8603_SurryCountyElkin_GWMR_DIN28069_20161020

Surry County Closed C&D and Closed MSWLF, Elkin
Elkin, North Carolina
October 2016
Permit Number: 86-03
Semi-Annual Water Quality Monitoring Report
Prepared for
PO Box 97
Garner, NC 27529
License No, C-0281
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G16025.0
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedure Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Groundwater Samples Page 2
Surface Water Samples Page 2
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 3
FIGURES
Topographic Map with Site Location Figure 1
Single-Day Potentiometric Map of Uppermost Aquifer Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above Established SWSL, GWP, 2L, 2B or MCL (Appendix I) Table 5
Hydrologic Properties at Monitoring Well Locations Table 6
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
January 16, 2017
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Elkin
Permit No. 86-03
MESCO Project No. G16025.0
Event Date(s): October 20, 2016
Dear Ms. Drummond;
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the fall 2016 event performed at the Surry County closed construction and
demolition (C&D) and closed municipal solid waste landfill (MSWLF). NCDEQ Solid Waste Rules 15A NCAC
13B.1632 requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents
the quality of the ground and surface waters during this monitoring event performed on October 20, 2016.
Laboratory analytical results indicate volatile organic compounds (VOCs) persist within three wells that monitor the
uppermost aquifer. The surface water samples collected from the discharge feature remain unimpacted.
Background
The Surry County closed C&D and MSWLF, permit #86-03, is located at Elkin Landfill Road (SR 1191), Elkin,
Surry County, North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to
operating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two units. The first
area was closed prior to October 1991 with a 24 inch final soil cover. The second area was closed with a cohesive
cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec, and 18 inches of erosive layer
prior to December 31, 1998 in accordance with the Transition Plan. C&D was placed on top of the cohesive capped
unit until 2008.
This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and
as a condition of the post-closure portion of the permit to operate. Water quality at this facility has been monitored
at least semi-annually since 1989 with historical data available since 1994. The SWS approved a modification to the
assessment monitoring program on October 15, 2014 (DIN:21983) which entails a subset of wells be sampled for
Appendix II parameters once every three years.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums, this report contains sampling procedures, field and laboratory results, ground/surface water
characterization, and findings. Well construction summary table, field observations table, field parameter data table,
sampling and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates
table, potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed
herein.

Sampling Procedure
MESCO personnel performed this sampling event utilizing portable monitoring methodology in accordance with the
site-specific Sampling and Analysis Plan (SAP) and the NCDENR SWS guidance document Solid Waste SectionGuidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. Water samples were collected
from nine downgradient groundwater monitoring wells (MW-2, MW-3, MW-3A, MW-4, MW-5, MW-6, MW-7S,
MW-7D and MW-8), one background well (MW-1), and two surface water points (SW-1 and SW-2). Monitoring
locations are shown on the single-day potentiometric map (Figure 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function andintegrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times
the volume of standing water in the well or until dry. Surface water samples were collected from Snow Creek
discharge feature at previously designated locations. During well purging and surface water sample collection therequired field parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved
containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-
certified laboratory under proper chain of custody (C-O-C) protocols within the specified hold times for each
analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, specific conductance,
temperature and visual turbidity. MW-7D exhibited a higher than normal pH and water level which is likely caused
a reaction with the limestone in the grout. A summary of the field parameter data is presented in Table 3 and the
field sampling data sheet is enclosed in Appendix B.
Laboratory Results
All water samples were analyzed for the Appendix I list of VOCs and total unfiltered metals listed in 40 CFR 258.
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the laboratory analysis. A
sampling and analysis table summarizing the locations, constituents, and methods is presented as Table 4.
Laboratory results and C-O-Cs are presented in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L) or Maximum Contaminant Levels (MCL) also recognized as “Federal
Primary Drinking Water Standards”.
Groundwater Samples
The only inorganic constituents detected in excess of its respective 2L/GWP Standard were total arsenic and total
vanadium in sample MW-2.
One or more Appendix I VOC(s) were detected in quantifiable concentrations above their respective 2L Standards
in samples collected from MW-2, MW-3 and MW-3A. Inconsistent with previous events contaminants were not
detected above 2L/GWP Standards in samples collected from MW-6 and MW-8, located along the northern property
boundary.
Surface Water Samples
Target constituent(s) were not detected in either surface water sample in concentrations exceeding the SWSL or
applicable 2B Standard.
Groundwater and Surface Water Characterization
A single-day potentiometric map constructed from groundwater levels collected during this event is presented as
Figure 2. Groundwater flow rates and directions were calculated and are included in Table 6. Groundwater flows
generally southwest, towards the Snow Creek discharge feature. Groundwater average linear velocity rates
calculated from modified Darcy's equation indicate flow rates ranged from approximately 17 ft/yr (MW-3A) to 722
ft/yr (MW-6). Groundwater average linear velocity rates averaged approximately 211 ft/yr in wells screened in theregolith aquifer and 231 ft./yr. in the wells screened in the upper bedrock. Snow Creek, monitored at SW-1 and
SW-2, was visually observed to have a moderate gage height, moderate volume and low turbidity.
2
Figures
Topographic Map with Site Location
Surry County Closed MSW/C&D Landfill - Elkin
FIGURE 1
QUADRANGLE LEGEND
1” = 2000'
Landfill Road (Off Joe Mill Ln SR 1121)
Elkin, NC 28621
Lat:36-17-49.4007
Long:-80-46-20.6499
Northing:931704.33
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Tables
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
October 20, 2016
Latitude Longitude
(inches)(ft)
MW-1 11/28/89 4 74.56 64.56 10 Soil 1042 1041 985 53.88 36.29711 -80.77236
MW-2 11/08/89 4 79 69 10 Soil 948 947 890 57.65 36.29572 -80.77620
MW-3 11/28/89 4 63 53 10 Soil 932 931 881 50.88 36.29362 -80.77646
MW-3A 09/16/94 2 40 24 16 Fractured Rock 927 924 894 32.09 36.29457 -80.77675
MW-4 09/15/94 2 29 13 16 Fractured Rock 933 929 921 11.53 36.29379 -80.77528
MW-5 09/15/94 2 31 16 15 Fractured Rock 949 845 937 11.50 36.29450 -80.77456
MW-6 09/15/94 2 66 51 15 Fractured Rock 1005 1002 954 50.25 36.29780 -80.77270
MW-7S 06/05/01 2 24 9 15 Fractured Rock 901 889 890 11.58 36.29407 80.77730
MW-7D 06/05/01 2 90 80 10 Fractured Rock 901 889 895 9.25 36.29407 80.77730
MW-8 06/04/01 2 67 52 15 Fractured Rock 1015 1013 973 40.78 36.29739 -80.77246
NOTE:
Monitoring Well Date Installed
Well Diameter
Total Well Depth
Top of Screen Depth
Screen Length Geology of Screened Interval
Top of Casing Elevation
Ground Elevation Groundwater Elevation Depth to Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 2
Field Observations of Monitoring Locations
October 20, 2016
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes 4” Diameter
MW-2 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge, hasp cracked
MW-3 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge
MW-3A Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-6 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-7S Yes Yes Yes Yes Yes Yes
MW-7D Yes Yes Yes Yes Yes Yes pH elevated likely grout intrusion
MW-8 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----
SW-2 Yes -----
Any unusual field conditions, observations, or events:
Facility no longer in operation or occupied since transfer station closed in ~ June 2010.
