510 EPA 8082
92301747006 OEXT/43124 GCSV/25307MW-5 EPA 3510 EPA 8082
92301747007 OEXT/43124 GCSV/25307MW-6R EPA 3510 EPA 8082
92301747008 OEXT/43124 GCSV/25307MW-8 EPA 3510 EPA 8082
92301747009 OEXT/43124 GCSV/25307MW-9S EPA 3510 EPA 8082
92301747010 OEXT/43124 GCSV/25307MW-9D EPA 3510 EPA 8082
92301747011 OEXT/43124 GCSV/25307MW-10 EPA 3510 EPA 8082
92301747012 OEXT/43124 GCSV/25307MW-11S EPA 3510 EPA 8082
92301747013 OEXT/43124 GCSV/25307MW-11D EPA 3510 EPA 8082
92301747014 OEXT/43124 GCSV/25307MW-12 EPA 3510 EPA 8082
92301747015 OEXT/43124 GCSV/25307MW-13 EPA 3510 EPA 8082
92301747001 OEXT/28682 GCSV/18710MW-1 EPA 8151 EPA 8151
92301747002 OEXT/28682 GCSV/18710MW-2 EPA 8151 EPA 8151
92301747003 OEXT/28682 GCSV/18710MW-3R EPA 8151 EPA 8151
92301747004 OEXT/28682 GCSV/18710MW-4S EPA 8151 EPA 8151
92301747005 OEXT/28682 GCSV/18710MW-4D EPA 8151 EPA 8151
92301747006 OEXT/28682 GCSV/18710MW-5 EPA 8151 EPA 8151
92301747007 OEXT/28682 GCSV/18710MW-6R EPA 8151 EPA 8151
92301747008 OEXT/28682 GCSV/18710MW-8 EPA 8151 EPA 8151
92301747009 OEXT/28682 GCSV/18710MW-9S EPA 8151 EPA 8151
92301747010 OEXT/28682 GCSV/18710MW-9D EPA 8151 EPA 8151
92301747011 OEXT/28682 GCSV/18710MW-10 EPA 8151 EPA 8151
92301747012 OEXT/28725 GCSV/18744MW-11S EPA 8151 EPA 8151
92301747013 OEXT/28725 GCSV/18744MW-11D EPA 8151 EPA 8151
92301747014 OEXT/28725 GCSV/18744MW-12 EPA 8151 EPA 8151
92301747015 OEXT/28725 GCSV/18744MW-13 EPA 8151 EPA 8151
92301747001 MPRP/22070 ICP/19750MW-1 EPA 3010A EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
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Huntersville, NC 28078
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Page 134 of 139
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92301747002 MPRP/22070 ICP/19750MW-2 EPA 3010A EPA 6010
92301747003 MPRP/22070 ICP/19750MW-3R EPA 3010A EPA 6010
92301747004 MPRP/22071 ICP/19749MW-4S EPA 3010A EPA 6010
92301747005 MPRP/22071 ICP/19749MW-4D EPA 3010A EPA 6010
92301747006 MPRP/22071 ICP/19749MW-5 EPA 3010A EPA 6010
92301747007 MPRP/22071 ICP/19749MW-6R EPA 3010A EPA 6010
92301747008 MPRP/22071 ICP/19749MW-8 EPA 3010A EPA 6010
92301747009 MPRP/22071 ICP/19749MW-9S EPA 3010A EPA 6010
92301747010 MPRP/22071 ICP/19749MW-9D EPA 3010A EPA 6010
92301747011 MPRP/22071 ICP/19749MW-10 EPA 3010A EPA 6010
92301747012 MPRP/22071 ICP/19749MW-11S EPA 3010A EPA 6010
92301747013 MPRP/22071 ICP/19749MW-11D EPA 3010A EPA 6010
92301747014 MPRP/22071 ICP/19749MW-12 EPA 3010A EPA 6010
92301747015 MPRP/22071 ICP/19749MW-13 EPA 3010A EPA 6010
92301747001 MERP/9633 MERC/9268MW-1 EPA 7470 EPA 7470
92301747002 MERP/9633 MERC/9268MW-2 EPA 7470 EPA 7470
92301747003 MERP/9633 MERC/9268MW-3R EPA 7470 EPA 7470
92301747004 MERP/9633 MERC/9268MW-4S EPA 7470 EPA 7470
92301747005 MERP/9633 MERC/9268MW-4D EPA 7470 EPA 7470
92301747006 MERP/9633 MERC/9268MW-5 EPA 7470 EPA 7470
92301747007 MERP/9633 MERC/9268MW-6R EPA 7470 EPA 7470
92301747008 MERP/9633 MERC/9268MW-8 EPA 7470 EPA 7470
92301747009 MERP/9633 MERC/9268MW-9S EPA 7470 EPA 7470
92301747010 MERP/9633 MERC/9268MW-9D EPA 7470 EPA 7470
92301747011 MERP/9633 MERC/9268MW-10 EPA 7470 EPA 7470
92301747012 MERP/9633 MERC/9268MW-11S EPA 7470 EPA 7470
92301747013 MERP/9633 MERC/9268MW-11D EPA 7470 EPA 7470
92301747014 MERP/9633 MERC/9268MW-12 EPA 7470 EPA 7470
92301747015 MERP/9633 MERC/9268MW-13 EPA 7470 EPA 7470
92301747001 OEXT/43142 MSSV/12410MW-1 EPA 3510 EPA 8270
92301747002 OEXT/43142 MSSV/12410MW-2 EPA 3510 EPA 8270
92301747003 OEXT/43142 MSSV/12410MW-3R EPA 3510 EPA 8270
92301747004 OEXT/43142 MSSV/12410MW-4S EPA 3510 EPA 8270
92301747005 OEXT/43142 MSSV/12410MW-4D EPA 3510 EPA 8270
92301747006 OEXT/43142 MSSV/12410MW-5 EPA 3510 EPA 8270
92301747007 OEXT/43142 MSSV/12410MW-6R EPA 3510 EPA 8270
92301747008 OEXT/43142 MSSV/12410MW-8 EPA 3510 EPA 8270
92301747009 OEXT/43142 MSSV/12410MW-9S EPA 3510 EPA 8270
92301747010 OEXT/43142 MSSV/12410MW-9D EPA 3510 EPA 8270
92301747011 OEXT/43142 MSSV/12410MW-10 EPA 3510 EPA 8270
92301747012 OEXT/43142 MSSV/12410MW-11S EPA 3510 EPA 8270
92301747013 OEXT/43142 MSSV/12410MW-11D EPA 3510 EPA 8270
92301747014 OEXT/43142 MSSV/12410MW-12 EPA 3510 EPA 8270
92301747015 OEXT/43142 MSSV/12410MW-13 EPA 3510 EPA 8270
92301747001 MSV/37336MW-1 EPA 8260
92301747002 MSV/37336MW-2 EPA 8260
92301747003 MSV/37336MW-3R EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
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[phone]
Page 135 of 139
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92301747
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92301747004 MSV/37336MW-4S EPA 8260
92301747005 MSV/37336MW-4D EPA 8260
92301747006 MSV/37336MW-5 EPA 8260
92301747007 MSV/37336MW-6R EPA 8260
92301747008 MSV/37336MW-8 EPA 8260
92301747009 MSV/37336MW-9S EPA 8260
92301747010 MSV/37336MW-9D EPA 8260
92301747011 MSV/37336MW-10 EPA 8260
92301747012 MSV/37336MW-11S EPA 8260
92301747013 MSV/37336MW-11D EPA 8260
92301747014 MSV/37336MW-12 EPA 8260
92301747015 MSV/37336MW-13 EPA 8260
92301747001 WET/45640MW-1 SM 4500-S2D
92301747002 WET/45640MW-2 SM 4500-S2D
92301747003 WET/45640MW-3R SM 4500-S2D
92301747004 WET/45640MW-4S SM 4500-S2D
92301747005 WET/45640MW-4D SM 4500-S2D
92301747006 WET/45640MW-5 SM 4500-S2D
92301747007 WET/45640MW-6R SM 4500-S2D
92301747008 WET/45640MW-8 SM 4500-S2D
92301747009 WET/45640MW-9S SM 4500-S2D
92301747010 WET/45641MW-9D SM 4500-S2D
92301747011 WET/45641MW-10 SM 4500-S2D
92301747012 WET/45641MW-11S SM 4500-S2D
92301747013 WET/45641MW-11D SM 4500-S2D
92301747014 WET/45641MW-12 SM 4500-S2D
92301747015 WET/45641MW-13 SM 4500-S2D
92301747001 WETA/27991MW-1 SM 4500-CN-E
92301747002 WETA/27991MW-2 SM 4500-CN-E
92301747003 WETA/27991MW-3R SM 4500-CN-E
92301747004 WETA/27991MW-4S SM 4500-CN-E
92301747005 WETA/27991MW-4D SM 4500-CN-E
92301747006 WETA/27991MW-5 SM 4500-CN-E
92301747007 WETA/27991MW-6R SM 4500-CN-E
92301747008 WETA/27991MW-8 SM 4500-CN-E
92301747009 WETA/27991MW-9S SM 4500-CN-E
92301747010 WETA/27991MW-9D SM 4500-CN-E
92301747011 WETA/27991MW-10 SM 4500-CN-E
92301747012 WETA/27991MW-11S SM 4500-CN-E
92301747013 WETA/27991MW-11D SM 4500-CN-E
92301747014 WETA/27991MW-12 SM 4500-CN-E
92301747015 WETA/27991MW-13 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 12:10 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 136 of 139
Page 137 of 139
Page 138 of 139
Page 139 of 139
#=CL#
July 01, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92301754
92301754
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CO. LINED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 16, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 27
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92301754001 LAGOON Water 06/15/16 15:34 06/16/16 08:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92301754001 LAGOON EPA 6010 16 PASI-AJMW, SH1
EPA 7470 1 PASI-ASER
EPA 8260 67 PASI-CNB
SM 5210B 1 PASI-AMLS
EPA 9040 1 PASI-AEWS
EPA 300.0 1 PASI-AMDW
EPA 353.2 1 PASI-ADMN
EPA 365.1 1 PASI-AWRC
SM 5220D 1 PASI-AWRC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Sample:LAGOON Lab ID:92301754001 Collected:06/15/16 15:34 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 4.8J ug/L 06/20/16 05:40 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 22:42 7440-38-206/17/16 21:0510.0 2.5 1
Barium 189 ug/L 06/20/16 22:42 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 22:42 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 22:42 7440-43-906/17/16 21:051.0 0.50 1
Chromium 13.3 ug/L 06/20/16 22:42 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt 9.9J ug/L 06/20/16 22:42 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 22:42 7440-50-806/17/16 21:0510.0 2.5 1
Lead 6.1J ug/L 06/20/16 22:42 7439-92-106/17/16 21:0510.0 2.5 1
Nickel 4.9J ug/L 06/20/16 22:42 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 22:42 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 22:42 7440-22-406/17/16 21:0510.0 2.5 1
Thallium 8.9 ug/L 06/20/16 22:42 7440-28-006/17/16 21:055.5 5.0 1
Tin ND ug/L 06/20/16 22:42 7440-31-506/17/16 21:051002.5 1
Vanadium ND ug/L 06/20/16 22:42 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 22:42 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/23/16 15:07 7439-97-606/21/16 18:110.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.6J ug/L 06/17/16 21:29 67-64-110010.0 1
Acetonitrile ND ug/L 06/17/16 21:29 75-05-855.0 2.2 1
Acrolein ND ug/L 06/17/16 21:29 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/17/16 21:29 107-13-12001.9 1
Allyl chloride ND ug/L 06/17/16 21:29 107-05-110.0 1.5 1
Benzene 3.5 ug/L 06/17/16 21:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 21:29 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 21:29 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 21:29 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 21:29 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 21:29 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 21:29 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 21:29 56-23-51.0 0.25 1
Chlorobenzene 0.38J ug/L 06/17/16 21:29 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 21:29 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 21:29 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 21:29 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/17/16 21:29 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 21:29 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 21:29 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 21:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 21:29 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 21:29 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/17/16 21:29 541-73-15.0 0.24 1
1,4-Dichlorobenzene 3.6 ug/L 06/17/16 21:29 106-46-71.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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[phone]
Page 5 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Sample:LAGOON Lab ID:92301754001 Collected:06/15/16 15:34 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 21:29 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/17/16 21:29 75-71-85.0 0.21 1
1,1-Dichloroethane 1.9J ug/L 06/17/16 21:29 75-34-35.0 0.32 1
1,2-Dichloroethane 4.6 ug/L 06/17/16 21:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 21:29 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 6.7 ug/L 06/17/16 21:29 156-59-25.0 0.19 1
trans-1,2-Dichloroethene 3.5J ug/L 06/17/16 21:29 156-60-55.0 0.49 1
1,2-Dichloropropane 1.1 ug/L 06/17/16 21:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/17/16 21:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/17/16 21:29 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/17/16 21:29 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 21:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 21:29 10061-02-61.0 0.26 1
Ethylbenzene 2.0 ug/L 06/17/16 21:29 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/17/16 21:29 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/17/16 21:29 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/17/16 21:29 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 21:29 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/17/16 21:29 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/17/16 21:29 126-98-71000.93 1
Methylene Chloride 3.8 ug/L 06/17/16 21:29 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 06/17/16 21:29 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 21:29 108-10-11000.33 1
Naphthalene 1.9J ug/L 06/17/16 21:29 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/17/16 21:29 107-12-01503.6 1
Styrene ND ug/L 06/17/16 21:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 21:29 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 21:29 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 21:29 127-18-41.0 0.46 1
Toluene 0.57J ug/L 06/17/16 21:29 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/17/16 21:29 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/17/16 21:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 21:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 21:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 21:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 21:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 21:29 108-05-450.0 0.35 1
Vinyl chloride 4.0 ug/L 06/17/16 21:29 75-01-41.0 0.62 1
Xylene (Total)2.6J ug/L 06/17/16 21:29 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %06/17/16 21:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 21:29 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 21:29 2037-26-570-130 1
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 36000 ug/L 06/22/16 08:49 B206/17/16 13:20200020001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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Page 6 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Sample:LAGOON Lab ID:92301754001 Collected:06/15/16 15:34 Received:06/16/16 08:06 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 90409040 pH
pH 6.2 Std. Units 06/30/16 17:55 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3950J ug/L 06/22/16 11:40 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 06/16/16 22:331000010.0 1
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus ND ug/L 06/22/16 15:23 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 114000 ug/L 06/22/16 18:3050000250002
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/9645
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1760108
