8603_SurryCountyElkin_GWMR_DIN28072_20151105

Surry County Closed C&D and Closed MSWLF, Elkin
Elkin, North Carolina
November 2015
Permit Number: 86-03
Semi-Annual Water Quality Monitoring Report
Prepared for
PO Box 97
Garner, NC 27529
License No, C-0281
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G15025.0
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Groundwater Samples Page 2
Surface Water Samples Page 2
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 3
FIGURES
Topographic Map with Site Location Figure 1
Single-Day Potentiometric Map of Uppermost Aquifer Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above Established SWSL, GWP, 2L, 2B or MCL (Appendix I) Table 5
Hydrologic Properties at Monitoring Well Locations Table 6
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
July 11, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Elkin
Permit No. 86-03
MESCO Project No. G15025.0
Event Date(s): November 5, 2015
Dear Ms. Drummond;
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the fall 2015 event performed at the Surry County closed construction and
demolition (C&D) and closed municipal solid waste landfill (MSWLF). NCDEQ Solid Waste Rules 15A NCAC
13B.1632 requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents
the quality of the ground and surface waters during this monitoring event performed on November 5, 2015.
Laboratory analytical results indicate volatile organic compounds (VOCs) persist within five wells that monitor the
uppermost aquifer. The surface water samples collected from the discharge feature remain unimpacted.
Background
The Surry County closed C&D and MSWLF, permit #86-03, is located at Elkin Landfill Road (SR 1191), Elkin,
Surry County, North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to
operating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two units. The first
area was closed prior to October 1991 with a 24 inch final soil cover. The second area was closed with a cohesive
cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec, and 18 inches of erosive layer
prior to December 31, 1998 in accordance with the Transition Plan. C&D was placed on top of the cohesive capped
unit until 2008.
This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and
as a condition of the post-closure portion of the permit to operate. Water quality at this facility has been monitored
at least semi-annually since 1989 with historical data available since 1994. The SWS approved a modification to the
assessment monitoring program on October 15, 2014 (DIN:21983) which entails a subset of wells be sampled for
Appendix II parameters once every three years with the next event scheduled for October 2017.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums, this report contains sampling procedures, field and laboratory results, ground/surface water
characterization, and findings. Well construction summary table, field observations table, field parameter data table,
sampling and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates
table, potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed
herein.

Sampling Procedure
MESCO personnel performed this sampling event utilizing portable monitoring methodology in accordance with the
site-specific Sampling and Analysis Plan (SAP) and the NCDENR SWS guidance document Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. Water samples were collected
from nine downgradient groundwater monitoring wells (MW-2, MW-3, MW-3A, MW-4, MW-5, MW-6, MW-7S,
MW-7D and MW-8), one background well (MW-1), and two surface water points (SW-1 and SW-2). Monitoring
locations are shown on the single-day potentiometric map (Figure 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and integrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of
three times the volume of standing water in the well or until dry. Surface water samples were collected from Snow
Creek discharge feature at previously designated locations. During well purging and surface water sample collection the required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-
preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported
to a NC-certified laboratory under proper chain of custody (C-O-C) protocols within the specified hold times for
each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, specific conductance,
temperature and visual turbidity. A summary of the field parameter data is presented in Table 3 and the field
sampling data sheet is enclosed in Appendix B.
Laboratory Results
All water samples were analyzed for the Appendix I list of VOCs and total unfiltered metals listed in 40 CFR 258.
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the laboratory analysis. A
sampling and analysis table summarizing the locations, constituents, and methods is presented as Table 4.
Laboratory results and C-O-Cs are presented in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a Class C
water body or Maximum Contaminant Levels (MCL) also recognized as “Federal Primary Drinking Water
Standards”.
Groundwater Samples
The only inorganic constituent detected in excess of its respective 2L Standard (2 µg/L) was total cadmium (5.5
µg/L) in sample MW-3.
One or more Appendix I VOC(s) were detected in quantifiable concentrations above their respective 2L Standards
in samples collected from MW-2, MW-3, MW-3A, MW-6 and MW-8.
Surface Water Samples
Target constituent(s) were not detected in either surface water sample in concentrations exceeding the applicable 2B
Standard.
Groundwater and Surface Water Characterization
A single-day potentiometric map constructed from groundwater levels collected during this event is presented as
Figure 2. Groundwater flow rates and directions were calculated and are included in Table 6. Groundwater flows generally southwest, towards the Snow Creek discharge feature. Groundwater average linear velocity rates
calculated from modified Darcy's equation indicate flow rates ranged from approximately 14 ft/yr (MW-3A) to 795
ft/yr (MW-6). Groundwater average linear velocity rates averaged approximately 211 ft/yr in MW-1 which the
construction records indicate monitors the regolith aquifer and 239 ft./yr. in the wells screened in the upper bedrock.
Snow Creek, monitored at SW-1 and SW-2, was visually observed to have a low gage height, low volume and low turbidity.
2
Figures
Topographic Map with Site Location
Surry County Closed MSW/C&D Landfill - Elkin
FIGURE 1
QUADRANGLE LEGEND
1” = 2000'
Landfill Road (Off Joe Mill Ln SR 1121)
Elkin, NC 28621
Lat:36-17-49.4007
Long:-80-46-20.6499
Northing:931704.33
Easting:1477683.95
Tables
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
November 5, 2015
Latitude Longitude
(inches)(ft)
MW-1 11/28/89 4 74.56 64.56 10 Soil 1042 1041 988 56.57 36.29711 -80.77236
MW-2 11/08/89 4 79 69 10 Soil 948 947 891 58.11 36.29572 -80.77620
MW-3 11/28/89 4 63 53 10 Soil 932 931 882 51.25 36.29362 -80.77646
MW-3A 09/16/94 2 40 24 16 Fractured Rock 927 924 895 32.21 36.29457 -80.77675
MW-4 09/15/94 2 29 13 16 Fractured Rock 933 929 921 11.97 36.29379 -80.77528
MW-5 09/15/94 2 31 16 15 Fractured Rock 949 845 937 11.90 36.29450 -80.77456
MW-6 09/15/94 2 66 51 15 Fractured Rock 1005 1002 956 50.90 36.29780 -80.77270
MW-7S 06/05/01 2 24 9 15 Fractured Rock 901 889 890 11.03 36.29407 80.77730
MW-7D 06/05/01 2 90 80 10 Fractured Rock 901 889 894 5.51 36.29407 80.77730
MW-8 06/04/01 2 67 52 15 Fractured Rock 1015 1013 975 41.39 36.29739 -80.77246
NOTE:
Monitoring Well Date Installed
Well Diameter
Total Well Depth
Top of Screen Depth
Screen Length Geology of Screened Interval
Top of Casing Elevation
Ground Elevation Groundwater Elevation Depth to Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 2
Table 5
Detections in Water Samples above SWSL, GWP, 2L, 2B or MCL (Appendix I)
November 5, 2015
Result Unit
MW-1 Zinc, total 11/05/15 19.2 5 10 1000 5000
MW-1 Cadmium, total 11/05/15 1.2 0.5 1 2 5
MW-2 11/05/15 17.6 0.33 1 6 75 L &/or LFG
MW-2 11/05/15 0.97J 0.24 1 0.4 5 L &/or LFG
MW-2 Benzene 11/05/15 2.9 0.25 1 1 5 L &/or LFG
MW-2 11/05/15 1.3 0.27 1 0.6 5 L &/or LFG
MW-2 11/05/15 12 0.23 3 50 100
MW-2 Barium, total 11/05/15 318 2.5 100 700 1300
MW-2 11/05/15 9 0.3 5 20 Ne
MW-2 Zinc, total 11/05/15 10.4 5 10 1000 5000
MW-2 Antimony, total 11/05/15 4.1J 3.8 6 NE 1 NE
MW-2 Vanadium, total 11/05/15 9.7J 2.5 25 NE 0.3 NE
MW-3 Benzene 11/05/15 2.9 0.25 1 1 5 L &/or LFG
MW-3 Vinyl chloride 11/05/15 1.4 0.62 1 0.03 2 L &/or LFG
MW-3 11/05/15 4.2 0.47 1 3 5 L &/or LFG
MW-3 Cadmium, total 11/05/15 5.5 0.5 1 2 5 N
MW-3 Nickel, total 11/05/15 74.7 2.5 50 100 NE
MW-3 11/05/15 25.9 0.19 5 70 70
MW-3 Barium, total 11/05/15 108 2.5 100 700 1300
MW-3 11/05/15 4.9 0.33 1 6 75
MW-3A 11/05/15 0.44J 0.24 1 0.4 5 L &/or LFG
MW-3A Vinyl chloride 11/05/15 1.5 0.62 1 0.03 2 L &/or LFG
MW-3A 11/05/15 12.7 0.33 1 6 75 L &/or LFG
MW-3A 11/05/15 17.5 0.19 5 70 70
MW-3A Vanadium, total 11/05/15 6.4J 2.5 25 NE 0.3 NE
MW-3A Nickel, total 11/05/15 58.6 2.5 50 100 NE
MW-3A Barium, total 11/05/15 566 2.5 100 700 1300
MW-3A 11/05/15 3.1 0.23 3 50 100
MW-3A Cobalt, total 11/05/15 72.8 2.5 10 NE 1 NE
MW-3A Zinc, total 11/05/15 15.5 5 10 1000 5000
MW-4 Zinc, total 11/05/15 11.9 5 10 1000 5000
MW-4 Cadmium, total 11/05/15 1.3 0.5 1 2 5
MW-6 Vinyl chloride 11/05/15 1.4 0.62 1 0.03 2 L &/or LFG
MW-6 11/05/15 3.4 0.33 1 6 75
MW-6 11/05/15 6.6 0.23 3 50 100
MW-6 Cobalt, total 11/05/15 12.6 2.5 10 NE 1 NE
MW-7D Zinc, total 11/05/15 11.2 5 10 1000 5000
MW-7S 11/05/15 12 0.19 5 70 70
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
ug/L
ug/L
1,4-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
ug/L
1,2-Dichloropropane ug/L
Chlorobenzene ug/L
ug/L
1,2-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Trichloroethene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
1,4-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
Chlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Surry County Closed C&D and Closed MSWLF, Elkin Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
MW-8 Benzene 11/05/15 1.6 0.25 1 1 5 L &/or LFG
MW-8 11/05/15 1.5 0.47 1 3 5
MW-8 11/05/15 2 0.33 1 6 75
MW-8 11/05/15 14 0.19 5 70 70
SW-1 Zinc, total 11/05/15 13.5 5 10 50 5000
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to SWS reporting instructions
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
ug/L
Trichloroethene ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard (NC SWS adopted)
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 2
Field Observations of Monitoring Locations
November 5, 2015
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes 4” Diameter