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears to
be Effective
Mod. gage & mod flow
Mod gage & mod flow
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 3
Field Parameter Data Summary
October 20, 2016
Parameter Temp.ORP DO pH TDS
Units C mg/L SU mg/L %/Vol Visual
MW-1 53.88 988.12 1042.00 17.6 NR NR 5.9 90 NR NR Clear
MW-2 57.65 890.35 948.00 16.3 NR NR 6.5 1820 NR NR Slight
MW-3 50.88 881.12 932.00 14.9 NR NR 5.9 520 NR NR Clear
MW-3A 32.09 894.41 926.50 15.2 NR NR 6.2 1430 NR NR Clear
MW-4 11.53 920.97 932.50 15.3 NR NR 6.4 90 NR NR Clear
MW-5 11.50 937.00 948.50 15.2 NR NR 6.4 80 NR NR Clear
MW-6 50.25 954.25 1004.50 15.4 NR NR 6.1 60 NR NR Clear
MW-7S 11.58 889.43 901.01 15.5 NR NR 6.5 460 NR NR Clear
MW-7D 9.25 891.70 900.95 15.1 NR NR 7.7 320 NR NR Clear
MW-8 40.78 974.09 1014.87 15.3 NR NR 6.7 200 NR NR Clear
Minimum 9.25 881.12 900.95 14.9 NR NR 5.9 60 NR NR Clear
Average 32.94 922.14 955.08 15.6 NR NR 6.4 507 NR NR Clear
Maximum 57.65 988.12 1042.00 17.6 NR NR 7.7 1820 NR NR Slight
SW-1 ---13.8 NR NR 7.1 130 NR -Clear
SW-2 ---13.2 NR NR 6.9 150 NR -Clear
Minimum ---13.2 NR NR 6.9 130 NR -Clear
Average ---13.5 NR NR 7.0 140 NR -Clear
Maximum ---13.8 NR NR 7.1 150 NR -Clear
NR = No Reading attempted
* = Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
Depth to
Water
Water
Elevation*
TOC
Elevation*
Specific
Conductance
Methane Gas in
Well Headspace
Turbidity of
Metals Sample
ft (btoc)ft (amsl)ft (amsl)mV umhos/cm
btoc = below top of casing
amsl = above mean sea level
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 4
Sampling and Analysis Summary
October 20, 2016
App. I Field Parameter
T o t a l M e t a l s
T e m p e r a t u r e
C o n d u c t i v i t y
T o t a l D i s s o l v e d S o l i d s (T D S )
p H T u r b i d i t y
L a b E P A 8 2 6 0 B
L a b E P A 6 0 0 0 /7 0 0 0
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d M e t e r
F i e l d V i s u a l
MW-1 x x x x x x x
MW-2 x x x x x x x
MW-3 x x x x x x x
MW-3A x x x x x x x
MW-4 x x x x x x x
MW-5 x x x x x x x
MW-6 x x x x x x x
MW-7S x x x x x x x
MW-7D x x x x x x x
MW-8 x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
App I & II = List from current 40 CFR 258
All wells listed on SAP presented
V O C s
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 2
Table 5
October 20, 2016
Result Unit
MW-2 10/20/16 13.2 0.33 1 6 75 L &/or LFG
MW-2 10/20/16 0.61j 0.24 1 0.4 5 L &/or LFG
MW-2 10/20/16 0.9j 0.27 1 0.6 5 L &/or LFG
MW-2 Benzene 10/20/16 2.2 0.25 1 1 5 L &/or LFG
MW-2 Arsenic,total 10/20/16 28.1 2.5 10 10 10 N
MW-2 Vanadium,total 10/20/16 5.1j 2.5 25 3.5 NE N
MW-2 Barium,total 10/20/16 234 2.5 100 700 2000
MW-2 Zinc,total 10/20/16 21.2 5 10 1003 NE
MW-2 10/20/16 8.9 0.23 3 50 100
MW-2 10/20/16 7.3 0.3 5 24 NE
MW-3 Benzene 10/20/16 3.5 0.25 1 1 5 L &/or LFG
MW-3 Vinyl chloride 10/20/16 0.76j 0.62 1 0.03 2 L &/or LFG
MW-3 Cadmium,total 10/20/16 1.9 0.5 1 2 5
MW-3 Zinc,total 10/20/16 12.9 5 10 1004 NE
MW-3 Copper,total 10/20/16 13 2.5 10 1000 NE
MW-3 10/20/16 5.1 0.33 1 6 75
MW-3 10/20/16 18.9 0.19 5 70 70
MW-3 10/20/16 2.1 0.47 1 3 5
MW-3A 10/20/16 14.5 0.33 1 6 75 L &/or LFG
MW-3A Benzene 10/20/16 1.3 0.25 1 1 5 L &/or LFG
MW-3A Vinyl chloride 10/20/16 2.6 0.62 1 0.03 2 L &/or LFG
MW-3A Barium,total 10/20/16 449 2.5 100 700 2000
MW-3A Cobalt,total 10/20/16 50.8 2.5 10 70 NE
MW-3A 10/20/16 4.7 0.23 3 50 100
MW-3A 10/20/16 18.4 0.19 5 70 70
MW-4 Cadmium,total 10/20/16 1.6 0.5 1 2 5
MW-6 Cobalt,total 10/20/16 17.6 2.5 10 70 NE
MW-6 10/20/16 3.9 0.23 3 50 100
MW-6 10/20/16 2.3 0.33 1 6 75
Detections in Water Samples above SWSL, GWP, 2L, 2B or MCL (Appendix I)
Sample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
1,4-Dichlorobenzene ug/L
1,2-Dichloroethane ug/L
1,2-Dichloropropane ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
1,2-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
Trichloroethene ug/L
1,4-Dichlorobenzene ug/L
ug/L
ug/L
ug/L
ug/L
Chlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
ug/L
ug/L
Chlorobenzene ug/L
1,4-Dichlorobenzene ug/L
Surry County Closed C&D and Closed MSWLF, Elkin Page 2 of 2
Result UnitSample
ID Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary Cause 8
MW-7S 10/20/16 5.1 0.19 5 70 70
MW-8 10/20/16 1.3 0.33 1 6 75
MW-8 10/20/16 7.4 0.19 5 70 70
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to SWS reporting instructions
j=The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
NE = Not Established
LFG = Landfill Gas
BOLD = Concentration > 2L, 2B, GWP or MCL Standard
cis-1,2-Dichloroethene ug/L
1,4-Dichlorobenzene ug/L
cis-1,2-Dichloroethene ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard (NC SWS adopted)
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
L = Leachate
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 6
October 20, 2016
(cm/second)(%)(feet/feet)(feet/year)
MW-1 9.90E-05 5 0.103 211 S51W 53.88 988 Clay
MW-2 2.00E-05 5 57.65 890**Clay
MW-3 5.00E-05 5 50.88 881**Clay
Minimum 2.70E-04 5 0.103 211 -50.88 882 -
Average 3.45E-04 5 0.103 211 -54.14 920 -
Maximum 4.20E-04 5 0.103 211 -57.65 891 -
MW-3A 2.50E-05 5 0.033 17 N52W 32.09 894 Fractured Rock
MW-4 4.20E-04 5 0.007 64 N74W 11.53 921 Fractured Rock
MW-5 2.70E-04 5 0.007 41 N85W 11.50 937 Fractured Rock
MW-6 1.20E-04 5 0.291 722 N09W 50.25 954 Fractured Rock
MW-7S 2.30E-04 5 0.096 458 S82W 11.58 889 Fractured Rock
MW-7D 9.25 892**Fractured Rock
MW-8 2.40E-05 5 0.174 86 N25W 40.78 974 Fractured Rock
Minimum 2.40E-05 5 0.007 17 -9.25 889 -
Average 1.82E-04 5 0.101 231 -23.85 924 -
Maximum 4.20E-04 5 0.291 722 -50.25 988 -
NOTE: Note: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
* = Elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average Linear
Velocity Rate
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation*
Screened Interval
Lithology
(ft btoc)(ft amsl)
na na na
na na na
na na na na na
Hydrologic gradient calculated from groundwater elevations recorded October 20, 2016.
** = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
Average Linear Velocity Rate (Q) is defined by modified Darcy's equation:
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e

Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
October 31, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92316975
92316975
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CO. CLOSED MSWLF-ELKIN
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 45
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 2 of 45
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID Matrix Date Collected Date Received
92316975001 MW-1 Water 10/20/16 17:00 10/21/16 09:20
92316975002 MW-2 Water 10/20/16 12:00 10/21/16 09:20
92316975003 MW-3 Water 10/20/16 11:30 10/21/16 09:20
92316975004 MW-3A Water 10/20/16 12:40 10/21/16 09:20
92316975005 MW-4 Water 10/20/16 13:10 10/21/16 09:20
92316975006 MW-5 Water 10/20/16 13:35 10/21/16 09:20
92316975007 MW-6 Water 10/20/16 15:20 10/21/16 09:20
92316975008 MW-7S Water 10/20/16 14:55 10/21/16 09:20
92316975009 MW-7D Water 10/20/16 14:30 10/21/16 09:20
92316975010 MW-8 Water 10/20/16 16:05 10/21/16 09:20
92316975011 SW-1 Water 10/20/16 10:40 10/21/16 09:20
92316975012 SW-2 Water 10/20/16 14:00 10/21/16 09:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 3 of 45
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92316975001 MW-1 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CCAH
92316975002 MW-2 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CCAH
92316975003 MW-3 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CCAH
92316975004 MW-3A EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CCAH
92316975005 MW-4 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CCAH
92316975006 MW-5 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CCAH
92316975007 MW-6 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92316975008 MW-7S EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92316975009 MW-7D EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92316975010 MW-8 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92316975011 SW-1 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92316975012 SW-2 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-1 Lab ID:92316975001 Collected:10/20/16 17:00 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/25/16 22:50 7440-36-010/24/16 20:506.0 3.8 1
Arsenic ND ug/L 10/25/16 22:50 7440-38-210/24/16 20:5010.0 2.5 1
Barium 26.3J ug/L 10/25/16 22:50 7440-39-310/24/16 20:501002.5 1
Beryllium ND ug/L 10/25/16 22:50 7440-41-710/24/16 20:501.0 0.50 1
Cadmium ND ug/L 10/25/16 22:50 7440-43-910/24/16 20:501.0 0.50 1
Chromium ND ug/L 10/25/16 22:50 7440-47-310/24/16 20:5010.0 2.5 1
Cobalt ND ug/L 10/25/16 22:50 7440-48-410/24/16 20:5010.0 2.5 1
Copper ND ug/L 10/25/16 22:50 7440-50-810/24/16 20:5010.0 2.5 1
Lead ND ug/L 10/25/16 22:50 7439-92-110/24/16 20:5010.0 2.5 1
Nickel ND ug/L 10/25/16 22:50 7440-02-010/24/16 20:5050.0 2.5 1
Selenium ND ug/L 10/25/16 22:50 7782-49-210/24/16 20:5010.0 5.0 1
Silver ND ug/L 10/25/16 22:50 7440-22-410/24/16 20:5010.0 2.5 1
Thallium ND ug/L 10/25/16 22:50 7440-28-010/24/16 20:505.5 5.0 1
Vanadium ND ug/L 10/25/16 22:50 7440-62-210/24/16 20:5025.0 2.5 1
Zinc ND ug/L 10/25/16 22:50 7440-66-610/24/16 20:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/24/16 00:40 67-64-110010.0 1
Acrylonitrile ND ug/L 10/24/16 00:40 107-13-12001.9 1
Benzene ND ug/L 10/24/16 00:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/24/16 00:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/24/16 00:40 75-27-41.0 0.18 1
Bromoform ND ug/L 10/24/16 00:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/24/16 00:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/24/16 00:40 78-93-31000.96 1
Carbon disulfide ND ug/L 10/24/16 00:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/24/16 00:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/24/16 00:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/24/16 00:40 75-00-310.0 0.54 1
Chloroform ND ug/L 10/24/16 00:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/24/16 00:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/24/16 00:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/24/16 00:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/24/16 00:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/24/16 00:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/24/16 00:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/24/16 00:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/24/16 00:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/24/16 00:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/24/16 00:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/24/16 00:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.36J ug/L 10/24/16 00:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/24/16 00:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/24/16 00:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/24/16 00:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/24/16 00:40 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-1 Lab ID:92316975001 Collected:10/20/16 17:00 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/24/16 00:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/24/16 00:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/24/16 00:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/24/16 00:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/24/16 00:40 108-10-11000.33 1
Styrene ND ug/L 10/24/16 00:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/24/16 00:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/24/16 00:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/24/16 00:40 127-18-41.0 0.46 1
