IDX GW Monitoring RPt Aug 2001 (SF)-OCR

*5991HSSF1066*
1111111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
DocumentType Progress/Monitoring Rpt (PRGMON)
RptSegment 1
DocDate
DocRcvd
Box
Accesslevel
Division
Section
Program
DocCat
9/28/2001
2/20/2007
SF1066
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
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TABLE OF CONTENTS
Certification Page ................................................................................................................ ii
List of Figures .................................................................................................................... iv
List of Tables ................................................................................................................... vii
1.0 INTRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS .......................................................................................................... 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3.1
3.2
APPENDIX A
APPENDIXB
Water Level Measurements ................................................................................. 3-1
Analytical Results ................................................................................................ 3-1
t
GROUNDWATER SAMPLING ANALYTICAL REPORTS
CONTAMINANT CONCENTRATIONS VERSUS TIME
80396910.01 Aug2001GW_Rpt.doc (9/27/01) 111
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LIST OF FIGURES
1-1 Topographic Map, Hamilton Beach<> Proctor-Silex, Inc.
2-1 Site Map, Washington Facility, Hamilton Beach<> Proctor-Silex, Inc.
3-1 Generalized Groundwater Flow Direction for Hydro geologic Unit A,
Washington Facility
3-2 Generalized Groundwater Flow Direction for Hydrogeologic Unit B,
Washington Facility
3-3 Approximate Distribution ofTCE in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
3-4 Approximate Distribution ofTCE in Unit~.
Hamilton Beach<>Proctor-Silex, Inc.
(U) Approximate Distribution of Trichloroethene, D-D',
Hamilton Beach<> Proctor-Silex, Inc.
~ Approximate Distribution ofTrichloroethene, E-E',
Hamilton Beach<> Proctor-Silex, Inc.
3-7 Approximate Distribution of cis-1,2-Dichloroethene in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
3-8 Approximate Distribution of cis-1,2-Dichloroethene in Unit B,
Hamilton Beach<> Proctor-Silex, Inc.
~ Approximate Distribution of cis-1,2-Dichloroethene, D-D',
Hamilton Beach<> Proctor-Silex, Inc.
~ Approximate Distribution of cis-1,2-Dichloroethene, E-E',
Hamilton Beach<> Proctor-Silex, Inc.
3-11
3-12
Approximate Distribution of 1,1-Dichloroethene in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
Approximate Distribution of 1, 1-Dichloroethene in Unit B,
Hamilton Beach<> Proctor-Silex, Inc.
Approximate Distribution of 1, 1-Dichloroethene, D-D',
Hamilton Beach<> Proctor-Silex, Inc.
Approximate Distribution of 1, 1-Dichloroethene, E-E',
Hamilton Beach<> Proctor-Silex, Inc.
80396910.01 Aug2001GW_Rpt.doc (9/27/01) iv
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LIST OF FIGURES (Continued)
3-15 Approximate Distribution of Vinyl Chloride in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
3-16 Approximate Distribution of Vinyl Chloride in Unit B,
Hamilton Beach<> Proctor-Silex, Inc.
® Approximate Distribution of Vinyl Chloride, D-D',
Hamilton Beach<> Proctor-Silex, Inc.
@ Approximate Distribution of Vinyl Chloride, E-E',
Hamilton Beach<> Proctor-Silex, Inc .
3-19 Approximate Distribution of 1,1,1-Trichloroethane in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
3-20 Approximate Di$tribution of 1, 1, 1-Trichloroethane in Unit B,
Hamilton Beach<> Proctor-Silex, Inc.
~ Approximate Distribution of 1,1,1-Trichloroethane, D-D', ---....... Hamilton Beach<> Proctor-Silex, Inc.
Q~ Approximate Distribution of 1, 1, 1-Trichloroethane, E-E',
Hamilton Beach<> Proctor-Silex, Inc.
3-23 Approximate Distribution of 1,2-Dichloroethane in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
3-24 Approximate Distribution of 1,2-Dichloroethane in Unit B,
Hamilton Beach<>Proctor-Silex, Inc.
I. @ Approximate Distribution of 1,2-Dichloroethane, D-D',
Hamilton Beach<>Proctor-Silex, Inc.
I Q:~) Approximate Distribution of 1,2-Dichloroethane, E-E',
Hamilton Beach<> Proctor-Silex, Inc.
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3-27 Approximate Distribution of 1,1-Dichloroethane in Unit A,
Hamilton Beach<> Proctor-Silex, Inc.
3-28 Approximate Distribution of 1,1-Dichloroethane in Unit B,
Hamilton Beach<> Proctor-Silex, Inc.
Approximate Distribution of 1,1-Dichloroethane, D-D',
Hamilton Beach<>Proctor-Silex, Inc.
80396910.01 Aug2001GW _Rpt.doc (9/27/01) v
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LIST OF FIGURES (Continued)
~ Approximate Distribution of 1, 1-Dichloroethane, E-E',
Hamilton BeachOProctor-Silex, Inc. ·
3-31 Approximate Distribution of Toluene in Unit A,
Hamilton BeachOProctor-Silex, Inc.
@ Cross-section Locations, Hamilton BeachOProctor-Silex, Inc.
3-33 Location of Surrounding Water Supply Wells,
Hamilton BeachOProctor-Silex, Inc.
80396910.01 Aug2001GW_Rptdoc (9/27/01) Vl
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LIST OF TABLES
2-1 Monitoring Well Construction Data for Sampled Wells
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
, /_ 1"1-u. '{i!Clfl-(_ -fu~ Water Level Measurements and Elevations, August 14, 2001 c:::-c Yool?-+
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina ')<-!
3-1
@~ Historical Water Level Elevations at MW-213
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
@ Historical Water Level Elevations at MW-214
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
@j:) Historical Water Level Elevations at MW-215
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-216
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-220
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
@ Historical Water Level Elevations at MW-224
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
@' Historical Water Level Elevations at MW-225
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
W:> Historical Water Level Elevations at MW-226
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
(~ Historical Water Level Elevations at MW-227
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
@ Historical Water Level Elevations at MW-228
Hamilton Beach</Proctor-Silex, Inc., Washington, North Carolina
~ /3-13} Historical Water Level Elevations at MW-230
\--,-/ Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
80396910.01 Aug2001GW_Rpt.doc (9/27/01) vii
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LIST OFT ABLES (Continued)
@Historical Water Level Elevations at MW-234
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-15 Field Measurements, August 2001
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-16 Summary of Qualified Groundwater Analytical Results: August 2001
Volatile Organic Compounds by Method 8260B
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
@ Historical Analytical Results for MW-213
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
~Historical Analytical Results for MW-214
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
@:::>Historical Analytical Results for MW-215
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
@ Historical Analytical Results for MW-216
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
~p Historical Analytical Results for MW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
~ Historical Analytical Results for MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
L:-~~ Historical Analytical Results for MW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
dW Historical Analytical Results for MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
~2$) Historical Analytical Results for MW-226
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
~Historical Analytical Results for MW-227
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
,,.---~
/ {_~Historical Analytical Results for MW-228 ·
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
80396910.01 Aug2001GW _Rpt.doc (9/27/01) viii
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LIST OF TABLES (Continued)
~ Historical Analytical Results for MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
----@ Historical Analytical Results for MW-234
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
80396910.01 Aug2001GW_Rpt.doc (9/27/01) ix
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1.0 INTRODUCTION
The Hamilton BeachOProctor-Silex (HBO PS) facility is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HBO PS since 1990 and previously leased by predecessor companies. The facility was
formerly involved in the final assembly, packaging, and warehousing of small electrical
household appliances.
Since 1992, when organic compounds were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
assessment (CSA). The results of the CSA indicated that a plume of organic compounds is
present in groundwater underlying the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer used at the facility.
A plan for corrective action at the site has been proposed. Until corrective action
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to
a monitoring program requested and approved by the North Carolina Department of
Environment and Natural Resources, Groundwater Section. Quarterly groundwater monitoring
is to be conducted in February, May, August, and November at seven wells: MW-220, -222,
-224, -225, -226, -230, and -234. These wells are located outside of the contaminant plume. In
February and August, the following six additional wells will be sampled: MW-213, -214, -215,
-216, -227, and -228. These wells are located within the contaminant plume. The purpose of the
monitoring program is to detect potential migration of the plume.
URS -Radian (URS) conducted groundwater sampling at the facility in August
2001. The sampling event included the measurement of water levels, temperature, pH, and
specific conductance; and the collection and analysis of samples from thirteen monitoring wells.
This report describes the sampling methods and presents the results for the quarterly sampling
event.
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2.0 FIELD METHODS
Groundwater was sampled on August 14 and 15, 2001 in general accordance with
the methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for this
site.
Thirteen monitoring wells were sampled. They included MW-213 through
MW-216, MW-220, MW-222, MW-224 through MW-228, MW-230, and MW-234. The
locations of the monitoring wells are shown in Figure 2-1. Details of well construction are
provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using inertial foot-valve pumps, with the
exception of wells MW-213, MW-215, and MW-228, which were purged with disposable
hailers. Temperature, pH, and specific conductance were measured and the data were recorded
in a field notebook. Purging continued until temperature, pH, and specific conductance
stabilized; a minimum of three well volumes was extracted; or the well was pumped dry. Each
of the wells was then sampled immediately following well purging using the inertial foot-valve
pump or bailer. For QA/QC purposes, duplicate samples were collected at wells MW-214 and -
226; and, a trip blank accompanied each sample shipment.
The groundwater samples were sent by overnight courier to STL in Austin, Texas,
for analysis of volatile organic compounds by EPA Method 8260B.
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3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the thirteen wells sampled and seven additional wells. Maps showing the
generalized direction of groundwater flow in hydrogeologic units A and B are included as
Figures 3-1 and 3-2, respectively. Historical water-level elevations in sampled wells are
included in Tables 3-2 to 3-14.
3.2 Analytical Results
Field measurements of water temperature, pH, and specific conductance are
summarized in Table 3-15. Qualified analytical results are summarized in Table 3-16. The
approximate extent of selected compounds that have been detected at concentrations exceeding
groundwater standards are illustrated in Figures 3-3 through 3-31. Cross-section locations are
shown in Figure 3-32. Both current and historical data were used to approximate the extent of
contaminants. Qualified data sheets and laboratory reports are included in Appendix A.
No analytes were detected above the groundwater standards in samples from
wells located near the perimeter of the site (MW-220, MW-222, MW-224, MW-225, MW-230,
and MW-234), nor were any analytes detected above the groundwater standards in the sample
from well MW-226, which is completed in the confined Limestone Aquifer. Also, no analytes
were detected above groundwater standards in samples collected from wells MW-215 and
MW-216 which are located 120 feet and 350 feet from the source area, respectively.
Concentrations of chemicals exceeding the standards were detected in samples from wells
MW-213, MW-214, MW-227, and MW-228. These four wells are located at, or within 150 feet
of, the source area.
Historical analytical results for the sampled wells are presented in Tables 3-17 to
3-29, and in graphs included as Appendix B. A comparison of the record for wells located near
80396910.01 Aug2001GW_Rpt.doc (9/27/01) 3-1
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the perimeter of the site suggests that the plume remains on-site, at least 200 feet from potential
receptors located north of Spring Road (Figure 3-33). The latest results for wells located at the
source area and other interior portions of the site are consistent with earlier results and indicate
no significant changes in chemical concentration and distribution have occurred.
80396910.0 I Aug200 I GW _ Rpt.doc (9/27 /0 I) 3-2
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FIGURES
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-~-------~--~---~--
Table 2-1
Monitoring Well Construction Data for Sampled Wells
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Top of Casing
Installation Elevation Total Depth Screen Interval Filter Pack Bentonite Seal
Well No. Date (ft. above MSL) (ft. bf!S) (ft. bf!S)
MW-213 1114/98 28.44 7.5 3 -7.5
MW-214 1116/98 27.93 21 14.5 -21
MW-215 1116/98 28.06 10 8.5 -10
MW-216 5/5/98 32.82 35 26-35
MW-220 5/5/98 31.50 34 25 -34
MW-222 5/6/98 35.11 40 31 -40
MW-224 11/13/98 33.43 34 25 -34
MW-225 11/13/98 33.43 10 4-10
MW-226 9/30/98 28.46 75 70 -75
MW-227 10/1/98 28.47 25.5 20.5 -25.5
MW-228 9/23/98 28.71 10 3 -10
MW-230 10/26/98 33.47 14 8 -14
MW-234 6/23/99 35.03 26 17 -26
Monitoring wells 213 through 215 installed by Groundwater Management Associates, Inc.
Monitoring wells 216, 220, and 222 installed by Radian Mobile Field Services.
Monitoring wells 226 through 228 installed by Parratt Wolff, Inc.
Monitoring wells 224, 225, 230, and 234 installed by Probe Technology, Inc.
80396910.0 I Aug2001 GW _ Rpt.doc (9/27 /0 I)
(ft. bf!S) (ft. b!!S)
2.5 -7.5 1.5 -2.5
13.5 -21 12.5 -13.5
8 -10 7-8
25 -35 24-25
24-34 23 -24
30-40 29-30
24-34 23 -24
3 -10 2-3
69 -75 67 -69
19.5 -25.5 17.5 -19.5
2 -10 1-2
7 -14 5-7
16-26 13 -16
Grout Seal
(ft. b!!s)
0-1.5
0 -12.5
0-7
0-24
0 0 23
0-29
0-23
0-2
0-67
0 -17.5
0-1
0-5
0-13
Well
MW-201S
MW-213
MW-214
MW-215
MW-216
MW-217
MW-220
MW-221
MW-222
MW-223
MW-224
MW-225
MW-226
MW-227
MW-228
MW-230
MW-233
MW-234
msl = mean sea level
Table 3-1
Water Level Measurements and Elevations
August 14, 2001
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Measuring Point
Elevation Depth to Water
(ft above msl)) (ft)
29.74 2.20
28.44 3.91
27.93 4.89
28.06 8.49
32.82 9.40
32.75 7.47
31.50 9.70
31.39 8.92
35.11 14.22
35.15 4.81
33.43 9.42
33.43 8.86
28.46 19.75
28.47 5.23
28.71 4.08
33.47 11.27
34.55 11.55
35.03 11.09
80396910.0 I Aug200 I GW _Rpt.doc (9/27 /01)
Water Level
Elevation
(ft above msl)
27.54
24.53
23.04
19.57
23.42
25.28
21.80
22.47
20.89
30.34
24.01
24.57
8.71
23.24
24.63
22.20
23.00
23.94
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Table 3-3
Historical Water Level Elevations at MW-214
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 24.95
November 16, 1998 22.18
February 2, 2000 25.38
May2, 2000 25.30
September 6, 2000 24.13
November 28, 2000 22.61
February 19, 2001 23.71
Mav 16, 2001 23.01
August 14, 2001 23.04
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
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Table 3-5
Historical Water Level Elevations at MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 24.39
November 16, 1998 22.37
February 2, 2000 24.84
Mav2, 2000 24.83
September 6, 2000 24.12
November 28, 2000 22.81
February 19, 2001 23.61
May 16, 2001 23.20
August 14, 2001 23.42
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
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Table 3-6
Historical Water Level Elevations at MW-220
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 25.13
November 16, 1998 20.55
July 1, 1999 21.50
October 20, 1999 25.63
February 2, 2000 25.85
Mav 2, 2000 25.81
September 6, 2000 22.90
November 28, 2000 21.71
February 19, 2001 23.45
May 16, 2001 21.95
August 14, 2001 21.80
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
Table 3-7
Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 22.34
November 16, 1998 19.99
July 1, 1999 20.61
October 20, 1999 24.22
February 2, 2000 23.34
May2, 2000 23.58
September 6, 2000 21.50
November 28, 2000 20.52
February 19, 2001 21.34
May 16, 2001 20.91
August 14, 2001 20.89
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
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Table 3-8
Historical Water Level Elevations at MW-224
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 23.64
July 1, 1999 24.39
October 20, 1999 26.88
February 2, 2000 26.73
May 2, 2000 26.48
September 6, 2000 25.99
November 28, 2000 24.36
February 19, 2001 25.23
May 16, 2001 24.23
Aul!Ust 14, 2001 24.01
msl = mean sea level
80396910.01 Aug2001GW _Rpt.doc (9/27/01)
Table 3-9
Historical Water Level Elevations at MW-225
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 24.36
July 1, 1999 24.50
October 20, 1999 27.24
February 2, 2000 26.59
Mav2, 2000 26.40
September 6, 2000 27.22
November 28, 2000 24.38
February 19, 2001 25.01
May 16, 2001 24.21
Aul!llst 14, 2001 24.57
msl = mean sea level
80396910.01 Aug2001GW _Rpt.doc (9/27/01)
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Table 3-10
Historical Water Level Elevations at MW-226
Hamilton BeachO Proctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 8.43
Julv l, 1999 8.54
October 20, 1999 11.11
Februarv 2, 2000 10.23
May2, 2000 10.81
September 6, 2000 9.41
November 28, 2000 9.19
Februarv 19, 2001 9.20
Mav 16, 2001 9.31
August 14, 2001 8.71
msl =mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
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Table 3-12
Historical Water Level Elevations at MW-228
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 23.01
February 2, 2000 24.63
May2, 2000 26.36
September 6, 2000 25.44
November 28, 2000 23.74
February 19, 2001 24.51
May 16, 2001 24.24
August 14, 2001 24.63
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
Table 3-13
Historical Water Level Elevations at MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 21.14
July 1, 1999 21.80
October 20, 1999 27.71
February 2, 2000 27.44
Mav2, 2000 26.53
September 6, 2000 23.07
November 28, 2000 21.87
February 19, 2001 23.17
Mav 16, 2001 22.17
August 14, 2001 22.20
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-14
Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
July 1, 1999 23.24
October 20, 1999 25.71
February 2, 2000 25.67
Mav2, 2000 25.56
September 6, 2000 25.04
November 28, 2000 23.23
February 19, 2001 24.20
Mav 16, 2001 23.53
August 14, 2001 23.94
msl = mean sea level
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
Well Date Time
MW-213 8/15/01 09:31
MW-214 8/15/01 09:00
MW-215 8/15/01 09:02
MW-216 8/14/01 15:09
MW-220 8/14/01 13:21
MW-222 8/14/01 14:40
MW-224 8114/01 13:47
MW-225 8/14/01 13:45
12:47
MW-226 8/14/01 12:52
12:55
13:00
MW-227 8/15/01 09:50
MW-228 8/15/01 10:00
MW-230 8/14/01 11:25
MW-234 8/14/01 14:20
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
Table 3-15
Field Measurements
August2001
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Volume Purged
(Gal) Pur2in2 Criteria
1.7 3 well volumes
8.0 3 well volumes
1.0 3 well volumes
0.8 3 well volumes
0.75 3 well volumes
0.8 3 well volumes
0.75 3 well volumes
0.03 drv
9.0
10.0 Stabilized parameters
12.0
13.0
10.0 3 well volumes
3.0 3 well volumes
0.1 3 well volumes
0.5 3 well volumes
Specific
Temperature Conductance
(oC) (µS) oH
28.0 335 4.7
22.0 250 5.9
24.5 170 5.4
17.0 450 7.6
18.0 110 6.0
19.0 370 7.0
20.0 345 7.2
26.5 230 4.8
20.0 465 7.2
20.0 450 7.4
20.0 460 7.4
20.0 465 7.4
20.0 550 6.7
25.0 2600 3.2
23.0 170 4.6
19.0 140 6.1
-------------------
-------------------
Sample ID
Date of Sampling
Analyte (µg/L)
Acetone
Benzene
2-Butanone (MEK)
n-Butylbenzene
Carbon Disulfide
Carbon Tetrachloride
Chloroethane
Chloroform
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Ethylbenzene
Isopropylbenzene
Methylene chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
1, 1, I-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
1,2,4-Trimethvlbenzene
80396910.0 l Aug200 l GW _Rpt.doc (9/27 /0 l)
Table 3-16
Summary of Qualified Groundwater Analytical Results: August 2001
Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Washington, North Carolina
MW-213 MW-214 MW-215 MW-216
8/15/01 8/15/01 8/15/01 8/14/01
ND (2.19) ND (0.876) ND (0.438) ND (0.438)
ND (0.320) 0.395 J 0.142 J ND (0.0641)
ND (1.00) ND (0.400) ND (0.200) ND (0.200)
ND (0.510) ND (0.204) ND (0.102) ND (0.102)
ND (0.342) ND (0.137) ND (0.0684) ND (0.0684) UJ
ND (0.326) ND (0.130) ND (0.0652} ND (0.0652)
ND (0.462) ND (0.185) UJ ND (0.0925) ND (0.0925)
ND (0.448) ND (0.179) ND (0.0896) ND (0.0896)
128 143 5.72 ND (0.124)
3.09 ND (0.204) UJ ND (0.102) ND (0.102)
405 16.7 3.48 ND (0.122)
37.4 11.7 0.0775 J ND (0.112)
1.30 J 0.578 J ND(0.119) ND (0.119)
ND (0.680) ND (0.272) ND (0.136) ND (0.136)
ND (0.466) ND (0.186) ND (0.0931) ND (0.0931)
ND (0.630) ND (0.252) U ND (l.05)U ND (0.126)
8.56 J ND (0.160) ND (0.0801) ND (0.0801)
ND (0.700) ND (0.280) ND (0.140) ND (0.140)
ND (0.488) ND (0.195) ND (0.0977) ND (0.0977)
23.9J ND (0.288) UJ ND (0.144) UJ ND (0.144)
ND (0.318) ND (0.127) 0.228 J ND (0.0637)
4.29 ND (0.338) 2.26 ND (0.169)
1.92J ND (0.164) ND (0.0821) ND (0.0821)
467 0.357 J 0.242 J ND (0.137)
ND (0.620) ND (0.248) ND (0.124) ND (0.124)
MW-220 MW-222
8/14/01 8/14/01
ND (0.438) ND (0.438)
ND (0.0641) ND (0.0641)
ND (0.200) ND (0.200)
ND (0.102) ND (0.102)
ND (0.0684) UJ ND (0.0684) UJ
ND (0.0652) ND (0.0652)
ND (0.0925) 'ND (0.0925)
ND (0.0896) . ND (0.0896)
0.530 ND (0.124)
ND (0.102) ND (0.102)
ND (0.122) ND (0.122)
ND (0.112) 0.157 J
ND (0.119) ND (0.119)
ND (0.136) ND (0.136)
ND (0.0931) ·ND (0.0931)
ND (0.126) .: ND (0.126)
ND (0.0801) ND (0.0801)
ND (0.140) ND (0.140)
ND (0.0977) ND (0.0977)
ND (0.144) ND (0.144)
ND (0.0637) ND (0.0637)
ND (0.169) ND (0.169)
ND (0.0821) ND (0.0821)
ND (0.137) ND (0.137)
ND (0.124) ND (0.124)
Sample ID MW-213
Date of Sampling 8/15/01
Analyte (µg/L)
1,3 ,5-Trimethylbenzene ND (0.452)
Vinyl chloride 17.4
m&p-Xylene ND (0.835)
o-Xvlene 0.715 J
Target analytes not listed were not detected.
Bold values exceed Standards.
ND ( ) =Not detected at specified detection limit.
J = Estimated value.
Table 3-16 (Continued)
MW-214 MW-215
8/15/01 8/15/01
ND (0.181) ND (0.0905)
11.6 ND (0.114)
ND (0.334) ND (0.167)
ND (0.169) ND (0.0844)
U =Not present above the associated level, blank contamination present.
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
MW-216 MW-220 MW-222
8/14/01 8/14/01 8/14/01
ND (0.0905) ND (0.0905) ND (0.0905)
ND (0.114) ND (0.114) ND (0.114)
ND (0.167) ND (0.167) ND (0.167)
ND (0.0844) ND (0.0844) ND (0.0844)
- - - - -·-- - - - - - - -·-- --· -
-------------------
Table 3-16 (Continued)
Sample ID MW-224 MW-225 MW-226 MW-227 MW-228 MW-230 MW-234
Date of Sampling 8/14/01 8/14/01 8/14/01 8/15/01 8/15/01 8/14/01 8/14/01
Analyte (µf!./L)
Acetone ND (0.438) ND (0.438) ND (0.438) 34.7 J 638 J ND (0.438) ND (0.438)
Benzene ND (0.0641) ND (0.0641) ND (0.0641) 0.978 J 43.9J ND (0.0641) ND (0.0641)
2-Butanone (MEK) ND (0.200) ND (0.200) ND (0.200) ND (24.0) UJ 548J ND (0.200) ND (0.200)
n-Butylbenzene ND (0.102) ND (0.102) ND (0.102) ND (0.334) UJ 23.9J ND (0.102) ND (0.102)
Carbon Disulfide 0.515 J ND (0.0684) UJ ND (0.0684) UJ ND (0.341) UJ ND (3.41) UJ ND (0.0684) UJ ND (0.0684) UJ
Carbon Tetrachloride ND (0.0652) ND(0.0652) ND (0.0652) ND (0.508) UJ 27.6J ND (0.0652) ND (0.0652)
Chloroethane ND (0.0925) ND (0.0925) ND (0.0925) 63.4 J 119 J ND (0.0925) ND "(0.0925)
Chloroform ND (0.0896) ND (0.0896) ND (0.0896) 1.83 J 9.82 J ND (0.0896) ND (0.0896)
1; 1-Dichloroethane ND (0.124) ND (0.124) ND (0.124) 3,410 12,600 ND (0.124) ND (0.124)
1,2-Dichloroethane ND (0.102) ND (0.102) ND (0.102) 25.2 J 91.3 J ND (0.102) ND (0.102)
1, 1-Dichloroethene ND (0.122) ND (0.122) ND (0.122) 855 35,100 ND (0.122) ND (0.122)
cis-1,2-Dichloroethene ND (0.112) ND (0.112) ND (0.112) 456J 1,650 J 0.119 J ND (0.112)
trans-1,2-Dichloroethene ND (0.119) ND (0.119) ND (0.119) 8.97 J 13.1 J ND (0.119) ND (0.119)
Ethylbenzene ND (0.136) ND (0.136) ND (0.136) 0.784 J 561 J ND (0.136) ND (0.136)
Isopropylbenzene ND (0.0931) ND (0.0931) ND (0.0931) ND (0.167) UJ 40.l J ND (0.0931) ND (0.0931)
Methylene chloride ND (0.126) ND (0.126) ND (0.126) 2.68 J 13.4J ND (0.126) ND (0.126)
Naphthalene ND (0.0801) ND (0.0801) ND (0.0801) 6.88 J 662 J ND (0.0801) ND (0.0801)
n-Propylbenzene ND (0.140) ND (0.140) ND (0.140) ND (0.400) UJ 229 J ND (0.140) ND (0.140)
Styrene ND (0.0977) ND (0.0977) ND (0.0977) ND (0.181) UJ 12.9 J ND (0.0977) ND (0.0977)
Tetrachloroethene ND (0.144) ND (0.144) ND (0.144) ND (1.14) UJ 19.6J ND (0.144) ND (0.144)
Toluene ND (0.0637) ND (0.0637) ND (0.0637) 26.2J 1,390 J ND (0.0637) ND (0.0637)
1, 1, I -Trichloroethane ND (0.169) ND (0.169) ND (0.169) 4,480 76,100 ND (0.169) ND (0.169)
1, 1,2-Tric:;hloroethane ND (0.0821) ND (0.0821) ND (0.0821) 3.62J 28.0J ND (0.0821) ND (0.0821)
Trichloroethene ND (0.137) ND (0.137) ND (0.137) 105J 8,300 0.140 J ND (0.137)
1,2,4-Trimethylbenzene ND (0.124) ND (0.124) ND (0.124) ND (0.198) UJ 1,370 J ND (0.124) ND (0.124)
1,3,5-Trimethylbenzene ND (0.0905) ND (0.0905) ND(0.0905) ND (0.385) UJ 340J ND (0.0905) ND (0.0905)
Vinyl chloride ND (0.114) ND(0.114) ND (0.114) 9.02J 174 J ND (0.114) ND (0.114)
m&p-Xylene ND (0.167) ND (0.167) ND (0.167) 2.12 J 1,640 J ND (0.167) ND (0.167)
o-Xvlene ND (0.0844) ND (0.0844) ND (0.0844) 2.09J 1,350 J ND (0.0844) ND (0.0844)
Target analytes not listed were not detected.
ND ()=Not detected at specified detection limit.
Bold values exceed Standards.
J = Estimated value.
U = Not present above the associated level, blank contamination present.
80396910.0 I Aug200 I GW _ Rpt.doc (9/27 /0 I)
Groundwater
Analyte Standard
Benzene 1
n-Butylbenzene 70
sec-Butvlbenzene 70
Chloroform 0.19
1,2-Dichlorobenzene 620
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
Ethvlbenzene 29
Isopropylbenzene 70
p-lsopropyltoluene -
Napthalene 21
Tetrachloroethene 0.7
Tetrahydrofuran -
Toluene 1000
1, 1, I-Trichloroethane 200
1,1,2-Trichloroethane -
Trichloroethene 2.8
Trichlorofluoromethane 2100
1,2,4-Trimethylbenzene 350
1,3,5-Trimethvlbenzene 350
Vinyl chloride O.o15
m&p-Xvlene 530
o-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value. ,
ND =Not detected at (detection limit).
80396910.01 Aug2001GW _Rpt.doc (9/27/01)
Table 3-17
Historical Analytical Results for MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November February May September
1998 2000 2000 2000
0.724 ND (0.984) 0.495 J ND (0.492)
0.240 ND (1.28) 0.184 J ND (0.642)
0.315 ND (1.49) 0.268 J ND (0.745)
0.793 ND (1.34) 0.577 ND (0.670)
0.642 ND (1.84) 0.349 J ND (0.920)
351 245 178 156
7.02 6.12 J 4.49 4.05
867 492 401 391
39.3 40.8 40.6 45.l
2.22 ND (1.63) 1.41 1.33 J
2.03 ND (1.10) 0.727 0.292 J
0.618 ND (0.948) 0.400 J ND (0.474)
ND (0.106) ND (904) 0.182 J ND (0.452)
15.7 J ND (2.12) 16.7 ND (1.06)
61.3 44.4 34.4 33.l
7.63 J ND (8.4) ND (0.402) ND (4.02)
1.48 ND (1.36) 0.335 J ND (0.680)
1.09 ND (0.662) 0.928 ND (0.331)
6.03 2.16 J 3.17 2.23 J
515 446 479 510
0.575 ND (4.16) 1.26 ND (2.08)
ND (0.0952) ND (1.50) 0.509 J ND (0.749)
ND (0.0800) ND(0.872) 0.248 J ND {0.436)
38.7 29.3 16.0 17.8
1.57 ND (2.74) 0.935 J ND (1.37)
3.43 ND (1.43) 1.59 1.66 J
February August
2001 2001
0.465 J ND (0.320)
ND (0.510) ND (0.510)
ND (0.525) ND (0.525)
ND (0.448) ND (0.448)
ND (0.482) ND (0.482)
173 128
3.68 3.09
433 405
37.1 37.4
0.937 J 1.30 J
0.170J ND (0.680)
ND (0.466) ND (0.466)
ND (0.575) ND (0.575)
7.69J 8.56J
28.8 23.9 J
ND (4.50) ND (4.50)
ND (0.318) ND (0.318)
ND (0.845) 4.29
2.68 1.92 J
426 467
ND (0.530) ND (0.530)
ND (0.620) ND (0.620)
ND {0.452) ND (0.452)
19.2 17.4
0.363 u ND (0.835)
0.815 J 0.715 J
-------------------
-------------------
Groundwater
Analvte Standard
Benzene 1
Chlo roe thane 2800
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
p-lsopropyltoluene -
Trichloroethene 2.8
Vinvl chloride 0.015
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND =Not detected at (detection limit).
Table 3-18
Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November February May September
1998 2000 2000 2000
0.172 J 0.315J 0.304 J 0.280 J
0.485 J 0.904 0.705 0.649 J
108 179 173 159
0.303 J 0.633 0.607 0.576 J
8.16 13.8 15.4 13.7
6.86 11.7 12.0 11.6
0.478 0.701 0.794 0.683 J
0.181 J ND (0.0452) ND (0.0452) ND(0.0904)
ND (0.587) U 0.289 J 0.494 J ND (0.489) U
8.84 11.5 9.73 9.35
U =Not present above the associated level; blank contamination is present.
80396910.0 I Aug200 I GW _ Rpt.doc (9/27 /0 I)
February August
2001 2001
0.396 J 0.395 J
ND (0.462) ND (0.185) UJ
162 143
ND (0.510) ND (0.204) UJ
16.8 lp.7
12.9 .tl.7
0.708 J 0.578 J
ND (0.575) ND(0.230)
ND (0.685) 0.357 J
11.8 11.6
Groundwater
Analvte Standard
Benzene l
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Ethylbenzene 29
Methyl t-butvl ether 200
Tetrahydrofuran -
Toluene 1,000
1, 1, I-Trichloroethane 200
Trichloroethene 2.8
Vinyl chloride 0.015
m&o-Xvlene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND =Not detected at (detection limit).
Table 3-19
Historical Analytical Results for MW-215
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November February May September
1998 2000 2000 2000
0.0963 J 0.114 J ND (0.0492) ND (0.0492)
4.30 4.07 3.43 3.16
3.85 3.02 1.93 l.75
ND (0.104) U 0.0401 J 0.0409 J 0.0496 J
0.0601 J ND (0.0552) ND (0.0552) ND (0.0552)
1.22 ND (0.0469) 1.10 0.937 J
58.6 19.1 15.0 12.2
ND (0.141) ND (0.0680) ND (0.0680) ND (0.0680)
ND (0.0965) ND (0.0331) ND (0.0331) ND (0.0331)
ND (0.322)U 0.138 J 0.1241 ND (0.116) U
0.381 J ND (0.0574) ND (0.0574) ND (0.0574)
0.0885 J ND (0.137) ND (0.137) ND (0.137)
U =Not present above the associated level; blank contamination is present.
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
February August
2001 2001
ND (0.0641) 0.142 J
3.55 5.72
2.38 3.48
ND (0.112) 0.0775 J
ND (0.136) ND (0.136)
0.427 J ND (0.116)
6.41 ND (0.900)
ND (0.0637) 0.228 J
ND (0.169) 2.26
ND (0.137) 0.242 J
ND (0.114) ND (0.114)
ND (0.167) ND (0.167)
-------------------
-------------------
Groundwater May
Analvte Standard 1998
Toluene 1000 0.171
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at {detection limit).
Table 3-20
Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November February May
1998 2000 2000
ND (0.0522) UJ ND (0.0680) ND (0.0680)
UJ = Not detected and the detection limit is estimated.
80396910.0 I Aug200 I GW _Rpt.doc (9/27 /0 I)
September February August
2000 2001 2001
ND (0.0680) ND (0.0637) ND (0.0637)
Table 3-21
Historical Analytical Results for MW-220
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Groundwater May
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
1, 1-Dichloroethane 700 ND (0.0576)
Methyl t-butyl ether 200 ND (0.0365)
Groundwater September
Analvte Standard 2000
Carbon disulfide 700 ND (0.0484)UJ
1,1-Dichloroethane 700 ND (0.0487)
Methyl t-butyl ether 200 ND (0.0469)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
UJ = Not detected and the detection limit is estimated.
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
November July
1998 1999
ND (0.0547) 0.426 J
ND (0.0576) ND (0.0736)
ND (0.0365) UJ ND (0.0334)
November February
2000 2001
ND (0.0684) ND (0.0684) UJ
0.426 J 0.456 J
ND (0.116) ND (0.116)
October
1999
0.162
ND (0.0588)
ND (0.0512)
May
2001
ND (0.0684)
ND (0.124)
ND (0.116)
February May
2000 2000
ND (0.0484) UJ ND (0.0484)
ND (0.0487) ND (0.0487)
ND (0.0469) 0.441 J .
August
2001
ND (0.0684) UJ
0.530
ND (0.116)
-------------------
-------------------
Table 3-22
Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc.
