IDX GW Monitoring Rpt Feb 2000 (SF)-OCR

*5931HSSF1066*
1111111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
oocumentType Progress/Monitoring Rpt (PRGMON)
RptSegment 1
DocDate
DocRcvd
Box
Accesslevel
Division
Section
Program
DocCat
4/18/2000
2/20/2007
SF1066
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
.1
~ 1\2:J RADIAN INTERNATIONAL
~ A DAMES & MOORE GROUP COMPANY
GROUNDWATER
MONITORING REPORT.
FOR FEBRUARY 2000
S\E6
Hamilton Beach 9Proctor-Silex, Inc.
Washington, North Carolina Facility
Prepared for:
Hamilton Beach oProctor-Silex, Inc.
4421 Waterfront Drive
Glen Allen, Virginia 23060
Prepared by:
Radian International
1600 Perimeter Park Drive
Morrisville, North Carolina 27709
April 2000
I
I
I
.I
I
I
I
I
I
'I
I
I
I
I
I
I
I
I
CERTIFICATION PAGE
GROUNDWATER MONITORING REPORT
FOR FEBRUARY 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
I, James Nark:unas, a Licensed Geologist in the State of North Carolina, certify that
this report and its contents have been prepared under my direct control and personal
superv1s10n.
650138.0901 Feb2000GW _Rpt.doc (04/04/00) 11
I
I
I
I
I
I
I
I
I
I
I·
I ,,
I
I
I
I
I
I
TABLE OF CONTENTS
Certification Page ................................................................................................................ ii
List of Figures .................................................................................................................... iv
List of Tables ...................................................................................................................... v
1.0 INTRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS ............................................................................ --. ............................. 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3.1 Water Level Measurements ................................................................................. 3-1
3.2 Analytical Results ................................................................................................. 3-1
APPENDIX A GROUNDWATER SAMPLING ANALYTICAL REPORTS
650138.0901 Feb2000GW _Rpt.doc (04/04/00) iii
I
I
I
I
I
I
I
I
I
I
I
I
I
I
·1
I
I
I
LIST OF FIGURES
1-1 Topographic Map, Hamilton BeachOProctor-Silex, Inc.
2-1 Site Map, Washington Facility, Hamilton BeachOProctor-Silex, Inc.
3-1 Generalized Groundwater Flow Direction for Hydrogeologic Unit A,
Washington Facility
3-2 Generalized Groundwater Flow Direction for Hydrogeologic Unit E,
Washington Facility
3-3 Summary of Volatile Organic Compounds (February 2000)
3-4 Location of Surrounding Water Supply Wells, Hamilton BeachO Proctor-Silex, Inc.
650138.0901 Feb2000GW _Rpt.doc (04/04/00) lV
I
I
.1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
2-1
3-1
3-2
3-3
3-4
3-5
LIST OF TABLES
Monitoring Well Construction Data for Sampled Wells
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
Water Level Measurements and Elevations, February 2, 2000
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-213
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-214
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-215
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-216
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-6 Historical Water Level Elevations at MW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-7 Historical Water Level Elevations at MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-8 Historical Water Level Elevations at MW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-9 Historical Water Level Elevations at MW-225
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-10 Historical Water Level Elevations at MW-226
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-11 Historical Water Level Elevations at MW-227
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-12 Historical Water Level Elevations at MW-228
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-13 Historical Water Level Elevations at MW-230
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
80396902.01 Feb2000GW _Rpt.doc (04/04/00) v
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
LIST OF TABLES (Continued)
3-14 Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-15 Field Measurements, February 2, and 3, 2000
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-16 Summary of Qualified Groundwater Analytical Results: February 2000
Volatile Organic Compounds by Method 8260B
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-17 Historical Analytical Results for MW-213
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-18 Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-19 Historical Analytical Results for MW-215
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-20 Historical Analytical Results for MW-216
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-21 Historical Analytical Results for MW-220
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-22 Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-23 Historical Analytical Results for MW-224
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-24 Historical Analytical Results for MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-25 Historical Analytical Results for MW-226
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-26 Historical Analytical Results for MW-227
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-27 Historical Analytical Results for MW-228
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
80396902.0 I Feb2000GW _ Rpt.doc (04/04/00) vi
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I·
I
I
I
LIST OF TABLES (Continued)
3-28 Historical Analytical Results for MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-29 Historical Analytical Results for MW-234
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
80396902.01 Feb2000GW _Rpt.doc (04/04/00) vu
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1.0 INTRODUCTION
The Hamilton Beach<> Proctor-Silex (HB<>PS) facility is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HB<>PS since 1990 and previously leased by predecessor companies. The facility is involved
in the final assembly, packaging, and warehousing of small electrical household appliances.
Since 1992, when organic compounds were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
assessment (CSA). The results of the CSA indicated that a plume of organic compounds is
present in groundwater underlyii;ig the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer used at the facility.
A plan for corrective action at the site has been proposed. Until corrective action
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to
a monitoring program requested and approved by the North Carolina Department of
Environment and Natural Resources, Groundwater Section. The purpose of the monitoring
program is to sample selected downgradient monitoring wells to detect potential migration of the
plume.
Radian International (Radian) conducted groundwater sampling at the facility in
February 2000. The sampling event included the measurement of water levels, temperature, pH,
and specific conductance; and the collection and analysis of samples from seven monitoring
wells. This report describes the sampling methods and presents the results for the third quarterly
sampling event.
80396902.01 Feb2000GW _Rpt.doc (04/04/00) 1-1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
.1
2.0 FIELD METHODS
Groundwater was sampled on February 2 and 3, 2000, in general accordance with
the methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for this
site.
Thirteen monitoring wells were sampled. They included MW-213 through
MW-216, MW-220, MW-222, MW-224 through MW-228, MW-230, and MW-234. The
locations of the monitoring wells are shown in Figure 2-1. Details of well construction are
provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using dedicated inertial foot-valve pumps.
Temperature, pH, and specific conductance were· measured and the data were recorded in a field
notebook. Purging continued until temperature, pH, and specific conductance stabilized; a
minimum of three well volumes was extracted; or the well was pumped dry. Each of the wells
was then sampled immediately following well purging using the dedicated inertial foot-valve
pump.
The groundwater samples were sent by overnight courier to STL (formerly
Radian Analytical Services) in Austin, Texas, for analysis of volatile organic compounds by
EPA Method 8260B.
80396902.01 Feb2000GW _Rpt.doc (04/04/00) 2-1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the thirteen wells sampled and seven additional wells. Maps showing the
generalized direction of groundwater flow in hydrogeologic units A and B are included as
Figures 3-1 and 3-2, respectively. Historical water-level elevations in sampled wells are
included in Tables 3-2 to 3-14.
3.2 Analytical Results
Field measurements of water temperature, pH, and specific conductance are
summarized in Table 3-15. Qualified analytical results are summarized in Table 3-16.and on
Figure 3-3. Qualified data sheets and laboratory reports are included in Appendix A.
No analytes were detected above the groundwater standards in samples from
wells l~cated near the perimeter of the site (MW-220, MW-222, MW-224, MW-225, MW-230,
and MW-234), nor were any analytes detected in the sample from well MW-226, which is
competed in the confined Limestone Aquifer. Also, no analytes were detected above
.... groundwater standards in samples col~ wells MW-215 and MW-216, which are
located 120 feet and 350 feet from the source area, respectively. Concentrations of chemicals
exceeding the standards were detected in samples from wells MW-213, MW-214, MW-227, and
MW-228. These four wells are located at, or within 150 feet of, the source area.
Historical analytical results for the sampled wells are included in Tables 3-17 to
3-29. A comparison of the record for wells located near the perimeter of the site suggests that the
plume .remains on-site, at least 200 feet from potential receptors located north of Spring Road
(Figure 3-4). The latest results for wells located at the source area and other interior portions of
the site are consistent with earlier results and indicate no significant changes in chemical
concentration and distribution have occurred.
80396902.01 Feb2000GW _Rpt.doc (04/04/00) 3-1
I.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I.
FIGURES
I
I
I
I
I
I
I
I TABLES
I
I
I
I
I
I
I
I
I
I
I
-------------------
Table 2-1
Monitoring Well Construction Data for Sampled Wells
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Top of Casing
Installatic;m Elevation Total Depth Screen Interval Filter Pack Bentonite Seal
Well No. Date (ft. above MSL) (ft. bes) (ft. bes)
MW-213 1/14/98 28.44 7.5 3 -7.5
MW-214 1/16/98 27.93 21 14.5 -21
MW-215 1/16/98 28.06 10 8.5 -10
MW-216 5/5/98 32.82 35 26 -35
MW-220 5/5/98 31.50 34 25 -34
MW-222 5/6/98 35.11 40 31 -40
MW-224 11/13/98 33.43 34 25 -34
MW-225 11/13/98 33.43 10 4-10
MW-226 9/30/98 28.46 75 70 -75
MW~227 10/1/98 28.47 25.5 20.5 -25.5
MW~228 9/23/98 28.71 10 3 -10
MW-230 10/26/98 33.47. 14 8 -14
MW-234 6/23/99 35.03 26 17 -26
Monitoring wells 213 through 215 installed by Groundwater Management Associates, Inc.
Monitoring wells 216, 220, and 222 installed by Radian Mobile Field Services.
Monitoring wells 226 through 228 installed by Parratt Wolff, Inc.
Monitoring wells 224, 225, 230, and 234 installed by Probe Technology, Inc.
80396902.0 I Feb2000GW _ Rpt.doc (04/04/00)
fft. bl!S) fft. bl!s)
2.5 -7.5 1.5 -2.5
13.5 -21 12.5 -13.5
8 -10 7-8
25 -35 24-25
24-34 23 -24
30-40 29 -30
24-34 23 -24
3 -10 2-3
69-75 67 -69
19.5 25.5 17.5 -19.5
2 -10 1-2
7 -14 5-7
16-26 13 -16
Grout Seal
(ft. bl!S)
0-1.5
0: 12.5
0-7
0-24
0-23
0-29
0-23
0-2
0-67
0 -17.5
0-1
0-5
0-13
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-1
Water Level Measurements and Elevations
February 2, 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Measuring Point Water Level
Elevation Elevation
Well (ft above msl)) Depth to Water (ft) (ft above msl)
MW-201S 29.74 1.63 28.11
MW-208 32.11 5.55 26.56
MW-213 28.44 2.03 26.41
MW-214 27.93 2.55 25.38
MW-215 28.06 . 2.83 25.23
MW-216 32.82 7.98 24.84
MW-217 32.75 7.44 25.31
MW-219 31.83 6.45 25.38
MW-220 31.50 5.65 25.85
MW-221 31.39 7.10 24.29
MW-222 35.11 11.77 23.34
MW-223 35.15 7.22 27.93
MW-224 33.43 6.70 26.73
MW-225 33.43 6.84 23.59
MW-226 28.46 18.23 10.23
MW-227 28.47 2.59 25.88
MW-228 28.71 4.08 24.63
MW-230 33.47 6.03 27.44
MW-233 34.55 9.00 25.55
MW-234 35.03 9.36 25.67
msl = mean sea level
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-2
Historical Water Level Elevations at MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM = Not measured
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
25.54
24.21
NM
NM -
26.41
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-3
Historical Water Level Elevations at MW-214
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM =Not measured
80396902.01 Feb2000GW_Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
24.95
22.18
NM
NM
25.38
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-4
Historical Water Level Elevations at MW-215
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM =Not measured
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
24.97
24.19
NM
NM -
25.23
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-5
Historical Water Level Elevations at MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date·
May 13, 1998
November 16, 1998
Julv 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM =Not measured
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
24.39
22.37
NM
NM -
24.84
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-6
Historical Water Level Elevations at MW-220
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 25.13
November 16, 1998 20.55
July 1, 1999 21.50
October 20, 1999 25.63 -
February 2, 2000 25.85
msl = mean sea level
80396902.0 I Feb2000GW _Rpt.doc (04/04/00)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-7
Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 22.34
November 16, 1998 19.99
July 1, 1999 20.61
October 20, 1999 24.22 -
February 2, 2000 23.34
msl = mean sea level
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-8
Historical Water Level Elevations at MW-224
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM =Not measured
80396902.0 I Feb2000GW _Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
NM
23.64
24.39
26.88
26.73
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-9
Historical Water Level Elevations at MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
Februarv 2, 2000
msl = mean sea level
NM =Not measured
80396902.0 I Feb2000GW _Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
NM
24.36
24.50
27.24 -
26.59
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-10
Historical Water Level Elevations at MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM =Not measured
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Water Level Elevation
(ft. above msl)
NM
8.43
8.54
11.11
10.23
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
,I
I
I
Table 3-11
Historical Water Level Elevations at MW-227
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
msl = mean sea level
NM = Not measured
80396902.01 Feb2000GW _Rptdoc (04/04/00)
Water Level Elevation
(ft. above msl)
NM
22.38
NM
25.82
25.88
--~-~~-~~~--~--~---·
Well Date Time
MW-213 2/3/00 08:10
MW-214 213100 08:27
MW-215 2/3/00 08:40
MW-216 212100 15:30
MW-220 212100 15:10
MW-222 2/2/00 14:25
MW-224 2/2/00 13:30
MW-225 212100 13:35
MW-226 212100 12:55
13:00
13:05
13:10
MW-227 2/3/00 09:03
MW-228 2/3/00 09:30
MW-230 212100 14:45
MW-234 212100 14:05
Table 3-15
Field Measurements
February 2, 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Volume Purged
(Gal) Pur2in2 Criteria
2.6 3 well volumes
9.0 3 well volumes
2.0 Orv
0.8 3 well volumes
0.9 3 well volumes
0.9 3 well volumes
0.6 Dry
0.2 3 well volumes
9.0 Stabilized parameters
12
16
20
11 Drv
3.5 3 well volumes
0.3 Dry
0.5 3 well volumes
Specific
Temperature Conductance
(oC) (µS) pH
18.5 275 5.6
21.5 300 6.1
18.0 160 5.9
17.5 360 7.2
17.0 100 6.1
17.0 330 7.0
15.0 290 7.7
11.5 135 5.7
20.0 400 7.7
19.0 440 7.7
19.0 430 7.7
19.0 435 7.7
20.0 420 7.0
16.5 2200 3.6
15.0 220 5.1
17.5 125 6.2
--~-~--~~-~-~~--~-~
Table 3-16
Summary of Qualified Groundwater Analytical Results: February 2000
Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Washington, North Carolina
Sample ID MW-213
Date of Sampling 213100
Analyte (µg/L)
Benzene ND (0.984)
Chloroethane ND (1.51)
1, 1-Dichloroethane 245
1,2-Dichloroethane 6.12 J
1, 1-Dichloroethene 492
cis-1,2-Dichloroethene 40.8
trans-1,2-Dichloroethene ND (l.63)
Ethylbenzene ND (1.10)
Methyl t-butyl ether ND (0.938)
Tetrachloroethene 44.4
Tetrahydrofuran ND (8.4)
Toluene ND (1.36)
l, 1, I-Trichloroethane ND (0.662)
1, 1,2-Trichloroethane 2.16 J
Trichloroethene 446
1,2,4-Trimethylbenzene ND (1.50)
Vinyl chloride 29.3
m&p-Xylene ND (2.74)
o-Xylene ND (1.43)
Target analytes not listed were not detected.
ND ()=Not detected at specified detection limit.
Bold values exceed Standards.
J = Estimated value.
80396902.0 I Feb2000GW _ Rpt.doc (04/04/00)
MW-214 MW-215 MW-216
213100 213100 212100
0.315 J 0.114 J ND (0.0492)
0.904 ND (0.0756) ND (0.0756)
179 4.07 ND (0.0487)
0.633 ND (0.0499) ND (0.0499)
13.8 3.02 ND (0.0697)
11.7 0.0401 J ND (0.0603)
0.701 ND (0.0813) ND (0.0813)
ND (0.0552) ND (0.0552) ND (0.0552)
ND (0.0469) ND (0.0469) ND (0.0469)
ND (0.0568) ND (0.0568) ND (0.0568)
ND (0.402) 19.l ND (0.402)
ND (0.0680) ND (0.0680) ND (0.0680)
ND (0.0331) ND (0.0331) ND (0.0331)
ND (0.0952) ND (0.0952) ND (0.0952)
0.289 J 0.138 J ND (0.0905)
ND (0.0749) ND (0.0749) ND (0.0749)
. 11.5 ND (0.0574) ND (0.0574)
ND(0.137) ND (0.137) ND (0.137)
ND (0.0713) ND (0.0713) ND (0.0713)
MW-220
212100
ND (0.0492)
ND (0.0756)
ND (0.0487)
ND (0.0499)
ND (0.0697)
ND (0.0603)
ND (0.0813)
ND (0.0552)
ND (0.0469)
ND (0.0568)
ND (0.402)
ND (0.0680)
ND (0.0331)
ND (0.0952)
ND (0.0905)
ND (0.0749)
ND {0.0574)
ND (0.137)
ND (0.0713)
MW-222
212100
ND (0.0492)
ND (0.0756)
ND (0.0487)
ND (0.0499)
ND (0.0697)
ND (0.0603)
ND (0.0813)
ND (0.0552)
ND (0.0469)
ND (0.0568)
ND (0.402)
ND(0.0680)
ND (0.0331)
ND (0.0952)
ND (0.0905)
ND (0.0749)
ND (0.0574)
ND (0.137)
ND (0.0713)
-------. -
_ .. _ .. _ .... ________ _
Table 3-16 (Continued)
Sample ID MW-224 MW-225 MW-226 MW-227 MW-228 MW-230 MW-234
Date of Sampling 212100 212100 212100 2/3/00 2/3/00 212100 212100
Analyte (µ.g/L)
Benzene ND (0.0492) ND (0.0492) ND (0.0492) ND (0.984) ND (246) ND (0.049?) ND (0.0492)
Chloroethane ND (0.0756) ND (0.0756) ND (0.0756) ND (1.51) ND (378) ND (0.0756) ND (0.0756)
1, 1-Dichloroethane ND (0.0487) ND (0.0487) ND (0.0487) 844 16,200 0.189 J ND (0.0487)
1,2-Dichloroethane ND (0.0499) ND (0.0499) ND (0.0499) 4.40 J ND (250) ND (0.0499) ND (0.0499)
1, 1-Dichloroethene ND (0.0697) ND (0.0697) ND (0.0697) 108 71,800 0.148 J ND (0.0697)
cis-1,2-Dichloroethene ND (0.0603) ND (0.0603) ND (0.0603) 105 1, 970 J 0.354 J ND (0.0603)
trans-1,2-Dichloroethene ND (0.0813) ND (0.0813) ND (0.0813) ND (1.63) ND (406) ND (0.0813) ND (0.0813)
Ethylbenzene ND (0.0552) ND (0.0552) ND (0.0552) ND (1.10) 414J ND (0.0552) ND (0.0552)
Methyl t-butyl ether ND (0.0469) ND (0.0469) ND (0.0469) ND (9.38) ND (234) ND (0.0469) ND (0.0469)
Tetrachloroethene ND (0.0568) ND (0.0568) ND (0.0568) ND (1.14) ND (284) ND (0.0568) ND (0.0568)
Tetrahydrofuran ND (0.402) ND (0.402) ND (0.402) ND (8.04) ND (2010) ND (0.402) ND (0.402)
To!Uene ND (0.0680) ND (0.0680) ND (0.0680) 3.56 J 1,610 J 0.284J ND (0.0680)
1, 1, I -Trichloroethane ND (0.0331) ND (0.0331) ND (0.0331) 310 135,000 ND (0.0331) ND (0.0331)
1, 1,2-Trichloroethane ND (0.0952) ND (0.0952) ND (0.0952) ND (1.90) ·ND (476) ND (0.0952) ND (0.0952)
Trichloroethene ND (0.0905) ND (0.0905) ND (0.0905) 12.9 15,000 0.661 ND (0.0905)
1,2,4-Trimethylbenzene ND (0.0749) ND (0.0749) ND (0.0749) ND (1.50) 1,220 J ND (0.0749) ND (0.0749)
Vinyl chloride ND (0.0574) ND (0.0574) ND(0.0574) ND (1.15) ND (287) ND (0.0574). ND (0.0574)
m&p-Xylene ND (0.137) ND (0.137) ND (0.137) ND (0.13'.7) 1,760 ND (0.137) ND (0.137)
o-Xylene ND (0.0713) ND (0.0713) ND (0.0713) ND(0.0713) 1,370 ND (0.0713) ND (0.0713)
Target analytes not listed were not detected.
ND ( ) = Not detected at specified detection limit.
Bold values exceed Standards. ·
J = Estimated value.
80396902.01 Feb2000GW _Rpt.doc (04104100)
---~-~~~-~--~---~--
.
Analyte
Benzene
n-Butylbenzene
sec-Butyl benzene
Chloroform
1,2-Dichlorobenzene
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Ethylbenzene
Isopropylbenzene
Napthalene
Tetrachloroethene
Tetrahydrofuran
Toluene
1, 1, I -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Table 3-17
Historical Analytical Results for MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater November
Standard Mav 1998 1998 Julv 1999
1 NS 0.724 NS
70 NS 0.240 NS
70 NS 0.315 NS
0.19 NS 0.793 NS
620 NS 0.642 NS
700 NS 351 NS
0.38 NS 7.02 NS
7 NS 867 NS
70 NS 39.3 NS
70 NS 2.22 NS
29 NS 2.03 NS
70 NS 0.618 NS
21 NS 15.7 J NS
0.7 NS 61.3 NS
-NS 7.63 J NS
1000 NS 1.48 NS
200 NS 1.09 NS
-NS 6.03 NS
2.8 NS 515 NS
2100 NS 0.575 NS
0.015 NS 38.7 NS
October 1999
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
February 2000
ND (0.984)
ND (1.28)
ND (1,.49)
ND (1.34)
ND (1.84)
245
6.Ii J -
492
40.8
ND (1.63)
ND (I.IO)
ND (0.948)
ND (2.12)
44.4
ND (8.4)
ND (1.36)
ND (0.662)
2.16 J
446
ND (4.16)
29.3
o ...
O-
P-
-r
-
.
._
~-----~-----~-~-~~-
Groundwater
Analyte Standard
m&p-Xylene 530
o-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
la c:\hamilton\washington\csa-rpt (4/4/00)
Table 3-17 (Continued)
November
May 1998 1998 Julv 1999 October 1999 February 2000
NS 1.57 NS NS ND (2.74)
NS 3.43 NS NS ND (1.43) -
~----~----~-~~--~~-
Table 3-18
Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc.
Grqundwater
-Analyte Standard
Benzene 1
Chloroethane 2800
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
p-Isopropyltoluene -
Trichloroethene 2.8
Vinyl chloride 0.015
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
November
May 1998 1998 July 1999
NS 0.172 J NS
NS 0.485 J NS
NS 108 NS
NS 0.303 J NS
NS 8.16 NS
NS 6.86 NS
NS 0.478 NS
NS 0.181 J NS
NS ND (0.587) U NS
NS 8.84 NS
U = Not present above the asociated level; .blank contamination is present.
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
-------·--------
October 1999 February 2000
NS . 0.315 J
NS 0.904
NS 179
NS 0.633 +
NS 13.8
NS 11.7
NS 0.701
NS ND (0.0452)
NS 0.289 J
NS 11.5
----~------~~------
Table 3-19
Historical Analytical Results for MW-215
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analvte Standard
Benzene 1
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Ethylbenzene 29
Methyl t-butyl ether 200
Tetrahydrofuran -
Trichloroethene 2.8
Vinyl chloride 0.015
m&p-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
November
Mav 1998 1998
NS 0.0963 J
NS 4.30
NS 3.85
NS ND(0.104) U
NS 0.0601 J
NS 1.22
NS 58.6
NS ND (0.322) U
NS 0.381 J
NS 0.0885 J
U = Not present above the associated level; blank contamination is present.
80396902.0 I Feb2000GW _Rpt.doc (04/04/00)
Julv 1999
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
October 1999 Februarv 2000
NS 0.114 J
NS 4.07
NS 3.02
NS 0.0401 J
NS ND(0.0552)
NS ND (0.0469)
NS 19.1
NS 0.138 J
NS ND (0.0574)
NS ND (0.137)
----~~-------~-----
Table 3-20
Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analvte Standard
Toluene 1000
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
November
Mav 1998 1998
0.171 ND (0.0522) UJ
UJ = Not detected and the detection limit is estimated.