Toluene ND ug/L 10/24/16 00:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/24/16 00:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/24/16 00:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/24/16 00:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/24/16 00:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/24/16 00:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/24/16 00:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/24/16 00:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/24/16 00:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/24/16 00:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/24/16 00:40 17060-07-070-130 1
Toluene-d8 (S)98 %10/24/16 00:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-2 Lab ID:92316975002 Collected:10/20/16 12:00 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/25/16 22:53 7440-36-010/24/16 20:506.0 3.8 1
Arsenic 28.1 ug/L 10/25/16 22:53 7440-38-2 B10/24/16 20:5010.0 2.5 1
Barium 234 ug/L 10/25/16 22:53 7440-39-310/24/16 20:501002.5 1
Beryllium ND ug/L 10/25/16 22:53 7440-41-710/24/16 20:501.0 0.50 1
Cadmium ND ug/L 10/25/16 22:53 7440-43-910/24/16 20:501.0 0.50 1
Chromium ND ug/L 10/25/16 22:53 7440-47-310/24/16 20:5010.0 2.5 1
Cobalt 4.9J ug/L 10/25/16 22:53 7440-48-410/24/16 20:5010.0 2.5 1
Copper ND ug/L 10/25/16 22:53 7440-50-810/24/16 20:5010.0 2.5 1
Lead ND ug/L 10/25/16 22:53 7439-92-110/24/16 20:5010.0 2.5 1
Nickel 10.4J ug/L 10/25/16 22:53 7440-02-010/24/16 20:5050.0 2.5 1
Selenium ND ug/L 10/25/16 22:53 7782-49-210/24/16 20:5010.0 5.0 1
Silver ND ug/L 10/25/16 22:53 7440-22-410/24/16 20:5010.0 2.5 1
Thallium ND ug/L 10/25/16 22:53 7440-28-010/24/16 20:505.5 5.0 1
Vanadium 5.1J ug/L 10/25/16 22:53 7440-62-210/24/16 20:5025.0 2.5 1
Zinc 21.2 ug/L 10/25/16 22:53 7440-66-610/24/16 20:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.3J ug/L 10/24/16 00:58 67-64-110010.0 1
Acrylonitrile ND ug/L 10/24/16 00:58 107-13-12001.9 1
Benzene 2.2 ug/L 10/24/16 00:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/24/16 00:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/24/16 00:58 75-27-41.0 0.18 1
Bromoform ND ug/L 10/24/16 00:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/24/16 00:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/24/16 00:58 78-93-31000.96 1
Carbon disulfide ND ug/L 10/24/16 00:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/24/16 00:58 56-23-51.0 0.25 1
Chlorobenzene 8.9 ug/L 10/24/16 00:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/24/16 00:58 75-00-310.0 0.54 1
Chloroform ND ug/L 10/24/16 00:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/24/16 00:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/24/16 00:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/24/16 00:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/24/16 00:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/24/16 00:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene 7.3 ug/L 10/24/16 00:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene 13.2 ug/L 10/24/16 00:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/24/16 00:58 110-57-61001.0 1
1,1-Dichloroethane 0.58J ug/L 10/24/16 00:58 75-34-35.0 0.32 1
1,2-Dichloroethane 0.61J ug/L 10/24/16 00:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/24/16 00:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/24/16 00:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/24/16 00:58 156-60-55.0 0.49 1
1,2-Dichloropropane 0.90J ug/L 10/24/16 00:58 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/24/16 00:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/24/16 00:58 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-2 Lab ID:92316975002 Collected:10/20/16 12:00 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/24/16 00:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/24/16 00:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/24/16 00:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/24/16 00:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/24/16 00:58 108-10-11000.33 1
Styrene ND ug/L 10/24/16 00:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/24/16 00:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/24/16 00:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/24/16 00:58 127-18-41.0 0.46 1
Toluene 0.48J ug/L 10/24/16 00:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/24/16 00:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/24/16 00:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/24/16 00:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/24/16 00:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/24/16 00:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/24/16 00:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/24/16 00:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/24/16 00:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/24/16 00:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %10/24/16 00:58 17060-07-070-130 1
Toluene-d8 (S)99 %10/24/16 00:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3 Lab ID:92316975003 Collected:10/20/16 11:30 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/25/16 22:56 7440-36-010/24/16 20:506.0 3.8 1
Arsenic ND ug/L 10/25/16 22:56 7440-38-210/24/16 20:5010.0 2.5 1
Barium 81.9J ug/L 10/25/16 22:56 7440-39-310/24/16 20:501002.5 1
Beryllium ND ug/L 10/25/16 22:56 7440-41-710/24/16 20:501.0 0.50 1
Cadmium 1.9 ug/L 10/25/16 22:56 7440-43-910/24/16 20:501.0 0.50 1
Chromium ND ug/L 10/25/16 22:56 7440-47-310/24/16 20:5010.0 2.5 1
Cobalt ND ug/L 10/25/16 22:56 7440-48-410/24/16 20:5010.0 2.5 1
Copper 13.0 ug/L 10/25/16 22:56 7440-50-810/24/16 20:5010.0 2.5 1
Lead ND ug/L 10/25/16 22:56 7439-92-110/24/16 20:5010.0 2.5 1
Nickel 38.3J ug/L 10/25/16 22:56 7440-02-010/24/16 20:5050.0 2.5 1
Selenium ND ug/L 10/25/16 22:56 7782-49-210/24/16 20:5010.0 5.0 1
Silver ND ug/L 10/25/16 22:56 7440-22-410/24/16 20:5010.0 2.5 1
Thallium ND ug/L 10/25/16 22:56 7440-28-010/24/16 20:505.5 5.0 1
Vanadium ND ug/L 10/25/16 22:56 7440-62-210/24/16 20:5025.0 2.5 1
Zinc 12.9 ug/L 10/25/16 22:56 7440-66-610/24/16 20:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/24/16 01:15 67-64-110010.0 1
Acrylonitrile ND ug/L 10/24/16 01:15 107-13-12001.9 1
Benzene 3.5 ug/L 10/24/16 01:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/24/16 01:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/24/16 01:15 75-27-41.0 0.18 1
Bromoform ND ug/L 10/24/16 01:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/24/16 01:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/24/16 01:15 78-93-31000.96 1
Carbon disulfide ND ug/L 10/24/16 01:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/24/16 01:15 56-23-51.0 0.25 1
Chlorobenzene 0.87J ug/L 10/24/16 01:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/24/16 01:15 75-00-310.0 0.54 1
Chloroform ND ug/L 10/24/16 01:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/24/16 01:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/24/16 01:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/24/16 01:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/24/16 01:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/24/16 01:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/24/16 01:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene 5.1 ug/L 10/24/16 01:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/24/16 01:15 110-57-61001.0 1
1,1-Dichloroethane 0.48J ug/L 10/24/16 01:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/24/16 01:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/24/16 01:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 18.9 ug/L 10/24/16 01:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/24/16 01:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/24/16 01:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/24/16 01:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/24/16 01:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3 Lab ID:92316975003 Collected:10/20/16 11:30 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/24/16 01:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/24/16 01:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/24/16 01:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/24/16 01:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/24/16 01:15 108-10-11000.33 1
Styrene ND ug/L 10/24/16 01:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/24/16 01:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/24/16 01:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/24/16 01:15 127-18-41.0 0.46 1
Toluene ND ug/L 10/24/16 01:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/24/16 01:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/24/16 01:15 79-00-51.0 0.29 1
Trichloroethene 2.1 ug/L 10/24/16 01:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/24/16 01:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/24/16 01:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/24/16 01:15 108-05-450.0 0.35 1
Vinyl chloride 0.76J ug/L 10/24/16 01:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/24/16 01:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/24/16 01:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/24/16 01:15 17060-07-070-130 1
Toluene-d8 (S)100 %10/24/16 01:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3A Lab ID:92316975004 Collected:10/20/16 12:40 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/25/16 23:00 7440-36-010/24/16 20:506.0 3.8 1
Arsenic ND ug/L 10/25/16 23:00 7440-38-210/24/16 20:5010.0 2.5 1
Barium 449 ug/L 10/25/16 23:00 7440-39-310/24/16 20:501002.5 1
Beryllium ND ug/L 10/25/16 23:00 7440-41-710/24/16 20:501.0 0.50 1
Cadmium ND ug/L 10/25/16 23:00 7440-43-910/24/16 20:501.0 0.50 1
Chromium ND ug/L 10/25/16 23:00 7440-47-310/24/16 20:5010.0 2.5 1
Cobalt 50.8 ug/L 10/25/16 23:00 7440-48-410/24/16 20:5010.0 2.5 1
Copper ND ug/L 10/25/16 23:00 7440-50-810/24/16 20:5010.0 2.5 1
Lead ND ug/L 10/25/16 23:00 7439-92-110/24/16 20:5010.0 2.5 1
Nickel 41.0J ug/L 10/25/16 23:00 7440-02-010/24/16 20:5050.0 2.5 1
Selenium ND ug/L 10/25/16 23:00 7782-49-210/24/16 20:5010.0 5.0 1
Silver ND ug/L 10/25/16 23:00 7440-22-410/24/16 20:5010.0 2.5 1
Thallium ND ug/L 10/25/16 23:00 7440-28-010/24/16 20:505.5 5.0 1
Vanadium ND ug/L 10/25/16 23:00 7440-62-210/24/16 20:5025.0 2.5 1
Zinc ND ug/L 10/25/16 23:00 7440-66-610/24/16 20:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/24/16 01:32 67-64-110010.0 1
Acrylonitrile ND ug/L 10/24/16 01:32 107-13-12001.9 1
Benzene 1.3 ug/L 10/24/16 01:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/24/16 01:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/24/16 01:32 75-27-41.0 0.18 1
Bromoform ND ug/L 10/24/16 01:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/24/16 01:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/24/16 01:32 78-93-31000.96 1
Carbon disulfide ND ug/L 10/24/16 01:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/24/16 01:32 56-23-51.0 0.25 1
Chlorobenzene 4.7 ug/L 10/24/16 01:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/24/16 01:32 75-00-310.0 0.54 1
Chloroform ND ug/L 10/24/16 01:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/24/16 01:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/24/16 01:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/24/16 01:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/24/16 01:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/24/16 01:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene 4.0J ug/L 10/24/16 01:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene 14.5 ug/L 10/24/16 01:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/24/16 01:32 110-57-61001.0 1
1,1-Dichloroethane 1.0J ug/L 10/24/16 01:32 75-34-35.0 0.32 1
