IDX_COMP_SITE_ASSMT_RESULTS_SUMMARY_CONTD-OCR

*331HSSF2021 *
11111111111111111111111111
DocumentlD NONCD00018l4
Site Name HAMILTON BEACH/PROCTOR SI LEX
oocumentType Site Assessment Rpt (SAR)
RptSegment 7
DocDate
DocRcvd
Box
Accesslevel
Division
Section
Program
DocCat
1/1/1999
2/20/2007
SF2021
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
• 06/ll/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
.'\n-',~e
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
l, 1--Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate -
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
0598HBWW2l6
9805252-0lA
A0515823
05/13/98
05/16/98 02:08:00
100
Water
ug/L
received
Cone. DL
ND 22.1
ND 8.47
ND 13.l
ND 25.3
ND 15.l
ND 12.3
ND 5.82
ND 22.0
ND 20.6
ND 76.8
ND 31.4
ND 8.66
ND 17.8
ND 18.8
ND 24.2
ND 13.9
ND 29.4
18.5 B 12.2
ND 18.1
ND 160
• R B S U L T S S UM M ARY (Cont'd)
0598HBWW216 0598HBWW217
9805252-0lB 9805252-02A
80516819 A05l5824
05/13/98 05/13/98
05/16/98 20:07:00 05/16/98 02:39:00
1 100
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.0618 ND 22.1
ND 0. 0631 ND 8.47
ND 0.0397 ND 13.l
ND 0.0769 ND 25.3
ND 0.0444 ND 15.1
ND 0.0421 ND 12.3
ND 0.0643 ND 5.82
ND 0.0361 ND 22.0
ND 0.0928 ND 20.6
ND 0.115 ND 76.8
ND 0.232 ND 31.4
ND 0.0291 ND 8.66
ND 0.0661 ND 17.8
ND 0.106 ND 18.8
ND 0.130 NI/ 24.2
ND 0.0365 ND 13.9
ND 0.160 ND 29.4
0.168 B 0.137 19.4 B 12.2
ND 0.578 ND 18.1
ND 0.390 ND 160
-
• Work Order # 9805252
Page _8_
0598HBWW217
9805252-028
80516820
05/13/98
05/16/98 20:34:00
1
Water
ug/L
received
Cone. DL
ND 0.0618
ND 0.0631
ND 0.0397
ND 0.0769
ND 0.0444
ND 0.0421
·ND 0.0643
ND 0.0361
0.0933 0. 0928
ND 0 .115
ND 0.232
ND 0.0291
ND 0.0661 -ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0.0797 BJ 0.137
ND 0.578
ND 0.390
06/11/98 11:17:53
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
-J.-.-2-, 4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
0598H8WW216
9805252-0lA
A0515823.
05/13/98
05/16/98 02:08:00
100
Water
ug/L
received
.
Cone. DL
ND 23.8
ND 12.4
ND 22.4
ND 17.3
ND 18.4
ND 43.7
ND 9.73
ND 34.3
ND 26.~
ND 16.8
ND 14. 7
ND 18.1
ND 10.3
ND 23.2
ND 12.3
ND 13. 7
ND 14.9
ND 27.3
ND 12.8
ND 23.0
R B S U L T S S U M M A R Y (Cont'd)
0598H8WW216 0598H8WW217
9805252-018 9805252-02A
80516819 A0515824
05/13/98 05/13/98
05/16/98 20:07:00 05/16/98 02:39:00
1 100
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.0577 ND 23.8
ND 0.0578 ND 12.4
ND 0.0848 ND 22.4
ND 0.102 ND 17.3
ND 0.0515 ND 18.4
ND 0.489 ND 43.7
0.171 0.0522 ND 9.73
ND 0.0896 ND 34.3
ND 0 .113 ND 26.3 --
ND 0.0658 ND 16.8
ND 0.0602 ND 14.7
ND 0.0892 ND 18.l
ND 0.0473 ND 10.3
ND 0.0514 ND 23.2
ND 0.0986 ND 12.3
ND 0.0952 ND 13. 7
ND 0.0800 ND 14. 9
ND 0.0929 ND 27.3
ND 0.0639 ND 12.8
ND 0.115 ND 23.0
•
Work Order # 9805252
Page 2.._
0598H8WW217
9805252-028
80516820
05/13/98
05/16/98 20:34:00
1
Water
ug/L
received
Cone. DL
ND 0.0577
ND 0.0578
ND 0.0848 .
ND 0.102
ND 0.0515
ND 0.489
0.521 0.0522
ND 0. 0896
ND 0 .113"
ND 0.0658
ND 0.0602
ND 0. 0892
ND 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
ND 0.0639
0.284 0.115
•
• 06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
o-Xylene
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
0598HBWW216
9805252-0lA
A0515823
05/13/98
05/16/98 02:08:00
100
Water
ug/L
received
Cone.
ND
Recovery
\
94
99
96
DL
12.6
• R BS ULT S S UM MARY (Cont'd)
0598HBWW216
9805252-0lB
B0516819
05/13/98
05/16/98 20:07:00
1
Water
ug/L
received
Cone.
ND
Recovery
\
97
95
103
DL
0.0414
0598HBWW217
9805252-02A
A0515824
05/13/98
05/16/98 02:39:00
100
Water
ug/L
received
Cone.
ND
Recovery
\
95
101
98
DL
12.6
Work Order # 9805252
Page .!Q_
0598HBWW217
9805252-02B
B0516820
05/13/98
05/16/98 20:34:00
l
Water
ug/L
received
Cone.
ND
Recovery
\
97
97
88
DL
0.0414
•
06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Aero le in
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chlo roe thane
•
TRIP BLANK
9805252-03A
A0515822
05/13/98
05/16/98 01:37:00
1
Water
ug/L
received
Cone. DL
ND 0.757
ND 5.10
ND 1. 66
ND 0.220
ND 0.0786
ND 0.0756
ND 0.125
ND 0.112
ND 0.117
ND 0.133
ND 0.222
ND 0. 729
ND 0.369
ND 0.261
ND 0.174
ND 0.106
ND 0.168
ND 0.0831
ND 0.0968
ND 0.172
RESULTS SUMMARY (Cont'd)
Cone. DL
---
'
•
Cone. DL
Work Order tt 9805252
Page 11...
Cone. DL
•
• 06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
2-Chloroethyl vinyl ether
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
l,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
TRIP BLANK
9805252-03A
A0515822
05/13/98
05/16/98 01:37:00
1
Water
ug/L
received
Cone. DL
ND 0.225
ND 0.0927
ND 0.166
ND 0.115
ND 0.112
ND 0.209
ND 0.245
ND l. 24
ND 0.134
ND 0.168
ND 0.175
ND 0.707
0.262 B 0.128
ND 0.0938
ND 0.177
ND 0.0783
ND 0.0566
ND 0.116
ND 0.145
ND 0.152
• RESULTS S UM MAR Y (Cont'd}
Cone. DL Cone. DL
Work Order # 9805252
Page ~
Cone.
•
DL
-
06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,l~Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl rnethacrylate
---
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodornethane
Isopropylbenzene
p-Isopropyltoluene
Methyl rnethacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
•
TRIP BLANK
9805252-03A
A0515822
05/13/98
05/16/98 01:37:00
1
Water
ug/L
received
Cone. DL
ND 0.221
ND 0.0847
ND 0.131
ND 0.253
ND 0.151
ND 0.123
ND 0.0582
ND 0.220
ND 0.206
ND 0.768
ND 0.314
ND 0.0866
ND 0.178
ND 0.188
ND 0.242
ND 0.139
ND 0.294
0.224 B 0.122
ND 0.181
ND 1.60
RBS 0 LT S SUH HAR Y (Cont'd)
Cone. DL Cone.
--- -
•
DL
-
Work Order n 9805252
Page lL
Cone.
-----
DL
•
• 06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
TRIP BLANK
9805252-03A
A0515822
05/13/98
05/16/98 01:37:00
1
Water
ug/L
received
Cone. DL
ND 0.238
ND 0.124
ND 0.224
ND 0.173
ND 0.184
ND 0.437
ND 0.0973
ND 0.343
ND 0.263
ND 0.168
ND 0.147
ND 0.181
ND 0.103
ND 0.232
ND 0.123
ND 0.137
ND 0.149
ND 0.273
ND 0.128
ND 0.230
• RESULTS S UM MARY (Cont'd)
Cone. DL Cone.
'
DL
Work Order # 9805252
Page .!.1_
Cone.
•
DL
'
06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
a-Xylene
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-de
•
TRIP BLANK
9805252-03A
A0515822
05/13/98
05/16/98 01:37:00
1
Water
ug/L
received
Cone. DL
ND 0.126
Recovery
\
95
-~
102
96
R B S U LT S S UM MAR Y (Cont•d)
Cone. DL Cone.
Recovery Recovery
\ %
~-
•
DL
-
Work Order ff 9805252
Page .l2__
-
Cone. DL
Recovery
%
-
•
• 06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDA980210000000
Calibration Date ~0~2~/~l~0~/~9~8'--~~~-
Sequence/Analysis Time
1 05/15/98 15:15:00
2 05/15/98 15:47:00
3 05/15/98 15:47:00
4 05/15/98 16:17:00
5 05/15/98 16:47:00
~ 05/15/98 17:16:00
7 05/15/98 17:46:00
8 05/15/98 18:16:00
9 05/15/98 18:45:00
10 05/15/98 19:15:00
11 05/15/98 19:44:00
12 05/15/98 20:14:00
13 05/15/98 20:43:00
14 05/15/98 21:13:00
15 05/15/98 21:42:00
16 05/15/98 22:11:00
17 05/15/98 22:41:00
18 05/15/98 23:10:00
19 05/15/98 23:39:00
20 05/16/98 00:09:00
21 05/16/98 00:38:00
22 05/16/98 01:08:00
23 05/16/98 01:37:00
24 05/16/98 02: 08: 00
25 05/16/98 02:39:00
26 05/16/98 03:10:00
27 05/16/98 03:39:00
28 05/16/98 04:08:00
29 05/16/98 04:38:00
• ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDA80515153701
Analysis Start Date/Time 05/15/98 15:37:00
Analysis Stop Date/Time 05/16/98 05:08:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
VS TD CAL Continuing Calibration
MIBCCAL Continuing Calibration
LCS981905 Lab Control Sample
LCS981906 Lab Control Sample
Work Order # 9805252
Page 1§.._
Instrument ~
Analyst !:!§B
Reviewer ~A~P~S'--~~~~~~~-
Analysis File #
A0515801
A0515802
Verification A0515802
Verification A0515803
A0515804
A0515805
LCSD981907 Lab Control Sample Duplicate A0515806
BLK981295 Blank, Method A0515807 -9805104-0lA Sample A0515808
9805107-09C Sample A0515809
9805180-01.A Sample A0515810
9805180-04A Matrix Spike A0515811
9805180-05A Matrix Spike Duplicate A0515812
9805180-02A Sample A0515813
9805180-03A Sample A0515814
9805191-0lA Sample A0515815
9805191-02A Sample A0515816
9805306-0lA Sample A0515817
9805189-03A Sample A0515818
9805280-lOA Sample A0515819
9805280-llA Sample A0515820
9805280-12A Sample A0515821
TRIP BLANK 9805252-03A Sample A0515822
0598HBWW216 9805252-0lA Sample A0515823
0598HBWW217 9805252-02A Sample A0515824
9805282-0lA Sample A0515825
SB Blank, System A0515826
9804738-0lA Blank, Refrigerator A0515827
9804738-02A Blank, Refrigerator A0515828
•
06/11/98 11:17:53
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDB980218000100
Calibration Date ~0~2~/1~8~/~9~8"-~~~-
Sequence/Analysis Time
l 05/16/98 11:57:00
2 05/16/98 12:24:00
3 05/16/98 12:24:00
4 05/16/98 12:52:00
5 05/16/98 13:19:00
6 05/16/98 13:46:00
7 05/16/98 14:13:00 -----------------------~-----------------
8 05/16/98 14:40:00
9 05/16/98 15:08:00
10 05/16/98 15:35:00
11 05/16/98 16:02:00 -12 05/16/98 16:29:00
13 05/16/98 16:57:00
14 05/16/98 17:24:00
15 05/16/98 17:51:00
-OS/16/98 16 18:18:00
17 05/16/98 18:45:00
18 05/16/98 19:13:00
19 05/16/98 19:40:00
20 05/16/98 20:07:00
21 05/16/98 20:34:00
22 05/16/98 21:01:00
23 05/16/98 21:29:00
24 05/16/98 21:56:00
25 05/16/98 22:23:00
26 05/16/98 22:50:00
27 05/16/98 23:18:00
28 05/16/98 23:45:00
•
ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDB8051612240l
Analysis Start Date/Time 05/16/98 12:24:00
Analysis Stop Date/Time 05/16/98 23:45:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
Work Order # 9805252
Page lL
Instrument ~
Analyst !.:!!IB
Reviewer ~A~P~S~~~~~~~~
Analysis File #
B05168.0l
B0516802
VSTDCAL Continuing Calibration Verification B0516802
LCS981953 Lab Control Sample B0516803
LCSD9819524 Lab Control Sample Duplicate B0516804
BLK981312. Blank, Method B0516805
9805292-0lA __ -~~ple ------------_ B0516806 --------------------------------------------------
9805292-02A Sample B0516807
9805292-03A Sample B0516808
9805292-04A Matrix Spike B0516809
9805292-05A Matrix Spike Duplicate B0516810
9805292-06A Sample B05168ll
9805292-07A Sample B0516812
9805292-08A Sample B0516813
9805292-09A Sample 80516814
---
9805292-lOA Sample B0516815
9805292-llA Sample B0516816
9805292-l2A Sample B0516817
9805292-13A Sample B0516818
0598HBWW216 9805252-0lB Sample 80516819
0598HBWW217 9805252-02B Sample B0516820
9805282-0lB Sample B051682l
9805306-0lB Sample B0516822
9805315-0lA sample 80516823
9805326-0lA Sample B0516824
9805326-04A Sample B0516825
9805326-02A Matrix Spike B0516826
9805326-03A Matrix Spike Duplicate 80516827
• •
• 06/11/98 11:17:53
Method Volatile Organics SW8260B
Lab Sample ID
File ID
Project Sample
ID/Description
Specification# ~~~~
Analyte
• • ANALYTICAL PROTOCOL SUMMARY work Order # 9805252
COMMBHTS/HARRATIVB Page ll_
Flag Comment/Narrative Corrective Action
06/11/98 11:17:37
Report RADIAN CORPORATION
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _...,R=a=d=i=a~n-=-In~t=e=r~n=a=t=io=n~a=lL,_L~L=C.._
By _ _..1~4~0~4~6....::S~um"""'m~i=t_D::.:.r~.L·-B:::;ld~q::i.:..._B,,_
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0598HBWSOl
•
ID/
NORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON,NC
Case # ~N~A.._ _______ _
SDG # .N~A _______ _
RAS # 80304AJAL
Lab Sample ID Test Code(s)
OlA GASSSAGU
02A MS GASS SAMS
OJA MSD GASSSAMS
•
TPH
TPH
TPH
Work Order # 9805253
Page _1_
RCN 650138.0502
New York ELAP ID #: 10915
Method Desciption
Purgeables ~---~---·---------------··
Purgeables
Purgeables
•
• 06/11/98 11:17:37 • WORK ORDBR COHHBHTS
For this protocol, the CCV and LCS are one and the same standard/analysis.
This CCV/LCS is a second source standard and it meets the tightest criteria
of the two. It can be found under the LCS listing in the report.
• work Order tt 9805253
Page _2 _
06/11/98 11:17:37
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
STATB CBRTIFICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Hearth
Wisconsin Department of Natural Resources
•
Work Order U 9805253
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• • 06/11/98 11:17:37 ANALYTICAL PROTOCOL SUMMARY
FLAG DBFIHITIOHS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
NA Analyte concentration not available for this analysis.
NC RPD and/or % Recovery not calculated. See Narrative for explanation.
ND Not detected. No instrument response for analyte or result less than zero.
NR Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
NS Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit {and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. 'The pattern does not match that of Diesel.
E
F
Analyte concentration exceeded calibration range.
Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions {MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order # 9805253
Page _4_ •
06/11/98 11:17:37
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method TPH-Gasoline by mod.SW8015
Project Sample ID/Description
0598HBWS01
•
ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9805253-0lA GASSSAGU NA
•
Work Order tt 9805253
Page _5_
Analysis Batch tt
GCURI280518131101
•
• 06/11/98 11:17:37
Method TPH-Gasoline by mod.SW8015
Test Code GASSSAGU
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Gasoline
Unidentified organics
.
Surrogate{s)
Chlorobenzene
0598HBWS01
9805253-0lA
U2051803
05/13/98
05/18/98 17:56:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone. DL
ND 1420
449 BJ 1420
Recovery
%
104
• RESULTS SUMMARY
Cone. DL Cone.
Recovery Recovery
% %
DL
Work Order ft 9805253
Page _6_
Cone. DL
Recovery
%
•
06/11/98 11:17:37
Method TPH-Gasoline by mod.SW8015
Test Code GASSSAGU
Initial Calibration # URI2980320000000
Calibration Date ~0~3~/~2~0~/~9~8'--~~~-
Sequence/Analysis Time
1 05/18/98 16:14:00
2 05/18/98 17:05:00
3 05/18/98 17:56:00
4 05/18/98 18:47:00
5 05/18/98 19:39:00
b 05/18/98 20:30:00
7 05/18/98 21:21:00
8 05/18/98 22:12:00
9 05/18/98 23:04:00
10 05/19/98 09:39:00
11 05/19/98 11:01:00
•
ANALYSIS BATCH SUMMARY
Analysis Batch # GCURI280518131101
Analysis Start Date/Time 05/18/98 13:11:00
Analysis Stop Date/Time 05/19/98 11:01:00
Project Sample ID Lab Sample ID Sample Type
LCSG981013 Lab Control Sample
BLK98539 Blank, Method
0598HBWS01 9805253-0lA Sample
0598HBWS01 9805253-02A Matrix Spike
I ccy
0598HBWS01 9805253-03A Matrix Spike Duplicate
9805190-0lA Sample
9805190-02A Sample
LCSG981014 Lab Control Sample I CCV
LCSG981015 Lab Control Sample I CCV
1LCSG981016 Lab Control Sample I CCV
LCSDG98102i. Lab Control Sample I CCV
•
Work Order # 9805253
Page 1._
Instrument ~
Analyst ill!.£
Reviewer ;T~LA'-'-~~~~~~~~
Analysis File II
U2051801
U2051802
U2051803
U2051804
U2051805
U2051806
U205J.807
Duplicate U2051808
Duplicate U2051809
Duplicate U2051810
Duplicate U2051811
•
• 06/11/98 11:17:37
Method TPH-Gasoline by mod.SW8015 Specificationtt GASS
Lab Sample ID
File ID
Project Sample
ID/Description Analyte
• ANALYTICAL PROTOCOL SUMMARY
COMMBRTS/HARRATIVB
Flag Comment/Narrative Corrective Action
• work Order ff 9805253
Page _a_
06/18/98 13:42:34
Report RADIAN CORPORATION
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Pre.-..1 red _....:,:R,,a"'d"'i""'a"'n'-"I""n"'t"'e"'r.,,n,,,a"'t"'i"'o"'n"'a"'l ..... .....::L:::L;;;;C:....
By _ _,:1;!4~0;!4~6_.:::S'-"ue.:m~m~i"=t:....!:D::r..:·..1.•....:;B~l"'d~g'-'.-"'B'­
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0598HBWS01
•
ID/
MORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON,NC
Case # ~N~A~-------­
SDG # ::;N::..:A:.......-------
RAS # 80304AJAL
Lab Sample ID Test Code(s)
OlA 355SSAOO
CKlSSAOO
DSLSSAEL
Method
Work Order # 9805254
Page _1_
RCN 650138. 0502
New York ELAP ID #: 10915
Desciption
---
Sonication Extract SW846
Primary KD cone. SW846
TPH Extractables
• 06/18/98 13:42:34
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York.
Oklahoma
South Carolina
Utah
Wisconsin
• STA TB C B R T I F I C A T I O N S
Agency
Department of Pollution Control and E:cology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9805254
Page _2_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
06/18/98 13:42:34 AHALYTICAL PROTOCOL SUMMARY
Flag
< DL
NA
NC
ND
NR
NS
A
B
c
D
E
F
G
H -I
J
K
M
p
Q
R
s
T
x
y
z
•
F L A G D B F I H I T I 0 H S
Definition
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPO and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero).
Confirming data obtained using second GC column or GCMS.
Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
Analyte concentration exceeded calibration range.
Interference or coelution suspected. See Narrative for explanation.
Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
Presence of analyte previously confirmed by historical data.
Analyte identification suspect. See Narrative for explanation.
Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
Peak did not meet method identification criteria. Analyte not detected on other GC column.
Result modified from previous Report. See Narrative for explanation.
Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
QC result does not meet tolerance in Protocol Specification.
Result reported elsewhere.
Analyte concentration obtained usiny Method of Standard Additions (MSA) .
Second column confirmational analysis not performed.
See Narrative for explanation.
See Narrative for explanation.
See Narrative for explanation.
•
Work Order # 9805254
Page _3_
•
• 06/18/98 13:42:34
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method TPH-Diesel by mod. SW8015
Project Sample ID/Description
0598HBWS01
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9805254-0lA DSLSSAEL 3550980521101000
Work Order tt 9805254
Page _4_
Analysis Batch #
TPGC1280527120001
•
06/18/98 13:42:34
Method TPH-Diesel by mod. SW8015
Test Code DSLSSAEL
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Diesel
Jet fuel JP4
Kerosene
Unidentified organics
Surrogate(s)
Octacosane
•
0598HBWS01
9805254-0lA
U8E27015
05/13/98
05/21/98
05/28/98 10:09:00
1.0000
Solid
ug/g
dry weight
Cone. DL
ND 0.886
ND 3.98
ND 2.44
108 BA
Recovery
- ----
\
155 Q
RBSULTS SUMMARY
Cone. DL Cone.
Recovery Recovery
-\ \
•
DL
-
Work Order ff 9805254
Page _5_
Cone. DL
Recovery
\
•
• 06/18/98 13:42:34
Method TPH-Diesel by mod. SW8015
Test Code DSLSWAEL
Initial Calibration ff GC12980522110000
Calibration Date ~0~5~/~2~2~/~9~8'------
Sequence/Analysis Time
1 05/27/98 11:26:00
2 05/27/98 12:13:00
3 05/27/98 13:00:00
4 05/27/98 13:47:00
5 05/27/98 14:33:00
6 05/27/98 15:20:00
7 05/27 /98 16:07:00
8 05/27/98 16:54:00
9 05/27/98 17:41:00
10 05/27/98 18:28:00
11 05/27/98 19:15:00
12 05/27/98 20:01:00
l3 05/27 /98 20:48:00
14 05/28/98 09:23:00
15 05/28/98 10:09:00
16 05/28/98 10:56:00
17 05/28/98 11:43:00
18 05/28/98 12:29:00
19 05/28/98 13:16:00
• ANALYSIS BATCH SUMMARY
Analysis Batch tt TPGC1280527120001
Analysis Start Date/Time 05/27/98 12:00:00
Analysis Stop Date/Time 05/28/98 13:16:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
PRIMER_LUBE Sample
SB Blank, System
ccv_JET Continuing Calibration
CCV_KER Continuing Calibration
ccv_DSL Continuing Calibration
BLK98163l Blank, Method
LCS982394 Lab Control Sample
Work Order ff 9805254
Page _6_
Instrument ~
Analyst t:!fil1
Reviewer ~T~LA::..:... _______ _
Analysis File ff
UBE27001
U8E27002
U8E27003
Verification U8E27004
Verification U8E27005
Verification U8E27006
U8E27007
U8E27008 -
LCSD982394 Lab Control Sample Duplicate U8E27009
9805174-0lA Sample U8E27010
9805174-03A Matrix Spike U8E270ll
9805174-04A Matrix Spike Duplicate U8E27012
9805174-02A Sample U8E27013
SB Blank, System .U8E27014
0598HBWS0l 9805254-0lA Sample U8E27015
SB Blank, System U8E27016
CCV_JET Continuing Calibration Verification UBE27017
CCV_KER Continuing Calibration Verification U8E27018
ccv_DSL Continuing Calibration Verification U8E27019
•
-
06/18/98 13:42:34
Method TPH-Diesel by mod. SW8015
Lab Sample ID
File ID
•
Project Sample
ID/Description
Specif icationtt DSLS
Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMBNTS/NARRATIVR
Flag Comment/Narrative
•
Corrective Action
Work Order U 9805254
Page _7 _
•
• 06/18/98 13:42:34 • QUALITY CONTROL BXCBPTIOH RBPOR·.r
SUMMARY
QCER # Analysis Batch Number
980528-09 GC12980527120000
.
Work Order ff 9805254
Page _8_ •
06/11/98 11:20:51
Report RADIAN CORPORATION
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _,;R::;a::;d:.oi::;a"'n'-=I~no::t::;e;,:r~n"'a"'t~i::;o:...n:i:a:=l:.<1..,..:,L,.L,.c,_
By ~-=1~4~0~4~6....:::S~u~m~m~i~t--=D~r~·~·....:::B~l~d~s~·--=B~
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0598HBWS01
•
ID/
NOR~ ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON,NC
Case # ~N~A'--------~­
SDG # ~N~A'--~~~~~~~
RAS # 80304AJAL
Lab Sample ID Test Code(s)
OlA CKlSSAOO
IRXESAOG
SONESAOO
•
Work Order # 9805255
Page _1_
RCN 650138.0502
New York ELAP ID #: 10915
Method Desciption
Primary KD cone. SW846
IR analysis
Sonication Extraction
•
• 06/11/98 11:20:51
State
Arkansas
California
Kansas
Louisiana !
North Carol!ina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB C B R T I P I C A T I 0 l!f S
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9805255
Page _2_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
06/11/98 11:20:51 AHALYTICAL PROTOCOL SUMMARY
PL.AG DBPIHITIOHS
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPO and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
--
p Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation.
• •
Work Order # 9805255
Page _3_
•
• 06/11/98 11:20:51
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Oil and Grease by E413.2
Project Sample ID/Description
0598HBWS01
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch ff
9805255-0lA IRXESAOG DIST980514093100
Work Order ff 9805255
Page L
Analysis Batch ff
WLPEIR80515093001
•
06/11/98 11:20:51
Method Oil and Grease by E413.2
Test Code IRXESAOG
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Oil and Grease
•
0598HBWS01
9805255-0lA
PEIR0515-18
05/13/98
05/15/98
05/15/98 09:30:00
1
Solid
mg/kg
dry weight
Cone. DL
127 8.20
RBSOLTS SUMMARY
Cone. DL Cone.
•
DL
Work Order # 9805255
Page _5_
Cone. DL
•
• 06/11/98 11:20:51
Method Oil and Grease by E413.2
Test Code IRXESAOG
Initial Calibration # PEIR980515093000
Calibration Date ~0~5~/~1~5~/~9~8'------
Sequence/Analysis Time
1 05/15/98 09:30:00
2 05/15/98 09:30:00
3 05/15/98 09:30:00
4 05/15/98 09:30:00
5 05/15/98 09:30:00
6 05/15/98 09:30:00
7 05/15/98 09:30:00
8 05/15/98 09:30:00
9 05/15/98 09:30:00
10 05/15/98 09:30:00
11 05/15/98 09:30:00
12 05/15/98 09:30:00
13 05/15/98 09:30:00
14 05/15/98 09:30:00
15 05/15/98 09:30:00
16 05/15/98 09:30:00
17 05/15/98 09:30:00
18 05/15/98 09:30:00
19 05/15/98 09:30:00
20 05/15/98 09:30:00
• ANALYSIS BATCH SUMMARY
Analysis Batch # WLPEIR80515093001
Analysis Start Date/Time 05/15/98 09:30:00
Analysis Stop Date/Time
Work Order tt 9805255
Page _6_
Instrument ~
Analyst !!!'.!!:!
Reviewer :D::L,,,,c'----------
Project Sample ID Lab Sample ID Sample Type Analysis File #
CAL_l Initial Calibration Standard 1 PEIR0515-1
CAL_2 Initial Calibration Standard 2 PEIR0515-2
CAL_3 Initial Calibration Standard 3 PEIR0515-3
CAL_4 Initial Calibration Standard 4 PEIR0515-4
CAL_5 Initial Calibration Standard 5 PEIR0515-5
CAL_6 Initial Calibration Standard 6 PEIR0515-6
ISV Second Source Standard PEIR0515-7
rev Continuing Calibration Verification PEIR0515-8
CCV Continuing Calibration Verification PEIR0515-9
REAG_BLK Blank, Reagent PEIR0515-10
BLK981613 Blank, Method PEIR0515-11
LCS982365 Lab Control Sample PEIR0515-12
LCSD982365 Lab Control Sample Duplicate PEIR0515-13
9805171-0lA Sample PEIR0515-14
9805171-02A Sample PEIR0515-15
9805171-03A Matrix Spike PEIR0515-16
9805171-04A Matrix Spike Duplicate PEIR0515-17
0598HBWS01 9805255-0lA Sample PEIR0515-18
REAG_BLK Blank, Reagent PEIR0515-19
CCV Continuing Calibration Verification PEIR0515-20
•
06/11/98 11:20:51
Method Oil and Grease by E413.2 Specification# HCTE
Lab Sample ID
File ID
Project Sample
ID/Description Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Comment/Narrative Corrective Action
Work Order # 9805255
Page _7_
•
• 06/11/98 11:21:59
Previously Reported on 05/18/98.
Report Form
Work Order Summary
State Certifications
Flag Definitions
• RADIAH AHALYTICAL SERVICES
FPAS RBPORT
TABLB OF COHTBHTS
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Analytical Batch ID
Protocol Summary for Percent moisture, SW846
Results Summary
Analysis Batch Summary EXMSRS80515082501
Comments/Narrative
• Work Order U 9805256
Certified By IJ _ ___/ ~
Date ____ t,_-'-r_z._.-_-J_.P'----
Pages
From To
1 1
2 2
3 3
4 4
5 5
6 6
7 7
06/11/98 11:21:59
Report RADIAN CORPORATION
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared ~-"R=a=d=i=a-n'--"I_n=t=e=r-n=a=t=i=o-n=a=l~,-=L=L=C'-­
By ~-=1~4=0~4=6_,.S~u~m~m~i~t_..D=r~·~·_..B~l~d~q~._..B~
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0598HBWS01
•
ID/
NOR~ ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON,NC
Case # ~N-A:...-~~~-~~-~
SDG # •N-A~~~~~~~~
RAS # 80304AJAL
Lab Sample ID Test Code(s)
OlA MSRSSAOO
•
Work Order # 9805256
Page _1_
RCN 650138.0502
New York ELAP IO #: 10915
Method Desciption
Percent Moisture SW846
•
• 06/11/98 11:21:59
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATE CERTIFICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9805256
Page L
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
06/11/98 11:21:59 ANALYTICAL PROTOCOL SUMMARY
FLAG DBPIHITIOHS
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPO and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
c Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on oth~1 ,JC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary_and sec:on9ary GC columns di-ffer by g1'ea~er than a factor oi'. 3-.-
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation.
• •
Work Order # 9805256
Page _3_
•
• 06/11/98 11:21:59
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Percent moisture, SW846
Project Sample ID/Description
0598HBWS01
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9805256-0lA MSRSSAOO NA
Work Order # 9805256
Page _4_
Analysis Batch #
EXMSRS80515082501
•
06/11/98 11:21:59
Method Percent moisture, SW846
Test Code MSRSSAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte.
Percent moisture
•
0598HBWS01
9805256-0lA
MSRS051508-ll
05/13/98
05/15/98 08:25
l
Solid
\
Cone. DL
19.4
RBSOLTS SUMMARY
Cone. DL Cone.
•
DL
Work Order II 98.05256
Page _5_
Cone. DL
•
• 06/11/98 11:21:59
Method Percent moisture, SW846
Test Code MSRSSAOO
Initial Calibration ff _N_A __ ~~~-~~
Calibration Date ~N~A'--~~-~~~-
Sequence/Analysis Time
1 05/15/98 08 :25
2 05/15/98 08:25:00
3 05/15/98 08 :25
4 05/15/98 08:25
5 05/15/98 08 :25
r 05/15/98 08:25
7 05/15/98 08:25:00
8 05/15/98 08:25
9 05/15/98 08:25
10 05/15/98 08:25
11 05/15/98 08:25
• ANALYSIS BATCH SUMMARY
Analysis Batch tt EXMSRS80515082501
Analysis Start Date/Time 05/15/98 08:25:00
Analysis Stop Date/Time 05/18/98 09:45:00
Project Sample ID Lab Sample ID Sample Type
9805229-0lA Sample
9805229-02A Sample Duplicate
9805229-03A Sample
9805229-04A Sample
9805229-05A Sample
9805232-0lA Sample
9805232-02A Sample Duplicate
9805232-03A Sample
9805232-04A Sample
9805232-05A Sample
0598HBWS01 9805256-0lA Sample
Work Order ff 9805256
Page _6_
Instrument ~
Analyst ACR
Reviewer -~---~-~~-
Analysis File ff
MSRS051508-l
MSRS051508-2
MSRS051508-3
MSRS051508-4
MSRS051508-5
MSRS051508-6
MSRS051508-7
MSRS051508-8
MSRS051508-9
MSRS051508-10
MSRS051508-ll
•
06/ll/98 11:21:59
Method Percent moisture, SW846 Specification# MSRS D
Lab Sample ID
File ID
•
Project Sample
ID/Description Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMKHTS/HARRATIVK
Flag Comment/Narrative
•
Corrective Action
Work Order # 9805256
Page ]__
•
06/11/98 11:23:09
Report RADIAN CORPORATION
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared --"R"'a"'d"'i"'a"'n'-"I"'n"'t"'e:.:r.!'n~a"'t"'i"'o::.:n~a:.:l"-'~L::L"'C"­
By --"1'-'4'-"0c.:4"'6'-"S"'u"'m"'m"'i"'t'-"D;::r_, ..... , --=B'-=l"'d"'qc.:.·-=B'-
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0598HBWWT1
•
ID/
MOR~ ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case# -.N.A...._ _______ _
SDG # ~N~A _______ _
RAS # 80304AJAL
Lab Sample ID Test Code(s)
OlA 826SWACM
OlB SPAREBOO
OlC SPAREBOO
•
Method
Work Order # 9805282
Page _1_
RCN 650138.0502
New York ELAP ID #: 10915
Desciption
Volatile Organics by GC/MS
Spare Sample
Spare Sample
•
• 06/11/98 11:23:09 • NORK ORDER COMMBHTS
The standard Method 8260A surrogate tolerances are laboratory derived from
historical data. Project specific tolerances may differ.
• Work Order # 9805282
Page _2_
06/11/98 11:23:09
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATB CBRTIPICATIOBS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah ~cpartment of Health
Wisconsin Department of Natural Resources
•
Work Order # 9805282
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• • 06/11/98 11:23:09 ANALYTICAL PROTOCOL SUMMARY
FLAG DEFINITIONS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
NA Analyte concentration not available for this analysis.
NC RPD and/or % Recovery not calculated. See Narrative for explanation.
ND Not detected. No instrument response for analyte or result less than zero.
NR Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
NS Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did.not meet method identification criteria. Analyte not detected on other GC column.
M
p
Result modified from previous Report.
Analyte not confirmed. Results from
See Narrative for explanation.
primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions {MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order # 9805282
Page _4_ •
06/11/98 11:23:09
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method Volatile Organics SW8260B
Project Sample ID/Description
0598HBWWT1
0598HBWWT1
•
Al!IALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9805282-0lA 826SWACM NA
9805282-0lC 826SWACM NA
•
Work Order H 9805?.82
Page L
Analysis Batch tt
MSMSDA80515153701
MSMSDB80518130901
•
• 06/11/98 11:23:09
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
0598HBWWT1
9805282-0lA
A05l5825
05/12/98
05/16/98 03:10:00
100
Water
ug/L
received
Cone. DL
435 75.7
ND 510
ND 166
ND 22.0
23.9 7.86
ND 7.56
ND 12.5
ND 11.2
ND 11. 7
ND 13.3
ND 22.2
1610 72.9
ND 36.9
ND 26.1
ND 17.4
ND 10.6
ND 16.8
ND 8.31
ND 9.68
ND 17.2
• RESULTS SUMMARY
0598HBWWT1
9805282-0lC
B0518806
05/12/98
05/18/98 14:58:00
1000
Water
ug/L
received
Cone. DL
ND 413
ND 5720
ND 7170
ND 333
ND 37.5
ND 92.8
ND 62.4
ND 82.8
ND 63.4
ND 54.7
ND 46.7
ND 222
ND 116
ND 78.2
ND 82.3
ND 54.7
ND 57.6
ND 71.9
ND 45.3
ND 44.1
Cone. DL
Work Order # 9805282
Page _6_
Cone.
•
DL
06/11/98 11:23:09
Method Volatile Organics SWB260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
2-Chloroethyl vinyl ether
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
·Dibromochloromethane-
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
059BHBWWT1
9805282-0lA
A0515825
05/12/98
05/16/98 03:10:00
100
Water
ug/L
received
Cone. DL
ND 22.5
ND 9.27
ND 16.6
ND 11.5
ND 11.2
ND 20.9
ND 24.5
ND 124
ND 13.4
ND 16.8
ND 17.5
ND 70.7
27.7 B 12.8
ND 9.38
ND 17.7
ND 7.83
6030 5.66
198 11. 6
9460 14.5
1570 15.2
R B S ULT S S 0 M MARY (Cont'd)
0598HBWWT1
9805282-0lC
80518806
05/12/98
05/18/98 14:58:00
1000
Water
ug/L
received
Cone. DL
ND 144
ND 48.0
ND 60.5
ND 52.1
ND 60.5
ND 88.1
ND 53.8
ND 194
-ND--76.9
ND 43.5
ND 118
ND 412
ND 73.3
ND 46.9
ND 46.6
ND 176
3830 57.6
ND 34.8
6540 71.5
1120 38.3
•
Cone. DL
Work Order # 9805282
Page _7_
Cone.
---
DL
•
• 06/11/98 11:23:09
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
0598HBWWT1
9805282-0lA
A0515825
05/12/98
05/16/98 03:10:00
100
Water
ug/L
received
Cone. DL
7.62 J 22.1
ND 8.47
ND 13.1
ND 25.3
ND 15.1
ND 12.3
ND 5.82
ND 22.0
87.9 20.6
ND 76.8
ND 31.4
ND 8.66
ND 17.8
ND 18.8
ND 24.2
ND 13.9
ND 29.4
23.5 B 12.2
313 18.1
ND 160
• R B S U LT S S UM MA R Y (Cont'd)
0598HBWWT1
9805282-0lC
80518806
05/12/98
05/18/98 14:58:00
1000
Water
ug/L
received
Cone. DL
ND 61. 8
ND 63.1
ND 39.7
ND 76.9
ND 44.4
ND 42.1
ND 64.3
ND 36.1
ND 92.8
ND 115
ND 232
ND 29.1
ND 66.1
ND 106
ND 130
' ND 36.5
ND 160
199 B 137
ND 578
ND 390
Cone. DL
Work Order U 9805282
Page _8_
Cone.
•
DL
06/11/98 11:23:09
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1-.-2, 3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
•·
0598HBWWT1
9805282-0lA
A0515825
05/12/98
05/16/98 03:10:00
100
Water
ug/L
received
Cone. DL
41.0 23.8
ND 12.4
ND 22.4
ND 17.3
ND 18.4
ND 43.7
387 9.73
-@ -34.3
ND 26.3
26500 ER 16.8
41.6 14.7
1860 18.1
ND 10.3
ND 23.2
ND 12.3
404 13.7
91.9 14.9
ND 27.3
ND 12.8
254 23.0
R B S ULT S S UM MAR Y (Cont'd)
0598HBWWT1
9805282-0lC
80518806
05/12/98
05/18/98 14:58:00
1000
Water
ug/L
received
Cone. DL
ND 57.7
ND 57.8
ND 84.8
ND 102
ND 51. 5
ND 489
289 52.2
ND 89.6
ND 113
18100 65.8
ND 60.2
1430 89.2
ND 47.3
ND 51.4
ND 98.6
258 95.2
ND 80.0
ND 92.9
ND 63.9
198 115
•
Cone. DL
Work Order # 9805282
Page _9_
Cone.
--
DL
•
• 06/11/98 11:23:09
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
/\n3.l:·~c
o-Xylene
.
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
0598HBWWT1
9805282-0lA
A0515825
05/12/98
05/16/98 03:10:00
100
Water
ug/L
received
Cone. DL
251 12.6
Recovery
\
96
95
98
• RESULTS S UM MAR Y (Cont'd)
0598HBWWT1
9805282-0lC
30518806
05/12/98
05/18/98 14:58:00
1000
water
ug/L
received
Cone. DL
ND 41.4
Recovery
\
97
95
102
Cone. DL
Recovery
\
work Order # 9805282
Page !Q...
Cone. DL
Recovery
\
•
06/11/98 11:23:09
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration tt MSDA980210000000
Calibration Date ~Oz2~/zl~0~/9~8""-~~~-
Sequence/Analysis Time
l 05/15/98 15:15:00
2 05/15/98 15:47:00
3 05/15/98 15:47:00
4 05/15/98 16:17:00
5 05/15/98 16:47:00
6 05/15/98 17:16:00
7 05/15/98 1.7:46:00
8 05/15/98 18:16:00
9 05/15/98 18:45:00
10 05/15/98 19:15:00
11 05/15/98 19:44:00
12 05/15/98 20:14:00
13 05/15/98 20:43:00
14 05/15/98 21:13:00
15 05/15/98 21:42:00
16 05/15/98 22:11:00
17 05/15/98 22:41:00
18 05/15/98 23:10:00
19 05/15/98 23:39:00
20 05/16/98 00:09:00
21 05/16/98 00:38:00
22 05/16/98 01:08:00
23 05/16/98 01:37:00
24 05/16/98 02:08:00
25 05/16/98 02:39:00
26 05/16/98 03:10:00
27 05/16/98 03:39:00
28 05/16/98 04:08:00
29 05/16/98 04:38:00
•
ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDA80515153701
Analysis Start Date/Time 05/15/98 15:37:00
Analysis Stop Date/Time 05/16/98 05:08:00
Work Order # 9805282
Page 11...
Instrument ~
Analyst !:!§R
Reviewer ~A~PS""-~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File tt
SB Blank, System A05l5801
BFB GC/MS tune files A0515802
VS TD CAL Continuing Calibration Verification A0515802
MIBCCAL Continuing Calibration Verification A0515803
LCS981905 Lab Control Sample A0515804
LCS981906 Lab Control Sample A0515805
LCSD981907 Lab Control Sample Duplicate A0515806
BLK981295 Blank, Method A0515807
9805104-0lA Sample A0515808
9805107-09C Sample A0515809
9805180-0lA Sample A0515810
9805180-04A Matrix Spike A0515811
9805l80-05A Matrix Spike Duplicate A0515812
9805l80-02A Sample A0515813
9805180-03A Sample A0515814
-----9-0-05191-o lA Sample -A05-158-15
9805191-02A Sample A05l5816
9805306-0lA Sample A0515817
9805189-03A Sample A05l5818
9805280-lOA Sample AOS15819
9805280-llA Sample AOS15820
9805280-12A Sample A0515821
9805252-03A Sample A0515822
9805252-0lA Sample A0515823
9805252-02A Sample A0515824
0598HBWWT1 9805282-0lA Sample A0515825
SB Blank, System A0515826
9804738-0lA Blank, Refrigerator A0515827
9804738-02A Blank, Refrigerator A0515828
• •
• 06/11/98 11:23:09
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDB980218000100
Calibration Date ~0~2L/=1~8L/~9~8~~~~
Sequence/Analysis Time
1 05/18/98 12:42:00
2 05/18/98 13:09:00
3 05/18/98 13:09:00
4 05/18/98 13:37:00
5 05/18/98 14:04:00
6 05/18/98 14:31:00
7 05/18/98 14:58:00
8 05/18/98 16:36:00
9 05/18/98 17:19:00
10 05/18/98 18:19:00
11 05/18/98 18:19:00
12 05/18/98 18:46:00
13 05/18/98 19:13:00
14 05/18/98 19:41:00
15 05/18/98 20:08:00
16 05/18/98 20:35:00
17 05/18/98 21:02:00
18 05/18/98 21:29:00
19 05/18/98 21:57:00
20 05/18/98 22:24:00
21 05/18/98 22:51:00
22 05/18/98 23:18:00
23 05/18/98 23:45:00
24 05/19/98 00:13:00
25 05/19/98 00:40:00
26 05/19/98 01:07:00
27 05/19/98 01:34:00
28 05/19/98 02:01:00
29 05/19/98 02:29:00
• ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDB80518130901
Analysis Start Date/Time 05/18/98 13:09:00
Analysis Stop Date/Time 05/19/98 02:29:00
Work Order # 9805282
Page 1L
Instrument ~
Analyst~
Reviewer ~A~P~S~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File ll
SB Blank, System 80518801
BFB GC/MS tune files 80518802
VSTDCAL Continuing Calibration Verification 80518802
LCS981955 Lab Control Sample B0518803
LCSD981956 Lab Control Sample Duplicate B0518804
BLK981313 Blank, Method 80518805
0598HBWWT1 9805282-0lC Sample 80518806
9805141-0lT Sample B0518807
9805142-0lU Sample 80518808
BFB GC/MS tune files B0518809
VS TD CAI,. Continuing Calibration Verification B0518809
9805143-0lR Sample B0518810
9805145-0lS Sample 80518811
9805146-0lR Sample 80518813
9805147-0lS Sample B0518814
9805217-0lQ Sample B0518815
9805219-0lQ Sample B0518816
9805317-0lA Sample B0518817
9805317-02A Sample B0518818
9805317-03A Sample B0518819
9805317-04A Sample B0518820
9805317-05A Sample B0518821
9805317-06A Sample B0518822
9805317-07A Sample B0518823
9805317-08A Sample 80518824
9805317-09A Sample 80518825
9805317-lOA Sample 80518826
9805317-llA Matrix Spike B0518827
9805317-12A Matrix Spike Duplicate 80518828
•
06/11/98 11:23:09
Method Volatile Organics SWB260B
Lab Sample ID
File ID
•
Project Sample
ID/Description
Specification# ~~~~
Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMENTS/NARRATIVE
Flag Comment/Narrative
•
Corrective Action
Work Order # 9805282
Page l.L
•
•·
GROUNDWATER SCREENING RESULTS
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0210
Lab Name: AMS, Inc. SC Cert.: 07007 ---·--------,_ _____ ___,
NC Cert.: 538 Client: Radian ----
Matrix: (s0il/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: yocQ!:_ ID: 0.25 (mm)
Location: yvashin Project: Hamilton
Lab Sample ID: C1-4 -----·
Lab File ID: C1-4.D
Date Received: 04/14/98 ---
Date Analyzed: 04/15/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 U ---------·· 7 4-87-3 Chloromethane 1 U -----------7q:-9J-.1_ __________ Vinyl Chloride 1 U
7 4-83-9 Bromomethane 1 U
75-QO_-_;L _________ Chloroeth._a_n_e ______________ 1'----L.1L. __ ;
75-69-4 Trichlorofluoromethane 1 U ·
75-35-4 1, 1-Dichloroethene 1 U 1
75-09-2 Methylene Chloride 1 U ·----~+---· --1
, _J§§:qQ-5 trans-1,2-Dichloroethene 1 U
75-34-3 1, 1-Dichloroethane 1 U
·----·-· 2,2-Dichloropropane 1 U
.. ~4.0-59..:Q___ , cis-1,2-Dichloroethene 1 U i
67-66-3 ; Chloroform 1 .. ~
7 4-97-5 . Bromochloromethane 1 --i--J,J___,
71-55-6 -; 1 1L1-Trichloroethane 1 1 U ·
.. ____ . , 1 , 1-DichJ.9ropropene 1 U
56-23-5 · Carbon Tetrachloride 1 U . ·-· ----197-:06-1._ ___ __j_J,-Dichloroethane 1 U
71-43-2 Benzene 1 U ·-·----·-----"-~----------.7~9_1_-6 --· Trichloroethene 1 U ___ ,
78-87-5 1,2-Dichloropropane 1 Id _ _;
75-27-4 Bromodichloromethane + 1 U :
--7 4.:g5:3-· Dibromomethane 1 LJ-1 ----10061-01-5 ' cis-1,3-Dichloropropene 1 U
108-88-3 Toluene -·-·-· --~----1'-----"u _ _,
10061-02-6 trans-1,3-Dichloropropene 1 U
79-00-5 1, 1,2-Trichloroethansi___ 1 U __,
----·~~1,~3_-D_ichloropr_gpane. 1 U ·
1~('-1_§-4 Tetrachloroethene _____ 1 U
124-48-1 Dibromochloromethane 1 U ---·-·---· -j 106-93-4 1 2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U i 100-41-4 Ethylbenzer}e --l--1 U
630-20-6 1, 1, 1,2-Tetrachloroethane I 1 U
'·· .:!_08-38-3 meta, para-Xylene 2 U___J
95-47-6 ortho-Xylene 1 : U 1 -------1 -+-u··-"l .. 1JJ0-42:§______ Styrene ----------------------l-----
98-82-8 lsopropylbenzene _t__ 1 1 U :
75-25-2 Bromoform 1 U ·-1 -----------· -~-----...J
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0210 Lab Name: AMS, Inc. ----'-----------SC Cert.: 07007 -----L--------'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER -----Lab Sample ID: C1-4 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ~l:-__
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab File ID: C1-4.D --
Date Received: 04/14/98
Date Analy:ied: 04/15/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 1 ,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u ---· --Bromobenzene 1 u
1, 3, 5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u -----
I 4-Chlorotoluene 1 u -·-· .. --·-
tert-Butylbenzene I 1 u ------.•.
1,2,4-Trimethylbenzene 1 u
sec-Bu!Ylbenzene 1 u
·-----· ___ _129ra-lsopropyltoluene 1 u
541-73-1 1,3-Dichlorobenzene 1 u
10.§:46-7 1,4-Dichlorobenzene 1 u
I n-Butvlbenzene : 1 I u
95-50-1 I 1.2-Dichlorobenzene 1 u
~~1~:1L _____ I 1,2-Dibromo-3-chloroorooane 1 u I
120-82-1 I 1 2 4-Trichlorobenzene ' 1 u
(uL)
--1
I ---;
!
-I I 8768-3~ _____ H_e=x~a=c~hl~o~ro~b~u~ta~d_1e~n~e _______ -+-_____ 1 _ _,__U_~
. 91_-20_:-_3 _ -----'---'--'N=a=ph:..:..:t::..:.ha=l-=-en'--'-'e=------------+-----1~_,_--'U=-----'
1 2 3-Trichlorobenzene 1 U .. ·-______ __:-=..i=.:::_!..::.:.=.:..=.:..:=:.====-------.--J'------~---'--'='--
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
• Lab Name: A_M_S--'--, l_n_c. __________ SC Cert.:O _7_0_0_7 __
98-0192
•
•
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Lab Sample ID: C1-19 -------
Lab File ID: C1-19.D
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75 34 3 1 1 o· hi th 1 u ---IC oroe ane I i -2 2-Dichloroorooane 1 u !
-·---540-59-0 cis-1 2-Dichloroethene 1 u i
67-66-3 ; Chloroform 1 i u I
74-97-5 Bromochloromethane 1 ! u ' i
71-55-6 1 1 1-Trichloroethane 1 u i
1.1-Dichloropropene 1 u i ------56-23-5 Carbon Tetrachloride 1 u i -. -----107-06-2 1,2-Dichloroethane 1 U
_?.1_-4_3_-2 ______ B_e~n_ze_n_e __________ -+------1~_,___u_~
79-01-6 Trichloroethene 1 U ~ ·------------------------+---------+-----! 78-87-5 1 2-Dichloro ro ane 1 U
75-27-4 1 Bromodichloromethane 1 U i -=-='-'--=------'--'0~"'-'-'-"-'--'-'~--'"-'-'-'--"-'-'---'--"------'~-----'---1--u~·---, 7 4-95-3 Dibromomethane 1
10061-01-5 cis-1, 3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 trans-1,3-Dichloropropene 1 U
79-00-5 1, 1,2-Trichloroethane 1 U
1 ,3-Dichloropropane 1 U
127-1~8~-4...:..._ ____ T~e~t~ra~c~h=lo~ro~e~th~e~n~e--------+------'1-+-~U-~
124-48-1 Dibromochloromethane 1 U
1
1
1
6
. ---06-93-4
08-90-7
00-41-4
30-20-6
I
'
1 2-Dibromoethane I
Chlorobenzene
Ethvlbenzene
1 1 1 2-Tetrachloroethane
1 u
1 u I
1 u I I
1 u ! ----;
108 38 3 meta.para Xylene 2 UU ~1 95-47-6 ortho-Xylene I 1 .
i ---
100-42-5 Styrene 1 _ __1_-1--_U --1
98-82~-8=-----~--ls_o~p_ro_,P~Y_lb_e_n_ze_n_e _______ ~~----~1 _ _,_____..o..U_~·
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0192
Lab Name: AMS, Inc. SC Cert.: 07007 --'----------~ ----'---~~~~~~
NC Cert.: 538 Client: Radian Location: Washilil Project: Hamilton ----
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0 (g/ml) ML
LOW
GC Column: ~QCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Lab Sample ID: C1-19 -----
Lab File ID: C1-19.D
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0
! -----
Soil Aliquot Volume:
i CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
79-34-5 1 1 2 2-Tetrachloroethane 1 U
(uL)
9£2::-}_8:4 ________ 1~,2~,3_-T_r_ic_h_lo __ r~op~r_o~pa_n_e ______ ~ ____ 1_-+-_U __
n-Propylbenzene 1 1 U
Bromobe~ene 1 ; U _______ 1_3_5 __ -T-rim-et-h-yl_b_e_n_z_e_n_e _____ _,_~----1~r---u--
2-Chlorotoluene 1 U-~
4-Chlorotoluene 1 U
··---------~_t_ert_-_B_u~ty_lb_e_n_ze_n_e _______ ~ _____ 1_~_U _ __,
1,2,4-Trimethylbenzene 1 U
sec-Butylbenzene 1 U
.-----~~P-=ar_a-lsopropyltoluene 1 U
541-7~3~-~1 ____ ~1~,3~-D~i=ch~l=or~o~b=en~z=e~n~e-------1------1-'-----!-----'U~-
106-46-7 1,4-Dichlorobenzene 1 U -----~'--------------!------+-~____,
95-50-1
!36-1_2-8
120-82-1 ·----87-68-3
91-20-3
n-Butylbenzene 1 U
' 1 ,2-Dichlorobenzene 1 U
1 2-Dibromo-3-chloro ro ane 1 U
1,2 4-Trichlorobenzene 1 U
Hexachlorobutadiene · 1 U
Naphthalene 1 U
1,2,3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
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•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
•
98-0187
Lab Name: A_M_S_, l_n_c. _________ SC Cert.: _07_0_0_7 __ .....__ _____ __,
•
•
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0 (g/ml) ML ---
LOW
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: C5-8 -------
Lab File ID: C5-8.D -----
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 I Dichlorodifluoromethane I 1 u '
74-87-3 Chloromethane 1 u ! ·--
75-01-4 : Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u J
I
75-00-3 Chloroethane 1 u !