Groundwater May
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
1, 1-Dichloroethane 700 ND (0.0576)
1, 1-Dichloroethene 7 0.0908 J
cis-1,2-Dichloroethene 70 ND (0.0383)
Toluene 1,000 0.156 J
Groundwater September
Analvte Standard 2000
Carbon disulfide 700 ND (0.0484)
UJ
1, 1-Dichloroethane 700 0.328 J
1, 1-Dichloroethene 7 0.0766 J
cis-1,2-Dichloroethene 70 0.139 J
Toluene 1,000 · ND (0.0680)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
UJ = Not detected and the detection limit is estimated.
Washington, North Carolina
November July
1998 1999
ND (0.0547) 0.388 J
ND (0.0576) ND (0.0736)
ND (0.0715) ND (0.102)
ND (0.223) U ND (0.0595)
ND (0.0522) ND (0.0766)
November February
2000 2001
ND (0.0684) ND (0.0684)
UJ
ND (0.124) 0.589
0.0668 J 0.102 J
0.124 J 0.222 J
ND (0.137) ND (0.0637)
U = Not present above the associated level, blank contamination present.
80396910.01 Aug2001 GW _Rpt.doc (9/27/01)
October
1999
0.0944
ND (0.0588)
ND (0.0819)
ND (0.0407)
ND (0.0645)
May
2001
ND (0.0684)
0.536
0.0793 J
0.260 J
ND (0.0637)
February May
2000 2000
ND (0.0484) UJ ND (0.0484)
ND (0.0487) 0.338 J
ND (0.0697) ND (0.279) U
ND (0.0603) ND (0.0603)
ND (0.0680) ND (0.0680)
August
2001
ND (0.0684) UJ
ND (0.124)
ND (0.122)
0.157 J
ND (0.0637)
Table 3-23
Historical Analytical Results for MW-224
Hamilton BeachOProctor-Silex, Inc.
Groundwater November
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
Toluene 1,000 ND (0.0522)
Groundwater November
Analyte Standard 2000
Carbon disulfide 700 0.697 J
Toluene 1,000 ND (0.0637)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND =Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396910.01 Aug2001GW _Rpt.doc (9127/01)
Washington, North Carolina
July October February
1999 1999 2000
2.22 2.72 ND (1.05) UJ
ND (0.0766) ND (0.0645) ND (0.0680)
February May August
2001 2001 2001
ND (0.571) UJ 0.715 J 0.515 J
ND (0.0637) ND (0.0637) ND (0.0637)
May September
2000 2000
ND (0.334) U 0.350 J
0.0542 J ND (0.0680)
-------------------
-------------------
Table 3-24
Historical Analytical Results for MW-225
Hamilton Beach¢Proctor-Silex, Inc.
Groundwater November
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
Chloroform 0.19 ND (0.0480)
Groundwater November
Analyte Standard 2000
Carbon disulfide 700 ND (0.0684)
Chloroform 0.19 ND (0.0896)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND== Not detected at (detection limit).
NS == Not sampled.
UJ == Not detected and the detection limit is estimated.
80396910.0 l Aug200 l OW_ Rpt.doc (9/27 /0 l)
Washington, North Carolina
July October February
1999 1999 2000
ND (0.864) 0.0691 ND (0.0484) UJ
ND (0.0424) 0.171 ND (0.0670)
February May August
2001 2001 2001
ND (0.511) UJ ND (0.0684) ND (0.0684)
ND (0.0896) ND (0.0896) ND (0.0896)
May2000 September
2000
ND (0.0484) ND (0.0484) UJ
ND (0.0670) ND (0.0670)
Table 3-25
Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc.
Groundwater November
Analvte Standard 1998
Carbon disulfide 700 ND (0.0547)
Groundwater November
Analvte Standard 2000
Carbon disulfide 700 ND (0.0684)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
Washington, North Car:olina
July October February
1999 1999 200
ND (0.864) 0.0950 ND (0.0484) UJ
February May August
2001 2001 2001
ND (0.0684) UJ ND (0.0684) ND (0.0684) UJ
May September
2000 2000
ND (0.0484) UJ 0.210 J
-------------------
-------------------
Groundwater
Analvte Standard
Acetone 700
Benzene 1
2-Butanone (MEK) 170
n-Butvlbenzene 70
Carbon disulfide 700
Carbon tetrachloride 0.3
Chloroethane 2800
Chloroform 0.19
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
1, 1-Dichloropropene -
Ethylbenzene 29
Isopropylbenzene 70
p-lsoproovltoluene -
Methyl t-butyl ether 200
Methylene chloride 5
Napthalene 21
n-Propylbenzene 70
1, 1,2,2-Tetrachloroethane 0.17
Tetrachloroethene 0.7
Toluene 1000
1, 1, I -Trichloroethane 200
1, 1,2-Trichloroethane -
Trichloroethene 2.8
1,2, 4-Trimethvlbenzene 350
1,3 ,5-Trimethylbenzene 350
80396910.0 I Aug200 I GW _Rpt.doc (9/2710 I)
Table 3-26
Historical Analytical Results for MW-227
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
November February May September
1998 2000 2000 2000
29.9J ND (5.72) 19.1 J ND (14.3) UJ
0.668 J ND (0.984) 0.622 J ND (2.46)
42.5 J ND (3.58) 40.2 J ND (8.95)
0.437 J ND (l.28) ND (0.0642) UJ ND (3.21)
0.573 J ND (0.968) ND (0.0484) UJ ND (2.42) UJ
ND (0.0576) UJ ND (I.73) 26.2 J ND (4.34) UJ
2.14 J ND (I.51) 14.6 J 26.3
1.64 J ND (1.34) 1.17 J ND (3.35)
4,620 844 3,360 1,340
19.5 J 4.40J 20.2 ND (2.50)
705 108 644 249
228 105 381 211
3.66J ND (l.63) 7.93 J ND (4.06)
ND (0.0444) UJ ND (0.928) 0.182J ND (2.32)
3.58 J ND (9.38) 0.454 J ND (2.76)
0.392 J ND (0.948) ND (0.0474) UJ ND (2.37)
0.194 J ND (0.904) ND (0.0452) UJ ND (2.26)
ND (0.0365) UJ ND (0.938) 0.322 J ND (2.34)
ND (1.13) UJ ND (1.59) 0.982 u ND (3.98) U
3.73 J ND (2.12) ND (0.982) UJ ND (5.30)
2.25 J ND (l.77) ND (0.0886) UJ ND (4.43)
ND (0.102) UJ ND (1.58) 1.48 J ND (4.74)
1.41 J ND (l.14) ND (0.0568) UJ ND(2.84) UJ
29.6J 3.56J 13.8J 8.92 J
3,200 310 2,440 J 1,220
3.20J ND (1.90) 2.95 J ND (4.76)
810 12.9 48.9 J ND (36.9) U
10.8 J ND (1.50) 0.720 J ND (3.74)
3.37 J ND (0.872) 0.646 J ND(2.18)
February August
2001 2001
ND (4.38) 34.7 J
ND (0.0641) 0.978 J
25.2 ND (24.0). UJ
ND (1.02) ND (0.334) UJ
ND (0.684) UJ ND (0.341) UJ
ND (0.652) ND (0.508) UJ
24.6 63.4 J
ND (0.896) 1.83 J
2,300 3,410
10.8 25.2 J
332 855
240 456 J
5.48 8.97 J
ND (0.994) ND (0.385) UJ
ND (1.36) 0.784 J
ND (0.931) ND (0.167) UJ
ND (1.15) ND (0.394) UJ
ND (1.16) ND (0.428) UJ
ND (1.26) U 2.68 J
ND (0.0801) UJ 6.88 J
ND (1.40) ND (0.400) UJ
ND (0.870) ND (0.740) UJ
ND (1.44) ND (1.14} UJ
10.7 26.2 J
1,760 4,480
ND (0.821) 3.62 J
39.6 105 J
ND (1.24) ND (0.198) UJ
ND (0.905} ND (0.385) UJ
Table 3-26 (Continued)
Groundwater
Analyte Standard
Vinyl chloride .015
m&p-Xylene 530
o-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter .
. J = Estimated value.
ND= Not detected at (detection limit).
November February
1998 2000
5.70 J ND (1.15)
8.78 J ND (2.74)
8.91 J ND (1.43)
U = Not present above the associated level, blank contamination present.
UJ =Not detected and the detection limit is estimated.
80396910.0 I Aug200 I GW _Rpt.doc (9/27 /0 I)
May
2000
5.51 J
0.956 J
0.995 J
September February August
2000 2001 2001
ND (115) 4.73 9.02J
1,520 J ND (1.67) 2.12 J
1,240 ND (0.844) 2.09J
-------------------
-------------------
Groundwater
Analyte Standard
Acetone 700
Benzene 1
2-Butanone (MEK) 170
n-B utylbenzene 70
sec-Butvlbenzene 70
Carbon tetrachloride 0.3
Chloroethane 2800
Chloroform 0.19
Chloromethane 2.6
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
1, 1-Dichloropropene -
Ethvlbenzene 29
2-Hexanone -
Isoproovlbenzene 70
p-lsopropyltoluene -
Methyl t-butyl ether 200
4-Methvl-2-oentanone (MIBK) -
Methylene chloride 5
Naothalene 21
n-Propylbenzene 70
Stvrene 100
1, 1, 1,2-Tetrachloroethane -
1, 1,2,2-Tetrachloroethane 0.17
Tetrachloroethene 0.7
Toluene 1000
80396910.01 Aug2001GW_Rpt.doc (9127/01)
Table 3-27
Historical Analytical Results for MW-228
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
November February May
1998 2000 2000
307 J ND (1,430) 360J
51.3 J ND (246) 56.5 J
21.3 J ND (895) 382J
15.6 J ND (321) 9.88 J
5.27 J ND (372) 7.96 J
42.2J ND (434) 26.2J
74.7 J ND (378) 89.8 J
12.8 J ND (335) 9.62 J
ND (0.0521) UJ ND (410) 1.33 J
24,100 16,200 14,500
ND (0.0348) UJ ND (250) ND (0.0499) UJ
96,500 71,800 53,400
3,330 1,970 J 2,360
24.2 J ND (406) 17.0 J
ND (0.0444) UJ ND (232) 1.51 J
544 414J 555 J
45.1 J ND (835) 38.8 J
41.5 J ND (237) 33.7 J
6.80J ND (226) ND (0.0452) UJ
5.21 J ND (234) 20.8 J
12.3 J ND (422) 17.5 J
ND (6.22) UJ ND (398) ND (3.64) UJ
608 ND (530) 246J
200 ND (443) 302 J
ND (0.0578) UJ ND (361) ND (0.0722) UJ
0.810 J ND (474) 0.844 J
0.688 J ND (396) ND (0.0792) UJ
30.5 J ND (284) 32.4 J
1,460 1,610 J 1,520
September February August
2000 2001 2001
ND (572) UJ ND (87.6) 638 J
ND (98.4) 38.7 J 43.9 J
ND (358) 500 J 548 J.
ND (128) 28.9 J 23.9 J
ND (149) 9.56 J ND (3.28) UJ
ND (173) UJ 23.0 J 27.6J
ND (151) 97.3 J 119 J
ND (134) 7.64 J 9.82 J
ND (164) UJ ND (6.35) UJ ND (5.22)UJ
11,900 10,200 12,600
ND (99.8) 79.9 J 91.3 J
31,200 29,800 35,100
2,380 3,740 J 1,650 J
ND (163) 22.5 J 13.l J
ND (92.8) ND (4.97) UJ ND (3.85) UJ
506J 970 J 561 J
ND (334) ND (8.45) UJ ND (36.2) UJ
ND (94.8) 63.8 J 40.lJ
ND (90.4) ND (5.75) UJ ND (3.94) UJ
ND (93.8} ND (5.80) UJ ND (4.28) UJ
ND (169) ND (8.90) UJ ND (6.66) UJ
ND(280)U ND (6.30) UJ 13.4 J
ND (212) 973 J 662J
ND (177) 354 J 229 J
ND (144) 28.3 J 12.9 J
ND (190) ND (5.55) UJ ND (5.98)UJ
ND (158) ND (4.35) UJ ND (7.40) UJ
ND (114) 18.6 J 19.6 J
1,340 1,610 1,390 J
Groundwater
Analvte Standard
· 1,1,1-Trichloroethane 200
1, 1,2-Trichloroethane -
Trichloroethene 2.8
Trichloro fluoromethane 2100
1, 1,2-Trichlorotrifluoroethane 210,000
1,2,4-Trimethvlbenzene 350
1,3,5-Trimethvlbenzene 350
Vinvl chloride 0.15
m&p-Xylene 530
o-Xvlene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
VJ= Not detected and the detection limit is estimated.
80396910.01 Aug2001 GW _ Rpt.doc (9/27/01)
Table 3-27 (Continued)
November February May
1998 2000 2000
173,000 135,000 121,000 J
49.3 J ND (476) 38.0 J
22,800 15,000 13,300
12.7 J ND (1,040) 8.12 J
ND (0.0986) ND (383) 0.947 J
1,270 1,220 J 1,190 J
309 ND (218) 407 J
314 ND (287) 194 J
1,540 1,760 1,680 J
1,330 1,370 1,350
September February August
2000 2001 2001
64,400 50,500 76,100
ND (190) 25.l J 28.0 J
11,500 15,400 8,300
ND (416) 28.2 ND (6.00) UJ
ND (153) UJ ND (6.15) UJ ND (6.04) UJ
933 J 2,110 J 1,370 J
ND (87.2) 530J 340J
ND (115) 492 174 J
1,520 J 2,530 1,640 :J
1,240 2,150J 1,350 J
-------------------
-------------------
Groundwater
Analvte Standard
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
Cis-1,2-Dichloroethene 70
Toluene 1,000
Trichloroethene 2.8
Groundwater
Analvte Standard
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Toluene 1,000
Trichloroethene 2.8
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND =Not detected at (detection limit).
Table 3-28
Historical Analytical Results for MW-230
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
November July October
1998 1999 1999
ND (0.0576) ND (0.0736) 0.265
ND (0.306) U ND (0.102) 0.133
ND (2.67) U ND (0.0595) 0.304
ND (0.0522) 0.286 ND (0.309) U
ND {2.05) U ND (0.0929) 0.921
November February May
2000 2001 2001
ND (0.124) ND (0.124) ND (0.124)
ND (0.122) ND (0.122) ND (0.122)
0.142 J 0.0969 J 0.288 J
ND (0.0637) ND (0.0637) ND (0.0637)
0.235 J 0.160 J 0.292 J
U =Not present above the associated level; blank contamination is present.
80396910.01 Aug2001GW_Rpt.doc (9/27/01)
February May September
2000 2000 2000
0.189 J ND <0.348) U ND W.0487)
0.148 J 0.593 ND (0.0697)
0.354 J 0.573 0.102 J.
0.284 J 0.0826 J 0.126 J
0.661 J 1.11 ND (0.355) U
August
2001
ND (0.124)
ND f0.122)
0.119 J
ND (0.0637)
0.140 J
Table 3-29
Historical Analytical Results for MW-234
Hamilton BeachO Proctor-Silex, Inc.
Groundwater July
Analvte Standard 1999
Carbon disulfide 700 ND (0.864)
1, 1-Dichloroethene 7 ND (0.102)
Groundwater February
Analyte Standard 2001
Carbon disulfide 700 ND (0.0684) UJ
1, 1-Dichloroethene 7
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
ND (0.122)
UJ =Not detected and the detection limit is estimated.
80396910.0 I Aug200 I GW _ Rpt.doc (9/27 /0 I)
Washington, North Carolina
October February May
1999 2000 2000
0.0600 ND (0.0484) UJ ND (0.0484)
ND (0.0819) ND (0.0697) 0.145 J
May August
2001 2001
ND (0.0684) ND (0.0684)
ND (0.122) ND (0.122)
September November
2000 2000
ND (0.0484) UJ ND (0.0684)
ND (0.0697) ND (0.122)
-------------------
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APPENDIX A
GROUNDWATER SAMPLING ANALYTICAL REPORTS
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QUALIFIED DATA
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Introduction
Hamilton Beach<>Proctor-Silex, Washington, NC
Data Evaluation Report
URS-Radian, August 2001
URS-Radian collected thirteen groundwater samples (0801HBWW -213 through-216, -220, -222, -224
through-228, -230, and -234) and two field duplicates at the Hamilton Beach<>Proctor Silex facility in
Washington, NC on August 14 and 15, 2001. The samples were submitted to Severn Trent Laboratories
(STL) in Austin, Texas for the determination of volatile organic compounds (VOC) by SW-846 Method
8260B. A trip blank was included with each shipment of samples to the laboratory for the analysis of voe.
URS-Radian reviewed the analytical results, which were reported by the laboratory under work order
numbers 20108105 and 20108116, The data evaluation was modeled after the National Functional
Guidelines for Organic Data Review (EPA, October 1999). Qualitative and quantitative limitations
associated with the analytical results were identified and defined based on the results of specific quality
control (QC) criteria, Accuracy was determined from the review of spike recoveries. Precision was based
on the evaluation of laboratory duplicate results, Sensitivity was evaluated by comparing reported
detection limits to project-specific maximum reporting limits. Representativeness was evaluated from the
review of holding time and blank data. Sample results have been appropriately qualified based on the
criteria of the data review process. The results of the data review are summarized below.
Sample Condition upon Receipt and Boldin~ Times
All samples were received intact and in good condition by STL on August 15 and 16, 2001, 2001. The
temperature of sample containers upon receipt at the laboratory was within laboratory specification limits
of 1-4°C. Air bubbles were not observed any volatile organic analysis (VOA) vials.
Technical hold times were assessed by comparing the sampling dates with that of the analysis date. All
samples, except samples 0801HBWW227 and 228, were analyzed for VOC within EPA-established
holding times of seven days for unpreserved samples. Samples 0801HBWW227 and 228 were reanalyzed
for VOC on August 27, twelve days after sample collection. Volatile organic results associated with the
August 27 analysis were qualified as estimated (J, UJ).
Calibration
Gas chromatograph/mass spectrometer (GC/MS) instrument tuning and performance checks are performed
to ensure the instrument's ability to provide appropriate mass-resolution, identification, and sensitivity. All
samples were analyzed for voe within twelve hours of the performance check standard. The tuning
compound mass-ion abundance criteria for the VOA were reported within control limits.
Control limits for initial and continuing calibrations are established to ensure that the instrument is capable
of producing accurate quantitative and qualitative data at the beginning and throughout each of the
analyses. Since the results of the initial calibration were not included in the laboratory report, the
evaluation was based on the review of continuing calibration data. Laboratory specifications were met
during the volatile organic continuing calibration conducted on instruments MSDA and MSDB. The
recovery of the continuing calibration standard, however, was not within 80-120% recovery of the true
value for the following target analytes:
0801 HB-PS Wash DE.doc
Page 1 of4
09110/01
Analyte concentrations that are greater than the calibration range, which are presented in the report with E-
flagged, are not as accurate as those results obtained from a diluted analysis that fall within the calibration
range. The E-flagged data are considered unusable (R) since data that are more accurate is available.
Results flagged by the laboratory with an F, indicating that interference or co-elution is suspected, are
considered estimated (J).
0801 HB-PS Wash DE.doc
Page4 of4
09/10/01
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---~~-~~---~~~~~-~­
SECTION IV
Analytical Results
MS-VOA
SW8260B
• 'r. Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
·sromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Daterrime Collected
Dateffime Prepared
Daterrime Analyzed
Dilution Factor
Instrument
Units
. . . CA5 .. _,:;> :. :.
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -08/20/200 I I 0:08
0801HBWD998
2010810503
Aaueous
Received
NA
08/14/2001 13:10
08/15/2001 21:10
08115/200 l 21: l 0
1.0000
MSDA
ug/L
cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND ( ,1.,:\
ND
ND
ND
ND
ND
ND
LIMS Workorder; 80396910 [20 I 08105] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0801HBWW216 0801HBWW220
2010810509 2010810504
Aaueous Aaueous
Received Received
NA NA
08/14/200 l 15: 15 08/ 14/200 l 13 :25
08/15/2001 23:59 08/15/2001 21 :3 8
08/15/200 I 23 :59 08/15/2001 21:38
l.0000 1.0000
MSDA MSDA
ug/L ug/L
Cone Flaa DL RL Cone Flaa DL
ND 0.438 0.000 ND 0.438
ND 6.82 0.000 ND 6.82
ND 3.79 0.000 ND 3.79
ND 0.446 0.000 ND 0.446
ND 0.0641 0.000 ND 0.0641
ND 0.0998 0.000 ND 0.0998
ND 0.131 0.000 ND 0.131
ND 0.118 0.000 ND 0.118
ND 0.170 0.000 ND 0.170
ND 0.199 0.000 ND 0.199
ND 0.200 0.000 ND 0.200
ND 0.102 0.000 ND 0.102
ND 0.105 0.000 ND 0.105
ND 0.0911 0.000 ND 0.0911
ND " ' 0.0684 0.000 ND \.A.:\" 0.0684
ND 0.0652 0.000 ND 0.0652
ND I 0.114 0.000 ND 0.114
ND 0.0842 0.000 ND 0.0842
ND 0.0925 0.000 ND 0.0925
ND 0.0896 0.000 ND 0.0896
ND 0.0938 0.000 ND 0.0938
Page 4
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled a lier the National Fimctiona/ Guidelines for Organic and Inorganic Da/ll Rei•iew
(US EPA, October 1999 and February 1994, respectively).
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
or 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter«. . CAS: .. _ < A¥,l~ ;;';'.
Chloromethane 74-87-3
3-Chloroorvoene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
l 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene l l0-57-6
1 4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-l
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l .1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
l 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloronronane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SEC!ION IV -Analytical Results -08/20/2001 10:08
0801HBWD998
2010810503
.Cone . Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND IA...::S-
ND
ND
ND
NB-a.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
O.~~:;z
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.136
0.331
0.169
0801HBWW216 0801HBWW220
2010810509 2010810504
RL Cone ·Flaa DL RL Cone Flaa DL
0.000 ND 0.127 0.000 ND 0.127
0.000 ND 0.0777 0.000 ND 0.0777
0.000 ND 0.178 0.000 ND 0.178
0.000 ND 0.0974 0.000 ND 0.0974
0.000 ND 0.548 0.000 ND 0.548
0.000 ND 0.140 0.000 ND 0.140
0.000 ND 0.137 0.000 ND 0.137
0.000 ND 0.148 0.000 ND 0.148
0.000 ND \A.°3" 0.780 0.000 ND l.A."::S 0.780
0.000 ND 0.150 0.000 ND 0.150
0.000 ND 0.0965 0.000 ND 0.0965
0.000 ND 0.0846 0.000 ND 0.0846
0000 NI;)-e. O.:B:;i 0.660" N&-Q 0:23'7
0.000 ND 0.124 0.000 0.530 0.124
0.000 ND 0.102 0.000 ND 0.102
0.000 ND 0.122 0.000 ND 0.122
0.000 ND 0.112 0.000 ND 0.112
0.000 ND 0.119 0.000 ND 0.119
0.000 ND 0.0869 0.000 ND 0.0869
0.000 ND 0.135 0.000 ND 0.135
0.000 ND 0.160 0.000 ND 0.160
0.000 ND 0.0994 0.000 ND 0.0994
0.000 ND 0.0818 0.000 ND 0.0818
0.000 ND I 0.0908 0.000 ND 0.0908
0.000 ND 0.101 0.000 ND 0.101
0.000 ND 0.136 0.000 ND 0.136
0.000 ND 0.331 0.000 ND 0.331
0.000 ND 0.169 0.000 ND 0.169
Page 5
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled al\er the National fi111ctio11al Guidelines fur Organic mid /11urga11ic Dt1111 Re1•iew
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.600
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 46 --EP~erl~Fcbr .. 4,re-ly).-· - - - -... -_ .. -- -- -
--~~~-~~-~-~~~-----
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter .. ; ·.CAS :· .. ,·
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isopronvltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butyl ether CMTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
1 1.1.2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
l 2.3-Trichlorobenzene 87-61-6
1 2 4-Trichlorobenzene 120-82-1
l, 1 I-Trichloroethane 71-55-6
1 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloroorooane 96-18-4
1 1.2-Trichlorotrifluoroethane 76-13-1
124-Trimethvlbenzene 95-63-6
1.3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWD998
2010810503
,. .Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NET fl
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
8.0948 0.eee
0.114 0.000
0801HBWW216 080 l HB WW220
2010810509 2010810504
·cone Flaa DL RL Cone Flaa DL
ND 0.109 0.000 ND 0.109
ND 0.0931 0.000 ND 0.0931
ND 0.115 0.000 ND 0.115
ND 0.131 0.000 ND 0.131 .
ND 0.116 0.000 ND 0.116
ND 0.178 0.000 ND _0.178
ND 0.126 0.000 ND 0.126
ND 0.0801 0.000 ND 0.0801
ND 1.59 0.000 ND l.59
ND 0.140 0.000 ND 0.140
ND 0.0977 0.000 ND 0.0977
ND 0.111 0.000 ND 0.111
ND 0.0870 0.000 ND 0.0870
ND 0.144 0.000 ND 0.144
ND 0.900 0.000 ND 0.900
ND 0.0637 0.000 ND -0.0637
ND 0.551 0.000 ND 0.551
ND 0.135 0.000 ND 0.135
ND 0.169 0.000 ND 0.169
ND 0.0821 0.000 ND 0.0821
ND 0.137 0.000 ND 0.137
ND 0.106 0.000 ND 0.106
ND 0.288 0.000 ND 0.288
ND I 0.123 0.000 ND 0.123
ND 0.124 0.000 ND 0.124
ND 0.0905 0.000 ND 0.0905
NB-R. 0.0948 0.000 NB (<._ a.e~zis
ND 0.114 0.000 ND 0.114
Page 6
Sample resulls have been qualified by URS-Radian based on the results or the data review process, which is modeled a tier the N11tio1111/ F1111ctio1111/ G11i<le/i11es for Organic 1111d Jnorg1111ic 011111 Re1•iL'w
(US EPA, October 1999 and February 1994, respectively).
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 46
.,
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
: .. CAS-.
106-42-3
95-47-6
SECTION IV -Analytical Results -08/20/2001 10:08
080IHBWD998
2010810503
.. Cone Flaa
ND
ND
LJMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.167 0.000
0.0844 0.000
080IHBWW216 080IHBWW220
2010810509 2010810504
Cone Flaa DL RL Cone Flaa DL RL
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 7 of 46
Sample results have been qualified by_ URS-Radian based on the results of the data review process, which is modeled a lier 1/u• Nmio1111/ Flmc1io11a/ G11iileli11es for Organic mid Inorg1111ic 011111 Re1•iew
--EP.mJierl~Fcbn-4,re .. ly).-... -... ~ 1111 .... - - - - -
--~---~--~~-~~--~
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
1-Bromo-4-fluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Daterrime Collected
Daterrime Prepared
Daterrime Analyzed
Dilution Factor
Instrument
Units
..
--··>· ...
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWD998
2010810503
Aqueous
Received
NA
08/14/2001 13:10
08/15/2001 21:10
08/15/2001 21:10
1.0000
MSDA
ug/L
·% Recovesv
101
107
104
LIMS Workorder: 80396910 [20 I 08105) Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
080 I HBWW2 I 6 080JHBWW220
2010810509 2010810504
Aqueous Aaueous
Received Received
NA NA
08/14/2001 15:15 08/14/2001 13:25
08/15/2001 23:59 08/15/2001 21:38
08/15/2001 23 :59 08/15/2001 21:38
1.0000 . 1.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recovesv Limits
100 77-117 JOO 77-117
109 61-143 109 61-143
105 87-113 105 87-113
Page !!
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled a tier the N111io1111/ F1111ctio11a/ Guidelines for Organic 1111<1 /11org1111ic D11111 Re1•iew
(US EPA, October 1999 and February 1994, respectively).
- -
F
of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l .3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
CAS. ',";. ~
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWW222
2010810508
Aaueous
Received
NA
08/14/200 I 14:45
08/15/2001 23:31
08/15/200123:31
1.0000
MSDA
u~/L
.Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND I•\
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL
0.438
6.82
3.79
0.446
0.0641
0.0998
0.131
0.118
0.170
0.199
0.200
0.102
0.105
0.0911
0.0684
0.0652
0.114
0.0842
0.0925
0.0896
0.0938
0801HBWW224 080 I HBWW225
2010810505 2010810506
Aaueous Aaueous
Received Received
NA NA
08/14/2001 13:50 08/14/2001 13:55
08/15/200 l 22:06 08/15/200 l 22:34
08/15/2001 22:06 08/15/2001 22:34
l.0000 1.0000
MSDA MSDA
u~ ul!/L
RL Cone Flaa DL RL Cone Flaa DL
0.000 ND 0.438 0.000 ND 0.438
0.000 ND 6.82 0.000 ND 6.82
0.000 ND 3.79 0.000 ND 3.79
0.000 ND 0.446 0.000 ND 0.446
0.000 ND 0.0641 0.000 ND 0.0641
0.000 ND 0.0998 0.000 ND 0.0998
0.000 ND 0.131 0.000 ND 0.131
0.000 ND 0.118 0.000 ND 0.118
0.000 ND 0.170 0.000 ND 0.170
0.000 ND 0.199 0.000 ND 0.199
0.000 ND 0.200 0.000 ND 0.200
0.000 ND 0.102 0.000 ND 0.102
0.000 ND 0.105 0.000 ND 0.105
0.000 ND 0.0911 0.000 ND 0.0911
0.000 0.515 J 0.0684 0.000 ND V....\ 0.0684
0.000 ND 0.0652 0.000 ND 0.0652
0.000 ND I 0.114 0.000 ND 0.114
0.000 ND 0.0842 0.000 ND 0.0842
0.000 ND 0.0925 0.000 ND 0.0925
0.000 ND 0.0896 0.000 ND 0.0896
0.000 ND 0.0938 0.000 ND 0.0938
Page 9
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled alicr //1£' Nmio11a/ Fl111c1io11a/ G11idelines for Organic and Inorganic Daw Rel'lell'
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 46
--EP~er191mFcbn~4,re .. ly). -· - -.. .. -.. ~ - - - - -
-~--~--~~~~-~------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Rarameter:·' · ·
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
• .( .w,~ CAS ,~~ ~~l~-~:h~
74-87-3
107-05-1
95-49-8
106-43-4
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-l
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene I 10-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-l
Dichlorodi fluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
I .2-Dichloroethane 107-06-2
l. 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-l ,2-Dichloroethene 156-60-5
1,2-Dichlbroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1,3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWW222
2010810508
:cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND \ A..-:S
ND
ND
ND
Nfr ~
ND
ND
ND
0.157 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
e.:H7'
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.136
0.331
0.169
0801HBWW224 0801HBWW225
2010810505 2010810506
RL .cone Flaa DL RL Cone Flaa DL
0.000 ND 0.127 0.000 ND 0.127
0.000 ND 0.0777 0.000 ND 0.0777
0.000 ND 0.178 0.000 ND 0.178
0.000 ND 0.0974 0.000 ND 0.0974°
0.000 ND 0.548 0.000 ND 0.548
0.000 ND 0.140 0.000 ND 0.140
0.000 ND 0.137 0.000 ND 0.137
0.000 ND 0.148 0.000 ND ·:o.148
0.000 ND \A.:S 0.780 .0.000 ND l 1.. "\ 0.780
0.000 ND 0.150 0.000 ND 0.150
0.000 ND 0.0965 0.000 ND 0.0965
0.000 ND 0.0846 0.000 ND 0.0846
6.600-Nf) ~ O.:Hil 6.666 ·ND R 9.;!~:;I
0.000 ND 0.124 0.000 ND 0.124
0.000 ND 0.102 0.000 ND 0.102
0.000 ND 0.122 0.000 -ND 0.122
0.000 ND 0.112 0.000 ND 0.112
0.000 ND 0.119 0.000 ND 0.119
0.000 ND 0.0869 0.000 ND 0.0869
0.000 ND 0.135 0.000 ND 0.135
0.000 ND 0.160 0.000 ND 0.160
0.000 ND 0.0994 0.000 ND 0.0994
0.000 ND 0.0818 0.000 ND 0.0818
0.000 ND I 0.0908 0.000 ND 0.0908
0.000 ND 0.101 0.000 ND 0.101
0.000 ND 0.136 0.000 ND 0.136
0.000 ND 0.33 l 0.000 ND 0.331
0.000 ND 0.169 0.000 ND 0.169
Page 10
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled alicr the N111io1111/ J-i111ctio11n/ G11ide/i11esfor Organic mu/ Inorganic Dt11n Rel'iew
(US EPA, October 1999 and February 1994, respectively).
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.888
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter .. CASc
lodomethane 74-88-4
lsoproovlbenzene 98-82-8
4-lsooropvltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Propanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
1 1 1.2-Tetrachloroethane 630-20-6
1 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2.3-Trichlorobenzene 87-61-6
l 2.4-Trichlorobenzene 120-82-1
l 1.1-Trichloroethane 71-55-6
l 1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
l 2.3-Trichloroorooane 96-18-4
1.1 2-Trichlorotrifluoroethane 76-13-1
1.2 4-Trimethvlbenzene 95-63-6
1,3,5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results-08/20/2001 10:08
0801HBWW222
2010810508
, ' Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NB--~
ND
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
Q.Q948 6.60&
0.114 0.000
0801HBWW224 0801HBWW225
2010810505 2010810506
Cone Flag DL RL Cone Flaa DL RL
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 0.000 ND 0.115 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.126 0.000 ND 0.126 0.000
ND 0.0801 0.000 ND 0.0801 0.000
ND 1.59 0.000 ND 1.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.0870 0.000 ND 0.0870 0.000
ND 0.144 0.000 ND 0.144 0.000
ND 0.900 0.000 ND 0.900 0.000
ND 0.0637 0.000 ND 0.0637 0.000
ND 0.551 0.000 ND 0.551 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 0.000 ND 0.288 0.000
ND I 0.123 0.000 ND 0.123 0.000
ND 0.124' 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
NB-~ Q.Q948 Q.QQQ -ND ~ 0.Q9~8 9.QQQ
ND 0.114 0.000 ND 0.ll4 0.000
Page II of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is moddcd alicr 1/ie N111io1111/ F1111clio1111/ G11ide/i11es for Organic 11111/ /11org1111ic Daw Rwi£'11'
46
-..,EP ..... erl .. Fcbr .. 94.rc-ly) ..... -.. -·-... -.... - - -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
. Surrogate Comoound .. . ' .... ·, , .
1-Bromo-4-fluorobenzene
l 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -08/20/2001 10:08
080 I HBWW222
2010810508
Aaueous
Received
NA
08/14/2001 14:45
08/15/200 l 23 :31
08/15/200 l 23 :31
1.0000
MSDA
ue:/L
%Recover\/
101
113
107
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0801HBWW224 0801HBWW225
2010810505 2010810506
Aaueous Aqueous
Received Received
NA NA
08/14/2001 13:50 08/14/2001 13:55
08/15/2001 22:06 08/15/2001 22:34
08/15/2001 22:06 08/15/2001 22:34
1.0000 1.0000
MSDA MSDA
ue:/L ug/L
% Recoverv Limits F % Recoverv Limits
98 77-117 JOO 77-117
107 61-143 107 61-143
103 87-113 105 87-113
Page 13 or
-Sample results have been qualifie~ fy Uf)S-Radian based on the resulls of the data review 11.rocess, w~ich is modeled alier the N111io11a/ F1111ctio1111/ G11ide/i11esfor Org1111ic mu/ bwrgmzic D11w Re1•iell'
.. EP~erl ... Febr 4,re~ly).--· -.. - - -... ~ .. -·-
F
46
-
---~-~~~~~~-~------
SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbehzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chlorofonn
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -08/20/2001 !0:08
0801HBWW226
2010810502
AQueous
Received
NA
08/14/2001 13:05
08/15/2001 20:41
08/15/200 l 20:41
1.0000
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND \,\.::r
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.09 l l 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0801HBWW230 0801HBWW234
2010810501 2010810507
Aaueous Aaueous
Received Received
NA NA
08/14/200111:35 08/14/2001 14:25
08/15/2001 20: 13 08/15/200 l 23 :03
08/15/2001 20:13 08/15/2001 23 :03
1.0000 1.0000
MSDA MSDA
u!!IL u!!IL
Cone Flag DL RL Cone Flaa DL RL
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
ND I~;:::} 0.0684 0.000 ND ~:\ 0.0684 0.000
ND 0.0652 0.000 ND 0.0652 0.000
ND I 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page 14 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled alicr rlie Nario11al F1111crio11u/ G11ideli11esfor Organic mu/ Inorganic Daill Re1•iew
(US EPA, October 1999 and February 1994, respectively).