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Julv 1999
NS
October 1999 February 2000
NS ND (0.0680)
----------------~--
Table 3-21
Historical Analytical Results for MW-220
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analvte Standard
Carbon disulfide 700
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
Washington, North Carolina
November
Mav1998 1998
ND (0.0547) ND (0.0547)
UJ = Not detected and the detection limit is estimated.
80396902.0 I Feb2000GW _ Rpt.doc (04/04/00)
Julv 1999
0.426 J
October 1999 February 2000
0.162 ND (0.0484) UJ
--------------~----
Table 3-22
Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analvte Standard
Carbon disulfide 700
1, 1-Dichloroethene 7
Toluene 1,000
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
Washington, North Carolina
Mav1998 November 1998 July 1999
ND (0.0547) ND (0.0547) 0.388 J
0.0908 J ND (0.0715) ND (0.102)
0.156 J ND (0.0522) ND (0.0766)
UJ = Not detected and the detection limit is estimated.
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
October 1999 February 2000
0.0944 ND (0.0484) UJ
ND (0.0819) ND (0.0697)
ND (0.0645) ND (0.0680)
-------------------
Table 3-23
Historical Analytical Results for MW-224
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analyte Standard
Carbon disulfide 700
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
May1998 November 1998 July 1999
NS ND (0.0547) 2.22
UJ = Not detected and the detection limit is estimated.
80396902.0 I Feb2000GW _ Rpt.doc (04/04/00)
October 1999 February 2000
2.72 ND (1.05) UJ
-------------------
Table 3-24
Historical Analytical Results for MW-225
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analvte Standard
Carbon disulfide 700
Chloroform 0.19
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
Mav 1998 November 1998 July 1999
NS ND (0.0547) ND <0.864)
NS ND (0.0480) ND <0.0424)
UJ = Not detected and the detection limit is estimated.
80396902.01 Feb2000GW _ Rpt.doc (04/04/00)
October 1999 February 2000
0.0691 ND (0.0484) UJ
0.171 ND (0.0670)
-------------------
Grouµdwater
Analyte Standard
Carbon disulfide 700
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND = Not detected at (detection limit).
NS = Not sampled.
Table 3-25
Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Mav 1998 November 1998 Julv 1999
NS ND (0.0547) ND (0.864)
UJ = Not detected and the detection limit is estimated.
80396902.01 Feb2000GW _Rpt.doc (04104100)
October 1999 Februarv 200
0.0950 ND (0.0484) UJ
-------------------
Table 3-26
Historical Analytical Results for MW-227
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater November
Analyte Standard May 1998 1998 Julv 1999
Acetone 700 NS 29.9J NS
Benzene 1 NS 0.668 J NS
2-Butanone (MEK) 170 NS 42.5 J NS
n-Butylbenzene 70 NS 0.437 J NS
Carbon disulfide 700 NS 0.573 J NS
Chloroethane 2800 NS 2.14J NS
Chloroform 0.19 NS 1.64 J NS
1, 1-Dichloroethane 700 NS 4,620 NS
1,2-Dichloroethane 0.38 NS 19.5 J NS
1, 1-Dichloroethene 7 NS 705 NS
cis-1,2-Dichloroethene 70 NS 228 NS
trans-1,2-Dichloroethene 70 NS 3.66 J NS
Ethylbenzene 29 NS 3.58 J NS
Isopropylbenzene 70 NS 0.392 J NS
p-Isopropyltoluene -NS 0.194 J NS
Napthalene 21 NS 3.73 J NS
n-Propylbenzene 70 NS 2.25 J NS
Tetrachloroethene 0.7 NS 1.41 J NS
Toluene 1000 NS 29.6J NS
1, 1, I -Trichloroethane 200 NS 3,200 NS
1, 1,2-Trichloroethane -NS 3.20 J NS
80396902.0 I Feb2000GW _Rpt.doc (04/04/00)
October 1999
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
February 2000
ND (5.72)
ND (0.984)
ND (3.58)
ND (1.28)
ND (0.968)
ND (1.51)
ND (1.34)
844
4.40 J
108
105
ND (1.63)
ND (9.38)
ND (0.948)
ND (0.904)
ND (2.12)
ND (1.77)
ND (1.14)
3.56 J
310
ND (1.90)
I -
-
....
, -
-------------------
Groundwater
Analvte Standard
Trichloroethene 2.8
1,2,4-Trimethylbenzene 350
1,3 ,5-Trimethylbenzene 350
Vinyl chloride 0.15
m&p-Xylene 530
o-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated v~lue.
ND= Not detected at (detection limit).
NS = Not sampled. ·
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Table·3-26 (Continued)
November
Mav1998 1998 Julv 1999 October 1999 Februarv 2000
NS 810 NS NS 12.9
NS 10.8 J NS NS ND (1.50)
NS 3.37 J NS NS ND (0.872)
NS 5.70 J NS NS ND (1.15)
NS 8.78 J NS NS ND (2.74)
NS 8.91 J NS NS ND (1.43)
--------------------
Analyte
Acetone
Benzene
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
Carbon tetrachloi,ide
Chloroethane
Chloroform
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Ethylbenzene
2-Hexanone
Isopropylbenzene
p-Isopropyltoluene
Methyl t-butyl ether
4-Methyl-2-pentanone (MIBK)
Napthalene
n-Propylbenzene
1, 1, 1,2-Tetrachloroethane
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Table 3-27
Historical Analytical Results for MW-228
Hamilton BeachOProctor-Silt:x, Inc.
Washington, North Carolina
Groundwat November
er Standard May1998 1998 July 1999
700 NS 307 J NS
1 NS 51.3 J NS
170 NS 21.3 J NS
70 NS 15.6 J NS
70 NS 5.27 J NS
0.3 NS 42.2 J NS
2800 NS 74.7 J NS
0.19 NS 12.8 J NS
700 NS 24,100 NS
7 NS 96,500 NS
70 NS 3,330 NS
70 NS 24.2 J NS
29 NS 544 NS
-NS 45.l J NS
70 NS 41.5 J NS
-NS 6.80 J NS
200 NS 5.21 J NS
NS 12.3 J NS
21 NS 608 NS
70 NS 200 NS
-NS 0.810 J NS
October 1999 February 2000
NS ND (1,430)
NS ND (246) -
NS ND (895) -
NS ND (321) ....
NS ND (372) -
NS ND (434) -
NS ND (378) -
NS ND (335)
NS 16,200 ~
NS 71,800
NS 1,970 J
NS ND (406) -
NS 414J
NS ND (835) '
NS ND (237)
I NS ND (226) . -
NS ND (234) -
NS ND (422)
NS ND (530) .,..
NS ND (443)
NS ND (474) ......
--------------------
Groundwat
Analvte er Standard
I, 1,2,2-Tetrachloroethane 0.17
Tetrachloroethene 0.7
Toluene 1000
1, 1, I-Trichloroethane 200
1, 1,2-Trichloroethane -
Trichloroethene 2.8
Trichlorofluoromethane 2100
1,2,4-Trimethylbenzene 350
1,3 ,5-Trimethylbenzene 350
Vinvl chloride 0.15
m&p-Xylene 530
o-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND:== Not detected at (detection limit).
NS = Not sampled.
80396902.01 Feb2000GW _Rpt.doc (04/04/00)
Table 3-27 (Continued)
November
Mavl998 1998
NS 0.688 J
NS 30.5 J
NS 1,460
NS 173,000
NS 49.3 J
NS 22,800
NS 12.7 J
NS 1,270
NS 309
NS 314
NS 1,540
NS 1,330
Julv 1999 October 1999 February 2000
NS NS ND (396)
NS NS ND (284) i-
NS NS 1,610 J
NS NS 135,000
NS NS ND (476)
NS NS 15,000 -
NS NS ND {1,040)
. NS NS 1,220 J -
NS NS ND (218) --
NS NS ND (287) ,
NS NS 1,760 .,...
NS NS 1,370
-------------------
Table 3-29
Historical Analytical Results for MW-234
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater
Analvte Standard
Carbon disulfide 700
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
Mayl998 November 1998
NS NS
U = Not present above the associated level; blank contamination is present.
UJ = Not detected and the detection limit is estimated.
80396902.0 I Feb2000GW _Rpt.doc (04/04/00)
Julv 1999
ND (0.864)
October 1999 February 2000
0.0600 ND (0.0484) UJ
I
I
I
I
I
I
I
I
1·
I
I
I
I
I
I
I
I
I
I
APPENDIX A
GROUNDWATER SAMPLING ANALYTICAL REPORTS
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
QUALIFIED DATA
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Chloromethane 74-87-3
3-Ch loroorooene 107-05-1
4-Chlorotoluene 106-43-4
2-Chlorotoluene 95-49-8
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I A-Dichloro-2-butene 110-57-6
I A-Dichlorobenzene 106-46-7
I 3-Dichlorobenzene 541-73-1
1,2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1,2-Dichloroethane 107-06-2
I, 1-Dich loroethane 75-34-3
cis-1 2-Dichloroethene 156-59-2
trans-1,2-Dichloroethene 156-60-5
1 1-Dichloroethene 75-35-4
I 3-Dichloroorooane 142-28-9
1,2-Dichloroorooane 78-87-5
2.2-Dich loroorooane 594-20-7
cis-1.3-Dichloroorooene 10061-01-5
1 1-Dichloroorooene 563-58-6
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW226
2000201201
Cone Flag
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workordcr: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0821
0.111
0.0762
0.113
1.05
0.0564
0.152
0.0939
0.390
0.0587
0.0591
0.0920
0.113
0.0499
0.0487
0.0603
0.0813
0.0697
0.0451
0.0670
0.0714
0.0366
0.0464
0.0658
0.0647
0.0552
0.212
0.167
0200HBWW224 0200HBWW225
2000201202 2000201203
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND 0.0762 0.000 ND 0.0762 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0499 0.000 ND 0.0499 0.000
6.000 ND 0.0487 0.000 ND 0.0487 0.000
0.000 ND 0.0603 0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000 ND 0.0813 0.000
0.000 ND 0.0697 0.000 ND 0.0697 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0366 0.000 ND 0.0366 0.000
0.000 ND 0.0464 0.000 ND 0.0464 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000 ND 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 5 of
.\'a'.11pl." re~11/t~· lwve bel!11. q11a/ified b~· R11diw'. "!"'JW1(io1111/ ba~<·d 011ih<'1Tlli·1w of thl' d11t11 revit•11• proces.1·. which 1':. 111odl'!t·d a/lei the ( u111rnci /.abomlm;i• /'rngram Naiioua/ /·'1111ciumal (,"uil/dill<''
{01 (hg11111c m11/ /11org11111c f l11w Rel'll'll' (11 .. \. El!.4. October 1999 11ml /·l'i1n1111:r l'J'J.1. resp .. ctive~r).
43
... .., - -.. .. .. .. .. , ".. ---... .. ~ - - -
S-NIJll' --.. -·-Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
l-Bromo-4-tluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Tim·e Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/16/2000 22: I 0
0200HBWW226
2000201201
Aaueous
RECEIVED
NA
02/02/2000 13: 15
02/04/2000 17:56
02/04/2000 17:56
1
MSDA
uQ:/L
% Recoverv
104
105
99
LIMS Workordcr: Little Washington, NC [20002012) Hamilton Beach-Proctor Silex
STLAuslin
Limits
77-117
61-143
87-113
... ...... -.. , .. ~-
0200HBWW224 0200HBWW225
2000201?02 2000201203
Aaueous Aaueous
RECEIVED RECEIVED
NA NA
02102i2000 13:40 02/02/2000 13:45
02/04/2000 19:20 02/04/2000 19:48
02/04/2000 19:20 02/04/2000 19:48
1 l
MSDA MSDA
ue:/L u2JL
F % Recoverv Limits F % Recoverv Limits
104 77-117 102 77-117
104 61-143 106 61-143
98 87-113 98 87-113
Page· 8
Sample res11/1s hm•e bee11111w/ified by Rmlia11 /111ema1io1111/ basl'd 011 J/w rrit!'ria of till' i/11111 re1•h•11• procen-, which i> """'"'""•!/la 1/ie ( u111rm·1 l.11/mr111tJ1)' /'rogmm N111io1111/ V1111c1i111111/ (i11ii!.·li11<•1
for Organic a111/ /11org1111ic l>11111 Re1•ii•11· (I 1.S. EPA, October 199911111/ i-l'lin1111:r llJ'J.I. n•rpfftil'e/_r). ·
....
F
of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Aceton itri le
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
tert-Butv I benzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW234
2000201204
Aqueous
RECEIVED
NA
02/02/2000 14: 10
02/04/2000 20: 16
02/04/200020:16
1
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND \.>..:>
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STL Austin
DL
0.286
l.67
0.983
0.0901
0.0492
0.0622
0.139
0.0683
0.136
0.106
0.179
0.0642
0.0745
0.0958
0.0484
0.0867
0.0839
0.0473
0.0756
0.0670
0.113
~l)'-~o 2-?'1
0200HBWD998 0200HBWW222
2000201205 2000201206
Aqueous Aaueous
RECEIVED RECEIVED
NA NA
02/02/2000 14: 15 02/02/2000 14:30
02/04/2000 20:44 02/04/2000 21 : 12
02/04/2000 20:44 02/04/2000 21: 12
1 I
MSDA MSDA
Ul!/L ug/L
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.286 0.000 ND 0.286 0.000
0.000 ND 1.67 0.000 ND 1.67 0.000
0.000 ND 0.983 0.000 ND 0.983 0.000
0.000 ND 0.0901 0.000 ND 0.0901 0.000
0.000 ND 0.0492 0.000 ND 0.0492 0.000
0.000 ND 0.0622 0.000 ND 0.0622 0.000
0.000 ND 0.139 0.000 ND 0.139 0.000
0.000 ND 0.0683 0.000 ND 0.0683 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.179 0.000 ND 0.179 0.000
0.000 ND 0.0642 0.000 ND 0.0642 0.000
0.000 ND 0.0745 0.000 ND 0.0745 0.000
0.000 ND 0.0958 0.000 ND 0.0958 0.000
0.000 ND LA.J 0.0484 Q.000 I ND I t-:S 0.0484 0.000
0.000 ND 0.0867 0.000 ND 0.0867 0.000
0.000 ND 0.0839 0.000 ND 0.0839 0.000
0.000 ND 0.0473 0.000 ND 0.0473 0.000
0.000 ND 0.0756 0.000 ND 0.0756 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
Page 9 or
Sample l"l!Slt/t~ lwve bee111111alijied by R111fi1111 J111en1111icmal based u11 th<' l"rit<'ria of the data l"C'l'i<'ll' process. which i.1 111tJ/h·/,·tf t!f11·r the Cumract L11/>on11111;1• l'rogrum N11tioua/ 1:11111 1w1111/ (iuid.-Ji111•1
for Organic mu/ l11org1111ic D111t1 Re1•i1·w (U.S. El'A. October 19991111d J-c/1r11arr /IJ9./. re.1pectil•C'(rJ .
43 ... , -. 1111 ........... -........ - -I .. , ...... i--
.. .. -; -s-mi0Nrv-ml .. -........ -........ --! -..
Ana1ytica1 Results
MS-VOA
.SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chiorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
ln~trument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
. 544-10-5
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW230
2000201207
Aaueous
RECEIVED
NA
02/02/2000 14:50
02/04/2000 21 :40
02/04/2000 21 :40
1
MSDA
ug/L
Cone Flag
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND lA:r
ND
ND
ND
ND
ND
ND
L.IMS Wmkorder: Little Washington, NC (20002012] Ilamilton Beach-Proctor Silex
STLAustin
DL RL
0.286 0.000
1.67 0.000
0.983 0.000
0.0901 0.000
0.0492 . 0.000
0.0622 0.000
0.139 0.000
0.0683 ·0.000
0.136 0.000
0.106 0.000
0.179 0.000
0.0642 0.000
0.0745 0.000
0.0958 0.000
0.0484 0.000
0.0867 0.000
0.0839 0.000
0.0473 0.000
0.0756 0.000
0.0670 0.000
0.113 0.000
0200HBWW220 0200HBWW216
2000201208 2000201209
Aaueous Aaueous
RECEIVED RECEIVED
NA NA
02/02/2000 15: 15 02/02/2000 15:35
02/04/2000 22:07 02/04/2000 22:35
02/04/2000 22:07 0210412000 22:35
1 1
MSDA MSDA
ug/L ug/L
Cone Flag DL RL Cone Flaa DL RL
ND 0.286 0.000 ND 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 .. 0.000
ND 0.106 0.000 ND 0.106 -0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
ND \A:S 0.0484 0.000 ND LL:S 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Pago: 14 of
St1111p/e results l1111•e bee11 q11t1/ijied by R111lit111 !111en111tion11/ bmetl VII the <rit<"ria oj the tl111tt rel'h'1t' procels, which il 111otlt"i.-tl t!ft<'f' the (imtract /.a/1orn1111:i-/'rogram Na1im111/ Fi111c110111ii (i1titll'/i11"'
jvr Org1111ic mu/ !norgt111ic i>lllt1 Re1•iew (l l.S El'A. October /9!1911111/ l·l'l•nuu:r /!JC){ 1'1'-fP('CtiPe~r/.
-13
SECTION IV
Analytical Results
MS-VOA.
SW8260B
Continued
Parameter
Chloromethane
3-Ch loroprooene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
1 2-Dibromo-3-chloropropane 96-12-8
Dibromoch loromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
L4-Dichlorobenzene 106-46-7
l J-Dich lorobenzene 541-73-1
1.2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1 2-Dichloroethane 107-06-2
I 1-Dichloroethane 75-34-3
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dich loroethene 156-60-5
1 1-Dichloroethene 75-35-4
l 3-Dichloroprooane 142-28-9
1.2-Dich loropropane 78-87-5
2.2-Dichloroprooane 594-20-7
cis-1,3-Dichloropropene 10061-01-5
1, 1-Dichloroorooene 563-58-6
trans-I 3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02116/200022:10
0200HBWW230
2000201207
Cone· Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.189 J
0.354 J
ND
0.148 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0821
0.111
0.0762
0.113
1.05
0.0564
0.152
0.0939
0.390
0.0587
0.0591
0.0920
0.113
0.0499
0.0487
0.0603
0.0813
0.0697
0.0451
0.0670
0.0714
0.0366
0.0464
0.0658
0.0647
0.0552
0.212
0.1'67
0200HBWW220 0200HBWW216
2000201208 2000201209
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND 0.0762 0.000 ND 0.0762 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0499 0.000 ND 0.0499 0.000
-0.000 ND 0.0487 0.000 ND 0.0487 0.000
0.000 ND 0.0603 0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000 ND 0.0813 0.000
0.000 ND 0.0697 0.000 ND 0.0697 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0366 0.000' ND 0.0366 0.000
0.000 ND 0.0464 0.000 ND 0.0464 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000 ND 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 15 of
Sm11p/e results hill'<' bee11 q1111/ijied by Rmli1111 illtem11tiu11a/ bml'd uu th<'< ritt'ri11 of tlll' tla/l/ re1•ii•11• proce.1·.~. ll'hich fa 11wtl..tnl '!lier the ( '011tract l.11/wm1111:)' /'m1':r11111 Na1i111w/ f-iuwtw1111/ (i111d..ti11n
fur Org1111ic 11111/ fllorg11nic /J11w Re1•it•1r (11.S. El'A. Ociob<'I' 199911111/ h•hruan 199./. resp1"C·t11·e~1 ).
43
-------~~--~~-~-~--
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
o-Xvlene/m-Xvlene
Client Sample ID
Lab Sample ID
CAS
95-47-6
106-42-3
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW230
2000201207
Cone Flaa
ND
ND
UMS Workordcr: Lillie Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0713 0.000
0.137 0.000
0200HBWW220 0200HBWW216
2000201208 2000201209
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0713 0.000 ND 0.0713 0.000
ND 0.137 0.000 ND 0.137 0.000
Pag.: 17 of
S11111p/e results hm•e bee1111wzlified by R1ulim1 /ll/('/"lllllio1111/ b11sed v11 th<' 1 r111·ri11 oj 1/1<• tla//l re1•iell' process. 11'/rich i; 111oti<'il'll 1!/ler tire Cv1111 act L11bom101y l'rogm111 N11tio1111/ h1111·t1e11111/ U11itlcli111•,
for Organic mu/ l11org11nic I>ma Re1•ic•w (US. EPA. Oc1011er 1999 1111d /·elmuu:r 199./. re~pl'Ctil'e(rJ.
43
~----~~~~--~~-~~~--
----SECTION IV
............ _ -.......... ____ _
Analytical Results
Surrogates
MS-VOA
SW8260B
Surro~ate Compound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/16/2000 22:IO
0200HBWW230
2000201207
Aoueous
RECEIVED
NA
02/02/2000 14:50
02/04/2000 21 :40
02/04/2000 21 :40
I
MSDA
ug/L
% Recovery
103
106
97
LIMS Workordcr: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0200HBWW220 0200HBWW216
2000201208 2000201209
Aqueous Aqueous
RECEIVED RECEIVED
NA NA
02/02/2000 15: 15 02/02/2000 15:35
02/04/2000 22:07 02/04/2000 22:35
02/04/2000 22:07 02/04/2000 22:35
I I
MSDA MSDA
ug/L ug/L
% Recovery Limits F % Recoverv Limits
JOI 77-117 104 77-117
107 61-143 106 61-143
99 87-113 99 87-113
Page I8
S1tmp/e res11/1s /1tl\'I! been qrw/ijied by Rmliw1 /111enw1ion11/ bt1s<'tl u11 th<' <'l'itl'ria 11} th<' d1tlll n•1•h•11• process. which i~ t111Jtl<'i1·d '!/lei the Cu111rac1 l.11bor111m:1• /'rogrw11 N111io1111/ F1111cticm11/ Guidc/1111"
fur Org11nic a111//11org11nic lJa111 Re1•i1•11· (U..\'. El'A, Ocmber 1999 aml l·<'br11111y /!N-1. r<'.1p1·c1i1•e{1J.
F
of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Aceton itri le
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromoch loromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prep~red
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/16/2000 22:10
TRIP BLANK
2000201210
Aaueous
RECEIVED
NA
02/02/2000 13:00
02/04/2000 23:03
02/04/2000 23 :03
1
MSDA
U!!/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.405 J
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.286 0.000 NA NA
1.67 0.000 NA NA
0.983 0.000 NA NA
0.0901 0.000 NA NA
0.0492 0.000 NA NA
0.0622 0.000 NA NA
0.139 0.000 NA NA
0.0683 0.000 NA NA
0.136 0.000 NA NA
0.106 0.000 NA NA
0.179 0.000 NA NA
0.0642 0.000 NA NA
0.0745 0.000 NA NA
0.0958 0.000 NA NA
0.0484 0.000 NA NA
0.0867 0.000 NA NA
0.0839 0.000 NA NA
0.0473 0.000 NA NA
0.0756 0.000 NA NA
0.0670 0.000 NA NA
0.113 0.000 NA NA
Page 19
Sample rl!s11/1s hm•e bee11111utlifled by Rculi1111 lmenw1iu1wl basl'il 011 the< n1eri11 of tlte d11lll rel'i<'ll' procr:ss, wlticlt il 1111nle!C'd 1i/1er 1/te Cu111r11<·1 l.abo/"11/0I)' /'ro.~1'<u1I N111ioua/ J-iuw11e11111t (iuidc·Ju 11"
fur Organic mu/ fllorg1111ic I>11111 Re1•it•11· (U.S. El'A. October /9991111d / l'i11w11y 199./. n'.~p1·c1frel,1J.
of 43
-----.. .. -.. - -.. --: -.. _.. - -
.... -SECTION IV -......... -.. -.. - -... ..
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
1.2-Dibron1o-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I .4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1,3-Dichlorobenzene 541-73-1
1 2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1.2-Dich loroethane 107-06-2
I 1-Dichloroethane 75-34-3
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
I, 1-Dich loroethene 75-35-4
1,3-Dichloroorooane 142-28-9
I 2-Dichloroprooane 78-87-5
2 2-Dichloropropane 594-20-7
cis-1 3-Dichloroorooene 10061-01-5
1.1-Dichloropropene 563-58-6
trans-1 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethyl benzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/16/2000 22:10
I TRIP BLANK
2000201210
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
1.