75-69-4 I Trichlorofluoromethane 1 u ' l
75-35-4 ' 1 1-Dichloroethene 1 u i
-
75-09-2 Methylene Chloride 1 u
156-60-5 ! trans-1 2-Dichloroethene 1 u -75-34-3 ; 1 1-Dichloroethane 1 u
' 2 2-Dichloroorooane 1 u I -540-59-0 I cis-1 2-Dichloroethene 1 u I
67-66-3 I Chloroform 1 u I -74-97-5 I Bromochloromethane 1 u
' 71-55-6 I 1 11-Trichloroethane 1 u
~ I 1 1-Dichloroorooene 1 u i
~ 56-23-5 i Carbon Tetrachloride 1 u
107-06-2 I 1 2-Dichloroethane 1 u --------71-43-2 Benzene 1 u
79-01-6 Trichloroethane 1 u l -
I
! 78-87-5 1,2-Dichloroorooane - 1 u I
75-27-4 i Bromodichloromethane 1 u I -74-95-3 i Dibromomethane I 1 u I -i 10061-01-5 I cis-1,3-Dichloropropene I 1 u
108-·88-3 I Toluene 1 u I J
10061-02-6 I trans-1 3-Dichloroorooene 1 u ! I -79-00-5 ! 1 1 2-Trichloroethane i 1 u i -i 1 3-Dichloroorooane 1 u
. _j27-18-4 I Tetrachloroethene I 1 u J
i l
124-48-1 ! Dibromochloromethane 1 u ! J
106-93-4 ! 1 2-Dibromoethane 1 u I
108-90-7 Chlorobenzene i 1 u I
100-41-4 I Ethvlbenzene 1 u i
630-20-6 i 1 1, 1 2-Tetrachloroethane i 1 u !
108-38-3 ' meta, para-Xylene I 2 u I
95-47-6 i ortho-Xylene I 1 u I ---l
100-42-5 I Stvrene 1 U I
98-82-8 lsopropylbenzene I 1 u i
J I I 75-25-2 i Bromoform J 1 u i J
FORM IVOA 3/90
1A AMS SAMPLE NO.
Lab Name:
NC Cert.:
VOLATILE Off.GANlCS ANALYSIS DATA SHEET
I i
SC Cert.: 07007 ----
98-0187
AMS, Inc.
538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER I Lab Sample ID: C5-8
I -------
5.0 (g/ml) ML
I ---
Lab File ID: C5-8.D
Level: (low/med)
% Moisture: not dee.
bOW -I
GC Column: v9coL _ ID: o~_ (mm)
Date Recei\~ed: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1. 0 -----
Soil Extract Volume:
CAS NO.
79-34-5
96-18-4
---/(uL) Soil Aliquot Volume:
I
COMPoLND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGIL ----
1, 1 ,2,2+Tetrachloroethane
1, 2, 3-THchloropropane
Q
1 u
1 u
(uL)
1 u . _____ . _____ n-~P_r~op~y~lb_e_n_ze~n_e _______________ -'-~
Bromo6enzene 1 u
1 u_ 1, 3, 5-lirimethylbenzene
2-Chloriotoluene 1 u
1 u .. -· ----------------+-------------------+-----< 4-Chlorotoluene
1 u
1 u
____ .. _____ te_rt_-_B_uty,..._lb_e_nz_e_n_e _______________ _
1 ,2,4-lirimethylbenzene
sec-Butylbenzene 1 u
para-lsbpropyltoluene 1 u
541-73-1 1 3-Dicihlorobenzene 1 u
1 u
1 u
106-46-7 1 ,4-Dichlorobenzene ·----~--,-------------+--------t----l
1 ri-Bu !benzene
95-50-1 1 2-Didhlorobenzene 1 u
8?-_®_-3____ ___ Hexachlorobutadiene
1 I u
1 I u
1
. i u
96-12-8 1 ,2-Dibromo-3-chloropropane
120-82-1 112,4-ltrichlorobenzene
91-20-_3 _____ N_a~p_ht~h_al_e_ne _________ ~---------;
1,2 3-l!richlorobenzene
1 u
1 u
FORM I VOA 3/90
•
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
sc cert.: 07007 .___9_8_-0_18_8 _ __.I · Lab Name: AMS, Inc. ----'---------~ ----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: C5-17 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C5-17.D
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
----
79-34-5 ... --.. ------~~------------_,_ ________ _
96-18-4 ----~---~~-------'--------'-----.
1 1,2 2-Tetrachloroethane 1 u
1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u ' I 2-Chlorotoluene 1 u .
4-Chlorotoluene "----! 1 u i tert-Butylbenzene 1 u ~ 1,2A-Trimethylbenzene 1 u
sec-Butylbenzene 1 u
para-lsopropyltoluene 1 u
541-73-1 1,3-Dichlorobenzene 1 u
106-46-7 1 4-Dichlorobenzene 1 u --···-· -------~------------.--------t-----'
--··.
95-50-1
96-12-8
120-82-1
. 87-68-3
91-20-3
I n-Butvlbenzene 1 I u ~
1 2-Dichlorobenzene 1 I u I
1 2-Dibromo-3-chloroorooane 1 I u i
1 2 4-Trichlorobenzene i 1 ! u ' Hexachlorobutad1ene · 1 U
Naph~alene . i 1 U
1,2 3-richlorobenzene ' 1 U .-.. ·-------~~-----------~--------
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-01890
Lab Name: AMS, Inc. SC Cert.: 07007 ~~~~~~~--~~~ ~~~~ '--~~~~~-'
NC Cert.: 538 Client: Radian Location: ~ashin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER Lab Sample ID: C5-30 X10
0.5 (g/ml) M_L __ _ Lab File ID: C5-300.D
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL) ------
Date Receiv'ed: 04/14/98
Date Analyzed: 04/15/98
!
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGtL
---··· 75-71-8 Dichlorodifluoromethane 10 ·---·---------74-87-3 Chloromethane 10 ··-·----·----· 75-01-4 Vinyl Chloride 10 --··--·--7 4.-§~_:g_ ___ ---I Bromomethane 10
75-00-3 Chloroethane 10
75-69-4 Trichlorofluoromethane 10
75-35-4 1, 1-Dichloroethene 44
75-09-2 Meth lene Chloride 10
156-60-5 trans-1 2-Dichloroethene 10
75-34-3 1, 1-Dichloroethane 550
-------· 2,2-DichloroQrOQane 10
540-59-0 cis-1 ,2-Dichloroethene 390
67-66-3 Chloroform i 10
74-97-5 Bromochloromethane 10
: _}1_-.?5-6 i 1 1.1-Trichloroethane 10
j_:L.1-Dichloroorooene 10
_56:f.3-5 Carbon Tetrachloride 10
107-06-2 1 2-Dichloroethane 12
71-43-2 Benzene 10
79-01-6 Trichloroethene 6
78-87-5 1 ,2-DichloroQroQane 10
75-27-4 Bromodichloromethane 10 ·-·--·-------74-95-3 , Pibr9_!}1omethane 10
10061-01-5 · cis-1 ,3-DichloroQroQene 10
108-88-3 Toluene 10
10061-02-6 trans-1,3-DichloroQrOQene 10
79-00-5 1, 1 ,2-Trichloroethane 10
1,3-DichloroQr.QRa~~L. 10
127-18-4 Tetrachloroethene 10
124-48-1 Dibromochloromethane 10
106-93-4 1 ,2-Dibromoethane 10
108-90-7 Chlorobenzene 10
100-41-4 Ethylbenzene 10 -
930-20:6 1, 1, 1 ,2-Tetrachloroethane 10
1 OJ~:.~?:~-_ meta, 12ara-Xylene 20
95-47-6 ortho-Xylene 10
100-42-5 S!Yrene 10
~8_-8_2-8 ls0Qro12ylbenzene 10 '
75:7..9-:f. ----'--Bromoform 10
FORM I VOA
i I
(UL)
Q
u u u u u u
u u
u
u --1 u
u I u i u
u !
J u u u u u
u " u.--J u u u u u u u u u u u
J __ u ___
3/90
•
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-01890
Lab Name: AMS, Inc. SC Cert.: 07007 ~~~~~~-~~~~~-~~~-'--~~~~~-'
NC Cert.: 538 Client: Radian Location: '0'ashin Project: Hamilton
Matrix: (soil/water) WATER Lab Sample ID: C5-30 X10
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
0.5
LOW
(g/ml) ML __
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab File ID: C5-30D.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
79-34-5 __ . ··-1_J ,2,2-Tetrachloroethane I 10
96-18-4 1,2,3-Trichloropropane + 10
n-Propylbenzene 10
Bromobenzene 10
1 3 5-Trimeth !benzene 10
2-Chlorotoluene 10
4-Chlorotoluene 10
tert-Bu!Ylbenzene 10
1 ,2,4-Trimethylbenzene 10
sec-Bu!Ylbenzene 10
ara-lso ro !toluene 10 ·------541-73-1 1 3-Dichlorobenzene 10 ~--~----~JA:Dichlorobenzene 106-46-7 -... ~· -10
n-Butvlbenzene I 10
95-50-1 ! 1 2-Dichlorobenzene 10
96-12-8 ! 1 2-Dibromo-3-chloroorooane 10
120-82-1 I 1 2 4-Trichlorobenzene 10
87-68-3 Hexachlorobutadiene 10
91-20-3 Naphthalene 10 ..
1 2 3-Trichlorobenzene 10
FORM I VOA
I
I
(uL)
Q
u
u
u
u u
u
u
u
u u
u J u I ·-1 u _J u
u
u
u u I u !
u I I
3/90
1A AMS SAMPLE NO.
VOLAT<ILE ORGANICS ANALYSIS DATA SHEET
98-0188
Lab Name: AMS, Inc. SC Cert.: 07007 --------------~-
NC Cert.: 538 Client: Radian Location: Washi,n Project: Hamilton
WATER Lab Sample ID: C5-17 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ~_!::_ __ Lab File ID:. C5-17.D
Level: (low/med) LOW Date Received: 04/13/98 ----
% Moisture: not dee. Date Analy:zied: 04/13/98
Dilution Factor: 1.0 -----GC Column: VOCOL ID: Q~ (mm)
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
--·-------------------------------.---..,
75-71-8 __ _ __ ---=D:.-'.ic=h.:..:_lo=r...::.o=di-'-'-flu~_o;:_cr..c..om~et-"-h=a.:...:-ne"'------------'-1-+----"'-U---i
74-87-3 -----'C'--'-h'--lo_ro-'-m_et_h_a_ne ________ ~ _____ 1_..___U-'--~
7_5_-01:!_ ____ --'-V...:..:.in:...Ly-'-I C=-h'""'l-"-o'-'-rid-'eo.__.. ________ '--------'-1 _,___U"--_
71.:-§.~--Bromomethane 1 U
7§:00~-----~--=C-'-h-'-lo-'-ro-'-e'-th_a_n_e ______________ 1 _;..-_U __ J
75-69-4 Trichlorofluoromethane 1 U ~
75-35-4 1 1-Dichloroethene 1 U
75-09-2 Methylene Chloride 1 U =-='-----'-'-'c:..=c:...z..:.;=:...;:c......::..;...:..:.==:..:: _______ +-------'--~_.......:o_-~
156-60-5 trans-1,2-Dichloroethene 1 U
75-34-3 1, 1-Dichloroethane 1 U
540-59-0
67 66 3 --
7 4-97-5
7 1-55-6
-.
!
2,2-Dichloropropane 1 U
cis-1,2-Dichloroethene 1 U
Chloroform 1 U I
Bromochloromethane i 1 u
1 1 1-Trichloroethane I 1 u
1 1-Dichloroorooene I 1 u
'
I
i
I --56235=------l-C=a=r~b=on'-'--'-T=-et~ra=c=h=lo~ri=d=e-------+-----1'-'-.+l---=U'--~
j_Q7-06-2'-------1-",2"""-=D"'""'ic'-h_lo_ro_e_th_a_n_e _______ ...-____ 1_+' __ u--i
71-43-2 Benzene ~ I ~
79-01-6 Trichloroethene
78-87-5 1,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 ' trans-1,3-Dichloropropene 1 U
79-00-5 1 1 2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
_1_06-93-4 1,2-Dibromoethane ! 1 1 U
108-90-7 Chlorobenzene 1 U
100-41-4 Eth !benzene 1 U
630-20-6 1, 1, 1,2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U · 100-42=--5-----S=ty~re:....:n'-'-e'-'-"'-'~----------1-----1 --.--Ul
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
•
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•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0191
Lab Name: AMS, Inc. SC Cert.: 07007 ---------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton ---
Matrix: (soil/water) WATER Lab Sample ID: C6-26
Sample wt/vol: 5.0 (g/ml) ML Lab File ID: C6-26.D
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0
---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 U
7 4-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U _7_4 ___ 83 ___ 9 _____ B_ro~m-o_m_e_t-ha_n_e ________ _,_ ____ 1 _ _,__u--'
--'-~-'------------------+----75 -00 -3 Chloroethane 1 U
_ 7§-69-4 Trichlorofluoromethane 1 U
75-35-4 1 1-Dichloroethene 1 U -----~------------· 75-09-2 Methylene Chloride 1 U
_1_§§-60-5 trans-1,2-Dichloroethene 1 U
l§:34_-3 _____ 1~,1_-_D_ic_h_lo_ro_e_th_a_n_e ___ _,_ ___ .__ ____ 29_-,--------;
2 2 D. hi 1 -IC oroorooane ' I u -------' 540-59-0 cis-1 2-Dichloroethene 1 I u '
67-66-3 Chloroform 1 u
74-97-5 Bromochloromethane 1 u ' i I
71-55-6 1 1 1-Trichloroethane 1 u
I 1 1-Dichloroorooene 1 u l I
: 56-23-5 ! Carbon Tetrachloride 1 u
107-06-2 1 2-Dichloroethane . 1 u
71-43-2 Benzene 1 I u i I
' I !~-:Q.1:6 Trichloroethene 1 U ,
78-87-5 1,2-Dichloropropane 1 U · -'-''------~-~~~'----'------!-------f--~u --i. 75-27-4 Bromodichloromethane 1 1
7 4-95-3 Dibromomethane 1 U ·
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 ' trans-1 3-Dichloro ro ene 1 U
79-00-5 1, 1,2-Trichloroethane 1 U
1 ,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
.. 1~06~3-4....:..._ ___ '--"1=,2~-D~·='b~ro~m~o~e=th~a=n=e ______ __,1--____ 1_-1-_U"-----;
1Q_?:9Q::?________ Chlorobenzene 1 U
100-41~-4_.:__ ____ E=t~h~Yl~b~en~z~e~n~e---------+-----1~ U
630-20-6 1, 1, 1 ,2-Tetrachloroethane 1 U . J_08-~38"'---"-3 _____ m_e_ta~,~Pa_r_a-_X~y_le_n_e _______ -+-____ 2_-+-_U_--j1
95-4 7-6 ___ ,....=.o"""rt'-'-ho"'--"--X"'-yl=e'-'-ne"'------------1------1-'---1---'U"'-.__j
100-42-5 Styrene 1 U ·
98-82-8 lsopropylbenzene 1 UU \
75-25-2 Bromoform 1
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-1)211
Lab Name: AMS, Inc. SC Cert.: 07007 --'-----------~ ----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample lb: C7-5 Matrix: (soil/water)
Sample wt/vol:
------
5.0 (g/ml) ML ---
Level: (low/med) LOW ----
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C7-5.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (ul) Soil Aliquot Volume:
GAS NO.
-
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3 ; 75-69-4
75-35-4 ....
75-09-2
_156-60-5
75-34-3
540-59-0
-· 6~-66-3
74-97-5
i· 71-55-6
·-----· 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
74-95-3 ..
10061-01-5 ·-
_108-88-3
10061-02-6
79-00-5 ·-
-·-127-18-4
124-48-1 ' 106-93-4 ·-
... J_Q~:.90-7
100-41 4 -
6
1
9
1
9
7
30-20-6
08-38-3
5-47-6
00-42-5
8-82-8
5-25-2
-
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg) UG/L ----
Dichlorodifluoromethane
Chloromethane
Vinvl Chloride
Bromomethane I i
Chloroethane I
Trichlorofluoromethane I
I
' 1 1-Dichloroethene i
Methvlene Chloride
trans-1 2-Dichloroethene
1 1-Dichloroethane
2 2-Dichloroorooane I
' cis-1 2-Dichloroethene
I Chloroform I
i Bromochloromethane
I 1.1 1-Trichloroethane I
! 1 1-Dichloroorooene
' Carbon Tetrachloride ' 1 2-Dichloroethane
' Benzene
Trichloroethene
I 112-Dichloroorooane
Bromodichloromethane I
I
' Dibromomethane I
I ! cis-1 3-Dichloroorooene I
I I Toluene I
I trans-1 3-Dichloropropene
: 1 1.2-Trichloroethane I I : 1,3-Dichloropropane
: Tetrachloroethene I
' Dibromochloromethane !
I 1 2-Dibromoethane
Chlorobenzene i
Ethvlbenzene
1 1 1 2-Tetrachloroethane I
meta ,oara-Xvlene I i
ortho-Xvlene I
I
Stvrene
I sooroovlbenzene I i
Bromoform i
FORM I VOA
Q
1 u
1 u
1 u
1 u
1 u
1 u·
1 . u
1 u
1 u
1 u
1 u
1 u
1 .. u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
2 u
1 u
1 u
1 u
1 u
(ul)
i
I
i
!
'. i
I
I
I
!
I
I
I
i
I
I
I
!
i
I
I
!
I I
l
I
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0211 Lab Name: AMS, Inc. SC Cert.: 07007 ----------------....._~~~~~--'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
I WATER Lab Sample ID: C7-5 Matrix: (soil/water)
Sample wt/vol:
-------I 5.0 (g/ml) ML C7-5.D ---Lab File ID:.
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Recei~ed: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
79-34-5 1 1 2 2-Tetrachloroethane 1 U
(ul)
----~~~-------------;-------~---' 96-18-4 ----~-1_,_,2~•..o..3-_T_ri~ch'-l_or-"o-'-'"p~ro"""'p""""'a_ne"'-------+-----_1-'---+---'U _ __,
n-Propylbenzene 1 U
, _______ Bromobenzene 1 U
__ ~--~1~·~3~,5--T~r~im~e~th~Y~lb~e~n=z~en~e=-------'------1,__-1-___::U~___,
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1,2,4-Trimethylbenzene 1 U
sec-Butylbenzene 1 U
para-lsopropyltoluene 1 U
541 73 1 1 3 D' hi b 1 u --. -IC oro enzene : . -106-46-7 ; 1 4-Dichlorobenzene 1 u i I -I n-Butvlbenzene 1 u !
95-50-1 I 1,2-Dichlorobenzene 1 u ! -96-12-8 i 1 2-Dibromo-3-chloroorooane 1 u i
1_?0-82-1 ' 1,2,4-Trichlorobenzene _.1 ! u !
87 -68-3 Hexachlorobutadtene 1 U
91-20-3 ---~-N_a~ph_th_a_le_n_e _________ ~ ____ 1_.....___u _
__ ___ -------'---1 ~2~3~-T_r_ic~h_lo-'--ro""'"b_e-'--n~z_en_e'-------~~----1 _ __,___U~._j
FORM I VOA 3/90
•
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0212
Lab Name: AMS, Inc. SC Cert.: 07007 ---'------~--------'--~~~~~--'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER
5_.o___ (g/ml) ry1L __
Level: (low/med) L<?'vY_ __ .
% Moisture: not dee.
GC Column: VQ~_O_L_ ID: 9±§__ (mm)
Soil Extract Volume: (uL) ----
Lab Sample ID: C7-24 -----
Lab File ID: C7-24.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
···-·· 75-71-8 Dichlorodifluoromethane 1 u I ···-----74-87-3 Chloromethane 1 u : -=---i
75-01-4 Vinyl Chloride 1 u ·-... -·---· ?.4.:?3:.~ -Bromomethane 1 u
75-00-3 Chloroethane 1 u -·· -------75-69-4 Trichlorofluoromethane 1 u ·--------75-35-4 1 1-Dichloroethene 1 u
75-09-2 Methylene Chloride 1 u -------· 156-60-5 trans-1,2-Dichloroethene 1 u ·---------75-34-3 1, 1-Dichloroethane 1 u ----
-------2,2-DichloroQroQane 1 u
_§.40-§_~:P ___ cis-1 ,2-Dichloroethene 1 u
67-66-3 Chloroform 1 u --------· u ! .Z1.:-§)7-5 Bromochloromethane 1
71-55-6 1, 1, 1-Trichloroethane 1 u---1 . -----·---I 1, 1-DichloroQrOQene 1 LJ I ------·--· :____i ~§-~.?-=-~----. Carbon Tetrachloride 1 u
107-06-2 1 2-Dichloroethane 1 u -i ------71-43-2 Benzene 1 u I
I
79-01-6 Trichloroethene 1 u ' -. ·-· ·---· --i ??._-87-5 1,2-DichloroQrOQane 1 u I
75-27-4 Bromodichloromethane 1 u !
I
74-95-3 Dibromomethane 1 u I
.1-0061-01-5 cis-1 3-Dichloropropene I 1 u
108-88-3 Toluene ! 1 u
10061-02-6 trans-1, 3-DichloroQrOQene I 1 u
79-00-5 1, 1,2-Trichloroethane I 1 u
1,3-DichloroQroQane 1 u -127-18-4 Tetrachloroethene 1 u
124-48-1 Dibromochloromethane 1 u
106-93-4 1,2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u ·-·--·-----·-··· -
100-41-4 Ethyl benzene 1 u
630-20-6 1 1j,2-Tetrachloroethane 1 u I _J
108-38-3 meta,Qara-Xylene 2 u :
-~~-4_?_:-§_ __ ortho-Xylerie 1 u
100-42-5 Styrene 1 u ·------98-82-8 I SOQrOQY !benzene 1 u
75-25-2 _ . _____ i:i~QfflOf_Q!IlJ. . _ _ _ 1 u
FORM IVOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0212
Lab Name: AMS, Inc. SC Cert.: 07007 ~-'-----------~ ---~I-~~~~~~---'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
----I
WATER
5.0 (g/ml) ML
Lab Sample IQ: C7-24 -----
Lab File ID: C7-24.D
Matrix: (soil/water)
Sample wt/vol: ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Aliquot V0lume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L a
(uL)
u Z.~:34-5 ---~-1~, 1"'""',_2~,2_-T_e_tr_a_c_hl_or_o~e_th_;_a_ne _____ -;--____ 1_+-----"---i u 96-18-4 ---~-1-'-'"'=2,<...;:;3_-T'-'-r'-'-ic-'-'h'"""lo-'ro'""p-'-ro""""p'"""'a"""'n""""e ___________ -'1--1-----"'-
, n-Propylbenzene 1 u--!
Bromobenzene 1 u
1 3 5-Trimeth !benzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
tert-Butylbenzene 1 u
1,2,4-Trimethylbenzene 1 u
sec-Butylbenzene 1 u
para-lsopropyltoluene 1 u
u . ?41:?3-1 ___ ~_1-L..,3_-_D_ic_h_lo_ro_b_e_nz_e_n_e ______ -+ _____ 1 _+----"---i
u 106-46-7·-----+--'1-L-4"--=D-'ic-'-'h"""'lo"'""ro'-'b'-e-'-'nz_e"-n""""e ______ -+----·--'-1-+------"---i
n-Butvlbenzene : 1 U·· ---' I ' 95-50-1 1 2-Dichlorobenzene 1 ' u i
96-12-8 I 1 2-0ibromo-3-chloroorooane I 1 i u I
120-82-1 i 1 2.4-Trichlorobenzene I 1 I u
87-68-3 Hexachlorobutadiene I 1 I· u
91-20-3 Naphthalene u
1 2 3-Trichlorobenzene 1 u
FORM I VOA 3/90
•
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0226
Lab Name: AMS, Inc. SC Cert.: 07007 ----------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton ----
Matrix: (soil/water) WATER Lab Sample ID: C8-5 -------
Sample wt/vol: 5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C8-5.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane I 1 u --74-87-3 Chloromethane I 1 u ..
75-01-4 Vinvl Chloride I 1 u
74-83-9 Bromomethane : 1 u
75-00-3 Chloroethane 1 I u
75-69-4 ; Trichlorofluoromethane 1 u
I
·-75-35-4 i 1, 1-Dichloroethene 1 u
75-09-2 I Methvlene Chloride 1 u .. -
156-60-5 i trans-1 2-Dichloroethene 1 u
75-34-3 i 1, 1-Dichloroethane 1
2 2-Dichloroorooane 1 u --540-59-0 ! cis-1 2-Dichloroethene 1 u . -
67-66-3 Chloroform ! 1 u I
74-97-5 i Bromochloromethane I 1 u -71-55-6 1 1 1-Trichloroethane 1 u -: 1 1-Dichloroorooene 1 u ·-~3-5 I Carbon Tetrachloride I 1 u
107-06-2 I 1 2-Dichloroethane 1 u I -71-43-2 Benzene 1 u -
' 79-01-6 , Trichloroethene 1 u
78-87-5 1 2-Dichloroorooane I 1 u
75-27-4 I Bromodichloromethane i 1 u
7 4-95-3 D1bromomethane 1 u
10061-01-5 _c_is_-1, .. 3 _-D_ichloropropene 1 u
Toluene _ J08-88-3 i I 1 u ' 10061-02-6 : trans-1 3-Dichloroorooene 1 u
79-00-5 1 1 2-Trichloroethane : 1 u
; 1 3-Dichloroorooane : 1 u
127-18-4 ' Tetrachloroethene 1 u -124-48-1 ' Dibromochloromethane 1 u
.J.96-93-4 1 2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u -100-41-4 Ethvlbenzene 1 u
630-20-6 1 1 1 2-Tetrachloroethane 1 u
108-38-3 meta.oara-Xvlene 2 u
95-47-6 ortho-Xvlene 1 u
100-42-5 Stvrene 1 u
98-82-8 lsooroovlbenzene l 1 u
15-?5-2 ___ _-'.·--=B-'--'ro'-'-'m""'o'--'-fo-'-'r-'--'m.:.__ ________ __J_ _____ :1 u
FORM I VOA
(uL)
I
i I
I
I
I
I
I
I
I -j
_j
I
!
I
i
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET.
SC Cert.: 07007 ~ 98-0226
Lab Name: AMS, Inc. ----'----------~.
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C8-5 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML Lab File ID: C8-5.D --------
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1 ."o -----
Soil Aliquot Volume:
CONCENTRATION UNliT"S:
(ug/L or ug/Kg) UG/L Q ----
79-34-5 1, 1 2 2-Tetrachloroethane 1 U
(uL)
96-18~-4-'----·-1-=2~3--T~r~ic-'-h~lo-'-ro'-"--'-ro~a~n~e-------+-----1'---1----"U-~
n-Propylbenzene 1 U
Bromobenzene 1 U
_______________ 1-'-'-'-"-'3~5--T'-'-r-"-im-'-e'-'-th'""'"wC-'Clb-'-'e'-'-n-'-ze-'n-'-'e'-------+-----'1-+--"U _ _,
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U -------------~--'----'-'----'-'---'-----------+-------+---~ tert-Butylbenzene 1 U
I -----, .. -rime 1v enzene i 1 2 4 T . th lb 1 U
, sec-Butvlbenzene 1 u . --; oara-lsooroovltoluene ! u -1 1 ---·--541-73-1 1,3-Dichlorobenzene 1 u
106-46-7 I 1 4-Dichlorobenzene 1 u I
! n-Butvlbenzene 1 u ..
' 95-50-1 i 1 2-Dichlorobenzene 1 u i
96-12-8 : 1 2-Dibromo-3-chloroorooane 1 u I
120-82-1 i 1 2 4-Trichlorobenzene 1 u :
I
87-68-3 Hexachlorobutadiene 1 u '
91-20-3 Na hthalene 1 I u I
·-I 1,2)-Trichlorobenzene 1 u
FORM I VOA 3/90
•
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-02270
Lab Name: AMS, Inc. SC Cert.: 07007 -------------
NC Cert.: 538 Client:· Radian Location: Washin Project: Hamilton ----
Matrix: (soil/water)
Sample wt/vol:
WATER
0.5 (g/ml) ML
Lab Sample ID: C8-24 X10
Lab File ID: C8-24D.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
GAS NO. COMPOUND
Date Received: 04/14/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q ----
. _z_~-71-8 Dichlorodifluoromethane 10 U
7 4-87 -3 Chloromethane 10 U
(ul)
75-01-4 Vinyl Chloride 10 U -----~------------+-------+-----< 74-83-9 _____ Br_o_m_o_m_e_th_a_n_e ________ -,--____ 1'--'0-+----"U _ _,
75-Q_Q-] _________ Chloroethane 1 O U
75-69-4 Trichlorofluoromethane 10 U
7~-:3_5-1_____ 1,1-Dichloroethene 54
75-09-2 __ ~et~ylene_Chlori . ..c..de-"-----·---+----10 _., __ U __
156-60-5 trans-1,2-Dichloroethene 1 O U -· ----~---------: I 75-34-3 1 1-Dichloroethane 980
2,2-Dichloropropane 10 u 1
540-59-0 cis-1,2-Dichloroethene I 110 I • 67-66-3 Chloroform 10 u ' : i
74-97-5 Bromochloromethane 10 u I
71-55-6 ! 1.1 1-Trichloroethane 10 u i
I 1 1-Dichloropropene 10 u I --·--·--' l I I --. q_~ _?3_5 __ Carbon Tetrachloride 10 U
107-06-2 1,2-Dichloroethane 30 -----~-------------+--------+-----< 71-43-2 _____ B_en_z_e_n~e __________ .....;_ ____ 1~0'----+---'U'---1
79-01-6 Trichloroethene 20 ' ------78-87-5 1 2-Dichloro ro ane 10 U -----------~---~~--------:--------+----l 75-27-4 Bromodichloromethane 10 U
7 4-95-3 Dibromomethane 10 U . ·-1-0-06_1 ___ 0_1--5-----...--c-is---1,-3--D-ic_h_lo_r_o_pr_o_p-en-e------+-----1-o-·-1-~
108-88-3 Toluene 11 10 , U I
n 19061-02-6 trans-1,3-Dichloropropene : -10 I u _ __;
__ .7-9-00-5 1, 1 ,2-Trichloroethane 10 U ;
' 1,3-Dichloropro_,p_a_n_e ________ , _____ 10_-+-_U_-l
127-18-4 Tetrachloroethene 10 U . -----------~~-
124-48-1 ____ '-D=ib"-'ro""-m"'-'o'--=c-'-'-h'-"-lo-'--'ro'-'-'m-'-'e"-"th-""a'-"n-"-e· 1 O U
-~~~:~;1-~~jDib~omoethane ~~ ~ - -oro enzene I I ---------
9-4 .:1-:-:~t -----10
63
10
95
10
0-20-6
8-38-3
-47-6
0-42-5
··--· ---------Ethylbenzene ____
1, 1, 1,2-Tetrachloroethane
meta. Para-Xylene
ortho-Xvlene
Stvrene
10 I u
10 u
20 u '
10 u
10 u
i)Ji §_?_L ______ l_s_,op~r_O~PY~lb_e_n_z_e_ne _______ .~ ____ 1_0_..---11 _ _.J
75-25-2 Bromoform 10 ! U i - -
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-02270 Lab Name: AMS, Inc. SC Cert.: 07007 1 -------------
NC Cert.: 538 Client: Radian Location: Wash.in Project: Hamilton • Matrix: (soil/water) WATER Lab Samplt:; ID: C8-24 X10
Sample wt/vol: 0.5 (g/ml) ML Lab File ID: C8-24D.O ---
Level: (low/med) LOW Date Received: 04/14/98
% Moisture: not dee. Date Analyzed: 04/16/98 ---·---------
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0 -------
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 ---~....:.1-'-'1'""',2=-,,=2-_,T-'-e~tr=ac=h~lo=r~oe-'--t"""'h=an'-'-e=------t-------'-1-"--0-r---_U.o...._..~
96-18_-4.;__ ___ .i---..:1~,2=·~3-_,T~ri=ch~l=or~o=p~ro=p=a~ne=-------~----'1~0_..__--=U--:
n-Propylbenzene 1 O U
Bromobenzene 1 O U
1,~§::-Irimethylbenzene 10 U
2-h oroto uene I I ----------CI I 10 U
I 4-Chlorotoluene 10 u i --·· ; tert-Butvlbenzene I 10 : u i
I 1 2 4-Trimethvlbenzene 10 u i '-! i sec-Butvlbenzene 10 u
I para-lsopropyltoluene I 10 u ' ! 541 73 1 · 1 3 Dichlorobenzene 10 u --1 • --i ,, -I
106-46-7 I 1.4-Dichlorobenzene 10 u l ' I n-Butvlbenzene 10 u I
L. I i
: 95-50-1 I 1 2-Dichlorobenzene 10 u
'.. 96-12-8 i 1 2-Dibromo-3-chloropropane 10 u --120-82-1 I 1_,li~.::rrichlorobenzene 10 u
87-68-3 Hexachlorobutadiene ~o I u -·----·--·----=...=.:-==.::.~-===-=-'-'..::..------.......-----'-'--+-~--;
9} ::-_20-~----_. ------~--.:...:N=a.i::.:Ph:..:..:t::...:.ha=l=en:.:.:e~.---------!----_..:..1 O=---t----'U~--1
1,2,3-Trichlorobenzene 10 U
•
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
•
98-0227
Lab Name: _A_M_S...;.., _ln_c_. _________ SC Cert.: _07_0_0_7 __ ....__ _____ _,
•
•
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER
5.0 (g/ml) ML
Lab Sample ID: C8-24 ------
Lab File ID: C8-24.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
' 75-71-8 Dichlorodifluoromethane I 1 U
7 4-87-3 Chloromethane I 1 U
(uL)
___ 7_5-_0_1-_4 _____ V_i_ny~l_C_h_lo_ri_de ________ -+-j ______ 1_+--_u_._j
7 4-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
! 75-69-4 Trichlorofluoromethane 1 U
1 75-35-4 : 1 1-Dichloroethene 69
;-75-09-2 Methvlene Chloride 2
l 156-60-5 trans-1 2-Dichloroethene 1 U
I 75-34-3 I 1.1-Dichloroethane 1300 E
' 2 2-Dichloroorooane 1 U .. ·-·---------~~~-~~--------t-------t-----1
.. 540-59-0 1 cis-1 2-Dichloroethene 35
l 67-66-3 1 Chloroform 1 U
! 7 4-97-5 ! Bromochloromethane 1 U
;_.?1-:.5'"""5_-_6 ___ __,_:_1~1~1_-T_r_ic_h_lo_ro_e_th_a_n_e ______ +--____ 1 ____ U_
I 1 1-Dichloroorooene 1 U l L---------l-'-~~--'-'--'-"---"-"-~""---------1-------+----l 56-23-5 I Carbon Tetrachloride 1 U
' 107-06-2 1 1 2-Dichloroethane 24
. 71-43-2 Benzene 1
! u ·-i
~ 79-01-6 ' Trichloroethene 2
: 78-87-5 i 1 2-Dichloroorooane 1 U i 75-27-4 i Bromodichloromethane 1 U
: 10061-01-5 1 cis-1 3-Dichloroorooene 1 U
L 108-88-3 1 Toluene 1 U
, 10061-02-6 I trans-1 3-Dichloroorooene 1 U I l 79-00-5 : 1, 1,2-Trichloroethane O J
i 1 3-Dichloroorooane 1 U
l-"12~7~-~18~-4-'----:l-'-T~e=tra=c=h~lo=r~oe=t~he=n~e:;__ ______ -1-____ 1_-1----.,.u-,----1
. 124-48-1 i Dibromochloromethane 1 U
1_ 106-93-4 1 2-Dibromoethane 1 U
1 108-90-7 Chlorobenzene 1 U 1
1 100-41-4 Ethvlbenzene 1 U i 630-20-6 I 1 1 1 2-Tetrachloroethane 1 U
'..1_<2§~~3~8-~3'------,--~m~e=ta=·==oar=a~-X~~~ile=n=e'---------t-----0~-t--J'°-_,
95-47-6 ortho-Xvlene 1 U
i 100-42-5 , Stvrene 1 U
~-82-8 ' lsooroovlbenzene 1 I U
75-25-2 Bromoform 1 I U
FORM IVOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0227
Lab Name: AMS, Inc. SC Cert.: 07007 --'------~----------~~~~~~--'
NC Cert.: 538 Client: Radian Location: Wash~ Project: Hamilton
Lab Samplei ID: C8-24 Matrix: (soil/water)
Sample wUvol:
WATER
5.0
-------
(g/ml) ML Lab File ID: C8-24.D ---
Level: (low/med) LOW Date Recei~ed: 04/14/98
' % Moisture: not dee. Date Analyzed: 04/15/98
Dilution Factor: 1.0
!
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (ul) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO . COMPOUND (ug/L or ug/Kg) UG'/L Q
. . -I 79-34-5 1 1 2 2-Tetrachloroethane 1 u I
96-18-4 1,2 3-Trichloropropane 1 u~ n-Propylbenzene 1 u -·----: Bromobenzene 1 u . -I 1 3 5-Trimethylbenzene 1 u
I 2-Chlorotoluene 1 U· : -4-Chlorotoluene 1 u ------tert-Butvlbenzene I 1 u ~ '
I 1 2.4-Trimethvlbenzene 1 u ·-· I sec-Butvlbenzene I 1 u i
1 oara-lsooroovltoluene 1 u I I
541-73-1 i 1 3-Dichlorobenzene 1 u
106-46-7 I 1 4-Dichlorobenzene 1 u
' i n-Butvlbenzene 1 u
-95_-50-1 l 1 2-Dichlorobenzene 1 u
,_9_6-12-8 I 1 2-Dibromo-3-chloroprooane 1 u
120-82-1 I 1,2 4-Trichlorobenzene 1 u
87-68-3 1 Hexachlorobutadiene 1 u
91-20-3 Naohthalene 1 u
1,2,3-Trichlorobenzene 1 u
FORM I VOA 3/90
•
•
•
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-01930
Lab Name: AMS, Inc. SC Cert.: 07007 -----------~ ----~~~~~~~
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water) WATER Lab Sample ID: C9-4 X10 -------
Sample wt/vol: 0.5 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C9-4D.D
Date Received: 04/14/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 10 u -74-87-3 Chloromethane 10 u
75-01-4 I Vinyl Chloride 11 ' I
74-83.,.9 Bromomethane 10 u
75-00-3 I Chloroethane 10 u I -------75-69-4 I Trichlorofluoromethane 10 u
75-35-4 1 1-Dichloroethene 120
75-09-2 Methvlene Chloride 10 u
I 156-60-5 trans-1 2-Dichloroethene 7 J
! 75-34-3 I 1 1-Dichloroethane 390
I 2 2-Dichloroorooane 10 u ' I 540-59-0 cis-1 2-Dichloroethene 960 I
l
' 67-66-3 Chloroform 10 u
' 74-97-5 Bromochloromethane 10 u I 11-55-s 1 1 1-Trichloroethane 10 u l. I I 1 1-Dichloroprooene 10 u
I 56-23-5 I Carbon Tetrachloride 10 u . ··--· -------·----107-06-2 I 1 2-Dichloroethane 13 : 71-43-2 l Benzene 10 u I ,-
79-01-6 I Trichloroethene 480
i 78-87-5 1 2-Dichloropropane 10 u
I 75-27-4 Bromodichloromethane 10 u I
l-74-95-3 Dibromomethane 10 u
: 10061-01-5 cis-1 3-Dichloropropene 10 u
108-88-3 Toluene 10 u
10061-02-6 trans-1 3-Dichloropropene 10 u
79-00-5 1 1 2-Trichloroethane 10 u
I 1 3-Dichloroprooane 10 u
127-18-4 Tetrachloroethene 10 u
124-48-1 Dibromochloromethane 10 u
' 106-93-4 1 2-Dibromoethane I 10 u
108-90-7 Chlorobenzene 10 u -100-41-4 i Ethvlbenzene 10 u --I 630-20-6 1 1 1 2-Tetrachloroethane 10 u
108-38-3 i meta,oara-Xvlene 20 u
95-47-6 ortho-Xvlene 10 u
100-42-5 I Styrene 10 u
98-82-8 lsooroovlbenzene 10 u
' 75-25-2 I Bromoform 10 u ' ·-
FORM I VOA
(ul)
I
l
I
! I --
i
I
i
i
J !
-1
I
I i
I
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-01930
Lab Name: AMS, Inc. --'----------SC Cert.: 07007
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C9-4 X10 Matrix: (soil/water)
Sample wt/vol:
-------
Level: (low/med)
% Moisture: not dee.
~~----(g/ml) ~.!:._ __
LOW
Lab File ID: C9-4D.D
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/14/98
Date Analy~ed: 04/16/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
79-34-5 -. -· ---1,1,2,2-Tetrachloroethane 10 U
96-18-4 1 ,2,3-Trichloropropane 10 U
n-Propylbenzene 10 U
Bromobenzene 10 U
(uL)
---------------------------------+----i 1,3,5-Trimethylbenzene 10 U
2-Chlorotoluene 10 U
----I 4-Chlorotoluene 10 U
tert-Butvlbenzene I 10 u i
1 2 4-Trimethvlbenzene I 10 u I
' i ----
I sec-Butvlbenzene i 10 u I ---·· -I ! ----------Ul 541-73-1 ! 1 3-Dichlorobenzene 10
-~·~P_a_ra_ls_o~p_ro~p~yl_to_lu_e_n_e ______ ~ ____ 1_0_~ U
106-46-7 ! 1,4-Dichlorobenzene i 10 .. U ) -------I n-Butvlbenzene 10 u I : I --I 95-50-1 I 1 ,2-Dichlorobenzene I 10 u I
96-12-8 ; 1.2-Dibromo-3-chloropropane I 10 u j
120-82-1 I 1,2,4-Trichlorobenzene I 10 I u i
87-68-3 Hexachlorobutadiene 10 U
91-20~-3~------'N~a=p~h=th=a~le~n~e _________ _,__ ___ ~1~0-+--~U---j
1,2,3-Trichlorobenzene 10 U
FORM IVOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
•
98-0193
Lab Name: A._M_S_,_l_nc_. _________ SC Cert.: _07_0_0_7 __ ,__ _____ _.
•
•
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C9-4 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML Lab File ID: C9-4.D --------
Level: (low/med) LOW Date Received: 04/13/98
% Moisture: not dee. Date Analyzed: 04/13/98 --
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (ul)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
----------" . -----75-71-8 Dichlorodifluoromethane 1 u
7 4-87-3 Chloromethane 1 u
75-01-4 ._V_i_ny~l_C_h_lo_ri_d_e ________ ~ _____ 9 ___ __,
7 4-83-9 Bromomethane 1
75-00-3 Chloroethane 1
75-69-4 Trichlorofluoromethane 1
u
u
u
__ 7_5-_3_5-4 1, 1-Dichloroethene 120 E , ,-u--, 75-09-2 Methylene Chloride · 1
156-60-5 trans-1 2-Dichloroethene 6 ·-·i
75-34-3 ' 1 1-Dichloroethane 300 E , -----'-'--"-----!--= -I ______ 2~,2_-_D_ic_h_lo_ro~p_ro~p_a_n_e ______ ~L _____ 1--; __ u _ _,
540 59 0 --. 1 2 D" hi th 900 E CJS--IC oroe ene
67-66-3 Chloroform 1 u --74-97-5 : Bromochloromethane 1 u
71-55-6 1.1 1-Trichloroethane 1 u --I
I 1 1-Dichloropropene 1 u ----·--56-23-5
--107 06 2
71-43-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
108-88-3
10061-02-6
I
!
'
' !
Carbon Tetrachloride
1 ,2 D1chloroethane -
Benzene
Trichloroethene
1 2-Dichloropropane
Bromodichloromethane
Dibromomethane
cis-1 3-Dichloropropene
Toluene
trans-1 13-Dichloropropene '
1
8
1
370
1
1
1
1
1
1
I
I
I
I
l
I
I
u I I
I
u
E !
u I
u I
u !
u 1
u '
u -j
I
I I 79-0.~0~-5'--____ 1~,1~,2_-_T_n_ch_lo_r_o_et_h_a_ne ______ -+-_____ 1-,,___U_-;
113-Dichloropropane 1 U
127-18-4 ' Tetrachloroethene 1 U
124-4.~8-~1'-----~D~ib~r~o~m~o~ch~l~or~o~m~e~th~a-~n~e _____ -+--_____ 1_..--_U_-i
106-93-_4'--~----1~,2_-_D_ib_ro_m_o_e_t_ha_n_e _______ -i--____ 1_r-_U_-j
108-90-7 Chlorobenzene 1 U -· u I 100-41-4 Ethvlbenzene 1
630-20-6 1 1 1 2-Tetrachloroethane 1 u
108-38-3 meta.oara-Xvlene 2 u
96-47-6 ortho-Xvlene I 1 u
100-42-5 Stvrene 1 u ~?:81_:§____ lsopropylbenzene 1_-+---_U __ j
7~-2-~-~ _______ Br_o_m_o_fo_r_m _________ ~ _____ 1_~_u_~
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0193
Lab Name: AMS, Inc. SC Cert.: 07007 ---·----~~~-~~~~~~---'
NC Cert.: 538 ----Client: Radian Location: Wash:in Project: Hamilton
Lab Sample ID: C9-4 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) M_L __ _ Lab File ID:, C9-4.D
Level: (low/med) LOW Date Received: 04/13/98
% Moisture: not dee. Date Analyzed: 04/13/98 I
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume:
CAS NO.
79-34-5
96-18-4
--
----
·-·---
--
-··---
l
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg) UG/L
1, 1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
n-Propylbenzene
8 b romo enzene
1 3,5-Trimethvlbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butvlbenzene
1 2 4-Trimethvlbenzene
sec Butylbenzene -_______ ,_
· oara-lsooroovltoluene ----541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene i
' n-Butvlbenzene I --95-50-1 I 1 2-Dichlorobenzene
96-12-8 ! 1 2-Dibromo-3-chloroorooane
120-82-1 ! 1 2 4-Trichlorobenzene
87-68-3 Hexachlorobutadiene ------
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
(uL)
Q
u
u
u
u
u
u ' u !
u
u 1 u
u :
u I
I u i
u !
u i
u I
u I
u :
91-20-3 Na1;1hthalene 1 U ________ ------1-,2~;-3--T-ri-ch-l-or_o_b-en_z_e_n_e------r------1_.,__U___,
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
•
98-0194
b Name: A_M_S_:•:_l_nc_. _________ SC Cert.: 0_7_0_07 ___ '----------J
NC Cert.: 538 Client: Radian Location: Washin. Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
~_.o__ (g/ml) M_L __
LOW
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (ul)
Lab Sample ID: C9-25 -----
Lab File ID: C9-25.D
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 U
7 4-87 -3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1. ___ u"-.
7 4-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
(ul)
75-6_9_-4'-----+--T_ri_ch_l_or_o_fl_uo_r~o_m_e~th_a~ne ______ ;__ ___ -'-1-+--_U~~
75-35-4 ____ __,__1'-'--1-'--=D-'-'ic'""'h"""'lo-'--ro-'-e:C.Oth'--'-e"-'-n-'-"e ______ ---+ ·-----'1'----+---=U'----
75-09-2 ; Methylene Chloride 1 U
156-60-5 trans-1 2-Dichloroethene 1 U • 75-34-3 ' 1, 1-Dichloroethane 3
2,2-Dichloropropane 1 u
540-59-0 cis-1 2-Dichloroethene 3
67-66-3 Chloroform 1 U
74-97-5 Bromochloromethane 1 U
71-55-6 1, 1, 1-Trichloroethane 1 U
1, 1-Dichloropropene 1 U
_56_-2_3_-?::.__ ___ __;:C~a~rb~o"-'-n-'-T-'-e~t~ra=c~h=lo~rid=e. ___________ 1'---~U'----
107-06-2 1,2-Dichloroethane 1 __ __;:U::.___
71-43-2 Benzene 1 U
79-01-6 Trichloroethene 0 J
_]8:-87_-_5__ 1,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 trans-1,3-Dichloropropene 1 U
79-00-5 1 1 2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
106-93-4 1,2-Dibromoethane 1 U
108-90-7 ____ _.c::C...:..;h"""lo'-'-ro-'-'b'-'e'-'-n=ze.::..;n-'-'e'---------------1-'------'U=---
1 00-41-4 Ethylbenzene 1 ----'U'---_
630-20-6 1 1 1 2-Tetrachloroethane 1 U • 108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U
100-42-5 Styrene 1 U
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0194
Lab Name: AMS, Inc. SC Cert.: 07007 ------------~ ----'--~~~~~~ I
NC Cert.: 538 Client: Radian Location: Washin !Project: Hamilton
Lab Sample I~: C9-25 __ _ Matrix: (soil/water)
Sample wt/vol:
WATER
5.0 (g/ml) ML Lab File ID: , C9-25.D
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0
---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0_1§_ (mm) -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
(uL)
79-34-5 ____ --'-1 ~1~2~2~-_T_et_ra_c_h_lo_r_oe_t_ha_n_e _________ --'-1 ___ U'--_
96-18-~4 ____ __:.1=,2~,3~-~T~ric=h~lo~r~o,p~r~o~p=an~e'-------------'-1 ___ U-=--~
n-Propylbenzene 1 ___ u __
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1 ,2,4-Trimethylbenzene 1 U
sec-Butylbenzene 1 U
para-lsopropyltoluene 1 U
541-73-1 1 3-Dichlorobenzene 1 U
106-46-7 1 4-Dichlorobenzene 1 U
n-Butylbenzene 1 U
95-50-1 1 ,2-Dichlorobenzene 1 U
96-12-8 1 ,2-Dibromo-3-chloropropane 1 U
120-82-1 1 2 4-Trichlorobenzene 1 U
87 -68-3 Hexachlorobutadiene 1 U
91-20-3'-------'-N=a=p-'-'ht.:.:..h=a=le~n~e _____________ __;.1 __ -=u-
1 2 3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
.ab Name:
98-0231
AMS, Inc. -------SC Cert.: 07007 ·---------~-------'
NC Cert.: 538 Client: Radian Location: Washir:i Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
Lab Sample ID: C10-4 -------
(g/ml) ML Lab File ID: C10-4.D ---
Level: (low/med) LOW Date Received: 04/15/98
Date Analyzed: 04/15/98 % Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0 ---
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
•
•
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q -----
75-71-8 Dichlorodifluoromethane 1 U
7 4-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
7 4-83-9 Bromomethane 1 U
75-00-_3 ____ --'C~h~lo~r~o_et~h~a_ne _______________ 1:__ _ ___:U=---
75-69-4 Trichlorofluoromethane 1 U
75-35-4 1 1-Dichloroethene 1 U
7§:-0~_-:.?___ Methylene Chloride 1 U
156-60-5 trans-1,2-Dichloroethene 1 U
75-34-3 1 1-Dichloroethane 1 U
2,2-Dichloropropane 1 U
540-59-0
67-66-3
cis-1 2-Dichloroethene O J ___ ..::..:..;:;-'-C=-.:::-'-=~...0....0.."-=~-------------.----;
Chloroform 1 U
74-97-5 Bromochloromethane 1 U
71-55-6 1, 1, 1-Trichloroethane 1 U
1, 1-Dichloropropene 1 U
56-23-5 Carbon Tetrachloride 1 U
107-06-2 1 2-Dichloroethane 1 U ----~----------------------71-43-2 Benzene 1 U
79-91-f?.____ Trichloroethene 2
~~-8--~--=~----1,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U ' .~1~0~06~1~-~0~2-6----~tr~an~s~-~1~,3--D-i-c-ht-o-ro-p-ro_p_e_n_e----------~1--'---=u-:
79-00-5 1, 1 2-Trichloroethane 1 U ·------~-------------------~---i 1,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U ----------------------------'-----"----' 124-48-1 Dibromochloromethane 1 U
106-93-4 1,2-Dibromoethane 1 U
108-9Q-7____ _ ______ Chlorobenzene 1 U
100-4~1~-~4 ____ ~E=t~hY~l~be~n~z~e~n~e ______________ 1'---'----=U=--_,
630-20-6 1 1 1 2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U --------~-------------------'-~ 100-42-5 Styrene 1 U
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0231
Lab Name: AMS, Inc. SC Cert.: 07007 ~--------~-~ ---~ ........... ~~~~~-'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0 (g/ml) ML ---
LOW
GC Column: VOCOL ID: 0.25 (mm)
Lab Sample ID: C10-4 , I
Lab File ID: C10-4.D
Date Received; 04/15/98
Date Analyzed: 04/15/98 -
Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
79-34-5 1 1 2 2-Tetrachloroethane 1
Q
u
1 96-18_-4 ____ ~1~,2~,_3-_T_ri_ch_l_or_o~p_ro~p_a_ne_~--------------u
541-73-1
106-46-7
n-Propylbenzene
Bromobenzene
1, 3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
para-lsopropyltoluene
1 3-Dichlorobenzene
1 4-Dichlorobenzene
n-Butylbenzene
~..§:-fill: 1 ____ -·-1,2-Dichlorobenzene
9.9-J?..:-§.. -· ___ --~-1,2-.Dibromo-3-chloropropane
120-82-1 1,2,4-Trichlorobenzene
87-68-3 Hexachlorobutadiene
91-20-3 Naphthalene
1 2 3-Trichlorobenzene
FORM I VOA
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
(uL)
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
.ab Name:
98-0229
AMS, Inc. --------·-·--SC Cert.: 07007
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: C10-25 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML Lab File ID: C10-25.D ---
Level: (low/med) LOW Date Received: 04/15/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0
% Moisture: r.iot dee.
GC Column: VOCOL ID: 0.25 (mm) ------
Soil Extract Volume: (uL} Soil Aliquot Volume:
•
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
-
75-71-8 Dichlorodifluoromethane 1 U
74-87_-3~----~C-'-h~lo-'-ro~m-'-'-et_h_a_ne __________ . ___ _.:..1_...__-=-U
75-01-4 Vinyl Chloride 1 U
7 4-83-9 Bromomethane 1 U
?_5-QQ_:-_3__ _ _ Chloroethane 1 U
75-69-4 Trichlorofluoromethane 1 U
75-35-4 1 1-Dichloroethene 1 U
75-09-2 Methylene Chloride 1 U
156-60-'5 trans-1 ,2-Dichloroethene 1 U
7 5-34-3 1, 1-Dichloroethane 1 U
540-59--0
67-60-'3
74-97-5
71-55-6
56-23-5
107-06-2
71-43-2
79-01-6
78-87-'5 -------75-27-4
74-95-3
10061-01-5
108-88-'3
10061-02-6
79-00-5
: 2 2-Dichloropropane I 1 u
' cis-1 2-Dichloroethene I 1 u
l Chloroform I 1 u
I Bromochloromethane . I 1 u
1 1, 1, 1-Tnchloroethane 1 U
1, 1-Dichloropropene 1 U
Carbon Tetrachloride 1 U
1 ,2-Dichloroethane 1 U
Benzene 1 U
Trichloroethene 1 U
1 ,2-Dichloropropane 1 U
Bromodichloromethane 1 U
Dibromomethane 1 U
cis-1 3-Dichloro ro ene 1 U
Toluene 1 U
1 trans-1 3-Dichloro ro ene 1 U
1 1 2-Trichloroethane 1 U
(uL)
I
·----·------~1-'-"'-°'"3-~D'-'ic-'-'h-'-lo-'-r--'o-"-p"""""'ro'"Lp""""a"""'n-'-e ____________ 1~_,__U-=---
127-18-4 • Tetrachloroethene 1 U -------------------------~-. 1 ?_4:-:48:.L Dibromochloromethane ------~----_1_~_U
106-93-4 1 ,2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U
1 QQ:-:1_1-_:!___ Ethylbenzene ______ 1 U
630-20-6 1,1,1,2-Tetrachloroethane 1 U • 108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U
100-42-'5 Styrene 1 U ·-----,--~-------------;-------+---98-82 -8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U ·----------=-.o.___----------~
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0229
Lab Name: AMS, Inc. SC Cert.: 07007 -------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton ---1 i Lab Sample UJl: C10-25 Matrix: (soil/water)
Sample wt/vol:
WATER
5_0
LOW
-------
(g/ml) ML Lab File ID: C10-25.D ---
Level: (low/med)
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
GAS NO. COMPOUND
Date Received: 04/15/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
(uL)
79-34-5 1 1,2,2-Tetrachloroethane 1 U -----~~--------------------96 -18 -4 _ J_ ,2,3-Tric_hloropropane ______________ 1 __ ----'U'---
n-Propylbenzene 1 U
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Bu !benzene 1 U
1 2,4-Trimeth !benzene 1 U
sec-Butylbenzene 1 U
para-lsopropyltoluene 1 U
1 3-Dichlorobenzene 1 U 541-73-1
106-46-7 1,4-Dichlorobenzene 1 ___ U __
n-Butylbenzene 1 U
~-~-!?.Q-1 ____ 1"'-''=2--'-D-'-ic"""'"h"'"-lo_r-"-o"-be"""'"n __ z-'-e'-'-ne'------------1'--+-__;;U:..........