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/23/16 14:390.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1760109LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1760110MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92302009004
1760111
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 104 75-12591 13 252.5ND 2.6 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/22071
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758286
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 06/20/16 04:323.8
Arsenic ug/L ND 10.0 06/20/16 21:432.5
Barium ug/L ND 100 06/20/16 21:432.5
Beryllium ug/L ND 1.0 06/20/16 21:430.50
Cadmium ug/L ND 1.0 06/20/16 21:430.50
Chromium ug/L ND 10.0 06/20/16 21:432.5
Cobalt ug/L ND 10.0 06/20/16 21:432.5
Copper ug/L ND 10.0 06/20/16 21:432.5
Lead ug/L ND 10.0 06/20/16 21:432.5
Nickel ug/L ND 50.0 06/20/16 21:432.5
Selenium ug/L ND 10.0 06/20/16 21:435.0
Silver ug/L ND 10.0 06/20/16 21:432.5
Thallium ug/L ND 5.5 06/20/16 21:435.0
Tin ug/L ND 100 06/20/16 21:432.5
Vanadium ug/L ND 25.0 06/20/16 21:432.5
Zinc ug/L 8.7J 10.0 06/20/16 21:435.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758287LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 542500 108 80-120
Arsenic ug/L 521500 104 80-120
Barium ug/L 530500 106 80-120
Beryllium ug/L 502500 100 80-120
Cadmium ug/L 545500 109 80-120
Chromium ug/L 525500 105 80-120
Cobalt ug/L 538500 108 80-120
Copper ug/L 519500 104 80-120
Lead ug/L 533500 107 80-120
Nickel ug/L 524500 105 80-120
Selenium ug/L 529500 106 80-120
Silver ug/L 255250 102 80-120
Thallium ug/L 509500 102 80-120
Tin ug/L 544500 109 80-120
Vanadium ug/L 514500 103 80-120
Zinc ug/L 531500 106 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758288MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301747004
1758289
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 106 75-125105 1 25500ND529523
Arsenic ug/L 500 102 75-125103 1 25500ND511516
Barium ug/L 500 105 75-125105 0 2550051.7J 579 578
Beryllium ug/L 500 101 75-125101 0 25500ND506505
Cadmium ug/L 500 107 75-125107 0 25500ND535535
Chromium ug/L 500 104 75-125105 1 25500ND522525
Cobalt ug/L 500 106 75-125106 0 25500ND529530
Copper ug/L 500 103 75-125104 1 25500ND517520
Lead ug/L 500 104 75-125105 0 25500ND522524
Nickel ug/L 500 104 75-125104 0 25500ND518520
Selenium ug/L 500 104 75-125104 0 25500ND520519
Silver ug/L 250 102 75-125103 1 25250ND255257
Thallium ug/L 500 99 75-125100 1 25500ND500505
Tin ug/L 500 107 75-125107 0 25500ND537537
Vanadium ug/L 500 104 75-125104 0 25500ND522523
Zinc ug/L 500 104 75-125104 0 25500ND522523
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/37336
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758547
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/17/16 13:300.33
1,1,1-Trichloroethane ug/L ND 1.0 06/17/16 13:300.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/17/16 13:300.40
1,1,2-Trichloroethane ug/L ND 1.0 06/17/16 13:300.29
1,1-Dichloroethane ug/L ND 5.0 06/17/16 13:300.32
1,1-Dichloroethene ug/L ND 5.0 06/17/16 13:300.56
1,1-Dichloropropene ug/L ND 5.0 06/17/16 13:300.49
1,2,3-Trichloropropane ug/L ND 1.0 06/17/16 13:300.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/17/16 13:300.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/17/16 13:302.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/17/16 13:300.27
1,2-Dichlorobenzene ug/L ND 5.0 06/17/16 13:300.30
1,2-Dichloroethane ug/L ND 1.0 06/17/16 13:300.24
1,2-Dichloropropane ug/L ND 1.0 06/17/16 13:300.27
1,3-Dichlorobenzene ug/L ND 5.0 06/17/16 13:300.24
1,3-Dichloropropane ug/L ND 1.0 06/17/16 13:300.28
1,4-Dichlorobenzene ug/L ND 1.0 06/17/16 13:300.33
2,2-Dichloropropane ug/L ND 15.0 06/17/16 13:300.13
2-Butanone (MEK)ug/L ND 100 06/17/16 13:300.96
2-Hexanone ug/L ND 50.0 06/17/16 13:300.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/17/16 13:300.33
Acetone ug/L ND 100 06/17/16 13:3010.0
Acetonitrile ug/L ND 55.0 06/17/16 13:302.2
Acrolein ug/L ND 53.0 06/17/16 13:301.6
Acrylonitrile ug/L ND 200 06/17/16 13:301.9
Allyl chloride ug/L ND 10.0 06/17/16 13:301.5
Benzene ug/L ND 1.0 06/17/16 13:300.25
Bromochloromethane ug/L ND 3.0 06/17/16 13:300.17
Bromodichloromethane ug/L ND 1.0 06/17/16 13:300.18
Bromoform ug/L ND 3.0 06/17/16 13:300.26
Bromomethane ug/L ND 10.0 06/17/16 13:300.29
Carbon disulfide ug/L ND 100 06/17/16 13:301.2
Carbon tetrachloride ug/L ND 1.0 06/17/16 13:300.25
Chlorobenzene ug/L ND 3.0 06/17/16 13:300.23
Chloroethane ug/L ND 10.0 06/17/16 13:300.54
Chloroform ug/L ND 5.0 06/17/16 13:300.14
Chloromethane ug/L ND 1.0 06/17/16 13:300.11
Chloroprene ug/L ND 20.0 06/17/16 13:300.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/17/16 13:300.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/17/16 13:300.13
Dibromochloromethane ug/L ND 3.0 06/17/16 13:300.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758547
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/17/16 13:300.21
Dichlorodifluoromethane ug/L ND 5.0 06/17/16 13:300.21
Ethyl methacrylate ug/L ND 10.0 06/17/16 13:300.20
Ethylbenzene ug/L ND 1.0 06/17/16 13:300.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/17/16 13:300.71
Iodomethane ug/L ND 10.0 06/17/16 13:300.32
Isobutanol ug/L ND 100 06/17/16 13:3035.0
Methacrylonitrile ug/L ND 100 06/17/16 13:300.93
Methyl methacrylate ug/L ND 30.0 06/17/16 13:302.0
Methylene Chloride ug/L ND 1.0 06/17/16 13:300.97
Naphthalene ug/L ND 10.0 06/17/16 13:300.24
Propionitrile ug/L ND 150 06/17/16 13:303.6
Styrene ug/L ND 1.0 06/17/16 13:300.26
Tetrachloroethene ug/L ND 1.0 06/17/16 13:300.46
Toluene ug/L ND 1.0 06/17/16 13:300.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/17/16 13:300.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/17/16 13:300.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/17/16 13:301.0
Trichloroethene ug/L ND 1.0 06/17/16 13:300.47
Trichlorofluoromethane ug/L ND 1.0 06/17/16 13:300.20
Vinyl acetate ug/L ND 50.0 06/17/16 13:300.35
Vinyl chloride ug/L ND 1.0 06/17/16 13:300.62
Xylene (Total)ug/L ND 5.0 06/17/16 13:300.66
1,2-Dichloroethane-d4 (S)%95 70-130 06/17/16 13:30
4-Bromofluorobenzene (S)%96 70-130 06/17/16 13:30
Toluene-d8 (S)%99 70-130 06/17/16 13:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758548LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.750 93 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 47.250 94 79-124
1,1,2-Trichloroethane ug/L 47.650 95 85-125
1,1-Dichloroethane ug/L 47.750 95 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,1-Dichloropropene ug/L 46.450 93 74-135
1,2,3-Trichloropropane ug/L 45.450 91 75-130
1,2,4-Trichlorobenzene ug/L 52.150 104 75-134
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 51.450 103 83-124
1,2-Dichlorobenzene ug/L 51.050 102 80-133
1,2-Dichloroethane ug/L 42.450 85 67-128
1,2-Dichloropropane ug/L 46.050 92 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758548LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.850 98 77-130
1,3-Dichloropropane ug/L 44.950 90 76-131
1,4-Dichlorobenzene ug/L 48.050 96 78-130
2,2-Dichloropropane ug/L 50.350 101 40-160
2-Butanone (MEK)ug/L 90.7J100 91 61-144
2-Hexanone ug/L 95.2100 95 68-143
4-Methyl-2-pentanone (MIBK)ug/L 90.6J100 91 72-135
Acetone ug/L 87.3J100 87 48-146
Acetonitrile ug/L 447500 89 62-150
Acrolein ug/L 181250 72 24-160
Acrylonitrile ug/L 242250 97 40-160
Allyl chloride ug/L 48.950 98 66-137
Benzene ug/L 48.550 97 80-125
Bromochloromethane ug/L 50.950 102 71-125
Bromodichloromethane ug/L 51.950 104 78-124
Bromoform ug/L 45.850 92 71-128
Bromomethane ug/L 47.350 95 40-160
Carbon disulfide ug/L 51.4J50 103 50-160
Carbon tetrachloride ug/L 51.050 102 69-131
Chlorobenzene ug/L 47.650 95 81-122
Chloroethane ug/L 42.750 85 39-148
Chloroform ug/L 47.450 95 73-127
Chloromethane ug/L 49.150 98 44-146
Chloroprene ug/L 46.550 93 75-145
cis-1,2-Dichloroethene ug/L 47.950 96 74-124
cis-1,3-Dichloropropene ug/L 49.950 100 72-132
Dibromochloromethane ug/L 47.950 96 78-125
Dibromomethane ug/L 46.550 93 82-120
Dichlorodifluoromethane ug/L 39.550 79 34-157
Ethyl methacrylate ug/L 46.450 93 82-121
Ethylbenzene ug/L 47.550 95 79-121
Hexachloro-1,3-butadiene ug/L 53.250 106 72-131
Iodomethane ug/L 114100 114 39-154
Isobutanol ug/L 11601000 116 34-160
Methacrylonitrile ug/L 448500 90 74-134
Methyl methacrylate ug/L 48.650 97 84-124
Methylene Chloride ug/L 45.950 92 64-133
Naphthalene ug/L 48.950 98 73-133
Propionitrile ug/L 474500 95 73-140
Styrene ug/L 49.150 98 84-126
Tetrachloroethene ug/L 45.150 90 78-122
Toluene ug/L 48.350 97 80-121
trans-1,2-Dichloroethene ug/L 48.750 97 71-127
trans-1,3-Dichloropropene ug/L 48.050 96 69-141
trans-1,4-Dichloro-2-butene ug/L 59.7J50 119 40-160
Trichloroethene ug/L 46.450 93 78-122
Trichlorofluoromethane ug/L 45.050 90 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758548LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 46.050 92 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758549MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747001
1,1,1,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,1-Trichloroethane ug/L 23.120 116 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.520 103 70-130ND
1,1,2-Trichloroethane ug/L 20.120 101 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 23.220 116 70-166ND
1,1-Dichloropropene ug/L 21.720 109 70-130ND
1,2,3-Trichloropropane ug/L 19.820 99 70-130ND
1,2,4-Trichlorobenzene ug/L 21.320 106 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.420 112 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.520 112 70-130ND
1,2-Dichlorobenzene ug/L 22.120 111 70-130ND
1,2-Dichloroethane ug/L 19.220 95 70-130ND
1,2-Dichloropropane ug/L 20.320 102 70-130ND
1,3-Dichlorobenzene ug/L 21.620 108 70-130ND
1,3-Dichloropropane ug/L 20.120 101 70-130ND
1,4-Dichlorobenzene ug/L 20.820 104 70-130ND
2,2-Dichloropropane ug/L 21.120 106 70-130ND
2-Butanone (MEK)ug/L 38.4J40 96 70-130ND
2-Hexanone ug/L 39.8J40 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.0J40 93 70-130ND
Acetone ug/L 38.7J40 97 70-130ND
Acetonitrile ug/L 197200 99 70-130ND
Acrolein ug/L 91.3100 91 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 21.620 108 70-130ND
Benzene ug/L 21.620 108 70-148ND
Bromochloromethane ug/L 22.420 112 70-130ND
Bromodichloromethane ug/L 21.820 109 70-130ND
Bromoform ug/L 21.920 110 70-130ND
Bromomethane ug/L 25.920 129 70-130ND
Carbon disulfide ug/L 22.8J20 114 70-130ND
Carbon tetrachloride ug/L 24.820 124 70-130ND
Chlorobenzene ug/L 21.620 108 70-146ND
Chloroethane ug/L 20.520 103 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758549MATRIX SPIKE SAMPLE:
MSSpike
Result
92301747001
Chloroform ug/L 21.120 105 70-130ND
Chloromethane ug/L 22.820 114 70-130ND
Chloroprene ug/L 21.120 106 70-130ND
cis-1,2-Dichloroethene ug/L 21.720 109 70-130ND
cis-1,3-Dichloropropene ug/L 20.320 101 70-130ND
Dibromochloromethane ug/L 21.920 109 70-130ND
Dibromomethane ug/L 20.120 101 70-130ND
Dichlorodifluoromethane ug/L 17.620 88 70-130ND
Ethyl methacrylate ug/L 21.220 106 70-130ND
Ethylbenzene ug/L 21.520 107 70-130ND
Hexachloro-1,3-butadiene ug/L 21.520 108 70-130ND
Iodomethane ug/L 55.4 M14013970-130ND
Isobutanol ug/L 470400 118 70-130ND
Methacrylonitrile ug/L 192200 96 70-130ND
Methyl methacrylate ug/L 21.1J20 105 70-130ND
Methylene Chloride ug/L 21.120 102 70-130ND
Naphthalene ug/L 20.120 101 70-130ND
Propionitrile ug/L 192200 96 70-130ND
Styrene ug/L 21.920 110 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 21.420 107 70-155ND
trans-1,2-Dichloroethene ug/L 22.420 112 70-130ND
trans-1,3-Dichloropropene ug/L 19.520 98 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.2J20 76 70-130ND
Trichloroethene ug/L 21.020 105 69-151ND
Trichlorofluoromethane ug/L 21.720 108 70-130ND
Vinyl acetate ug/L 40.1J40 100 70-130ND
Vinyl chloride ug/L 21.420 107 70-130ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747002
1758550SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 2.7J 0 302.7J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747002
1758550SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 1.7J 0 301.7J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 0.67J 300.64J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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Page 16 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301747002
1758550SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 0.48J 300.49J
Trichlorofluoromethane ug/L 0.21J 300.22J
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%93 497
4-Bromofluorobenzene (S)%97 298
Toluene-d8 (S)%99 1100
REPORT OF LABORATORY ANALYSIS
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Page 17 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/45587
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758066
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 06/22/16 08:492000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758067LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 218000198000 110 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301510001
1758068SAMPLE DUPLICATE:
BOD, 5 day ug/L 5490000 2 105590 mg/L
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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[phone]
Page 18 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/45895
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92301754001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301754001
1768326SAMPLE DUPLICATE:
