8603_SurryCountyElkin_GWMR_DIN28071_20160516

Surry County Closed C&D and Closed MSWLF, Elkin
Elkin, North Carolina
May 2016
Permit Number: 86-03
Semi-Annual Water Quality Monitoring Report
Prepared for
PO Box 97
Garner, NC 27529
License No, C-0281
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G16025.0
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Groundwater Samples Page 2
Surface Water Samples Page 2
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 3
FIGURES
Topographic Map with Site Location Figure 1
Single-Day Potentiometric Map of Uppermost Aquifer Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above Established SWSL, GWP, 2L, 2B or MCL (Appendix I) Table 5
Hydrologic Properties at Monitoring Well Locations Table 6
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
October 28, 2016
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Elkin
Permit No. 86-03
MESCO Project No. G16025.0
Event Date(s): May 16, 2016
Dear Ms. Drummond;
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the spring 2016 event performed at the Surry County closed construction and
demolition (C&D) and closed municipal solid waste landfill (MSWLF). NCDEQ Solid Waste Rules 15A NCAC
13B.1632 requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents
the quality of the ground and surface waters during this monitoring event performed on May 16, 2016. Laboratory
analytical results indicate volatile organic compounds (VOCs) persist within five wells used to monitor the
uppermost aquifer. The surface water samples collected from the discharge feature remain unimpacted.
Background
The Surry County closed C&D and MSWLF, permit #86-03, is located at Elkin Landfill Road (SR 1191), Elkin,
Surry County, North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to
operating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two units. The first
area was closed prior to October 1991 with a 24 inch final soil cover. The second area was closed with a cohesive
cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec, and 18 inches of erosive layer
prior to December 31, 1998 in accordance with the Transition Plan. C&D was placed on top of the cohesive capped
unit until 2008.
This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and
as a condition of the post-closure portion of the permit to operate. Water quality at this facility has been monitored
at least semi-annually since 1989 with historical data available since 1994. The SWS approved a modification to the
assessment monitoring program on October 15, 2014 (DIN:21983) which entails a subset of wells be sampled for
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums, this report contains sampling procedures, field and laboratory results, ground/surface water
characterization, and findings. Well construction summary table, field observations table, field parameter data table,
sampling and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates
table, potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed
herein.

Sampling Procedure
MESCO personnel performed this sampling event utilizing portable monitoring methodology in accordance with the
site-specific Sampling and Analysis Plan (SAP) and the NCDENR SWS guidance document Solid Waste SectionGuidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. Water samples were collected
from nine downgradient groundwater monitoring wells (MW-2, MW-3, MW-3A, MW-4, MW-5, MW-6, MW-7S,
MW-7D and MW-8), one background well (MW-1), and two surface water points (SW-1 and SW-2). Monitoring
locations are shown on the single-day potentiometric map (Figure 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function andintegrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of
three times the volume of standing water in the well or until dry. Surface water samples were collected from Snow
Creek discharge feature at previously designated locations. During well purging and surface water samplecollection the required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-
preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported
to a NC-certified laboratory under proper chain of custody (C-O-C) protocols within the specified hold times for
each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, specific conductance,
temperature and visual turbidity. MW-7D exhibited a higher than normal pH and water level which is likely caused
a reaction with the limestone in the grout. A summary of the field parameter data is presented in Table 3 and the
field sampling data sheet is enclosed in Appendix B.
Laboratory Results
All water samples were analyzed for the Appendix I list of VOCs and total unfiltered metals listed in 40 CFR 258.
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the laboratory analysis. A
sampling and analysis table summarizing the locations, constituents, and methods is presented as Table 4.
Laboratory results and C-O-Cs are presented in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater that
attain or were above the current SWSL, Groundwater Protection Standards (GWP) or Maximum Contaminant
Levels (MCL) also recognized as “Federal Primary Drinking Water Standards”.
Groundwater Samples
The only inorganic constituent detected above the SWSL and in excess of its respective 2L/GWP Standard was total
arsenic in sample MW-2 (39/10 ug/L) and total thallium in sample MW-3A (5.7/0.28 ug/L).
One or more Appendix I VOC(s) were detected in quantifiable concentrations above their respective 2L Standardsin samples collected from MW-2, MW-3, MW-3A, MW-6 and MW-8.
Surface Water Samples
Target constituent(s) were not detected in either surface water sample in concentrations exceeding the applicable 2B
Standard.
Groundwater and Surface Water Characterization
A single-day potentiometric map constructed from groundwater levels collected during this event is presented as
Figure 2. Groundwater flow rates and directions were calculated and are included in Table 6. Groundwater flows
generally southwest, towards the Snow Creek discharge feature. Groundwater average linear velocity ratescalculated from modified Darcy's equation indicate flow rates ranged from approximately 16 ft/yr (MW-3A) to 836
ft/yr (MW-6). Groundwater average linear velocity rates averaged approximately 199 ft/yr in wells screened in the
regolith aquifer and 249 ft./yr. in the wells screened in the upper bedrock. Snow Creek, monitored at SW-1 and
SW-2, was visually observed to have a moderate gage height, moderate volume and low turbidity.
2
Figures
Tables
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
May 16, 2016
Latitude Longitude
(inches)(ft)
MW-1 11/28/89 4 74.56 64.56 10 Soil 1042 1041 985 56.57 36.29711 -80.77236
MW-2 11/08/89 4 79 69 10 Soil 948 947 890 58.11 36.29572 -80.77620
MW-3 11/28/89 4 63 53 10 Soil 932 931 881 51.25 36.29362 -80.77646
MW-3A 09/16/94 2 40 24 16 Fractured Rock 927 924 894 32.21 36.29457 -80.77675
MW-4 09/15/94 2 29 13 16 Fractured Rock 933 929 921 11.97 36.29379 -80.77528
MW-5 09/15/94 2 31 16 15 Fractured Rock 949 845 937 11.90 36.29450 -80.77456
MW-6 09/15/94 2 66 51 15 Fractured Rock 1005 1002 954 50.90 36.29780 -80.77270
MW-7S 06/05/01 2 24 9 15 Fractured Rock 901 889 890 11.03 36.29407 80.77730
MW-7D 06/05/01 2 90 80 10 Fractured Rock 901 889 895 5.51 36.29407 80.77730
MW-8 06/04/01 2 67 52 15 Fractured Rock 1015 1013 973 41.39 36.29739 -80.77246
NOTE:
Monitoring Well Date Installed
Well Diameter
Total Well Depth
Top of Screen Depth
Screen Length Geology of Screened Interval
Top of Casing Elevation
Ground Elevation Groundwater Elevation Depth to Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 2
Field Observations of Monitoring Locations
May 16, 2016
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes 4” Diameter
MW-2 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge, hasp cracked
MW-3 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge
MW-3A Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-6 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-7S Yes Yes Yes Yes Yes Yes
MW-7D Yes Yes Yes Yes Yes Yes pH elevated likely grout intrusion
MW-8 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----
SW-2 Yes -----
Any unusual field conditions, observations, or events:
Facility no longer in operation or occupied since transfer station closed in ~ June 2010.