99-1 ~-8. _________ 1~,_2-_D_ib_r_o_m_o_-3_-.c_h_lo_r_o~pr_o~p_an_e_ 1 U
120-82-1 1 2,4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20-3-'--____ N_a~p_h_th_a_le_n_e ________________ 1_-------'U'--__.
1 2 3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0230
.ab Name: AMS, Inc. SC Cert.: 07007
-~------~~-----~
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wUvol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: C10-49 -------
Lab File ID: ,C10-49.D
Date Received: 04/15/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u
75-00-3 Chloroethane 1 u
c 75-69-4 Trichlorofluoromethane 1 u
75-35-4 1, 1-Dichloroethene 1 u
75-09-2 Methylene Chloride 1 u
156-60-5 trans-1 2-Dichloroethene 1 u • 75-34-3 1 1-Dichloroethane 1 u
2 2-Dichloro ro ane 1 u
540-59-0 cis-1 2-Dichloroethene 1 u
67-66-3 Chloroform 1 u
74-97-5 Bromochloromethane 1 u '
1, 1, 1-Trichloroethane
----j
71-55-6 1 u I
1 1-Dichloro ro ene 1 u
56-23-5 Carbon Tetrachloride 1 u -------i. 107-06-2 1 2-Dichloroethane 1 I u
71-43-2 Benzene 1 u
79-01-6 Trichloroethene 1 u
78-87-5 1,2-DichloroQroQane 1 u
75-27-4 Bromodichloromethane 1 u
74-95-3 Dibromomethane 1 u -------· 10061-01-5 cis-1, 3-DichloroQrOQene 1 u
108-88-3 Toluene 1
10061-02-6 trans-1,3-DichloroQrOQene 1 u
79-00-5 1 1 2-Trichloroethane 1 u
1,3-DichloroQroQane 1 u
127-18-4 Tetrachl'oroethene 1 u ~
124-48-1 Dibromochloromethane 1 u
106-93-4 1,2-Dibromoethane 1 u
108-90-7 Chiaro benzene 1 u
100-41-4 Ethyl benzene 1 u
630-20-6 1 1 1 2-Tetrachloroethane 1 u • 108-38-3 meta,Qara-Xylene 2 u
95-47-6 ortho-Xylene 1 u
100-42-5 Styrene 1 u
98-82-8 lsoQroQylbenzene 1 u
75-25-2 Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
.ab Name:
98-0195
AMS, Inc. SC Cert.: 07007 ----------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wUvol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0 ·---
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Lab Sample ID: C11-4
Lab File ID: C11-4.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
•
CAS NO.
75-71-8
?4-87-3_
75-01-4
_74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg) UG/L ----
Dichlorodifluoromethane 1
Chloromethane 1
Vinyl Chloride 1
Bromomethane 1
Chloroethane 18
Trichlorofluoromethane 1
1, 1-Dichloroethene 6
Methylene Chloride 3
trans-1,2-Dichloroethene 1
1 1-Dichloroethane 73
2,2-Dichloropropane 1
540-59-0 cis-1,2-Dichloroethene 42
Q
u
u
u
u
u
u
67 -66-3 .. , Chloroform 1 U
(uL)
74-97_-5=-----+---'B~r~o~m~o_ch_l_or~o~m~e~th~a~n~e __________ __.:1_--'-__:::U __
? 1-55-6 1, 1, 1-Trichloroethane 4
1, 1-Dichloropropene 1 U
56-23-5 Carbon Tetrachloride 1 U
107-06-2 1,2-Dichloroethane 1 U
71-43-2 Benzene 1 U
79-01-6 Trichloroethene 1 U
78-87-5 1,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 trans-1,3-Dichloropropene 1 U
I~-00-5 1, 1 2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127 -18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
.1.96-93-4 1,2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U
100-41-4 Ethyl benzene 1 U
_630-20-6 1 1 1 2-Tetrachloroethane 1 U • 108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U
100-42-5 Styrene 1 U
98~~2-~------'ls~o~p~ro~P~Y_lb_e~nz=e~n~e--------'-----~1 __ ~U=---~
7~-~~~:.._ ___ -=B~ro=m~o=f~o~rm'-'----~------------'-1-~~U:::_~
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0195
Lab Name: AMS, Inc. SC Cert.: 07007 -------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
I
WATER Lab Sample ID:' C11-4 Matrix: (soil/water)
Sample wt/vol:
-----
5.0 (g/ml) ML Lab File ID: C11-4.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
GAS NO. COMPOUND
Date Received:: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q ----
79-34-5 1, 1 2,2-Tetrachloroethane 1 U
(uL)
96-18-4 _____ 1~,2~,3_-_T_ri_ch_lo_r_o~p_ro~p_a_ne ___________ 1 ___ u __
n-Propylbenzene 1 U
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1,2,4-Trimethylbenzene 1 U
sec-Butyl benzene 1 U
-para-lsopropyltoluene 1 U
541-73-1 1,3-Dichlorobenzene 1 U
106-46-7 1 4-Dichlorobenzene 1 U
n-Butylbenzene 1 U
95-50-1 1,2-Dichlorobenzene 1 U
96-12-8 1,2-Dibromo-3-chloropropane 1 U
120-82-1 1,2,4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20-3 ------'N-'--a"""'p'-'-h-'--th-'a_le_n-'e ______________ 1'----'----""u'---~
1,2,3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO. • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0196
Lab Name: AMS, Inc. SC Cert.: 07007 ,_ _____ _.. -----'----------------'-
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton ----
Lab Sample ID: C11-25 Matrix: (soil/water)
Sample wt/vol:
WATER.
5.0
-------
(g/ml) _M_L __
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C11-25.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L a
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 ' Bromomethane 1 u
75 00 3 --I Chloroethane 1 u
75-69-4 I Trichlorofluoromethane I 1 u
75-35-4 I 1 1-Dichloroethene I 1 u I I • l 75-09-2 I Methvlene Chloride I 1 u
! 156-60-5 I trans-1 2-Dichloroethene I 1 u
75-34-3 I 1 1-Dichloroethane 1 1 u '
I 2 2-Dichloroorooane I 1 u
540-59-0 I cis-1,2-Dichloroethene ! 1 U ..
I 67-66-3 I Chloroform i 1 u
74-97-5 i Bromochloromethane i 1 u l
i 71-55-6 I 1 1 1-Trichloroethane I 1 u ; I 1 1-Dichlor I I e , opropen 1 u
56-23-5 Carbon Tetrachloride 1 u
107-06-2 1,2-Dichloroethane 1 u
71-43-2 Benzene 1 u
79-01-6 Trichloroethane 1 u -I 78-87-5 1 2-Dichloroorooane I 1 u
75-27-4 ! Bromodichloromethane i 1 u
74-95-3 ! Dibromomethane I 1 u I
10061-01-5 cis-1,3-Dichloroorooene I 1 u
108-88-3 ! Toluene i 1 u
10061-02-6 trans-1 3-Dichloroorooene 1 u
79-00-5 ! 1 1 2-Trichloroethane I 1 u !
! 1.3-Dichloroorooane I 1 u
-i 127 18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
(uL}
L
l
i I
-
i
~
i
-
i
i
:
I
L
!
j
!
!
106-93-4 1,2-Dibromoethane 1 __,_-"U'----'
108-90-7 Chlorobenzene 1 U
100-41-4 Ethyl benzene 1 U • 630-20-6 1, 1, 1,2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U
100-42-5 Styrene 1 U
98-82-.8.;o_ _____ l=-s_op~r_o"".:"py~l_be=n-=z'"""e""""ne~------~-----'1'---'----=U'--__,
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0196
Lab Name: AMS, Inc. SC Cert.: 07007 ,_ _____ __,
-----------~ ----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C11-25 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C11-25.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Vdlume:
CAS NO.
I
79-34-5
96-18-4
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
91-20-3
CONCENTRATION UNIT$:
COMPOUND (ug/L or ug/Kg)·
i
i
'
!
: '
I
:
i
i
1, 112,2-Tetrachloroethane
1 ,2,3-Trichloropropane
n-Propylbenzene
Bromobenzene
1 ,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butvlbenzene
1 2 4-Trimethvlbenzene
sec-Butvlbenzene
oara-lsooroovltoluene
1 3-Dichlorobenzene
1 4-Dichlorobenzene
n-Butvlbenzene
1.2-Dichlorobenzene
1,2-Dibromo-3-chloropropane
1 2 4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1 2 3-Trichlorobenzene
FORM I VOA
UG/L
i
!
!
I I
I
!
I ' !
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Q
u
u
u
u
u
u
u
u
u
u u u
u u u u
u
u
u
u
(uL)
'
:
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0197 • Lab Name: AMS, Inc. SC Cert.: 07007 , _____ --1 -----'-----------~ --~--
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton ----
Matrix: (soil/water) WATER Lab Sample ID: C12-4 -------
Sample wt/vol: 5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C12-4.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor:-1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
•
•
CAS NO.
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
540-59-0
67-66-3 -
i 74-97-5
71-55-6 ..
56-23-5
.. ~07-06-2
71-43-2
79-01-6
78-87-5 : 75-27-4
74-95-3
10061-01-5
108-88-3
10061-02-6
79-00-5
127-18-4
124-48-1
106-93-4
108-90-7
100-41-4
630-20-6
108-38-3
95-47-6
100-42-5
98-82-8
J!?_-25-2
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg)
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
' Trichlorofluoromethane
' 1 1-Dichloroethene .
Methvlene Chloride
l trans-1 2-Dichloroethene
i 1 1-Dichloroethane
l 2 2-Dichloroorooane
I cis-1 2-Dichloroethene
I Chloroform I
I Bromochloromethane
I 1 , 1, 1-Trichloroethane I ~ 1, 1-Dichloropropene
Carbon Tetrachloride
1,2-Dichloroethane
Benzene
1 Trichloroethene
I 1 2-Dichloroorooane . Bromodichloromethane !
I Dibromomethane
; cis-1,3-Dichloroorooene
Toluene
trans-1 13-Dichloropropene
1 1 2-Trichloroethane
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1 2-Dibromoethane
' Chlorobenzene
Ethylbenzene
111, 1,2-Tetrachloroethane
meta, para-Xylene
ortho-Xylene
Styrene
lsopropylbenzene
Bromoform
FORM I VOA
UG/L
l
I
!
I
i
I
!
I
!
! I
1
1
1
1
1
1
2
1
1
4
1
1
1
1
6
1
1
1
1
1
1
1
1
1
1
1
f
1
1
1
1
1
1
1
2
1
1
1
1
Q
u
u
u
u
u u
u
u
u u u
u
u
u
u
u
u
u
u
u
u u u u u
(ul)
I
~
-
u LJ[_
u
u u u
u
u
u u
u
3/90
1A AMS SAMPLE NO. • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0198
Lab Name: AMS, Inc. SC Cert.: 07007 ~------1 -----------~ -----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton ----
Matrix: (soil/water)
Sample wUvol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
Lab Sample ID: C12-18 ------
(g/ml) ML Lab File ID: C12-18.D ---
GC Column: VOCOL ID: 9.25 (mm)
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1. 0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 U
74-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
74-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
75-69-4 Trichlorofluoromethane 1 U
75-35-4 1 1-Dichloroethene 1 U • 75-09-2 Methylene Chloride 1 U
156-60-5 trans-1 2-Dichloroethene 1 U
75-34-3 1 1-Dichloroethane 1 U
2,2-Dichloropropane 1 I U
540-59-0 cis-1,2-Dichloroethene 1 I U
67 -66-3 Chloroform 1 I U
7 4-97 -5 Bromochloromethane 1 I U
(uL)
71-55-6 1, 1, 1-Trichloroethane 1 j U
________ 1,~1_-D_i_ch_l_or_o~p_ro~p_e_ne ______ ___, _____ 1__;___~
•
56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
108-88-3
10061-02-6
79-00-5
Carbon Tetrachloride 1 ; U
1 2-Dichloroethane 1 U
Benzene 1 U
Trichloroethene 1 U
1,2-Dichloropropane 1 U
Bromodichloromethane 1 U
Dibromomethane 1 U
cis-1,3-Dichloropropene 1 U
Toluene 1 U
trans-1,3-Dichloropropene 1 U
1 1 2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127 -18-4 T etrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
106-93-4 1 2-Dibromoethane 1 ->---~·
108-90-7 Chlorobenzene .1 U
100-41-4 Ethyl benzene 1 U
630-20-6 1, 1, 1,2-Tetrachloroethane 1 U -~
108-38-3 meta,para-Xylene 2 U '
95-47_-6=-------o~rt~h~o~-X~v,~le~n~e _____________ ___;1 __ --=u---l
100-42-~5 _____ s_w~r_e_ne _______________ --'-1_,___U~__.
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0198
Lab Name: AMS, Inc. SC Cert.: 07007 --'-----------~ ----'--~~~~~......J
NC Cert.: 538 Client: Radian Location: Washin • Project: Hamilton
Lab Sample jD: C12-18 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C12-18.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
79-34-5 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1 ,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
' tert-Butylbenzene 1 u
1,2,4-Trimethylbenzene 1 u
! sec-Butvlbenzene i 1 u
: oara-lsooroovltoluene I 1 u ' 541-73-1 ; 1 3-Dichlorobenzene ! 1 u
106-46-7 ! 1 4-Dichlorobenzene : 1 u
i n-Butvlbenzene I 1 u
I
(uL)
i
l
:
!
I I
1 95-50-1 1 2-Dichlorobenzene 1 U -···-'------r-~• 0-.---~-'-----------~--....:.......--:--=----' 96-12-8 1,2-Dibromo-3-chloropropane 1 U
120-82-1 1 2,4-Trichlorobenzene 1 U
_8~7~-~68~-~3 ___ __,_-'-'H~ex~a~c~h~lo_ro~b~u=ta=d~ie~n~e'-------------~1-1--~U~~
91-20-3 Naphthalene 1 U
1,2,3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO. • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0199
Lab Name: AMS, Inc. SC Cert.: 07007 '---------' ~--'--~~-----~-~ --~--
NC Cert.: 538 Client: Radian Location: Washin ·Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0 (g/ml) ML ---
LOW
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: C12-29 -------
Lab File ID: C12-29.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND . (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 u I
I
74-87-3 Chloromethane ' 1 u
75-01-4 I Vinyl Chloride 1 u
74-83-9 '! Bromomethane ! 1 u I
-75-00-3 I Chloroethane I 1 u i •·
75-69-4 Trichlorofluoromethane 1 u 1 ; 75-35-4 1 1-Dichloroethene 1 u • i 75-09-2 Methvlene Chloride 1 u i
i 156-60-5 trans-1 2-Dichloroethene 1 u l
I 75-34-3 1 1-Dichloroethane 1 u !
I 2 2-Dichloroorooane 1 u l
540-59-0 cis-1 2-Dichloroethene 1 u I
67-66-3 Chloroform 1 u l
I 74-97-5 Bromochloromethane 1 ll__J
! 71-55-6 1 1.1-Trichloroethane 1 u i I 1 1-Dichloroorooene I 1 u I
I --!
56-23-5 Carbon Tetrachloride ! 1 u
107-06-2 1,2-Dichloroethane 1 u
71-43-2 Benzene 1 u
79-01-6 i Trichloroethene I 1 u
78-87-5 I 1 2-Dichloroorooane 1 u
75-27-4 I Bromodichloromethane l 1 u !
74-95-3 l Dibromomethane 1 u
10061-01-5 I cis-1 3-Dichloroorooene I
I I 1 u !
I 108-88-3 I Toluene ! 1 u i I
' 10061-02-6 I trans-1 3-Dichloroorooene ! 1 u I
l 79-00-5 I 1 1 2-Trichloroethane 1 1 u ' I 1 3-Dichloroorooane ! 1 u !
i I
I 127-18-4 Tetrachloroethene 1 u
124-48-1 I Dibromochloromethane i 1 u !
I I 106-93-4 1 2-Dibromoethane ' 1 u
108-90-7 I Chlorobenzene i 1 u I
100-41-4 I Ethvlbenzene ' 1 u i I • 630-20-6 I 1 1 1 2-Tetrachloroethane I 1 u I
108-38-3 I meta,oara-Xvlene I 2 u i I
95-47-6 ! ortho-Xvlene ! 1 u i
100-42-5 i Stvrene I 1 u ! I ' --98 82 8 ! lsopropylbenzene 1 u
75-25-2 Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0199
Lab Name: AMS, Inc. SC Cert.: 07007 --'-----------------~~~~~~---
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: C12-29 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML Lab File ID: C12-29.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1. 0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 U
96-18-4 1,2,3-Trichloropropane 1 U
n-Propylbenzene 1 U
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1,2,4-Trimethylbenzene 1 U
' sec-Butylbenzene 1 U
para-lsopropyltoluene 1 U
541-73-1 1,3-Dichlorobenzene 1 U
106-46-7 1,4-Dichlorobenzene 1 U
(uL)
------i--n~-B_u_ty~l_b_en_z~e_n_e ___________ ~ 1__,_~U'--~
95-50-1 1,2-Dichlorobenzene 1 U
96-12-8 1,2-Dibromo-3-chloropropane 1 U
120-82-1 1,2,4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U ------+-------< 91-20-3 Naphthalene 1 U
1,2 3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO. • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0200
Lab Name: AMS, Inc. SC Cert.: 07007 ._ _____ __,
-~---------~ ---~ -
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: C13-3 Matrix: (soil/water)
Sample wUvol:
WATER
5.0
-------
(g/ml) ML Lab File ID: C13-3.D ---
Level: (low/med) LOW Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (ul)
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 ' Dichlorodifluoromethane 1 U
74-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
74-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
75-69-4 Trichlorofluoromethane 1 U
75-35-4 ' 1 , 1-Dichloroethene 1 U • 75-09-2 Methylene Chloride i 1 U
156-60-5 trans-1 2-Dichloroethene I 1 U i
; 75-34-3 1 1-Dichloroethane 1 U I
2,2-Dichloropropane 1 U
540-59-0 cis-1,2-Dichloroethene 1 U
67-66-3 Chloroform 1 U
74-97-5 Bromochloromethane 1 U
71-55-6 1 '. 1, 1-Trichloroethane 1 U
1 1-Dichloropropene 1 U
56-23-5 Carbon Tetrachloride 1 U
107-06-2 1,2-Dichloroethane 1 U
71-43-2 Benzene 1 U
79-01-6 Trichloroethene 1 U
78-87-5 1,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
74-95-3 ' Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 trans-1,3-Dichloropropene 1 U
79-00-5 1, 1,2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U _:..:::o..:..._.;_:;_-'"-------"-''"'-'------------------,---124-48 -1 Dibromochloromethane 1 U
_1~0=6~-9~3~-4...:...__ ____ 1~·=2-~D~ib=r=o~m=o=et~h=a~ne"--------------1'--+---=-U --1
108-90-7 Chlorobenzene 1 U
100-41-4 Ethylbenzene 1 U • 630-20-6 1 1 1 2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U
95-47~-6=--------'o~rt=h~o-~X~v~le~n~e----------'--------'1--1----=u~
100-42-5 Styrene 1 U
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET • 98-0232
Lab Name: AMS, Inc. SC Cert.: 07007 ...._ _____ __.
.~~~~~~~~-~~~ ~---
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: C13-24 ------Matrix: (soil/water)
Sample wt/vol:
WATER
5.0 (g/ml) _M_L __ Lab File ID: C13-24.D
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (ul)
GAS NO. COMPOUND
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1. O -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
(ul)
75-71-8 Dichlorodifluoromethane 1 U ·~~---''--~~~i--~~~-~~-~~~-~~4--~~--'---'---"'---
•
I i I
i
' >
l
•
74-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
74-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
75-69-4 Trichlorofluoromethane 1 U
75-35-4 1, 1-Dichloroethene 1 U
75-09-2 Meth lene Chloride 1 U
156-60-5 trans-1 2-Dichloroethene 1 U
75-34-3 1, 1-Dichloroethane 1 U
i 22 o· hi ... -IC oroorooane 1 u
540-59-0 i cis-1 2-Dichloroethene 1 u
67·-B15-3 I Chloroform 1 u
74-97-5 Bromochloromethane 1 u
71-55-6 1.11-Trichloroethane 1 u
1, 1-Dichloroorooene 1 u
56-23-5 Carbon Tetrachloride 1 u
107-06-2 ! 1 ,2-Dichloroethane ! 1 u
71-43-2 Benzene 1 u
79-01-6 ' Trichloroethene 1 u
78..187-5 1,2-Dichloropropane 1 u
75-27-4 Bromodichloromethane 1 u
74-95-3 ' Dibromomethane I 1 u i I
10061-01-5 ' cis-1 ,3-Dichloroorooene 1 u -·
..
100-88-3
10061-02-6
79-00 5 -
121-18-4
124-48-1
106-93-4
108-90-7
100-41-4
630-20-6
108-38-3
95-47-6
100-42-5
98-82-8
. _75-25-2
I Toluene
I trans-1,3-Dichloroorooene
1, 1,2 Trichloroethane -
1 ,3-Dichloropropane
1 Tetrachloroethene
Dibromochloromethane
1 ,2-Dibromoethane
Chlorobenzene
Ethylbenzene
1, 1, 1 ,2-Tetrachloroethane
meta, para-Xylene
ortho-Xylene
Styrene
tsopropylbenzene
Bromoform
FORM I VOA
I
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
....,
' I
-
'
3/90
1A AMS SAMPLE NO. • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-02280
Lab Name: AMS, Inc. SC Cert.: 07007 ----~---~-~-------~~~~~~---'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water) WATER Lab Sample ID: C14-5 X10
Sample wt/vol: 0.5 (g/ml) ML Lab File ID: C14-5D.D -------
Level: (low/med) LOW ----
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Received: 04/15/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q ----
(uL)
. 75-71-8 ·------"""'D--'-icO..C.h--'-lo~r_od_ifl_u-'o--'-ro-'--m_e_t_ha_n_e _____ _._ ___ ----'-10.::__--1---'U"----1
7 4-87-3 Chloromethane 10 U
75 01-4 v· I Chi "d 10 U -' mv on e i :
74-83-9 j Bromomethane : 10 u I
I
i 75-00-3 Chloroethane I 10 u
I 75-69-4 Trichlorofluoromethane I 10 u I I
I 75-35-4 1 1-Dichloroethene 18 • ! 75-09-2 Methvlene Chloride 10 u
i 156-60-5 trans-1 2-Dichloroethene 10 u
: 75-34-3 1.1-Dichloroethane I 87 i 2 2-Dichloroorooane 10 u I
I I
I 540-59-0 i cis-1 2-Dichloroethene 290
67-66-3 ' Chloroform I 10 u !
I 74-97-5 Bromochloromethane 10 u ! 1 1 1-Trichloroethane '10 u I 71-55-6
I 1.1-Dichloroorooene 10 u
! 56-23-5 Carbon Tetrachloride i 10 u i
107-06-2 1 2-Dichloroethane I 10 u i
71-43-2 I Benzene 10 u i ' 79-01-6 l Trichloroethane 66 I
\ 78-87-5 i 1 2-Dichloroorooane i 10 u I
I 75-27-4 Bromodichloromethane l 10 u ...
74-95-3 Dibromomethane i 10 u
10061-01-5 I cis-1 3-Dichloropropene I 10 u I ...
108-88-3 Toluene 10 u :
10061-02-6 I trans-1, 3-DichloroQroQene i 10 u
79-00-5 ! 1 1 2-Trichloroethane I 10 u I
I I I 1 3-Dichloroorooane j 10 u I
I 127-18-4 I Tetrachloroethene ! 10 u ; l 124-48-1 ! Dibromochloromethane I 10 u i I I
I 106-93-4 I 1 2-Dibromoethane I 10 u ! I
I 108-90-7 I Chlorobenzene ! 10 u I
I I
• I 100-41-4 i Ethylbenzene ! 10 u I I
' I 1 1 1 2-Tetrachloroethane 630-20-6 i 10 u i I
108-38-3 i meta,Qara-Xylene ! 20 u !
~ I
95-47-6 ortho-Xylene 10 u
100-42-5 s rene 10 u
i 98-82-8 lsoQroQylbenzene 10 u ..
75-25-2 Bromoform 10 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-02280
Lab Name: AMS, Inc. SC Cert.: 07007 ---------------------·--------'--------'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
0.5
LOW
Lab Sample ID: C14-5 X10
(g/ml) ML Lab File ID: C14-5D.D ---
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/15/98
Date Analyzed: 04/16/98
Dilution Factor; 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 ' 1, 1 ,2,2-Tetrachloroethane 10 U
96-18-4 1 ,2,3-Trichloropropane 1 O U
n-Propylbenzene 1 O U
Bromobenzene 10 U
1 ,3,5-Trimethylbenzene 10 U
2-Chlorotoluene 10 U
4-Chlorotoluene 1 O U
tert-Butylbenzene 1 O U
1 ,2,4-Trimethylbenzene 10 U
sec-Butylbenzene 1 O U
(uL)
~------+---<p~a~ra~-~ls~o~p~ro~P~Y~lto~lu~e~n~e-----~------~1~0--+----=U__;
541-73-1 1,3-Dichlorobenzene 10 U
106-4.6-7
n-Butylbenzene 10 U !
1,4-Dichlorobenzene 10 U
95-50-1 1 2-Dichlorobenzene 10 U
96-12-8 1 2-Dibromo-3-chloro ro ane 10 U
120-82-1 1 2 4-Trichlorobenzene 1 0 U
87-68-3 Hexachlorobutadiene 10 U
91-20-3 Naphthalene 10 U
1 2 3-Trichlorobenzene 10 U
FORM IVOA 3/90
•
•
•
1A AMS SAMPLE NO . • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0228 Lab Name: AMS, Inc. SC Cert.: 07007 .__ _____ _. --'------------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wUvol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0 (g/ml) ML ---
LOW
GC Column: VOCOL ID: 0.25 (mm)
Lab Sample ID: C14-5 -----
Lab File ID: C14-5.D
Date Received: 04/15/98
Date Analyzed: 04/15/98
Dilution Factor: 1. O -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
, 75-71-8 Dichlorodifluoromethane 1 U
7 4-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
7 4-83-9 Bromomethane 1 U ---'------+-----------------+----~---+----_7~5~-~00~-~3 ___ --+_C~hl~o~ro~e~th_a_n~e ________ __.. _____ 1'---!---'u~----l
75-69-4 Trichlorofluoromethane 1 U
· 75-35-4 1 1-Dichloroethene 17 ·-I I • 75-09-2 Methylene Chloride I 1 u ;
·-----· I 156-60-5 trans-1 2-Dichloroethene 5
75-34-3 j 1 1-Dichloroethane 37
2.2-Dichloropropane 1 u I
I 540-59-0 cis-1 2-Dichloroethene 210 E ; I
! 67-66-3 Chloroform 1 u
74-97-5 Bromochloromethane 1 u !
71-55-6 1 1 1-Trichloroethane 1 u !
1 1-Dichloropropene 1 u !
56-23-5 I Carbon Tetrachloride 1 u
107-06-2 I 1 2-Dichloroethane ! 1 u !
71-43-2 Benzene 1 u
79-01-6 -----1--T_ri_ch_l_or_o_e_th_e_n_e ________ ..--____ 6_2_+--_ ___,
78-87-5 1 ,2-Dichloropropane 1 u
75-27-4 Bromodichloromethane 1 u --i
' I I 74-95-3 Dibromomethane 1 u
: 10061-01-5 I cis-1 3-Dichloroorooene 1 u !
l ! 108-88-3 I Toluene 1 u :
10061-02-6 I trans-1 3-Dichloroorooene ' 1 u
I 79-00-5 i 1 1 2-Trichloroethane 1 u : I
I 1 3-Dichlorooropane ! 1 u I -· 127-18-4 I Tetrachloroethene I 1 u
124-48-1 I Dibromochloromethane ! 1 u
106-93-4 i 1 2-Dibromoethane ! 1 u ;
108-90-7 Chlorobenzene 1 u ----100-41-4 i Ethvlbenzene 1 u • 630-20-6 I 1, 1, 1,2-Tetrachloroethane i 1 u '
I I -I 108-38-3 ! meta, oara-Xvlene 2 u '
95-47-6 I ortho-Xvlene 1 u ---;
100-42-5 I S!vrene 1 u I ..
98-82-8 I lsopropylbenzene 1 u I
75-25-2 ' Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0228
Lab Name: AMS, Inc. SC Cert.: 07007 , --'------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: C14-5 ------
Lab File ID: C14-5.D
Date Received: 04/15/98
Date Analyzed: 04/15/98
Dilution Fader: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/~ Q
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 u
96-18-4 1 ,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1 ,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
i tert-Butvlbenzene 1 u
I 1 2.4-Trimethvlbenzene 1 u
! sec-Butvlbenzene 1 u
para-Isopropyltoluene 1 u
541-73-1 1 3-Dichlorobenzene 1 u
; 106-46-7 1 4-Dichlorobenzene 1 u
n-Butvlbenzene 1 u
95-50-1 1 ,2-Dichlorobenzene 1 u
96-12-8 1 2-Dibromo-3-chloro ro ane 1 u
120-82-1 1 2 4-Trichlorobenzene 1 u
87-68-3 Hexachlorobutadiene 1 u
91-20-3 Naphthalene 1 u
1 2 3-Trichlorobenzene 1 u
FORM I VOA
(uL)
i i
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET'
98-0224
Lab Name: AMS, Inc. --'---------SC Cert.: 07007 ----
NC Cert.: 538 Client: Radian Location: Washiri Project: Hamilton
WATER Lab Sample ID: C14-23 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: . C14-23.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 1 ,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u -1 3 5-Trimethvlbenzene I 1 u ' 2-Chlorotoluene i i 1 u
I 4-Chlorotoluene : 1 u
tert-Butvlbenzene : I 1 u I
! 1 2 4-Trimethvlbenzene I 1 u '
·---~
I sec-Butylbenzene ; 1 u .. I : oara-lsooroovltoluene i 1 u
(uL)
-
---! 541 7~3~1---~'~1~3-=D~1=c~hl~o~ro=b~e~nz=e~n=e ___________ ~1-:---~U=-__,
106-46-7 1_4-Dichlorobenzene 1 U
n-But !benzene 1 U
95-50-1 1 2-Dichlorobenzene 1 U
_:;_96~--"1=2....::-8:__ ___ ;..........;1""',2"""-=D=ib ....... ro ....... m_o~--"'3-'-c'"'"'h~lo:..o..ro""""p'-'-r"""'op"-'a=n=e-__ ........J.!._,..----'1'---+---=U'--_,
120-82-1 1,2,4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20,~-3=----~N~a=p~h=th~a=le=n=e=----------~-.........L------'1'--~-=U=---
1 ,2,3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO. • VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0225 Lab Name: AMS, Inc. SC Cert.: 07007 ....._ _____ __. ·---'---------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C14-51 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML Lab File ID: C14-51.D ---
Level: (low/med) LOW Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) ------
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
•
•
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
-
!
----
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u
75 00 3 --I Chi th oroe ane 1 u
75-69-4 ! Trichlorofluoromethane I 1 u
75-35-4 I 1 1-Dichloroethene l ·1 u
75-09-2 I Methylene Chloride I 1 u I
156-60-5 I trans-1 2-Dichloroethene l 1 u !
75-34-3 I 1 1-Dichloroethane I 15 i I
! 2 2-Dichloroorooane I 1 u
I 540-59-0 I cis-1 2-Dichloroethene j 25 I ··--l I 67-66-3 Chloroform 1
74-97-5 Bromochloromethane I 1
71-55-6 1.1 1-Trichloroethane i 1
1 1-Dichloroorooene ' 1 i
56-23-5 ~ Carbon Tetrachloride I 1
107-06-2 1 2-Dichloroethane 1
71-43-2 Benzene 1
u
u u u
u
u
u
~
79-01-6 ____ ,_T_ri_c_hl_or_o_e_th_e_ne ________ -+-------'-1-"-6_,__ __
78-87-5 1 ,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1 3-Dichloro ro ene 1 U
108-88-3 Toluene 1 U
10061-02-6 trans-1,3-Dichloropropene 1 U
_7~9~-~0~0-~5 ___ ~,__:..1~,1~,2~-T~r~ic~h~lo~ro~e~t~ha=n~e;__ _____ -1-_____ 1.:.._-1-__;V __
1 ,3-Dichloropropane 1 U
127 -18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
106-93-4 1 2-Dibromoethane 1 U
108-90.~-7 ___ --'-_C~h~lo~r~o~be_n_z~e~ne ________ --l------~1-"----=-U~
100-41-4 Ethylbenzene 1 U
630-20-6 1, 1, 1 ,2-Tetrachloroethane 1 U
108-38-~3-----'--~m~e~ta~·~Pa~r_a_-X~Y~le~n~e ____ . ___ _,_ ____ 2=--_,_---'U=---__,
95-4 7 -6 ortho-Xylene 1 U
100-42-5 Styrene 1 U
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0208
Lab Name: AMS, Inc. SC Cert.: 07007 .__ _____ __.
-----------~ -----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C15-5 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C15-5.D
Date Receiv~d: 04/14/98
I
Date Analyzed: 04/15/98
Dilution Fact0r: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
GAS NO.
79-34-5
96-18-4
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
91-20-3
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg)
!
I I I
1, 1,2,2-Tetrachloroethane
1 ,2,3-Trichloropropane
n-Propylbenzene
Bromobenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butvlbenzene
1,2,4-Trimethylbenzene
sec-Butvlbenzene
! para-lsooroovltoluene
i 1 3-Dichlorobenzene
i 1,4-Dichlorobenzene
i n-Butvlbenzene
I 1 2-Dichlorobenzene
I 1 2-Dibromo-3-chloroorooane
' 1 2 4-Trichlorobenzene
Hexachlorobutad1ene
Naphthalene
1 2 3-Trichlorobenzene
FORM I VOA
UG/L
i
I I !
I
l
i
I
I
!
!
I I
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Q
u
u
u
u
u
u
u u u u u u
u u u
u
u
u
u
u
(uL)
I
:
I
:
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0209
.ab Name: AMS, Inc. SC Cert.: 07007 ----------------""-~~~~~~
NC Cert.: 538 Client: Radian Location: Washiri Project: Hamilton
Lab Sample ID: C15-24 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML Lab File ID: C15-24.D ---
Level: (low/med) LOW ----
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
GAS NO. COMPOUND
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q ----
(ul)
-·-----·-----------------------~---
•
•
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
--540 59 0 -----67-66-3
74-97-5
71-55-6
56-23-5 -107-06-2
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1, 1-Dichloroethene
Meth lene Chloride
1 trans-1 2-Dichloroethene
1, 1-Dichloroethane
2,2-Dichloropropane
--· cis 1 2 Dichloroethene
I Chloroform
' Bromochloromethane
! 1 1 1-Trichloroethane
I 1 1-Dichloroprooene
: Carbon Tetrachloride
' 1 2-Dichloroethane
71-43-2 Benzene
79-01-6 Trichloroethene
78-87-5 1 ,2-Dichloropropane
7 5-27 -4 Bromodichloromethane
7 4-95-3 Dibromomethane
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
' 1 u
l 1 u
I 1 u I
! 1 u !
I 1 u I
! 1 u I
I
1 u
1 u
1 u
1 u
1 u
1 u
1 u 10061-01-5 cis-1 ,3-Dichloropropene ---~-~---~~--------------.---~ 1 u
1 u ---j 108-88-3 1 Toluene
10061-02-6 trans-1 ,3-Dichloropropene
79-00-5 1, 1 ,2-Trichloroethane 1 u
1 ,3-Dichloropropane 1 u
127-18-4 Tetrachloroethene 1 u
124-48-1 ' Dibromochloromethane 1 u
106-93-4 1 2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u
100-41-4 Ethylbenzene 1 u
630-20-6 1 1 1 2-Tetrachloroethane 1 u
108-38-3 meta, para-Xylene 2 u
1 u 95-47-6 ortho-Xylene --------~--~-------------~---"---100-42-5 Styrene 1 u
-9_8_-_82_-_8 n lsopropylbenzene 1 u
75-25-2 Bromoform 1 u
.FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0233
81JlbName:
~CCert.:
AMS, Inc. SC Cert.: 07007 ......__ _____ __, ------------------
538 Client: Radian Location: Washin· Project: Hamilton
Lab Sample ID: C16-4 Matrix: (soil/water)
Sample wt/vol:
WATER
0.5
-------
(g/ml) M_L __ Lab File ID: Ci6-4.D
Level: (low/med) LOW Date Received: 04/15/98 ---
% Moisture: not dee. Date Analyzed: 04/16/98
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 10 u
7 4-87 -3 Chloromethane 1 O u
75-01-4 Vinyl Chloride 10 u
7 4-83-9 Bromomethane 1 O u
75-00-3 Chloroethane 1 O u
75-69-4 Trichlorofluoromethane 10 u
7 5-35-4 1, 1-Dichloroethene 25
75-09-2 Meth lene Chloride 10 U
• --'-15_6_-_60~-~5 ___ -;-_tr_a_ns_-_1~,2_-D_i_ch_l_or_o_et_h_e_ne _____ _,;. _____ 5"---!----'J~_J
75-34-3 1 1-Dichloroethane 150 1 .-=--:'-'-'~---+--''-'--'--=-'-''-""----'~~-------· ·-----'--"-..::...._ ___ -...;
.. .. _ .. ---__ 2~,2_-_D_ic_h_lo~r:o~p_r~op~a_n_e ______ -,....; ____ 1_0_+--_u _ ___,
cis-1 ,2-Dichloroethene 51 540-59-0
67-66 -3 I Chi f 1 ore arm 0 u I
74-97-5 I Bromochloromethane ! 10 u i : 71-55-6 : 1.1.1-Trichloroethane 10 u ! I• I ! 1 1-Dichlorooropene 10 u
56-23-5 I Carbon Tetrachloride I 10 u '
' 107-06-2 1 2-Dichloroethane 10 u
71-43-2 Benzene 10 u
79-01-6 Trichloroethene 10 u
78-87-5 1,2-Dichloropropane 10 u
75-27-4 Bromodichloromethane 10 u
74-95-3 Dibromomethane 10 u -----·---10061-01-5 cis-1,3-Dichloropropene 10 u .
--;
108-88-3 Toluene 10 u
10061-02-6 trans-1,3-Dichloropropene 10 u
_79-00-§ .. ____ , 1 1 2-Trichloroethane 10 u
1,3-Dichloropropane 10 u
127-18-4 Tetrachloroethene 10 u
124-48-1 Dibromochloromethane 10 u
106-93-4 1,2-Dibromoethane 10 u
108-90-7 I Chlorobenzene 10 u
100-41-4 I Ethylbenzene 10 u
630-20-6 ! 1, 1, 1,2-Tetrachloroethane 10 u
19-8-.3?.:l_ -------meta, para-Xylene .. __________ 20 u • 95-47-6 ortho-Xylene 10 u
100-42-5 S!vrene 10 u
98-82-8 lsopropylbenzene 10 u
75-25-2 Bromoform 10 u . ---··-
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0233 Lab Name: AMS, Inc. SC Cert.: 07007 ---'-----------------~~~~~~~
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: C16-4 Matrix: (soil/water)
Sample wUvol:
WATER
0.5
-------
Level: (low/med) LOW
% Moisture: not dee.
(g/ml) ML ---Lab File ID: C16-4.D
Date Received: 04/15/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 GC Column: '{OCO.!::__ ID: 0.25 (mm) -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/l., --+----Q
79-34-5 1, 1,2,2-Tetrachloroethane 10 u
96-18-4 1 ,2,3-Trichloropropane 10 u
n-Propylbenzene 10 u
Bromobenzene 10 u
1 ,3,5-Trimethylbenzene 10 u
2-Chlorotoluene 10 u
' 4 Chlorotoluene -: 10 I u
tert-Butvlbenzene i 10 I u
1 2.4-Trimethvlbenzene I 10 ' u
sec-Butvlbenzene I 10 \ u
para-lsopropyltoluene I 10 ! u
' 541-73-1 1 3-Dichlorobenzene 10 u
106-46-7 1 :4-Dichlorobenzene 10 u
1 n-Butvlbenzene I 10 i u
95-50-1 1 2-Dichlorobenzene l 10 i u
96-12-8 1.2-Dibromo-3-chloroorooane I 10 i u
120-82-1 1 2 4-Trichlorobenzene ! 10 i u I
87-68-3 Hexachlorobutadiene I 10 I u
91-20-3 Naphthalene 10 u
1 2 3-Trichlorobenzene 10 u
FORM I VOA
(UL)
i
'
'
:
'
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0234
Lab Name: AMS, Inc. SC Cert.: 07007 ~---'-----------------~~~~~~--'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample 1.D: C16-18 Matrix: (soil/water)
Sample wt/vol:
I -------
0.5 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: , C16-18.D
Date Received: 04/15/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (ul) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/I., Q
79-34-5 1, 1,2,2-Tetrachloroethane 10 u
96-18-4 1,2,3-Trichloropropane 10 u
n-Propylbenzene 10 u
Bromobenzene 10 u
1,3,5-Trimethylbenzene 10 u
2-Chlorotoluene 10 u
4-Chlorotoluene 10 u
i tert-Butvlbenzene i 10 u
! 1 2.4-Trimethvlbenzene 10 u ; ! sec-Butvlbenzene 10 u
' I oara-lsooroovltoluene 10 u
541-73-1 I 1 3-Dichlorobenzene 10 u
106-46-7 I 1 4-Dichlorobenzene 10 u
I n-Butvlbenzene 10 u ---·---L 95-50-1 i 1,2-Dichlorobenzene 10 u
96-12-8 I 1 2-Dibromo-3-chlorooropane 10 I u
120-82-1 1 2.4-Trichlorobenzene 10 I u
87-68-3 Hexachlorobutad1ene 10 u
91-20-3 Naphthalene 10 u
1 2 3-Trichlorobenzene 10 u
FORM I VOA
(ul)
l
I
!
'
!
I
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0235
•
ab Name: AMS, Inc. SC Cert.: 07007 ~-------J -----'---------------~ -
C Cert.: 538 Client: Radian Location: Wash in· Project: Hamilton
WATER Lab Sample ID: C16-28 Matrix: (soil/water)
Sample wt/vol:
-------
0.5 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C16-28.D
Date Received: 04/15/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 10 u
74-87-3 Chloromethane 10 u
75-01-4 Vinyl Chloride 10 u
74-83-9 Bromomethane 10 u
75-00-3 Chloroethane 10 u
75-69-4 I Trichlorofluoromethane i 10 u
75-35-4 1 1-Dichloroethene 10 u
75-09-2 I Methvlene Chloride 10 u
156-60-5 \ trans-1,2-Dichloroethene 10 u l
• 75-34-3 1 1-Dichloroethane 10 u -; -' -j i 2 2-Dichloroorooane 10 u I
540-59-0 I cis-1 2-Dichloroethene 10 u l
67-66-3 I Chloroform 10 u .. I I
74-97-5 I Bromochloromethane 10 u I I
.]1-55-6 I 1 1 1-Trichloroethane 10 ! u ! I
i 1 1-Dichloroorooene 10 j u !
56-23-5 I Carbon Tetrachloride 10 ! u
107-06-2 1,2-Dichloroethane 10 u
71-43-2 Benzene 10 u
79-01-6 Trichloroethene 10 u
78-87-5 1,2-Dichloro12ro12ane 10 u
75-27-4 Bromodichloromethane 10 u
74-95-3 Dibromomethane 10 u
10061-01-5 cis-1 3-Dichloro ro ene 10 u
108-88-3 1 Toluene 10 u
10061_-02-6 trans-1 3-Dichloro ro ene 10 u
79-00-5 1, 1,2-Trichloroethane 10 u
1,3-Dichloro12ro12ane 10 u
127-18-4 Tetrachloroethene 10 u
124-48-1 Dibromochloromethane 10 u
106-93-4 1,2-Dibromoethane 10 u
108-90-7 Chlorobenzene 10 u
100-41-4 Ethyl benzene 10 u
630-20-6 1, 1, 1,2-Tetrachloroethane 10 u
108-38-3 meta, 12ara-Xylene 20 u _,
• 95-47-6 ortho-X lene 10 u
100-42-5 10 u
~~-§~_-8 ··-10 u
75-25-2 Bromoform 10 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0235 Lab Name: AMS, Inc. SC Cert.: 07007 .... _____ ___.
--'----------~ ---~
NC Cert.: 538 Client: Radian Location: Washini Project: Hamilton
WATER Lab Sample ID: C16-28 Matrix: (soil/water)
Sample wt/vol:
-------
0.5 (g/ml) ML Lab File ID: C16-28.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/15/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 O U
96-18-4 1,2,3-Trichloropropane 1 o U
n-Propylbenzene 10 U
Bromobenzene 1 O U
1,3,5-Trimethylbenzene 10 U
2-Chlorotoluene 1 O U
4-Chlorotoluene 10 U
tert-Butylbenzene 1 O U
1 ,2.4-Trimethylbenzene 10 U
sec-Butylbenzene 1 O U
para-lsopropyltoluene 10 U
541-73-1 1 ,3-Dichlorobenzene 10 U
(ul)
1g~:;46-7 -----.,...-1~,4_-_D_ic_h_lo_ro_b_e_n_ze_n_e ______ -,-____ 1_0_-+-_U~
I n-Butvlbenzene I 10 I u
95-50-1 1 2-0ichlorobenzene I 10 u I ; 96-12-8 1 2-Dibromo-3-chloroorooane I 10 u ;
120-82-1 1 ,2,4-Trichlorobenzene 10 u I
! I I .
87-68-3 i Hexachlorobutadiene l 10 u I
91-20-3 1 Naphthalene ' 10 u I
1,2,3-Trichlorobenzene 10 u
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0206 ~bName:
1illlllc cert.:
AMS, Inc. SC Cert.: 07007 -~~------------~ ~~~~~~ ......
538 Client: Radian Location: Washin · Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
Lab Sample ID: C17-4 -------
(g/ml) ML Lab File ID: C11-4.D ---
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
•
•
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 U
74-87-3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
74-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
75-69-4 Trichlorofluoromethane 1 U
75-35-4 1, 1-Dichloroethene 1 U
75-09-2 Methylene Chloride 1 U
156-60-5 trans-1,2-Dichloroethene 1 U
75-34-3 ' 1, 1-Dichloroethane 1 U
_______ i-=2=,2~-D~i=c~hl~or~o~p~ro~p~a~ne""---~-----''---~--1·=---1--l.:!____;.
..
'
-
,.
540-59-0
67-66-3
74-97-5
71-55-6
56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
108-88-3
10061-02-6
79-00-5
127-18-4
124-48-1
106-93-4
108-90-7
100-41-4
630-20-6
108-38-3
95-47-6
100-42-5
98-82-8
75-25-2
cis-1 2-Dichloroethene 1 U i
I Chloroform : 1 u
! Bromochloromethane 1 u I
! 1 1.1-Trichloroethane 1 u I
i 1 1-Dichloroorooene 1 u :
Carbon Tetrachloride 1 u
1,2-Dichloroethane 1 u
Benzene 1 u
Trichloroethene 1 u
1,2-Dichloropropane 1 u
' Bromodichloromethane 1 u
Dibromomethane 1 u
cis-1,3-Dichloropropene 1 u
Toluene 1 u
trans-1,3-Dichloropropene 1 u --+---1 u ' 1, 1,2-Trichloroethane
1,3-Dichloropropane 1 u
Tetrachloroethene 1 u
Dibromochloromethane 1 u
1 2-Dibromoethane 1 u
Chlorobenzene 1 u
Ethyl benzene 1 u
1, 1, 1,2-Tetrachloroethane 1 u
meta, para-Xylene 2 u
ortho-Xylene 1 u
Styrene 1 u
lsopropylbenzene 1 u
Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0206
Lab Name: AMS, Inc. SC Cert.: 07007 --'------------------~~~~~~--'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: Cl7-4 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---Lab File ID: , C17-4.D
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1 1,2 2-Tetrachloroethane 1 U
96-18-4 1,2,3-Trichloropropane 1 U
n-Propylbenzene 1 U
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Bu !benzene 1 U
1 2 4-Trimeth !benzene 1 U
sec-Butylbenzene 1 U
(ul)
--------J'--'"'-p=ar~a~-l~s~op~r~o~py~lt~o~lu~e~ne-'------------~1-+--...:U .
1 3-Dichlorobenzene 1 U____, 541-73-1
106-46-7 1,4-Dichlorobenzene 1 U
n-Butylbenzene 1 U ··
95-50-1 1 ,2-Dichlorobenzene 1 U
96-12-8 1 ,2-Dibromo-3-chloropropane 1 U
120-82-1 1 ,2,4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20-3 Naphthalene 1 U
1 ,2 3-Trichlorobenzene 1 U
FORMIVOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0207
.ab Name:
. NC Cert.:
AMS, Inc. SC Cert.: 07007 ---"----------------~~~~~~-'
538 Client: Radian Location: Washin · Project: Hamilton
Lab Sample ID: C17-25 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C17-25.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CAS NO.
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg)
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1 , 1-Dichloroethene
Methvlene Chloride
trans-1 2-Dichloroethene
1 1 1-Dichloroethane
UG/L
1
1
1
1
1
1
1
1
1
1
1
Q
u
u
u
u
u
u
u
u
u
u
2,2-Dichloropropane • ' ___, u
I 540-59-0 i cis-1 2-Dichloroethene I 1 u -67-66-3 ! Chloroform i 1 u I
74-97-5 i Bromochloromethane I 1 u I
71-55-6 I 1 1.1-Trichloroethane 1 u :
I 1, 1-Dichloropropene I 1 u I
56-23~-~5-----i--C~a=r~b=o~n~T~et~ra=c~h~lo~r=1d=e------+-------1=------+---.:::U=----
107-06-2 1 ,2-Dichloroethane 1 U
71-43-2 Benzene 1 U
79-01-6 Trichloroethene 1 U
78-87-5 1 ,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
108-88-3 Toluene 1 U
10061-02-6 trans-1 , 3-Dichloropropene 1 ·--l--'U=------~
79-00-5 1, 1 ,2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
106-93-4 1,2-Dibromoethane 1 U
108-90-7 1 Chlorobenzene 1 U
100-41-4 1 Ethylbenzene 1 U
630-20-6 1, 1, 1,2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U • 95-47_-6"-------'o~rt~h~o~-X~y_le~n~e _________ _,__ ___ ----"'1-+--=-U~
1'00-42-5 Styrene 1 U
98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0207 Lab Name: AMS, Inc. SC Cert.: 07007 --'----------~ ----,___~~~~~-'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C17-25 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C17-25.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Fact9r: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/l,. Q
-
-
-
·--'------
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 U
96-1~8-~4 ____ ---'-1=,2~,3~-~T~ric_h_lo~r~o~pr_o~p~an~e'--------~-----'-1-'--_U::;_~
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
91-20-3
n-Propylbenzene 1 U
Bromobenzene 1 U
1 3 5-Trimeth !benzene 1 U
' 2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1 ,2,4-Trimethylbenzene 1 U
sec-Butyl benzene 1 U
1 oara-lsooroovltoluene ! 1 u
i 1 3-Dichlorobenzene
i 1 4-Dichlorobenzene
I n-Butvlbenzene
I 1 2-Dichlorobenzene
i 1 2-Dibromo-3-chloroorooane
1 2 4-Trichlorobenzene
, Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
FORM I VOA
I
I
I
I
' !
1
1
1
1
1
1
1
1
1
u
u
u
u
u
u
u
u
u
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0204 A'3b Name:
~CCert.:
AMS, Inc. SC Cert.: 07007 L----------1 ----'-----------~------
538 Client: Radian Location: Washin" Project: Hamilton
Lab Sample ID: C18-5 Matrix: (soil/water)
Sample wtlvol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C18-5.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
•
•
CAS NO.
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
540-59-0
67-66-3
74-97-5
71-55-6
56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
108-88-3
10061-02-6
79-00-5
127-18-4
124-48-1
106-93-4
108-90-7
100-41-4
630-20-6
108-38-3
95-47-6
100-42-5
98-82-8
75-25-2
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg) UG/L
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1 , 1-Dichloroethene
Meth lene Chloride
trans-1 ,2-Dichloroethene
1, 1-Dichloroethane
' 2,2-Dichloropropane
1 cis-1 ,2-Dichloroethene
Chloroform
Bromochloromethane
1, 1, 1-Trichloroethane
1, 1-Dichloropropene
Carbon Tetrachloride
1 2-Dichtoroethane
Benzene
Trichloroethene
I 1 ,2-Dichloro ro ane
I Bromodichloromethane
Dibromomethane
cis-1 3-Dichloro ro ene
Toluene
trans-1 ,3-Dichloropropene
1 1 2-Trichloroethane
1 ,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
Ethylbenzene
1, 1, 1 ,2-Tetrachloroethane
meta, para-Xylene
ortho-Xylene
Styrene
lsopropylbenzene
Bromoform
FORM I VOA
(uL)
Q
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u·
1 u
1 u ..,
1 u
1 u ·---l
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
2 u
1 u
1 u
1 u
1 u
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0204
Lab Name: AMS, Inc. SC Cert.: 07007 -----------~ ----'--~~~~~--'
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Samplei!D: C18-5 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML Lab File ID:' C18-5.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
GAS NO. COMPOUND
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 U -----~~-------------~----~-~
(uL)
96-18-4 1,2,3-Trichloro.i;i_ro~i;i~a_n'--'-e-------~---1"'---"U:...___
n-Proi;iylbenzene 1 U
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1,2,4-Trimethylbenzene 1 U
sec-Butylbenzene 1 U
para-lsoi;iroi;iyltoluene 1 U
541-73-1 1,3-Dichlorobenzene 1 U
106-46-7 1,4-Dichlorobenzene 1 U -----~------·------+------+----_______ n~·=B~u~ty~l b~e_nz=e~n~e ________ _,_ ____ 1.:...___,_~~
95-50-1 1,2-Dichlorobenzene 1 u 1
96-12-8 1,2-Dibromo-3-chloropropane 1 U
120-82-1 1 2 4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20-3 Nai;ihthalene 1 U
1,2 3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0205 ~bName:
~CCert.:
AMS, Inc. SC Cert.: 07007 ~------J ---=------------------
538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: C18-25 Matrix: (soil/water)
Sample wUvol:
-------
5.0 (g/ml) _M_L __
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: C18-25.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 u -74-87-3 I Chloromethane I 1 u
75-01-4 : Vinvl Chloride I 1 u .
74-83-9 Bromomethane i 1 u I
75-00-3 Chloroethane I 1 u I
I 75-69-4 Trichlorofluoromethane 1 u
75-35-4 11-Dichloroethene 1 u
I 75-09-2 Methvlene Chloride 1 u i 156-60-5 trans-1 2-Dichloroethene 1 u • I 75-34-3 1 1-Dichloroethane 1 u
! i 2.2-Dichloroprooane 1 u I
: 540-59-0 ! cis-1 2-Dichloroethene 1 u l I
I 67-66-3 Chloroform .1 u .. 1
74-97-5 Bromochloromethane 1 -l u I
71-55-6 1 1 1-Trichloroethane 1 u .
1 1-0ichloroorooene 1 u I
56-23-5 Carbon Tetrachloride 1 u
107-06-2 1 2-Dichloroethane j 1 u !
71-43-2 I Benzene 1 u I I I ·-! I 79-01-6 I Tnchloroethene 1 u I 78-87-5 i 1 2-Dichloroorooane I 1 u \
75-27-4 I Bromodichloromethane I 1 u I
: i
74-95-3 I Dibromomethane I 1 u !