pH Std. Units 6.2 H6096.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92302154003
1768327SAMPLE DUPLICATE:
pH Std. Units 6.8 H6096.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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[phone]
Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/28034
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1761159
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 06/22/16 09:111000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1761160LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 20200J20000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1761161MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301165008
1761162
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 103 90-110105 1 10200006.5 mg/L 27100J 27400J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1761163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301938001
1761164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 98 90-11098 0 10200005330J24900J25000J
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 20 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/27983
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1757926
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 06/16/16 22:1710.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1757927LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 26102500 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1757928MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301640001
1757929
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M1250011090-110113 1 1025006.5 mg/L 9230 9300
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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Huntersville, NC 28078
[phone]
Page 21 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/28029
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1760465
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Phosphorus ug/L ND 50.0 06/22/16 15:0125.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1760466LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 26202500 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1760467MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301789002
1760468
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 101 90-110104 3 1025000.12 mg/L 2640 2720
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1760469MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301476001
1760470
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 100 90-11098 1 1025002.0 mg/L 4540 4490
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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[phone]
Page 22 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/28049
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92301754001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1761910
Associated Lab Samples:92301754001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 06/22/16 18:3012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1761911LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 702000750000 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1761912MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301874001
1761913
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 30000000 91 90-11091 0 33000000011500
mg/L
3880000
0
3880000
0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1761914MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301726002
1761915
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 99 90-11099 0 3750000228 mg/L 971000 971000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/01/2016 04:38 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 23 of 27
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
Common Laboratory Contaminant.C9
Analysis initiated outside of the 15 minute EPA required holding time.H6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 24 of 27
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92301754
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92301754001 MPRP/22071 ICP/19749LAGOONEPA 3010A EPA 6010
92301754001 MERP/9645 MERC/9283LAGOONEPA 7470 EPA 7470
92301754001 MSV/37336LAGOONEPA 8260
92301754001 WET/45587 WET/45595LAGOONSM 5210B SM 5210B
92301754001 WET/45895LAGOONEPA 9040
92301754001 WETA/28034LAGOONEPA 300.0
92301754001 WETA/27983LAGOONEPA 353.2
92301754001 WETA/28029LAGOONEPA 365.1
92301754001 WETA/28049LAGOONSM 5220D
REPORT OF LABORATORY ANALYSIS
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Page 25 of 27
Page 26 of 27
Page 27 of 27
#=CL#
June 24, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92301667
92301667
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY MSWLF SWS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 16, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Lab ID Sample ID Matrix Date Collected Date Received
92301667001 SW-1 Water 06/15/16 16:00 06/16/16 11:35
92301667002 SW-2 Water 06/15/16 15:45 06/16/16 11:35
92301667003 SW-3 Water 06/14/16 15:10 06/16/16 11:35
92301667004 SW-4 Water 06/14/16 16:05 06/16/16 11:35
92301667005 SWN-1 Water 06/15/16 14:50 06/16/16 11:35
92301667006 SWN-2 Water 06/15/16 10:05 06/16/16 11:35
92301667007 SW-A Water 06/15/16 09:10 06/16/16 11:35
92301667008 SW-B Water 06/15/16 08:05 06/16/16 11:35
REPORT OF LABORATORY ANALYSIS
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Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92301667001 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667002 SW-2 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667003 SW-3 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667004 SW-4 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667005 SWN-1 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667006 SWN-2 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667007 SW-A EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
92301667008 SW-B EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-1 Lab ID:92301667001 Collected:06/15/16 16:00 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 16:44 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 20:50 7440-38-206/17/16 21:0510.0 2.5 1
Barium 23.1J ug/L 06/20/16 20:50 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 20:50 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 20:50 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 20:50 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 20:50 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 20:50 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 20:50 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 20:50 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 20:50 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 20:50 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 20:50 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 20:50 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 20:50 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 14:04 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 14:04 107-13-12001.9 1
Benzene ND ug/L 06/17/16 14:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 14:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 14:04 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 14:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 14:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 14:04 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 14:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 14:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 14:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 14:04 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 14:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 14:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 14:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 14:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 14:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 14:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 14:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 14:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 14:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 14:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 14:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 14:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 14:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 14:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 14:04 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 14:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 14:04 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-1 Lab ID:92301667001 Collected:06/15/16 16:00 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 14:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 14:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 14:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 14:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 14:04 108-10-11000.33 1
Styrene ND ug/L 06/17/16 14:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 14:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 14:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 14:04 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 14:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 14:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 14:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 14:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 14:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 14:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 14:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 14:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 14:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 14:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 14:04 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 14:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-2 Lab ID:92301667002 Collected:06/15/16 15:45 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 16:48 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:03 7440-38-206/17/16 21:0510.0 2.5 1
Barium 24.4J ug/L 06/20/16 21:03 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:03 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:03 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:03 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:03 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:03 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:03 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:03 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:03 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:03 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:03 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:03 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:03 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 14:22 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 14:22 107-13-12001.9 1
Benzene ND ug/L 06/17/16 14:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 14:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 14:22 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 14:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 14:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 14:22 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 14:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 14:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 14:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 14:22 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 14:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 14:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 14:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 14:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 14:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 14:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 14:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 14:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 14:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 14:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 14:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 14:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 14:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 14:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 14:22 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 14:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 14:22 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-2 Lab ID:92301667002 Collected:06/15/16 15:45 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 14:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 14:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 14:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 14:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 14:22 108-10-11000.33 1
Styrene ND ug/L 06/17/16 14:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 14:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 14:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 14:22 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 14:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 14:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 14:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 14:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 14:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 14:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 14:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 14:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 14:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 14:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 14:22 17060-07-070-130 1
