IDX GW Monitoring Report Sep 2000 (SF)-OCR

*5951HSSF1066*
1111111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
oocumentType Progress/Monitoring Rpt (PRGMON)
RptSegment 1
OocDate
OocRcvd
Box
Access Level
Division
Section
Program
DocCat
10/9/2000
2/20/2007
SF1066
·PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
State of North Carolina
Department of Environment
and Natural Resources
Washington Regional Office
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Mr. Mario Kuhar
.,.
DIVISION OF WATER QUALITY
GROUNDWATER SECTION
October 9, 2000
Hamilton Beach<> Proctor Silex, Inc.
4421 Water Front Drive
Glen Allen, Virginia 23060
RE: Quarterly Groundwater Sampling
Hamilton Beach/Proctor Silex
Washington, North Carolina -Beaufort County
Groundwater Incident Number -14338
Dear Mr. Kuhar:
IF;}\ -·~ n ,,;,,..-__ __
NCDENR
NoRTH Co.Rouru. DEPARTMe<T OF
ENVIRONMENT ANO N"1"URAI.. REsouRcES
The Washington Regional Office received the above report, prepared by Radian International,
dated November 3, 2000. We appreciate you submitting this report to our office.
Please continue to monitor groundwater quality until four consecutive quarterly monitoring
events reveal contaminant levels below the groundwater standards listed in Title 15A North Carolina
Administrative Code, Subchapter 2L (15A NCAC 2L).
We appreciate your cooperation along with your effort to protect the state's groundwater
resources. Should you have any questions regarding this matter, please don't hesitate to call me at
252-946-6481, extension 335.
Sincerely,
Willie Hardison
Groundwater Supervisor
Groundwater Section
cc: Radian International -PO Box 13000, Research Triangle Park, NC 27709
WaROV"'
943 Washington Square Mall, Washington, North Carolina 27889 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer
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GROUNDWATER MONITORING REPORT
FOR SEPTEMBER 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
Prepared for:
Hamilton Beach<> Proctor-Silex, Inc.
4421 Waterfront Drove
Glen Allen, Virginia 23060
Prepared by:
Radian International
P.O. Box 13000 ·
R-eseareh-Triangle Park, North Carolina 27709-
November 2000
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CERTIFICATION PAGE
GROUNDWATER MONITORING REPORT
FOR SEPTEMBER 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
I, Craig L. Kennedy, a Licensed Geologist in the State of North Carolina, certify that
this report and its contents have been prepared under my direct control and personal
superv1s10n.
650138.0901 Sept2000GW _ Rpt.doc (10/27 /00) 11
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TABLE OF CONTENTS
Certification Page ................................................................................................................ ii
List of Figures ........................................................... : ........................................................ iv
List of Tables ...................................................................................................................... v
1.0 INTRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS ............................................................................................. : ............ 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3.1 Water Level Measurements ................................................................................. 3-1
3 .2 Analytical Results ................................................................................................ 3-1
APPENDIX A GROUNDWATER SAMPLING ANALYTICAL REPORTS
APPENDIX B CONTAMINANT CONCENTRATIONS VERSUS TIME
650138.0901 Sept2000GW _Rpt.doc (10/27/00) iii
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LIST OF FIGURES
1-1 Topographic Map, Hamilton Beach<>Proctor-Silex;Inc.
2-1 Site Map, Washington Facility, Hamilton Beach<>Proctor-Silex, Inc.
3-1 Generalized Groundwater Flow Direction for Hydrogeologic Unit A,
Washington Facility
3-2 Generalized Groundwater Flow Direction for Hydrogeologic Unit B,
Washington Facility
3-3 Approximate Distribution ofTCE in Unit A
3-4 Approximate Distribution ofTCE in Unit B
3-5 Approximate Distribution ofTrichloroethene, D-D'
3-6 · Approximate Distribution ofTrichloroethene, E-E' ·
3-7 Approximate Distribution of cis-1,2-DCE in Unit A
3-8 Approximate Distribution of cis-1,2-DCE in Unit B
3-9 Approximate Distribution of cis-1,2-DCE, D-D'
3-10 Approximate Distribution of cis-1,2-DCE, E-E'
3-11 Approximate Distribution of 1,1-DCE in Unit A
3-12 Approximate Distribution of 1,1-DCE in Unit B
3-13 Approximate Distribution of 1,1-DCE, D-D'
3-14 Approximate Distribution of 1,1-DCE, E-E'
3-15 App_roximate Distrib\ltion of Vinyl Chloride in Unit A
3-16 Approximate Distribution of Vinyl Chloride in Unit B
3-17 Approximate Distribution of Vinyl Chloride, D-D'
3-18 Approximate Distribution of Vinyl Chloride, E-E'
3-19 Approximate Distribution of 1,1,1-TCA in Unit A
3-20 Approximate Distribution of 1,1,1-TCA in Unit B
650138.0901 Sept2000GW _Rpt.doc (10/27/00) iv
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LIST OF FIGURES (Continued)
3-21 Approximate Distribution of 1,1,1-TCA, D-D'
3-22 Approximate Distribution of 1,1,1-TCA, E-E'
3-23 Approximate Distribution of 1,2-DCA in Unit A
3-24 Approximate Distribution of 1,2-DCA in Unit B
3-25 Approximate Distribution of 1,2-DCA, D-D'
3-26 App~oximate Distribution of 1,2-DCA, E-E'
3-27 Approximate Distribution of 1,1-DCA in Unit A
3-28 Approximate Distribution of 1,1-DCA in Unit B
3-29 Approximate Distribution of 1,1-DCA, D-D'
3-30 Approximate Distribution of 1,1-DCA, E-E'
3-31 Approximate Distribution of Toluene in Unit A
3-32 Cross-section Locations
3-33 Location of Surrounding Water Supply Wells
80396902.01 Sept2000GW_Rpt.doc (10/27/00) v
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2-1
3-1
3-2
LIST OF TABLES
Monitoring Well Construction Data for Sampled Wells
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Water Level Measurements and Elevations, September 6, 2000
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-213
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-3 Historical Water Level Elevations at MW-214
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-4 Historical Water Level Elevations at MW-215
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-5 Historical Water Level Elevations at MW-216
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-6 Historical Water Level.Elevations at MW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-7 Historical Water Level Elevations at MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-8 Historical Water Level Elevations at MW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-9 Historical Water Level Elevations at MW-225
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina·
3-10 Historical Water Level Elevations at MW-226
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-11 Historical Water Level Elevations at MW-227
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-12 Historical Water Level Elevations at MW-228
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-13 Historical Water Level Elevations at MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
80396902.01 Sept2000GW_Rpt.doc (10/27/00) vi
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LIST OF TABLES (Continued)
3-14 Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-15 Field Measurements, September 6, and 7, 2000
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-16 Summary of Qualified Groundwater Analytical Results: September 2000
Volatile Organic Compounds by Method 8260B
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-17 Historical Analytical Results for MW-213
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-18 Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-19 Historical Analytical Results for MW-215
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-20 Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-21 Historical Analytical Results for MW-220
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-22 Historical Analytical Results for MW-222
HamiltQn Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-23 Historical Analytical Results for MW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-24 Historical Analytical Results for MW-225
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-25 Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-26 Historical Analytical Results for MW-227
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-27 Historical Analytical Results for MW-228
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
80396902.01 Sept2000GW _Rpt.doc (10/27/00) Vil
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LIST OF TABLES (Continued)
3-28 Historical Analytical Results for MW-230
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-29 Historical Analytical Results for MW-234
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
80396902.01 Sept2000GW _Rpt.doc (10/27/00) Vlll
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1.0 INTRODUCTION
The Hamilton Beach<> Proctor-Silex (HB<>PS) facilify is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HB<> PS since 1990 and previously leased by predecessor companies. The facility was
formerly involved in the final assembly, packaging, and warehousing of small electrical
household appliances.
Since 1992, \Yhen organic compounds were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
_assessment (CSA). The results of the CSA indicated that a plume. of organic compounds is
present in groundwater underlying the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer used at the facility.
A plan for corryctive action at the site has been proposed. Until corrective action
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to
a monitoring program requested and approved by the North Carolina Department of
Environment and Natural Resources, Groundwater Section. The purpose of the monitoring
program is to sample selected downgradient monitoring wells to detect potential migration of the
plume.
Radian International (Radian) conducted groundwater sampling at the facility in
September 2000. The sampling event included the measurement of water levels, temperature,
pH, and specific conductance; and the collection and analysis of samples from thirteen
monitoring wells. This report describes the sampling methods and presents the results for the
quarterly sampling event.
80396902.01 Sept2000GW _Rpt.doc (10/27/00) 1-1
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2.0 FIELD METHODS
Groundwater was sampled on September 6 and 7, 2000, in general accordance
with the methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for
this site.
Thirteen monitoring wells were sampled. They included MW-213 through
MW-216, MW-220, MW-222, MW-224 through MW-228, MW-230, and MW-234. The
locations of the monitoring wells are shown in Figure 2-1. Details of well construction are.
provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using inertial foot-valve pumps, with the
exception of well MW-228 which was purged with a bailer. Temperature, pH, and specific
conductance were measured and the data were recorded in a field notebook. Purging continued
until temperature, pH, and specific conductance stabilized; a minimum of three well volumes
was extracted; or the well was pumped dry. Each of the wells was then sampled immediately
following well purging using the inertial foot-valve pump or bailer.
The groundwater samples were sent by overnight courier to STL in Austin, Texas,
for analysis of volatile organic compounds by EPA Method 8260B.
80396902.01 Sept2000GW _Rpt.doc (10/27/00) 2-1
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3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the thirteen wells sampled and seven additional wells. Maps showing the
generalized direction of groundwater flow in hydrogeologic units A and B are included as
Figures 3-1 and 3-2, respectively. Historical water-level elevations in sampled wells are
included in Tables 3-2 to 3-14.
3.2 Analytical Results
Field measurements of water temperature, pH, and specific conductance are
summarized in Table 3-15. Qualified analytical results are summarized in Table 3-16. The
approximate extent of selected compounds which have been detected at concentrations
exceeding groundwater standards are illustrated in Figures 3-3 through 3-31. Cross-section
locations are shown in Figure 3-32. Both current and historical data were used to approximate
the extent of contaminants. Qualified data sheets and laboratory reports are included in
Appendix A.
No analytes were detected above the groundwater standards in samples from
wells located near the perimeter of the site (MW-220; MW-222, MW-224, MW-225, MW-230,
and MW-234), nor were any analytes detected above the groundwater standards in the sample
from well MW-226, which i~ completed in the confined Limestone Aquifer. Also, no analytes
were detected above groundwater standards in samples collected from wells MW-215 and
MW-216, which are located 120 feet and 350 feet from the source area, respectively.
Concentrations of chemicals exceeding the standards were detected in samples from wells
MW-213, MW-214, MW-227, and MW-228. These four welis are located at, or within 150 feet
of, the source area.
80396902.01 Sept2000GW _Rpt.doc (10/27/00) 3-1
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Historical analytical results for the sampled wells are presented in Tables 3-17 to
3-29, a~d in graphs included as Appendix B. A comparison of the record for wells located ne~r
the perimeter of the site suggests that the plume remains on-site, at least 200 feet from potential
receptors located north of Spring Road (Figure 3-33). The latest results for wells located at the
source area and other interior portions of the site are consistent with earlier results and indicate
no significant changes in chemical concentration and distribution have occurred.
650138.0901 Sept2000GW _Rpt.doc (10/27/00) 3-2 Hamilton Beach<>Proctor-Silex, Inc.
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FIGURES
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TABLES
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Table 2-1
Monitoring Well Construction Data for Sampled Wells
H;amilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Top of Casing
lnstallatihn Elevation Total Depth Screen Interval Filter Pack Bentonite Seal
Well No. Date I (ft. above MSL) (ft. b2s) (ft. b2s)
MW-213 1114/98 28.44 7.5 3 -7.5
MW-214 1/16/98 27.93 21 14.5 -21
MW-215 1/16/98 28.06 10 8.5 -IO
MW-216 5/5/98 32.82 35 26-35
MW-220 5/5/98 31.50 34 25 -34
MW-222 5/6/98 35.11 40 31 -40
MW-224 11113/98 33.43 34 25 -34
MW-225 11/13/98 33.43 10 4-10
MW-226 9/30/98 28.46 75 70-75
MW-227 10/1/98 28.47 25.5 20.5 -25.5
MW-228 9/23/98 28.71 10 3 -IO
MW-230 10/26/98 33.47 14 8 -14
MW-234 6/23/99 35.03 26 17 -26
Monitoring wells 213 through 215 installed by Groundwater Management Associates, Inc.
Monitoring wells 216, 220, and 222 installed by Radian Mobile Field Services.
Monitoring wells 226 through 228 installed by Parratt Wolff, Inc.
Monitoring wells 224, 225, 230, and 234 installed by Probe Technology, Inc.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
(ft. b2s) (ft. b2s)
2.5 -7.5 1.5 -2.5
13.5 -21 12.5 -13.5
8 -10 7-8
25 -35 24-25
24-34 23 -24
30-40 29-30
24-34 23 -24
3 -10 2-3
69 -75 67 -69
19.5 25.5 17.5 -19.5
2-IO 1 - 2
7 -14 5-7
16 -26 13 -16
Grout Seal
(ft. b2s)
0 -1.5
0 -12.5
0-7
0-24
0 23
0-29
0-23
0-2
0-67
0 -17.5
0-1
0-5
0 -13
Table 3-1
Water Level Measurements and Elevations
September 6, 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Measuring Point Water Level
Elevation Elevation
Well (ft above msl)) Depth to Water (ft) (ft above msl)
MW-2018 29.74 1.35 28.39
MW-208 32.li 5.28 26.83
MW-213 28.44 3.66 24.78
MW-214 27.93 3.80 24.13
MW-215 48.06 4.13 23.93
MW-216 32.82 8.70 24.12
MW-217 32.75 6.89 25.86
MW-219 31.83 6.28 25.55
MW-220 31.50 8.60 22.90
MW-221 31.39 8.03 23.36
MW-222 35.11 13.61 21.50
MW-223 35.15 3.94 31.21
MW-224 33.43 7.44 25.99
MW-225 33.43 6.21 27.22
MW-226 "28.46 19.05 9.41
MW-227 28.47 4.02 24.45
MW-228 28.71 3.27 25.44
MW-230 33.47 10.40 23.07
MW-233 34.55 10.53 24.02
MW-234 35.03 9.99 25.04
msl = mean sea level
80396902.0 I Sept2000GW _ Rpt.doc (I 0/27 /00)
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Table 3-2
Historical Water Level Elevations at MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
Mav2, 2000
September.6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
25.54
24.21
NM
NM
26.41
26.33
24.78
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Table 3-4
Historical Water Level Elevations at MW-215
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
Mav2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
(ft. above msl)
24.97
24.19 -NM
NM
25.23
24.84
23.93
Table 3-5
Historical Water Level Elevations at MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
24.39
22.37
NM
NM
24.84
24.83
24.12
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Table 3-7
Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
Mav 13, 1998 22.34
November 16, 1998 19.99
July 1, 1999 20.61
October 20, 1999 24.22
February 2, 2000 23.34
May 2, 2000 23.58
September 6, 2000 21.50
msl = mean sea level
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
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Table 3-8
Historical Water Level Elevations at MW-224
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, ·1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
23.64
24.39
26.88
26.73
26.48
25.99
Table 3-9
Historical Water Level Elevations at MW-225
Hamilton Beach~Proctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
Februarv 2, 2000
Mav2,2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
24.36
24.50
27.24
26.59
26.40
27.22
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Table 3-10
Historical Water Level Elevations at MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
8.43
8.54
11.11
10.23
10.81
9.41
Table 3-11
Historical Water Level Elevations at MW-227
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July l, 1999
October 20, 1999
February 2, 2000
May2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
22.38
NM
25.82
25.88
25.83
24.45
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Table 3-12
Historical Water Level Elevations at MW-228
Hamilton BeachOProctor-Silex, Inc.
Washi~gton, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
September-6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
23.01
NM
NM
24.63
26.36
25.44
Table 3-13
Historical Water Level Elevations at MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July l, 1999
October 20, 1999
February 2, 2000
Mav2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rptdoc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
21.14
21.80
27.71
27.44
26.53
23.07
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
II
Ii
II
'I I
I
I
I
I
I
I
I
I
I
I
I
I
I.
I
I
I
I
I
I
Table 3-14
Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
September 6, 2000
msl = mean sea level
NM =Not measured
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Water Level Elevation
(ft. above msl)
NM
NM
23.24
25.71
25.67
25.56
25.04
I
i
Well Date !.Time
MW-213 917100 I 08:55
MW-214 917100 09:15
MW-215 917100 09:30
MW-216 916100 13:56
MW-220 916100 13:35
MW-222 916100 14:18
MW-224 916100 11:54
MW-225 916100 11.47
11:13
MW-226 916100 11:18
11:23
MW-227 917100 09:50
MW-228 917100 10:05
MW-230 916100 14:40
MW-234 916100 13:20
Table 3-15
Field Measurements
September 6, 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Volume Purged
(Gal) Pur2in2 Criteria
2.0 3 well volumes
9.0 3 well volumes
1.7 Dry
1.0 3 well volumes
0.75 3 well volumes
1.0 3 well volumes
1.0 3 well volumes
0.18 3 well volumes
9.0
13.0 Stabilized parameters
17.0
10.5 3 well volumes
3.5 3 well volumes
0.25 3 well volumes
0.5 3 well volumes
Specific
Temperature Conductance
. (oC) (µS) pH
27.0 370 5.3
22.5 280 5.9
24.7 240 6.2
18.7 420 7.4
18.4 110 4.3
18.6 370 7.2
18.2 290 6.5
22.l 180 4.7
19.8 455 7.5
19.8 455 7.4
19.7 455 7.4
21.0 470 7.2
24.0 220 3.3
20.0 215 4.4
24.0 140 6.4
------------~--~---
--------~--~---~---
Table 3-16
Summary of Qualified Groundwater Analytical Results: May 2000
. Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Washington, North Carolina
Sample ID I MW-213 i
Date of Sampling I 917100
Analyte (µg/L)
Benzene I ND (0.492)
Chloroethane I ND (0.756) I
1, 1-Dichloroethane I 156
1,2-Dichloroethane ' 4.05J
1, 1-Dichloroethene 391
cis-1,2-Dichloroethene 45.1
trans-1,2-Dichloroethene 1.33 J
Ethylbenzene 0.292 J
Methyl t-butyl ether ND (0.469)
Tetrachloroethene 33.1
Tetrahydrofuran ND (4.02)
Toluene ND (0.680)
1, 1, I -Trichloroethane ND (0.331)
1, 1,2-Trichloroethane 2.23J
Trichloroethene 510
1,2,4-Trimethylbenzene ND (0.749)
Vinyl chloride ' 17.8
m&p-Xylene ND (1.37)
o-Xylene 'I 1.66 J
Target analytes not listed were not detected.
Bold values exceed Standards.
ND ( ) =Not detected at specified detection limit.
J = Estimated value.
MW-214
917100
0.280 J
0.6491
159
0.576 J
13.7
11.6
0.683 J
ND (0.110)
ND (0.0938)
ND (0.114)
ND (0.804)
ND (0.136)
ND (0.0662)
ND (0.190)
ND (0.489) U
ND (0.150)
9.35
ND (0.274)
ND (0.143)
U = Not present above the associated level, blank contamination present.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
MW-215 MW-216
917100 916100
ND (0.0492) ND (0.0492)
ND (0.0756) ND (0.0756)
3.16 ND (0,0487)
ND (0.0499) ND (0.0499)
1.75 ND (0.0697)
0.0496 J ND (0.0603)
ND (0.0813) ND (0.0813)
ND (0.0552) ND (0.0552)
0.937 J ND (0.0469)
ND (0.0568) ND (0.0568)
12.2 ND (0.402)
ND (0.0680) ND (0.0680)
ND (0.0331) ND (0.0331)
ND (0.0952) ND (0.0952)
ND (0.116) U ND (0.0905)
ND (0.0749) ND (0.0749)
ND (0.0574) ND (0.0574)
ND (0.137) ND (0.137)
ND (0.0713) ND (0.0713)
MW-220 MW-222
916100 916100
ND (0.0492) ND (0.0492)
ND (0.0756) ND (0.0756)
'ND (0.0487) , .. 0.328 J
ND (0.0499) ~-~ ND (0.0499)
ND (0.0697) 0.0766 J
ND (0.0603) 0.139 J
ND (0.0813) ND (0.0813)
ND (0.0552) ND (0.0552)
ND (0.0469) ND (0.0469)
ND (0.0568) ND (0.0568)
ND (0.402) ..• ND (0.402)
ND (0.0680) ND (0.0680)
ND (0.0331) ND (0.0331)
ND (0.0952) ND (0.0952)
ND (0.0905) ND (0.0905)
ND (0.0749) ND (0.0749)
ND (0.0574) ND (0.0574)
ND (0.137) ND (0.137)
ND (0.0713) ND (0.0713)
Sample ID M)V-224
Date of Sampling 916100
Analyte (µg/L) I
Benzene ND(0.0492)
Chloroethane ND ~0.0756)
1, 1-Dichloroethane ND ~0.0487)
1,2-Dichloroethane ND (0.0499)
1, 1-Dichloroethene ND (0.0697)
cis-1,2-Dichloroethene ND (0.0603)
trans-1,2-Dichloroethene ND (0.0813)
Ethylbenzene ND (0.0552)
Methyl t-butyl ether ND (0.0469)
Tetrachloroethene ND (0.0568)
Tetrahydrofuran ND(0.402)
Toluene ND (0.0680)
l, 1, I -Trichloroethane ND (0.0331)
l, 1,2-Trichloroethane ND (0.0952)
Trichloroethene ND (0.0905) U
1,2,4-Trimethylbenzene ND (0.0749)
Vinyl chloride ND(0.0574)
m&p-Xylene ND (0.137)
o-Xylene ND (0.0713)
Target analytes not listed were not detected.
ND ( ) =Not detected at specified detection limit.
Bold values exceed Standards.
J = Estimated value.
Table 3-16 (Continued)
MW-225 MW-226 MW-227
916100 916100 917100
ND (0.0492) ND(0.0492) ND (2.46)
ND (0.0756) ND (0.0756) 26.3
ND (0.0487) ND (0.0487) 1,340
ND (0.0499) ND(0.0499) ND(2.50)
ND (0.0697) ND (0.0697) 249
ND (0.0603) ND (0.0603) 211
ND (0.0813) ND(0.0813) ND (4.06)
ND (0.0552) ND (0.0552) ND (2.76)
ND (0.0469) ND (0.0469) ND (2.34)
ND (0.0568) ND (0.0568) ND (2.84)
. ND (0.402) ND (0.402) ND (20.1)
ND (0.0680) ND (0.0680) 8.9iJ
ND (0.0331) ND (0.0331) 1,220
ND (0.0952) ND (0.0952) ND (4.76)
ND (0.0905) ND (0.0945) U ND(36.9)U
ND (0.0749) ND (0.0749) ND (3.74)
ND (0.0574) ND (0.0574) ND(2.87)
ND (0.137) ND (0.137) ND (6.85)
ND (0.0713) ND (0.0713) ND (3.56)
U =Not present above the associated level, blank contamination present.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
MW-228 MW-230 MW-234
917100 916100 916100
ND (98.4) ND (0.0492) ND (0.0492)
ND (151) ND (0.0756) ND (0.0756)
11,900 ND (0.0487) ND (0.0487)
ND (99.8) ND (0.0499) ND (0.0499)
31,200 ND (0.0697) ND (0.0697)
2,380 0.102 J ND (0.0603)
ND (163) ND (0.0813) ND (0.0813)
506J ND (0.0552) ND (0.0552)
ND (93.8) ND (0.0469) ND (0.0469)
ND (114) ND (0.0568) ND (0.0568)
ND (804) ND (0.402) ND (0.402)
1,340 0.126 J ND (0.0680)
64,400 ND (0.0331) ND (0.0331)
ND{l90) ND (0.0952) ND (0.0952)
11,500 ND (0.355) U ND (0.0905)
933J ND (0.0749) ND (0.0749)
ND (115) ND (0.0574) ND (0.0574)
1,520 J ND (0.137) ND (0.137)
1,240 ND (0.0713) ND (0.0713)
--------~----------
------~----~----~-~
Groundw~ter
Analyte Standard
Benzene 1
n-Butylbenzene_ 70
sec-Butylbenzene 70
Chloroform 0.19
1,2-Dichlorobenzene 620
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
Ethylbenzene 29
Isopropylbenzene 70
p-Isopropyltoluene -
Napthalene 21
Tetrachloroethene 0.7
Tetrahydrofuran -
Toluene 1000
1, 1, I-Trichloroethane 200
1, 1,2-Trichloroethane -
Trichloroethene 2.8
Table 3-17
Hist~rical Analytical Results for MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
May November July October
1998 1998 1999 1999
NS 0.724 NS NS
NS 0.240 NS NS
NS 0.315 NS NS
NS 0.793 NS . NS
NS 0.642 NS NS
NS 351 NS NS
NS 7.02 NS NS
NS 867 NS NS
NS 39.3 NS NS
NS 2.22 NS NS
NS 2.03 NS NS
NS 0.618 NS NS
NS ND (0.106) NS NS
NS 15.7 J NS NS
NS 61.3 NS NS
NS 7.63 J NS NS
NS 1.48 NS NS
NS. 1.09 NS NS
NS 6.03 NS NS
NS 515 NS NS
February May September
2000 2000 2000
ND (0.984) 0.495 J ND (0.492)
ND (1.28) 0.184 J ND_ (0.642) . """""
ND (1.49) 0.268 J ~: ND (Q.745)
ND (1.34) 0.577 ND .(0.670)
ND (1.84) 0.349 J ND (0.920)
245 178 156
6.12 J 4.49 .4.05
492 401' 391
40.8 40.6 --45.1 ..