10061-01-5 I cis-1 3-0ichloroorooene I 1 u ' ·-! Toluene I ! 108-88-3 ! 1 u I
10061 02-6 I t 1 3 D" hi 1 u -rans--IC oroorooene I
79-00-5 1 1.2-Trichloroethane I 1 I u I
1 3-Dichlorooropane 1 I u ! ·-
127-18-4 Tetrachloroethene 1 I u I
124-48-1 i Oibromochloromethane i 1 I u
I ! 106-93-4 1 1 ,2-01bromoethane 1 u
108-90-7 ! Chlorobenzene 1 u
100-41-4 j · Ethylbenzene
1 1, 1, 1 ,2-Tetrachloroethane
1 u
630-20-6 1 u
108-38-3 I meta.oara-Xvlene ! 2 u I • 95-47-6 ! ortho-Xvlene ! 1 u I
100-42-5 i Stvrene i 1 u '
98-82-8 I lsooroovlbenzene l 1 u
I ; 75-25-2 1 Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0205
Lab Name: AMS, Inc. SC Cert.: 07007 ~~~~--~~----------~~~~~~--1
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Samp1em: C18-25 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: ' C18-25.D
I Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (ul) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/~
-~--
Q
79-34-5 1 1 2 2-Tetrachloroethane 1 u
(uL)
u 96-18_-4~----1~·=2~,3--T~r_ic_h~lo_ro~p_ro~p_a_n_e ________ ~--1"'---_,____;:=---
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
91-20-3
n-Propylbenzene 1
Bromobenzene 1
1 ,3,5-Trimethylbenzene 1
2-Chlorotoluene 1
4-Chlorotoluene 1
tert-Butylbenzene 1
1,2,4-Trimethylbenzene 1
sec-Butylbenzene 1
para-lsopropyltoluene 1
1 3-Dichlorobenzene 1
1,4-Dichlorobenzene 1
n-Butylbenzene 1
1 2-Dichlorobenzene 1
1 '.2-Dibromo-3-chloropropane 1
1,2,4-Trichlorobenzene 1
Hexachlorobutadiene 1
Naphthalene 1
1 2 3-Trichlorobenzene 1
FORM I VOA
u
u
u
u
u
u
u
u
u
u
u
u ____, u
u
u
u
u
u
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0221
AMS, Inc. SC Cert.: 07007 ~---'------------.bName:
NC Cert.: 53 8 Client: Radian Location: Washin· Project: Hamilton
WATER
5.0 (g/ml) ML
Lab Sample ID: G1-20
Lab File ID: G1-20.D
Matrix: (soil/water)
Sample wt/vol: ---
Level: (low/med) LOW Date Received: 04/14/98
% Moisture: not dee. Date Analyzed: 04/14/98
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L ----
(ul)
Q
75-71~-8::__ ___ --=D~ic=h~lo=r~o=di~flu=o~r~om~et=h=a~ne=--------4------~1-4---_U=---~
7 4-87 -3 Chloromethane 1 U
75-01-4 Vinyl Chloride 1 U
7 4 83 9 B om meth 1 U --' r 0 ane --75-00-3 I Chloroethane 1 u
75-69-4 I Trichlorofluoromethane i 1 u ;
I
75-35-4 I 1 1-Dichloroethene I 1 u '
75-09-2 i Methylene Chloride 1 u -I
156-60-5 I trans-1 2-Dichloroethene I 1 u I
1 • 75-34-3 I 1 1-Dichloroethane 1 1 u l
I 2 2-Dichloroorooane ! 1 u -540-59-0 i cis-1 2-Dichloroethene I 1 u I :
67-66-3 i Chloroform I 1 u --,
I ..
74-97-5 ! Bromochloromethane I 1 u I
; 71-55-6 i 1.1 1-Trichloroethane ! 1 u !
i 1 1-Dichloroorooene 1 1 u I
56-2 -i ar on Te c lorid I 35 Cb tra h e 1 U
107-06-2 1 2-Dichloroethane 1 U
71-43-2 ' Benzene 1 _,____U:;___
79-01-._6 ___ ~~T.:...:.ric=h=lo=r-=-oe.:::..;t::...:h=enc:..:e:;__ ____________ 1-=--~~U~_
78-87-5 1 2-Dichloro ro ane 1 U
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061 __ -0~1~-~5---+-~c~is_-1~,3~-~D_ic~h~lo~ro~p~ro~p~e~n~e----~-----'-----1-'---t----'U:;___
108-88-3 Toluene 1 U
10061-02-6 trans-1 3-Dichloro ro ene 1 U
79-00-5 1, 1,2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
106-93-4 1 2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U
100-41-4 Ethyl benzene O J
630-20-6 1, 1, 1,2-Tetrachloroethane 1 ___._......:U"--~
__ 108-38-3 meta, para-Xylene O J • ~~:47-6"--------'o=rt=h=o~-X~y~le~n=e----------'------__:_1_-!----"=-u __
100-42-5 Styrene 1 U --< 98-82-8 lsopropylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
1
98-0221
Lab Name: AMS, Inc. SC Cert.: 07007 .___ _____ __. --'-------------------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
I
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
Lab Sample ID: G1-20 -----
(g/ml) M_L __ Lab File ID: G1-20.D
GC Column: VOCOL ID: q.3§_ (mm)
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L ----'------Q
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 U
96-18-4 1,2,3-Trichloropropane 1 U
n-Propylbenzene 1 U
Bromobenzene 1 U
1 ,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Butylbenzene 1 U
1 ,2,4-Trimethylbenzene 1 U
sec-Butylbenzene 1 U
para-lsopropyltoluene 1 U
541-73-1 1,3-Dichlorobenzene 1 U
106-46-7 1,4-Dichlorobenzene 1 U
n-Butylbenzene 1 U
95-50-1 1,2-Dichlorobenzene 1 U
96-12-8 1,2-Dibromo-3-chloropropane 1 U
120-82-1 1,2,4-Trichlorobenzene. 1 U
(uL)
87-68-3 _____ --'-H_e'-xa'-c_h_lo_ro_b'""""'u_ta_d_ie_n_e__________ 1 __._"""""'u __
91-20_-_3 _____ N_ap~h_t_ha_l_en_e ______________ 1 ___ u __
1,2,3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0222
.ab Name: AMS, Inc. SC Cert.: 07007 '---------1 --'----------~ ----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: G1-30 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab File ID: G1-30.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 u
(uL)
7 4-87-3==---------'C::....:h=lo::....:r-=-o'-'-m'--'-e-'-th=a"-'n..::..e ___________ _ 1 __ ;___.::u:___ _
_7.5-01-4 Vinyl Chloride 1 u
7 4-83-9 Bromomethane 1 u
75-00-3 Chloroethane 1 u
75-69-4 Trichlorofluoromethane 1 u
75-35-4 1, 1-Dichloroethene 1 u
75-09-2 Methylene Chloride 1 u
:. 156-60-5 trans-1,2-Dichloroethene 1 u • ~ 75-34-3 1, 1-Dichloroethane 1 u
2,2-Dichloropropane 1 u
540-59-0 cis-1 ,2-Dichloroethene 1 u
67-66-3 I Chloroform ' 1 u
74-97-5 I Bromochloromethane ' 1 u I I
71-55-6 i 1 1 1-Trichloroethane I 1 u ... I I 1 1-Dichloroorooene ! 1 u
56-23-5 I Carbon Tetrachloride 1 U
107-06-2 1 2-Dichloroethane 1 U
71-43-2 1 Benzene 1 U
79-01-6 · Trichloroethene 1 U
78-87-5 1 ,2-Dichloropropane 1 U
75-27-4 Bromodichloromethane 1 U
74-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloropropene 1 U
. 108-88-3 Toluene 1 U
10061-02-6 trans-1,3-Dichloropropene 1 U
79-00-5 1 1 2-Trichloroethane 1 U
1,3-Dichloroproparie 1' U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane 1 U
)0~~3_-4o.__ ____ 1~,2~-~D-'-ib'--'-ro-'-m~oe=t~ha=n~e:_._ ______ .;__ ___ __;_1_.,----=-U~
108-90-7 Chlorobenzene 1 U
100-41-4 Ethylbenzene 1 U
630-20-6 1, 1, 1,2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U • 95-47-6 ortho-Xylene 1 U
100-42-5 Styrene 1 U
-~8-82-=-8'------~ls::-...:o=p-'-ro"--"p'-'-y""'lb=e"--'n=-ze=n=e'---------------'-1-,....----'U~-
75-25-2 Bromoform 1 U
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0222 Lab Name: AMS, Inc. SC Cert.: 07007 .__ _____ __,
-----------~ ----
NC Cert.: 538 Client: Radian Location: Washin. Project: Hamilton
Lab Sample lb: G1-30 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: G1-30.D
Date Receiv~d: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/l, Q
79-34_-5 _____ 1~·~1,~2~,2_-T_e_t_ra_c_h_lo_ro_e_th_a_n_e ____ ~----1 u
96-18-4 1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
tert-Bu !benzene 1 u
1 2 4-Trimeth !benzene 1 u
sec-Butyl benzene 1 u
para-lsopropyltoluene 1 u
541-73-1 I 1 3-0ichlorobenzene i 1 u
106-46-7 i 1 4-Dichlorobenzene 1 u
i n-Butvlbenzene I 1 u
95-50-1 ' 1 2-Dichlorobenzene : 1 u
(uL)
'
I
'
~6-1 __ 2-_8 ___ ~-1~,2_-D_i_b_ro_m_o_-_3-_c_h_Io_ro~p_ro~p_a_n_e ________ 1 _.--'U'-__,
120-82-1 1,2,4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20-3 Naphthalene 1 U
1,2 3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0223 ~bName:
~CCert.:
AMS, Inc. SC Cert.: 07007 ----'----------~ ----....__~~~~~--'
538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: G1-40 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: G1-40.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 I Bromomethane 1 u I
75-00-3 ! Chloroethane : 1 u
75-69-4 Trichlorofluoromethane 1 u
i 75-35-4 1 1-Dichloroethene I 1 u ! ,
' 75-09-2 Methvlene Chloride \ 1 u
156-60-5 trans-1 2-Dichloroethene I 1 u ' I • ' 75-34-3 1 1-Dichloroethane 1 u
: 2.2-Dichlorooropane I 1 u ' 540-59-0 cis-1 2-Dichloroethene 1 u
; 67-66-3 Chloroform 1 u
I 74-97-5 Bromochloromethane 1 u ! 71-55-6 1 1 1-Trichloroethane 1 u
1 1-Dichloroorooene 1 u
56-23-5 Carbon Tetrachloride I 1 u I
107-06-2 1 2-Dichloroethane : 1 u
.. 71-43-2 Benzene ' 1 u
79-01-6 l Trichloroethene i 1 u I
78-87-5 I 1 2-Dichloroorooane I 1 u -75-27-4 Bromodichloromethane I 1 u ..
74-95-3 Dibromomethane i 1 u
10061-01-5 i cis-1 3-Dichloroorooene ' 1 u I
108-88-3 I Toluene ! 1 u
10061-02-6 trans-1 3-Dichloroorooene I 1 u
79-00-5 1, 1 ,2-Tnchloroethane I 1 u
1 3-Dichloro ro ane 1 u
127-18-4 Tetrachloroethene 1 u
124-48-1 Dibromochloromethane 1 u
106-93-4 1,2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u
100-41-4 I Eth lb IV enzene 1 u
630-20-6 I 1 1 1 2-Tetrachloroethane I 1 u -108-38-3 meta, oara-Xvlene ; 2 u • 95-47-6 ortho-Xvlene I 1 u
100-42-5 Stvrene I 1 u I -· 98-82-8 lsopropylbenzene I 1 u I 75-25-2 Bromoform 1 u
FORM I VOA
(ul)
'
I
I
I
i
I
I
I
'
I
I
I
I
'
I I
I
!
I
I '
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0223
Lab Name: AMS, Inc. SC Cert.: 07007 -~--------------
NC Cert.: 538 Client: Radian Location: Washir] Project: Hamilton ·----
Lab Sample ID: G1-40 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: G1-40.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (ul) Soil Aliquot Volume:
CONCENTRATION UNl\S:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/4 ----'----Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 1 ,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u.
Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u -4-Chlorotoluene I 1 u --
! tert-Butvlbenzene I 1 u -I 1 2 4-Trimethvlbenzene 1 u '.
sec-Butvlbenzene : 1 u
• oara-lsooronvltoluene I 1 u
541-73-1 1.3-Dichlorobenzene i 1 u
106-46-7 I 1 4-Dichlorobenzene : ! 1 u
I n-Bu!z'.lbenzene I 1 u
95-50-1 I 1 2-Dichlorobenzene ! I 1 u
96-12-8 1 ,2-Dibromo-3-chloropropane I 1 u I
120-82-1 1,2,4-Trichlorobenzene 1 u
87-68-3 Hexachlorobutadiene 1 u
91-20-3 Naphthalene 1 u
1 ,2,3-Trichlorobenzene 1 u
FORM I VOA
(uL)
I
:
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0215
Lab Name: AMS, Inc. SC Cert.: 07007 --'-----------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: G2-20 Matrix: (soil/water)
Sample wUvol:
WATER
5.0
-------
(g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: ! G2-20.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 u
96-18-4 1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1 ,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
tert-Bu !benzene 1 u
1,2,4-Trimethylbenzene 1 u
sec-Butyl benzene 1 u
para-lsopropyltoluene 1 u
541-73-1 1, 3-Dichlorobenzene 1 u
-j ! -I 106-46 7 1 4 Dichlorobenzene 1 u
i n-Butvlbenzene I 1 u I -95-50-1 ' 1 2-Dichlorobenzene ; 1 u
96-12-8 i 1 2-Dibromo-3-chloroorooane l 1 u
120-82-1 I 11214-Trichlorobenzene ! 1 u
87-68-3 Hexachlorobutad1ene 1 u
91-20-3 Naphthalene 1 u
1 ,2 3-Trichlorobenzene 1 u
FORM I VOA
(uL)
I
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0216
AabName:
~CCert.:
AMS, Inc. SC Cert.: 07007 ~---'-~~~~~~~~~~--~-'---~~~~~--'
538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: G2-30 -------
Lab File ID: G2-30.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 I Dichlorodifluoromethane 1 u I
74-87-3 Chloromethane I 1 u
75-01-4 ' Vinyl Chloride 1 u
74-83-9 ; Bromomethane ' 1 u
75-00-3 : Chloroethane I 1 u
75-69-4 Trichlorofluoromethane i 1 u
75-35-4 I 1 1-Dichloroethene I 1 u I
75-09-2 ! Methylene Chloride 1 u i
' 156-60-5 I trans-1 2-Dichloroethene 1 u i • 75-34-3 I 1 1-Dichloroethane 1 u I I
! 2 2-Dichloroorooane 1 u l !
540-59-0 i cis-1 2-Dichloroethene 1 u :
I 67-66-3 ' Chloroform 1 u I
I :
i 74-97-5 I Bromochloromethane 1 u : __J
' 71-55-6 I 1 1.1-Trichloroethane 1 u I !
i I 1 1-Dichloroorooene 1 u I ' I
56-23-5 ! Carbon Tetrachloride 1 u I
I
107-06-2 ! 1,2-Dichloroethane 1 u
I 71-43-2 · Benzene I 1 u -79-01-6 Trichloroethene 1 u
78-87-5 I 1.2-Dichloropropane i 1 u
75-27-4 : Bromodichloromethane 1 u
74-95-3 ! Dibromomethane 1 u
. '10061-01-5 cis-1 3-Dichloropropene 1 I u I
108-88-3 Toluene ' 0 J I I I 1006 1-02-6 I rans--IC 1 3 D' hi oroorooene 1 u -I I 79-00-5 1 1 2-Trichloroethane I 1 u
: 1 3-Dichloroorooane ! 1 u
127-18-4 Tetrachloroethene i 1 u . -,
: 124-48-1 Dibromochloromethane I 1 u
106-93-4 1 2-Dibromoethane 1 u
--! 108 90 7 Chlorobenzene 1 u
100-41-4 Ethylbenzene 1 u
630-20-6 I 1 1 1 2-Tetrachloroethane ' 1 u
108-38-3 I meta .oara-Xvlene I 2 u I • 95-47-6 ortho-Xvlene ' 1 u l I
100-42-5 Stvrene ! 1 u
98-82-8 lsooroovlbenzene l 1 u
75-25-2 Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0217
AabName:
~CCert.:
AMS, Inc. SC Cert.: 07007 -----------~ ----......... ~~~~~~
538 Client: Radian Location: Washiri Project: Hamilton
WATER Lab Sample ID: G2-40 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: G2-40.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ----
Soil Extract Volume: (uL) Soil Aliquot Volume:
•
•
CAS NO.
·-
f
i
:
r
'
'
75-71-8
74-87-3
75-01-4
74-83-9
75 00 3 --
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
540-59-0
67-66-3
74-97-5
71-55-6
56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
: 74-95-3
10061-01-5
108-88-3 I• : 10061-02-6 ·-
' 79-00-5
127-18-4
124-48-1
106-93-4
108-90~7
100-41-4
630-20-6
108-38-3
95-47-6
100-42-5
98-82-8
75-25-2
CONCENTRATION UNITS:
COMPOUND (ug/L or ug/Kg) UG/L
Dichlorodifluoromethane
' Chloromethane
!
Vinyl Chloride
Bromomethane
Chi th oroe ane
I Trichlorofluoromethane
I 1 1-Dichloroethene
I Methvlene Chloride
! trans-1 12-Dichloroethene
I 1, 1-Dichloroethane i 2 2-Dichloropropane !
I cis-1,2-Dichloroethene
I Chloroform I
i Bromochloromethane
! 1 1 1-Trichloroethane
i 1 1-Dichlorooropene
; Carbon Tetrachloride
1,2-Dichloroethane
Benzene
Trichloroethane
1,2-DichloroQrOQane
Bromodichloromethane
Dibromomethane
cis-1,3-DichloroQroQene
Toluene
trans-1,3-DichloroQrOQene
1, 1,2-Trichloroethane
1,3-DichloroQroQane
' Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
Ethylbenzene
1, 1, 1,2-Tetrachloroethane
meta,Qara-Xylene
ortho-Xylene
' S!Yrene
lsoQroQylbenzene
Bromoform
FORM I VOA
----
i
i ' I
I
I I
! I
I
I
I I
I
i
i
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
Q
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u u
u
u
u
u
u
u u
u
u
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u u
u
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(uL)
!
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!
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i
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~
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0218
.mfbName:
~CCert.:
AMS, Inc. SC Cert.: 07007 ·-~-------1 :___::_~-----------------
538 Client: Radian Location: Washin· Project: Hamilton
WATER Lab Sample ID: G3-20 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml} _M_L __ Lab File ID: G3-20.D
Level: (low/med) LOW Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) -------'-
Soil Extract Volume: (uL} Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 U
74-87~-=3 ____ ~___::.C~h~lo~ro~m~e~t~ha=n=e;__ _______ __,__ ____ 1'---1-__::U;____;
75-01-4 Vinyl Chloride 1 U
7 4-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
75-69-4 \ Trichlorofluoromethane I 1 u i ·-i 75-35-4 i 1 1-Dichloroethene 1 u : l 75-09-2 Methvlene Chloride 1 u
i 156-60-5 I trans-1 2-Dichloroethene 1 u : • : 75-34-3 1 1-Dichloroethane 1 u I
2 2-Dichloroorooane 1 u !
540-59-0 cis-1.2-Dichloroethene I 1 u I I
' Chloroform l I 67-66-3 1 u
'--74-97-5 Bromochloromethane 1 u l
71-55-6 I 1.1 1-Trichloroethane 1 u. !
1 1-Dichloroorooene 1 u ' l
56-23-5 Carbon Tetrachloride I 1 u I
I ---I 107 06 2 1,2 D1chloroethane 1 u
71-43 2 -I Benzene : 1 u
79-01-6 ! Trichloroethene 1 u '
78-87-5 1.2-Dichloroorooane 1 u '
75-27-4 Bromodichloromethane 1 u ~
74-95-3 Dibromomethane 1 u 1
:
10061-01-5 i cis-1 3-Dichloroorooene 1 u ~
108-88-3 Toluene 1 u I
I I : ----'-10=0~6~1-'0=2~-6.=:,_ __ ,---=:tra='-'n~s~1~,3~0~1~c~hl=o~ro=p~ro=p=e~ne:::_ ____ j__ ___ _..!_1_1---~U=----4
79-00-5 1 1 1 2-Trichloroethane 1 U
1,3-Dichloropropane 1 U
127 -18-4 Tetrachloroethene 1 U
1~4_-4_8_-_1 _____ ;_D_ib-'"r-'-om_oc_h_lo=r_.;:;.o.:.;.m~e-"-th~a""'n-"-e __________ _:_1 __ '----'U=--___,
106-93-4 1,2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U
100-41-4 Ethyl benzene 1 U -I I 630-20-6 1 1 1 2-Tetrachloroethane ! 1 u :
I
108-38-3 I meta.oara-Xvlene I 2 u
95-47-6 I ortho-Xvlene l 1 u i !
100-42-5 I Stvrene I 1 u ' :
--! I • . _ 98 8~ ____ 1_so~p_ro~p~y_lb_e"'""n=ze-'--'n_e _______ ~---1 __,.--=U'----
75-25.~-2~ ____ B_r_o_m_o_fo_rm~---------------'1 __ --=u __
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0218
Lab Name: AMS, Inc. SC Cert.: 07007 --'-----------
NC Cert.: 538 Client: Radian Location: Washin 'Project: Hamilton
WATER Lab Sample ID: G3-20 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) __ M __ L __
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
lab File ID: G3-20.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1. o -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 , 1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
' tert-Butvlbenzene I 1 u ' I
! 1 2 4-Trimethvlbenzene ·1 1 u -I I sec-Butvlbenzene 1 u -para-I so pro pylto lu ene I 1 u
541-73-1 I 1 3-Dichlorobenzene i 1 : u
106-46-7 I 1 4-Dichlorobenzene I 1 u I
n-Butylbenzene 1 u
95-50-1 1 2-Dichlorobenzene 1 u
. 96-12-8 1 2-Dibromo-3-chloro ro ane 1 u
120-82-1 1,2,4-Trichlorobenzene 1 u
87-68-3 Hexachlorobutadiene 1 u
91-20-3 Na~hthalene 1 u
1,2 3-Trichlorobenzene 1 u
FORM I VOA
(ul)
--;
__,
1
3/90
•
•
•
1A AMS SAMPLE NO.
. 98-0219
A"1b Name:
~CCert.:
VOLATILE ORGANICS ANALYSIS DATA SHEET I
AMS, Inc. SC Cert.: _07_0_0_7 __ .___ _____ __.
538 Client: Radian Location: Washin· Project: Hamilton
Matrix: (soil/water) WATER Lab Sample ID: G3-30 -------
Sample wt/vol: 5.0 (g/ml) ML Lab File ID: G3-30.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Received: 04/13/98
Date Analyzed: 04/14/98 ---
Dilution Factor: 1.0 ------
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 U
7 4-87 -3 Chloromethane 1 U
(uL)
75-01-4 ____ ~_V_in~y_IC_h_l_or_id_e _______________ 1 ___ u __
7 4-83-9 Bromomethane 1 U
75-00-3 Chloroethane 1 U
75-69-4 Trichlorofluoromethane 1 U
75-35-4 1 1-Dichloroethene 1 U
75-09-2 Methylene Chloride 1 U -------~-~------------------+--156-60-5 trans-1 ,2-Dichloroethene 1 U • 75-34-3 1 1-Dichloroethane 1 U
2,2-Dichloropropane 1 U
540-59-0 cis-1 2-Dichloroethene 1 u
67-66-3 i Chloroform 1 u .. I
74-97-=5 i Bromochloromethane 1 ·u ~
: 71-55-6 i 1 1 1-Trichloroethane u ! 1 ..
I 1, 1-Dichloro2roQene I 1 u
56-23-5 Carbon Tetrachloride 1 u
107-06-2 1 2-Dichloroethane 1 u
71-43-2 Benzene 1 u
79-01-6 Trichloroethene 1 u
78-87-5 1 2-Dichloro ro ane 1 u
75-27-4 Bromodichloromethane 1 u
74-95-3 Dibromomethane 1 u
10061-01-5 cis-1,3-DichloroQroQene 1 u
108-88-3 Toluene 1 u -·· 10061-02-6 trans-1,3-DichloroQroQene 1 u
79-00-5 1'.1,2-Trichloroethane 1 u
1 u 1 3-DichloroQroQane
127-18-4 Tetrachloroethene 1 u
124-48-1 I Dibromochloromethane 1 u
106-93-4 1 2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u
100-41-4 Ethylbenzene 1 u
630-20-6 1 1 1 ,2-Tetrachloroethane 1 u
108-38-3 meta,Qara-Xylene 2 u • 95-47-6 ortho-Xylene 1 u
100-42-5 S!Yrene 1 u
98-82-8 lsoQroQylbenzene 1 u
75-25-2 Bromoform 1 u
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0219
Lab Name: AMS, Inc. SC Cert.: 07007 ~~--~-----~~ ---~ ,__ __________ ~
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: G3-30 Matrix: (soil/water}
Sample wt/vol:
-------
5.0 (g/ml} ML ---
Level: (low/med} LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm}
Soil Extract Volume: (uL)
Lab File ID: G3-30.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 u
96-18-4 1 ,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
(uL)
----tert-Butylbenzene 1 u
1 ,2,4-Trimethylbenzene 1 u
sec-Butylbenzene 1 u
para-lsopropyltoluene 1 u
541 73 1 --1 3 D. hi b -IC oro enzene I 1 u I
106-46-7 i 1 4-Dichlorobenzene 1 u ' :
! n-Butvlbenzene I 1 u I
95-50-1 I 1 2-Dichlorobenzene I 1 u I
. 96-12-8 1,2-Dtbromo-3-chloropropane 1 u
' 120-82-1 1,2,4-Trichlorobenzene 1 u
87-68-3 Hexachlorobutadiene 1 u ·---· 91-20-3 Naphthalene 1 u
1 2,3-Trichlorobenzene 1 u
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0220
AabName:
~CCert.:
AMS, Inc. SC Cert.: 07007 '------....1 :.._______!.___________ -----
538 Client: Radian Location: Washin Project: Hamilton
Lab Sample ID: G3-40 Matrix: (soil/water)
Sample wt/vol:
WATER
5.0
-------
(g/ml) _M_L __
Level: (low/med) LOW
Lab File ID: G3-40.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) -----
Soil Extract Volume: (ul) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u
75-00-3 1 Chloroethane u
75-69-4 I Trichlorofluoromethane 1 u
i 75-35-4 I 1 1-Dichloroethene 1 u
75-09-2 ! Methvlene Chloride 1 u -
I 156-60-5 I trans-1 2-Dichloroethene I 1 u • ! 75-34-3 I 1 1-Dichloroethane 1 u
I. I 2 2-Dichloroorooane 1 u
I 540-59-0 I cis-1 2-Dichloroethene 1 u I
! 67-66-3 I Chloroform 1 u
! 74-97-5 I Bromochloromethane 1 u
l 71-55-6 I 1 1.1-Trichloroethane 1 u
I i 1 1-Dichloroorooene 1 u
I 56-23-5 i Carbon Tetrachloride 1 u ' 1,2-Dichloroethane 107-06-2 : I 1 u
71-43-2 Benzene 1 u
79 01 6 --Trichloroethene 1 u
78-87-5 ; 1 2-Dichloroorooane 1 u I
' 75-27-4 i Bromodichloromethane I 1 u r 74-95-3 I Dibromomethane l 1 u
10061-01-5 i cis-1 3-Dichloroorooene I 1 u
I 108-88-3 I Toluene I 1 u
! --I - -10061 02 6 , trans 1,3 D1chloropropene 1 U
79-00-5 1 1 2-Trichloroethane 1 U
1 3-Dichloro ro ane 1 U
127-18-4 Tetrachloroethene 1 U
124-48-1 Dibromochloromethane · 1 U
106-93-4 1 2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U
100-41-4 Ethyl benzene 1 U
630-20-6 1, 1, 1,2-Tetrachloroethane 1 U
108-38-3 meta, para-Xylene 2 U
95-47-6 ortho-Xylene 1 U
100-42-5 Styrene 1 U
(uL)
!
I
---;
i :
i
l I
i -1
I
I --;
• _9~8~-=82=-~8 ____ __:...;ls~o~p~ro~P~Y~lb=en~z=e~n~e _______ -1-____ 1.:.._-1---=U~ '
75-25-2 Bromoform 1 U --!
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0220
Lab Name: AMS, Inc. SC Cert.: 07007 , ______ __; --'--------------~ -
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
WATER Lab Sample ID: G3-40 Matrix: (soil/water)
Sample wt/vol:
-------
5.0 (g/ml) ML Lab File ID: G3-40.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Sci! Extract Volume: (uL)
CAS NO. COMPOUND
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ------
Soil Aliquot Vdlume:
CONCENTRATION UNIT$:
(ug/L or ug/Kg) UG/L Q ----
79-34-5 ! 1, 1,2,2-Tetrachloroethane 1 U
(uL)
_96::18-4 _____ 1 ~·2~13_-T_r_ic_h_lo_ro_,p~r_o~pa_n_e __________ __;_1 ____,_-'U=----
n-Propylbenzene 1 U
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U
4-Chlorotoluene 1 U
tert-Bu !benzene 1 U
1 2 4-Trimeth !benzene 1 U
sec-Butylbenzene 1 U
para-lsopropyltoluene 1 U
L.. 541-73-1 1,3-Dichlorobenzene 1 U
:. 106-46-7 1,4-Dichlorobenzene 1 U
' n-Butylbenzene 1 U
95-50-1 1,2-Dichlorobenzene 1 U
96:~~2~-8=------~1~,2=-~D~ib=r~om'-'-'-"-o~-3~-c=h=lo=r~op=r~o~pa=n~e=---------~1"---l------=U"--~
120-82-1 1 2 4-Trichlorobenzene 1 U
87-68-3 Hexachlorobutadiene 1 U
91-20-3 Naphthalene 1 U
1,2,3-Trichlorobenzene 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0216MS
.ab Name:
NC Cert.:
AMS, Inc. SC Cert.: 07007 ...._ ____ __.
------------~ ----
538 Client: Radian Location: Washiri Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER
5.0 (g/ml) ML
Lab Sample ID: G2-30 MS
Lab File ID: G2-30MS.D ---
Level: (low/med) LOW Date Received: 04/14/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) ------
Soil Extract Volume: (ul) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
··-----------------------. -----~---75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u
75-00-3 Chloroethane 1 u
75-69-4 ' Trichlorofluoromethane I 1 u i ' I
75-35-4 l 1 1-Dichloroethene I 54 ! I :
: 75-09-2 I Methvlene Chloride I 1 u i I
156-60-5 I trans-1 2-Dichloroethene I 1 u I ! l 1 1-Dichloroethane I I ' 75-34-3 I 1 u ···-I 212-Dichloropropane 1 u ' ----! • 540 59 0 cis 1 2 Dichloroethene 1 u ----
67-66-3 Chloroform I 1 u I l
I 74-97-5 Bromochloromethane I 1 u ' J. I . ---'
l 71-55-6 1 1 1-Trichloroethane I_ 1 u !
I 1 1-Dichloroorooene I 1 u I ; I
56-23-5 I Carbon Tetrachloride I 1 u ! I
107-06 2 -! 1 2-Dichloroethane ! 2 I I
71-43-2 Benzene 49
79-01-6 Trichloroethene 48
78-87-5 1,2-Dichloropropane 1 u
75-27-4 i Bromodichloromethane i 1 u i i
74-95-3 : Dibromomethane ; 1 u ' I
10061-01-5 I cis-1 3-Dichloropropene ! 1 u i i
108-88-3 l Toluene I 52 I
10061-02-6 ; trans-1, 3-Dichloropropene I 1 u i I ---l 1,1 12-Trichloroethane 1 U i ·--t--u-;---j 1,3-Dichloropropane 1 J 1
79-00-5
:. 127-18-4 Tetrachloroethene 1 U !
124-48-1 Dibromochloromethane 1 U """1
106-93-4 1,2-Dibromoethane 1 U
108-90-7 Chlorobenzene 49
100-41-4 Ethyl benzene 1 U
630-20-6 111, 1,2-Tetrachloroethane 1 U
• 108-3~8~-3=-----'-~mc.:.=et=a~,p~a~ra~-~X~yl=e~ne~--------+----~2'--+---=U-~
· 95-4 7 -6 ortho-X lene 1 U
100-42-5 S rene 1 U
98-82-8 lsopropylbenzene 1 U
75-25~-2=-____ B_r_o_m_o_fo_r_m _________ ~ _____ 1 __ ---'-u __
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0216MS Lab Name: AMS, Inc. SC Cert.: 07007
~---'----~-~------~---
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Lab Sample ID: G2-30 MS
Lab File ID: G2-30MS.D
Date Received: 04/14/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
GAS NO. COMPOUND (ug/L or ug/Kg) UG/L, Q
79-34-5 ' 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 1,2, 3-T richloropropane 1 u
n-Propylbenzene 1 u
, Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u ·-I tert-Butvlbenzene I 1 u
1,2 4-Trimethvlbenzene ! 1 u
: sec-Butvlbenzene ! 1 u
' oara-lsooroovltoluene I 1 u r
541-73-1 I 1,3-Dichlorobenzene : 1 u
106-46-7 1 4-Dichlorobenzene ! 1 u
I n-Butylbenzene 1 u ; I I I 95-50-1 1 1 2-Dichlorobenzene 1 u l ' 96-12-8 ; 1 2-Dibromo-3-chloro.orooane i 1 u
120-82-1 ! 1 2 4-Trichlorobenzene i 1 u I
87-68-3 ! Hexachlorobutadiene I 1 u I
91-20-3 NaQhthalene 1 u
! 1 2 3-Trichlorobenzene 1 u -----
FORM I VOA
(uL)
I
I :
' I I
i
!
I : I I
I
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
98-0216MSD
-ab Name:
~CCert.:
AMS, Inc. SC Cert.: 07007 -~--------------~~~~~~~
538 Client: Radian Location: Washin Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Lab Sample ID: G2-30 MSD
Lab File ID: G2-30MSD.D
Date Received: 04/14/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0 ----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 I Bromomethane ! 1 u
75-00-3 ' Chloroethane I 1 u
: 75-69-4 Trichlorofluoromethane 1 u
; 75-35-4 1 1-Dichloroethene 57 i
I 75-09-2 Methvlene Chloride 1 u
i 156-60-5 trans-1 2-Dichloroethene 1 u • I 75-34-3 1 1-Dichloroethane 1 u
I 2 2-Dichloropropane 1 u
I 540-59-0 cis-1 2-Dichloroethene 1 u l
67-66-3 Chloroform I 1 u
I 74-97-5 Bromochloromethane 1 u
l 71-55-6 1 1.1-Trichloroethane 1 u
I 1 1-Dichlorooropene 1 u
56-23-5 1 Carbon Tetrachloride l 1 u ·-----107-06-2 I 1 2-Dichloroethane i 2
71-43-2 Benzene 49 I ! 79-01-6 Trichloroethene 52 I
78-87-5 ! 1 2-Dichloroorooane 1 u ! 75-27-4 Bromodichloromethane 1 u I
! 74-95-3 Dibromomethane 1 u
10061-01-5 I cis-1.3-Dichloroorooene 1 u
I 108-88-3 Toluene 52
! 10061-02-6 trans-1 3-Dichloropropene 1 u
79-00-5 1.1 2-Trichloroethane 1 u
I 1 1 3-Dichloro~ro~ane I -1 u
; 127-18-4 Tetrachloroethene 1 u
124-48-1 l Dibromochloromethane 1 u I
106-93-4 1 2-Dibromoethane 1 u
i 108-90-7 Chlorobenzene 53
100-41-4 ! Ethvlbenzene 1 u
: 630-20-6 i 1 1 1 2-Tetrachloroethane I 1 u
I 108-38-3 meta .oara-Xvlene 2 u
95-47-6 ortho-Xvlene 1 u
100-42-5 Stvrene i 1 u
L 98-82-8 lsooropvlbenzene 1 u • 75-25-2 Bromoform I 1 I u
FORM I VOA
(uL)
!
I
!
I
I
! :
1
!
I
'
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: I 98-021 SMSD AMS, Inc. SC Cert.: 07007 _ ~---'-~--~----~-------
NC Cert.: 538 Client: . Radian Location: Washin Project: Hamilton
Matrix: (soil/water) WATER Lab Sample ID: G2-30 MSD
Sample wUvol: 5.0 (g/ml) M_L __ _ Lab File ID: G2-30MSD.D ----
Level: (low/med) LOW Date Received: 04/14/98
Date Analyzed: 04/16/98
Dilution Factor: 1.0
----
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm) -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 U
96-18-4 1,2,3-Trichloropropane 1 U
n-Propylbenzene 1 U
Bromo~~ene 1 U
1,3,5-Trimethylbenzene 1 U
(uL)
2-Chlorotoluene 1 U ~---------~------~----+------<---"---< 4-Chlorotoluene 1 U
1-; tert-Bu!J'lbenzene I 1 u
i I 1 2 4-Trimethvlbenzene I 1 u ' j
' I : sec-Butvlbenzene I 1 u L
: oara-lsooroovltoluene i 1 u ' ~
--541 73 1 ! 1,3 D1chlorobenzene -1 u
106-46-7 i 1 4-Dichlorobenzene 1 ! u I r
i i n-Butvlbenzene 1 u
95-50-1 I 1 2-Dichlorobenzene 1 u I 1 2-Dibromo-3-chloroorooane l 96-12-8 i 1 u
120-82-1 i 1 2.4-Trichlorobenzerie 1 u " 8 -68-7 3 Hexachlorobutadiene 1 u
91-20-3 Naphthalene 1 u
1,2,3-Trichlorobenzene 1 u
FORM I VOA 3/90
•
•
•
4A AMS SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
BLANK1
.Lab Name:
NC Cert.:
SC Cert.: 07007 AMS, Inc.
538 Client: Radian Location: Washi'n Project: Hamilton
•
•
Lab File ID: BLANK1.D
Date Analyzed: 04/13/98
GC Column: VOCOL ID: 0.25 (mm)
Instrument ID: GC/MS
Lab Sample ID: Reagent Blank
Time Analyzed: 13:59 -----
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
I I AMS SAMPLE NO.
I 01
02
03
04
05
06
07
08
!
i
i
I
i
I I
I
98-0188
98-0189
98-0191
98-0190
98-0187
98-0192
98-0193
98-0194
COMMENTS:
page 1 of 1
LAB
SAMPLE ID
C5-17
C5-30
C6-26
C6-8
C5-8
C1-19
C9-4
C9-25
FORM IVVOA
I LAB TIME I FILEID ANALYZED
I ' C5-17.D 15:04 I
C5-30.D 16:10
C6-26.D I 17:18
C6-8.D ' 18:32
C5-8.D i 19:34
C1-19.D 20:35
C9-4.D 21:34
C9-25.D 22:34 I _ ___)
3/90
4A AMS SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
BLANK2
Lab Name: AMS, Inc. SC Cert.: 07007 .__ ____ ___.
~----'-~~~~-~-~-~ ~~-~
NC Cert.: 538 Client: Radian Location: Washin Prpject: Hamilton
Lab File ID: BLANK2.D Lab Sample IQ: Reagent Blank
Date Analyzed: 04/14/98 Time Analyzed: 01:08 -----
GC Column: VOCOL ID: 0.25 (mm) Heated Purge: (Y/N) N
Instrument ID: GC/MS
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
I !
' I I AMS SAMPLE NO. i
011 98-0195
021 98-0196
03! 98-0197
04[ 98-0198
051 98-0199
061 98-0200
07: 98-0232
08l 98-0204
09 98-0205
10 98-0216
11 98-0217
12 98-0219
13 98-0220
COMMENTS:
page 1 of 1
LAB
SAMPLE ID
C11-4
C11-25
C12-4
C12-18
C12-29
C13-3
C13-24
C18-5
C18-25
G2-30
G2-40
G3-30
G3-40
FORM IVVOA
LAB
FILEID
C11-4.D
C11-25.D
C12-4.D
C12-18.D
C12-29.D
C13-3.D
C13-24.D
C18-5.D
C18-25.D
G2-30.D
. G2-40.D
G3-30.D
G3-40.D
I
TIME
ANALYZED
02:06
03:03
04:00
04:57
05:55
06:52
07:49
08:46
09:45
12:38
13:38
14:54
15:53
I :
i
•
•
• 3/90
4A AMS SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
BLANK3
•
ab Name: AMS, Inc. SC Cert.: 07007 ..._ ____ ___. ~--'---------------~
C Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab File ID: BLANK4.D
Date Analyzed: 04/14/98
GC Column: VOCOL ID: 0.25 (mm)
Instrument ID: GC/MS ------
Lab Sample ID: Reagent Blank
Time Analyzed: 19:23 -----
Heated Purge: (YIN) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
: I LAB LAB TIME
I AMS SAMPLE NO. I SAMPLE ID FILE ID ANALYZED ' ' I '
I 98-0218 G3-20 G3-20.D ! 16:52 '·-I I 98-0221 G1-20 G1-20.D 20:23 i
i. 98-0222 G1-30 G1-30.D I 21:22
I 98-0223 G1-40 G1-40.D 22:21 ' 98-0215 G2-20 G2-20.D i 23:20 j'
01
02
03
04
05
06
07
08
09
10
11
____.. ii 98-0226 C8-5 C8-5.D 00:20 :
•j 98-0206 C17-4 C17-4.D 01:19 I
I 98-0209 C15-24 C15-24.D ! 02:18 :
ti 98-0224 C14-23 C14-23.D 03:16 I
I 98-0221 C8-24 CS-24.D 04:15 1
.I 98-0225 C14-51 C14-51.D 05:14 I •
COMMENTS: •
page 1 of 1 FORM IVVOA 3190
4A AMS SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
BLANK4 Lab Name: AMS, Inc. SC Cert.: 07007 -----· -~~~~~~~ ~-~-'----~~~~~
NC Cert.: 538 Client:
Lab File ID: BLANK5.D
Date Analyzed: 04/15/98
GC Column: VOCOL ID: 0.25
Instrument ID: GC/MS
Radian
(mm)
Location: Washin Project: Hamilton
Lab Sample ID: Reagent Blank
Time Analyzed: 08:45 -----
Heated Purge: (Y/N) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
I AMS SAMPLE NO. i
I 01
02
03
04
05
06
07
08
09
98-0228
I 98-0229
! 98-0207
I 98-0211
l 98-0208
I 98-0212
l 98-0210
I 98-0230 I 98-0231
COMMENTS:
page 1 of 1
LAB
SAMPLE ID
C14-5
C10-25
C17-25
C7-5
C15-5
C7-24
C1-4
C10-49
C10-4
FORM IVVOA
LAB TIME
FILEID ANALYZED I
I I
C14-5.D I 09:44
C10-25.D 10:45 :
C17-25.D 11:46 I
C7-5.D I 12:53
C15-5.D : 14:57
C7-24.D 16:05 -4 C1-4.D I 17:13
C10-49.D I 18:20 I
I
C10-4.D I 19:23 l I
•
•
•
3/90
4A AMS SAMPLE NO.
VOLATILE METHOD BLANK SUMMARY
•
ab Name: AMS, Inc.
C Cert.: 538 Client: Radian
Lab File ID: BLANK6.D
Date Analyzed: 04/15/98
GC Column: VOCOL ID: 0.25 (mm)
instrument ID: GC/MS
BLANKS
SC Cert.: 07007
Location: Washin Project: Hamilton
Lab Sample ID: Reagent Blank
Time Analyzed: 22: 13 -----
Heated Purge: (YIN) N
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
•
•
i I
I AMS SAMPLE NO. I
,
01
02
03
04
05
06
07
08
09
10
11
I
I
I
1i
98-01890
98-01930
98-02270
98-02280
98-0233
98-0234
98-0235
98-0216MS
98-0216MSO
98-0213
98-0214
COMMENTS:
page 1 of 1
LAB
SAMPLE ID
CS-30 X10
C9-4 X10
C8-24 X10
C14-5 X10
C16-4
C16-18
C16-28
G2-30 MS
G2-30 MSD
CSS-9
CSS-11
FORM IVVOA
LAB
I
TIME
FILEID ANALYZED
C5-30D.D 23:14
C9-4D.D 00:15
C8-24D.D I 01:16
C14-5D.D 02:16
C16-4.D ' 03:17
C16-18.D 04:16
C16-28.D 05:16
G2-30MS.D i 06:15
G2-30MSD.D 07:14
CSS-9.D 08:13
CSS-11.D 09:13
i
I
'
3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK1
Lab Name: AMS, Inc. SC Cert.: 07007 --'-----------------~~~~~~---'
NC Cert.: 538 Client: Radian Location: Washin · Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
WATER
5.0 (g/ml} ML
Lab Sample l_D: Reagent Blank
Lab File ID: BLANK1.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
CAS NO. COMPOUND
Date Receive,d: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume:
CONCENTRATION UNll!"S:
(ug/L or ug/Kg) UG/L ---'-----Q
~-75-71-8 Dichlorodifluoromethane 1 U
7 4-87 -3 Chtoromethane 1 U
(uL)
.___TI)-0~1_-4-'------'-V~i~ny~l~C~h~lo~r~id~e ________ __,_ ____ ~1'---'---=U-~
: 7 4-83-9 Bromomethane 1 U ------+---------------------t-~----l 75-00-3 Chloroethane 1 U
9 T. hi fl h 75-6 -4 ! nc oro uoromet ane I 1 u I
i 75-35-4 I 1.1-Dichloroethene I 1 u i
75-09-2 I Methvlene Chloride I 1 u I
I-156-60-5 ! trans-1 2-Dichloroethene ! 1 u I I
75-34-3 I 1 1-Dichloroethane ; 1 u I
i ! 2,2-DichloroQroQane I 1 u I I
540-59-0 cis-1 2-Dichloroethene 1 u
67-66-3 Chloroform 1 u
74-97-5 Bromochloromethane 1 u
71-55-6 1 1 1-Trichloroethane 1 u
1 1-Dichloro ro ene 1 u
56-23-5 Carbon Tetrachloride 1 u
L 107-06-2 1,2-Dichloroethane 1 u
71-43-2 Benzene 1 u
79-01-6 Trichloroethene 1 u
78-87-5 ' . I 1 2-Dich oropropane 1 I u
75-27-4 Bromodichloromethane I 1 u I
: 74-95-3 Dibromomethane I 1 u
10061-01-5 cis-1 3-Dichloropropene I 1 u I
108-88-3 Toluene i 1 u ! ; I
I 10061-02-6 trans-1 3-Dichloroorooene I 1 u I
._1_9-00-5 1 1 2-Trichloroethane i 1 u !
1.3-Dichloroorooane ! 1 u ' '---I 127-18-4 l Tetrachloroethene I 1 u I
i 124-48-1 i Dibromochloromethane I 1 u i I I
' 106-93-4 I 1 2-Dibromoethane ! 1 u I
108-90-7 Chlorobenzene 1 u
100-41-4 Ethylbenzene 1 u
630-20-6 1, 1, 1,2-Tetrachloroethane 1 u
108-38-3 meta,Qara-Xylene 2 u
95-47-6 ortho-Xylene 1 ·--'--"u--;
1 u
1 u
75-25-2 ! Bromoform 1 u
FORM I VOA 3/90
•
•
••
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK1
.ab Name: AMS, Inc. SC Cert.: 07007
NC Cert.: 538 Client: Radian Location: Washiri Project: Hamilton
Matrix: (soil/water) WATER Lab Sample ID: Reagent Blank
Sample wt/vol: 5.0 (g/ml) ML Lab File ID: BLANK1.D ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Date Received: 04/13/98
Date Analyzed: 04/13/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (ul) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 , 1, 1,2,2-Tetrachloroethane 1 U
96-18-4 1,2,3-Trichloropropane 1 U
(uL)
n-Propylbenzene ____________ 1_+--_u __
Bromobenzene 1 U
1,3,5-Trimethylbenzene 1 U
' 2-Chlorotoluene I 1 u I
I 4-Chlorotoluene I 1 u
I tert-Butvlbenzene i 1 u
I 1 2.4-Trimethvlbenzene i 1 u I • ! sec-Butvlbenzene i 1 u I
! oara-lsooroovltoluene ! 1 u
541-73-1 I 1 3-Dichlorobenzene i 1 u I
106-46-7 I 1 4-Dichlorobenzene I ·1 u I
I n-Butvlbenzene ! 1 u !
95-50-1 I 1 2-Dichlorobenzene I 1 u !
96-12-8 I 1 2-Dibromo-3-chloroorooane I 1 u I
I
120-82-1 1,2,4-Tnchlorobenzene 1 u
87-68-3 Hexachlorobutadiene 1 u
91-20-3 Naphthalene 1 u
1 ,2,3-Trichlorobenzene 1 u
•
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name:
! I BLANK2
AMS, Inc. SC Cert.: 07007 . ------------------
NC Cert.: 538 Client: Radian Location: Washin !Project: Hamilton ----
Matrix: (soil/water) WATER Lab Sample ID: Reagent Blank
Sample wt/vol: 5.0 (g/ml) ML ---
Level: (low/med) LOW
% Moisture: not dee.
GC Column: VOCOL ID: 0.25 (mm)
Lab File ID: BLANK2.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 ------
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodiftuoromethane 1 u
74-87-3 Chloromethane 1 u
75 01 4 v· I Chi "d 1 u --mv on e I I
74-83-9 Bromomethane ! 1 u ..
75-00-3 i Chloroethane ' I 1 u
75-69-4 I Trichlorofluoromethane ' 1 u
75-35-4 I 1 1-Dichloroethene I 1 u
75-09-2 i Methvlene Chloride 1 u
156-60-5 I trans-1 2-Dichloroethene I 1 u
75-34-3 I 1 1-Dichloroethane 1 u
i 2 2-Dichloroorooane 1 u -540-59-0 I cis-1 2-Dichloroethene I 1 u
67-66-3 I Chloroform I 1 u
74-97-5 I Bromochtoromethane 1 u ' 71-55-6 ' 1 1 1-Trichloroethane I 1 u
I 1 1-Dichloroorooene 1 u
56-23-5 I Carbon Tetrachloride 1 u
107-06-2 ! 1.2-Dichtoroethane 1 u
71-43-2 Benzene 1 --------;---------------;------~ u
79-01-6 Trichloroethene 1 u
78-87-5 I 1,2-Dichloropropane I 1 u
75-27-4 I Bromodichloromethane I 1 u I
74-95-3 i Dibromomethane i 1 u
10061-01-5 cis-1 3-Dichloroorooene i 1 u
108-88-3 i Toluene I 1 u
10061-02-6 I trans-1 3-Dichloroorooene I 1 u '
79-00-5 i 1 1 2-Trichloroethane I 1 u I i
I 1 3-Dichloroorooane I 1 u
127-18-4 : Tetrachloroethene I 1 u
124-48-1 D1bromochloromethane 1 u
106-93-4 1 2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u
100-41-4 Ethyl benzene 1 u
630-20-6 1, 1, 1,2-Tetrachloroethane 1 u
108-38-3 ' meta,para-Xylene 2 u
95-47-6 ortho-Xylene 1 u
100-42-5 Styrene 1 u
98-82-8 lsopropylbenzene 1 u
75-25-2 Bromoform 1 u
FORM I VOA
(uL)
:
'
'
I
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK2
•
ab Name: AMS, Inc. SC Cert.: 07007 ----'-----------------~-------'
C Cert.: 538
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
Client: Radian
WATER
5.0 (g/ml) ML ---
LOW
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Location: Washin Project: Hamilton
Lab Sample ID: Reagent Blank
Lab File ID: i3LANK2.D
Date Received: 04/13/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1 2 2-Tetrachloroethane 1 u
96-18-4 1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
(uL)
Bromobenzene 1 u -~ 1 ,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
4-Chlorotoluene 1 u
tert-Butylbenzene 1 u
1 2 4-Trimeth !benzene 1 u
sec-Bu I benzene 1 u
ara-lso ro ltoluene 1 u
1 3-Dichlorobenzene 1 u
1 :4-Dichlorobenzene 1 u .. • 541-73-1
106-46-7
n-Bu I benzene 1 u
' 1 2-Dichlorobenzene 1 u l----------.--~------------+----~--1--~---1
95-50-1
1 ,2-Dibromo-3-chloropropane 1 u I
1 2 4-Trichlorobenzene 1 u ---,
I
Hexachlorobutadiene 1 u ~
96-12-8
120-82-1
87-68-3
91-20-3 Naphthalene 1 u
1 2 3-Trichlorobenzene 1 u
•
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK3
Lab Name: AMS, Inc. SC Cert.: 07007 -~-~------~-------~~~~~~---'
NC Cert.: 538 Client: Radian Location: Washin 1 Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: Reagent Blank ,f
Lab File ID: BLANK4.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
----75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u
75-00-3 Chloroethane 1 u
75-69-4 Trichlorofluoromethane 1 u
75-35-4 ' 1, 1-Dichloroethene 1 u
75-09-2 Meth lene Chloride 1 u
156-60-5 trans-1,2-Dichloroethene 1 u
75-34-3 1, 1-Dichloroethane 1 I u
2,2-Dichloro1;1ro1;1ane 1 I u I
540-59-0 cis-1,2-Dichloroethene 1 i u
67-66-3 Chloroform 1 I u
74-97-5 Bromochloromethane 1 I u I
(uL)
71-55-6 1 , 1, 1-Trichloroethane 1 u : --'
1, 1-Dichloro1;1ro1;1ene 1 u
56-23-5 Carbon Tetrachloride 1 u
107-06-2 1 2-Dichloroethane 1 u --,
'
71-43-2 Benzene 1 u
79-01-6 Trichloroethene 1 u
78-87-5 1,2-DichloroQroQane 1 u
75-27-4 Bromodichloromethane 1 u
74-95-3 Dibromomethane 1 u
10061-01-5 cis-1 ,3-Dichloro1;1ro1;1ene 1 u
108-88-3 Toluene 1 u
10061-02-6 trans-1,3-Dichloro1;1r:o1;1ene 1 u
79-00-5 1, 1,2-Trichloroethane 1 u
1 ,3-Dichloro1;1ro1;1ane 1 u
127-18-4 Tetrachloroethene 1 u
124-48-1 Dibromochloromethane 1 u
106-93-4 1 2-Dibromoethane 1 u
108-90-7 Chlorobenzene 1 u
100-41-4 I Ethylbenzene 1 u
630-20-6 1, 1, 1,2-Tetrachloroethane 1 u
108-38-3 meta11;1ara-Xylene I I 2 u
. 95-47-6 -ortho-Xylene 1 u
100-42-5 S!Yrene 1 u
98-82-8 ls0Qro1;1ylbenzene 1 u
75-25-2 Bromoform 1 u
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK3
•
ab Name: AMS, Inc. SC Cert.: 07007 ---'-----------------._ _____ __,
C Cert.: 538
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
Client: Radian
WATER
5.0 (g/ml) ML ---
LOW
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Location: Washiri Project: Hamilton
Lab Sample ID: Reagent Blank
Lab File ID: BLANK4.D
Date Received: 04/14/98
Date Analyzed: 04/14/98
Dilution Factor: 1.0 -
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
(uL)
_7_9_-3_4_-5o__ ____ 1~,1~,2~,~2_-T_e_tr_a_ch_lo_r_o_et_h_a_ne ______ +j_ ____ 1-'----1-__::U:_._~
96-18-4 ' 1 ,2,3-Trichloropropane 1 U
n-Propylbenzene 1 U
Bromobenzene 1 U
1 ,3,5-Trimethylbenzene 1 U
2-Chlorotoluene 1 U -oro o uene I 4 Chi t I 1 U
i tert-Butvlbenzene 1 u !
. ----I I
1 2 4-Trimethvlbenzene ! 1 u I I • ! sec-Butvlbenzene 1 u ! I
i para-lsoproovltoluene I 1 u i ·-I 541-73-1 ! 1 3-Dichlorobenzene ' 1 u I ; I
' 106-46-7 1 4-Dichlorobenzene I 1 u i ' n-Butvlbenzene I -1 u I
I
' 95-50-1 1 2-Dichlorobenzene I 1 u !