MESCO moved tree blocking path leading to MW-2.
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears to
be Effective
Mod. gage & mod flow
Low gage & low flow
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 3
Field Parameter Data Summary
May 16, 2016
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L %/Vol Visual
MW-1 54.55 985.00 1042.00 15.1 NR NR 6.1 83 NR NR Clear
MW-2 57.15 890.00 948.00 15.1 NR NR 6.6 1678 NR NR Slight
MW-3 49.35 881.00 932.00 14.3 NR NR 6.0 336 NR NR Slight
MW-3A 31.05 894.00 926.50 14.6 NR NR 6.3 879 NR NR Clear
MW-4 11.45 921.00 932.50 12.7 NR NR 6.3 46 NR NR Clear
MW-5 11.32 937.18 948.50 12.3 NR NR 6.3 68 NR NR Clear
MW-6 46.79 954.00 1004.50 14.6 NR NR 6.0 325 NR NR Clear
MW-7S 11.04 890.00 901.01 12.2 NR NR 6.3 395 NR NR Clear
MW-7D 1.64 895.00 900.95 12.5 NR NR 8.5 257 NR NR Clear
MW-8 40.14 973.00 1014.87 15.1 NR NR 5.9 220 NR NR Clear
Minimum 1.64 881 901 12.2 NR NR 5.9 46 NR NR Clear
Average 31.45 922 955 13.9 NR NR 6.4 429 NR NR Clear
Maximum 57.15 985 1042 15.1 NR NR 8.5 1678 NR NR Slight
SW-1 ---11.7 NR NR 7.2 74 NR -Clear
SW-2 ---11.6 NR NR 7.2 83 NR -Clear
Minimum ---11.6 NR NR 7.2 74 NR -Clear
Average ---11.7 NR NR 7.2 79 NR -Clear
Maximum ---11.7 NR NR 7.2 83 NR -Clear
NR = No Reading attempted
* = Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
Depth to
Water
Water
Elevation*
TOC
Elevation*
Specific
Conductance
Methane Gas in
Well Headspace
Turbidity of
Metals Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
btoc = below top of casing
amsl = above mean sea level
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 4
Sampling and Analysis Summary
May 16, 2016
App. I Field Parameter
T o t a l M e t a l s
T e m p e r a t u r e
C o n d u c t i v i t y
T o t a l D i s s o l v e d S o l i d s (T D S )
p H T u r b i d i t y
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d V i s u a l
MW-1 x x x x x x x
MW-2 x x x x x x x
MW-3 x x x x x x x
MW-3A x x x x x x x
MW-4 x x x x x x x
MW-5 x x x x x x x
MW-6 x x x x x x x
MW-7S x x x x x x x
MW-7D x x x x x x x
MW-8 x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
App I & II = List from current 40 CFR 258
All wells listed on SAP presented
V O C s
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 2
Table 5
May 16, 2016
Result Unit
MW-2 5/16/16 9 0.3 5 24 NE
MW-2 5/16/16 0.77J 0.24 1 0.4 5 L &/or LFG
MW-2 5/16/16 1.2 0.27 1 0.6 5 L &/or LFG
MW-2 5/16/16 16.6 0.33 1 6 75 L &/or LFG
MW-2 Antimony, total 5/16/16 4J 3.8 6 NE 1.4 6 N
MW-2 Arsenic, total 5/16/16 39 2.5 10 10 10 N
MW-2 Barium, total 5/16/16 194 2.5 100 700 1300
MW-2 Benzene 5/16/16 2.3 0.25 1 1 5 L &/or LFG
MW-2 Cadmium, total 5/16/16 1.7 0.5 1 2 5
MW-2 5/16/16 10.6 0.23 3 50 100
MW-2 Vanadium, total 5/16/16 5.5J 2.5 25 NE 3.5 NE N
MW-2 Zinc, total 5/16/16 15.6 5 10 1000 NE
MW-3 5/16/16 6 0.33 1 6 75
MW-3 Benzene 5/16/16 3.4 0.25 1 1 5 L &/or LFG
MW-3 5/16/16 21.8 0.19 5 70 70
MW-3 5/16/16 1.8 0.47 1 3 5
MW-3 Vinyl chloride 5/16/16 0.86J 0.62 1 0.03 2 L &/or LFG
MW-3A 5/16/16 12.4 0.33 1 6 75 L &/or LFG
MW-3A Antimony, total 5/16/16 4.7J 3.8 6 NE 1.4 6 N
MW-3A Barium, total 5/16/16 457 2.5 100 700 1300
MW-3A Benzene 5/16/16 1.2 0.25 1 1 5 L &/or LFG
MW-3A 5/16/16 4 0.23 3 50 100
MW-3A 5/16/16 18.6 0.19 5 70 70
MW-3A Cobalt, total 5/16/16 23.3 2.5 10 NE 70 NE
MW-3A Thallium, total 5/16/16 5.7 5 5.5 NE 0.28 2 N
MW-3A Vinyl chloride 5/16/16 2.7 0.62 1 0.03 2 L &/or LFG
MW-5 Cadmium, total 5/16/16 1.4 0.5 1 2 5
MW-6 5/16/16 4 0.33 1 6 75
MW-6 5/16/16 10 0.23 3 50 100
MW-6 Cobalt, total 5/16/16 12.1 2.5 10 NE 70 NE
MW-6 Vinyl chloride 5/16/16 1.9 0.62 1 0.03 2 L &/or LFG
MW-7S 5/16/16 6.5 0.19 5 70 70
Detections in Water Samples above SWSL, GWP, 2L, 2B or MCL (Appendix I)
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
1,2-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
1,2-Dichloropropane ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Trichloroethene ug/L
ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
Chlorobenzene ug/L
ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Surry County Closed C&D and Closed MSWLF, Elkin Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
MW-8 5/16/16 2.2 0.33 1 6 75
MW-8 Benzene 5/16/16 1.5 0.25 1 1 5 L &/or LFG
MW-8 5/16/16 15.2 0.19 5 70 70
MW-8 5/16/16 1 0.47 1 3 5
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to SWS reporting instructions
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
NE = Not Established
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
1,4-Dichlorobenzene ug/L
ug/L
cis-1,2-Dichloroethene ug/L
Trichloroethene ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard (NC SWS adopted)
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 6
May 16, 2016
(cm/second)(%)(feet/feet)(feet/year)
MW-1 9.90E-05 5 0.097 199 S53W 54.55 985 Clay
MW-2 2.00E-05 5 57.15 890**Clay
MW-3 5.00E-05 5 49.35 881**Clay
Minimum 2.70E-04 5 0.097 199 -49.35 882 -
Average 3.45E-04 5 0.097 199 -53.68 920 -
Maximum 4.20E-04 5 0.097 199 -57.15 891 -
MW-3A 2.50E-05 5 0.031 16 N55W 31.05 894 Fractured Rock
MW-4 4.20E-04 5 0.009 74 N79W 11.45 921 Fractured Rock
MW-5 2.70E-04 5 0.008 42 N89W 11.32 937 Fractured Rock
MW-6 1.20E-04 5 0.337 836 N10W 46.79 954 Fractured Rock
MW-7S 2.30E-04 5 0.093 441 S80W 11.04 890 Fractured Rock
MW-7D 1.64 895**Fractured Rock
MW-8 2.40E-05 5 0.165 82 N27W 975.00 973 Fractured Rock
Minimum 2.40E-05 5 0.008 16 -1.64 890 -
Average 1.82E-04 5 0.107 249 -155.47 924 -
Maximum 4.20E-04 5 0.337 836 -975.00 973 -
NOTE: Note: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
* = Elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average Linear
Velocity Rate
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation*
Screened Interval
Lithology
(ft btoc)(ft amsl)
na na na
na na na
na na na na na
Hydrologic gradient calculated from groundwater elevations recorded November 5, 2015.
** = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
Average Linear Velocity Rate (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e

Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
May 26, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92298161
92298161
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CO. CLOSED MSWLF-ELKIN
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 41
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
Asheville Certification IDs2225 Riverside Drive, Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 41
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID Matrix Date Collected Date Received
92298161001 MW-1 Water 05/16/16 14:00 05/18/16 15:10
92298161002 MW-2 Water 05/16/16 13:15 05/18/16 15:10
92298161003 MW-3 Water 05/16/16 12:00 05/18/16 15:10
92298161004 MW-3A Water 05/16/16 12:35 05/18/16 15:10
92298161005 MW-4 Water 05/16/16 09:15 05/18/16 15:10
92298161006 MW-5 Water 05/16/16 08:40 05/18/16 15:10
92298161007 MW-6 Water 05/16/16 14:40 05/18/16 15:10
92298161008 MW-7S Water 05/16/16 11:00 05/18/16 15:10
92298161009 MW-7D Water 05/16/16 10:15 05/18/16 15:10
92298161010 MW-8 Water 05/16/16 15:30 05/18/16 15:10
92298161011 SW-1 Water 05/16/16 09:35 05/18/16 15:10
92298161012 SW-2 Water 05/16/16 11:25 05/18/16 15:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 41
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92298161001 MW-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161002 MW-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161003 MW-3 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161004 MW-3A EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161005 MW-4 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161006 MW-5 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161007 MW-6 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161008 MW-7S EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161009 MW-7D EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161010 MW-8 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161011 SW-1 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
92298161012 SW-2 EPA 6010 15 PASI-ACDF
EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-1 Lab ID:92298161001 Collected:05/16/16 14:00 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 10:50 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 10:50 7440-38-205/20/16 10:4510.0 2.5 1
Barium 26.5J ug/L 05/25/16 10:50 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 10:50 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 10:50 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 10:50 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 10:50 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 10:50 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 10:50 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 10:50 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 10:50 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 10:50 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 10:50 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 10:50 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 10:50 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 19:34 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 19:34 107-13-12001.9 1
Benzene ND ug/L 05/18/16 19:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 19:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 19:34 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 19:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 19:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 19:34 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 19:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 19:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 19:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 19:34 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 19:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 19:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 19:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 19:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 19:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 19:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 19:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 19:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 19:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 19:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 19:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 19:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.2J ug/L 05/18/16 19:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 19:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 19:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 19:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 19:34 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-1 Lab ID:92298161001 Collected:05/16/16 14:00 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 19:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 19:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 19:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 19:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 19:34 108-10-11000.33 1
Styrene ND ug/L 05/18/16 19:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 19:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 19:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 19:34 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 19:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 19:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 19:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 19:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 19:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 19:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 19:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 19:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 19:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/18/16 19:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %05/18/16 19:34 17060-07-070-130 1
Toluene-d8 (S)100 %05/18/16 19:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-2 Lab ID:92298161002 Collected:05/16/16 13:15 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 4.0J ug/L 05/25/16 10:53 7440-36-005/20/16 10:456.0 3.8 1
Arsenic 39.0 ug/L 05/25/16 10:53 7440-38-205/20/16 10:4510.0 2.5 1
Barium 194 ug/L 05/25/16 10:53 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 10:53 7440-41-705/20/16 10:451.0 0.50 1
Cadmium 1.7 ug/L 05/25/16 10:53 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 10:53 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt 2.5J ug/L 05/25/16 10:53 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 10:53 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 10:53 7439-92-105/20/16 10:4510.0 2.5 1
Nickel 9.1J ug/L 05/25/16 10:53 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 10:53 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 10:53 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 10:53 7440-28-005/20/16 10:455.5 5.0 1
Vanadium 5.5J ug/L 05/25/16 10:53 7440-62-205/20/16 10:4525.0 2.5 1
Zinc 15.6 ug/L 05/25/16 10:53 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 19:51 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 19:51 107-13-12001.9 1
Benzene 2.3 ug/L 05/18/16 19:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 19:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 19:51 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 19:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 19:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 19:51 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 19:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 19:51 56-23-51.0 0.25 1
Chlorobenzene 10.6 ug/L 05/18/16 19:51 108-90-73.0 0.23 1
Chloroethane 0.76J ug/L 05/18/16 19:51 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 19:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 19:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 19:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 19:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 19:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 19:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene 9.0 ug/L 05/18/16 19:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene 16.6 ug/L 05/18/16 19:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 19:51 110-57-61001.0 1
1,1-Dichloroethane 0.65J ug/L 05/18/16 19:51 75-34-35.0 0.32 1
1,2-Dichloroethane 0.77J ug/L 05/18/16 19:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 19:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/18/16 19:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 19:51 156-60-55.0 0.49 1
1,2-Dichloropropane 1.2 ug/L 05/18/16 19:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 19:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 19:51 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-2 Lab ID:92298161002 Collected:05/16/16 13:15 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 19:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 19:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 19:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 19:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 19:51 108-10-11000.33 1
Styrene ND ug/L 05/18/16 19:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 19:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 19:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 19:51 127-18-41.0 0.46 1
Toluene 0.44J ug/L 05/18/16 19:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 19:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 19:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 19:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 19:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 19:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 19:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 19:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 19:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/18/16 19:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %05/18/16 19:51 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 19:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3 Lab ID:92298161003 Collected:05/16/16 12:00 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 21:38 7440-36-005/20/16 10:456.0 3.8 1
Arsenic 9.6J ug/L 05/25/16 21:38 7440-38-2 B05/20/16 10:4510.0 2.5 1
Barium 88.6J ug/L 05/25/16 21:38 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 21:38 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 21:38 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 21:38 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 21:38 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 21:38 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 21:38 7439-92-105/20/16 10:4510.0 2.5 1