Toluene-d8 (S)101 %06/17/16 14:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-3 Lab ID:92301667003 Collected:06/14/16 15:10 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 16:51 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:06 7440-38-206/17/16 21:0510.0 2.5 1
Barium 15.6J ug/L 06/20/16 21:06 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:06 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:06 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:06 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:06 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:06 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:06 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:06 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:06 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:06 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:06 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:06 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:06 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 14:56 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 14:56 107-13-12001.9 1
Benzene ND ug/L 06/17/16 14:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 14:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 14:56 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 14:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 14:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 14:56 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 14:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 14:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 14:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 14:56 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 14:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 14:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 14:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 14:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 14:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 14:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 14:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 14:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 14:56 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 14:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 14:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 14:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 14:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 14:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 14:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 14:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 14:56 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-3 Lab ID:92301667003 Collected:06/14/16 15:10 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 14:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 14:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 14:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 14:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 14:56 108-10-11000.33 1
Styrene ND ug/L 06/17/16 14:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 14:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 14:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 14:56 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 14:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 14:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 14:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 14:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 14:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 14:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 14:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 14:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 14:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 14:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 14:56 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 14:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-4 Lab ID:92301667004 Collected:06/14/16 16:05 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 16:54 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:09 7440-38-206/17/16 21:0510.0 2.5 1
Barium 15.9J ug/L 06/20/16 21:09 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:09 7440-41-706/17/16 21:051.0 0.50 1
Cadmium 0.59J ug/L 06/20/16 21:09 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/24/16 14:53 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:09 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:09 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:09 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:09 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:09 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:09 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:09 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:09 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 7.1J ug/L 06/20/16 21:09 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 15:13 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 15:13 107-13-12001.9 1
Benzene ND ug/L 06/17/16 15:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 15:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 15:13 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 15:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 15:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 15:13 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 15:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 15:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 15:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 15:13 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 15:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 15:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 15:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 15:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 15:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 15:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 15:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 15:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 15:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 15:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 15:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 15:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 15:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 15:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 15:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 15:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 15:13 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-4 Lab ID:92301667004 Collected:06/14/16 16:05 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 15:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 15:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 15:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 15:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 15:13 108-10-11000.33 1
Styrene ND ug/L 06/17/16 15:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 15:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 15:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 15:13 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 15:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 15:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 15:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 15:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 15:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 15:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 15:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 15:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 15:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 15:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 15:13 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 15:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SWN-1 Lab ID:92301667005 Collected:06/15/16 14:50 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 16:57 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:12 7440-38-206/17/16 21:0510.0 2.5 1
Barium 16.8J ug/L 06/20/16 21:12 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:12 7440-41-706/17/16 21:051.0 0.50 1
Cadmium 1.3 ug/L 06/20/16 21:12 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:12 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:12 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:12 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:12 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:12 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:12 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:12 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:12 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:12 7440-62-206/17/16 21:0525.0 2.5 1
Zinc 13.8 ug/L 06/20/16 21:12 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 15:30 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 15:30 107-13-12001.9 1
Benzene ND ug/L 06/17/16 15:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 15:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 15:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 15:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 15:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 15:30 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 15:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 15:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 15:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 15:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 15:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 15:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 15:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 15:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 15:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 15:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 15:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 15:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 15:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 15:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 15:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 15:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 15:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 15:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 15:30 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 15:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 15:30 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SWN-1 Lab ID:92301667005 Collected:06/15/16 14:50 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 15:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 15:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 15:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 15:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 15:30 108-10-11000.33 1
Styrene ND ug/L 06/17/16 15:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 15:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 15:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 15:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 15:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 15:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 15:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 15:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 15:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 15:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 15:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 15:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 15:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 15:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %06/17/16 15:30 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 15:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SWN-2 Lab ID:92301667006 Collected:06/15/16 10:05 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 17:00 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:15 7440-38-206/17/16 21:0510.0 2.5 1
Barium 24.0J ug/L 06/20/16 21:15 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:15 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:15 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:15 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:15 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:15 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:15 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:15 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:15 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:15 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:15 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:15 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:15 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 15:47 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 15:47 107-13-12001.9 1