96-12-8 1 2-Dibromo-3-chloropropane ! 1 u I I r 120-82-1 1 2 4-Trichlorobenzene i 0 J J l
87-68-3 Hexachlorobutad1ene 1 U
91-20~-~3 _____ N_a~p_h_th_a_le_n_e ______________ 1 _ _.____;;:U_~
1,2 3-Trichlorobenzene 1 U
•
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK4 Lab Name: AMS, Inc. SC Cert.: 07007 ~-----------------~~~~~~--'
NC Cert.: 538 Client: Radian Location: Washin !Project: Hamilton
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: Reagent Blank
Lab File ID: BLANK5.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q ----
' 75-71-8 I Dichlorodifluoromethane I 1 u I
74-87-3 I Chloromethane I 1 u
75-01-4 l Vinvl Chloride i 1 u
74-83-9 ! Bromomethane I 1 u
75-00-3 1 Chloroethane 1 u
i 75-69-4 I Trichlorofluoromethane 1 u
75-35-4 ! 1 1-Dichloroethene I 1 u
! 75-09-2 Methvlene Chloride I I 1 u
I 156-60-5 I trans-1 2-Dichloroethene 1 u
i 75-34-3 1, 1-Dichloroethane 1 u
i 2 2-Dichloroorooane I 1 u ~ cis-1 2-Dichloroethene I 540-59-0 1 u
I 67-66-3 Chloroform 1 u !-Bromochloromethane I 74-97-5 1 u
' 71-55-6 111-Trichloroethane 1 u .. I
! 1 1-Dichloroorooene 1 u
; 56-23-5 Carbon Tetrachloride 1 u
i 107-06-2 1.2-Dichloroethane 1 u
71-43-2 I Benzene 1 u
79-01-6 ! Trichloroethene ! 1 u
78-87-5 I 1 2-Dichloroorooane 1 u
I 75-27-4 Bromodichloromethane 1 u
! 74-95-3 Dibromomethane 1 u
I 10061-01-5 cis-1 3-Dichloroorooene I 1 u : ! 108-88-3 Toluene 1 u
I 10061-02-6 trans-1 3-Dichloroorooene I 1 u
79-00-5 1 1 2-Trichloroethane 1 u
! 1 3-Dichloroorooane i 1 u
127-18-4 Tetrachloroethene I 1 u -i 124-48-1 Dibromochloromethane i 1 u
-I -I ' -106 93 4 1,2 D1bromoethane 1 u
108-90-7 Chlorobenzene 1 u
100-41-4 Ethylbenzene 1 u
630 20 6 1 1 1 2 Tetrachloroethane 1 u --I -
I 108-38-3 I meta, oara-Xvlene 2 u
l 95-47-6 ortho-Xvlene 1 u
' 100-42-5 Stvrene 1 u
98-82-8 lsooroovlbenzene 1 u
75-25-2 Bromoform 1 u
FORM I VOA
(uL)
!
I
!
!
!
l I
i
I :
I
!
I
I
!
I
!
I
3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANK4
AabName:
~CCert.:
AMS, Inc. SC Cert.: 07007 ~-'-~~~~~~----------~~~~~~---'
538 Client: Radian Location: Washin· Project: Hamilton
Matrix: (soil/water)
Sample wUvol:
Level: (low/med)
% Moisture: not dee.
WATER
5.0
LOW
(g/ml) ML ---
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: Reagent Blank
Lab File ID: BLANK5.D
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1,2,2-Tetrachloroethane 1 u
96-18-4 1,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
Bromobenzene 1 u
1,3,5-Trimethylbenzene 1 u
2-Chlorotoluene 1 u
' 4 Chlorotoluene -I 1 u
! tert-Butvlbenzene ! 1 u ' I 1 2.4-Trimethvlbenzene I I 1 u
I I sec-Butvlbenzene i 1 u
I I oara-lsooroovltoluene i 1 u
(uL)
i
'
I
I • ! 541-73-1 ! 1 3-Dichlorobenzene I 1 u ~ I --l
' 106-46-7 1 4-Dichlorobenzene I 1 u I
' I n-Butvlbenzene I 1 u '
I 95-50-1 i 1.2-Dichlorobenzene I 1 u I
! 96-12-8 I 1.2-Dibromo-3-chloroorooane ' I 1 u i
120-82-1 1,2,4-Trichlorobenzene !
' 1 u i
87-68-3 Hexachlorobutadiene 1 I u
91-20-3 Naphthalene 1 u
1,2,3-Trichlorobenzene 1 u
•
FORM I VOA 3/90
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANKS
Lab Name: AMS, Inc. SC Cert.: 07007
----------~
NC Cert.: 538
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
Client: Radian
WATER
5.0
LOW
(g/ml) M_L __ _
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume: (uL)
----
Location: Washin Project: Hamilton
Lab Sample i'D: Reagent Blank
Lab File ID: BLANK6.D
Date Receive<ii: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 ------
Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8 Dichlorodifluoromethane 1 u
74-87-3 Chloromethane 1 u
75-01-4 Vinyl Chloride 1 u
74-83-9 Bromomethane 1 u
75-00-3 ' Chloroethane 1 u
75-69-4 Trichlorofluoromethane 1 u
75-35-4 1, 1-Dichloroethene 1 u ' I 75-09-2 ' Methvlene Chloride ! 1 u : 156-60-5 ! trans-1 2-Dichloroethene I 1 u I
75-34-3 i 1 1-Dichloroethane : 1 u
I 212-Dichloro12ro12ane 1 u
----540 59 0 , c1s 1 ,2 D1chloroethene 1 u -' 67-66-3 I Chloroform 1 u I
74-97-5 I Bromochloromethane 1 u
71-55-6 l 1 1 1-Trichloroethane I 1 u
1 1 1-Dichloroorooene 1 u
56-23-5 I Carbon Tetrachloride ! 1 u
107-06-2 1 ,2-Dichloroethane 1 U
71-43-2 ' Benzene 1 U
79-01-6 Trichloroethene 1 U
(uL)
!
I
78-87-5=----4--1~,2~-~D~ic~h~lo~ro~12~r=o12~a~n=e ______ _,_~---~1--1--=U __
75-27-4 Bromodichloromethane 1 U
7 4-95-3 Dibromomethane 1 U
10061-01-5 cis-1,3-Dichloro12ro12ene 1 U
108-88-3 Toluene 1 U
10061-02-6 , trans-1 , 3-Dichloroorooene 1 U
79-00-5 I 1 1 2-Trichloroethane 1 U
i 1 3-Dichloroorooane 1 U
. 127-18-4 I Tetrachloroethene 1 U
._ 124-48-1 Dibromochloromethane 1 U
106-93-4 1 ,2-Dibromoethane 1 U
108-90-7 Chlorobenzene 1 U
100-41-4 ____ E_th~Y~lb_e_n_z_en_e _______________ 1_-i---_U~
630-20-6 ' 1, 1 1 2-Tetrachloroethane 1 U
108-38-3 meta112ara-Xylene 2 U
95-47-6 ortho-Xylene 1 U
100-42-5 Styrene_ 1 U -----~--98-82-8 lso12ro12ylbenzene 1 U
75-25-2 Bromoform 1 U
FORM I VOA 3/90
•
•
•
1A AMS SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
BLANKS
•
bName: AMS, Inc . SC Cert.: 07007
C Cert.: 538
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
Client: Radian Location: Washin· Project: Hamilton
WATER Lab Sample ID: Reagent Blank
5.0 (g/ml) ML Lab File ID: BLANK6.D ---
LOW
GC Column: VOCOL. ID: 0.25 (mm)
Date Received: 04/14/98
Date Analyzed: 04/15/98
Dilution Factor: 1.0 -----
Soil Extract Volume: (uL) Soil Aliquot Volume:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
79-34-5 1, 1 ,2,2-Tetrachloroethane 1 u
96-18-4 1 ,2,3-Trichloropropane 1 u
n-Propylbenzene 1 u
' Bromobenzene 1 u
1 ,3,5-Trimethylbenzene 1 u
' 2-Chlorotoluene I 1 u : ' i 4-Chlorotoluene I 1 u
tert-Butvlbenzene 1 u
I 1,214-Trimethylbenzene 1-1 u
sec-Butvlbenzene I 1 u • l oara-lsooroovltoluene 1 u
541-73-1 ! 1 3-Dichlorobenzene I 1 u
106-46-7 ! 1 4-Dichlorobenzene I 1 u
: n-Butvlbenzene 1 u
95-50-1 1 2-Dichlorobenzene 1 u
' 96-12-8 1 2-Dibromo-3-chloroorooane 1 u .
120-82-1 ' 1 2,4-Trichlorobenzene 1 u I
87-68-3 Hexachlorobutadiene 1 u
91-20-3 Naphthalene 1 u
1 ,2,3-Trichlorobenzene 1 u
•
FORM I VOA
(ul)
I
!
I
I
I
!
I
I
!
!
3/90
2A
WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name: AMS, Inc. SC Cert.: 07007
-----------~ ----
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
MS SAMPLE NI
SMC1
#
SMC2
#
SMC3
#
TOT
OUT I
011 BLANK1
021 98-0188
03i 98-0189 --..
04l 98-0191
05[ 98-0190
06l 98-0187
071 98-0192
081 98-0193
091 98-0194
101. BLANK2
11 1 98-0195 -· 12! 98-0196
131 98-0197
141 98-0198
15i 98-0199
-~--. -·---
I 98-0200 !_ 16
17
18
19
20
21
22
23
24
25
I 98-0232
! 98-0204
I 98-0205
I I 98-0216
i 98-0217
J 98-0219
' 98-0220 I
I 98-0218
! BLANK3
--
95
95
102
102
99
102
102
106
103
106
105
107
110
99
109
104
102
108
108
106
102
96
101
100
105
I
:
101
99
102
101
101
100
99
99
100
99
100
100
100
100
99
100
100
100
100
96
100
95
100
97
100
92
93
95
92
99
94
88
95
89
90
90
90
89
91
92
91
91
91
89
94
91
91
92
98
90
0
0
0
0
0
0 o I
o I
Q
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
i
i
I
I
I
'
' 26! 98-0221 107 101 92 0
27' 98-0222 104 101 92 0 ·-----------------------281_98_-0_2_23 ___ +--_1-'0'-"5 __ --'-1 o"-1 __ ____,8_9 ___ -'o'---;
291 98-0215 105 100 88 0
30
31
32
33
I
I
I
i
98-0226
98-0206
98-0209
98-0224
SMC1
SMC2
SMC3
105 i 100
106 101
102 101
102 101
= Dibromofluoromethane
= Toluene-dB
= 4-Bromofluorobenzene
91
92
97
93
0
0
0
0
QC LIMITS
(86-118)
(88-110)
(86-115)
# Column to be used to flag recovery values
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
page 1 of 2 FORM II VOA-1
•
•
3/90 •
2A
WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
•
ab Name:
C Cert.:
AMS, Inc. SC Cert.: 07007 --------------~~~~~-
538 Client: Radian Location: Washiri Project:
SMC1
, MS SAMPLE N #
34! 98-0227 1 06
35! 98-0225 107
361
37!
381
39 ' --l
BLANK4
98-0228
98-0229
98-0207
l 107 I
I 98
l 100
: 103
'
SMC2
#
102
101
100
100
100
101
'
'
i
SMC3
#
96
93
89
94
92
91
!
I
TOT
OUT
0
0
0
0
0
0
401 98 0211 106 102 89 0 -I
41! 98-0208 104 97 95 0
421 98-0212 108 102 93 0
I
431 98-0210 __ __:..10-=-4-'-----'1-"0=2 __ ----'9-'-7 ___ __;0:.__
441 98-0230 99 100 95 0
45i 98-0231 108 101 104 0
46!-BLANK5 103 99 99 0
47! 98-01890 103 101 92 0
48\ 98-01930 108 102 97 0
491 98-02270 108 102 98 0
50! 98-02280 104 101 93 0
51! 98-0233 104 102 98 0
• 52j. 98-0234 103 102 94 0
53!. -98-0235 105 102 93 0
•
541 98-0216MS 101 102 93 0
55j 98-0216MSO 103 102 98 0
SMC1
SMC2
SMC3
= Oibromofluoromethane
= Toluene-dB
4-Bromofluorobenzene
# Column to be used to flag recovery values
QC LIMITS
(86-118)
(88-110)
(86-115)
* Values outside of contract required QC limits
D System Monitoring Compound diluted out
page 2 of 2 FORM II VOA-1
Hamilton
3/90
SOIL VOLATILE SYSTEM Mo;·: :-::::RING COMPOUND RECOVERY
Lab Name: AMS, Inc.
NC Cert.: 538
Level: (low/med)
·MS SAMPLE N
011 98-0213
021 98-0214
SMC1
SMC2
SMC3
Client: Radian
LOW
SMC1 SMC2 I SMC3
# # #
107 87 110
111 93 100
= Dibromofluoromethane
= Toluene-dB
4-Bromofluorobenzene
SC Cert.: 07007
Location: Wash in
TOT
OUT
0
0
QC LIMITS
(80-120)
(81-117)
(74-121)
# Column to be Wot: J to flag recovery values
* Values outside s. contract required QC limits
D System Monitoring Compound diluted out
page 1 of 1 FORM II VOA-2
Project: Hamilton •
•
3/90 •
3A
WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
•
ab Name:
C Cert.:
AMS, Inc. SC Cert.: 07007
~-'----------~ ~-----
538 Client: Radian Location: Washin· Project: Hamilton
Matrix Spike -AMS SAMPLE N 98-0216 ------
I SPIKE SAMPLE MS
I ADDED !coNCENTRATloNicoNCENTRATION
COMPOUND j (ug/L) '. (ug/L) ! (ug/L)
MS I
% l REC#I
I QC I
LIMITS I
I
REC.
i 1, 1-Dichloroethene 50 I 0.0 54 108 ! 72 -123 I
; Benzene 50 I 0.0 49 98 i 76 -121 I, ~-----------Ir-----~·-------,--------+-----'-----~ , Trichloroethene 50 I 0.0 48 ! 96 / 7 4 -119
•~-------------1!-----+---------'--------+----+------1
:
'.
' l I
Toluene i 50 i 0.96 I 52 102 I 78 -125
Chlorobenzene 50 I 0.0 I 49 I 98 ! 77 -1221
COMPOUND
1, 1-Dichloroethene
Benzene
Trichloroethene
Toluene
Chlorobenzene
SPIKE
ADDED
(ug/L)
50
50
50
50
50
MSD MSD \
! CONCENTRATION! % !
(ug/L) ) REC# \
I 57 I 114 I I
! 49 I 98
! 52 104 I
52 i 102
53 I 106
# Column to be used to flag recovery and RPO values with an asterisk
* Values outside of QC limits
RPO: 0 out of 5 outside limits
% I
RPO#\
QC LIMITS
RPO I REC.
5 15 I 72 -123 \
0 15 I 76 -121 I I 8 18 74 -119 i
0 20 I i 78 -125
8 20 I 77 -122
•
Spike Recovery: O out of 10 outside limits
COMMENTS:
FORM Ill VOA-1 3/90
5A
VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: AMS, Inc. SC Cert.: 07007
~----~------~---
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab File ID: BFB1.D BFB Injection Date: 04/13/98
Instrument ID: GC/MS BFB Injection Time: 12:32 -----
GC Column: VOCOL ID: 0.25 (mm) Heated Purge: (Y/N) N
% RELATIVE
m/e ION ABUNDANCE CRITERIA ABUNDANCE
50 8.0 -40.0% of mass 95 18.6
75 30.0 -66.0% of mass 95 44.0
95 Base peak, 100% relative abundance 100.0
96 5.0 -9.0% of mass 95 6.6
173 Less than 2.0% of mass 174 0.0 0.0)1 !
174 50.0 -120.0% of mass 95 67.1
175 4.0 -9.0% of mass 174 4.9 7.3)1 :
176 93.0 -101.0% of mass 174 67.6 ( 100.7)1 I
177 5.0 -9.0% of mass 176 4.4 ( 6.6)2 !
1-Value is % mass 17 4 2-Value is% mi:iss 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
I 1· I : AMS SAMPLE NO. I
I BLANK1
l 98-0188
I 98-0189
I 98-0191
! 98-0190
l 98-0187
I 98-0192 I
l 98-0193
01
02
03
04
05
06
07
08
09 i 98-0194
page 1 of 1
LAB
SAMPLE ID
REAGENT BLANK
C5-17
C5-30
C6-26
C6-8
C5-8
C1-19
C9-4
C9-25
LAB
FILEID
BLANK1.D
C5-:17.D
C5-30.D
C6-26.D
C6-8.D
C5-8.D
C1-19.D
C9-4.D
C9-25.D
FORMVVOA
I DATE ; TIME I ANALYZED I ANALYZED ! •,
04/13/98 I .. 13:59
04/13/98 15:04
04/13/98 16:10 -04/13/98 17:18
04/13/98 18:32
04/13/98 19:34
04/13/98 20:35
I 04/13/98 21:34
04/13/98 22:34
3/90
•
•
•
•
•
•
Lab Name:
NC Cert.:
Lab File ID:
5A
VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
AMS, Inc. SC Cert.: 07007
538 Client: Radian Location: Washin Project:
BFB2.D BFB Injection Date:
Hamilton
04/13/98
Instrument ID: GC/MS BFB Injection Time: 23:33 -----------
GC Column: VOCOL ID: 0.25 (mm) Heated Purge: (Y/N) N
m/e
50
75
95
' 96
173
174
175
176
177
;
I
I
ION ABUNDANCE CRITERIA
% RELATIVE
ABUNDANCE i
8.0 -40.0% of mass 95 18.6 I ------------+----------l
30.0 -66.0% of mass 95 44.0 I
---------------1c--------~ Base peak, 100% relative abundance 100.0 !
~--------!-----------< 5.0 -9.0% of mass 95 6.6 I -------------!-----------! Less than 2 0% of mass 174 0 0 0 0 )1 ~
50.0 -120.0% of mass 95 67.1
4.0 -9.0% of mass 174 4.9 ( 7.3)1
93.0-101.0% of mass 174 67.6 ( 100.7)1
5.0 -9.0% of mass 176 4.4 ( 6.6)2
1-Value is % mass 17 4 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
-
I AMS SAMPLE NO.
BLANK2
98-0195
98-0196
I 98-0197
01
02
03
04
05
06
07
08
09
10
I 98-0198
I· 98-0199
98-0200
98-0232
98-0204
98-0205
page 1 of 1
LAB LAB
SAMPLE ID FILEID
REAGENT BLANK BLANK2.D
C11-4 C11-4.D
C11-25 C11-25.D
C12-4 C12-4.D
C12-18 C12-18.D
C12-29 C12-29.D
C13-3 C13-3.D
C13-24 C13-24.D
C18-5 C18-5.D
C18-25 C18-25.D
FORMVVOA
DATE TIME
I ANALYZED ANALYZED
I 04/14/98 01:08
04/14/98 02:06 :
04/14/98 03:03
04/14/98 I 04:00
' 04/14/98 i 04:57
' 04/14/98 i 05:55
04/14/98 I 06:52 I
04/14/98 07:49 !
04/14/98 I 08:46 :
04/14/98 09:45 I
3/90
5A
VOLATILE ORGANIC INSTRUMENT PERFORMANC~ CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: AMS, Inc. SC Cert.: 07007 --'---------------
NC Cert.: 538 Client:
Lab File ID: BFB3.D -----
Instrument ID: GC/MS
Radian Location: Washin Project: Hamilton
BFB Injection Date: 04/14/98
BFB Injection Time: 10:39 -----------
GC Column: VOCOL ID: 0.25 (mm) Heated Purge: (Y/N) N
m/e ION ABUNDANCE CRITERIA
I
50 ! 8.0 -40.0% of mass 95
I 75 I 30.0 -66.0% of mass 95 I
95 Base peak, 100% relative abundance
' ! 96 5.0 -9.0% of mass 95 !
! 173 Less than 2.0% of mass 174
174 50.0 -120.0% of mass 95
175 4.0 -9.0% of mass 174
: 176 93.0 -101.0% of mass 174
177 5.0 -9.0% of mass 176
1-Value is% mass 174
I
2-Value is% mass 176
% RELATIVE
ABUNDANCE
18.4
41.0
100.0
6.7
0.0 ( 0.0)1
64.1
I
I
I
I
!
5.0 ( 7.8)1 '
64.4 ( 100.6)1
4.4 ( 6.8)2
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
I
j AMS SAMPLE NO. !
01
02
03
04
05
I 98-021s
l 98-0217
I 98-0219
98-0220
I 98-0218
page 1 of 1
LAB LAB
SAMPLE ID FILEID
G2-30 G2-30.D
G2-40 G2'40.D
G3-30 G3-30.D
G3-40 G3-40.D
G3-20 G3-20.D
FORMVVOA
I DATE I TIME
I ANALYZED 1 ANALYZED
04/14/98 I 12:38 I
04/14198 I 13:38
04/14/98 I 14:54 !
I
04/14/98 I 15:53 i
! 04/14/98 I 16:52 I
3/90
•
•
•
•
•
•
SA
VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: AMS, Inc.
NC Cert.: 538 Client: Radian
Lab File ID: BFB4.D
Instrument ID: GC/MS ------
GC Column: VOCOL ID: 0.25 (mm)
m/e ION ABUNDANCE CRITERIA
50 8.0 -40.0% of mass 95
75 30.0 -66.0% of mass 95
95 Base peak, 100% relative abundance
96 5.0 -9.0% of mass 95
173 Less than 2.0% of mass 174
174 50.0 -120.0% of mass 95
175 4.0-9.0% of mass 174
176 93.0-101.0% of mass 174
177 5.0 -9.0% of mass 176
1-Value is % mass 17 4
SC Cert.: 07007
Location: Washin Project: Hamilton
04/14/98 BFB Injection Date:
BFB Injection Time: 17:45
Heated Purge: (Y/N) N
% RELATIVE
ABUNDANCE'
18.4
41.5
100.0
6.5
I
! I
I
0.0 0.0)1 I
65.2
4.6 7.0)1 I
65.3 100.3)1
4.3 6.6)21
2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
LAB LAB DATE TIME i l AMS SAMPLE NO. ! SAMPLE ID I FILEID ANALYZED ANALYZED i
I BLANK3
I 98-0221
I 98-0222 I
I 98-0223
i 98-0215
i 98-0226
' 98-0206
01
02
03
04
05
06
07
08
09
10
11
L 98-0209
I 98-0224
! 98-0227
i 98-0225 I
page 1 of 1
REAGENT BLANK BLANK4.D
G1-20 G1-20.D
G1-30 G1-30.D
G1-40 G1-40.D
G2-20 G2-20.D
CS-5 C8-5.D
C17-4 C17-4.D
C15-24 C15-24.D
C14-23 C14-23.D
C8-24 CS-24.D
C14-51 C14-51.D
FORMVVOA
04/14/98 19:23 I
04/14/98 20:23 I
04/14/98 21:22
04/14/98 22:21
I 04/14/98 23:20
I 04/15/98 00:20 :
04/15/98 01:19 !
04/15/98 02:18 :
04/15/98 03:16
04/15/98 04:15 i
04/15/98 05:14 '
3/90
SA
VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: AMS, Inc. SC Cert.: 07007
~-~~---~~~------
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab File ID: BFBS.D BFB lnjecti<:m Date: 04/15/98
Instrument ID: GC/MS BFB Injection Time: 07:19 -----
GC Column: VOCOL ID: 0.25 (mm) Heated Purge: (YIN) N
% RELATIVE
m/e ION ABUNDANCE CRITERIA ABUNDANCE
50 8.0 -40.0% of mass 95 18.5
75 30.0 -66.0% of mass 95 41.8
95 Base peak, 100% relative abundance 100.0
96 5.0 -9.0% of mass 95 7.2 I
I
173 Less than 2.0% of mass 174 0.0 0.0)1 :
174 50.0 -120.0% of mass 95 62.4
175 4.0 -9.0% of mc;iss 174 4.8 ( 7.7)1 i
176 93.0-101.0% of mass 174 62.5 ( 100.2)1 !
177 5.0 -9.0% of mass 176 4.1 ( 6.5)2 l
1-Value is % mass 17 4 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
i ! AMS SAMPLE NO.
i 01
02
03
04
05
06
07
08
09
10
BLANK4
i 98-0228
·I 98-0229
I 98-0207 -I 98-0211
I 98-0208
I 98-0212
l 98-0210 I 98-0230
I 98-0231
page 1 of 1
LAB
SAMPLE ID
REAGENT BLANK
C14-5
C10-25
C17-25
C7-5
C15-5
C7-24
C1-4
C10-49
C10-4
LAB
FILEID
BLANK5.D
C14-5.D
C10-25.D
C17-25.D
C7-5.D
C15-5.D
C7-24.D
C1-4.D
C10-49.D
C1b-4.D
FORMVVOA
l. DATE j TIME
1
ANALYZED \ ANALYZED ;
04/15/98 08:45
I 04/15/98 09:44 !
04/15/98 10:45
04/15/98 11:46
: 04/15/98 I 12:53
I 04/15/98 I 14:57
I 04/15/98 : 16:05
! 04/15/98 l 17:13 '
,, 04/15/98 l 18:20
04/15/98 ! .,
j 19:23
3/90
•
•
•
•
•
•
5A
VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK
BROMOFLUOROBENZENE (BFB)
Lab Name: AMS, Inc. SC Cert.: 07007
NC Cert.: 538 Client: Radian Location: Washin Project: Hamilton
Lab File ID: BFB6.D BFB Injection Date: 04/15/98
Instrument ID: GC/MS BFB Injection Time: 20:29
GC Column: VOCOL ID: 0.25 (mm) Heated Purge: (YIN) N
% RELATIVE I
! I
! m/e ION ABUNDANCE CRITERIA ABUNDANCE I
50 8.0 -40.0% of mass 95 18.4
:
75 ' 30.0 -66.0% of mass 95 41.6
i I Base peak, 100% relative abundance 100.0 95 :
96 5.0 -9.0% of mass 95 6.4
173 Less than 2.0% of mass 174 0.0 0.0 1 I ) I
174 50.0 -120.0% of mass 95 67.3 I
I
175 4.0 -9.0% of mass 174 4.9 7.3)1 !
176 93.0 -101.0% of mass 174 67.1 99.7)1 i
177 5.0 -9.0% of mass 176 4.5 6.8)2 1
1-Value is % mass 17 4 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
-
i i
i AMS SAMPLE NO.
I
I '
01
02
03
04
05
06
07
08
09
10
11
12
I L...
I
I
I I I
BLANKS
98-01890
98-01930
98-02270
98-02280
98-0233
98-0234
98-0235
98-0216MS
98-0216MSO
98-0213
98-0214
page 1 of 1
!
I
LAB ! LAB
I SAMPLE ID ! FILEID
REAGENT BLANK BLANK6.D
C5-30 X10 C5-30D.D
C9-4 X10 C9-4D.D
C8-24 X10 C8-24D.D
C14-5 X10 C14-5D.D
C16-4 C16-4.D
C16-18 C16-18.D
C16-28 C16-28.D
G2-30 MS G2-30MS.D
G2-30 MSD G2-30MSD.D
CSS-9 CSS-9.D
CSS-11 CSS-11.D
FORMVVOA
I ! DATE
I
TIME
ANALYZED I ANALYZED
04/15/98 22:13 I
04/15/98 23:14 I
04/16/98 00:15 I
! 04/16/98 01:16 I
; 04/16/98 02:16
04/16/98 03:17
04/16/98 I 04:16 :
~ 04/16/98 05:16 i
: 04/16/98 06:15 ! I
04/16/98 07:14 i
04/16/98 08:13 I I
04/16/98 09:13 I
3/90
09/30/98 16:31:26
H<.:1->ort RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _-!;Ro::a.;,:d:.:i.::a"'n'-"I"'n~t.::e:.r,,,,n""a~t.:i.::o,.,n""a-"l_,_,_,,L"'L"'C'­
By --"1~4.::0~4.::6_,,S.::u~m~m.:i~t_,,D.:r~._,_,~B.:l.::d~g~.~B­
P. 0. Box 201088
Aust in, TX 78720-1088
CSC JAI,INDSEY
Project Sample
Description
0998HBWE01
0998HBWSOURCE
•
ID/
WORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # .N~A'----------­
SDG # ~N~A---~~~-­
RAS # 80903AJAL
Lab Sample ID Test Code{s)
OlA 352SWAOO
827SWBCM
CKlSWAOO
02A 352SWAOO
827SWBCM
CKlSWAOO
028 SPAREBOO
•
Work Orde1 U YH09490
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
M~thod Descipt1on
Liquid/Liq Extract SW846
Sem1volatiles by GC/MS
Prim<Jry KD cone. SW84G
Liquid/Liq Extract SW846
Sem1volatiles by GC/MS
Primary KD cone. SW846
Spart: Sample
--
•
09/30/98 16:31:26 ANALYTICAL PROTOCOL SUMMARY
P L A G D B P I N I T I 0 N S
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A
B
c
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero).
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and seconda:r;:y qc columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation .
• •
Work Order tt 9809490
Page _3_
•
OY/30~:31:26
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Mt.:thod Sem1volariles by SW8270C
Project Sample ID/Description
0998HBWE01
0998HBWSOURCE
A N A L Y T :C C A L .T 0 C 0 L S U M M A R Y
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9809490-0lA 827SWBCM 3520980923133000
9809490-02A 827SWBCM 3520980923133000
Work Order tt 9809490
Page _4_
Analysis Batch U
MSMSD280925102101
MSMSD280925102101
•
OY/30/98 16:31:26
Mdbod Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Dale Analyzed:
Dilulion l'actor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
.Benz lal <!_nth~acene
Benz(a)pyrene
Benzidine
Benzo(blfluoranthene
Benzo(g,h,ilperylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol
p-Chloroaniline
•
0998HBWE01
9809490-0lA
Y9362
09/21/98
09/23/98 13:30:00
09/25/98 18:04
1
Water
ug/L
received
Cone. DL
ND 0.455
ND 0.366
ND 0.163
ND 0.493
ND 8.27
ND 0.661
ND 0.379
ND 0 .192
ND 0. 287 -
ND 27.9
ND 0.284
ND 0.303
ND 0.576
ND 29.9
ND 0.675
ND 0.419
ND 0.105
ND 0.0566
ND 0.447
ND 0. 841
RESULTS SUMMARY
0998HBWSOURCE
9809490-02A
Y9363
09/21/98
09/23/98 13:30:00
09/25/98 18: 43
1
Water
ug/L
received
Cone. DL
ND 0 .455
ND 0.366
ND 0.163
ND 0.493
ND 8.27
ND 0.661
ND 0.379
ND 0 .192
·--ND 0.287
ND 27.9
ND 0.284
ND 0.303
ND 0.576
ND 29.9
ND 0.675
ND 0.419
' ND 0.105
ND 0.0566
ND 0.447
ND 0.841
•
Cunc. DL
----
Work Order tt 9809490
Page _5_
Cone:.
-
DL
-
•
09/30.J:31:2~
M'-'tliud Semivoldtiles by SW8270C
Test Code 827SWBCM .
Project Sample ID:
l1C1b ID:
F'ile ID:
Date Collected:
Date Prepared:
Dilte Analyzed:
lliluLion Factor:
Matrix:
Units:
H"port as:
Column:
Analyte
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
b1s(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
D1-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
-
0958HB\\E01
9809490-0lA
Y9362
09/21/98
09/23/98 13:30:00
09/25/98 18: 04
1
Water
ug/L
received
Cone. DL
ND 0.194
ND 0.237
ND 0 .149
ND 0.192
ND 0.559
ND 0.115
ND 0.335
ND 0.274
ND 0.169
ND 0.169
ND 0.223
ND 0.240
ND 0.139 . ND 0.340
ND 0 .484
ND 0.442
ND 1. 09
ND o. 377
ND 0.255
ND 0.207
RESULTS .MARY
0 9 9S HBWS(IURCE
9809490-U2A
Y9363
09/21/98
09/23/98 13:30:00
09/25/98 18:43
1
Water
ug/L
received
Cone. DL
ND 0.194
ND 0.237
ND 0.149
ND 0.192
ND 0.559
ND 0.115
ND 0.335
ND 0.274
0.788 0.169
ND 0.169
ND 0.223
ND 0. 240
ND 0.139
ND 0. 340
ND 0.484
ND 0.442
ND 1.09
ND 0.377
ND 0.255
ND 0.207
(Cont'd)
Ccnc. DL
Work Order U 9809490
Page _6_
Cone.
•
l
DL
09/30/98 16:31:26
Method Semivolatiles by SW8270C
Test Code 827SWBCM .
Project Sample ID:
I.ab ID:
File ID:
Date Collected:
Date Prepared:
l.>ute Analyzed:
Dilution Factor:
Matrix:
Uni ts:
f<eport as:
Column:
Analyte
p-Dimethylaminoazobenzene
1,12-Dimethylbenz(a)anthracene
3,3'-Dimethylbenzidine
Di methyl phenethylam·ine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
l,3-Dinitrobenzene -
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulfonate
bis(2-Etllylhexyl)phthalate
Fluoranthene
F"luorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
•
0998HBWE01
9809490-0lA
Y9362
09/21/98
09/23/98 13:30:00
09/25/98 18:04
1
Water
ug/L
received
Cone. DL
ND 0.753
ND 0.365
ND 3 -4 7
ND 12.3
ND 0.379
ND 0.256
ND 9 .43
ND 0.497
ND 5-~6-0--
ND 0.422
ND 0.424
ND 0.607
ND 0.333
2.08 J 4.83
ND 0.228
ND 0.304
ND 0.390
ND 0.618
ND 4. 96
ND 0.303
R BS ULT S SUMMAR Y (Cont'd)
0998HBWSOURCE
9809490-02A
Y9363
09/21/98
09/23/98 13:30:00
09/25/98 18:43
1
Water
ug/L
received
Cone. DL
ND 0 .753
ND 0.365
ND 3.47
ND 12.3
ND 0.379
ND 0.256
ND 9.43
ND 0 .497
-ND 5.60
ND 0.422
ND 0.424
ND 0.607
ND 0.333
ND 4.83
ND 0.228
ND 0.304
ND 0.390
ND 0.618
ND 4.96
ND 0.303
•
Cone. DL
Work Order II 9809490
Page _7_
Cone. DL
-
---
•
(J'J/30/.: 31. 26
M..th<,d SemivoJaLiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
[,db ID:
File ID:
Date Collected:
Oate Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
l!exaehloropropene
Indeno(l,2,3-ed)pyrene
Isophorone
Isosafrole
Ke pone
M£thapyrilene
Methyl methanesulfonate
3-Methyleholanthrene
2-Methylnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N·Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N·Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
0998HBWE01
9809490-0lA
Y9362
09/21/98
09/23/98 13:30:00
09/25/98 18: 04
1
Water
ug/L
received
Cone. DL
ND 0. 774
ND 0.200
ND 0.0934
ND 1. 20
ND 17.9
ND 8 .92
ND 0.397
ND 6.93
ND 0.290
ND 0.215
ND 0.202
ND 0.536
ND 0.340
ND 0.509
ND 0.581
ND 0.758
ND 0.915
ND 0.181
ND 0.758
ND 0.378
RESULTS .MARY
0998HBWSOURCE
9809490·02A
Y9363
09/21/98
09/23/98 13:30:00
09/25/98 18: 43
1
Water
ug/L
received
Cone. DL
ND 0.774
ND 0.200
ND 0.0934
ND 1.20
ND 17. 9
ND 8.92
ND 0.397
ND 6.93
ND 0.290
ND 0.215
ND 0.202
ND 0.536
ND 0.340
ND 0.509
ND 0.581
ND 0.758
ND 0.915
ND 0.181
ND 0.758
ND 0.378
(Cont'd)
Cone. DL
work Order H 9809490
Page _8_
Cone.
•
·-
DL
09/30/.:31:26
Mdhod Semjvolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
o, e Analyzed:
D1 lution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
sym-Trinitrobenzene
0998HBWE01
9809490-0lA
Y9362
09/21/98
09/23/98 13:30:00
09/25/98 18:04
1
Water
ug/L
received
Cone. DL
ND 0.266
ND 0.795
ND 0.482
ND 0.367
ND 0.661
ND 1. 34
ND 0,325
ND 0. 892
ND 0.347
ND 1.22
RESULTS .MARY (Cont.'d)
0998HBWSOURCE
9809490-02A
Y9363
09/21/98
09/23/98 13:30:00
09/25/98 18:43
1
Water
ug/L
received
Cone. DL
ND 0.266
ND 0.795
ND 0.482
ND 0.367
ND 0.661
ND 1. 34
ND 0.325
ND 0.892
ND 0.347
ND 1.22
Cone. DL
Work Order # 9809490
Page lQ_
Cone.
•
DL
09/30/98 16:31:26
Muthod Semivolatiles by SW8270C
Test Code 827SWBCM .
Project Sample! TD:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
·N·i·trobenzene--d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribromophenol
•
0998HBWE0l
9809490-0lA
Y9362
09/21/98
09/23/98 13:30:00
09/25/98 18:04
1
Water
ug/L
received
Cone. DL
Recovery
%
99
97
99 ----
106
95
93
R B S 0 LT S S 0 MM A R Y (Cont'd)
0998HBWSOURCE
9809490-02A
Y9363
09/21/98
09/23/98 13:30:00
09/25/98 18:43
l
Water
ug/L
received
Cone. DL
Recovery
%
96
90
97
101
96
91
•
Cone. DL
Recovery
%
Work Order tt 9809490
Page l.J:_
Cone. DI.
Recovery
%
-
·-
•
09/30~:31:26
Method Semivolatiles by SW8270C
Test Code 827SWBOO
initial Calibration H MSD2980821083300
C\il ibrat io11 Dale _0_8_/_2_1~/~9~8 ____ _
Sequence/Analysis Time
1 09/25/98 10:21
2 09/25/98 10:41
3 09/25/98 13:27
4 09/25/98 14 :06
5 09/25/98 14:46
6 09/25/98 15:25
7 09/25/98 16:05
8 09/25/98 16:44
9 09/25/98 17:24
10 09/25/98 18: 04
11 09/25/98 18:43
12 09/25/98 19:23
Project
ANALYSIS BA.SUMMARY
Analysis Batch ff SMSD280925102101
Analysis Start Date/Time 09/25/98 10:21:00
Analysis Stop Date/Time 09/25/98 19:23:00
Sample ID Lab Sample ID Sample Type
TUNE GC/MS tune f i lt:s
Work Order ff 9809490
Page lL
Instrument ~
Analyst !:!£1
Reviewer ~S~D~K'----------
Analysis File #
Y9350
SSTD050 Continuing CalibraLion Verification Y9351
LCS984972 Lab Control Sample Y9355
LCSD984972 Lab Control Sample Duplicate Y9356
BLK983262 Blank, Method Y9357
9809458-0lA Sample Y9358
9809458-03A Matrix Sp1kte Y9359
9809458-04A Matrix Spike Duplicate Y9360
9809458-02A Sample Y9361
0998HBWE01 9809490-0lA Sample Y9362
0998HBWSOURCE 9809490-02A Sample Y9363
DCS984973 Detectability Check Sample Y9364
•
09/30/98 16:31:26
Method Semivolatiles b·f $;-i8270C'
l.ab Sample ID
Pile ID
•
Project Sample
ID/Description
Sp.:cificat;,onll _s_2_;_s __
Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMEHTS/HARRATIVK
Flag Comment/Narrative
t
•
Corrective Action
Work Order II 9809490
Page .ll...
•
10/05/98 16:48:24
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared ~-R_a_d~i~a_n~I_n~t_e~r-n_a_t~i~o_n_a~l~·-L~L~C­
By ~-=1~4~0~4~6-=S~u~m~m~i~t-=D~r~·~·-=B~l~d~s~·-=B'­
P. o. Box 201088
Austin TX 78720-1088
CSC JALINDSEY
Project Sample
Description
-
0998HBWE01
•
ID/
NORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # _N_A~-------­
SDG # N~A""-~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA 352SWAOO
CKlSWAOO
DSLSWAEL
•
Work Order ft 9809491
Page _1_
RCN 650138.0602
New York ELAP ID#: 10915
Method Desciption
Liquid/Liq Extract SW846
Primary KD cone. SW846
TPH Extractables
•
10/05.6:48:24
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
STATE CBRT.ATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order It 9809491
Page _2_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
10/05/98 16:48:24 ANALYTICAL PROTOCOL SUMMARY
F L A G D K F I N I T I 0 N S
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previou9~Y confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Resul-ts from primary and secondary GC _i;:glum11_s_ di:ffer by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation.
• •
Work Order # 9809491
Page _3_
•
10/05/~:48:24
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method TPfl-Diesel by mod. SW8015
Project Sample ID/Description
0998HBWE01
A N A L Y T I C AL .T 0 C 0 L S U H H A R Y
Extraction/Digestion
Lab Sample ID Test Code (s) Batch #
98094 91-0lA DSLSWAWT 3520980923115000
Work Order # 9809491
Page _4_
Analysis Batch JI
TPGC1380928120003
•
10/05/98 16:48:24
Method TPH-Diesel by mod. SW8015
Test Code DSLSWAWT
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Diesel
Jet fuel JP4
Kerosene
Lubricating oil
Unidentified organics
Surrogate(s)
Octacosane
•
0998HBWE01
9809491-0lA
V8128087
09/21/98
09/23/98
10/01/98 12:05:00
1. 0000
Water
mg/L
received
Cone. DL
ND 0.0221
ND 0. 0272
ND 0. 0116
ND
0.0267 B
Recovery
%
96
RESULTS SUMMARY
Cone. DL Cone.
Recovery -Recov_ery
% %
•
DL
work Order # 9809491
Page _5_
Cone. DL
Recovery
% -
•
10/05~6:48:24
Method TPH-Diesel by mod. SW8015
Test Code DSLSWAEL
Initial Calibration ff GC13980918120000
Calibration Date _0~9~/_1~8~/~9~8 ____ _
Sequence/Analysis Time
75 10/01/98 02:45:00
76 10/01/98 03:32:00
77 10/01/98 04:18:00
78 10/01/98 05:05:00
79 10/01/98 05:51:00
80 10/01/98 06:38:00
81 10/01/98 07:24:00
82 10/01/98 08:11:00
83 10/01/98 08:58:00
84 10/01/98 09:44:00
85 10/01/98 10:31:00
86 10/01/98 11:18:00
87 10/01/98 12:05:00
88 10/01/98 12:52:00
89 10/01/98 13:38:00
90 10/01/98 14; 25: 00
91 10/01/98 15:12:00
92 10/01/98 15:59:00
93 10/01/98 16:46:00
94 10/01/98 17:33:00
Project Sample
0998HBWE01
ANALYSIS BA. SUMMARY
Analysis Batch tt TPGC1380928120003
Analysis Start Date/Time 09/28/98 12:00:00
Analysis Stop Date/Time 10/01/98 17:33:00
ID Lab Sample ID Sample Type
CCV_JET Continuing
CCV_KER Continuing
CCV_DSL Continuing
Calibration
Calibration
Calibration
BLK983161 Blank, Method
LCS984804 Lab Control Sample
Work Order ff 9809491
Page _6_
Instrument Q£1l...__
Analyst MRA
Reviewer _J_S~E ________ _
Analysis File ff
Verification V8I28075
Verification V8I28076
Verification V8I28077
V8I28078
V8I28079
LCSD984804 Lab Control Sample Duplicate V8I28080
DCS984805 Detectability Check Sample V8I28081
9809451-03A Sample V8I28082
9809451-04A Matrix Spike V8I28083
9809451-05A Matrix Spike Duplicate V8128084
9809451-0lA Sample V8I28085
9809451-02A Sample V8128086
9809491-0lA Sample V8I28087
9809310-04A Sample V8I28088
98093·10-05A Sample V8128089
9809310-08A Sample V8I28090
SB Blank, System V8128091
CCV_JET Continuing Calibration Verification V8I28092
CCV_KER Continuing Calibration Verification V8I28093
CCV DSL Continuing Calibration Verification V8!28094
•
10/05/98 16:48:24
Method TPH-Diesel by mod. SW8015
Lab Sample ID
File ID
•
Project Sample
ID/Description
Specif icationU -D~S~L-S_~
Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Comment/Narrative
•
Corrective Action
Work Order U 9809491
Page _7_
•
10/01/98 14:18:22
Repurl RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Pre pa red _ __:.;R::::ao:dc:i.:::a"-'n'-'I"'n"'t"'e"'r"'n"'a"'t"'i"'o:!'n::::ac:l..J.,_;L::L::::C;....
By _ _:l_,4_,,0_,4.,,6-"S"'u"'m"'m"'i"'t-""D'"'r..:.·..L• -"Bc:l::::d"'q..:.·-=B'-
P. o. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWE01
•
ID/
WORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # "'N"'A'----------
SDG # "'N'"'A _______ _
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA IRXEWAOG
SEPEWAOO
02A AS IRXEWAOG
SEPEWAOO
OJA ASD IRXEWAOG
SEPEWAOO
•
Work Order # 9809492
Page _1_
RCN 650138.0602
New York ELAP ID U: 10915
Method Desciption
IR analysis
Sep Funnel Extraction
IR dnalys1s
Sep Funnel Extraction
IR ar.alysis
Sep Funnel Extraction
•
10/01/98 14:18:22 ANALYTICAL PROTOCOL SUMMARY
F L A G D R F I N l T I 0 N S
Flag Definition
< DL
NA
NC
ND
NR
NS
A
B
c
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube 011.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match thaL 0( 01esel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydroc"arbon mix eluting in the Jet Fuel range. The pattern does not match thilL of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC coluo1n.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Resu·lts ·f·I'Om--primary and_ secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column conf irmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation .
• •
Work Order ff 9809492
Page ]_
•
lU/01/98 14:18:22
Method Oil and Grease by E413.2
Test Code IRXEWAOG
Project Sample ID:
L,1b lD:
File ID:
Date Collected:
Date Prepared:
l>ate Analyzed:
Dilution Factor:
Matrix:
Units:
l<eport as:
Column:
Analyte
011 and Grease
•
0998HBWE01
9809492-0lA
PEIR0924-56
09/21/98
09/24/98
09/24/98 16:00:00
1
Water
mg/L
received
Cone. DL
0.178 B 0.0980
RESULTS SUMMARY
Cone. DL Cone.
•
DL
Work Order tt 9809492
Page _s_
Cone. DL
•
10/01~4:18:22
Method IR Analysis
Test Code IRXEWAOG
Initial Calibration II PEIR980924160000
Calibration Date ~0~9~/~2~4~/~9~8 ____ _
Sequence/Analysis Time
1 09/24/98 16:00:00
2 09/24/98 16:00:00
3 09/24/98 16:00:00
4 09/24/98 16:00:00
5 09/24/98 16:00:00
6 09/24/98 16:00:00
7 09/24/98 16:00:00
8 09/24/98 16:00:00
9 09/24/98 16:00:00
51 09/24/98 16:00:00
52 09/24/98 16:00:00
53 09/24/98 16:00:00
54 09/24/98 16:00:00
SS 09/24/98 16:00:00
56 09/24/98 16:00:00
S7 09/24/98 16:00:00
58 09/24/98 16:00:00
59 09/24/98 16:00:00
60 09/24/98 16:00:00
ANALYSIS BAA SUMMARY
Analysis Batch~LPEIR80924160003
Analysis Start Date/Time 09/24/98 16:00:00
Analysis Stop Date/Time
work Order II 9809492
Page _6_
Instrument ~
Analyst gQQ
Reviewer ~L~K~H ________ _
Project Sample ID Lab Sample ID Sample Type Analysis File II
CAL_STDl Initial Calibration Standard 1 PEIR0924-l
CAL_STD2 Initial Calibration Standard 2 PEIR0924-2
CAL_STD3 Initial Cali brat ion Standard 3 PEIR0924-3
CAL STD4 Initial Calibration Standard 4 PEIR0924-4
I CAL_STD5 Initial Calibration Standard 5 PEIR0924-5
CAL_STD6 Initial Calibration Standard 6 PEIR0924-6
ISV Second Source Standard PEIR0924-7
ICV Initial Calibration Verification PEIR0924 -8
REAG_BLK Blank, Reagent PEIR0924-9
CCV Continuing Calibration Verification PEIR0924-51
REAG_BLANK Blank, Reagent PEIR0924-52
BLK983294 Blank, Method PEIR0924 -53
LCS98501S Lab Control Sample PEIR0924-S4
LCSD98501S Lab Control Sample Duplicate PEIR0924 -S5
0998HBWE01 9809492-0lA Sample PEIR0924-56
0998HBWE01 9809492-02A Analytical Spike PEIR0924-57
0998HBWE01 9809492-03A Analytical Spike Duplicate PEIR0924-58
REAG_BLANK Blank, Reagent PEIR0924-59
CCV Continuing Calibration Verification PEIRO 924 -6 0
••
10/01/98 14:1E:22
Method IR Analysis Specificationtt ONGE
Lab Sample ID Project Sample
File IU ID/Description Analyte
•
ANALYT!CAb PROTOCOL SUMMARY
C 0 M M B N T S / N A R R A T I V K
Flag Comment/Narrative
•
Corrective Action
work Order II .2..1!.Q~
Pt.tqe ] __
•
10/05/98 17:42:05
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _.:.;R.,,a"'d"'i"'a"'n~I"'n"'t"'e'"*r"'n"'a"'t"'i"'o::.n~a"'l'"''-.!L~Lo::C::....
By --=l-=4-=0-=4-=6'-"S"'u:.::m:::m:.::i"'t'-"D:.:r-=._.,_.B,..l"=d:::q1.:._.B,_
P. 0. Box 201088
Austin, TX 78720-1088
GSC .JALINDSEY_
Project Sample
Description
0998HBWG11-17
0998HBWG9-17
0998HBWSOURCE
-
0998HBWE01
0998HBWG10-28
0998HBWG11-6
0998HBWG10-17
0998HBWG10-6
•
-
ID/
NORK ORDBR SOMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # .N.A.._ _______ _
SDG # ;.;N;.:A'---------
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA 826SWACM
OlB SPAREBOO
OlC SUBSPROO
02A 826SWACM
02B SPAREBOO
02C SPAREBOO
03A 826SWACM
OJB SPAREBOO
03C SPAREBOO
04A 826SWACM
04B SPAREBOO
04C SPAREBOO
05A 826SWACM
OSB SPAREBOO
osc SUBS PROO
06A 826SWACM
06B SPAREBOO
06C SPAREBOO
07A 826SWACM
07B SPAREBOO
07C SPAREBOO
OBA 826SWACM
OBB SPAREBOO
•
Work Order # 9809493
Page _1_
RCN 650138. 0602
New York ELAP lD #: 10915
Method Desciption
Volatile Organics by GC/MS
Spare Sample
· Substitute Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
--Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Substitute Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
•
• 10/05/98 17:42:05
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Pre pa red _ _.R:.::a:.::do.-:i:.::a,,_n~I"-n,..t:.::e:..!r:..!n~a:.::t:..!i:.::o~n~a~l:...1--..!L~L~C=­
By _ _.1'"'4'""0'"'4'""6'-"S"'u"'m"'m'-'i'-'t'-"D:.:r...:·...<•_.B,_,l:.::d:.::qL:._.B,_
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWG10-6
0998HBWG9-6
0998HBWG11-28
0998HBWG9-28
TRIP BLANK
ID/
• ii 0 R K 0 R D B R S U H HAR Y· (Cont'd)
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # ~N~A'-~~~~~~~-
SDG # ... N~A _______ _
RAS # 80903AJAL
Lab Sample ID Test Code(s)
08C SPAREBOO
09A 826SWACM
09B SPAREBOO
09C SPAREBOO
lOA 826SWACM
lOB SPAREBOO
lOC SUBS PROO
llA 826SWACM
llB SPAREBOO
llC SPAREBOO
12A 826SWACM
Work Order # 9809493
Page L
RCN 650138. 0602
New York ELAP ID #: 10915
Method Desciption
Spare Sample
Volatiie Organics by GC/MS
. Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Substitute Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
•
10/05/98 17:42:05
•
WORK ORDER COMMENTS
The standard Method 8260A surrogate tolerances are laboratory derived from
historical data. Project specific tolerances may differ .
•
Work Order # 9809493
Page _3_
•
• 10/05/98 17:42:05
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATE CERTIFICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order tt 9809493
Page _4_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
10/05/98 17:42:05 ANALYTICAL PROTOCOL SUMMARY
Flag
< DL
NA
NC
ND
NR
NS
A
B
c
D
E
F
G
H
I
J
-K
M
p
Q
R
s
T
x
y
z
•
FLAG DEFINITIONS
Definition
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this a~alysis.
RPO and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
Analyte concentration exceeded calibration range.
Interference or coelution suspected. See Narrative for explanation.
Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
Presence of analyte previously confirmed by historical data.
Analyte identification suspect. See Narrative for explanation.
Result is less than st~ted Detection Limit but greater than or equal to specified Reporting Limit.
I.>,eak did pot; meet method identification criteria. A.-ialyte r1c1:: detected on other GC colu!lln.
See -Narrative for explanation-.--
-
Result modified from previous Report.
Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
QC result does not meet tolerance in Protocol Specification.
Result reported elsewhere.
Analyte concentration obtained using Method of Standard Additions (MSA) .
Second column conf irmational analysis not performed.
See Narrative for explanation.
See Narrative for explanation.
See Narrative for explanation.
•
Work Order U 9809493
Page _5_
•
• 10/05/98 17:42:05
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Volatile Organics SW8260B
Project Sample ID/Description
0998HBWE01
0998HBWG10-17
0998HBWG10-28
0998HBWG10-6
0998HBWG10-6
0998HBWG11-17
0998HBWG11-28
0998HBWG11-6
0998HBWG11-6
0998HBWG9-17
0998HBWG9-28
u998HBWG9-6
0998HBWSOURCE
TRIP BLANK
Lab
9809493-04A
9809493-0?A
9809493-0SA
9809493-08A
9809493-08B
9809493-0lA
9809493-lOA
9809493-06A
9809493-0GB
9809493-02A
9809493-llA
9809493-09A
9809493-03A
9809493-12A
ANALYTICAL .TOCOL SUMMARY
Extraction/Digestion
Sample ID Test Code(s) Batch #
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
Work Order # 9809493
Page _6 _
Analysis Batch #
MSMSDA80924173301
MSMSDA80924173301
MSMSDA80924173301
MSMSDA80924173301
MSMSDA80924173301
MSMSDA80925151401
MSMSDA80924173301
MSMSDA80925151401
MSMSDA80928155101
MSMSDA80925151401
MSMSDA80924173301
MSMSDA80924173301
MSMSDA80924173301
MSMSDA80924173301
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
-BrornobenzeQe _
Bromochlorornethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
carbon tetrachloride
2-~hloro-1,3-butadiene
Cl orobenzene
Crloroethane
•
0998HBWE01
9809493-04A
A0924807
09/21/98 08:00
00:00:00
09/24/98 19:55:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.834
1. 39
6.54
0.502
0.0847
0_115
0.114
if.169
0.0830
0.346
0.122
0.415
0.104
0.0858
0.0738
0.136
0.137
0.142
0.103
0.146
RBSULTS SUMMARY
0998HBWG10-17
9809493-07A
A0924809
09/21/98 10:45
00:00:00
09/24/98 20:51:00
1
Water
ug/L
received
Cone.
5.66
ND
ND
ND
0.136
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.834
1. 39
6.54
0.502
0.0847
0.115
0 .114
0 .16-9-
0. 0830
0.346
0.122
0.415
0.104
0.0858
0.0738
0.136
0.137
0 .142
0.103
0.146
0998HBWG10-28
9809493-05A
A0924808
09/21/98 11:00
00:00:00
09/24/98 20:23:00
1
Water
ug/L
received
Cone.
5.34
ND
ND
ND
0.300
ND
ND
ND
ND
ND
ND
2.38
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.834
1. 39
6.54
0.502
0.0847
0.115
0 .114
0.169
0.0830
0.346
0.122
0.415
0.104
0.0858
0.0738
0.136
0.137
0.142
0.103
0.146
Work Order # 9809493
Page _7_
0998HBWG10-6
9809493-08A
A0924810
09/21/98 10:40
00:00:00
09/24/98 21:19:00
1
Water
ug/L
received
Cone.
8.15
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.834
1. 39
6.54
0.502
0. 084 7
0.115
0.114
0.169
0.0830
0.346
0.122
0.415
0.104
0.0858
0.0738
0 .136
0.137
0.142
0.103
0.146
•
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
2-Chloroethyl vinyl ether
ChloroforM
l··Chlorohexane
Chloromethane
3-Chloroprcpene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
0998HBWE01
9809493-04A
A0924807
09/21/98 08:00
00:00:00
09/24/98 19:55:00
l
Water
ug/L
received
Cone.