ND (1.63) 1.41 ·I.33 J
ND (1.10) 0.727 0.292 J
ND (0.948) 0.400 J ND (0.474)
ND (904) 0.182 J ND (0.452)
ND (2.12) 16.7 ND{l.06)
44.4 34.4 33.1
ND (8.4) ND (0.402) ND (4.02)
ND (1.36) 0.335 J ND (0.680)
ND (0.662) 0.928 ND (0.331)
2.16 J 3.17 2.23 J
446 479 510
Groundwa~er May
Analvte Standard 1998
Trichlorofluoromethane 2100 ' NS
1,2,4-Trimethylbenzene 350 NS
1,3,5-Trimethylbenzene 350 NS
Vinvl chloride 0.015 I NS
m&p-Xylene 530 NS
o-Xylene 530 I NS I
I
Target analytes not listed wer~ not detected.
All samples reported in micrograms per liter.
J = Estimated value. ,
ND= Not detected at (detection limit).
NS = Not sampled.
la c:\hamilton\washington\csa-rpt (10/27/00)
Table 3-17 (Continued)
November July
1998 1999
0.575 NS
ND (0.0952) NS
ND (0.0800) NS
38.7 NS
1.57 NS
3.43 NS
October February May September
1999 2000 2000 2000
NS ND (4.16) 1.26 ND (2.08) .,
NS ND (1.50) 0.509 J ND (0.749)
NS ND (0.872) 0.248 J ND (0.436)
NS 29.3 16.0 17.8
NS ND (2.74) 0.935 J ND (1.37)
NS ND (1.43) 1.59 1.66 J
- - -·-- --· -·-- -~ - - - --\ - -
-------------------
Analyte
Groundwa~er Standar~
Benzene 1 :
Chloroethane 2800
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
Table 3-18
Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc.
Wash~ngton, North Carolina
May November July October·
1998 1998 1999 1999
NS 0.172 J NS NS
NS 0.485 J NS NS
NS 108 NS NS
NS 0.303 J NS NS
NS 8.16 NS NS
NS 6.86 NS NS
NS 0.478 NS NS
February
2000
"0.315 J
0.904
179
0.633
13.8
11.7
0.701
p-Isopropyltoluene -NS 0.181 J NS NS ND (0.0452)
Trichloroethene 2.8 NS
Vinyl chloride 0.015 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value. '
ND= Not detected at (detection limit).
NS = Not sampled.
ND (0.587) U NS
8.84 NS
U = Not present above the associated level; blank contamination is present.
80396902.01 Sept2000GW_Rpt.doc (10/27/00)
NS 0.289 J
NS 11.5
May September
2000 2000
0.304 J 0.280 J
0.705 0.649 J
173 159
0.607 0.576 J
15.4 13".7
12.0 11.6
0.794 0.683 J
ND (0.0452) ND (0.0904)
0.494 J ND (0.489) U
9.73 9.35
Table 3-19
Historical Analytical Results for MW-215
Hamilton Beach¢Proctor-Silex, Inc .
Groundwate,r May
Analyte Standard I 1998
Benzene 1 NS
1, 1-Dichloroethane 700 NS
1, 1-Dichloroethene 7 NS
cis-1,2-Dichloroethene 70 NS
Ethylbenzene 29 NS
Methyl t-butyl ether 200 NS
Tetrahydrofuran -NS
Trichloroethene 2.8 NS
Vinyl chloride 0.015 NS
m&p-Xylene 530 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
. Washington, North Carolina
November July October
1998 1999 1999
0.0963 J NS NS
4.30 NS NS
3.85 NS NS
ND(0.104) U NS NS
0.0601 J NS NS
1.22 NS NS
58.6 NS NS
ND (0.322) U NS NS
0.381 J NS NS
0.0885 J NS NS
U = Not present above the associated level; blank contamination is present.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
February
2000
0.114 J
4.07
3.02
0.0401 J
ND (0.0552)
ND (0.0469)
19.1
0.138 J
ND (0.0574)
ND (0.137)
May September
2000 2000
ND (0.0492) ND (0.0492)
3.43 3.16
1.93 1.75
0.0409 J 0.0496 J
ND (0.0552) ND (0.0552)
1.10 0.937 J
15.0 12.2
0.124J ND (0.116) U
ND (0.0574) ND (0.0574)
ND (0.137) ND (0.137)
--------~---~------
------------~·------
Table 3-20
Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater j May November
Analvte Standard t 1998 1998
Toluene 1000 i 0.171 ND (0.0522) UJ
I
Target analytes not listed wertr not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detect~on limit).
NS = Not sampled.
UJ = Not detected and the detection limit is estimated.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
July October
1999 1999
NS NS
February
2000
ND (0.0680)
May September
. 2000 2000
ND (0.0680) ND (0.0680)
Table 3-21
Historical Analytical Results for MW-220
Hamilton BeachOProctor-Silex, Inc.
Groundwater
I
May
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
Methyl t-butyl ether 200 ND (0.0365)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
Washington, North Carolina
November July October
1998 1999 1999
ND (0.0547) 0.426 J 0.162
ND (0.0365) UJ ND (0.0334) ND (0.0512)
UJ = Not detected and the detection limit is estimated.
80396902.0 l Sept2000GW _ Rpt.doc (I 0/27 /00)
February May September
2000 2000 2000
ND (0.0484) UJ ND (0.0484) ND (0.0484)UJ
. ND (0.0469) 0.441 J ND (0.0469)
-----------~-------
-------------------
Table 3-22
Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater May
Analvte Standard 1998
Carbon disulfide 700 : ND (0.0547)
1, 1-Dichloroethane 700 I ND (0.0576) I '
1,1-Dichloroethene 7 ! 0.0908 J
cis-1,2-Dichloroethene 70 I ND (0.0383)
Toluene 1,000 0.156 J
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
November
1998
ND (0.0547)
ND (0.0576)
ND (0.0715)
ND (0.223) U
ND (0.0522)
UJ = Not detected and the detection limit is estimated.
U =Not present above the associated level, blank contamination present.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
July October
1999 1999
0.388 J 0.0944
ND(0.0736) ND (0.0588)
ND (0.102) ND <0.0819)
ND (0.0595) ND (0.0407)
ND (0.0766) ND <0.0645)
February May September 2000 2000 2000
ND <0.0484) UJ ND <0.0484) ND <0.0484) UJ
ND(0.0487) 0.338 J 0.328 J
ND (0.0697) ND(0.279)U 0.0766 J
ND <0.0603) ND <0.0603) 0.139 J
ND (0.0680) ND (0.0680) ND (0.0680)
Groundwater ~fay
Analyte Standard ~998
Table 3-23
Historical Analytical Results for MW-224
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November July October
1998 1999 1999
February
2000
Carbon disulfide 700 ;NS ND (0.0547) 2.22 2.72 ND (1.05) UJ
Toluene 1,000 'NS ND(0.0522)
I I Target analytes not listed were not detected.
All samples reported in micro&rams per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
UJ = Not detected and the detection limit is estimated.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
ND(0.0766) ND(0.0645) (0.0680)
May September
2000 2000 .
ND (0.334) U 0.350 J
0.0542 J (0.0680)
-----------------~-
------------~------
Table 3-24
Historical Analytical Results for MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater ~ay November
Analyte Standard 98 1998
Carbon disulfide 700 NS ND (0.0547)
Chloroform 0.19 NS ND (0.0480)
Target analytes not hsted werF not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
UJ = Not detected and the detection limit is estimated.
80396902.0 I Sept2000GW _ Rpt.doc (I 0/27 /00)
July October
1999 1999
ND (0.864) 0.0691
ND (0.0424) 0.171
February
2000
ND (0.0484) UJ
ND (0.0670)
September
May2000 2000
ND (0.0484) ND (0.0484) UJ
ND (0.0670) ND (0.0670)
Groundwater May
Analyte Standard 199,8
Carbon disulfide 700 NS
I I
Table 3-25
Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November July October February
1998 1999 1999 200
ND (0.0547) ND (0.864) 0.0950 ND (0.0484) UJ
Target analytes not listed were not detected.
All samples reported in microgra,ms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
NS = Not sampled.
UJ = Not detected and the detection limit is estimated.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
May September
2000 2000
ND (0.0484) UJ 0.210 J
-------------------
-------------------
Groundw~ter May
Analyte Standar4t 1998
Acetone 700 I NS
Benzene I NS
2-Butanone (MEK) 170 NS
n-Butylbenzene 70 NS
Carbon disulfide 700 NS
Carbon tetrachloride 0.3 NS
Chloroethane 2800 NS
Chloroform 0.19 NS
1, 1-Dichloroethane 700 NS
1,2-Dichloroethane 0.38 NS
1, 1-Dichloroethene 7 NS
cis-1,2-Dichloroethene 70 NS
trans-1,2-Dichloroethene 70 NS
1, 1-Dichloropropene NS -
Ethylbenzene 29 NS
Isopropylbenzene 70 NS
p-Isopropyltoluene -NS
Methyl t-butyl ether 200 NS
Methylene chloride 5 NS
Napthalene 21 NS
n-Propylbenzene 70 NS
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Table 3-26
Historical Analytical Results for MW-227
Hamilton BeachOProctor-Silex, Inc.
· Washington, North Carolina
November July October February
1998 1999 1999 2000
29.9 J NS NS ND (5.72)
0.668 J NS NS ND (0.984)
42.5 J NS NS ND (3.58)
0.437 J NS NS ND (1.28)
0.573 J NS NS ND (0.968)
ND (0.0576) UJ NS NS ND (1.73)
2.14 J NS NS ND (1.51)
1.64J NS NS ND (1.34) ·
4,620 NS NS 844
19.5 J NS NS 4.40 J
705 NS NS 108
228 NS NS 105
3.66 J NS NS ND (1.63)
ND (0.0444) UJ NS NS ND (0.928)
3.58 J NS NS ND (9.38)
. 0.392 J NS NS ND (0.948)
0.194 J NS NS ND (0.904)
ND (0.0365) UJ NS NS ND (0.938)
ND (l.13)UJ NS NS ND (1.59)
.. 3.73 J NS NS ND (2.12)
2.25 J NS NS ND (l.77)
May September
2000 2000
19.1 J ND (14.3) UJ
0.622 J ND (2.46)
40.2J ND (8.95)
ND (0.0642) UJ ND (3.21)
ND (0.0484) UJ ND (2.42) UJ
26.2J ND (4.34) UJ
14.6 J 26.3
1.17 J ND (3.35)
3,360 1,340
20.2 ND (2.50)
644 249
381 211
7.93 J ND (4.06)
0.182 J ND (2.32)
0.454 J ND (2.76)
ND (0.0474) UJ ND (2.37)
ND (0.0452) UJ ND (2.26)
0.322 J ND (2.34)
0.982 u ND (3.98) U
ND (0.982) UJ ND (5.30)
ND (0.0886) UJ ND (4.43)
Table 3-26 (Continued)
Groundw~ter May
I Analyte Standa~d 1998
1, 1,2,2-Tetrachloroethane 0.17 ' NS
Tetrachloroethene 0.7 NS
Toluene 1000 i NS
1, 1, I-Trichloroethane 200 I NS
I, 1,2-Trichloroethane -I NS
Trichloroethene 2.8 I NS
I
1,2,4-Trimethylbenzene 350 I NS
1,3,5-Trimethylbenzene 350 NS
Vinyl chloride 0.15 NS
m&p-Xylene 530 NS
o-Xylene 530 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
November
1998
ND (0.102) UJ
1.41 J
29.6 J
3,200
3.20 J
810
10.8 J
3.37 J
5.70J
8.78 J
8.91 J
U =Not present above the associated level, blank contamination present.
UJ = Not detected and the detection limit is estimated.
80396902.01 Sept2000GW_Rpt.doc (10/27/00)
July October
1999 1999
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
February May September
2000 .. 2000 2000
ND (1.58) 1.48 J ND(4.74)
ND (1.14) ND (0.0568) UJ ND (2.84)UJ
3.56 J 13.8J 8.92 J
310 2,440 J 1,220
ND (1.90) 2.95 J ND (4.76)
12.9 48.9 J ND (36.9)U
ND (1.50) 0.720 J ND (3.74)
ND (0.872) 0.646 J ND (2.18)
ND (1.15) 5.51 J ND (115)
ND (2.74) 0.956 J 1,520 J
ND (1.43) 0.995 J 1,240
-------------------
-------------------
Groundwater
Analyte I Sta.ndard
Acetone voo
Benzene • 1
2-Butanone (MEK) 170
n-Butylbenzene 70
sec-Butylbenzene 70
Carbon tetrachloride 0.3
Chloroethane 2800
Chloroform 0.19
Chloromethane 2.6
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
1, 1-Dichloropropene -
Ethylbenzene 29
2-Hexanone -
Isopropylbenzene 70
p-Isopropyltoluene -
Methyl t-butyl ether 200
4-Methyl-2-pentanone (MIBK)
Napthalene 21
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
Table 3-27
Historical Analytical Results for MW-228
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
May November July October February
1998 1998 1999 1999 2000
NS 307 J NS NS ND (1,430)
NS 51.3 J NS NS ND (246)
NS 21.3 J NS NS ND (895)
NS 15.6 J NS NS ND (321)
NS 5.27 J NS NS ND (372)
NS 42.2J NS NS ND (434)
NS 74.7 J NS NS ND (378)
NS 12.8 J NS NS ND (335)
NS ND (0.0521) UJ NS NS ND (410)
NS· 24,100 NS NS 16,200
NS 96,500 NS NS 71,800
NS 3,330 NS NS 1,970 J
NS 24.2J NS NS Nb (406)
NS ND (0.0444) UJ NS NS ND (232)
NS 544 NS NS 414J
NS 45.1 J NS NS ND (835)
NS 41.5 J NS NS ND (237)
NS 6.80 J NS NS ND (226)
NS 5.21 J NS NS ND (234)
NS 12.3 J NS NS ND (422)
NS 608 NS NS ND (530)
May September
2000 2000
360 J ND (572) UJ
56.5 J ND (98.4)
382 J ND (358)
9.88 J ND (128)
7.96J ND (149)
26.2 J ND (173) UJ
89.8 J ND (151)
9.62J ND (134)
1.33 J ND (164) UJ
14,500 11,900
53,400 31,200
2,360 2,380
17.0 J ND (163)
1.51 J ND (92.8)
555 J 506 J
38.8 J ND (334)
33.7 J ND (94.8)
ND (0.0452) UJ ND (90.4)
20.8 J ND (93.8)
17.5 J ND (169)
246 J ND (212)
Groubdwater May I Analyte Standard 1998
n-Propylbenzene 70 NS
1, l, 1,2-Tetrachloroethane -NS
1, 1,2,2-Tetrachloroethane 0.17 NS
Tetrachloroethene 0.7 NS
Toluene 1000 NS
1, 1, I -Trichloroethane 400 NS
1, 1,2-Trichloroethane -NS
Trichloroethene 2.8 NS
Trichlorofluoromethane 2100 NS
l ,l ,2-Trichlorotrifluoroethane 210,000 NS
1,2,4-Trimethylbenzene 350 NS
1,3,5-Trimethylbenzene 350 NS
Vinyl chloride 0.15 NS
m&p-Xylene 530 NS
o-Xylene 530 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
Table 3-27 (Continued)
November July October
1998 1999 1999
200 NS NS
0.810 J NS NS
0.688 J NS NS
30.5 J NS NS
1,460 NS NS
173,000 NS NS
49.3 J NS NS
22,800 NS NS
12.7 J NS NS
ND (0.0986) NS NS
1,270 NS NS
309 NS NS
314 NS NS
1,540 NS NS
1,330 NS NS
ND= Not detected at (detection limit).
NS = Not sampled.
VJ= Not detected and the detection limit is estimated.
80396902.01 Sept2000GW _Rpt.doc (10/27/00)
February May September
2000 2000 2000
ND (443) 302 J ND (177)
ND (474) 0.844 J ND (190)
ND (396) ND (0.0792) UJ ND (158)
ND (284) 32.4 J ND (114)
1,610 J 1,520 1,340
135,000 121,000 J 64,400
ND (476) 38.0 J ND (190)
15,000 13,300 11,500
ND (1,040) 8.12 J ND (416)
ND (383) 0.947 J ND (153) UJ
1,220 J 1,190 J 933 J
ND (218) 407 J ND (87.2)
ND (287) 194 J ND (l 15)
1,760 1,680 J 1,520 J
1,370 1,350 1,240
-------------------
-------------------
Table 3-28
Historical Analytical Results for MW-230
Hamilton BeachOProctor-Silex, Inc.
Groundwater May
I' Analyte Standard 1998
1, 1-Dichloroethane 700 I NS I
1, 1-Dichloroethene 7 1 · NS
Cis-1,2-Dichloroethene 70 I NS
Toluene 1,000' NS
Trichloroethene 2.8 I NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
November July October
1998 1999 1999
ND (0.0576) ND (0.0736) 0.265
ND (0.306) U ND (0.102) 0.133
ND (2.67)U ND (0.0595) 0.304
ND (0.0522) 0.286 ND (0.309) U
ND (2.05) U ND (0.0929) 0.921
U = Not present above the associated level; blank contamination is present.
80396902.01 Sept2000GW _Rptdoc (10/27/00)
February May Septembei:
2000 2000 2000
0.189 J ND (0.348) U ND (0.0487)
0.148 J 0.593 ND (0.0697)
0.354 J 0.573 0.102 J
0.284 J 0.0826 J 0.126 J --
0.661 J 1.11 ND (0.355) U
Table 3-29
Historical Analytical Results for MW-234
Hamilton. BeachOProctor-Silex, Inc.
Groundwater ~ay November
Analvte Standard l998 1998
Carbon disulfide 700 ·NS NS
1, 1-Dichloroethene 7 1NS NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
July October February
1999 1999 2000
ND (0.864) 0.0600 ND (0.0484) UJ
ND (0.102) ND (0.0819) ND C0.0697)
UJ = Not detected and the detection limit is estimated.
80396902.01 Sept2000GW_Rpt.doc (10/27/00)
May September
2000 2000
ND (0.0484) ND (0.0484) UJ
0.145 J ND (0.0697)
-------------------
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APPENDIX A
GROUNDWATER SAMPLING ANALYTICAL REPORTS
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QUALIFIED DATA
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Introduction
Hamilton Beach<>Proctor-Silex, Washington, NC
Data Validation Report
URS-Radian, October 2000
URS-Radian collected thirteen groundwater samples (0900HBWW-213 through -216, -220 -222,
-224 through -228, -230, and -234) and two field duplicates at the Hamilton Beach<>Proctor Silex facility
in Washington, NC on September 6 and 7, 2000. The samples were submitted to Severn Trent Laboratories
(STL) in Austin, Texas for the determination of volatile organic compounds (VOC) by SW-846 Method
8260B. A trip blank was included with each shipment of samples to the laboratory for the analysi$ of
voe.
Radian reviewed the analytical results, which were reported by th~ laboratory under work order numbers
20009024 and 20009035. The data evaluation was modeled after the National Functional Guidelines for
Organic Data Review (EPA, October 1999). Accuracy was determined from the review of holding times,
spike recoveries, tuning result, continuing calibration results, and blank contamination. Precision was
based on the evaluation of field and laboratory duplicate results. Sample results have been appropriately
qualified based on the criteria of the data review process. The results of the data evaluation are
suinmarized below.
Sample Condition upon Receipt and Holding Times
All samples were received intact and in good condition by STL on September 7 and 8, 2000. The
temperature of the sample containers upon receipt at the laboratory was within laboratory specification
limits of2-6°C. Except for the trip blank received September 8, air bubbles were not observed any volatile
organic analysis (VOA) vials. A small air bubble (I-millimeter) was observed in one of two VOA vials
received for Trip Blank 2. Qualification of the data is not required since vials were available for analysis
that did not contain air bubble greater than 6 mm in diameter.
Technical hold times were assessed by comparing the sampling dates with that of the analysis date.
Samples were analyzed for VOC within EPA-established holding times of seven days for unpreserved
samples.
Calibration
Gas chromatograph/mass spectrometer (GC/MS) instrument tuning and performance checks are performed
to ensure the instrument's ability to provide appropriate mass-resolution, identification, and sensitivity. All
samples were analyzed for VOC within twelve hours of the performance check standard. The tuning
compound mass-ion abundance criteria for the VOA were reported within control limits.
Control limits-for initia:hm:d-continuing calibrations are establislred to ensure that the instrument is capable
of producing accurate quantitative and qualitative data at the beginning and throughout each of the
analyses. Since the results of the initial calibration were not included in the laboratory report, the
evaluation was based on the review of the continuing calibration data. Laboratory specifications were met
during all volatile organic continuing calibrations conducted on instrument MSDA; however, project
specifications of 80-120% recovery were not met for the following target analytes:
Date of
Continuing
Calibration Results
September 8 Acetone (77%), acrolein (44%), bromomethane (66%), carbon disulfide·
@14:09 (72%), carbon tetrachloride (74%R), chloromethane (70%), 3-
0900 HB-PS Wash DE.doc
Page 1 of3
10/27/00
Associated
samples
All samples
analyzed on
Date of
Continuing Associated
Calibration Results samples
chloropropene (63%), trans-1,4-dichloro-2-butene (48%), instrument
dichlorodifluoromethane ( 48% ), hexachloro-1,3-butadiene (133%R), MSDA.
iodomethane (73%), naphthalene (125%), 1,2,3-Trichlorobenzene (159%),
1,2,4-trichlorobenzene ( 13 5% ), l, 1,2-trichlorotrifluoroethane (71 % ).
September 11 Acrolein (76%), carbon disulfide (168%), dichlorodifluoromethane September
@14:07 (140%), trichlorofluoromethane (152%). 11 analysis
of Trip
Blank 1
Results for the compounds where the recovery was less than 80% during the continuing calibration. have
been qualified as estimated (J, UJ) in associated samples. Positive sample results were qualified as
estimated (J) when the recovery exceeded 120% in the continuing calibration.
Blank Contamination
Laboratory blanks are clean liquid and/or solid matrix samples prepared by the analytical laboratory and
analyzed in the same manner as the field samples. Laboratory blanks are used to ensure that the field
samples are not contaminated during the sample preparation, sample analysis, or from previous samples
(instrument carry-over). Trip blanks are analyte-free water samples that accompany volatile investigative
samples during all stages of shipment, storage, and analysis. The trip blanks are used to assess the potential
for artificial introduction of volatile compounds into the investigative samples during the transportation and
sample handling processes.
Methylene chloride, a common laboratory blank contaminant, was detected at a concentration of2.27 parts
per billion (ppb) in the laboratory blank. Hexachloro-1,3-butadiene (0.326 J ppb), 1,2,3-trichlorobenzene
(0.902 J ppb), 1,2,4-trichlorobenzene (0.425 J ppb), and trichloroethene (0.894 J ppb) were also detected in
the laboratory blank. VOC were not detected in either trip blank. Sample results that were not
significantly greater (ten times for methylene chloride, five times for all others) than that detected in the
blanks have been qualified due to the presence of blank contamination. Affected results have been flagged
"ND" and detection limits elevated to the amount present in the sample and flagged with a "U".
Surroeate Spikes
Surrogate compound percent recoveries are used to assess extraction efficiencies, possible matrix effects,
and overall analytical accuracy during organic analyse~.
Acceptable sample results were obtained for the surrogate spikes during the VOA of all project samples.
Surrogate spike criteria were not met during the September 8 analysis of Trip Blank 1. The recovery (84%)
for the surrogate toluene-d8 was slightly less than laboratory specification limits of 87-113%. The volatile
organic results from the September 8 analysis of Trip Blank 1 have been qualified as estimated (J, UJ).
Laboratory Control Samples
Laboratory control samples (LCS) are blank samples fortified (spiked) with known concentrations of
analyte of interest. The percent recoveries and/or duplicate results of the LCS and their duplicates are used
to assess extraction efficiencies and overall analytical accuracy and precision.
Laboratory specifications were met during all LCS analyses, except September 8. The relative percent
difference (18%) between the LCS and its duplicate was greater than laboratory specification limits (16%)
for 1,3-dichloropropane. Associated sample results were qualified as estimated (J, UJ). In addition, the
LCS and LCSD recovery (169 and 170%) for 1,2,3-trichlorobenzene was greater than the upper control
0900 HB-PS Wash DE.doc
Page 2 of3
10/27/00
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limit of 140%. Qualification of the data was not warranted since 1,2,3-Trichlorobenzene was not detected
in any samples.
Project1 specifications were met for most target analytes during the LCS analyses of September 8 and 11.
The recovery for carbon disulfide (153 and 155%) and dichlorodifluoromethane (48 and 49%) were not
within 60 to 140% of the true value di.iring the LCS analyses conducted September 8. Positive carbon
disulfide results for samples that were associated with the September 8 LCS analyses were qualified as
estimated (J). Associated positive and non-detect sample results for dichlorodifluoromethane were
qualified as estimated (J) and unusable (R), respectively.
Matrix Spikes
Matrix spikes (MS) are samples spiked with known concentrations of analytes of interest. MS percent
recoveries and duplicate results are used to assess extraction efficiencies, possible matrix effects, and
overall analytical accuracy and precision.