46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter ,(_CAS, · .. :., t
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l, 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SEC~ION IV -Analytical Results -08/20/2001 10:08
0801HBWW226
2010810502
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND LI.::)
ND
ND
ND
=Nfi" R
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
~~;i 0.006-"'
0.124 0.000
0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0801HBWW230 0801HBWW234
2010810501 2010810507
Cone Flaa DL RL Cone Flaa DL RL
ND 0.127 0.000 ND 0.127 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND 0.548 0.000 ND 0.548 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND \.A::s 0.780 0.000 ND \A..-:\ 0.780 0.000
ND 0.150 0.000 ND 0.150 0.000
ND 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
NB-f' O.J~;i 0.066 ·NB-K 8.~H 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 ND 0.122 0.000
0.119 J 0.112 0.000 ND 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND 0.0818 0.000 ND 0.0818 0.000
ND I 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.331 0.000 ND 0.33 I 0.000
ND 0.169 0.000 ND 0.169 0.000
Page 15 of
-~pie ;e,uly l:vc ~re qualificd~S-Radir ba~cd on !he (csults of the data rcycw nrocess!:li/ci is modeled alkr tlw N111io11al F1111ctio1wl G11ideli11es for Organic and Jnorg1111ic Dt1111 Re1•irn· _
.. EP . rl Fcbn~4.re ·Iv)-._. .. -... - - - - -
46 ..
---~-~~~~~-----~~--
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
· ... Parametelit;/\ -".: :. : :.··:·:-~'f:J:, J, 1r:~cAs!Jj!(.1~it
Iodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I l, l,2-Tetrachloroethane 630-20-6
l 1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
l.2.4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloroorooane 96-18-4
1.1 2-Trichlorotrifluoroethane 76-13-1
1.2 4-Trimethvlbenzene 95-63-6
1.3.5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWW226
2010810502
::iconc:.c ..... Flaa
ND
ND
ND
ND
ND
N:>
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
-Ne-K
ND
LIMS Workorder: 80396910 (20108105] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
-0.Q948 0.000
0.114 0.000
0801HBWW230 0801HBWW234
2010810501 2010810507
Coric Flag DL RL Cone Flaa DL
ND 0.109 0.000 ND 0.109
ND 0.0931 0.000 ND 0.0931
ND 0.115 0.000 ND 0.115
ND 0.131 0.000 ND 0.131
ND 0.116 0.000 ND 0.116
ND 0.178 0.000 ND .0.178
ND 0.126 0.000 ND ... 0.126
ND 0.0801 0.000 ND ·. ·0.0801
ND 1.59 0.000 ND 1.59
ND 0.140 0.000 ND 0.140
ND 0.0977 0.000 ND 0.0977
ND 0.111 0.000 ND 0.111
ND 0.0870 0.000 ND 0.0870
ND 0.144 0.000 ND 0.144
ND 0.900 0.000 ND 0.900
ND 0.0637 0.000 ND -0.0637
ND 0.551 0.000 ND 0.551
ND 0.135 0.000 ND 0.135
ND 0.169 0.000 ND 0.169
ND 0.0821 0.000 ND 0.0821
0.140 J 0.137 0.000 ND 0.137
ND 0.106 0.000 ND 0.106
ND 0.288 0.000 ND 0.288
ND I 0.123 0.000 ND 0.123
ND 0.124 0.000 ND 0.124
ND 0.0905 0.000 ND 0.0905
N& fZ_ '6.0948 0.000 -Nf) ~ 0.0948
ND 0.114 0.000 ND 0.114
Page 16
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled a lier the Nmio11a/ F1111ctio11a/ G11ide/i11esfor Org1111ic 111u/ /11org1111ic 011111 Re1•iew
(US EPA, October 1999 and Fcb1uary 1994, respectively).
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.600
0.000
of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
. CAS .·,,::.~1,.·;,.:,
106-42-3
95-47-6
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWW226
2010810502
iCone Flaa
ND
ND
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Sile.-
STL Austin
DL RL.
0.167 0.000
0.0844 0.000
0801HBWW230 0801HBWW234
2010810501 2010810507
Cone. Flan DL RL Cone Flaa DL RL
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 17 of
Sample results have been qualified by URS-Radian based on the results or the data review process, which is modeled a lier the National Flmctio11al G11ideli11es for Orgm1ic and /11orga11ic Dara Re1•iew
46
-~EP ... Jerl ... Febr .. 94,re~ly).,.. -.. --'.-1--------
------~~~~-~-~---~--
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound :;_-~,.-,.~.:.~~);. -~· _ .. :{}. ~i~l
1-Bromo-4-fluorobenzene
l 2-Dichloroethane-d4
Toluene-dB
SECTION IV -Analytical Results -08/20/2001 I 0:08
0801HBWW226
2010810502
Aaueous
Received
NA
08/14/2001 13:05
08/15/200 l 20:41
08/15/2001 20:41
1.0000
MSDA
ul!IL
·%RecoveN
99
106
103
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0801HBWW230 0801HBWW234
2010810501 2010810507
Aaueous Aaueous
Received Received
NA NA
08/14/2001 11:35 08/14/2001 14:25
08115/200 l 20: 13 08/15/2001 23 :03
08/15/200 l 20: 13 08/15/200 I 23 :03
1.0000 1.0000
MSDA MSDA
u!!IL ug/L
o/o Recovery Limits F o/o Recoverv Limits
99 77-117 100 77-117
106 61-143 110 61-143
105 87-113 104 87-113
Page 18
Sample results have been qualified by URS-Radian based on the results or the data review process, which is modeled atier the N111io11al ri111c1io11a/ G11i</e/i11es for Organic wul J11orga11ic D11lll Re1•iew
(US EPA, October 1999 and February 1994, respectively).
F
of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Dateffime Collected
Dateffime Prepared
Dateffime Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -08120/2001 10:08
TRlPBLANK
2010810510
Aaueous
Received
NA
08/15/2001 00:00
08/15/2001 19:45
08/15/2001 19:45
1.0000
MSDA
u!!IL
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND l• \
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Fla~ DL RL Cone Flaa DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000 I
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
Page 19 of
-Sample results have been qualified by URS-Radian based on the results uf the dala 1evicw process, which is modeled aflcr 1/w Natio1111/ F1111c1io11a/ G11itleli11es for Org1111ic w11/ /11org1111ic Dall/ Rel'ie11•
-SEP~erl-fl!br-94.rcm9'elv).,. - ---.. --.. - - -·-
46 -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter~-. ·. CAS~-.i~;;~: .. ,~r~ .
Iodomethane 74-88-4
Isonronvlbenzene 98-82-8
4-Isonronvltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-nentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Nanhthalene 91-20-3
Pronanenitrile 107-12-0
n-Pronvlbenzene 103-65-1
Stvrene 100-42-5
1 1.1.2-Tetrachloroethane 630-20-6
l 1.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2 3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
1.1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloronronane 96-18-4
l 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
l 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -08/20/2001 10:08
I TRIP BLANK
2010810510
.,Cone .... Flaa
ND
ND
ND
ND
ND
ND
0.159 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NB 1(
ND
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flao DL RL Cone Flaa DL RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000 I
0.124 0.000
0.0905 0.000
it.0948 6.666
0.114 0.000
Page 21 of -Sample results have been qualified by URS-Radian based on the results of the data 1evicw process, which is modeled after th<' N11tim111/ F1111ctio1111/ G11itleli11esfur Organic 1111d /11urg1111ic /)a/ti Re1•icw
-EP~erl .. Febn .. 4.re~ly)... - - -·--... -·-- - -
46
-
- --SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
.. -
Client Sample ID
Lab Sample ID
-..
I TRIP BLANK
2010810510
--
Parameter -: .. ;.CASi.:li'·;.: . .:·~ ;cone Flaa DL . RL
n-Xvlene/m-Xvlene 106-42-3 ND
o-Xvlene 95-47-6 ND
SECTION IV • Analytical Results • 08/20/200 I I 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.167 0.000
0.0844 0.000
-' .. -.. --.. -
Cone.: Flaa DL RL Cone Flaa DL
Page 22
Sample results have been qualified by URS-Radian based on the resulls of lht: data review process, which is modeled a lier 1/w Natio1111/ Fimc1io1111/ G11i</e/i11es fur Orgm1ic 1111d /11org1111ic Daw Re1•iell'
(US EPA, October 1999 and Fcb1 uary 1994, respectively).
- -
RL
of 46
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surronate Gomoound . ~.· . ' ,. ,~
l-Bromo-4-fluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -08/20/2001 I 0:08
TRIP BLANK
2010810510
Aoueous
Received
NA
08/15/200 l 00:00
08/15/2001 19:45
08/15/2001 19:45
1.0000
MSDA
m!IL
--% Recoverv
99
107
102
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
Limits F %Recoverv Limits F % Recoverv Limits
77-117
61-143
87-113
Page 23
Sample results have been qualified by URS-Radian based on the results ol'thc data 1cvicw process, which is moddcd after 1/i,• Nmio1111/ J-i111ctio11a/ G11ide/i11esfor Organic 111111 J11org1111ic Daw Re1•i1•11•
F
of 46
--EP~ierl .. Fchn .. 4,re~ly).:-·---· ·-- - - - --- -
----~--~----------­ECTION IV
nalytical Results
IS-VOA
W8260B
Client Sam~le ID
Lab Sample ID
Matrix
Reported As
% Moisture
Dateffime Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
0801HBWD999
2010811602
Aaueous
Received
NA
08/15/2001 09:10
08/20/2001 17:29
08120/2001 17:29
l.0000
MSDA
ug/L
0801HBWD999 0801HBWW213
2010811602 2010811604
Aaueous Aaueous
Received Received
NA NA
08/15/2001 09:10 08/ l 512001 09:35
OS/21/2001 03:57 08/20/200 I 18:56
08/21/2001 03:57 08/20/2001 18:56
5.0000 10.0000
MSDA MSDA
ug/L ug/L
~i~Barame~?::.;~~'·';,;,;;:-~'f;;ii'j i";!qille.As~iit;.~:l;i ~~di1Qi~tu1~a1i¥iWaiJlr.1~r1"~,,.,.i~B~~~~ ..... ! . :;i'i* .. ·1'~. '• f,!hfJ~·:~. ' 3P.:F.J.!i1 • .·}"'.e.'"1'!""--..· •• ~ • • • f w :i:::;i , •• •• 1, ,, •• • .. ... • • -ffil1 kec>.11-ci~i.~Eiaa ·, ~~,o~~~1Rt: ... ·~~i:i· ;i;:(fo"fic!t;;~.::'-?';Eiaa~.;;.li![>'U'.1:iij~i~1!~Rli¥~J~.;;;]
<\cetone 67-64-1 ND 0.438 0.000
<\cetonitrile 75-05-8 ND
<\crolein 107-02-8 ND
<\crvlonitrile 107-13-1 ND
3enzene 71-43-2 0.335
3romobenzene 108-86-1 ND
3romochloromethane 74-97-5 ND
3romodichloromethane 75-27-4 ND
3romoform 75-25-2 ND
3romomethane 74-83-9 ND
!-Butanone fMEK) 78-93-3 ND
i-Butvlbenzene 104-51-8 ND
;ec-Butvlbenzene 135-98-8 ND
ert-Butvlbenzene 98-06-6 ND
:::arbon disulfide 75-15-0 ND
:::arbon tetrachloride 56-23-5 ND
~-Chloro-1.3-butadiene 126-99-8 ND
:::hlorobenzene 108-90-7 ND
:::hloroethane 75-00-3 0.722
:::hlorofonn 67-66-3 ND
. -Chlorohexane 544-10-5 ND
CTION IV -Analytical Results -09/04/2001 14:52
\o1S Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
·LAustin
6.82 0.000
3.79 0.000
0.446 0.000
J 0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
ND ~ ::.£~ ~.~~; NH ~ ~.:;u u.Ul}U
1'10 34.1 0.0'4'0 N~ 68.2 o.1lbo
J\D 19.0 0.~00 N) 37.9 0. WO
1' D 2.23 atooo N) 4.46 O) JOO
1' D 0.320 n.ooo ND 0.641 c1.ooo
1' D 0.499 /0.000 ]\ D 0.998 /J.000
1' D 0.655 I o.ooo J\D 1.31 /o.ooo
J\D 0.590 I o.ooo l'iD ---l.18 I o.ooo
l'iD 0.850 I 0.000 1' D 1.70 I o.ooo
1' I) o.995 I 0.000 1' D l.99 I 0.000
liD 1.00 I 0.000 l D 2.00 I 0.000
1' D 0.510/ 0.000 lD 1.02 I 0.000
l'ID 0.52'1 0.000 JD 1.05 I 0.000
1' D 0.451 0.000 1' D 0.91 l / 0.000
J D 0.34,1 0.000 1' D 0.684/ 0.000
JD 0.316 0.000 ND 0.65i 0.000
1D 0.5/70 0.000 ND 1.14 0.000
1' D o.'11' 0.000 ND 0.8• 2 0.000
1' D 0. ~62 0.000 N ) 0.9J>5 0.000
J>;D OM48 0.000 ND o.896 0.000
M1 ,, 0. ~~ r-. ............
~--N;} , O.!J':Tii U.lluu---
. Page 4 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled after 1/w N(l/io11a/ J-imctio11a/ G11ideli11es for Organic mul /11orga11ic Data Review
(US EPA, October 1999 and Fcbruary 1994, respectively).
6'
ECTION IV
nalytical Results
IS-VOA
W8260B
Client Sample ID
Lab Sample ID
080 l HBWD999
2010811602
Continued
li~Rafanieter.#}·~ .. , .. ;.;. .• ,. : ...... !;jijj11t!i1:r~9'!·,'!.w~ (!;~~--<lti~
~ "•'•"\ • -:·.: ) ~ ~"": "·~~ .r.·~'
Chloromethane 74-87-3 ND
3-Chloropropene 107-05-1 ND
i-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
1 2-Dibromo-3-chloroorooane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
I 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
:rans-I 4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
1.3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 NS
1.1-Dichloroethane 75-34-3 1~:;i
1.2-Dichloroethane 107-06-2 0.590
1.1-Dichloroethene 75-35-4 16.0
;is-1 2-Dichloroethene 156-59-2 11.8
rans-1.2-Dichloroethene 156-60-5 0.692
I 2-Dichloroorooane 78-87-5 ND
I 3-Dichloropronane 142-28-9 ND
? 2-Dichforooronane 594-20-7 ND
I 1-Dichloroorooene 563-58-6 ND
;is-1.3-Dichloronronene 10061-01-5 ND
rans-I 3-Dichloroorooene 10061-02-6 ND
~thvl methacrvlate 97-63-2 ND
~thvlbenzene 100-41-4 ND
:Iexachloro-1 3-butadiene 87-68-3 ND
!-Hexanone 591-78-6 ND
CTION IV -Analytical Results -09/04/2001 14:52
"1S Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
'LAustin
.. , ... ,er ia~rmll!i;;r.fEWP"a1~·"_ .. ", '·'"11
tl a . ~ ·1·..:! E.iF-r~ . ~-~ .. ·.;.t:r.r
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
R 0.2:97 6.660
ER O:t2'4 9.990
3" 0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0801HBWD999 0801HBWW213
2010811602 2010811604
Jit~~o.r.1c.::~~~~:~·'E1aaii.itDt''·;j .. 'ii~~u:.:~~ ,, .. conc:\ia.. Ela<J·1i~'ill1\;::";;:,;i; :: :Rl:ft.tiiifu.i;;,,,,,~ .1.. } • • . .. ... .~ '~"11, t • •• !L~!~ . .
M'l't R. 0 --·"· u.uuu N'JD R. 1.:; u.11110
N16 0.388 0.000 NI~ 0.777 0.000
ND 0.890 o.lloo N~ l.78 o.boo
Nb 0.487 <l.ooo ND 0.974 d.ooo
1' D 2.74 /o.000 NH 5.48 b.000
1' D 0.700 I o.ooo NI~ 1.40 /0.000
lD 0.685 I 0.000 NJ> 1.37 I o.ooo
1 D 0.140 I 0.000 NI> 1.48 I 0.000
JD 3.90 I 0.000 N) 7.80 0.000
l D 0.15ci 0.000 NI 1.50 0.000
D o.4im 0.000 NI 0.965 0.000
1~D 0.413 0.000 NI 0.846 0.000
rn . " 1.cu u.111111 NI 2.37 0.000
143 0.620 0.000 13 1.24 0.000
Ml ~ o.::: -NI 1.02 0.000 v.vv.,
15 [> 0.610 o.oob 39 1.22 0.000
11 l 0.560 0.000 38 9 1.12 0.000
N 0.595 0./)00 N[ 1.19 0.000
N> 0.434 liooo NI 0.86) 0.000
N> 0.675 (l.000 NI 1.3 0.000
N) 0.800 /0.000 NI 1.61 0.000
} ") 0.497 I o.ooo NI 0.914 0.000
l-D 0.409 I o.ooo NI 0. 18 0.000
lD o.454 I 0.000 NI 0.1 08 0.000
D 0.505/ 0.000 N[ 1. 1 0.000
l~D 0.68.6 0.000 N[ U6 0.000
D I.66 0.000 NI 3 31 0.000
~ I' 0 ,.,, -............ -Nb.. LI l:~ tl.6t!O .u 'J V.vvu-
Page 5 of 6'
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled allcr the Na1iom1/ F1111ctio11al G11it/eli11es fur Organic m11/ ltwrgm11c Daill Re1•iew
·-... EP .... erl .. Febn~4.re.~ly).. ·-- -·-- - - - -·-- -
-·------------------ECTION IV
nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWD999
2010811602
0801HBWD999 0801HBWW213
2010811602 2010811604
~'l>~t.anmteiii_ifillik.i!lli;.:ir.<l~~~ ~:::::!~·~ I~~~~·~~~~~ i~Coric~;~:~?-Eliii~e~« .. :d'ii&~"ll;~ C81:fo-;. ~~Htlaa~iitlt-~1~~~~:: Rt:d.'.'::~~~ ~,.,,. ... -.~ .. ···: ·.Fl '"·"""(jg'""''"'.--.· RI.::~"'"· .,,. -one-.. ,, ·,;· . an;:~'!r. =-§ti""':"· .. ·J"".,.:a.~ i;. • • I • .r,~ ~-·--!"'~ '• ••
Codomethane 74-88-4 ND 0.109 0.000 Mlil ""
d - -v.J~J JU U.Ul MD (l.. 1 --,vJ ~. 00
!sonropylbenzene 98-82-8 ND 0.0931 0.000 N) 0.466 0.0 10 N~ 0.931 0. 000
t-lsopropvltoluene 99-87-6 ND 0.115 0.000 N t> 0.575 O.<l )0 l' ) 1.15 OJ )00
Methvl methacrvlate 80-62-6 ND 0.131 0.000 1' i) 0.655 0.~00 l'D 1.31 c(ooo
Methvl tert-butvl ether (MTBE) 1634-04-4 ND 0.116 0.000 }I D 0.580 o.kloo lD l.16 .000
t-Methyl-2-pentanone (MIBK) 108-10-1 ND 0.178 0.000 1' n 0.890 (/.000 m I.78 .000
Methvlene chloride 75-09-2 0.179 ~ 1 "11> ~.126 0.000 l D 0.630 b.ooo >JD -.· 1.26 0.000
Naphthalene 91-20-3 ND 0.0801 0.000 1 D 0.400 /0.000 ND "' 0.801 0.000
Prooanenitrile 107-12-0 ND l.59 0.000 l D 7.95 I o.ooo ND 15.9 0.000
l-Propvlbenzene 103-65-1 ND 0.140 0.000 l D 0.700 I o.ooo ND 1.40 I o.ooo
3tvrene 100-42-5 ND 0.0977 0.000 l D 0.488 I 0.000 ND 0.977 ./ 0.000
l l.l.2-Tetrachloroethane 630-20-6 ND 0.111 0.000 1 D 0.555 I 0.000 ND 1.11 I 0.000
l .l 2.2-Tetrachloroethane 79-34-5 ND 0.0870 0.000 1 D o.435 I 0.000 ND o.870 I 0.000
fetrachloroethene 127-18-4 ND It.""\' 0.144 0.000 l D 0.72 0 I 0.000 ) 1.7 1 .44 I 0.000
retrahvdrofuran 109-99-9 ND 0.900 0.000 1' D 4.50 0.000 m 9.oo I 0.000
foluene 108-88-3 ND 0.0637 0.000 l D 0.318 0.000 m 0.631 0.000
l.2 3-Trichlorobenzene 87-61-6 ND 0.551 0.000 }I D 2.76 0.000 m 5.51/ 0.000
l ,2 4-Trichlorobenzene 120-82-1 ND 0.135 0.000 l' D 0.67' 0.000 m l.31 0.000
l, l, l -Trichloroethane 71-55-6 ND 0.169 0.000 }I n 0.84 0.000 .76 1 l.61• 0.000
I.I 2-Trichloroethane 79-00-5 ND 0.0821 0.000 N n 0.41) 0.000 ~D o.Rl.11 0.000
rrichloroethene 79-01-6 0.343 J 0.137 0.000 N) 0.6E5 0.000 49 I.:~7 0.000
rrichlorofluoromethane 75-69-4 ND 0.106 0.000 N Ll oso 0.000 m I/o6 0.000
I 2.3-Trichloroorooane 96-18-4 ND 0.288 0.000 ND 1.4 0.000 m l88 0.000
1.1 2-Trichlorotrifluoroethane 76-13-1 ND 0.123 0.000 Nil 0.l 15 0.000 m .23 0.000
l ,2 4-Trimethvlbenzene 95-63-6 ND 0.124 0.000 N) O.c 120 0.000 J~D .24 0.000
1.3 5-Trimethvlbenzene 108-67-8 ND 0.0905 0.000 ND O.' 52 0.000 Jm b.905 0.000
vinvl acetate 108-05-4 NE>--fZ_ O,Q948 Q.QQQ ND 0. 74 0.000 l1D ~.948 0.000
vinvl chloride 75-01-4 11.9 0.114 0.000 I l.!l 1:.r 0. '.';~ v.vvv Jc+.4 \i ... i 't u.uOO
CTION IV -Analytical Results-09/04/2001 14:52
\1S Workorder: 80396910 [20108116} Hamilton Beach-Proctor Silex
'LAustin Page 6 of
Sample results have been qualified by URS-Radian based on the resulls of the data review process, which is modeled a lier 1he Nlltionlll Fw1c1io11al C11ideli11esfur Orgllnic· lllld /11orgm1ic Dlllll Re1•iell'
(US EPA. October 1999 and February J 994. respectively).
6"
ECTION IV
nalytical Results
S-VOA
N8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
OatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
~B'lr.am1r··"b•,,,; i-:~~1:,.J:i~:::!Pj -"'!-~ .. -:. .,.., 'lo• .. ~~u.cs1iif'~j-~' ~*: .... · 1.!~ :;:' .. ·
\cetone 67-64-1
\cetonitrile 75-05-8
\crolein 107-02-8
\crvlonitrile 107-13-1
3enzene 71-43-2
3romobenzene 108-86-1
3romochloromethane 74-97-5
3romodichloromethane 75-27-4
3romofonn 75-25-2
3romomethane 74-83-9
!-Butanone lMEK) 78-93-3
i-Butvlbenzene 104-51-8
iec-Butvlbenzene 135-98-8
ert-Butvlbenzene 98-06-6
::arbon disulfide 75-15-0
::arbon tetrachloride 56-23-5
!-Chloro-1.3-butadiene 126-99-8
::hlorobenzene 108-90-7
::hloroethane 75-00-3
::hloroform 67-66-3
. -Chlorohexane 544-10-5
CTION IV -Analytical Results -09/0412001 14:52
080IHBWW213
2010811604
Aaueous
Received
NA
08/15/2001 09:35
08/21/2001 04:25
08/2112001 04:25
5.0000
MSDA
u2/L
~b"ft·~~~~•aa .. ··-~ ob--· · · ... ,. :R'IJ!•ll.L1ilf•~;:-~g< > -.... ~ ;; ;~::-: ~H~ ~ .. : ol;,!; j 0.
ND 2.19 0.000
ND 34.1 0.000
ND 19.0 0.000
ND 2.23 0.000
ND 0.320 0.000
ND 0.499 0.000
ND 0.655 0.000
ND 0.590 0.000
ND 0.850 0.000
ND 0.995 0.000
ND 1.00 0.000
ND 0.510 0.000
ND 0.525 0.000
ND 0.456 0.000
ND 0.342 0.000
ND 0.326 0.000
ND 0.570 0.000
ND 0.421 0.000
ND 0.462 0.000
ND 0.448 0.000
ND 0.469 0.000
~S Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
'LAustin
0801HBWW214 080IHBWW214
2010811601 2010811601
Aaueous Aaueous
Received Received .
NA NA
08/15/200 l 09:05 08/15/200 l 09:05
08/20/2001 18:26 08/21/2001 04:54
08/20/200 l 18:26 08/21/2001 04:54
5.0000 2.0000
MSDA MSDA
Ul!IT. ug/L
1~~~:3~~~e1aa~!~aL:~~~·.:··?·~Rt~~-::·i;~~;~ ""G · · · ·'-·'*"1·1r.1 1a !~·toe ·: ::-.'.·'-~'a~~iiii"""" ~ .. oncY:-~-:1 ... :mt r· a ·;: 1: :ot~· ... ~.::-:~1m
~t R .., 1n -· fl .ill}(} ND 0.876 0.000
N) 34.l o.oifo ND 13.6 0.000
NJ> 19.0 o.<Joo ND 7.58 0.000
N> 2.23 olloo ND 0.892 0.000
0. 76 J' 0.320 1fooo 0.395 J 0.128 0.000
N) 0.499 ~.000 ND 0.200 0.000
1' n 0.655 ).000 ND 0.262 0.000
1'0 0.590 0.000 ND 0.236 0.000
JI D 0.850 0.000 ND 0.340 0.000
1'0 0.995 0.000 ND 0.398 0.000
NO 1.00 0.000 ND 0.400 0.000
1' ) 0.510 0.000 ND 0.204 0.000
ND 0.525 0.000 ND 0.210 0.000
N) 0.456 0.000 ND 0.182 0.000
N> 0.342 I 0.000 ND 0.137 0.000
ND 0.326 / 0.000 ND 0.130 0.000
N~ 0.570/ 0.000 ND 0.228 0.000
N) 0.42 I/ 0.000 ND 0.168 0.000
N) 0.46'' 0.000 ND tA.J 0.185 0.000
Nb 0.4<W 0.000 ND 0.179 0.000
Nb ~II o.~ U.ln1u ND 0.188 0.000
Page 9 of 6'
Sample results have been qualified by URS-Radian based on the results uf thi: data ri:vicw process, which is modeled a tier 1he Nmium1/ F1111c1io11a/ G11it/e/i11es fur Organic mu/ l11urgm1ic Daw Rel'il'll'
-..,EP~erl'9mFcbnm194.re, .. ly)._ ·---- -- -- -- --
-----~-------------ECTION IV
nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW213
2010811604
~~:ie.arai11~ter;;~Gi:i~~:r"~1ftI".llii:i~ ~ri.·K~?'5?~~ :tt;l;:~1n~~F.fad~~&r~u~ig~~~Bi1'~~::~~
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
l .2-Dibromo-3-chloroorooane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1.2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-I 4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
1.3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 N1T"
l, 1-Dichloroethane 75-34-3 128
1.2-Dichloroethane 107-06-2 3.09
l, 1-Dichloroethene 75-35-4 405
::is-1.2-Dichloroethene 156-59-2 37.4
:rans-I 2-Dichloroethene 156-60-5 1.30
1.2-Dichlorooronane 78-87-5 ND
1.3-Dichloroorooane 142-28-9 ND
Z.2-Dichloroorooane 594-20-7 ND
I, 1-Dichloroorooene 563-58-6 ND
::is-1 3-Dichloroorooene 10061-01-5 ND
rans-1.3-Dichloroorooene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 ND
H:exachloro-1 3-butadiene 87-68-3 ND
~-Hexanone 591-78-6 ND
:cnON IV -Analytical Results -09/04/2001 14:52
MS Workorder: 80396910 (20108116] Hamilton Beach-Proctor Silex
'LAustin
0.635 0.000
0.388 0.000
0.890 0.000
0.487 0.000
2.74 0.000
0.700 0.000
0.685 0.000
0.740 0.000
3.90 0.000
0.750 0.000
0.482 0.000
0.423 0.000
'2... U8 6.6M•
0.620 0.000
0.510 0.000
0.610 0.000
0.560 0.000
J 0.595 0.000
0.434 0.000
0.675 0.000
0.800 0.000
0.497 0.000
0.409 0.000
0.454 0.000
0.505 0.000
0.680 0.000
1.66 0.000
0.845 0.000
0801HBWW214 0801HBWW214
2010811601 2010811601
:;:Gafib?~lfil~~Ei~lai:i~~Dlli~i\:ri!l~R~fo:i~~'i:· ·conch :· ;-::'f=rtaaJ:·~:.ol!iiJ:.:.~::.:.=;J{LP·2~
N1 " l\ r-.,. ::: ... o ND 0.254 0.000
NI 0.388 o.coo ND 0.155 0.000
NT 0.890 0. 00 ND 0.356 0.000
NII 0.487 0. lOO ND 0.195 0.000
NP 2.74 0 000 ND 1.10 0.000
NP 0.700 0 000 ND .. 0.280 0.000
ND 0.685 ( .000 ND -0.274 0.000
N> 0.740 .000 ND 0.296 0.000
N> 3.90 .000 ND 1.56 0.000
N) 0.750 J0.000 ND 0.300 0.000
N) 0.482 /o.ooo ND 0.193 0.000
ND 0.423 I o.ooo ND 0.169 0.000
N) 1.18 I o.ooo NB-'2 0.4=t4 e.eee
l 3 0.620 I o.ooo 143 0.248 0.000
1' [) 0.510 0.000 ND \A.I-0.204 0.000
11.6 0.610 I 0.000 16.7 -0.244 0.000
11.5 o.s6o I 0.000 11.7 0.224. 0.000
0 444 lA 0.595 I 0.000 0.578 J 0.238 0.000
NO 0.434 0.000 ND 0.174 0.000
Nn 0.675 0.000 ND 0.270 0.000
Nn 0.800 0.000 ND 0.320 0.000
'II n 0.49 0.000 ND 0.199 0.000
ND 0.40f 0.000 ND 0.164 0.000
l' [) 0.4~ # 0.000 ND 0.182 0.000
1' D 0.51 5 0.000 ND 0.202 0.000
l-J) 0.6 0 0.000 ND 0.272 0.000
i-h 1.60 0.000 ND 0.662 0.000
N[R ',, o.~ v:UUU ND 0.338 0.000
Page 10 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is moddcd after 1/11• Nmio11al Fr111c1io11a/ G11ideli11esfor Organic m11//11orga11ic Dalli Re1•iell'
(US EPA, October 1999 and Fc:bruary 1994, respectively).
ECTION IV
nalytical Results
S-VOA
W8260B
Client Sample ID
Lab Sample ID
:::ontinued
&earamefef.~Bi.Z'J.:::-~:-?·~";;a:il~·::~ '~:'lMl"$1!~'1'¥-f:l~
lodomethane 74-88-4
!soproov I benzene 98-82-8
t-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
\1ethvl tert-butvl ether (MTBE) 1634-04-4
t-Methvl-2-nentanone <MIBK) 108-10-l
Methylene chloride 75-09-2
~anhthalene 91-20-3
?rooanenitrile 107-12-0
1-Propylbenzene 103-65-1
3tvrene 100-42-5
I 1.1.2-Tetrachloroethane 630-20-6
I 1.2.2-Tetrachloroethane 79-34-5
fetrachloroethene 127-18-4
fetrahvdrofuran 109-99-9
foluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
l ,2 4-Trichlorobenzene 120-82-1
1.1 I -Trichloroethane 71-55-6
I. J 2-Trichloroethane 79-00-5
frichloroethene 79-01-6
frichlorofluoromethane 75-69-4
l .2.3-Trichlorooronane 96-18-4
I 1.2-Trichlorotrifluoroethane 76-13-1
l 2.4-Trimethv lbenzene 95-63-6
l 3,5-Trimethylbenzene 108-67-8
linvl acetate 108-05-4
linvl chloride 75-01-4
CTION IV -Analytical Results -09/04/2001 14:52
080IHBWW213
2010811604
iii!OiJ~G~~~~~·aa~~~hi~~·~RL:·:: ::)~~
ND 0.545 0.000
ND 0.466 0.000
ND 0.575 0.000
ND 0.655 0.000
ND 0.580 0.000
ND 0.890 0.000
ND 0.630 0.000
8.56 0.400 0.000
ND 7.95 0.000
ND 0.700 0.000
ND 0.488 0.000
ND 0.555 0.000
ND 0.435 0.000
23.9 ., 0.720 0.000
ND 4.50 0.000
ND 0.318 0.000
ND 2.76 0.000
ND 0.675 0.000
4.29 0.845 0.000
1.92 J 0.410 0.000
467 0.685 0.000
ND 0.530 0.000
ND 1.44 0.000
ND 0.615 0.000
ND 0.620 0.000
ND 0.452 0.000
N& fl 9.474 0.000
17.4 0.570 0.000
~S Workorder: 80396910 (20108116) Hamilton Beach-Proctor Silex
'LAustin
080IHBWW214 080IHBWW214
2010811601 2010811601
ai~onc51~~~1cl'a~~ol!t.it,t~:.i;;tf.U!.. _.. ··.:·:~ :~eonC:~f.~~f.~lii1aa~~1r,Dlt'.1;,i;ifi:lll~~Rrn11l1~ :;~~
·MI) !<. 0 --.J~-V.lJllV ND 0.218 0.000
Nb 0.466 o.Qbo ND 0.186 0.000
Nl 0.575 o.boo ND 0.230 0.000
ND 0.655 <iooo ND 0.262 0.000
N> 0.580 0.000 ND 0.232 0.000
N> 0.890 A>.000 ND 0.356 0.000
N> 0.630 /0.000 ~NDY< 0.252tA. 0.000
N> 0.400 0.000 ND 0.160 0.000
NI> 7.95 I o.ooo ND 3.18 0.000
N) 0.700 I 0.000 ND 0.280 0.000
N1 0.488 0.000 ND 0.195 0.000
Nb 0.555 0.000 ND 0.222 0.000
ND 0.435 0.000 ND 0.174 0.000
1' n 0.720 0.000 ND \A:.) 0.288 0.000
Nn 4.50 I 0.000 ND 1.80 0.000
1' n 0.318 / 0.000 ND 0.127 0.000
ND 2.16 I 0.000 ND 1.10 0.000
NO 0.67 0.000 ND 0.270 0.000
1' ) 0.8 4, 0.000 ND 0.338 0.000
ND 0.4 ) 0.000 ND 0.164 0.000
ND 0.6 5 0.000 0.357 J 0.274 0.000
N1 0.5 0 0.000 ND 0.212 0.000
NJ 1.4 t 0.000 ND 0.576 0.000
Nn 0. 15 0.000 ND 0.246 0.000
Nh 0. 26 0.000 ND 0.248 0.000
ND 0. 52 0.000 ND 0.181 0.000
Nb 04 74 0.000 ~ R 9.196 6.eee
11 LK • 11 oi~ -V.Uvv l l.6 0.228 0.000
Page 11 of
Sample results have been qualified by URS-Radian based on the results uf the data review process, which is modeled after Liie Nmio1111/ l·i111c1io11a/ G11ide/i11es for Orgt111ic 11111/ l11orgt111ic Dt1W Rel'iew
·-mliiEP']ilierl9-Fchn .. 4,re .. lv)._ ·-- - - - - - - - - - -
-------·------------ECTION IV
nalytical Results
IS-VOA
W8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Datefflme Collected
Dateffime Prepared
Datefflme Analyzed
Dilution Factor
Instrument
Units
0801HBWW215
2010811603
Aaueous
Received
NA
08/15/2001 09:20
08/20/2001 17:58
08/20/2001 17:58
1.0000
MSDA
m?/L
~~~·amete~:;r.~-:~-\:1•0~ ~........:,.!~-~ ·~~~-:~· 1:'1"t ;w~, .. ~h·· ~·~~kii:~:~~Elab~ijt.fil0U~~'f~ii1;:;r~Rt;~:-.,__.::I1i; ....... ' ~ ·r.