1,2-Dichloroethane 0.31J ug/L 10/24/16 01:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/24/16 01:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 18.4 ug/L 10/24/16 01:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/24/16 01:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/24/16 01:32 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/24/16 01:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/24/16 01:32 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-3A Lab ID:92316975004 Collected:10/20/16 12:40 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/24/16 01:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/24/16 01:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/24/16 01:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/24/16 01:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/24/16 01:32 108-10-11000.33 1
Styrene ND ug/L 10/24/16 01:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/24/16 01:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/24/16 01:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/24/16 01:32 127-18-41.0 0.46 1
Toluene ND ug/L 10/24/16 01:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/24/16 01:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/24/16 01:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/24/16 01:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/24/16 01:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/24/16 01:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/24/16 01:32 108-05-450.0 0.35 1
Vinyl chloride 2.6 ug/L 10/24/16 01:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/24/16 01:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/24/16 01:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/24/16 01:32 17060-07-070-130 1
Toluene-d8 (S)100 %10/24/16 01:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-4 Lab ID:92316975005 Collected:10/20/16 13:10 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/25/16 23:03 7440-36-010/24/16 20:506.0 3.8 1
Arsenic ND ug/L 10/25/16 23:03 7440-38-210/24/16 20:5010.0 2.5 1
Barium 11.8J ug/L 10/25/16 23:03 7440-39-310/24/16 20:501002.5 1
Beryllium ND ug/L 10/25/16 23:03 7440-41-710/24/16 20:501.0 0.50 1
Cadmium 1.6 ug/L 10/25/16 23:03 7440-43-910/24/16 20:501.0 0.50 1
Chromium ND ug/L 10/25/16 23:03 7440-47-310/24/16 20:5010.0 2.5 1
Cobalt ND ug/L 10/25/16 23:03 7440-48-410/24/16 20:5010.0 2.5 1
Copper ND ug/L 10/25/16 23:03 7440-50-810/24/16 20:5010.0 2.5 1
Lead ND ug/L 10/25/16 23:03 7439-92-110/24/16 20:5010.0 2.5 1
Nickel ND ug/L 10/25/16 23:03 7440-02-010/24/16 20:5050.0 2.5 1
Selenium ND ug/L 10/25/16 23:03 7782-49-210/24/16 20:5010.0 5.0 1
Silver ND ug/L 10/25/16 23:03 7440-22-410/24/16 20:5010.0 2.5 1
Thallium ND ug/L 10/25/16 23:03 7440-28-010/24/16 20:505.5 5.0 1
Vanadium ND ug/L 10/25/16 23:03 7440-62-210/24/16 20:5025.0 2.5 1
Zinc 6.7J ug/L 10/25/16 23:03 7440-66-610/24/16 20:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/24/16 01:49 67-64-110010.0 1
Acrylonitrile ND ug/L 10/24/16 01:49 107-13-12001.9 1
Benzene ND ug/L 10/24/16 01:49 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/24/16 01:49 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/24/16 01:49 75-27-41.0 0.18 1
Bromoform ND ug/L 10/24/16 01:49 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/24/16 01:49 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/24/16 01:49 78-93-31000.96 1
Carbon disulfide ND ug/L 10/24/16 01:49 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/24/16 01:49 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/24/16 01:49 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/24/16 01:49 75-00-310.0 0.54 1
Chloroform ND ug/L 10/24/16 01:49 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/24/16 01:49 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/24/16 01:49 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/24/16 01:49 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/24/16 01:49 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/24/16 01:49 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/24/16 01:49 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/24/16 01:49 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/24/16 01:49 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/24/16 01:49 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/24/16 01:49 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/24/16 01:49 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.49J ug/L 10/24/16 01:49 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/24/16 01:49 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/24/16 01:49 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/24/16 01:49 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/24/16 01:49 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-4 Lab ID:92316975005 Collected:10/20/16 13:10 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/24/16 01:49 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/24/16 01:49 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/24/16 01:49 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/24/16 01:49 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/24/16 01:49 108-10-11000.33 1
Styrene ND ug/L 10/24/16 01:49 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/24/16 01:49 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/24/16 01:49 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/24/16 01:49 127-18-41.0 0.46 1
Toluene ND ug/L 10/24/16 01:49 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/24/16 01:49 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/24/16 01:49 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/24/16 01:49 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/24/16 01:49 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/24/16 01:49 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/24/16 01:49 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/24/16 01:49 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/24/16 01:49 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/24/16 01:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/24/16 01:49 17060-07-070-130 1
Toluene-d8 (S)99 %10/24/16 01:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-5 Lab ID:92316975006 Collected:10/20/16 13:35 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/25/16 23:06 7440-36-010/24/16 20:506.0 3.8 1
Arsenic ND ug/L 10/25/16 23:06 7440-38-210/24/16 20:5010.0 2.5 1
Barium 11.0J ug/L 10/25/16 23:06 7440-39-310/24/16 20:501002.5 1
Beryllium ND ug/L 10/25/16 23:06 7440-41-710/24/16 20:501.0 0.50 1
Cadmium 0.79J ug/L 10/25/16 23:06 7440-43-910/24/16 20:501.0 0.50 1
Chromium ND ug/L 10/25/16 23:06 7440-47-310/24/16 20:5010.0 2.5 1
Cobalt ND ug/L 10/25/16 23:06 7440-48-410/24/16 20:5010.0 2.5 1
Copper ND ug/L 10/25/16 23:06 7440-50-810/24/16 20:5010.0 2.5 1
Lead ND ug/L 10/25/16 23:06 7439-92-110/24/16 20:5010.0 2.5 1
Nickel ND ug/L 10/25/16 23:06 7440-02-010/24/16 20:5050.0 2.5 1
Selenium ND ug/L 10/25/16 23:06 7782-49-210/24/16 20:5010.0 5.0 1
Silver ND ug/L 10/25/16 23:06 7440-22-410/24/16 20:5010.0 2.5 1
Thallium ND ug/L 10/25/16 23:06 7440-28-010/24/16 20:505.5 5.0 1
Vanadium ND ug/L 10/25/16 23:06 7440-62-210/24/16 20:5025.0 2.5 1
Zinc ND ug/L 10/25/16 23:06 7440-66-610/24/16 20:5010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/24/16 02:06 67-64-110010.0 1
Acrylonitrile ND ug/L 10/24/16 02:06 107-13-12001.9 1
Benzene ND ug/L 10/24/16 02:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/24/16 02:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/24/16 02:06 75-27-41.0 0.18 1
Bromoform ND ug/L 10/24/16 02:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/24/16 02:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/24/16 02:06 78-93-31000.96 1
Carbon disulfide ND ug/L 10/24/16 02:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/24/16 02:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/24/16 02:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/24/16 02:06 75-00-310.0 0.54 1
Chloroform ND ug/L 10/24/16 02:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/24/16 02:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/24/16 02:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/24/16 02:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/24/16 02:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/24/16 02:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/24/16 02:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/24/16 02:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/24/16 02:06 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/24/16 02:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/24/16 02:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/24/16 02:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.53J ug/L 10/24/16 02:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/24/16 02:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/24/16 02:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/24/16 02:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/24/16 02:06 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-5 Lab ID:92316975006 Collected:10/20/16 13:35 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/24/16 02:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/24/16 02:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/24/16 02:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/24/16 02:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/24/16 02:06 108-10-11000.33 1
Styrene ND ug/L 10/24/16 02:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/24/16 02:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/24/16 02:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/24/16 02:06 127-18-41.0 0.46 1
Toluene ND ug/L 10/24/16 02:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/24/16 02:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/24/16 02:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/24/16 02:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/24/16 02:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/24/16 02:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/24/16 02:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/24/16 02:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/24/16 02:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/24/16 02:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/24/16 02:06 17060-07-070-130 1
Toluene-d8 (S)98 %10/24/16 02:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-6 Lab ID:92316975007 Collected:10/20/16 15:20 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/27/16 19:57 7440-36-010/25/16 18:556.0 3.8 1
Arsenic ND ug/L 10/27/16 19:57 7440-38-210/25/16 18:5510.0 2.5 1
Barium 82.1J ug/L 10/27/16 19:57 7440-39-310/25/16 18:551002.5 1
Beryllium ND ug/L 10/27/16 19:57 7440-41-710/25/16 18:551.0 0.50 1
Cadmium 0.80J ug/L 10/27/16 19:57 7440-43-910/25/16 18:551.0 0.50 1
Chromium ND ug/L 10/27/16 19:57 7440-47-310/25/16 18:5510.0 2.5 1
Cobalt 17.6 ug/L 10/27/16 19:57 7440-48-410/25/16 18:5510.0 2.5 1
Copper 3.2J ug/L 10/27/16 19:57 7440-50-810/25/16 18:5510.0 2.5 1
Lead ND ug/L 10/27/16 19:57 7439-92-110/25/16 18:5510.0 2.5 1
Nickel ND ug/L 10/27/16 19:57 7440-02-010/25/16 18:5550.0 2.5 1
Selenium ND ug/L 10/27/16 19:57 7782-49-210/25/16 18:5510.0 5.0 1
Silver ND ug/L 10/27/16 19:57 7440-22-410/25/16 18:5510.0 2.5 1
Thallium ND ug/L 10/27/16 19:57 7440-28-010/25/16 18:555.5 5.0 1
Vanadium ND ug/L 10/27/16 19:57 7440-62-210/25/16 18:5525.0 2.5 1
Zinc 8.5J ug/L 10/27/16 19:57 7440-66-610/25/16 18:5510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/16 01:40 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/16 01:40 107-13-12001.9 1