Benzene ND ug/L 06/17/16 15:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 15:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 15:47 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 15:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 15:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 15:47 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 15:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 15:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 15:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 15:47 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 15:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 15:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 15:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 15:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 15:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 15:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 15:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 15:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 15:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 15:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 15:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 15:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 15:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 15:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 15:47 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 15:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 15:47 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SWN-2 Lab ID:92301667006 Collected:06/15/16 10:05 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 15:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 15:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 15:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 15:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 15:47 108-10-11000.33 1
Styrene ND ug/L 06/17/16 15:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 15:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 15:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 15:47 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 15:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 15:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 15:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 15:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 15:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 15:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 15:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 15:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 15:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %06/17/16 15:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 15:47 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 15:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-A Lab ID:92301667007 Collected:06/15/16 09:10 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 17:03 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:19 7440-38-206/17/16 21:0510.0 2.5 1
Barium 23.8J ug/L 06/20/16 21:19 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:19 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:19 7440-43-906/17/16 21:051.0 0.50 1
Chromium 3.0J ug/L 06/20/16 21:19 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:19 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:19 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:19 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:19 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:19 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:19 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:19 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:19 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:19 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 16:04 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 16:04 107-13-12001.9 1
Benzene ND ug/L 06/17/16 16:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 16:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 16:04 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 16:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 16:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 16:04 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 16:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 16:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 16:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 16:04 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 16:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 16:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 16:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 16:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 16:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 16:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 16:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 16:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 16:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 16:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 16:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 16:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 16:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 16:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 16:04 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 16:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 16:04 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-A Lab ID:92301667007 Collected:06/15/16 09:10 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 16:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 16:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 16:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 16:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 16:04 108-10-11000.33 1
Styrene ND ug/L 06/17/16 16:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 16:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 16:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 16:04 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 16:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 16:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 16:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 16:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 16:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 16:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 16:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 16:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 16:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 16:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/17/16 16:04 17060-07-070-130 1
Toluene-d8 (S)99 %06/17/16 16:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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[phone]
Page 18 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-B Lab ID:92301667008 Collected:06/15/16 08:05 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/21/16 17:06 7440-36-006/17/16 21:056.0 3.8 1
Arsenic ND ug/L 06/20/16 21:22 7440-38-206/17/16 21:0510.0 2.5 1
Barium 23.5J ug/L 06/20/16 21:22 7440-39-306/17/16 21:051002.5 1
Beryllium ND ug/L 06/20/16 21:22 7440-41-706/17/16 21:051.0 0.50 1
Cadmium ND ug/L 06/20/16 21:22 7440-43-906/17/16 21:051.0 0.50 1
Chromium ND ug/L 06/20/16 21:22 7440-47-306/17/16 21:0510.0 2.5 1
Cobalt ND ug/L 06/20/16 21:22 7440-48-406/17/16 21:0510.0 2.5 1
Copper ND ug/L 06/20/16 21:22 7440-50-806/17/16 21:0510.0 2.5 1
Lead ND ug/L 06/20/16 21:22 7439-92-106/17/16 21:0510.0 2.5 1
Nickel ND ug/L 06/20/16 21:22 7440-02-006/17/16 21:0550.0 2.5 1
Selenium ND ug/L 06/20/16 21:22 7782-49-206/17/16 21:0510.0 5.0 1
Silver ND ug/L 06/20/16 21:22 7440-22-406/17/16 21:0510.0 2.5 1
Thallium ND ug/L 06/20/16 21:22 7440-28-006/17/16 21:055.5 5.0 1
Vanadium ND ug/L 06/20/16 21:22 7440-62-206/17/16 21:0525.0 2.5 1
Zinc ND ug/L 06/20/16 21:22 7440-66-606/17/16 21:0510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/17/16 16:21 67-64-110010.0 1
Acrylonitrile ND ug/L 06/17/16 16:21 107-13-12001.9 1
Benzene ND ug/L 06/17/16 16:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/17/16 16:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/17/16 16:21 75-27-41.0 0.18 1
Bromoform ND ug/L 06/17/16 16:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/17/16 16:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/17/16 16:21 78-93-31000.96 1
Carbon disulfide ND ug/L 06/17/16 16:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/17/16 16:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/17/16 16:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/17/16 16:21 75-00-310.0 0.54 1
Chloroform ND ug/L 06/17/16 16:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/17/16 16:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/16 16:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/17/16 16:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/16 16:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/17/16 16:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/17/16 16:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/17/16 16:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/17/16 16:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/17/16 16:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/17/16 16:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/17/16 16:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/17/16 16:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/17/16 16:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/17/16 16:21 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/17/16 16:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/17/16 16:21 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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Page 19 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Sample:SW-B Lab ID:92301667008 Collected:06/15/16 08:05 Received:06/16/16 11:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 06/17/16 16:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/17/16 16:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/17/16 16:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/17/16 16:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/16 16:21 108-10-11000.33 1
Styrene ND ug/L 06/17/16 16:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/16 16:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/16 16:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/17/16 16:21 127-18-41.0 0.46 1
Toluene ND ug/L 06/17/16 16:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/17/16 16:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/17/16 16:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/17/16 16:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/17/16 16:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/17/16 16:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/17/16 16:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/17/16 16:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/17/16 16:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/16 16:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/17/16 16:21 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/16 16:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/22070
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92301667001, 92301667002, 92301667003, 92301667004, 92301667005, 92301667006, 92301667007,
92301667008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758278
Associated Lab Samples:92301667001, 92301667002, 92301667003, 92301667004, 92301667005, 92301667006, 92301667007,
92301667008
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 06/21/16 16:043.8
Arsenic ug/L ND 10.0 06/20/16 20:012.5
Barium ug/L ND 100 06/20/16 20:012.5
Beryllium ug/L ND 1.0 06/20/16 20:010.50
Cadmium ug/L ND 1.0 06/20/16 20:010.50
Chromium ug/L ND 10.0 06/24/16 14:472.5
Cobalt ug/L ND 10.0 06/20/16 20:012.5
Copper ug/L ND 10.0 06/20/16 20:012.5
Lead ug/L ND 10.0 06/20/16 20:012.5
Nickel ug/L ND 50.0 06/20/16 20:012.5
Selenium ug/L ND 10.0 06/20/16 20:015.0
Silver ug/L ND 10.0 06/20/16 20:012.5
Thallium ug/L ND 5.5 06/20/16 20:015.0
Vanadium ug/L ND 25.0 06/20/16 20:012.5
Zinc ug/L ND 10.0 06/20/16 20:015.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758279LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 523500 105 80-120
Arsenic ug/L 513500 103 80-120
Barium ug/L 525500 105 80-120
Beryllium ug/L 503500 101 80-120
Cadmium ug/L 537500 107 80-120
Chromium ug/L 518500 104 80-120
Cobalt ug/L 533500 107 80-120
Copper ug/L 514500 103 80-120
Lead ug/L 526500 105 80-120
Nickel ug/L 520500 104 80-120
Selenium ug/L 524500 105 80-120
Silver ug/L 257250 103 80-120
Thallium ug/L 505500 101 80-120
Vanadium ug/L 520500 104 80-120
Zinc ug/L 522500 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1758280MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301640001
1758281
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125103 0 25500ND517516
Arsenic ug/L 500 111 75-125100 10 25500ND556504
Barium ug/L 500 111 75-125103 6 25500111666626
Beryllium ug/L 500 106 75-12599 6 25500ND530497
Cadmium ug/L 500 115 75-125105 10 25500ND575523
Chromium ug/L 500 103 75-125102 1 25500ND516513
Cobalt ug/L 500 115 75-125104 9 255004.7J 578 526
Copper ug/L 500 102 75-125101 1 25500ND509505
Lead ug/L 500 113 75-125103 10 25500ND568515
Nickel ug/L 500 112 75-125102 9 255003.8J 562 514
Selenium ug/L 500 111 75-125102 8 25500ND554510
Silver ug/L 250 101 75-125101 0 25250ND252252
Thallium ug/L 500 108 75-12598 9 25500ND541493