Acetone 67-64-1 ND
A.cetonitrile 75-05-8 ND
A.crolein 107-02-8 ND
A.crvlonitrile 107-13-1 ND
Benzene 71-43-2 0.142
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bro mo methane 74-83-9 ND
i-Butanone (MEK) 78-93-3 ND
l-Butvlbenzene 104-51-8 ND
;ec-Butvlbenzene 135-98-8 ND
:ert-Butvlbenzene 98-06-6 ND
:arbon disulfide 75-15-0 ND
:arbon tetrachloride 56-23-5 ND
2-Chloro-1.3-butadiene 126-99-8 ND
:hlorobenzene 108-90-7 ND
:hloroethane 75-00-3 ND
::::hloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
:CTION IV -Analytical Results -09/04/2001 14:52
\1S Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
'LAustin
0.438 0.000
6.82 o.ooo·
3.79 0.000
0.446 0.000
J 0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0801HBWW215 0801HBWW227
2010811603 2010811605
AQueous Aqueous
Received Received
NA NA
08/15/2001 09:20 08/15/2001 09:55
08/21/2001 03:29 08/20/200 l 19:26
08/21/2001 03:29 08/20/2001 19:26
1.0000 50.0000
MSDA MSDA
ug/L ug/L
il!eorri~~-R1aa::_··~ou~~:.-·:~'Wf.{li~:*~~;:;: ·~GoriC~5i~U~Efaff~:m~~~:.~im1R~.i~~~
ND 0.438 0.000 ND '2 ')1 n --
V.JW
ND 6.82 0.000 ND 341 0.0/JO
ND 3.79 0.000 ND 190 0.100
ND 0.446 0.000 N) 22.3 0. ~00
0.185 J 0.0641 0.000 JI D 3.20 Oj 000
ND 0.0998 0.000 JD 4.99 c'ooo
ND 0.131 0.000 JD 6.55 ( .000
ND 0.118 0.000 UD -· 5.90 .000
ND 0.170 0.000 lD -8.50 ).000
ND 0.199 0.000 l'D 9.95 /0.000
ND 0.200 0.000 JI D 10.0 I o.ooo
ND 0.102 0.000 NP 5.10 I o.ooo
ND 0.105 0.000 N) 5.25 I 0.000
ND 0.0911 0.000 N:l 4.56 I 0.000
ND 0.0684 0.000 NJ~ 3.42 I 0.000
ND 0.0652 0.000 N~ 3.26 / 0.000
ND 0.114 0.000 ND 5.7o/ 0.000
ND 0.0842 0.000 N) 4.2/ 0.000
ND 0.0925 0.000 6' .6 4.<12 0.000
ND 0.0896 0.000 N b 4lt8 0.000
ND 0.0938 0.000 ~ ,.; ,.,,. ;;.;;oo
Page 14 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled alier 1/ie N111io11al F1111c1io11a/ G11ide/i11esfor Organic 111111 l11org1111ic Daw Rel'ie11·
(US EPA, October 1999 and February 1994, respectively).
ECTION IV
nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW215 0801 HB WW2 l 5 0801HBWW227
2010811603 2010811603 2010811605
~~ea'fame~-:·1·M~'·B~-.~~fl~ ~GA~~~''.'.tf ';:Q)nc<\,~-~~1aai~i·-01£~ .:·~i!:R1-i'if.im:r1u::1:. .. . ==b..;..;..u. :. ,:-"t!;i ~~-~-~ _f ...... o{ ;.~ ~ ~ton~~i;.:·Jilam ·1•·• DL<· ~ ~ ·. ·:.R.b.~~~ ,rconc:~:.;;~i!.!llF.laal~D·~-~~~;Rlif.:·:,. ~;!iJ.i
Chloromethane 74-87-3 ND
3-Chlorooronene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
1 2-Dibromo-3-chloroorooane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-1.4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
I 2-Dichlorobenzene 95-50-1 ND
1.3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 N&-
1.1-Dichloroethane 75-34-3 5.72
l 2-Dichloroethane 107-06-2 ND
l .1-Dichloroethene 75-35-4 3.48
;is-1.2-Dichloroethene 156-59-2 0.0775
rans-1 2-Dichloroethene 156-60-5 ND
I 2-Dichloropropane 78-87-5 ND
l 3-Dichloroorooane 142-28-9 ND
~ 2-Dichloroprooane 594-20-7 ND
I 1-Dichloroorooene 563-58-6 ND
~is-1.3-Dichloroorooene 10061-01-5 ND
rans-1.3-Dichloroorooene 10061-02-6 ND
~thvl methacrvlate 97-63-2 ND
~thvlbenzene 100-41-4 ND
:Iexachloro-1.3-butadiene 87-68-3 ND
!-Hexanone 591-78-6 ND
:CTION IV .. Analytical Results -09/04/2001 14:52
..is Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
'LAustin
0.127 0.000 ND
0.0777 0.000 ND
0.178 0.000 ND
0.0974 0.000 ND
0.548 0.000 ND
0.140 0.000 ND
0.137 0.000 ND
0.148 0.000 ND
0.780 0.000 ND
0.150 0.000 ND
0.0965 0.000 ND
0.0846 0.000 ND
~ Q..~3T 6.660• Nft'
" 0.124 0.000 5.16
0.102 0.000 ND
0.122 0.000 3.67
::r k1 0.112 0.000 0.116
0.119 0.000 ND
0.0869 0.000 ND
0.135 0.000 ND
0.160 0.000 ND
0.0994 0.000 ND
0.0818 0.000 ND
0.0908 0.000 ND
0.101 0.000 ND
0:136 0.000 ND
0.331 0.000 ND
0.169 0.000 ND
0.127 0.000 N1P ' -.... ~ (\(\(\
' O.JJ
0.0777 0.000 NO 3.88 o.ifoo
0.178 0.000 ND 8.90 i.ooo
0.0974 0.000 Nb 4.87 . /0.000
0.548 0.000 1' b 27.4 I o.ooo
0.140 0.000 l'D 7.00 I 0.000
0.137 0.000 JD 6.85/ 0.000
0.148 0.000 HD 7.4</ 0.000
0.780 0.000 10 3</o 0.000
0.150 0.000 fm 'f.50 0.000
0.0965 0.000 f.rD /4.82 0.000
0.0846 0.000 fm 1~
"' ')'l
(\ ooo
fZ. 9.%3T 6.666 NB-R. I t.8 0.00Q
0.124 0.000 3410 6.20 0.000
0.102 0.000 ~ ,r·(l.. ~.rn 9.999
0.122 0.000 855 6.10 0:000
J 0.112 0.000 a+. ~ 5. --u.JUY
0.119 0.000 8.66 J 5.95 O.MO
0.0869 0.000 NI 4.34 CY.'ooo
0.135 0.000 N> 6.75 A>.000
0.160 0.000 N> 8.00 I o.ooo
0.0994 0.000 ND 4.97 I 0.000
0.0818 0.000 1' b 4.09/ 0.000
0.0908 0.000 D 4.~ 0.000
0.101 0.000 l~D 5Jl5 0.000
0.136 0.000 D l8o 0.000
0.331 0.000 D /16.6 0.000
0.169 0.000 ID ,I; ....... ...
u.~ u.1rl'tl1
Page 15 of
Sample results have ~cen qualified by URS-Radian based on the results of the data 1cvicw process, which is modeled after the N(//ilmal F1111ctio11al G111de/i11es for Org1111ic mu/ l11orga11ic Data Re1•iew
-m9>EP'911iierl F.:br 94.re99ety).-- - - - - - - - - - --
-------------------ECTION IV
nalytical Results
IS-VOA
W8260B
Client Sample ID
Lab Sample ID
Continued
~i·:ai'"1St-·.-.· .. -· .. ·'.ui~;r,,. ·-I m 8F£tifi~~i'i · .!-l,i ;,.r~ ~A'S::--"'"'~:--,
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-nentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Pronanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
l I 1.2-Tetrachloroethane 630-20-6
l 1.2.2-Tetrachloroethane 79-34-5
fetrachloroethene 127-18-4
r etrahvdrofuran 109-99-9
foluene 108-88-3
I 2.3-Trichlorobenzene 87-61-6
1 2.4-Trichlorobenzene 120-82-1
l I. I -Trichloroethane 71-55-6
l, 1 2-Trichloroethane 79-00-5
frichloroethene 79-01-6
frichlorofluoromethane 75-69-4
1.2 3-Trichloroorooane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
I 2.4-Trimethvlbenzene 95-63-6
I 3.5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
vinvl chloride 75-01-4
:crroN IV -Analytical Results -09/04/2001 14:52
0801HBWW215
2010811603
;"~-"=''~ ··::~!fl:ila~f!i~~Ea•~:f~ :C: I • •
ND 0.109 0.000
ND 0.0931 0.000
ND 0.115 0.000
ND 0.131 0.000
ND 0.116 0.000
ND 0.178 0.000
1.05 v-... t N\) o~ 0.000
ND 0.0801 0.000
ND 1.59 0.000
ND 0.140 0.000
ND 0.0977 0.000
ND 0.1I1 0.000
ND 0.0870 0.000
ND \A,-3° 0.144 0.000
ND 0.900 0.000
0.228 J 0.0637 0.000
ND 0.551 0.000
ND 0.135 0.000
2.26 0.169 0.000
ND 0.0821 0.000
0.242 J 0.137 0.000
ND 0.106 0.000
ND 0.288 0.000
ND 0.123 0.000
ND 0.124 0.000
ND 0.0905 0.000
Ne-(2.. 0.99~8 0.000
ND 0.114 0.000
\tS Workorder: 80396910[20108116] Hamilton Beach-Proctor Silex
'LAustin
0801HBWW215 0801HBWW227
2010811603 2010811605
sirslin'?"""·'··-.. Fl ... ,_"Ollf1ltz·~""·1.ol!Rll.. · · :·~~ !B. ;. · .. , Pr.i:~~~·: , aa ·1,i.: '~#.fi.'llfi . '~:. ·-;, :::i,1 · ~co'nc"{~·¥.:~~Eia1iJi;:·.oL'·.:'.:,~'1i.if~R~~~ ~~.::!1,;:;;. .t •• • ..~.cl • r.r . _ .. r ~ ..
ND 0.109 0.000 ND R .c; AC I'\ "'"''
ND 0.0931 0.000 NI 4.66 0.000
ND 0.115 0.000 NI 5.75 o.doo
ND 0.131 0.000 N> 6.55 olloo
ND 0.116 0.000 N> 5.80 <Y.ooo
ND 0.178 0.000 N> 8.90 0.ooo
0.686 IA. y'tJD ~ 0.000 Nil> 6.30 /0.000
ND 0.0801 0.000 N > 4.00 I o.ooo
ND 1.59 0.000 N D 79.5 I 0.000
ND 0.140 0.000 l' D 7.oo I 0.000
ND 0.0977 0.000 l D 4.88 / 0.000
ND 0.111 0.000 l D 5.55/ 0.000
ND 0.0870 0.000 ID 4.3i 0.000
ND ~J 0.144 0.000 ~D 1.to 0.000
ND 0.900 0.000 m 4fo 0.000
ND 0.0637 0.000 5.7 •. 3'.18 0.000
ND 0.551 0.000 m 11.7.6 0.000
ND 0.135 0.000 ~ ':! l.:: ... ,.. £\ ............... . --· -
2.54 0.169 0.000 4480 8.45 0.000
ND 0.0821 0.000 NU R. ~ "' -r..--. ·-v.uuJ
0.333 J 0.137 0.000 11 ~ 6.85 o.ffoo
ND 0.106 0.000 NJ> 5.30 i.ooo
ND 0.288 0.000 Nll 14.4 /0.000
ND 0.123 0.000 N) 6.15 I 0.000
ND 0.124 0.000 ]\ D 6.20/ 0.000
ND 0.0905 0.000 JD 4.51" 0.000
ND '2.._ g.,o~4g Q.QOO JD 4.14 0.000
ND 0.114 0.000 J ID 5~0 ..
Page 16 of
Sample results have been qualified by URS-Radian based on the results of the data ll!vicw process, which is modeled after the Nmio1111/ F1111c1io1111/ G11ille/i11esfur Organic and /11orga11ic Daw Rel'ie11•
(US EPA, October 1999 and F.:bruary 1994, respectively).
ECTION IV
nalytical Results
IS-VOA
W8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
080 I HBWW227
2010811605
Aaueous
Received
NA
08/15/2001 09:55
08/27/2001 21 :25
08/27 /200 I 21 :25
5.0000
MSDB
ul!/L
080 IHBWW228 0801HBWW228
2010811606 2010811606
Aaueous Aaueous
Received Received
NA NA
08/15/200 I I 0:05 08/15/2001 10:05
08/20/2001 20:24 08/27/2001 20:56
08/20/2001 20:24 08/27/2001 20:56
1000.0000 50.0000
MSDA MSDB
m!IL uQ/L
!1:..•-' ·~ .... '" ·~~'!:"""'~~l•i!i&<ilct::\....:'_~:;_;:~ ~'''~?i~;.;.·i1.:?'! ~"°"=:'fi':p.eo•a·"...:~r:Qir.\r.>£'ii!f;if,l.~;,;w":li•;l<i;f·.::v~~ ~~~o'·n··~rJ"'"'~F.·i .. a·~1:.;;~~o· "i:!-".&il!:»JL:" .. <R'~~.l~;i;;_',:,. ,::-rf-n·;;;.;>J.,:.·~t;·ii'~f!;i,1 •.1~w.1!i<1•,·'~'·:o·i;:,iiirg/· :;;i~ ~~~'.tl"J~1!'ffi.:-, ~ :: ~JI> • It lU . -.l.~:¥1.rt~~g~ . -Jr; \i v.J..11"~1fi"~H ,, IY • ·-&;;,t:: •• .!::m!nt'"~" ~ , .. ••· .. ··-·~~u W•Oifv, 1'1luU~fi.;i;-;-:t,i·:1li~B~!':"~,~.fl
Acetone 67-64-1 34.7 '1" i 10.1 0.000 N "> (( 4~~ u.rnJ\1 638 :!" 107 0.000
Acetonitrile 75-05-8 ND VW 40.1 0.000 Nb 6820 0.0~0 ND IA.°3 401 0.000
Acrolein 107-02-8 ND \ 6.87 0.000 N) 3790 0.1 )0 ND I 68.7 0.000
Acrvlonitrile 107-13-1 ND ~ 0.642 0.000 N) 446 0. 00 ND ~ 6.42 0.000
Benzene 71-43-2 0.978 J 0.200 0.000 Nh 64.l 0 )00 43.9 ::> 2.00 0.000
Bromobenzene 108-86-1 ND \1\."S 0.500 0.000 N "> 99.8 0 )00 ND \.A."S 5.00 0.000
Bromochloromethane 74-97-5 ND 0.540 0.000 N n 131 0 000 ND 5.40 0.000
Bromodichloromethane 75-27-4 ND 0.374 0.000 N n 118 C.000 ND 3.74 0.000
Bromoform 75-25-2 ND 0.909 o.ooo l'-n 170 tooo ND 9.09 o.ooo
Bromomethane 74-83-9 ND 0.768 0.000 1' D 199 /0.000 ND •v 7.68 0.000
l-Butanone (MEK) 78-93-3 ND 24.0 0.000 l'-n 200 I 0.000 548 :f 240 0.000
l-Butvlbenzene 104-51-8 ND 0.334 0.000 l'-n 102 I 0.000 23.9 J 3.34 0.000
iec-Butvlbenzene 135-98-8 ND 0.328 0.000 N f1 105 I 0.000 ND \A3' 3.28 0.000
:ert-Butvlbenzene 98-06-6 ND 0.399 0.000 Nh 9l.l I 0.000 ND i 3.99 0.000
:arbon disulfide 75-15-0 ND 0.341 0.000 l'-D 68.4 / 0.000 ND tJ., 3.41 0.000
:arbon tetrachloride 56-23-5 ND 0.508 0.000 Nh 65.2 I 0.000 27.6 ::r 5.08 0.000
l-Chloro-1.3-butadiene 126-99-8 ND 0.666 0.000 l'-n 114 f 0.000 ND lA:T 6.66 0.000
:hlorobenzene 108-90-7 ND ,v 0.356 0.000 1' n 84.2/ 0.000 ND IA.:l' 3.56 0.000
:hloroethane 75-00-3 63.4 ::r 0.555 0.000 1' D 92.::l 0.000 119 ~r 5.55 0.000
:hloroform 67-66-3 1.83 J 0.553 0.000 l'-D 89.6 0.000 9.82 J 5.53 0.000
1-Chlorohexane 544-10-5 ND \A'J 0.618 0.000 1' D ~ './ 93':&-Q.QQ9 ND \A.J 6.18 0.000
:CT.ION IV -Analytical Results -09/04/2001 14:52
MS Workorder: 80396910 (20108116) Hamilton Beach-Proctor Silex
'LAuslin Page 19 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled after rhe Nariona/ F1111clio11a/ G11ideli11es for Orga11ic 11111/ ltwrg1111ic Daw Re1•ie11·
--EP~er19-Fchr9m'4,rc~ly)._ - - - - - - - - - - - -
________________ , __ _
ECTION IV
nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW227
2010811605
.... . -·w.iiii . --.. a~:J~at'amete· · · ·~~}lrn~ji''~;·;m, .... i:!::c~sili11ii:0~ :;conc_~_..,);:Lf:1aa.,:.., oa;J;;;..~:ii'~1:Rll.~~~
Chloromethane 74-87-3 ND
3-Chloropropene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
l .2-Dibromo-3-chloropropane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
rans-I 4-Dichloro-2-butene I 10-57-6 ND
I .4-Dichlorobenzene 106-46-7 ND
l 2-Dichlorobenzene 95-50-1 ND
l 3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
l 1-Dichloroethane 75-34-3 i886
I 2-Dichloroethane 107-06-2 25.2
I 1-Dichloroethene 75-35-4 '844
;is-1 .2-Dichloroethene 156-59-2 456
rans-I 2-Dichloroethene 156-60-5 8.97
l 2-Dichloropropane 78-87-5 ND
I 3-Dichloropropane 142-28-9 ND
! 2-Dichloroorooane 594-20-7 ND
l I-Dichlorooropene 563-58-6 ND
;is-1.3-Dichlorooronene 1006I-OI-5 ND
rans-I 3-Dichloronropene 1006I-02-6 ND
3thvl methacrvlate 97-63-2 ND
3thvlbenzene 100-4I-4 0.784
:Iexachloro-1 3-butadiene 87-68-3 ND
~-Hexanone 591-78-6 ND
:CTION IV -Analytical Results-09/04/2001 14:52
\.iS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
"LAustin
.~ 0.522 0.000
0.309 0.000
0.509 0.000
0.361 0.000
5.20 0.000
0.467 0.000
0.356 0.000
0.516 0.000
7.29 0.000
0.334 0.000
0.503 0.000
0.320 0.000 ,I 1.33 0.000
~R Q.2!32! OOQQ
:::r 0.543 0.000
~ tr.598 0.000
J"" 0.442 0.000
T 0.370 0.000
I~ 'J 0.402 0.000
0.208 0.000
0.550 0.000
0.385 0.000
0.600 0.000
0.517 0.000 ,., 0.734 0.000
J 0.446 0.000
lA.'J 3.23 0.000
l.lJ 3.62 0.000
0801HBWW228 0801HBWW228
2010811606 2010811606
~anc~~~1ao;~;~p-~;~~;:,. RL:--;~~1$: ~coiic:11~~l~-1t:E.1a·al!i'i!'.DIEiltl-.:· ". RL: ;,ii~:tl!;·:.:"
ND R. 1:-.............. ND t.A:r 5.22 0.000 v • .JUU
ND 77.7 0.000 ND 3.09 0.000
N) 178 0.~00 ND 5.09 0.000
ND 97.4 o/ooo ND 3.61 0.000
ND 548 f/.000 ND 52.0 0.000
1' D 140 b.ooo ND --4.67 0.000
l\ ') 137 /0.000 ND 3.56 0.000
l\D 148 I o.ooo ND 5.16 0.000
iD 780 I 0.000 ND 72.9 0.000
1' D 150 I 0.000 ND 3.34 0.000
1' D 96.5/ 0.000 ND 5.03 0.000
iD 84.6' 0.000 ND 3.20 0.000
~B , 23d..---v.JUU ND ,, 13.3 0.000
12600 I24 0.000 89lQ ~R 2.32! o.ooo
Ne-~ 192! Q.000 91.3 3 5.43 0.000
35100 122 0.000 ~5966 ER ).+8 Q.QQQ
t3i 0 R I.: A I650 '3 4.42 0.000 v. CXJ
NI 119 0.000 13.l J 3.70 0.000
NI 86.9 cY.ooo ND \A.3 4.02 0.000
N[ 135 ,-0.ooo ND 2.08 0.000
NJ I60 I o.ooo ND 5.50 0.000
NP 99.4 I 0.000 ND 3.85 0.000
N> 81.8 I 0.000 ND 6.00 0.000
N) 90.8/ 0.000 ND 5.I7 0.000
N) 101/. 0.000 ND ~¥ 7.34 0.000
4' 6 .1 13.b 0.000 561 :J 4.46 0.000
N) 3Al 0.000 ND Ii"\ 32.3 0.000
~ ,' 1£n ,.. --.,.. ND IA J" 36.2 0.000 ·--v. -
Page 20 of
Sample results have been qualified by URS-Radian based on the results nf the data review process, which is modeled a lier the Ni1tio1111/ F1111ctio1w/ Guidelines fur Organic 11111/ lnurg1111ic Daw Rel'iew
(US EPA, October 1999 and February 1994, respectively).
ECTION IV
nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW227 0801HBWW228 0801HBWW228
2010811605 2010811606 2010811606
~~~rariie'·t-'e'··r··~:'::·: . • .,;q~~~r,~~11~f.i!.·a5·:::1~ f~j\'~ih:il~;i;.laia :i.Afifl".\i\~lii~i;illigJ;1R· .•. :: i .. :·:·:t: ~G~rffi:~iillll\~la•;:;t;ti_f r;\i·;ll,,~_·RL·,~b.§;:;;.~ i~r.on"c· '!,·•~; .i .. d.1::11~a .. ·~,:z:L 0 1 :r.:i1'1"'1::¥:;J.01~.~~i~m.';· ' ~:G ... ~·'"'-r"" .. ~ gr.1 ~ ~~···· .F.: .:.-i~~~:=:sr.::n:.-~-:. &. • .. , .. 't' ... ·'""· n-i ,,.. •M -:.a::ll.:i-, ·---~ . ..l.i• ~~ .til·· ~n~ _1,..'1~-~ .• a..: .... ,~m .... rr;-J • ..,111\a..;~~~ •.•
Iodomethane 74-88-4 ND {1-:T 0.143 0.000 NI: 12. l nn n nM ND lAJ 1.43 0.000
lsooroovlbenzene 98-82-8 ND 0.167 0.000 N[ 93. l 0.0(.)t) 40. l J 1.67 0.000
4-Isopropvltoluene 99-87-6 ND 0.394 0.000 Nf 115 0.ClOO ND \A,J 3.94 0.000
Methvl methacrvlate 80-62-6 ND 1.21 0.000 N[ 131 0.~00 ND 12.l 0.000
Methvl tert-butvl ether <MTBE) 1634-04-4 ND 0.428 o.ooo N[ 116 CV.ooo ND 4.28 0.000
4-Methvl-2-nentanone (MIBK) 108-10-1 ND • 0.666 0.000 Nf 178 D.000 ND 1 I 6.66 0.000
Methvlene chloride 75-09-2 2.68 J 0.270 0.000 NI 126 /0.000 13.4 J 2.70 0.000
Naohthalene 91-20-3 6.88 -:I' 0.170 0.000 NI 80.l I 0.000 662 ::::r 1.70 0.000
Prooanenitrile 107-12-0 ND \A.:S 33.7 0.000 Nl 1590 I 0.000 ND "'\ 337 0.000
n-Proovlbenzene 103-65-1 ND 0.400 0.000 NI 140 I 0.000 229 :J 4.00 0.000
Stvrene 100-42-5 ND 0.181 0.000 NI 97.7 / 0.000 12.9 J 1.81 0.000
l l.l 2-Tetrachloroethane 630-20-6 ND 0.598 0.000 N > 111 I 0.000 ND 11\.J 5.98 0.000
1.1.2 2-Tetrachloroethane 79-34-5 ND 0.740 0.000 N > 87./J 0.000 ND IA.1 7.40 0.000
fetrachloroethene 127-18-4 ND 1.14 0.000 2 0 J 14'4 0.000 19.6 J 11.4 0.000
fetrahvdrofuran 109-99-9 ND I' 7.03 0.000 1' n 9bO 0.000 ND lAJ 70.3 0.000
foluene 108-88-3 26.2 J 0.285 0.000 1 >20 '13.7 0.000 1390 'J 2.85 0.000
123-Trichlorobenzene 87-61-6 ND LAT 0.472 0.000 llD /551 0.000 ND 1.i..\ 4.72 0.000
1.2.4-Trichlorobenzene 120-82-1 ND IAT 0.472 0.000 }115 ~· 1 :~:; ~-.: ND !A.:J 4.72 0.000
1.1 I-Trichloroethane 71-55-6 3959 ER 9.219 9.999 76100 169 0.000 49499 ~R 2.19 0.000
1.1 2-Trichloroethane 79-00-5 3.62 J 0.600 0.000 Nfr R. 82.1 0.060 28.0 ~f 6.00 0.000
frichloroethene 79-01-6 105 :T 0.324 0.000 8300 137 0.000 8550 £R 3.24 9.000
frichlorofluoromethane 75-69-4 ND v:J' 0.600 0.000 NB R 1"" ~.""~ ND ~'3' 6.00 0.000
1.2 3-Trichloroorooane 96-18-4 ND 0.760 0.000 ND 288 0.000 ND lA.3 7.60 0.000
l.l.2-Trichlorotrifluoroethane 76-13-1 ND 0.604 0.000 Nr 123 <r.'ooo ND ir. T 6.04 0.000
l 2.4-Trimethvlbenzene 95-63-6 ND 0.198 0.000 11 0 124 · /0.000 1370 .J 1.98 0.000
l.3.5-Trimethvlbenzene 108-67-8 ND W 0.385 0.000 300 J 90.5 / 0.000 340 .:r 3.85 0.000
Vinvl acetate 108-05-4 .WU. fL 9.540 0.000 Nb 94.8/ 0.000 N& ~ ..,.. :. ::: ~.-".:: {;,Ji()
Vinvl chloride 75-01-4 9.02 3 0.372 0.000 l4J:) ~L-111i n non 174 \ 3.72 0.000
® H~ct~ Q/\Nt>'V, ~\Lu-~ltC>/t>t
Page 21 of
:CTION IV -Analytical Results -09/04/2001 14:52
\1S Workorder: 80396910 (20108116] Hamilton Beach-Proctor Silex
'LAustin
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled after the National F1111crio11a/ G11ide/i11es for Organic 1111d /11org1111ic D11111 Review
-..,EP,...erl911mi!Febr~4.re-ely)._ - - - - - - - - - - - -
-------------------ECTION IV
nalytical Results
IS-VOA
W8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
TRIP BLANK
2010811607
Aaueous
Received
NA
08/15/2001 00:00
08/20/2001 14:39
08/20/2001 14:39
1.0000
MSDA
ug/L
~ifP.aram~et' ,/[:.~)~~~~~ §~BAS}~~~ ~1m~ii~1~~"~-s1aw11~lifi',l-''._.~;a11~~-P.i.~!i~
i\cetone 67-64-1 ND
i\cetonitrile 75-05-8 ND
i\crolein 107-02-8 ND
i\crvlonitrile 107-13-1 ND
3enzene 71-43-2 ND
3romobenzene 108-86-1 ND
3romochloromethane 74-97-5 ND
3romodichloromethane 75-27-4 ND
3romofonn 75-25-2 ND
3romomethane 74-83-9 ND
!-Butanone <MEK) 78-93-3 ND
1-Butvlbenzene 104-51-8 ND
iec-Butvlbenzene 135-98-8 ND
ert-Butvlbenzene 98-06-6 ND
:arbon disulfide 75-15-0 ND
:arbon tetrachloride 56-23-5 ND
?-Chloro-1 3-butadiene 126-99-8 ND
:hlorobenzene 108-90-7 ND
:hloroethane 75-00-3 ND
:hlorofonn 67-66-3 ND
. -Chlorohexane 544-10-5 ND
CTlON IV -Analytical Results -09/0412001 14:52
v!S Workorder: 80396910 [20108U6] Hamilton Beach-Proctor Silex
LAuslin
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
~e-onc'-. · .... :~f!ta"ii~J;ioi::.:. ~~ll~~~::,~ .. -~-·+,;;t""''·-;•:!ffiEI ·ra--·-:ruol.J~"".,.... ~ill!iVt!''-o.nc-J!~"::.1. . a ~ ··-, · ., · -~_,_, . .~::• ?.; :1
Page 24 of
Sample results have been qualified by URS-Radian based on the results or th.: data review process, which is modeled aft..:r 1/w N111ia1111/ F1111c1io1111/ G11ide/i11es far Organic 1111<1 /11urgm1ic Daw Rel'iew
(US EPA, October 1999 and February 1994, respectively).
ECTION IV
nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
I TRIP BLANK
2010811607
t:1P.arame1i'::."·' , ... .,. ... ~~~iilarn ' .,;. *'""'"~A"§':;~. ::F· • "f(i.' • l{~u~:".":-=•aa~Diml"1lfuir.;~.:;c•,·-s.e"'~'~i;.;t},
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
J .2-Dibromo-3-chloronronane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
J .2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
Ians-1 4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
1.3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 •NfT
1.1-Dichloroethane 75-34-3 ND
l 2-Dichloroethane 107-06-2 ND
I 1-Dichloroethene 75-35-4 ND
;is-I 2-Dichloroethene 156-59-2 ND
:rans-1.2-Dichloroethene 156-60-5 ND
l 2-Dichloroorooane 78-87-5 ND
I 3-Dichloroorooane 142-28-9 ND
!.2-Dichloroorooane 594-20-7 ND
1.1-DichlorooronP.ne 563-58-6 ND
;is-1 3-Dichloroorooene 10061-01-5 ND
rans-I 3-Dichloronronene 10061-02-6 ND
~thvl methacrvlate 97-63-2 ND
3thvlbenzene 100-41-4 ND
iexachloro-1.3-butadiene 87-68-3 ND
?-Hexanone 591-78-6 ND
:CTION IV -Analytical Results -09/0412001 14:52
\.fS Workorder: 80396910(20108116] Hamilton Beach-Proctor Silex
'LAustin
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
t<.. 0.2~9 Q,000
0.124 0.000
0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
j;!6nn1a'f,tJ.fY,~::Flaa .. ,i.DL;;~mW~!. ~-.. ,:: .. 1~ ·"c · .. .;:_.;.,.;.Fnat""~oL;"""·•·im·!e~t-'""·1~ ff: .. oncr;;;t;4\1:n:· a ~'!.;:: ·_ . :~~~~!~~~~ i! . ' ~-~ 1jff.~:'
Page 25 of
Sample results have been qualified by URS-Radian based on the results 111' the data review process, which is modeled after r/le Nmio1111/ F1111crio11a/ G11itleli11es for Org1111ic 11111/ /norg1111ic Daw Re1•iew
-· ..,EP.,..,erl~Febr-.i4.re-ely)._ - - - - - - - - - - - -
- - - ----------------ECTION IV
.nalytical Results
IS-VOA
W8260B
Continued
Client Sample ID
Lab Sample ID
I TRIP BLANK
2010811607
~·-""" . '· m"'r'"'. -~=,.._,.;_:.,··,·~" ... ·-'"'iiilili:S-iiie"'·ri"'f.'·~~E(lcu-.·. ore·"·'"'~· ~c·~-~~,_,·fif''ia··~B .. :·~~Rl::f~llffi:"·····"" "'.:G,~"-· . ~~~rt&''""""'iDll!i::i:.· -· "'"'Rtf.ilf~.iiir16' -~·-•11 eei;!l!.':f.·;·•'' .-;·· .~;:.;:;·· ·•··· "''O 0$~ .. ·.a~-, .. .;; .. :·' . ·.::;;,·on··-~ a ~i;,-:o· "'i§,"'-~;,".;. "'· ,_;;l\l!...~:;;'~onc:.::;,:.;: ,,a·~!ii' w;1.~1~. 01,"=.: :.-1
lodomethane 74-88-4 ND
Isooroovlbenzene 98-82-8 ND
4-Isooroovltoluene 99-87-6 ND
Methvl methacrvlate 80-62-6 ND
Methvl tert-butvl ether fMTBE) 1634-04-4 ND
4-Methvl-2-oentanone (MIBK) 108-10-1 ND
Methylene chloride 75-09-2 0.180
Naohthalene 91-20-3 ND
Propanenitrile 107-12-0 ND
n-Provvlbenzene 103-65-1 ND
Stvrene 100-42-5 ND
l, 1, 1,2-Tetrachloroethane 630-20-6 ND
1 l 2.2-Tetrachloroethane 79-34-5 ND
fetrachloroethene 127-18-4 ND
fetrahvdrofuran 109-99-9 ND
foluene 108-88-3 ND
l 2 3-Trichlorobenzene 87-61-6 ND
I 2,4-Trichlorobenzene 120-82-1 ND
I 1, I -Trichloroethane 71-55-6 ND
l 1.2-Trichloroethane 79-00-5 ND
frichloroethene 79-01-6 ND
frichlorofluoromethane 75-69-4 ND
l 2 3-Trichlorouronane 96-18-4 ND
l,l 2-Trichlorotrifluoroethane 76-13-1 ND
l.2 4-Trimethvlbenzene 95-63-6 ND
l .3 5-Trimethv I benzene 108-67-8 ND
Vinvl acetate 108-05-4 'Nf)'""
Vinvl chloride 75-01-4 ND
:CTION IV -Analytical Results -09/04/2001 14:52
\.tS Workorder: 80396910 [20!08116] Hamilton Beach-Proctor Silex
'LAustin
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
J 0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
I A-:\ 0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
f2.-0:6~z18 0.006 ..
0.114 0.000
Page 26
Sample results have been qualified by URS-Radian based on the results of the data 1evicw process, which is modeled after the Natiu1111/ F1mctiu1wl G11ideli11esfur Organic mu/ 111urg1111ic Daw Rel'iell'
(US EPA, October 1999 and February 1994, respectively)
of
I
I
I
I
I
I
I
I
I LABORATORY REPORTS
I
I
I
I
I
I
I
I
I
I
-~--~-~----~-~-~---
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DateITime Collected
DateITime Prepared
DateITime Analyzed
Dilution Factor
Instrument
Units
0801HBWD998
2010810503
Aqueous
Received
NA
08/14/2001 13:10
08/15/2001 21: IO
08/15/2001 21:10
1.0000
MSDA
ug/L
~~:f~{i~aramete~~~~i~r;~:~~~~1~ '.;,;"'.-'.\f;C)'.&'{;ii12;;:tl;~J!i :t.GonC.~l~Elao~i:DLi~;;·~t~ 3Rl/ ;~ /f:.::
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone <MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butvlbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 ND
Carbon tetrachloride 56-23-5 ND
2-Chloro-1.3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chloroethane 75-00-3 ND
Chloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
SECTION IV -Analytical Results -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0801HBWW216 0801HBWW220
2010810509 2010810504
Aaueous Aaueous
Received Received
NA NA
08/14/2001 15:15 08/14/2001 13:25
08/15/2001 23:59 08/15/2001 21:38
08/15/2001 23:59 08/15/2001 21:38
1.0000 1.0000
MSDA MSDA
uu!T ug/l
:·'con~::~Ai:::flan:· ·,oL: · .···. '. RL .. _: ,·«' co·nc:. . ' . F.fi'ia" · . DL :· RL . '
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0.000
ND ·0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
ND 0.0684 0.000 ND 0.0684 0.000
ND ' 0.0652 0.000 ND 0.0652 0.000
ND I 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page 4 of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWD998
2010810503
· , .. '.Paramitfi·r;· .:,:; ·: · ::; ;;<.:(: ,-.....,-:~CA'S~~~ r:..cone\., ~ .. ,, °Flao;: .:OL' .)'.