Benzene 0.51J ug/L 10/30/16 01:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/16 01:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/16 01:40 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/16 01:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/16 01:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/16 01:40 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/16 01:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/16 01:40 56-23-51.0 0.25 1
Chlorobenzene 3.9 ug/L 10/30/16 01:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/16 01:40 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/16 01:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/16 01:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/16 01:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/16 01:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/16 01:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/16 01:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.5J ug/L 10/30/16 01:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.3 ug/L 10/30/16 01:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/16 01:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/16 01:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/16 01:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/16 01:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 3.1J ug/L 10/30/16 01:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/16 01:40 156-60-55.0 0.49 1
1,2-Dichloropropane 0.34J ug/L 10/30/16 01:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/16 01:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/16 01:40 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-6 Lab ID:92316975007 Collected:10/20/16 15:20 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/16 01:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/16 01:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/16 01:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/16 01:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/16 01:40 108-10-11000.33 1
Styrene ND ug/L 10/30/16 01:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/16 01:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/16 01:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/16 01:40 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/16 01:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/16 01:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/16 01:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/16 01:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/16 01:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/16 01:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/16 01:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/16 01:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/16 01:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/30/16 01:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/30/16 01:40 17060-07-070-130 1
Toluene-d8 (S)101 %10/30/16 01:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7S Lab ID:92316975008 Collected:10/20/16 14:55 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/27/16 20:07 7440-36-010/25/16 18:556.0 3.8 1
Arsenic ND ug/L 10/27/16 20:07 7440-38-210/25/16 18:5510.0 2.5 1
Barium 46.5J ug/L 10/27/16 20:07 7440-39-310/25/16 18:551002.5 1
Beryllium ND ug/L 10/27/16 20:07 7440-41-710/25/16 18:551.0 0.50 1
Cadmium 0.53J ug/L 10/27/16 20:07 7440-43-910/25/16 18:551.0 0.50 1
Chromium ND ug/L 10/27/16 20:07 7440-47-310/25/16 18:5510.0 2.5 1
Cobalt ND ug/L 10/27/16 20:07 7440-48-410/25/16 18:5510.0 2.5 1
Copper ND ug/L 10/27/16 20:07 7440-50-810/25/16 18:5510.0 2.5 1
Lead ND ug/L 10/27/16 20:07 7439-92-110/25/16 18:5510.0 2.5 1
Nickel ND ug/L 10/27/16 20:07 7440-02-010/25/16 18:5550.0 2.5 1
Selenium ND ug/L 10/27/16 20:07 7782-49-210/25/16 18:5510.0 5.0 1
Silver ND ug/L 10/27/16 20:07 7440-22-410/25/16 18:5510.0 2.5 1
Thallium ND ug/L 10/27/16 20:07 7440-28-010/25/16 18:555.5 5.0 1
Vanadium ND ug/L 10/27/16 20:07 7440-62-210/25/16 18:5525.0 2.5 1
Zinc ND ug/L 10/27/16 20:07 7440-66-610/25/16 18:5510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/16 01:56 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/16 01:56 107-13-12001.9 1
Benzene ND ug/L 10/30/16 01:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/16 01:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/16 01:56 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/16 01:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/16 01:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/16 01:56 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/16 01:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/16 01:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/16 01:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/16 01:56 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/16 01:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/16 01:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/16 01:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/16 01:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/16 01:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/16 01:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/16 01:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/16 01:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/16 01:56 110-57-61001.0 1
1,1-Dichloroethane 0.74J ug/L 10/30/16 01:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/16 01:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/16 01:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 5.1 ug/L 10/30/16 01:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/16 01:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/16 01:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/16 01:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/16 01:56 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7S Lab ID:92316975008 Collected:10/20/16 14:55 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/16 01:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/16 01:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/16 01:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/16 01:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/16 01:56 108-10-11000.33 1
Styrene ND ug/L 10/30/16 01:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/16 01:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/16 01:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/16 01:56 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/16 01:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/16 01:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/16 01:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/16 01:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/16 01:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/16 01:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/16 01:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/16 01:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/16 01:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %10/30/16 01:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/30/16 01:56 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/16 01:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7D Lab ID:92316975009 Collected:10/20/16 14:30 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/27/16 20:10 7440-36-010/25/16 18:556.0 3.8 1
Arsenic ND ug/L 10/27/16 20:10 7440-38-210/25/16 18:5510.0 2.5 1
Barium 11.8J ug/L 10/27/16 20:10 7440-39-310/25/16 18:551002.5 1
Beryllium ND ug/L 10/27/16 20:10 7440-41-710/25/16 18:551.0 0.50 1
Cadmium ND ug/L 10/27/16 20:10 7440-43-910/25/16 18:551.0 0.50 1
Chromium ND ug/L 10/27/16 20:10 7440-47-310/25/16 18:5510.0 2.5 1
Cobalt ND ug/L 10/27/16 20:10 7440-48-410/25/16 18:5510.0 2.5 1
Copper ND ug/L 10/27/16 20:10 7440-50-810/25/16 18:5510.0 2.5 1
Lead ND ug/L 10/27/16 20:10 7439-92-110/25/16 18:5510.0 2.5 1
Nickel ND ug/L 10/27/16 20:10 7440-02-010/25/16 18:5550.0 2.5 1
Selenium ND ug/L 10/27/16 20:10 7782-49-210/25/16 18:5510.0 5.0 1
Silver ND ug/L 10/27/16 20:10 7440-22-410/25/16 18:5510.0 2.5 1
Thallium ND ug/L 10/27/16 20:10 7440-28-010/25/16 18:555.5 5.0 1
Vanadium ND ug/L 10/27/16 20:10 7440-62-210/25/16 18:5525.0 2.5 1
Zinc 5.9J ug/L 10/27/16 20:10 7440-66-610/25/16 18:5510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/16 02:13 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/16 02:13 107-13-12001.9 1
Benzene ND ug/L 10/30/16 02:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/16 02:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/16 02:13 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/16 02:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/16 02:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/16 02:13 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/16 02:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/16 02:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/16 02:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/16 02:13 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/16 02:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/16 02:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/16 02:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/16 02:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/16 02:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/16 02:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/16 02:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/16 02:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/16 02:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/16 02:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/16 02:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/16 02:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.59J ug/L 10/30/16 02:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/16 02:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/16 02:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/16 02:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/16 02:13 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-7D Lab ID:92316975009 Collected:10/20/16 14:30 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/16 02:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/16 02:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/16 02:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/16 02:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/16 02:13 108-10-11000.33 1
Styrene ND ug/L 10/30/16 02:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/16 02:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/16 02:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/16 02:13 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/16 02:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/16 02:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/16 02:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/16 02:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/16 02:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/16 02:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/16 02:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/16 02:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/16 02:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %10/30/16 02:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/30/16 02:13 17060-07-070-130 1
Toluene-d8 (S)103 %10/30/16 02:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-8 Lab ID:92316975010 Collected:10/20/16 16:05 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/27/16 20:13 7440-36-010/25/16 18:556.0 3.8 1
Arsenic ND ug/L 10/27/16 20:13 7440-38-210/25/16 18:5510.0 2.5 1
Barium 47.5J ug/L 10/27/16 20:13 7440-39-310/25/16 18:551002.5 1
Beryllium ND ug/L 10/27/16 20:13 7440-41-710/25/16 18:551.0 0.50 1