Nickel 35.8J ug/L 05/25/16 21:38 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 21:38 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 21:38 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 21:38 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 21:38 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 21:38 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 20:08 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 20:08 107-13-12001.9 1
Benzene 3.4 ug/L 05/18/16 20:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 20:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 20:08 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 20:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 20:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 20:08 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 20:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 20:08 56-23-51.0 0.25 1
Chlorobenzene 1.2J ug/L 05/18/16 20:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 20:08 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 20:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 20:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 20:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 20:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 20:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 20:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 20:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene 6.0 ug/L 05/18/16 20:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 20:08 110-57-61001.0 1
1,1-Dichloroethane 0.57J ug/L 05/18/16 20:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 20:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 20:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 21.8 ug/L 05/18/16 20:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 20:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 20:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 20:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 20:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3 Lab ID:92298161003 Collected:05/16/16 12:00 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 20:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 20:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 20:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 20:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 20:08 108-10-11000.33 1
Styrene ND ug/L 05/18/16 20:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 20:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 20:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 20:08 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 20:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 20:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 20:08 79-00-51.0 0.29 1
Trichloroethene 1.8 ug/L 05/18/16 20:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 20:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 20:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 20:08 108-05-450.0 0.35 1
Vinyl chloride 0.86J ug/L 05/18/16 20:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 20:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %05/18/16 20:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %05/18/16 20:08 17060-07-070-130 1
Toluene-d8 (S)102 %05/18/16 20:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3A Lab ID:92298161004 Collected:05/16/16 12:35 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony 4.7J ug/L 05/25/16 21:46 7440-36-005/20/16 10:456.0 3.8 1
Arsenic 2.8J ug/L 05/25/16 21:46 7440-38-2 B05/20/16 10:4510.0 2.5 1
Barium 457 ug/L 05/25/16 21:46 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 21:46 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 21:46 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 21:46 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt 23.3 ug/L 05/25/16 21:46 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 21:46 7440-50-805/20/16 10:4510.0 2.5 1
Lead 2.8J ug/L 05/25/16 21:46 7439-92-105/20/16 10:4510.0 2.5 1
Nickel 25.4J ug/L 05/25/16 21:46 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 21:46 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 21:46 7440-22-405/20/16 10:4510.0 2.5 1
Thallium 5.7 ug/L 05/25/16 21:46 7440-28-005/20/16 10:455.5 5.0 1
Vanadium 2.9J ug/L 05/25/16 21:46 7440-62-205/20/16 10:4525.0 2.5 1
Zinc 5.6J ug/L 05/25/16 21:46 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 20:25 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 20:25 107-13-12001.9 1
Benzene 1.2 ug/L 05/18/16 20:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 20:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 20:25 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 20:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 20:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 20:25 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 20:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 20:25 56-23-51.0 0.25 1
Chlorobenzene 4.0 ug/L 05/18/16 20:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 20:25 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 20:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 20:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 20:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 20:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 20:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 20:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene 3.6J ug/L 05/18/16 20:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene 12.4 ug/L 05/18/16 20:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 20:25 110-57-61001.0 1
1,1-Dichloroethane 1.1J ug/L 05/18/16 20:25 75-34-35.0 0.32 1
1,2-Dichloroethane 0.32J ug/L 05/18/16 20:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 20:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 18.6 ug/L 05/18/16 20:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 20:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 20:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 20:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 20:25 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3A Lab ID:92298161004 Collected:05/16/16 12:35 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 20:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 20:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 20:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 20:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 20:25 108-10-11000.33 1
Styrene ND ug/L 05/18/16 20:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 20:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 20:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 20:25 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 20:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 20:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 20:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 20:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 20:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 20:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 20:25 108-05-450.0 0.35 1
Vinyl chloride 2.7 ug/L 05/18/16 20:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 20:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/18/16 20:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %05/18/16 20:25 17060-07-070-130 1
Toluene-d8 (S)102 %05/18/16 20:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-4 Lab ID:92298161005 Collected:05/16/16 09:15 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 21:50 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 21:50 7440-38-205/20/16 10:4510.0 2.5 1
Barium 26.7J ug/L 05/25/16 21:50 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 21:50 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 21:50 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 21:50 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 21:50 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 21:50 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 21:50 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 21:50 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 21:50 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 21:50 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 21:50 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 21:50 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 21:50 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 20:42 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 20:42 107-13-12001.9 1
Benzene ND ug/L 05/18/16 20:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 20:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 20:42 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 20:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 20:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 20:42 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 20:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 20:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 20:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 20:42 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 20:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 20:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 20:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 20:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 20:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 20:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 20:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 20:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 20:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 20:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 20:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 20:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/18/16 20:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 20:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 20:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 20:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 20:42 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-4 Lab ID:92298161005 Collected:05/16/16 09:15 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 20:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 20:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 20:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 20:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 20:42 108-10-11000.33 1