ND
3. 77
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.101
0.158
0.122
0.162
0 .116
0.122
0.0996
1.10
0.127
0.150
0.209
0.561
0.0895
0.0658
0.110
0.300
0.110
0.123
0 .148
0.106
• RESULTS S UH HAR Y (Cont'd)
0998HBWG10-17
9809493-07A
A0924809
09/21/98 10:45
00:00:00
09/24/98 20:51:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.101
0.158
0.122
0.162
0.116
0.122
0.0996
1.10
0.127
0.150
0.209
0.561
0.0895
0.0658
0.110
0.300
0.110
0.123
0.148
0.106
0998HBWG10-28
9809493-05A
A0924808
09/21/98 11:00
00:00:00
09/24/98 20:23:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
NC
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.101
0.158
0.122
0.162
0. llF
0.122
0.0996
1.10
0.127
0.150
0 .209
0.561
0.0895
0.0658
0.110
0.300
0.110
0.123
0 .148
0.106
Work Order tt 9809493
Page _8_
0998HBWG10-6
9809493-08A
A0924810
09/21/98 10:40
00: 00 :'00
09/24/98 21:19:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.101
0.158
0.122
0.162
0.116
0.122
0.0996
1.10
0.127
0.150
0.209
0.561
0.0895
0.0658
0.110
0.300
0.110
0.123
0.148
0.106
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
--trans-1, 3-Dichloropropene
Ethyl methacrylate
Ethyl benzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
•
0998HBWE01
9809493-04A
A0924807
09/21/98 08:00
00:00:00
09/24/98 19:55:00
l
Water
ug/L
received
Cone. DL
ND 0.150
ND 0.132
ND 0.0646
ND 0.121
ND 0.147
ND 0.106
ND 0 .140 -
ND 0.0248
ND 0.121
ND 0.222
ND 0.237
ND 0. 0817
ND 0.0864
ND 0.0669
ND 0 .104
ND 0.105
ND 0 .203
l. 62 B 0.128
ND 0.103
ND l.17
R B S ULT S S D MM AR Y (Cont'd)
0998HBWG10-17 0998HBWG10-28
9809493-07A 9809493-05A
A0924809 A0924808
09/21/98 10:45 09/21/98 11 :00
00:00:00 00:00:00
09/24/98 20:51:00 09/24/98 20:23:00
l l
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.150 ND 0.150
ND 0.132 ND 0.132
ND 0.0646 ND 0.0646
ND 0.121 ND 0.121
ND 0.147 ND 0.147
ND 0.106 ND 0.106
ND 0 .140 ND 0 .140
ND -o-: 0248 ND 0. 0_24_8_
0.227 0.121 0.452 0.121
ND 0.222 ND 0.222
ND 0.237 ND 0.237
ND 0.0817 ND 0.0817
ND 0.0864 ND 0.0864
ND 0.0669 ND 0.0669
ND 0.104 ND 0.104
ND 0.105 ND 0.105
ND 0.203 ND 0.203
0.258 B 0.128 0.227 B 0.128
ND 0.103 ND 0.103
ND l.17 ND l.17
•
Work Order # 9809493
Page _9_
0998HBWG10-6
9809493-08A
A0924810
09/21/98 10:40
00:00:00
09/24/98 21:19:00
l
Water
ug/L
received
Cone. DL
ND 0.150
ND 0.132
ND 0.0646
ND 0.121
ND 0.147
ND 0.106
ND 0 .140
ND 0.0248
0.0394 J 0.121
ND 0.222
ND 0.237
ND 0.0817
ND 0.0864
ND 0.0669
ND 0 .104
ND 0.105
ND 0.203
0.247 B 0.128
ND 0.103
ND l.17
•
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
0998HBWE01
9809493-04A
A0924807
09/21/98 08:00
00:00:00
09/24/98 19:55:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0857
0.0927
0.101
0.152
0.142
0.573
0.123
0.148
0.0937
0.108
0. 0832
0.161
0.130
0.109
0.169
0.0730
0.0898
0.0780
0.136
0.211
• R B S ULT S S UM MAR Y (Cont'd)
0998HBWG10-17
9809493-07A
A0924809
09/21/98 10:45
00:00:00
09/24/98 20:51:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
0.304
ND
2.23
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.840
DL
0.0857
0.0927
0.101
0.152
0.142
0.573
0.123
0.148
0.0937
0.108
0. 0832
0.161
0.130
0.109
0.169
0.0730
0.0898
0.0780
0.136
0.211
0998HBWG10-28
9809493-05A
A0924808
09/21/98 11:00
00:00:00
09/24/98 20:23:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
0.475
ND
3.42
ND
ND
ND
ND
ND
.ND
ND
ND
ND
ND
ND
ND
l.25
DL
0.0857
0.0927
0.101
0.152
0.142
0.573
0.123
0.148
0.0937
0.108
0.0832
0.161
0.130
0.109
0.169
0.0730
0.0898
0.0780
0.136
0.211
Work Order # 9809493
Page lQ_
0998HBWG10-6
9809493-08A
A0924810
09/21/98 10:40
00:00:00
09/24/98 21:19:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
0 .217
ND
0.970
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0857
0.0927
0.101
0.152
0.142
0.573
0.123
0.148
0.0937
0.108
0.0832
0.161
0.130
0.109
0.169
0.0730
0.0898
0.0780
0.136
0.211
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
o-Xylene
Surrogate(s)
-
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
0998HBWE01
9809493-04A
A0924807
09/21/98 08:00
00:00:00
09/24/98 19:55:00
1
Water
ug/L
received
Cone.
ND
Recovery
%
92
103
98
PL
0.0951
RR SULT S S 0 MM ARY (Cont'd)
0998HBWG10-17
9809493-0?A
A0924809
09/21/98 10:45
00:00:00
09/24/98 20:51:00
1
Water
ug/L
received
Cone.
0.264
Recovery
%
93
103
95
DL
0.0951
0998HBWG10-28
9809493-05A
A0924808
09/21/98 11:00
00:00:00
09/24/98 20:23:00
l
Water
ug/L
received
Cone.
0.374
Recovery
%
94
103
97
DL
0.0951
---
Work Order tt 9809493
Page ll__
0998HBWG10-6
9809493-08A
A0924810
09/21/98 10:40
00:00:00
09/24/98 21:19:00
l
Water
ug/L
received
Cone. DL
ND 0.0951
Recovery
%
92
102
84 Q
•
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix: -
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acryloni tr ile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-au·tanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
0998HBWG10-6
9809493-088
A0924830
09/21/98 10:40
00:00:00
09/25/98 11:41:00
1
Water
ug/L
received
Cone. DL
7.97 0.834
ND l. 39
ND 6.54
ND 0.502
ND 0.0847
ND 0 .115
ND 0.114
ND 0.169
ND 0.0830
ND 0.346
ND 0.122
ND 0 .415
ND 0.104
ND 0.0858
ND 0.0738
ND 0.136
ND 0.137
ND 0.142
ND 0.103
ND 0.146
• R E SULT S SUMMARY (Cont'd)
0998HBWGll-17 0998HBWG11-28
9809493-0lA 9809493-lOA
A0925810 A0924812
09/21/98 08:55 09/21/98 09:15
00:00:00 00:00:00
09/25/98 18:59:00 09/24/98 22:16:00
2 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND Y l. 67 5.51 0.834
ND y ·2.78 ND 1.39
ND y 13.1 ND 6.54
ND Y l. 00 ND 0.502
0.223 y 0.169 0.324 0.0847
ND y 0.230 ND 0.115
ND y 0.228 ND 0.114
ND y 0.338 ND 0.169
ND y 0.166 ND 0.0830
ND y 0.692 ND 0.346
ND y 0.244 ND 0.122
ND Y 0.830 ND 0.415
ND Y 0.208 ND 0 .104
ND y 0.172 ND 0.0858
ND y 0.148 ND 0.0738
ND y 0.272 ND 0.136
ND y 0.274 ND 0.137
ND y 0.284 ND 0.142
ND y 0.206 ND 0.103
ND y 0 .292 ND 0 .146
Work Order tt 9809493
Page g_
0998HBWGll-6
9809493-06A
A0925812
09/21/98 08:45
00:00:00
09/25/98 19:55:00
2
Water
ug/L
received
Cone. DL
ND YR l. 67
ND YR 2.78
ND YR 13.1
ND YR l. 00
ND YR 0.169
ND YR 0.230
ND YR 0.228
ND YR 0.338
ND YR 0.166
ND YR 0.692
ND YR 0.244
ND YR 0.830
ND YR 0.208
ND YR 0.172
ND YR 0.148
ND YR 0.272
ND YR 0.274
ND YR 0.284
ND YR 0.206
ND YR 0.292
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
2-Chloroethyl vinyl ether
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Cfilorotoruene
l,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
l,2-Dichlorobenzene
l,3-Dichlorobenzene
l,4-Dichlorobenzene
Dichlorodif luoromethane
l,l-Dichloroethane
l,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
•
0998HBWGl0-6
9809493-088
A0924830
09/21/98 10:40
00:00:00
09/25/98 11:41:00
1
Water
ug/L
received
Cone. DL
ND 0.101
ND 0.158
ND 0.122
ND 0.162
ND 0.116
ND 0.122
ND 0.0996
--ND 1.10
ND 0.127
ND 0.150
ND 0. 209
ND 0.561
ND 0.0895
ND 0.0658
ND 0.110
ND 0.300
ND 0.110
ND 0.123
ND 0.148
ND 0.106
R B S 0 L T S S 0 M M A R Y (Cont'd)
0998HBWGll-l7 0998HBWGll-28
9809493-0lA 9809493-lOA
A0925810 A0924812
09/21/98 08:55 09/21/98 09:15
00:00:00 00:00:00
09/25/98 18:59:00 09/24/98 22:16:00
2 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND y 0.202 ND 0.101
ND y 0.316 ND 0.158
ND Y 0.244 ND 0.122
ND y 0.324 ND 0.162
ND y 0.232 ND 0.116
ND Y 0.244 ND 0.122
ND Y 0.199 ND 0. 0996
--ND Y 2.20 tiD 1.10 ---
ND Y 0.254 ND 0.127
ND y 0.300 ND 0.150
ND y 0.418 ND 0.209
ND Y 1.12 ND 0.561
ND y 0.179 ND 0.0895
ND y 0.132 ND 0.0658
ND y 0.220 ND 0.110
ND y 0.600 ND 0.300
ND y 0.220 ND 0.110
ND y 0. 246 ND 0.123
ND y 0.296 ND 0 .148
ND y 0.212 ND 0.106
•
Work Order # 9809493
Page D_
0998HBWGll-6
9809493-0GA
A0925812
09/21/98 08:45
00:00:00
09/25/98 19:55:00
2
Water
ug/L
received
Cone. DL
ND YR 0.202
ND YR 0.316
ND YR 0.244
ND YR 0.324
ND YR 0.232
ND YR 0.244
ND YR 0.199
ND YR 2.20
-ND YR 0.254
ND YR 0.300
ND YR 0.418
ND YR l.12
ND YR 0.179
ND YR 0.132
ND YR 0.220
ND YR 0.600
ND YR 0.220
ND YR 0.246
ND YR 0.296
ND YR 0.212
•
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
trans-1,2-Dichloroethene
1,2-Dichloropropane
l,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-l,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
0998HBWG10-6
9809493-088
A0924830
09/21/98 10:40
00:00:00
09/25/98 11:41:00
l
Water
ug/L
received
Cone. DL
ND 0.150
ND 0.132
ND 0.0646
ND 0.121
ND 0.147
ND 0.106
ND 0 .140
ND 0.0248
0. 04 74 J 0.121
ND 0.222
ND 0.237
ND 0. 0817
ND 0.0864
ND 0.0669
ND 0.104
ND 0.105
ND 0.203
0.281 B 0.128
ND 0.103
ND l. l 7
• RESULTS SUMMARY (Cont'd)
0998HBWG11-l 7 0998HBWG11-28
9809493-0lA 9809493-lOA
A0925810 A0924812
09/21/98 08:55 09/21/98 09:15
00:00:00 00:00:00
09/25/98 18:59:00 09/24/98 22:16:00
2 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND y 0.300 ND 0.150
ND y 0.264 ND 0.132
ND y 0.129 ND 0.0646
ND y 0.242 ND 0.121
ND y 0.294 ND 0.147
ND y 0.212 ND 0.106
ND Y 0.280 ND 0 .140
ND y 0. 0496 ND 0.0248
0.216 YJ 0.242 0.346 0.121
ND y 0.444 ND 0.222
ND y 0.474 ND 0.237
ND Y 0.163 ND 0. 0817
ND Y 0.173 ND 0.0864
ND y 0.134 ND 0.0669
ND y 0.208 ND 0.104
ND y 0.210 ND 0.105
ND y 0 .406 ND 0.203
0.826 BY 0.256 0.256 B 0.128
ND Y 0.206 ND 0.103
ND Y 2.34 ND l.17
Work Order tt 9809493
Page .!!._
0998HBWG11-6
9809493-06A
A0925812
09/21/98 08:45
00:00:00
09/25/98 19:55:00
2
Water
ug/L
received
Cone. DL
ND YR 0.300
ND YR 0.264
ND YR 0.129
ND YR 0.242
ND YR 0.294
ND YR 0.212
ND YR 0.280
ND YR 0.0496
ND YR 0.242
ND YR 0.444
ND YR 0.474
ND YR 0.163
ND YR 0.173
ND YR 0.134
ND YR 0.208
ND YR 0.210
ND YR 0 .406
0.844 YR 0.256
ND YR 0.206
ND YR 2.34
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Uni ts:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrac~loroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
•
0998HBWG10-6
9809493-088
A0924830
09/21/98 10 :40
00:00:00
09/25/98 11:41:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
0.224
ND
0.996
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0857
0.0927
0.101
0.152
0.142
0.573
0.123
0 .148
0.0937
0.108
0. 0832
0.161
0.130
0_109
0,169
0.0730
0.0898
0.0780
0.136
0.211
RESULTS S UM M A R Y (Cont'd)
0998HBWG11-l 7
9809493-0lA
A0925810
09/21/98 08:55
00:00:00
09/25/98 18:59:00
2
Water
ug/L
received
Cone.
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
2.71 y
ND Y
ND Y
ND Y
ND Y
ND Y
ND y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
0.954 y
•
DL
0.171
0.185
0.202
0.304
0.284
l.lS
0.246
·o .296-
0 .101
0.216
0.166
0.322
0.260
0.218
0.338
0 .146
0.180
0.156
0.272
0.422
0998HBWG11-28
9809493-lOA
A0924812
09/21/98 09:15
00:00:00
09/24/98 22:16:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
0.457
ND
3.36
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
o. 677
DL
0.0857
0.0927
0.101
0.152
0.142
0.573
0.123
0.148
0.0937
0.108
0.0832
0.161
0.130
0.109
0 .169
0.0730
0.0898
0.0780
0.136
0 .211
Work Order # 9809493
Page ~
0998HBWG11-6
9809493-06A
A0925812
09/21/98 08:45
00:00:00
09/25/98 19:55:00
2
Water
ug/L
received
Cone.
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
l. 64 YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
ND YR
DL
0 .171
0.185
0.202
0.304
0.284
1.15
0.246
0.296
0.187
0.216
0.166
0 .322
0.260
0 .218
0.338
0.146
0.180
0.156
0. 272
0.422
•
• 10/05/~B 17:42:05
Method Volatile Organics SWB260B
Test Code B26SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
a-Xylene
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
099BHBWG10-6
9B09493-0BB
A0924B30
09/21/9B 10:40
00:00:00
09/25/9B 11:41:00
1
Water
ug/L
received
Cone. DL
ND 0.0951
Recovery
%
92
106
BB
• RESULTS SUMMARY (Cont'd}
099BHBWG11-17
9B09493-01A
A0925B10
09/21/98 OB:55
00:00:00
09/25/98 18:59:00
2
Water
ug/L
received
Cone. DL
ND Y 0.190
Recovery
%
94 y
107 y
9B y
099BHBWG11-2B
9809493-lOA
A0924812
09/21/9B 09:15
00:00:00
09/24/9B 22:16:00
1
Water
ug/L
received
Cone.
0 .240
Recovery
%
94
103
99
DL
0.0951
Work Order.# 9B09493
Page .!:.£._
099BHBWG11-6
9B09493-06A
A0925812
09/21/9B 08:45
00:00:00
09/25/9B 19:55:00
2
Water
ug/L
received
Cone. DL
ND YR 0.190
Recovery
%
91 YR
106 YR
B4 Q YR
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column_:
Analyte
Acetone
Acetonitrile
Aero le in
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
-
Bromobenzene ---
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l,3-butadiene
Chlorobenzene
Chloroethane
•
0998HBWGll-6
9809493-068
A0928806
09/21/98 08:45
00:00:00
09/28/98 17:44:00
2
Water
ug/L
received
Cone. DL
ND y l. 67
ND Y 2.78
ND y 13.1
ND Y l. 00
ND Y 0.169
ND Y 0.230
ND y 0.228
ND y 0.338
ND y 0.166
ND Y 0.692
ND y 0.244
ND y 0.830
ND y 0.208
ND y 0.172
ND y 0 .148
ND y 0.272
ND Y 0.274
ND Y 0.284
ND Y 0.206
ND Y 0.292
RESULTS S UH HA R Y (Cont'd)
0998HBWG9-17 0998HBWG9-28
9809493-02A 9809493-llA
A0925811 A09248l3
09/21/98 13:10 09/21/98 13 :30
00:00:00 00:00:00
09/25/98 19:27:00 09/24/98 22:44:00
2 l
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND Y 1.67 6.87 0.834
ND y 2.78 ND l. 39
ND y 13.1 ND 6.54
ND Y l. 00 ND 0.502
0.229 y 0.169 0.354 0.0847
ND Y 0.230 ND 0.115
ND Y 0.228 ND 0.114
ND Y -0.3-39 ND---0.169
ND y 0.166 ND 0.0830
ND y 0.692 ND 0.346
ND y 0.244 ND 0.122
ND y 0.830 ND 0.415
ND Y 0.208 ND 0.104
ND y 0.172 ND 0.0858
ND y 0.148 ND 0.0738
ND y 0.272 ND 0.136
ND Y 0.274 ND 0.137
ND Y 0.284 ND 0 .142
ND y 0.206 ND 0.103
ND y 0.292 ND 0.146
•
Work Order U 9809493
Page 1L
0998HBWG9-6
9809493-09A
A0924Bll
09/21/98 13 :OS
00:00:00
09/24/98 21:48:00
l
Water
ug/L
received
Cone. DL
7.02 0.834
ND l. 39
ND 6.54
ND 0.502
ND 0.0847
ND 0.115
ND 0 .114
ND 0.169
---
ND 0.0830
ND 0.346
ND 0.122
ND 0.415
ND 0.104
ND 0.0858
ND 0.0738
ND 0.136
ND 0.137
ND 0.142
ND 0.103
ND 0.146
•
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
2-Chloroethyl vinyl ether
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
0998HBWG11-6
9809493-06B
A0928806
09/21/98 08:45
00:00:00
09/28/98 17:44:00
2
Water
ug/L
received
Cone.
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
DL
0.202
0.316
0.244
0.324
0.232
0.244
0.199
2.20
0.254
0.300
0.418
1.12
0.179
0.132
0.220
0.600
0.220
0.246
0 .296
0.212
• R B S U L T S S UM MA R Y (Cont'd)
0998HBWG9-17
9809493-02A
A0925811
09/21/98 13:10
00:00:00
09/25/98 19:27:00
2
Water
ug/L
received
Cone.
ND y
ND Y
ND y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND Y
ND y
ND Y
ND Y
ND Y
ND Y
ND Y
ND y
DL
0.202
0.316
0.244
0.324
0.232
0.244
0.199
2.20
0.254
0.300
0.418
1.12
0.179
0.132
0.220
0.600
0.220
0.246
0.296
0.212
0998HBWG9-28
9809493-llA
A0924813
09/21/98 13:30
00:00:00
09/24/98 22:44:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.29
ND
0.598
ND
DL
0.101
0.158
0.122
0.162
0.116
0.122
0. 0996
1.10
0.127
0.150
0.209
0.561
0.0895
0.0658
0.110
0.300
0.110
0.123
0.148
0.106
Work Order # 9809493
Page 1_L
0998HBWG9-6
9809493-09A
A0924811
09/21/98 13:05
00:00:00
09/24/98 21:48:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
0.354
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.41
ND
3.52
ND
DL
0.101
0.158
0.122
0.162
0 .116
0.122
0.0996
1.10
0.127
0.150
0.209
0.561
0.0895
0.0658
0.110
0.300
0.110
0.123
0 .148
0.106
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
•
0998HBWG11-6
9809493-06B
A0928806
09/21/98 08:45
00:00:00
09/28/98 17:44:00
2
Water
ug/L
received
Cone. DL
ND y 0.300
ND y 0.264
ND y 0.129
ND y 0.242
ND y 0.294
ND y 0.212
ND y_ o_.200
ND y 0. 0496
ND Y 0.242
ND Y 0.444
ND Y 0.474
ND y 0.163
ND y 0.173
ND y 0.134
ND Y 0.208
ND y 0.210
ND y 0 .406
0.608 BY 0.256
ND y 0.206
ND y 2.34
RBS 0 LT S S 0 MM ARY (Cont'd)
0998HBWG9-17 0998HBWG9-28
9809493-02A 9809493-llA
A0925811 A0924813
09/21/98 13:10 09/21/98 13:30
00:00:00 00:00:00
09/25/98 19:27:00 09/24/98 22:44:00
2 1
Water Water
ug/L ug/L
received received
Cone. PL Cone. DL
ND Y 0.300 ND 0.150
ND y 0.264 ND 0.132
ND y 0.129 ND 0.0646
ND y 0.242 ND 0.121
ND y 0.294 ND 0.147
ND y 0.212 ND 0.106
ND Y 0.280 ND 0 .140
-.
ND y 0. 04 96 --NE>· 0 .02.48
0.248 y 0.242 0.407 0.121
ND Y 0.444 ND 0.222
ND y 0.474 ND 0.237
ND Y 0.163 ND 0. 0817
ND y 0.173 ND 0.0864
ND y 0.134 ND 0.0669
ND Y 0.208 ND 0.104
ND Y 0.210 ND 0.105
ND y 0.406 ND 0.203
0.695 BY 0.256 0.262 B 0.128
ND y 0.206 ND 0.103
ND y 2.34 ND 1.17
•
Work Order # 9809493
Page 12._
0998HBWG9-6
9809493-09A
A0924811
09/21/98 13:05
00:00:00
09/24/98 21:48:00
l
Water
ug/L
received
Cone. DL
ND 0.150
ND 0 .132
ND 0.0646
ND 0.121
ND 0.147
ND 0.106
ND 0.140
ND 0. 0248
0.139 0.121
ND 0.222
ND 0.237
ND 0.0817
ND 0.0864
ND 0.0669
ND 0.104
ND 0.105
ND 0.203
0.334 B 0.128
ND 0.103
ND 1.17
•
• 10/05/98 17:~2:05
Method '!olatile Organics SWC:?.60B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrof uran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
0998HBWG11-6
9809493-068
A0928806
09/21/98 08:45
00:00:00
09/28/98 17:44:00
2
Water
ug/L
received
Cone. DL
ND Y 0.171
ND y 0.185
ND y 0.202
ND y 0.304
ND y 0.284
ND Y 1.15
1.41 y 0.246
ND y 0.296
ND Y 0.187
0.232 BY 0.216
ND y 0.166
ND y 0.322
ND y 0.260
ND y 0.218
ND y 0.338
ND y 0.146
ND Y 0.180
ND y 0.156
ND y 0.272
ND y 0.422
• RESULTS S UH H A R Y (Cont'd)
0998HBWG9-17 0998HBWG9.-28
9809493-02A 9809493-llA
A0925811 A0924813
09/21/98 13:10 09/21/98 13:30
00:00:00 00:00:00
09/25/98 19:27:00 09/24/98 22:44:00
2 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND y 0.171 ND 0.0857
ND Y 0.185 ND 0.0927
ND y 0.202 ND 0.101
ND y 0.304 ND 0.152
0 .461 y 0.284 0.562 0.142
ND y 1.15 ND 0.573
3.23 y 0.246 3.34 0.123
ND y 0.296 ND 0.148
ND y 0.187 ND 0.0937
ND y 0.216 ND 0.108
ND y 0.166 ND 0.0832
ND y 0.322 0.901 0.161
ND y 0.260 ND 0.130
ND Y 0.218 ND 0.109
ND Y p.338 ND 0.169
ND y 0.146 ND 0.0730
ND Y 0.180 ND 0.0898
ND y 0.156 ND 0.0780
ND y 0.272 ND 0.136
1.05 y 0.422 0.880 0.211
Work Order # 9809493
Page 1Q_
0998HBWG9-6
9809493-09A
A0924811
09/21/98 13:05
00:00:00
09/24/98 21:48:00
1
Water
ug/L
received
Cone. DL
ND 0.0857
ND 0. 0927
ND 0.101
ND 0.152
0.596 0.142
ND 0.573
l. 88 0.123
ND 0.148
ND 0.0937
2.37 0.108
ND 0.0832
3.21 0.161
ND 0.130
ND 0.109
ND 0.169
ND 0.0730
ND 0.0898
ND 0.0780
ND 0.136
0.375 0.211
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
o-Xylene
Su=ogate(s)
l,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
0998HBWG11-6
9809493-06B
A0928806
09/21/98 08:45
00:00:00
09/28/98 17:44:00
2
Water
ug/L
received
Cone.
ND Y
Recovery
%
92 y
108 y
88 '{
DL
0.190
R E S U L T S S UM M AR Y (Cont'd)
0998HBWG9-17
9809493-02A
A0925811
09/21/98 13:10
00:00:00
09/25/98 19:27:00
2
Water
ug/L
received
Cone.
ND Y
Recovery
%
94 '{
106 '{
96 '{
•
DL
0.190
-
0998HBWG9-28
9809493-llA
A0924813
09/21/98 13: 30
00:00:00
09/24/98 22:44:00
l
Water
ug/L
received
Cone.
0. 349
Recovery
%
92
102
98
DL
0.0951
Work Order n 9809493
Page £!__
0998HBWG9-6
9809493-09A
A0924811
09/21/98 13:05
00:00:00
09/24/98 21:48:00
l
Water
ug/L
received
Cone. DL
ND 0.0951
Recovery
%
94
104
91
••
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
2-Chloroethyl vinyl ether
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
-4-Chlorotoluene
l,2-Dibromo-3-chloropropane
Dibromochloromethane
l,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
l,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
l,2-Dichloroethane
l,1-Dichloroethene
cis-1,2-Dichloroethene
•
0998HBWSOURCE
9809493-03A
A0924806
09/21/98 08:15
00:00:00
09/24/98 19:27:00
1
Water
ug/L
received
Cone. DL
ND 0.101
7.93 0.158
ND 0.122
ND 0.162
ND 0.116
ND 0.122
-----ND 0.0996
ND l.10
l. 84 0.127
ND 0.150
ND 0.209
ND 0.561
ND 0.0895
ND 0.0658
ND 0.110
ND 0.300
ND 0.110
ND 0.123
ND 0 .148
ND 0.106
RESULTS S UM MA R Y (Cont'd)
TRIP BLANK
9809493-l2A
A0924814
09/21/98
00:00:00
09/24/98 23:12:00
1
Water
ug/L
received
Cone. DL
ND 0.101
ND 0.158
ND 0.122
ND 0.162
ND 0.116
ND 0.122
ND 0.0996
ND ·-i ~TO
ND 0.127
ND 0.150
ND 0.209
ND 0.561
ND 0.0895
ND 0.0658
ND 0.110
ND 0.300
ND 0.110
ND 0.123
ND 0.148
ND 0.106
•
Cone. DL
Work Order tt 9809493
Page 1l_
Cone.
-
DL
••
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
0998HBWSOURCE
9809493-03A
A0924806
09/21/98 08:15
00:00:00
09/24/98 19:27:00
1
Water
ug/L
received
Cone. DL
ND 0.150
ND 0.132
ND 0.0646
ND 0.121
ND 0.147
ND 0.106
ND 0.140
ND 0.0248
ND 0.121
ND 0.222
ND 0.237
ND 0.0817
ND 0.0864
ND 0.0669
ND 0.104
ND 0.105
ND 0.203
0.276 B 0.128
ND 0.103
ND 1.17
• RBSULTS S UM MARY (Cont'd)
TRIP BLANK
9809493-12A
A0924814
09/21/98
00:00:00
09/24/98 23:12:00
1
Water
ug/L
received
Cone. DL
ND 0.150
ND 0.132
ND 0.0646
ND 0.121
ND 0.147
ND 0.106
ND 0 .140
ND 0. 0248
ND 0 .121
ND 0.222
ND 0.237
ND 0.0817
ND 0.0864
ND 0.0669
ND 0.104
ND : 0.105
ND 0.203
0.318 B 0.128
ND 0.103
ND 1.17
Cone. DL
Work Order # 9809493
Page~
Cone.
•
DL
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
-Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
•
0998HBWSOURCE
9809493-03A
A0924806
09/21/98 08:15
00:00:00
09/24/98 19:27:00
1
Water
ug/L
received
Cone. DL
ND 0.0857
ND 0.0927
ND 0.101
ND 0.152
ND 0.142
ND 0.573
ND 0.123 -
ND 0.148
ND 0.0937
ND 0.108
ND 0.0832
ND 0.161
ND 0.130
ND 0.109
ND 0.169
ND 0.0730
ND 0.0898
ND 0.0780
ND 0.136
ND 0.211
RESULTS S U M M A R Y (Cont'd)
TRIP BLANK
9809493-12A
A0924814
09/21/98
00:00:00
09/24/98 23:12:00
1
Water
ug/L
received
Cone. DL
ND 0.0857
ND 0.0927
ND 0.101
ND 0.152
ND 0.142
ND 0.573
ND 0.123
ND 0 ,14_8
ND 0.0937
ND 0.108
ND 0.0832
ND 0.161
ND 0.130
ND 0.109
ND 0.169
ND 0.0730
ND 0.0898
ND 0.0780
ND 0.136
ND 0.211
•
Cone. DL
Work Order # 9809493
Page~
Cone.
-
DL
•
lG/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code ~?~
Initial Calibration U MSDA9809J6000000
Calibration Date _0_9_/_16_/_9~8~~~~-
Sequence/Analysis Time
1 09/24/98 17:05:00
2 09/24/98 17:33:00
3 09/24/98 17:33:00
4 09/24/98 18:02:00
5 09/24/98 18:31:00
6 09/24/98 18:59:00
7 09/24/98 19:27:00
8 09/24/98 19:55:00
9 09/24/98 20:23:00
10 09/24/98 20:51:00
11 09/24/98 21:19:00
12 09/24/98 21:48:00
13 09/24/98 22:16:00
14 09/24/98 22:44:00
15 09/24/98 23:12:00
16 09/24/98 23:40:00
17 09/25/98 00:08:00
18 '09/25/98 00:36:00
19 09/25/98 01:04:00
20 09/25/98 01:33:00
21 09/25/98 02:01:00
22 09/25/98 02:29:00
23 09/25/98 02:57:00
24 09/25/98 03:25:00
25 09/25/98 03:53:00
26 09/25/98 04:21:00
27 09/25/98 04:51:00
28 09/25/98 05:20:00
29 09/25/98 10:45:00
30 09/25/98 11:13:00
•
ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDA80924173301
Analysis Start Date/Time Q1L24/98 17:33:00
Analysis. Stop Date/Time 0~/2~,/18 .. !1.L'22..:.QQ
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
VSTDCAL Continuing Calibration
LCS984877 Lab Control Sample
Work Order # 9809493
Page ~
Instrument MSDA
Ana~yst !lli£
Revi~wer _A_P_S~~~~~~~~
Analysis File jj
A0924801
A0924802
Verification A0924802
A0924803
LCSD984878 Lab Control Sample Duplicate A0924804
BLK983206 Blank, Method A0924805
0998HBWSOURCE 9809493-03A Sample A0924806
0998HBWE01 9809493-04A Sample A0924807
0998HBWG10-28 9809493-05A Sample A0924808
0998HI:JWG10-17 9809493-0?A Sample A0924809
0998HBWG10-6 9809493-08A Sample A0924810
0998HBWG9-6 9809493-09A Sample A0924811
0998HBWG11-28 9809493-lOA Sample A0924812
0998HBWG9-28 --9809493-llA Sample A0924813
TRIP BLANK 9809493-12A - -Sample A0924814 ---
9809405-0lA Sample A0924815
9809405-02A Sample A0924816
9809405-03A Sample A0924817
9809401-0lA Sample A0924818
9809401-08A Matrix Spike A0924819
9809401-09A Matrix Spik_; Duplicate A0924820
9809401-02A Sample A0924821
9809401-03A Sample A0924822
9809363-05A Sample A0924823
9809363-06A Sample A0924824
9809363-07A Sample A0924825
9809369-03B Sample A0924826
9809369-04B Sample A0924827
SB Blank, System A0924828
BFB GCiMs tune files A0924829
• •
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWA00
Initial Calibration II MSDA980916000000
Calibration Date ~0-9./~1~6·/-9~8~~~~-
Sequence/Analysis Time
31 09/25/98 11:13:00
32 09/25/98 11:41:00
33 09/25/98 12:09:00
34 09/25/98 12:37:00
35 09/25/98 13:05:00
• AH ALYS I S BATCH S UM MARY (cont'd)
Analysis Batch II MSMSDA80924173301
Analysis Start Date/Time 09/24/98 17:33:00
Analysis·Stop Date/Time 09/25/98 13:05:00
Project Sample ID Lab Sample ID Sample Type
Work Order II 9809493
Page £§__
Instrument ~
Analyst ill!£
Reviewer ~A~P~S~~~~~~~~-
Analysis File II
VSTDCAL Continuing Calibration Verification A0924829
0998HBWG10-6 9809493-088 Sample A0924830
9809405-028 Sample A0924831
9809405-0lB Sample A0924832
9809363-058 Sample A0924833
•
10/05/96 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDA980916000000
Calibration Date "'0""'9,,_/-=l ... 6._/=-9=-8 ___ _
Sequence/Analysis Time
1 09/25/98 14:46:00
2 09/25/98 15:14:00
3 09/25/98 15:14:00
4 09/25/98 15:42:00
5 09/25/98 16:10:00
6 09/25/98 16:38:00
7 09/25/98 17:07:00
8 09/25/98 17:35:00
9 09/25/98 18:03:00
10 09/25/98 18:31:00
11 09/25/98 18:59:00
12 09/25/98 19:27:00
13 09/25/98 19:55:00
14 09/25/98 20:24:00
15 09/25/98 20:52:00
16 09/25/98 21:20:00
17 09/25/98 21:48:00
16 09/25/98 22:16:00
19 09/25/98 22:44:00
20 09/25/98 23:12:00
21 09/25/98 23:40:00
22 09/26/98 00:09:00
23 09/26/98 00:37:00
24 09/26/98 01:05:00
25 09/26/98 01:33:00
26 09/26/98 02:01:00
27 09/26/98 02:29:00
28 09/26/98 02:57:00
•
ANALYSIS BATCH SOHHARY
Analysis Batch # MSMSDA80925151401
Analysis Start Date/Time 09/25/98 15:14:00
Analysis Stop Date/Time 09/26/98 02:57:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
VS TD CAL Continuing Calibration
LCS984879 Lab Control Sample
Work Order # 9809493
Page l.2_
Instrument MSDA
Analyst !2§£
Reviewer ~A~P=S-------~
Analysis File #
A0925801
A0925802
Verification A0925802
A0925803
LCSD9848780 Lab Control Sample Duplicate A0925804
BLK983207 Blank, Method A0925805
9809519-06A Sample A0925806
9809519-07A Matrix Spike A0925807
9809519-08A Matrix Spike Duplicate A0925808
9809519-02A Sample A0925809
0998HBWG11-17 9809493-0lA Sample A0925810
0998HBWG9-17 9809493-02A Sample A0925811
0998HBWG11-6 9809493-06A Sample A0925812
9809519-0lA Sample A0925813
-98095-19---03A SampJe A0925814
9809519-04A Sample A0-92581:5
9809519-05A Sample A0925816
9809519-0~A S.:!mp!e A092S817
9809528-02A Sample A0925818
9809528-08A Sample A0925819
9809527-07A Sample A0925820
9809527-llA Sample A0925821
9809401-04A Sample A0925822
9809401-05A Sample A0925823
9809401-06A Sample A0925824
9809401-07A Sample A0925825
9809391-0lA Sample A0925826
9809391-02A Sample . A0925827
• •
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDA980916000000
Calibration Date ~0~9~/1~6~/~9~8::.--~~~-
Sequence/Analysis Time
1 09/28/98 15:23:00
2 09/28/98 15:51:00
3 09/28/98 15:51:00
4 09/28/98 16:19:00
5 09/28/98 16:47:00
6 09/28/98 17:16:00
7 09/28/98 17:44:00
8 09/28/98 18:12:00
9 09/28/98 18:40:00
'-:. 10 09/28/98 19:08:00
11 09/28/98 19:38:00
12 09/28/98 20:07:00
13 09/28/98 20:35:00
14 09/28/98 21:04:00
15 09/28/98 21:32:00
16 09/28/98 22:00:00
17 09/28/98 22:28:00
18 09/28/98 22:56:00
19 09/28/98 23:24:00
20 09/28/98 23:52:00
21 09/29/98 00:20:00
22 09/29/98 00:49:00
23 09/29/98 01:17:00
24 09/29/98 01:45:00
25 09/29/98 02:13:00
26 09/29/98 02:41:00
27 09/29/98 03:09:00
28 09/29/98 03:37:00
29 09/29/98 05:54:00
30 09/29/98 06:22:00
• ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDA80928155101
Analysis Start Date/Time 09/28/S8 15:51:00
Analysis Stop Date/Time 09/29/98 08:44:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
VSTDCAL Continuing Calibration
LCS984881 Lab Control Sample
Work Order # 9809493
Page lQ_
Instrument ~
Analyst ~
Reviewer ~A~P~S~~~~~~~~
Analysis File U
A0928801
A0928802
Verification A0928802
A0928803
LCSD9848782 Lab Control Sample Duplicate A0928804
BLK983208 Blank, Method A0928805
0998HBWG11-6 9809493-06B Sample A0928806
9809528-02C Sample A0928807
9809528-08B Sample A0928808
9809527-llB Sample A0928809
9809527-07B Sample A0928810
9809519-0lB Sample A0928811
9809519-03B Sample A0928812
9809519-05B Sample A0928813
9809519-09B Sample A0928814
9809401-04B Sample A0928815
9809401-05B Sample A0928816
9809401-06B Sample A0928817
9809401-07B Sample A0928818
9809464-0lA Sample A0928819
9809464-03A Matrix Spike A0928820
9809464-04A Matrix Spike Duplicate A0928821
9809464-02A Blank, TCLP Extraction A0928822
9809469-0lA Sample A09288?3
9809469-02A Sample A0928824
9809469-03A Sample A0928825
9809469-04A Sample A0928826
9809469-05A Sample . A0928827
SB Blank, System A0928828
BFB GC/MS tune files A0928829
•
10/05/98 17:42:05
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDA980916000000
Calibration Date ~0~9L/~1~6L/~9~8~~~~-
Sequence/Analysis Time
31 09/29/98 06:22:00
32 09/29/98 06:50:00
33 09/29/98 07:18:00
34 09/29/98 07·:46:00
35 09/29/98 08:14:00
36 09/29/98 08:44:00
•
Project Sample
AN ALY S I S BATCH S 0 MM ARY (cont'd)
Analysis Batch # MSMSDA80928155101
Analysis Start Date/Time 09/28/98 15:51:00
Analysis Stop Date/Time 09/29/98 08:44:00
ID Lab Sample ID Sample Type
Work Order # 9809493
Page lL
Instrument ~
Analyst ~
Reviewer ~A~P~S~~~~~~~~-
Analysis File #
VSTDCAL Continuing Calibration Verification A0928829
9809519-09C Sample A0928831
9809519-0lC Sample A0928832
9809519-03C Sample A0928833
9809469-028 Sample A0928834
9809469-0lB Sample A0928835
• •
• 10/05/98 17:42:05
Method Volatile Organics SW8260B
Lab Sample ID
File ID
9809493-0lA
A0925810
9809493-0ZA
A0925811
9809493-0GA
A092s012
9809493-068
A0928806
Project Sample
ID/Description
0998HBWG11-17
0998HBWG9-17
0998HBWG11-6
0998HBWG11-6
Specification#
Analyte
All analytes
All analytes
All analytes
All analytes
• ARALYTICAL PROTOCOL SUMMARY
COMMBRTS/RARRATIVB
Flag Comment/Narrative
y
y
y
y
This sample was analyzed at 2X due to a large
amount of sediment in the VOA vial (limited
sample).
This sample was analyzed at 2X due to a large
amount of sediment in the VOA vial (limited
sample).
This sample was analyzed at 2X due to a large
amount of sediment in the VOA vial (limited
sample) .
This sample was analyzed at 2X due to a large
amount of sediment in the VOA vial (limited
sample).
Work Order #.93
Page R._
Corrective Action
10/05/98 17:42:05
•
0 U A L I T Y C 0 H T 11 0 L B JI: C B P T I 0 H R B P 0 R T
SUMMARY
QCER # Analysis Batch Number
980922-02
980925-07 MSMSDA980925151400
•
Work Order # 9809493
Page l]_
•
10/01/98 08:34:15
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared ~--"'R_a_d_i_a~n'-'"I_n_t_e_r_n_a_t_i_o~n_a_l~,-"L_L~C­
By ~-=1~4~0~4~6-"S~u~m~m~i~t-""D~r~·~·-""B~l~d~q~·-=B­
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWE01
TRIP BLANK
•
ID/
NORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # ~N_A ________ _
SDG # ~NA'"'-~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA GASSWAGU
018 SPAREBOO
OlC SPAREBOO
02A GASSWAGU
•
Work Order # 9809494
Page _1_
RCN 650138.0602
New York ELAP ID#: 10915
Method Desciption
Gas/BTEX by Purge&Trap GC
Spare Sample
Spare Sample
Gas/BTEX by Purge&Trap GC
•
• lO/Ol/98 08:34:15
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Pre pared --"R:=a"'d:..:i:=a::;n'--=I"'n"'t"'e"'r-"n:::a:..:t:..:i;;;:o::.n:::a:..:l:.<,...:;L:..:L:..:C;...
By _ _:l,:o4~0,:o4~6~S"'u"'m"'m::ic::t_::D::r...:._.,_::B::l:.::d::=9L.:·.....::B:...
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWE01
TRIP BLANK
ID/
• WOR~ ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case H .N.A.._ ___ ~-~--
SDG # ~N~A'---------­
RAS II 80903AJAL
Lab Sample ID Test Code(s)
OlA GASSWAGU
OlB SPAREBOO
OlC SPAREBOO
02A GASSWAGU
Work Order # 9809494
Page _1_
RCN 650138.0602
New York ELAP ID#: 10915
Method Desciption
Gas/BTEX by Purge&Trap GC
Spare Sample
Spare Sample
Gas/BTEX by Purge&Trap GC
•
10/01/98 08:34:15 MOii.iC Oii.DBi!. COMMBllTS
• •
Work Order U 9809494
Page L_
•
• 10/01/98 08:34:15
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIPICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order U 9809494
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
10/01/98 08:34:15 ANALYTICAL PROTOCOL SUMMARY
P L A G D R P I Ii I T I 0 Ii S
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
A
B
c
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit iand greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
·M
p
Result modified from p.revio.us Report.
Analyte not confirmed. Results from
See Narra_tive for explanation.
primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s Analyte concentration obtained using Method of Standard Additions (MSA).
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation .
• •
Work Order # 9809494
Page _4_
•
• 10/01/98 08:34:15
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Gas/BTEX by Purge&Trap GC
Project Sample ID/Description
0998HBWE01
TRIP BLANK
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sal!'ple ID Test Code(s) Batch H
9809494-0lA GASSWAGU NA
9809494-02A GASSWAGU NA
Work Order # 9809494
Page _s_
Analysis Batch u
GC!DA280927121101
GC!DA280927121101
•
10/01/98 08:34:15
Method TPH-Gasoline by SW8015B
Test Code GASSWAGU
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Gasoline
Unidentified organics
Surrogate(sl
Chlorobenzene
•
0998HBWE01
9809494-0lA
12092710
09/21/98
09/27/98 21:02:00
l
Water
ug/L
received
SECONDARY
Cone. DL
ND 10.6
5.23 B
Recovery
\
98
RBSULTS SUMMARY
TRIP BLANK
9809494-02A
12092712
09/21/98
09/27/98 22:51:00
l
Water
ug/L
received
SECONDARY
Cone. DL
ND 10.6
4.18 B
Recovery
\
95
•
Cone. DL
Recovery
\
Work Order tt 9809494
Page _6_
Cone. DL
Recovery
\
•
• 10/01/98 08:34:15
Method Gas/BTEX by Purqe&Trap GC
Test Code GASSWABG
Initial Calibration II IDA2980526070001
Calibration Date ~0=5~/=2=6~/=9=8 ____ _
Sequence/Analysis Time
l 09/27/98 12:11:00
2 09/27/98 13:05:00
3 09/27/98 14:00:00
4 09/27/98 14:55:00
5 09/27/98 15:49:00
6 09/27/98 17:09:00
7 09/27/98 18:19:00
8 09/27/98 19:13:00
9 09/27/98 20:07:00
10 09/27/98 21:02:00
11 09/27/')8 21:57:00
12 09/27/98 22:51:00
13 09/27/98 23:46:00
14 09/28/98 00:41:00
15 09/28/98 01:35:00
16 09/28/98 02:30:00
17 09/28/98 03:25:00
18 09/28/98 04 :20:00.
19 09/28/98 05:14:00
20 09/28/98 06:09:00
21 09/28/98 07:04:00
22 09/28/98 08:16:00
23 09/28/98 09:11:00
24 09/28/98 10:06:00
25 09/28/98 11:00:00
26 09/28/98 11:59:00
27 09/28/98 13:00:00
• AHALYSIS BATCH SUMMARY
Analysis Batch II GCIDA280927121101
Analysis Start Date/Time 09/27/98 12:11:00
Analysis Stop Date/Time 09/28/98 13:00:00
Work Order tt 9809494
Page _7_
Instrument ~
Analyst ~
Reviewer J~S~E~'---------
Project Sample ID Lab Sample ID Sample Type Analysis File II
CCV Continuing Calibration Verification 12092701
CCVG Continuing Calibration Verification I2092702
BLK983315 Blank, Method I2092703
LCS985054 Lab Control Sample I CCV 12092704
LCSG985055 Lab Control Sample I CCV I2092705
9809341-07B Sample 12092706
9809341-08B Sample 12092707
9809341-09B Sample 12092708
9809341-lOB Sample 12092709
0998HBWE01 9809494-0lA Sample 12092710
SB Sample 12092711
TRIP BLANK 9809494-02A Sample I2092712
9809455-06A Sample 12092713
9809455-02A Sample 12092714
9809455-03A Matrix Spike 12092715
9809455-04A Matrix ·spike Duplicate I2092716
SB Sample !2092717
9809455-0lA Sample 12092718
9809455-05A Sample 12092719
CCV Continuing Calibration Verification I2092720
CCVG Continuing Calibration Verification I2092721
9809341-09C Sample I2092722
9809341-lOC Sample I2092723
CCV Continuing Calibration Verification I2092724
CCVG Continuing Calibration Verification I2092725
CCVG Continuing Calibration Verification I2092726
CCVG Continuing Calibration Verification I2092727
•
10/01/98 08:34:15
Method Gas/BTEX by Purqe&Trap GC Specification# ;G~AS;;S~~
Lab Sample ID
File ID
•
Project Sample
ID/Description ·Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Convnent/N~rrative
•
Corrective Action
Work Order U 9809494
Page _8 _
•
• 09/25/98 15:11:17
Report Form
Work Order Summary
State Certifications
Flag Definitions
• RADIAN ANALYTICAL S~RVICBS
FPAS REPORT
TAB LB OF CONTENTS
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Analytical Batch ID
Protocol Summary for Percent moisture, SW846
Results Summary
Analysis Batch Summary EXMSRS80924163901
Comments/Narrative
-
Work Order H 98094~
Certified By ~~~if::I~:::::·:::....~~!!:'.:::;,;;;~!':"~,.--~
Date ~~~2--~'~l-·__._(Lj>~~~
Pages
From To
1 1
2 2
3 3
4 4
5 7
8 8
9 9
09/25/98 15:11:17
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared ·Radian International, LLC
By ---=1~4~0~4~6--=S~u~m~m~i~t-"D~r~·~·-"B~l~d~g~.-"B­
P. o. Box 201088
Austin TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWPOSB
•
ID/
NORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID VOLATILES
Case # .N.A.._ _______ _
SDG # ~NA~~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA MSRSSAOO
02A MSRSSAOO
03A MSRSSAOO
04A MSRSSAOO
05A MSRSSAOO
06A MSRSSAOO
07A MSRSSAOO
08A MSRSSAOO
09A MSRSSAOO
lOA MSRSSAOO
•
Percent
Percent
Percent
Percent
Percent
Percent
Percent
Percent
Percent
Percent
Work Order # 9809495
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
•
• 09/25/98 15:11:17
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATR CERTIFICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department· of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order ff 9809495
Page L
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
09/25/98 15:11:17 ANALYTICAL PROTOCOL SUMMARY
Flag
< DL
NA
NC
ND
NR
NS
A
B
c
FLAG DBFINITIONS
Definition
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence o.f hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit {and greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
p Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions {MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation .
• •
Work Order tt 9809495
Page _3_
•
• 09/25/98 15:11:17
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Percent moisture, SW846
Project Sample ID/Description
0998HBWF22A
0998HBWF22B
0998HBWF23A
0998HBWF23B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWP05B
ANALYTICAL
Lab Sample ID
9809495-03A
9809495-04A
9809495-02A
9809495-0lA
9809495-05A
9809495-0GA
9809495-07A
9809495-0SA
9809495-09A
9809495-lOA
• PROTOCOL SUMMARY
Extraction/Digestion
Test Code(sl Batch II
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
MSRSSAOO NA
Work Order # 9809495
Page _4_
Analysis Batch II
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
EXMSRS80924163901
•
09/25/98 15:11:17
Method Percent moisture, SW846
Test Code MSRSSAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Percent moisture
•
0998HBWF22A
9809495-03A
MSRS092416-3
09/21/98
09/24/98 16:39
l
Solid
%
Cone.
13.6
RHSULTS SUMMARY
0998HBWF22B
9809495-04A
MSRS092416-4
09/21/98
09/24/98 16:39
l
Solid
%
DL Cone. DL
17.0
•
0998HBWF23A
9809495-02A
MSRS092416-2
09/21/98
09/24/98 16:39
l
Solid
%
Cone. DL
16.3
Work Order # 9809495
Page _s_
0998HBWF238
9809495-0lA
MSRS092416-l
09/21/98
09/24/98 16:39
1
Solid
%
Cone.
19.l
DL
•
• 09/25/98 15:11:17
Method Percent moisture, SW846
Test Code MSRSSAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Percent moisture
0998HBWP01A
9809495-05A
MSRS092416-5
09/21/98
09/24/98 16:39
1
Solid
\
Cone. DL
17.4
• R B s u LT s ·s u MM AR y (Cont'd)
0998HBWP01B 0998HBWP03A
9809495-0GA 9809495-07A
MSRS092416-6 MSRS092416-7
09/21/98 09/21/98
09/24/98 16:39 09/24/98 16:39
1 1
Solid Solid
% %
Cone. DL Cone.
22.l 14 .1
DL
Work Order # 9809495
Page _6_
0998HBWP03B
9809495-08A
MSRS092416-8
09/21/98
09/24/98 16:39
1
Solid
%
Cone. DL
19.4
•
09/25/98 15:11:17
Method Percent moisture, SW846
Test Code MSRSSAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Percent moisture
•
0998HBWP05A
9809495-09A
MSRS092416-9
09/21/98
09/24/98 16:39
1
Solid
"'
Cone.
11. 9
RESULTS S 0 MM ARY (Cont'd)
0998HBWP058
9809495-lOA
MSRS092416-10
09/21/98
09/24/98 16:39
1
Solid
"'
DL Cone. DL
14.l
•
Cone. DL
Work Order # 9809495
Page _7_
Cone. DL
•
• 09/25/98 15:11:17
Method Percent moisture, SW846
Test Code MSRSSAOO
Initial Calibration # _N_A~~~~~~~~
Calibration Date ~N~A"--~~~~~~-
Sequence/Analysis Time
1 09/24/98 16:39
2 09/24/98 16:39
3 09/24/98 16:39
4 09/24/98 16:39
5 09/24/98 16:39
6 09/24/98 16:39
7 09/24/98 16:39
8 09/24/98 16:39
9 09/24/98 16:39
10 09/24/98 16:39
11 09/24/98 16:39
12 09/24/98 16:39
13 09/24/98 16:39
14 09/24/98 16:39
15 09/24/98 16:39
16 09/24/98 16:39
17 09/24/98 16:39:00
• ANALYSIS BATCH SUMMARY
·Analysis Batch # EXMSRS80924163901
Analysis Start Date/Time 09/24/98 16:39:00
Analysis Stop Date/Time 09/25/98 13:24:00
Project Sample ID Lab Sample ID Sample Type
0998HBWF23B 9809495-0lA Sample
0998HBWF23A 9809495-02A Sample
0998HBWF22A 9809495-03A Sample
0998HBWF22B 9809495-04A Sample
0998HBWP01A 9809495-0SA Sample
0998HBWP01B 9809495-06A Sample
0998HBWP03A 9809495-07A Sample
0998HBWP03B 9809495-08A Sample
0998HBWP05A 9809495-09A Sample
0998HBWP05B 9809495-lOA Sample
9809511-0lA Sample
9809511-02A Sample
9809511-03A Sample
9809511-04A Sample
9809511-05A Sample
9809511-06A Sample
9809511-07A Sample Duplicate
Work Order # 9809495
Page _8 _
Instrument ~
Analyst DNM
Reviewer
Analysis File U
MSRS092416-l
MSRS092416-2
MSRS092416-3
MSRS092416-4
MSRS092416-5
MSRS092416-6
MSRS092416-7
MSRS092416-8
MSRS092416-9
MSRS092416-10
MSRS092416-ll
MSRS092416-12
MSRS092416-13
MSRS092416-14
MSRS092416-15
MSRS092416-16
MSRS092416-17
•
09/25/98 15:11:17
Method Percent moisture, SW846
Lab Sample ID
File ID
•
Project Sample
ID/Description
Specification# MSRS D
Analyte
AHALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Comment/Narrative
•
Corrective Action
Work Order # 9809495
Page _9_
•
10/02/98 14:57:20
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HIL~ • .filL._-
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _.,R"'a"'d"'i"'a~n"-=I~n~t~e:.;rc.!;n~a~t~i,.::o~n!l:a!.!l:...1•.....:!:L~L!!:C:...
By --=1"'4"'0'-'4"'6'-"S"'u"'m"'m"'i"'t'-"D:::r'-'.-''-.!:B"'l,.::d!l:qL..:·-.!:B~
P. o. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
•
ID/
NOR~ ORDBR SUMMARY
Client Code HAM BEACH NC
Cl ".ent !.'AMILTON BEACH
Facility riASH!NGTON NC
Work ID VOLATILES
Case # ~N~A'--~~~~~~~~
SDG # ~NA:.:.-~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA 354SSAOO
827SSBCM
CKlSSAOO
02A 354SSAOO
827SSBCM
CKlSSAOO
03A 354SSAOO
827SSBCM
CKlSSAOO
04A 354SSAOO
827SSBCM
CKlSSAOO
OSA 354SSAOO
827SSBCM
CKlSSAOQ
06A 354SSAOO
827SSBCM
CKlSSAOO
07A 354SSAOO
827SSBCM
CKlSSAOO
OBA 354SSAOO
827SSBCM
•
Work Order # 9809496
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
•
• 10/02/98 14:57:20
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -~R~a._.d ... i ... a~n--=I'-"n""t'"'e""r"'n""a"'t""i"'o""n:.::a:.::l;.,,-=L:.::L:.::C:....