The criteria for precision were met during the volatile organic MS and MS duplicate (MSD) analysis of
sample 0900HBWW226. The recoveries of the MS and MSD analysis were met for all analytes, except as
follows:
Analyte Recovery,% Lab Specification Action
Limits, %R
Acrolein 39 and38 70-130 UJ Non-detect result in parent sample
3-Chloropropene 62 (MSD) 70-130 No action, only one of the two
recoveries did not meet lab specs.
trans-1,4-Dichloro-2-butene 55 and49 70-130 UJ Non-detect result in parent sample
1,2,3-Trichlorobenzene 147 and 146 66-140 None, analyte was not detected in
parent sample.
Field Duplicates
Field duplicate ·samples are used to demonstrate acceptable precision during the sample collection process.
After considering blank contamination, acceptable precision was observed during the analysis of field
duplicate' samples 0900HBWW224 and 0900HBWD998, and 0900HBWW227 and 0900HBWD999.
Sample Results
Sample results tliat are within the calibration range of the least diluted analysis are considered rn'ore
accurate than those obtained from a more diluted analysis. Less accurate analytical results have been
flagged unusable (R).
The laboratory flagged s~ple results less than the practical quantitation limit and sample detection limit
with a J and U, respectively. All positive sample results that are less than the practical quantitation limit
are considered estimated (J).
1 The recovery of either the LCS or LCSD must be within 60-140%.
0900 HB-PS Wash DE.doc
Page 3 of3
10/27/00
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
.
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
1-Chlorohexane )
Client Sample ID .
Lab Sample ID ·
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepa~ed
DatefTime Analyzed
Dilution Factor I
Instrument ·
Units ·
CAS
67-64-1
75-05-8.
!07-02-8
!07-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
!04-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
AQueous
Received
NA
09/06/2000 12:05
09/08/2000 19:45
09/08/2000 19:45
1.0000
MSDA
U!!/L
Cone Flaa DL
ND \A.::S 0.286
ND 1.67
ND \A.-:S 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND LA. '3 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
0.413 J 0.0484
ND \A.-:S 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N (20009024) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 .. 2000902406
AQueous AQueous
Received Received
NA NA
09/06/2000 14:00 09/06/2000 13:40
09/08/2000 21 :09 09/08/2000 20:41
09/08/2000 21 :09 09/08/2000 20:41
1.0000 1.0000
MSDA MSDA
U!!./L ug/L
Cone Flan DL RL Cone Flaa DL
ND V-3 0.286 0.000 ND LAS 0.286
ND 1.67 0.000. ND 1.67
ND \,l:l 0.983 0.000 ND I.>..:! 0.983
ND 0.0901 0.000 ND 0.0901
ND 0.0492 0.000 ND 0.0492
ND 0.0622 0.000 ND 0.0622
ND 0.139 0.000 ND 0.139
ND 0.0683 0.000 ND 0.0683
ND 0.136 0.000 ND 0.136
ND \,A.:! 0.106 0.000 ND \A-:S 0.106
ND 0.179 0.000 ND 0.179
ND 0.0642 0.000 ND 0.0642
ND 0.0745 0.000 ND 0.0745
ND 0.0958 0.000 ND 0.0958
ND v...:S 0.0484 0.000 ND UJ 0.0484
ND 1.1.;:) 0.0867 0.000 ND U.J 0.0867
ND 0.0839 0.000 ND 0.0839
ND 0.0473 0.000 ND 0.0473
ND 0.0756 0.000 ND 0.0756
ND 0.0670 0.000 ND 0.0670
ND 0.113 . 0.000 ND 0.113
Page 4
Sample n•sufll lum• lx•en t/11ttlified by Rmlimt /mcnwtioiw/ basi•tl 011 lit<' c·n11•ri11 of the t/11111 re~·ic•n• process, which il 11101/dc1/ 11jia tht' Co111rnc1 l.11/xm//01:1• l'rogrn111 National 1-'1111cti111111/ G11itldi111•,
for Organic am/ /11org1mic /)11/a Re1•if•11· (t l.S: £1'.-f. October 199911111/ /·cbrrrm:r 1994. r·c•spu111·e(1·J. ·
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of SS
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethanc
3-Ch loroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloropropane 96-12-8
Dibromoch loromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1.3.-Dich lorobenzene 541-73-1
Di ch lorodi fluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
I 3-Dichloropropane 142-28-9
2 2-Dichloroorooane 594-20-7
1.1-Dichloropropene 563-58-6
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cis-1 3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroprooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
Cone Flaa DL
ND ~:s 0.0821
ND \A°""S 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND \A.-S 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND ~ 0.1 IJ
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND lAj 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND rj 0.212
ND 0.167
I.IMS Workonlcr: 756200.UA-l.illlc Washington, N 1200090241 I lamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
o.ooo·
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
() 000-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 2000902406
Cone Flaa OL RL Cone Flaa OL RL
ND \X3 0.0821 0.000 ND \}..~ 0.0821 0.000
ND lA. :r 0.111 0.000 ND uw 0.111 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND 1.05 0.000 ND 1.05 0.000
ND 0.0564 0.000 ND 0.0564 0.000
ND 0.152 0.000 ND 0.152 0.000
ND 0.0939 0.000 ND 0.0939 0.000
ND i.A.:l 0.390 0.000 ND \A:! 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591 0.000
N0 ~ 0.113 0.660 bJ.D It. {k-113 Q.QQQ
ND 0.0487 0.000 ·ND 0.0487 0.000
ND 0.0499 0.000 ND 0.0499 0.000
ND 0.0697 0.000 ND 0.0697 0.000
ND 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND vl~ 0.0451 0.000 ND iA:"f' 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND 0.0658 0.000 ND 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND ~ 0.212 0.000 ND a' 0.212 0.000
ND 0.167 0.000 ND 0.167 0.000
Page 5 of 55
Sampll' n·su/rs '"""' ix'<'ll t/11tilifh•d by Rtulian flll<'l"lllllio11til bast•tl 011 rh<' , ,.,-,..,.;., 11/ rlw 1(11111 re•'i<'w pron·H. w/iicll il 111111fdctf 11ji<'I" rhe Cv111ruc/ l.11fHJ1'1/I01Y l'rogrum N111io1111/ F1mclimra/ Ci11itldi11t•\
-~nnic-org11~1Rt•1·-\"f.l'-l11'r/ ... //-c/ ... !1!14.mfjfrel1!----------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsoorooylbenzene 98-.82-8
4-lsoorooyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butyl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
I, I 12-Tetrachloroethane 630-20-6
I 1.2.2-Tetrachloroethane 79-34-5
T etrach loroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
I ,I I-Trichloroethane 71-55-6
I, I 2-Trichloroethane 79-00-5
Trich loroethene 79-01-6
Trichlorotluoromethane 75-69-4
1.2.3-Trichloroorooane 96-18-4
I, 1.2-Trich lorotritluoroethane 76-13-1
I 2.4-Trimethylbenzene 95-63-6
I 3.5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
·2000902404
Cone Flaa DL
ND lA::l 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND Ff 0.0796
ND
,
O.i06
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND z 0.467
ND ·s 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND U..J' 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N (200090241 Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 2000902406
Cone Flag DL RL Cone Flag DL RL
ND 11~ 0.0616 0.000 ND "'--:s-0.0616 0.000
ND 0.0474 0.000 ND 0.0474 0.000
ND 0.0452 0.000 ND 0.0452 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0469 0.000 ND ··-0.0469 0.000
ND 0.0845 0.000 ND -· 0.0845 0.000
ND B' 0.0796 0.000 ND ~ 0.0796 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.688 0.000 ND 0.688 0.000
ND 0.0886 0.000 ND 0.0886 0.000
ND 0.0722 0.000 ND 0.0722 0.000
ND 0.0948 0.000 ND 0.0948. 0.000
ND 0.0792 0.000 ND 0.0792 0.000
ND 0.0568 0.000 ND . -0.0568 0.000
ND 0.402 0.000 ND -·-0.402 0.000
ND 0.0680 0.000 ND 0.0680 0.000-
ND .B 0.467 0.000 ND a 0.467 0.000
ND ll' 0.118 0.000 ND lit 0.118 0.000
ND 0.0331 0.000 ND I 0.0331 0.000
ND 0.0952 0.000 ND 0.0952 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.208 0.000 ND 0.208 0.000
ND 0.0543 0.000 ND 0.0543 0.000
ND u:s 0.0766 0.000 ND \,\3 0.0766 0.000
ND 0.0749 0.000 ND 0.0749 0.000
ND 0.0436 0.000 ND 0.0436 0.000
ND 0.0438 0.000 ND 0.0438 0.000
ND 0.0574 0.000 ND 0.0574 0.000
Page 6 uf
. · · / / C J l · t · • /' · 1gr 1111 Nt1tioi111/ /-'11111·1im111/ G11it/1·/im·1 Smupli· 1 t'Jlllll' hm·•• bt'l'll qiw/ijit'd by Rmlimr /uti·nwtiomrl balt'il u11 tht' "' i1cri1111f tht' 1/11111 l'l!~·il•w proceH. w/11d1 tl mod<' nl 1tj1cr I 1e 0111rnct ·" n1111 "'.I 11
•
1
for Organic and /11org11n11· /)11/11 /l1•1•i1•11· (II .. \' £1'!1. Octo/lt'r 1999 mu/ 1-<'lll'lttll'I' /1)94. H'.1pt·c111·elrJ. .
55
SECTION IV
Analytical .Results
MS-VOA
SW8260B
Continued
Parameter
p-X vlene/m-X vlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
Cone Flaa DL
ND 0.137
ND 0.0713
I.IMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 2000902406
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 7 of
-St1mp/e l'l'llll/J hlll'•' bl.·i•ll qut1/ifit•d by Rmlillll liiti•nwtiumil bm<'il 1111 11,.., ,.,, .. ,.;.,of tlil' ilutu re~·ii'll' pron•u, which il mmldt'd 1tjt<'r the Co11trnc1 /.11/111rn1m:1• /'rugrmu Natimwl F11111 tio11al (i11iddi111'\
.anic.rg1mi-R1•ri1•n·(ll.SF.l' .• wr/9_1 .. ·111-94.1-1•1.'i,rJ._ - - - - - - --
55
-
-- ----- - -SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
l-Bromo-4-tluorobenzene
I .2-Dichloroethane-d4
Toluene-dB
Client Sample ID
Lab S~mple ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepar~d
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
AQueous
Received
NA
09/06/2000 12:05
09/08/2000 19:45
09/08/2000 19:45
l.0000
MSDA
ug/L
% Recovery Limits
84 77-117
101 61-143
93 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20009024) Hamilton Beach-Proctor Silex
STl. Austin
-
F
-- -- - - -
0900HBWW2 I 6 0900HBWW220
2000902407 2000902406
AQueous Aqueous
Received Received
NA NA
09/06/2000 14:00 09/06/2000 13 :40
09/08/2000 21 :09 09/08/2000 20:41
09/08/2000 21 :09 09/08/2000 20:41
1.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recovery Limits F % Recovery Limits
99 77-117 100 77-117
100 61-143 IOI 61-143
94 87-113 93 87-113
Page 8
· · / / / · l C · · I / · 1 n• l'rugmm Natio1111/ Fwu·tio11al (i11idd111<"
S11111p/t' n·~11/ts /um• m'l'll 1/lllllijicd by Rmlimr lllll'l'llllliu1111( b11s1·1l Ull ,,, .. critcri11 of 1/11· '''"" rt.'~·it•n• profflS, wluclr ll /Ill)( , .... ll}l<'I' I IC Ull/I ti( I .II""" II . •
for Orv,anic mrd l11orl!11nit· flat a R1•1•it•w (I 1.S F.1'1. Ortolwr 1999 11111/ l-1•f>r111irr 1994. n·1-,x·1·111·efrJ.
--
F
or 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
-
Bromoch loromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butylbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix·
Reported As
o/o Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW222
2000902408
Aaueous
Received
NA
09/06/2000 14:20
09/08/2000 21 :37
09/08/2000 21 :37
1.0000
MSOA
ug/L
Cone Flaa DL
ND IA~ 0.286
ND 1.67
ND \A.-S 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 1,,cs 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND u.::s 0.0484
ND \A'S 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
I.IMS Workordcr: 756200.UA-Litlle Washington, N (200090241 Hamilton Beach-P_roctor Silex
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
---
0900HBWW224 0900HBWW225
2000902402 2000902403
Aaueous Aaueous
Received Received
NA NA
09/06/2000 12:00 09/06/2000 12: 15
09/08/2000 18:49 09/08/2000 19: 17
09/08/2000 18:49 09/08/2000 19: 17
1.0000 1.0000
MSDA MSDA
Ul!./L ug/L
Cone Flaa DL RL Cone Flaa DL RL
ND V..3 0.286 0.000 ND \.A'3' 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND I.A.'.\ 0.983 0.000 ND \.A.."J 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 . 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND I J "'.'\ 0.106 0.000 ND u::s 0.106 0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0,0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
0.350 J 0.0484 0.000 ND IJ\ 0.0484 0.000
ND \ 1 "'l" 0.0867 0.000 ND I l :3 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
STL Austin Page: 9 of 55
Sampl<' rt'sults lml'I' lx·en IJlllllijicd by Rllllillll fillt'l'llllliomrl bast•tl 011 Ifie: t'l'lll'l'it1 of tlw 11tr111 rc1•i<•w proc·css, wlriclr i~ 1110tll'k1l t1jl('f tlr<' Collll'llCI J.11/1<11·11101:1• /'rugrnm Natio1111/ f-"1mctir111al Ciuidcli1w\
for Org11nic a111/ liro1~i:1mic IJ11111 Rt•1•i1'1r (11.S. El'.~. Octolr<'r 1999 m11/ h•/1r1111rr 1994, n'SfX'C'ti1•elyJ. · -------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsoorooyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butyl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) I08-IO-I
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile I07-12-0
n-Prooylbenzene 103-65-1
Styrene 100-42-5
I.I I 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene I08-88-3
1.2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
I. I I-Trichloroethane 71-55-6
I 1.2-Trichloroethane 79-00-5
Trich loroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloroorooane 96-18-4
I I 2-Trichlorotritluoroethane 76-13-1
1.2 4-Trimethylbenzene 95-63-6
1.3.5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride .. 75-01-4
SECTION IV -Analytical Results -09118/2000 19:53
0900HBWW222
2000902408
Cone Flaa DL
ND 1.1.:! 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND ft 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND Fi 0.467
ND ft 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND \A.."1 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Litlle Washington, N (20009024] Hamilton Beach-Proctor Silex
STl. Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW224 0900HBWW225
2000902402 2000902403
Cone Flaa DL RL Cone Flaa DL
ND 11 :\ 0.0616 0.000 ND \ i::I 0.0616
ND 0.0474 0.000 ND 0.0474
ND 0.0452 0.000 ND 0.0452
'ND 0.114 0.000 ND 0.114
ND 0.0469 0.000 ND 0.0469
ND 0.0845 0.000 ND 0.0845
ND ~ 0.0796 0.000 ND u 0.0796
ND 0.106 0.000 ND 0.106
ND 0.688 0.000 ND 0.688
ND 0.0886 0.000 ND 0.0886
ND 0.0722 0.000 ND 0.0722
ND 0.0948 0.000 ND 0.0948
ND 0.0792 0.000 ND 0.0792
ND 0.0568 0.000 ND 0.0568
ND 0.402 0.000 ND 0.402
ND . 0.0680 0.000 ND 0.0680
ND Al 0.467 0.000 ND n 0.467
ND B 0.118 0.000 ND 8 0.118
ND 0.0331 0.000 ND 0.0331
ND 0.0952 0.000 ND 0.0952
-~ l.INb 0.09051,.l 0.000 ND 0.0905
ND 0.208 0.000 ND 0.208
ND 0.0543 0.000 ND 0.0543
ND \.\ -:r 0.0766 0.000 ND \A.:f 0.0766
ND 0.0749 0.000 ND -0.0749
ND 0.0436 0.000 ND 0.0436
ND 0.0438 0.000 ND 0.0438
ND 0.0574 0.000 ND 0.0574
Page II
.fomp/e n•mlts 11111.,. bl't'll lflllllijit'd by R11tlit1ll fiiU'nmriumil bas<'tl u11 th<' 1 r11.-ri<1 of th<' dur11 n.'~·it•11• prOC'l!SS, which fa mutfcl.-1111.Jkr rlie Cu11rrncr l.t1/H11·11rui:1· l'rugrnm N11tia1111/ F1111ctimml Ciuitldim"
... anic'ill''.~trni.RC'1'iiiill.F.l>.1.11•r/9T11111(.'·••l11;•94_,._e~rJ._ - - - - ---W -
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 55
--
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
-Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepar•d
DatefTlme Analyz,d
Dilution Factor
Instrument
Units
Surroaate Compound
l -Rromo-4-fluorobenzene
I 2-Dichloroethanc-d4
Toluene-d8
SECTION IV -Analytical Results -09118/2000 19:53
0900HBWW222
2000902408
Aaueous
Received
NA
09/06/2000 14:20
09/08/2000 21 :37
09/08/2000 21 :37
1.0000
MSDA
ug/L
% Recoverv Limits
99 77-117
103 61-143
-95 87-113
I.IMS Workordcr: 756200.UA-Lilllc Washington, N (20009024) Hamilton Beach-Proctor Silex
STI. Austin
F
0900HBWW224 0900HBWW225
2000902402 2000902403
Aaueous Aaueous
Received Received
NA NA
09/06/2000 12:00 09/06/2000 12:15
09/08/2000 18:49 09/08/2000 19: 17
09/08/2000 18:49 09/08/2000 19: 17
1.0000 1.0000
MSDA MSDA
ue./L ue./L
% Recoverv Limits F % Recoverv Limits
98 77-117 98 77-117
97 61-143 99 61-143
95 87-113 92 87-113
Page 13 of
· · / / · I C · · / { · t ·1• l'r Jgmm N111io1111/ /-"1111ctimral Ci11idl'lim" -~results /11m• b<'<'ll •11111/ifh•d by R11tli1111 lill!'l"lltllio1111/ b11s<•1l o11 tli<' critl"rill of 1/11• d11111 re1•i,•11• proC<'lS, w/11d1 ll mm/1· ,., uj1c1 11<' 01111 II! I ·" Hll 11 o1. ',
--nnic~1x11n-R<'1'i~F.l'-/wr/-1!/1'11-994.-floe~1>. .. -~ -~ --l - -
F
55
-
-~· - ---- --· - -·-~ -·~ .. - - -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
-
Bromochloromethane
Bromodich loromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Dateffime Collect~d
Dateffime Prepar,d
Dateffime Analyzid
Dilution Factor
Instrument ·
Units !
CAS
67-64-1
75-05-8
107-02-8
l07-i3-I
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW226
2000902401
Aqueous
Received
NA
09/06/2000 11 :25
09/08/2000 16:0 I
09/08/2000 16:0 I
1.0000
MSDA
ug/L
Cone Flaa DL
ND \A3 0.286
ND 1.67
ND ~ 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND \A."3' 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
0.210 J 0.0484
ND \A;:l 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
l.IMS Workordcr: 756200.UA-Little Washington, N (20009024] Hamilton Beach-Proctor Silex
STL Austin
0900HBWW230 0900HBWW234
2000902409 .. 2000902405
Aaueous Aqueous
Received Received
NA NA
09/06/2000 14:50 09/06/2000 13 :25
09/08/2000 22:05 09/08/2000 20: 13
09/08/2000 22:05 09/08/2000 20: 13
1.0000 1.0000
MSDA MSDA
ug/L ug/L
RL Cone Flag DL RL Cone Flag DL
0.000 ND I .LS' 0.286 0.000 ND (A.:f 0.286
0.000 ND 1.67 0.000 ND 1.67
0.000 ND \A..':S 0.983 0.000 ND U,"3" 0.983
0.000 ND 0.0901 0.000 ND 0.0901
0.000 ND 0.0492 0.000 ND 0.0492
0.000 ND 0.0622 0.000 ND 0.0622
0.000 ND 0.139 0.000 ND .. ~ 0.139
0.000 ND 0.0683 0.000 ND 0.0683
0.000 ND 0.136 0.000 ND 0.136
0.000 ND lA -:f 0.106 0.000 ND \.)..,°'! 0.106
0.000 ND 0.179 0.000 ND 0.179
0.000 ND 0.0642 0.000 ND 0.0642
0.000 ND 0.0745 0.000 ND 0.0745
0.000 ND 0.0958 0.000 ND 0.0958
0.000 ND u::\ 0.0484 0.000 ND u.-:r 0.0484
0.000 ND u '3 0.0867 0.000 ND IA:\ 0.0867
0.000 ND 0.0839 0.000 ND 0.0839
0.000 ND 0.0473 0.000 ND 0.0473
0.000 ND 0.0756 0.000 ND 0.0756
0.000 ND 0.0670 0.000 ND 0.0670
0.000 ND 0.113 0.000 ND 0.113
Page 14
Sampll' l'l'lrtlll /11m• bl'l'll t/lllllijh·d by R111/i1111 llll<'l'llllliumtl bast'tl u11 iii<'' 11tl'ri11 of thl' tlaw re~·it•w proC'elS. which il "'.111/clt-d •!ficr tile Cu111rnct l.11bm·11111i:1• l'rngmm N111iu1111/ F1111cti111111/ (i11idcli111·,
for Organic 11111/ f11org1mi1· /l11t11 R1•1•i1•11· (I l.S. £/'.(October 19991/111/ I dm1111·1· 1994. r1'.1pt·c1t1·c~rJ.
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 55
-~------~~-~-------SECTION IV
Analytical .Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsoorooylbenzene 98-82-8
4-lsoorooYltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
4-MethYl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanen itrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
I I, 1,2-Tetrachloroethane 630-20-6
I I 2.2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
I 2,4-Trichlorobenzene 120-82-1
I I.I-Trichloroethane 71-55-6
I 1,2-Trichloroethane 79-00-5
Tri ch loroethene 79-01-6
Trichlorotluoromethane 75-69-4
I 2,3-Trichloropropane 96-18-4
I 1.2-Trichlorotritluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1.3 5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW226
2000902401
Cone Flaa DL
ND \A-S 0.0616
ND 0.0474
ND 0.0452
ND ·0.114
ND 0.0469
ND 0.0845
ND g 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND g 0.467
ND 'i 0.118
ND 0.0331
ND 0.0952
0.0945 lA i ND ~
ND 0.208
ND 0.0543
ND u..:r 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N (20009024) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW230 0900HBWW234
2000902409 2000902405
Cone Flaa DL RL Cone Flaa DL RL
ND v...::r 0.0616 0.000 ND v.:r 0.0616 0.000
ND 0.0474 0.000 ND 0.0474 0.000
ND 0.0452 0.000 ND 0.0452 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0469 0.000 ND 0.0469 ·o.ooo
ND -0.0845 0.000 ND 0.0845 0.000
ND ;« 0.0796 0.000 ND z .. _,.,, 0.0796 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.688 0.000 ND 0.688 0.000
ND 0.0886 0.000 ND 0.0886 0.000
ND 0.0722 . 0.000 ND 0.0722 0.000
ND 0.0948 0.000 ND 0.0948• 0.000
ND 0.0792 0.000 ND 0.0792 0.000
ND 0.0568 0.000 ND . 0.0568 0.000
ND 0.402 0.000 ND .-7' 0.402 0.000
0.126 j 0.0680 0.000 ND 0.0680 0.000
ND ~ 0.467 0.000 ND B 0.467 0.000
ND g 0.118 0.000 ND ·g-0.118 0.000
ND. 0.0331 0.000 ND 0.0331 0.000
ND 0.0952 0.000 ND 0.0952 0.000
0.355 lA. f'ND Q.896~ 0.000 ND 0.0905 0.000
ND 0.208 0.000 ND 0.208 0.000
ND 0.0543 0.000 ND 0.0543 0.000
ND H'.S 0.0766 0.000 ND ~ 0.0766 0.000
ND 0.0749 0.000 ND 0.0749 0.000
ND 0.0436 0.000 ND 0.0436 0.000
ND 0.0438 0.000 ND 0.0438 0.000
ND 0.0574 0.000 ND 0.0574 0.000
Page 16 of
S11111ple H'lllfll /1111•1• bt't'll t/llt1lifiL'd by R111/i1111 /u/N11tlliu1111/ bt1s<·ti "" rhi· 'ritl'ri<I of ill<' tfultl ff~·it·11' procel5. which il mutldnl 1ijl<'I' ."I<' Cumrncl l.11bm·111m:1· l'rogrnm NQ1iu1111l F1111ctio11al (i11idl'li11t•\
for Or.~anic and /11orf!tmi1· /111111 R1•1•i1•11· (l l.S F.l'.4. Oc10/wr 199911111/ f-l'l1ru11rr 1994. n•1pn·m·e/rJ.