DL RL Cone Flan DL RL Cone Flan DL RL
0.0821 0.000 NA NA
0.111 0.000 NA NA
0.0762 0.000 NA NA
0.113 0.000 NA NA
1.05 0.000 NA NA
0.0564 0.000 NA NA
0.152 0.000 NA NA --
0.0939 0.000 NA NA -
0.390 0.000 NA NA
0.0587 0.000 NA NA
0.0591 0.000 NA NA
0.0920 0.000 NA NA
0.113 0.000 NA NA
0.0499 0.000 NA NA
0.0487 -0.000 NA -· NA
0.0603 0.000 NA NA -~
0.0813 0.000 NA NA
0.0697 0.000 NA NA
0.0451 0.000 NA NA
0.0670 0.000 NA NA
0.0714 0.000 NA NA
0.0366 0.000 NA NA
0.0464 0.000 NA NA
0.0658 0.000 NA NA
0.0647 0.000 NA NA
0.0552 0.000 NA NA
0.212 0.000 NA NA
0.167 0.000 NA NA
Page 20
Sample results lu11•e b<'£'11111111/ified by Rmli1111 /111em11tio1111/ based u111he c-ritai111Jj the t/11111 rel'iew process, 11'11ich i> 11wc/.-J,·cl 11jta the Co111ract l.11bora1111:i· l'rogra111 N111io1111/ F1111ctic11w/ (i11itl1·/1111·'
for Organic 11111l /11org11nic lJma Re1•i,.11· (U.S. £/'A, October 1999 111U/ I i·hrwu:r / ':)'.J.I. re.1p1·cti1·e~r1.
of
-
43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsoproovlbenzene 98-82-8
4-lsooropyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I I 1,2-Tetrachloroethane 630-20-6
l 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
l 2,4-Trichlorobenzene 120-82-1
I 2.3-Trichlorobenzene 87-61-6
1 I. I-Trichloroethane 71-55-6
l 1.2-Trichloroethane 79-00-5
Trich loroethene 79-01-6
Trichlorofluoromethane 75-69-4
l .2 3-Trichloroorooane 96-18-4
I. I 2-Trichlorotrifluoroethane 76-13-1
1.3 5-Trimethvlbenzene 108-67-8
1.2 4-Trimethvlbenzene 95-63-6
Vinyl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/16/2000 22:10
I TRIP BLANK
2000201210
Cone Flaa
ND
ND
ND
ND
ND
ND
0.0745 :r 0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workord.:r: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.0616 0.000 NA NA
0.0474 0.000 NA NA
0.0452 0.000 NA NA
0.114 0.000 NA NA
0.0469 0.000 NA NA
0.0845 0.000 NA NA
0.0796 0.000 NA NA
0.106 0.000 NA NA
0.688 0.000 NA NA
0.0886 0.000 NA NA
0.0722 0.000 NA NA
0.0948 0.000 NA NA
0.0792 0.000 NA NA
0.0568 0.000 NA NA
0.402 0.000 NA NA
0.0680 0.000 NA NA
0.118 0.000 NA NA
0.467 0.000 NA NA
0.0331 0.000 NA NA
0.0952 0.000 NA NA
0.0905 0.000 NA NA
0.208 0.000 NA NA
0.0543 0.000 NA NA
0.0766 0.000 NA NA
0.0436 0.000 NA NA
0.0749 0.000 NA NA
0.0438 0.000 NA NA
0.0574 0.000 NA NA
Pag.: 21
Sample results h11ve been 1J11t1lified by R111/i1111 /11ter11111iu1111/ bmed u11th"1·n'icri11 of the c/11111 re1•it•11• prOC'('SS, wilich fa lll<Jtll'inl 11ft•·r tit<! ( 'u11u 11c·1 l.11bonttm:I' Program N11tio1111/ F1111ctw1111/ (iuic/1'1111<•,
fur Organic mul bwrganic /J/1/11 Re1•iew (/l.S. EPA. Oc1ober /9991111tl I-el>n1111T /<)9./, resp<·c/il'e~)).
of 43
----~~--~--~---~---
.. ..
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
---·--
Client Sample ID
Lab Sample ID
TRIP BLANK
2000201210
- ---.. ---.. -
Parameter CAS Cone Flaa DL RL Cone Flaa DL RL Cone Flag DL RL
o-Xvlene 95-47-6 ND
n-Xvlene/m-Xvlene 106-42-3 ND
SECTION IV -Analytical Results -02/16/2000 22:10
LIMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
0.0713 0.000 NA NA
0.137 0.000 NA NA
Page 22
S"mple rl!s1t/1~· /1111•e bee11 q11a/ijil!d by Rmlit111 /111em111iu11a/ bmed 011 the rri1eri11 of the d111t1 n'1•h•11• process. whic·h fa uwdt'i<'d t!/ia 1/Je Cu111rm·1 l.11b11rn101:i-/'rngrnm N111io11a/ 1-'1111ct1<111al G11iill'ii111·,
fur Organic m11/ /11orga11ic Daw Rel'/cll' (l l.S £/'A. Ocwber IYY9 t1111l 1-<'hn1111:1· /IJIJ./, n'.1pcc1il'e(rJ.
of 43
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surrogate Compound
1-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -02/16/200022:10
TRIP BLANK
2000201210
Aaueous
RECEIVED
NA
02/02/2000 13:00
02/04/2000 23:03
02/04/2000 23:03
l
MSDA
ug/L
% Recoverv
101
103
98
LIMS Workordcr: Lillie 'Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustiu
Limits F % Recoverv Limits F % Recoverv Limits
77-117 77-117 77-117
61-143 61-143 61-143
87-113 87-113 87-113
Page 23
Sample results full'<' bee11 q1111lijied by Rmli1111 lu1em111iu1111I b11sed 011 th<' .-ntt'ria of the i/11111 re1•it•w process. which il lll<uli·l.-d 11/1er the ( 'u1111'11ct l.11bom101:i• l'rogr11111 N111io1111I Fwu 1w1111I G11idl'iu1n
fur Organic afl(f /nurg1111ic />alll Re1'1·1·11· (l ! .. \'. El'A. Octob1·1· /999111ul h•l11·11w:i· IY<J-1. re1p1·c1fre~1 ).
of --·---------; .. __
' -.. -·-
F
43
-
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surrogate Comoound
l-Bromo-4-fluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
Client Sample ID.
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWW213
2000202501
Aqueous
RECEIVED
NA
02/03/200008:15
02/05/2000 00:57
02/05/2000 00:57
20
MSDA
ug/L
% Recoverv
100
101
97
LIMS Workorder: Little Washington, NC (20002025) Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0200HBWW227 0200HBWD999
2000202504 2000202505
Aaueous Aqueous
RECEIVED RECEIVED
NA NA
02/03/2000 09:20 02/03/2000 09:25
02/05/2000 01 :27 02/05/2000 01 :57
02/05/2000 0 I :27 02/05/2000 0 I :57
100 100
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits
104 77-117 101 77-117
103 61-143 103 61-143
98 87-113 101 87-113
Page 13
Samp/1! results lun•e beell t/1tt1lifii!d by Riuliim lntl!ml//ional basl'd 011 tit<' rr1tc1111 of rite t/11111 re1•i1'11' procl!SS, n·lticlt i~ 11wdt'lnl 11jicl' tlte ( u1111"11c1 l.11bora101.i l'rogrw11 N111io1111/ F111wtio1111/ U11idd11w1
/01· Organic awl li10l'g11nic /Jaw Re1•i1•11· (l I..\'. £/'A. Ocwber /99911111/ /-d1r11111:r /IJIJ.f. l'l!.\pl'clil'l'(rJ.
F
or 5.J
-----------~-------
i I
I
I
I
,, -i
I
I
I
I
I RAW DATA
I
I
I
I
I
I
I
I
I
I
I
SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -Laboratory Analytical Report
Table of Contents
Report Surrmaries . . . .
Workorder Surrmary
Protocol Surrmary
Corrments and Flag Definitions
Standard Flag Definitions
Analyst Corrments . . . .
Sarrple Condition Corrments .
Analytical Results . . . . . . . . .
SW8260B . . . . . . . . .
Calibration and Quality Control Results
SW8260B . . . . . . . . . . .
Batch Surrmaries .
SW8260B .
Certifications . . .
Calibration Verification Results
Mass Spectrometer Tune
Method Blank Results
Spiked Sarrple Results .
Control Sarrple Results
Extraction/Digestion Batch Surrmary
Extraction/Digestion Batch Surrrnary
Analysis Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -02/17/200021:18
LIMS Workorder: Little Washington, NC (20002025] Hamilton Beach-Proctor Silex
STLAustin
Page
i
1
1
1
1
3
3
3
3
4
4
24
24
24
32
34
38
42
50
50
50
50
52
52
54
-------------------
-------------------SECTION II
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex
Client Code: HB-PS
Project Name: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
Facility Name: NC
Workorder Summary
Client Sample ID Lab Sample ID Sample Matrix
0200HBWW213 2000202501 Aqueous
0200HBWW214 2000202502 Aaueous
0200HBWW215 2000202503 Aqueous
0200HBWW227 2000202504 Aaueous
0200HBWD999 2000202505 Aqueous
0200HBWW228 2000202506 Aaueous
TRIP BLANK 2000202507 Aqueous
Protocol Summary
Lab Date& Time
Client Sample ID Sample ID Collected
Method: SW8260B
0200HBWW2 l 3 2000202501 02/03/00 08: 15
0200HBWW214 2000202502 02/03/00 08:35
0200HBWW214 2000202502 02/03/00 08:35
0200HBWW2 l 5 2000202503 02/03/00 08:45
0200HBWW215 2000202503 02/03/00 08:45
0200HBWW227 2000202504 02/03/00 09:20
0200HBWW227 2000202504 02/03/00 09:20
0200HBWD999 2000202505 02/03/00 09:25
0200HBWD999 2000202505 02/03/00 09:25
0200HBWW228 2000202506 02/03/00 09:35
SECTION II -Report Summaries -02/17 /2000 2I:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Method Citation Method Description
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
Date& Time Prep Date& Time Analysis Date & Time
Received Batch ID Prepared Batch ID Analvzed
02104100 09:00 1462 02105100 00:57 1462 02105100 00:57
02/04/00 09:00 1462 02/04/00 23 :31 1462 02/04/00 23:31
02104100 09:00 1482 02/08/00 01 :31 1482 ' 02/08/00 01 :31
02/04/00 09:00 1462 02/04/00 23:59 1462 02/04/00 23:59
02/04/00 09:00 1482 02/07/00 22:35 1482 02/07/00 22:35
02104100 09:00 1462 02105100 01 :27 1462 02/05/00 0 I :27
02/04/00 09:00 1482 02/07 /00 23 :04 1482 02/07/00 23:04
02/04/00 09:00 1462 02/05/00 0 I: 57 1462 02/05/00 0 I :57
02/04/00 09:00 1482 02/07/00 23:34 1482 02/07100 23 :34
02/04/00 09:00 1462 02105100 02:25 1462 02105100 02:25
-
Hold Time S >ec
Prep Analvsis
Spec Actua SPec Actua
7D 2D 70 20
70 ID 70 JD
70 50 70 50
7D ID 7D ID
7D 40 70 40
7D 20 70 20
7D 40 70 40
70 20 70 20
70 40 70 40
70 2D 70 20
Page I of 54
SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
Lab Date& Time Date& Time Prep
Client Samnle ID SamnlelD Collected Received Batch ID
Method: SW8260B continued -I TRIP BLANK I 2000202507 I 02103100 os:oo I 02104100 o9:oo I 1462
SECTION II -Report Summaries -02/17/2000 21 :18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Hold Time S11ec
Date& Time Analysis Date & Time Preo Analvsis
Preoared Batch ID Analvzed Soec Actua Soec Actual
I 02105100 00:21 I 1462 I 02/05/00 00:27 I 7D 2D I 70 20
Page 2 of 54
-------------------
--------SECTION Ill
Comments and Flag Definitions
MS-VOA
Standard Data Qualifiers
Flaa Definition
E Analvte concentration exceeded calibration range
J Result> or= MDL and <POL
NA Not analyzed/Not available
ND Not detected at the specified reoortin!! limit
0 Result does not meet tolerance in Protocol Soecification
R Result reported elsewhere
u Result less than sample soecific method detection limit
v Carrvover suspected.
Analyst Comments
I Flag I Affected Sample I Method
Sample Condition Comments
I Affected Sample I Comment
SECTION III -Comments and Flag Definitions -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
---- - - -- -- -
I Comment
Page 3 of 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/17/200021:18
0200HBWW214
2000202502
Aaueous
RECEIVED
NA
02/03/2000 08:35
02/04/2000 23: 31
02/04/2000 23 :31
I
MSDA
u11:/L
Cone Flaa
ND
ND
ND
ND
0.315 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.904
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL
0.286
1.67
0.983
0.0901
0.0492
0.0622
0.139
0.0683
0.136
0.106
0.179
0.0642
0.0745
0.0958
0.0484
0.0867
0.0839
0.0473
0.0756
0.0670
0.113
0200HBWW2 l 5 TRIP BLANK
2000202503 2000202507
Aaueous Aaueous
RECEIVED RECEIVED
NA NA
02/03/2000 08:45 02/03/2000 08:00
02/04/2000 23:59 02/05/2000 00:27
02/04/2000 23:59 02/05/2000 00:27
I 1
MSDA MSDA
u11:/L u11:/L
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 0.286 0.000 ND 0.286 0.000
0.000 ND 1.67 0.000 ND 1.67 0.000
0.000 ND 0.983 0.000 ND 0.983 0.000
0.000 ND 0.0901 0.000 ND 0.0901 0.000
0.000 0.114 J 0.0492 0.000 ND 0.0492 0.000
0.000 ND 0.0622 0.000 ND 0.0622 0.000
0.000 ND 0.139 0.000 ND 0.139 0.000
0.000 ND 0.0683 0.000 ND 0.0683 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.179 0.000 ND 0.179 0.000
0.000 ND 0.0642 0.000 ND 0.0642 0.000
0.000 ND 0.0745 0.000 ND 0.0745 0.000
o:ooo ND 0.0958 0.000 ND 0.0958 0.000
0.000 ND 0.0484 0.000 ND 0.0484 0.000
0.000 ND 0.0867 0.000 ND 0.0867 0.000
0.000 ND 0.0839 0.000 ND 0.0839 0.000
0.000 ND 0.0473 0.000 ND 0.0473 0.000
0.000 ND 0.0756 0.000 ND 0.0756 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
Page 4 of 54
-------------------
-.. - -~ ---..... - - - - --)·-- -·SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloropropene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
I 2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1,4-Dichloro-2-butene . 110-57-6
1.4-Dichlorobenzene 106-46-7
1,3-Dichlorobenzene 541-73-1
1.2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
I 2-Dichloroethane 107-06-2
1.1-Dichloroethane 75-34-3
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
l, 1-Dichloroethene 75-35-4
1.3-Dichloropropane 142-28-9
1,2-Dichloropropane 78-87-5
2.2-Dichloroorooane 594-20-7
cis-1 3-Dichloropropene 10061~01-5
1 1-Dichlorooropene 563-58-6
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -0211712000 21: 18
0200HBWW214
2000202502
Cone Flag
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.633
169 ER
11.7
0.701
13.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0821 0.000
0.111 0.000
0.0762 0.000
0.113 0.000
1.05 0.000
0.0564 0.000
0.152 0.000
0.0939 0.000
0.390 0.000
0.0587 0.000
0.0591 0.000
0.0920 0.000
0.113 0.000
0.0499 0.000
0.0487 0.000
0.0603 0.000
0.0813 0.000
0.0697 0.000
0.0451 0.000
0.0670 0.000
0.0714 0.000
0.0366 0.000
0.0464 0.000
0.0658 0.000
0.0647 0.000
0.0552 0.000
0.212 0.000
0.167 0.000
0200HBWW215 TRIP BLANK
2000202503 2000202507
Cone Flag DL RL Cone Flag DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 1.05 0.000 ND 1.05 0.000
ND 0.0564 0.000 ND 0.0564 0.000
ND 0.152 0.000 ND '(':,.-' 0.152 0.000
ND 0.0939 0.000 ND 0.0939 0.000
ND 0.390 0.000 ND 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0591 0.000 ND 0.0591 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0499 0.000 ND 0.0499 0.000
4.07 v 0.0487 0.000 ND ... 0.0487 0.000
0.0401 u 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
3.02 0.0697 0.000 ND 0.0697 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0658 0.000 ND 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND 0.212 0.000 ND 0.212 0.000
ND 0.167 0.000 ND 0.167 0.000
Page 5 of 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
lsopropylbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I. I. I 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2 4-Trichlorobenzene 120-82-1
1 2.3-Trichlorobenzene 87-61-6
1 1.1-Trichloroethane 71-55-6
l 1,2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2 3-Trichloroorooane 96-18-4
l l 2-Trichlorotrifluoroethane 76-13-1
1 3 5-Trimethvlbenzene 108-67-8
1.2 4-Trimethvlbenzene 95-63-6
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWW214
2000202502
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.289 J
ND
ND
ND
ND
ND
ND
11.5
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
DL
0.0616
0.0474
0:0452
0.114
0.0469
0.0845
0.0796
0.106
0.688
0.0886
0.0722
0.0948
0.0792
0.0568
0.402
0.0680
0.118
0.467
0.0331
0.0952
0.0905
0.208
0.0543
0.0766
0.0436
0.0749
0.0438
0.0574
0200HBWW2 l 5 TRIP BLANK
2000202503 2000202507
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
0.000 1.76 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND 0.0796 0.000 0.0668 u 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.000 19.l 0.402 0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND 0.118 0.000 ND 0.118 0.000
0.000 ND 0.467 0.000 ND 0.467 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000 0.138 J 0.0905 0.000 ND 0.0905 0.000
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 6 of 54
-.. - -~ ---... _ - - - -,--..-1 - -
- - - -.. _ - -~-·--.-... --· -... - -SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
n-Xvlene/m-Xvlene
Client Sample ID
Lab Sample ID
CAS
95-47-6
106-42-3
SECTION IV -Analytical Results -02/17/2000 21 :18
0200HBWW214
2000202502
-Cone Flaa
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0713 0.000
0.137 0.000
0200HBWW215 TRIP BLANK
2000202503 2000202507
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0713 0.000 ND 0.0713 0.000
ND 0.137 0.000 ND 0.137 0.000
Page 7 of 54
--~-~---~~-~~-~~--­SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWW213
2000202501
Aqueous
RECEIVED
NA
02/03/2000 08:15
02/05/2000 00:57
02/05/2000 00:57
20
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL RL
5.72 0.000
33.4 0.000
19.7 0.000
1.80 0.000
0.984 0.000
1.24 0.000
2.78 0.000
1.37 0.000
2.72 0.000
2.12 0.000
3.58 0.000
1.28 0.000
1.49 0.000
1.92 0.000
0.968 0.000
1.73 0.000
1.68 0.000
0.946 0.000
1.51 0.000
1.34 0.000
2.26 0.000
0200HBWW227 0200HBWD999
2000202504 2000202505
Aqueous Aqueous
RECEIVED RECEIVED
NA NA
02/03/2000 09:20 02/03/2000 09:25
02/05/2000 01 :27 02/05/2000 01 :57
02/05/2000 01 :27 02/05/2000 01 :57
100 100
MSDA MSDA
ug/L ug/L
Cone Flag DL RL Cone Flag DL RL
ND 28.6 0.000 ND 28.6 0.000
ND 167 0.000 ND 167 0.000
ND 98.3 0.000 ND 98.3 0.000
ND 9.01 0.000 ND 9.01 0.000
ND 4.92 0.000 ND 4.92 0.000
ND 6.22 0.000 ND 6.22 0.000
ND 13.9 0.000 ND 13.9 .. 0.000
ND 6.83 0.000 ND -6.83 0.000
ND 13.6 0.000 ND 13.6 0.000
ND 10.6 0.000 ND 10.6 0.000
ND 17.9 0.000 ND 17.9 0.000
ND 6.42 0.000 ND 6:42 0.000
ND 7.45 0.000 ND 7.45 0.000
ND 9.58 0.000 ND 9.58 0.000
ND 4.84 0.000 ND 4.84 0.000
ND 8.67 0.000 ND 8.67 0.000
ND 8.39 0.000 ND 8.39 0.000
ND 4.73 0.000 ND 4.73 0.000
ND 7.56 0.000 ND 7.56 0.000
ND 6.70 0.000 ND 6.70 0.000
ND 11.3 0.000 ND 11.3 0.000
Page 9 of 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloropropene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.3-Dichlorobenzene 541-73-1
1,2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1 2-Dichloroethane 107-06-2
1 1-Dichloroethane 75-34-3
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1 1-Dichloroethene 75-35-4
I 3-Dichloroorooane 142-28-9
1 2-Dichlorooropane 78-87-5
2.2-Dichloroorooane 594-20-7
cis-1 3-Dichloroorooene 10061-01-5
1.1-Dichlorooropene 563-58-6
trans-1,3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/17/200021:18
0200HBWW213
2000202501
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
6.12 J
245
40.8
ND
492
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC (20002025] Hamilton Beach-Proctor Silex
STL Austin
DL
1.64
2.22
1.52
2.26
21.0
1.13
3.04
1.88
7.80
1.17
1.18
1.84
2.26
0.998
0.974
1.21
1.63
1.39
0.902
1.34
1.43
0.732
0.928
l.32
1.29
1.10
4.24
3.34
0200HBWW227 0200HBWD999
2000202504 2000202505
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 8.21 0.000 ·ND 8.21 0.000
0.000 ND 11.1 0.000 ND 11.l 0.000
0.000 ND 7.62 0.000 ND 7.62 0.000
0.000 ND 11.3 0.000 ND 11.3 0.000
0.000 ND 105 0.000 ND 105 0.000
0.000 ND 5.64 0.000 ND 5.64 0.000
0.000 ND 15.2 0.000 ND 15.2 0.000
0.000 ND 9.39 0.000 ND 9.39 0.000
0.000 ND 39.0 0.000 ND 39.0 0.000
0.000 ND 5.87 0.000 ND 5.87 0.000
0.000 ND 5.91 0.000 ND 5.91 0.000
0.000 ND 9.20 0.000 ND 9.20 0.000
0.000 ND 11.3 0.000 ND 11.3 0.000
0.000 ND 4.99 0.000 ND 4.99 0.000
0.000 1110 4.87 0.000 1160 4.87 0.000
0.000 128 6.03 0.000 138 6.03 0.000
0.000 ND 8.13 0.000 ND 8.13 0.000
0.000 135 6.97 0.000 145 6.97 0.000
0.000 ND 4.51 0.000 ND 4.51 0.000
0.000 ND 6.70 0.000 ND 6.70 0.000
0.000 ND 7.14 0.000 ND 7.14 0.000
0.000 ND 3.66 0.000 ND 3.66 0.000
0.000 ND 4.64 0.000 ND 4.64 0.000
0.000 ND 6.58 0.000 ND 6.58 0.000
0.000 ND 6.47 0.000 ND 6.47 0.000
0.000 ND 5.52 0.000 ND 5.52 0.000
0.000 ND 21.2 0.000 ND 21.2 0.000
0.000 ND 16.7 0.000 ND 16.7 0.000
Page 10 of 54
---~~---~~-~~--~---
.. ~---.., ....... ----.. , ..... ,-........
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10--1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I 1, 1,2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2,4-Trichlorobenzene 120-82-1
I 2.3-Trichlorobenzene 87-'61-6
I I I -Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloroorooane 96-18-4
1 1.2-Trichlorotrifluoroethane 76-13-1
I 3,5-Trimethvlbenzene 108-67-8
I 2,4-Trimethvlbenzene 95-63-6
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/I 7/2000 2I:18
0200HBWW213
2000202501
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
• ND
ND
ND
ND
ND
ND
44.4
ND
ND
ND
ND
ND
2.16 J
446
ND
ND
ND
ND
ND
ND
29.3
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL RL
1.23 0.000
0.948 0.000
0.904 0.000
. 2.28 0.000
0.938 0.000
1.69 0.000
1.59 0.000
2.12 0.000
13.8 0.000
1.77 0.000
1.44 0.000
1.90 0.000
1.58 0.000
1.14 0.000
8.04 0.000
1.36 0.000
2.36 0.000
9.34 0.000
0.662 0.000
1.90 0.000
1.81 0.000
4.16 0.000
1.09 0.000
1.53 0.000
0.872 0.000
1.50 0.000
0.876 0.000
1.15 0.000.