Styrene ND ug/L 05/18/16 20:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 20:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 20:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 20:42 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 20:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 20:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 20:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 20:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 20:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 20:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 20:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 20:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 20:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %05/18/16 20:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %05/18/16 20:42 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 20:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-5 Lab ID:92298161006 Collected:05/16/16 08:40 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 21:53 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 21:53 7440-38-205/20/16 10:4510.0 2.5 1
Barium 22.0J ug/L 05/25/16 21:53 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 21:53 7440-41-705/20/16 10:451.0 0.50 1
Cadmium 1.4 ug/L 05/25/16 21:53 7440-43-905/20/16 10:451.0 0.50 1
Chromium 2.9J ug/L 05/25/16 21:53 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 21:53 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 21:53 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 21:53 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 21:53 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 21:53 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 21:53 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 21:53 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 21:53 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 21:53 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 20:59 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 20:59 107-13-12001.9 1
Benzene ND ug/L 05/18/16 20:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 20:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 20:59 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 20:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 20:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 20:59 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 20:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 20:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 20:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 20:59 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 20:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 20:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 20:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 20:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 20:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 20:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 20:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 20:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 20:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 20:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 20:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 20:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/18/16 20:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 20:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 20:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 20:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 20:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-5 Lab ID:92298161006 Collected:05/16/16 08:40 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 20:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 20:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 20:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 20:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 20:59 108-10-11000.33 1
Styrene ND ug/L 05/18/16 20:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 20:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 20:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 20:59 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 20:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 20:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 20:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 20:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 20:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 20:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 20:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 20:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 20:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %05/18/16 20:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %05/18/16 20:59 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 20:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-6 Lab ID:92298161007 Collected:05/16/16 14:40 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 21:56 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 21:56 7440-38-205/20/16 10:4510.0 2.5 1
Barium 79.9J ug/L 05/25/16 21:56 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 21:56 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 21:56 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 21:56 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt 12.1 ug/L 05/25/16 21:56 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 21:56 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 21:56 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 21:56 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 21:56 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 21:56 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 21:56 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 21:56 7440-62-205/20/16 10:4525.0 2.5 1
Zinc 7.1J ug/L 05/25/16 21:56 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 21:16 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 21:16 107-13-12001.9 1
Benzene 0.84J ug/L 05/18/16 21:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 21:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 21:16 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 21:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 21:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 21:16 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 21:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 21:16 56-23-51.0 0.25 1
Chlorobenzene 10.0 ug/L 05/18/16 21:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 21:16 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 21:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 21:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 21:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 21:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 21:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 21:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene 2.5J ug/L 05/18/16 21:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.0 ug/L 05/18/16 21:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 21:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 21:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 21:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 21:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.2J ug/L 05/18/16 21:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 21:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 21:16 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 21:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 21:16 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-6 Lab ID:92298161007 Collected:05/16/16 14:40 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 21:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 21:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 21:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 21:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 21:16 108-10-11000.33 1
Styrene ND ug/L 05/18/16 21:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 21:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 21:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 21:16 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 21:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 21:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 21:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 21:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 21:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 21:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 21:16 108-05-450.0 0.35 1
Vinyl chloride 1.9 ug/L 05/18/16 21:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 21:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %05/18/16 21:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %05/18/16 21:16 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 21:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7S Lab ID:92298161008 Collected:05/16/16 11:00 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 21:59 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 21:59 7440-38-205/20/16 10:4510.0 2.5 1
Barium 73.4J ug/L 05/25/16 21:59 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 21:59 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 21:59 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 21:59 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 21:59 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 21:59 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 21:59 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 21:59 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 21:59 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 21:59 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 21:59 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 21:59 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 21:59 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 21:33 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 21:33 107-13-12001.9 1
Benzene ND ug/L 05/18/16 21:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 21:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 21:33 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 21:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 21:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 21:33 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 21:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 21:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 21:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 21:33 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 21:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 21:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 21:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 21:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 21:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 21:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 21:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 21:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 21:33 110-57-61001.0 1