55
SECTION IV
Analytical· Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW226
2000902401
Cone Flaa DL
ND 0.137
ND 0.0713
l.IMS Workordcr: 756200.UA-Littlc Washington, N (20009024) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0900HBWW230 0900HBWW234
2000902409 2000902405
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 17 of
Sm11ple re~ults '"""' bi.•<•11 q1111lifled by R1111i1111 l11t£•n1111io1111I btrst•tl o11 tlr<' crrkri11 t1f tlw ""'" ll:'·1·it•11• proct.'u, w/1id1 fa motfdetl trjicr tire Co11tn1ct l.t1fH11·111m:1• l'n1grn111 Ntr1io1111/ l:1111ctimral Ci11itldi11e'
-gt1ni~rg11...,Rr1• ... S.El'*liflwr1111fh"/-994:..,1•e(1;--~ - - --· ----
55
-
------~--------~---SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Ch loromethane
3-Ch loroprooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroprooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
frans-1 4-Dichloro-2-butene 110-57-6
1,4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3,Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dithloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
I 3-Dichloroorooane 142-28-9
2.2-Dichloroprooane 594-20-7
I. l'-Dich Ioroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexach ioro-1.3-butadiene 87-68-3
2-Hexanone " 591-78-6
SECTION IV -Analytical Results -09118/2000 19:53
TRIP BLANK I
2000902410
Cone Flaa. DL
ND v\S ll 0.0821
! ND I 0.111
I. ND I 0.113 I
I ND F 0.0762
ND I 1.05
I ND I 0.0564
ND I 0.152
ND I 0.0939
ND I 0.390
ND I 0.0587
ND I 0.0920
ND '/ F 0.0591
NB-~ t 9.11~
NDi~ ~ I 0.0487
ND 0.0499
ND F 0.0697
ND I 0.0603
ND F 0.0813
ND I 0.0670
ND F 0.0451
ND I 0.0714
ND F 0.0464
ND 0.0366
ND i 0.0658
ND ! 0.0647
ND ' 0.0552
ND I 0.212
ND 'VI n 0.167
I.IMS Workorder: 7~6200.UA-Little Washington, N (20009024] Hamilton Beach-Proctor Silex
STL Austin
TRIP BLANK I
2000902410
RL Cone Flaa DL RL Cone Flaa DL
0.000 ND 0.130 0.000
0.000 ND 0.0252 0.000
0.000 ND 0.0689 0.000
0.000 ND 0.0788 0.000
0.000 ND 1.18 0.000 ·-._-,
0.000 ND 0.0469 0.000 --
0.000 ND 0.0713 0.000
0.000 ND 0.114 0.000
0.000 ND 0.336 0.000
0.000 ND 0.0493 0.000
0.000 ND 0.0488 0.000
0.000 ND 0.0467 0.000
Q.Q~ ND 0.175 0.000
0.000 ND 0.0416 0.000 -·
0.000 ND 0.0619 0.000 .·
0.000 ND 0.0436 0.000
0.000 ND 0.0437 0.000
0.000 ND 0.0906 0.000
0.000 ND 0.0321 0.000
0.000 ND 0.0789 0.000
0.000 ND 0.0670 0.000
0.000 ND 0.0563 0.000
0.000 ND 0.0486 0.000
0.000 ND 0.0793 0.000 . 0.000 ND 0.0961 0.000
0.000 ND 0.0539 0.000
0.000 ND 0.369 0.000
0.000 ND 0.168 0.000
Page 20
S11111pfl' n•s11/1s ""'''' i><.•£•11 •JIWlijil!d by R111/i1111 llllt'l'lltllio1111/ bml'tl VII the •·ntaill of th•• 1/11111 re~·it·w prol'l!SS, wliicli fa mutlt'lnl 11jil'r th<• Ccmtrncl l.11born1111y l'rngrnm N111iu1111l /-"1111climwl (i11itl.-li111"
fur Organic a111/ l1101~r:1rnic 1>11111 Re1•i•·n· (11 . .\'. £1'1t. Octo/ll'r /999 11111/ fr/1rn111:r 111114. n•1p<·c·111·e~rJ.
RL
of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsoproovlbenzene 98-82-8
4-lsooropvltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-pentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Propanen itrile 107-12-0
n-Proov !benzene 103-65-1
Stvrene 100-42-5
1.1.1 2-Tetrachloroethane 630-20-6
I 1.2 2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
I 2.4-Trichlorobenzene 120-82-1
I I. I-Trichloroethane 71-55-6
I.I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloropropane 96-18-4
I I 2-Trichlorotrifluoroethane 76-13-1
1.2 4-TrimethyJbenzene 95-63-6
I 3.5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride .. 75-01-4
SECTION IV -Analytical Results· 09/18/2000 19:53
TRIP BLANK I
2000902410
Cone Flag DL
ND \1-:S 0.0616
I ND ~ 0.0474
'. ND 0.0452
i. ND I 0.114
ND I 0.0469
ND I 0.0845
ND F 0.0796
ND I O.I06
ND F 0.688
ND I 0.0886
ND F 0.0722
ND F 0.0948
ND I 0.0792
ND R 0.0568
ND F 0.402
ND R 0.0680
ND F 0.467
ND R 0.118
ND F 0.0331
ND F 0.0952
ND F 0.0905
ND F 0.208
ND F 0.0543
ND I 0.0766
ND F 0.0749
ND F 0.0436
ND R 0.0438
ND I F~ 0.0574
LIMS Workorder: 756200.UA-Little Washington, N 1200090241 Hamilton Beach-Proctor Silex
STLAustin
TRIP BLANK I
2000902410
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0556 0.000
0.000 ND 0.0361 0.000
0.000 ND 0.0532 0.000
0.000 ND 0.150 0.000
0.000 ND 0.0493 0.000 .
0.000 ND 0.0894 0.000
0.000 ND 0.0789 0.000
0.000 ND 0.112 0.000
0.000 ND 0.733 0.000
0.000 ND 0.0824 0.000
0.000 ND 0.0525 0.000
0.000 ND 0.0831 0.000
0.000 ND 0.0774 0.000
0.000 ND O.I09 0.000
0.000 ND 0.512 0.000
0.000 ND 0.0359 0.000
0.000 ND 0.263 0.000
0.000 ND 0.177 0.000
0.000 ND 0.0183 0.000
0.000 ND 0.133 0.000
0.000 ND 0.0494 0.000
0.000 ND 0.0665 0.000
0.000 ND 0.0843 0.000
0.000 ND 0.170 0.000
0.000 ND 0.0478 0.000 -
0.000 ND 0.0393 0.000
0.000 ND 0.0425 0.000
0.000 ND 0.0555 0.000
Page 21 of 55
l · / · l J J rj' J C 1 · ·1 I 1/>11rnton• J'rugrnm National rum ti1111a/ G11iddi111•\ Smnph• rt'llllts ""''" fx•c•n qrw/ijied bJ· R111/i1111 /11u•m111ior111/ bal1•1/ 011 tlr<' 1 ntcri11 11/ /hi' d11U1 fc•~·it•11• proceu. II' uc· r ll 111111 <' ,., " tcr t '" 011 1 "' ·1 . •
-~anic~1:i:11n-Rr1·i-\'F.l'tllll"'''",' .... lh•f1
-
994..im"'e(rJ-__ - - - --- - -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
-Matrix
Surrnnate Comoound
l-Bromo-4-fluorobenzene
t 2-Dichloroethane-d4
Toluene-d8
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyz,d
Dilution Factor :
Instrument
Units
SECTION IV -Analytical Results -09/18/2000 19:53
TRIP BLANK I
2000902410
Aaueous
Received
NA
09/06/2000 11 :04
09/08/2000 22:33
09/08/2000 22:33
1.0000
MSDA
Ui!:/L
% Recoverv Limits
99 77-117
103 61-143
84 87-113
I.IMS Workorder: 756200.UA-Lillle Washington. N (20009024] Hamilton Beach-Proctor Silex
STL Austin
TRIP BLANK I
2000902410
Aaueous
Received
NA
09/06/2000 11 :04
09/11/2000 15:55
09/11/2000 15:55
1.0000
MSDB
ug/L
F % Recoverv Limits F 0/e Recoverv Limits F
93 77-117
107 61-143
0 97 87-113
Page 23 of 55
Sample rt•mlts hm•i• b<'t'll lflllllijied b)' Rt11liim lmam1tiumil bas(•tl 011 thl'1 ,.,-,..,.;11 of tlw dalll re1•i('I•' proceH. which il 11111dl'/1·d 11jia 1/ie C1111trnct l.11b11r111111:1• l'rngra111 N111iu1111l F1111c1im111l Ci11itldim•1
-~11ni(l~1:~11,...Re1·i-\0 F.l'tlil'/"•1·/ .. //1•/l•\194 .... 11·elrJ-, - - -·--~-- - -
--------------~~---SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Buty I benzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collect•d
Date/Time Prepar~d
Date/Time Analyzld
Dilution Factor
Instrument .
Units 1
'
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Aaueous
Received
NA
09/07/2000 10:00
09/09/2000 0 I :54
09/09/2000 0 I :54
50.0000
MSDA
ug/L
Cone Flaa DL
ND lA.:S 14.3
ND 83.5
ND l..A..:S 49.2
ND 4.50
ND 2.46
ND 3.11
ND 6.95
ND 3.42
ND 6.80
ND IA"3" 5.30
ND 8.95
ND 3.21
ND 3.72
ND 4.79
ND \A.::S 2.42
ND \·l"S 4.34
ND 4.20
ND 2.36
23.0 . J 3.78
ND 3.35
ND 5.65
I.IMS Workordcr: 756200.UA-Little Washington. N (20009035) Hamilton Beach-Proctor Silex
STLAuslin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Aaueous Aaueous
Received Received
NA NA
09/07/2000 09:00 09/07/2000 09:20
09/09/2000 00:26 09/09/2000 00:54
09/09/2000 00:26 09/09/2000 00:54
10.0000 2.0000
MSDA MSDA
ug/L ug/L
Cone Flaa DL RL Cone Flaa DL
ND vw 2.86 0.000 ND !.....__\ 0.572
ND 16.7 0.000 ND 3.34
ND IA.:J 9.83 0.000 ND \,er 1.97
ND 0.901 0.000 ND 0.180
ND 0.492 0.000 0.280 J 0.0984
ND 0.622 0.000 ND 0.124
ND 1.39 0.000 ND ?0.278
ND 0.683 0.000 ND -0.131
ND 1.36 0.000 ND 0.272
ND ~ 1.06 0.000 ND u"J 0.212
ND. 1.79 0.000 ND 0.358
ND 0.642 0.000 ND 0.128
ND 0.745 0.000 ND 0.149
ND 0.958 0.000 ND 0.192
ND 1A::J 0.484 0.000 ND \A°1 0.0968
ND II °:\ 0.867 0.000 ND 11 -:r 0.173
ND 0.839 0.000 ND 0.168
ND 0.473 0.000 ND 0.0946
ND 0.756 0.000 0.649 J 0.151
ND 0.670 0.000 ND 0.134
ND 1.13 0.000 ND 0.226
Page 4
. · / · / · If / r;· f C · ·t J / · //Ofl' /'rogrnm Natimwl Frmctirmal (i11iddi1W\
Strmpk reJ11/u /1111·•• bi•en qrwlified by R111/im~ /1111•1w11io1111/ bm1•d 011 tlrt' '..,.'.,,.,.'.''. '~ tlrl' ~''.'-"' .':"~''.1'11'. procelS, w 11c r u ''.w'" n 11 tcr t '" 0111111' ·11 '"' 1 · •
for Organic m11/ /1101:i:1111ic I 111/ll Re1•il'll' (II . .\. f./'.-f. Oc111/J1·r 1999 11111/ 1-t /1111111 I 1994. 1< SfH. ctn ef.1 J.
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 34
SECTION IV
Analytical Results
MS-VOA
SWB260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Chloromethane 74-87-3
3-Chloroprooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroprooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1 J-Dichloroorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
i Cone Flaa DL
ND \.A:S" 4.10
I ND \A':S 5.55
ND 5.65
ND 3.81
ND 52.5
ND 2.82
ND 7.60
ND 4.70
ND \.A:S-19.5
ND 2.94
ND 4.60
ND 2.96
N9--R.... 5.6§
1370 2.44
ND 2.50
238 3.48
205 3.02
ND 4.0o
ND 3.35
ND IA'.\ 2.26
ND 3.57
ND 2.32
ND 1.83
ND 3.29
ND 3.24
ND 2.76
ND .8 10.6
ND 8.35
I.IMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.888
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Cone Flaa DL RL Cone Flaa DL RL
ND IA:S 0.821 0.000 ND u:-s 0.164 0.000
ND 11 ·:r 1.11 0.000 ND \A.J 0.222 0.000
ND 1.13 0.000 ND 0.226 0.000
ND 0.762 0.000 ND 0.152 0.000
ND 10.5 0.000 ND 2.10 0.000
ND 0.564 0.000 ND 0.113 0.000
ND 1.52 0.000 ND 0.304 0.000
ND 0.939 0.000 ND 0.188 0.000
ND l>..~ 3.90 0.000 ND 11 ::s 0.780 0.000
ND 0.587 0.000 ND 0.117 0.000
ND 0,920 0.000 ND 0.184 0.000
ND 0.591 0.000 ND 0.118 0.000
NS-Q 1.13 6.eee N9 R. o.~6 9.9QO
156 0.487 0.000 159 0.0974 0.000
4.05 J 0.499 0.000 0.576 J 0.0998 0.000
391 0.697 0.000 13.7 0.139 0.000
45.I 0.603 0.000 11.6 0.121 0.000
1.33 J 0.813 0.000 0.683 J 0.163 0.000
ND 0.670 0.000 ND 0.134 0.000
ND \ """\ 0.451 0.000 ND IA.~ 0.0902 0.000
ND 0.714 0.000 ND 0.143 0.000
ND 0.464 0.000 ND 0.0928 0.000
ND 0.366 0.000 ND 0.0732 0.000
ND 0.658 0.000 ND 0.132 0.000
ND 0.647 0.000 ND 0.129 0.000
0.292 ::) IA 0.552 0.000 ND 0.110 0.000
ND ·w-2.12 0.000 ND £ 0.424 0.000
ND 1.67 0.000 ND 0.334 0.000
STL Austin Page 5 of 34
.\i1111ph• remits /1111•1• bc•e11 qrwlified by R11tli1111 brtt•n111tio1111/ basl'tl o11 th<' t'l"ll<'rill 11/ tlll' 1/11111 rel'i<'ll' pron!SS, whiclr fa 11wcldnl after tire Co1111·11ct l.11IHJ1't1tun• /'mgnmr N11tio1111/ h111cti1111al <i11icldi111'\
-... gani'llliio1-g11 ... 1Rt•1•i11i1.'i.£/'i1Wfwr .. 1llcl-l994 .• 111·el_1 .. ·-- - --· ·-- - -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID '
Lab Sample ID
Continued
Parameter CAS I
lodomethane 74-88-4 I
lsooroovlbenzene 98-82-8 ;
4-lsoorooyltoluene 99-87-6
Methvl methacrvlate 80-62-6 '
Methyl tert-butyl ether <MTBE) 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanen itrile 107-12-0
n-Prooylbenzene 103-65-1
Stvrene 100-42-5
I I.I 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1 2 3-Trichlorobenzene 87-61-6
I 2.4-Trichlorobenzene 120-82-1
I I I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloroorooane 96-18-4
I, I 2-Trichlorotrifluoroethane 76-13-1
I 2 4-Trimethylbenzene · 95-63-6
1.3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Cone Flaa DL
ND LA.~ 3.08
ND 2.37
ND 2.26
ND . 5.70
ND 2.34
ND 4.22
ND g 3.98
ND 5.30
ND 34.4
ND 4.43
ND 3.61
ND 4.74
ND 3.96
ND 2.84
ND 20.l
8.65 J 3.40
ND !if 23.4
ND It 5.90
1160 1.66
ND 4.76
35.5 LL f\.\D ~
ND 10.4
ND 2.72
ND \A.'S 3.83
ND 3.74
ND 2.18
ND 2.19
ND 2.87
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STl. Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Cone Flaa DL RL Cone Flaa DL
ND 11 '3° 0.616 0.000 ND \A..~ 0.123
ND 0.474 0.000 ND 0.0948
ND 0.452 0.000 ND 0.0904
ND 1.14 0.000 ND 0.228
ND 0.469 0.000 ND 0.0938
ND 0.845 0.000 ND -0.169
ND a 0.796 0.000 ND ~ 0.159
ND 1.06 0.000 ND 0.212
ND 6.88 0.000 ND 1.38
ND 0.886 0.000 ND 0.177
ND 0.722 0.000 ND 0.144
ND 0.948 0.000 ND 0.190-
ND 0.792 0.000 ND 0.158
33.1 0.568 0.000 ND -0.114
ND 4.02 0.000 ND -0.804
ND 0.680 0.000 ND 0.136
ND pr· 4.67 0.000 ND .8 0.934
ND ,ff 1.18 0.000 ND B' 0.236
ND 0.331 0.000 ND 0.0662
2.23 J 0.952 0.000 ND 0.190
510 0.905 0.000 0.489 v... /' Nt> &.-Htt"
ND 2.08 0.000 ND 0.416
ND 0.543 0.000 ND 0.109
ND \XS 0.766 0.000 ND \A..-S 0.153
ND 0.749 0.000 ND 0.150
ND 0.436 0.000 ND 0.0872
ND 0.438 0.000 ND 0.0876
17.8 0.574 0.000 9.35 0.115
Page 6
.'iampfl' t'<'mlll J,111.,. bt•i•ir qmrlijh>d by Rmlimr flll<'fllllliami/ basl'd 011 1/ie cn"icri11 of tlil' 1/11111 l'<'l'l.<'11' process. ll'flicfl il 111mldl'll 11/ier 1/re Ccmtmcl /.11/nm11m:i• l'rogrnm Na1ia11t1f F111u·1i1111al (i11iddi111''
for Organic 11111/ "1org11nic /lt//tl Re1•i1•11· (f l.S. F./'.~. Oc10/1er 1999 m11/ /·l'lw111wr 1!194. l'C'.IJX'l'lil'elrJ.
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 34
SECTION IV
Analytical .Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Cone Flaa DL
ND 6.85
ND 3.56
I.IMS Workordcr: 756200.UA-Litlle Washington, N (200090351 Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0900HBWW213 09001-IBWW214
2000903501 2000903502
Cone Flag DL RL Cone Flaa DL RL
ND 1.37 0.000 ND 0.274 0.000
1.66 J 0.713 0.000 ND 0.143 0.000
Page 7 of
.\i1111ple n•s11lll /11m• bl'C'll qualified bJ' R1111it111 /111<•n1111im111l b11s1·1l u11 ih<' < ril<'ri11of1/11• 11111111·e.••i<•11• proceu. which i!. modl'ii'1/ 11jlcr 1he Cu111r11cl l.11/11m1101y l'rngrnm N111io1111l f-'11111·11111111/ (i11it/di111'\
tliignnicllliio1:~"liili"R1•1·11if"' El'A "[/Ol"'rlllid/-1·/-/V94 .• t11·el1,.. - - -:-·-- - --
34
-
- - - -- --- -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
-Matrix
Reported As
% Moisture
Dateffime Collect~d
Dateffime Prepared
Datefflme Analyzed
Dilution Factor I : Instrument ' ·
Units
Surroaate Comoound
I-Bromo-4-fluorobenzene
1·2-Dich loroethane-d4
Toluene-dB
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Aaueous
Received
NA
09/07/2000 10:00
09/09/2000 0 I :54
09/09/2000 0 I :54
50.0000
MSDA
ug/L
%Recovery Limits
99 77-117
102 61-143
93 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STL Austin
-- -- - --·-
0900HBWW213 0900HBWW214
2000903501 2000903502
Aaueous Aaueous
Received Received
NA NA
09/07 /2000 09:00 09/07/2000 09:20
09/09/2000 00:26 0910912000 00:54
. 09/09/2000 00:26 09/09/2000 00:54
10.0000 2.0000
MSDA MSDA
ug/L ug/L
F % Recoverv Limits F % Recovery Limits
96 77-117 98 77-117
99 61-143 100 61-143
94 87-113 93 87-113
Page 8
. · · / · / C · · I I · t ·1· l'r 1gr11111 N11tiu1111/ F1t11C"timral (i11i1/l'ii11t"
Simrph• rt'lll/U '"""' bt'l'll <Jlllllified by Rmlimr J111a11111iu1111l biuctl u11th<'1 ri1t·rit1 oj tl11• 1ltrtt1 re~·il'11'. proceu. w/11d1 u mm/d<'1 11jtcr t 1e Ull/llll I ·11 """
01. 1
•
for Organic n11tl /11org11nic 1'11111 R<'1'il'll" (l t.S· £/'A. Octobl'r 199911111/ h•lwr111rr /1)1)4, n·.~JX·t•t11·c~1 J.
--
F
of 34
SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
.
Bromochloromethane
Bromodich loromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analy<ted
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWW215
2000903503
Aaueous
Received
NA
09/07/2000 09:35
09/08/2000 23 :29
09/08/2000 23 :29
1.0000
MSDA
ug/L
Cone Flaa DL
ND lA.:S 0.286
ND 1.67
ND \A:f 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND IA "°J 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND v.::s 0.0484
ND u..:\ 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Lillle Washington, N (20009035) Hamilton Beach~Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW227 0900HBWW228
2000903504 2000903505
Aaueous Aqueous
Received Received
NA NA
09/07/2000 09:55 09/07 /2000 I 0: I 0
09/09/2000 0 I :24 09/08/2000 23 :57
09/09/2000 0 I :24 09/08/2000 23:57
50.0000 2000.0000
MSDA MSDA
ug/L Ul!/L
Cone Flaa DL RL Cone Flag DL RL
ND (}.::r 14.3 0.000 ND \.l.-:5' 572 0.000
ND 83.5 0.000 ND 3340 0.000
ND \A,"l" 49.2 0.000 ND u-:\ 1970 0.000
ND 4.50 0.000 ND 180 0.000
ND 2.46 0.000 ND 98.4 0.000
ND 3.11 0.000 ND 124 0.000
ND 6.95 0.000 ND 278 0.000
ND 3.42 0.000 ND 137 0.000
ND 6.80 0.000 ND 272 0.000
ND I .l ::f 5.30 0.000 ND \A.,.\ 212 0.000
ND 8.95 0.000 ND 358 0.000
ND 3.21 0.000 ND 128 0.000
ND 3.72 0.000 ND 149 0.000
ND 4.79 0.000 ND 192 0.000
ND \A.::S 2.42 0.000 ND \XS 96.8 0.000
ND \;\.::\ 4.34 0.000 ND \,\ -s 173 0.000
ND 4.20 0.000 ND 168 0.000
ND 2.36 0.000 ND 94.6 0.000
26.3 3.78 0.000 ND 151 0.000
ND 3.35 0.000 ND 134 0.000
ND 5.65 0.000 ND 216 0.000
Page 9 of 34 -~/<' l'l'lll/B 1111,.,. b<'<'ll t/milified by Rmlimr lillc•tmlliutwl basc•il 011 '""1 ntaill t1/ tltc• tlt1ftl n·~·ic•u• pro«els. which il Jtwddl'll ttji('I' tit<' Co1111·11cl l.t1IHJrt11oi:1• l'rogm111 N111io1111/ Fr111c1im111/ (i11iddi111·,
-r1?11nr-1or1?1-11Re-.S F.-o/11·r-11//"1-l\194-·/ll'<'f... - - - -·-- - - -
- - - - - - - - - - - - - - --·-- -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Ch loromethane
3-Ch loroprooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloroprooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibtomomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3~Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
-trans-I 2-Dichloroethene 156-60-5
I 2-Dichloroorooane 78-87-5
I 3-Dichloropropane 142-28-9
2 2-Dichloroprooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1.3-Dichlorooropene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexach loro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWW2 I 5
2000903503
; Cone Flag DL '
ND lA-:5 0.0821
~ ND IA:\ 0.111
ND 0.113
: ND 0.0762 I
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND lA~ 0.390
ND 0.0587
ND 0.0920
ND 0.0591
.WQ.. p.__ 0.11~
3.16 0.0487
ND 0.0499
1.75 0.0697
0.0496 J )if 0.0603
ND 0.0813
ND 0.0670
ND l,\.~ 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND g 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.889-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW227 0900HBWW228
2000903504 2000903505
Cone Flaa DL RL Cone Flaa DL RL
ND lA..J 4.10 0.000 ND I.A.~ 164 0.000
ND l .l '3" 5.55 0.000 ND l.A.J 222 0.000
ND 5.65 0.000 ND 226 0.000
ND 3.81 0.000 ND 152 0.000
ND 52.5 0.000 ND ~ ._2100 0.000
ND 2.82 0.000 ND .-113 0.000
ND 7.60 0.000 ND 304 0.000
ND 4.70 0.000 ND 188 0.000
ND \A.°S 19.5 0.000 ND Ll."1 780 0.000
ND 2.94 0.000 ND 117 0.000
ND 4.60 0.000 ND 184 0.000
ND 2.96 0.000 ND 118 0.000
N& R... 5.(i~ Q.QQQ Ne f:. ~;26 0.000
1340 2.44 0.000 11900 --,~97.4 0.000
ND 2.50 0.000 ND -99.8 0.000
249 3.48 0.QOO 31200 139 0.000
211 3.02 0.000 2380 121 0.000
ND 4.06 0.000 ND 163 0.000
ND 3.35 0.000 ND 134 0.000
ND I A..-S 2.26 0.000 ND ~:s 90.2 0.000
ND 3.57 0.000 ND 143 0.000
ND 2.32 0.000 ND 92.8 0.000
ND 1.83 0.000 ND 73.2 0.000
ND 3.29 0.000 ND 132 0.000
ND 3.24 0.000 ND 129 0.000
ND 2.76 0.000 506 J 110 0.000
ND rJ 10.6 0.000 ND . Jf 424 0.000
ND 8.35 0.000 ND 334 0.000
Page 10 of
Smup/1' l'l'Slllts ""''•' lx•t•ll l[lllllijied by Hmlimi /11/t'I 11111;u1111/ b(ISl'll uu til<' cri1.-ri11of1/w d111ll re1•i1•w proceJS, wltil'lt il 11w1/dol 11jit·1· 1/ie Co111rnc1 /.11/mn111J1:1• /'rn.i:rnm N111iot111/ l·imcliima/ (iuidditl<'.\
for Organic a111//11org1mic /)a/11 He1•i1•11· (11.S. El'A. Oc1obt'I' 199911111/ t-.·lw1111rr 1994. n'.1p<·c111·e(rJ.