0200HBWW227 0200HBWD999
2000202504 2000202505
Cone Flaa DL RL Cone Flaa DL RL
ND 6.16 0.000 ND 6.16 0.000
ND 4.74 0.000 ND 4.74 0.000
ND 4.52 0.000 ND 4.52 0.000
ND 11.4 0.000 ND 11.4 0.000
ND 4.69 0.000 ND 4.69 0.000
ND 8.45 0.000 ND ~·· 8.45 0.000
ND 7.96 0.000 ND --7.96 0.000
ND 10.6 0.000 ND 10.6 0.000
ND 68.8 0.000 ND 68.8 0.000
ND 8.86 0.000 ND 8.86 0.000
ND 7.22 0.000 ND 7.22 0.000
ND 9.48 0.000 ND 9.48 o:ooo
ND 7.92 0.000 ND 7.92 0.000
ND 5.68 0.000 ND 5.68 0.000
ND 40.2 0.000 ND 40.2 0.000
ND 6.80 0.000 ND 6.80 0.000
ND 11.8 0.000 ND 11.8 0.000
ND 46.7 0.000 ND 46.7 0.000
364 3.31 0.000 415 3.31 0.000
ND 9.52 0.000 ND 9.52 0.000
13.8 J 9.05 0.000 18.0 J 9.05 0.000
ND 20.8 0.000 ND 20.8 0.000
ND 5.43 0.000 ND 5.43 0.000
ND 7.66 0.000 ND 7.66 0.000
ND 4.36 0.000 ND 4.36 0.000
ND 7.49 0.000 ND 7.49 0.000
ND 4.38 0.000 ND 4.38 0.000
ND 5.74 0.000 ND 5.74 0.000
Page 11 or 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
o-Xvlene/m-Xvlene
Client Sample ID
Lab Sample ID
CAS
95-47-6
106-42-3
SECTION IV -Analytical Results -02117/2000 21 :18
0200HBWW213
2000202501
Cone Flaa
ND
ND
LIMS Workorder: Little Washington, NC (20002025] Hamilton Beach-Proctor Silex
STLAustin
0200HBWW227
2000202504
DL RL Cone Flaa DL
1.43 0.000 ND 7.13
. 2.74 0.000 ND 13.7
-~ .. -.. . ... ....... -.... -
0200HBWD999
2000202505
RL Cone Flaa DL RL
0.000 ND 7.13 0.000
0.000 ND 13.7 0.000
Page 12 of 54
.. --- -..
-~--~-~~-~~~-~-~---SECTION IV
Analytical Results
Surrogates
MS-VOA
SW82608
Surronate Comoound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/17 /2000 2I:18
0200HBWW213
2000202501
Aqueous
RECEIVED
NA
02/03/2000 08:15
02/05/2000 00:57
02/05/2000 00:57
20
MSDA
ug/L
% Recoverv
100
101
97
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0200HBWW227 0200HBWD999
2000202504 2000202505
Aqueous Aqueous
RECEIVED RECEIVED
NA NA
02/03/2000 09:20 02/03/2000 09:25
02/05/2000 01 :27 02/05/2000 01 :57
02/05/2000 0 I :27 02/05/2000 01 :57
100 100
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits F
104 77-117 101 77-117
103 61-143 103 61-143
98 87-113 101 87-113
Page 13 of 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/17/2000 21: I 8
0200HBWW228
2000202506
Aqueous
RECEIVED
NA
02/03/2000 09:35
02/05/2000 02:25
02/05/2000 02:25
5000
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL RL
1430 0.000
8350 0.000
4920 0.000
450 0.000
246 0.000
311 0.000
695 0.000
342 0.000
680 , 0.000
530 0.000
895 0.000
321 0.000
372 0.000
479 0.000
242 0.000
434 0.000
420 0.000
236 0.000
378 0.000
335 0.000
565 0.000
0200HBWW215 0200HBWW227
2000202503 2000202504
Aqueous Aqueous
RECEIVED RECEIVED
NA NA
02/03/2000 08:45 02/03/2000 09:20
02/07/2000 22:35 02/07 /2000 23 :04
02/07/2000 22:35 02/07/2000 23:04
1 20
MSDA MSDA
ug/L ug/L
Cone Flag DL RL Cone Flaa DL RL
ND 0.286 0.000 ND 5.72 0.000
ND 1.67 0.000 ND 33.4 0.000
ND 0.983 0.000 ND 19.7 0.000
ND 0.0901 0.000 ND 1.80 0.000
0.114 J 0.0492 0.000 ND 0.984 0.000
ND 0.0622 0.000 ND 1.24 0.000
ND 0.139 0.000 ND 2.78 0.000
ND 0.0683 0.000 ND 1.37 0.000
ND 0.136 0.000 ND 2.72 0.000
ND 0.106 0.000 ND 2.12 0.000
ND 0.179 0.000 ND 3.58 0.000
ND 0.0642 0.000 ND 1.28 0.000
ND 0.0745 0.000 ND 1.49 0.000
ND 0.0958 0.000 ND 1.92 0.000
ND 0.0484 0.000 ND 0.968 0.000
ND 0.0867 0.000 ND 1.73 0.000
ND 0.0839 0.000 ND 1.68 0.000
ND 0.0473 0.000 ND 0.946 0.000
ND 0.0756 0.000 ND 1.51 0.000
ND 0.0670 0.000 ND 1.34 0.000
ND 0.113 0.000 ND 2.26 0.000
Page 14 of 54 - - - -.. \_ -·-.... _ .. -.. ---· .. - -
_ .................................. -..
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter .
Chloromethane
3-Chloropropene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
1 2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
1 3-Dichlorobenzene 541-73-1
1.2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1 2-Dichloroethane 107-06-2
1 1-Dichloroethane 75-34-3
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1 1-Dichloroethene 75-35-4
1 3-Dichloroprooane 142-28-9
1 2-Dichloropropane 78-87-5
2 2-Dichloroorooane 594-20-7
cis-1 J-Dichloropropene 10061-01-5
1 1-Dichloroorooene 563-58-6
trans-I 3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/17 /2000 21: 18
0200HBWW228
2000202506
.Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
16200
1970 J
ND
71800
ND
ND
ND
ND
ND
ND
ND
414 J
ND
ND
LIMS Wbrkorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
0200HBWW215
2000202503
DL RL Cone Flaa
410 0.000 ND
555 0.000 ND
381 0.000 ND
565 0.000 ND
5250 0.000 ND
282 0.000 ND
760 0.000 ND
470 0.000 ND
1950 0.000 ND
294 0.000 ND
296 0.000 ND
460 0.000 ND
565 0.000 ND
250 0.000 ND
244 0.000 4.08
302 0.000 ND
406 0.000 ND
348 0.000 2.99
226 0.000 ND
335 0.000 ND
357 0.000 ND
183 0.000 ND
232 0.000 ND
329 0.000 ND
324 0.000 ND
276 0.000 ND
1060 0.000 ND
835 0.000 ND
0200HBWW227
2000202504
DL RL Cone Flaa DL RL
0.0821 0.000 ND 1.64 0.000
0.111 0.000 ND 2.22 0.000
0.0762 0.000 ND 1.52 0.000
0.113 0.000 ND 2.26 0.000
1.05 0.000 ND 21.0 0.000
0.0564 0.000 ND 1.13 0.000 .. · 0.152 0.000 ND 3.04 0.000
0.0939 0.000 ND 1.88 0.000
0.390 0.000 ND 7.80 0.000
0.0587 0.000 ND 1.17 0.000
0.0591 0.000 ND 1.18 0.000
0.0920 0.000 ND 1.84 0.000
0.113 0.000 ND 2.26 0.000
0.0499 0.000 4.40 J 0.998 0.000
0.0487 0.000 844 .. 0.974 0.000
0.0603 0.000 105 1.21 0.000
0.0813 0.000 ND 1.63 0.000
0.0697 0.000 108 1.39 0.000
0.0451 0.000 ND 0.902 0.000
0.0670 0.000 ND 1.34 0.000
0.0714 0.000 ND 1.43 0.000
0.0366 0.000 ND 0.732 0.000
0.0464 0.000 ND 0.928 0.000
0.0658 0.000 ND 1.32 0.000
0.0647 0.000 ND 1.29 0.000
0.0552 0.000 ND I.IO 0.000
0.212 0.000 ND 4.24 0.000
0.167 0.000 ND 3.34 0.000
Page 15 of 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Propanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1.1 1 2-Tetrachloroethane 630-20-6
1 1 2,2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2.4-Trichlorobenzene 120-82-1
1 2,3-Trichlorobenzene 87-61-6
1 1.1-Trichloroethane 71-55-6
1 1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2.3-Trichloroorooane 96-18-4
l 1,2-Trichlorotrifluoroethane 76-13-1
1 3.5-Trimethvlbenzene 108-67-8
1 2,4-Trimethvlbenzene 95-63-6
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/171200021:18
0200HBWW228
2000202506
Cone Flan
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1610 J
ND
ND
135000
ND
15000
ND
ND
ND
ND
1220 J
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL
308
237
226
570
234
422
398
530
3440
443
361
474
396
284
2010
340
590
2340
166
476
452
1040
272
383
218
374
219
287
0200HBWW215 0200HBWW227
2000202503 2000202504
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 1.23 0.000
0.000 ND 0.0474 0.000 ND 0.948 0.000
0.000 ND 0.0452 0.000 ND 0.904 0.000
0.000 ND 0.114 0.000 ND 2.28 0.000
0.000 1.81 0.0469 0.000 ND 0.938 0.000
0.000 ND 0.0845 0.000 ND 1.69 0.000
0.000 ND 0.0796 0.000 ND 1.59 0.000
0.000 ND 0.106 0.000 ND 2.12 0.000
0.000 ND 0.688 0.000 ND 13.8 0.000
0.000 ND 0.0886 0.000 ND 1.77 0.000
0.000 ND 0.0722 0.000 ND 1.44 0.000
0.000 ND 0.0948 0.000 ND 1.90 0.000
0.000 ND 0.0792 0.000 ND 1.58 0.000
0.000 ND 0.0568 0.000 ND 1.14 0.000
0.000 17.l 0.402 0.000 ND 8.04 0.000
0.000 ND 0.0680 0.000 3.56 J 1.36 0.000
0.000 ND 0.118 0.000 ND 2.36 0.000
0.000 ND 0.467 0.000 ND 9.34 0.000
0.000 ND 0.0331 0.000 310 0.662 0.000
0.000 ND 0.0952 0.000 ND 1.90 0.000
0.000 0.141 J 0.0905 0.000 12.9 1.81 0.000
0.000 ND 0.208 0.000 ND 4.16 0.000
0.000 ND 0.0543 0.000 ND 1.09 0.000
0.000 ND 0.0766 0.000 ND 1.53 0.000
0.000 ND 0.0436 0.000 ND 0.872 0.000
0.000 ND 0.0749 0.000 ND 1.50 0.000
0.000 ND 0.0438 0.000 ND 0.876 0.000
0.000 ND 0.0574 0.000 ND 1.15 0.000
Page 16 or 54 - - - - - - -......... ,._ --.. --.. -..
-~~-~~-~~~~~~~~-~-~
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
-
o-Xvlene/m-Xvlene
Client Sample ID
Lab Sample ID
.CAS.
95-47-6
106-42-3
SECTION IV -Analytical Results -02/17/200021:18
0200HBWW228
2000202506
Cone Flaa
1370 J
1760 J
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Sil!;!x
STL Austin
DL RL
356 0.000
685 0.000
0200HBWW215 0200HBWW227
2000202503 2000202504
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0713 0.000 ND 1.43 0.000
ND . 0.137 0.000 ND 2.74 0.000
Page 17 of 54
-~~--~-~~~~~-~~~~~~
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS.
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWD999
2000202505
Aaueous
RECEIVED
NA
02/03/2000 09:25
02/07/2000 23:34
0210112000 23 :34
20
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL
5.72
33.4
19.7
1.80
0.984
1.24
2.78
1.37
2.72
2.12
3.58
1.28
1.49
1.92
0.968
1.73
1.68
0.946
1.51
1.34
2.26
0200HBWW214
2000202502
Aaueous
RECEIVED
NA
02/03/2000 08:35
02/08/2000 01:31
02/08/2000 01 :3 I
5
MSDA
ug/L
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 1.43 0.000 NA
0.000 ND 8.35 0.000 NA
0.000 ND 4.92 0.000 NA
0.000 ND 0.450 0.000 NA
0.000 ND 0.246 0.000 NA
0.000 ND 0.311 0.000 NA
0.000 ND 0.695 0.000 NA
0.000 ND 0.342 0.000 NA
0.000 ND 0.680 0.000 NA
0.000 ND 0.530 0.000 NA
0.000 ND 0.895 0.000 NA
0.000 ND 0.321 0~000 NA
0.000 ND 0.372 0.000 NA
0.000 ND 0.479 0.000 NA
0.000 ND 0.242 0.000 NA
0.000 ND 0.434 0.000 NA
0.000 ND 0.420 0.000 NA
0.000 ND 0.236 0.000 NA
0.000 ND 0.378 0.000 NA
0.000 ND 0.335 0.000 NA
0.000 ND 0.565 0.000 NA
Page 19 of 54
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
1.3-Dichlorobenzene 541-73-1
1,2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1.2-Dichloroethane 107-06-2
l, 1-Dichloroethane 75-34-3
cis-1.2-Dichloroethene 156-59-2
trans-1 2-Dichloroethene 156-60-5
1 1-Dichloroethene 75-35-4
1,3-Dichloropropane 142-28-9
1 2-Dichloroorooane 78-87-5
2 2-Dichloropropane 594-20-7
cis-1 3-Dichloroorooene 10061-01-5
1 1-Dichloropropene 563-58-6
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWD999
2000202505
Cone Flag
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.65 J
839
99.3
1.91 J
103
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LJMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
0200HBWW214
2000202502
DL RL Cone Flag DL RL Cone Flan DL RL
1.64 0.000 ND 0.410 0.000 NA
2.22 0.000 ND 0.555 0.000 NA
1.52 0.000 ND 0.381 0.000 NA
2.26 0.000 ND 0.565 0.000 NA
21.0 0.000 ND 5.25 0.000 NA
1.13 0.000 ND 0.282 0.000 NA
3.04 0.000 ND 0.760 0.000 NA
1.88 0.000 ND 0.470 0.000 NA
7.80 0.000 ND 1.95 0.000 NA
1.17 0.000 ND 0.294 0.000 NA
1.18 0.000 ND 0.296 0.000 NA
1.84 0.000 ND 0.460 0.000 NA
2.26 0.000 ND 0.565 0.000 NA
0.998 0.000 ND 0.250 0.000 NA
0.974 0.000 179 0.244 0.000 NA
1.21 0.000 11.3 0.302 0.000 NA
1.63 0.000 0.670 J 0.406 0.000 NA
1.39 0.000 14.0 0.348 0.000 NA
0.902 0.000 ND 0.226 0.000 NA
1.34 0.000 ND 0.335 0.000 NA
1.43 0.000 ND 0.357 0.000 NA
0.732 0.000 ND 0.183 0.000 NA
0.928 0.000 ND 0.232 0.000 NA
1.32 0.000 ND 0.329 0.000 NA
1.29 0.000 ND 0.324 0.000 NA
1.10 0.000 ND 0.276 0.000 NA
4.24 0.000 ND 1.06 0.000 NA
3.34 0.000 ND 0.835 0.000 NA
Page 20 of 54
--· . .W - -.. -.... - -.... \ ........... ..
-----~-~---~~~~~~--SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1, 1 1 2-Tetrachloroethane 630-20-6
I I 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2 4-Trichlorobenzene 120-82-1
1·23-Trichlorobenzene 87-61-6
I I I -Trichloroethane 71-55-6
I 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorotluoromethane 7·5-69-4
I 2 3-Trichloroorooane 96-18-4
I I 2-Trichlorotritluoroethane 76-13-1
I 3 5-Trimethvlbenzene 108-67-8
1 2 4-Trimethvlbenzene 95-63-6
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWD999
2000202505
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.51 J
ND
ND
299
ND
12.0
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL
1.23
0.948
0.904
2.28
0.938
1.69
1.59
2.12
13.8
1.77
1.44
1.90
1.58
1.14
8.04
1.36
2.36
9.34
0.662
1.90
1.81
4.16
1.09
1.53
0.872
1.50
0.876
1.15
0200HBWW214
2000202502
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 0.308 0.000 NA
0.000 ND 0.237 0.000 NA
0.000 ND 0.226 0.000 NA
0.000 ND 0.570 0.000 NA
0.000 ND 0.234 0.000 NA
0.000 ND 0.422 0.000 NA ',
0.000 ND 0.398 0.000 NA '•
0.000 ND 0.530 0.000 NA
0.000 ND 3.44 0.000 NA
0.000 ND 0.443 0.000 NA
0.000 ND 0.361 0.000 NA
0.000 ND 0.474 0.000 NA
0.000 ND 0.396 0.000 NA
0.000 ND 0.284 0.000 NA
0.000 ND 2.01 0.000 NA "
0.000 ND 0.340 0.000 NA
0.000 ND 0.590 0.000 NA
0.000 ND 2.34 0.000 NA
0.000 ND 0.166 0.000 NA
0.000 ND 0.476 0.000 NA
0.000 0.565 J 0.452 0.000 NA
0.000 ND 1.04 0.000 NA
0.000 ND 0.272 0.000 NA
0.000 ND 0.383 0.000 NA
0.000 ND 0.218 0.000 NA
0.000 ND 0.374 0.000 NA
0.000 ND 0.219 0.000 NA
0.000 11.0 0.287 0.000 NA
Page 21 of 54
--~----~----~-~-~~-SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoourid
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/17/2000 21:18
0200HBWD999
2000202505
Aqueous
RECEIVED
NA
02/03/2000 09:25
02/07 /2000 23 :34
02/07 /2000 23 :34
20
MSDA
ue/L
% Recoverv
101
104
102
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Limits
77-117
61-143
87-113
0200HBWW214
2000202502
Aqueous
RECEIVED
NA
. 02/03/2000 08:35
02/08/2000 01 :31
02/08/2000 01 :31
5
MSDA
u!!IL
F % Recoverv Limits F % Recoverv Limits F
99 77-117 77-117
101 61-143 61-143
101 87-113 87-113
Page 23 of 54
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1462 Instrument Data File: A0204002.D
Instrument ID: MSDA Analyst: JEC
Parameter Reference Value Measured Cone
Acetone 20 19.7
Acetonitrile 100 88.5
Acrolein 100 86.6
Acrylonitrile 20 20.3
Benzene 20 19.5
Bromobenzene 20 19.4
Bromochloromethane 20 19.9
Bromodichloromethane 20 18.3
Bromoform 20 17.1
Brom om ethane 20 19.7
2-Butanone (MEK) 20 21.8
sec-Butv I benzene 20 19.3
tert-Butvlbenzene 20 19.6
n-Butvlbenzene 20 20.2
Carbon disulfide 20 15.8
Carbon tetrachloride 20 20.l
2-Chloro-1.3-butadiene 20 20.3
Chlorobenzene 20 19.8
Chloroethane 20 20.l
Chloroform 20 19.8
1-Chlorohexane 20 20.8
Chloromethane 20 19.l
3-Chloroorooene 20 17.2
4-Chlorotoluene 20 19.0
2-Chlorotoluene 20 19.3
1 2-Dibromo-3-chloroorooane 20 21.1
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025) Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:02/04/2000 16:04
Units: ug/L
%Recovery Flag QC Limits %Recovery
98
89
87
102
97
97
100
91
85
98
109
96
98
101
79
100
102
99
101
99 80-120
104
96
86
95
97
106
Page 24 of 54
-------~------~----
--~~-----~-------~~ SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1462 Instrument Data File: A0204002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 18.0
l 2-Dibromoethane 20 21.0
Dibromomethane 20 21.8
trans-1.4-Dichloro-2-butene 20 17.2
l 3-Dichlorobenzene 20 19.4
1 2-Dichlorobenzene 20 20.2
l 4-Dichlorobenzene 20 19.4
Dichlorodifluoromethane 20 23.l
l 2-Dichloroethane 20 20.3
l 1-Dichloroethane 20 19.9
cis-1 2-Dichloroethene 20 20.2
trans-I 2-Dichloroethene 20 20.1
1 1-Dichloroethene 20 20.2
1 3-Dichloronronane 20 20.7
1 2-Dichloronrooane 20 19.6
2 2-Dichloronronane 20 23.5
cis-1 3-Dichloronronene 20 20.4
trans-1-3-Dichloronronene 20 20.0
1 1-Dichloronronene 20 21.2
Ethvl methacrvlate 20 20.3
Ethvlbenzene 20 20.l
Hexachloro-1 3-butadiene 20 19.2
2-Hexanone 20 23.0
lodomethane 20 19.7
Isonronvlbenzene 20 20.2
4-lsonronvltoluene 20 20.0
SECTION V -Calibration and QC Information -02/17/2000 21 :18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:02/04/2000 16:04
Units: ug/L
%Recoveni Flaa QC Limits %Recoverv
90
105
109
86
97 -.-;:
101
97
115
102
99
101
100
101 80-120
103
98 8o"~l20
118
102
100
106
101
100 80-120
96
115
98
101
100
Page 25 of 54
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1462 Instrument Data File: A0204002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Methvl methacrvlate 20 20.7
Methvl tert-butvl ether (MTBE) 20 22.2
4-Methvl-2-nentanone (MIBK) 20 21.5
Methvlene chloride 20 18.6
Naohthalene 20 22.9
Prooanenitrile 100 107
n-Pronvlbenzene 20 19.l
Stvrene 20 20.7
1 L1 2-Tetrachloroethane 20 20.0
1 1.2 2-Tetrachloroethane 20 21.5
Tetrachloroethene 20 21.5
Tetrahvdrofuran 20 22.4
Toluene 20 19.6
1 2.4-Trichlorobenzene 20 22.6
1 2.3-Trichlorobenzene 20 26.l
I 1 2-Trichloroethane 20 20.8
1 1 I-Trichloroethane 20 21.4
Trichloroethene 20 20.4
Trichlorofluoromethane 20 28.6
1.2 3-Trichloronrooane 20 21.8
1.1 2-Trichlorotrifluoroethane 20 21.7
1 3 5-Trimethvlbenzene 20 19.2
1 2 4-Trimethvlbenzene 20 19.4
Vinvl acetate 20 19.6
Vinvl chloride 20 20.7
o-Xvlene 20 20.2
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:02/04/2000 16:04
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
103
111
107
93
115
107
95
103
100
108
108
112
98 80-120
113
131
104
107
102
143
109
108
96
97
98
104 80-120
101
Page 26 or 54
--------------~-~~~
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1482 Instrument Data File: A0207002.D
Instrument ID: MSDA Analyst: MER
Parameter Reference Value Measured Cone
Acetone 20 21.9
Acetonitrile 100 88.2
Acrolein 100 77.7
Acrvlonitrile 20 20.6
Benzene 20 19.9
Bromobenzene 20 20.1
Bromochloromethane 20 20.3
Bromodichloromethane 20 21.7
Bromoform 20 22.6
Brom om ethane 20 19.8
2-Butanone (MEK) 20 22.7
tert-Buty I benzene 20 19.4
sec-Butvlbenzene 20 19.4
n-Butvlbenzene 20 20.3
Carbon disulfide 20 19.5
Carbon tetrachloride 20 22.4
2-Chloro-1 3-butadiene 20 19.8
Chlorobenzene 20 20.3
Chloroethane 20 19.6
Chloroform 20 19.9
1-Chlorohexane 20 21.0
Chloromethane 20 18.5
3-Chloroorooene 20 19.8
2-Chlorotoluene 20 19.3
4-Chlorotoluene 20 18.9
1.2-Dibromo-3-chloropropane 20 22.9
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS W?rkorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:02/07/2000 16:53
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
110
88
78
103
99
100
102
109
113
99
114
97
97
102