MW-2 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge, hasp cracked
MW-3 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge
MW-3A Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-6 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-7S Yes Yes Yes Yes Yes Yes
MW-7D Yes Yes Yes Yes Yes Yes
MW-8 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----Low gage & low flow
SW-2 Yes -----Low gage & low flow
Any unusual field conditions, observations, or events:
Facility no longer in operation or occupied since transfer station closed in ~ June 2010.
All paths leading to monitoring locations well maintained by County.
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears to
be Effective
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 3
Field Parameter Data Summary
November 5, 2015
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L %/Vol Visual
MW-1 56.57 985 1042 17.1 NR NR 5.93 110 50 NR Clear
MW-2 58.11 890 948 15.7 NR NR 6.41 1710 850 NR Slight
MW-3 51.25 881 932 14.8 NR NR 5.97 490 220 NR Clear
MW-3A 32.21 894 927 15.1 NR NR 6.51 1210 600 NR Clear
MW-4 11.97 921 933 13.8 NR NR 6.35 60 20 NR Clear
MW-5 11.90 937 949 15.1 NR NR 6.51 30 10 NR Clear
MW-6 50.90 954 1005 15.3 NR NR 5.99 60 20 NR Clear
MW-7S 11.03 890 901 15.4 NR NR 6.53 460 210 NR Clear
MW-7D 5.51 884 901 15.1 NR NR 10.01 310 150 NR Clear
MW-8 41.39 973 1015 14.9 NR NR 5.91 210 140 NR Clear
Minimum 5.51 881 901 13.8 NR NR 5.91 30 10 NR Clear
Average 33.08 921 955 15.2 NR NR 6.61 465 227 NR Clear
Maximum 58.11 985 1042 17.1 NR NR 10.01 1710 850 NR Slight
SW-1 ---12.3 NR NR 7.11 100 40 -Clear
SW-2 ---11.9 NR NR 7.03 100 40 -Clear
Minimum ---11.9 NR NR 7.03 100 40 -Clear
Average ---12.1 NR NR 7.07 100 40 -Clear
Maximum ---12.3 NR NR 7.11 100 40 -Clear
NR = No Reading attempted
* = Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
Depth to
Water
Water
Elevation*
TOC
Elevation*
Specific
Conductance
Methane Gas in
Well Headspace
Turbidity of
Metals Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
btoc = below top of casing
amsl = above mean sea level
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 4
Sampling and Analysis Summary
November 5, 2015
Field Parameter
To
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pH Tu
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8
2
6
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M
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Fi
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V
i
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MW-1 x x x x x x x
MW-2 x x x x x x x
MW-3 x x x x x x x
MW-3A x x x x x x x
MW-4 x x x x x x x
MW-5 x x x x x x x
MW-6 x x x x x x x
MW-7S x x x x x x x
MW-7D x x x x x x x
MW-8 x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
All wells listed on SAP presented
App. I
VO
C
s

App I & II = List from current 40 CFR 258
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 2
Table 5
Detections in Water Samples above SWSL, GWP, 2L, 2B or MCL (Appendix I)
November 5, 2015
Result Unit
MW-1 Zinc, total 11/05/15 19.2 5 10 1000 5000
MW-1 Cadmium, total 11/05/15 1.2 0.5 1 2 5
MW-2 11/05/15 17.6 0.33 1 6 75 L &/or LFG
MW-2 11/05/15 0.97J 0.24 1 0.4 5 L &/or LFG
MW-2 Benzene 11/05/15 2.9 0.25 1 1 5 L &/or LFG
MW-2 11/05/15 1.3 0.27 1 0.6 5 L &/or LFG
MW-2 11/05/15 12 0.23 3 50 100
MW-2 Barium, total 11/05/15 318 2.5 100 700 1300
MW-2 11/05/15 9 0.3 5 20 Ne
MW-2 Zinc, total 11/05/15 10.4 5 10 1000 5000
MW-2 Antimony, total 11/05/15 4.1J 3.8 6 NE 1 NE
MW-2 Vanadium, total 11/05/15 9.7J 2.5 25 NE 0.3 NE
MW-3 Benzene 11/05/15 2.9 0.25 1 1 5 L &/or LFG
MW-3 Vinyl chloride 11/05/15 1.4 0.62 1 0.03 2 L &/or LFG
MW-3 11/05/15 4.2 0.47 1 3 5 L &/or LFG
MW-3 Cadmium, total 11/05/15 5.5 0.5 1 2 5 N
MW-3 Nickel, total 11/05/15 74.7 2.5 50 100 NE
MW-3 11/05/15 25.9 0.19 5 70 70
MW-3 Barium, total 11/05/15 108 2.5 100 700 1300
MW-3 11/05/15 4.9 0.33 1 6 75
MW-3A 11/05/15 0.44J 0.24 1 0.4 5 L &/or LFG
MW-3A Vinyl chloride 11/05/15 1.5 0.62 1 0.03 2 L &/or LFG
MW-3A 11/05/15 12.7 0.33 1 6 75 L &/or LFG
MW-3A 11/05/15 17.5 0.19 5 70 70
MW-3A Vanadium, total 11/05/15 6.4J 2.5 25 NE 0.3 NE
MW-3A Nickel, total 11/05/15 58.6 2.5 50 100 NE
MW-3A Barium, total 11/05/15 566 2.5 100 700 1300
MW-3A 11/05/15 3.1 0.23 3 50 100
MW-3A Cobalt, total 11/05/15 72.8 2.5 10 NE 1 NE
MW-3A Zinc, total 11/05/15 15.5 5 10 1000 5000
MW-4 Zinc, total 11/05/15 11.9 5 10 1000 5000
MW-4 Cadmium, total 11/05/15 1.3 0.5 1 2 5
MW-6 Vinyl chloride 11/05/15 1.4 0.62 1 0.03 2 L &/or LFG
MW-6 11/05/15 3.4 0.33 1 6 75
MW-6 11/05/15 6.6 0.23 3 50 100
MW-6 Cobalt, total 11/05/15 12.6 2.5 10 NE 1 NE
MW-7D Zinc, total 11/05/15 11.2 5 10 1000 5000
MW-7S 11/05/15 12 0.19 5 70 70
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
ug/L
ug/L
1,4-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
ug/L
1,2-Dichloropropane ug/L
Chlorobenzene ug/L
ug/L
1,2-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Trichloroethene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
ug/L
1,4-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
Chlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Surry County Closed C&D and Closed MSWLF, Elkin Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
MW-8 Benzene 11/05/15 1.6 0.25 1 1 5 L &/or LFG
MW-8 Trichloroethene 11/05/15 1.5 ug/L 0.47 1 3 5
MW-8 1,4-Dichlorobenzene 11/05/15 2 ug/L 0.33 1 6 75
MW-8 cis-1,2-Dichloroethene 11/05/15 14 ug/L 0.19 5 70 70
SW-1 Zinc, total 11/05/15 13.5 ug/L 5 10 50 5000
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to SWS reporting instructions
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard (NC SWS adopted)
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 6
November 5, 2015
(cm/second)(%)(feet/feet)(feet/year)
MW-1 9.90E-05 5 0.103 211 S52W 56.57 985 Clay
MW-2 2.00E-05 5 58.11 890**Clay
MW-3 5.00E-05 5 51.25 881**Clay
Minimum 2.70E-04 5 0.103 211 -51.25 882 -
Average 3.45E-04 5 0.103 211 -55.31 920 -
Maximum 4.20E-04 5 0.103 211 -58.11 891 -
MW-3A 2.50E-05 5 0.027 14 N53W 32.21 894 Fractured Rock
MW-4 4.20E-04 5 0.008 72 N79W 11.97 921 Fractured Rock
MW-5 2.70E-04 5 0.007 41 N87W 11.90 937 Fractured Rock
MW-6 1.20E-04 5 0.320 795 N12W 50.90 954 Fractured Rock
MW-7S 2.30E-04 5 0.091 433 S81W 11.03 890 Fractured Rock
MW-7D 5.51 895**Fractured Rock
MW-8 2.40E-05 5 0.161 80 N28W 41.39 973 Fractured Rock
Minimum 2.40E-05 5 0.007 14 -5.51 890 -
Average 1.82E-04 5 0.102 239 -23.56 924 -
Maximum 4.20E-04 5 0.320 795 -50.90 973 -
NOTE: Note: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
* = Elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
** = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average Linear
Velocity Rate
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation*
Screened Interval
Lithology
(ft btoc)(ft amsl)
na na na
na na na
na na na na na
Hydrologic gradient calculated from groundwater elevations recorded November 5, 2015.
Average Linear Velocity Rate (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e
-=
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
November 21, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92275192
92275192
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
SURRY CO. CLOSED MSWLF-ELKIN
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 06, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 41
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 41
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID Matrix Date Collected Date Received
92275192001 MW-1 Water 11/05/15 17:30 11/06/15 07:45
92275192002 MW-2 Water 11/05/15 15:15 11/06/15 07:45
92275192003 MW-3 Water 11/05/15 14:10 11/06/15 07:45
92275192004 MW-3A Water 11/05/15 13:15 11/06/15 07:45
92275192005 MW-4 Water 11/05/15 11:00 11/06/15 07:45
92275192006 MW-5 Water 11/05/15 11:30 11/06/15 07:45
92275192007 MW-6 Water 11/05/15 10:00 11/06/15 07:45
92275192008 MW-7S Water 11/05/15 16:10 11/06/15 07:45
92275192009 MW-7D Water 11/05/15 16:35 11/06/15 07:45
92275192010 MW-8 Water 11/05/15 17:00 11/06/15 07:45
92275192011 SW-1 Water 11/05/15 12:00 11/06/15 07:45
92275192012 SW-2 Water 11/05/15 11:45 11/06/15 07:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 3 of 41
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92275192001 MW-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192002 MW-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192003 MW-3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192004 MW-3A EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192005 MW-4 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192006 MW-5 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192007 MW-6 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192008 MW-7S EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192009 MW-7D EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192010 MW-8 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192011 SW-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
92275192012 SW-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CNB
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 4 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-1 Lab ID:92275192001 Collected:11/05/15 17:30 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:30 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:30 7440-38-211/10/15 20:0010.0 2.5 1
Barium 25.8J ug/L 11/11/15 18:30 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:30 7440-41-711/10/15 20:001.0 0.50 1
Cadmium 1.2 ug/L 11/11/15 18:30 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:30 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 18:30 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:30 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:30 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 18:30 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:30 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:30 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:30 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 18:30 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 19.2 ug/L 11/11/15 18:30 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 03:50 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 03:50 107-13-12001.9 1