Vanadium ug/L 500 102 75-125102 0 255004.6J 514 517
Zinc ug/L 500 112 75-125102 9 2550012.1 573 522
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/37327
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92301667001, 92301667002, 92301667003, 92301667004, 92301667005, 92301667006, 92301667007,
92301667008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758196
Associated Lab Samples:92301667001, 92301667002, 92301667003, 92301667004, 92301667005, 92301667006, 92301667007,
92301667008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/17/16 13:130.33
1,1,1-Trichloroethane ug/L ND 1.0 06/17/16 13:130.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/17/16 13:130.40
1,1,2-Trichloroethane ug/L ND 1.0 06/17/16 13:130.29
1,1-Dichloroethane ug/L ND 5.0 06/17/16 13:130.32
1,1-Dichloroethene ug/L ND 5.0 06/17/16 13:130.56
1,2,3-Trichloropropane ug/L ND 1.0 06/17/16 13:130.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/17/16 13:132.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/17/16 13:130.27
1,2-Dichlorobenzene ug/L ND 5.0 06/17/16 13:130.30
1,2-Dichloroethane ug/L ND 1.0 06/17/16 13:130.24
1,2-Dichloropropane ug/L ND 1.0 06/17/16 13:130.27
1,4-Dichlorobenzene ug/L ND 1.0 06/17/16 13:130.33
2-Butanone (MEK)ug/L ND 100 06/17/16 13:130.96
2-Hexanone ug/L ND 50.0 06/17/16 13:130.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/17/16 13:130.33
Acetone ug/L ND 100 06/17/16 13:1310.0
Acrylonitrile ug/L ND 200 06/17/16 13:131.9
Benzene ug/L ND 1.0 06/17/16 13:130.25
Bromochloromethane ug/L ND 3.0 06/17/16 13:130.17
Bromodichloromethane ug/L ND 1.0 06/17/16 13:130.18
Bromoform ug/L ND 3.0 06/17/16 13:130.26
Bromomethane ug/L ND 10.0 06/17/16 13:130.29
Carbon disulfide ug/L ND 100 06/17/16 13:131.2
Carbon tetrachloride ug/L ND 1.0 06/17/16 13:130.25
Chlorobenzene ug/L ND 3.0 06/17/16 13:130.23
Chloroethane ug/L ND 10.0 06/17/16 13:130.54
Chloroform ug/L ND 5.0 06/17/16 13:130.14
Chloromethane ug/L ND 1.0 06/17/16 13:130.11
cis-1,2-Dichloroethene ug/L ND 5.0 06/17/16 13:130.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/17/16 13:130.13
Dibromochloromethane ug/L ND 3.0 06/17/16 13:130.21
Dibromomethane ug/L ND 10.0 06/17/16 13:130.21
Ethylbenzene ug/L ND 1.0 06/17/16 13:130.30
Iodomethane ug/L ND 10.0 06/17/16 13:130.32
Methylene Chloride ug/L ND 1.0 06/17/16 13:130.97
Styrene ug/L ND 1.0 06/17/16 13:130.26
Tetrachloroethene ug/L ND 1.0 06/17/16 13:130.46
Toluene ug/L ND 1.0 06/17/16 13:130.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/17/16 13:130.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1758196
Associated Lab Samples:92301667001, 92301667002, 92301667003, 92301667004, 92301667005, 92301667006, 92301667007,
92301667008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 06/17/16 13:130.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/17/16 13:131.0
Trichloroethene ug/L ND 1.0 06/17/16 13:130.47
Trichlorofluoromethane ug/L ND 1.0 06/17/16 13:130.20
Vinyl acetate ug/L ND 50.0 06/17/16 13:130.35
Vinyl chloride ug/L ND 1.0 06/17/16 13:130.62
Xylene (Total)ug/L ND 5.0 06/17/16 13:130.66
1,2-Dichloroethane-d4 (S)%96 70-130 06/17/16 13:13
4-Bromofluorobenzene (S)%97 70-130 06/17/16 13:13
Toluene-d8 (S)%100 70-130 06/17/16 13:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758197LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.950 94 80-125
1,1,1-Trichloroethane ug/L 50.650 101 71-129
1,1,2,2-Tetrachloroethane ug/L 47.450 95 79-124
1,1,2-Trichloroethane ug/L 46.350 93 85-125
1,1-Dichloroethane ug/L 47.050 94 73-126
1,1-Dichloroethene ug/L 49.650 99 66-135
1,2,3-Trichloropropane ug/L 45.350 91 75-130
1,2-Dibromo-3-chloropropane ug/L 50.350 101 71-133
1,2-Dibromoethane (EDB)ug/L 50.650 101 83-124
1,2-Dichlorobenzene ug/L 50.250 100 80-133
1,2-Dichloroethane ug/L 41.150 82 67-128
1,2-Dichloropropane ug/L 45.850 92 75-132
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2-Butanone (MEK)ug/L 90.5J100 90 61-144
2-Hexanone ug/L 95.1100 95 68-143
4-Methyl-2-pentanone (MIBK)ug/L 89.5J100 90 72-135
Acetone ug/L 85.7J100 86 48-146
Acrylonitrile ug/L 240250 96 40-160
Benzene ug/L 48.350 97 80-125
Bromochloromethane ug/L 50.450 101 71-125
Bromodichloromethane ug/L 50.250 100 78-124
Bromoform ug/L 45.650 91 71-128
Bromomethane ug/L 47.850 96 40-160
Carbon disulfide ug/L 51.4J50 103 50-160
Carbon tetrachloride ug/L 50.450 101 69-131
Chlorobenzene ug/L 47.950 96 81-122
Chloroethane ug/L 43.850 88 39-148
Chloroform ug/L 47.550 95 73-127
Chloromethane ug/L 48.450 97 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1758197LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 47.850 96 74-124
cis-1,3-Dichloropropene ug/L 48.750 97 72-132
Dibromochloromethane ug/L 47.150 94 78-125
Dibromomethane ug/L 45.250 90 82-120
Ethylbenzene ug/L 47.450 95 79-121
Iodomethane ug/L 112100 112 39-154
Methylene Chloride ug/L 45.650 91 64-133
Styrene ug/L 49.550 99 84-126
Tetrachloroethene ug/L 45.050 90 78-122
Toluene ug/L 47.950 96 80-121
trans-1,2-Dichloroethene ug/L 48.750 97 71-127
trans-1,3-Dichloropropene ug/L 47.950 96 69-141
trans-1,4-Dichloro-2-butene ug/L 58.0J50 116 40-160
Trichloroethene ug/L 46.050 92 78-122
Trichlorofluoromethane ug/L 45.350 91 53-137
Vinyl acetate ug/L 104100 104 40-160
Vinyl chloride ug/L 46.050 92 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758198MATRIX SPIKE SAMPLE:
MSSpike
Result
92301667001
1,1,1,2-Tetrachloroethane ug/L 21.320 107 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.820 99 70-130ND
1,1,2-Trichloroethane ug/L 19.920 99 70-130ND
1,1-Dichloroethane ug/L 21.120 105 70-130ND
1,1-Dichloroethene ug/L 22.720 114 70-166ND
1,2,3-Trichloropropane ug/L 18.920 95 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.220 106 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.620 108 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 18.620 92 70-130ND
1,2-Dichloropropane ug/L 20.120 100 70-130ND
1,4-Dichlorobenzene ug/L 20.220 101 70-130ND
2-Butanone (MEK)ug/L 37.4J40 93 70-130ND
2-Hexanone ug/L 37.6J40 94 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 36.3J40 91 70-130ND
Acetone ug/L 36.5J40 87 70-130ND
Acrylonitrile ug/L 101J100 101 70-130ND
Benzene ug/L 21.420 107 70-148ND
Bromochloromethane ug/L 21.720 109 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1758198MATRIX SPIKE SAMPLE:
MSSpike
Result
92301667001
Bromodichloromethane ug/L 21.420 107 70-130ND
Bromoform ug/L 20.820 104 70-130ND
Bromomethane ug/L 23.920 120 70-130ND
Carbon disulfide ug/L 22.0J20 110 70-130ND
Carbon tetrachloride ug/L 24.420 122 70-130ND
Chlorobenzene ug/L 20.820 104 70-146ND
Chloroethane ug/L 20.920 105 70-130ND
Chloroform ug/L 21.320 107 70-130ND
Chloromethane ug/L 21.620 108 70-130ND
cis-1,2-Dichloroethene ug/L 21.320 106 70-130ND
cis-1,3-Dichloropropene ug/L 20.120 101 70-130ND
Dibromochloromethane ug/L 21.420 107 70-130ND
Dibromomethane ug/L 19.520 98 70-130ND
Ethylbenzene ug/L 20.820 104 70-130ND
Iodomethane ug/L 50.240 126 70-130ND
Methylene Chloride ug/L 20.720 100 70-130ND
Styrene ug/L 21.020 105 70-130ND
Tetrachloroethene ug/L 20.220 101 70-130ND
Toluene ug/L 21.320 106 70-155ND
trans-1,2-Dichloroethene ug/L 22.020 110 70-130ND
trans-1,3-Dichloropropene ug/L 19.020 95 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.3J20 77 70-130ND
Trichloroethene ug/L 20.520 103 69-151ND
Trichlorofluoromethane ug/L 21.520 107 70-130ND
Vinyl acetate ug/L 38.4J40 96 70-130ND
Vinyl chloride ug/L 20.820 104 70-130ND
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301667002
1758199SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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Page 26 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301667002
1758199SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%95 196
4-Bromofluorobenzene (S)%96 097
Toluene-d8 (S)%99 1101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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Page 27 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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Page 28 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92301667
SURRY MSWLF SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92301667001 MPRP/22070 ICP/19750SW-1 EPA 3010A EPA 6010
92301667002 MPRP/22070 ICP/19750SW-2 EPA 3010A EPA 6010
92301667003 MPRP/22070 ICP/19750SW-3 EPA 3010A EPA 6010
92301667004 MPRP/22070 ICP/19750SW-4 EPA 3010A EPA 6010
92301667005 MPRP/22070 ICP/19750SWN-1 EPA 3010A EPA 6010
92301667006 MPRP/22070 ICP/19750SWN-2 EPA 3010A EPA 6010
92301667007 MPRP/22070 ICP/19750SW-A EPA 3010A EPA 6010
92301667008 MPRP/22070 ICP/19750SW-B EPA 3010A EPA 6010
92301667001 MSV/37327SW-1 EPA 8260
92301667002 MSV/37327SW-2 EPA 8260
92301667003 MSV/37327SW-3 EPA 8260
92301667004 MSV/37327SW-4 EPA 8260
92301667005 MSV/37327SWN-1 EPA 8260
92301667006 MSV/37327SWN-2 EPA 8260
92301667007 MSV/37327SW-A EPA 8260
92301667008 MSV/37327SW-B EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/24/2016 05:51 PM
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Page 29 of 31
Page 30 of 31
Page 31 of 31
#=CL#
June 28, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92302049
92302049
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 20, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92302049
SURRY BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92302049001 EB Water 06/17/16 00:00 06/20/16 06:33
92302049002 FB Water 06/17/16 00:00 06/20/16 06:33
92302049003 TB Water 06/17/16 00:00 06/20/16 06:33
REPORT OF LABORATORY ANALYSIS
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Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92302049
SURRY BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92302049001 EB EPA 6010 16 PASI-AJMW
EPA 8260 67 PASI-CNB
SM 4500-CN-E 1 PASI-AAES2
92302049002 FB EPA 6010 16 PASI-AJMW
EPA 8260 67 PASI-CNB
92302049003 TB EPA 8260 67 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Sample:EB Lab ID:92302049001 Collected:06/17/16 00:00 Received:06/20/16 06:33 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/26/16 20:24 7440-36-006/23/16 21:256.0 3.8 1
Arsenic ND ug/L 06/26/16 20:24 7440-38-206/23/16 21:2510.0 2.5 1
Barium ND ug/L 06/26/16 20:24 7440-39-306/23/16 21:251002.5 1
Beryllium ND ug/L 06/26/16 20:24 7440-41-706/23/16 21:251.0 0.50 1
Cadmium ND ug/L 06/26/16 20:24 7440-43-906/23/16 21:251.0 0.50 1
Chromium ND ug/L 06/26/16 20:24 7440-47-306/23/16 21:2510.0 2.5 1
Cobalt ND ug/L 06/26/16 20:24 7440-48-406/23/16 21:2510.0 2.5 1
Copper ND ug/L 06/26/16 20:24 7440-50-806/23/16 21:2510.0 2.5 1
Lead ND ug/L 06/26/16 20:24 7439-92-106/23/16 21:2510.0 2.5 1
Nickel ND ug/L 06/26/16 20:24 7440-02-006/23/16 21:2550.0 2.5 1
Selenium ND ug/L 06/26/16 20:24 7782-49-206/23/16 21:2510.0 5.0 1
Silver ND ug/L 06/26/16 20:24 7440-22-406/23/16 21:2510.0 2.5 1
Thallium ND ug/L 06/26/16 20:24 7440-28-006/23/16 21:255.5 5.0 1
Tin 2.8J ug/L 06/26/16 20:24 7440-31-506/23/16 21:251002.5 1
Vanadium ND ug/L 06/26/16 20:24 7440-62-206/23/16 21:2525.0 2.5 1
Zinc ND ug/L 06/26/16 20:24 7440-66-606/23/16 21:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/22/16 17:41 67-64-110010.0 1
Acetonitrile ND ug/L 06/22/16 17:41 75-05-855.0 2.2 1
Acrolein ND ug/L 06/22/16 17:41 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/22/16 17:41 107-13-12001.9 1
Allyl chloride ND ug/L 06/22/16 17:41 107-05-110.0 1.5 1
Benzene ND ug/L 06/22/16 17:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/22/16 17:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/22/16 17:41 75-27-41.0 0.18 1
Bromoform ND ug/L 06/22/16 17:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/22/16 17:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/22/16 17:41 78-93-31000.96 1
Carbon disulfide ND ug/L 06/22/16 17:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/22/16 17:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/22/16 17:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/22/16 17:41 75-00-310.0 0.54 1
Chloroform ND ug/L 06/22/16 17:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/22/16 17:41 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/22/16 17:41 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/22/16 17:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/22/16 17:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/22/16 17:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/22/16 17:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/22/16 17:41 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/22/16 17:41 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/22/16 17:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/22/16 17:41 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/22/16 17:41 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/22/16 17:41 75-34-35.0 0.32 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Sample:EB Lab ID:92302049001 Collected:06/17/16 00:00 Received:06/20/16 06:33 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloroethane ND ug/L 06/22/16 17:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/22/16 17:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/22/16 17:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/22/16 17:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/22/16 17:41 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/22/16 17:41 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/22/16 17:41 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/22/16 17:41 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/22/16 17:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/22/16 17:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/22/16 17:41 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/22/16 17:41 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/22/16 17:41 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/22/16 17:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/22/16 17:41 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/22/16 17:41 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/22/16 17:41 126-98-71000.93 1