34
SECTION IV
Analytical ·Results
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroov !benzene 98-82-8
4-lsopropyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanen itrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
1 1.1.2-Tetrachloroethane 630-20-6
I 1,2,2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahvdro furan 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
1.1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloroorooane 96-18-4
I 1 2-Trichlorotriflu.oroethane 76-13-1
1.2.4-Trimethvlbenzene 95-63-6
I 3 5-Trimethylbenzene !08-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWW215
2000903503
Cone Flaa DL
ND \A.:3' 0.0616
ND 0.0474
ND 0.0452
' ND 0.114
0.937 J 0.0469
ND 0.0845
ND It 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND . 0.0568
12.2 0.402
ND 0.0680
ND H 0.467
ND It 0.118
ND 0.0331
ND 0.0952
O.l 16lA-I.ND ~
ND 0.208
ND 0.0543
ND \A.J 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
UMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW227 0900llBWW228
2000903504 2000903505
Cone Flaa DL RL Cone Flaa DL RL
ND I A ::S 3.08 0.000 ND 1.A.-s' 123 0.000
ND 2.37 0.000 ND 94.8 0.000
ND 2.26 0.000 ND 90.4 0.000
ND 5.70 0.000 ND 228 0.000
ND 2.34 0.000 ND 93.8 0.000
ND 4.22 0.000 ND 169 0.000
~ tJ\) ~ 3.981.A. 0:000 280 I>--~ND~ 0.000
ND 5.30 0.000 ND 212 0.000
ND 34.4 0.000 ND 1380 0.000
ND 4.43 0.000 ND 177 0.000
ND 3.61 0.000 ND 144 0.000
ND 4.74 0.000 ND 190 -0.000
ND 3.96 0.000 ND 158 0.000
ND 2.84 0.000 ND 114 0.000
ND 20.I 0.000 ND 804 0.000
8.92 J 3.40 0.000 1340 136 0.000
ND ,r( 23.4 ·o.ooo ND H 934 0.000
ND ll' 5.90 0.000 ND .n-236 0.000
122_0 1.66 0.000 64400 66.2 0.000
ND 4.76 0.000 ND 190 0.000
36.9 IA-Nt> ~ 0.000 11500 181 0.000
ND 10.4 0.000 ND 416 0.000
ND 2.72 0.000 ND 109 0.000
ND \\ "'.\ 3.83 0.000 ND u-.s 153 0.000 -ND 3.74 0.000 933 J 150 0.000
ND 2.18 0.000 ND 87.2 0.000
ND 2.19 0.000 ND 87.6 0.000
ND 2.87 0.000 ND 115 0.000
Page 11 of 34
Sampk resu/IJ /um• b<'l'll l/lllllijied by Rllllimr fnl<'i·mrtiumil basi•d 011 1/ie < ,.;,, ·ria 11/ 1/w 1/11w re_1•it•u• pr0<·ess. wliid1 il 11111ddt'1l 11jlcr 1'1e Co111rncl l.11/HJ1"lllt11:1· /'rngrnm Nt11imw/ l.-11111"1il111t1/ <iuiddilln
--·gnni'lli*o'".l!"'iiil" R,., .• s El9i1irlwr 111d l-cl-l9!J4 .• 111'£'iJ-- - - - - - - - -
---SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
---
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:58
!
1 ·
!
---
0900HBW,W215
2000903503
Cone Flaa DL
ND 0.137
ND 0.0713
. LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STLAustin
------ ---
0900HBWW227 0900HBWW228
2000903504 2000903505
RL Cone Flaa DL RL Cone Flaa DL
0.000 ND 6.85 0.000 1520 J 274
0.000 ND 3.56 0.000 1240 143
;t.
Page 12
Samp/i• n•rnlts 111,..,, m'l'll ,11wlified by Rmlimi lllll'r/llrtio1111/ bascil o11 tlrl' cr11 .. ri11 of tlil' d11ta H'l'i°<'ll' procelS, whiclr il 11ro1ldnl 1tji<'r the Co11tmct /,11/HJrt11tJn• l'rugrn111 N11tio1wl f"1111cti<J1U1I G11irll'li111"
(or Org11nic m11l ltro1:1!11nic ll11tcr Re1•i1•11· (l l.S F.!'.~. Ocwlwr 1999 mul I dwuarr 1994, n•.1p1·1'1il'e~rl.
--
RL
0.000
0.000
of 34
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
-Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time PrepanKt
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
1-Bromo-4-fluorobenzene
I ;2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analylical Results -09/18/2000 19:58
0900HBWW2 I 5
2000903503
Aaueous
Received
NA
09/07/2000 09:35
09/08/2000 23:29
09/08/2000 23:29
1.0000
MSDA
ug/L
0/o Recoverv Limits
99 77-117
98 61-143
93 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STLAustin
F
0900HBWW227 0900HBWW228
2000903504 2000903505
Aqueous Aaueous
Received Received
NA NA
09/07/2000 09:55 09/07 /2000 I 0: I 0
09/09/2000 0 I :24 09/08/2000 23:57
09/09/2000 0 I :24 09/08/2000 23:57
50.0000 2000.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recovery Limits F
98 77-117 99 77-117
101 61-143 99 61-143
94 87-113 93 87-113
Page 13 of 34
St1mph• n•s1tlts lwl'I' h<'l'll l/lllilijicd by Rt11lit1n lnt<'l'llt1li1J1utl basl'il 011 the, ntl'rill of tire"""' re~·h•1t• proC'eu, wliidi ;~ mudded '!fll'I' 1/ie Cc1111r11ct l.11b11r111m:1• l'rngr11111 N11ti1J1111l Fwu timwl G11idt'lit11·'
-~ani~i:i:11~Re1·-SEl._,berl .. di<'l~!l94 ... 11·e~1 .. - - - - - - - - -
----- - - --· - -SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Ace ton itri le
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
.
Bromochloromethane
Bromodich loromethane
Bromoform
Brom om ethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Ch loro-1.3-butadiene
Chlorobenzene
Ch loroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As ,
% Moisture !
DatefTlme Collect'd
DatefTime Prepar~d
DatefTime Analyz,d
Dilution Factor
Instrument I
Units '
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5 ' 75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6 '
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3 I
67-66-3
544-10-5
SECTION IV -Analytical Rcsults-09118/2000 19:58
TRIPBLANK2
2000903507
Aqueous
Received
NA
09/07/2000 08:55
09/08/2000 23:01
09/08/2000 23:01
1.0000
MSDA
ug/L
Cone Flaa DL
ND Id 0.286
ND . 1.67
ND \A~ 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND \A:J 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND Vl::f 0.0484
ND \.\ :\ 0.0867
ND 0.0839
ND 0.0473.
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STLAustin
RL Cone
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
-- - ---
Flaa DL RL Cone Flaa DL
.•
~
Page 14
. . . ,·, I .r I c· . . I I . I . • l'r Wrtllll N11ti01111l /-°11111'tio11al (i11iddi111·1
lift db R I. I . . · / b .. , 11 th • criteria or till' ,/11tt1 rei•i<•w pron!ss. w/11d1 u mm ,. c1 11;ta t 1e 01111 mt .11 """ OIJ '"' Smnplt• rt•s11/ts /1111··· bt'('/l 1[1111 I It.' r Ill 11111 lllt 11111/Wllll 115(1 u ' . ~ . • . . • . .
fiw Organic m11//t101:'!1111ic />11w R1'1•it·11· (11.S F.':"i.· Octo/wr /99911111//·1•/w11111T 1994. "1pNt11e/1J.
- -
RL
of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
!07-05-1
95-49-8
!06-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene I I0-57-6
1.4-Dichlorobenzene !06-46-7
1.2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichlorooronane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
I 1-Dichloroprooene 563-58-6
: .
~
cis-1 3-Dichloroorooehe 10061-01-5
trans-I 3-Dichloronro""'ne 10061-02-6
Ethvl methacrvlate 97-63-2
Ethyl benzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone " 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:58
I TRIP BLANK 2
2000903507
Cone Flaa DL
ND \An"' 0.0821
ND ~"J 0.111
ND 0.113 . ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND \A.:J 0.390
ND 0.0587
ND 0.0920
ND 0.0591
~ a. 0.11~
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND \A.:S 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND I! 0.212
·ND 0.167
I.IMS Workordcr: 756200.UA-Little Washington, N (20009035] Hamilton Bcach-Proclor Silex
STLAustin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.996
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 15 of 34
S"mplt• n•s11//s /1111'1' (x•en q1111/ifii:d by R111/i1111 1111,•1m11iu1m/ basetl u11 th<' critt"ri11 t1/ tlrl' ''"'" l"l!~'i''"' prOC"l!SS. wlriclr fa mudl'ktl 11jicr tire Ccmtrncl l.11IH1rn1m:1· /'rugrnm Natium1/ /-"1111c1tmral G11iddim•\
-~gani-rorg1~11He._-.s.£,_o/1<·r-11/l·c-/!l94-"lll'el-'llll - - - - - - - - -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical ResullS -09/18/2000 19:58
TRIP BLANK 2
2000903507
Cone Flaa DL
I ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flag DL RL Cone Flaa DL RL
0.000
0.000
Page 17 of -~h· resu/u lull't' bl.'C'll 1(1"'/ijil.'d "J' Rmlimr fn/<'rlllltioiwl /Jm'('(/ "" the,_.,.;, .. ,.;,, of 1/u• t111111 re~·ii•w proc·t•ss, wlridr il mud<'lcd 11jil.'r thl.' Ccmtrnct l.11IH1rt111J1:1· l'mgrnm N111io1111/ l:1111ct1111111/ G11h/di11<'\
--gani.-1org11 11Re1 . .'i.E~~l1t·r-11/fr-/1194.-·111·e/.1-·-- - - - - - -
34
-
---------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
-Matrix·
Surrogate Comoound
l-Bromo-4-fluorobenzene
I· 2-Dichloroethane-d4
Toluene-d8
Reported As
% Moisture
Date/Time Collect,d
Date/Time Prepanpd
Date/Time Analyz'd
Dilu~ion Factor ·
Instrument
Units
SECTION IV -Analytical Results -09/18/2000 19:58
TRIPBLANK2
2000903507
Aqueous
Received
NA
09/07/2000 08:55
09/08/2000 23:01
09/08/2000 23 :0 I
1.0000
MS"DA
ug/L
% Recovery Limits
95 77-117
100 61-143
92 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-.Proctor Silex
STL. Austin
----- ---
F % Recoverv Limits F % Recoverv Limits
Page 18
Samplt• n'lt1fll hm•e bi.•en qmi/ijil!d by Rt11liml /lll<'rl1t1lioi1t1/ bas<'d 1111 th<',,.,, .. ,.;,, of the tft1/t1 n·~·i<'ll' pron•lS, whidi il 111otfdctl 11Jicr the Co11tmct I.11/xm11m:1• l'rugmm N111im111/ l-"lmctimwl G11id1·/i111••
for Organic 11111/ ftrorg11nic [)11111 R<•1•i1•11· (l l.S. El' A. October 1999 mu/ h•/lr11t111' 1994. n·.1p<'Ctll'elyJ.
--
F
of 34
I
I
I
I
I
I
I
1·
RAW DATA
I
I
I
I
I
I ---
I
I
I
I
I
SECTION II
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex Project Name: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
Client Code: HB-PS Facility Name: NC
Workorder Summary
La bi
Client Sample ID SamolelD Samole Matrix
0900HBWW226 2000902401 Aaueous
0900HBWW224 2000902402 Aaueous
0900HBWW225 2000902403 Aaueous
0900HBW0998 2000902404 Aaueous
0900HBWW234 2000902405 Aaueous
0900HBWW220 2000902406 Aaueous
0900HBWW216 2000902407 Aaueous
0900HBWW222 2000902408 Aaueous
0900HBWW230 2000902409 Aaueous
TRIP BLANK 1 2000902410 Aaueous
Protocol Summary
Lab Date& Time
Client Sample ID Samole ID Collected
Method· SW8260B .
0900HBWW226 2000902401 09106100 11 :25
0900HBWW224 2000902402 09106100 12:00
0900HBWW225 2000902403 09106100 12:15
SECTION II -Report Summaries -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Method Citation
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Date& Time Prep
Received Batch ID
09107100 10:20 8021
09107100 10:20 8021
09/07100 10:20 8021
Method Descriotion
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Hold Time S >ec
Date& Time Analysis Date& Time Preo Analvsis
Preoared Batch ID Analvzed Soec Actua Soec Actua
09/08/00 16:0 I 8021 09/08/00 16:0 I 70 20 70 20
09/08/00 18:49 8021 09/08/00 18:49 70 20 70 20
09/08/00 19: 17 8021 09/08/00 19: 17 70 20 70 20
Page I of 55
-------------------
--· - - - - - - - - - - - - - - - - -SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
:
Lab Date &Jime
Client Samole ID Samole ID Collected
Method· SW8260B continued -
0900HBWD998 2000902404 09106100 12:05
0900HBWW234 2000902405 09106100 13 :25
0900HBWW220 2000902406 09106100 13 :40
0900HBWW216 2000902407 09/06/00 14:00
0900HBWW222 2000902408 09106100 14:20
0900HBWW230 2000902409 09106100 14:50
TRIP BLANK I 2000902410 09106100 11 :04
TRIP BLANK I 2000902410 09/06100 11 :04
SECTION II -Report Summaries· 09/18/2000 19:53
I.IMS Workordcr: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Date& Time Prep
Received Batch ID
09/07/00 10:20 8021
09/07100 I 0:20 8021
09/07100 I 0:20 8021
09/07/00 10:20 8021
09/07/00 10:20 8021
09/07/00 10:20 8021
09/07/00 10:20 8021
09/07100 I 0:20 8043
Hold Time S oec
Date& Time Analysis Date& Time PreD Analvsis
Pre oared Batch ID Analvzed Spec Actua Soec Actua
09/08/00 19:45 8021 09/08/00 19:45 7D 2D 7D 2D
09/08/00 20: 13 8021 09/08/00 20: 13 7D 2D 7D 2D
09/08/00 20:41 8021 09/08/00 20:41 7D 2D 7D 2D
09/08/00 21 :09 8021 09/08/00 21 :09 7D 2D 7D 2D
09/08/00 21 :37 8021 09/08/00 21 :37 7D 2D 7D 2D
09/08/00 22:05 8021 09/08/00 22:05 7D 2D 7D 2D
09/08/00 22:33 8021 09/08/00 22:33 7D 2D 70 20
09111100 15:55 8043 09/11/00 15:55 70 50 70 SD
Page 2 of 55
- - - - - - - - -·-- - - - - - - - -
SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l .3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzf!d
Dilution Factor ·
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
I 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
Aqueous
Receiv~d
NA
0910612000 12:05
09/08/2000 19:45
09/08/2000 19:45
1.0000
MSDA
ug/L
Cone Flag DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
0.413 J 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
UMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 2000902406
Aqueous Aqueous
Received Received
NA NA
09/06/2000 14:00 09/06/2000 13:40
09/08/2000 21 :09 09/08/2000 20:41
09/08/2000 21 :09 09/08/2000 20:41
1.0000 1.0000
MSDA MSDA
ug/L ug/L
Cone Flag DL RL Cone Flag DL RL
ND 0.286 0.000 ND 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND ·0.0622 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
ND 0.0484 0.000 ND 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 4 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Ch loromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
l 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
l 2-Dichloroorooane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
I
cis-1.3-Dichloroorooene 10061-01-5
trans-1,3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
Cone Flaa DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND B 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 2000902406
Cone Flag DL RL Cone Flaa DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.11:3 0.000 ND 0.113 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND 1.05 0.000 ND 1.05 0.000
ND 0.0564 0.000 ND 0.0564 0.000
ND 0.152 0.000 ND 0.152 0.000
ND 0.0939 0.000 ND 0.0939 0.000
ND 0.390 0.000 ND 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0487 0.000 ND 0.0487 0.000
ND 0.0499 0.000 ND 0.0499 0.000
ND 0.0697 0.000 ND 0.0697 0.000
ND 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND 0.0658 0.000 ND 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND B 0.212 0.000 ND B 0.212 0.000
ND 0.167 0.000 ND 0.167 0.000
Page S of 55
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
Isoorooylbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MJBK) 108-10-l
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanen itrile 107-12-0
n-Prooylbenzene 103-65-1
Styrene 100-42-5
I I I 2-Tetrachloroethane 630-20-6
I, 1,2,2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1,2,3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
I. I. I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloronrooane 96-18-4
I I 2-Trichlorotrifluoroethane 76-13-1
I 2 4-Trimethylbenzene 95-63-6
1.3 5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinyl chloride .. 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
; Cone Flaa DL
ND 0.0616
! ND 0.0474
i,. ND 0.0452
I ND 0.114 I ' ND 0.0469
ND 0.0845
ND B 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND B 0.467
ND B 0.118
ND. 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND -0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workordcr: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
0900HBWW216 0900HBWW220
2000902407 2000902406
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND . 0.0845 0.000 .. 0.000 ND B 0.0796 0.000 ND B . 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND . 0.0568 0.000
0.000 ND 0.402 0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND B 0.467 0.000 ND B 0.467 0.000
0.000 ND B 0.118 0.000 ND B 0.118 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.000 ND 0.0749 0.000 ND • 0.0149 0.000
0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 6 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
Cone Flan DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0900HBWW216 0900HBWW220
2000902407 2000902406
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 7 of 55
-------------------
--------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Compound
l-Brorno-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID ·
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor !
Instrument
Units
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWD998
2000902404
Aaueous
Received
NA
09/06/2000 12:05
09/08/2000 19:45
09/08/2000 19:45
1.0000
MSDA
ug/L
% Recovery Limits
84 77-117
IOI 61-143
93 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
F
0900HBWW216 0900HBWW220
2000902407 2000902406
Aaueous Aqueous
Received Received
NA NA
09/06/2000 14:00 09/06/2000 13:40
09/08/2000 21 :09 09/08/2000 20:41
09/08/2000 21 :09 09/08/2000 20:41
1.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recovery Limits F
99 77-117 100 77-117
100 61-143 IOI 61-143
94 87-113 93 87-113
Page 8 of 55
SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepare~
Date/Time Analyze~
Dilution Factor '
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW222
2000902408
Aaueous
Received
NA
09/06/2000 14:20
09/08/2000 21:37
09/08/2000 21 :37
1.0000
MSDA
u!!IL
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N [20009044] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW224 0900HBWW225
2000902402 2000902403
Aaueous Aaueous
Received Received
NA NA
09/06/2000 12:00 0910612000 12: 15
09/08/2000 18:49 09/08/2000 19: 17
09/08/2000 18:49 09/08/2000 19: 17
1.0000 1.0000
MSDA MSDA
uir/L ug/L
Cone Flag DL RL Cone Flag DL RL
ND 0.286 0.000 ND 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
0.350 J 0.0484 0.000 ND 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 9 of 55
-------------------
-------------~-----SECTION IV
Analytical Results
MS-VOA
.SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1,4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorod ifl uoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
1 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1 J-Dichloroorooene 10061-01-5
trans-1.3-D'ichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethyl benzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW222
2000902408
! Cone Flaa DL
' ND 0.0821
I ND 0.111
I ND 0.113
I ND 0.0762
I ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
0.328 J 0.0487
ND 0.0499
0.0766 J 0.0697
0.139 J 0.0603
ND 0.08.13
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND B 0.212
ND 0.167
LIMS Workorder: 756200.UA-Liltle Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
0900HBWW224 0900HBWW225
2000902402 2000902403
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0762 0.000 ND 0.0762 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0487 0.000 ND 0.0487 0.000
0.000 ND 0.0499 0.000 ND 0.0499 0.000
0.000 ND 0.0697 0.000 ND 0.0697 0.000
0.000 ND 0.0603 0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000 ND 0.0813 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0464 0.000 ND 0.0464 0.000
0.000 ND 0.0366 0.000 ND 0.0366 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552. 0.000 ND 0.0552 0.000
0.000 ND B 0.212 0.000 ND B 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 10 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID .
Lab Sample ID ·
Continued
Parameter CAS '
lodomethane 74-88-4 !
lsooroovlbenzene 98-82-8 I
4-lsooroov !toluene 99-87-6 I
Methvl methacrvlate 80-62-6 I
Methvl tert-butvl ether (MTBE) 1634-04-4 !
4-Methvl-2-oentanone <MIBK) I 08-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Pro pan en itrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
1 I 1,2-Tetrachloroethane 630-20-6
I I 2 2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
1,2,4-Trichlorobenzene 120-82-1
1 I 1-Trich loroethane 71-55-6
I, I 2-Trichloroethane 79-00-5
Trichloroethene 79-0I-6
Trichlorotluoromethane 75-69-4
1,2 3-Trichloroorooane 96-18-4
I. I 2-Trichlorotritluoroethane 76-I3-I
I .2 4-Trimethvlbenzene 95-63-6
I 3,5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-0I-4
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW222
2000902408
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND B 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND B 0.467
ND B 0.118
ND 0.033 I
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Liltle Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW224 0900HBWW225
2000902402 2000902403
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0616 0.000 ND 0.0616 0.000
ND 0.0474 0.000 ND 0.0474 0.000
ND 0.0452 0.000 ND 0.0452 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0469 0.000 ND 0.0469 0.000
ND 0.0845 0.000 ND 0.0845 0.000
ND B 0.0796 0.000 ND B 0.0796 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.688 0.000 ND 0.688 0.000
ND 0.0886 0.000 ND 0.0886 0.000
ND 0.0722 0.000 ND 0.0722 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.0792 0.000 ND 0.0792 0.000
ND 0.0568 0.000 ND 0.0568 0.000
ND 0.402 0.000 ND 0.402 0.000
ND 0.0680 0.000 ND 0.0680 0.000
ND B 0.467 0.000 ND B 0.467 0.000
ND B 0.118 0.000 ND B 0.118 0.000
ND 0.0331 O.ObO ND 0.0331 0.000
ND 0.0952 0.000 ND 0.0952 0.000
0.0493 u 0.0905 0.000 ND 0.0905 0.000
ND 0.208 0.000 ND 0.208 0.000
ND 0.0543 0.000 ND 0.0543 0.000
ND 0.0766 0.000 ND 0.0766 0.000
ND 0.0749 0.000 ND 0.0749 0.000
ND 0.0436 0.000 ND 0.0436 0.000
ND 0.0438 0.000 ND 0.0438 0.000
ND 0.0574 0.000 ND 0.0574 0.000
Page 11 or 55
--------------------
-------------------SECTION IV
Analytical· Results
MS-VOA
SW82608
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW222
2000902408
I Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workordcr: 756200.UA-Littlc Washington, N (20009024] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0900HBWW224 0900HBWW225
2000902402 2000902403
Cone Flan DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 12 of 55
SECTION IV
Analytical .Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor ·
Instrument
Units
Surroaate Compound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW222
2000902408
Aaueous
Received
NA
09/06/2000 14:20
09/08/2000 21 :37
09/08/2000 2 l :37
1.0000
MSDA
ug/L
% Recoverv Limits
99 77-117
103 61-143
95 87-113
UMS Workordcr: 756200.UA-Littlc Washington, N (20009024] Hamilton Beach-Proctor Silex
STLAustin
F
0900HBWW224 0900HBWW225
2000902402 2000902403
Aaueous Aqueous
Received Received
NA NA
09/06/2000 12:00 09/06/2000 12: 15
09/08/2000 18:49 09/08/2000 19: 17
09/08/2000 18:49 09/08/2000 19: 17
1.0000 1.0000
MSDA MSDA
U!!/L ug/L
% Recoverv Limits F % Recoverv Limits F
98 77-117 98 77-117
97 61-143 99 61-143
95 87-113 92 87-113
Page 13 or 55
-------------------
- -·-- - - - - - - - - - - - - -·--SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene,
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab S~mple ID
Matrix
Reported As
% Moisture
Date/Time Collect~d
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW226
2000902401
Aoueous
Received
NA
09/06/2000 11 :25
09/08/2000 16:01
09/08/2000 16:0 I
1.0000
MSDA
U!!/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND .0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
0.210 J 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
I.IMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-P.roctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW230 0900HBWW234
2000902409 2000902405
Aoueous Aaueous
Received Received
NA NA
09/06/2000 14:50 09/06/2000 13 :25
09/08/2000 22:05 09/08/2000 20: 13
09/08/2000 22:05 09/08/2000 20: 13
1.0000 1.0000
MSDA MSDA
U!!/L ug/L
Cone Flaa DL RL Cone Flaa DL RL
ND 0.286 0.000 ND 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND . 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
No· 0.0484 0.000 ND 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 14 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Ch loromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Ch lorotoluene 106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1,2-DiChloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1,2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I, 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene I 00-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000· 19:53
0900HBWW226
2000902401
Cone Flaa DL
ND 0.0821
' ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND B 0.212
ND 0.167
LIMS Workorder: 756200.U,6.-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW230 0900HBWW234
2000902409 2000902405
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND 1.05 0.000 ND 1.05 0.000
ND 0.0564 0.000 ND 0.0564 0.000
ND 0.152 0.000 ND 0.152 0.000
ND 0.0939 0.000 ND 0.0939 0.000
ND 0.390 0.000 ND 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0487 0.000 ND 0.0487 0.000
ND 0.0499 0.000 ND 0.0499 0.000
ND 0.0697 0.000 ND 0.0697 0.000
0.102 J 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND 0.0658 0.000 ND 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND B 0.212 0.000 ND B 0.212 0.000
ND 0.167 0.000 ND 0.167 0.000
Page 15 of 55
-------------~-----
- - -·-- - - - - - - - - - - - - - -
SECTION IV
Analytical Results
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
lsoorooylbenzene 98-82-8
4-lsopropyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
4-Methyl-2-pentanone <MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-ProoYlbenzene 103-65-1
Styrene 100-42-5
I I 1.2-Tetrachloroethane 630-20-6
I I 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1,2 4-Trichlorobenzene 120-82-1
I I. I-Trichloroethane 71-55-6
I 1,2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2.3-Trichloroorooane 96-18-4
1 1,2-Trichlorotrifluoroethane 76-13-1
I 2.4-Trimethylbenzene 95-63-6
I 3 5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinyl chloride .. 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW226
2000902401
I Cone Flaa DL
ND 0.0616
' ND 0.0474 i
i. ND 0.0452 l
I ND 0.114
ND 0.0469
ND 0.0845
ND B 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND B 0.467
ND B 0.118
ND 0.0331
ND 0.0952
0.0945 J 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Littlc Washington, N (20009024] Hamilton Beach-Proctor Silex
STLAustin
0900HBWW230 0900HBWW234
2000902409 2000902405
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
0.000 ND 0.0469 0.000 ND . -0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND B 0.0796 0.000 ND B 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
O.ObO ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.000 ND 0.402 0.000 ND 0.402 0.000
0.000 0.126 J 0.0680 0.000 ND 0.0680 0.000
0.000 ND B 0.467 0.000 ND B 0.467 0.000
0.000 ND B 0.118 0.000 ND B 0.118 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000. 0.355 J 0.0905 0.000 ND 0.0905 0.000
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 16 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results· 09/18/2000 19:53
0900HBWW226
2000902401
Cone Flaa DL
ND 0.137
ND 0.0713
' I.