Benzene ND ug/L 11/09/15 03:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 03:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 03:50 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 03:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 03:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 03:50 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 03:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 03:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 03:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 03:50 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 03:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 03:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 03:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 03:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 03:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 03:50 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 03:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/09/15 03:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 03:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 03:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 03:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 03:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.91J ug/L 11/09/15 03:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 03:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 03:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 03:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 03:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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Huntersville, NC 28078
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Page 5 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-1 Lab ID:92275192001 Collected:11/05/15 17:30 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 03:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 03:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 03:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 03:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 03:50 108-10-11000.33 1
Styrene ND ug/L 11/09/15 03:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 03:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 03:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 03:50 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 03:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 03:50 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 03:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 03:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 03:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 03:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 03:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 03:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 03:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %11/09/15 03:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %11/09/15 03:50 17060-07-070-130 1
Toluene-d8 (S)100 %11/09/15 03:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 6 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-2 Lab ID:92275192002 Collected:11/05/15 15:15 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony 4.1J ug/L 11/11/15 18:33 7440-36-011/10/15 20:006.0 3.8 1
Arsenic 5.6J ug/L 11/11/15 18:33 7440-38-211/10/15 20:0010.0 2.5 1
Barium 318 ug/L 11/11/15 18:33 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:33 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 18:33 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:33 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt 9.6J ug/L 11/11/15 18:33 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:33 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:33 7439-92-111/10/15 20:0010.0 2.5 1
Nickel 13.6J ug/L 11/11/15 18:33 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:33 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:33 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:33 7440-28-011/10/15 20:005.5 5.0 1
Vanadium 9.7J ug/L 11/11/15 18:33 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 10.4 ug/L 11/11/15 18:33 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 18.1J ug/L 11/09/15 04:07 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 04:07 107-13-12001.9 1
Benzene 2.9 ug/L 11/09/15 04:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 04:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 04:07 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 04:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 04:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 04:07 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 04:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 04:07 56-23-51.0 0.25 1
Chlorobenzene 12.0 ug/L 11/09/15 04:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 04:07 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 04:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 04:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 04:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 04:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 04:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 04:07 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene 9.0 ug/L 11/09/15 04:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene 17.6 ug/L 11/09/15 04:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 04:07 110-57-61001.0 1
1,1-Dichloroethane 0.96J ug/L 11/09/15 04:07 75-34-35.0 0.32 1
1,2-Dichloroethane 0.97J ug/L 11/09/15 04:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 04:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/09/15 04:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 04:07 156-60-55.0 0.49 1
1,2-Dichloropropane 1.3 ug/L 11/09/15 04:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 04:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 04:07 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-2 Lab ID:92275192002 Collected:11/05/15 15:15 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 04:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 04:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 04:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 04:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 04:07 108-10-11000.33 1
Styrene ND ug/L 11/09/15 04:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 04:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 04:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 04:07 127-18-41.0 0.46 1
Toluene 0.39J ug/L 11/09/15 04:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 04:07 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 04:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 04:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 04:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 04:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 04:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 04:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 04:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %11/09/15 04:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)117 %11/09/15 04:07 17060-07-070-130 1
Toluene-d8 (S)100 %11/09/15 04:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3 Lab ID:92275192003 Collected:11/05/15 14:10 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:36 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:36 7440-38-211/10/15 20:0010.0 2.5 1
Barium 108 ug/L 11/11/15 18:36 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:36 7440-41-711/10/15 20:001.0 0.50 1
Cadmium 5.5 ug/L 11/11/15 18:36 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:36 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt 9.5J ug/L 11/11/15 18:36 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:36 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:36 7439-92-111/10/15 20:0010.0 2.5 1
Nickel 74.7 ug/L 11/11/15 18:36 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:36 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:36 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:36 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 18:36 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 8.7J ug/L 11/11/15 18:36 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 04:24 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 04:24 107-13-12001.9 1
Benzene 2.9 ug/L 11/09/15 04:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 04:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 04:24 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 04:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 04:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 04:24 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 04:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 04:24 56-23-51.0 0.25 1
Chlorobenzene 1.2J ug/L 11/09/15 04:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 04:24 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 04:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 04:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 04:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 04:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 04:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 04:24 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 04:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.9 ug/L 11/09/15 04:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 04:24 110-57-61001.0 1
1,1-Dichloroethane 0.99J ug/L 11/09/15 04:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 04:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 04:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 25.9 ug/L 11/09/15 04:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 04:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 04:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 04:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 04:24 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3 Lab ID:92275192003 Collected:11/05/15 14:10 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 04:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 04:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 04:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 04:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 04:24 108-10-11000.33 1
Styrene ND ug/L 11/09/15 04:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 04:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 04:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 04:24 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 04:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 04:24 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 04:24 79-00-51.0 0.29 1
Trichloroethene 4.2 ug/L 11/09/15 04:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 04:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 04:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 04:24 108-05-450.0 0.35 1