Methylene Chloride 1.4 ug/L 06/22/16 17:41 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 06/22/16 17:41 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/22/16 17:41 108-10-11000.33 1
Naphthalene ND ug/L 06/22/16 17:41 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/22/16 17:41 107-12-01503.6 1
Styrene ND ug/L 06/22/16 17:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/22/16 17:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/22/16 17:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/22/16 17:41 127-18-41.0 0.46 1
Toluene ND ug/L 06/22/16 17:41 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/22/16 17:41 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/22/16 17:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/22/16 17:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/22/16 17:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/22/16 17:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/22/16 17:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/22/16 17:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/22/16 17:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/22/16 17:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %06/22/16 17:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %06/22/16 17:41 17060-07-070-130 1
Toluene-d8 (S)99 %06/22/16 17:41 2037-26-570-130 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/24/16 17:51 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Sample:FB Lab ID:92302049002 Collected:06/17/16 00:00 Received:06/20/16 06:33 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 06/26/16 20:33 7440-36-006/23/16 21:256.0 3.8 1
Arsenic ND ug/L 06/26/16 20:33 7440-38-206/23/16 21:2510.0 2.5 1
Barium ND ug/L 06/26/16 20:33 7440-39-306/23/16 21:251002.5 1
Beryllium ND ug/L 06/26/16 20:33 7440-41-706/23/16 21:251.0 0.50 1
Cadmium ND ug/L 06/26/16 20:33 7440-43-906/23/16 21:251.0 0.50 1
Chromium ND ug/L 06/26/16 20:33 7440-47-306/23/16 21:2510.0 2.5 1
Cobalt ND ug/L 06/26/16 20:33 7440-48-406/23/16 21:2510.0 2.5 1
Copper ND ug/L 06/26/16 20:33 7440-50-806/23/16 21:2510.0 2.5 1
Lead ND ug/L 06/26/16 20:33 7439-92-106/23/16 21:2510.0 2.5 1
Nickel ND ug/L 06/26/16 20:33 7440-02-006/23/16 21:2550.0 2.5 1
Selenium ND ug/L 06/26/16 20:33 7782-49-206/23/16 21:2510.0 5.0 1
Silver ND ug/L 06/26/16 20:33 7440-22-406/23/16 21:2510.0 2.5 1
Thallium ND ug/L 06/26/16 20:33 7440-28-006/23/16 21:255.5 5.0 1
Tin 2.9J ug/L 06/26/16 20:33 7440-31-506/23/16 21:251002.5 1
Vanadium ND ug/L 06/26/16 20:33 7440-62-206/23/16 21:2525.0 2.5 1
Zinc ND ug/L 06/26/16 20:33 7440-66-606/23/16 21:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/22/16 17:58 67-64-110010.0 1
Acetonitrile ND ug/L 06/22/16 17:58 75-05-855.0 2.2 1
Acrolein ND ug/L 06/22/16 17:58 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/22/16 17:58 107-13-12001.9 1
Allyl chloride ND ug/L 06/22/16 17:58 107-05-110.0 1.5 1
Benzene ND ug/L 06/22/16 17:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/22/16 17:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/22/16 17:58 75-27-41.0 0.18 1
Bromoform ND ug/L 06/22/16 17:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/22/16 17:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/22/16 17:58 78-93-31000.96 1
Carbon disulfide ND ug/L 06/22/16 17:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/22/16 17:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/22/16 17:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/22/16 17:58 75-00-310.0 0.54 1
Chloroform ND ug/L 06/22/16 17:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/22/16 17:58 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/22/16 17:58 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/22/16 17:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/22/16 17:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/22/16 17:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/22/16 17:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/22/16 17:58 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/22/16 17:58 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/22/16 17:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/22/16 17:58 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/22/16 17:58 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/22/16 17:58 75-34-35.0 0.32 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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Huntersville, NC 28078
[phone]
Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Sample:FB Lab ID:92302049002 Collected:06/17/16 00:00 Received:06/20/16 06:33 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloroethane ND ug/L 06/22/16 17:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/22/16 17:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/22/16 17:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/22/16 17:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/22/16 17:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/22/16 17:58 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/22/16 17:58 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/22/16 17:58 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/22/16 17:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/22/16 17:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/22/16 17:58 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/22/16 17:58 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/22/16 17:58 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/22/16 17:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/22/16 17:58 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/22/16 17:58 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/22/16 17:58 126-98-71000.93 1
Methylene Chloride 1.4 ug/L 06/22/16 17:58 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 06/22/16 17:58 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/22/16 17:58 108-10-11000.33 1
Naphthalene ND ug/L 06/22/16 17:58 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/22/16 17:58 107-12-01503.6 1
Styrene ND ug/L 06/22/16 17:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/22/16 17:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/22/16 17:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/22/16 17:58 127-18-41.0 0.46 1
Toluene ND ug/L 06/22/16 17:58 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/22/16 17:58 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/22/16 17:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/22/16 17:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/22/16 17:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/22/16 17:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/22/16 17:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/22/16 17:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/22/16 17:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/22/16 17:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)93 %06/22/16 17:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/22/16 17:58 17060-07-070-130 1
Toluene-d8 (S)99 %06/22/16 17:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Sample:TB Lab ID:92302049003 Collected:06/17/16 00:00 Received:06/20/16 06:33 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/22/16 18:15 67-64-110010.0 1
Acetonitrile ND ug/L 06/22/16 18:15 75-05-855.0 2.2 1
Acrolein ND ug/L 06/22/16 18:15 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/22/16 18:15 107-13-12001.9 1
Allyl chloride ND ug/L 06/22/16 18:15 107-05-110.0 1.5 1
Benzene ND ug/L 06/22/16 18:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/22/16 18:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/22/16 18:15 75-27-41.0 0.18 1
Bromoform ND ug/L 06/22/16 18:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/22/16 18:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/22/16 18:15 78-93-31000.96 1
Carbon disulfide ND ug/L 06/22/16 18:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/22/16 18:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/22/16 18:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/22/16 18:15 75-00-310.0 0.54 1
Chloroform ND ug/L 06/22/16 18:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/22/16 18:15 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/22/16 18:15 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/22/16 18:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/22/16 18:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/22/16 18:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/22/16 18:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/22/16 18:15 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/22/16 18:15 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/22/16 18:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/22/16 18:15 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/22/16 18:15 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/22/16 18:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/22/16 18:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/22/16 18:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/22/16 18:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/22/16 18:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/22/16 18:15 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/22/16 18:15 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/22/16 18:15 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/22/16 18:15 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/22/16 18:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/22/16 18:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/22/16 18:15 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/22/16 18:15 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/22/16 18:15 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/22/16 18:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/22/16 18:15 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/22/16 18:15 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/22/16 18:15 126-98-71000.93 1
Methylene Chloride 1.3 ug/L 06/22/16 18:15 75-09-2 C91.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92302049
SURRY BLANKS
Sample:TB Lab ID:92302049003 Collected:06/17/16 00:00 Received:06/20/16 06:33 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 06/22/16 18:15 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/22/16 18:15 108-10-11000.33 1
Naphthalene ND ug/L 06/22/16 18:15 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/22/16 18:15 107-12-01503.6 1
Styrene ND ug/L 06/22/16 18:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/22/16 18:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/22/16 18:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/22/16 18:15 127-18-41.0 0.46 1
Toluene ND ug/L 06/22/16 18:15 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/22/16 18:15 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/22/16 18:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/22/16 18:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/22/16 18:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/22/16 18:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/22/16 18:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/22/16 18:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/22/16 18:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/22/16 18:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %06/22/16 18:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %06/22/16 18:15 17060-07-070-130 1
Toluene-d8 (S)101 %06/22/16 18:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/22154
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92302049001, 92302049002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1762638
Associated Lab Samples:92302049001, 92302049002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 06/26/16 20:183.8
Arsenic ug/L 4.7J 10.0 06/26/16 20:182.5
Barium ug/L ND 100 06/26/16 20:182.5
Beryllium ug/L ND 1.0 06/26/16 20:180.50
Cadmium ug/L ND 1.0 06/26/16 20:180.50
Chromium ug/L ND 10.0 06/26/16 20:182.5
Cobalt ug/L ND 10.0 06/26/16 20:182.5
Copper ug/L ND 10.0 06/26/16 20:182.5
Lead ug/L ND 10.0 06/26/16 20:182.5
Nickel ug/L ND 50.0 06/26/16 20:182.5
Selenium ug/L ND 10.0 06/26/16 20:185.0
Silver ug/L ND 10.0 06/26/16 20:182.5
Thallium ug/L ND 5.5 06/26/16 20:185.0
Tin ug/L ND 100 06/26/16 20:182.5
Vanadium ug/L ND 25.0 06/26/16 20:182.5
Zinc ug/L 8.9J 10.0 06/26/16 20:185.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1762639LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 494500 99 80-120
Arsenic ug/L 484500 97 80-120
Barium ug/L 502500 100 80-120
Beryllium ug/L 489500 98 80-120
Cadmium ug/L 500500 100 80-120
Chromium ug/L 495500 99 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 495500 99 80-120
Lead ug/L 494500 99 80-120
Nickel ug/L 502500 100 80-120
Selenium ug/L 489500 98 80-120