Cadmium ND ug/L 10/27/16 20:13 7440-43-910/25/16 18:551.0 0.50 1
Chromium ND ug/L 10/27/16 20:13 7440-47-310/25/16 18:5510.0 2.5 1
Cobalt 4.4J ug/L 10/27/16 20:13 7440-48-410/25/16 18:5510.0 2.5 1
Copper ND ug/L 10/27/16 20:13 7440-50-810/25/16 18:5510.0 2.5 1
Lead ND ug/L 10/27/16 20:13 7439-92-110/25/16 18:5510.0 2.5 1
Nickel 9.5J ug/L 10/27/16 20:13 7440-02-010/25/16 18:5550.0 2.5 1
Selenium ND ug/L 10/27/16 20:13 7782-49-210/25/16 18:5510.0 5.0 1
Silver ND ug/L 10/27/16 20:13 7440-22-410/25/16 18:5510.0 2.5 1
Thallium ND ug/L 10/27/16 20:13 7440-28-010/25/16 18:555.5 5.0 1
Vanadium ND ug/L 10/27/16 20:13 7440-62-210/25/16 18:5525.0 2.5 1
Zinc ND ug/L 10/27/16 20:13 7440-66-610/25/16 18:5510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/16 02:30 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/16 02:30 107-13-12001.9 1
Benzene 0.63J ug/L 10/30/16 02:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/16 02:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/16 02:30 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/16 02:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/16 02:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/16 02:30 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/16 02:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/16 02:30 56-23-51.0 0.25 1
Chlorobenzene 0.45J ug/L 10/30/16 02:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/16 02:30 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/16 02:30 67-66-3 B5.0 0.14 1
Chloromethane ND ug/L 10/30/16 02:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/16 02:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/16 02:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/16 02:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/16 02:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.72J ug/L 10/30/16 02:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.3 ug/L 10/30/16 02:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/16 02:30 110-57-61001.0 1
1,1-Dichloroethane 0.61J ug/L 10/30/16 02:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/16 02:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/16 02:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.4 ug/L 10/30/16 02:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/16 02:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/16 02:30 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/16 02:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/16 02:30 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:MW-8 Lab ID:92316975010 Collected:10/20/16 16:05 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/16 02:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/16 02:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/16 02:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/16 02:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/16 02:30 108-10-11000.33 1
Styrene ND ug/L 10/30/16 02:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/16 02:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/16 02:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/16 02:30 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/16 02:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/16 02:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/16 02:30 79-00-51.0 0.29 1
Trichloroethene 0.73J ug/L 10/30/16 02:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/16 02:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/16 02:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/16 02:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/16 02:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/16 02:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/30/16 02:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/30/16 02:30 17060-07-070-130 1
Toluene-d8 (S)101 %10/30/16 02:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-1 Lab ID:92316975011 Collected:10/20/16 10:40 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/27/16 20:16 7440-36-010/25/16 18:556.0 3.8 1
Arsenic ND ug/L 10/27/16 20:16 7440-38-210/25/16 18:5510.0 2.5 1
Barium 16.8J ug/L 10/27/16 20:16 7440-39-310/25/16 18:551002.5 1
Beryllium ND ug/L 10/27/16 20:16 7440-41-710/25/16 18:551.0 0.50 1
Cadmium ND ug/L 10/27/16 20:16 7440-43-910/25/16 18:551.0 0.50 1
Chromium ND ug/L 10/27/16 20:16 7440-47-310/25/16 18:5510.0 2.5 1
Cobalt ND ug/L 10/27/16 20:16 7440-48-410/25/16 18:5510.0 2.5 1
Copper ND ug/L 10/27/16 20:16 7440-50-810/25/16 18:5510.0 2.5 1
Lead ND ug/L 10/27/16 20:16 7439-92-110/25/16 18:5510.0 2.5 1
Nickel ND ug/L 10/27/16 20:16 7440-02-010/25/16 18:5550.0 2.5 1
Selenium ND ug/L 10/27/16 20:16 7782-49-210/25/16 18:5510.0 5.0 1
Silver ND ug/L 10/27/16 20:16 7440-22-410/25/16 18:5510.0 2.5 1
Thallium ND ug/L 10/27/16 20:16 7440-28-010/25/16 18:555.5 5.0 1
Vanadium ND ug/L 10/27/16 20:16 7440-62-210/25/16 18:5525.0 2.5 1
Zinc ND ug/L 10/27/16 20:16 7440-66-610/25/16 18:5510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/16 02:47 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/16 02:47 107-13-12001.9 1
Benzene ND ug/L 10/30/16 02:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/16 02:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/16 02:47 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/16 02:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/16 02:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/16 02:47 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/16 02:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/16 02:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/16 02:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/16 02:47 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/16 02:47 67-66-3 B5.0 0.14 1
Chloromethane ND ug/L 10/30/16 02:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/16 02:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/16 02:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/16 02:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/16 02:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/16 02:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/16 02:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/16 02:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/16 02:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/16 02:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/16 02:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/16 02:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/16 02:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/16 02:47 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/16 02:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/16 02:47 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-1 Lab ID:92316975011 Collected:10/20/16 10:40 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/16 02:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/16 02:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/16 02:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/16 02:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/16 02:47 108-10-11000.33 1
Styrene ND ug/L 10/30/16 02:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/16 02:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/16 02:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/16 02:47 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/16 02:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/16 02:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/16 02:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/16 02:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/16 02:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/16 02:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/16 02:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/16 02:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/16 02:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/30/16 02:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/30/16 02:47 17060-07-070-130 1
Toluene-d8 (S)101 %10/30/16 02:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-2 Lab ID:92316975012 Collected:10/20/16 14:00 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 10/27/16 20:29 7440-36-010/25/16 18:556.0 3.8 1
Arsenic ND ug/L 10/27/16 20:29 7440-38-210/25/16 18:5510.0 2.5 1
Barium 16.9J ug/L 10/27/16 20:29 7440-39-310/25/16 18:551002.5 1
Beryllium ND ug/L 10/27/16 20:29 7440-41-710/25/16 18:551.0 0.50 1
Cadmium ND ug/L 10/27/16 20:29 7440-43-910/25/16 18:551.0 0.50 1
Chromium ND ug/L 10/27/16 20:29 7440-47-310/25/16 18:5510.0 2.5 1
Cobalt ND ug/L 10/27/16 20:29 7440-48-410/25/16 18:5510.0 2.5 1
Copper ND ug/L 10/27/16 20:29 7440-50-810/25/16 18:5510.0 2.5 1
Lead ND ug/L 10/27/16 20:29 7439-92-110/25/16 18:5510.0 2.5 1
Nickel ND ug/L 10/27/16 20:29 7440-02-010/25/16 18:5550.0 2.5 1
Selenium ND ug/L 10/27/16 20:29 7782-49-210/25/16 18:5510.0 5.0 1
Silver ND ug/L 10/27/16 20:29 7440-22-410/25/16 18:5510.0 2.5 1
Thallium ND ug/L 10/27/16 20:29 7440-28-010/25/16 18:555.5 5.0 1
Vanadium ND ug/L 10/27/16 20:29 7440-62-210/25/16 18:5525.0 2.5 1
Zinc ND ug/L 10/27/16 20:29 7440-66-610/25/16 18:5510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/30/16 03:04 67-64-110010.0 1
Acrylonitrile ND ug/L 10/30/16 03:04 107-13-12001.9 1
Benzene ND ug/L 10/30/16 03:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/30/16 03:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/30/16 03:04 75-27-41.0 0.18 1
Bromoform ND ug/L 10/30/16 03:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/30/16 03:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/30/16 03:04 78-93-31000.96 1
Carbon disulfide ND ug/L 10/30/16 03:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/30/16 03:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/30/16 03:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/30/16 03:04 75-00-310.0 0.54 1
Chloroform ND ug/L 10/30/16 03:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/30/16 03:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/30/16 03:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/30/16 03:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/30/16 03:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/30/16 03:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/30/16 03:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/30/16 03:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/30/16 03:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/30/16 03:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/30/16 03:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/30/16 03:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/30/16 03:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/30/16 03:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/30/16 03:04 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/30/16 03:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/30/16 03:04 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
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Page 27 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Sample:SW-2 Lab ID:92316975012 Collected:10/20/16 14:00 Received:10/21/16 09:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 10/30/16 03:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/30/16 03:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/30/16 03:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/30/16 03:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/30/16 03:04 108-10-11000.33 1
Styrene ND ug/L 10/30/16 03:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/30/16 03:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/30/16 03:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/30/16 03:04 127-18-41.0 0.46 1