98
112
99
101
98
100 80-120
105
92
99
96
94
115
Page 28 of 54
---~----------~--~~
---~~----------~---­SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1482 Instrument Data File: A0207002.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 22.8
1 2-Dibromoethane 20 22.l
Dibromomethane 20 22.4
trans-I 4-bichloro-2-butene 20 22.1
1 2-Dichlorobenzene 20 20.4
1 4-Dichlorobenzene 20 19.8
I 3-Dichlorobenzene 20 19.7
Dichiorodifluoromethane 20 22.5
1 1-Dichloroethane 20 19.5
1 2-Dichloroethane 20 21.4
1 1-Dichloroethene 20 19.8
cis-1-2-Dichloroethene 20 20. l
trans-1 2-Dichloroethene 20 19.6
1 2-Dichloronronane 20 20.2
1 3-Dichloronronane 20 21.3
2.2-Dichloronronane 20 23.8
1.1-Dichloronronene 20 21.l
trans-1 3-Dichloronronene 20 21.6
cis-1.3-Dichloroorooene 20 21.4
Ethvl methacrvlate 20 21.4
Ethvlbenzene 20 20.4
Hexachloro-1 3-butadiene 20 19.2
2-Hexanone 20 24.4
lodomethane 20 19.9
Isonronvlbenzene 20 20.2
4-lsonronvltoluene 20 20.1
SECTION V -Calibration and QC lnfonnation -02/17/2000 21 :18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Dateffime Analyzed:02/07/2000 16:53
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
114
110
112
1 IO
102
99
99
112
97
107
99 80-120
101
98
101 80-120
107
119
106
108
107
107
102 80-120
96
122
99
101
100
Page 29 of 54
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1482 Instrument Data File: A0207002.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Methyl methacrvlate 20 22.3
Methyl tert-butvl ether (MTBE) 20 22.9
4-Methyl-2-oentanone (MIBK) 20 23.I
Methylene chloride 20 18.7
Naphthalene 20 24.3
Prooanenitrile 100 I I I
n-Prooylbenzene 20 I8.8
Stvrene 20 21.1
I. I 2 2-Tetrachloroethane 20 22.9
I. I I 2-Tetrachloroethane 20 21.2
Tetrachloroethene 20 21.5
Tetrahvdrofuran 20 22.3
Toluene 20 20.1
I 2.3-Trichlorobenzene 20 27.3
1 2.4-Trichlorobenzene 20 23.1
I I ,2-Trichloroethane 20 21.8
1 I. I -Trichloroethane 20 21.7
Trichloroethene 20 20.5
Trichiorofluoromethane 20 29.8
I 2 3-Trichloroorooane 20 23.2
l I 2-Trichlorotrifluoroethane 20 21.2
I 2 4-Trimethylbenzene 20 19.5
l 3 5-Trimethvlbenzene 20 19.6
Vinyl acetate 20 20.3
Vinyl chloride 20 20.3
o-Xylene 20 20.4
SECTION V -Calibration and QC Information -02/17/200021:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:02/07/2000 16:53
Units: ug/L
%Recoveni Flaa QC Limits %Recoverv
111
II4
116
93
12I
111
94
106
115
106
108
11 I
100 80-120
I36
Il6
109
109
102
149
116 '
106
97
98
101
102 80-I20
102
Page 30 of 54
---~---------------
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 1462
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
Instrument Data File: A0204002.D
Injection Time: 02/04/2000 16:04
Ion Abundance Criteria
Lower Limit Unner Limit
15 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 02/04/2000 16:04
Analyst: JEC
% Relative Abundance
20.3
41.8
100
6.7
0
76.7
7.4
95.8
6.4
Page 32 of 54 _____ , _____________ _
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 1482
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
Instrument Data File: A0207002.D
Injection Time: 02/07/2000 16:53
Ion Abundance Criteria
Lower Limit Uooer Limit
15 / 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -02/17/2000 21 :18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Date Analyzed: 02/07/2000 16:53
Analyst: MER
% Relative Abundance
20.4
42.3
100
6.7
0
77.7
6.7
96.2
6.6
Page 33 of 5.J
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrv lonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
tert-Butvlbenzene
n-Butvlbenzene
sec-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
98-06-6
104-51-8
135-98-8
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
SECTION V -Calibration and QC Information -02/17/2000 21:18
1002850
Method Blank
Aqueous
02/04/2000 17:28
02/04/2000 17:28
MSDA
ug/L
Cone Flaa
2.65 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
1002896
Method Blank
Aqueous
02/07 /2000 18: 18
02/07 /2000 18: 18
MSDA
ug/L
DL RL Cone Flaa DL RL Cone Flag DL RL
0.286 0.000 ND 0.286 0.000
1.67 0.000 ND 1.67 0.000
0.983 0.000 ND 0.983 0.000
0.0901 0.000 ND 0.0901 0.000
0.0492 0.000 ND 0.0492 0.000
0.0622 0.000 ND 0.0622 0.000
0.139 0.000 ND 0.139 0.000
0.0683 0.000 ND 0.0683 0.000
0.136 0.000 ND 0.136 0.000
0.106 0.000 ND 0.106 0.000
0.179 0.000 ND 0.179 0.000
0.0958 0.000 ND 0.0958 0.000
0.0642 0.000 ND 0.0642 0.000
0.0745 0.000 ND 0.0745 0.000
0.0484 0.000 ND 0.0484 0.000
0.0867 0.000 ND 0.0867 0.000
0.0839 0.000 ND 0.0839 0.000
0.0473 0.000 ND 0.0473 0.000
0.0756 0.000 ND 0.0756 0.000
0.0670 0.000 ND 0.0670 0.000
0.113 0.000 ND 0.113 0.000
0.0821 0.000 ND 0.0821 0.000
0.111 0.000 ND 0.111 0.000
0.113 0.000 ND 0.113 0.000
0.0762 0.000 ND 0.0762 0.000
Page 34 of 54
-------------------
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1,3-Dichlorobenzene 541-73-1
1 .4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
Dichloroditluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
cis-1.2-Dichloroethene 156-59-2
trans-1 2-Dichlotoethene 156-60-5
1.1-Dichloroethene 75-35-4
1,3-Dichloropropane 142-28-9
2.2-Dichloroorooane 594-20-7
1,2-Dichloropropane 78-87-5
trans-I 3-Dichloroorooene 10061-02-6
cis-1,3-Dichloropropene 10061-01-5
1.1-Dichloroorooene 563-58-6
Ethvl methacrvlate 97-63-2
Ethyl benzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
Iodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
SECTION V -Calibration and QC Information -02/1712000 21: 18
1002850
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
DL
1.05
0.0564
0.152
0.0939
0.390
0.0591
0.0587
0.0920
0.113
0.0487
0.0499
0.0603
0.0813
0.0697
0.0451
0.0714
0.0670
0.0658
0.0366
0.0464
0.0647
0.0552
0.212
0.167
0.0616
0.0474
0.0452
0.114
0.0469
1002896
RL Cone Flag DL RL Cone Flag DL RL
0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000
0.000 ND 0.0591 0.000
0.000 ND 0.0587 0.000 --
0.000 ND 0.0920 0.000 --
0.000 ND 0.113 0.000
0.000 ND 0.0487 0.000
0.000 ND 0.0499 0.000
0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000
0.000 ND 0.0697 0.000
0.000 ND 0.0451 0.000
0.000 ND 0.0714 0.000 --
0.000 ND 0.0670 0.000
0.000 ND 0.0658 0.000
0.000 ND 0.0366 0.000
0.000 ND 0.0464 0.000
0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000
0.000 ND 0.167 0.000
0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000
0.000 ND 0.114 0.000
0.000 ND 0.0469 0.000
Page 35 of 54
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
4-Methyl-2-pentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1.1.2-Tetrachloroethane 630-20-6
I 1.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1 2 4-Trichlorobenzene 120-82-1
1.2 3-Trichlorobenzene 87-61-6
1,1 2-Trichloroethane 79-00-5
1. I I-Trichloroethane 71-55-6
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1,2,3-Trichloroorooane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
1,3,5-Trimethvlbenzene 108-67-8
I 2.4-Trimethylbenzene 95-63-6
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
o-Xylene 95-47-6
o-Xvlene/m-Xvlene 106-42-3
SECTION V -Calibration and QC Information -02/17/200021:18
1002850
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
1002896
DL RL Cone Flaa DL RL Cone Flag DL RL
0.0845 0.000 ND 0.0845 0.000
0.0796 0.000 ND 0.0796 0.000
0.106 0.000 ND 0.106 0.000
0.688 0.000 ND 0.688 0.000
0.0886 0.000 ND 0.0886 0.000
0.0722 0.000 ND 0.0722 0.000
0.0948 0.000 ND 0.0948 0.000
0.0792 0.000 ND 0.0792 0.000
0.0568 0.000 ND 0.0568 0.000
0.402 0.000 ND 0.402 0.000
0.0680 0.000 ND 0.0680 0.000
0.118 0.000 ND 0.118 0.000
0.467 0.000 ND 0.467 0.000
0.0952 0.000 ND 0.0952 0.000
0.0331 0.000 ND 0.0331 0.000
0.0905 0.000 ND 0.0905 0.000
0.208 0.000 ND 0.208 0.000
0.0543 0.000 ND 0.0543 0.000
0.0766 0.000 ND 0.0766 0.000
0.0436 0.000 ND 0.0436 0.000
0.0749 0.000 ND 0.0749 0.000
0.0438 0.000 ND 0.0438 0.000
0.0574 0.000 ND 0.0574 0.000
0.0713 0.000 ND 0.0713 0.000
0.137 0.000 ND 0.137 0.000
Page 36 of 54
-------------------
--------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Surroaate C.omoound
l-Bromo-4-fluorobenzene
1,2-Dich Ioroethane-d4
Toluene-d8
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
SECTION V -Calibration and QC Information -02/17/2000 21 :18
1002850
Method Blank
Aaueous
02/04/2000 17:28
02/04/2000 17:28
MSDA
ug/L
% Recoverv
105
104
JOO
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Limits
77-117
61-143
87-113
1002896
Method Blank
Aqueous
02/07 /2000 18: 18
02/07 /2000 18: 18
MSDA
ug/L
F % Recoverv Limits F % Recoverv Limits F
104 77-117
106 61-143
98 87-113 ..
Page 37 of 54
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Client Sample ID:
Sample Type:
Prep Batch ID:
Analysis Batch ID:
zzzzzzzzzz
Matrix Spike
1462
1462
p aren ts amp.e
2000201201
Oil Fae: 1
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
s "k d s iPI e ample
Lab ID: 1002851
Oil Fae: 1
.File. ID: A0204007.D
Parameter Cone Fla Sok Cone Cone %Rec Fla
Acetone 20 18.6
Benzene 20 20.0
Bromobenzene 20 20.7
Bromochloromethane 20 19.9
Bromodichloromethane 20 20.8
Bromoform 20 20.9
Bromomethane 20 20.2
2-Butanone (MEK) 20 20.8
tert-Butvlbenzene 20 20.5
sec-Butvlbenzene 20 20.5
n-Butvlbenzene 20 21.0
Carbon disulfide 20 20.4
Carbon tetrachloride 20 22.1
Chlorobenzene 20 20.4
Chloroethane 20 20.2
Chloroform 20 20.1
Chloromethane 20 15.2
2-Chlorotoluene 20 20.5
4-Chlorotoluene 20 19.6
1 2-Dibromo-3-chloropropane 20 20.6
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -02/17/200021:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
93
100
104
100
104
104
101
104
103
102
105
102
111
102
101
100
76
102
98
103
Lab ID:
DU Fae:
File ID:
Sok Cone
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Reported As:
% Moisture:
Analyst:
RECEIVED
NA
MER
S "k dS ip1 e I D r ampe up 1cate
1002852
1
A0204008.D
Cone %Rec Fla RPO Fla
18.3 92 1.1
21.1 105 4.9
20.8 104 0
21.3 106 5.8
21.4 107 2.8
20.5 102 1.9
21.2 106 4.8
19.4 97 7
21.2 106 2.9
21.0 105 2.9
21.8 109 3.7
20.2 101 1
23.0 115 3.5
21.1 106 3.8
21.5 ' 107 5.8
21.4 107 6.8
16.3 81 6.4
21.0 105 2.9
20.7 104 5.9
21.3 106 2.9
QC Limits
%Rec RPO
71-133 17
77-129 14
Page 38 of 54
-------------------
________ , __________ _
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Parameter
Dibromochloromethane
1.2-Dibtomoethane
Dibromomethane
1,2-Dichlorobenzene
1.3-Dichlorobenzene
1.4-Dichlorobenzene
Dichlorodifluoromethane
I, 1-Dichloroethane
1.2-Dichloroethane
l, 1-Dichloroethene
trans-1.2-Dichloroethene
cis-1 2-Dichloroethene
1,2-Dichloroprooane
2.2-Dichloropropane
1,3-Dichloroprooane
1.-1-Dichloroorooene
trans-I 3-Dichloroorooene
cis-1 3-Dichloroorooene
Ethvlbenzene
Hexachloro-1 3-butadiene
2-Hexanone
lodomethane
Isooroovlbenzene
4-lsooroovltoluene
4-Methvl-2-oentanone (MIBK)
.
p t f d aren con mue
2000201201
Oil Fae: 1
Cone Fla
s 'k d s •DI e f d amoi e con mue
Lab ID: 1002851
Oil Fae: 1
File ID: A0204007.D.
Sok Cone Cone %Rec Fla
20 21.7 108
20 21.1 105
20 21.3 107
20 20.3 101
20 20.1 101
20 20.l 100
20 22.6 113
20 20.2 101
20 20.4 102
20 20.8 104
20 20.2 101
20 20.4 102
20 19.7 98
20 22.3 112
20 21.1 105
20 22.0 110
20 20.9 104
20 21.0 105
20 21.0 105
20 19.5 97
20 21.8 109
20 20.2 101
20 21.3 107
20 20.7 104
20 20.8 104
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025) Hamilton Beach-Proctor Silex
STLAustin
s 'k d s 1p1 e amp e up 1ca econ mue l D r t f d
Lab ID: 1002852
Oil Fae: 1 QC Limits
File ID: A0204008.D
Sok Cone Cone %Rec Fla RPO Fig %Rec RPO
20 21.3 106 1.9
20 21.6 108 2.8
20 22.4 112 4.6
20 21.3 107 5.8
20 20.6 103 2
20 21.1 106 5.8
20 23.7 118 4.3
20 21.5 107 5.8
20 21.5 107 4.8
20 21.8 109 4.7 47-175 25
20 21.5 107 5.8
20 21.6 108 5.7
20 20.6 103 5
20 23.2 116 3.5 "·
20 21.4 !07 1.9
20 22.4 112 1.8
20 21.1 105 1
20 21.6 108 2.8
20 21.5 108 2.8
20 20.2 I 10 l 4
20 21.6 108 0.9
20 21.5 107 5.8
20 22.0 110 2.8
20 21.6 108 3.8
20 20.8 104 0
Page 39 of 54
-------------------SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW82608
Lab ID: 1002851
Surroaate Comoounds %Recoverv
l-Bromo-4-fluorobenzene 103
1 2-Dichloroethane-d4 102
Toluene-d8 99
Note: Spike Concentration for solid matrices not adj.usted for percent moisture.
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Lab ID: 1002852
Flaas %Recoverv Flaas QC Recoverv Limits
105 77-117
105 61-143
100 87-113
Page 41 of 54
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 1462 [MSV/1053]
1462
1462
Lab ID:
File ID:
Instrument ID: MSDA
Column:
Units: ug/L_
Matrix: Aqueous
C t l S on ro ampe
1002848
A0204003.D
Parameter· Sok Amt Cone %Rec Fla
Acetone 20
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone (MEK) 20
sec-Butvlbenzene 20
n-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
Chloromethane 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1.2-Dibromo-3-chloropropane 20
Dibromochloromethane 20
1.2-Dibromoethane 20
Dibromomethane 20
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
19.6 98
19.3 96
21.1 106
21.5 108
20.0 100
19.7 98
20.2 101
20.0 100
18.8 94
19.6 98
19.9 100
17.1 85
21.5 107
20.5 103
18.0 90
20.8 104
15.2 76
19.6 98
19.3 97
22.3 112
20.4 102
23.0 115
23.0 115
Lab ID:
File ID:
Sok Amt.
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Reported As:
% Moisture:
Analyst:
RECEIVED
NA
MER
C t l S on ro ampe up rca e l D r t
1002849
A0204004.D
Cone %Rec Fla RPO Fla
18.7 93 5.2
19.5 98 2.1
21.3 107 0.9
22.3 111 2.7
21.8 109 8.6
22.1 111 12
20.7 104 2.9
23.9 120 18
19.5 98 4.2
20.3 101 3
20.3 101 I
18.9 94 10
22.1 110 2.8
21.4 107 3.8
18.8 94 4.3
21.4 107 2.8
15.7 79 3.9
20.3 102 4
20.3 101 4
24.1 121 7.7
23.0 115 12
23.4 117 1.7
23.3 116 0.9
QC Limits
%Rec RPO
0.1-240 71
71-133 17
67-127 12
61-145 21
57-135 19
23-151 17
34-128 25
0.1-214 39
45-160 31
28-184 30
65-148 27
29-223 23
46-150 23
77-129 14 . 39-133 27
64-146 16
18-140 26
70-136 24
74-132 23
39-171 25
45-137 15
19-187 19
52-138 21
Page 42 of 54
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
I .2-Dichlorobenzene
I .4-Dichlorobenzene
I .3-Dichlorobenzene
Dichlorodifluoromethane
I, 1-Dichloroethane
l 2-Dichloroethane
1 1-Dichloroethene
trans-I 2-Dichloroethene
cis-1 2-Dichloroethene
I ,2-Dichloropropane
2 2-Dichloroorooane
I 3-Dichloroprooane
1 1-Dichlorooropene
cis-1,3-Dichloroorooene
trans-I 3-Dichloroprooene
Ethvlbenzene
Hexachloro-1 3-butadiene
2-Hexanone
lodomethane
lsooroovlbenzene
4-Isopropyltoluene
4-Methvl-2-oentanone (MIBK)
Methvlene chloride
Naphthalene
n-Proovlbenzene
Styrene
1 I 2.2-Tetrachloroethane
1 1 1 2-Tetrachloroethane
Tetrachloroethene
Toluene
1 2 3-Trichlorobenzene
SECTION V -Calibration and QC Information -02ll7/2000 21 :18
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
LIMS Workorder: Littli;: Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL.Austin
C t IS on ro f d am pie con mue
1002848 Lab ID:
A0204003.D File ID:
Cone %Rec Fla Sok Amt
20.7 I04 20
20.3 IOI 20
20.2 IOI 20
15.4 77 20
19.3 97 20
20.7 I04 20
19. l 96 20
20.0 IOO 20
19.7 98 20
19.2 96 20
23.4 117 20
21.8 I09 20
21.5 107 20
20.9 I04 20
22.1 110 20
20.4 102 20
18. I 90 20
23.7 118 20
20.l IOI 20
20.4 I02 20
19.6 98 20
23.5 117 20
18.3 91 20
24.6 123 20·
18.9 95 20
21.2 106 20
23.3 116 20
22.0 110 20
22.5 112 20
20.2 IOl 20
28.I 140 20
C t IS on ro ampe up 1cate contmue I D r d
1002849
A0204004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
21.1 I05 I 67-135 14
20.8 104 2.9 70-132 13
20.6 I03 2 68-134 14
15.8 79 2.6 0.1-166 26
20.1 100 3 66-138 19
21.1 I05 1 48-152 23
20.1 IOI 5.1 47-175 25
21.0 105 4.9 62-146 22
20.2 IOI 3 .. -66-144 18
19.7 99 3.1 61-133 17
23.5 I 18 0.9 40-168 30
22.5 113 3.6 70-128 16
22.0 110 2.8 71-155 31
20.9 I05 I 36-142 16
22.6 113 2.7 34-138 21
20.7 I04 1.9 75-131 14
19.0 95 5.4 46-150 34
24.0 120 1.7 .• 22-164 34
20.8 I04 2.9
21.4 I07 4.8 54-152 26
20.2 101 3 41-165 28
22.7 114 2.6 27-149 36
19.2 96 5.3 36-166 23
25.3 127 3.2 32-172 22
19.7 98 3.1 61-143 28
22.l I IO 3.7 68-136 14
23.6 118 1.7 47-143 20
22.8 114 3.6 63-141 20
23.1 116 3.5 69-137 16
20.6 I03 2 70-132 17
29.7 148 0 5.6 66-140 20
Page 43 of 54
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
1.2 4-Trichlorobenzene
1.1 2-Trichloroethane
I. I I-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2 3-Trichloroorooane
1.2 4-Trimethv I benzene
1.3 5-Trimethvibenzene
Vinvl acetate
Vinyl chloride
o-Xvlene
o-Xvlene/m-Xviene
SECTION V -Calibration and QC Information -02/17/2000 21 :18
Lab ID:
File ID:
SpkAmt
20
20
20
20
20
20
20
20
20
20
20
40
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
c ontro IS amp e contmue d
1002848 Lab ID:
A0204003.D File ID:
Cone %Rec Fla Sok Amt
24.5 122 20
20.8 104 20
21.l 106 20
21.3 106 20
24.0 120 20
23.1 116 20
20.0 100 20
19.2 96 20
17.9 89 20
18.5 92 20
20.2 101 20
40.6 lOI 40
c ontro IS I D ampe uplicate continued
1002849
A0204004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
24.9 124 1.6 66-144 22
21.4 I07 2.8 67-135 17
21.8 109 2.8 49-155 24
21.7 109 2.8 71-129 17
26.6 133 10 39-147 29
23.0 115 0.9 64-140 I8
20.3 102 2 54-156 25
20.0 100 4.1 62-144 25
18.3 92 3.3 0.1-164 31
19.0 95 3.2 24-I38 27
21.4 107 5.8 77-131 I5
42.6 106 4.8 76-I34 15
Page 44 of 54
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Lab ID: 1002848
Surroaate Compounds %Recoverv
l-Bromo-4-fluorobenzene 104
l ,2-Dichloroethane-d4 106
Toluene-d8 99
SECTION V -Calibration and QC Information -02/17/200021:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Lab ID: 1002849
Flaas %Recoverv Flaas QC Recoverv Limits
105 77-117
108 61-143
98 87-113
Page 45 of 54
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 1482 [MSV/1054)
1482
1482
Lab ID:
File ID!