LIMS Workordcr: 756200.UA·i uh: Washington, N [20009024] llamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0900HBWW230 0900HBWW234
2000902409 2000902405
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 17 of 55
--------------~----
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collect~d
Date/Time Prepare~
Date/Time Analyz~d
Dilution Factor 1
Instrument
Units
Surroaate Comoound
J-Bromo-4-fluorobenzene
I .2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/18/2000 19:53
0900HBWW226
2000902401
Aaueous
Received
NA
0910612000 11 :25
09/08/2000 16:0 I
09/08/2000 16:0 I
1.0000
MSDA
u11:/L
% Recoverv Limits
98 77-117
99 61-143
94 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
F
0900HBWW230 0900HBWW234
2000902409 2000902405
Aqueous Aqueous
Received Received
NA NA
09/06/2000 14:50 0910612000 13:25
09/08/2000 22:05 09/08/2000 20: 13
09/08/2000 22:05 09/08/2000 20: 13
1.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits F
99 77-117 98 77-117
JOO 61-143 103 61-143
94 87-113 93 87-113
Page 18 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepare~
Date/Time Analyzed
Dilution Factor 1
Instrument
Units
CAS
67-64-l
75-05-8
107-02-8
107-13-l
71-43-2
108-86-l
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:53
TRIP BLANK I
2000902410
Aaueous
Received
NA
0910612000 I I :04
09/08/2000 22:33
09/08/2000 22:33
l.0000
MSDA
W!/L
Cone Flaa DL
ND R 0.286
ND R l.67
ND R 0.983
ND R 0.0901
ND R 0.0492
ND R 0.0622
ND R 0.139
ND R 0.0683
ND R 0.136
ND R 0.106
ND R 0.179
ND R 0.0642
ND R 0.0745
ND R 0.0958
ND R 0.0484
ND R 0.0867
ND R 0.0839
ND R 0.0473
ND R 0.0756
ND R 0.0670
ND R 0.113
LIMS Workorder: 756200.UA-Littie Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
TRIP BLANK I
2000902410
Aaueous
Received
NA
09/06/2000 I I :04
09/l I/2000 15:55
09/l I/2000 15:55
1.0000
MSDB
U!!/L
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.499 0.000
0.000 ND 4.47 0.000
0.000 ND 0.942 0.000
0.000 ND 0.344 0.000
0.000 ND 0.0353 0.000
0.000 ND 0.0802 0.000
0.000 ND 0.0810 0.000
0.000 ND 0.0567 0.000
0.000 ND 0.118 0.000
0.000 ND 0.0844 0.000
0.000 ND 0.105 0.000
0.000 ND 0.0761 0.000
0.000 ND 0.0671 0.000
0.000 ND 0.0266 0.000
0.000 ND 0.0380 0.000
0.000 ND 0.0930 0.000
0.000 ND 0.0815 0.000
0.000 ND 0.0258 0.000
0.000 ND 0.0701 0.000
0.000 ND 0.0712 0.000
0.000 ND 0.0885 0.000
Page 19 of 55
-------------------
---·----------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
I 06-43-4
I ,2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1,2-Dichlorobenzene 95-50-1
1.3-Dich lorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloropropane 78-87-5
1 3-Dichloroorooane 142-28-9
2 2-Dichloroprooane 594-20-7
I 1-Dichloropropene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1,3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:53
TRIP BLANK 1
2000902410
I Cone Flaa DL
' ND R 0.0821 I
I ND R 0.111
I ND R 0.113
I ND R 0.0762
I ND R 1.05
ND R 0.0564
ND R 0.152
ND R 0.0939
ND R 0.390
' ND R 0.0587
ND R 0.0920
ND R 0.0591
ND R 0.113
ND R 0.0487
ND R 0.0499
ND R 0.0697
ND R 0.0603
ND R 0.0813
ND R 0.0670
ND R 0.0451
' ND R 0.0714
ND R 0.0464
ND R 0.0366
ND R 0.0658
ND R 0.0647
ND R 0.0552
ND R 0.212
ND R 0.167
LIMS Workordcr: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
sn; Austin
TRIP BLANK I
2000902410
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 0.130 0.000
0.000 ND 0.0252 0.000
0.000 ND 0.0689 0.000
0.000 ND 0.0788 0.000
0.000 ND 1.18 0.000 -0.000 ND 0.0469 0.000
0.000 ND 0.0713 0.000
0.000 ND 0.114 0.000
0.000 ND 0.336 0.000
0.000 ND 0.0493 0.000
0.000 ND 0.0488 0.000
0.000 ND 0.0467 0.000
0.000 ND 0.175 0.000
0.000 ND 0.0416 0.000
0.000 ND 0.0619 0.000
0.000 ND 0.0436 0.000
0.000 ND 0.0437 0.000
0.000 ND 0.0906 0.000
0.000 ND 0.0321 0.000
0.000 ND 0.0789 0.000
0.000 ND 0.0670 0.000
0.000 ND 0.0563 0.000
0.000 ND 0.0486 0.000
0.000 ND 0.0793 0.000
0.000 ND 0.0961 0.000
0.000" ND 0.0539 0.000
0.000 ND 0.369 0.000
0.000 ND 0.168 0.000
Page 20 of 55
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Jodomethane 74-88-4
Jsopropylbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile I 07-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I l.l 2-Tetrachloroethane 630-20-6
I I 2,2-Tetrachlornethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-1
I I. I -Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloropropane 96-18-4
I.I 2-Trich lorotrifluoroethane 76-13-1
1.2 4-Trimethylbenzene 95-63-6
I 3.5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:53
TRIP BLANK I
2000902410
! Cone Flaa DL
ND R 0.0616
I ND R 0.0474
' ND R 0.0452 I
I ND R 0.114
I ND R 0.0469
ND R 0.0845
ND R 0.0796
ND R 0.106
ND R 0.688
ND R 0.0886
ND R 0.0722
ND R 0.0948
ND R 0.0792
ND R 0.0568
ND R 0.402
ND R 0.0680
ND R 0.467
ND R 0.1 f8
ND R 0.0331
ND R 0.0952
ND R 0.0905
ND R 0.208
ND R 0.0543
ND R 0.0766
ND R 0.0749
ND R 0.0436
ND R 0.0438
ND R 0.0574
UMS Workorder: 756200.UA-Little Washington, N (20009024) Hamilton Beach-Proctor Silex
STLAustin
TRIP BLANK I
2000902410
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0556 0.000
0.000 ND 0.0361 0.000
0.000 ND 0.0532 0.000
0.000 ND 0.150 0.000
0.000 ND 0.0493 0.000
0.000 ND 0.0894 0.000
0.000 ND 0.0789 0.000
0.000 ND 0.112 0.000
0.000 ND 0.733 0.000
0.000 ND 0.0824 0.000
0.000 ND 0.0525 0.000
0.000 ND 0.0831 0.000
0.000 ND 0.0774 0.000
0.000 ND 0.109 0.000
0.000 ND 0.512 0.000
0.000 ND 0.0359 0.000
0.000 ND 0.263 0.000
0.000 ND 0.177 0.000
0.000 ND 0.0183 0.000
0.000 ND 0.133 0.000
0.000 ND 0.0494 0.000
0.000 ND 0.0665 0.000
0.000 ND 0.0843 0.000
0.000 ND 0.170 0.000
0.000 ND 0.0478 0.000
0.000 ND 0.0393 0.000
0.000 ND 0.0425 0.000
0.000 ND 0.0555 0.000
Page 21 of 55
-------------------
-------------------SECTION IV
Analytical ·Results
MS-VOA
SW8260B
Continued
Parameter
p-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:53
TRIP BLANK I
2000902410
I Cone Flaa DL
ND R 0.137
ND R 0.0713
LIMS Workordcr: 756200.UA-Liltle Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
TRIP BLANK I
2000902410
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0861 0.000
0.000 ND 0.0361 0.000
Page 22 of 55
SECTION IV
Analytical ·Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collect~d
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor
Instrument
Units
Surroaate Comoound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/18/2000 19:53
TRIP BLANK I
2000902410
Aaueous
Received
NA
09/06/2000 11 :04
09/08/2000 22:33
09/08/2000 22:33
1.0000
MSDA
ug/L
% Recoverv Limits
99 77-117
103 61-143
84 87-113
UMS Workordcr: 756200.UA-Littlc Washington, N (20009024] Hamilton Beach-Proctor Silex
STL Austin
TRIP BLANK I
20009024.10
Aaueous
Received
NA
09/06/2000 1 I :04
09/11/2000 15:55
09/11/2000 15:55
1.0000
MSDB
ug/L
F % Recoverv Limits F % Recoverv Limits F
93 77-117
107 61-143
0 97 87-113
Page 23 of 55
- --· - - - - - - - - - - - - - - - -
- - - ----------------
SECTIONV
Calibration and QC Information ·
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 8021 Instrument Data File: A0908002.D
Instrument ID: MSDA Analyst: JEC
Parameter Reference Value Measured Cone
Acetone 20 ! 15.5
Acetonitrile 100 87.5
Acrolein 100 44.5
Acrvlonitrile 20 17.2
Benzene 20 19.6
Bromobenzene 20 20.1
Bromochloromethane 20 23.5
Bromodichloromethane 20 16.8
Bromoform 20 18.2
Bromomethane 20 13.1
2-Butanone (MEK) 20 19.0
n-Butvlbenzene 20 19.4
sec-Butvlbenzene 20 19.8
tert-Butylbenzene 20 19.2
Carbon disulfide 20 14.3
Carbon tefrachloride 20 14.8
2-Chloro-1 3-butadiene 20 20.4
Chlorobenzene 20 21.5
Ch loroethane 20 18.3
Chloroform 20 20.6
I -Ch lorohexane 20 22.7
Chloromethane 20 13.9
3-Chloropropene 20 12.7
2-Chlorotoluene 20 19.9
4-Chlorotoluene 20 19.7
I 2-Dibromo-3-chloroprooane 20 20.2
SECTION V -Calibration and QC Information -09/18/2000 19:53 .
UMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:09/08/2000 14:09
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
77
87
44
86
98
IOI
118
84
91
66
95
97
99
96
72
74
102
108
91
103 80-120
114
70
63
99
98
IOI
Page 24 or 55
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 8021 Instrument Data File: A0908002.D
Instrument ID: MSDA Analyst: jEc
Continued
Parameter Reference 'Value Measured Cone
Dibromochloromethane 20 I 17.8
I 2-Dibromoethane 20 19.7
Dibromomethane 20 18.7
trans-I .4-Dichloro-2-butene 20 9.68
I 4-Dichlorobenzene 20 18.8
1.2-Dichlorobenzene 20 19.3
I 3-Dichlorobenzene 20 19.0
Dichlorodifluoromethane 20 9.55
I 1-Dichloroethane 20 19.4
1,2-Dichloroethane 20 18.7
1.1-Dichloroethene 20 16.9
cis-1 2-Dichloroethene 20 22.5
trans-1,2-Dichloroethene 20 19.4
1.2-Dichloroprooane 20 18.9
1.3-Dichloroorooane 20 19.3
2.2-Dichloroorooane 20 21.1
I 1-Dichloropropene 20 18.9
cis-1.3-Dichloroorooene 20 17.1
trans-I 3-Dichloroorooene 20 16.4
Ethvl methacrvlate 20 19.1
Ethvlbenzene 20 21.0
Hexachloro-1.3-butadiene 20 26.6
2-Hexanone 20 17.2
lodomethane 20 14.6
lsooroovlbenzene 20 20.9
4-lsoproovltoluene 20 19.7
SECTION V -Calibrqtion and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:09/08/2000 14:09
Units: ug/L
%Recoverv Flag QC Limits %Recoverv
89
99
93
48
94
97
95
48
97
93
84 80-120
113
97
95 80-120
97
105
94
85
82
96
105 80-120
133
86
73
105
99
Page 25 of 55
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW82608
Sample Type: Continuing Calibration Check I Analysis Batch ID:
-Instrument ID:
8021 1 Instrument Data File:
MSDA Analyst:
Continued
Parameter Reference Value Measured Cone
Methvl methacrvlate 20 : 18.7
Methyl tert-butyl ether (MTBE) 20 : . 19.2
4-Methyl-2-oentanone (MIBK) 20 i 18.8
Methvlene chloride 20 18.6
Naphthalene ' 20 24.9
Prooanenitrile 100 96.l
n-Prooylbenzene 20 20.4
Styrene 20 21.2
I I. I 2-Tetrachloroethane 20 20.l
I, 1,2 2-Tetrachloroethane 20 20.5
Tetrachloroethene 20 22.4
Tetrah vd rofuran 20 21.2
Toluene 20 20.4
I 2 3-Trichlorobenzene 20 31.8
I 2 4-Trichlorobenzene 20 26.9
I I I-Trichloroethane 20 20.8
I I 2-Trichloroethane 20 20.7
Trichloroethene 20 21.8
Trichlorofluoromethane 20 21.2
1,2 3-Trichloroorooane 20 18.9
I I 2-Trichlorotrifluoroethane 20 14.2
1,2,4-Trimethvlbenzene 20 18.8
13 5-Trimethylbenzene 20 18.7
Vinyl acetate 20 19.8
Vinyl chloride 20 16.6
o-Xvlene/m-Xylene 40 42.9
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024) Hamilton Beach-Pr~ctor Silex
STLAustin
A0908002.D
JEC
Flaa %Recoverv
93
96
94
93
125
96
102
106
IOI
102
112
106
102
159
135
104
104
109
106
95
71
94
94
99
83
107
Date/Time Analyzed:09/08/2000 14:09
Units: ug/L
Flaa QC Limits %Recoverv
80-120
80-120
Page 26 of 55
-------------------SECTIONV
Calibration and QC Information
Calibration Verification·Results
MS-VOA
SW82608
Sample Type: Continuing Calibration Check
Analysis Batch ID: 8043 Instrument Data File: 80911002.D
Instrument ID: MSDB Analyst: JEC
Parameter Reference!Value Measured Cone
Acetone 20 21.0
Acetonitrile 100 I 100
Acrolein 100 ' 75.8
Acrvlonitrile 20 19.9
Benzene 20 20.2
Bromobenzene 20 20.6
Bromochloromethane 20 19.2
Bromodichloromethane 20 20.0
Bromoform 20 18.3
Bromomethane 20 18.3
2-Butanone (MEK) 20 17.6
n-Butvlbenzene 20 22.0
sec-Butvlbenzene 20 21.9
tert-Butvlbenzene 20 21.9
Carbon disulfide 20 33.5
Carbon tetrachloride 20 19.6
2-Chloro-I 3-butadiene 20 20.3
Ch lorobenzene 20 19.5
Chloroethane 20 21.3
Chloroform 20 20.6
1-Chlorohexane 20 21.2
Chloromethane 20 21.5
3-Chloroorooene 20 22.1
2-Chlorotoluene 20 21.7
4-Chlorotoluene 20 21.7
I 2-Dibromo-3-chloroorooane 20 18.6
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N (20009024] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:09/l l/2000 14:07
Units: ug/L
%Recoverv Fla Cl QC Limits %Recoverv
105
.100
76
99
101
103
96
100
92
92
88
110
109
110
168
98
102
98
106
103 80-120
106
107
111
108
109
93
Page 28 or 55
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibratipn Check
Analysis Batch ID: 8043 Instrument Data File: 80911002.D
Instrument ID: MSDB Analys_t: ·JEC
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 19.7
I 2-Dibromoethane 20 19.2
Dibromomethane 20 19.7
trans-I 4-Dichloro-2-butene 20 20.0
I 4-Dichlorobenzene 20 20.I
1,2-Dichlorobenzene 20 20.3
I ,3-Dichlorobenzene 20 20.5
Dichloroditluoromethane 20 27.9
I, 1-Dichloroethane 20 20.8
I 2-Dichloroethane 20 20.3
1.1-Dichloroethene 20 21.4
cis-1,2-Dichloroethene 20 20.6
trans-1,2-Dichloroethene 20 19.5
1,2-Dichloroorooane 20 20.3
I 3-Dichloroorooane 20 19.6
2 2-Dichloroorooane 20 22.2
I 1-Dichloroorooene 20 20.6
cis-1 3-Dichloroorooene 20 19.7
trans-I 3-Dichloroorooene 20 20.3
Ethvl methacrvlate 20 19.2
Ethvlbenzene 20 20.7
Hexachloro-1 3-butadiene 20 17.8
2-Hexanone 20 18.1
lodomethane 20 17.7
lsooroovlbenzene 20 20.5
4-lsooroovltoluene 20 21.9
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workordcr: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:09/l l/2000 14:07
Units: ug/L
%Recoverv Flag QC Limits %Recoverv
99
96
98
100
100
IOI
103
140
104
102
107 80-120
103
98
IOI 80-120
98
111
103
99
102
96
104 80-120
89
90
89
103
110
----------------
Page 29 of 55
-- -
- ------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibratio,n Check
Analysis Batch ID: 8043 Instrument Data File: 80911002.D
Instrument ID: MSDB Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Methyl methacrylate 20 I 19.8
Methyl tert-butvl ether (MTBE) 20 i 20.6
4-MethYl-2-oentanone (MIBK) 20 I 18.8
Methylene chloride 20 I 19.6
Naohthalene 20 17.5
Propanenitrile 100 102
n-Proovlbenzene 20 22.7
Styrene 20 20.l
1 I.I 2-Tetrachloroethane 20 19.9
I 1,2 2-Tetrachloroethane 20 19.9
Tetrachloroethene 20 20.1
Tetrahvdrofuran 20 19.8
Toluene 20 21.0
1.2 3-Trich lorobenzene 20 17.5
1.2 4-Trich lorobenzene 20 18.5
I I I-Trichloroethane 20 20.6
I. I 2-Trichloroethane 20 20.0
Trichloroethene 20 19.8
Trichlorofluoromethane 20 30.4
I 2 3-Trichloroorooane 20 19.0
I 1.2-Trichlorotrifluoroethane 20 18.8
I 2,4-TrimethYlbenzene 20 22.3
1.3.5-Trimethvlbenzene 20 22.1
Vinyl acetate 20 21.9
Vinyl chloride 20 21.4
o-Xylene/m-Xvlene 40 41.2
SECTION V -Calibration and QC Information -09/18/2000 I 9:53
UMS Workorder: 756200.UA-Little Washi~gton, N (20009024] Hamilton Beach-Proctor Silex
STLAustin
Flaa
.
Date/Time Analyzed:09/11/2000 14:07
Units: ug/L
%Recoverv Flaa QC Limits %Recovery
99
103
94
98
87
102
114
100
99
99
100
99
105 80-120
87
n
103
100
99
152
95
94
112
111
110
107 80-120
103
Page 30 of 55
-------- - - - --------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 8021
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
I I i
:
'
Instrument Data File: A0908002.D
Injection Tjme: 09/08/2000 14:09
Ion Abundance Criteria
Lower limit Uooer Limit
15 40
30 60
JOO 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024) Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 09/08/2000 14:09
Analyst: JEC
% Relative Abundance
21.7
39
100
6
0
73.7
6.5
98.6
6.3
Page 32 of 55
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 8043
Instrument ID: MSDB
Mass/Enerav
50
75
95
96
173
174
175
176
177
I
I
Instrument Data File: 80911002.D
Injection Time: 09/11/2000 14:07
Ion Abundance Criteria
Lower Limit Uooer Limit
15 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workordcr: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 09/11/2000 14:07
Analyst: JEC
% Relative Abundance
33.2
48.2
100
6.6
0
71.5
7.3
98.5
6.6
Page 33 or 55
- -- - - - --------- - - - -
-------------------
SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Ch loromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepar~d
Date/Time Analyz~d
Instrument ·
Units
CAS
67-64-1 i
75-05-8
107-02-8
. 107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
SECTION V -Calibration and QC Information -09/18/2000 19:53
1014308
Method Blank
Aaueous
09/08/2000 15:33
09/08/2000 15:33
MSDA
ug/L
Cone Flag DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
UMS Workordcr: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
1014397
Method Blank
Aqueous
09/11/2000 15:28
09/11/200015:28
MSDB
ug/L
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 0.499 0.000
0.000 ND 4.47 0.000
0.000 ND 0.942 0.000
0.000 ND 0.344 0.000
0.000 ND 0.0353 0.000
0.000 ND 0.0802 0.000
0.000 ND 0.0810 0.000
0.000 ND 0.0567 0.000
0.000 ND 0.118 0.000
0.000 ND 0.0844 0.000
0.000 ND 0.105 0.000
0.000 ND 0.0761 0.000
0.000 ND 0.0671 0.000
0.000 ND 0.0266 0.000
0.000 ND 0.0380 0.000
0.000 ND 0.0930 0.000
0.000 ND 0.0815 0.000
0.000 ND 0.0258 0.000
0.000 ND 0.0701 0.000
0.000 ND 0.0712 0.000
0.000 ND 0.0885 0.000
0.000. ND 0.130 0.000
0.000 ND 0.0252 0.000
0.000 ND 0.0689 0.000
0.000 ND 0.0788 0.000
Page 34 or 55
SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
I 2-Dibromo-3-chloroorooane 96-12-8
Oibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4 I
Dibromomethane 74-95-3 !
trans-1,4-0ichloro-2-butene 110-57-6 I
1.4-Dichlorobenzene 106-46-7
1 2-0ichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Oichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1 2-Dich1oroethene 156-59-2
trans-1,2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
l 3-Dichloroorooane 142-28-9
2,2-Dichloroorooane 594-20-7
l, 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
EthYlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
lodomethane 74-88-4
lsoorooylbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
SECTION V -Calibration and QC Information -09/18/2000 19:53
1014308
Cone Flaa DL
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
0.326 J 0.212
ND 0.167
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
1014397
RL Cone Flaa DL RL Cone Flag DL RL
0.000 ND 1.18 0.000
0.000 ND 0.0469 0.000
0.000 ND 0.0713 0.000
0.000 ND 0.114 0.000
0.000 ND 0.336 0.000
0.000 ND 0.0493 0.000
0.000 NO 0.0488 0.000
0.000 ND 0.0467 0.000
0.000 ND 0.175 0.000
0.000 ND 0.0416 0.000
0.000 ND 0.0619 0.000
0.000 ND 0.0436 0.000
0.000 ND 0.0437 0.000
0.000 ND 0.0906 0.000
0.000 ND 0.0321 0.000
0.000 ND 0.0789 0.000
0.000 ND 0.0670 0.000
0.000 ND 0.0563 0.000
0.000 ND 0.0486 0.000
0.000 ND 0.0793 0.000
0.000 ND 0.0961 0.000
0.000 ND 0.0539 0.000
0.000 ND 0.369 0.000
0.000 ND 0.168 0.000
0.000 ND 0.0556 0.000
0.000 ND 0.0361 0.000
0.000 ND 0.0532 0.000
0.000 ND 0.150 0.000
0.000 ND 0.0493 0.000
Page 35 of 55
-------------------
-------------------SECTION V
Calibration and QC Information
Method ·Blank Results
MS-VOA
SW8260B
Method Blank ID 1
Continued
Parameter CAS :
4-Methvl-2-pentanone (MIBK) 108-10-1 '
Methvlene chloride 75-09-2
Naohthalene 91-20-3 I
Propanenitrile 107-12-0 I. !