Vinyl chloride 1.4 ug/L 11/09/15 04:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 04:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %11/09/15 04:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %11/09/15 04:24 17060-07-070-130 1
Toluene-d8 (S)101 %11/09/15 04:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3A Lab ID:92275192004 Collected:11/05/15 13:15 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:39 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:39 7440-38-211/10/15 20:0010.0 2.5 1
Barium 566 ug/L 11/11/15 18:39 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:39 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 18:39 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:39 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt 72.8 ug/L 11/11/15 18:39 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:39 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:39 7439-92-111/10/15 20:0010.0 2.5 1
Nickel 58.6 ug/L 11/11/15 18:39 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:39 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:39 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:39 7440-28-011/10/15 20:005.5 5.0 1
Vanadium 6.4J ug/L 11/11/15 18:39 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 15.5 ug/L 11/11/15 18:39 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 04:42 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 04:42 107-13-12001.9 1
Benzene 0.62J ug/L 11/09/15 04:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 04:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 04:42 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 04:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 04:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 04:42 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 04:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 04:42 56-23-51.0 0.25 1
Chlorobenzene 3.1 ug/L 11/09/15 04:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 04:42 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 04:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 04:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 04:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 04:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 04:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 04:42 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene 3.9J ug/L 11/09/15 04:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene 12.7 ug/L 11/09/15 04:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 04:42 110-57-61001.0 1
1,1-Dichloroethane 1.3J ug/L 11/09/15 04:42 75-34-35.0 0.32 1
1,2-Dichloroethane 0.44J ug/L 11/09/15 04:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 04:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 17.5 ug/L 11/09/15 04:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 04:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 04:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 04:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 04:42 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3A Lab ID:92275192004 Collected:11/05/15 13:15 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 04:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 04:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 04:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 04:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 04:42 108-10-11000.33 1
Styrene ND ug/L 11/09/15 04:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 04:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 04:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 04:42 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 04:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 04:42 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 04:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 04:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 04:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 04:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 04:42 108-05-450.0 0.35 1
Vinyl chloride 1.5 ug/L 11/09/15 04:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 04:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %11/09/15 04:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)118 %11/09/15 04:42 17060-07-070-130 1
Toluene-d8 (S)101 %11/09/15 04:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-4 Lab ID:92275192005 Collected:11/05/15 11:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:42 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:42 7440-38-211/10/15 20:0010.0 2.5 1
Barium 20.2J ug/L 11/11/15 18:42 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:42 7440-41-711/10/15 20:001.0 0.50 1
Cadmium 1.3 ug/L 11/11/15 18:42 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:42 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 18:42 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:42 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:42 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 18:42 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:42 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:42 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:42 7440-28-011/10/15 20:005.5 5.0 1
Vanadium 3.3J ug/L 11/11/15 18:42 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 11.9 ug/L 11/11/15 18:42 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 04:59 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 04:59 107-13-12001.9 1
Benzene ND ug/L 11/09/15 04:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 04:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 04:59 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 04:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 04:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 04:59 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 04:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 04:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 04:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 04:59 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 04:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 04:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 04:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 04:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 04:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 04:59 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 04:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/09/15 04:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 04:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 04:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 04:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 04:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/09/15 04:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 04:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 04:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 04:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 04:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-4 Lab ID:92275192005 Collected:11/05/15 11:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 04:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 04:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 04:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 04:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 04:59 108-10-11000.33 1
Styrene ND ug/L 11/09/15 04:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 04:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 04:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 04:59 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 04:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 04:59 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 04:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 04:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 04:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 04:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 04:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 04:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 04:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %11/09/15 04:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %11/09/15 04:59 17060-07-070-130 1
Toluene-d8 (S)101 %11/09/15 04:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-5 Lab ID:92275192006 Collected:11/05/15 11:30 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/20/15 01:20 7440-36-011/17/15 22:006.0 3.8 1
Arsenic ND ug/L 11/20/15 01:20 7440-38-211/17/15 22:0010.0 2.5 1
Barium 22.2J ug/L 11/20/15 01:20 7440-39-311/17/15 22:001002.5 1
Beryllium ND ug/L 11/20/15 01:20 7440-41-711/17/15 22:001.0 0.50 1
Cadmium ND ug/L 11/20/15 01:20 7440-43-911/17/15 22:001.0 0.50 1
Chromium 3.1J ug/L 11/20/15 01:20 7440-47-311/17/15 22:0010.0 2.5 1
Cobalt ND ug/L 11/20/15 01:20 7440-48-411/17/15 22:0010.0 2.5 1
Copper ND ug/L 11/20/15 01:20 7440-50-811/17/15 22:0010.0 2.5 1
Lead ND ug/L 11/20/15 01:20 7439-92-111/17/15 22:0010.0 2.5 1
Nickel ND ug/L 11/20/15 01:20 7440-02-011/17/15 22:0050.0 2.5 1
Selenium ND ug/L 11/20/15 01:20 7782-49-211/17/15 22:0010.0 5.0 1
Silver ND ug/L 11/20/15 01:20 7440-22-411/17/15 22:0010.0 2.5 1
Thallium ND ug/L 11/20/15 15:10 7440-28-011/17/15 22:005.5 5.0 1
Vanadium ND ug/L 11/20/15 01:20 7440-62-211/17/15 22:0025.0 2.5 1
Zinc ND ug/L 11/20/15 01:20 7440-66-611/17/15 22:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 05:16 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 05:16 107-13-12001.9 1
Benzene ND ug/L 11/09/15 05:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 05:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 05:16 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 05:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 05:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 05:16 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 05:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 05:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 05:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 05:16 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 05:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 05:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 05:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 05:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 05:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 05:16 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 05:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/09/15 05:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 05:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 05:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 05:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 05:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/09/15 05:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 05:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 05:16 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 05:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 05:16 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-5 Lab ID:92275192006 Collected:11/05/15 11:30 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 05:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 05:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 05:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 05:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 05:16 108-10-11000.33 1