Toluene ND ug/L 10/30/16 03:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/30/16 03:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/30/16 03:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/30/16 03:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/30/16 03:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/30/16 03:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/30/16 03:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/30/16 03:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/30/16 03:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/30/16 03:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/30/16 03:04 17060-07-070-130 1
Toluene-d8 (S)100 %10/30/16 03:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
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Page 28 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
334174
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92316975001, 92316975002, 92316975003, 92316975004, 92316975005, 92316975006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1852647
Associated Lab Samples:92316975001, 92316975002, 92316975003, 92316975004, 92316975005, 92316975006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/25/16 21:363.8
Arsenic ug/L 3.3J 10.0 10/25/16 21:362.5
Barium ug/L ND 100 10/25/16 21:362.5
Beryllium ug/L ND 1.0 10/25/16 21:360.50
Cadmium ug/L ND 1.0 10/25/16 21:360.50
Chromium ug/L ND 10.0 10/25/16 21:362.5
Cobalt ug/L ND 10.0 10/25/16 21:362.5
Copper ug/L ND 10.0 10/25/16 21:362.5
Lead ug/L ND 10.0 10/25/16 21:362.5
Nickel ug/L ND 50.0 10/25/16 21:362.5
Selenium ug/L ND 10.0 10/25/16 21:365.0
Silver ug/L ND 10.0 10/25/16 21:362.5
Thallium ug/L ND 5.5 10/25/16 21:365.0
Vanadium ug/L ND 25.0 10/25/16 21:362.5
Zinc ug/L ND 10.0 10/25/16 21:365.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1852648LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 508500 102 80-120
Arsenic ug/L 493500 99 80-120
Barium ug/L 506500 101 80-120
Beryllium ug/L 500500 100 80-120
Cadmium ug/L 502500 100 80-120
Chromium ug/L 490500 98 80-120
Cobalt ug/L 508500 102 80-120
Copper ug/L 516500 103 80-120
Lead ug/L 496500 99 80-120
Nickel ug/L 494500 99 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 251250 100 80-120
Thallium ug/L 523500 105 80-120
Vanadium ug/L 489500 98 80-120
Zinc ug/L 496500 99 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
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Huntersville, NC 28078
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Page 29 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1852649MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92317009002
1852650
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125100 2 25500ND510502
Arsenic ug/L 500 100 75-12598 2 25500ND501492
Barium ug/L 500 102 75-125102 1 2550026.0 537 534
Beryllium ug/L 500 101 75-125101 0 25500ND507506
Cadmium ug/L 500 101 75-125100 1 25500ND503500
Chromium ug/L 500 99 75-12599 0 25500ND493493
Cobalt ug/L 500 101 75-125100 1 25500ND507501
Copper ug/L 500 104 75-125104 0 25500ND522520
Lead ug/L 500 98 75-12597 1 25500ND492488
Nickel ug/L 500 99 75-12598 1 25500ND493490
Selenium ug/L 500 102 75-125100 2 25500ND510502
Silver ug/L 250 100 75-125100 0 25250ND251250
Thallium ug/L 500 104 75-125102 1 25500ND522515
Vanadium ug/L 500 99 75-12599 0 25500ND495496
Zinc ug/L 500 100 75-125101 1 25500ND500505
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
334367
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92316975007, 92316975008, 92316975009, 92316975010, 92316975011, 92316975012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1853514
Associated Lab Samples:92316975007, 92316975008, 92316975009, 92316975010, 92316975011, 92316975012
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/27/16 19:513.8
Arsenic ug/L ND 10.0 10/27/16 19:512.5
Barium ug/L ND 100 10/27/16 19:512.5
Beryllium ug/L ND 1.0 10/27/16 19:510.50
Cadmium ug/L ND 1.0 10/27/16 19:510.50
Chromium ug/L ND 10.0 10/27/16 19:512.5
Cobalt ug/L ND 10.0 10/27/16 19:512.5
Copper ug/L ND 10.0 10/27/16 19:512.5
Lead ug/L ND 10.0 10/27/16 19:512.5
Nickel ug/L ND 50.0 10/27/16 19:512.5
Selenium ug/L ND 10.0 10/27/16 19:515.0
Silver ug/L ND 10.0 10/27/16 19:512.5
Thallium ug/L ND 5.5 10/27/16 19:515.0
Vanadium ug/L ND 25.0 10/27/16 19:512.5
Zinc ug/L ND 10.0 10/27/16 19:515.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1853515LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 504500 101 80-120
Arsenic ug/L 490500 98 80-120
Barium ug/L 497500 99 80-120
Beryllium ug/L 503500 101 80-120
Cadmium ug/L 501500 100 80-120
Chromium ug/L 495500 99 80-120
Cobalt ug/L 507500 101 80-120
Copper ug/L 514500 103 80-120
Lead ug/L 498500 100 80-120
Nickel ug/L 493500 99 80-120
Selenium ug/L 510500 102 80-120
Silver ug/L 253250 101 80-120
Thallium ug/L 514500 103 80-120
Vanadium ug/L 496500 99 80-120
Zinc ug/L 509500 102 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1853516MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92316975007
1853517
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12599 2 25500ND481493
Arsenic ug/L 500 96 75-12598 2 25500ND481492
Barium ug/L 500 100 75-125101 1 2550082.1J 582 588
Beryllium ug/L 500 98 75-12599 1 25500ND492495
Cadmium ug/L 500 98 75-125100 2 255000.80J 490 500
Chromium ug/L 500 96 75-12597 1 25500ND483488
Cobalt ug/L 500 97 75-12599 2 2550017.6 502 512
Copper ug/L 500 102 75-125105 2 255003.2J 515 526
Lead ug/L 500 95 75-12597 2 25500ND476484
Nickel ug/L 500 95 75-12597 2 25500ND477486
Selenium ug/L 500 98 75-12599 2 25500ND489496
Silver ug/L 250 99 75-125101 1 25250ND248252
Thallium ug/L 500 96 75-12598 2 25500ND484495
Vanadium ug/L 500 97 75-12599 1 25500ND488494
Zinc ug/L 500 97 75-12599 2 255008.5J 495 505
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
334225
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92316975001, 92316975002, 92316975003, 92316975004, 92316975005, 92316975006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1852812
Associated Lab Samples:92316975001, 92316975002, 92316975003, 92316975004, 92316975005, 92316975006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/23/16 17:340.33
1,1,1-Trichloroethane ug/L ND 1.0 10/23/16 17:340.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/23/16 17:340.40
1,1,2-Trichloroethane ug/L ND 1.0 10/23/16 17:340.29
1,1-Dichloroethane ug/L ND 5.0 10/23/16 17:340.32
1,1-Dichloroethene ug/L ND 5.0 10/23/16 17:340.56
1,2,3-Trichloropropane ug/L ND 1.0 10/23/16 17:340.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/23/16 17:342.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/23/16 17:340.27
1,2-Dichlorobenzene ug/L ND 5.0 10/23/16 17:340.30
1,2-Dichloroethane ug/L ND 1.0 10/23/16 17:340.24
1,2-Dichloropropane ug/L ND 1.0 10/23/16 17:340.27
1,4-Dichlorobenzene ug/L ND 1.0 10/23/16 17:340.33
2-Butanone (MEK)ug/L ND 100 10/23/16 17:340.96
2-Hexanone ug/L ND 50.0 10/23/16 17:340.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/23/16 17:340.33
Acetone ug/L ND 100 10/23/16 17:3410.0
Acrylonitrile ug/L ND 200 10/23/16 17:341.9
Benzene ug/L ND 1.0 10/23/16 17:340.25
Bromochloromethane ug/L ND 3.0 10/23/16 17:340.17
Bromodichloromethane ug/L ND 1.0 10/23/16 17:340.18
Bromoform ug/L ND 3.0 10/23/16 17:340.26
Bromomethane ug/L ND 10.0 10/23/16 17:340.29
Carbon disulfide ug/L ND 100 10/23/16 17:341.2
Carbon tetrachloride ug/L ND 1.0 10/23/16 17:340.25
Chlorobenzene ug/L ND 3.0 10/23/16 17:340.23
Chloroethane ug/L ND 10.0 10/23/16 17:340.54
Chloroform ug/L ND 5.0 10/23/16 17:340.14
Chloromethane ug/L ND 1.0 10/23/16 17:340.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/23/16 17:340.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/23/16 17:340.13
Dibromochloromethane ug/L ND 3.0 10/23/16 17:340.21
Dibromomethane ug/L ND 10.0 10/23/16 17:340.21
Ethylbenzene ug/L ND 1.0 10/23/16 17:340.30
Iodomethane ug/L ND 10.0 10/23/16 17:340.32
Methylene Chloride ug/L ND 1.0 10/23/16 17:340.97
Styrene ug/L ND 1.0 10/23/16 17:340.26
Tetrachloroethene ug/L ND 1.0 10/23/16 17:340.46
Toluene ug/L ND 1.0 10/23/16 17:340.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/23/16 17:340.49
trans-1,3-Dichloropropene ug/L ND 1.0 10/23/16 17:340.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1852812
Associated Lab Samples:92316975001, 92316975002, 92316975003, 92316975004, 92316975005, 92316975006
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 10/23/16 17:341.0
Trichloroethene ug/L ND 1.0 10/23/16 17:340.47
Trichlorofluoromethane ug/L ND 1.0 10/23/16 17:340.20
Vinyl acetate ug/L ND 50.0 10/23/16 17:340.35
Vinyl chloride ug/L ND 1.0 10/23/16 17:340.62
Xylene (Total)ug/L ND 5.0 10/23/16 17:340.66
1,2-Dichloroethane-d4 (S)%104 70-130 10/23/16 17:34
4-Bromofluorobenzene (S)%97 70-130 10/23/16 17:34
Toluene-d8 (S)%100 70-130 10/23/16 17:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1852813LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.650 95 80-125
1,1,1-Trichloroethane ug/L 44.150 88 71-129
1,1,2,2-Tetrachloroethane ug/L 45.950 92 79-124
1,1,2-Trichloroethane ug/L 43.950 88 85-125
1,1-Dichloroethane ug/L 43.150 86 73-126
1,1-Dichloroethene ug/L 49.650 99 66-135
1,2,3-Trichloropropane ug/L 46.950 94 75-130
1,2-Dibromo-3-chloropropane ug/L 44.850 90 71-133
1,2-Dibromoethane (EDB)ug/L 48.450 97 83-124
1,2-Dichlorobenzene ug/L 50.150 100 80-133
1,2-Dichloroethane ug/L 41.350 83 67-128
1,2-Dichloropropane ug/L 42.750 85 75-132
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2-Butanone (MEK)ug/L 79.3J100 79 61-144
2-Hexanone ug/L 89.6100 90 68-143
4-Methyl-2-pentanone (MIBK)ug/L 83.8J100 84 72-135
Acetone ug/L 85.0J100 85 48-146
Acrylonitrile ug/L 229250 92 40-160
Benzene ug/L 46.750 93 80-125
Bromochloromethane ug/L 45.450 91 71-125
Bromodichloromethane ug/L 46.050 92 78-124
Bromoform ug/L 46.250 92 71-128
Bromomethane ug/L 42.150 84 40-160
Carbon disulfide ug/L 58.7J50 117 50-160
Carbon tetrachloride ug/L 49.450 99 69-131
Chlorobenzene ug/L 47.350 95 81-122
Chloroethane ug/L 39.450 79 39-148
Chloroform ug/L 41.450 83 73-127
Chloromethane ug/L 37.650 75 44-146
cis-1,2-Dichloroethene ug/L 42.850 86 74-124
cis-1,3-Dichloropropene ug/L 43.050 86 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 34 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1852813LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 48.250 96 78-125
Dibromomethane ug/L 47.250 94 82-120
Ethylbenzene ug/L 47.950 96 79-121
Iodomethane ug/L 92.7100 93 39-154
Methylene Chloride ug/L 45.650 91 64-133
Styrene ug/L 48.050 96 84-126
Tetrachloroethene ug/L 45.750 91 78-122
Toluene ug/L 45.450 91 80-121
trans-1,2-Dichloroethene ug/L 47.150 94 71-127
trans-1,3-Dichloropropene ug/L 42.450 85 69-141
trans-1,4-Dichloro-2-butene ug/L 41.8J50 84 40-160
Trichloroethene ug/L 45.150 90 78-122
Trichlorofluoromethane ug/L 44.750 89 53-137
Vinyl acetate ug/L 87.5100 87 40-160
Vinyl chloride ug/L 36.350 73 58-137
Xylene (Total)ug/L 142150 95 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1852814MATRIX SPIKE SAMPLE:
MSSpike
Result
92316711001
1,1,1,2-Tetrachloroethane ug/L 20.820 104 70-130ND
1,1,1-Trichloroethane ug/L 20.420 102 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.620 98 70-130ND
1,1,2-Trichloroethane ug/L 18.820 94 70-130ND
1,1-Dichloroethane ug/L 19.320 97 70-130ND
1,1-Dichloroethene ug/L 23.920 120 70-166ND
1,2,3-Trichloropropane ug/L 20.020 100 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.020 100 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.920 105 70-130ND
1,2-Dichlorobenzene ug/L 22.120 110 70-130ND
1,2-Dichloroethane ug/L 18.720 93 70-130ND
1,2-Dichloropropane ug/L 18.220 91 70-130ND
1,4-Dichlorobenzene ug/L 21.520 107 70-130ND
2-Butanone (MEK)ug/L 37.8J40 95 70-130ND
2-Hexanone ug/L 41.5J40 104 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 37.4J40 93 70-130ND