Instrument ID:
Column:
Units:
Matrix:
c ontro IS
1002894
MSDA
ug/L
Aqueous
amoe
A0207003.D
Parameter SpkAmt Cone %Rec Fla
Acetone 20
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Brom om ethane 20
2-Butanone <MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
Chlorornethane 20
2-Chlorotoluene 20
4-Chlorotoluene 20
l .2-Dibromo-3-chloropropane 20
Dibromochloromethane 20
1.2-Dibromoethane 20
Dibromomethane 20
SECTION V -Calibration and QC Information-02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
19.4 97
20.0 100
21.0 105
22.2 111
22.8 114
24.4 122
20.3 102
22.9 115
20.2 101
19.3 96
20.0 100
18.6 93
23.5 118
20.5 103
18.7 94
21.2 106
15.5 77
19.4 97
19.5 97
25.6 128
23.9 120
23.9 119
24.6 123
Lab ID:
File ID:
SpkAmt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Reported As:
% Moisture:
Analyst:
RECEIVED
NA
MER
c ontro IS a mole D I' uo 1cate
1002895
A0207004.D
Cone %Rec Fla RPO Fla
18.5 92 5.3
19.2 96 4.1
20.6 103 1.9
21.5 108 2.7
22.2 111 2.7
23.9 119 2.5
20.0 100 2
22.9 114 0.9
19.6 98 3
18.3 92 4.3
18.9 95 5.1
18.3 91 2.2
22.I 111 6.1
20.2 101 2
18.7 93 1.1
20.6 103 2.9
14.9 75 2.6
19.1 95 2.1
18.9 94 3.1
24.5 123 4
23.3 117 2.5
22.8 114 4.3
23.l 116 5.9
QC Limits
%Rec RPO
0.1-240 71
71-133 17
67-127 12
61-145 21
57-135 19
23-151 17
34-128 25
0.1-214 39
28-184 30
45-160 31
65-148 27
29-223 23
46-150 23
77-129 14
39-133 27
64-146 16
18-140 26
70-136 24
74-132 23
39-171 25
45-137 15
19-187 19
52-138 21
Page 46 of 54
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
I 4-Dichlorobenzene
I 2-Dichlorobenzene
1 3-Dichlorobenzene
Dichlorodifluoromethane
I 2-Dichloroethane
1.1-Dichloroethane
cis-1,2-Dichloroethene
1.1-Dichloroethene ·
trans-] 2-Dichloroethene
2,2-Dichloronropane
1.2-Dichloroorooane
1,3-Dichloropropane
cis-1.3-Dichloroorooene
I, 1-Dichloropropene
trans-I 3-Dichloroorooene
Ethylbenzene
Hexachloro-1.3-butadiene
2-Hexanone
Iodomethane
Isooroovlbenzene
4-Isoproovltoluene
4-Methvl-2-oentanone (MIBK)
Methylene chloride
Naohthalene
n-Propylbenzene
Stvrene
1.1 2 2-Tetrachloroethane
1.1 I 2-Tetrachloroethane
Tetrachloroethene
Toluene
1.2 3-Trichlorobenzene
SECTION V -Calibration and QC Information -02/17/2000 21:18
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
C t IS on ro f d amp econ mue
1002894 Lab ID:
A0207003.D File ID:
Cone %Rec Fla Sok Amt
20.6 103 20
21.0 105 20
20.0 100 20
16.0 80 20
21.7 108 20
20.0 100 20
20.0 100 20
19.3 97 20
20.5 103 20
24.9 124 20
20.2 101 20
22.8 114 20
22.0 110 20
22.6 113 20
22.9 114 20
20.6 103 20
18.8 94 20
25.0 125 20
20.3 101 20
20.8 104 20
19.5 98 20
24.7 124 20
19.0 95 20
-25.7 128 20
18.6 93 20
21.3 106 20
24.5 123 20
22.7 113 20
22.6 113 20
20.2 101 20
30.4 152 Q 20
C t IS on ro ampe up 1ca e con mue I D I' t f d
1002895
A0207004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
19.7 99 4 70-132 13
20.5 103 1.9 67-135 14
19.6 98 2 68-134 14
15.1 76 5.1 0.1-166 26
20.9 105 2.8 48-152 23
19.4 97 3 66-138 19
19.6 98 2 66-144 18
19.0 95 2.1 47-175 25
19.4 97 6 62-146 22
23.2 116 6.7 ---40-168 30
19.4 97 4 61-133 17
22.1 110 3.6 70-128 16
21.4 107 2.8 36-142 16
21.1 105 7.3 71-155 31
22.0 110 3.6 34-138 21
19.5 97 6 75-131 14
17.9 90 4.3 46-150 34
24.0 120 4.1 22-164 34
20.3 102 I
19.8 99 4.9 54-152 26
19.0 95 3.1 41-165 28
23.6 118 5 27-149 36
18.5 92 3.2 36-166 23
25.0 125 2.4 32-172 22
18.4 92 I.I 61-143 28
20.5 103 2.9 68-136 14
23.4 117 5 47-143 20
21.9 109 3.6 63-141 20
21.8 109 3.6 69-137 16
19.1 96 5.1 70-132 17
28.1 140 8.2 66-140 20
Page 47 or 54
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
1,2,4-Trichlorobenzene
1.1.1-Trichloroethane
1.1.2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1 2.3-Trichloroorooane
1 3.5-Trimethvlbenzene
1 2 4-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
o-Xvlene
o-Xvlene/m-Xvlene
SECTION V -Calibration and QC Information -02117/2000 21 :IS
lab ID:
File ID:
SpkAmt
20
20
20
20
20
20
20
20
20
20
20
40
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
C t IS on ro amp e contmue d
1002894 lab ID:
A0207003.D File ID:
Cone %Rec Fla SpkAmt
24.7 123 20
21.9 109 20
21.6 108 20
21.9 110 20
26.6 133 20
24.2 121 20
19.l 95 20
20.0 100 20
18.4 92 20
18.7 94 20
20.8 104 20
41.6 104 40
c ontro IS I D r ampe up 1cate contmue d
1002895
A0207004.D QC limits
Cone %Rec Fla RPO Fla %Rec RPO
24.6 123 0 66-144 22
21.l 105 3.7 49-155 24
21.4 107 0.9 67-135 17
21.0 105 4.7 71-129 17
25.4 127 4.6 39-147 29
23.6 118 2.5 64-140 18
18.9 95 0 62-144 25
19.1 96 4.1 54-156 25
17.9 89 3.3 0.1-164 31
17.9 90 4.3 24-138 27
20.0 100 3.9 77-131 15
39.5 99 4.9 76-134 15
Page 48 of 54
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Lab ID: 1002894
Surrogate Compounds %Recovery.
1-Bromo-4-fluorobenzene 106
l.2-Dichloroethane-d4 106
Toluene-d8 101
SECTION V -Calibration and QC Information -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
Flags
Lab ID: 1002895
%Recovery Flags QC Recoverv Limits
103 77-117
108 61-143
100 87-113
Page 49 of 54
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 1462
Client Samole ID Lab Sample ID
INSTRUMENT OC 1000
INSTRUMENT OC 1406
LCS for HBN 1462 rMSV/10531 1002848
LCSD for HBN 1462 rMSV/10531 1002849
MB for HBN 1462 rMSV/10531 1002850
zzzzzzzzzz 2000201201 zzzzzzzzzz 1002851 zzzzzzzzzz 1002852 zzzzzzzzzz 2000201202 zzzzzzzzzz 2000201203 zzzzzzzzzz 2000201204 zzzzzzzzzz 2000201205 zzzzzzzzzz 2000201206 zzzzzzzzzz 2000201207 zzzzzzzzzz 2000201208 zzzzzzzzzz 2000201209 zzzzzzzzzz 2000201210
0200HBWW214 2000202502
0200HBWW215 2000202503
TRIP BLANK 2000202507
0200HBWW213 2000202501
0200HBWW227 2000202504
0200HBWD999 2000202505
0200HBWW228 2000202506
Extraction Batch ID: 1482
ECTJON VI -Batch Summaries -02/17/2000 21 :18
Start Date/Time: 02/04/2000 16:04
Stop Date/Time: 02/05/2000 02:25
SamoleTvoe Matrix
GC/MS Tune Aaueous
Continuing Calibration Check Aaueous
Lab Control Sample Aaueous
Lab Control Samole Duolicate Aaueous
Method Blank Aaueous
Field Samole Aaueous
Matrix Soike Aaueous
Matrix Soike Duplicate Aqueous
Field Sample Aaueous
Field Samole Aqueous
Field Sample Aaueous
Field Samole Aqueous
Field Sample Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Start Date/Time: 02/07/2000 16:53
Stop Date/Time: 02/08/2000 02:28
LIMS Workorder: Little Washington, NC (20002025] Hamilton Beach-Proctor Silex
STL Austin
Analyst: JEC
Samole Size
Initial Final Preoaration Method
15 mL 15mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
Analyst: MER
Page 50 of 54
-------------------
-------------------SECTIONVI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Client Samole ID · Lab Sample ID
INSTRUMENT QC 1000
INSTRUMENT OC 1406
LCS for HBN 1482 rMSV/10541 1002894
LCSD for HBN 1482 fMSV/10541 1002895
MB for HBN 1482 rMSV/10541 1002896 zzzzzzzzzz 2000202702 zzzzzzzzzz 1002897 zzzzzzzzzz 1002898 zzzzzzzzzz 2000202703 zzzzzzzzzz 2000202704 zzzzzzzzzz 2000202705 zzzzzzzzzz 2000202708 zzzzzzzzzz 2000202709
0200HBWW2 I 5 2000202503
0200HBWW227 2000202504
0200HBWD999 2000202505 zzzzzzzzzz 2000202701 zzzzzzzzzz 2000202706 zzzzzzzzzz 2000202707
0200HBWW214 2000202502 zzzzzzzzzz 2000202701 zzzzzzzzzz 2000202707
SECTION VI -Batch Summaries -02/17/2000 21 :I-8
SamoleTvoe
GC/MS Tune
Continuing Calibration Check
Lab Control Samole
Lab Control Sample Duplicate
Method Blank
Field Sample
Matrix Soike
Matrix Spike Duolicate
Field Samole
Field Sample
Field Sample
Field Samole
Field Sample
Field Samole
Field Sample
Field Samole
Field Sample
Field Samole
Field Sample
Field Samole
Field Sample
Field Samole
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STL Austin
amoe 1ze S I s·
Matrix Initial Final Preoaration Method
Aqueous 15 mL 15 mL SW8260B
Aqueous 15mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B --
Aqueous 15 mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B ..
Aqueous 15 mL 15 mL SW8260B
Page 51 of 5-1
-------------------SECTIONVI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 1482
Seauence Client Samole ID
1 INSTRUMENT QC
2 INSTRUMENT QC
continued
3 LCS for HBN 1482 rMSV/10541
4 LCSD for HBN 1482 rMSV/10541
5 MB for HBN 1482 rMSV/10541
6 zzzzzzzzzz
7 zzzzzzzzzz
8 zzzzzzzzzz
9 zzzzzzzzzz
10 zzzzzzzzzz
11 zzzzzzzzzz
12 zzzzzzzzzz
13 zzzzzzzzzz
14 0200HBWW215
15 0200HBWW227
16 0200HBWD999
17 zzzzzzzzzz
18 zzzzzzzzzz
19 zzzzzzzzzz
20 0200HBWW214
21 zzzzzzzzzz
22 zzzzzzzzzz
SECTION VI -Batch Summaries -02/I7/2000 2I :18
Lab Sample ID
1000
1406
1002894
1002895
1002896
2000202702
1002897
1002898
2000202703
2000202704
2000202705
2000202708
2000202709
2000202503
2000202504
2000202505
2000202701
2000202706
2000202707
2000202502
2000202701
2000202707
LIMS Workorder: Little Washington, NC [20002025] Hamilton Beach-Proctor Silex
STLAustin
Analvsis
Date Time SampleTvpe Analvsis File ID Sub-Batch ID
02/07/2000 16:53:00 GC/MS Tune A0207002.D 0
02/07/2000 16:53:00 Continuing Calibration Check A0207002.D . 0
02/07/2000 17:22:00 Lab Control Sample A0207003.D 0
02/07/2000 17:50:00 Lab Control Samole Duplicate A0207004.D 0
02/07/2000 18: 18:00 Method Blank A0207005.D 0
02/07/2000 18:46:00 Field Sample A0207006.D 0
02/07/2000 19:15:00 Matrix SPike A0207007.D 0
02/07/2000 19:43:00 Matrix Spike Duplicate A0207008.D '' 0
02/07/2000 20:12:00 Field Samole A0207009.D 0
02/07/2000 20:40:00 Field Sample A0207010.D 0
02/07/2000 21:09:00 Field Sample A020701 l.D 0
02/07/2000 21:37:00 Field Sample A0207012.D 0
02/07/2000 22:06:00 Field Sample A0207013.D 0
02/07/2000 22:35:00 Field Samole A0207014.D 0
02/07/2000 23:04:00 Field Sample A0207015.D 0
02/07/2000 23:34:00 Field Sample A0207016.D ' 0
02/08/2000 00:04:00 Field Sample A0207017.D -0
02/08/2000 00:33:00 Field Samole A0207018.D 0
02/08/2000 01:03:00 Field Sample A0207019.D 0
02/08/2000 01:31:00 Field Samole A0207020.D ·O
02/08/2000 02:00:00 Field Samole A0207021.D 0
02/08/2000 02:28:00 Field Sample A0207022.D 0
Page 53 or 54
SECTION VII
Certifications
State/Aaencv
Arkansas Department of Pollution Control and Ecolo!!:v
California Environmental Laboratory Accreditation Program I Waste Water/Hazardous Waste
Kansas Department of Health and Environment I Solid and Hazardous Waste/Drinking Water
Louisiana Department of Environmental Qualitv. ELAP I Waste Water/Hazardous Waste/Air/Emissions
New Jersev Deoartment of Environmental Protection
New York State Department of Health I Waste Water/Hazardous Waste
North Carolina Dept. of Natural Resources & Communitv Development I Waste Water
Oklahoma Water Resources Board I Waste Water
South Carolina Dept. of Health & Environmental Control
Utah Department of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources
US Air Force/AFCEE
US Armv Corns of Engineers (ACE)
US Department of Agriculture I Restricted Soils Permit
SECTION VII -Certifications -02/17/2000 21:18
LIMS Workorder: Little Washington, NC [20002025) Hamilton Beach-Proctor Silex
STLAustin --- --------
ID#
2257
E-10165
82005
10915
302
8720
82003002
RADC
999885260
Participating Laboratory
S-42350
Page 54 of 54 - ----- - -
SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -Laboratory Analytical Report
Table of Contents
Report Sumnaries . . . .
Workorder Surrmary
Protocol Sumnary
Corrments and Flag Definitions
Standard Flag Definitions
Analyst Corrments . . . .
Sarrple Condition Corrments
Analytical Results . . . . . . . . .
SW8260B . . . . . . . . . .
Calibration and Quality Control Results
SW8260B .......... .
Batch Sumnaries .
SW8260B
Certifications . . .
Calibration Verification Results
Mass Spectrometer Tune
Method Blank Results
Spiked Sarrple Results .
Control Sarrple Results
Extraction/Digestion Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -02/16/2000 22:10
LJMS Workorder: Littk Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Page
i
1
1
1
1
3
3
3
3
4
4
24
24
24
28
29
33
37
41
41
41
42
43
- - -'-·lllE ------- - --:-- - - -
--·------ -----~ -... _ ~-- -SECTION II
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex
Client Code: HB-PS
Project Name: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
Facility Name: NC
Workorder Summary
Client Sample ID Lab Sample ID Sample Matrix
0200HBWW226 2000201201 Aqueous
0200HBWW224 2000201202 Aqueous
0200HBWW225 2000201203 Aqueous
0200HBWW234 2000201204 Aqueous
0200HBW0998 2000201205 Aqueous
0200HBWW222 2000201206 Aqueous
0200HBWW230 2000201207 Aqueous
0200HBWW220 2000201208 Aqueous
0200HBWW216 2000201209 Aqueous
TRIP BLANK 2000201210 Aqueous
Protocol Summary
Lab -Date & Time
Client Sample ID Samole ID Collected
Method· SW8260B
0200HBWW226 2000201201 02/02/00 13: 15
0200HBWW224 2000201202 02102100 13:40
0200HBWW225 2000201203 02102100 13:45
0200HBWW234 2000201204 02/02/00 14:10
0200HBW0998 2000201205 02/02/00 14: 15
0200HBWW222 2000201206 02102100 14:30
0200HBWW230 2000201207 02/02/00 14:50
SECTION II -Report Summaries -02/16/2000 22: I 0
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Method Citation Method Descriotion
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles by GC/MS
SW8260B Volatiles bv GC/MS
SW8260B Volatiles by GC/MS
Date& Time Prep Date& Time Analysis Date & Time
Received Batch ID Prepared Batch ID Analyzed
02/03/00 09:00 1462 02/04/00 17:56 1462 02/04/00 17:56
02/03/00 09:00 1462 02/04/00 I 9 :20 1462 02/04/00 19:20
02/03/00 09:00 1462 02104100 19:48 1462 02/04/00 19:48
02/03/00 09:00 1462 02104100 20: 16 1462 02/04/00 20: 16
02/03/00 09:00 1462 02/04/00 20:44 1462 02/04/00 20:44
02/03/00 09:00 1462 02/04/00 21: 12 1462 02/04/00 21 : 12
02/03/00 09:00 1462 02/04/00 21 :40 1462 02104100 21 :40
Hold Time S1lec
Prep Anal vs is
Soec Actua Spec Actua
70 20 70 20
70 20 70 20
70 20 70 20
70 20 70 20
70 20 70 20
70 20 70 20
70 20 70 20
Page I of 43
SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
Lab Date & Time
Client Samole ID SamolelD Collected
Method: SW8260B continued -
0200HBWW220 2000201208 02102100 15: 15
0200HBWW216 2000201209 02102100 15:35
TRIP BLANK 2000201210 02102100 13:00
SECTION 11-Report Summaries -02/16/2000 22:10
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
Date& Time Prep
Received Batch ID
02/03/00 09:00 1462
02/03/00 09:00 1462
02/03/00 09:00 1462
Hold Time S1>ec
Date& Time Analysis Date&Time Prep Analvsis
Prepared Batch ID Analvzed Soec Actua Soec Actua
02/04/00 22:07 1462 02/04/00 22:07 70 20 70 20
02/04/00 22:35 1462 02/04/00 22:35 70 2D 70 20
02/04/00 23 :03 1462 02/04/00 23:03 70 2D 70 20
Page 2 of 43
----------------·---~·---
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromoch loromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -0211612000 22:10
0200HBWW226
2000201201
Aqueous
RECEIVED
NA
02/02/2000 13: 15
02/04/2000 17":56
02/04/2000 17:56
1
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STL Austin
0200HBWW224
2000201202
Aqueous
RECEIVED
NA
02/02/2000 13:40
02/04/2000 19:20
02/04/2000 19:20
I
MSDA
ug/L
DL RL Coric Flaa DL
0.286 0.000 ND 0.286
1.67 0.000 ND 1.67
0.983 0.000 ND 0.983
0.0901 0.000 ND 0.0901
0.0492 0.000 ND 0.0492
0.0622 0.000 ND 0.0622
0.139 0.000 ND 0.139
0.0683 0.000 ND 0.0683
0.136 0.000 ND 0.136
0.106 0.000 ND 0.106
0.179 0.000 ND 0.179
0.0642 0.000 ND 0.0642
0.0745 0.000 ND 0.0745
0.0958 0.000 ND 0.0958
0.0484 0.000 1.05 0.0484
0.0867 0.000 ND 0.0867
0.0839 0.000 ND 0.0839
0.0473 0.000 ND 0.0473
0.0756 0.000 ND 0.0756
0.0670 0.000 ND 0.0670
0.113 0.000 ND 0.113
.. ____ ..._ -. ___ __,_ - -·--· -
0200HBWW225
2000201203
Aqueous
RECEIVED
NA
02/02/2000 13:45
02/04/2000 19:48
02/04/2000 19:48
I
MSDA
ug/L.
RL Cone Flaa DL RL
0.000 ND 0.286 0.000
0.000 ND 1.67 0.000
0.000 ND 0.983 .0.000
0.000 ND 0.0901 0.000
0.000 ND 0.0492 0.000
0.000 ND 0.0622 0.000
0.000 ND 0.139 0.000
0.000 ND 0.0683 0.000
0.000 ND 0.136 0.000
0.000 ND 0.106 0.000
0.000 ND 0.179 0.000
0.000 ND 0.0642 0.000
0.000 ND 0.0745 0.000
0.000 ND 0.0958 0.000
0.000 ND 0.0484 0.000
0.000 ND 0.0867 0.000
0.000 ND 0.0839 0.000
0.000 ND 0.0473 0.000
0.000 ND 0.0756 0.000
0.000 ND 0.0670 0.000
0.000 ND 0.113 0.000
Page 4 of 43
----- -
-----..... ___ _
~ -. -. .. , ...... -. SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Ch loromethane
3-Chloroorooene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS ··
74-87-3
107-05-1
I 06-43-4
95-49-8
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.3-Dichlorobenzene 541-73-1
1,2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1,2-Dichloroethane 107-06-2
1.1-Dichloroethane 75-34-3
cis-1,2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
I, 1-Dichloroethene 75-35-4
1.3-Dich Ioroorooane 142-28-9
1,2-Di ch loroorooane 78-87-5
2.2-Dich!oroorooane 594-20-7
cis-1 3-Dichloroorooene 10061-01-5
1 1-Dichloroorooene 563-58-6
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 J-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW226
2000201201
..
cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
0200HBWW224
2000201202
DL RL Cone Flaa DL
0.0821 0.000 ND 0.0821
0.111 0.000 ND 0.111
0.0762 0.000 ND 0.0762
0.113 0.000 ND 0.113
1.05 0.000 ND 1.05
0.0564 0.000 ND 0.0564
0.152 0.000 ND 0.152
0.0939 0.000 ND 0.0939
0.390 0.000 ND 0.390
0.0587 0.000 ND 0.0587
0.0591 0.000 ND 0.0591
0.0920 0.000 ND 0.0920
0.113 0.000 ND 0.113
0.0499 0.000 ND 0.0499
0.0487 ttOOO ND 0.0487
0.0603 0.000 ND 0.0603
0.0813 0.000 ND 0.0813
0.0697 0.000 ND 0.0697
0.0451 0.000 ND 0.0451
0.0670 0.000 ND 0.0670
0.0714 0.000 ND 0.0714
·o.0366 0.000 ND 0.0366
0.0464 0.000 ND 0.0464
0.0658 0.000 ND 0.0658
0.0647 0.000 ND 0.0647
0.0552 0.000 ND 0.0552
0.212 0.000 ND 0.212
0.167 0.000 ND 0.167
-.. .. ... - -
0200HBWW225
2000201203
RL Cone Flaa DL RL
0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000
0.000 ND 0.0762 0.000
0.000 ·ND 0.113 0.000
0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000
0.000 ND 0.0591 0.000
0.000 ND 0.0920 0.000
0.000 ND 0.113 0.000
0.000 ND 0.0499 0.000
0.000 ND 0.0487 0.000 -· 0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000
0.000 ND 0.0697 0.000
0.000 ND 0.0451 0.000
0.000 ND 0.0670 0.000
0.000 ND 0.0714 0.000
0.000 ND 0.0366 0.000
0.000 ND 0.0464 0.000
0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000
0.000 ND 0.167 0.000
Page 5 · of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrylate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MlBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Pro pan en itrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
LI l 2-Tetrachloroethane 630-20-6
I 1 2.2-Tetrach loroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2.4-Trichlorobenzene 120-82-1
l 2,3-Trich lorobenzene 87-61-6
1 I. I-Trichloroethane 71-55-6
1 1,2-Trichloroethane 79-00-5
Tri ch loroethene 79-0i-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloropropane 96-18-4
1 I 2-Trichlorotrifluoroethane 76-13-1
I 3 5-Trimethvlbenzene 108-67-8
1,2 4-Trimethvlbenzene 95-63-6
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results-02/16/2000 22:10
0200HBWW226
2000201201
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012) Hamilton Beach-Proctor Silex
STL Austin
0200HBWW224 0200HBWW225
2000201202 2000201203
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.0616 0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.0474 0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.0452 0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.114 0.000 ND 0.114 0.000 ND 0.114 0.000
0.0469 0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.0845 0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.0796 0.000 ND 0.0796 0.000 ND 0.0796 0.000
0.106 0.000 ND 0.106 0.000 ND 0.106 0.000
0.688 0.000 ND 0.688 0.000 ND 0.688 0.000
0.0886 0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.0722 0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.0948 0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.0792 0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.0568 0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.402 0.000 ND 0.402 0.000 ND 0.402 0.000
0.0680 0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.118 0.000 ND 0.118 0.000 ND 0.118 0.000
0.467 0.000 ND 0.467 0.000 ND 0.467 0.000
0.0331 0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.0952 0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.0905 0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.208 0.000 ND 0.208 0.000 ND 0.208 0.000
0.0543 0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.0766 0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.0436 0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.0749 0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.0438 0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.0574 0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 6 of 43
... -.... -.... ---·-- - - -.... , .. - -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
l-Bromo-4-tluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -02/16/2000 22: I 0
0200HBWW226
2000201201
Aaueous
RECEIVED
NA
02/02/2000 13: 15
02/04/2000 17:56
02/04/2000 17:56
l
MSDA
ug/L
% Recoverv
104
105
99
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0200HBWW224 0200HBWW225
2000201202 2000201203
Aaueous Aaueous
RECEIVED RECEIVED
NA NA
02/02/2000 13:40 02/02/2000 13:45
02/04/2000 19:20 02/04/2000 19:48
02/04/2000 19:20 02/04/2000 19:48
1 1
MSDA MSDA
ug/L U2"/L
% Recoverv Limits F % Recoverv· Limits
104 77-117 102 77-117
104 61-143 106 61-143
98 87-113 98 87-113
Page 8
-------." . ____ , ___ .. ___ !._
F
of 43 -...