Styrene ND ug/L 11/09/15 05:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 05:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 05:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 05:16 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 05:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 05:16 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 05:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 05:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 05:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 05:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 05:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 05:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 05:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %11/09/15 05:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %11/09/15 05:16 17060-07-070-130 1
Toluene-d8 (S)101 %11/09/15 05:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-6 Lab ID:92275192007 Collected:11/05/15 10:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:45 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:45 7440-38-211/10/15 20:0010.0 2.5 1
Barium 74.9J ug/L 11/11/15 18:45 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:45 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 18:45 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:45 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt 12.6 ug/L 11/11/15 18:45 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:45 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:45 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 18:45 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:45 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:45 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:45 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 18:45 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 8.3J ug/L 11/11/15 18:45 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 05:34 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 05:34 107-13-12001.9 1
Benzene 0.73J ug/L 11/09/15 05:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 05:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 05:34 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 05:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 05:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 05:34 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 05:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 05:34 56-23-51.0 0.25 1
Chlorobenzene 6.6 ug/L 11/09/15 05:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 05:34 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 05:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 05:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 05:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 05:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 05:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 05:34 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene 1.9J ug/L 11/09/15 05:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.4 ug/L 11/09/15 05:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 05:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 05:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 05:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 05:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.2J ug/L 11/09/15 05:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 05:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 05:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 05:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 05:34 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-6 Lab ID:92275192007 Collected:11/05/15 10:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 05:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 05:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 05:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 05:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 05:34 108-10-11000.33 1
Styrene ND ug/L 11/09/15 05:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 05:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 05:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 05:34 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 05:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 05:34 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 05:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 05:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 05:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 05:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 05:34 108-05-450.0 0.35 1
Vinyl chloride 1.4 ug/L 11/09/15 05:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 05:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %11/09/15 05:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %11/09/15 05:34 17060-07-070-130 1
Toluene-d8 (S)101 %11/09/15 05:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7S Lab ID:92275192008 Collected:11/05/15 16:10 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:49 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:49 7440-38-211/10/15 20:0010.0 2.5 1
Barium 49.1J ug/L 11/11/15 18:49 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:49 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 18:49 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:49 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 18:49 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:49 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:49 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 18:49 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:49 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:49 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:49 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 18:49 7440-62-211/10/15 20:0025.0 2.5 1
Zinc ND ug/L 11/11/15 18:49 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 05:51 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 05:51 107-13-12001.9 1
Benzene ND ug/L 11/09/15 05:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 05:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 05:51 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 05:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 05:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 05:51 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 05:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 05:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 05:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 05:51 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 05:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 05:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 05:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 05:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 05:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 05:51 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 05:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.34J ug/L 11/09/15 05:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 05:51 110-57-61001.0 1
1,1-Dichloroethane 1.6J ug/L 11/09/15 05:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 05:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 05:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 12.0 ug/L 11/09/15 05:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 05:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 05:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 05:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 05:51 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7S Lab ID:92275192008 Collected:11/05/15 16:10 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 05:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 05:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 05:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 05:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 05:51 108-10-11000.33 1
Styrene ND ug/L 11/09/15 05:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 05:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 05:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 05:51 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 05:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 05:51 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 05:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 05:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 05:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 05:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 05:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 05:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 05:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %11/09/15 05:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %11/09/15 05:51 17060-07-070-130 1
Toluene-d8 (S)102 %11/09/15 05:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7D Lab ID:92275192009 Collected:11/05/15 16:35 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:52 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:52 7440-38-211/10/15 20:0010.0 2.5 1
Barium 10.9J ug/L 11/11/15 18:52 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:52 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 18:52 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:52 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 18:52 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:52 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:52 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 18:52 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:52 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:52 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:52 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 18:52 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 11.2 ug/L 11/11/15 18:52 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 06:08 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 06:08 107-13-12001.9 1