Acetone ug/L 42.3J40 96 70-130ND
Acrylonitrile ug/L 94.1J100 94 70-130ND
Benzene ug/L 21.320 106 70-148ND
Bromochloromethane ug/L 19.820 99 70-130ND
Bromodichloromethane ug/L 19.620 98 70-130ND
Bromoform ug/L 19.220 96 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 35 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1852814MATRIX SPIKE SAMPLE:
MSSpike
Result
92316711001
Bromomethane ug/L 18.120 90 70-130ND
Carbon disulfide ug/L 27.6J M12013870-130ND
Carbon tetrachloride ug/L 22.720 113 70-130ND
Chlorobenzene ug/L 20.920 104 70-146ND
Chloroethane ug/L 18.920 94 70-130ND
Chloroform ug/L 18.720 93 70-130ND
Chloromethane ug/L 18.620 93 70-130ND
cis-1,2-Dichloroethene ug/L 19.620 98 70-130ND
cis-1,3-Dichloropropene ug/L 18.020 90 70-130ND
Dibromochloromethane ug/L 20.520 103 70-130ND
Dibromomethane ug/L 19.820 99 70-130ND
Ethylbenzene ug/L 21.620 108 70-130ND
Iodomethane ug/L 38.140 95 70-130ND
Methylene Chloride ug/L 19.720 99 70-130ND
Styrene ug/L 20.920 104 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 20.220 101 70-155ND
trans-1,2-Dichloroethene ug/L 21.220 106 70-130ND
trans-1,3-Dichloropropene ug/L 17.720 89 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.0J20 90 70-130ND
Trichloroethene ug/L 20.920 104 69-151ND
Trichlorofluoromethane ug/L 22.220 111 70-130ND
Vinyl acetate ug/L 38.7J40 97 70-130ND
Vinyl chloride ug/L 17.920 87 70-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92316711003
1852815SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
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[phone]
Page 36 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92316711003
1852815SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 1.4 2 301.3
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.59J 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 0.81J 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103 0103
4-Bromofluorobenzene (S)%97 196
Toluene-d8 (S)%98 197
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
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Huntersville, NC 28078
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Page 37 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
335031
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92316975007, 92316975008, 92316975009, 92316975010, 92316975011, 92316975012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1857205
Associated Lab Samples:92316975007, 92316975008, 92316975009, 92316975010, 92316975011, 92316975012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/30/16 00:150.33
1,1,1-Trichloroethane ug/L ND 1.0 10/30/16 00:150.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/30/16 00:150.40
1,1,2-Trichloroethane ug/L ND 1.0 10/30/16 00:150.29
1,1-Dichloroethane ug/L ND 5.0 10/30/16 00:150.32
1,1-Dichloroethene ug/L ND 5.0 10/30/16 00:150.56
1,2,3-Trichloropropane ug/L ND 1.0 10/30/16 00:150.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/30/16 00:152.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/30/16 00:150.27
1,2-Dichlorobenzene ug/L ND 5.0 10/30/16 00:150.30
1,2-Dichloroethane ug/L ND 1.0 10/30/16 00:150.24
1,2-Dichloropropane ug/L ND 1.0 10/30/16 00:150.27
1,4-Dichlorobenzene ug/L ND 1.0 10/30/16 00:150.33
2-Butanone (MEK)ug/L ND 100 10/30/16 00:150.96
2-Hexanone ug/L ND 50.0 10/30/16 00:150.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/30/16 00:150.33
Acetone ug/L ND 100 10/30/16 00:1510.0
Acrylonitrile ug/L ND 200 10/30/16 00:151.9
Benzene ug/L ND 1.0 10/30/16 00:150.25
Bromochloromethane ug/L ND 3.0 10/30/16 00:150.17
Bromodichloromethane ug/L ND 1.0 10/30/16 00:150.18
Bromoform ug/L ND 3.0 10/30/16 00:150.26
Bromomethane ug/L ND 10.0 10/30/16 00:150.29
Carbon disulfide ug/L ND 100 10/30/16 00:151.2
Carbon tetrachloride ug/L ND 1.0 10/30/16 00:150.25
Chlorobenzene ug/L ND 3.0 10/30/16 00:150.23
Chloroethane ug/L ND 10.0 10/30/16 00:150.54
Chloroform ug/L 0.17J 5.0 10/30/16 00:150.14
Chloromethane ug/L ND 1.0 10/30/16 00:150.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/30/16 00:150.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/30/16 00:150.13
Dibromochloromethane ug/L ND 3.0 10/30/16 00:150.21
Dibromomethane ug/L ND 10.0 10/30/16 00:150.21
Ethylbenzene ug/L ND 1.0 10/30/16 00:150.30
Iodomethane ug/L ND 10.0 10/30/16 00:150.32
Methylene Chloride ug/L ND 1.0 10/30/16 00:150.97
Styrene ug/L ND 1.0 10/30/16 00:150.26
Tetrachloroethene ug/L ND 1.0 10/30/16 00:150.46
Toluene ug/L ND 1.0 10/30/16 00:150.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/30/16 00:150.49
trans-1,3-Dichloropropene ug/L ND 1.0 10/30/16 00:150.26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1857205
Associated Lab Samples:92316975007, 92316975008, 92316975009, 92316975010, 92316975011, 92316975012
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 10/30/16 00:151.0
Trichloroethene ug/L ND 1.0 10/30/16 00:150.47
Trichlorofluoromethane ug/L ND 1.0 10/30/16 00:150.20
Vinyl acetate ug/L ND 50.0 10/30/16 00:150.35
Vinyl chloride ug/L ND 1.0 10/30/16 00:150.62
Xylene (Total)ug/L ND 5.0 10/30/16 00:150.66
1,2-Dichloroethane-d4 (S)%95 70-130 10/30/16 00:15
4-Bromofluorobenzene (S)%97 70-130 10/30/16 00:15
Toluene-d8 (S)%100 70-130 10/30/16 00:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1857206LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.350 97 80-125
1,1,1-Trichloroethane ug/L 48.050 96 71-129
1,1,2,2-Tetrachloroethane ug/L 47.650 95 79-124
1,1,2-Trichloroethane ug/L 47.350 95 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 55.750 111 66-135
1,2,3-Trichloropropane ug/L 45.250 90 75-130
1,2-Dibromo-3-chloropropane ug/L 46.950 94 71-133
1,2-Dibromoethane (EDB)ug/L 48.250 96 83-124
1,2-Dichlorobenzene ug/L 50.850 102 80-133
1,2-Dichloroethane ug/L 44.250 88 67-128
1,2-Dichloropropane ug/L 46.950 94 75-132
1,4-Dichlorobenzene ug/L 48.950 98 78-130
2-Butanone (MEK)ug/L 98.5J100 99 61-144
2-Hexanone ug/L 99.8100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.2J100 98 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 268250 107 40-160
Benzene ug/L 50.950 102 80-125
Bromochloromethane ug/L 49.550 99 71-125
Bromodichloromethane ug/L 48.050 96 78-124
Bromoform ug/L 45.750 91 71-128
Bromomethane ug/L 46.550 93 40-160
Carbon disulfide ug/L 61.6J50 123 50-160
Carbon tetrachloride ug/L 50.450 101 69-131
Chlorobenzene ug/L 47.950 96 81-122
Chloroethane ug/L 45.050 90 39-148
Chloroform ug/L 47.350 95 73-127
Chloromethane ug/L 53.750 107 44-146
cis-1,2-Dichloroethene ug/L 48.550 97 74-124
cis-1,3-Dichloropropene ug/L 46.650 93 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1857206LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 49.150 98 78-125
Dibromomethane ug/L 47.850 96 82-120
Ethylbenzene ug/L 48.750 97 79-121
Iodomethane ug/L 98.2100 98 39-154
Methylene Chloride ug/L 55.550 111 64-133
Styrene ug/L 48.750 97 84-126
Tetrachloroethene ug/L 41.950 84 78-122
Toluene ug/L 48.850 98 80-121
trans-1,2-Dichloroethene ug/L 51.950 104 71-127
trans-1,3-Dichloropropene ug/L 45.850 92 69-141
trans-1,4-Dichloro-2-butene ug/L 34.7J50 69 40-160
Trichloroethene ug/L 47.850 96 78-122
Trichlorofluoromethane ug/L 49.950 100 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 45.450 91 58-137
Xylene (Total)ug/L 145150 97 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1857207MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92317563005
1857208
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 97 70-13095 2 3020ND19.3 19.0
1,1,1-Trichloroethane ug/L 20 105 70-130104 1 3020ND21.0 20.8
1,1,2,2-Tetrachloroethane ug/L 20 97 70-13095 2 3020ND19.4 19.0
1,1,2-Trichloroethane ug/L 20 97 70-13096 1 3020ND19.4 19.3
1,1-Dichloroethane ug/L 20 108 70-130106 2 3020ND21.6 21.2
1,1-Dichloroethene ug/L 20 124 70-166125 1 3020ND24.8 25.0
1,2,3-Trichloropropane ug/L 20 94 70-13094 0 3020ND18.8 18.7
1,2-Dibromo-3-chloropropane ug/L 20 95 70-13094 1 3020ND19.0 18.8
1,2-Dibromoethane (EDB)ug/L 20 98 70-13098 0 3020ND19.7 19.6
1,2-Dichlorobenzene ug/L 20 104 70-130102 2 3020ND20.8 20.4
1,2-Dichloroethane ug/L 20 95 70-13093 2 3020ND19.1 18.8
1,2-Dichloropropane ug/L 20 98 70-13097 1 3020ND19.6 19.5
1,4-Dichlorobenzene ug/L 20 99 70-13097 1 3020ND19.8 19.5
2-Butanone (MEK)ug/L 40 106 70-130103 3 3040ND42.4J 41.1J
2-Hexanone ug/L 40 104 70-130103 1 3040ND41.7J 41.1J
4-Methyl-2-pentanone(MIBK)ug/L 40 103 70-130102 0 3040ND41.1J 41.0J
Acetone ug/L 40 107 70-130104 3 3040ND43.6J 42.2J
Acrylonitrile ug/L 100 116 70-130114 1 30100ND116J114J
Benzene ug/L 20 107 70-148107 0 3020ND21.5 21.5
Bromochloromethane ug/L 20 106 70-130105 1 3020ND21.1 20.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1857207MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92317563005
1857208
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 20 99 70-130100 1 3020ND19.8 20.0
Bromoform ug/L 20 88 70-13086 2 3020ND17.5 17.2
Bromomethane ug/L 20 81 70-13084 4 3020ND16.2 16.9
Carbon disulfide ug/L M12013670-130135 1 3020ND27.2J 27.0J
Carbon tetrachloride ug/L 20 110 70-130110 0 3020ND22.0 22.0
Chlorobenzene ug/L 20 99 70-14698 1 3020ND19.9 19.7
Chloroethane ug/L 20 99 70-13098 1 3020ND19.8 19.6
Chloroform ug/L 20 102 70-130102 0 3020ND20.4 20.4
Chloromethane ug/L 20 117 70-130117 0 3020ND23.4 23.3
cis-1,2-Dichloroethene ug/L 20 104 70-130104 0 3020ND20.9 20.8
cis-1,3-Dichloropropene ug/L 20 90 70-13091 2 3020ND17.9 18.2
Dibromochloromethane ug/L 20 97 70-13095 2 3020ND19.5 19.1
Dibromomethane ug/L 20 98 70-13098 0 3020ND19.6 19.7
Ethylbenzene ug/L 20 104 70-130101 2 3020ND20.7 20.2
Iodomethane ug/L 40 107 70-130104 3 3040ND42.9 41.7
Methylene Chloride ug/L 20 109 70-130108 1 3020ND21.8 21.5
Styrene ug/L 20 100 70-13097 3 3020ND19.9 19.4
Tetrachloroethene ug/L 20 88 70-13085 3 3020ND17.6 17.0
Toluene ug/L 20 103 70-155104 1 3020ND20.7 20.8
trans-1,2-Dichloroethene ug/L 20 114 70-130113 1 3020ND22.7 22.6
trans-1,3-Dichloropropene ug/L 20 88 70-13090 2 3020ND17.6 18.0
trans-1,4-Dichloro-2-butene ug/L M1206870-13069 1 3020ND13.7J 13.8J
Trichloroethene ug/L 20 101 69-151101 0 3020ND20.2 20.2
Trichlorofluoromethane ug/L 20 115 70-130113 2 3020ND23.0 22.6
Vinyl acetate ug/L 40 75 70-13077 3 3040ND30.0J 30.9J
Vinyl chloride ug/L 20 100 70-130100 1 3020ND19.9 20.1
1,2-Dichloroethane-d4 (S)%95 70-13095
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%99 70-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 45
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 45
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92316975
SURRY CO. CLOSED MSWLF-ELKIN
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92316975001 334174 334382MW-1 EPA 3010A EPA 6010
92316975002 334174 334382MW-2 EPA 3010A EPA 6010
92316975003 334174 334382MW-3 EPA 3010A EPA 6010
92316975004 334174 334382MW-3A EPA 3010A EPA 6010
92316975005 334174 334382MW-4 EPA 3010A EPA 6010
92316975006 334174 334382MW-5 EPA 3010A EPA 6010
92316975007 334367 334530MW-6 EPA 3010A EPA 6010
92316975008 334367 334530MW-7S EPA 3010A EPA 6010
92316975009 334367 334530MW-7D EPA 3010A EPA 6010
92316975010 334367 334530MW-8 EPA 3010A EPA 6010
92316975011 334367 334530SW-1 EPA 3010A EPA 6010
92316975012 334367 334530SW-2 EPA 3010A EPA 6010
92316975001 334225MW-1 EPA 8260
92316975002 334225MW-2 EPA 8260
92316975003 334225MW-3 EPA 8260
92316975004 334225MW-3A EPA 8260
92316975005 334225MW-4 EPA 8260
92316975006 334225MW-5 EPA 8260
92316975007 335031MW-6 EPA 8260
92316975008 335031MW-7S EPA 8260
92316975009 335031MW-7D EPA 8260
92316975010 335031MW-8 EPA 8260
92316975011 335031SW-1 EPA 8260
92316975012 335031SW-2 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/31/2016 05:14 PM
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[phone]
Page 43 of 45
Page 44 of 45
Page 45 of 45
Appendix B
Field Sampling Parameter Data Sheet(s)