n-Propylbenzene 103-65-1 I
Stvrene 100-42-5
I I 1,2-Tetrachloroethane 630-20-6
1.1 2 2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
1.1 I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorotluoromethane 75-69-4
1,2 3-Trichloroorooane 96-18-4
I. I 2-Trichlorotritluoroethane 76-13-1
1,2 4-Trimethvlbenzene 95-63-6
I 3,5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
o-Xvlene/m-Xvlene 106-42-3
o-Xvlene 95-47-6
SECTION V -Calibration and QC Information -09/18/2000 19:53
1014308
Cone Flaa DL
ND 0.0845
2.27 0 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
0.902 J 0.467
0.425 J 0.118
ND 0.0331
ND 0.0952
0.0894 u 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20009Q24] Hamilton Beach-Proctor Silex
STLAustin
1014397
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 0.0894 0.000
0.000 ND 0.0789 0.000
0.000 ND 0.112 0.000
0.000 ND 0.733 0.000 -0.000 ND 0.0824 0.000
0.000 ND 0.0525 0.000 -·
0.000 ND 0.0831 0.000
0.000 ND 0.0774 0.000
0.000 ND 0.109 0.000
0.000 ND 0.512 0.000
0.000 ND 0.0359 0.000
0.000 ND 0.263 0.000
0.000 ND 0.177 0.000
0.000 ND 0.0183 0.000
0.000 ND 0.133 0.000
0.000 ND 0.0494 0.000 ·-
0.000 ND 0.0665 0.000
0.000 ND 0.0843 0.000
0.000 ND 0.170 0.000
0.000 ND 0.0478 0.000
0.000 ND 0.0393 0.000
0.000 ND 0.0425 0.000
0.000 ND 0.0555 0.000
0.000 ND 0.0861 0.000
0.000 ND 0.0361 0.000 -
Page 36 of 55
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
Surrogate Comoound
1-Bromo-4-fluorobenzene
I .2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -09/ 18/2000 19:53
1014308
Method Blank
Aaueous
09/08/2000 15:33
09/08/2000 15:33
MSDA
u11:/L
% Recoverv Limits
98 77-117
103 61-143
92 87-I 13
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
1014397
Method Blank
Aaueous
09/11/2000 15:28
09/1112000 15:28
MSDB
u11:/L
F % Recovery Limits F % Recoverv Limits F
93 77-117
105 61-143
JOO 87-113
Page 37 of 55
-------------------
-------·-------·--·---SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Client Sample ID:
Sample Type:
Prep Batch ID:
Analysis Batch ID:
0900HBWW226
Matrix Spike
8021
8021
p a rent s amp:e
2000902401
Oil Fae: I
1.0000
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
S "k dS iPI e ampe
Lab ID: 1014309
Oil Fae: 1.0000
File ID: A0908007.D
Parameter Cone Fla Sok Cone Cone %Rec Fla
Acetone ND 20 14.6
Acetonitrile ND 100 80.7
Acrolein ND 100 38.6
Acrylonitrile ND 20 15.8
Benzene ND 20· 18.I
Bromobenzene ND 20 18.5
Bromochloromethane ND 20 21.5
Bromodichloromethane ND 20 15.7
Bromoform ND 20 17.2
Bromomethane ND 20 I 1.9
2-Butanone (MEK) ND 20 18.6
n-Butvlbenzene ND 20 17.7
sec-Butvlbenzene ND 20 18.0
tert-Butvlbenzene ND 20 17.4
Carbon disulfide 0.210 J 20 16. I
Carbon tetrachloride ND 20 14.3
2-Ch loro-I .3-butadiene ND 20 19.7
Chlorobenzene ND 20 19.6
Chloroethane . ND 20 17.6
Chloroform ND 20 19.2
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024].Hamilton Beach-Proctor Silex
STL Austin
73
81
39 0
79
90
92
107
79
86
60
93
88
90
87
79
72
98
98
88
96
Lab ID:
Oil Fae:
File ID:
Spk Cone
20
JOO
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
JEC Analyst:
s "k d s iPI e amp e up1ca e I D r t
1014310
1.0000
A0908008.D
Cone %Rec Fla
14.2 71
81.9 82
38.5 38 0
15.8 79
18.2 91
18.1 91
21.9 110
15.4 77
15.5 78
12.2 61
19.6 98
18.1 90
18.5 92
18.0 90
13.3 66
13.8 69
19.9 99
20.1 IOI
17.9 89
19.4 9i
QC Limits
RPO Fla %Rec RPO
2.8 0.1-240 71
1.2 70-130 25
2.6 70-130 25
0 70-130 25
I. I 71-133 17
I. I 67-127 12
2.8 61-145 21
2.6 57-135 19
9.8 ,, -23-151 17
1.7 34-128 25
5.2 0.1-214 39
2.2 28-184 30
2.2 45:160 31
3.4 65-148 27
18 29-223 23
4.3 46-150 23
I 70-130 25
3 77-129 14
I. I 39-133 27
I 64-146 16
Page 38 of 55
SECTIONV
Calibration and QC Information·
Spiked Sample Results
MS-VOA
SW8260B
p arent contmue
2000902401
Oil Fae: I
d s .k d s IOI e amn e contmue d
LablO: 1014309
Oil Fae: 1.0000
1.0000 ' FilelO: A0908007.D
Parameter Cone Fla Sok Cone Cone
1-Chlorohexane ND 20 21.0
Ch loromethane ND 20 12.1
3-Chloropropene ND 20 14.5
2-Chlorotoluene ND 20 18.6
4-Chlorotoluene ND 20 17.9
I 2-Dibromo-3-chloroorooane ND 20 17.4
Dibromochloromethane ND 20 16.8
I 2-Dibromoethane ND 20 18.4
Dibromomethane ND 20 16.6
trans-1,4-Dichloro-2-butene ND 20 11.0
I 4-Dichlorobenzene ND 20 17.2
1,2-Dichlorobenzene ND 20 17.9
1.3-Dichlorobenzene ND 20 17.2
Dichlorodifluoromethane ND 20 8.98
I 1-Dichloroethane ND 20 18.5
1.2-Dichloroethane ND 20 17.2
1 1-Dichloroethene ND 20 16.5
cis-1 2-Dichloroethene ND 20 21.1
trans-1 2-Dichloroethene ND 20 19.0
1.2-Dich loropropane ND 20 17.5
1,3-Dichloroorooane ND 20 17.0
2.2-Dichloroorooane ND 20 19.9
I, 1-Dichloroprooene ND 20 16.6
cis-1,3-Dichloroorooene ND 20 17.2
trans-1 3-Dichloropropene ND 20 15.7
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
105
60
72
93
90
87
84
92
83
55 0
86
90
86
45
92
86
83
105
95
87
85
99
83
86
78
s ioike dS amoe uo 1cate contmue I D r d
LablO: 1014310
Oil Fae: 1.0000 QC Limits
FilelO: A0908008.D
Sok Cone Cone %Rec Fla RPO Fla %Rec RPO
20 21.7 109 3.7 70-130 25
20 12.2 61 1.7 18-140 26
20 12.4 62 0 15 70-130 25
20 18.9 94 I. I 70-136 24
20 18.2 91 1.1 74-132 23
20 16.9 85 2.3 39-171 25
20 15.8 79 6.1 45-137 15
20 18.9 95 3.2 19-187 19
20 17.0 85 2.4 52-138 21
20 9.76 49 0 12 70-130 25
20 17.3 86 0 70-132 13
20 18.1 91 I. I 67-135 14
20 17.7 88 2.3 68-134 14
20 9.08 45 0 0.1-166 26
20 18.3 92 0 66-138 19
20 17.2 86 0 48-152 23
20 16.6 83 0 47-175 25
20 21.1 106 0.9 66-144 18
20 19.2 96 I 62-146 22
20 17.7 89 2.3 61-133 17
20 17.9 90 5.7 70-128. 16
20 20.3 IOI 2 40-168 30
20 17.8 89 7 71-155 31
20 16.1 81 6 36-142 16
20 15.5 78 0 34-138 21
Page 39 of 55
-------------~-----
- - - -......... - - - -.. ~--·--·-- -
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW82608
p arent contmue d
Oil Fae:
s "k s >DI ed amn e contmued
Lab ID: 1014309
Oil Fae: 1.0000
2000902401
1.0000 File ID: A0908007.D
Parameter Cone I Fla Sok Cone Cone
Ethvl methacrvlate ND I 20 17.3
Ethyl benzene ND I 20 19.6
Hexachloro-I ,3-butadiene ND I B 20 23.9
2-Hexanone ND I 20 16.7
Iodomethane ND ' 20 14.8
lsooroovlbenzene ND ' 20 19.6
4-Isopropyltoluene ND 20 18.0
Methvl methacrvlate ND 20 16.4
Methvl tert-butyl ether (MTBE) ND . I 20 17.7
4-Methvl-2-pentanone (MIBK) ND 20 16.4
Methvlene chloride ND B 20 17.2
Naphthalene ND 20 23.4
Prooanenitrile ND 100 89.9
n-Proovlbenzene ND 20 18.9
Styrene ND 20 19.4
I. I 1 2-Tetrachloroethane ND 20 18.2
I. I 2 2-Tetrachloroethane ND 20 18.3.
Tetrachloroethene ND. 20 20.6
Tetrahydrofuran ND 20 20.I
Toluene ND 20 18.9
I 2,3-Trichlorobenzene ND B 20 29.3
I 2.4-Trichlorobenzene ND B 20 24.3
I I.I -Trichloroethane ND 20 19.4
I 1,2-Trichloroethane ND 20 18.6
Trichloroethene 0.0945 J 20 19.9
Note: Spike Concentration for solid matrices not ~djusted for percent moisture.
·SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Littlc Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
%Rec Fla
86
98
119
84
74
98
90
82
88
82
86
117
90
94
97
91
91
103
100
95
147 0
122
97
93
99
Soiked s amoe up 1cate contmue I D r d
Lab ID: 1014310
Oil Fae: 1.0000 QC Limits
File ID: A0908008.D
Sok Cone Cone %Rec Fla RPO Fla %Rec RPO
20 18.0 90 4.5 70-130 25
20 20.5 103 5 75-131 14
20 25.2 126 5.7 46-150 34
20 16.9 85 1.2 ., 22-104 34
20 15.3 76 2.7 70-130 25
20 20.0 100 2 54-152 26
20 18.1 90 0 41-165 28
20 16.9 85 3.6 70-130 25
20 19.8 99 12 70-.130 25
20 16.1 81 1.2 27-149 36
20 17.2 86 0 36-166 23
20 24.3 122 4.2 32-172 22
100 93.1 93 3.3 70-130 25
20 18.9 94 0 .. 61-143 28
20 19.9 100 3 68-136 14
20 19.0 95 4.3 63-141 20
20 19.3 96 5.3 47-143 20
20 21.3 107 3.8 69-137 16
20 18.2 91 9.4
20 19.7 98 3.1 70-132 17
20 29.3 146 0 0.7 66-140 20
20 25.2 126 3.2 66-144 22
20 19.6 98 I 49-155 24
20 19.4 97 4.2 67-135 17
20 20.3 IOI 2 71-129 17
Page 40 of 55
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
p t f d aren con mue
2000902401
Oil Fae: 1
s "k d s iDI e amn e contmued
LablO: 1014309
Oil Fae: 1.0000
1.0000 File ID: A0908007.D
Parameter Cone ' Fla Sok Cone Cone
Trichlorofluoromethane ND ! 20 20.0
1.2 3-Trichloroprooane ND ' 20 17.1
I I 2-Trichlorotrifluoroethane ND : 20 14.0
I 2 4-Trimethvlbenzene ND 20 17.2
1.3 5-Trimethvlbenzene ND 20 17.4
Vinvl acetate ND 20 18.3
Vinvl chloride ND 20 15.6
o-X vlene/m-X vlene ND 40 39.1
o-Xvlene ND 20 20.1
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024) Hamilton Beach-Proctor Silex
STL Austin
%Rec Fla
100
86
70
86
87
92
78
98
IOI
Spiked Samole Duolicate contmue d
Lab ID: 1014310
Oil Fae: 1.0000 QC Limits
File ID: A0908008.D
Sok Cone Cone %Rec Fla RPO Fla %Rec RPO
20 20.5 103 3 39-147 29
20 18.0 90 4.5 64-140 18
20 13.9 69 1.4
20 17.5 88 2.3 54-156 25
20 17.7 88 I. I 62-144 25
20 18.7 94 2.2 0.1-164 31
20 15.6 78 0 24-138 27
40 41.1 103 5 76-134 15
20 20.6 103 2 77-131 15
Page 41 of 55 ----~·-.... - --· ---/--· -~ ... - -
SECTION V
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
Parameter
Acetone
Benzene
Bromobenzene
Bromochloromethane
LCSforHBN8021 [MSY/1313]
8021
8021
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
Ch lorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
I 2-Dibromo-3-chloroorooane
Dibromochloromethane
1.2-Dibromoethane
Dibromomethane
I 4-Dichlorobenzene
SECTION V -Calibration and QC Information -09/18/2000 19:53
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
c ontro IS a mole
Lab ID: 1014306
File ID: A0908003.D
Sok Amt Cone %Rec Fla
20 15.4 77
20 18.2 91
20 19.2 96
20 22.4 112
20 16.5 82
20 18.I 90
20. 12.5 63
20 20.6 103
20 19.0 95
20 20.0 100
20 18.5 93
20 15.0 75
20 14.4 72
20 20.5 102
20 16.4 82
20 19.7 98
20 11.5 57
20 19.5 97
20 19.0 95
20 19.1 95
20 18.1 ·· 90
20 19.9 100
20 17.7 89
20 18.2 91
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STLAustin
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
JEC Analyst:
Control s a mole D r uo 1cate
1014307
A0908004.D
Cone %Rec Fla
15.0 75
18.4 92
19.0 95
22.7 113
16.6 83
17.6 88
12.9 65
18.2 91
18.6 93
19.7 99
18.2 91
15.9 79
14.5 73
20.2 IOI
16.9 84
19.9 99
11.9 60
19.0 95
18.9 94
18.7 93
18.2 91
19.3 97"
17.9 89
18.I 91
QC Limits
RPO Fla %Rec RPO
2.6 0.1-240 71
I. I 71-133 17
I 67-127 12
0.9 61-145 21
1.2 57-135 19
2.2 23-151 17
3.1 34-128 25
12 0.1-214 39
2.1 28-184 30
1 45-160 31
2.2 65-148 27
5.2 29-223 23
1.4 46-150 23
I 77-129 14
2.4 39-133 27
1 64-146 16
5.1 18-140 26
2.1 70-136 24
I. I 74-132 23
2.1 39-171 25
I.I 45-137 15
3 19-187 19
0 52-138 21
0 70-132 13
Page 43 of 55
-~------~---~~--~--
mm.-' - - - - - -.. ) .. · -....... -----..
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
. Lab ID:
c ontrol s amole contmue
1014306 l File ID: A0908003.D
Parameter Sok Amt Cone
I 2-Dichlorobenzene I 20. 19.0.
1 3-Dichlorobenzene I 20 18.2
Dichloroditluoromethane ' 20 9.54
I 1-Dichloroethane I 20 18.4
I 2-Dichloroethane I 20 17.8
I 1-Dichloroethene 20 16.1
cis-I .2-Dichloroethene 20 20.9
trans-I 2-Dichloroethene 20 18.7
1 2-Dichloroorooane 20 18.6
1.3-Dichloroorooane 20 15.3
2 2-Dichloropropane 20 20.6
I 1-Dichloroorooene 20 17.3
cis-I .3-Dichloroorooene 20 16.4
trans-I 3-Dichloroorooene 20 15.6
Ethvlbenzene 20 20.4
Hexachloro-1 3-butadiene 20 26.4
2-Hexanone 20 17.8
lodomethane 20 15.2
lsoproovlbenzene 20 20.7
4-lsooroovltoluene 20 18.9
4-Methvl-2-oentanone (MIBK) 20 17.9
Methylene chloride 20 17.7
Naphthalene 20 26.4
n-Proovlbenzene 20 20.4
Styrene 20 21.2
I. I. I 2-Tetrachloroethane 20 19.7
I, 1,2 2-Tetrachloroethane 20 20.4
Tetrachloroethene 20 22.4
Toluene 20 19.5
I 2,3-Trichlorobenzene 20 33.8
I 2 4-Trichlorobenzene 20 27.5
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workordcr: 756200.UA-Little Washington, N (20009024] llamilton Beach-Proctor Silex
STLAustin
%Rec Fla
95
91
48
92
89
80
105
93
93
76
103
86
82
78
102
132
89
76
103
94
90
89
132
102
106
99
102
I 12
97
169 0
137
d
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Control s amoe uo 1cate con mue I D r r d
1014307
A0908004.D QC Limits
Cone %Rec Fla RPO Fig %Rec RPO
18.7 94 I. I 67-135 14
18.0 90 I. I 68-134 14
9.79 49 2.1 0.1-166 26
18.4 92 0 66-138 19
18.0 90 I. I 48-152 23
16.5 82 2.5 47-175 25
21.8 109 3.7 66-.144 18
19.1 96 3.2 62-146 22
18.2 91 2.2 .,_ 61-133 17
18.3 91 18 0 70-128 16
20.7 103 0 40-168 30
17.2 86 0 71-155 31
17.1 86 4.8 36-142 16
15.9 79 1.3 34-138 21
20.9 104 1.9 75-131 14
25.7 128 3.1 46-150 34
18.0 90 I. I 22-164 34
16.1 81 6.4 "
20.3 IOI 2 54-152 26
18.7 93 I. I 41-165 28
18.1 91 I. I 27-149 36
17.9 90 I. I 36-166 23
26.5 132 0 32-172 22
19.8 99 3 61-143 28
20.6 103 2.9 68-136 14
19.4 97 2 63-141 20
19.9 100 2 47-143 20
21.0 105 6.5 69-137 16
19.4 97 0 70-132 17
33.9 170 0 0.6 66-140 20
27.8 139 1:4 66-144 22
Page 44 of 55
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Lab ID:
c ontro IS amp e contmue
1014306
File ID: A0908003.D
Parameter Sok Amt Cone
I I. I-Trichloroethane 20 19.9
I I 2-Trichloroethane 20 19.4
Trichloroethene : 20 20.8 -Trichlorofluoromethane 20 17.3
I 2 3-Trichloropropane I 20 18.8
I 2 4-Trimethvlbenzene I 20 18.2
1.3 5-Trimethylbenzene I 20 18.7
Vinvl acetate : 20 16.4
Vinyl chloride 20 14.7
o-Xvlene/m-Xvlene 40 41.6
o-Xvlene 20 20.6
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workordcr: 756200.UA-Liule Washington, N [20009024] llamilton Beach-Proctor Silex
STL Austin
%Rec Fla
100
97
104
86
94
91
93
82
74
104
103
d
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
40
20
c ontro IS ampe up 1cate contmue I D r d
1014307
A0908004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
19.9 99 I 49-155 24
19.4 97 0 67-135 17
20.8 104 0 71-129 17
18.1 90 4.5 39-147 29
18.7 93 I. I 64-140 18
17.7 88 3.4 54-156 25
18.1 90 3.3 62-144 25
15.1 75 8.9 0.1-164 31
14.9 75 1.3 24-138 27
40.5 101 2.9 76-134 15
20.3 102 1 77-131 15
Page 45 of 55
~-------~--~~~-----
~--------~--~~~-~-~
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Surroaate Comoounds
l-Bromo-4-fluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
'
SECTION V -Calibration and QC Information -09/18/2000 19:53
Lab ID: 1014306
%Recoverv
99
98
92
l.IMS Workorder: 756200.UA-Linle Washington, N (20009024] Hamilton Beach-Proctor Silex
STL Austin
Lab ID: 1014307
Fla as %Recoverv Flags QC Recoverv Limits
98 77-117
100 61-143
94 87-113
Page 46 of 55
SECTION V
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
Parameter
Acetone
Benzene
Bromobenzene
Bromoch loromethane
LCS for HBN 8043 [MSV/1314]
8043
8043
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
Ch lorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloroorooane
Dibromochloromethane
I 2-Dibromoethane
Dibromomethane
1.4-Dichlorobenzene
SECTION V -Calibration and QC Information -09/18/2000 19:53
Instrument ID: MSDB
Units: ug/L
Matrix: Aqueous
Control Samole
Lab ID: 1014395
File ID: 80911003.D
Sok Amt Cone %Rec Fla
20 22.2 111
20 19.3 96
20 20.5 103
20 18.9 94
20 20.3 101
20 19.0 95
20 16.7 83
20 19.7 98
20 21.9 109
20 23.0 115
20 21.0 105
20 31.0 155
20 18.8 94
20 19.7 99
20 17.7 89
20 20.6 103
20 16.5 83
20 21.4 107
20 21.6 108
20 19.2 96
20 20.4 102
20 19.8 99
20 19.5 97
20 20.3 IOI
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
JEC Analyst:
Control Sample Duolicate
1014396
80911004.D
Cone %Rec Fin
. 21.2 106
18.8 94
19.9 100
18.I 91
19.7 98
18.1 91
16.0 80
17.5 88
20.9 104
21.8 109
20.8 104
30.5 153
17.9 90
19.1 95
17.1 85
19.5 98
15.8 79
20.9 104
21.4 107
18.4 92
19.6 98
19.1 96
18.9 95
19.6 98
QC Limits
RPO Fin %Rec RPO
4.6 0.1-240 71
2.1 71-133 17
3 67-127 12
3.2 61-145 21
3 57-135 19
4.3 23-151 17
3.7 34-128 25
11 0.1-214 39
4.7 28-184 30
5.4 45-160 31
I 65-148 27
1.3 29-223 23
4.3 46-150 23
4.1 77-129 14
4.6 39-133 27
5 64-146 16
4.9 18-140 26
2.8 70-136 24
0.9 74-132 23
4.3 39-171 25
4 . 45-137 15
3.1 19-187 19
2.1 52-138 21
3 70-132 13
Page 47 or 55
--------~----~--~-~
_____________ ! _______ _
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
! LablO:
c ontrol s amnle continued
1014395
File ID: 80911003.D
Parameter Sok Amt Cone
1.2-Dichlorobenzene 20 20.4
I 3-Dichlorobenzene 20 20.3
Dichlorodifluoromethane 20 16.1
I 1-Dichloroethane 20 20.3
1,2-Dichloroethane 20 20.6
l 1-Dichloroethene 20 20.2
cis-1,2-Dichloroethene 20 20.3
trans-1.2-Dichloroethene 20 19.0
I 2-Dichloroorooane 20 20.2
1,3-Dichloropropane 20 20.0
2.2-Dichloroorooane 20 21.5
I, 1-Dichloroprooene 20 19.9
cis-1 3-Dichloroorooene 20 19.5
trans-1.3-Dichloroorooene 20 19.9
Ethylbenzene 20 20.3
Hexachloro-1 3-butadiene 20 17.7
2-Hexanone 20 18.7
lodomethane 20 16.9
lsooroovlbenzene 20 20.4
4-lsooroovltoluene 20 21.5
4-Methvl-2-pentanone (MIBK) 20 20.7
Methvlene chloride . 20 19.8
Naphthalene 20 18.3
n-Proovlbenzene 20 22.6
Styrene 20 20.6
I 1.1.2-Tetrachloroethane 20 19.7
I I 2,2-Tetrachloroethane 20 20.4
Tetrachloroethene 20 19.7
Toluene 20 20.8
1,2 3-Trichlorobenzene 20 17.8
1.2.4-Trichlorobenzene 20 18.8
SECTION V -Calibration and QC Information -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
%Rec Fla
102
102
80
102
103
101
102
95
IOI
100
108
JOO
97
100
101
89
94
85
102
108
104
99
92
113
103
99
102
99
104
89
94
LablO:
FilelO:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Control s a mole D r uo 1cate contmue d
1014396
80911004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
19.6 98 4 67-135 14
19.8 99 3 68-134 14
15.0 75 6.5 0.1-166 26
19.5 97 5 66-138 19
20.0 100 3 48-152 23
19.3 97 4 47-175 25
19.4 97 5 66-144 18
18.2 91 4.3 --... 62-146 22
19.7 99 2 --· 61-133 17
19.3 96 4.1 -~ 70-128 16
19.4 97 11 40-168 30
18.7 93 7.3 71-155 31
18.9 94 3.1 36-142 16
19.3 96 4.1 34-138 21
19.6 98 3 75_·131 14
16.9 85 4.6 46-150 34
17.9 90 4.3 --22-164 34
16.7 83 2.4 ,,....
19.4 97 5 54-152 26
20.5 103 4.7 41-165 28
19.5 97 7 27-149 36
19.0 95 4.1 36-166 23
18.0 90 2.2 32-172 22
21.9 110 2.7 61-143 28
19.7 99 4 68-136 14
19.4 97 2 63-141 20
19.7 98 4 47-143 20
18.7 93 6.3 69-137 16
19.9 100 3.9 70-132 17
17.5 88 1.1 66-140 20
18.8 94 0 66-144 22
Page 48 of 55
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Control Samole continued
Lab ID: 1014395
File ID: 80911003.D
Parameter Sok Amt Cone
I. I I-Trichloroethane 20 19.9
I, I 2-Trichloroethane 20 19.6
Tri ch loroethene 20 19.0
Trich lorofluoromethane i 20 23.0
I 2,3-Trichloroorooane 20 19.5
I 2 4-Trimethvlbenzene 20 21.8
I 3.5-Trimethvlbenzene ' 20 22.8
Vinyl acetate 20 20.6
Vinvl chloride 20 16.9
o-X ylene/m-X vlene 40 42.1
o-Xvlene 20 20.3
SECTION V -Calibration and QC Information -0911812000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
%Rec Fla
99
98
95
115
97
109
114
103
84
105
102
Control Sample Duolicate continued
Lab ID: 1014396
File ID: 80911004.D
Sok Amt Cone %Rec Fig RPO Fla
20 18.3 92 7.3
20 19.4 97 I
20 18.2 91 4.3
20 21.5 108 6.3
20 19.0 95 2.1
20 21.5 107 1.9
20 21.6 108 5.4
20 20.1 100 3
20 16.0 80 4.9
40 39.4 99 5.9
20 19.1 96 6.1
--.. -·----------·---1
QC Limits
%Rec RPO
49-155 24
67-135 17
71-129 17
39-147 29
64-140 18
54-156 25
62-144 25
0.1-164 31
24-138 27
76-134 15
77-131 15
Page 49 or 55
-· - -
-------~-----------SECTION V
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Surrogate Compounds
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
'
I i
!