1,1-Dichloroethane 1.0J ug/L 05/18/16 21:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 21:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 21:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 6.5 ug/L 05/18/16 21:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 21:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 21:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 21:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 21:33 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7S Lab ID:92298161008 Collected:05/16/16 11:00 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 21:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 21:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 21:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 21:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 21:33 108-10-11000.33 1
Styrene ND ug/L 05/18/16 21:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 21:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 21:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 21:33 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 21:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 21:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 21:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 21:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 21:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 21:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 21:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 21:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 21:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %05/18/16 21:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %05/18/16 21:33 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 21:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7D Lab ID:92298161009 Collected:05/16/16 10:15 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 22:02 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 22:02 7440-38-205/20/16 10:4510.0 2.5 1
Barium 11.5J ug/L 05/25/16 22:02 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 22:02 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 22:02 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 22:02 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 22:02 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 22:02 7440-50-805/20/16 10:4510.0 2.5 1
Lead 4.8J ug/L 05/25/16 22:02 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 22:02 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 22:02 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 22:02 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 22:02 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 22:02 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 22:02 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 21:50 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 21:50 107-13-12001.9 1
Benzene ND ug/L 05/18/16 21:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 21:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 21:50 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 21:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 21:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 21:50 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 21:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 21:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 21:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 21:50 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 21:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 21:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 21:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 21:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 21:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 21:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 21:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 21:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 21:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 21:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 21:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 21:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.78J ug/L 05/18/16 21:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 21:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 21:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 21:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 21:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7D Lab ID:92298161009 Collected:05/16/16 10:15 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 21:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 21:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 21:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 21:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 21:50 108-10-11000.33 1
Styrene ND ug/L 05/18/16 21:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 21:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 21:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 21:50 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 21:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 21:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 21:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 21:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 21:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 21:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 21:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 21:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 21:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %05/18/16 21:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %05/18/16 21:50 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 21:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-8 Lab ID:92298161010 Collected:05/16/16 15:30 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 22:14 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 22:14 7440-38-205/20/16 10:4510.0 2.5 1
Barium 65.8J ug/L 05/25/16 22:14 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 22:14 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 22:14 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 22:14 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt 4.0J ug/L 05/25/16 22:14 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 22:14 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 22:14 7439-92-105/20/16 10:4510.0 2.5 1
Nickel 13.4J ug/L 05/25/16 22:14 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 22:14 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 22:14 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 22:14 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 22:14 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 22:14 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 22:07 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 22:07 107-13-12001.9 1
Benzene 1.5 ug/L 05/18/16 22:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 22:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 22:07 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 22:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 22:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 22:07 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 22:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 22:07 56-23-51.0 0.25 1
Chlorobenzene 1.3J ug/L 05/18/16 22:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 22:07 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 22:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 22:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 22:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 22:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 22:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 22:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.2J ug/L 05/18/16 22:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.2 ug/L 05/18/16 22:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 22:07 110-57-61001.0 1
1,1-Dichloroethane 0.87J ug/L 05/18/16 22:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 22:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 22:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 15.2 ug/L 05/18/16 22:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 22:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 22:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 22:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 22:07 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-8 Lab ID:92298161010 Collected:05/16/16 15:30 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 22:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 22:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 22:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 22:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 22:07 108-10-11000.33 1
Styrene ND ug/L 05/18/16 22:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 22:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 22:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 22:07 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 22:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 22:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 22:07 79-00-51.0 0.29 1
Trichloroethene 1.0 ug/L 05/18/16 22:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 22:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 22:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 22:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 22:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 22:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %05/18/16 22:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %05/18/16 22:07 17060-07-070-130 1
Toluene-d8 (S)100 %05/18/16 22:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-1 Lab ID:92298161011 Collected:05/16/16 09:35 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 22:18 7440-36-005/20/16 10:456.0 3.8 1
Arsenic 2.8J ug/L 05/25/16 22:18 7440-38-2 B05/20/16 10:4510.0 2.5 1
Barium 16.7J ug/L 05/25/16 22:18 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 22:18 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 22:18 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 22:18 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 22:18 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 22:18 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 22:18 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 22:18 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 22:18 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 22:18 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 22:18 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 22:18 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 22:18 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 22:41 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 22:41 107-13-12001.9 1