By --=l'-'4'-"0'-'4'-"6'-=S'-"u"'m"'m!:i'-"t'-"D:.:r;..:._,,__.B,_,l:.::d:::qt.:·'--':B<-
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWP03B
0998HBWP05A
0998HBWP05B
ID/
• W 0 R K 0 RD BR S UM MARY (Cont'd)
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID VOLATILES
Case# ""N"'A'----------
SDG # •N:.::A~~~~~~~~
RAS II 80903AJAL
Lab Sample ID Test Code(s)
OBA CKlSSAOO
09A 354SSAOO
827SSBCM
CKlSSAOO
lOA 354SSAOO
827SSBCM
CKlSSAOO
Work Order # 9809496
Page £._
RCN 65ill38. 0602
New York ELAP ID #: 10915
Method Desciption
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Soxhlet Extraction SW846
Semivolatiles by GC/MS
Primary KO cone. SW846
•
10/02/98 14:57:20
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATB CBRTIPICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9809496
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• 10/02/98 14:57:20 ANALYTICAL • PROTOCOL SUMMARY
F L A G D B F I N I T I 0 N S
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of _hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
8 Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero).
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match.that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M
p
Result modified from previous Report.
Analyte not confirmed. Results from
See Narrative for explanation.
primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere .
. S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order ff 9809496
Page _4_ •
10/02/98 14:57:20
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Semivolatiles by SW8270C
Project Sample ID/Description
0998HBWF22A
0998HBWF22B
0998HBWF22B
0998HBWF23A
0998HBWF23B
0998HBWF23B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWP05B
•
ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code (s) Batch II
9809496-03A 827SSBCM 3540980928110500
9809496-04A 827SSBCM 3540980928110500
9809496-04A 827SSBCM 3540980928110500
9809496-02A 827SSBCM 3540980928110500
9809496-0lA 827SSBCM 3540980928110500
9809496-0lA 827SSBCM 3540980928110500
9809496-0SA 827SSBCM 3540980928110500
9809496-06A 827SSBCM 3540980928110500
9809496-0?A 827SSBCM 3540980928110500
9809496-0BA 827SSBCM 3540980928110500
9809496-09A 827SSBCM 3540980928110500
9809496-lOA 827SSBCM 354 0980928110500
•
Work Order # 9809496
Page _5 _
Analysis Batch It
MSMSD280929132301
MSMSD180930103701
MSMSD280929132301
MSMSD280929132301
MSMSD180930103701
MSMSD280929132301
MSMSD280929132301
MSMSD280929132301
MSMSD280929132301
MSMSD280929132301
MSMSD280929132301
MSMSD280929132301
•
• 10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date P1epared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
Benz(a)anthracene
Benz(a)pyrene
Benzidine
Benzo(bJfluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol l 1-Chloroaniline
0998HBWF22A
9809496-03A
Y9390
09/21/98
09/28/98 11:05:00
09/29/98 22:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
0.0134
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.414 J
ND
ND
ND
ND
ND
ND
DL
0.0139
0.0126
0. 0114
0.0120
0.0797
0.0154
0.0141
0.0174
0.0127
O.Sl'5
0.0107
0.00908
0.0224
1.41
0.0268
0.0265
0.00789
0.00943
0.0218
0.0124
• RBSOLTS SUMMARY
0998HBWF22B
9809496-04A
Y9391
09/21/98
09/28/98 11:05:00
09/29/98 23:07
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND X
ND
ND X
ND X
ND X
0.0912 J
ND
ND
0.0867
ND
ND
ND
DL
0. 0145
0. 0131
0.0118
0.0125
0.0831
0.0160
0. 014 7
0.0182
0.0132
0.538
0.0112
0.00948
0.0233
1.47
0.0280
0. 0277
0.00823
0.00984
0.0228
0.0129
0998HBWF22B
9809496-04A
W8430
09/21/98
09/28/98 11:05:00
09/30/98 14: 26
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND X
ND
ND X
ND X
ND X
0.0803 J
ND
ND
0.0703
ND
ND
ND
DL
0.0248
0.0183
0.00952
0.0207
0.0446
0.0280
0.0202
0.0216
0.0333
1. 21
0.0281
0. 0271
0.0144
0.124
0. 0426
0.0406
0.0118
0.00703
0.0335
0.0104
Work Order # 9809496
Page _6_
0998HBWF23A
9809496-02A
Y9389
09/21/98
09/28/98 11:05:00
09/29/98 21:48
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.170 J
ND
ND
ND
ND
ND
ND
DL
.0.0143
0. 0130
0. 0117
0.0124
0.0822
0.0158
0. 0145
0.0179
0.0131
0.532
0.0110
0.00937
0.0231
1.45
0.0277
0.0274
0. 00814
0.00973
0.0225
0.0128
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
:late Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
bis{2-Chloroethoxy)methane
bis{2-Chloroethyl)ether
bis{2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Diallate
Dibenz{a,h}anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3°-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
•
0998HBWF22A
9809496-03A
Y9390
09/21/98
09/28/98 11:05:00
09/29/98 22:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0197
0.0150
0.0120
0.0145
0.0217
0.00612
0.0109
0.0188
0.00654
0.0120
0.0183
0.00947
0.00939
0.0172
0. 0118
0.0237
0.0129
0.0189
0.0132
0.0100
RB S ULT S SUMMARY (Cont'd)
0998HBWF22B
9809496-04A
Y939l
09/21/98
09/28/98 11:05:00
09/29/98 23:07
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND X
ND
ND X
ND
ND
ND
ND '
ND
ND
ND
ND
DL
0.0206
0.0157
0.0125
0.0151
0.0226
0.00638
0.0114
0.0196
0.00683
0.0125
0.0191
0.00988
0.00980
0.0179
0.0123
0.0247
0. 0135
0.0197
0. 0138
0.0104
•
0998HBWF22B
9809496-04A
W8430
09/21/98
09/28/98 11:05:00
09/30/98 14: 26
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
0. 020-0
ND X
ND
ND X
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0241
0.0237
0.0260
0.0151
0.0231
0.0300
0.0147
0.0250
0. 009'1-4
0.00498
0.0336
0.0164
0.0129
0.0159
0.0202
0.0208
0. 0134
0.0179
0.0158
0.0136
Work Order # 9809496
Page _7_
0998HBWF23A
9809496-02A
Y9389
09/21/98
09/28/98 11:05:00
09/29/98 21:48
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND·
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0203
0.0155
0.0124
0.0149
0. 0224
0.00631
0. 0112
0.0194
0. 0067-5---
0. 0124
0.0189
0.00977
0.00969
0.0177
0.0122
0.0245
0. 0133
0.0195
0.0137
0.0103
•
• 10/02/98 14:57:20
Method Semivolatiles by S~8270C
Test Code 827SSBCM .
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
p-Dimethylaminoazobenzene
7,12-Dimethylbenz(a)anthracene
3,3'-Dimethylbenzidine
Dimethylphenethylamine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
1,3-Dinitrobenzene
2,4-Dinitrophenol
2,4-Dinitr.otoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulfonate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
0998HBWF22A
9809496-03A
Y9390
09/21/98
09/28/98 11:05:00
09/29/98 22:27
1
Solid
ug/g
dry weight
Cone. DL
ND 0.0142
ND 0.0177
ND 0.0762
ND 0.785
ND 0. 0130
ND 0.0112
ND 1. 05
ND 0.0322
ND 1.21
ND 0.0171
ND 0. 0271
ND 0. 0142
ND 0.0150
0.0470 J 0.0470
ND 0.0139
ND 0.0131
ND 0.0143
ND 0.0196
ND 0.427
ND 0.0190
• R KS ULT S SUMMARY (Cont'd)
0998HBWF22B 099811BWF2:!B
9809496-04A 9809496-04A
Y9391 W8430
09/21/98 09/21/98
09/28/98 11:05:00 09/28/98 11:05:00
09/29/98 23:07 09/30/98 14:26
1 1
Solid Solid
ug/g ug/g
dry weight dry weight
Cone. DL Cone. DL
ND 0. 0148 ND 0.0243
ND x 0.0185 ND x 0.0655
ND 0.0795 ND 0.153
ND 0.819 ND 0.839
ND 0.0135 ND 0.0293
ND 0. 0117 ND 0.00803
ND 1.09 ND 0.0345
ND 0.0336 ND .o. 0450
ND 1.27 ND 1.15
ND 0.0179 ND 0.0269
ND 0.0283 ND 0.0349
ND 0. 014 8 ND 0.0178
ND 0.0157 ND 0.0538
0.184 0.0490 0 .248 0.0426
0. 0104 J 0.0145 ND 0.0241
ND 0.0137 ND 0.0312
ND 0.0149 ND 0.0331
ND 0.0205 ND 0.0214
ND 0.446 ND 0.0562
ND 0.0198 ND 0.0514
Work Order # 9809496
Page _8_
0998HBWF23A
9809496-02A
Y9389
09/21/98
09/28/98 11:05:00
09/29/98"21:48
1
Solid
ug/g
dry weight
Cone. DL
ND 0.0146
ND 0.0183
ND 0.0786
ND 0.810
ND 0.0134
ND 0. 0116
ND 1. 08
ND 0.0332
ND 1.25
ND 0.0177
ND 0.0280
ND 0.0146
ND 0.0155
0.103 0. 0484
ND 0.0143
ND 0.0135
ND 0.0147
ND 0.0202
ND 0.441
ND 0.0196
•
...
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Indeno(l,2,3-cd)pyrene
Isophorone
Isosafrole
Kepone
Methapyrilene
Methyl met:hanesulfonat:e
3-Met:hylcholant:hrene
2-Methylnaphthalene
4-Met:hylphenol/3-Met:hylphenol
2-Methylphenol
N-Nit:roso-di-n-butylamine
N-Nit:roso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
~-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
•
0998HBWF22A
9809496-03A
Y9390
09/21/98
09/28/98 11:05:00
09/29/98 22:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.472 F
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0217
0.00843
0.00824
0.0416
0. 724
0.797
0.0154
0.0450
0. 0138
0.0182
0.0216
0.0144
0.0108
0.0327
0.0134
0.0306
0. 0346
0.0281
0.0458
0.0172
RESULTS SUMMARY (Cont'd)
0998HBWF22B
9809496-04A
Y9391
09/21/98
09/28/98 11:05:00
09/29/98 23:07
1
Solid
ug/g
dry weight
Cone.
ND
ND X
ND
ND
ND
ND
ND
ND X
0.0739
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0992
DL
0.0227
0.00880
0.00859
0.0434
0.755
0.831
0.0161
0.0470
0.0144
0.0190
0.0225
0.0150
0. 0113
0.0341
0.0140
0.0320
0.0361
0.0293
0.0478
0.0180
•
0998HBWF22B
9809496-04A
W8430
09/21/98
09/28/98 11:05:00
09/30/98 14:26
1
Solid
ug/g
dry weight
Cone.
ND
ND X
ND
ND
ND
ND
ND
ND X
0.0699
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0960
DL
0.0347
0. 0311
0.0199
0.0384
0.647
0.896
0.0202
0.0209
0.0194
0.0239
0. 0204
0.0316
0.0381
0.0426
0.0356
0.0590
0.0250
0.0330
0.0450
0.0202
Work Order # 9809496
Page _9_
0998HBWF23A
9809496-02A
Y9389
09/21/98
09/28/98 11:05r00
09/29/98 21:48
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.324 F
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0224
0.00870
o.ooa5o
0.0429
0.746
0.822
0.0159
0.0465
0. Oi-43
0.0188
0.0223
0.0148
0. 0112
0.0337
0. 0138
0.0316
0.0357
0.0289
0. 0472
0.0177
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM .
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
sym-Trinitrobenzene
•
0998HBWF22A
9809496-03A
Y9390
09/21/98
09/28/98 11:05:00
09/29/98 22:27
l
Solid
ug/g
dry weight
Cone. DL
ND 0.0191
ND 0.0393
ND 0.0274
ND 0.0210
ND 0.0275
ND 0.0152
ND 0. 0136
ND o. 0206
ND 0.0243
ND 0.048l.
R B S 0 LT S S 0 MM A R Y (Cont'd)
0998HBWF22B 0998HBWF22B
9809496-04A 9809496-04A
Y9391 W8430
09/21/98 09/21/98
09/28/98 11:05:00 09/28/98 11:05:00
09/29/98 23:07 09/30/98 14:26
l l
Solid Solid
ug/g ug/g
dry weight dry weight
Cone. DL Cone. DL
0.0249 0.0199 ND 0.015l.
ND 0.0410 ND 0.0318
ND 0.0286 ND 0.0283
ND 0.0219 ND 0.0204
ND 0.0287 ND 0. 0406
ND O.Ol.59 ND 0.0236
ND 0.0142 ND 0. 0170
ND 0.0215 ND 0.0256
ND 0.0253 ND 0. 0241
ND 0.0502 ND 0. 0271
•
Work Order # 9809496
Page .u_
0998HBWF23A
9809496-02A
Y9389
09/21/98
09/28/98 11:05:00
09/29/98 21:48
l
Solid
ug/g
dry weight
Cone. DL
ND 0.0197
ND 0. 04 05
ND 0.0282
ND 0.0217
ND 0.0283
ND 0.0157
ND 0. 0140
ND 0.0213
ND. 0.0251.
ND 0. 0496
•
• 10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribromophenol
0998HBWF22A
9809496-03A
Y9390
09/21/98
09/28/98 11:05:00
09/29/98 22:27
1
Solid
ug/g
dry weight
Cone.
Recovery
\
93
94
95
109
90
97
DL
• R B s u LT s s u MM AR y (cont'd)
0998HBWF22B
9809496-04A
Y9391
09/21/98
09/28/98 11:05:00
09/29/98 23:07
l
Solid
ug/g
dry weight
Cone.
Recovery
\
94
92
95
106
109
96
DL
0998HBWF22B
9809496-04A
W8430
09/21/98
09/28/98 11:05:00
09/30/98 14:26
l
Solid
ug/g
dry weight
Cone.
Recovery
\
94
88
92
90
108
88
DL
Work Order # 9809496
Page g_
0998HBWF23A
9809496-02A
Y9389
09/21/98
09/28/98 11:05:00
09/29/98 21:48
l
Solid
ug/g
dry weight
Cone.
Recovery ..
96
91
94
109
92
100
DL
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
Benz(a)anthracene
· l3ehz (al pyrene
Benzi dine
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol
p-Chloroaniline
•
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND X
ND
ND X
ND X
ND X
ND
ND
ND
0.194
ND
ND
ND
DL
0.0148
0.0134
0.0121
0.0128
0.0851
0.0164
0.0150
0.0186
0.0135
0.551
0.0114
0.00970
0.0239
1.50
0.0287
0.0283
0.00843
0.0101
0.0233
0.0132
RESULTS S UM MAR Y (Cont'd)
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.156
ND
ND
ND
DL
0.0254
0.0187
0.00974
0.0212
0. 0456
0.0286
0.0207
0. 0221
0.0341
1.24
0.0288
0.0278
0.0148
0.127
0.0436
0.0415
0.0121
0. 00720
0.0343
0.0106
•
0998HBWP01A
9809496-0SA
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0. 0214
ND
ND
ND
DL
0.0145
0.0132
0. 0119
0.0126
0.0833
0.0161
0.0147
0.0182
0. 013.'.?
0.539
o. 0112
0.00950
0.0234
1.47
0.0281
0. 0277
0.00825
0.00986
0.0228
0. 0130
Work Order # 3809496
Page !l_
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0154
0.0140
0.0126
0.0133
0.0885
0.0171
0.0157
0.0193
0. 0141
0.573
0. 0119
O.OlOl
0. 0249
1.57
0.0298
0.0295
0.00877
0.0105
0.0243
0. 0138
•
• 10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
I liethylphthalate
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
0. 0572
ND
ND X
ND
ND X
ND
ND
ND
ND
ND
ND
ND
ND
DL
0. 0211
0.0161
0.0128
0.0155
0.0232
0.00654
0. 0116
0.0201
0.00699
0.0128
0.0195
0.0101
0.0100
0.0183
0.0126
0.0253
0.0138
0.0201
0.0141
0.0107
• RB SULT S SUMMAR Y (Cont'd)
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0246
0.0243
0.0266
0.0155
0.0236
0.0307
0.0151
0.0256
0.00966
0.00510
0.0344
0.0168
0.0132
0.0162
0.0207
0.0213
0.0137
0.0183
0.0162
0.0139
0998HBWP01A
9809496-05A
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0206
0.0157
0.0126
0.0151
0.0227
0.00640
0. 0114
0.0196
0.00684
0.0126
0.0191
0.00990
0.00982
0.0180
0.0124
0.0248
0.0135
0.0197
0.0138
0.0105
Work Order # 9809496
Page .!i_
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0219
0.0167
0.0133
0.0161
0.0241
0.00680
0.0121
0.0209
0. 00727
0.0133
0.0203
0.0105
0.0104
0.0191
0.0131
0.0263
0.0143
0.0210
0.0147
0. 0111
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
•late Analyzed:
Jilution Factor:
Matrix:
Units:
Report as:
Column:
A,nalyte
p-Dimethylaminoazobenzene
7,12-Dimethylbenz(a)anthracene
3,3'-Dimethylbenzidine
Dimethylphenethylamine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
1,3-Dinitrobenzene
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulf onate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
•
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
ND
ND X
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.170
ND
ND
ND
ND
ND
ND
DL
0.0151
0.0190
0. 0814
0.839
0.0139
0.0120
1.12
0.0344
1.30
0.0183
0.0289
0.0151
0.0161
0.0502
0. 0148
0.0140
0.0153
0.0210
0.456
0.0203
R B S ULT S S UM M A R Y (Cont'd)
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.217
ND
ND
ND
ND
ND
ND
DL
0.0249
0.0670
0.157
0.859
0.0300
0.00822
0.0354
0.0461
l.1:8
0. 0275
0.0358
0.0182
0.0551
0.0436
0. 0247
0.0320
0.0339
0.0219
0.0576
0.0526
•
0998HBWP01A
9809496-05A
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0612
ND
ND
ND
ND
ND
ND
DL
0.0148
0.0186
0.0797
0.821
0.0136
0.0117
1.09
0.0337
1.27
0.0179
0.0283
0.0148
0.0157
0. 0491
0.0145
0.0137
0.0149
0.0205
0.447
0.0199
Work Order H 9809496
Page l,L
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0217 J
ND
ND
ND
ND
ND
ND
DL
0.0157
0.0197
0.0847
0.873
0.0144
0.0124
1.16
0.0358
1.35
0.0190
0.0301
0.0157
0.0167
0.0522
0.0154
0. 0145
0.0159
0.0218
0.475
0. 0211
•
• 10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Indeno(l,2,3-cd)pyrene
Isophorone
Isosaf role
Kepone
Methapyrilene
Methyl methanesulfonate
3-Methylcholanthrene
2-Methylnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
ND
ND X
ND
ND
ND
ND
ND
ND X
0.0327
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0247
DL
0.0232
0.00900
0.00880
0.0444
0.773
0.851
0.0165
0.0481
0.0148
0.0195
0.0231
0.0154
0.0116
0.0350
0.0143
0.0327
0.0370
0.0300
0.0489
0.0184
• R E SULT S SUMMARY (Cont'd)
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
0.0301
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0229
DL
0.0356
0.0319
0.0204
0.0393
0.662
0.917
0.0206
0.0214
0.0199
0.0245
0.0209
0.0324
0.0390
0.0436
0.0364
0.0604
0.0256
0.0338
0.0461
0.0207
0998HBWP01A
9809496-05A
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0227
0.00881
0.00861
0.0435
0.757
0.833
0.0161
0. 0471
0. 0144
0.0191
0.0226
0.0151
0.0113
0.0342
0.0140
0.0320
0.0362
0.0293
0. 04 79
0:0180
Work Order # 9809496
Page ,!§._
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0242
0.00937
0.00915
0.0462
0.804
0.885
0.0172
0.0500
0.0154
0.0203
0. 0240
0.0160
0.0120
0.0364
0.0149
0.0340
0.0385
0.0312
0.0509
0.0191
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,4-Naphthoquinone
1-Naphthylamine
2-Naphthylamine
5-Nitro-o-toluidine
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2~Nitrophenol-
4 -Nitrophenol
4-Nitroquinoline-l-oxide
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
i'henol
2-Picoline
Pronamide
•
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0273
ND
ND
ND
DL
0. 0411
0.0724
0.0641
0.0149
0.0147
0.0362
0.0319
0.0366
0.0226
l.26
0.925
0.0277
0.0296
0.0551
l.18
0.00921
0.0251
0.0103
0.0436
0.0106
RESULTS S 0 M M A R Y (Cont 1d)
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
l
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0364
ND
ND
ND
DL
0.0428
0.0448
l. 08
0.0399
0.0352
0.0403
0.0377
0.0208
0.017"1
0.864
0.831
0.0401
0.0625
0.0715
0.975
0.0380
0.0244
0.0149
0.0363
0.0127
•
0998HBWPOlA
9809496-05A
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ti°D
ND
ND
ND
ND
ND
ND
ND
DL
0.0402
0.0708
0.0628
0. 0146
0.0144
0.0355
0.0312
0.0359
0. 02r6
1.24
0.906
0. 0271
0.0290
0.0539
1.16
0.00902
0.0246
0.0101
0.0427
0.0103
Work Order U 9809496
Page 12-
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
NO-
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0428
0.0753
0.0667
0.0155
0.0153
0.0377
0.0332
0.0381
0.-02-29
l.31
0.962
0.0288
0.0308
0.0573
l.23
0.00958
0.0261
0.0107
0.0453
0.0110
•
I
• 10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
sym-Trinitrobenzene
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0. 0204
0.0419
0.0292
0.0225
0.0294
• 0.0163
0.0145
0.0220
0. 0259
0.0514
• R B S U L T S S U M MAR Y (Cont'd)
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0154
0.0325
0.0290
0.0209
0. 0415
0.0241
0.0174
0.0262
0.0247
0.0277
0998HBWP01A
9809496-05A
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0200
0. 0411
0.0286
0.0220
0.0287
0.0159
0.0142
0.0216
0.0254
0.0503
Work Order U 9809496
Page lL
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0212
0. 0436
0.0304
0.0234
0.0305
0.0169
0.0151
0.0229
0.0270
0.0535
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
N:Ctrobenzene-d5
Phenol-d5
Terphenyl-d14
2,4,?-Tribromophenol
•
0998HBWF23B
9809496-0lA
Y9388
09/21/98
09/28/98 11:05:00
09/29/98 21:08
1
Solid
ug/g
dry weight
Cone.
Recovery
't
94
94
94
105
104
92
DL
R B S U LT S S UM MA R Y (Cont'd}
0998HBWF23B
9809496-0lA
W8429
09/21/98
09/28/98 11:05:00
09/30/98 13:46
1
Solid
ug/g
dry weight
Cone.
Recovery
't
95
90
90
89
104
93
•
DL
0998HBWP01A
9809496-05A
Y9392
09/21/98
09/28/98 11:05:00
09/29/98 23:47
1
Solid
ug/g
dry weight
Cone.
Recovery
\
96
89
89
106
96
103
DL
work Order # 9809496
Page 1.2_
-
0998HBWP01B
9809496-06A
Y9393
09/21/98
09/28/98 11:05:00
09/30/98 00:27
1
Solid
ug/g
dry weight
Cone.
Recovery
\
93
87
89
100
88
94
DL
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
bi-n-butylphthaiate
Di-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3 1-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
•
0998HBWP03A
9809496-07A
Y9394
09/21/98
09/28/98 11:05:00
09/30/98 01:06
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0198
0.0151
0.0121
0.0146
0.0218
0.00616
0. 0110
0.0189
0. 0"0658
0.0121
0.0184
0.00953
0.00945
0.0173
0. 0119
0.0239
0.0130
0.0190
0.0133
0.0101
R B S 0 LT S S 0 M M A R Y (Cont'd)
0998HBWP03B
9809496-0BA
Y9395
09/21/98
09/28/98 11:05:00
09/30/98 01:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0. 0211
0.0161
0.0129
0.0155
0.0233
0.00656
0. 0117
0.0201
0.00701
0.0129
0.0196
0.0101
0.0101
0.0184
0.0127
0.0254
0. 0138
0.0202
0.0142
0.0107
•
0998HBWP05A
9809496-09A
Y9396
09/21/98
09/28/98 11:05:00
09/30/98 02:26
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
0.0141 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0193
0.0147
0. 0118
0.0142
0.0213
0.00600
0.0107
0.0184
0.00641
0.0118
0.0179
0.00928
0. 00920
0.0168
0. 0116
0.0232
0.0126
0.0185
0. 0130
0.00981
Work Order # 9809496
Page ~
0998HBWP05B
9809496-lOA
Y9397
09/21/98
09/28/98 11:05:00
09/30/98 03:06
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0198
0.0152
0.0121
0.0146
0.0219
0.00616
o. 0110
0.0189
0. 00659
0.0121
0.0184
0.00954
0.00946
0. 0173
0.0119
0.0239
0.0130
0.0190
0.0133
0.0101
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
, )ate Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Indeno(l,2,3-cd)pyrene
Isophorone
Isosafrole
Ke pone
Methapyrilene
Methyl methanesulfonate
3-Methylcholanthrene
~-Methytnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
•
0998HBWP03A
9809496-07A
Y9394
09/21/98
09/28/98 11:05:00
09/30/98 01:06
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
·ND
ND
ND
DL
0.0219
0.00848
0.00829
0.0418
0.728
0.802
0.0155
0.0453
-0.0139
0.0184
0.0217
0.0145
0.0109
0.0329
0. 0135
0.0308
0.0348
0.0282
0. 0461
0.0173
RBSULTS S U M M A R Y (Cont'd)
0998HBWP03B
98094 96-08A
Y9395
09/21/98
09/28/98 11:05:00
09/30/98 01:46
l
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0233
0.00904
0.00883
0.0446
0.776
0.854
0.0165
0. 0483
0.0148
0.0196
0.0231
0.0154
0. 0116
0.0351
0.0144
0.0328
0.0371
0.0301
0.0491
0.0184
•
0998HBWP05A
9809496-09A
Y9396
09/21/98
09/28/98 11:05:00
09/30/98 02:26
l
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0213
0.00826
0.00807
0.0407
0.709
0.781
0.0151
0. 0441
0. 01.35
0.0179
0.0212
0. 0141
0.0106
0.0321
0. 0131
0.0300
0.0339
0.0275
0. 0449
0.0169
Work Order # 9809496
Page 3.L_
0998HBWP05B
9809496-lOA
Y9397
09/21/98
09/28/98 11:05:00
09/30/98 03:06
l
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0219
o .. 0084 9
0.00830
0.0419
0. 729
0.802
0.0155
0.0454
---0. 013-9-
0. 01&4
0.0217
0.0145
0.0109
0.0330
0.0135
0.0309
0.0348
0,0283
0.0461
0.0173
•
10/02/9~7:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,4-Naphthoquinone
1-Naphthylamine
2-Naphthylamine
5-Nitro-o-toluidine
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-1-oxide
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
2-Picoline
Pronamide
0998HBWP03A
9809496-07A
Y9394
09/21/98
09/28/98 11:05:00
09/30/98 01:06
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0387
0.0682
0.0604
0.0141
0.0139
0. 0341
0.0300
0.0345
0.0208
1.19
0.871
0.0261
0.0279
0.0519
1.12
0.00867
0.0236
0.00968
0.0410
0.00995
RESULTS S.ARY
0998HBWP03B
9809496-08A
Y9395
09/21/98
09/28/98 11:05:00
09/30/98 01:46
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0413
0.0726
0.0644
0.0150
0.0148
0.0364
0.0320
0.0368
0.0221
1.27
0.928
0.0278
0.0297
0.0553
1.19
0.00924
0.0252
0.0103
0.0437
0.0106
(Cont'd)
0998HBWP05A
9809496-09A
Y9396
09/21/98
09/28/98 11:05:00
09/30/98 02:26
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0377
0.0664
0.0588
0.0137
0. 0135
0.0332
0.0292
0.0336
0.0202
1.16
0. 849
0.0254
0.0272
0.0505
1.09
0.00845
0.0230
0.00943
0. 0400
0.00969
Work Order # 9809496
Page £1.._
0998HBWP05B
9809496-lOA
Y9397
09/21/98
09/28/98 11:05:00
09/30/98 03: 06
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0388
0.0682
0.0605
0.0141
0.0139
0.0342
0.0300
0.0345
0.0208
1.19
0.872
0.0261
0.0280
0.0519
1.12
0.00868
0.0236
0.00969
0. 0411
0.00996
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetraehlorophenol
o-Toluidine
1,2,4-Triehlorobenzene
2,4,5-Triehlorophenol
2,4,6-Triehlorophenol
sym-Trinitrobenzene
•
0998HBWP03A
9809496-07A
Y9394
09/21/98
09/28/98 11:05:00
09/30/98 01:06
--
1
Solid
ug/g
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND - -
ND
ND
DL
0.0192
0,0395
0.0275
0. 0211
0. 0277
0.0153
0.0137
0.0208
0.0244
0.0484
R BS ULT S SUMMARY (Cont'd)
0998HBWP03B 0998HBWP05A
9809496-08A 9809496-09A
Y9395 Y9396
09/21/98 09/21/98
09/28/98 11:05:00 09/28/98 11:05:00
09/30/98 01:46 09/30/98 02:26
1 l
Solid Solid
ug/g ug/g
dry weight dry weight
Cone. DL Cone. DL
ND 0.0205 0.00834 J 0.0187
ND 0.0421 ND 0.0385
ND 0.0293 ND 0.0268
ND 0.0225 ND 0.0206
ND 0.0295 ND 0.0269
ND 0.0163 ND 0. 0149
ND 0.0146 ND 0.0133
ND 0.0221 ND 0.0202
-
ND 0.0260 ND 0.0238
ND 0.0516 ND 0. 0472
•
Work Order # 9809496
Page lL
0998HBWP05B
9809496-lOA
Y9397
09/21/98
09/28/98 11:05:00
09/30/98 03:06
l
Solid
ug/g
dry weight
Cone. DL
ND 0. 0192
ND 0.0395
ND 0.0276
ND 0.0212
ND 0.0277
ND 0.0154
ND 0.0137
ND 0.0208
-ND 0.0245
ND 0.0485
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SWBOO
Initial Calibration # MSD1980917083000
Calibration Date ~0~9~/~1~7~/~9~8'--~~~-
Sequence/Analysis Time
1 09/30/98 10:37
2 09/30/98 10:59
3 09/30/98 11 :47
4 09/30/98 12:26
5 09/30/98 13:06
6 09/30/98 13:46
7 09/30/98 14:26
ANALYSIS BATCH SUMMARY
Analysis Batch II MSMSD180930103701
Analysis Start Date/Time 09/30/98 10:37:00
Analysis Stop Date/Time 09/30/98 14:26:00
Project Sample ID Lab Sample ID Sample Type
TUNE GC/MS tune
SSTD050 Continuing
LCS984996 Lab Control
LCSD984996 Lab Control
files
Work Order # 9809496
Page 'D_
Instrument !1fil2!.__..
Analyst ~
Reviewer ~KM~G"--~~~~~-
Analysis File II
W8424
Calibration Verification W8425
Sample W8426
Sample Duplicate W8427
BLK983280 Blank, Method W8428
0998HBWF23B 9809496-0lA Sample W8429
0998HBWF22B 9809496-04A Sample W8430
·-----
••
--
•
• 10/02/98 14:57:20
Method Semivolatiles by SW8270C
Test Code 827SWBOO
Initial Calibration # MSD2980821083300
Calibration Date ~08~/~2~1~/~9~8'--~~~-
Sequence/Analysis Time
1 09/29/98 13:23
2 09/29/98 13:44
3 09/29/98 14:26
4 09/29/98 15:06
5 09/29/98 15:45
6 09/29/98 16:25
7 09/29/98 17:05
8 09/29/98 17:44
9 09/29/98 18:24
10 09/29/98 19:28
11 09/29/98 19 :49
12 09/29/98 20:28
13 09/29/98 21:08
14 09/29/98 21 :48
15 09/29/98 22:27
16 09/29/98 23:07
17 09/29/98 23:47
18 09/30/98 00:27
19 09/30/98 01:06
20 09/30/98 01:46
21 09/30/98 02:26
22 09/30/98 03:06
23 09/30/98 03 :46
24 09/30/98 04:25
25 09/30/98 05:05
26 09/30/98 05:45
27 09/30/98 06:25
28 09/30/98 07:05
29 09/30/98 07:45
• ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSD28092913230l
Analysis Start Date/Time 09/29/98 13:23:00
Analysis Stop Date/Time 09/30/98 07:45:00
Work Order # 9809496
Page~
Instrument ~
Analyst §ms
Reviewer ~KM~G~~~~~~~~-
Project Sample ID Lab Sample ID Sample Type Analysis File #
TUNE GC/MS tune files Y9376
SSTD050 Continuing Calibration Verification Y9377
LCS984996 Lab Control Sample Y9378
LCSD984996 Lab Control Sample Duplicate Y9379
BLK983280 Blank, Method Y9380
9809512-06A Sample Y9381
9809512-07A Matrix Spike Y9382
9809512-08A Matrix Spike Duplicate Y9383
9809512-04A Sample Y9384
TUNE GC/MS tune files Y9385
SSTD050 Continuing Calibration Verification Y9386
9809512-05A Sample Y9387
0998HBWF23B 9809496-0lA Sample Y9388
0998HBWF23A 9809496-02A Sample Y9389
0998HBWF22A 9809496-03A Sample Y9390
0998HBWF22B 9809496-04A Sample Y9391
0998HBWP01A 9809496-05A Sample Y9392
0998HBWP01B 9809496-06A Sample Y9393
0998HBWP03A 9809496-07A Sample Y9394
0998HBWP03B 9809496-08A Sample Y9395
0998HBWP05A 9809496-09A Sample Y9396
0998HBWP05B 9809496-lOA Sample Y9397
9809,UO-OlA Sample Y9398
9809410-02A Sample Y9399
9809410-05A Matrix Spike Y9400
9809410-06A Matrix Spike Duplicate Y9401
9809410-03A Sample Y9402
9809410-04A Sample Y9403
DCS984997 Detectability Check Sample Y9404
•
10/02/98 14:57:20
Method Semivolatiles by SW8270C
Lab Sample ID
File ID
9809496-0lA
Y9388
9809496-02A
Y9389
9809496-03A
Y9390
9809496-04A
Y9391
9809496-0?A
Y9394
•
Project Sample
ID/Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP03A
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Specification# ~8~2~7~S~~
Analyte
Perylene-dl2
4-Methylphenol/3-Methylphenol
4-Methylphenol/3-Methylphenol
Perylene-d12
Benzo(b)/Benzo(k)fluoranthene
Flag Comment/Narrative
X The area counts for perylene-dl2 were low.
F
F
x
Probable cause is matrix effect. The X flag
indicates which analytes are quantitated with
this internal standard and that
concentrations may be biased high.
The F flag indicates that 3-methylphenol
coelutes with 4-methylphenol. The calibration
response factor is based on 4-methylphenol
only. Any identification for 4-methylphenol
should be regarded as a possible sum of the
two indistinguishable isomers.
The F flag indicates that 3-methylphenol
coelutes with 4-methylphenol. The calibration
response factor is based on 4-methylphenol
only. Any identification for 4-methylphenol
should be regarded as a possible sum of the
two indistinguishable isomers.
The area counts for perylene-d12 were low.
Probable cause is matrix effect. The X flag
indicates which analytes are quantitated with
this internal standard and that
concentrations may be biased high".
F · The F flag indicates that benzo(b) and
benzo(k)fluoranthene are not resolved in
this sample. The unresolved peak is
integrated twice and a result is calculated
with each response factor .
•
Work Order U 9809496
Page 3.2_
Corrective Action
The sample will be reanalyzed.
The sample will be reanalyzed.
The reported numbers represent the average of
the two results and the average is reported
for each analyte.
•
10/02/98 14:~
Method Semivolatiles by SW8270C
Lab Sample ID
File ID
9809496-04A
W8430
Project Sample
ID/Description
0998HBWF22B
Specificationn B27S
Analyte
Perylene-d12
ANALYTICAL
COMMBHTS
P·~OCOL
/HARRATIV
Flag Comment/Narrative
SUMMARY
B (Cont'd)
X The area counts for perylene-dl2 were low.
Probable cause is matrix effect. The X flag
indicates which analytes are quantitated with
this internal standard and that
concentrations may be biased high.
Work Order
Corrective Action
Samples were previously analyzed with
similar results.
Page lQ._
10/02/98 14:57:20
•
QUALITY COllTROL RXCRPTIOll RRPORT
SUMMARY
QCER ff Analysis Batch Number
980929-11 MSD2980929132300
- -
•·
Work Order ff 9809496
Page l.L
•
10/05/98 16:48:59
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -~R=a=d=i=a~n:.....:I~n~t~e=r~n~a~t=i"'o~n~a"'l~·-=L~L~C:....
By ---"'l-"4-"0-=4-"6---"S""u"'m:;:.m.,,i'""t'-"D"'r-'.-''--"B"'l"'d"'qL.:.--"B:....
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
•
ID/
--
WOR~ ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID VOLATILES
Case # _N_A~-------­
SDG # ~NA:..:...~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA 355SSAOO
CKlSSAOO
DSLSSAEL
02A 355SSAOO
CKlSSAOO
DSLSSAEL
03A 355SSAOO
CKlSSAOO
DSLSSAEL
04A 355SSAOO
CKlSSAOO
DSLSSAEL
05A 355SSAOO
CKlSSAOO
DSLSSAEL
06A ' 355SSAOO
CKlSSAOO
DSLSSAEL
OTA 355SSAOO
CKlSSAOO
DSLSSAEL
OBA 355SSAOO
CKlSSAOO
••
Work Order tt 9809497
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Sonication Extract SW846
Primary KD cone. SW846
TPH Extractables
Sonication Extract SW846
Primary KD cone. SW846
TPH Extractables
Soni cation Extract SW846
Primary KD cone. SW846
---
TPH Extractables
Sonication Extract SW846
Primary KD cone. SW846
TPH Extractables
Sonication Extract SW846
Primary KD cone. SW846
TPH Extractables
Sonication Extract SW846
Primary KD cone. SW846
TPH Extractables
Soni cation Extract SW846
Primary KD cone. SW846
TPH Extractables
Sonication Extract SW846
Primary KD cone . SW846
•
•• 10/05/98 16:48:59
Report RADIAN INTERNATI~O~N~A~L"'---~
'1'0 3200 E. CHAPEL illLL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared --"R~a=d~i=a-n--=I-n=t=e~r~n=a=t~i=o~n=a~l~·-=L~L~C._
By ---=1~4~0~4~6_,,S~u~m~m~i=t~D~r~·~·-=B~l=d~g~._.B~
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWP03B
0998HBWP05A
0998HBWP05B
ID/
• if 0 R K 0 R D B R S UH H AR Y (Cont'd)
Client Code HAM BEACH NC
Client HAMXilfC:.:..·N,_,,B"'E::.A:;,C::;H:._ ______ _
Facility WASHINGTON,NC
Work ID VOLATILES
Case # ~N•A"--------­
SOG # ~N~A~~~~~~~~
RAS # 80903!\JAL
Work Order # 9809497
Page L
RCN 650138.0602
New York ELAP ID #: 10915
Lab Sample ID Test Code(s) Method Desciption
OBA DSLSSAEL TPH Extractables
09A 355SSAOO Sonication Extract SW846
CKlSSAOO Primary KD cone. SW846
DSLSSAEL TPH Extractables
lOA 355SSAOO Sonication Extract SW846
CKlSSAOO Primary KD cone. SW846
DSLSSAEL TPH Extractables
•
10/05/98 16:48:59
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATB CERTIFICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9809497
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• 10/05/98 16:48:59
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method TPH-Diesel by mod. SW8015
Project Sample ID/Description
0998HBWF22A
0998HBWF22B
0998HBWF23A
0998HBWF23B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWP05B
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch jj
9809497-03A DSLSSAEL 3550980924103000
9809497-04A DSLSSAEL 3550980924103000
9809497-02A DSLSSAEL 3550980924103000
9809497-0lA DSLSSAEL 3550980924103000
9809497-05A DSLSSAEL 3550980924103000
9809497-0GA DSLSSAEL 3550980924103000
9809497-07A DSLSSAEL 3550980924103000
9809497-08A DSLSSAEL 3550980924103000
9809497-09A DSLSSAEL 3550980924103000
9809497-lOA DSLSSAEL 3550980924103000
Work Order II 9809497
Page _5_
Analysis Batch II
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
TPGC1381002120001
•
10/05/98 16:48:59 ANALYTICAL PROTOCOL SUMMARY
FLAG DBFIHITIOHS
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K
M
p
Peak did not meet method identification criteria. Analyte not detected on other GC column.
Result modified from previous Report.
Analyte not confirmed. Results from
See Narrative for explanation.
primary and secondary GC columns differ by greater than a factor of 3·.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
•
Work Order ff 9809497
Page _4_
•
10/05/98 16:48:59
Method TPH-Diesel by mod. SW8015
Test Code DSLSSAEL .
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Diesel
Jet fuel JP4
Kerosene
Unidentified organics
Surrogate(s)
Octacosane
•
RESULTS SUMMARY
0998HBWF22A 0998HBWF22B
9809497-03A 9809497-04A
V8J02036 V8J02049
09/21/98 09/21/98
09/24/98 09/24/98
10/04/98 16:20:00 10/05/98 02:26:00
1.0000 50.0000
Solid Solid
ug/g ug/g
dry weight dry weight
Cone. DL Cone. DL
ND 0.980 1820 BX 51. 0
ND 3.30 ND 172
ND 2.96 ND 154
12.8 BDA ND
Recovery Recovery
\ --%
127 2420 Q
•
0998HBWF23A
9809497-02A
V8J02035
09/21/98
09/24/98
10/04/98 15:10:00
1. 0000
Solid
ug/g
dry weight
Cone. DL
ND 1. 01
ND 3.41
ND 3.Q6
5.37 BDA
Recovery
\
123
Work Order ff 9809497
Page _6 _
0998HBWF23B
9809497-0lA
V8J02048
09/21/98
09/24/98
10/05/98 01:39:00
50.0000
Solid
ug/g
dry weight
Cone. DL
1730 BX 52.5
ND 177
ND 159
ND
Recovery
-%
2120 Q
•
• 10/0S/98 16:48:59
Method TPH-Diesel by mod. SW8015
Test Code DSLSWAEL
Initial Calibration # GC13981002120000
Calibration Date ~l~0~/~0~2~/~9~8'------
Sequence/Analysis Time
1 10/02/98 15:50:00
2 10/02/98 16:38:00
3 10/03/98 14:22:00
4 10/03/98 15:09:00
5 10/03/98 15:56:00
6 10/03/98 16:42:00
7 10/03/98 17:29:00
8 10/03/98 18:15:00
9 10/03/98 19:02:00
10 10/03/98 19:48:00
11 10/03/98 20:35:00
12 10/03/98 21:21:00
13 10/03/98 22:08:00
14 10/03/98 22:54:00
15 10/03/98 23:41:00
16 10/04/98 00:27:00
17 10/04/98 01:13:00
18 10/04/98 02:00:00
19 10/04/98 02:46:00·
20 10/04/98 03:33:00
21 10/04/98 04:19:00
22 10/04/98 05:05:00
23 10/04/98 05:52:00
24 10/04/98 06:38:00
25 10/04/98 07:25:00
26 10/04/98 08:11:00
27 10/04/98 08:57:00
28 10/04/98 09:44:00
29 10/04/98 10:30:00
30 10/04/98 11:17:00
• ANALYSIS BATCH SUMMARY Work Order U 9809497
Page _9_ Analysis Batch # TPGC1381002120001
Analysis· Start Date/Time 10/02/98 12: 00: 00
Analysis Stop Date/Time 10/05/98 05:32:00
Instrument ~
Analyst M@
Reviewer ~J~S~E'----------
Project Sample ID Lab Sample ID Sample Type Analysis File #
SB Blank, System V8J02001
ccv_DSL Continuing Calibration Verification V8J02002
SB Blank, System V8J02003
ClJ_JET Initial Calibration Standard 1 V8J02004
C2J_JET Initial Calibration Standard 2 V8J02005
C3J_JET Initial Calibration Standard 3 V8J02006
C4J_JET Initial Calibration Standard 4 V8J02007
C5J_JET Initial Calibration Standard 5 V8J02008 -C6J_JET Initial Calibration Standard 6 V8J02009
C7J_JET V8J02010
ClK_KER Initial Calibration Standard l V8J02011
C2K_KER Initial Calibration Standard 2 V8J02012
C3K_KER Initial Calibration Standard 3 V8J02013
C4K_KER Initial Calibration Standard 4 V8J02014
C5K_KER Initial Calibration Standard 5 V8J02015
C6K_KER Initial Calibration Standard 6 V8J02016
C7K_KER V8J02017
ClD_DSL Initial Calibration Standard 1 V8J02018
C2D_DSL Initial Calibration Standard 2 V8J02019
C3D_DSL Initial Calibration Standard 3 V8J02020
C4D_DSL Initial Calibration Standard 4 V8J02021
C5D_DSL Initial Calibration Standard 5 V8J02022
C6D_DSL Initial Calibration Standard 6 V8J02023
C7D_DSL V8J02024
CCV_JET Continuing Calibration Verification V8J02025
CCV_KER Continuing Calibration Verification V8J02026
CCV_DSL Continuing Calibration Verification V8J02027
BLK983263 Blank, Method V8J02028
LCS984970 Lab Control Sample V8J02029
LCSD984970 Lab Control Sample Duplicate V8J02030
•
10/05/98 16:48:59
Method TPH-Diesel by mod. SW8015
Test Code DSLSSAEL .
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Diesel
Jet fuel JP4
Kerosene
Unidentified organics
Surrogate (s)
Octacosane
•
0998HBWP05A
9809497-09A
V8J02042
09/21/98
09/24/98
10/04/98 21:00:00
1. 0000
Solid
ug/g
dry weight
Cone. DL
ND 0.964
ND 3.24
ND 2.92
27.0 BDA
Recovery
-------,--
145
RBS ULT S SUMMARY (Cont'd)
0998HBWP058
9809497-lOA
V8J02047
09/21/98
09/24/98
10/05/98 00:53:00
1.0000
Solid
ug/g
dry weight
Cone. DL
ND 0.987
ND 3.32
ND 2.98
3.58 BDA
Recovery
\
129
•
Cone. DL
Recovery
% ---
Work Order It 9809497
Page _8_
Cone. DL
Recovery
---%
•
10/05/98 1~9
Method TPH-Diesel by mod. SW8015
Lab Sample ID
File ID
9809497-0lA
V8J02048
9809497-04A
V8J02049
Project Sample
ID/Description
0998HBWF23B
0998HBWF22B
Specification# ~D~S~L~S~~
Analyte
DIESEL
DIESEL
AN A L Y T I C AL .0 T 0 C 0 L
COMMRNTS/NARRAT
SUMMARY
I V R
Flag Comment/Narrative
x The chromatogram indicates a multi-component
hydrocarbon eluting in the Diesel range. The
pattern of the hydrocarbon is not an exact
match, possibly due to weathering, but is too
similar to the Diesel pattern to rule out the
identification of Diesel in this sample.
x The chromatogram indicates a multi-component
hydrocarbon eluting in the Diesel range. The
pattern of the hydrocarbon is not an exact
match, possibly due to weathering, but is too
similar to the Diesel pattern to rule out the
identification of Diesel in this sample.
Corrective Action
The reported value for
due to interference by
the sample.
The reported value for
due to interference by
the sample.
Work Order~9497
Page ll_
Diesel is biased high
Lube Oil present in
Diesel is biased high
Lube Oil present in
10/05/98 16:48:59
Method TPH-Diesel by mod. SW8015
Test Code.DSLSWAEL
Initial Calibration # GC13981002120000
Calibration Date ~l~0•/~0~2~/~9~8'--~~~-
Sequence/Analysis Time
31 10/04/98 12:03:00
32 10/04/98 12:50:00
33 10/04/98 13:37:00
34 10/04/98 14:23:00
35 10/04/98 15:10:00
36 10/04/98 16:20:00
37 10/04/98 17:07:00
38 10/04/98 17:53:00
39 10/04/98 18:40:00
40 10/04/98 19:27:00
41 10/04/98 20:13:00
42 10/04/98 21:00:00
43 10/04/98 21:46:00
44 10/04/98 22:33:00
45 10/04/98 23:20:00
46 l0/05/98 00:06:00 -
47 10/05/98 00:53:00
48 10/05/98 01:39:00
49 10/05/98 02:26:00
so 10/05/98 03:12:00
51 10/05/98 03:59:00
52 10/05/98 04:45:00
53 10/05/98 05:32:00
•
A H A L Y S I S B A T C H S U M M .A R Y (cont'd)
Analysis Batch # TPGC1381002120001
Analysis Start Date/Time 10/02/98 12:00:00
Analysis Stop Date/Time 10/05/98 05:32:00
Project Sample ID Lab Sample ID Sample Type
9809513-06A Sample
A980951307A Matrix Spike
A980951308A Matrix Spike Duplicate
0998HBWF23B 9809497-0lA Sample
0998HBWF23A 9809497-02A Sample
0998HBWF22A 9809497-03A Sample
0998HBWF22B 9809497-04A Sample
0998HBWP01A 9809497-0SA Sample
0998HBWP01B 9809497-06A Sample
0998HBWP03A 9809497-07A Sample
0998HBWP03B 9809497-08A Sample
0998HBWPOSA 9809497-09A Sample
SB Blank, System
CCV_JET Continuing Calibration
CCV_KER Continuing Calibration
CCV_DSL Cont·inui.ng Cali:bration
0998HBWPOSB 9809497-lOA Sample
0998HBWF23B 9809497-0lA Sample
0998HBWF22B 9809497-04A Sample
SB Blank, System
CCV_JET Continuing Calibration
CCV_KER Continuing Calibration
CCV_DSL Continuing Calibration
•
Work Order U 9809497
Page 1.Q_
Instrument §£11.._
Analyst ~
Reviewer ~J~S~E'--~~~~~~~-
Analysis File #
V8J02031
V8J02032
V8J02033
VBJ02034
V8J02035
V8J02036
V8J02037
V8J02038
V8J02039
V8J02040
V8J02041
V8J02042
V8J02043
Verification V8J0204'4
Verification VBJ02045
Verification ~ --V8J02046
V8J02047
V8J02048
V8J02049
V8J02050
Verification V8J02051
Verification V8J02052
Verification V8J02053
•
• 10/01/98 10:01:16
Report Form
Work Order Summary
State Certifications
Flag Definitions
R A D I A !ii AH ALY.AL SERVICES
FPAS REPORT
TABLE OF CO!ilTENTS
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Analytical Batch ID
Protocol Summary for IR Analysis
Results Summary
Analysis Batch Summary WLPEIR80924160002
Comments/Narrative
Quality Control Exception Report Summary
Work Order tt 98094~
~ ~ I -· -Certified B~@-,,,,__,
Date O / J'
Pages
From To
1 2
3 3
4 4
5 5
6 8
9 10
11 11
12 12
10/05/98 16:48:59
•
QUALITY CONTROL BXCBPTIOR RB PORT
SUMMARY
QCER # Analysis Batch Number
981005-02 TPGC13981002120000
•
Work Order # 9809497
Page g_
•
10/01/98 10:01:16
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -~R"'a"'d"'i"'a"'n'-'"I"'n"'t"'e"'r"'n"'a"'t"'i"'o"'n"'a"'l"',-"L"'L'"'C"-
By 14046 Summit Dr., Bldg. B
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWPOSA
0998HBWP05B
0998HBWF23B
ID/
--
WORI ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # ~N~A'---------­
SDG # N~A..._~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA IRXESAOG
SONESAOO
02A IRXESAOG
SONESAOO
03A IRXESAOG
SONESAOO
04A IRXESAOG
SONESAOO
-
OSA IRXESAOG
SONESAOO
06A IRXESAOG
SONESAOO
07A IRXESAOG
SONESAOO
OBA IRXESAOG
SONESAOO
09A IRXESAOG
SONESAOO
lOA IRXESAOG
SONESAOO
llA MS IRXESAOG
SONESAOO
12A MSD IRXESAOG
•
Work Order # 9809498
Page L..
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extrqction
-
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
Sonication Extraction
IR analysis
• 10/01/98 10:01:16 • PROTOCOL ANALYTICAL SUMMARY
FLAG DBFINITIOHS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
NA Analyte concentration not available for this analysis.
NC RPD and/or % Recovery not calculated. See Narrative for explanation.
ND Not detected. No instrument response for analyte or result less than zero.
NR Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
NS Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit ·cand greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Resuft is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order # 9809498
Page L •
10/0l/98 10:01:16
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATE CBRTIFICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9809498
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• 10/01/98 10:01:16
Method Oil and Grease by E413.2
Test Code IRXESAOG
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Oil and Grease
• RESULTS SUMMARY
0998HBWF22A 0998HBWF22B
9809498-03A 9809498-04A
PEIR0924-31 PEIR0924-32
09/21/98 09/21/98
09/24/98 09/24/98
09/24/98 16:00:00 09/24/98 16:00:00
1 5
Solid Solid
mg/kg mg/kg
dry weight dry weight
Cone. DL Cone. DL
26.2 B 7.82 5760 B 40.5
0998HBWF23A
9809498-02A
PEIR0924-30
09/21/98
09/24/98
09/24/98 16:00:00
1
Solid
mg/kg
dry weight
Cone. DL
30.2 B 8.06
Work Order # 9809498
Page _6_
0998HBWF23B
9809498-0lA
PEIR0924-25
09/21/98
09/24/98
09/24/98 16:00:00
5
Solid
mg/kg
dry weight
Cone. DL
•
4830 B 41.6
10/01/98 10:01:16
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method IR Analysis
Project Sample ID/Description
0998HBWF22A
0998HBWF22B
0998HBWF23A
0998HBWF23B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWPOSA
0998HBWPOSB
•
ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch II
9809498-03A IRXESAOG SOIL980924140000
9809498-04A IRXESAOG SOIL980924140000
9809498-02A IRXESAOG SOIL980924140000
9809498-0lA IRXESAOG SOIL980924140000
9809498-0SA IRXESAOG SOIL980924140000
9809498-0GA IRXESAOG SOIL980924140000
9809498-0?A IRXESAOG SOIL980924140000
9809498-0BA IRXESAOG SOIL980924140000
9809498-09A IRXESAOG SOIL980924140000
9809498-lOA IRXESAOG SOIL980924140000
•
Work Order II 9809498
Page L
Analysis Batch II
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
WLPEIR80924160002
•
10/01/98 10:01:16
Method Oil and Grease by E413.2
Test Code IRXESAOG
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as: .