-----~~~~~-~---~---SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW234 ·
2000201204
Aoueous
RECEIVED
NA
02/02/2000 14: I 0
02/04/2000 20: 16
02/04/2000 20: 16
1
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Lillie Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
DL RL
0.286 0.000
1.67 0.000
0.983 0.000
0.0901 0.000
0.0492 0.000
0.0622 0.000
0.139 0.000
0.0683 0.000
0.136 0.000
0.106 0.000
0.179 0.000
0.0642 0.000
0.0745 0.000
0.0958 0.000
0.0484 0.000
0.0867 0.000
0.0839 0.000
0.0473 0.000
0.0756 0.000
0.0670 0.000
0.113 0.000
0200HBWD998 0200HBWW222
2000201205 2000201206
Aoueous Aqueous
RECEIVED RECEIVED
NA NA
02/02/2000 14: 15 02/02/2000 14:30
02/04/2000 20:44 02/04/2000 21: 12
02/04/2000 20:44 02/04/2000 21 : 12
I I
MSDA MSDA
ug/L ug/L
Cone Flaa DL RL Cone Flaa DL RL
ND 0.286 0.000 ND 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND
., . 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 . 0.000
ND 0.179 0.000 ND. 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
ND 0.0484 0.000 ND 0.0484 0.000
ND 0.0867 0.000 ND 0.0867. 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 Nb 0.0473 0.000
ND 0.0756 0.000 ND 0.0756. 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 9 of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloropropene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
I 2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-J ,4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
1.3-Dichlorobenzene 541-73-1
1.2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
1.2-Dich loroethane 107-06-2
1.1-Dichloroethane 75-34-3
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.1-Dichloroethene 75-35-4
I 3-Dichloropropane 142-28-9
1 2-Dichloropropane 78-87-5
2 2-Dichloropropane 594-20-7
cis-1 3-Dichloroprooene 10061-01-5
I 1-Dichloropropene 563-58-6
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW234
2000201204
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0821
0. I 11
0.0762
0.113
1.05
0.0564
0.152
0.0939
0.390
0.0587
0.0591
0.0920
0.113
0.0499
0.0487
0.0603
0.0813
0.0697
0.0451
0.0670
0.0714
0.0366
0.0464
0.0658
0.0647
0.0552
0.212
0.167
0200HBWD998 0200HBWW222
2000201205 2000201206
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND 0.0762 0.000 ND 0.0762 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0499 0.000 ND 0.0499 0.000
6.000 ND 0.0487 0.000 ND 0.0487 0.000
0.000 ND 0.0603 0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000 ND 0.0813 0.000
0.000 ND 0.0697 0.000 ND 0.0697 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0366 0.000 ND 0.0366 0.000
0.000 ND 0.0464 0.000 ND 0.0464 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000 ND 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 10 of 43
-------~-~-----~~--
~---~-~~--~-~~-~~--SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
Isoorooylbenzene 98-82-8
4-lsoproovltoluene 99-87-6
Methyl methacrylate 80-62-6
Methvl tert-butyl ether (MTBE) I634-04-4
4-Methyl-2-pentanone (MJBK) I 08-I 0-I
Methvlene chloride 75-09-2
Naphthalene 9I-20-3
Prooanenitrile 107-I2-0
n-Propylbenzene I03-65-l
Stvrene 100-42-5
I I. I 2-Tetrach loroethane 630-20-6
I I ,2 2-Tetrachloroethane 79-34-5
Tetrachloroethene .127-I8-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2 4-Trichlorobenzene I20-82-1
I .2 3-Trichlorobenzene 87-6I-6
I I I-Trichloroethane 7I-55-6.
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-0I-6
Trichlorofluoromethane 75-69-4
I ,2 3-Trichloroorooane 96-I 8-4
I. I 2-Trichlorotrifluoroethane 76-I 3-I
1,3 5-Trimethylbenzene 108-67-8
L2 4-Trimethylbenzene 95-63-6
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW234
200020I204
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
DL
0.06I6
0.0474
0.0452
0.114
0.0469
0.0845
0.0796
0.106
0.688
0.0886
0.0722
0.0948
0.0792
0.0568
0.402
0.0680
0.118
0.467
0.0331
0.09.52
0.0905
0.208
0.0543
0.0766
0.0436
0.0749
0.0438
0.0574
0200HBWD998 0200HBWW222
200020I205 200020I206
. RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.06I6 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND 0.I 14 0.000 ND 0.114 0.000
0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND 0.0796 0.000 ND ... 0.0796 0.000
0.000 ND 0.106 0.000 ND 7;:· O. I 06 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND 0.0568 0.000
-0.000 ND 0.402 0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND 0.118 0.000 ND O.I I8 0.000
0.000 ND 0.467 0.000 ND 0.467 0.000
0.000 .ND 0.033 I 0.000 ND 0.033 I 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000.
0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 11 of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
o-Xvlene/m-Xvlene
Client Sample ID
Lab Sample ID
CAS
95-47-6
106-42-3
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW234
2000201204
·Cone Flag
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0713 0.000
0.137 0.000
0200HBWD998 0200HBWW222
2000201205 2000201206
Cone Flaa DL RL Cone Flaa Dl RL
ND 0.0713 0.000 ND 0.0713 0.000
ND 0.137 0.000 ND 0.137 0.000
Page 12 of 43
----~-~------------
-~~-~~~~-----~-~---SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed·
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/16/2000 22: I 0
0200HBWW234
2000201204
Aaueous
RECEIVED
NA
02/02/2000 14:10
02/04/2000 20: 16
02/04/2000 20:16
1
MSDA
U!:!:IL
% Recoverv
103
106
97
UMS Workordcr: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0200HBWD998 0200HBWW222
2000201205 2000201206
Aaueous Aaueous
RECEIVED RECEIVED
NA NA
02/02/2000 14:15 02/02/2000 14:30
02/04/2000 20:44 02/04/2000 21: 12
02/04/2000 20:44 02/04/2000 21: 12
1 1
MSDA MSDA
ug/L ug:/L
% Recoverv Limits F % Recoverv Limits F
104 77-117 101 77-117
108 61-143 107 61-143
100 87-113 99 87-113
·Page 13 of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodich Ioromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/16/2000 22: I 0
0200HBWW230
2000201207
Aaueous
RECEIVED
NA
02/02/2000 14:50
02/04/2000 21 :40
02/04/2000 2 I :40
1
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL
0.286
1.67
0.983
0.0901
0.0492
0.0622
0.139
0.0683
0.136
0.106
0.179
0.0642
0.0745
0.0958
0.0484
0.0867
0.0839
0.0473
0.0756
0.0670
0.113
0200HBWW220 0200HBWW216
2000201208 2000201209
Aqueous Aqueous
RECEIVED RECEIVED
NA NA
02/02/2000 15: I 5 02/02/2000 15:35
02/04/2000 22:07 02/04/2000 22:35
02/04/2000 22:07 02/04/2000 22:35
I I
MSDA MSDA
ug/L ug/L
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.286 0.000 ND 0.286 0.000
0.000 ND 1.67 0.000 ND 1.67 0.000
0.000 ND 0.983 0.000 ND 0.983 0.000
0.000 ND 0.0901 0.000 ND 0.0901 0.000
0.000 ND 0.0492 0.000 ND 0.0492 0.000
0.000 ND 0.0622 0.000 ND 0.0622 0.000
0.000 ND 0.139 0.000 ND 0.139 0.000
-0.000 ND 0.0683 0.000 ND 0.0683 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.179 0.000 ND 0.179 0.000
0.000 ND 0.0642 0.000 ND 0.0642 0.000
0.000 ND 0.0745 0.000 ND 0.0745 0.000
0.000 ND 0.0958 0.000 ND 0.0958 0.000
0.000 ND 0.0484 0.000 ND 0.0484 0.000
0.000 ND 0.0867 0.000 ND 0.0867 0.000
0.000 ND 0.0839 0.000 ND 0.0839 0.000
0.000 ND 0.0473 0.000 ND 0.0473 0.000
0.000 ND 0.0756 0.000 ND 0.0756 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.113 0.000 ND 0. I 13 0.000
Page 14 of 43
-~-~-~-------------
-----~-~-----~~--~­SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloropropene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
·CAs:·
74-87-3
107-05-1
I 06-43-4
95-49-8
1.2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 '4-Dichloro-2-butene 110-57-6'
1.4-Dichlorobenzene 106-46-7
1,3-Dichlorobenzene 541-73-1
1.2-Dichlorobenzene ' 95-50-1
Dichloroditluoromethane 75-71-8
I 2-Dichloroethane 107-06-2
I, 1-Dichloroethane 75-34-3
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.1-Dichloroethene 75-35-4
1,3-Dichloroorooane 142-28-9
1.2-Dichlorooropane 78-87-5
2 2-Dichloroorooane 594-20-7
cis-1 3-Dichloroprooene 10061-01-5
I 1-Dichloroorooene 563-58-6
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/16/2000 22: I 0
0200HBWW230
2000201207
.cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.189 J
0.354 J
ND
0.148 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0821
0.111
0.0762
0.113
1.05
0.0564
0.152
0.0939
0.390
0.0587
' 0.0591
0.0920
0.113
0.0499
0.0487
0.0603
0.0813
0.0697
0.045·1
0.0670
0.0714
0.0366
0.0464
0.0658
0.0647
0.0552
0.212
0.167
0200HBWW220 0200HBWW216
2000201208 2000201209
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND. 0.111 0.000 ND 0.111 0.000
0.000 ND 0.0762 0.000 ND 0.0762 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND .. 0.0564 0.000
0.000 ND 0.152 0.000 ND ;-· 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0499 0.000 ND 0.0499 0.000
D.000 ND 0.0487 0.000 ND .. 0.0487 0.000
0.000 ND 0.0603 0.000 ND . 0.0603 0.000
0.000 ND 0.0813 0.000 ND 0.0813 0.000
0.000 ND 0.0697 0.000 ND 0.0697 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0366 0.000 ND 0.0366 0.000
0.000 ND 0.0464 0.000 ND 0.0464 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000 ND 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 15 of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
Isoproovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-l
Styrene 100-42-5
1.1 I 2-Tetrachloroethane 630-20-6
1J 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2 4-Trichlorobenzene 120-82-1
I 2 3-Trichlorobenzene 87-61-6
I I I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1,2,3-Trichloroorooane 96-18-4
I I .2-Trichlorotrifluoroethane 76-13-1
I 3,5-Trimethvlbenzene 108-67-8
I 2 4-Trimethvlbenzene 95-63-6
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW230
2000201207
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.284 J
ND
ND
ND
ND
0.661
ND
ND
ND
ND
ND
ND
ND
LJMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
0200HBWW220 0200HBWW216
2000201208 2000201209
DL RL Cone Flag DL RL Cone Flaa DL RL
0.0616 0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.0474 0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.0452 0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.114 0.000 ND 0.114 0.000 ND 0.114 0.000
0.0469 0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.0845 0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.0796 0.000 ND 0.0796 0.000 ND 0.0796 0.000
0.106 0.000 ND 0.106 0.000 ND 0.106 0.000
0.688 0.000 ND 0.688 0.000 ND 0.688 0.000
0.0886 0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.0722 0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.0948 0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.0792 0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.0568 0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.402 0.000 ND 0.402 0.000 ND 0.402 0.000
0.0680 0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.118 0.000 ND 0. I 18 0.000 ND 0.118 0.000
0.467 0.000 ND 0.467 0.000 ND 0.467 0.000
0.0331 0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.0952 0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.0905 0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.208 0.000 ND 0.208 0.000 ND 0.208 0.000
0.0543 0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.0766 0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.0436 0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.0749 0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.0438 0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.0574 0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 16 of 43 ----.--------·----,--.. -
--~~~-~~----~--~---SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
o-Xvlene/m-Xvlene
Client Sample ID
Lab Sample ID
CAS
95-47-6
106-42-3
SECTION IV -Analytical Results -0211612000 22:10
0200HBWW230
2000201207
Cone Flag
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0713 0.000
0.137 0.000
0200HBWW220 0200HBWW216
2000201208 2000201209
Cone Flaa DL RL Cone Flag DL RL
ND 0.0713 0.000 ND 0.0713 0.000
ND 0.137 0.000 ND 0.137 0.000
Page 17 of 43
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surrogate Comoound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -02/16/2000 22:10
0200HBWW230
2000201207
Aaueous
RECEIVED
NA
02/02/2000 14:50
02/04/2000 21 :40
02/04/2000 21 :40
1
MSDA
ug/L
% Recoverv
103
106
97
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-ll3
0200HBWW220 0200HBWW216
2000201208 2000201209
Aaueous Aaueous
RECEIVED RECEIVED
NA NA
02/02/2000 15: 15 02/02/2000 15:35
02/04/2000 22:07 02/04/2000 22:35
02/04/2000 22:07 02/04/2000 22:35
1 I
MSDA MSDA
ue:/L ue:/L
o/o Recovery Limits F o/o Recoverv Limits F
IOI 77-117 104 77-117
107 61-143 106 61-143
99 87-113 99 87-113
Page 18 of 43 - -.... -·-.., - - - - - -·--.. -.. -
---~-----~--------­SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bro mod ich loromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
. tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -02/16/2000 22:10
TRIP BLANK
2000201210
Aqueous
RECEIVED
NA
02/02/2000 13:00
02/04/2000 23:03
02/04/2000 23 :03
1
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.405 J
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.286 0.000 NA NA
l.67 0.000 NA NA
0.983 0.000 NA NA
0.0901 0.000 NA NA
0.0492 0.000 NA NA
0.0622 0.000 NA NA
0.139 0.000 NA NA
0.0683 0.000 NA NA -
0.136 0.000 NA NA
0.106 0.000 NA NA
0.179 0.000 NA NA
0.0642 0.000 NA NA
0.0745 0.000 NA NA
0.0958 0.000 NA NA
0.0484 0.000 NA NA
0.0867 0.000 NA NA
0.0839 0.000 NA NA
0.0473 0.000 NA NA
0.0156 0.000 NA NA
0.0670 0.000 NA NA
0.113 0.000 NA NA
Page 19 of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
4-Chlorotoluene
2-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
106-43-4
95-49-8
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1,4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.3-Dichlorobenzene 541-73-1
I ,2-Dichlorobenzene 95-50-1
Dichlorodifluoromethane 75-71-8
l 2-Dichloroethane 107-06-2
1 1-Dichloroethane 75-34-3
cis-I 2-Dichloroethene 156-59-2
trans-I .2-Dichloroethene 156-60-5
I 1-Dichloroethene 75-35-4
1,3-Dichloroorooane 142-28-9
1.2-Dichloroorooane 78-87-5
2.2-Dichloropropane 594-20-7
'
cis-1,3-Dichloroorooene 10061-01-5
I, 1-Dichloropropene 563-58-6
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -02/16/2000 22: I 0
I TRIP BLANK ~000201210
, Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [200020I2] Hamilton Beach-Proctor Silex
STL Austin
DL RL Cone Flaa DL RL Cone Flag DL RL
0.0821 0.000 NA NA
0.111 0.000 NA NA
0.0762 0.000 NA NA
0.113 0.000 NA NA
1.05 0.000 NA NA
0.0564 0.000 NA NA
0.152 0.000 NA NA
0.0939 0.000 NA NA
0.390 0.000 NA NA
0.0587 0.000 NA NA
0.0591 0.000 NA NA
0.0920 0.000 NA NA
0.113 0.000 NA NA
0.0499 0.000 NA NA
0.0487 -0.000 NA NA
0.0603 0.000 NA NA
0.0813 0.000 NA NA
0.0697 0.000 NA NA
0.0451 0.000 NA NA
0.0670 0.000 NA NA
0.0714 0.000 NA NA
0.0366 0.000 NA NA
0.0464 0.000 NA NA
0.0658 0.000 NA NA
0.0647 0.000 NA NA
0.0552 0.000 NA NA
0.212 0.000 NA NA
0.167 0.000 NA NA
Page 20 of 43
-------------------
~--------------~--­SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
isoorooylbenzene 98-82-8
4-lsoproovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone (MI BK) 108-10-1
Methylene chloride 75-09~2
Naohthalene 91-20-3
Pro pan en itrile 107-12-0
n-Propylbenzene I 03-65-1
Styrene 100-42-5
I 1.1.2-Tetrachloroethane 630-20-6
l 1.2,2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1,2 4-Trichlorobenzene 120-82-1
I 2 3-Trichlorobenzene 87-61-6
I I I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Tri ch loroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloropropane 96-18-4
I, I 2-Trichlorotrifluoroethane 76-13-1
1.3 5-Trimethylbenzene 108-67-8
I 2 4-Trimethvlbenzene 95-63-6
Vinyl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -02/16/2000 22: I 0
I TRIP BLANK
2000201210
Cone Flaa
ND
ND
ND
ND
ND
ND
0.0745 u
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.0616 0.000 NA NA
0.0474 0.000 NA NA
0.0452 0.000 NA NA
0.114 0.000 NA NA
0.0469 0.000 NA NA
0.0845 0.000 NA NA
0.0796 0.000 NA NA --
0.106 0.000 NA NA
0.688 0.000 NA NA
0.0886 0.000 NA NA
0.0722 0.000 NA NA
0.0948 0.000 NA NA
0.0792 0.000 NA NA
0.0568 0.000 NA NA
0.402 0.000 NA NA . -
0.0680 0.000 NA NA . --
0.118 0.000 NA NA
0.467 0.000 NA NA
0.0331 0.000 NA NA
0.0952 0.000 NA NA
0.0905 0.000 NA NA
0.208 0.000 NA NA
0.0543 0.000 NA NA
0.0766 0.000 NA NA
0.0436 0.000 NA NA
0.0749 0.000 NA NA
0.0438 0.000 NA NA
0.0574 0.000 NA NA
Page 21 of 43
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene
o-X vlene/m-X vlene
Client Sample ID
Lab Sample ID
CAS
95-47-6
106-42-3
SECTION IV -Analytical Results -02/16/2000 22:10
I TRIP BLANK
2000201210
Cone Flaa
ND
ND
LJMS Workordcr: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0713
0.137
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 NA NA
0.000 NA NA
Page 22 of 43
-------------------
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surro~ate Compound
l -Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
TRIP BLANK
2000201210
Aaueous
RECEIVED
NA
02/02/2000 I 3 :00
02/04/2000 23:03
02/04/2000 23:03
1
MSDA
ue:/L
% Recoverv
101
103
98
SECTION IV -Analytical Results-02/16/2000 22:10 .
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
Limits F % Recoverv ~Limits F % Recoveiv Limits F
77-117 77-117 77-117
61-143 61-143 61-143
87-113 87-113 87-113
Page 23 of 43
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1462 Instrument Data File: A0204002.D
Instrument ID: MSDA Analyst: JEC
Parameter Reference Value Measured Cone
Acetone 20 19.7
Acetonitrile 100 88.5
Acrolein 100 86.6
Acrvlonitrile 20 20.3
Benzene 20 19.5
Bromobenzene 20 19.4
Bromochloromethane 20 19.9
• Bromodichloromethane 20 18.3
Bromoform 20 17. l
Bromomethane 20 19.7
2-Butanone (MEK) 20 21.8
n-Butylbenzene 20 20.2
sec-Butvlbenzene 20 19.3
tert-Butvlbenzene 20 19.6
Carbon disulfide 20 15.8
Carbon tetrachloride 20 20.I
2-Chloro-I 3-butadiene 20 20.3
Chlorobenzene 20 19.8
Chloroethane 20 20.1
Chloroform 20 19.8
1-Ch lorohexane 20 20.8
Chloromethane 20 19.1
3-Chloroprooene 20 17.2
4-Chlorotoluene 20 19.0
2-Chlorotoluene 20 19.3
I 2-Dibromo-3-chlorooropane 20 21.1
SECTION V -Calibration and QC Information -02/16/2000 22:10
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:02/04/2000 16:04
Units: ug/L
%Recovery Flaa QC Limits %Recoverv
98
89
87
102
97
97
100
91
85
98
109 .
IOI
96
98
79
100
102
99
101
99 80-120
104
96
86
95
97
106
Page 24 of 43
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1462 Instrument Data File: A0204002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 18.0
1,2-Dibromoethane 20 21.0
Dibromomethane 20 21.8
trans-1,4-Dichloro-2-butene 20 17.2
1 3-Dichlorobenzene 20 19.4
1 2-Dichlorobenzene 20 20.2
14-Dichlorobenzene 20 19.4
Dichlorodifluoromethane 20 23.1
1 2-Dichloroethane 20 20.3
I 1-Dichloroethane 20 19.9
1 1-Dichloroethene 20 20.2
trans-I 2-Dichloroethene 20 20.1
cis-1 2-Dichloroethene 20 20.2
2 2-Dichloroorooane 20 23.5
I 2-Dichloronronane 20 19.6
I 3-Dichloroorooane 20 20.7
I 1-Dichloronrooene 20 21.2
trans-I 3-Dichloroorooene 20 20.0
. cis-1-3-Dichloroorooene 20 20.4
Ethvl methacrvlate 20 20.3
Ethvlbenzene 20 20.1
Hexachloro-1-3-butadiene 20 19.2
2-Hexanone 20 23.0
Iodomethane 20 19.7
Isooroovlbenzene 20 20.2
4-lsonronvltoluene 20 20.0
SECTION V -Calibration and QC Information -02/16/200022:10
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
Flaa·
..
Date/Time Analyzed:02/04/2000 16:04
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
90
105
109
86
97
101
97
115
102
99
101 80-120
100
IOI
I I8
98 80-I20
103
I06
100
I02
101 '
100 80-120
96
115
98
101
100
Page 25 of 43
SECTION V
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 1462 Instrument Data File: A0204002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Methvl methacrvlate 20 20.7
Methvl tert-butvl ether <MTBE) 20 22.2
4-Methvl-2-oentanone (MJBK) 20 21.5
Methvlene chloride 20 18.6
Nanhthalene 20 22.9
Prooanenitrile 100 107
n-Proovlbenzene 20 19.1
Stvrene 20 20.7
I 1.1-2-Tetrachloroethane 20 20.0
I 1 2.2-Tetrachloroethane 20 21.5
Tetrachloroethene 20 21.5
Tetrahvdrofuran 20 22.4
Toluene 20 19.6
1 2.3-Trichlorobenzene 20 26.1
I 24-Trichlorobenzene 20 22.6
I LI-Trichloroethane 20 21.4
1 I 2-Trichloroethane 20 20.8
Trichloroethene 20 20.4
Trichlorofluoromethane 20 28.6
1.2 3-Trichloronrooane 20 21.8
1 1.2-Trichlorotrifluoroethane 20 21.7
1 3.5-Trimethvlbenzene 20 19.2
1.2.4-Trimethvlbenzene 20 19.4
Vinvl acetate 20 19.6
Vinvl chloride 20 20.7
o-Xvlene 20 20.2
SECTION V -Calibration and QC Information -02/16/2000 22:10
LIMS Workordcr: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:02/04/2000 16:04
Units: ug/L
%Recoveni Flaa QC Limits %Recoverv
103
111
107
93
115
107
95
103
100
108
108
112
98 80-120
131
113
107
104
102
143
109
108
96
97
98
104 80-120
101
Page 26 of 43
-------------------
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 1462
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
Instrument Data File: A0204002.D
Injection Time: 02/04/2000 16:04
, Ion Abundance Criteria
Lower Limit Uooer Limit ,
15 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -02/16/2000 22:10
LIMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 02/04/2000 16:04
Analyst: JEC
% Relative Abundance
20.3
41.8
100
6.7
0
76.7
7.4
95.8
6.4
Page 28 of 43
-------------------
'
----------~-------­SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
tert-Butvlbenzene
sec-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Ch Iorobenzene
Chloroethane
Chloroform
I-Ch lorohexane
Ch loromethane
3-Chloroprooene
4-Chloro,toluene
2-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
98-06-6
135-98-8
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
106-43-4
95-49-8
'.
SECTION V -Calibration and QC Information -02/16/2000 22: I 0
1002850
Method Blank
Aaueous
02/04/2000 17:28
02/04/2000 17:28
MSDA
ug/L
Cone Flaa
2.65 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.286 0.000
1.67 0.000
0.983 0.000
0.0901 0.000
0.0492 0.000
0.0622 0.000
0.139 0.000
0.0683 0.000
0.136 0.000
0. 106 0.000
0.179 0.000
0.0642 0.000
0.0958 0.000
0.0745 0.000
0.0484 0.000
0.0867 0.000
0.0839 0.000
0.0473 0.000
0.0756 0.000
0.0670 0.000
0. 113 0.000
0.0821 0.000
0.111 0.000
0.0762 0.000
0.113 0.000
Page 29 of 43
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I ,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-l .4-Dichloro-2-butene 110-57-6
I 2-Dichlorobenzene 95-50-1
I 4-Dichlorobenzene 106-46-7
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1,2-Dichloroethane I 07-06-2
1.1-Dichloroethane 75-34-3
I, 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
2 2-Dichloroorooane 594-20-7
1 3-Dichloroprooane 142-28-9
1 2-Dichloroorooane 78-87-5
1 1-Dichloroorooene 563-58-6
cis-1,3-Dichloroorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrylate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 J-butadiene 87-68-3
2-Hexanone 591-78-6
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsoorooyltoluene 99-87-6
Methyl methacrylate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
SECTION V -Calibration and QC Information -02116/2000 22:10
1002850
cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workordcr: Litlle Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL Cone Flaa DL RL
1.05 0.000
0.0564 0.000
0.152 0.000
0.0939 0.000
0.390 0.000
0.0920 0.000
0.0587 0.000
0.0591 0.000
0.113 0.000
0.0499 0.000
0.0487 0.000
0.0697 0.000
0.0603 0.000
0.0813 0.000
0.0714 0.000 .