Benzene ND ug/L 11/09/15 06:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 06:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 06:08 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 06:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 06:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 06:08 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 06:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 06:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 06:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 06:08 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 06:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 06:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 06:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 06:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 06:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 06:08 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 06:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/09/15 06:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 06:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 06:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 06:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 06:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.72J ug/L 11/09/15 06:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 06:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 06:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 06:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 06:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7D Lab ID:92275192009 Collected:11/05/15 16:35 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 06:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 06:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 06:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 06:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 06:08 108-10-11000.33 1
Styrene ND ug/L 11/09/15 06:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 06:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 06:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 06:08 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 06:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 06:08 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 06:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 06:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 06:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 06:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 06:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 06:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 06:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %11/09/15 06:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %11/09/15 06:08 17060-07-070-130 1
Toluene-d8 (S)102 %11/09/15 06:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-8 Lab ID:92275192010 Collected:11/05/15 17:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 18:55 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 18:55 7440-38-211/10/15 20:0010.0 2.5 1
Barium 38.6J ug/L 11/11/15 18:55 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 18:55 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 18:55 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 18:55 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 18:55 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 18:55 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 18:55 7439-92-111/10/15 20:0010.0 2.5 1
Nickel 7.5J ug/L 11/11/15 18:55 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 18:55 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 18:55 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 18:55 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 18:55 7440-62-211/10/15 20:0025.0 2.5 1
Zinc ND ug/L 11/11/15 18:55 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 06:26 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 06:26 107-13-1 M12001.9 1
Benzene 1.6 ug/L 11/09/15 06:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 06:26 74-97-5 M13.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 06:26 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 06:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 06:26 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 06:26 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 06:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 06:26 56-23-5 M11.0 0.25 1
Chlorobenzene 0.74J ug/L 11/09/15 06:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 06:26 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 06:26 67-66-3 M15.0 0.14 1
Chloromethane ND ug/L 11/09/15 06:26 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 06:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 06:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 06:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 06:26 74-95-3 L3,M010.0 0.21 1
1,2-Dichlorobenzene 0.88J ug/L 11/09/15 06:26 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.0 ug/L 11/09/15 06:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 06:26 110-57-61001.0 1
1,1-Dichloroethane 1.1J ug/L 11/09/15 06:26 75-34-3 M15.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 06:26 107-06-2 M11.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 06:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 14.0 ug/L 11/09/15 06:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 06:26 156-60-5 M15.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 06:26 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 06:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 06:26 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-8 Lab ID:92275192010 Collected:11/05/15 17:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 06:26 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 06:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 06:26 74-88-4 M110.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 06:26 75-09-2 M11.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 06:26 108-10-1 M11000.33 1
Styrene ND ug/L 11/09/15 06:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 06:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 06:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 06:26 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 06:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 06:26 71-55-6 L3,M01.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 06:26 79-00-51.0 0.29 1
Trichloroethene 1.5 ug/L 11/09/15 06:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 06:26 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 06:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 06:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 06:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 06:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)111 %11/09/15 06:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)121 %11/09/15 06:26 17060-07-070-130 1
Toluene-d8 (S)103 %11/09/15 06:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-1 Lab ID:92275192011 Collected:11/05/15 12:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 19:07 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 19:07 7440-38-211/10/15 20:0010.0 2.5 1
Barium 22.0J ug/L 11/11/15 19:07 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 19:07 7440-41-711/10/15 20:001.0 0.50 1
Cadmium 0.63J ug/L 11/11/15 19:07 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 19:07 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 19:07 7440-48-411/10/15 20:0010.0 2.5 1
Copper 3.1J ug/L 11/11/15 19:07 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 19:07 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 19:07 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 19:07 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 19:07 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 19:07 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 19:07 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 13.5 ug/L 11/11/15 19:07 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 06:43 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 06:43 107-13-12001.9 1
Benzene ND ug/L 11/09/15 06:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 06:43 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 06:43 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 06:43 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 06:43 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 06:43 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 06:43 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 06:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 06:43 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 06:43 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 06:43 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 06:43 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 06:43 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 06:43 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 06:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 06:43 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 06:43 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/09/15 06:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 06:43 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 06:43 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 06:43 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 06:43 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/09/15 06:43 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 06:43 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 06:43 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 06:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 06:43 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-1 Lab ID:92275192011 Collected:11/05/15 12:00 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 06:43 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 06:43 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 06:43 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 06:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 06:43 108-10-11000.33 1