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
1 2-Dibromo-3-chloronronane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1.2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-1.4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
1 3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
1 1-Dichloroethane 75-34-3 ND
1 2-Dichloroethane 107-06-2 ND
1 1-Dichloroethene 75-35-4 ND
cis-1 2-Dichloroethene 156-59-2 ND
trans-I 2-Dichloroethene 156-60-5 ND
1 2-Dichloronronane 78-87-5 ND
1 3-Dichloronronane 142-28-9 ND
2 2-Dichlorooronane 594-20-7 ND
1 1-Dichloronronene 563-58-6 ND
cis-1.3-Dichlorooronene 10061-01-5 ND
trans-1.3-Dichlorooronene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 ND
Hexachloro-1 3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
0.237
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.136
0.33 l
0.169
··RL'<-.<·
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
-...__ -------,, ..,. -
0801HBWW216 0801HBWW220
2010810509 2010810504
.:conc'-:.l: Flaa . DL RL Cone Flaa .:Dl.i.:: ··RL
ND 0.127 0.000 ND 0.127 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND 0.548 0.000 ND 0.548 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND 0.780 0.000 ND 0.780 0.000
ND 0.150 0.000 ND 0.150 0.000
ND 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
ND 0.237 0.000 ND 0.237 0.000
ND 0.124 0.000 0.530 0.124 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 ND 0.122 0.000
ND 0.112 0.000 ND 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND 0.0818 0.000 ND 0.0818 0.000
ND I 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.331 0.000 ND 0.331 0.000
ND 0.169 0.000 ND 0.169 0.000
Page 5 of 46 ----------- -
-~--~~~-~--~-~-~~--
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWD998
2010810503
cJiParametefo :C""°··.· -: : -~;(:;~-'\~~~ ~:.;ih:c>.:s~~rM0~ ~C>rio~;-f; ,~'.'-Rlaa: _, :OL . '.. :•· : Rt..._:
Iodomethane 74-88-4 ND
Isonronv I benzene 98-82-8 ND
4-lsooroovltoluene 99-87-6 ND
Methvl methacrvlate 80-62-6 ND
Methyl tert-butvl ether rMTBE) 1634-04-4 ND
4-Methv 1-2-oentanone (MIBK) 108-10-1 ND
Methvlene chloride 75-09-2 ND
Naohthalene 91-20-3 ND
Pronanenitrile 107-12-0 ND
n-Proov I benzene 103-65-1 ND
Stvrene 100-42-5 ND
I 1 l.2-Tetrachloroethane 630-20-6 ND
1.1.2 2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 ND
Tetrahvdrofuran 109-99-9 ND
Toluene 108-88-3 ND
1 2.3-Trichlorobenzene 87-61-6 ND
1 2 4-Trichlorobenzene 120-82-1 ND
1.1 I -Trichloroethane 71-55-6 ND
1 I 2-Trichloroethane 79-00-5 ND
Trichloroethene 79-01-6 ND
Trichlorofluoromethane 75-69-4 ND
1.2.3-Trichloronronane 96-18-4 ND
1.1.2-Trichlorotrifluoroethane 76-13-1 ND
l 2.4-Trimethvlbenzene 95-63-6 ND
1.3.5-Trimethvlbenzene 108-67-8 ND
Vinvl acetate 108-05-4 ND
Vinvl chloride 75-01-4 ND
SECTION IV -Analytical Results -08/20/200 I I 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
l.59 0.000
0.140 0.000
0.0977 0.000
0.11 I 0.000
0.0870 0.000
0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
. •.:
0801HBWW216 0801HBWW220
2010810509 2010810504
:"Coh1fi:: . ~Etaa . DL · :RL .. Cone· .f1aa·· ·aL'·. · RL
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 0.000 ND 0.115 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND -~ 0.178 0.000
ND 0.126 0.000 ND .·--0.126 0.000
ND 0.0801 . 0.000 ND 0.0801 0.000
ND l.59 0.000 ND l.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.0870 0.000 ND 0.0870 0.000
ND 0.144 0.000 ND 0.144 0.000
ND 0.900 0.000 ND ·-. 0.900 0.000
ND 0.0637 0.000 ND • O· 0.0637 0.000
ND 0.551 0.000 ND 0.551 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 0.000 ND 0.288 0.000
ND I 0.123 0.000 ND 0.123 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.114 0.000 ND 0.114 0.000
Page 6 of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
·.:: :f P.anunetell;/ ;.'. · ; · · {.
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
0801HBWD998
2010810503
·. :·~~·:1~cA~~onc··· ,. Flaa-· .:.,-' ,,,,,.. "' -• ' ' >,:;.._,,. -
106-42-3 ND
95-47-6 ND
SECTION IV· Analytical Results -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
·DL· ... RL ...
0.167 0.000
0.0844 0.000
0801HBWW216 0801HBWW220
2010810509 2010810504
:Cone· -:Flaa-DL RL Cone .Flaa DL · RL
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 7 of 46 ---- -...... - ----~ -.. --·· - - -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
o/o Moisture
Datefrime Collected
Datefrime Prepared
Datefrime Analyzed
Dilution Factor
Instrument
Units
~; ~,{Q.earameter :;~:;,;;_·,;:. ::::. ~;-:.l~i'.\~1~ \~:BAS{t~¥t~'~
Acetone 67-64-1
Acetonitrile 75-05-8
Acrolein 107-02-8
Acrvlonitrile 107-13-1
Benzene 71-43-2
Bromobenzene 108-86-1
Bromochloromethane 74-97-5
Bromodichloromethane 75-27-4
Bromoform 75-25-2
Bromomethane 74-83-9
2-Butanone (MEK) 78-93-3
n-Butvlbenzene 104-51-8
sec-Butvlbenzene 135-98-8
tert-Butvlbenzene 98-06-6
Carbon disulfide 75-15-0
Carbon tetrachloride 56-23-5
2-Chloro-1 3-butadiene 126-99-8
Chlorobenzene 108-90-7
Chloroethane 75-00-3
Chloroform 67-66-3
1-Chlorohexane 544-10-5
SECTION IV -Analytical Results -08/20/2001 10:08
0801HBWW222
2010810508
Aaueous
Received
NA
08/14/2001 14:45
08/15/2001 23:31
08/15/2001 23:31
1.0000
MSDA
ul!l'L
mon~e:~~~ifilaa·< Jo1.;· .. :". ·Rt.:::(
ND 0.438 0.000
ND 6.82 0.000
ND 3.79 0.000
ND 0.446 0.000
ND 0.0641 0.000
ND 0.0998 0.000
ND 0.131 0.000
ND 0.118 0.000
ND 0.170 0.000
ND 0.199 0.000
ND 0.200 0.000
ND 0.102 0.000
ND 0.105 0.000
ND 0.0911 0.000
ND 0.0684 0.000
ND 0.0652 0.000
ND 0.114 0.000
ND 0.0842 0.000
ND 0.0925 0.000
ND 0.0896 0.000
ND 0.0938 0.000
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
-. _.: -~
0801HBWW224 0801HBWW225
2010810505 2010810506
Aaueous Aaueous
Received Received
NA NA
08/14/2001 13:50 08/14/2001 13:55
08/15/2001 22:06 08/15/2001 22:34
08/15/2001 22:06 08/15/200 l 22:34
1.0000 1.0000
MSDA MSDA
ul!!L ul!l'L
:iConc~~::-:; Flaa\. oL~ .. :· ' .. ·RL .. -;·:.~ Cone: ... ·:;flaci .:;DL~ .... RL "
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
0.515 J 0.0684 0.000 ND 0.0684 0.000
ND ' 0.0652 0.000 ND 0.0652 0.000
ND I 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page 9 of 46
-----~~--~-~~-~----
.. - ---.•. -. -· --..
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW222
2010810508
:::•'.iWFiaramete'r~~1;.~~'.fa%:~i~i!-~~ ,~-: '..>') "OUC~~{/:ff.laa;.#;0C)L;-;;,.,?') :.:;;1~Rh~ }[t~-.<: ;;,;,
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chloroto luene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
1 2-Dibromo-3-chloroorooane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-1 4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
1 3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
1 1-Dichloroethane 75-34-3 ND
1 2-Dichloroethane 107-06-2 ND
1 1-Dichloroethene 75-35-4 ND
cis-1 2-Dichloroethene 156-59-2 0.157
trans-1 2-Dichloroethene 156-60-5 ND
1 2-Dichloroorooane 78-87-5 ND
1 3-Dichlorooronane 142-28-9 ND
2 2-Dichloroorooane 594-20-7 ND
1 1-Dichloroorooene 563-58-6 ND
cis-1.3-Dichloroorooene 10061-01-5 ND
trans-1.3-Dichloroorooene 10061-02-6 ND
Ethvl methacivlate 97-63-2 ND
Ethv lbenzene 100-41-4 ND
Hexachloro-1 3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -08/20/200 I I 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0.000
0.122 0.000
J 0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
--.. -~ .. -.... -
0801HBWW224 0801HBWW225
2010810505 2010810506
i.'G_orfo~.i,~,;;.FJaa~,_,;:DL "-":, .. -~RL: -~-·:;.,;'.'. :cone~ f.13({,:::rJl)t.:K.-:.;,.:,: ?RL.
ND 0.127 0.000 ND 0.127 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND 0.548 0.000 ND 0.548 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND 0.780 .0.000 ND 0.780 0.000
ND 0.150 0.000 ND 0.150 0.000
ND 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
ND 0.237 0.000 ND 0.237 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 ND 0.122 0.000
ND 0.112 0.000 ND 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND 0.0818 0.000 ND 0.0818 0.000
ND I 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.331 0.000 ND 0.331 0.000
ND 0.169 0.000 ND 0.169 0.000
Page 10 of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
080 IHBWW222
2010810508
~.Rarametei.;,",..".~; ·: · .:: ·;. '.:-:; .. ·:·,_;oAs~'::~::~: >~Cone· . -~Flaa·· Dl
Iodomethane 74-88-4 ND
lsooroovlbenzene 98-82-8 ND
4-Isooroov ltoluene 99-87-6 ND
Methvl methacrvlate 80-62-6 ND
Methvl tert-butvl ether (MTBE) 1634-04-4 ND
4-Methvl-2-oentanone <MIBK) 108-10-1 ND
Methvlene chloride 75-09-2 ND
Naohthalene 91-20-3 ND
Prooanenitrile 107-12-0 ND
n-Proovlbenzene 103-65-1 ND
Stvrene 100-42-5 ND
l,l 1 2-Tetrachloroethane 630-20-6 ND
1.1 2 2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 ND
Tetrahvdrofuran 109-99-9 ND
Toluene 108-88-3 ND
1 2 3-Trichlorobenzene 87-61-6 ND
1.2.4-Trichlorobenzene 120-82-1 ND
1. l .1-Trichloroethane 71-55-6 ND
1.1.2-Trichloroethane 79-00-5 ND
Trichloroethene 79-01-6 ND
Trichlorofluoromethane 75-69-4 ND
1 2.3-Trichlorooronane 96-18-4 ND
1.1.2-Trichlorotrifluoroethane 76-13-1 ND
1.2.4-Trimethvlbenzene 95-63-6 ND
1.3.5-Trimethvlbenzene 108-67-8 ND
Vinvl acetate 108-05-4 ND
Vinvl chloride 75-01-4 ND
SECTION IV -Analytical Results -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
0.109
0.0931
0.115
0.131
0.116
0.178
0.126
0.0801
1.59
0.140
0.0977
0.111
0.0870
0.144
0.900
0.0637
0.551
0.135
0.169
0.0821
0.137
0.106
0.288
0.123
0.124
0.0905
0.0948
0.114
.. Rl.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0801HBWW224 0801HBWW225
2010810505 2010810506
·cone:· · Flaa DL · RL ·cone Flaa DL RL
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 0.000 ND 0.115 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.126 0.000 ND 0.126 0.000
ND 0.0801 0.000 ND 0.0801 0.000
ND 1.59 0.000 ND 1.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 0.000
ND 0.11 l 0.000 ND 0.11 l 0.000
ND 0.0870 0.000 ND 0.0870 0.000
ND 0.144 0.000 ND 0.144 0.000
ND 0.900 0.000 ND 0.900 0.000
ND 0.0637 0.000 ND 0.0637 0.000
ND 0.551 0.000 ND 0.551 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 0.000 ND 0.288 0.000
ND I 0.123 0.000 ND 0.123 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.114 0.000 ND 0.114 0.000
Page 11 of 46
~----~----~~-------
-~--~--~-~~~-~~-~--
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
0801HBWW226
2010810502
Aaueous
Received
NA
08/14/2001 13:05
08/15/2001 20:41
08/15/2001 20:41
1.0000
MSDA
ug/L
. ::>.·ea:ra'mete11,:~::· .. ', ·:::.: .. · · .. ~:-.\.·:·,:: 1-. :,·cKsr:;,:S:' .. ·:. 4Con"c.,,i.'·.;: .. E1aa::.'0L ,
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone <MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butvlbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 ND
Carbon tetrachloride 56-23-5 ND
2-Chloro-l 3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chloroethane 75-00-3 ND
Chloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
SECTION IV -Analytical Results -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.438
6.82
3.79
0.446
0.0641
0.0998
0.131
0.118
0.170
0.199
0.200
0.102
0.105
0.0911
0.0684
0.0652
0.114
0.0842
0.0925
0.0896
0.0938
:'.Rl ' . ...
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0801HBWW230 0801HBWW234
2010810501 2010810507
Aaueous Aaueous
Received Received
NA NA
08/14/2001 11:35 08/14/2001 14:25
08/15/2001 20: 13 08/15/2001 23:03
08/15/2001 20:13 08/15/2001 23:03
1.0000 1.0000
MSDA MSDA
u!!IL ug/L
. ·cone .~: .:.;Flaa· ot: RI.: .'Cone ·Flaa DL RL
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0. I 18 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
ND 0.0684 0.000 ND 0.0684 0.000
ND 0.0652 0.000 ND 0.0652 0.000
ND I 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page 14 of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW226
20I08I0502
~:;.1>.ara'met«tr,:~ ~,v:,: .::' ···t~. :::, ;~;~~~, i:Bonc·~ } .. '"~:fiaa ~ oL. , . ·. ':RL ,, ,,', ~ .. 4
'_•,' '1
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
I .2-Dibromo-3-chloroorooane 96-I2-8 ND
Dibromochloromethane 124-48-I ND
I 2-Dibromoethane I06-93-4 ND
Dibromomethane 74-95-3 ND
trans-I 4-Dichloro-2-butene I 10-57-6 ND
I .4-Dichlorobenzene I06-46-7 ND
I 2-Dichlorobenzene 95-50-I ND
I .3-Dichlorobenzene 541-73-I ND
Dichlorodifluoromethane 75-7I-8 ND
1.1-Dichloroethane 75-34-3 ND
1.2-Dichloroethane 107-06-2 ND
1. I-Dichloroethene 75-35-4 ND
cis-I .2-Dichloroethene I56-59-2 ND
trans-1.2-Dichloroethene I56-60-5 ND
1.2-Dichloroorooane 78-87-5 ND
1.3-Dichloroorooane 142-28-9 ND
2.2-Dichloroorooane 594-20-7 ND
1. I-Dichloroorooene 563-58-6 ND
cis-1.3-Dichloroorooene 1006I-OI-5 ND
trans-I 3-Dichloronronene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 ND
Hexachloro-I .3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -08120/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
O.I40 0.000
0.137 0.000
0.148 0.000
0.780 0.000
O.I50 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
O.I24 0.000
0.102 0.000
O.I22 0.000
0.112 0.000
O.I I9 0.000
0.0869 0.000
0.135 0.000
O.I60 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
O.lOI 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0801HBWW230 0801HBWW234
201081050I 2010810507
.. cone'--:. '/'Flaa.·. ·DI:. • .. ·· . RL Cone Flaa ·oi.: RL
ND 0.127 0.000 ND O.I27 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND O.I78 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND 0.548 0.000 ND 0.548 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND 0.780 0.000 ND 0.780 0.000
ND O.I50 0.000 ND O.I50 0.000
ND 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
ND 0.237 0.000 ND 0.237 0.000
ND 0.124 0.000 ND O.I24 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 ND O.I22 0.000
O.I 19 J 0.112 0.000 ND 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND O.I35 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND j 0.0818 0.000 ND 0.0818 0.000
ND I 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.331 0.000 ND 0.331 0.000
ND 0.169 0.000 ND 0.169 0.000
Page 15 of 46
----~-------~~-~-~-
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0801HBWW226
2010810502
:::·~·.Ji>aramefer>"-'; .. ·'· .:::'"·r:·1 .~~~ ·~.:~~1$' .. .,. onc:'L~_,,:.::1;.1aa:;· ... oi.: :~; A''
o-Xvlene/m-Xvlene 106-42-3 ND
o-Xvlene 95-47-6 ND
SECTION IV -Analytical Results -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Sile.'
STLAustin
0.167
0.0844
RL'.
0.000
0.000
0801HBWW230 0801HBWW234
2010810501 2010810507
' : ., ''. ~ ' ~\ Conc;;,:-.~d~laa,'" ·,oL · ;RL· : ·Cone. Ebia ·: ·oB:' ·'. : . · RL
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 17 of 46 - -.. - --· - ---.. - - -... - - - -..
SECTION IV
Analytical Results
MS-VOA
SW82608
· <'Parameter . ,.
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
''
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
""-:-.· :·cA's~<" ,:·" ,._;.
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -08/20/2001 10:08
TRIP BLANK
2010810510
Aaueous
Received
NA
08/15/2001 00:00
08/15/2001 19:45
08/15/2001 19:45
1.0000
MSDA
u!!IL
,-conci ;: : : Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
DL RL cone · :Fiaa . DL RL Cone Flaa DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000 I
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
Page 19 of 46
-----~---~~~~~--~--
~--------~~-~-~----
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
I TRIP BLANK
2010810510
: ;::::::!:P.itamltter.;'i,~{::rl:.':,~.::''.:i/::0:§t.1~ ~e:1~,;.,-v~1!'~~ l!.Gonc~?,$:1~Fiaa~::..-~oe:. '· ·::.
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
1.2-Dibromo-3-chloronronane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-1.4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
I 3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
l 1-Dichloroethane 75-34-3 ND
I 2-Dichloroethane 107-06-2 ND
l 1-Dichloroethene 75-35-4 ND
cis-1 2-Dichloroethene 156-59-2 ND
trans-1 2-Dichloroethene 156-60-5 ND
I 2-Dichloronronane 78-87-5 ND
1.3-Dichloroorooane 142-28-9 ND
2.2-Dichloronrooane 594-20-7 ND
1 1-Dichlorooronene 563-58-6 ND
cis-1.3-Dichloroorooene 10061-01-5 ND
trans-1.3-Dichloronronene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethv !benzene 100-41-4 ND
Hexachloro-1 3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -08/20/200 l l 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
0.237
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.136
0.331
0.169
,-';R.'L: ::•.-;;.:· ';cfonc.:· ·::.:~.·, 111aa:.·· OL. ·;· .. ;Rb·:-;··:., ·.;cone; 'Fl•fo .. · ot RL
0.000
0.000
0.000
0.000
0.000
0.000 ··-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 I
0.000
0.000
0.000
0.000
Page 20 of 46
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
I TRIP BLANK
2010810510
· .. ·:;'Parameter·-:'. .. :; ·., --· ·.;. · .. · /.f:':CAS~ ,..eon"C;i.'-·'>·Fila:.' DL '.' ., .... '"'·"' ,., .. ~"·'·. a . . .
Iodomethane 74-88-4 ND
Isooropylbenzene 98-82-8 ND
4-Isooronvltoluene 99-87-6 ND
Methyl methacrvlate 80-62-6 ND
Methyl tert-butvl ether <MTBE) 1634-04-4 ND
4-Methvl-2-oentanone (MIBK) 108-10-1 ND
Methylene chloride 75-09-2 0.159
Naohthalene 91-20-3 ND
Prooanenitrile 107-12-0 ND
n-Propylbenzene 103-65-1 ND
Stvrene 100-42-5 ND
1.1 1 2-Tetrachloroethane 630-20-6 ND
1 1.2.2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 ND
Tetrahvdrofuran 109-99-9 ND
Toluene 108-88-3 ND
1 2 3-Trichlorobenzene 87-61-6 ND
1.2,4-Trichlorobenzene 120-82-1 ND
1.1.1-Trichloroethane 71-55-6 ND
1.1.2-Trichloroethane 79-00-5 ND
Trichloroethene 79-01-6 ND
Trichlorofluoromethane 75-69-4 ND
1.2.3-Trichloroorooane 96-18-4 ND
1.1 2-Trichlorotrifluoroethane 76-13-1 ND
1.2.4-Trimethvlbenzene 95-63-6 ND
1.3 5-Trimethylbenzene 108-67-8 ND
Vinyl acetate 108-05-4 ND
Vinvl chloride 75-01-4 ND
SECTION IV -Analytical Results -08/20/200 l l 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.109
0.0931
0.115
0.131
0.116
0.178
J 0.126
0.0801
1.59
0.140
0.0977
0.111
0.0870
0.144
0.900
0.0637
0.551
0.135
0.169
0.0821
0.137
0.106
0.288
0.123
0.124
0.0905
0.0948
0.114
Rl«"· cone ··· .. ,Flaa DL RL Cone Flaa· DL '• RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 I
0.000
0.000
0.000
0.000
Page 21 of 46
~-----------~---~--
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
surroaata .. c.omoound : <:: '. ' • y ,,.,~ , ,,, ·~ > ~: '' :·.
1-Bromo-4-fluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -08/20/200 l l 0:08
TRIP BLANK
2010810510
Aqueous
Received
NA
08/15/2001 00:00
08/15/2001 19:45
08/15/2001 19:45
1.0000
MSDA
ug/L
· '.%.Recoveiv·: · ·
99
107
102
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
Limits· ., F Ofo·Recoverv ·. Limits F -% Recoverv Limits F
77-117
61-143
87-113
Page 23 of 46
-~--------~--------
-~~--~---~~--------
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13047 Instrument Data File: A0815102.D
Instrument ID: MSDA Analyst: BJP
'Paribneter::: ~_:,L~ ··; :~: .. .. , !,:;;, f~f;~~ :~:Rerefinc'WN'ama~1
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone <MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1 3~butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroprooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1 2-Dibromo-3-chloroorooane 20
SECTION V -Calibration and QC Information -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
~·MEiasured cone -. :·F1aa. :.
21.l
172
101
107
20.8
18.7
20.7
19.l
16.2
20.1
23.8
21.6
20.9
20.5
15.7
20.5
21.8
19.1
21.7
20.6
22.2
21.8
16.2
20.2
19.9
19.l
Dateffime Analyzed:08/15/2001 17:22
Units: ug/L
· ::%Recoverv Flaa ·QC Limits %Recoverv .
105
172
101
107
104
93
103
96.
81
101
119
108
105
. 103
79
103
109
96
108
103 80-120
111
109
81 I
101
100
96
Page 24 of 46
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13047 Instrument Data File: A08I5102.D
Instrument ID: MSDA Analyst: BJP
Continued :e:a'tlrtieter·< ::~.'-~·.' · ;.,::,-'\< ,t, <.--•·Y;·:8}'. :,R&fer•n~awarua;; .;-,Measured :cone .
Dibromochloromethane 20
I .2-Dibromoethane 20
Dibromomethane 20
trans-I 4-Dichloro-2-butene 20
1.4-Dichlorobenzene 20
l 2-Dichlorobenzene 20
I 3-Dichlorobenzene 20
Dichlorodifluoromethane 20
1.1-Dichloroethane 20
1 2-Dichloroethane 20
1 1-Dichloroethene 20
cis-1.2-Dichloroethene 20
trans-I 2-Dichloroethene 20
1.2-Dichloroorooane 20
1.3-Dichloroorooane 20
2 2-Dichloroorooane 20
1.1-Dichloroorooene 20
cis-1.3-Dichloronrooene 20
trans-1.3-Dichloroorooene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1.3-butadiene 20
2-Hexanone 20
Iodomethane 20
Isooroovlbenzene 20
4-Isonronvltoluene 20
SECTION V -Calibration and QC lnfonnation -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
16.9
I9.5
20.4
13.4
I8.9
I8.7
19.l
22.7
22.5
20.3
22.5
21.2
21.5
21.3
18.9
22.0
21.3
17.3
17.3
19.5
19.9
21.6
22.3
25.l
20.4
21.4
Ffaa:. ..
Date!fime Analyzed:08/15/200I I 7:22
Units: ug/L
. %Rec0ve0i .'Flaa· : QC Limits %Rec6verv
85
98
102
67
94
93
95
114
112
101
112 80-120
106
107
107 80-120
95
110
107
87
86
98
99 80-120
108
111 I
125
102
107
Page 25 of 46
-~-------~---------
-~~----------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13047 Instrument Data File: A0815102.D
Instrument ID: MSDA Analyst: BJP
Continued ··Parameter.: .·::.·L~_ .. ·, .. ., .. · ,~:·: r ·:·. >Referenca1va11fi~~
Methvl methacrvlate 20
Methyl tert-butvl ether <MTBE) 20
4-Methvl-2-oentanone (MIBK) 20
Methvlene chloride 20
Naphthalene 20
Prooanenitrile 100
n-Proovlbenzene 20
Stvrene 20
L lJ 2-Tetrachloroethane 20
l.1.2 2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
l 2.3-Trichlorobenzene 20
l 2.4-Trichlorobenzene 20
1.1 I -Trichloroethane 20
1.1.2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
1.2 3-Trichloroorooane 20
1.1.2-Trichlorotrifluoroethane 20
1 2.4-Trimethvlbenzene 20
1 3.5-Trimethvlbenzene 20
Vinvl acetate 20
Vinvl chloride 20
o-Xvlene/m-Xvlene 40
SECTION V -Calibration and QC Information -08/20/200 I I 0:08
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
:;:Measured·conc .. ·Flaa·
21.0
21.5
21.8
21.0
18.3
121
20.6
19.9
20.2
20.4
17.6
23.5
19.7
18.5
19.8
22.5
18.4
21.8
21.9
20.9
24.6
19.9
20.l
22.5
22.0
40.7
Dateffime Analyzed:08/15/2001 17:22
Units: ug/L
,~%Recoverii Flaa QC Limits %Recoverv
105
108
109
105
91
121
103
99 -
101
102
88
117
98 80-120
93
99
113
92
109
109
104
123
100
100 I
112
110 80-120
102
Page 26 or 46
- -'-- -.. .. - - - - -
___ .. __ _
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW82608
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13047 Instrument Data File: A0815130.D
Instrument ID: MSDA Analyst: BJP
·. earameter.::::i:i:~::;~.:.iJ~~';:; :,; :f:~~;1:1~! ~iRifeieiU:~lu'i~·
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone <MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1 3-butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroprooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1 2-Dibromo-3-chloroorooane 20
SECTION V -Calibration and QC lnfonnation -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
f-?Measurecfconc .Flaa : .
22.1
168
91.7
106
20.5
19.3
21.0
21.5
20.2
19.6
27.4
20.7
20.3
20.3
20.6
21.7
21.6
19.1
21.5
20.6
21.2
21.5
20.5
19.2
19.5
19.1
..
Dateffime Analyzed:08/16/2001 06:32
Units: ug/L
._ ":%Re;coverJ t·F1aa · ·' :ac .Limits ·%Recoverv
111
168
92
106
102
97
105
107
101
98
137
103
102
101
103
109
108
96
107
103 80-120
106
107
103 I
96
98
96
Page 28 of 46
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13047 Instrument Data File: A0815130.D
Instrument ID: MSDA Analyst: BJP
Continued
P'aram·eter\··, .. ;·: ;.: . -:-: ·:. · .. Ret••t,nCSatvataa:::: . ·Measured Cone
Dibromochloromethane 20
1.2-Dibromoethane 20
Dibromomethane 20
trans-1.4-Dichloro-2-butene 20
l 4-Dichlorobenzene 20
1.2-Dichlorobenzene 20
1.3-Dichlorobenzene 20
Dichlorodifluoromethane 20
1 1-Dichloroethane 20
l 2-Dichloroethane 20
1.1-Dichloroethene 20
cis-1.2-Dichloroethene 20
trans-1.2-Dichloroethene 20
1.2-Dichloronronane 20
1.3-Dichlorooronane 20
2 2-Dichloronronane 20
1 1-Dichloronronene 20
cis-1.3-Dichloronronene 20
trans-1-3-Dichloronrooene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1.3-butadiene 20
2-Hexanone 20
Iodomethane 20
Isooronvlbenzene 20
4-Isonronvltoluene 20
SECTfON V -Calibration and QC Infonnation -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
20.l
20.1
20.7
18.7
18.9
19.0
19.1
21.5
23.2
21.0
21.1
20.7
20.8
21.7
20.2
16.4
21.4
20.l
19.2
20.1
19.8
21.2
22.2
22.8
20.0
20.2
.Flaa
Dateffime Analyzed:08/16/2001 06:32
Units: ug/L
. o/oRecoveni Flag QC Limits %Recoverv
100
101
103
93
94
95
95
108
116
105
106 80-120
103
104
108 80-120
101
82
107
100
96
100
99 80-120
106
111 I
114
100
101
Page 29 of 46
---------------~---
--~------------~---
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13047 Instrument Data File: A0815130.D
Instrument ID: MSDA Analyst: BJP
Continued
~~parameter:;~~>/~~~:~!~-:-~:"·;,:'~:/-:·-~-;.~:i~::~;. ~Referentatvam~;
Methvl methacrvlate 20
Methyl tert-butvl ether (MTBE) 20
4-Methvl-2-oentanone (MIBK) 20
Methylene chloride 20
Naohthalene 20
Prooanenitrile 100
n-Proovlbenzene 20
Stvrene 20
1 1 1.2-Tetrachloroethane 20
1.1 2.2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahydrofuran 20
Toluene 20
1 2.3-Trichlorobenzene 20
l 2.4-Trichlorobenzene 20
l l I -Trichloroethane 20
l, l 2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
1.2 3-Trichlorooronane 20
1.1 2-Trichlorotrifluoroethane 20
1.2 4-Trimethvlbenzene 20
1 3.5-Trimethylbenzene 20
Vinvl acetate 20
Vinyl chloride 20
n-Xvlene/m-Xylene 40
SECTION V -Calibration and QC lnfonnation -08/20/2001 I 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
1~Me·asurectConc ·Flaa·
21.3
20.7
22.7
21.4
19.3
115
19.5
19.6
20.2
18.9
28.2
24.9
19.4
19.6
19.7
21.3
19.3
21.8
21.l
21.6
23.4
19.7
19.9
12.8
21.4
39.5
"
Dateffime Analyzed:08/16/2001 06:32
Units: ug/L
: %Rec6ve'ni ;Flaa·· QC Limits %Recoverv . ·
106
103
113
107
96
115
98
98
101
94
141
125
97 80-120
98
98
107
97
109
105
108
117
99
100 I
64
107 80-120
99
Page 30 of 46
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
1027440
Method Blank
Aaueous
08/15/2001 19: 17
08/15/2001 19:17
MSDA
ug/L
::~-:.: ,~P,arilmetef;,:;_ "~.::.j_:~r,·; :c'::.;',!.:t: "1%3'.Bisr~~m .:.. ~-: > • ~<'l»; ~~!kt~ treon'ii~':'./F1aa: J:>L -:
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone (MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butvlbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 ND
Carbon tetrachloride 56-23-5 ND
2-Chloro-1.3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chloroethane 75-00-3 ND
Chloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
Chloromethane 74-87-3 ND
3-Chloronronene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
SECTION V -Calibration and QC Information -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
0.438
6.82
3.79
0.446
0.0641
0.0998
0.131
0.118
0.170
0.199
0.200
0.102
0.105
0.0911
0.0684
0.0652
0.114
0.0842
0.0925
0.0896
0.0938
0.127
0.0777
0.178
0.0974
, RL-'cone/ .Flaa DL RL __ Cone F.laa Dl 'RL
' 0.000
0.000
0.000
0.000
0.000
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 . 0.000
0.000
0.000
0.000
0.000 '
0.000 I
0.000
0.000
0.000
0.000
Page 34 of 46
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
"·. Pa·rameteii· :· '. ; ~ ·< \ , .. :' :· ;(,:2CAS!-~4t~~1,_~~:
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
1 3-Dichloroprooane 142-28-9
2 2-Dichloroorooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1 3-Dichloroprooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
Iodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether <MTBE) 1634-04-4
1027440
~cone:· ..
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -08/20/200110:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
Flaa DL · RL Cone 'Flaa DL · RL .Cone· Flaa. DL RL
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0.109 0.000 I
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
Page 35 of 46
-----------------;--
-----------------·---SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Continued
Method Blank ID 1027440
· ~i~~eara'm'eter;,~~~3;,0·f'·it.~:;~:,{~:. "~~ffOJrs~~z;9il~ v.,......,, .... j.)'!;,:;., ' tsonc:~,;:;:~?:~ ·Flaa··:,'.:oL . '•
4-Methvl-2-nentanone (MIBK) 108-10-1 ND
Methvlene chloride 75-09-2 ND
Naphthalene 91-20-3 ND
Pronanenitrile 107-12-0 ND
n-Proovlbenzene 103-65-1 ND
Stvrene 100-42-5 ND
l,l I 2-Tetrachloroethane 630-20-6 ND
1.1 2.2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 ND
Tetrahvdrofuran 109-99-9 ND
Toluene 108-88-3 ND
1.2.3-Trichlorobenzene 87-61-6 ND
1 2.4-Trichlorobenzene 120-82-1 ND
I I I -Trichloroethane 71-55-6 ND
I 1.2-Trichloroethane 79-00-5 ND
Trichloroethene 79-01-6 ND
Trichlorofluoromethane 75-69-4 ND
1.2 3-Trichlorooronane 96-18-4 ND
1 1.2-Trichlorotrifluoroethane 76-13-1 ND
1 2.4-Trimethvlbenzene 95-63-6 ND
1.3.5-Trimethvlbenzene 108-67-8 ND
Vinvl acetate 108-05-4 ND
Vinvl chloride 75-01-4 ND
o-Xvlene/m-Xvlene 106-42-3 ND
o-Xvlene 95-47-6 ND
SECTION V -Calibration and QC Information -08/20/200 I 10:08
LIMS Workorder: 80396910 (20108105] Hamilton Beach-Proctor Silex
STLAustin
0.178
0.126
0.0801
1.59
0.140
0.0977
0.111
0.0870
0.144
0.900
0.0637
0.551
0.135
0.169
0.0821
0.137
0.106
0.288
0.123
0.124
0.0905
0.0948
0.114
0.167
0.0844
:RL .; · · 'cone:·~"<: :;F.iaa: · ·oL · ~RL ., Cone Flaa .. ':. DL':•'\ . .RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 I
Page 36 of 46
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
1027440
Method Blank
Aaueous
08/15/2001 19: 17
08/15/2001 19:17
MSDA
ug/L
. surroaate:.comnound;: ·>·' i :.1~.t1''"·~~~~11ij1~~·Reci>verv:,·-..... !:':Um1ts
l-Bromo-4-fluorobenzene 101
1 2-Dichloroethane-d4 108
Toluene-d8 105
SECTION V -Calibration and QC Information -08/20/200 I 10:08
LIMS Workorder: 80396910 (20108105] Hamilton Beach-Proctor Silex
STLAustin
77-117
61-143
87-113
.. ,. .f . .'. :·%'·Recover'/'. limits F %Reco.verv; limits F
Page 37 of 46
--·---------------·--
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
',_ 't.