Benzene ND ug/L 05/18/16 22:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 22:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 22:41 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 22:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 22:41 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 22:41 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 22:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 22:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 22:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 22:41 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 22:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 22:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 22:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 22:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 22:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 22:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 22:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 22:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 22:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 22:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 22:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 22:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/18/16 22:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 22:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 22:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 22:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 22:41 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-1 Lab ID:92298161011 Collected:05/16/16 09:35 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 22:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 22:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 22:41 74-88-4 M110.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 22:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 22:41 108-10-11000.33 1
Styrene ND ug/L 05/18/16 22:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 22:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 22:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 22:41 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 22:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 22:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 22:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 22:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 22:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 22:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 22:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 22:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 22:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %05/18/16 22:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %05/18/16 22:41 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/16 22:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-2 Lab ID:92298161012 Collected:05/16/16 11:25 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 05/25/16 22:21 7440-36-005/20/16 10:456.0 3.8 1
Arsenic ND ug/L 05/25/16 22:21 7440-38-205/20/16 10:4510.0 2.5 1
Barium 16.3J ug/L 05/25/16 22:21 7440-39-305/20/16 10:451002.5 1
Beryllium ND ug/L 05/25/16 22:21 7440-41-705/20/16 10:451.0 0.50 1
Cadmium ND ug/L 05/25/16 22:21 7440-43-905/20/16 10:451.0 0.50 1
Chromium ND ug/L 05/25/16 22:21 7440-47-305/20/16 10:4510.0 2.5 1
Cobalt ND ug/L 05/25/16 22:21 7440-48-405/20/16 10:4510.0 2.5 1
Copper ND ug/L 05/25/16 22:21 7440-50-805/20/16 10:4510.0 2.5 1
Lead ND ug/L 05/25/16 22:21 7439-92-105/20/16 10:4510.0 2.5 1
Nickel ND ug/L 05/25/16 22:21 7440-02-005/20/16 10:4550.0 2.5 1
Selenium ND ug/L 05/25/16 22:21 7782-49-205/20/16 10:4510.0 5.0 1
Silver ND ug/L 05/25/16 22:21 7440-22-405/20/16 10:4510.0 2.5 1
Thallium ND ug/L 05/25/16 22:21 7440-28-005/20/16 10:455.5 5.0 1
Vanadium ND ug/L 05/25/16 22:21 7440-62-205/20/16 10:4525.0 2.5 1
Zinc ND ug/L 05/25/16 22:21 7440-66-605/20/16 10:4510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/18/16 23:15 67-64-110010.0 1
Acrylonitrile ND ug/L 05/18/16 23:15 107-13-12001.9 1
Benzene ND ug/L 05/18/16 23:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/18/16 23:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/18/16 23:15 75-27-41.0 0.18 1
Bromoform ND ug/L 05/18/16 23:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/18/16 23:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/18/16 23:15 78-93-31000.96 1
Carbon disulfide ND ug/L 05/18/16 23:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/18/16 23:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/18/16 23:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/18/16 23:15 75-00-310.0 0.54 1
Chloroform ND ug/L 05/18/16 23:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/18/16 23:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/16 23:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/18/16 23:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/16 23:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/18/16 23:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/18/16 23:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 05/18/16 23:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/18/16 23:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 05/18/16 23:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/18/16 23:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/18/16 23:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/18/16 23:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/18/16 23:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/18/16 23:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 05/18/16 23:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/18/16 23:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-2 Lab ID:92298161012 Collected:05/16/16 11:25 Received:05/18/16 15:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 05/18/16 23:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 05/18/16 23:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/18/16 23:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 05/18/16 23:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/16 23:15 108-10-11000.33 1
Styrene ND ug/L 05/18/16 23:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/16 23:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/16 23:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/18/16 23:15 127-18-41.0 0.46 1
Toluene ND ug/L 05/18/16 23:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 05/18/16 23:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/18/16 23:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/18/16 23:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/18/16 23:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/18/16 23:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/18/16 23:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/18/16 23:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/18/16 23:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %05/18/16 23:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %05/18/16 23:15 17060-07-070-130 1
Toluene-d8 (S)100 %05/18/16 23:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/21768
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92298161001, 92298161002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1737616
Associated Lab Samples:92298161001, 92298161002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 05/25/16 09:233.8
Arsenic ug/L ND 10.0 05/25/16 09:232.5
Barium ug/L ND 100 05/25/16 09:232.5
Beryllium ug/L ND 1.0 05/25/16 09:230.50
Cadmium ug/L ND 1.0 05/25/16 09:230.50
Chromium ug/L ND 10.0 05/25/16 09:232.5
Cobalt ug/L ND 10.0 05/25/16 09:232.5
Copper ug/L ND 10.0 05/25/16 09:232.5
Lead ug/L ND 10.0 05/25/16 09:232.5
Nickel ug/L ND 50.0 05/25/16 09:232.5
Selenium ug/L ND 10.0 05/25/16 09:235.0
Silver ug/L ND 10.0 05/25/16 09:232.5
Thallium ug/L ND 5.5 05/25/16 09:235.0
Vanadium ug/L ND 25.0 05/25/16 09:232.5
Zinc ug/L ND 10.0 05/26/16 03:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1737617LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 478500 96 80-120
Arsenic ug/L 469500 94 80-120
Barium ug/L 479500 96 80-120
Beryllium ug/L 484500 97 80-120
Cadmium ug/L 482500 96 80-120
Chromium ug/L 484500 97 80-120
Cobalt ug/L 476500 95 80-120
Copper ug/L 492500 98 80-120
Lead ug/L 473500 95 80-120
Nickel ug/L 483500 97 80-120
Selenium ug/L 473500 95 80-120
Silver ug/L 246250 99 80-120
Thallium ug/L 466500 93 80-120
Vanadium ug/L 482500 96 80-120
Zinc ug/L 480500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1737618MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92298058007
1737619
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-12597 2 25500ND495487
Arsenic ug/L 500 97 75-12597 0 25500ND488488
Barium ug/L 500 97 75-12596 1 25500144630626
Beryllium ug/L 500 100 75-12599 1 25500ND501494
Cadmium ug/L 500 98 75-12597 1 25500ND490487
Chromium ug/L 500 98 75-12598 0 25500ND490489
Cobalt ug/L 500 95 75-12594 1 25500ND473470
Copper ug/L 500 100 75-12599 1 25500ND501498
Lead ug/L 500 95 75-12595 0 25500ND475473
Nickel ug/L 500 95 75-12595 1 255005.3 483 479
Selenium ug/L 500 96 75-12596 0 25500ND483482
Silver ug/L 250 100 75-12599 1 25250ND251248
Thallium ug/L 500 95 75-12595 1 25500ND476478
Vanadium ug/L 500 99 75-12599 1 25500ND499495
Zinc ug/L 500 96 75-12596 0 25500ND486483
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/21769
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92298161003, 92298161004, 92298161005, 92298161006, 92298161007, 92298161008, 92298161009,
92298161010, 92298161011, 92298161012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1737620
Associated Lab Samples:92298161003, 92298161004, 92298161005, 92298161006, 92298161007, 92298161008, 92298161009,
92298161010, 92298161011, 92298161012
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 05/25/16 21:223.8
Arsenic ug/L 5.0J 10.0 05/25/16 21:222.5
Barium ug/L ND 100 05/25/16 21:222.5
Beryllium ug/L ND 1.0 05/25/16 21:220.50
Cadmium ug/L ND 1.0 05/25/16 21:220.50
Chromium ug/L ND 10.0 05/25/16 21:222.5
Cobalt ug/L ND 10.0 05/25/16 21:222.5
Copper ug/L ND 10.0 05/25/16 21:222.5
Lead ug/L ND 10.0 05/25/16 21:222.5
Nickel ug/L ND 50.0 05/25/16 21:222.5
Selenium ug/L ND 10.0 05/25/16 21:225.0
Silver ug/L ND 10.0 05/25/16 21:222.5
Thallium ug/L ND 5.5 05/25/16 21:225.0
Vanadium ug/L ND 25.0 05/25/16 21:222.5
Zinc ug/L ND 10.0 05/25/16 21:225.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1737621LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 463500 93 80-120
Arsenic ug/L 449500 90 80-120