Styrene ND ug/L 11/09/15 06:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 06:43 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 06:43 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 06:43 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 06:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 06:43 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 06:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 06:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 06:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 06:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 06:43 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 06:43 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 06:43 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)113 %11/09/15 06:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)123 %11/09/15 06:43 17060-07-070-130 1
Toluene-d8 (S)103 %11/09/15 06:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-2 Lab ID:92275192012 Collected:11/05/15 11:45 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 11/11/15 19:10 7440-36-011/10/15 20:006.0 3.8 1
Arsenic ND ug/L 11/11/15 19:10 7440-38-211/10/15 20:0010.0 2.5 1
Barium 20.9J ug/L 11/11/15 19:10 7440-39-311/10/15 20:001002.5 1
Beryllium ND ug/L 11/11/15 19:10 7440-41-711/10/15 20:001.0 0.50 1
Cadmium ND ug/L 11/11/15 19:10 7440-43-911/10/15 20:001.0 0.50 1
Chromium ND ug/L 11/11/15 19:10 7440-47-311/10/15 20:0010.0 2.5 1
Cobalt ND ug/L 11/11/15 19:10 7440-48-411/10/15 20:0010.0 2.5 1
Copper ND ug/L 11/11/15 19:10 7440-50-811/10/15 20:0010.0 2.5 1
Lead ND ug/L 11/11/15 19:10 7439-92-111/10/15 20:0010.0 2.5 1
Nickel ND ug/L 11/11/15 19:10 7440-02-011/10/15 20:0050.0 2.5 1
Selenium ND ug/L 11/11/15 19:10 7782-49-211/10/15 20:0010.0 5.0 1
Silver ND ug/L 11/11/15 19:10 7440-22-411/10/15 20:0010.0 2.5 1
Thallium ND ug/L 11/11/15 19:10 7440-28-011/10/15 20:005.5 5.0 1
Vanadium ND ug/L 11/11/15 19:10 7440-62-211/10/15 20:0025.0 2.5 1
Zinc 6.4J ug/L 11/11/15 19:10 7440-66-611/10/15 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/09/15 07:18 67-64-110010.0 1
Acrylonitrile ND ug/L 11/09/15 07:18 107-13-12001.9 1
Benzene ND ug/L 11/09/15 07:18 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 11/09/15 07:18 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 11/09/15 07:18 75-27-41.0 0.18 1
Bromoform ND ug/L 11/09/15 07:18 75-25-23.0 0.26 1
Bromomethane ND ug/L 11/09/15 07:18 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 11/09/15 07:18 78-93-31000.96 1
Carbon disulfide ND ug/L 11/09/15 07:18 75-15-01001.2 1
Carbon tetrachloride ND ug/L 11/09/15 07:18 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 11/09/15 07:18 108-90-73.0 0.23 1
Chloroethane ND ug/L 11/09/15 07:18 75-00-310.0 0.54 1
Chloroform ND ug/L 11/09/15 07:18 67-66-35.0 0.14 1
Chloromethane ND ug/L 11/09/15 07:18 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/15 07:18 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 11/09/15 07:18 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/15 07:18 106-93-41.0 0.27 1
Dibromomethane ND ug/L 11/09/15 07:18 74-95-3 L310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 11/09/15 07:18 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 11/09/15 07:18 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 11/09/15 07:18 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 11/09/15 07:18 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 11/09/15 07:18 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 11/09/15 07:18 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 11/09/15 07:18 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 11/09/15 07:18 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 11/09/15 07:18 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 11/09/15 07:18 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 11/09/15 07:18 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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Page 27 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-2 Lab ID:92275192012 Collected:11/05/15 11:45 Received:11/06/15 07:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 11/09/15 07:18 100-41-41.0 0.30 1
2-Hexanone ND ug/L 11/09/15 07:18 591-78-650.0 0.46 1
Iodomethane ND ug/L 11/09/15 07:18 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 11/09/15 07:18 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/09/15 07:18 108-10-11000.33 1
Styrene ND ug/L 11/09/15 07:18 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/15 07:18 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/15 07:18 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 11/09/15 07:18 127-18-41.0 0.46 1
Toluene ND ug/L 11/09/15 07:18 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 11/09/15 07:18 71-55-6 L31.0 0.48 1
1,1,2-Trichloroethane ND ug/L 11/09/15 07:18 79-00-51.0 0.29 1
Trichloroethene ND ug/L 11/09/15 07:18 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 11/09/15 07:18 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 11/09/15 07:18 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 11/09/15 07:18 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 11/09/15 07:18 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 11/09/15 07:18 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)110 %11/09/15 07:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)123 %11/09/15 07:18 17060-07-070-130 1
Toluene-d8 (S)101 %11/09/15 07:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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Page 28 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/19999
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92275192001, 92275192002, 92275192003, 92275192004, 92275192005, 92275192007, 92275192008,
92275192009, 92275192010, 92275192011, 92275192012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1603342
Associated Lab Samples:92275192001, 92275192002, 92275192003, 92275192004, 92275192005, 92275192007, 92275192008,
92275192009, 92275192010, 92275192011, 92275192012
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 11/11/15 17:473.8
Arsenic ug/L ND 10.0 11/11/15 17:472.5
Barium ug/L ND 100 11/11/15 17:472.5
Beryllium ug/L ND 1.0 11/11/15 17:470.50
Cadmium ug/L ND 1.0 11/11/15 17:470.50
Chromium ug/L ND 10.0 11/11/15 17:472.5
Cobalt ug/L ND 10.0 11/11/15 17:472.5
Copper ug/L ND 10.0 11/11/15 17:472.5
Lead ug/L ND 10.0 11/11/15 17:472.5
Nickel ug/L ND 50.0 11/11/15 17:472.5
Selenium ug/L ND 10.0 11/11/15 17:475.0
Silver ug/L ND 10.0 11/11/15 17:472.5
Thallium ug/L ND 5.5 11/11/15 17:475.0
Vanadium ug/L ND 25.0 11/11/15 17:472.5
Zinc ug/L ND 10.0 11/11/15 17:475.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1603343LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 510500 102 80-120
Arsenic ug/L 494500 99 80-120
Barium ug/L 500500 100 80-120
Beryllium ug/L 494500 99 80-120
Cadmium ug/L 489500 98 80-120
Chromium ug/L 475500 95 80-120
Cobalt ug/L 495500 99 80-120
Copper ug/L 500500 100 80-120
Lead ug/L 493500 99 80-120
Nickel ug/L 486500 97 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 231250 93 80-120
Thallium ug/L 410500 82 80-120
Vanadium ug/L 476500 95 80-120
Zinc ug/L 494500 99 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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[phone]
Page 29 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1603344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92273910001
1603345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 108 75-125102 6 25500ND539510
Arsenic ug/L 500 105 75-125100 5 25500ND526500
Barium ug/L 500 106 75-125100 5 2550047.7 578 548
Beryllium ug/L 500 106 75-12599 6 25500ND528496
Cadmium ug/L 500 103 75-12597 6 25500ND516485
Chromium ug/L 500 100 75-12594 6 25500ND502471
Cobalt ug/L 500 104 75-12598 6 2550038.4 557 526
Copper ug/L 500 105 75-12599 6 25500ND525495
Lead ug/L 500 103 75-12597 6 25500ND515484
Nickel ug/L 500 102 75-12596 6 255003.0J 512 481
Selenium ug/L 500 104 75-12598 6 25500ND524494
Silver ug/L 250 98 75-12591 7 25250ND245228
Thallium ug/L 500 86 75-12581 6 25500ND432407
Vanadium ug/L 500 101 75-12595 6 25500ND508476
Zinc ug/L 500 104 75-12598 6 25500ND523491
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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[phone]
Page 30 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20056
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92275192006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1608949
Associated Lab Samples:92275192006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 11/20/15 01:143.8
Arsenic ug/L ND 10.0 11/20/15 01:142.5
Barium ug/L ND 100 11/20/15 01:142.5
Beryllium ug/L ND 1.0 11/20/15 01:140.50
Cadmium ug/L ND 1.0 11/20/15 01:140.50
Chromium ug/L ND 10.0 11/20/15 01:142.5
Cobalt ug/L ND 10.0 11/20/15 01:142.5
Copper ug/L ND 10.0 11/20/15 01:142.5
Lead ug/L ND 10.0 11/20/15 01:142.5
Nickel ug/L ND 50.0 11/20/15 01:142.5
Selenium ug/L ND 10.0 11/20/15 01:145.0
Silver ug/L ND 10.0 11/20/15 01:142.5
Thallium ug/L ND 5.5 11/20/15 15:045.0
Vanadium ug/L ND 25.0 11/20/15 01:142.5
Zinc ug/L ND 10.0 11/20/15 01:145.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1608950LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 484500 97 80-120
Arsenic ug/L 474500 95 80-120
Barium ug/L 488500 98 80-120
Beryllium ug/L 487500 97 80-120
Cadmium ug/L 489500 98 80-120
Chromium ug/L 486500 97 80-120
Cobalt ug/L 488500 98 80-120
Copper ug/L 490500 98 80-120
Lead ug/L 480500 96 80-120
Nickel ug/L 489500 98 80-120
Selenium ug/L 474500 95 80-120
Silver ug/L 234250 94 80-120
Thallium ug/L 487500 97 80-120
Vanadium ug/L 486500 97 80-120
Zinc ug/L 481500 96 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608951MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275192006
1608952
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12594 0 25500ND474474
Arsenic ug/L 500 93 75-12593 0 25500ND467465
Barium ug/L 500 98 75-12597 1 2550022.2J 512 507
Beryllium ug/L 500 99 75-12597 1 25500ND493487
Cadmium ug/L 500 97 75-12596 1 25500ND483480
Chromium ug/L 500 97 75-12597 1 255003.1J 490 486
Cobalt ug/L 500 96 75-12595 1 25500ND480477
Copper ug/L 500 98 75-12598 1 25500ND491488
Lead ug/L 500 94 75-12594 1 25500ND472468
Nickel ug/L 500 96 75-12596 1 25500ND483480
Selenium ug/L 500 93 75-12592 1 25500ND467462
Silver ug/L 250 93 75-12593 0 25250ND233232
Thallium ug/L 500 96 75-12597 1 25500ND483489
Vanadium ug/L 500 97 75-12597 0 25500ND484483
Zinc ug/L 500 95 75-12594 1 25500ND475470
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1608967MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92275823005
1608968
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 95 75-12593 3 25500ND478466