'·'
•' :~ <; v''
eanim~ter!: .
1 2-Dichlorobenzene
1.3-Dichlorobenzene
•,
'
Dichlorodifluoromethane
1.1-Dichloroethane
1 2-Dichloroethane
L 1-Dichloroethene
cis-1.2-Dichloroethene
trans-I 2-Dichloroethene
1 2-Dichloronrooane
l 3-Dichloronronane
2 2-Dichloroorooane
l 1-Dichloronrooene
cis-1.3-Dichloroorooene
trans-L3-Dichloroorooene
Ethvlbenzene
Hexachloro-1 3-butadiene
2-Hexanone
Iodomethane
Isonroovlbenzene
4-Isooroovltoluene
' . '
4-Methvl-2-oentanone (MIBK)
Methvlene chloride
Naohthalene
n-Proovlbenzene
Stvrene
I l 1.2-Tetrachloroethane
l 1.2.2-Tetrachloroethane
Tetrachloroethene
Toluene
123-Trichlorobenzene
1.2 4-Trichlorobenzene
., ·.· :~:;~£i)'.·n,,:.· .. 1 •• •
SECfION V • Calibration and QC Information -08/20/200 I I 0:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
Control Samnle continued
.Lag Ip: 1.027438
·File.ID: A0815103.D ,_,
.. snkAmt. ::cone. . · %Recfi'a ·
20 17.9 90
20 17.6 88
20 8.39 42
20 21.7 109
20 20.2 101
20 21.2 106
20 19.7 98
20 20.9 104
20 20.7 103
20 18.5 93
20 20.9 104
20 19.8 99
20 19.l 95
20 18.l 91
20 18.5 92
20 19.7 99
20 25.3 127
20 21.2 106
20 18.9 95
20 19.7 98
20 24.l 120
20 20.l 100
20 18.8 94
20 18.9 95
20 18.6 93
20 19.l 96
20 19.9 99
20 17.2 86
20 18.1 90
20 18.4 92
20 19.6 98
Control Samnle Dunhcate contmue d
·Lab ID: ' :,..., ' .1027439
. File ID: . A0815104.D QC L~mits
Sok.Amt Cone %Rec Fla RPO.Fla .. %Rec RPO
20 18.2 91 1.1 67-135 14
20 18.0 90 2.2 68-134 14
20 8.16 41 2.4 0.1-166 26
20 23.l 116 6.2 66-138 19
20 20.4 102 1 48-152 23
20 20.8 104 1.9 47-175 25
20 19.7 98 0 66-144 18
20 20.0 100 3.9 62-146 22
20 20.8 104 l 61-133 17
20 18.4 92 l.l 70-128 16
20 21.6 108 3.8 40-168 30
20 19.7 99 0 71-155 31
20 20.8 104 9 36-142 16
20 18.9 94 3.2 34-138 21
20 18.3 91 1.1 75-131 14
20 19.3 96 3.1 46-150 34
20 25.7 129 1.6 22-164 34
20 22.0 110 3.7
20 18.3 92 3.2 54-152 26
20 19.8 99 1 41-165 28
20 24.8 124 3.3 27-149 36
20 19.9 100 0 36-166 23
20 19.2 96 2.1 32-172 22
20 18.5 92 3.2 61-143 28
20 18.7 93 0 68-136 14
20 18.7 93 3.2 63-141 20
10 19.7 99 0 47-143 20
20 17.3 86 0 69-137 16
20 17.7 88 2.2 70-132 17
20 19.3 97 5.3 66-140 20
20 19.8 99 1 66-144 22
Page 39 of 46
--------~----------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Control Samole continued Control Samo e up 1cate con mue I D r r d
\'~~tfjji;;:~i.?'i)i\il-l~,[!ill}!~/103ii\3~, : < ' "'.~,~ID:, 1017439 .. , .. ·.. . . ·. ·.,, .. ,. . . .;::::z~, ·?';-~:,~:l'.•i!·r•:; ·•:n«-:·;:;."" ;;~( :nEile,,ID:;;,-,,-.:;;::A081.5103.ID': .. -~:·i'.~ .. ~•/,.,,;,;;Eale'.JD: .... , AOS.15104.Q,," ·. -, . · :.«. -:,; 1.c;;l,C..~i~!~S
J ';t~~ ..... ~. '.«'.:(·;.<.t• .. ,. ""'x'"" ""'$oi(;1(""f' _, '"C"" ~ ... ., .. ,..,? "o/c'R-,,~ Fl(fS""Stikl.( "'f 'f "c. ~· « • • • • 'o/c R Fia . .. RPO' Fla"'.. 'o/c Ree· . 'RPO '..~ ~arame ·'' ;,., r.;,.,-,.. '.~ 1« m ·\if~:' Jl:. one:."'°,~<.,·:. o ec;· . ., .. : i'. . m " ·one. , .:: .. o ec , '. ·:. '· o · · . ··
l I. I -Trichloroethane
l, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
l 2.3-Trichloroorooane
1,2 4-Trimethvlbenzene
L3 5-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
o-Xvlene/m-Xvlene
o-Xvlene
SECTION V -Calibration and QC Information -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
20
20
20
20
20
20
20
20
20
40
20
20.4 102 20
I6.4 82 20
20.l 100 20
16.6 83 20
20.l 100 20
18.6 93 20
19.5 98 20
6.58 33 20
I4.8 74 20
38.0 95 40
I8.0 90 20
20.9 104 1.9 49-I55 24
16.8 84 2.4 67-I35 17
20.0 100 0 71-129 17
16.4 82 1.2 39-I47 29
I9.9 99 l 64-I40 18
I8.3 92 1.1 54-156 25
I9.6 98 0 62-144 25
6.66 33 0 0.1-164 31
14.9 74 0 24-138 27
36.5 91 4.3 76-134 15
17.7 89 I.I 77-131 15
Page 40 of 46
-------------------SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 13047 Start Dateffime: 08/15/2001 17:22 Analyst:
Stop Dateffime: 08/16/2001 13:10
'f~,i;Y.J::·'·,.:;{:t~ .. :~;:·i;:.~:.: ~.· ... : .·.:··~;. : ... :,. ::;;.~ \<~·~ .. "~::::._:. ,., .. : «:' -: · .Samole Size.'_ · ·. -• <, :,·~~~~f+.~~~~:: <}jt; ·:;, .;'~:{, ,«.:i~~:\\~:3,: .,, : < ·s1 aliinre" !"?-'.:'..0; :.·': :~ ' ' '/)' •• ,N.,_,..._;,/~f:i,.. ·f1~"-;;;5 """'j~f'"'f·" ., ... ,.-:_, .. , .... :. 0 · .,-.-• ft.ft'""·"_.,.,~ ... ·~ .. "'· . ·r .. t""i "·'''"" ~'F·' .. , .... ,. ': a;: ·:1«~!!. am e~·voe-., :':.' .. :'«".::· arix~:-.:.-><· · : m1a~.: .. ,.r:. ma,.,,, ...
INSTRUMENT QC 1000
INSTRUMENT OC 1406
LCS for HBN 13047 fMSV/16211 1027438
LCSD for HBN 13047 fMSV/1621'1 1027439
MB for HBN 13047 fMSV/16211 1027440
TRIP BLANK 2010810510
0801HBWW230 2010810501
0801HBWW226 2010810502
0801HBWD998 2010810503
0801HBWW220 2010810504
0801HBWW224 2010810505
0801HBWW225 2010810506
0801HBWW234 2010810507
0801HBWW222 2010810508
0801HBWW216 2010810509 zzzzzzzzzz 2010809501 zzzzzzzzzz 2010809502
zzzzzzzzzz 2010809503
zzzzzzzzzz 2010809507
zzzzzzzzzz 2010809508
zzzzzzzzzz 2010809509
zzzzzzzzzz 2010809504
zzzzzzzzzz 2010809505
zzzzzzzzzz 2010809506
zzZ:Zzzzzzz 2010809510
INSTRUMENT OC 1000
INSTRUMENT QC 1406
zzzzzzzzzz 2010809510
SECTION VI -Batch Summaries -08/20/2001 10:08
LIMS Workorder: 80396910 [20108105] Hamilton Beach-Proctor Silex
STLAustin
GC/MS Tune
Continuing Calibration Check
Lab Control Samole
Lab Control Samole Dunlicate
Method Blank
Field Samnle
Field Sample
Field Samole
Field Samole
Field Samole
Field Samole
Field Sample
Field Samole
Field Samole
Field Sample
Field Samnle
Field Samnle
Field Samole
Field Samnle
Field Sample
Field Samole
Field Samole
Field Samole
Field Sample
Field Samole
GC/MS Tune
Continuing Calibration Check
Field Samole
Aaueous 15mL 15 mL
Aoueous 15mL 15mL
Aaueous 15 mL 15 mL
Aaueous 15 mL 15 mL
Aaueous 15 mL 15 mL
Aaueous 15mL 15 mL
Aoueous 15 mL 15 mL
Aaueous 15mL 15 mL
Aoueous 15 mL , 15 mL
Aaueous 15 mL 15 mL
Aaueous 15 mL 15 mL
Aoueous 15mL 15 mL
Aaueous 15mL 15 mL
Aaueous 15mL 15 mL
Aaueous 15mL 15 mL
Aaueous 15mL 15 mL
Aoueous 15 mL 15 mL
Aaueous 15mL 15 mL
Aoueous 15mL 15mL
Aaueous 15 mL 15 mL
Aoueous 15mL 15mL
Aaueous 15mL 15 mL
Aaueous 15mL 15 mL
Aaueods 15 mL 15 mL
Aaueous 15mL 15mL
Aoueous 15 mL 15 mL
Aoueous 15 mL 15 mL
Aaueous 15 mL 15 mL
BJP
«f>r~~~~ti'a~}M~tfi~~ .
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Page 42 of 46
-------------------SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 13047 Instrument ID: MSDA Analyst: BJP
: ·~: ~~i:~i::~ )·::.~~;~::; ~;;~:~~~~ -:, : ~ .. ~~~'' :?_/:'~~;~:--~:~iy~~'~ ~~~: :Seauenerh :1enent:siiam'D1aJ0::i:~Z£
, .. , ~~·.·. :._ , ~, · ' . ~An81VSi&~·. <:·/, .. ' ·_.; ~ · .·· -:_: . iii~ti~s~futi1~;io. ~·. Date.·~',,· ':c.'., tirrleJ.:,:;/;.(.;, '.·t.Samo1&,:fvs>e
..
· .. Arialvsis: File~·ID \, : •. 1
1 INSTRUMENT OC
2 INSTRUMENT OC
3 LCS forHBN 13047 fMSV/16211
4 LCSD for HBN 13047 fMSV/16211
5 MB for HBN 13047 fMSV/16211
6 TRIP BLANK
7 0801HBWW230
8 0801HBWW226
9 0801HBWD998
IO 0801HBWW220
11 0801HBWW224
12 0801HBWW225
13 0801HBWW234
14 0801HBWW222
15 0801HBWW216
16 zzzzzzzzzz
17 zzzzzzzzzz
18 zzzzzzzzzz
19 zzzzzzzzzz
20 zzzzzzzzzz
21 zzzzzzzzzz
22 zzzzzzzzzz
23 zzzzzzzzzz
24 zzzzzzzzzz
25 zzzzzzzzzz
26 INSTRUMENT OC
27 INSTRUMENT OC
28 zzzzzzzzzz
29 zzzzzzzzzz
SECTION VI -Batch Summaries -08/20/200 I I 0:08
LJMS Workorder: 80396910 [20108105) Hamilton Beach-Proctor Silex
STLAustin
1000 08/15/2001
1406 08/15/2001
1027438 08/15/2001
1027439 08/15/2001
1027440 08/15/2001
2010810510 08/15/2001
2010810501 08/15/2001
2010810502 08/15/2001
2010810503 08/15/2001
2010810504 08/15/2001
2010810505 08/15/2001
2010810506 08/15/2001
2010810507 08/15/2001
2010810508 08/15/2001
2010810509 08/15/2001
2010809501 08/16/2001
2010809502 08/16/2001
2010809503 08/16/2001
2010809507 08/16/2001
2010809508 08/16/2001
2010809509 08116/2001
2010809504 08/16/2001
2010809505 08/16/2001
2010809506 08/16/2001
2010809510 08/16/2001
1000 08/16/2001
1406 08/16/2001
2010809510 08/16/2001
2010809506 08/16/2001
17:22:00 GC/MS Tune A0815102
17:22:00 Continuing Calibration Check A0815102.D
17:52:00 Lab Control Sample A0815103.D
18:20:00 Lab Control Sample Duplicate A0815104.D
19:17:00 Method Blank A0815106.D
19:45:00 Field Sample A0815107.D
20:13:00 Field Sample A0815108.D
20:41:00 Field Sample A0815109.D
21:10:00 Field Samole A0815110.D
21 :38:00 Field Sample A081511 l.D
22:06:00 Field Sample A0815112.D
22:34:00 Field Samole A0815113.D
23:03:00 Field Sample A0815114.D
23:31:00 Field Sample A0815115.D
23:59:00 Field Sample A0815116.D
00:27:00 Field Sample A0815117.D
00:56:00 Field Sample A0815118.D
01:24:00 Field Sample A0815119.D
01:52:00 Field Samole A0815120.D
02:21:00 Field Sample A0815121.D
02:49:00 Field Sample A0815122.D
03:17:00 Field Sample A0815123.D
03:46:00 Field Sample A0815124.D
04:14:00 Field Samole A0815125.D
04:41:00 I Field Sample A0815126.D
06:32:00 GC/MS Tune A08r5130.D
06:32:00 Continuing Calibration Check A0815130.D
10:21:00 Field Sample A0815132.D
10:51:00 Field Samole A0815133.D
Page 44
Sub-
·Batch ID
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
of 46
--SECTION VII
Certifications
- --- -
state1Aaerrcv~:~~~~; ~ -~-~~: ~·~ ::.~:'.-;:~;~;,:.,:_}:.~~:,: '*;.~:~~~ff~~i~t«i v ·/~~,;~~-1
:.: ~'<-~. -~ ..
Arkansas Department of Environmental Quality
- - -
..
''
California Environmental Laboratorv Accreditation Program I Waste Water/Hazardous Waste
Connecticut Department of Health/Waste Water/Trade Waste, Sewage/Effluent Soil
Florida Department of Environmental Protection. ComnOAP
Kansas Deoartment of Health and Environment I Solid and Hazardous Waste
-
"
'.
Louisiana Department of Environmental Quality, ELAP I Waste Water/Hazardous Waste/Air Emissions
Montana Department of Environmental Quality/Petroleum Release Section
New Jersey Department of Environmental Protection
New York State Department of Health /Waste Water/Hazardous Waste/Air
North Carolina Dept. of Natural Resources & Community Development I Waste Water
Oklahoma Department of Environmental Quality/General Water Qualitv/Sludge
Rhode Island Department of Health/Potable Water/Non-Potable and Waste Water
South Carolina Dept. of Health & Environmental Control
Tennessee UST
Texas(TNRCC)
Texas Department of Public Safety/Precursor Chemical and Lab Aooaratus
Utah Department of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources
US AirForce/AFCEE
US Armv Coros of Engineers (MRD.ACE)
US Department of Agriculture I Restricted Soils Permit
US Navv<NFESC)
SECTION VII -Certifications -08/20/200 I I 0:08
LIMS Workorder: 80396910 (20108105) Hamilton Beach-Proctor Silex
STLAustin
- - - - - - - -
•, -ID#
2411
PH-0761
QA Plan #900481
E-10165
Interim Accreditation
82005
10915
302
8720
127
82003
Participating Laboratorv
3039
RADC
999885260
Particioating Laboratorv
Participating Laboratorv
S-42350
Participating Laboratorv
Page 46 of 46
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
, ---earametef -
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
;
Bromochloromethane
.Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
-
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
; , OAS_',:._ ,, . "
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWD999
2010811602
Aaueous
Received
NA
08/15/2001 09:10
08/20/2001 17:29
08/20/2001 17:29
1.0000
MSDA
mdL
_,Con~•-.. flaa
ND
ND
ND
ND
0.335 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.722
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
D.L. ---Rt
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0801HBWD999 0801HBWW213
2010811602 2010811604
Aaueous Aaueous
Received Received
NA NA
08/15/2001 09:10 08/15/2001 09:35
08/2112001 03:57 08/20/2001 18:56
08/21/2001 03:57 08/20/2001 18:56
5.0000 10.0000
MSDA MSDA
ug/L ug/L
Cone Flad DL: ·. .RL Cone Flaa :DL -RL.-·
ND 2.19 0.000 ND 4.38 0.000
ND 34.l 0.000 ND 68.2 0.000
ND 19.0 0.000 ND 37.9 0.000
ND 2.23 0.000 ND 4.46 0.000
ND 0.320 0.000 ND 0.641 0.000
ND 0.499 0.000 ND 0.998 0.000
ND 0.655 0.000 ND 1.31 0.000
ND 0.590 0.000 ND 1.18 0.000
ND 0.850 0.000 ND 1.70 0.000
ND 0.995 0.000 ND 1.99 0.000
ND 1.00 0.000 ND 2.00 0.000
ND 0.510 0.000 ND 1.02 0.000
ND 0.525 0.000 ND 1.05 0.000
ND 0.456 0.000 ND 0.911 0.000
ND 0.342 0.000 ND 0.684 0.000
ND 0.326 0.000 ND 0.652 0.000
ND 0.570 0.000 ND 1.14 0.000
ND 0.421 0.000 ND 0.842 0.000
ND 0.462 0.000 ND 0.925 0.000
ND 0.448 0.000 ND 0.896 0.000
ND 0.469 0.000 ND 0.938 0.000
Page 4 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
,C'AS
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene '541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloroprooane 78-87-5
1 3-Dichloroorooane 142-28-9
2.2-Dichforopropane 594-20-7
1.1-Dichloroorooene 563-58-6
'.
cis-1.3-Dichloropropene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWD999
2010811602
,Cone Flaa,
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
157 ER
0.590
16.0
11.8
0.692
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
0.237
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.136
0.331
0.169
0801HBWD999 0801HBWW213
2010811602 2010811604
Rl Cone Flaa DL, RL Cone, Flaa, DL RL
0.000 ND 0.635 0.000 ND 1.27 0.000
0.000 ND 0.388 0.000 ND 0.777 0.000
0.000 ND 0.890 0.000 ND 1.78 0.000
0.000 ND 0.487 0.000 ND 0.974 0.000
0.000 ND 2.74 0.000 ND 5.48 0.000
0.000 ND 0.700 0.000 ND 1.40 0.000
0.000 ND 0.685 0.000 ND 1.37 0.000
0.000 ND 0.740 0.000 ND 1.48 0.000
0.000 ND 3.90 0.000 ND 7.80 0.000
0.000 ND 0.750 0.000 ND 1.50 0.000
0.000 ND 0.482 0.000 ND 0.965 0.000
0.000 ND 0.423 0.000 ND 0.846 0.000
0.000 ND 1.18 0.000 ND 2.37 0.000
0.000 143 0.620 0.000 137 1.24 0.000
0.000 ND 0.510 0.000 ND 1.02 0.000
0.000 15.6 0.610 0.000 396 1.22 0.000
0.000 11.1 0.560 0.000 38.9 1.12 0.000
0.000 ND 0.595 0.000 ND 1.19 0.000
0.000 ND 0.434 0.000 ND 0.869 0.000
0.000 ND 0.675 0.000 ND 1.35 0.000
0.000 ND 0.800 0.000 ND 1.60 0.000
0.000 ND 0.497 0.000 ND 0.994 0.000
0.000 ND 0.409 0.000 ND 0.818 0.000
0.000 ND 0.454 0.000 ND 0.908 0.000
0.000 ND 0.505 0.000 ND 1.01 0.000
0.000 ND 0.680 0.000 ND 1.36 0.000
0.000 ND 1.66 0.000 ND 3.3 I 0.000
0.000 ND 0.845 0.000 ND 1.69 0.000
Page 5 of 67
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
· . ·Barameter ~ ' . . .. ,.,G!S,i:. ;.~·::-· -,-... ,,':,
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1.1.1 2-Tetrachloroethane 630-20-6
1, 1 2,2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
l 2 3-Trichlorobenzene 87-61-6
124-Trichlorobenzene 120-82-1
1 1 I -Trichloroethane 71-55-6
1 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2,3-Trichloropropane 96-18-4
1 1.2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1 3.5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWD999
2010811602
;'Cone .. , flaa.
ND
ND
ND
ND
ND
ND
0.179 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.343 J
ND
ND
ND
ND
ND
ND
11.9
LIMS Workorder: 80396910[20108I16] Hamilton Beach-Proctor Silex
STLAustin
DL RL·
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
0801HBWD999 0801HBWW213
2010811602 2010811604
; Cone .. Flaa·· DL , . . ·RL. .. :cone· Flaa .. ;oL_,'. .: .. ~: Rl· .. .. . .
ND 0.545 0.000 ND 1.09 0.000
ND 0.466 0.000 ND 0.931 0.000
ND 0.575 0.000 ND 1.15 0.000
ND 0.655 0.000 ND 1.31 0.000
ND 0.580 0.000 ND 1.16 0.000
ND 0.890 0.000 ND 'J.78 0.000
ND 0.630 0.000 ND t.26 0.000
ND 0.400 0.000 ND 0.801 0.000
ND 7.95 0.000 ND 15.9 0.000
ND 0.700 0.000 ND 1.40 0.000
ND 0.488 0.000 ND 0.977 0.000
ND 0.555 0.000 ND 1.11 0.000
ND 0.435 0.000 ND 0.870 0.000
ND 0.720 0.000 21.7 1.44 0.000
ND 4.50 0.000 ND 9.00 0.000
ND 0.318 0.000 ND 0.637 0.000
ND 2.76 0.000 ND 5.51 0.000
ND 0.675 0.000 ND 1.35 0.000
ND 0.845 0.000 3.76 J 1.69 0.000
ND 0.410 0;000 ND 0.821 0.000
ND 0.685 0.000 449 1.37 0.000
ND 0.530 0.000 ND 1.06 0.000
ND 1.44 0.000 ND 2.88 0.000
ND 0.615 0.000 ND 1.23 0.000
ND 0.620 0.000 ND 1.24 0.000
ND 0.452 0.000 ND 0.905 0.000
ND 0.474 0.000 ND 0.948 0.000
11.0 0.570 0.000 17.4 l.14 0.000
Page 6 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results-09/04/2001 14:52
0801HBWD999
2010811602
Cone Fi a a
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.167 0.000
0.0844 0.000
0801HBWD999 0801HBWW213
2010811602 2010811604
Cone Flaa DL RL Cone Flaa DL RL
ND 0.835 0.000 ND 1.67 0.000
ND 0.422 0.000 ND 0.844 0.000
Page 7 of 67
-------------------
-~--~-------------­SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SurroaatttCoinoound :. ,_ .. '~, '
, >
l-Bromo-4-fluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWD999
2010811602
AQueous
Received
NA
08/15/2001 09:10
08/20/2001 17:29
08/20/2001 17:29
1.0000
MSDA
u!!IL
. • •.· % Re.co.verv
97
105
101
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
. Limits ff
77-117
61-143
87-113
0801HBWD999 0801HBWW213
2010811602 2010811604
AQueous AQueous
Received Received
NA NA
08/15/2001 09:10 08/15/2001 09:35
08/21/2001 03:57 08/20/2001 18:56
08/2112001 03:57 08/20/2001 18:56
5.0000 10.0000
MSDA MSDA
ug/L ug/L
%Recovew · Limit&. » F-. o/o Recove·rv· ·Limits· , . F .~. ., .
98 77-117 100 77-117
103 61-143 105 61-143
101 87-113 101 87-113
Page 8 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW213
2010811604
Aqueous
Received
NA
08/15/2001 09:35
08/21/2001 04:25
08/21/2001 04:25
5.0000
MSDA
ug/L
Cone Flaa.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
DL
2.19
34.1
19.0
2.23
0.320
0.499
0.655
0.590
0.850
0.995
1.00
0.510
0.525
0.456
0.342
0.326
0.570
0.421
0.462
0.448
0.469
0801HBWW214 0801HBWW214
2010811601 2010811601
Aqueous Aqueous
Received Received
NA NA
08/15/2001 09:05 08/15/2001 09:05
08/20/2001 18:26 08/21/2001 04:54
08/20/2001 18:26 08/21/2001 04:54
5.0000 2.0000
MSDA MSDA
ug/L ug/L
RL Cone Flaa DL RL Cone· Flaa DL RL ·
0.000 ND 2.19 0.000 ND 0.876 0.000
0.000 ND 34.1 0.000 ND 13.6 0.000
0.000 ND 19.0 0.000 ND 7.58 0.000
0.000 ND 2.23 0.000 ND 0.892 0.000
0.000 0.376 J 0.320 0.000 0.395 J 0.128 0.000
0.000 ND 0.499 0.000 ND 0.200 0.000
0.000 ND 0.655 0.000 ND 0.262 0.000
0.000 ND 0.590 0.000 ND 0.236 0.000
0.000 ND 0.850 0.000 ND 0.340 0.000
0.000 ND 0.995 0.000 ND 0.398 0.000
0.000 ND 1.00 0.000 ND 0.400 0.000
0.000 ND 0.510 0.000 ND 0.204 0.000
0.000 ND 0.525 0.000 ND 0.210 0.000
0.000 ND 0.456 0.000 ND 0.182 0.000
0.000 ND 0.342 0.000 ND 0.137 0.000
0.000 ND 0.326 0.000 ND 0.130 0.000
0.000 ND 0.570 0.000 ND 0.228 0.000
0.000 ND 0.421 0.000 ND 0.168 0.000
0.000 ND 0.462 0.000 ND 0.185 0.000
0.000 ND 0.448 0.000 ND 0.179 0.000
0.000 ND 0.469 0.000 ND 0.188 0.000
Page 9 of 67 -... - - - - - - - - -.. - - - - - -·-
---------~---------SECTION IV
Analytical Results
MS-VOA
SW82608
Continued
· · ~·. :Parameter .. ·
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
.. ' · ;: ;e.A.s:~,.: .. _; :-·~
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l. l-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichlorooropane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroprooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1,3-Dichloroorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW213
2010811604
:>Gone . ' Fiaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
128
3.09
405
37.4
1.30 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL RL ·
0.635 0.000
0.388 0.000
0.890 0.000
0.487 0.000
2.74 0.000
0.700 0.000
0.685 0.000
0.740 0.000
3.90 0.000
0.750 0.000
0.482 0.000
0.423 0.000
l.18 0.000
0.620 0.000
0.510 0.000
0.610 0.000
0.560 0.000
0.595 0.000
0.434 0.000
0.675 0.000
0.800 o,ooo
0.497 0.000
0.409 0.000
0.454 0.000
0.505 0.000
0.680 0.000
1.66 0.000
0.845 0.000
0801HBWW214 0801HBWW214
2010811601 2010811601
Cone ·Flaa· ·-DL RL. Cone :Flaa·· ·.ot:;·'··· .· RL·
ND 0.635 0.000 ND 0.254 0.000
ND 0.388 0.000 ND 0.155 0.000
ND 0.890 0.000 ND 0.356 0.000
ND 0.487 0.000 ND 0.195 0.000
ND 2.74 0.000 ND 1.10 0.000
ND 0.700 0.000 ND 0.280 0.000
ND 0.685 0.000 ND ~--<l'.274 0.000
ND 0.740 0.000 ND --:0.296 0.000
ND 3.90 0.000 ND 1.56 0.000
ND 0.750 0.000 ND 0.300 0.000
ND 0.482 0.000 ND 0.193 0.000
ND 0.423 0.000 ND 0.169 0.000
ND l.18 0.000 ND 0.474 0.000
153 0.620 0.000 143 0.248 0.000
ND 0.510 0.000 ND 0.204 0.000
15.6 0.610 0.000 16.7 -0.244 0.000
11.5 0.560 0.000 11.7 0.224 0.000
0.444 u 0.595 0.000 0.578 J 0.238 0.000
ND 0.434 0.000 ND 0.174 0.000
ND 0.675 0.000 ND 0.270 0.000
ND 0.800 0.000 ND 0.320 0.000
ND 0.497 0.000 ND 0.199 0.000
ND 0.409 0.000 ND 0.164 0.000
ND 0.454 0.000 ND 0.182 0.000
ND 0.505 0.000 ND 0.202 0.000
ND 0.680 0.000 ND 0.272 0.000
ND 1.66 0.000 ND 0.662 0.000
ND 0.845 0.000 ND 0.338 0.000
Page 10 of 67
·~
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter .OAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-Isoproovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) I634-04-4
4-Methvl-2-oentanone (MIBK) 108-IO-l
Methylene chloride 75-09-2
Naohthalene 91-20-3
Propanenitrile 107-I2-0
n-Proovlbenzene I03-65-1
Stvrene 100-42-5
l 1.1 2-Tetrachloroethane 630-20-6
I, I ,2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-I8-4
Tetrahvdrofuran I09-99-9
Toluene 108-88-3
I 2.3-Trichlorobenzene 87-6I-6
1 2,4-Trichlorobenzene 120-82-1
I I. I -Trichloroethane 71-55-6
I I .2-Trichloroethane 79-00-5
Trichloroethene 79-0I-6
Trichlorofluoromethane 75-69-4
1 2 3-Trichloroorooane 96-18-4
I, I 2-Trichlorotrifluoroethane 76-I3-I
1.2 4-Trimethvlbenzene 95-63-6
1,3 ,5-Trimethylbenzene 108-67-8
Vinvl acetate I08-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/04/2001 14:52
080IHBWW2I3
20108II604
,·.Cone Flaa
ND
ND
ND
ND
ND
ND
ND
8.56
ND
ND
ND
ND
ND
23.9
ND
ND
ND
ND
4.29
1.92 J
467
ND
ND
ND
ND
ND
ND
I7.4
LIMS Workorder: 803969!0[20!08116] Hamilton Beach-Proctor Silex
STLAustin
DL
0.545
0.466
0.575
0.655
0.580
0.890
0.630
0.400
7.95
0.700
0.488
0.555
0.435
0.720
4.50
0.3I8
2.76
0.675
0.845
0.410
0.685
0.530
1.44
0.6I5
0.620
0.452
0.474
0.570
0801HBWW2I4 080IHBWW2I4
201081160I 20108I I60I
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.545 0.000 ND 0.2I8 0.000
0.000 ND 0.466 0.000 ND O.I86 0.000
0.000 ND 0.575 0.000 ND 0.230 0.000
0.000 ND 0.655 0.000 ND 0.262 0.000
0.000 ND 0.580 0.000 ND 0.232 0.000
0.000 ND 0.890 0.000 ND 0.356 0.000
0.000 ND 0.630 0.000 O.I92 u 0.252 0.000
0.000 ND 0.400 0.000 ND 0.160 0.000
0.000 ND 7.95 0.000 ND 3.I8 0.000
0.000 ND 0.700 0.000 ND 0.280 0.000
0.000 ND 0.488 0.000 ND O.I95 0.000
0.000 ND 0.555 0.000 ND 0.222 0.000
0.000 ND 0.435 0.000 ND 0.174 0.000
0.000 ND 0.720 0.000 ND 0.288 0.000
0.000 ND 4.50 0.000 ND 1.80 0.000
0.000 ND 0.318 0.000 ND O.I27 0.000
0.000 ND 2.76 0.000 ND 1.10 0.000
0.000 ND 0.675 0.000 ND 0.270 0.000
0.000 ND 0.845 0.000 ND 0.338 0.000
0.000 ND 0.410 0.000 ND O.I64 0.000
0.000 ND 0.685 0.000 0.357 J 0.274 0.000
0.000 ND 0.530 0.000 ND 0.212 0.000
0.000 ND 1.44 0.000 ND 0.576 0.000
0.000 ND 0.6I5 0.000 ND 0.246 0.000
0.000 ND 0.620 0.000 ND 0.248 0.000
0.000 ND 0.452 0.000 ND 0.18I 0.000
0.000 ND 0.474 0.000 ND 0.190 0.000
0.000 10.8 0.570 0.000 I 1.6 0.228 0.000
Page 11 of 67
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
. Parameter .
n-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
'' ·--A. -.:·,C,'S.· ..
106-42-3
95-47-6
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW213
2010811604
_'/_ _Cone· ·.Flaa . ,,,· /'
ND
0.715 J
LIMS Workorder: 80396910 [20 I 08116] Hamilton Beach-Proctor Silex
STLAustin
DL
0.835
0.422
0801HBWW214 0801HBWW214
2010811601 2010811601
RL Cone Flaa DL RL .. Cone Flaa ··DL .. .. Rl'
0.000 ND 0.835 0.000 ND 0.334 0.000
0.000 ND 0.422 0.000 ND 0.169 0.000
Page 12 of 67
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Compound
1-Bromo-4-fluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW213
2010811604
Aaueous
Received
NA
08/15/2001 09:35
08/21/2001 04:25
08/21/2001 04:25
5.0000
MSDA
ug/L
%ReCOV81'.V
99
107
100
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0801HBWW214 0801HBWW214
2010811601 2010811601
Aaueous Aqueous
Received Received
NA NA
08/15/2001 09:05 08/15/2001 09:05
08/20/2001 18:26 08/21/2001 04:54
08/20/2001 18:26 08/21/2001 04:54
5.0000 2.0000
MSDA MSDA
ug/L ug/L
%Recovery Limits F %Recovery Limits ,f
100 77-117 94 77-117
106 61-143 106 61-143
104 87-113 104 87-113
Page 13 of 67
-------------------
-------~-----------SECTION IV
Analytical Results
MS-VOA
SW8260B
J~arameter.J · .: ·
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
"
Bromochloromethane
;
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
.,
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
;.'. '' < '' ' •, · ... :: .. ·.cAs.··
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW215
2010811603
Aaueous
Received·
NA
08/15/2001 09:20
08/20/2001 17:58
08/20/2001 17:58
1.0000
MSDA
m!IL
:cone.· : Flaa.: DL
ND 0.438
ND 6.82
ND 3.79
ND 0.446
0.142 J 0.0641
ND 0.0998
ND 0.131
ND 0.118
ND 0.170
ND 0.199
ND 0200
ND 0.102
ND 0.105
ND 0.0911
ND 0.0684
ND 0.0652
ND 0.114
ND 0.0842
ND 0.0925
ND 0.0896
ND 0.0938
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
'R,t_:<, "
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0801HBWW215 0801HBWW227
2010811603 2010811605
Aqueous Aqueous
Received Received
NA NA
08/15/2001 09:20 08/15/2001 09:55
08/21/2001 03:29 08/20/2001 19:26
08/21/2001 03:29 08/20/2001 19:26
1.0000 50.0000
MSDA MSDA
ug/L U!!:/l
.cone· " Flaa OL RL " Coric . Flaa 'bl ~ " RL'·~: ·.