Barium ug/L 514500 103 80-120
Beryllium ug/L 472500 94 80-120
Cadmium ug/L 480500 96 80-120
Chromium ug/L 491500 98 80-120
Cobalt ug/L 465500 93 80-120
Copper ug/L 500500 100 80-120
Lead ug/L 463500 93 80-120
Nickel ug/L 482500 96 80-120
Selenium ug/L 458500 92 80-120
Silver ug/L 244250 98 80-120
Thallium ug/L 446500 89 80-120
Vanadium ug/L 482500 96 80-120
Zinc ug/L 452500 90 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1737622MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92298161003
1737623
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12594 1 25500ND469473
Arsenic ug/L 500 90 75-12591 1 255009.6J 461 464
Barium ug/L 500 102 75-125103 1 2550088.6J 599 605
Beryllium ug/L 500 95 75-12596 2 25500ND474482
Cadmium ug/L 500 96 75-12597 1 25500ND481486
Chromium ug/L 500 98 75-12599 1 25500ND489495
Cobalt ug/L 500 91 75-12592 1 25500ND457461
Copper ug/L 500 99 75-125101 1 25500ND498504
Lead ug/L 500 91 75-12592 1 25500ND456460
Nickel ug/L 500 94 75-12595 1 2550035.8J 505 510
Selenium ug/L 500 92 75-12592 1 25500ND458462
Silver ug/L 250 97 75-12599 1 25250ND244246
Thallium ug/L 500 88 75-12590 2 25500ND443451
Vanadium ug/L 500 97 75-12598 1 25500ND485490
Zinc ug/L 500 89 75-12590 1 25500ND451456
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36901
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92298161001, 92298161002, 92298161003, 92298161004, 92298161005, 92298161006, 92298161007,
92298161008, 92298161009, 92298161010, 92298161011, 92298161012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1737288
Associated Lab Samples:92298161001, 92298161002, 92298161003, 92298161004, 92298161005, 92298161006, 92298161007,
92298161008, 92298161009, 92298161010, 92298161011, 92298161012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/18/16 13:530.33
1,1,1-Trichloroethane ug/L ND 1.0 05/18/16 13:530.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/18/16 13:530.40
1,1,2-Trichloroethane ug/L ND 1.0 05/18/16 13:530.29
1,1-Dichloroethane ug/L ND 5.0 05/18/16 13:530.32
1,1-Dichloroethene ug/L ND 5.0 05/18/16 13:530.56
1,2,3-Trichloropropane ug/L ND 1.0 05/18/16 13:530.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/18/16 13:532.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/18/16 13:530.27
1,2-Dichlorobenzene ug/L ND 5.0 05/18/16 13:530.30
1,2-Dichloroethane ug/L ND 1.0 05/18/16 13:530.24
1,2-Dichloropropane ug/L ND 1.0 05/18/16 13:530.27
1,4-Dichlorobenzene ug/L ND 1.0 05/18/16 13:530.33
2-Butanone (MEK)ug/L ND 100 05/18/16 13:530.96
2-Hexanone ug/L ND 50.0 05/18/16 13:530.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 05/18/16 13:530.33
Acetone ug/L ND 100 05/18/16 13:5310.0
Acrylonitrile ug/L ND 200 05/18/16 13:531.9
Benzene ug/L ND 1.0 05/18/16 13:530.25
Bromochloromethane ug/L ND 3.0 05/18/16 13:530.17
Bromodichloromethane ug/L ND 1.0 05/18/16 13:530.18
Bromoform ug/L ND 3.0 05/18/16 13:530.26
Bromomethane ug/L ND 10.0 05/18/16 13:530.29
Carbon disulfide ug/L ND 100 05/18/16 13:531.2
Carbon tetrachloride ug/L ND 1.0 05/18/16 13:530.25
Chlorobenzene ug/L ND 3.0 05/18/16 13:530.23
Chloroethane ug/L ND 10.0 05/18/16 13:530.54
Chloroform ug/L ND 5.0 05/18/16 13:530.14
Chloromethane ug/L ND 1.0 05/18/16 13:530.11
cis-1,2-Dichloroethene ug/L ND 5.0 05/18/16 13:530.19
cis-1,3-Dichloropropene ug/L ND 1.0 05/18/16 13:530.13
Dibromochloromethane ug/L ND 3.0 05/18/16 13:530.21
Dibromomethane ug/L ND 10.0 05/18/16 13:530.21
Ethylbenzene ug/L ND 1.0 05/18/16 13:530.30
Iodomethane ug/L ND 10.0 05/18/16 13:530.32
Methylene Chloride ug/L ND 1.0 05/18/16 13:530.97
Styrene ug/L ND 1.0 05/18/16 13:530.26
Tetrachloroethene ug/L ND 1.0 05/18/16 13:530.46
Toluene ug/L ND 1.0 05/18/16 13:530.26
trans-1,2-Dichloroethene ug/L ND 5.0 05/18/16 13:530.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1737288
Associated Lab Samples:92298161001, 92298161002, 92298161003, 92298161004, 92298161005, 92298161006, 92298161007,
92298161008, 92298161009, 92298161010, 92298161011, 92298161012
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 05/18/16 13:530.26
trans-1,4-Dichloro-2-butene ug/L ND 100 05/18/16 13:531.0
Trichloroethene ug/L ND 1.0 05/18/16 13:530.47
Trichlorofluoromethane ug/L ND 1.0 05/18/16 13:530.20
Vinyl acetate ug/L ND 50.0 05/18/16 13:530.35
Vinyl chloride ug/L ND 1.0 05/18/16 13:530.62
Xylene (Total)ug/L ND 5.0 05/18/16 13:530.66
1,2-Dichloroethane-d4 (S)%102 70-130 05/18/16 13:53
4-Bromofluorobenzene (S)%102 70-130 05/18/16 13:53
Toluene-d8 (S)%101 70-130 05/18/16 13:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1737289LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.950 100 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 48.850 98 79-124
1,1,2-Trichloroethane ug/L 48.950 98 85-125
1,1-Dichloroethane ug/L 47.250 94 73-126
1,1-Dichloroethene ug/L 51.050 102 66-135
1,2,3-Trichloropropane ug/L 47.950 96 75-130
1,2-Dibromo-3-chloropropane ug/L 50.450 101 71-133
1,2-Dibromoethane (EDB)ug/L 53.450 107 83-124
1,2-Dichlorobenzene ug/L 51.350 103 80-133
1,2-Dichloroethane ug/L 46.050 92 67-128
1,2-Dichloropropane ug/L 49.550 99 75-132
1,4-Dichlorobenzene ug/L 51.450 103 78-130
2-Butanone (MEK)ug/L 105100 105 61-144
2-Hexanone ug/L 110100 110 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 103100 103 48-146
Acrylonitrile ug/L 249250 100 40-160
Benzene ug/L 50.550 101 80-125
Bromochloromethane ug/L 47.450 95 71-125
Bromodichloromethane ug/L 48.450 97 78-124
Bromoform ug/L 43.750 87 71-128
Bromomethane ug/L 44.650 89 40-160
Carbon disulfide ug/L 50.6J50 101 50-160
Carbon tetrachloride ug/L 48.850 98 69-131
Chlorobenzene ug/L 50.550 101 81-122
Chloroethane ug/L 49.950 100 39-148
Chloroform ug/L 47.150 94 73-127
Chloromethane ug/L 41.950 84 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1737289LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.250 96 74-124
cis-1,3-Dichloropropene ug/L 52.350 105 72-132
Dibromochloromethane ug/L 50.850 102 78-125
Dibromomethane ug/L 50.850 102 82-120
Ethylbenzene ug/L 48.550 97 79-121
Iodomethane ug/L 85.8100 86 39-154
Methylene Chloride ug/L 50.550 101 64-133
Styrene ug/L 51.250 102 84-126
Tetrachloroethene ug/L 46.950 94 78-122
Toluene ug/L 49.350 99 80-121
trans-1,2-Dichloroethene ug/L 50.250 100 71-127
trans-1,3-Dichloropropene ug/L 50.050 100 69-141
trans-1,4-Dichloro-2-butene ug/L 52.6J50 105 40-160
Trichloroethene ug/L 48.250 96 78-122
Trichlorofluoromethane ug/L 49.850 100 53-137
Vinyl acetate ug/L 105100 105 40-160
Vinyl chloride ug/L 47.250 94 58-137
Xylene (Total)ug/L 144150 96 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1737291MATRIX SPIKE SAMPLE:
MSSpike
Result
92298161011
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 22.620 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.820 104 70-130ND
1,1,2-Trichloroethane ug/L 21.420 107 70-130ND
1,1-Dichloroethane ug/L 22.120 110 70-130ND
1,1-Dichloroethene ug/L 24.520 122 70-166ND
1,2,3-Trichloropropane ug/L 20.020 100 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.720 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.920 109 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 20.920 104 70-130ND
1,2-Dichloropropane ug/L 22.120 110 70-130ND
1,4-Dichlorobenzene ug/L 22.220 111 70-130ND
2-Butanone (MEK)ug/L 46.8J40 117 70-130ND
2-Hexanone ug/L 42.6J40 107 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.5J40 104 70-130ND
Acetone ug/L 43.2J40 108 70-130ND
Acrylonitrile ug/L 113J100 113 70-130ND
Benzene ug/L 22.920 115 70-148ND
Bromochloromethane ug/L 22.620 113 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1737291MATRIX SPIKE SAMPLE:
MSSpike
Result
92298161011
Bromodichloromethane ug/L 21.120 106 70-130ND
Bromoform ug/L 19.220 96 70-130ND
Bromomethane ug/L 12.0 M1206070-130ND
Carbon disulfide ug/L 24.9J20 125 70-130ND
Carbon tetrachloride ug/L 23.520 117 70-130ND
Chlorobenzene ug/L 22.720 113 70-146ND
Chloroethane ug/L 23.620 118 70-130ND
Chloroform ug/L 21.720 109 70-130ND
Chloromethane ug/L 18.820 94 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 21.220 106 70-130ND
Dibromochloromethane ug/L 21.220 106 70-130ND
Dibromomethane ug/L 21.320 106 70-130ND
Ethylbenzene ug/L 21.920 110 70-130ND
Iodomethane ug/L 22.9 M1405770-130ND
Methylene Chloride ug/L 22.320 112 70-130ND
Styrene ug/L 22.420 112 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 22.120 110 70-155ND
trans-1,2-Dichloroethene ug/L 23.520 118 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.7J20 99 70-130ND
Trichloroethene ug/L 22.320 111 69-151ND
Trichlorofluoromethane ug/L 24.420 122 70-130ND
Vinyl acetate ug/L 41.5J40 104 70-130ND
Vinyl chloride ug/L 22.420 112 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92298161010
1737290SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.88J 300.87J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 1.2J 2 301.2J
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92298161010
1737290SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 2.2 1 302.2
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 1.6 4 301.5
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 1.4J 5 301.3J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 15.1 1 3015.2
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 1.0 0 301.0
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%104 0103
4-Bromofluorobenzene (S)%99 2102
Toluene-d8 (S)%101 1100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 41
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 41
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92298161
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92298161001 MPRP/21768 ICP/19530MW-1 EPA 3010A EPA 6010
92298161002 MPRP/21768 ICP/19530MW-2 EPA 3010A EPA 6010
92298161003 MPRP/21769 ICP/19531MW-3 EPA 3010A EPA 6010
92298161004 MPRP/21769 ICP/19531MW-3A EPA 3010A EPA 6010
92298161005 MPRP/21769 ICP/19531MW-4 EPA 3010A EPA 6010
92298161006 MPRP/21769 ICP/19531MW-5 EPA 3010A EPA 6010
92298161007 MPRP/21769 ICP/19531MW-6 EPA 3010A EPA 6010
92298161008 MPRP/21769 ICP/19531MW-7S EPA 3010A EPA 6010
92298161009 MPRP/21769 ICP/19531MW-7D EPA 3010A EPA 6010
92298161010 MPRP/21769 ICP/19531MW-8 EPA 3010A EPA 6010
92298161011 MPRP/21769 ICP/19531SW-1 EPA 3010A EPA 6010
92298161012 MPRP/21769 ICP/19531SW-2 EPA 3010A EPA 6010
92298161001 MSV/36901MW-1 EPA 8260
92298161002 MSV/36901MW-2 EPA 8260
92298161003 MSV/36901MW-3 EPA 8260
92298161004 MSV/36901MW-3A EPA 8260
92298161005 MSV/36901MW-4 EPA 8260
92298161006 MSV/36901MW-5 EPA 8260
92298161007 MSV/36901MW-6 EPA 8260
92298161008 MSV/36901MW-7S EPA 8260
92298161009 MSV/36901MW-7D EPA 8260
92298161010 MSV/36901MW-8 EPA 8260
92298161011 MSV/36901SW-1 EPA 8260
92298161012 MSV/36901SW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/26/2016 04:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 41
Page 40 of 41
Page 41 of 41
Appendix B
Field Sampling Parameter Data Sheet(s)