Silver ug/L 241250 96 80-120
Thallium ug/L 493500 99 80-120
Tin ug/L 498500 100 80-120
Vanadium ug/L 492500 98 80-120
Zinc ug/L 492500 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1762640MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92302049001
1762641
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12598 0 25500ND490492
Arsenic ug/L 500 95 75-12596 1 25500ND477484
Barium ug/L 500 100 75-125100 0 25500ND498499
Beryllium ug/L 500 98 75-12597 1 25500ND489487
Cadmium ug/L 500 99 75-125100 1 25500ND494498
Chromium ug/L 500 98 75-12599 1 25500ND490493
Cobalt ug/L 500 99 75-125100 1 25500ND494498
Copper ug/L 500 98 75-12599 0 25500ND492494
Lead ug/L 500 98 75-12599 0 25500ND492494
Nickel ug/L 500 99 75-125100 1 25500ND497502
Selenium ug/L 500 96 75-12597 1 25500ND483487
Silver ug/L 250 96 75-12597 1 25250ND240241
Thallium ug/L 500 98 75-12599 1 25500ND491496
Tin ug/L 500 99 75-125100 1 255002.8J 498 502
Vanadium ug/L 500 98 75-12598 0 25500ND488490
Zinc ug/L 500 97 75-12598 1 25500ND487492
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/37389
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92302049001, 92302049002, 92302049003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1761865
Associated Lab Samples:92302049001, 92302049002, 92302049003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/22/16 13:580.33
1,1,1-Trichloroethane ug/L ND 1.0 06/22/16 13:580.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/22/16 13:580.40
1,1,2-Trichloroethane ug/L ND 1.0 06/22/16 13:580.29
1,1-Dichloroethane ug/L ND 5.0 06/22/16 13:580.32
1,1-Dichloroethene ug/L ND 5.0 06/22/16 13:580.56
1,1-Dichloropropene ug/L ND 5.0 06/22/16 13:580.49
1,2,3-Trichloropropane ug/L ND 1.0 06/22/16 13:580.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/22/16 13:580.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/22/16 13:582.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/22/16 13:580.27
1,2-Dichlorobenzene ug/L ND 5.0 06/22/16 13:580.30
1,2-Dichloroethane ug/L ND 1.0 06/22/16 13:580.24
1,2-Dichloropropane ug/L ND 1.0 06/22/16 13:580.27
1,3-Dichlorobenzene ug/L ND 5.0 06/22/16 13:580.24
1,3-Dichloropropane ug/L ND 1.0 06/22/16 13:580.28
1,4-Dichlorobenzene ug/L ND 1.0 06/22/16 13:580.33
2,2-Dichloropropane ug/L ND 15.0 06/22/16 13:580.13
2-Butanone (MEK)ug/L ND 100 06/22/16 13:580.96
2-Hexanone ug/L ND 50.0 06/22/16 13:580.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/22/16 13:580.33
Acetone ug/L ND 100 06/22/16 13:5810.0
Acetonitrile ug/L ND 55.0 06/22/16 13:582.2
Acrolein ug/L ND 53.0 06/22/16 13:581.6
Acrylonitrile ug/L ND 200 06/22/16 13:581.9
Allyl chloride ug/L ND 10.0 06/22/16 13:581.5
Benzene ug/L ND 1.0 06/22/16 13:580.25
Bromochloromethane ug/L ND 3.0 06/22/16 13:580.17
Bromodichloromethane ug/L ND 1.0 06/22/16 13:580.18
Bromoform ug/L ND 3.0 06/22/16 13:580.26
Bromomethane ug/L ND 10.0 06/22/16 13:580.29
Carbon disulfide ug/L ND 100 06/22/16 13:581.2
Carbon tetrachloride ug/L ND 1.0 06/22/16 13:580.25
Chlorobenzene ug/L ND 3.0 06/22/16 13:580.23
Chloroethane ug/L ND 10.0 06/22/16 13:580.54
Chloroform ug/L ND 5.0 06/22/16 13:580.14
Chloromethane ug/L ND 1.0 06/22/16 13:580.11
Chloroprene ug/L ND 20.0 06/22/16 13:580.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/22/16 13:580.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/22/16 13:580.13
Dibromochloromethane ug/L ND 3.0 06/22/16 13:580.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1761865
Associated Lab Samples:92302049001, 92302049002, 92302049003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/22/16 13:580.21
Dichlorodifluoromethane ug/L ND 5.0 06/22/16 13:580.21
Ethyl methacrylate ug/L ND 10.0 06/22/16 13:580.20
Ethylbenzene ug/L ND 1.0 06/22/16 13:580.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/22/16 13:580.71
Iodomethane ug/L ND 10.0 06/22/16 13:580.32
Isobutanol ug/L ND 100 06/22/16 13:5835.0
Methacrylonitrile ug/L ND 100 06/22/16 13:580.93
Methyl methacrylate ug/L ND 30.0 06/22/16 13:582.0
Methylene Chloride ug/L ND 1.0 06/22/16 13:580.97
Naphthalene ug/L ND 10.0 06/22/16 13:580.24
Propionitrile ug/L ND 150 06/22/16 13:583.6
Styrene ug/L ND 1.0 06/22/16 13:580.26
Tetrachloroethene ug/L ND 1.0 06/22/16 13:580.46
Toluene ug/L ND 1.0 06/22/16 13:580.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/22/16 13:580.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/22/16 13:580.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/22/16 13:581.0
Trichloroethene ug/L ND 1.0 06/22/16 13:580.47
Trichlorofluoromethane ug/L ND 1.0 06/22/16 13:580.20
Vinyl acetate ug/L ND 50.0 06/22/16 13:580.35
Vinyl chloride ug/L ND 1.0 06/22/16 13:580.62
Xylene (Total)ug/L ND 5.0 06/22/16 13:580.66
1,2-Dichloroethane-d4 (S)%92 70-130 06/22/16 13:58
4-Bromofluorobenzene (S)%93 70-130 06/22/16 13:58
Toluene-d8 (S)%100 70-130 06/22/16 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1761866LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.550 95 80-125
1,1,1-Trichloroethane ug/L 47.750 95 71-129
1,1,2,2-Tetrachloroethane ug/L 48.250 96 79-124
1,1,2-Trichloroethane ug/L 45.350 91 85-125
1,1-Dichloroethane ug/L 46.450 93 73-126
1,1-Dichloroethene ug/L 49.550 99 66-135
1,1-Dichloropropene ug/L 44.850 90 74-135
1,2,3-Trichloropropane ug/L 45.150 90 75-130
1,2,4-Trichlorobenzene ug/L 50.650 101 75-134
1,2-Dibromo-3-chloropropane ug/L 48.850 98 71-133
1,2-Dibromoethane (EDB)ug/L 51.150 102 83-124
1,2-Dichlorobenzene ug/L 50.750 101 80-133
1,2-Dichloroethane ug/L 39.150 78 67-128
1,2-Dichloropropane ug/L 45.550 91 75-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1761866LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.250 98 77-130
1,3-Dichloropropane ug/L 46.050 92 76-131
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2,2-Dichloropropane ug/L 48.050 96 40-160
2-Butanone (MEK)ug/L 84.5J100 84 61-144
2-Hexanone ug/L 89.1100 89 68-143
4-Methyl-2-pentanone (MIBK)ug/L 83.6J100 84 72-135
Acetone ug/L 75.9J100 76 48-146
Acetonitrile ug/L 403500 81 62-150
Acrolein ug/L 199250 80 24-160
Acrylonitrile ug/L 231250 92 40-160
Allyl chloride ug/L 49.550 99 66-137
Benzene ug/L 47.550 95 80-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 48.350 97 78-124
Bromoform ug/L 45.350 91 71-128
Bromomethane ug/L 41.050 82 40-160
Carbon disulfide ug/L 50.1J50 100 50-160
Carbon tetrachloride ug/L 47.550 95 69-131
Chlorobenzene ug/L 47.650 95 81-122
Chloroethane ug/L 45.750 91 39-148
Chloroform ug/L 45.450 91 73-127
Chloromethane ug/L 36.350 73 44-146
Chloroprene ug/L 43.750 87 75-145
cis-1,2-Dichloroethene ug/L 46.850 94 74-124
cis-1,3-Dichloropropene ug/L 48.450 97 72-132
Dibromochloromethane ug/L 46.850 94 78-125
Dibromomethane ug/L 42.650 85 82-120
Dichlorodifluoromethane ug/L 35.950 72 34-157
Ethyl methacrylate ug/L 44.350 89 82-121
Ethylbenzene ug/L 47.950 96 79-121
Hexachloro-1,3-butadiene ug/L 54.250 108 72-131
Iodomethane ug/L 77.8100 78 39-154
Isobutanol ug/L 8901000 89 34-160
Methacrylonitrile ug/L 422500 84 74-134
Methyl methacrylate ug/L 46.150 92 84-124
Methylene Chloride ug/L 44.750 89 64-133
Naphthalene ug/L 48.250 96 73-133
Propionitrile ug/L 408500 82 73-140
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 43.850 88 78-122
Toluene ug/L 46.550 93 80-121
trans-1,2-Dichloroethene ug/L 47.350 95 71-127
trans-1,3-Dichloropropene ug/L 45.950 92 69-141
trans-1,4-Dichloro-2-butene ug/L 51.0J50 102 40-160
Trichloroethene ug/L 43.150 86 78-122
Trichlorofluoromethane ug/L 47.050 94 53-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1761866LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 100100 100 40-160
Vinyl chloride ug/L 41.450 83 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1761867MATRIX SPIKE SAMPLE:
MSSpike
Result
92301923014
1,1,1,2-Tetrachloroethane ug/L 22.320 112 70-130ND
1,1,1-Trichloroethane ug/L 22.320 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.620 103 70-130ND
1,1,2-Trichloroethane ug/L 20.120 100 70-130ND
1,1-Dichloroethane ug/L 21.720 108 70-130ND
1,1-Dichloroethene ug/L 23.720 119 70-166ND
1,1-Dichloropropene ug/L 21.720 109 70-130ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 21.120 106 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.820 109 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.420 112 70-130ND
1,2-Dichlorobenzene ug/L 22.220 111 70-130ND
1,2-Dichloroethane ug/L 17.820 89 70-130ND
1,2-Dichloropropane ug/L 20.920 104 70-130ND
1,3-Dichlorobenzene ug/L 21.620 108 70-130ND
1,3-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 21.320 107 70-130ND
2,2-Dichloropropane ug/L 20.620 103 70-130ND
2-Butanone (MEK)ug/L 39.2J40 98 70-130ND
2-Hexanone ug/L 39.9J40 100 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 36.6J40 92 70-130ND
Acetone ug/L 34.2J40 82 70-130ND
Acetonitrile ug/L 187200 94 70-130ND
Acrolein ug/L 87.6100 88 70-130ND
Acrylonitrile ug/L 105J100 105 70-130ND
Allyl chloride ug/L 19.820 99 70-130ND
Benzene ug/L 22.420 112 70-148ND
Bromochloromethane ug/L 21.620 108 70-130ND
Bromodichloromethane ug/L 21.620 108 70-130ND
Bromoform ug/L 21.520 108 70-130ND
Bromomethane ug/L 20.020 100 70-130ND
Carbon disulfide ug/L 18.0J20 90 70-130ND
Carbon tetrachloride ug/L 24.620 123 70-130ND
Chlorobenzene ug/L 21.520 108 70-146ND
Chloroethane ug/L 22.920 115 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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[phone]
Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1761867MATRIX SPIKE SAMPLE:
MSSpike
Result
92301923014
Chloroform ug/L 20.520 103 70-130ND
Chloromethane ug/L 20.220 101 70-130ND
Chloroprene ug/L 19.3J20 97 70-130ND
cis-1,2-Dichloroethene ug/L 21.820 109 70-130ND
cis-1,3-Dichloropropene ug/L 21.020 105 70-130ND
Dibromochloromethane ug/L 21.720 109 70-130ND
Dibromomethane ug/L 19.120 95 70-130ND
Dichlorodifluoromethane ug/L 23.020 115 70-130ND
Ethyl methacrylate ug/L 20.820 104 70-130ND
Ethylbenzene ug/L 22.120 111 70-130ND
Hexachloro-1,3-butadiene ug/L 23.020 115 70-130ND
Iodomethane ug/L 29.140 73 70-130ND
Isobutanol ug/L 444400 111 70-130ND
Methacrylonitrile ug/L 184200 92 70-130ND
Methyl methacrylate ug/L 21.2J20 106 70-130ND
Methylene Chloride ug/L 21.120 101 70-130ND
Naphthalene ug/L 20.120 100 70-130ND
Propionitrile ug/L 182200 91 70-130ND
Styrene ug/L 21.720 109 70-130ND
Tetrachloroethene ug/L 20.520 102 70-130ND
Toluene ug/L 21.620 108 70-155ND
trans-1,2-Dichloroethene ug/L 22.820 114 70-130ND
trans-1,3-Dichloropropene ug/L 19.320 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 13.8J M1206970-130ND
Trichloroethene ug/L 20.320 102 69-151ND
Trichlorofluoromethane ug/L 23.620 118 70-130ND
Vinyl acetate ug/L 39.8J40 99 70-130ND
Vinyl chloride ug/L 22.120 110 70-130ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301923015
1761868SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 2.0J 2 302.1J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301923015
1761868SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 1.8J 5 301.9J
1,2-Dichloroethane ug/L 0.29J 300.29J
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 6.1 2 306.2
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L 2.7 2 302.8
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 2.2J 2 302.2J
Chloroethane ug/L 1.5J 5 301.6J
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 8.0 0 308.0
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L 84.6J 3085.7J
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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Huntersville, NC 28078
[phone]
Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92301923015
1761868SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 10.7 0 3010.7
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%94 094
4-Bromofluorobenzene (S)%94 194
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92302049
SURRY BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/28086
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92302049001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1764087
Associated Lab Samples:92302049001
Matrix:Water
AnalyzedMDL
Cyanide ug/L 6.0J 10.0 06/24/16 17:284.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1764088LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 109100 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1764089MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92301970001
1764090
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 100 75-12597 3 10100ND106103
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1764091MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92302724008
1764092
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 96 75-12596 0 10100ND99.6 99.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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[phone]
Page 20 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92302049
SURRY BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/28/2016 01:47 PM
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Huntersville, NC 28078
[phone]
Page 21 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92302049
SURRY BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92302049001 MPRP/22154 ICP/19811EBEPA 3010A EPA 6010
92302049002 MPRP/22154 ICP/19811FBEPA 3010A EPA 6010
92302049001 MSV/37389EBEPA 8260
92302049002 MSV/37389FBEPA 8260
92302049003 MSV/37389TBEPA 8260
92302049001 WETA/28086EBSM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 22 of 24
Page 23 of 24
Page 24 of 24
Appendix B
Field Sampling Parameter Data Sheet(s)