ND 0.438 0.000 ND 21.9 0.000
ND 6.82 0.000 ND 341 0.000
ND 3.79 0.000 ND 190 0.000
ND 0.446 0.000 ND 22.3 0.000
0.185 J 0.0641 0.000 ND 3.20 0.000
ND 0.0998 0.000 ND 4.99 0.000
ND ·o.131 0.000 ND 6.55 0.000
ND 0.118 0.000 ND 5.90 0.000
ND 0.170 0.000 ND 8.50 0.000
ND 0.199 0.000 ND 9.95 0.000
ND 0.200 0.000 ND 10.0 0.000
ND 0.102 0.000 ND 5.10 0.000
ND 0.105 0.000 ND 5.25 0.000
ND 0.0911 0.000 ND 4.56 0.000
ND 0.0684 0.000 ND 3.42 0.000
ND 0.0652 0.000 ND 3.26 0.000
ND 0.114 0.000 ND 5.70 0.000
ND 0.0842 0.000 ND 4.21 0.000
ND 0.0925 0.000 62.6 4.62 0.000
ND 0.0896 0.000 ND 4.48 0.000
ND 0.0938 0.000 ND 4.69 0.000
Page 14 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
, , _Parameter , CAS -' ~ ' , . ,
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1,4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I, 1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
• 1 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW215
2010811603
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.72 v
ND
3.48
0.0775 u
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
0801HBWW215 0801HBWW227
2010811603 2010811605
DL RL Cone Flaa DL RL Cone _Flaa DL 'R.L
0.127 0.000 ND 0.127 0.000 ND 6.35 0.000
0.0777 0.000 ND 0.0777 0.000 ND 3.88 0.000
0.178 0.000 ND 0.178 0.000 ND 8.90 0.000
0.0974 0.000 ND 0.0974 0.000 ND 4.87 0.000
0.548 0.000 ND 0.548 0.000 ND 27.4 0.000
0.140 0.000 ND 0.140 0.000 ND 7.00 0.000
0.137 0.000 ND 0.137 0.000 ND 6.85 0.000
0.148 0.000 ND 0.148 0.000 ND 7.40 0.000
0.780 0.000 ND 0.780 0.000 ND 39.0 0.000
0.150 0.000 ND 0.150 0.000 ND 7.50 0.000
0.0965 0.000 ND 0.0965 0.000 ND 4.82 0.000
0.0846 0.000 ND 0.0846 0.000 ND 4.23 0.000
0.237 0.000 ND 0.237 0.000 ND 11.8 0.000
0.124 0.000 5.16 0.124 0.000 3410 6.20 0.000
0.102 0.000 ND 0.102 0.000 23.7 J 5.10 0.000
0.122 0.000 3.67 0.122 0.000 855 6.10 0.000
0.112 0.000 0.116 J 0.112 0.000 514 5.60 0.000
0.119 0.000 ND 0.119 0.000 8.66 J 5.95 0.000
0.0869 0.000 ND 0.0869 0.000 ND 4.34 0.000
0.135 0.000 ND 0.135 0.000 ND 6.75 0.000
0.160 0.000 ND 0.160 0.000 ND 8.00 0.000
0.0994 0.000 ND 0.0994 0.000 ND 4.97 0.000
0.0818 0.000 ND 0.0818 0.000 ND 4.09 0.000
0.0908 0.000 ND 0.0908 0.000 ND 4.54 0.000
0.101 0.000 ND 0.101 0.000 ND 5.05 0.000
0.136 0.000 ND 0.136 0.000 ND 6.80 0.000
0.331 0.000 ND 0.331 0.000 ND 16.6 0.000
0.169 0.000 ND 0.169 0.000 ND 8.45 0.000
Page 15 of 67
-------~-----------
--~----------------SECTION IV
Analytical Results
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Continued
·_. : Parameter· · · ; ,._· · · ,_.,,_ ,,.~·.,cAs~· .:
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 9I-20-3
Prooanenitrile 107-I2-0
n-Proovlbenzene 103-65-1
Stvrene I00-42-5
I. I 1 2-Tetrachloroethane 630-20-6
I I 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-I8-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
1 2 4-Trichlorobenzene 120-82-1
1 1 I -Trichloroethane 71-55-6
1 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2,3-Trichloroorooane 96-I8-4
I I 2-Trichlorotrifluoroethane 76-13-I
1 2 4-Trimethvlbenzene 95-63-6
1,3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW215
2010811603
,/.j ~<Oonc· • . :r=1aa
ND
ND
ND
ND
ND
ND
1.05 J
ND
ND
ND
ND
ND
ND
ND
ND
0.228 J
ND
ND
2.26
ND
0.242 J
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
.DL
0.109
0.0931
0.115
0.131
0.116
O.I78
0.126
0.080I
1.59
O.I40
0.0977
O.I l I
0.0870
O.I44
0.900
0.0637
0.551
0.135
0.169
0.0821
0.137
0.106
0.288
O.I23
0.124
0.0905
0.0948
0.114
0801HBWW215 0801HBWW227
2010811603 2010811605
Ri. .. cone'. Flaa. DL RL, .Cone : Fiaa '-.DL·· · '..:RL.-.-..
0.000 ND 0.109 0.000 ND 5.45 0.000
0.000 ND 0.0931 0.000 ND 4.66 0.000
0.000 ND 0.115 0.000 ND 5.75 0.000
0.000 ND 0.13I 0.000 ND 6.55 0.000
0.000 ND O.l I6 0.000 ND 5.80 0.000
0.000 ND O.I78 0.000 ND 8.90 0.000
0.000 0.686 J 0.126 0.000 ND 6.30 0.000
0.000 ND 0.080I 0.000 ND 4.00 0.000
0.000 ND 1.59 0.000 ND 79.5 0.000
0.000 ND 0.140 0.000 ND 7.00 0.000
0.000 ND 0.0977 0.000 ND 4.88 0.000
0.000 ND 0.111 0.000 ND 5.55 0.000
0.000 ND 0.0870 0.000 ND 4.35 0.000
0.000 ND 0.144 0.000 ND 7.20 0.000
0.000 ND 0.900 0.000 ND 45.0 0.000
0.000 ND 0.0637 0.000 25.7 3.I8 0.000
0.000 ND 0.551 0.000 ND 27.6 0.000
0.000 ND 0.135 0.000 ND 6.75 0.000
0.000 2.54 0.169 0.000 4480 8.45 0.000
0.000 ND 0.082I 0.000 ND 4.10 0.000
0.000 0.333 J 0.137 0.000 112 6.85 0.000
0.000 ND 0.106 0.000 ND 5.30 0.000
0.000 ND 0.288 0.000 ND 14.4 0.000
0.000 ND O.I23 0.000 ND 6.I5 0.000
0.000 ND O.I24 0.000 ND 6.20 0.000
0.000 ND 0.0905 0.000 ND 4.52 0.000
0.000 ND 0.0948 0.000 ND 4.74 0.000
0.000 ND O.I 14 0.000 ND 5.70 0.000
Page 16 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
, . Parameter
p-Xvlene/m-Xvlene
o-Xvlene
''
Client Sample ID
Lab Sample ID
: : ... CA$ ...
106-42-3
95-47-6
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW215
2010811603
"I, ·.Cone Flaa
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL RL.
0.167 0.000
0.0844 0.000
0801HBWW215 0801HBWW227
2010811603 2010811605
Cone Flaa · DL RL Cone Flaa Jll' · .. RL.
ND 0.167 0.000 ND 8.35 0.000
ND 0.0844 0.000 ND 4.22 0.000
Page 17 of 67
--~----~-----------
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
-sws2sos
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
· · .Surroaate Compound:::. " ,, ,. . " • ·~ 'y": ~:
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW215
2010811603
Aqueous
Received
NA
08/15/2001 09:20
08/20/2001 17:58
08/20/2001 17:58
1.0000
MSDA
ug/L
· : % Recover1
95
105
102
LIMS Workorder: 80396910 [20!08116] Hamilton Beach-Proctor Silex
STLAustin
Limits. '•'
77-117
61-143
87-113
0801HBWW215 0801HBWW227
2010811603 2010811605
Aqueous Aqueous
Received Received
NA NA
08/15/2001 09:20 08/15/2001 09:55
08/21/2001 03 :29 08/20/2001 19:26
08/21/2001 03 :29 08/20i2001 19:26
1.0000 50.0000
MSDA MSDA
u!!IL u!!IL
F % Recoves:v Limits F % Recoverv· . limits ,,• f:'··
100 77-117 99 77-117
104 61-143 96 61-143
102 87-113 101 87-113
Page 18 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameier
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
" CAS ''' ..
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW227
2010811605
Aaueous
Received
NA
08/15/2001 09:55
08/27/2001 21 :25
08/27/2001 21 :25
5.0000
MSDB
ug/L
·Cone Flaa
34.7 F
ND
ND
ND
0.978 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
63.4
1.83 J
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
.. bL
10.7
40.1
'6.87
0.642
0.200
0.500
0.540
0.374
0.909
0.768
24.0
0.334
0.328
0.399
0.341
0.508
0.666
0.356
0.555
0.553
0.618
0801HBWW228 0801HBWW228
2010811606 2010811606
AQueous AQueous
Received Received
NA NA
08/15/2001 10:05 08/15/2001 10:05
08/20/2001 20:24 08/27/2001 20:56
08/20/2001 20:24 08/27/2001 20:56
1000.0000 50.0000
MSDA MSDB
ug/L ug/L
. RL Cone Flaa DL RL Cone. Flaa oL. RL
0.000 ND 438 0.000 638 107 0.000
0.000 ND 6820 0.000 ND 401 0.000
0.000 ND 3790 0.000 ND 68.7 0.000
0.000 ND 446 0.000 ND 6.42 0.000
0.000 ND 64.1 0.000 43.9 2.00 0.000
0.000 ND 99.8 0.000 ND 5.00 0.000
0.000 ND 131 0.000 ND 5.40 0.000
0.000 ND 118 0.000 ND 3.74 0.000
0.000 ND 170 0.000 ND 9.09 0.000
0.000 ND 199 0.000 ND 7.68 0.000
0.000 ND 200 0.000 548 240 0.000
0.000 ND 102 0.000 23.9 J 3.34 0.000
0.000 ND 105 0.000 ND 3.28 0.000
0.000 ND 91.1 0.000 ND 3.99 0.000
0.000 ND 68.4 0.000 ND 3.41 0.000
0.000 ND 65.2 0.000 27.6 5.08 0.000
0.000 ND 114 0.000 ND 6.66 0.000
0.000 ND 84.2 0.000 ND 3.56 0.000
0.000 ND 92.5 0.000 119 5.55 0.000
0.000 ND 89.6 0.000 9.82 J 5.53 0.000
0.000 ND 93.8 0.000 ND 6.18 0.000
Page 19 of 67
-------------------
--~------------~--­SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
· : · Parameter ·
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
< < < . ·1.cAs.': .. ,,.: . ·;.:;
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1,3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethylbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/04/200I I4:52
0801HBWW227
2010811605
~;Coner. ·Fiaa·
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1880 ER
25.2
844 ER
456
8.97
ND
ND
ND
ND
ND
ND
ND
0.784 J
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
·.oL·· RL
0.522 0.000
0.309 0.000
0.509 0.000
0.361 0.000
5.20 0.000
0.467 0.000
0.356 0.000
0.516 0.000
7.29 0.000
0.334 0.000
0.503 0.000
0.320 0.000
1.33 0.000
0.232 0.000
0.543 0.000
0.578 0.000
0.442 0.000
0.370 0.000
0.402 0.000
0.208 0.000
0.550 0.000
0.385 0.000
0.600 0.000
0.517 0.000
0.734 0.000
0.446 0.000
3.23 0.000
3.62 0.000
0801HBWW228 0801HBWW228
2010811606 2010811606
Cone Flaa ·oL.·· RL .Cone. Flaa ·'DL'." '< ·':RL
ND 127 0.000 ND 5.22 0.000
ND 77.7 0.000 ND 3.09 0.000
ND 178 0.000 ND 5.09 0.000
ND 97.4 0.000 ND 3.61 0.000
ND 548 0.000 ND 52.0 0.000
ND 140 0.000 ND 4.67 0.000
ND 137 0.000 ND 3.56 0.000
ND 148 0.000 ND ·5\16 0.000
ND 780 0.000 ND 72.9 0.000
ND 150 0.000 ND 3.34 0.000
ND Q6.5 0.000 ND 5.03 0.000
ND 84.6 0.000 ND 3.20 0.000
ND 237 0.000 ND 13.3 0.000
12600 124 0.000 8910 ER 2.32 0.000
ND 102 0.000 91.3 5.43 0.000
35100 122 0.000 25300 ER 5.78 0.000
1380 112 0.000 1650 4.42 0.000
ND 119 0.000 13.1 J 3.70 0.000
ND 86.9 0.000 ND 4.02 0.000
ND 135 0.000 ND 2.08 0.000
ND 160 0.000 ND 5.50 0.000
ND 99.4 0.000 ND 3.85 0.000
ND 81.8 0.000 ND 6.00 0.000
ND 90.8 0.000 ND 5.17 0.000
ND 101 0.000 ND 7.34 0.000
476 J 136 0.000 561 4.46 0.000
ND 331 0.000 ND 32.3 0.000
ND 169 0.000 ND 36.2 0.000
Page 20 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
'.. Parameter '. : ·o.u
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butvl ether <MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1.1.1 2-Tetrachloroethane 630-20-6
l, 1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2.3-Trichlorobenzene 87-61-6
1 2.4-Trichlorobenzene 120-82-1
1 1.1-Trichloroethane 71-55-6
1 1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2 3-Trichloroprooane 96-18-4
1 1,2-Trichlorotrifluoroethane 76-13-1
1 2.4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW227
2010811605
.cone Flaa.
ND
ND
ND
ND
ND
ND
2.68 J
6.88
ND
ND
ND
ND
ND
ND
ND
26.2
ND
ND
3050 ER
3.62
105
ND
ND
ND
ND
ND
ND
9.02
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL Ri..
0.143 0.000
0.167 0.000
0.394 0.000
1.21 0.000
0.428 0.000
0.666 0.000
0.270 0.000
0.170 0.000
33.7 0.000
0.400 0.000
0.181 0.000
0.598 0.000
0.740 0.000
1.14 0.000
7.03 0.000
0.285 0.000
0.472 0.000
0.472 0.000
0.219 0.000
0.600 0.000
0.324 0.000
0.600 0.000
0.760 0.000
0.604 0.000
0.198 0.000
0.385 0.000
0.540 0.000
0.372 0.000
0801HBWW228 0801HBWW228
2010811606 2010811606
Cone Fiaa DL RL Cone Flaa Dt · RL
ND 109 0.000 ND 1.43 0.000
ND 93.1 0.000 40.1 J 1.67 0.000
ND 115 0.000 ND 3.94 0.000
ND 131 0.000 ND 12.1 0.000
ND 116 0.000 ND 4.28 0.000
ND 178 0.000 ND 6.66 0.000
ND 126 0.000 13.4 J 2.70 0.000
ND 80.l 0.000 662 1.70 0.000
ND 1590 0.000 ND 337 0.000
ND 140 0.000 229 4.00 0.000
ND 97.7 0.000 12.9 J 1.81 0.000
ND 111 0.000 ND 5.98 0.000
ND 87.0 0.000 ND 7.40 0.000
270 J 144 0.000 19.6 J 11.4 0.000
ND 900 0.000 ND 70.3 0.000
1220 63.7 0.000 1390 2.85 0.000
ND 551 0.000 ND 4.72 0.000
ND 135 0.000 ND 4.72 0.000
76100 169 0.000 49400 ER 2.19 0.000
ND 82.1 0.000 28.0 6.00 0.000
8300 137 0.000 8550 ER 3.24 0.000
ND 106 0.000 ND 6.00 0.000
ND 288 0.000 ND 7.60 0.000
ND 123 0.000 ND 6.04 0.000
1120 124 0.000 1370 1.98 0.000
300 J 90.5 0.000 340 3.85 0.000
ND 94.8 0.000 ND 5.40 0.000
ND 114 0.000 174 3.72 0.000
Page 21 of 67
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
: . : Parameter '·'
< '•
n-Xvlene/m-Xvlene
o-Xvlene
' "
Client Sample ID
Lab Sample ID
'< CAS:3?.
106-42-3
95-47-6
SECTION IV -Analytical Results -09/04/2001 14:52
0801HBWW227
2010811605
-; ~;u;-: .:eC;nc <, . ·Flaa.
2.12 J
2.09 J
'LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
0801HBWW228 0801HBWW228
2010811606 2010811606
DL RL. 1 conc Flaa DL RL Cone Fiaa ':DL < < ··RL ·,
0.410 0.000 1350 167 0.000 1640 4.10 0.000
0.277 0.000 1150 84.4 0.000 1350 2.77 0.000
Page 22 of 67
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
· Surr~ate Compound ' , '','
l-Bromo-4-fluorobenzene
l ,2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results-09/04/2001 14:52
0801HBWW227
2010811605
Aaueous
Received
NA
08/15/2001 09:55
08/27/2001 21 :25
08/27/2001 21 :25
5.0000
MSDB
m!IL
%Recoverv
103
75
103
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
. Limits F
77-117
61-143
87-113
0801HBWW228 0801HBWW228
2010811606 2010811606
Aaueous Aaueous
Received Received
NA NA
08/15/2001 10:05 08/15/2001 10:05
08/20/2001 20:24 08/27/2001 20:56
08/20/2001 20:24 08/27/2001 20:56
1000.0000 50.0000
MSDA MSDB
ug/L ug/L
.%Recoverv limits F %Recoverv Limits 'F'
98 77-117 102 77-117
101 61-143 50 61-143 0
99 87-113 104 87-113
Page 23 of 67
-------------------
---------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
·" Parameter. . ·--"·
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
'.'
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
'' '• ·.,,·.cA.s , ',,,., -
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/04/2001 14:52
TRIP BLANK
2010811607
Aqueous
Received
NA
08/15/2001 00:00
08/20/2001 14:39
08/20/2001 14:39
1.0000
MSDA
ug/L
.c.onc ·Flaa ..
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20 I 08116] Hamilton Beach-Proctor Silex
STLAustin
DL.: .RL ·cone Flaa DL :·RL. cone. Flaa DL RL.·
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000 ··-0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
Page 24 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter·
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAs·
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1 2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/04/2001 14:52
I TRIPBLANK
2010811607
•Cone Flaa
ND
ND
·ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 (20108116] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL. Cone Flaa· DL RL
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
Page 25 of 67 -------------·------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
. : : --·Parameter'·.: ... · · ·";:CAS. > ·'·{ ' , ·-,,,;. ><
lodomethane 74-88-4
Isonronvlbenzene 98-82-8
4-Isonronvltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-nentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Nanhthalene 91-20-3
Pronanenitrile 107-12-0
n-Pronvlbenzene 103-65-1
Stvrene 100-42-5
1.1. l 2-Tetrachloroethane 630-20-6
1.1 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloronronane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/04/2001 14:52
I TRIP BLANK
2010811607
· .:C.onc •. Flaa
ND
ND
ND
ND
ND
ND
0.180 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone •Flaa :DL RL. · Coric· Flaa·. ':'.DL':: ; , . Rt. ...
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000 -" -0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000 --· 0.900 0.000 .. 0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
Page 26 of 67
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAtr· .· ·
106-42-3
95-47-6
SECTION IV -Analytical Results -09/04/2001 14:52
I TRIP BLANK
2010811607
·cone Flaa.
ND
ND
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.167 0.000
0.0844 0.000
Page 27 of 67
-------------------
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
suiroaata,Comoound 1 . :.--.-_+:,
·'
1-Bromo-4-fluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/04/2001 14:52
TRIP BLANK
2010811607
Aaueous
Received
NA
08/15/2001 00:00
08/20/2001 14:39
08/20/2001 14:39
1.0000
MSDA
u!!IL
i%RecoveN
98
104
102
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
Limits .F · o/o:.Recoverv t.imits 17. '%Recover/ limits ,. ' .. f· ~ ..
77-117
61-143
87-113
Page 28 of 67
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID:·
Instrument ID:
13103 Instrument Data File: A0820102.D
MSDA Analyst: BJP
Parameter Reference Value
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone (MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1.3-butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroorooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1.2-Dibromo-3-chloroorooane 20
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Measured Cone Flaa
18.9
150
94.9
97.8
18.0
17.4
18.4
18.8
19.3
18.3
25.1
19.5
18.4
18.1
19.0
20.9
19.4
17.0
19.9
18.4
19.0
21.l
21.2
18.2
17.6
19.2
Date!fime Analyzed:08/20/2001 12: 17
Units: ug/L
·. %Recoverv Fl.a a QC Limits %Recoverv
94
150
95
98
90
87
92
94
96
91
126
98
92
91
95
104
97
85
100
92 80-120
95
105
106
91
88
96
Page 29 of 67
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW82608
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13103 Instrument Data File: A0820102.D
Instrument ID: MSDA Analyst: BJP
Continued ·:.:earameter' , · > • -Refeteric•fYaluJl.:·
Dibromochloromethane 20
1 2-Dibromoethane 20
Dibromomethane 20
trans-1 4-Dichloro-2-butene 20
1 4-Dichlorobenzene 20
1 2-Dichlorobenzene 20
1 3-Dichlorobenzene 20
Dichlorodifluoromethane 20
1.1-Dichloroethane 20
1.2-Dichloroethane 20
1.1-Dichloroethene 20
cis-1.2-Dichloroethene 20
trans-1 2-Dichloroethene 20
1 2-Dichlorooronane 20
1 3-Dichloronronane 20
2 2-Dichloronronane 20
1 1-Dichloronronene 20
cis-13-Dichloronrooene 20
trans-I 3-Dichloronronene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1 3-butadiene 20
2-Hexanone 20
lodomethane 20
lsooronvlbenzene 20
4-Isonronvltoluene 20
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
. Measured Cone ·.Flaa .
18.8
18.1
18.6
20.6
17.6
17.5
17.5
22.6
20.9
18.8
19.2
18.6
18.5
19.3
17.5
21.8
19.3
19.8
19.5
18.8
17.5
19.6
21.6
19.9
17.5
18.9
Dateffime Analyzed:08/20/2001 12:17
Units: ug/L
%Recoverv· flaa QC .Limits %Recoverv :,, ·
94
90
93
103
88
87
87
113
105
94
96 80-120
93
92
97 80-120
88
109
96
99
98
94
87 80-120
98
108
100
88
95
Page 30 of 67
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13103 Instrument Data File: A0820102.D
Instrument ID: MSDA Analyst: BJP
Continued
·Parameter · Reference Value . ·
Methvl methacrvlate 20
Methvl tert-butvl ether <MTBE) 20
4-Methvl-2-oentanone (MIBK) 20
Methylene chloride 20
Naohthalene 20
Prooanenitrile 100
n-Proovlbenzene 20
Stvrene 20
1.1.1 2-Tetrachloroethane 20
I, 1.2 2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
I .2,3-Trichlorobenzene 20
I .2.4-Trichlorobenzene 20
I I. I -Trichloroethane 20
I I.2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
I 2.3-Trichloroorooane 20
I 1,2-Trichlorotrifluoroethane 20
I 2.4-Trimethvlbenzene 20
1,3 5-Trimethvlbenzene 20
Vinvl acetate 20
Vinvl chloride 20
o-Xvlene/m-Xvlene 40
SECTION V -Calibration and QC Infonnation -09/04/2001 14:52
LIMS Workorder: 80396910 (20108116) Hamilton Beach-Proctor Silex
STLAustin
Measured .Cone Flaa
19.9
18.6
20.5
19.0
I8.0
110
I8.4
18.I
I9.1
I8.4
15.0
23.3
I7.3
I8.0
I8.9
I9.8
16.6
18.3
I9.7
I9.8
22.2
18.0
18.1
22.6
20.7
35.3
Dateffime Analyzed:08/20/2001 12:17
Units: ug/L
%Recoverv Flan ·QC Limits %Recoverv
100
93
103
95
90
110
92
90·
95
92
75
116
86 80-I20
90
94
99
83
92
98
99
111
90
90
113
103 80-I20
88
Page 31 of 67 - - - - - - - --·-- - - - - - - - -
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13103 Instrument Data File: A0820129 .D
Instrument ID: MSDA Analyst: BJP
Parameter Reference Value
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromofonn 20
Bromomethane 20
2-Butanone <MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-l 3-butadiene ·20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroorooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1 2-Dibromo-3-chloroorooane 20
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 (20108116] Hamilton Beach-Proctor Silex
STLAustin
Measured Cone .Flaa
17.7
155
98.3
105
19.3
18.l
19.5
19.4
19.5
19.9
26.l
20.2
19.7
19.3
20.5
20.6
20.2
18.1
20.9
19.8
20.4
22.2
20.4
18.8
18.8
17.3 .
Dateffime Analyzed:08/21/2001 01:11
Units: ug/L
%Recoverv Flaa QC Limits %Recoveiv
88
155
98
105
97
90
98
97
97
99
131
101
98
97
102
103
101
91
104
99 80-120
102
111
102
94
94
87
Page 33 of 67
-------------------
- -------------- -SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: I 3103 Instrument Data File: A0820 I29 .D
Instrument ID: MSDA Analyst: BJP
Continued
· P.arameter . ... :.,-,, · -. , .ReferenCiaJl.a1u•L '' ,,
Dibromochloromethane 20
I .2-Dibromoethane 20
Dibromomethane 20
trans-I .4-Dichloro-2-butene 20
1.4-Dichlorobenzene 20
I ,2-Dichlorobenzene 20
I .3-Dichlorobenzene 20
Dichlorodifluoromethane 20
1 I-Dichloroethane 20
I 2-Dichloroethane 20
1.1-Dichloroethene 20
cis-1 2-Dichloroethene 20
trans-1.2-Dichloroethene 20
I ,2-Dichloroorooane 20
1.3-Dichloroorooane 20
2.2-Dichloroorooane 20
I .1-Dichloroorooene 20
cis-I 3-Dichloroorooene 20
trans-I 3-Dichloroorooene 20
Ethvl methacrvlate 20
Ethvlbeniene 20
Hexachloro-I 3-butadiene 20
2-Hexanone 20
lodomethane 20
Isooroovlbenzene 20
4-Isooroovltoluene 20
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
, • Meas:ured•Conc Flaa
18.8
19.2
20.0
20.4
I8.5
I8.1
I8.6
23.9
I9.7
20.0
20.6
I9.8
I9.5
20.4
I8.9
18.4
20.7
I9.8
19.2
19.4
I9.2
20.4
22.1
20.6
I9.2
I9.6
Dateffime Analyzed:08/2 l/200 I 01: 11
Units: ug/L
%Rec-0veni Flaa _. QC Limits. %Recoverv
94
96
IOO
102
92
91
93
120
99
100
103 80-120
99
97
102 80-120
95
92
104
99
96
97
96 80-I20
102
I 11
103
96
98
- - -
Page 34 of 67
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13103 Instrument Data File: A0820129 .D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter· Reference\lalu•
Methvl methacrvlate 20
Methvl tert-butvl ether (MTBE) 20
4-Methvl-2-oentanone (MIBK) 20
Methvlene chloride 20
Nanhthalene 20
Prooanenitrile 100
n-Proovlbenzene 20
Stvrene 20
I. I I .2-Tetrachloroethane 20
I. I 2.2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
1 2,3-Trichlorobenzene 20
1.2 4-Trichlorobenzene 20
1. I I -Trichloroethane 20
1.1 2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
1,2 3-Trichloronronane 20
1.1 2-Trichlorotrifluoroethane 20
I .2 4-Trimethvlbenzene 20
1.3 5-Trimethvlbenzene 20
Vinvl acetate 20
Vinvl chloride 20
o-Xvlene/m-Xvlene 40
SECTION V -Calibration and QC Information -09/0412001 14:52
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
Measured Cone Fi a a
20.2
19.9
21.7
20.2
I8.5
105
I9.7
18.8
19.3
19.6
15.7
22.9
18.7
18.8
19.3
20.0
I8.l
19.2
21.4
21.2
22.6
I9.I
I9.5
22.5
21.6
38.5
Dateffime Analyzed:08/21/200I 01:1 I
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
101
100
108
101
93
105
98
94
97
98
78
1I5
93 80-120
94
97
100
90
96
107
106
113
95
98
1 I2
108 80-I20
96
Page 35 of 67
-------------------
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13307 Instrument Data File: B0827102.D
Instrument ID: MSDB Analyst: BJP
Parameter' , Reference ¥'aiue_
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone rMEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1.3-butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloronronene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1 2-Dibromo-3-chloroorooane 20
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Measured .Cone F·laa
20.4
113
116
103
19.8
19.9
19.8
19.5
17.0
16.7
25.8
21.5
20.7
20.4
19.0
19.9
20.4
19.6
20.6
20.0
20.6
16.l
19.l
19.7
19.3
16.2
Dateffime Analyzed:08/27/2001 17 :29
Units: ug/L
. %Recoven . . Flaa QC timits %Recoverv
102
113
116
103
99
100
99
98
85
83
129
107
103
102
95
100
102
98
103
100 80-120
103
80
96
98
96
81
Page 37 of 67
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13307 Instrument Data File: B0827102.D
Instrument ID: MSDB Analyst: BJP
Continued
, Pa·rameter_ · · '' ' -_ Refer&.ncrrvaiue
Dibromochloromethane 20
1 2-Dibromoethane 20
Dibromomethane 20
trans-1.4-Dichloro-2-butene 20
1.4-Dichlorobenzene 20
1 2-Dichlorobenzene 20
1.3-Dichlorobenzene 20
Dichlorodifluoromethane 20
l, 1-Dichloroethane 20
l .2~Dichloroethane • 20
1.1-Dichloroethene 20
cis-1 2-Dichloroethene 20
trans-I 2-Dichloroethene 20
1.2-Dichloroprooane 20
1.3-Dichloroorooane 20
2.2-Dichloroorooane 20
1.1-Dichloroorooene 20
cis-1 3-Dichloropropene 20
trans-1.3-Dichlorooropene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1 3-butadiene 20
2-Hexanone 20
Iodomethane 20
Isooroovlbenzene 20
4-Isooroovltoluene 20
SECTION V -Calibration and QC Infonnation -09/04/2001 14:52
LIMS Workorder: 80396910[20108116] Hamilton Beach-Proctor Silex
STLAustin
-Measured Cone Flaa._
18.3
19.4
19.8
8.76
19.5
19.7
19.5
17.0
17.3
20.0
20.7
20.1
17.9
19.9
19.6
21.4
20.2
19.2
19.2
19.8
19.9
21.5
18.0
21.8
20.2
20.9
, Dateffime Analyzed:08/27/2001 17 :29
Units: ug/L
%Recoverv flaa QC .Limits %Recoverv
92
97
99
44
98
98
97
85
86
100
104 80-120
100
90
99 80-120
98
107
101
96
96
99
100 80-120
107
90
109
101
104
Page 38 of 67
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13307 Instrument Data File: B0827102.D
Instrument ID: MSDB Analyst: BJP
Continued
Parameter Reference Valueu
Methvl methacrvlate 20
Methyl tert-butvl ether rMTBE) 20
4-Methvl-2-oentanone (MIBK) 20
Methvlene chloride 20
Naohthalene 20
Prooanenitrile 100
n-Proovlbenzene 20
Stvrene 20
1.1.1.2-Tetrachloroethane 20
1.1.2 2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
1.2.3-Trichlorobenzene 20
1.2.4-Trichlorobenzene 20
1.1.1-Trichloroethane 20
1.1.2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
1.2.3-Trichloroorooane 20
1 1.2-Trichlorotrifluoroethane 20
1 2 4-Trimethvlbenzene 20
1 3 5-Trimethvlbenzene 20
Vinvl acetate 20
Vinvl chloride 20
o-Xvlene/m-Xvlene 40
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
Measured Cone Flaa
20.4
19.4
19.1
19.9
16.0
103
20.7
20.3
17.6
19.5
13.8
20.0
20.0
18.4
18.4
20.2
19.9
19.9
26.0
19.4
21.5
20.7
20.4
24.4
19.5
40.l
Dateffime Analyzed:08/27/2001 17:29
Units: ug/L
%Recoveni Flaa QC Limits .%Recoverv
102
97
96
99
80
103
103
101
88
97
69
100
100 80-120
92
92
101
100
100
130
97
107
103
102
122
97 80-120
100
Page 39 of 67
-------------------
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13307 Instrument Data File: B082713 l.D
Instrument ID: MSDB Analyst: BJP
Parameter. . ReferenC'e.Value. ,
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone <MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1.3-butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroorooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1.2-Dibromo-3-chloroorooane 20
SECTI<?N V -Calibration and QC lnfonnation -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Measured Cone Flaa
22.2
112
102
110
20.7
19.9
20.5
19.9
16.2
16.8
23.2
21.3
20.8
20.4
20.0
21.l
21.1
19.8
20.9
20.7
20.3
16.6
18.7
19.7
19.6
15.3
Dateffime Analyzed:08/28/2001 07:25
Units: ug/L
%Recoveni Fiaa QC Limits %Recoverv
111
112
102
110
104
100
103
99
81
84
116
106
104
102
100
106
106
99
105
104 80-120
102
83
93
98
98
77
Page 41 of 67
-------------------
--------------- - - - -SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13307 Instrument Data File: B082713 l.D
Instrument ID: MSDB Analyst: BJP
Continued
' Parameter.>, ; ·. Refere.rfoe vaiue· -' ', s:-
Dibromochloromethane 20
I 2-Dibromoethane 20
Dibromomethane 20
trans-I 4-Dichloro-2-butene 20
I 4-Dichlorobenzene 20
1 2-Dichlorobenzene 20
I 3-Dichlorobenzene 20
Dichlorodifluoromethane 20
I. I-Dichloroethane 20
1.2-Dichloroethane 20
I .1-Dichloroethene 20
cis-I .2-Dichloroethene 20
trans-I 2-Dichloroethene 20
I 2-Dichloroorooane 20
1.3-Dichloropropane 20
2.2-Dichloroorooane 20
1. I-Dichloroorooene 20
cis-1.3-Dichloroorooene 20
trans-I 3-Dichloroorooene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1 3-butadiene 20
2-Hexanone 20
Iodomethane 20
lsoproovlbenzene 20
4-Isooroovltoluene 20
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
.Measured Cone · Flaa
I8.3
20.0
20.9
7.42
I9.6
I9.6
I9.5
I7. I
I7.8
20.9
21.6
21.0
18.6
20.6
I9.9
I6.9
21.0
I8.8
I8.5
20.3
20.4
20.4
I9.6
22.I
20.9
20.9
Dateffime Analyzed:08/28/200I 07:25
Units: ug/L
%Recoverv Flaa --_QC Limits %Recoverv ·
9I
100
105
37
98
98
97
85
89
105
108 80-I20
105
93
103 80-I20
99
85
105
94
93
102
102 80-I20
102
98
I 11
105
104
Page 42 of 67
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 13307 Instrument Data File: B082713 l.D
Instrument ID: MSDB Analyst: BJP
Continued
Parameter Reference Value
Methvl methacrvlate 20
Methvl tert-butvl ether <MTBE) 20
4-Methvl-2-oentanone fMIBK) 20
Methvlene chloride 20
Naohthalene 20
Prooanenitrile 100
n-Proovlbenzene 20
Stvrene 20
1 1.1.2-Tetrachloroethane 20
1 1.2.2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
1 2.3-Trichlorobenzene 20
I 2.4-Trichlorobenzene 20
1 1.1-Trichloroethane 20
1 1 2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
1 2 3-Trichloroorooane 20
l, I 2-Trichlorotrifluoroethane 20
1.2 4-Trimethvlbenzene 20
1,3 5-Trimethvlbenzene 20
Vinvl acetate 20
Vinvl chloride 20
o-Xvlene/m-Xvlene 40
SECTION V -Calibration and QC Infonnation -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
. Measured Cone Flaa
21.0
17.8
20.4
20.6
17.0
101
20.3
20.5
16.3
17.l
25.3
19.2
20.4
19.0
18.9
21.2
20.4
22.9
27.6
20.7
21.7
20.5
20.4
9.37
20.0
40.9
Datetrime Analyzed:08/28/2001 07:25
Units: ug/L
%Recoverv .flaa ·QC Limits %Recoverv
105
89
102
103
85
101
102
103
82
86
126
96
102 80-120
95
95
106
102
114
138
104
109
103
102
47
100 80-120
102
Page 43 of 67
-------------------
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 13103 Instrument Data File: A0820102.D
Instrument ID: MSDA Injection Time: 08/20/2001 12:17
. . ·· : Ion Abundance Criteria
.Mass/Enerav . :;;;~~~:,;£ .. '.f;t!GIJarUmit .. · Unnar Limit
~ 15 40
75 30 60
95 100 100
96 5 9
' 173 0 2
174 50
175 5 9
176 95 101
177 5 9
SECTION V -Calibration and QC lnfonnation -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex.