Column:
Analyte
Oil and Grease
•
0998HBWPOlA
9809498-05A
PEIR0924-35
09/21/98
09/24/98
09/24/98 16:00:00
l
Solid
mg/kg
dry weight
Cone. DL
44.l B 8.27
R B S UL T S S UM MAR Y "(Cont'd)
0998HBWPOlB 0998HBWP03A
9809498.-0GA 9809498-07A
PEIR0924-36 PEIR0924-37
09/21/98 09/21/98
09/24/98 09/24/98
09/24/98 16:00:00 09/24/98 16:00:00
l l
Solid Solid
mg/kg mg/kg
dry weight dry weight
Cone. DL Cone. "DL
15.3 B 8.64 17.2 B 7.93
•
Work Order # 9809498
Page ']___
0998HBWP038
9809498-08A
PEIR0924-38
09/21/98
09/24/98
09/24/98 16:00:00
l
Solid
mg/kg
dry weight
Cone. DL
8.25 BJ 8.49
•
10/01/. 01: 16
Method IR Analysis
Test Code IRXEWAOG
Initial Calibration # PEIR980924160000
Calibration Date ;0;9L/=2~4L/;9~8~~~~-
Sequence/Analysis Time
39 09/24/98 16:00:00
40 09/24/98 16:00:00
41 09/24/98 16:00:00
4·2 09/24/98 16:00:00
43 09/24/98 16:00:00
44 09/24/98 16:00:00
45 09/24/98 16:00:00
46 09/24/98 16:00:00
47 09/24/98 16:00:00
48 09/24/98 16:00:00
49 09/24/98 16:00:00
so 09/24/98 16:00:00
51 09/24/98 16:00:00
52 09/24/98 16:00:00
Project ~ample
0998HBWP05A
0998HBWP05B
A N A L Y S I S B A T. S U M M A R Y
Analysis Batch # WLPEIR80924160002
(cont'd)
Analysis Start Date/Time 09/24/98 16:00:00
Analysis Stop Date/Time
ID Lab Sample ID Sample Type
9809498-09A Sample
9809498-lOA Sample
9809514-0lA Sample
9809514-02A Sample
9809514-03A Sample
98095l.4-04A Sample
CCV Continuing Calibration
REAG_BLANK Blank, Reagent
9809514-05A Sample
9809514-06A Sample
9809514-07A Matrix Spike
9809514-08A Matrix Spike Duplicate
CCV Continuing Calibration
REAG_BLANK Blank, Reagent
Work Order # 9809498
Page ,!Q_
Instrument f]lE__
Analyst fil2Q
Reviewer =L~K~H'--~~~~~~~-
Analysis File II
PEIR0924-39
PEIR0924-40
PEIR0924-41
PEIR0924-42
PEIR0924-43
PEIR0924 -44
Verification PEIR0924-45
PEIR0924-46
PEIRO 924-117
PEIR0924-48
PEIR0924-49
PEIR0924-50
Verification PEIR0924-51
PEIR0924-52
•
10/01/98 10:01:16
Method IR Analysis
Test Code IRXEWAOG
Initial Calibration # PEIR980924160000
Calibration Date ~0~9L/~2~4~/~9~8~~~~
Sequence/Analysis Time
1 09/24/98 16:00:00
2 09/24/98 16:00:00
3 09/24/98 16:00:00
4 09/24/98 16:00:00
5 09/24/98 16:00:00
6 09/24/98 16:00:00
7 09/24/98 16:00:00
8 09/24/98 16:00:00
9 09/24/98 16:00:00
18 09/24/98 16:00:00
19 09/24/98 16:00:00
20 09/24/98 16:00:00
21 09/24/98 16:00:00
22 09/24/98 16:00:00
23 09/24/98 16:00:00
24 09/24/98 1:6: oo: oo· --
25 09/24/98 16:00:00
26 09/24/98 16:00:00
27 09/24/98 16:00:00
28 09/24/98 16:00:00
29 09/24/98 16:00:00
30 09/24/98 16:00:00
31 09/24/98 16:00:00
32 09/24/98 16:00:00
33 09/24/98 16:00:00
34 09/24/98 16:00:00
35 09/24/98 16:00:00
36 09/24/98 16:00:00
37· 09/24/98 16:00:00
38 09/24/98 16:00:00
•
AHALYSIS BATCH SUMMARY
Analysis Batch # WLPEIR80924160002
Analysis Start Date/Time 09/24/98 16:00:00
Analysis Stop Date/Time
Work Order # 9809498
Page _9 _
Instrument ~
Analyst fil1Q
Reviewer ;L~K~H~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File It
CAL_STDl Initial Calibration Standard 1 PEIR0924-l
CAL_STD2 Initial Calibration Standard 2 PEIR0924-2
CAL_STD3 Initial Calibration Standard 3 PEIR0924-3
CAL_STD4 Initial Calibration Standard 4 PEIR0924-4
CAL_STDS Initial Calibration Standard 5 PEIR0924-5
CAL_STD6 Initial Calibration Standard 6 PEIR0924-6
ISV Second Source Standard PEIR0924-7
ICV Initial Calibration Verification PEIR0924-8
REAG_BLK Blank, Reagent PEIR0924-9
CCV Continuing Calibration Verification PEIR0924-18
REAG_BLANK Blank, Reagent PEIR0924-19
BLK983293 Blank, Method PEIR0924-20
LCS985014 Lab Control Sample PEIR0924-21
LCSD985014 Lab Control Sample Duplicate PEIR0924-22
A980949801A Sample PEIR0924-23
-A98094·9801A Sample --EEIR0924-24
0998HBWF23B 9809498-0lA Sample PEIR0924-25
0998HBWF23B 9809498-llA Matrix Spike PEIR0924-26
0998HBWF23B 9809498-12A . Matrix Spike Duplicate PEIR0924-27
0998HBWF23B 9809498-llA Matrix Spike PEIR0924-28
0998HBWF23B 9809498-12A Matrix Spike Duplicate PEIR0924-29
0998HBWF23A 9809498-02A. Sample PEIR0924-30
0998HBWF22A 9809498-03A Sample PEIR0924-31
0998HBWF22B 9809498-04A Sample PEIR0924-32
CCV Continuing Calibration Verification PEIR0924-33
REAG_BLANK Blank, Reagent PEIR0924-34
0998HBWP01A 9809498-0SA Sample PEIR0924-35
0998HBWP01B 9809498-06A Sample PEIR0924-36
0998HBWP03A 9809498-07A Sample PEIR0924-37
0998HBWP03B 9809498-08A Sample PEIR0924-38
• •
• 10/01/98 10:01:16 QUALITY COJITR.OL B.PTIOJI RB PORT
SUMMARY
QCER # Analysis Batch Number
980924-12 PEIR80924160000 02
Work Order # 9809498
Page 1d_ •
10/01/98 10:01:16
Method IR Analysis
Lab Sample ID
File ID
•
Project Sample
ID/Description
Specif icationtt ONGE
Analyte
ABALYTICAL PROTOCOL SUMMARY
COMMBBTS/BARRATIVE
Flag Comment/Narrative
•
Corrective Action
Work Order tt 9809498
Page l.L.
•
• 09/28/98 10:20:55
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _:.;R:::a:.::d:.:i"'.a"'n:_:I"'n"'t"'e"'r"'n"'a"'L"'1"'o"'n:::ao.;l:...<,--!L<>L:::C:....
By --=1"'4"'0"'4"'6'-=S""u:.:.:m:.:.:m"'i"'t'--"D:..:rc.:·...1.i-=B:..l:::d"'g'-'.-=B:....
P. o. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWPOSA
0998HBWPOSB
ID/
N 0 R K ORD BR • SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Fa~ility WASHINGTON NC
Work ID VOLATILES
Case # ~N~A'--------­
SDG # ~N~A----~-~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA PH_ESAOO
02A PH_ESAOO
03A PH_ESAOO
04A PH_ESAOO
05A PH_ESAOO
06A PH_ESAOO
07A PH_ESAOO
OSA PH_ESAOO
09A PH_ESAOO
lOA PH_ESAOO
pH
pH
pH
pH
pH
pH
pH
pH
pH
pH
Work Order # 9809499
Page _l_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
•
09/28/98 10:20:55
•
NORK ORDBR COMMBHTS
Prep batch weights were not recorded at time of prep. Samples were weighed at
20.0 +/-0.5 grams, but the exact weight was not recorded. The sample weight
will not affect pH results .
•
Work Order U 9809499
Page L
•
• 09/28/98 10:20:55
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method pH by SW904SC
Project Sample ID/Description
0998HBWF22A
0998HBWF22B
0998HBWF23A
0998HBWF23B
'0998HBWF23B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWPOSA
0998HBWPOSB
ANALYTICAL
Lab Sample ID
9809499-03A
9809499-04A
9809499-02A
9809499-0lA
9809499-0lA
9809499-0SA
9809499-0GA
9809499-0?A
9809499-08A
9809499-09A
9809499-lOA
P.T 0 C 0 L S U M M A R Y
Extraction/Digestion
1'est Code(s) Batch II
PH_ESAOO SOIL980923110000
PH_ESAOO SOIL980923110000
PH_ESAOO SOIL980923110000
PH_ESAOO SOIL980923110000
PH_ESAOO S01L980923110000
PH_ESAOO SOIL9 8 0 92 31100 0 0
PH_ESAOO SOIL980923110000
PH_ESAOO SOIL980923110000
PH_ESAOO SOIL980923110000
PH_ESAOO SOIL9.80923110000
PH_ESAOO SOIL980923110000
Work Order # 9809499
Page _s_
Analysis Batch II
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940_80923110001
WL940 80923110001 -
•
09/28/98 10:20:55 ANALYTICAL PROTOCOL SUMMARY
FLAG DEFINITIONS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available fqr this a~alysis. NA
NC
ND
NR
NS
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results--from --primary and secondary GC -columns differ by greater -than a factor-of 3. -
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation .
• •
Work Order U 9809499
Page _4_
•
09/28/98 10:20:55
Method pH by SW9045C
Test Code PH ESAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
[. .te Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
pH
•
0998HBWF22A
9809499-03A
9400923-9
09/21/98
09/23/98
09/23/98 11:00:00
1
Solid
pH units
received
Cone.
4.87
DL
RESULTS SUMMARY
0998HBWF22B
9809499-04A
9400923-10
09/21/98
09/23/98
09/23/98 11:00:00
1
Solid
pH units
received
Cone.
4.29
•
DL
0998HBWF23A
9809499-02A
9400923-8
09/21/98
09/23/98
09/23/98 11:00:00
1
Solid
pH units
received
Cone.
4. 72
DL
Work Order U 9809499
Page _6_
0998HBWF23B
9809499-0lA
9400923-6
09/21/98
09/23/98
09/23/98 11:00:00
1
Solid
pH units
received
Cone. DL
3.85
•
09/28/~:20:55
Method pH by SW9045C
Test Code PH ESAOO
Initial Calibration # ~N~A~------~
Calibration Date ~--------
Sequence/Analysis Time
1 09/23/98 11:00:00
2 09/23/98 11:00:00
3 09/23/98 11:00:00
4 09/23/98 11:00:00
5 09/23/98 11:00:00
6 09/23/98 11:00:00
7 09/23/98 11:00:00
8 09/23/98 11:00:00
9 09/23/98 11:00:00
10 09/23/98 11:00:00
11 09/23/98 11:00:00
12 09/23/98 11:00:00
13 09/23/98 11:00:00
14 09/23/98 11:00:00
15 09/23/98 11.:00:00
16 09/23/98 11:00:00
17 09/23/98 11:00:00
Project Sample
0998HBWF23B
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWPOSB
ANALYSIS BA. SUMMARY
Analysis Batch # WL940 80923110001
Analysis Start Date/Time 09/23/98 11:00:00
Analysis Stop Date/Time 09/23/98 13:00:00
IO Lab Sample ID Sample Type
STD_lO Initial Calibration
STD_? Initial Calibration
STD_4 Initial Calibration
LCS985016 Lab Control Sample
LCSD985016 Lab Control Sample
9809499-0lA Sample
9809499-0lA Sample Duplicate
9809499-02A Sample
9809499-03A Sample
9809499-04A Sample
9809499-05A Sample
9809499-0GA Sample
9809499-0?A Sample
9809499-08A Sample
9809499-09A Sample
9809499-lOA Sample
Standard
Standard
Standard
Duplicate
Work Order # 9809499
Page _9_
Instrument 21.Q.___
Analyst !1AT
Reviewer ~---------
Analysis File #
1 9400923-1
2 9400923-2
3 9400923-3
9400923-4
9400923-5
9400923-6
9400923-7
94 00923-8
9400923-9
9400923-10
9400923-11
9400923-12
94 00923 -13
9400923-14
9400923-15
9400923-16
CCV Continuing Calibration Verification 9400923-17
•
09/28/98 10:20:55
Method pH by SW904SC
Test Code PH ESAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
pH
•
0998HBWP03B
9809499-08A
9400923-14
09/21/98
09/23/98
09/23/98 11:00:00
1
Solid
pH units
received
Cone. DL
4.56
RESULTS S 0 MM ARY (Cont'd)
0998HBWP05A 0998HBWP05B
9809499-09A 9809499-lOA
9400923-15 9400923-16
09/21/98 09/21/98
09/23/98 09/23/98
09/23/98 11:00:00 09/23/98 11:00:00
1 1
Solid Solid
pH units pH units
received received
Cone. DL Cone. DL
5.19 4.45
•
Work Order H 9809499
Page _8_
Cone. DL
•
09/28/98 10:20:55
Method pH by SW9045C
Lab Sample ID
File ID
•
Project Sample
ID/Description
SpecificationU -P~H---~~
Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Comment/Narrative
•
Corrective Action
Work Order U 9809499
Page 1.Q_
•
• 10/01/98 16:27:30 If 0 R K ORDER C .. BHTS
Sample results for this method are not "B" flagged because the instrument
does a blank subtraction before calculating a result. The blank result reported
for this method is the number(in mgs/kg) that is subtracted, by the instrument,
from each subsequent result prior to reporting.
Work Order #
Page L
10/01/98 16:27:30
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ ...... R::::a::::d:::i::::a~n:.....::I..:;n:::t:::e:::r..:;n:::a:::t:::i:.::o::.n:::a:::l"''-=L:::L:::C=­
By --"'1"'4-"0"'4-"6'-"S"'u"'m"'m"'i'-"t'-"D"'r'"' . ..1.'---"B"'l'-"d::;qL:._.B:....
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWP01A
•
ID/
NORX ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # ,.N"'A'----------
SDG # ... N ... A _______ _
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA TOCRSAOO
•
Work Order # 9809500
Page L_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Total Organic Carbon
•
10/01/98 16:27:30
State
Arkansas
california
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STA TB C B R T I P I C A T I 0 JI S
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9809500
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• 10/01/98 16:27:30
Method Total organic carbon
Test Code TOCRSAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Total organic carbon
0998HBWP01A
9809500-0lA
CHNlOOl-9
09/21/98
10/01/98 09:53:00
1
Solid
mg/kg
dry weight
Cone. DL
624 230
• RESULTS SUMMARY
Cone. DL Cone. DL
Work Order # 9809500
Page _6_
Cone. DL
•
10/01/98 16:27:30
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method Total organic carbon
Project Sample ID/Description
0998HBWP01A
•
ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code (s) Batch II
9809500-0lA TOCRSAOO NA
•
Work Order # 9809500
Page _s_
Analysis Batch #
WLCHN_81001095301
•
• lO/Ol/98 16:27:30
Method Total organic carbon
Lab Sample ID
File ID
Project Sample
ID/Description
Specif icationjj
Analyte
• ANALYTICAL PROTOCOL SUMMARY
COMMEHTS/HARRATIVE
Flag Comment/Narrative
Work
Corrective Action
Order.09500
Page _a_
10/01/98 16:27:30
Method Total organic carbon
Test Code TOCRSAOO
Initial Calibration # ~N~A--~~~~~~­
Calibration Date ~~~~~~~~
Sequence/Ar:ialysis Time
1 10/01/98 09:53:00
2 10/01/98 09:53:00
3 10/01/98 09:53:00
4 10/01/98 OJJ:53:00
5 10/01/98 09:53:00
6 10/01/98 09:53:00
7 10/01/98 09:53:00
8 10/01/98 09:53:00
9 10/01/98 09:53:00
10 10/01/98 09:53:00
-11 10/01/98 09:53:00
12 10/01/98 09:53:00
13 10/01/98 09:53:00
14 10/01/98 09:53:00
•
ANALYSIS BATCH SOHM.ARY
Analysis Batch # WLCHN 81001095301
Analysis Start Date/Time 10/01/98 09:53:00
Analysis Stop Date/Time
Work Order # 9809500
Page _7_
Instrument .Qlli__
Analyst fil£
Reviewer =L~K~H~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File #
BLK Blank, System CHNlOOl-1
BLK Blank, System CHNlOOl-2
QC-STDl Initial Calibration Standard 1 CHNlOOl-3
QC-STD2 Initial Calibration Standard 2 CHNlOOl-4
ICV_ACET Initial Calibration Verification CHNlOOl-5
ICV_CYST Initial Calibration Verification CHNlOOl-6
LCS985097 Lab Control. Sample CHNlOOl-7
QC-CHECK Second Source Standard CHNlOOl-8
0998HBWP01A 9809500-0lA Sample CHNlOOl-9
9809516-0lA Sample CHNlOOl-10
9809516-02A Sample CHNlOOl-11
9809516-03A SamP.le Duplicate CHNlOOl-12
CCV_ACET Continuing Calibration Verification CHNlOOl-13
LCSD985097 Lab Control Sample Duplicate CHNlOOl-14
• •
10/07/9~09:10
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
STATB CBRTI.ATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9809501
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
10/07/98 09:09:10
•
Ii 0 R K 0 R D E R C 0 M M B H T S
The standard Method 8260A surrogate tolerances are laboratory derived from
historical data. Project specific tolerances may differ .
•
Work Order # 9809501
Page _2_
•
10/07/.:09:10
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Volatile Organics SW8260B
Project Sample ID/Description
0998HBWF22B
0998HBWF23B
0998HBWF22A
0998HBWF22A
0998HBWF22B
0998HBWF23A
0998HBWF23A
0998HBWF23B
0998HBWP01A
0998HBWP01A
0998HBWP01B
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWP05B
ANALYTICAL P.TOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9809501-04A 826MSBCM NA
9809501-0lA 826MSBCM NA
9809501-03A 826SSACM NA
9809501-03A 826SSACM NA
98'0950l-04A 826SSACM NA
9809501-02A 826SSACM NA
980950l-02A 826SSACM NA
9809501-0lA 826SSACM NA
9809501-05A 826SSACM NA
980950l-05A 826SSACM NA
9809501-0GA 826SSACM NA
9809501-0GA 826SSACM NA
9809501-0?A 826SSACM NA
9809501-08A 826SSACM NA
9809501-09A 826SSACM NA
9809501-lOA 826SSACM NA
Work Order # 9809501
Page _5 _
Analysis Batch #
MSMSDC81002131401
MSMSDC8100213140l
MSMSDC81002131401
MSMSDC81002131401
MSMSDC81002131401
MSMSDC8100213140l
MSMSDC81002131401
MSMSDC81002131401
MSMSDC81002131401
MSMSDC81002131401
MSMSDC8100213140l
MSMSDC81002131401
MSMSDC81002131401
MSMSDC81002131401
MSMSDC81002131401
MSMSDC81002131401
•
10/07/98 09:09:10 ANALYTICAL PROTOCOL SUMMARY
FLAG DBFINITIONS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal.to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
A
B
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Lfmit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M
p
Q
R
Result modified from previous Report. See Narrative for explanation.
Analyte not confirme~d. Results from primary and secondary GC columns differ by greater than a factor of 3.
QC result does not meet tolerance in Protocol Specification.
Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation .
• •
Work Order # 9809501
Page _4_
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826MSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Aerylonitrile
Benzene
1-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodiehloromethane
Bromof orm
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
see-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
•
0998HBWF22B
9809501-04A
Cl002861
09/21/98 14:50
01:12:00
10/03/98 03:56:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 289
ND 1140
ND 2060
ND 180
ND 160
ND 83.2
ND 102
ND 112
ND 442
ND 58.6
ND 151
900 151
ND 121
ND 119
ND 127
32.4 BJ 173
ND 150
ND 198
ND 113
ND 112
RBSULTS SUMMARY
0998HBWF23B
980950l-01A
C1002860
09/21/98 14:20
01:12:00
10/03/98 03:28:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 294
ND 1160
ND 2100
ND 183
ND 162
ND 84.6
ND 103
ND 114
ND 449
ND 59.6
ND 154
305 154
ND 123
ND 122
ND 129
33.4 BJ 176
ND 153
ND 202
ND 115
ND 114
•
Cone. DL
Work Order # 9809501
Page _6_
Cone. DL
•
• 10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826MSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrof uran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
0998HBWF22B
9809501-04A
C1002861
09/21/98 14:50
01:12:00
10/03/98 03:56:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 127
ND 84.2
ND 49 .4
ND 142
ND 156
87.0 J 130
ND 122
ND 128
7960 118
ND 73.6
1100 436
ND 239
ND 66.8
ND 163
296 122
ND 119
ND 593
ND 146
60.5 J 263
68.4 J 109
• RESULTS S UM MAR Y (Cont'd)
0998HBWF23B
9809501-0lA
C1002860
09/21/98 14:20
01:12:00
10/03/98 03:28:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 129
ND 85.7
ND 50.3
ND 144
ND 159
ND 132
ND 125
ND 131
1310 120
ND 74.9
293 J 443
ND 243
ND 68.0
ND 166
ND 125
ND 121
ND 603
ND 149
ND 267
ND 111
Cone. DL
Work Order # 9809501
Page _9_
Cone. DL
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826MSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
0998HBWF22B
9809501-04A
Cl002861
09/21/98 14 :50
01:12:00
10/03/98 03:56:00
l
Solid
ug/kg
dry weight
Cone. DL
ND 493
ND 64.9
ND 169
ND 136
ND 133
ND 95.0
ND 71.3
8 .11 J 116
ND J.15
ND 97.9
ND 152
ND 117
ND 120
ND 158
ND 253
ND 112
164 BJ 173
ND 91.0
ND 1300
ND 131
RBSULTS SUMMARY (Cont'd)
0998HBWF23B
9809501-0lA
Cl002860
09/21/98 14:20
01:12:00
10/03/98 03:28:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 502
ND 66.1
ND 172
ND 138
ND 136
ND 96.7
ND 72.6
ND 118
ND 117
ND 99.7
ND 155
ND 119
ND 122
ND 161
ND 258
ND 114
179 B 176
ND 92.6
ND 1320
ND 133
Cone. DL
Work Order # 9809501
Page _8_
Cone. DL
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826MSBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
0998HBWF22B
9809501-04A
Cl002861
09/21/98 14:50
01:12:00
10/03/98 03:56:00
1
Solid
ug/kg
dry weight
Cone. DL
Recovery
"'
59
74
55
RB S UL T S S UM MARY "(Cont'd)
0998HBWF23B
9809501-0lA
C1002860
09/21/98 14:20
01:12:00
10/03/98 03:28:00
1
Solid
ug/kg
dry weight
Cone. DL
Recovery
"'
60
75
54
•
Cone. DL
Recovery
%
Work Order # 9809501
Page lQ_
Cone. DL
Recovery
"'
•
10/07/.:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone{MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
0998HBWF22A
9809501-03A
C1002835
09/21/98 14:45
00:00:00
10/02/98 15:58:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
13.4
ND
1.48
ND
1. 78
2.62
ND
ND
0. 873 J
5.46 B
ND
6.42 J
13.9
DL
4.74
0.624
1. 63
1.30
1.28
0.913
0.685
1.11
1.10
0.941
1.46
1.13
1.15
1. 52
2.43
1. 08
1. 66
0.874
12.5
1.26
RESULTS .MARY
I.
0998HBWF22A
9809501-03A
C1002856
09/21/98 14:45
00:00:00
10/03/98 01:39:00
1
" .
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
15.8
ND
ND
ND
2.50 J
3.63 J
ND
ND
ND
11.6 B
ND
ND
15.7
DL
23.3
3.07
8.00
6.41
6.30
4.49
3.37
5.48
5.44
4.63
7.21
5.55
5.67
7.49
12.0
5.29
8.17
4.30
61. 3
6.18
{Cont'd)
0998HBWF228
9809501-04A
C1002836
09/21/98 14:50
00:00:00
10/02/98 16:26:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
44.7
ND
2.96 F
ND
9.70
9.68
ND
ND
1.52
10 .4 B
73.3
12.6 J
67.8
DL
4.89
0.644
1. 68
1.35
1. 32
0.943
0. 707
1.15
1.14
0.971
1.51
1.16
1.19
1.57
2.51
1.11
1. 71
0.902
12.9
1.30
Work Order # 9809501
Page ]d_ •
I
0998HBWF23A
9809501-02A
C1002834
09/21/98 14:15
00: 00.: 00
10/02/98 15:30:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
6.10
ND
ND
ND
0. 825 J
9.99
ND
ND
ND
4.61 B
ND
ND
4.07
DL
4.85
0.639
1. 66
1. 33
1. 31
0.935
0.701
1.14
1.13
0.963
1.50
1.15
1.18
1. 56
2.49
1.10
1. 70
0.895
12.8
1.29
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
l,2-Dibromo-3-chloropropane
Dibromoehloromethane
1,2-Dibromoethane
Dibromomethane
trans-l,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Diehlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Diehloroethane
1,2-Diehloroethane
1,1-Dichloroethene
cis-1,2-Diehloroethene
trans-1,2-Dichloroethene
•
0998HBWF22A
9809501-03A
Cl002835
09/21/98 14:45
00:00:00
10/02/98 15:58:00
l
Solid
ug/kg
dry weight
Cone. DL
l. 51 l. 06
ND 1.15
ND 1.13
ND 1.45
ND 1.07
ND 1.16
ND 0.990
ND 0.783
ND 0.559
ND 4.62
ND 0.818
ND 0.974
ND 1.12
ND l. 05
ND l. 76
125 2.62
45.0 B 1.21
83.0 l. 74
768 ER l. 53
19.2 2.27
R B S ULT S S UM MA R Y (Cont'd)
0998HBWF22A 0998HBWF22B
9809501-03A 9809501-04A
Cl002856 Cl002836
09/21/98 14:45 09/21/98 14 :50
00:00:00 00:00:00
10/03/98 01:39:00 10/02/98 16:26:00
l l
Solid Solid
ug/kg ug/kg
dry weight dry weight
Cone. DL Cone. DL
ND 5.24 9.53 1.10
ND 5.67 ND 1.19
ND 5.58 ND 1.17
ND 7.15 ND 1.50
ND 5.25 ND 1.10
ND 5.73 ND 1.20
ND 4.87 ND 1.02
ND 3.85 ND 0.808
ND 2.75 ND 0.577
ND 22.8 ND 4.77
ND 4.03 ND 0.845
ND 4.79 ND l. 01
ND 5.51 ND 1.16
ND 5.17 ND 1.08
ND 8.68 ND 1.82
105 12.9 1650 ER 2.70
51.4 B 5.96 151 B 1.25
79.9 8.57 2890 ER 1,80
826 7.55 2240 ER 1.58
16.1 11.2 80.1 2.35
•
Work Order ff 9809501
Page .Jd_
0998HBWF23A
9809501-02A
Cl002834
09/21/98 14 :15
o.o :00: 00
10/02/98 15:30:00
l
Solid
ug/kg
dry weight
Cone. DL
ND 1.03
ND 1.18
ND 1.16
ND 1.49
ND 1.09
ND 1.19
ND l. 01.
ND 0.802
ND 0.573
ND 4.73
ND 0.838
ND 0.998
ND 1.15
ND l. 08
ND l. 81
46.5 R 2.68
23.3 B l. 24
60.6 R l. 78
243 ER 1.57
5.19 2.33
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
•
0998HBWF22A
9809501-03A
C1002835
09/21/98 14:45
00:00:00
10/02/98 15:58:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
1.08 J
1.SO
66.1
ND
ND
727 ER
18.0
102
ND
ND
ND
19.0
7.82
2.26 J
ND
22.3
2S.1
DL
1.22
0.809
0.47S
1.36
1. so
1.2S
1.18
1.23
l.13
0.707
4.18
2.29
0.642
1.S7
1.18
1.14
S.69
1.41
2.S2
1.05
R B S U LT S S UM MAR Y (Cont'd)
0998HBWF22A
9809S01-03A
Cl0028S6
09/21/98 14:4S
00:00:00
10/03/98 01:39:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
78 .. 1
ND
ND
870
20.7
117
ND
ND
ND
24.8
9.78
ND
ND
28.7
32.8
•
DL
6.01
3.98
2.34
6.69
7.38
6.13
S.79
6.07
5.58
3.48
20.6
11.3
3.16
7.72
5.79
5.62
28.0
6.92
12.4
S.15
0998HBWF22B
9809501-04A
C1002836
09/21/98 14:50
00:00:00
10/02/98 16:26:00
1
Solid
ug/kg
dry weight
Cone.
0. 774 J
ND
ND
17.l
3.77 F
164
ND
ND
6730 ER
22.9
1770 ER
ND
ND
ND
322 ER
110
l. 89 J
ND
102
110
DL
1. 26
0.836
0.490
1.40
1. SS
1.29
1.21
1.27
l.17
0.730
4.32
2.37
0.663
1.62
1.21
1.18
5.88
1.45
2. 61
1. 08
Work Order ff 9809501
Page .!i_
0998HBWF23A
9809S01-02A
C1002834
09/21/98 14:15
00:00:00
10/02/98 15:30:00
l
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
3.24
ND
36.5
ND
ND
402 ER
12.0
128 R
ND
ND
ND
ND
ND
2.09 J
ND
S.9S
6.62
DL
1.2S
0.829
0.486
1.39
l.S3
1.28
1.20
1.26
1.16
o. 724
4.29
2.3S
0.6S8
1.61
1.20
1.17
5.83
1.44
2.59
1. 07
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
·Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
•
0998HBWF23A
9809S01-02A
Cl0028S5
09/21/98 14:1S
00:00:00
10/03/98 01:11:00
1
Solid
ug/kg
dry weight
Cone.
162 B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
42.0
ND
ND
ND
3.02 BJ
ND
ND
ND
ND
DL
14.0
S4.9
99.8
8.70
7. 71
4.02
4 .91
S.40
21.3
2. 83·
7.31
7.31
S.86
S.77
6.lS
8.3S
7.2S
9.S7
S.4S
5.42
R B S UL TS S UM MAR Y (Cont'd)
0998HBWF23B
9809S01-01A
Cl002833
09/21/98 14:20
00:00:00
10/02/98 15:02:00
1
Solid
ug/kg
dry weight·
Cone.
68.0 B
12.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
173
S.30
2.10
ND
0.866 BJ
ND
ND
ND
ND
•
DL
2.98
11. 7
21. 3
l. 85
1.64
0.8S7
l. OS
l.lS
4.SS
0.603
l.S6
l.S6
l.2S
1.23
l. 31
l. 78
l. SS
2.04
1.16
l. lS
0998HBWP01A
9809501-0SA
C1002837
09/21/98 1S:40
00:00:00
10/02/98 16:S3:00
l
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
2.89
11.4
20.7
l. 80
l. 60
0.832
l. 02
1.12
4.42
O.S86
l. Sl
l.Sl
1.21
1.20
1.27
l. 73
l. so
l. 98
1.13
1.12
Work Order ff 9809S01
Page 1§__
0998HBWP01A
9809S01-05A
C10028S7
09/21/98 15:40
00: 00.: 00
10/03/98 02:07:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
2.89
11.4
20.7
1.80
1.60
0.832
1. 02
1.12
4.42
O.S86
l.Sl
1. Sl
1.21
1.20
1.27
1.73
l. so
l. 98
1.13
1.12
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
•
0998HBWF23'A
9809501-02A
Cl002855
09/21/98 14:15
00:00:00
10/03/98 01:11:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 23.8
ND 3.14
ND 8.18
ND 6.55
ND 6.44
ND 4.59
ND 3.45
5.30 J 5.60
ND 5.56
ND 4.73
ND 7.37
ND 5.67
11.3 5.80
ND 7.66
ND 12.2
ND 5.41
11.1 B 8.35
ND 4.40
ND 62.6
ND 6.32
RESULTS S UM MARY (Cont'd}
0998HBWF23B 0998HBWP01A
9809501-0lA 9809501-0·5A
Cl002833 C1002837
09/21/98 14:20 09/21/98 15:40
00:00:00 00:00:00
10/02/98 15:02:00 10/02/98 16:53:00
1 1
Solid Solid
ug/kg ug/kg
dry weight dry weight
Cone. DL Cone. DL
ND 5.08 ND 4.94
ND 0.669 ND 0.650
ND 1. 74 ND 1.69
ND 1.40 ND 1.36
ND 1.37 ND 1.33
ND 0.979 ND 0.951
ND 0.734 ND 0. 713
8.07 1.19 ND 1.16
' ND 1.18 ND 1.:t5
2.27 1. 01 ND 0.980
ND 1.57 ND 1.53
2.32 1.21 ND 1.17
2.79 1.24 ND 1.20
ND 1.63 ND 1.59
ND 2.61 ND 2.53
1.14 il" 1.15 ND 1.12
6.98 B 1. 78 3.01 B 1.73
13.4 0.937 ND 0.910
7.66 J 13.3 ND 13.0
11.6 1.35 ND 1. 31
•
Work Order # 9809501
Page .lL
0998HBWP01A
9809501-05A
C1002857
09/21/98 15:40
00:00:00
10/03/98 02:07:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 4.94
ND 0.650
ND 1. 69
ND 1.36
ND 1. 33
ND 0.951
ND o. 713
ND 1.16
ND 1.15'
ND 0.980
ND 1.53
ND 1.17
ND 1.20
ND 1.59
ND 2.53
ND 1.12
3.40 B 1. 73
ND 0.910
ND 13.0
ND 1. 31
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Repo~rt as: .
Column:
Analyte
Surrogate(s}
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
0998HBWF23A
9809501-02A
Cl002855
09/21/98 14:15
00:00:00
10/03/98 01:11:00
1
Solid
ug/kg
dry weight
Cone. DL
Recovery
'I;
92
111
97
R E S 0 L T S S 0 MM AR Y "(Cont'd)
0998HBWF23B 0998HBWP01A
9809501-0lA 9809501-05A
Cl002833 Cl002837
09/21/98 14:20 09/21/98 15:40
00:00:00 00:00:00
10/02/98 15:02:00 10/02/98 16:53:00
1 l
Solid Solid
ug/kg ug/kg
dry weight dry weight
Cone. DL Cone. DL
Recovery Recovery
'I; 'I;
94 86
86 109
95 95
•
Work Order # 9809501
Page £Q_
0998HBWP01A
9809501-05A
Cl002857
09/21/98 15 :40
00:00:00
10/03/98 02:07:00
1
Solid
ug/kg
dry weight
Cone. DL
Recovery
'I;
84
113
95
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-l,4-Dichloro-2-butene
1,2-Dichlorobenzene
l,3-Dichlorobenzene
l,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-l,2-Dichloroethene
trans-1,2-Dichloroethene
•
0998HBWP01B
9809501-06A
Cl002838
09/21/98 15:40
00:00:00
10/02/98 17:22:00
l
Solid
ug/kg
dry weight
Cone. DL
ND 1.18
ND 1.28
ND 1.26
ND 1. 62
ND 1.19
ND 1. 30
ND 1.10
ND 0.872
ND 0.623
ND 5.15
ND 0.911
ND 1. 08
ND 1.25
ND 1.17
ND 1.96
ND 2.91
1.04 BJ 1. 35
0.919 RJ 1. 94
1.47 RJ 1. 71
ND 2.53
R B S ULT S S UM MAR Y (Cont'd)
0998HBWP01B 0998HBWP03A
9809501-06A 9809501-07A
Cl002858 Cl002839
09/21/98 15 :40 09/21/98 16:00
00:00:00 00:00:00
10/03/98 02:35:00 10/02/98 17:50:00
1 1
Solid Solid
ug/kg ug/kg
dry weight dry weight
Cone. DL Cone. DL
ND 1.17 ND 1.06
ND 1.27 ND 1.15
ND 1.25 ND 1.13
ND 1. 60 ND 1.45
ND 1.18 ND 1.06
ND 1.28 ND 1.16
ND 1. 09 ND 0.986
ND 0.863 ND 0.780
ND 0.616 ND 0.557
ND 5.10 ND 4.60
ND 0.902 ND 0.815
ND 1. 07 ND 0.970
ND 1.23 ND 1.11
ND 1.16 ND 1.05
ND 1. 94 ND 1. 76
ND 2.89 ND 2.61
ND 1. 33 0.822 BJ 1. 21
ND 1. 92 ND 1. 73
ND 1. 69 0.540 ZJ 1.53
ND 2.50 ND 2.26
•
Work Order # 9809501
Page ~
0998HBWP03B
9809501-08A
Cl002840
09/21/98 16:05
00:00-:00
10/02/98 18:17:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 1.13
ND 1.22
ND 1.20
ND 1.54
ND 1.13
ND 1.24
ND 1. 05
ND 0.831
ND 0.593
ND 4.91
ND 0.869
ND 1. 03
ND 1.19
ND 1.11
ND 1. 87
ND 2.78
0.828 BJ 1.28
ND 1. 85
0.349 ZJ 1. 63
ND 2.41
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
l,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
•
0998HBWP01B
9809501-06A
Cl002838
09/21/98 15:40
00:00:00
10/02/98 17:22:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
4.23 R
ND
0.977 RJ
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
1.36
0.901
0.529
1.51
1.67
1.39
1.31
1.37
1.26
0.787
4.66
2.55
0. 715
1.75
1.31
1.27
6.34
1.57
2.81
1.16
RKSULTS S UM MAR Y (Cont'd)
0998HBWP01B
9809501-06A
Cl002858
09/21/98 15:40
00:00:00
10/03/98 02:35:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
1. 35
0.892
0.524
1.50
1. 65
1.,37
1.30
1. 36
1.25
0.779
4. 61
2.53
0.708
1. 73
1.30
1.26
6.28
1.55
2.78
1.15
0998HBWP03A
9809501-07A
Cl002839
09/21/98 16:00
00:00:00
10/02/98 17:50:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
1. 80
ND
ND
2.04 z
ND
0.373 ZJ
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
1.22
0.806
0 .473
1.35
1.49
1.24
1.17
1.23
1.13
0. 704
4 .17
2.28
0.639
1. 56
1.17
1.14
5.67
1.40
2.51
1. 04
Work Order H 9809501
Page~
0998HBWP03B
9809501-08A
Cl002840
09/21/98 16:05
00:00:00
10/02/98 18:17:00
1
Solid
ug/kg
dry weight
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
1.39 z
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
1.30
0.859
0.504
1.44
1.59
1. 32
1.25
1. 31
1.20
0.750
4.44
2 .43
0.682
1.66
1.25
1.21
6.04
1.49
2.68
1.11
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Aero le in
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromod1chloromethane
Bromoform
Bromomethane
2-Butanone{MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chlo roe thane
•
0998HBWPOSA
9809501-09A
Cl002841
09/21/98 16:15
00:00:00
10/02/98 18:4'5:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 2.72
ND 10.7
ND 19.4
ND 1. 69
ND 1.50
ND 0. 782
ND 0.955
ND 1. OS
ND 4.15
ND 0.551
ND 1.42
ND 1.42
ND 1.14
ND 1.12
ND 1.20
0.391 BJ 1.62
ND 1.41
ND 1.86
ND 1. 06
ND 1.05
RESULTS S UM MARY 0(Cont'd)
0998HBWP05B
9809501-lOA
Cl002842
09/21/98 16:20
00:00:00
10/02/98 19:13:00
1
Solid
ug/kg
dry weight
Cone. DL
ND 2.79
ND 11.0
ND 19.9
ND 1. 74
ND 1.54
ND 0.804
ND 0.981
ND 1. 08
ND 4.21
ND 0.566
ND 1.46
ND 1.46
ND 1.17
ND 1.15
ND 1.23
ND : 1.67
ND 1.45
ND 1. 91
ND 1. 09
ND 1. 08
•
Cone. DL
Work Order # 9809501
Page _£L
Cone. DL
-
-
-
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutad±ene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
•
099BHBWP05A
9809501-09A
Cl002841
09/21/98 16:15
00:00:00
10/02/98 18:45:00
l
Solid
ug/kg
dry weight
Cone. DL
ND 4.64
ND 0.610
ND 1. 59
ND 1.27
ND 1.25
ND 0.894
ND 0.670
ND 1. 09
ND 1. 08
ND 0.921
ND 1.43
ND 1.10
ND 1.13
ND 1.49
ND 2.38
ND 1.05
1. 91 B 1.62
ND 0.855
ND 12.2
ND 1.23
R E SULT S S UM MARY (Cont'd)
099BHBWP05B
9809501-lOA
Cl002842
09/21/98 16:20
00:00:00
10/02/98 19:13:00
l
Solid
ug/kg
dry weight
Cone. DL
ND 4.77
ND 0.627
ND 1.63
ND 1.31
ND 1.29
ND 0.918
ND 0.689
ND 1.12
ND 1.11
ND o. 946
ND 1.47
ND 1.13
ND 1.16
ND 1.53
ND 2.45
ND 1. 08
2.63 B 1.67
ND 0.879
ND i2.s
ND 1.26
•
Cone. DL
Work Order # 9809501
Page £§___
Cone. DL
•
• 10/07/98 09:09:10
Method Volatile Organics SW6260B
Test Code 626SSAOO
Initial Calibration # MSDC960922000000
Calibration Date =0~9~/~2~2~/~9~6~~~~
Sequence/Analysis Time
1 10/02/98 12:46:00
2 10/02/96 13:14:00
3 10/02/98 13:14:00
4 10/02/96 13:41:00
5 10/02/98 14:08:00
6 10/02/98 14:35:00
7 10/02/98 15:02:00
8 10/02/98 15:30:00
9 10/02/96 15:56:00
10 10/02/98 16:26:00
11 10/02/98 16:53:00
12 10/02/96 17:22:00
13 10/02/96 17.:50:00
14 10/02/98 18:17:00
15 10/02/96 18:45:00
16 10/02/98 19:13:00
n 10/02/98 19:40:00
18 10/02/98 20:08:00
19 10/02/98 20:36:00·
20 10/02/98 21:03:00
21 10/02/98 21:31:00
22 10/02/98 21:59:00
23 10/02/98 22:26:00
24 10/02/98 22:53:00
25 10/02/98 23:21:00
26 10/02/98 23:49:00
27 10/03/98 00:16:00
28 10/03/98 00:44:00
29 10/03/98 00:44:00
30 10/03/98 01:11:00
ANALYSIS BAT.SUMMARY
Analysis Batch # MSMSDC61002131401
Analysis Start Date/Time 10/02/98 13:14:00
Analysis Stop Date/Time 10/03/98 04:22:00
Work Order # 9609501
Page .2_L
Instrument ~
Analyst !'::1!IB
Reviewer ~A-P=S~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File #
SB Blank, System Cl002626
BFB GC/MS tune files Cl002629
VSTDCAL Continuing Calibration Verification Cl002629
LCS984630 Lab Control Sample Cl002830
LCSD964631 Lab Control Sample Duplicate Cl002631
BLK963176 Blank, Method Cl002632
0998HBWF23B 9609501-0lA Sample Cl002633
0998HBWF23A 9609501-02A Sample Cl002634
0996HBWF22A 9809501-03A Sample Cl002635
0996HBWF22B 9609501-04A Sample Cl002636
0998HBWP01A 9809501-05A Sample Cl002637
0996HBWP01B 9609501-06A Sample Cl002638
0996HBWP03A 9809501-07A Sample Cl002839
0998HBWP03B 9609501-06A Sample Cl002840
0998HBWP05A 9609501-09A Sample Cl002641
0996HBWP05B 9809501-lOA Sample Cl002842
9809517-0lA Sample Cl002843
9809517-02A Sample Cl002844
9809517-03A Sample Cl002645
9809517-04A Matrix Spike Cl002846
9809517-05A Matrix Spike Duplicate Cl002847
9809517-06A. sample Cl002848
9809517-07A Sample Cl002849
9809517-08A Sample Cl002850
9809579-0lA Sample Cl002S51
9809579-02A Sample Cl002852
9809579-03A Sample Cl002853
BFB GC/MS tune files Cl002854
VS TD CAL Continuing Calibration Verification Cl002854
0998HBWF23A 9809501-02A Sample Cl002855
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-de
•
0998HBWPOSA
9809501-09A
Cl002841
09/21/98 16:15
00:00:00
10/02/98 18:45:00
l
Solid
ug/kg
dry weight
Cone. DL
Recovery
%
88
112
96
R B S ULT S S UM MAR Y (Cont'd)
0998HBWP05B
9809501-lOA
Cl002842
09/21/98 16:20
00:00:00
10/02/98 19:13:00
l
Solid
ug/kg
dry weight
Cone. DL
Recovery
%
93
109
96
•
Cone. DL
Rec'overy
%
Work Order # 9809501
Page 1Q_
Cone. DL
Recovery
%
•
• 10/07/98 09:09:10
Method Volatile Organics SW8260B
Lab Sainple ID
File ID
9809501-02A
C1002834
9809501-04A
Cl002836
9809501-04A
C1002836
9809501-05A
C1002837
9809501-0?A
C1002B39 ·
9809501-08A
Cl002840
9809501-09A
C1002841
Project Sample
ID/Description
0998HBWF23A
0998HBWF22B
0998HBWF228
0998HBWPOlA
0998HBWP03A
0998HBWP03B
0998HBWP05A
Specification#
Analyte
Several
2-Hexanone
Tetrahydrofuran
Several
C12DCE, TCE, lllTCA
C12DCE, lllTCA
1,1,1-Trichloroethane
ANALYTICAL .TOCO"L SUMMARY
COMMENTS/NARRATIVE
Flag Comment/Narrative
R
F
F
R
z
z
z
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results but only
at a higher dilution since some target
analytes are outside of the range of
calibration.
The F flag indicates that the concentration
for 2-hexanone may be. biased
due to interference by a non-target
analyte.
The F flag indicates that the concentration
for THF may be biased
due to interference by a non-target
analyte.
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results.
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL.
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL.
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL.
Work
Corrective Action
Order .9501
Pagel}_
10/07/98 09:09:10
Method Volatile Organics SW8260B
Test Code 826SSAOO
Initial Calibration U MSDC980922000000
Calibration Date -0~9~/2~2~/~9~8~~~~-
Sequence/Analysis Time
31 10/03/98 01:39:00
32 10/03/98 02:07:00
33 10/03/98 02:35:00
34 10/03/98 03:01:00
35 10/03/98 03:28:00
36 10/03/98 03:56:00
37 10/03/98 04:22:00
•
AH AL Y S I S B AT CH S UM MARY (cont'd)
Analysis Batch # MSMSDC81002131401
Analysis Start Date/Time 10/02/98 13:14:00
Analysis Stop Date/Time 10/03/98 04:22:00
Project Sample ID Lab Sample ID Sample Type
0998HBWF22A 9809501-03A Sample
0998HBWP01A 9809501-05A Sample
0998HBWP01B 9809501-06A Sample
BLK983177 Blank, Method
0998HBWF23B 9809501-0lA Sample
0998HBWF22B 9809501-04A Sample
9809581-0lA Sample
•
Work Order # 9809501
Page E_
Instrument !:12.Q£__
Analyst !1fill:
Reviewer _A_P_s~~~~~~~~
Analysis·File #
Cl002856
Cl002857
Cl002858
Cl002859
Cl002860
Cl002861
Cl002862
•
10/07/98 09:09:10
Method Volatile Organics SW8260B
Lab Sample ID
File ID
9809501-lOA
Cl002842
•
Project Sample
ID/Description
0998HBWP05B
Specif ication!I
Analyte
1,1,1-Trichloroethane
ANALYTICAL PROTOCOL SUMMARY
C 0 MM B HTS / HARR AT IV B (Cont'd}
Flag Comment/Narrative
z The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL .
•
Corrective Action
Work Order II 9809501
Page 11_
•
• 10/05/98 16:49:28 WORK ORDBR • C 0 M M B II T S Work Order # 9809.
Page _2_
io/05/98 16:49:28
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _....:.:R.;;a.;;d~ia~n::-I~n~t-..e~r~n~a~t~i~o~n~a~l~,-=L=L~C­
By _ _.1""4"'"04"'"6"-"S-..u"'m"'m"'i"'t~D'""r'"'.-''-"'B"'l"'d'"q"'". _B;;;...
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWF23B
0998HBWF23A
0998HBWF22A
0998HBWF22B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWP05A
0998HBWP05B
•
ID/
NOR~ OKDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID VOLATILES
Case# :.:N""A"----------
SDG # ~N~A--------­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA GASSSAGU
SHAREXOO
02A GASSSAGU
SHAREXOO
03A GASSSAGU
SHAREXOO
04A GASSSAGU
SHAREXOO
05A GASSSAGU
SHAREXOO
06A GASSSAGU
SHAREXOO
07A GASSSAGU
SHAREXOO
OBA GASSSAGU
SHAREXOO
09A GASSSAGU
SHAREXOO
lOA GASSSAGU
SHAREXOO
•
Work Order # 9809502
Page .!..__
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Sp'lit, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split,VO~/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BT.EX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
Gas/BTEX by Purge&Trap GC
Shared Split, VOA/Other Lab
•
• • 10/05/98 16:49:28 ANALYTICAL PROTOCOL SUMMARY
FLAG DBFIBITIONS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
NA Analyte concentration not available for this analysis.
NC RPD and/or % Recovery not calculated. See Narrative for explanation.
ND Not detected. No instrument response for analyte or result less than zero.
NR Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
NS Analyte not spiked.
A Presence o! hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order # 9809502
Page L •
10/05/98 16:49:28
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATB C B R T I F I C A T I 0 Iii S
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9809502
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• 10/05/98 16:49:28
Method Gas/BTEX by Purqe&Trap GC
Test Code GASSSAGU
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Gasoline
Unidentified organics
Surrogate{s)
Chlorobenzene
0998HBWF22A
9809502-03A
12093016
09/21/98
10/01/98 05:05:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
2300 BX
Recovery
\
108
DL
1270
• RESULTS SUMMARY
0998HBWF22B
9809502-04A
12093017
09/21/98
10/01/98 06:00:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
8780 BX
Recovery
\
107
DL
1320
0998HBWF23A
9809502-02A
I2093015
09/21/98
10/01/98 04:09:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
1140 B
Recovery
%
107
DL
1310
Work Order # 9809502
Page _6_
0998HBWF23B
9809502-0lA
12093014
09/21/98
10/01/98 03:14:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
3730 BX
Recovery
%
106
DL
1340
•
10/05/98 16:49:28
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method Gas/BTEX by Purge&Trap GC
Project Sample ID/Description
0998HBWF22A
0998HBWF22B
0998HBWF23A
0998HBWF23B
0998HBWP01A
0998HBWP01B
0998HBWP03A
0998HBWP03B
0998HBWPOSA
0998HBWP05B
•
ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9809502-03A GASSSAGU NA
9809502-04A GASSSAGU NA
9809502-02A GASSSAGU NA
9809502-0lA GASSSAGU NA
9809502-05A GASSSAGU NA
9809502-06A GASSSAGU NA
9809502-07A GASSSAGU NA
9809502-08A GASSSAGU NA
9809502-09A GASSSAGU NA
9809502-lOA GASSSAGU NA
•
Work Order # 9809502
Page _5_
Analysis Batch n
GCIDA28093015130l
GCIDA280930151301
GCIDA28093015130l
GCIDA280930151301
GCIDA280930151301
GCIDA280930151301
GCIDA280930151301
GCIDA280930151301
GCIDA280930151301
GCIDA280930151301
•
• 10/05/98 16:49:28
Method Gas/BTEX by Purqe&Trap GC
Test Code GASSSAGU
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Gasoline
Unidentified organics
Surrogate(s}
Chlorobenzene
0998HBWPOSA
9809502-09A
I2093027
09/21/98
10/01/98 18:34:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone. DL
ND 1230
942 B
Recovery
%
107
RRSULTS S.ARY
0998HBWPOSB
9809502-lOA
12093028
09/21/98
10/01/98 19:30:00
so
Solid
ug/kg
dry weight
PRIMARY
Cone. DL
ND 1250
849 B
Recovery
%
104
(Cont'd)
Cone. DL
Recovery
%
Work Order # 9809502
Page _8_
Cone. DL
Recovery
%
•
10/05/98 16:49:28
Method Gas/BTEX by Purqe&Trap GC
Test Code GASSSAGU
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Gasoline
Unidentified organics
Surrogate(s)
Chlorobenzene
••
0998HBWP01A
9809502-05A
I2093023
09/21/98
10/01/98 14:56:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
489 B
Recovery
%
109
DL
1290
R KS ULT S SUMMAR. Y '(Cont'd)
0998HBWP01B
9809502-0GA
I2093024
09/21/98
10/01/98 15:50:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
490 B
Recovery
%
103
DL
1410
0998HBWP03A
9809502-07A
I2093025
09/21/98
10/01/98 16:44:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone.
ND
360 B
Recovery
%
107
DL
1270
Work Order # 9809502
Page _7_
0998HBWP03B
9809502-08A
!2093026
09/21/98
10/01/98 17:39:00
50
Solid
ug/kg
dry weight
PRIMARY
Cone. DL
ND
415 B
1350
Recovery
%
110
•
\
l0/05/98 16:49:28
Method Gas/BTEX by Purqe&Trap GC
Test Code GASSWABG
Initial Calibration # IDA2980526070001
Calibration Date ~0-=5L/-=2~6~/~9~8-~-~
Sequence/Analysis Time
1 09/30/98 15:13:00
2 09/30/98 16:18:00
3 09/30/98 17:13:00
4 09/30/98 18:07:00
5 09/30/98 19:01:00
6 09/30/98 19:55:00
7 09/30/98 20:49:00
8 09/30/98 21:44:00
9 09/30/98 22:39:00
10 09/30/98 23:35:00
11 10/01/98 00:29:00
12 10/01/98 01:24:00
13 10/01/98 02:19:00
14 10/01/98 03:14:00
15 10/01/98 04:09:00
16 10/01/98 05:05:00
17 10/01/98 06:00:00
18 10/01/98 06:55:00
19 10/01/98 11:16:00
20 10/01/98 12:12:00
21 10/01/98 13:06:00
22 10/01/98 14:01:00
23 10/01/98 14:56:00
24 10/01/98 15:50:00
25 10/01/98 16:44:00
26 10/01/98 17:39:00
27 10/01/98 18:34:00
28 10/01/98 19:30:00
29 10/01/98 20:28:00
30 10/01/98 21:24:00
•
AllALYSIS BATCH SUMMARY
Analysis Batch # GCIDA280930151301
Analysis Start Date/Time 09/30/98 15:13:00
Analysis Stop Date/Time 10/01/98 21:24:00
Work Order # 9809502
Page _9 _
Instrument ~
Analyst 1tIB
Reviewer "'J-=S-=E'---------
Project Sample ID Lab Sample ID Sample Type Analysis File II
CCVG Continuing Calibration Verification I2092922
BLK983360 Blank, Method I2093002
LCSG985129 Lab Control Sample I CCV I2093003
BLK983361 Blank, Method I2093004
9809518-02A Sample 12093005
9809518-03A Sample I2093006
9809518-06A Sample I2093007
9809518-07A Sample I2093008
9809518-08A Sample I2093009
9809518-09A Sample I2093010
CCVG Continuing Calibration Verification I2093011
SB Sample I2093012
CCVG Continuing Calibration Verification I2093013
0998HBWF23B 9809502-0lA Sample I2093014
0998HBWF23A 9809502-02A Sample I2093015
0998HBWF22A 9809502-03A Sample I2093016
0998HBWF22B 9809502-04A Sample I2093017
SB Sample I2093018
CCVG Continuing Calibration Verification I2093019
9809518-04A Matrix Spike I2093020
9809518-05A Matrix Spike Duplicate I2093021
9809518-0lA. Sample I2093022
0998HBWP01A 9809502-05A Sample I2093023
0998HBWP01B 9809502-06A Sample I2093024
0998HBWP03A 9809502-07A Sample I2093025
0998HBWP03B 9809502-08A Sample I2093026
0998HBWP05A 9809502-09A Sample 12093027
0998HBWP05B 9809502-lOA Sample I2093028
CCVG Continuing Calibration Verification 12093029
CCVG Continuing Calibration Verification I2093030
• •
• 09/25/98 15:10:52
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _.:;R;=:a;=:d:.:i"'a"'n'-"I"'n"'t"'e"'r"'n"'a"'t~i:.::o"'n"'a'"'°l'-''-"L"'L""C'-­
By _ _:l..:4..::0..:4..::6c...::S"'u"'m"'m"'i"'t'--"D"'r'""'.-''-=B'-"l"'d:::gi..:·-=B'--
P. o. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
0998HBWP04B
0998HBWP04A
0998HBWP02A
099.8HBWP02B
0998HBWP06B
0998HBWP06A
ID/
-
• WORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case # ~N~A'---------­
SDG # ~N~A'------~~-­
RAS # 80903AJAL
Lab Sample ID Test Code (s)
OlA MSRSSAOO
02A MSRSSAOO
03A MSRSSAOO
04A MSRSSAOO
05A MSRSSAOO
06A MSRSSAOO
07A DUP MSRSSAOO
Percent
Percent
Percent
Percent
Percent
Percent
Percent
Work Order # 9809511
Page _1_
RCN 6501.38.0602
New York ELAP ID #: 1091.5
Method Desciption
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
Moisture SW846
•