Arsenic ug/L 500 94 75-12591 3 25500ND470457
Barium ug/L 500 98 75-12595 2 25500128618604
Beryllium ug/L 500 99 75-12596 3 25500ND494479
Cadmium ug/L 500 97 75-12594 3 25500ND486472
Chromium ug/L 500 98 75-12596 2 25500ND489478
Cobalt ug/L 500 96 75-12593 3 255004.6J 486 471
Copper ug/L 500 99 75-12596 3 25500ND496483
Lead ug/L 500 95 75-12592 3 25500ND475460
Nickel ug/L 500 97 75-12594 3 255003.7J 487 472
Selenium ug/L 500 94 75-12590 4 25500ND474456
Silver ug/L 250 94 75-12592 2 25250ND235229
Thallium ug/L 500 95 75-12593 2 25500ND476467
Vanadium ug/L 500 98 75-12596 2 25500ND489478
Zinc ug/L 500 96 75-12592 3 2550014.3 492 476
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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Huntersville, NC 28078
[phone]
Page 32 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34199
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92275192001, 92275192002, 92275192003, 92275192004, 92275192005, 92275192006, 92275192007,
92275192008, 92275192009, 92275192010, 92275192011, 92275192012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1601645
Associated Lab Samples:92275192001, 92275192002, 92275192003, 92275192004, 92275192005, 92275192006, 92275192007,
92275192008, 92275192009, 92275192010, 92275192011, 92275192012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 11/09/15 03:330.33
1,1,1-Trichloroethane ug/L ND 1.0 11/09/15 03:330.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 11/09/15 03:330.40
1,1,2-Trichloroethane ug/L ND 1.0 11/09/15 03:330.29
1,1-Dichloroethane ug/L ND 5.0 11/09/15 03:330.32
1,1-Dichloroethene ug/L ND 5.0 11/09/15 03:330.56
1,2,3-Trichloropropane ug/L ND 1.0 11/09/15 03:330.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 11/09/15 03:332.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/09/15 03:330.27
1,2-Dichlorobenzene ug/L ND 5.0 11/09/15 03:330.30
1,2-Dichloroethane ug/L ND 1.0 11/09/15 03:330.24
1,2-Dichloropropane ug/L ND 1.0 11/09/15 03:330.27
1,4-Dichlorobenzene ug/L ND 1.0 11/09/15 03:330.33
2-Butanone (MEK)ug/L ND 100 11/09/15 03:330.96
2-Hexanone ug/L ND 50.0 11/09/15 03:330.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 11/09/15 03:330.33
Acetone ug/L ND 100 11/09/15 03:3310.0
Acrylonitrile ug/L ND 200 11/09/15 03:331.9
Benzene ug/L ND 1.0 11/09/15 03:330.25
Bromochloromethane ug/L ND 3.0 11/09/15 03:330.17
Bromodichloromethane ug/L ND 1.0 11/09/15 03:330.18
Bromoform ug/L ND 3.0 11/09/15 03:330.26
Bromomethane ug/L ND 10.0 11/09/15 03:330.29
Carbon disulfide ug/L ND 100 11/09/15 03:331.2
Carbon tetrachloride ug/L ND 1.0 11/09/15 03:330.25
Chlorobenzene ug/L ND 3.0 11/09/15 03:330.23
Chloroethane ug/L ND 10.0 11/09/15 03:330.54
Chloroform ug/L ND 5.0 11/09/15 03:330.14
Chloromethane ug/L ND 1.0 11/09/15 03:330.11
cis-1,2-Dichloroethene ug/L ND 5.0 11/09/15 03:330.19
cis-1,3-Dichloropropene ug/L ND 1.0 11/09/15 03:330.13
Dibromochloromethane ug/L ND 3.0 11/09/15 03:330.21
Dibromomethane ug/L ND 10.0 11/09/15 03:330.21
Ethylbenzene ug/L ND 1.0 11/09/15 03:330.30
Iodomethane ug/L ND 10.0 11/09/15 03:330.32
Methylene Chloride ug/L ND 1.0 11/09/15 03:330.97
Styrene ug/L ND 1.0 11/09/15 03:330.26
Tetrachloroethene ug/L ND 1.0 11/09/15 03:330.46
Toluene ug/L ND 1.0 11/09/15 03:330.26
trans-1,2-Dichloroethene ug/L ND 5.0 11/09/15 03:330.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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[phone]
Page 33 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1601645
Associated Lab Samples:92275192001, 92275192002, 92275192003, 92275192004, 92275192005, 92275192006, 92275192007,
92275192008, 92275192009, 92275192010, 92275192011, 92275192012
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 11/09/15 03:330.26
trans-1,4-Dichloro-2-butene ug/L ND 100 11/09/15 03:331.0
Trichloroethene ug/L ND 1.0 11/09/15 03:330.47
Trichlorofluoromethane ug/L ND 1.0 11/09/15 03:330.20
Vinyl acetate ug/L ND 50.0 11/09/15 03:330.35
Vinyl chloride ug/L ND 1.0 11/09/15 03:330.62
Xylene (Total)ug/L ND 5.0 11/09/15 03:330.66
1,2-Dichloroethane-d4 (S)%116 70-130 11/09/15 03:33
4-Bromofluorobenzene (S)%113 70-130 11/09/15 03:33
Toluene-d8 (S)%101 70-130 11/09/15 03:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1601646LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.850 108 80-125
1,1,1-Trichloroethane ug/L 68.9 L05013871-129
1,1,2,2-Tetrachloroethane ug/L 51.850 104 79-124
1,1,2-Trichloroethane ug/L 55.450 111 85-125
1,1-Dichloroethane ug/L 59.150 118 73-126
1,1-Dichloroethene ug/L 60.850 122 66-135
1,2,3-Trichloropropane ug/L 57.050 114 75-130
1,2-Dibromo-3-chloropropane ug/L 48.350 97 71-133
1,2-Dibromoethane (EDB)ug/L 59.250 118 83-124
1,2-Dichlorobenzene ug/L 55.350 111 80-133
1,2-Dichloroethane ug/L 60.850 122 67-128
1,2-Dichloropropane ug/L 56.750 113 75-132
1,4-Dichlorobenzene ug/L 53.150 106 78-130
2-Butanone (MEK)ug/L 119100 119 61-144
2-Hexanone ug/L 112100 112 68-143
4-Methyl-2-pentanone (MIBK)ug/L 127100 127 72-135
Acetone ug/L 112100 112 48-146
Acrylonitrile ug/L 305250 122 40-160
Benzene ug/L 55.250 110 80-125
Bromochloromethane ug/L 59.650 119 71-125
Bromodichloromethane ug/L 55.150 110 78-124
Bromoform ug/L 52.350 105 71-128
Bromomethane ug/L 35.250 70 40-160
Carbon disulfide ug/L 44.4J50 89 50-160
Carbon tetrachloride ug/L 63.050 126 69-131
Chlorobenzene ug/L 54.450 109 81-122
Chloroethane ug/L 44.450 89 39-148
Chloroform ug/L 60.150 120 73-127
Chloromethane ug/L 43.150 86 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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[phone]
Page 34 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1601646LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 60.150 120 74-124
cis-1,3-Dichloropropene ug/L 51.750 103 72-132
Dibromochloromethane ug/L 51.050 102 78-125
Dibromomethane ug/L 61.1 L05012282-120
Ethylbenzene ug/L 56.450 113 79-121
Iodomethane ug/L 59.4100 59 39-154
Methylene Chloride ug/L 60.250 120 64-133
Styrene ug/L 50.750 101 84-126
Tetrachloroethene ug/L 55.650 111 78-122
Toluene ug/L 55.550 111 80-121
trans-1,2-Dichloroethene ug/L 62.150 124 71-127
trans-1,3-Dichloropropene ug/L 53.150 106 69-141
trans-1,4-Dichloro-2-butene ug/L 44.5J50 89 40-160
Trichloroethene ug/L 56.650 113 78-122
Trichlorofluoromethane ug/L 64.050 128 53-137
Vinyl acetate ug/L 120100 120 40-160
Vinyl chloride ug/L 49.350 99 58-137
Xylene (Total)ug/L 172150 114 81-126
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1601647MATRIX SPIKE SAMPLE:
MSSpike
Result
92275192010
1,1,1,2-Tetrachloroethane ug/L 25.120 125 70-130ND
1,1,1-Trichloroethane ug/L 31.0 M02015570-130ND
1,1,2,2-Tetrachloroethane ug/L 21.520 108 70-130ND
1,1,2-Trichloroethane ug/L 24.520 122 70-130ND
1,1-Dichloroethane ug/L 28.3 M12013670-1301.1J
1,1-Dichloroethene ug/L 28.120 141 70-166ND
1,2,3-Trichloropropane ug/L 24.520 123 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.920 95 70-130ND
1,2-Dibromoethane (EDB)ug/L 24.620 123 70-130ND
1,2-Dichlorobenzene ug/L 23.320 112 70-1300.88J
1,2-Dichloroethane ug/L 27.2 M12013570-130ND
1,2-Dichloropropane ug/L 25.820 129 70-130ND
1,4-Dichlorobenzene ug/L 24.920 115 70-1302.0
2-Butanone (MEK)ug/L 51.5J40 129 70-130ND
2-Hexanone ug/L 45.8J40 115 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 53.4J M14013470-130ND
Acetone ug/L 49.5J40 124 70-130ND
Acrylonitrile ug/L 134J M110013470-130ND
Benzene ug/L 26.520 124 70-1481.6
Bromochloromethane ug/L 26.1 M12013170-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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[phone]
Page 35 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1601647MATRIX SPIKE SAMPLE:
MSSpike
Result
92275192010
Bromodichloromethane ug/L 25.720 128 70-130ND
Bromoform ug/L 21.020 105 70-130ND
Bromomethane ug/L 11.8 M1205970-130ND
Carbon disulfide ug/L 22.3J20 112 70-130ND
Carbon tetrachloride ug/L 29.9 M12014970-130ND
Chlorobenzene ug/L 24.420 119 70-1460.74J
Chloroethane ug/L 21.020 105 70-130ND
Chloroform ug/L 26.5 M12013370-130ND
Chloromethane ug/L 22.020 110 70-130ND
cis-1,2-Dichloroethene ug/L 39.920 129 70-13014.0
cis-1,3-Dichloropropene ug/L 22.020 110 70-130ND
Dibromochloromethane ug/L 22.920 114 70-130ND
Dibromomethane ug/L 26.4 M02013270-130ND
Ethylbenzene ug/L 24.920 124 70-130ND
Iodomethane ug/L 21.4 M1405470-130ND
Methylene Chloride ug/L 27.6 M12013870-130ND
Styrene ug/L 23.420 117 70-130ND
Tetrachloroethene ug/L 25.320 126 70-130ND
Toluene ug/L 25.520 127 70-155ND
trans-1,2-Dichloroethene ug/L 28.1 M12014170-130ND
trans-1,3-Dichloropropene ug/L 23.620 118 70-130ND
trans-1,4-Dichloro-2-butene ug/L 16.1J20 80 70-130ND
Trichloroethene ug/L 27.420 130 69-1511.5
Trichlorofluoromethane ug/L 30.1 M12015070-130ND
Vinyl acetate ug/L 38.5J40 96 70-130ND
Vinyl chloride ug/L 23.620 118 70-130ND
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%110 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92275192011
1601648SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92275192011
1601648SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%121 2123
4-Bromofluorobenzene (S)%111 2113
Toluene-d8 (S)%101 2103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 37 of 41
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 41
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92275192
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92275192001 MPRP/19999 ICP/18033MW-1 EPA 3010 EPA 6010
92275192002 MPRP/19999 ICP/18033MW-2 EPA 3010 EPA 6010
92275192003 MPRP/19999 ICP/18033MW-3 EPA 3010 EPA 6010
92275192004 MPRP/19999 ICP/18033MW-3A EPA 3010 EPA 6010
92275192005 MPRP/19999 ICP/18033MW-4 EPA 3010 EPA 6010
92275192006 MPRP/20056 ICP/18088MW-5 EPA 3010 EPA 6010
92275192007 MPRP/19999 ICP/18033MW-6 EPA 3010 EPA 6010
92275192008 MPRP/19999 ICP/18033MW-7S EPA 3010 EPA 6010
92275192009 MPRP/19999 ICP/18033MW-7D EPA 3010 EPA 6010
92275192010 MPRP/19999 ICP/18033MW-8 EPA 3010 EPA 6010
92275192011 MPRP/19999 ICP/18033SW-1 EPA 3010 EPA 6010
92275192012 MPRP/19999 ICP/18033SW-2 EPA 3010 EPA 6010
92275192001 MSV/34199MW-1 EPA 8260
92275192002 MSV/34199MW-2 EPA 8260
92275192003 MSV/34199MW-3 EPA 8260
92275192004 MSV/34199MW-3A EPA 8260
92275192005 MSV/34199MW-4 EPA 8260
92275192006 MSV/34199MW-5 EPA 8260
92275192007 MSV/34199MW-6 EPA 8260
92275192008 MSV/34199MW-7S EPA 8260
92275192009 MSV/34199MW-7D EPA 8260
92275192010 MSV/34199MW-8 EPA 8260
92275192011 MSV/34199SW-1 EPA 8260
92275192012 MSV/34199SW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/21/2015 11:43 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 41
Page 40 of 41
Page 41 of 41
Appendix B
Field Sampling Parameter Data Sheet(s)