0.0451 0.000
0.0670 0.000
0.0464 0.000
0.0366 0.000
0.0658 0.000
0.0647 0.000
0.0552 0.000
0.212 0.000
0.167 0.000
0.0616 0.000
0.0474 0.000
0.0452 0.000
0.114 0.000
0.0469 0.000
Page 30 of 43
-------------------
-------------------SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS -,
4-Methyl-2-oentanone (MIBK) I 08-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene I 03-65-1
Stvrene 100-42-5
I.I 2 2-Tetrachloroethane 79-34-5
I, I I 2-Tetrachloroethane 630-20-6
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1,2.4-Trichlorobenzene 120-82-1
12 3-Trichlorobenzene 87-61-6
I , l I -Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorotluoromethane 75-69-4
I 2.3-Trich loroprooane 96-18-4
I 1.2-Trichlorotritluoroethane 76-13-1
I 3.5-Trimethvlbenzene 108-67-8
1.2.4-Trimethylbenzene 95-63-6
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
o-Xylene 95-47-6
p-Xvlene/m-Xvlene 106-42-3
': '.
SECTION Y -Calibration and QC Information -02/16/2000 22: I 0
1002850
Cone Flag
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
UMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
DL RL Cone Flag DL RL Cone Flaa DL RL
0.0845 0.000
0.0796 0.000
0.106 0.000
0.688 0.000
0.0886 0.000
0.0722 0.000
0.0792 0.000 -
0.0948 0.000 "
0.0568 0.000
0.402 0.000
0.0680 0.000
0.118 0.000
0.467 0.000
0.0331 0.000
0.0952 0.000
0.0905 0.000
0.208 0.000
0.0543 0.000
0.0766 0.000
0.0436 0.000
0.0749 0.000
0.0438 0.000
0.0574 0.000
0.0713 0.000
0.137 0.000
Page 31 of 43
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
Surroaate Comoound
1-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -02/16/2000 22: I 0
1002850
Method Blank
Aqueous
02/04/2000 17:28
02/04/2000 17:28
MSDA
ug/L
% Recoverv
105
104
100
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
Limits F % Recoverv Limits F % Recoverv limits F
77-117
61-143
87-113
Page 32 of 43
-------------------
--- - - - - - - - - - - - - - - - - -SECTION V
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Client Sample ID:
Sample Type:
Prep Batch ID:
Analysis Batch ID:
0200HBWW226
Matrix Spike
1462
1462
p aren ts amo!e
2000401201
DU Fae: 1
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
S 'k dS •PI e amp e
Lab ID: 1002851
Oil Fae: 1
File ID: A0204007.D
Parameter Cone Fla Sok Cone Cone %Rec Fig
Acetone ND 20 18.6
Benzene ND 20 20.0
Bromobenzene ND 20 20.7
Bromochloromethane ND 20 19.9
Bromodichloromethane ND 20 20.8
Bromoform ND 20 20.9
Bromomethane ND 20 20.2
2-Butanone (MEK) ND 20 20.8
sec-Butyl benzene ND 20 20.5
tert-Butvlbenzene ND 20 20.5
n-Butvlbenzene ND 20 21.0
Carbon disulfide ND 20 20.4
Carbon tetrachloride ND 20 22.1
Ch lorobenzene ND 20 20.4
Chloroethane ND 20 20.2
Chloroform ND 20 20.1
Chloromethane ND 20 15.2
4-Chlorotoluene ND 20 19.6
2-Chlorotoluene ND 20 20.5
I 2-Dibromo~3-chloroorooane ND 20 20.6
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -02/16/2000 22: I 0
LIMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
93
100
104
100
104
104
101
104 .. 102
103
105
102
111
102
101
100
76
98
102
103
Reported As: RECEIVED
% Moisture: NA
Analyst: MER
s "k d s ;p1 e ampe up 1cate I D r
Lab ID: 1002852
Oil Fae: 1 QC Limits
File ID: A0204008.D
SpkConc Cone o/oRec Fig RPO Fla %Rec RPO
20 18.3 92 1.1
20 21.1 105 4.9 71-133 17
20 20.8 104 0
20 21.3 106 5.8
20 21.4 107 2.8
20 20.5 102 1.9
20 21.2 106 4.8
20 19.4 97 7
20 21.0 105 2.9
20 21.2 106 2.9
20 21.8 109 3.7
20 20.2 IOI I
20 23.0 115 3.5
20 21.1 106 3.8 77-129 14
20 21.5 107 5.8
20 21.4 107 6.8
20 16.3 81 6.4
20 20.7 104 5.9
20 21.0 105 2.9
20 21.3 106 2.9
Page 33 of 43
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Parameter
Dibromochloromethane
1 2-Dibromoethane
bibromomethane
I 4-Dichlorobenzene
I 3-Dichlorobenzene
I 2-Dichlorobenzene
Dichlorodifluoromethane
I 2-Dichloroethane
1.1-Dichloroethane
1.1-Dichloroethene
trans-I 2-Dichloroethene
cis-1.2-Dichloroethene
1.2-Dichloroorooane
2 2-Dichloroorooane
I 3-Dichloroorooane
cis-1 3-Dichloroorooene
trans-I 3-Dichloroorooene
I, 1-Dichloroorooene
Ethvlbenzene
Hexachloro-1 3-butadiene
2-Hexanone
lodomethane
lsooroovlbenzene
4-Isooroovltoluene
4-Methvl-2-oentanone (MIBK)
p t f d aren con mue
2000201201
Oil Fae: 1
Cone Fla
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
s 'k d s •DI e amp e contmue d
Lab ID: 1002851
Oil Fae: 1
File ID: A0204007.D
Sok Cone Cone %Rec Fla
20 21.7 108
20 21.1 105
20 21.3 107
20 20.l 100
20 20.1 101
20 20.3 101
20 22.6 113
20 20.4 102
20 20.2 101
20 20.8 104
20 20.2 101
20 20.4 102
20 19.7 98
20 22.3 112
20 21.1 105
20 21.0 105
20 20.9 104
20 22.0 110
20 21.0 105
20 19.5 97
20 21.8 109
20 20.2 101
20 21.3 107
20 20.7 104
20 20.8 104
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -02/16/2000 22:10
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
s 'k d s iPI e ampe up 1cate contmue I D I' d
Lab ID: 1002852
Oil Fae: 1 QC Limits
File ID: A0204008.D
Sok Cone Cone %Rec Fla RPO Fla ·%Rec RPO
20 21.3 106 1.9
20 21.6 108 2.8
20 22.4 112 4.6
20 21.1 106 5.8
20 20.6 103 2
20 21.3 107 5.8
20 23.7 118 4.3
20 21.5 107 4.8
20 21.5 107 5.8
20 21.8 109 4.7 47-175 25
20 21.5 107 5.8
20 21.6 108 5.7
20 20.6 103 5
20 23.2 116 3.5
20 21.4 107 1.9
20 21.6 108 2.8
20 21.1 105 1
20 22.4 112 1.8
20 21.5 108 2.8
20 20.2 101 4
20 21.6 108 0.9
20 21.5 107 5.8
20 22.0 110 2.8
20 21.6 108 3.8
20 20.8 104 0
Page 34 of 43
-------------------
-------------------SECTION V
Calibration and QC Information
Spiked Sample Results
MS-VOA.
SW8260B
Parameter
Methvlene chloride
Naphthalene
n-Proovlbenzene
Stvrene
I I 2 2-Tetrachloroethane
I. I I 2-Tetrachloroethane
Tetrach loroethene
Toluene
I 2 4-Trichlorobenzene
I 2,3-Trichlorobenzene
1.1 2-Trichloroethane
I.I I-Trichloroethane
Trichloroethene
Trichlorofluoromethane
I 2.3-Trich loroorooane
I 3 5-Trimethvlbenzene
I 2 4-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
o-Xvlene
o-Xvlene/m-Xvlene
p t aren contmue d
20002.01201."" r\ :~·· on f:i.i~~· ·~:.': :·1,:.:.:
'. ..
cone-: . .'Fla·
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Soiked Samole continued
Lab ID: 1002851 ... '
Oil F~e: 1
'File ID: A0204007.D
Sok.Cone· Cone %Rec Fla
20 18.3 92.
20 21.7 108
20 20.3 101
20 21.4 107
20 21.4 107
20 20.5 103
20 22.4 112
20 20.7 103
20 22.3 111
20 23.9 120
20 20.7 104
20 21.9 110
20 20.8 104
20 28.2 -· 141
20 21.8 109
20 20.1 101
20 20.1 101
20 19.8 99
20 20.8 104
20 21.1 105
40 41.9 105
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -02/16/2000 22:10
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Procto~ Silex
STLAustin
Soiked Samole Duolicate continued
Lab ID: 1002852
Oil Fae: 1 . QC Limits
File ID: A0204008.D
Sok Cone Cone %Rec Fla RPO Fla. %Rec RPO
20 20.l IOI 9.3
20 24.l 120 11
20 20.9 105 3.9
20 21.8 109 1.9
20 21.6 108 0.9
20 21.7 108 4.7
20 22.7 114 1.8
20 21.l 106 2.9 70-132 17
20 23.6 118 6.1
20 27.5 138 14
20 21.5 107 2.8
20 23.0 115 4.4
20 21.5 107 2.8 71-129 17
20 28.7 143 1.4
20 21.7 109 0
20 21.0 105 3.9
20 21.1 105 3.9
20 20.0 100 I
20 22.0 110 5.6
20 21.4 107 1.9
40 43.9 110 4.7
Page 35 of 43
SECTION V
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Lab ID: 1002851 -' Surroaate Comoounds %Recoverv
J-Bromo-4-fluorobenzene 103
I 2-Dichloroethane-d4 102
Toluene-d8 99
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -02/16/2000 22:10
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
Lab ID: 1002852
Flaas %Recoveiv Fla as QC Recoveiv Limits
105 77-117
105 61-143
100 87-113
Page 36 of 43
- ------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Client Sample ID:
Prep Batch ID:
Analysis Batch lD:
LCS for HBN 1462 [MSV/1053]
1462
1462
.. .. '
Instrument ID:
Column:
Units:
Matrix:
C IS ontro
Lab ID: 1002848
File ID: A0204003.D
Parameter Sok Amt Cone
Acetone 20
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone (MEK) 20
n-Butvlbenzene 20
sec-Butv !benzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
Ch lorobenzene 20
Chloroethane 20
Chloroform 20
Chloromethane 20
2-Chlorotoluene 20
4-Chlorotoluene 20
l ,2-Dibromo-3-chloroorooane 20
Dibromochloromethane 20
1,2-Dibromoethane 20
Dibromomethane 20
SECTION V -Calibration and QC Information -02116/2000 22: I 0
LIMS Workordcr: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
19.6
19.3
21.1
21.5
20.0
19.7
20.2
20.0
19.6
18.8
19.9
17.1
21.5
20.5
18.0
20.8
15.2
19.6
19.3
22.3
20.4
23.0
23.0
MSDA
ug/L
Aqueous
amp e
%Rec Fla
98
96
106
108
100
98
IOI
100
98
94
100
85
107
103
90
104
76
98
97
112
102
115
115
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Reported As:
% Moisture:
Analyst:
RECEIVED
NA
MER
Control Sample Duplicate
1002849
A0204004.D
Cone %Rec Fla RPO Fla
18.7 93 5.2
19.5 98 2.1
21.3 107 0.9
22.3 111 2.7
21.8 109 8.6
22.I 111 12
20.7 104 2.9
23.9 120 18
20.3 IOI 3
19.5 98 4.2
20.3 IOI I
18.9 94 10
22.l 110 2.8
21.4 107 3.8
18.8 94 4.3
21.4 1107 2.8
15.7 79 3.9
20.3 102 4
20.3 101 4
24.1 121 7.7
23.0 115 12
23.4 117 1.7
23.3 116 0.9
QC Limits
%Rec RPO
0.1-240 71
71-133 17
67-127 12
61-145 21
57-135 19
23-151 17
34-128 25
0.1-214 39
28-184 30
45-160 31
65-148 27
29-223 23
46-150 23
77-129 14
39-133 27
64-146 16
18-140 26
70-136 24
74-132 23
39-171 25
45-137 15
19-187 19
52-138 21
Page 37 of 43
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Parameter
I 3-Dichlorobenzene
I 2-Dichlorobenzene
I 4-Dichlorobenzene
Dichlorodifluoromethane
I 2-Dichloroethane
I 1-Dichloroethane
cis-1.2-Dichloroethene
1.1-Dichloroethene
trans-I 2-Dichloroethene
1 3-Dichloroorooane
2 2-Dichloropropane
1 2-Dichloroorooane
cis-I .3-Dichloropropene
trans-I ,3-Dichloroorooene
1, 1-Dichloropropene
Ethvlbenzene
Hexachloro-1 3-butadiene
2-Hexanone
Iodomethane
lsooroov I benzene
4-lsooroovlto luene
4-Methvl-2-oentanone (MIBK)
Methvlene chloride
Naphthalene
n-Proovlbenzene
Styrene
1 1.2 2-Tetrachloroethane
1 1, 1 2-Tetrachloroethane
Tetrachloroethene
Toluene
I 2.4-Trichlorobenzene
SECTION V -Calibration and QC Information -02/16/2000 22:10
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
LIMS Workorder: Little Washington, NC (20002012] Hamilton Beach-Proctor Silex
STLAustin
C IS ontro amol e continued
1002848
A0204003.D
Cone %Rec Fin
20.2 IOI
20.7 104
20.3 101
15.4 77
20.7 104
19.3 97
19.7 98
19. l 96
20.0 100
21.8 109
23.4 117
19.2 96
20.9 104
22.l 110
21.5 107
20.4 102
18. l 90
23.7 118
20.l 101
20.4 102
19.6 98
23.5 117
18.3 91
24.6 123
18.9 95
21.2 106
23.3 116
22.0 110
22.5 112
20.2 101
24.5 122
Control Samole Duolicate continued
Lab ID: 1002849
File ID: A0204004.D QC Limits
Sok Amt Cone %Rec Fig RPO Fla %Rec RPO
20 20.6 103 2 68-134 14
20 21.1 105 I 67-135 14
20 20.8 104 2.9 70-132 13
20 15.8 79 2.6 0.1-166 26
20 21.1 105 1 48-152 23
20 20.1 100 3 66-138 19
20 20.2 101 3 66-144 18
20 20.I 101 5.1 47-175 25
20 21.0 105 4.9 62-146 22
20 22.5 113 3.6 70-128 16
20 23.5 118 0.9 40-168 30
20 19.7 99 3.1 61-133 17
20 20.9 105 1 36-142 16
20 22.6 113 2.7 34-138 21
20 22.0 110 2.8 71-155 31
20 20.7 104 1.9 75-131 14
20 19.0 95 5.4 46-150 34.
20 24.0 120 l.7 22-164 34
20 20.8 104 2.9
20 21.4 107 4.8 54-152 26
20 20.2 101 3 41-165 28
20 22.7 114 2.6 27-149 36
20 19.2 96 5.3 36-166 23
20 25.3 n1 3.2 32-172 22
20 19.7 98 3.1 61-143 28
20 22.1 110 3.7 68-136 14
20 23.6 118 1.7 47-143 20
20 22.8 114 3.6 63-141 20
20 23.1 116 3.5 69-137 16
20 20.6 103 2 70-132 17
20 24.9 124 1.6 66-144 22
Page 38 of 43
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
I 2 3-Trichlorobenzene
l I 2-Trichloroethane
l 1 I-Trichloroethane
Trichloroethene
Trichlorofluoromethane
I 2 3-Trichloroorooane
I 3 5-Trimethvlbenzene
1.2 4-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
o-Xvlene
o-X vlene/m-X vlene
:
SECTION V -Calibration and QC Information -02/16/2000 22:10
Lab ID:
File ID:
s·o-kAmt
20
20
20
20
20
20
20
20
20
20
20
40
LIMS Workorder: Little Washington, NC (20002012) Hamilton Beach-Proctor Silex
STLAustin
C t IS on ro t• d amo. e con mue
1ooza4a Lab ID:
A0204003.D File ID:
Coric %Rec Fla Sok Amt
28.I 140 20
20.8 104 20
21.1 I06 20
21.3 106 20
24.0 120 20
23.l 116 20
19.2 96 20
20.0 100 20
17.9 89 20
18.5 92 20
20.2 101 20
40.6 IOI 40
c ontro IS amp,e up1 tea econ mue I D r t t" d
1002849
A0204004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
29.7 148 0 5.6 66-140 20
21.4 107 2.8 67-135 I7
21.8 109 2.8 49-155 24
21.7 109 2.8 71-129 17
26.6 133 JO 39-147 29
23.0 115 0.9 64-140 18
20.0 100 4.1 62-144 25
20.3 102 2 54-156 25
18.3 92 3.3 . 0.1-I64 31 ..
19.0 95 3.2 24-138 27
21.4 107 5.8 77-131 15
42.6 106 4.8 76-I34 15
Page 39 of 43
SECTION V
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Lab ID: 1002848
Surroaate Comoounds %Recoverv
I-Bromo-4-fluorobenzene 104
I ,2-Dichloroethane-d4 106
Toluene-d8 99
SECTION V -Calibration and QC Information -02/J 6/2000 22: I 0
LJMS Workorder: Lillie Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
Lab ID: 1002849
Flaas %Recoverv Flaas QC Recoverv Limits
105 77-117
108 61-143
98 87-113
Page 40 of 43 ------------------ -
-------------------SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 1462
Client Samole ID Lab Samole ID ·
INSTRUMENT QC 1000
INSTRUMENT QC 1406
LCS for HBN 1462 rMSV/10531 1002848
LCSD for HBN 1462 rMSV/10531 1002849
MB for HBN 1462 rMSV/10531 1002850
0200HBWW226 2000201201
0200HBWW226 1002851
0200HBWW226 1002852
0200HBWW224 2000201202
0200HBWW225 2000201203
0200HBWW234 2000201204
0200HBWD998 2000201205
0200HBWW222 2000201206
0200HBWW230 2000201207
0200HBWW220 2000201208
0200HBWW216 2000201209
TRIP BLANK 2000201210 zzzzzzzzzz 2000202502 zzzzzzzzzz 2000202503
zzzzzzzzzz 2000202507
zzzzzzzzzz 2000202501
zzzzzzzzzz 2000202504
zzzzzzzzzz 2000202505
zzzzzzzzzz 2000202506
SECTION.YI -Batch Summaries -02/16/2000 22:10
Start Dateffime: 02/04/2000 16:04
Stop Dateffime: 02/05/2000 02:25
SamoleTvoe Matrix
GC/MS Tune Aqueous
Continuing Calibration Check Aaueous
Lab Control Sample Aqueous
Lab Control Samole Duolicate Aqueous
Method Blank Aqueous
Field Samole Aaueous
Matrix Spike Aqueous
Matrix Soike Duolicate Aaueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aaueous
LJMS Workorder: Lillie Washington, NC [20002012] Hamilton Beach-Proctor Silex
STL Austin
Analyst: JEC
Sample Size
Initial Final Preoaration Method
15 mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
Page 41 of 43
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 1462 Instrument ID: MSDA
Sequence Client Sample ID Lab Sample ID
I INSTRUMENT OC 1000
2 INSTRUMENT QC 1406
3 LCS for HBN I462 rMSV/10531 1002848
4 LCSD for HBN 1462 fMSV/10531 1002849
5 MB for HBN 1462 fMSV/10531 1002850
6 0200HBWW226 2000201201
7 0200HBWW226 1002851
8 0200HBWW226 1002852
9 0200HBWW224 2000201202
10 0200HBWW225 2000201203
11 0200HBWW234 2000201204
12 0200HBWD998 2000201205
13 0200HBWW222 2000201206
14 0200HBWW230 2000201207
15 0200HBWW220 2000201208
16 0200HBWW2 l 6 2000201209
17 TRIP BLANK 2000201210
18 zzzzzzzzzz 2000202502
19 zzzzzzzzzz 2000202503
20 zzzzzzzzzz 2000202507
21 zzzzzzzzzz 2000202501
22 zzzzzzzzzz 2000202504
23 zzzzzzzzzz 2000202505
24 zzzzzzzzzz 2000202506
SECTION VI -Batch Summaries -02/16/2000 22:10
LIMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
Analysis
Date Time
02/04/2000 16:04:00
02/04/2000 16:04:00
02/04/2000 16:32:00
02/04/2000 17:00:00
02/04/2000 17:28:00
02/04/2000 17:56:00
02/04/2000 18:24:00
02/04/2000 18:52:00
02/04/2000 19:20:00
02/04/2000 19:48:00
02/04/2000 20:16:00
02/04/2000 20:44:00
02/04/2000 21:12:00
02/04/2000 21:40:00
02/04/2000 22:07:00
02/04/2000 22:35:00
02/04/2000 23:03:00
02/04/2000 23:31:00
02/04/2000 23:59:00
02/05/2000 00:27:00
02/05/2000 00:57:00
02/05/2000 01:27:00
02/05/2000 01:57:00
02/05/2000 02:25:00
Analyst: JEC
SamoleType Analvsis File ID Sub-Batch ID
GC/MS Tune A0204002.D 0
Continuing Calibration Check A0204002.D 0
Lab Control Sample A0204003.D 0
Lab Control Samole Duolicate A0204004.D 0
Method Blank A0204005.D 0
Field Samole A0204006.D 0
Matrix Spike A0204007.D 0
Matrix Soike Duolicate A0204008.D 0
Field Sample A0204009.D 0
Field Samole A0204010.D 0
Field Sample A0204011.D 0
Field Samole A0204012.D 0
Field Sample A0204013.D 0
Field Samole A0204014.D 0
Field Sample A0204015.D 0
Field Samole A0204016.D 0
Field Sample A0204017.D 0
Field Sample A0204018.D 0
Field Samole A0204019.D 0
Field Sample A0204020.D 0
Field Samole A0204021.D 0
Field Sample A0204022.D 0
Field Samole A0204023.D 0
Field Sample A0204024.D 0
Page 42 of 43 ------------·-------
- -
SECTION VII
Certifications
State/Aoencv
----
Arkansas Department of Pollution Control and Ecolo!!v
-- --
California Environmental Laboratory Accreditation Program I Waste Water/Hazardous Waste
Kansas Department of Health and Environment I Solid and Hazardous Waste/Drinkin11: Water
-
Louisiana Department of Environmental Oualitv. ELAP I Waste Water/Hazardous Waste/Air/Emissions
New Jersey Department of Environmental Protection
New York State Deoartment of Health I Waste Water/Hazardous Waste
North Carolina Dept. of Natural Resources & Communitv Develonment I Waste Water
Oklahoma Water Resources Board I Waste Water
South Carolina Dept. of Health & Environmental Control
Utah Deoartment of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources
US Air Force/AFCEE
US Armv Corps of Engineers (ACE)
US Department of A!!riculture I Restricted Soils Permit
SECTION VII -Certifications -02/16/2000 22: I 0
UMS Workorder: Little Washington, NC [20002012] Hamilton Beach-Proctor Silex
STLAustin
-- ---- --
ID #
2257
E-10165
82005
10915
302
8720
82003002
RADC
999885260
Participating Laboratorv
S-42350
Page 43 of 43
Quality Control Exception Report
QCER #: 388 Analysis Date:
Status: Complete Spec:
Queue: MSV Instrument:
Analyst: MER Matrix:
HBN:
Work Order HSN Client
20002012 HB-PS
20002025 HB-PS
Analytical Problem Identification
LCS/LCSD Recovery
Analytical Probable Cause
Instrument
Analytical Corrective Action Taken
QCER written
Comments:
2/4/2000
07
MSDA
w
1053
csc
JAL
JAL
~ .,. :L 79~· Comni Ut>1:d. to 1•e1111tr succeu
File ID(s):
A02040-03/04
Recoveries of 1,2,3-Trichlorobenzene are above acceptance criteria in the LCS/D at 140% and 148%. This C0'11pound was not detected
in any of the samples in this batch.
February 07, 2000 QCER #: 388 Page 1of1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I