STLAustin
Date Analyzed: 08/20/2001 12:17
Analyst: BJP
% Relative Abundance .
20.1
39.3
100
7.3
0
70.4
7.8
98.3
6.5
Page 45 of 67
----------~----------
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 13103
Instrument ID: MSDA
Instrument Data File: A0820129.D
Injection Time: 08/21/2001 01:11
•" ', -,w ;', . '':.; .t ' .. 'Ion Abundance Criteria ~ -:, •,
,
•·.Mass/Eilerav: .· ' . ' -~--'.:? ... :: .. t:ower:limit •v' ~'<
50 15
75 30
95 100
96 5
173 0
174 50
175 5
176 95
177 5
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
', , Oos>er :Limit
40
60
100
9
2
9
101
9
Date Analyzed: 08/21/2001 01:11
Analyst: BJP
% Relati:ve Abundanc·e .
20.3
39.3
100
6.8
0
70.3
7.2
96.6
6.1
Page 46 of 67
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 13307
Instrument ID: MSDB
Instrument Data File: B0827102.D
Injection Time: 08/27/2001 17:29
',, .. ton Abundance Criteria ·,;·Hl,·' ~ ''<A
Mass/Ehernv : · / .. ~"' ~:.t'owarlimit
50 15
75 30
95 100
96 5
173 0
174 50
175 5
176 95
177 5
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Unner Limit .
40
60
100
9
2
9
101
9
Date Analyzed: 08/27/2001 17:29
Analyst: BJP
% Relative Abundance.
23.1
45.2
100
6.1
0
68.3
8
97.7
7
Page 47 of 67
-------------------
------~------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 13307
Instrument ID: MSDB
Instrument Data File: B0827131
Injection Time: 08/28/2001 07:25
; \· ,.,,, 'f ,,. · Ion Abundance Criteria .llilass/E~ercn/ ~ '.};>« ·, ':· _ ." Lower Limit ~-· _ · ·
50 15
75 30
95 100
96 5
173 0
174 50
175 5
J76 95
177 5
SECTI~N V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
l:Jooer Limit ..
40
60
100
9
2
9
101
9
Date Analyzed: 08/28/2001 07:25
Analyst: BJP
% Relative.Abundance
22.8
44.9
100
7
0
74.8
7.5
95.8
6.6
Page 48 of 67
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone fMEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
OAS ,
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
1027665
Method Blank
Aaueous
08/20/200114:11
08/20/2001 14:11
MSDA
ug/L
Cone. Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -09/04/2001 14:52
LJMS Workorder: 80396910 (20108116) Hamilton Beach-Proctor Silex
STLAustin
1028428
Method Blank
Aaueous
08/27/2001 19:20
08/27/2001 19:20
MSDB
U!!II,
DL . RL Cone Flaa DL RL Cone Flaa bl .RL
0.438 0.000 ND 2.14 0.000
6.82 0.000 ND 8.03 0.000
3.79 0.000 ND 1.37 0.000
0.446 0.000 ND 0.128 0.000
0.0641 0.000 ND 0.0401 0.000
0.0998 0.000 ND 0.100 0.000
0.131 0.000 ND 0.108 0.000
0.118 0.000 ND 0.0747 0.000
0.170 0.000 ND 0.182 0.000
0.199 0.000 ND 0.154 0.000
0.200 0.000 ND 4.80 0.000
0.102 0.000 ND 0.0668 0.000
0.105 0.000 ND 0.0655 0.000
0.0911 0.000 ND 0.0798 0.000
0.0684 0.000 ND 0.0682 0.000
0.0652 0.000 ND 0.102 0.000
0.114 0.000 ND 0.133 0.000
0.0842 0.000 ND 0.0712 0.000
0.0925 0.000 ND 0.111 0.000
0.0896 0.000 ND 0.111 0.000
0.0938 0.000 ND 0.124 0.000
0.127 0.000 ND 0.104 0.000
0.0777 0.000 ND 0.0618 0.000
0.178 0.000 ND 0.102 0.000
0.0974 0.000 ND 0.0722 0.000
Page 49 of 67
------~------------
-----~~----~-------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
_ _ .Parameter · · , , .' :Oli$'.j: _ ) +'
l ,2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-l ,4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1,2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloropropane 78-87-5
1.3-Dichloropropane 142-28-9
2.2-Dichloroorooane 594-20-7
1.1-Dichloropropene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1 3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethylbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
lodomethane 74-88-4
Isopropylbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
I 1021665
-:;.,:: i,¢.onc
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
_ Ftaa ..
1028428
DL RL Cone_ ,.
Flaa bl . RL Cone . Flaa ·~ Dl ··_RL '•
...
0.548 0.000 ND 1.04 0.000
0.140 0.000 ND 0.0934 0.000
0.137 0.000 ND 0.0712 0.000
0.148 0.000 ND 0.103 0.000
0.780 0.000 ND 1.46 0.000
0.150 0.000 ND 0.0667 0.000
0.0965 0.000 ND 0.101 0.000
0.0846 0.000 ND 0.0639 0.000 :"""':."~
0.237 0.000 ND 0.267 0.000 ---
0.124 0.000 ND 0.0465 0.000
0.102 0.000 ND 0.109 0.000
0.122 0.000 ND 0.116 0.000
0.112 0.000 ND 0.0883 0.000
0.119 0.000 ND 0.0740 0.000
0.0869 0.000 ND 0.0805 0.000
0.135 0.000 ND 0.0416 0.000 ~
0.160 0.000 ND 0.110 0.000 '"'.
0.0994 0.000 ND 0.0770 0.000
0.0818 0.000 ND 0.120 0.000
0.0908 0.000 ND 0.103 0.000
0.101 0.000 ND 0.147 0.000
0.136 0.000 ND 0.0891 0.000
0.331 0.000 ND 0.646 0.000
0.169 0.000 ND 0.723 0.000
0.109 0.000 ND 0.0286 0.000
0.0931 0.000 ND 0.0334 0.000
0.115 0.000 ND 0.0789 0.000
0.131 0.000 ND 0.241 0.000
0.116 0.000 ND 0.0856 0.000
Page 50 of 67
. ...,
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
'Parameter CAS'.
4-Methyl-2-nentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Pronanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 l 1.2-Tetrachloroethane 630-20-6
1 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-6I-6
1.2.4-Trichlorobenzene 120-82-1
1. I .1-Trichloroethane 7I-55-6
I. I 2-Trichloroethane 79-00-5
Trichloroethene 79-0I-6
Trichlorofluoromethane 75-69-4
I 2.3-Trichloroorooane 96-I8-4
1 1.2-Trichlorotrifluoroethane 76-I3-I
1 2.4-Trimethvlbenzene 95-63-6
l 3.5-Trimethvlbenzene I08-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
o-Xvlene/m-Xvlene 106-42-3
o-Xvlene 95-47-6
1027665
Cone
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
. Flaa
1028428
DL RL Cone Flaa DL RL Cone Flaa DL RL
0.178 0.000 ND 0.133 0.000
0.126 0.000 ND 0.0540 0.000
0.0801 0.000 ND 0.0340 0.000
1.59 0.000 ND 6.73 0.000
0.140 0.000 ND 0.0799 0.000
0.0977 0.000 ND 0.0362 0.000
0.111 0.000 ND 0.120 0.000
0.0870 0.000 ND 0.148 0.000
0.144 0.000 ND 0.228 0.000
0.900 0.000 ND 1.41 0.000
0.0637 0.000 ND 0.0570 0.000
0.551 0.000 ND 0.0944 0.000
0.135 0.000 ND 0.0943 0.000
0.169 0.000 ND 0.0438 0.000
0.082I 0.000 ND O.I20 0.000
0.137 0.000 ND 0.0648 0.000
0.106 0.000 ND 0.120 0.000
0.288 0.000 ND O.I52 0.000
0.123 0.000 ND 0.121 0.000
0.124 0.000 ND 0.0396 0.000
0.0905 0.000 ND 0.0770 0.000
0.0948 0.000 ND 0.108 0.000
0.114 0.000 ND 0.0744 0.000
0.167 0.000 ND 0.0819 0.000
0.0844 0.000 ND 0.0554 0.000
Page 51 of 67 ------.. ·------·-------
--~------~--------­SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Sample Type
Matrix
1027665
Method Blank
Aaueous
Date/Time Prepared
Date/Time Analyzed
Instrument
08/20/2001 14:11
08/20/2001 14:11
MSDA
Units ug/L
:_: .surroaate Comoound.-: .:'; ': :, :,;::, ,'-;;:, ,' /:'-,_'%(Recoyerv
l-Bromo-4-fluorobenzene 98
1.2-Dichloroethane-d4 102
Toluene-d8 103
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
, ' ' Limits
77-117
61-143
87-113
1028428
Method Blank
Aaueous
08/27/2001 19:20
08/27/2001 19:20
MSDB
ug/L
F , % Recoverv ·Limits_ F % Recover:\t; ,,Limits ' 'f '> ~ ~~-
101 77-117
103 61-143
104 87-113
Page 52 of 67
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS forHBN 13103 [MSV/1627]
13103
13103
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
% Moisture:
Analyst:
NA
BJP
Control Samp e Control Sample Duplicate . <~'i. : .. '. '. ii._ .. ';,,/ ._LaFI.rbe 1'00: 1027663 Lab ID: 1027664
. ·\,fo '!·· ... . ..... ..,._ ___ • _....,A_o_s_2...,.01 ..... o .... 3...,..D--,.. _____ l-F_._.i_..le_l...,..D_: ..... --..A_0_8_20_1_04_. ,_•D-,....-----r-------i QC Limit& 1---·~P~•~ra~m:.::.:.et~e~r ___ __. ___ ---'.~~---·------~:/~~t~~~::·~~-·-'.:~,1 ~~~S~io~k~A~m<==t--1~C=o=n~c:.._ ___ -J-~%~R=e~c~F~l....__a+.~S~10~k~Am~·~t=---+-'C~o~n=c"-----+-o/c~o~R~e~c~F~la.._l-!-"R~P=D~.F~.l....__a--+-~o/c~oR~a~c"--·~R~P~D=-i
Acetone 20 26.0 130 20 30.6 153 16 0.1-240 71
Benzene 20 21.l 106 20 21.2 106 0 71-133 17
Bromobenzene 20 18.2 91 20 18.l 91 0 67-127 12
Bromochloromethane 20 19.l 96 20 18.7 93 3.2 61-145 21
Bromodichloromethane 20 20.0 100 20 19.5 98 2 57-135 19
Bromoform 20 21.0 105 20 20.9 104 l 23-151 17
Bromomethane 20 14.4 72 20 14.4 72 0 34-128 25
2-Butanone <MEK) 20 25.6 128 20 24.6 123 4 0.1-214 39
n-Butvlbenzene 20 19.7 98 20 19.7 99 1 28-184 30
sec-Butvlbenzene 20 19 .5 98 20 19 .8 99 l 45-160 31
tert-Butvlbenzene 20 18.6 93 20 18.5 92 I.I 65-148 27
Carbon disulfide 20 18.0 90 20 18.0 90 0 29-223 23
Carbon tetrachloride 20 22.0 110 20 22.0 110 0 46-150 23
Chlorobenzene 20 17.9 89 20 17.8 89 0 77-129 14
Chloroethane 20 17.6 88 20 17.5 87 I.I 39-133 27
Chloroform 20 19.7 99 20 19.2 96 3.1 64-146 16
Chloromethane 20 13.3 66 20 13.4 67 1.5 18-140 26
2-Chlorotoluene 20 18.l 91 20 18.0 90 l.l 70-136 24
4-Chlorotoluene 20 18.6 93 20 18.4 92 I.I 74-132 23
I 2-Dibromo-3-chloroorooane 20 18.9 95 20 19.5 97 2.1 39-171 25
Dibromochloromethane 20 20.4 102 20 19.9 99 3 45-137 15
12-Dibromoethane 20 19.1 95 20 19.0 95 0 19-187 19
Dibromomethane 20 19.7 99 20 18.9 95 4.1 52-138 21
14-Dichlorobenzene 20 17.4 87 20 17.6 88 l.l 70-132 13
SECTION V -Calibration and QC Information -09/04/200! 14:52
LIMS Workorder: 80396910 (20108116] Hamilton Beach-Proctor Silex
STLAustin Page 53 of 67 - -.. - -.. - - -.. - - -·-- - - - -
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
1. 1. I -Trichloroethane
1.1 2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1.2.3-Trichloropropane
1 2 4-Trimethvlbenzene
1.3 5-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
n-Xvlene/m-Xvlene
o-Xvlene
" .. '~: "
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 (20108116) Hamilton Beach-Proctor Silex
STLAustin
LablPt
File ID:
·.SokAmt
20
20
20
20
20
20
20
20
20
40
20
C t IS on ro f d amp; e con mue
1027663 Lab ID:
A0820103.D File ID:
Cone %Rec Fla Sok Amt
20.9 105 20
17.7 89 20
19.2 96 20
15.9 79 20
20.8 104 20
18.4 92 20
19.0 95 20
7.37 37 20
14.6 73 20
36.5 91 40
18.0 90 20
C t IS on ro I D r ampe up11cate contmue d
1027664
A0820104.D QC Limits
Cone %Rec Fla RPO Fla .%Rec RPO
20.6 103 1.9 49-155 24
16.8 84 5.8 67-135 17
18.8 94 2.1 71-129 17
15.0 75 5.2 39-147 29
20.6 103 1 64-140 18
18.1 91 1.1 54-156 25
19.2 96 1 62-144 25
7.16 36 2.7 0.1-164 31
14.3 72 1.4 24-138 27
36.3 91 0 76-134 15
17.6 88 2.2 77-131 15
Page 55 of 67
-----~-------------
-----~-------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
,.,
· SurroaateComnounds
l-Bromo-4-fluorobenzene
l 2-Dichloroethane-d4
Toluene-d8
>' ,,
> '>
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 (20108116) Hamilton Beach-Proctor Silex
STLAustin
· La.blD:. 1027663
%Recoverv·
101
105
104
Lab ID: 1027664: .. , ' '>
Fla as %Recoverv Fla as QC Recoveni LimitS
100 77-117
103 61-143
102 87-113
Page 56 of 67
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 13307 [MSV/1640]
13307
13307
Lab ID:
Instrument ID: MSDB
Units: ug/L
Matrix: Aqueous
C t IS on ro amn.e
1028426
.·. f.'.ile ID: 80827103.D . , ' " . ,
.
Parameter . , , .. ..
, ,
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone fMEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
l .2-Dibromo-3-chloropropane
Dibromochloromethane
1 2-Dibromoethane
Dibromomethane
1 4-Dichlorobenzene
SECTION V -Calibration and QC Infonnation -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116) Hamilton Beach-Proctor Silex
STLAustin
Sok Amt Cone· ,_
"IORecfla
20 23.5 118
20 22.8 114
20 19.6 98
20 19.7 98
20 19.8 99
20 16.0 80
20 13.5 68
20 20.6 103
20 22.0 110
20 21.9 109
20 20.7 104
20 18.4 92
20 21.4 107
20 19.4 97
20 20.2 lOl
20 20.8 104
20 13.l 65
20 19.7 98
20 19.5 97
20 15.8 79
20 18.6 93
20 18.7 93
20 19.7 99
20 19.3 97
i.,ab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture:
Analyst:
NA
BJP
on ro amn.e un. 1ca e C t IS I D I' t
1028427
80827104.D
Cone
..
%Rec Fla
25.8 129
22.7 113
19.4 97
19.9 100
19.8 99
16.5 83
13.7 68
24.1 120
21.6 108
21.8 109
20.4 102
18.5 93
21.3 106
19.4 97
20.2 101
20.9 104
12.8 64
19.2 96
19.3 97
15.3 77
18.5 93
19.4 97
20.3 101
18.9 95
' Qq Limits
RPO Fia %Rec. :RPO
8.9 0.1-240 71
0.9 71-133 17
1 67-127 12
2 61-145 21
0 57-135 19
3.7 23-151 17
0 34-128 25
15 0.1-214 39
1.8 28-184 30
0 45-160 31
1.9 65-148 27
1.1 29-223 23
0.9 46-150 23
0 77-129 14
0 39-133 27
0 64-146 16
1.6 18-140 26
2.1 70-136 24
0 74-132 23
2.6 39-171 25
0 45-137 15
4.2 19-187 19
2 52-138 21
2.1 70-132 13
Page 57 of 67
-------------------
--~---~-----------­SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
·., .. .. ,_
:Parameter_ .,.
1 2-Dichlorobenzene
1 3-Dichlorobenzene
Dichlorodifluoromethane
1 1-Dichloroethane
1 2-Dichloroethane
1.1-Dichloroethene
cis-1 2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
1.3-Dichloroorooane
2.2-Dichloronronane
1 1-Dichlorooropene
cis-1.3-Dichloropropene
trans-I 3-Dichloroorooene
Ethvlbenzene
Hexachloro-1.3-butadiene
2-Hexanone
lodomethane
Isooroovlbenzene
4-Isooroovltoluene
..
4-Methvl-2-oentanone (MIBK)
Methvlene chloride
Nanhthalene
n-Pronvlbenzene
Stvrene
l 1.1.2-Tetrachloroethane
1.1 2 2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2 3-Trichlorobenzene
1.2 4-Trichlorobenzene
,, .. .. ,, ' '
> •, ·;~"F::O'•· .,'. :y ,'. < ••
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Lab 10·:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
c ontro IS amp e contmue d
1028426 lab ID:
80821103.D .. File 10:
·Cone -%Re.c Fla. Sok Amt
19.2 96 20
19.4 97 20
12.4 62 20
17.2 86 20
20.l 101 20
22.8 114 20
20.3 101 20
19.6 98 20
19.8 99 20
18.8 94 20
22.1 110 20
20.5 102 20
19.6 98 20
19.4 97 20
20.3 102 20
21.6 108 20
19.0 95 20
20.5 102 20
20.l 100 20
21.7 108 20
18.4 92 20
20.2 101 20
16.8 84 20
20.2 101 20
19.7 99 20
18.l 90 20
19.2 96 20
15.3 76 20
20.1 100 20
19.5 97 20
19.5 97 20
on ro amoe uo 1ca e con mue C t IS I D r t f d
1028427. .. ... ..
' . .. . . . . 6c L.i.Uits_ 80827104.D ·
Cone .. %Rec Fla ·RPO Fia ' : . %Rec · · RPO
18.7 93 3.2 67-135 14
18.9 94 3.1 68-134 14
12.7 64 3.2 0.1-166 26
17.7 89 3.4 66-138 19
20.2 101 0 48-152 23
23.2 116 l.7 47-175 25
20.4 102 1 66-144 18
20.2 101 3 62-146 22
20.2 101 2 61-133 17
19.0 95 1.1 70-128 16
22.6 113 2.7 .u40-168 30
20.7 104 1.9 c•71-155 31
19.6 98 0 36-142 16
19.2 96 1 34-138 21
20.5 103 1 75-131 14
20.8 104 3.8 46-150 34
19.1 95 0 22-164 34
20.8 104 1.9
20.5 103 3 54-152 26
21.3 106 1.9 41-165 28
20.3 101 9.3 27-149 36
20.5 103 2 36-166 23
16.7 83 1.2 32-172 22
20.l 100 l 61-143 28
20.l 100 1 68-136 14
19.3 96 6.5 63-141 20
19.3 96 0 47-143 20
17.5 88 15 69-137 16
20.2 101 1 70-132 17
19.4 97 0 66-140 20
19.4 97 0 66-144 22
Page 58 of 67
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
' ' :
, Parameter
I I I-Trichloroethane
1.1 2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
I 2 3-Trichloroorooane
l 2 4-Trimethvlbenzene
1 3.5-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
o-Xvlene/m-Xvlene
o-Xvlene
" . '
'' '' -' ' ' ;>', ~ ~ :, '
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Lab IP:
File ID:
Sok.Amt.
20
20
20
20
20
20
20
20
20
40
20
c ontro IS f d amp: e con mue
1028426
80827103.D
Cone ·%Rec Fla
21.2 106
18.9 95
20.2 101
24.3 122
18.8 94
20.9 104
21.3 106
7.32 37
17.l 85
40.7 102
19.4 97
on ro ampe up 1ca e con mue C t IS I D r t f d
Lab ID: 1028427 ''
File ID: 60827104.D QC l;.imits
Sok Amt Cone, %Rec Fla RPO Fla ,,%Rec· RPO
20 21.8 109 2.8 49-155 24
20 19.0 95 0 67-135 17
20 21.0 105 3.9 71-129 17
20 24.8 124 1.6 39-147 29
20 19.3 97 3.1 64-140 18
20 20.5 102 1.9 54-156 25
20 20.9 104 1.9 62-144 25
20 7.11 36 2.7 0.1-164 31
20 17.4 87 2.3 24-138 27
40 41.4 103 l 76-134 15
20 19.6 98 l 77-131 15
Page 59 of 67
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
... -. _; ,: . ,,.
"
,·sufroaate.-comnounCls:
l-Bromo-4-fluorobenzene
l 2-Dichloroethane-d4
Toluene-d8
'.
..
•·
..
·' ... .. ., ... ., , ., .. ; ''·. ~ <,. --,' ... , " ~-
SECTION V -Calibration and QC Information -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Lab ID;: 1028426 lab ID:. 1028427-.
%Recov:erv'. _· Fla as . 0iciRecover'1 'Flaas QC Re.coverv Limits
102 104 77-117
100 103 61-143
105 105 87-113
Page 60 of 67
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 13103
Client SamDI& ID ·: Lab $amnle ID
INSTRUMENT OC 1000
INSTRUMENT OC 1406
LCS for HBN 13103 rMSV /16271 1027663
LCSD for HBN 13103 fMSV /16271 1027664
MB for HBN 13103 rMSV /16271 1027665
TRIP BLANK 2010811607 zzzzzzzzzz 2010811810 zzzzzzzzzz 2010813603 zzzzzzzzzz 2010813601 zzzzzzzzzz 2010811906 zzzzzzzzzz 2010811907
0801HBWD999 2010811602
0801HBWW215 2010811603
0801HBWW214 2010811601
0801HBWW213 2010811604
0801HBWW227 2010811605 zzzzzzzzzz 2010814901
0801HBWW228 2010811606 zzzzzzzzzz 2010814201 zzzzzzzzzz 2010814202 zzzzzzzzzz 2010811801 zzzzzzzzzz 2010811802 zzzzzzzzzz 2010811803 zzzzzzzzzz 2010811804
INSTRUMENT OC 1000
INSTRUMENT OC 1406 zzzzzzzzzz 1027709 zzzzzzzzzz 1027710
SECTION VI-Batch Summaries -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Start Dateffime:
Stop Datetrime:
08/20/2001 12:17
08/21/2001 12:31
Samole Tvoe. Matrix ·
GC/MS Tune Aaueous
Continuing Calibration Check Aqueous
Lab Control Samole Aaueous
Lab Control Sample Duplicate Aqueous
Method Blank Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aaueous
Field Sample Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aaueous
Field Samole Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Samole Aqueous
Field Samole Aaueous
Field Sample Aqueous
GC/MSTune Aaueous
Continuing Calibration Check Aqueous
Matrix Soike Aaueous
Matrix Soike Duolicate Aqueous
Analyst: BJP
Sample Size
Initial. Final . Preoaration Method
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15 mL SW8260B
Page 61 of 67
-------------------
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 13307 continued
',',,
Cllent.sami>le 10. . ' ,'';' ','' , . lab samnle ID zzzzzzzzzz 2010819812 zzzzzzzzzz 2010816602
zzzzzzzzzz 2010819401
zzzzzzzzzz 2010818501 zzzzzzzzzz 2010818502
zzzzzzzzzz 2010819804 zzzzzzzzzz 2010819807 zzzzzzzzzz 2010816601
INSTRUMENT QC 1000
INSTRUMENT OC 1406 zzzzzzzzzz 1028429 zzzzzzzzzz 1028430 zzzzzzzzzz 2010819801 zzzzzzzzzz 2010819804 zzzzzzzzzz 2010819807 zzzzzzzzzz 2010818501 zzzzzzzzzz 2010818502 zzzzzzzzzz 2010815801 zzzzzzzzzz 2010816601 zzzzzzzzzz 2010816601
SECTION VI-Batch Summaries -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
SamDle Size ... '.
SamoleTvoe Matrix Initial Final Preoaration Method
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15 mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samnle Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15 mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
GC/MS Tune Aaueous 15mL 15mL SW8260B
Continuin!! Calibration Check Aaueous 15mL 15 mL SW8260B
Matrix Soike Aaueous 15mL 15mL SW8260B
Matrix Soike Duolicate Aaueous 15mL 15 mL SW8260B
Field Samole Aaueous 15mL 15 mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Page 63 of 67
-------------------
-------------------SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 13103
,i :: ,..'l ',' /\ ; , , , , , , , , , , '.~t{it:~\k{:;x. • Client,SamoleJD , : 1:<~:L .,:,:· , Seauence, ,'
1 INSTRUMENT QC
2 INSTRUMENT OC
3 LCSforHBN 13103 fMSV/16271
4 LCSD for HBN 13103 IMSV/16271
5 MB for HBN 13103 fMSV /16271
6 TRIP BLANK
7 zzzzzzzzzz
8 zzzzzzzzzz
9 zzzzzzzzzz
IO zzzzzzzzzz
11 zzzzzzzzzz
12 0801HBWD999
13 0801HBWW215
14 0801HBWW214
15 0801HBWW213
16 0801HBWW227
17 zzzzzzzzzz
18 0801HBWW228
19 zzzzzzzzzz
20 zzzzzzzzzz
21 zzzzzzzzzz
22 zzzzzzzzzz
23 zzzzzzzzzz
24 zzzzzzzzzz
25 INSTRUMENT QC
26 INSTRUMENT OC
27 zzzzzzzzzz
28 zzzzzzzzzz ,
29 0801HBWW215
SECTION VI -Batch Summaries -0910412001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Instrument ID: MSDA
, , , , , ,Analvsis : , ,
~ Lab, Sample 'ID . Date '• Time
1000 08/20/2001 12:17:00
1406 08/20/2001 12:17:00
1027663 08/20/2001 12:46:00
1027664 08/20/2001 13:14:00
1027665 08/20/2001 14:11:00
2010811607 08/20/2001 14:39:00
2010811810 08/20/2001 15:07:00
2010813603 08/20/2001 15:36:00
2010813601 08/20/2001 16:04:00
2010811906 08/20/2001 16:32:00
2010811907 08/20/2001 17:01:00
2010811602 08/20/2001 17:29:00
2010811603 08/20/2001 17:58:00
2010811601 08/20/2001 18:26:00
2010811604 08/20/2001 18:56:00
2010811605 08/20/2001 19:26:00
2010814901 08/20/2001 19:55:00
2010811606 08/20/2001 20:24:00
2010814201 08/20/2001 20:53:00
2010814202 08/20/2001 21:22:00
2010811801 08/20/2001 21:51:00
2010811802 08/20/2001 22:21:00
2010811803 08/20/2001 22:50:00
2010811804 08/20/2001 23:20:00
1000 08/21/2001 01:11:00
1406 08/21/2001 01:11:00
1027709 08/21/2001 02:06:00
1027710 08/21/2001 02:34:00
2010811603 08/21/2001 03:29:00
Analyst: BJP
'';, •" · ~;sub-' '' ' ', , , ~ , ,,
•,
· Samole Tvoe Analvsis File 10 , , J_ • ·~ :: ' Batch ID , ,
GC/MS Tune A0820102.D 0
Continuing Calibration Check A0820102.D 0
Lab Control Samole A0820103.D 0
Lab Control Sample Duplicate A0820104.D 0
Method Blank A0820106.D 0
Field Samole A0820107.D 0
Field Sample A0820108.D 0
Field Samole A0820109.D 0
Field Sample A0820110.D 0
Field Samole A08201 l l.D 0
Field Samole A0820112.D 0
Field Samole A0820113.D 0
Field Sample A0820114.D 0
Field Sample A0820115.D 0
Field Sample A0820116.D 0
Field Sample A0820117.D 0
Field Sample A0820118.D 0
Field Sample A0820119.D 0
Field Sample A0820120.D 0
Field Samole A0820121.D 0
Field Sample A0820122.D 0
Field Sample A0820123.D 0
Field Sample A0820124.D 0
Field Sample A0820125.D 0
GC/MS Tune A0820129.D 0
Continuing Calibration Check A0820129.D 0
Matrix Spike A0820131.D 0
Matrix Soike Duolicate A0820132.D 0
Field Sample A0820134.D 0
Page 64 of 67
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 13103 continued
,, < ,: < <
, ,.
. Seauence_ . Client Samole ID ,, >: ,; 'f, ~/.·:r:~:<:·
30 0801HBWD999
31 0801HBWW213
32 0801HBWW214
33 zzzzzzzzzz
34 zzzzzzzzzz
35 zzzzzzzzzz
36 zzzzzzzzzz
37 zzzzzzzzzz
Analysis Batch ID: 13307
,
seauence Client Samole ID
1 INSTRUMENT OC
2 INSTRUMENT OC
3 LCS for HBN 13307 fMSV/16401
4 LCSD for HBN 13307 fMSV/16401
5 MB for HBN 13307 fMSV/16401
6 zzzzzzzzzz
7 zzzzzzzzzz
8 0801HBWW228
9 0801HBWW227
10 zzzzzzzzzz
11 zzzzzzzzzz
12 zzzzzzzzzz
13 zzzzzzzzzz
14 zzzzzzzzzz
15 zzzzzzzzzz
16 zzzzzzzzzz
SECTION VI -Batch Summaries -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Anal vs is Spb ..
. Lab Samole ID Date ·· .. Time Samole.Tvoe · Analvsis File ID .. ,, ~-' ' Batch ID
2010811602 08/21/2001 03:57:00 Field Sample A0820135.D 0
2010811604 08/2112001 04:25:00 Field Samole A0820136.D 0
2010811601 08/21/2001 04:54:00 Field Samole A0820137.D 0
2010814901 08/21/2001 05:22:00 Field Samole A0820138.D 0
2010811801 08/21/2001 10:54:00 Field Sample A0820142.D 0
2010811802 08/21/2001 11:35:00 Field Samole A0820143.D 0
2010811803 08/21/2001 12:03:00 Field Samole A0820144.D 0
2010811804 08/21/2001 12:31:00 Field Sample A0820145.D 0
Instrument ID: MSDB Analyst: BJP
Anal.vsis. . Sub··
Lab samole ID Date Time SamoleTvoe Analvsis File ID Batch ID
1000 08/27/2001 17:29:00 GC/MS Tune B0827102.D 0
1406 08/27/2001 17:29:00 Continuing Calibration Check B0827102.D 0
1028426 08/27/2001 17:57:00 Lab Control Sample B0827103.D 0
1028427 08/27/2001 18:25:00 Lab Control Samole Duolicate 80827104.D 0
1028428 08/27/2001 19:20:00 Method Blank B0827106.D 0
2010819814 08/27/2001 19:59:00 Field Samole B0827107.D 0
2010816603 08/27/2001 20:26:00 Field Sample B0827108.D 0
2010811606 08/27/2001 20:56:00 Field Samole B0827109.D 0
2010811605 08/27/2001 21:25:00 Field Sample B0827110.D 0
2010819801 08/27/2001 23:17:00 Field Samole B0827114.D 0
2010819802 08/27/2001 23:45:00 Field Sample B0827115.D 0
2010819803 08/28/2001 00:14:00 Field Samole B0827116.D 0
2010819805 08/28/2001 00:42:00 Field Sample B0827117.D 0
2010819806 08/28/2001 01:11:00 Field Samole B0827118.D 0
2010819812 08/28/2001 01:39:00 Field Sample B0827119.D 0
2010816602 08/28/2001 02:07:00 Field Samole B0827120.D 0
Page 65 of 67
-------------------
-------------------SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 13307
, > : ,. ,.
> s·eauence ClientSamole ID
17 zzzzzzzzzz
18 zzzzzzzzzz
19 zzzzzzzzzz
20 zzzzzzzzzz
21 zzzzzzzzzz
22 zzzzzzzzzz
24 INSTRUMENT QC
25 INSTRUMENT QC
26 zzzzzzzzzz
27 zzzzzzzzzz
28 zzzzzzzzzz
29 zzzzzzzzzz
30 zzzzzzzzzz
31 zzzzzzzzzz
32 zzzzzzzzzz
33 zzzzzzzzzz
34 zzzzzzzzzz
35 zzzzzzzzzz
continued
». ~~;:;!:?~· . , ·: _,:~:;:,,·;,.:~. /;:::·L
SECTION VI-Batch Summaries -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
Lab Samole .ID
2010819401
2010818501
2010818502
2010819804
2010819807
2010816601
1000
1406
1028429
1028430
2010819801
2010819804
2010819807
2010818501
2010818502
2010815801
2010816601
2010816601
· Analvsis · » . Sub·-. ,,,
·oate Time .sarriilie tvoe . Analvsis File: ID · · · , ' ,, ·.Batch ID ''' ,
08/28/2001 02:36:00 Field Samole B0827121.D 0
08/28/2001 03:05:00 Field Sample B0827122.D 0 -
08/28/2001 03:34:00 Field Samole B0827123.D 0
08/28/2001 04:04:00 Field Samole B0827124.D 0
08/28/2001 04:33:00 Field Samole B0827125.D 0
08/28/2001 05:02:00 Field Sample B0827126.D 0
08/28/2001 07:25:00 GC/MS Tune B0827131 0
08/28/2001 07:25:00 Continuing Calibration Check B0827131.D > 0
08/28/2001 11:11:00 Matrix Soike B0827133.D 0
08/28/2001 11:39:00 Matrix Spike Duplicate-B0827134.D 0
08/28/2001 12:36:00 Field Samole B0827136.D 0
08/28/2001 13:04:00 Field Sample B0827137.D 0
08/28/2001 13:32:00 Field Samole B0827138.D 0
08/28/2001 14:01:00 Field Samole B0827139.D 0
08/28/2001 14:29:00 Field Samole B0827140.D 0
08/28/2001 14:57:00 Field Samole B0827141.D 0
08/28/2001 15:26:00 Field Samole B0827142.D 0
08/28/2001 17:34:00 Field Samole B0827145.D .. 0
Page 66 of 67
SECTION VII
Certifications
State/Aaencv
Arkansas Department of Environmental Quality
California Environmental Laboratorv Accreditation Prol!ram I Waste Water/Hazardous Waste
Connecticut Department of Health/Waste Waterffrade Waste. Sewage/Effluent. Soil
Florida Deoartment of Environmental Protection, ComoOAP
Kansas Department of Health and Environment I Solid and Hazardous Waste
Louisiana Deoartment of Environmental Oualitv, ELAP I Waste Water/Hazardous Waste/Air Emissions
Montana Department of Environmental Quality/Petroleum Release Section
New Jersey Deoartment of Environmental Protection
New York State Deoartment of Health /Waste Water/Hazardous Waste/Air
North Carolina Dept. ofNatural Resources & Community Development I Waste Water
Oklahoma Department of Environmental Quality/General Water Oualitv/Sludge
Rhode Island Deoartment of Health/Potable Water/Non-Potable and Waste Water
South Carolina Dept. of Health & Environmental Control
Tennessee UST
Texas(TNRCC)
Texas Department of Public Safetv/Precursor Chemical and Lab Aooaratus
Utah Department of Health I Solid and Hazardous Waste
Wisconsin Deoartment of Natural Resources
US Air Force/ AFCEE
US Army Corns of Engineers <MRD ACE)
US Department of Agriculture I Restricted Soils Permit
US Navv<NFESC)
SECTION VII-Certifications -09/04/2001 14:52
LIMS Workorder: 80396910 [20108116] Hamilton Beach-Proctor Silex
STLAustin
ID#
2411
PH-0761
QA Plan #900481
E-10165
Interim Accreditation
82005
10915
302
8720
127
82003
Participatinl! Laboratorv
3039
RADC
999885260
Participating Laboratorv
Participating Laboratorv
S-42350
Particioatinl! Laboratorv
Page 67 of 67
-------------------
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APPENDIXB
CONTAMINANT CONCENTRATIONS VERSUS TIME
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