!
' I
SECTION V -Calibration and QC Information -09118(2000 19:53
Lab ID: 1014395
o/oRecoverv
97
104
99
I.IMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Lab ID: 1014396
Flags %Recoverv Fla as QC Recoverv Limits
99 77-117
IOI 61-143
IOI 87-113
Page 50 of 55
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 8021
Client Sample ID
INSTRUMENT OC
INSTRUMENT QC
LCS for HBN 8021 fMSV/I 3131
LCSDforHBN 8021 fMSV/13131
MBforHBN8021 fMSV/13131
0900HBWW226
0900HBWW226
0900HBWW226 zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz
0900HBWW224
0900HBWW225
0900HBWD998
0900HBWW234
0900HBWW220
0900HBWW216
0900HBWW222
0900HBWW230
TRIP BLANK 1 zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz
SECTION VI -Batch Summaries -09/18/2000 19:53
!
Lab Sample ID
1000
1406
1014306
1014307
1014308
2000902401
1014309
1014310
2000903801
2000903802
2000903803
2000902402
2000902403
2000902404
2000902405
2000902406
2000902407
2000902408
2000902409
2000902410
2000903507
2000903503
2000903505
2000903501
2000903502
2000903504
2000903506
Start Date/Time: 09/08/2000 14:09
Stop Date/Time: 09/09/2000 0 I :54
SamPleTvoe Matrix
GC/MS Tune Aaueous
Continuing Calibration Check Aqueous
Lab Control Sample Aaueous
Lab Control Sample Duplicate Aqueous
Method Blank Aqueous
Field Sample Aaueous
Matrix Spike Aqueous
Matrix Spike Duplicate Aaueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aqueous
Field Sample Aaueous
Field Samole Aqueous
Field Sample Aaueous
Field Samole Aaueous
LIMS Workorder: 756200.UA-Little Washington, N [20009024) Hamilton Beach-Proctor Silex
STLAustin
Analyst: JEC
Sample Size
Initial Final Preparation Method
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15mL 15 mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
Page 51 or 55
-------------------
---------.. -------... --SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW82608
Extraction Batch ID: 8043
Client Samole ID
INSTRUMENT QC
INSTRUMENT QC
LCS for HBN 8043rMSV/13141
LCSD for HBN 8043 fMSV/13141
MB for HBN 8043 rMSV/13141
TRIP BLANK I zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz
SECTION VI -Batch Summaries -09/18/2000 19:53
l
Lab Samole ID
1000
1406
1014395
1014396
1014397
2000902410
2000905302
2000905301
1014398
1014399
2000902910
Start Date/Time:
Stop Date/Time:
09/1112000 14:07
0911112000 18:12
SamoleTvoe Matrix
GC/MS Tune Aaueous
Continuin!! Calibration Check Aaueous
Lab Control Samnle Aaueous
Lab Control Samole Duolicate Aaueous
Method Blank Aaueous
Field Samole Aaueous
Field Samole Aaueous
Field Samole Aaueous
Matrix Soike Aaueous
Matrix Soike Duolicate Aaueous
Field Samole Aaueous
LIMS Workorder: 756200.UA-Littlc Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Analyst: JEC
Sample Size
Initial Final Preoaration Method
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
Page 52 or 55
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 8021 Instrument ID: MSDA
Seauence Client Sample ID Lab Sample ID
1 INSTRUMENT OC 1000
2 INSTRUMENT QC 1406
3 LCS for HBN 8021 fMSV/13131 1014306
4 LCSD for HBN 8021 rMSV/13131 1014307
5 MB for HBN 8021 fMSV/13131 1014308
6 0900HBWW226 2000902401
7 0900HBWW226 1014309
8 0900HBWW226 1014310
9 zzzzzzzzzz 2000903801
10 zzzzzzzzzz 2000903802
11 zzzzzzzzzz 2000903803
12 0900HBWW224 2000902402
13 0900HBWW225 2000902403
14 0900HBWD998 2000902404
15 0900HBWW234 2000902405
16 0900HBWW220 2000902406
17 0900HBWW216 2000902407
18 0900HBWW222 2000902408
19 0900HBWW230 2000902409
20 TRIP BLANK 1 2000902410
21 zzzzzzzzzz 2000903507
22 zzzzzzzzzz 2000903503
23 zzzzzzzzzz 2000903505
24 zzzzzzzzzz 2000903501
25 zzzzzzzzzz 2000903502
26 zzzzzzzzzz 2000903504
27 zzzzzzzzzz 2000903506
SECTION VI -Batch Summaries -09/18/2000 19:53
LIMS Workorder: 756200.UA-Littlc Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Analysis
Date Time
09/08/2000 14:09:00
09/08/2000 14:09:00
09/08/2000 14:37:00
09/08/2000 15:05:00
09/08/2000 15:33:00
09/08/2000 16:01:00
09/08/2000 16:29:00
09/08/2000 16:57:00
09/08/2000 17:25:00
09/08/2000 17:53:00
09/08/2000 18:21:00
09/08/2000 18:49:00
09/08/2000 19:17:00
09/08/2000 19:45:00
09/08/2000 20:13:00
09/08/2000 20:41:00
09/08/2000 21:09:00
09/08/2000 21:37:00
09/08/2000 22:05:00
09/08/2000 22:33:00
09/08/2000 23:01:00
09/08/2000 23:29:00
09/08/2000 23:57:00
09/09/2000 00:26:00
0910912000 00:54:00
09/09/2000 01:24:00
09/09/2000 01 :54:00
Analyst: JEC
SampleTvpe Analysis File ID Sub-Batch ID
GC/MS Tune A0908002.D 0
Continuing Calibration Check A0908002.D 0
Lab Control Sample A0908003.D 0
Lab Control Sample Duolicate A0908004.D 0
Method Blank A0908005.D 0
Field Sample A0908006.D 0
Matrix Spike A0908007.D 0
Matrix Spike Duolicate A0908008.D 0
Field Sample A0908009.D 0
Field Sample A0908010.D 0
Field Samole A090801 l.D 0
Field Samole A0908012.D 0
Field Sample A0908013.D o-
Field Samole A0908014.D 0
Field Sample A0908015.D 0
Field Sample A0908016.D 0
Field Sample A0908017.D 0
Field Sample A0908018.D 0
Field Sample A0908019.D 0
Field Sample A0908020.D 0
Field Samole A0908021.D 0
Field Sample A0908022.D 0
Field Sample A0908023.D 0
Field Sample A0908024.D 0
Field Samole A0908025.D 0
Field Sample A0908026.D 0
Field Sample A0908027.D 0
Page 53 of 55
-------------------
-------------------SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 8043 Instrument ID: MSDB
!
Seauence Client Sample ID ' Lab Sample ID
I INSTRUMENT OC 1000
2 INSTRUMENT QC i 1406
3 LCS for HBN 8043 rMSV/13141: 1014395
4 LCSD for HBN 8043 fMSV/13141 1014396
5 MB for HBN 8043 fMSV/13141 ! 1014397
6 TRIP BLANK 1 2000902410
7 zzzzzzzzzz 2000905302
8 zzzzzzzzzz 2000905301
9 zzzzzzzzzz 1014398
10 zzzzzzzzzz 1014399
11 zzzzzzzzzz 2000902910
SECTION VI -Batch Summaries -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-Proctor Silex
STL Austin
Analysis
Date Time
09111/2000 14:07:00
09/11/2000 14:07:00
09111/2000 14:34:00
09111/2000 15:01:00
09/1112000 15:28:00
0911112000 15:55:00
0911112000 16:22:00
0911112000 16:49:00
0911112000 17:16:00
0911112000 17:44:00
09/1112000 18:12:00
Analyst: JEC
SamoleTvoe Analysis File ID Sub-Batch ID
GC/MS Tune B09I 1002.D 0
Continuing Calibration Check B0911002.D 0
Lab Control Sample B0911003.D 0
Lab Control Sample Duplicate B0911004.D 0
Method Blank B09I 1005.D 0
Field Sample B0911006.D 0
Field Samole B0911007.D .. 0 ..
Field Sample B0911008.D .. 0
Matrix Soike B0911009.D 0
Matrix Spike Duolicate B091 IOIO.D 0
Field Samole B091IOI1.D 0
Page 54 of 55
SECTION VII
Certifications
State/Aaencv
Arkansas Deoartment of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program I Waste Water/Hazardous Waste
Kansas Deoartment of Health and Environment I Solid and Hazardous Waste/Drinking Water
ID#
2257
E-10165
Louisiana Department of Environmental Quality, ELAP I Waste Water/Hazardous Waste/ Air/Emissions
New Jersev Deoartment of Environmental Protection
New York State Department of Health I Waste Water/Hazardous Waste
North Carolina Deot. of Natural Resources & Community Development I Waste Water
Oklahoma Water Resources Board I Waste Water
South Carolina Dept. of Health & Environmental Control
Utah Department of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources
US Air Force/AFCEE
US Army Corps of Engineers (ACE)
US Deoartment of Agriculture I Restricted Soils Permit
SECTION VII -Certifications -09/18/2000 19:53
LIMS Workorder: 756200.UA-Little Washington, N [20009024] Hamilton Beach-rroctor Silex
STLAustin
-< - ---- -- - -
82005
10915
302
8720
82003002
RADC
999885260
Participating Laboratory
S-42350
--< -- - -
Page 55 of 55
-- -
- - - - - - - - - - - - - - - - -·--SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -Labor9tory Analytical Report
Table of Contents
Report Surrrnaries . . . .
Workorder Surrmary
Protocol Surrmary
Corrments and Flag Oefinitions
Standard.Flag Definitions
Analyst Corrments . . . .
Sample Condition Corrments
Analytical Results .' . . . . . . . .
SW8260B . . . . . . . . . . . . .
Calibration and Quality Control Results
SW8260B .......... .
Batch Surrmaries .
SW8260B
Certifications .
Calibration Verification Results
Mass Spectrometer Tune
Method Blank Results
Control Sample Results
Extraction/D~gestion Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -09/I 8/2000 19:58
LIMS Workorder: 756200.UA-Little Washington, N (20009035) Hamilton Beach-Proctor Silex
STL Austin
·-.
Page
i
1
1
1
1
3
. . . 3
. . 3
3
. 4 .
4
19
19
19
23
24
28
32
32
32
33
34
SECTION II
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex Project Name: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
Client Code: HB-PS Facility Name: NC
Workorder Summary
Lab:
Client Samole ID samolelD Samole Matrix
0900HBWW213 2000903501 Aaueous
0900HBWW214 2000903502 Aaueous
0900HBWW215 2000903503 Aaueous
0900HBWW227 2000903504 Aaueous
0900HBWW228 2000903505 Aaueous
0900HBWD999 2000903506 Aaueous
TRIP BLANK2 2000903507 AaueQus
Protocol Summary
Lab Date&Time
Client Sample ID Samole ID Collected
Method· SW8260B
0900HBWW213 2000903501 09/07/00 09:00
0900HBWW214 2000903502 09/07/00 09:20
0900HBWW215 2000903503 09/07/00 09:35
0900HBWW227 2000903504 09/07/00 09:55
0900HBWW228 2000903505 09/07 /00 10: I 0
0900HBWD999 2000903506 09/07 /00 I 0:00
SECTION II· Report Summaries -09/18/2000 19:58
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
Method Citation
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Date& Time Prep
Received Batch ID
09/08/00 I 0:53 8021
09/08/00 10:53 8021
09/08/00 I 0:53 8021
09/08/00 10:53 8021
09/08/00 I 0:53 8021
09/08/00 I 0:53 8021
Method Description
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles by GC/MS
Volatiles bv GC/MS
Volatiles by GC/MS
Volatiles by GC/MS
Hold Time S >ec
Date& Time Analysis Date& Time Prep Analvsis
Pre oared Batch ID Analvzed Soec Actua Soec Actua
09/09/00 00:26 8021 09/09/00 00:26 7D 2D 7D 20
09/09/00 00:54 8021 09/09/00 00:54 7D 2D 7D 2D
09/08/00 23 :29 8021 09/08/00 23:29 7D ID 7D ID
09/09/00 0 I :24 8021 09/09/00 01 :24 7D 2D 7D 2D
09/08/00 23:57 8021 09/08/00 23:57 7D JD 7D ID
09/09/00 0 I :54 8021 09109100 0 I :54 7D 2D 7D 2D
Page I of 34
-------------------
-------------------SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
!
Labj Date& Time Date& Time Prep
Client Samole ID Sample ID Collected Received Batch ID
I
Method: SW8260B continued -I TRIP BLANK 2 I 2000903507 I 09/07100 08:55 I 09/08/00 I 0:53 I 8021
SECTION II -Report Summaries -09/18/2000 19:58
LIMS Workorder: 756200.UA-Littlc Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
Hold Time S11>ec
Date& Time Analysis Date& Time Preo Analvsis
Prepared Batch ID Analvzed Snee Actua Soec Actua
I 09/08/00 23 :0 I I 8021 I 09/08/00 23:0 I I 70 ID I 70 ID
Page 2 of 34
SECTION Ill
Comments and Flag Definitions
MS-VOA
Standard Data Qualifiers
Flaa Definition i
B Analvte detected in method blank and concentration > MDL
J Result> or= MDL and <POL '
NA Not analvzed/Not available I
ND Not detected at the soecified reoortin1:1 Ilmit
0 Result does not meet tolerance in Protoool Specification
u Result less than samole soecific method1detection limit
Analyst Comments
Affected Sam le Method
TRIPBLANK2 SW8260B
Sample Condition Comments
[Affected Sample Comment
SECTION 111-Comments and Flag Definitions -09/18/2000 19:58
LIMS Workordcr: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
- - ------
Comment
See CER # 1780 & 1782.
Page 3 of 34
- - - --- - --- -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-·1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor I ·
Instrument !
Units
CAS I
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
I 08-86.:1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3 .. 544-10-5
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Aqueous
Received
NA
09/07/2000 10:00
09/09/2000 0 I :54
09/09/2000 0 I :54
50.0000
MSDA
ug/L
Cone Flaa DL
ND 14.3
ND 83.5
ND 49.2
ND 4.50
ND 2.46
ND 3.1 I
ND 6.95
ND 3.42
ND 6.80
ND 5.30
ND 8.95
ND 3.21
ND 3.72
ND 4.79
ND 2.42
ND 4.34
ND 4.20
ND 2.36
23.0 J 3.78
ND 3.35
ND 5.65
· LIMS'Workordcr: 756200.UA-Littlc Washington, N [20009035] J-/amilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Aaueous Aqueous
Received Received
NA NA
09/07/2000 09:00 09/07/2000 09:20
09/09/2000 00:26 09/09/2000 00:54
09/09/2000 00:26 09/09/2000 00:54
10.0000 2.0000
MSDA MSDA
U2:/L U2:/L
Cone Flag DL RL Cone Flaa DL RL
ND 2.86 0.000 ND 0.572 0.000
ND 16.7 0.000 ND 3.34 0.000
ND 9.83 0.000 ND 1.97 0.000
ND 0.901 0.000 ND 0.180 0.000
ND 0.492 0.000 0.280 J 0.0984 0.000
ND 0.622 0.000 ND 0.124 0.000
ND 1.39 0.000 ND 0.278 0.000
ND 0.683 0.000 ND -· 0.137 0.000
ND 1.36 0.000 ND 0.272 0.000
ND 1.06 0.000 ND 0.212 0.000
ND 1.79 0.000 ND 0.358 0.000
ND 0.642 0.000 ND 0. 128 0.000
ND 0.745 0.000 ND 0.149 0.000
ND 0.958 0.000 ND 0.192 0.000
ND 0.484. 0.000 ND 0.0968 0.000
ND 0.867 0.000 ND 0. 173 0.000
ND 0.839 0.000 ND 0.168 0.000 -ND 0.473 0.000 ND 0.0946 0.000
ND 0.756 0.000 0.649 J 0.151 0.000
ND 0.670 0.000 ND 0.134 0.000
ND 1.13 0.000 ND 0.226 0.000
Page 4 of 34
SECTION IV
Analytical .Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Chloromethane 74-87-3
3-Chloropropene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
1 2-Dibromo-3-chloroprooane 96-12-8
Dibromochloromethane 124-48-1
l 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I, 1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
I 3-Dichloroprooane 142-28-9
2 2-Dichloroprooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1 3-Dichloropropene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
' Cone Flaa DL
ND 4.10
ND 5.55
ND 5.65
ND 3.81
ND 52.5
ND 2.82
ND 7.60
ND 4.70
ND 19.5
ND 2.94
ND 4.60
ND 2.96
ND 5.65
1370 2.44
ND 2.50
238 3.48
205 3.02
ND 4.06
ND 3.35
ND 2.26
ND 3.57
ND 2.32
ND 1.83
ND 3.29
ND 3.24
ND 2.76
ND B 10.6
ND 8.35
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Cone Flag DL RL Cone Flaa DL RL
ND 0.821 0.000 ND 0.164 0.000
ND 1.11 0.000 ND 0.222 0.000
ND 1.13 0.000 ND 0.226 0.000
ND 0.762 0.000 ND 0.152 0.000
ND 10.5 0.000 ND 2.10 0.000
ND 0.564 0.000 ND 0.113 0.000
ND 1.52 0.000 ND 0.304 0.000
ND 0.939 0.000 ND 0.188 0.000
ND 3.90 0.000 ND 0.780 0.000
ND 0.587 0.000 ND 0.117 0.000
ND 0.920 . 0.000 ND 0.184 0.000
ND 0.591 0.000 ND 0.118 -0.000
ND 1.13 0.000 ND 0.226 0.000
156 0.487 0.000 159 0.0974 0.000
4.05 J 0.499 0.000 0.576 J 0.0998 0.000
391 0.697 0.000 13.7 0.139 0.000
45.I 0.603 0.000 11.6 0.121 0.000
1.33 J 0.813 0.000 0.683 J 0.163 0.000
ND 0.670 0.000 ND 0.134 0.000
ND 0.451 0.000 ND 0.0902 0.000
ND 0.714 0.000 ND 0.143 0.000
ND 0.464 0.000 ND 0.0928 0.000
ND 0.366 0.000 ND 0.0732 0.000
ND 0.658 0.000 ND 0.132 0.000
ND 0.647 0.000 ND 0.129 0.000
0.292 u 0.552 0.000 ND 0.110 0.000
ND B 2.12 0.000 ND B 0.424 0.000
ND 1.67 0.000 ND 0.334 0.000
Page 5 of 34
-------------------
-------------·------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID .
Lab Sample ID
Continued
Parameter CAS I
lodomethane 74-88-4 I
Isoproovlbenzene 98-82-8 !
4-lsopropyltoluene 99-87-6 I
Methvl methacrvlate 80-62-6 ' l
' Methyl tert-butyl ether (MTBE) 1634-04-4 •
4-Methvl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanen itrile 107-12-0
n-Propylbenzene 103-65-1
Styrene 100-42-5
I, 1 I 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1,2,4-Trichlorobenzene 120-82-1
1 I. I -Trichloroethane 71-55-6
I 1.2-Trich loroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1,2,3-Trichloroorooane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
1,2,4-Trimethvlbenzene 95-63-6
I 3,5-Trimethylbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Cone Flag DL
ND 3.08
ND 2.37
ND 2.26
ND 5.70
ND 2.34
ND 4.22
ND B 3.98
ND 5.30
ND 34.4
ND 4.43
ND 3.61
ND 4.74
ND 3.96
ND 2.84
ND 20.1
8.65 J 3.40
ND B 23.4
ND B 5.90
1160 1.66
ND 4.76
35.5 4.52
ND 10.4
ND 2.72
ND 3.83
ND 3.74
ND 2.18
ND 2.19
ND 2.87
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.00(:)
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Cone Flaa DL RL Cone Flaa DL RL
ND 0.616 0.000 ND 0.123 0.000
ND 0.474 0.000 ND 0.0948 0.000
ND 0.452 0.000 ND 0.0904 0.000
ND 1.14 0.000 ND 0.228 0.000
ND 0.469 0.000 ND 0.0938 0.000
ND 0.845 0.000 ND . 0.169 0.000
ND B 0.796 0.000 ND B ... 0.159 0.000
ND 1.06 0.000 ND 0.212 0.000
ND 6.88 0.000 ND 1.38 0.000
ND 0.886 0.000 ND 0.177 0.000
ND 0.722 0.000 ND 0.144 0.000
ND 0.948 0.000 ND 0.190 0.000
ND 0.792 0.000 ND 0.158 0.000
33.I 0.568 0.000 ND 0.114 0.000
ND 4.02 0.000 ND . ~ 0.804 0.000 -ND 0.680 0.000 ND 0.136 0.000
ND B 4.67 0.000 ND B 0.934 0.000
ND B 1.18 0.000 ND B 0.236 0.000
ND 0.331 0.000 ND 0.0662 0.000
2.23 J 0.952 0.000 ND 0.190 0.000
510 0.905 0.000 0.489 J 0.181 0.000
ND 2.08 0.000 ND 0.416 0.000
ND 0.543 0.000 ND 0.109 0.000
ND 0.766 0.000 ND 0.153 0.000
ND 0.749 0.000 ND 0.150 0.000
ND 0.436 0.000 ND 0.0872 0.000
ND 0.438 0.000 ND 0.0876 0.000
17.8 0.574 0.000 9.35 0.115 0.000
Page 6 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-X ylene/m-X vlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
i Cone Flaa DL
ND 6.85
ND 3.56
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0900HBWW213 0900HBWW214
2000903501 2000903502
Cone Flaa DL RL Cone Flag DL RL
ND 1.37 0.000 ND 0.274 0.000
1.66 J 0.713 0.000 ND 0.143 0.000
Page 7 of 34
--- - - - - - - - - - - --· - - - - -
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepar~d
Date/Time Analyz~d
Dilution Factor !
Instrument
Units
Surrogate Compound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWD999
2000903506
Aaueous
Received
NA
09/07/2000 10:00
0910912000 01 :54
. 0910912000 01 :54
50.0000
MSDA
U!!/L
% Recoverv Limits
99 77-117
102 61-143
93 87-113
LIMS Workordcr: 756200.UA-Littlc Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
F
0900HBWW213 0900HBWW214
2000903501 2000903502
Aaueous Aqueous
Received Received
NA NA
09/07/2000 09:00 09/07/2000 09:20
09/09/2000 00:26 0910912000 00:54
09/09/2000 00:26 09/09/2000 00:54
10.0000 2.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recovery Limits F
96 77-117 98 77-117
99 61-143 100 61-143
94 87-113 93 87-113
Page 8 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butylbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Dateffime Collected
Dateffime Prepar~d
Dateffime Analyz,d
Dilution Factor ' ·
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25:-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
" 544-10-5
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWW215
2000903503
Aaueous
Received
NA
09/07/2000 09:35
09/08/2000 23:29
09/08/2000 23 :29
1.0000
MSDA
ue:/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745 .
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW227 0900HBWW228
2000903504 2000903505
Aaueous Aaueous
Received Received
NA NA
09/07/2000 09:55 09/07/2000 10: 10
09/09/2000 01 :24 09/08/2000 23:57
09/09/2000 01 :24 09/08/2000 23:57
. 50.0000 2000.0000
MSDA MSDA
Ull/L ug/L
Cone Flaa DL RL Cone Flaa DL RL
ND 14.3 0.000 ND 572 0.000
ND 83.5 0.000 ND 3340 0.000
ND 49.2 0.000 ND 1970 0.000
ND 4.50 0.000 ND 180 0.000
ND 2.46 0.000 ND 98.4 0.000
ND 3.11 0.000 ND 124 0.000
ND 6.95 0.000 ND 278 0.000
ND 3.42 0.000 ND 137 0.000
ND 6.80 0.000 ND 272 0.000
ND 5.30 0.000 ND 212 0.000
ND 8.95 0.000 ND 358 0.000
ND 3.21 0.000 ND 128 0.000
ND 3.72 0.000 ND 149 0.000
ND 4.79 0.000 ND 192 0.000
ND 2.42 0.000 ND 96.8 0.000
ND 4.34 0.000 ND 173 0.000
ND 4.20 0.000 ND 168 0.000
ND 2.36 0.000 ND 94.6 0.000
26.3 3.78 0.000 ND 151 0.000
ND 3.35 0.000 ND 134 0.000
ND 5.65 0.000 ND 226 0.000
Page 9 of 34
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Ch loromethane
3-Ch loroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID ,
Lab Sample ID ·
CAS l
74-87-3 I
I 07-05-1 I
95-49-8 I
106-43-4 I !
I 2-Dibromo-3-chloroorooane 96-12-8 l
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane . 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1,3-Dichloroorooane 142-28-9
2.2-Dich loroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene I 0061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/IS/2000 I9:58
0900HBWW215
2000903503
Cone Flan DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
3.16 0.0487
ND 0.0499
1.75 0.0697
0.0496 u 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND B 0.212
ND 0.167
LIMS Workorder: 756200.UA-Littie Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
0900HBWW227 0900HBWW228
2000903504 2000903505
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 4.10 0.000 ND 164 0.000
0.000 ND 5.55 0.000 ND 222 0.000
0.000 ND 5.65 0.000 ND 226 0.000
0.000 ND 3.81 0.000 ND 152 0.000
0.000 ND 52.5 0.000 ND 2100 0.000 ..
0.000 ND 2.82 0.000 ND 113 0.000
0.000 ND 7.60 0.000 ND 304 0.000
0.000 ND 4.70 0.000 ND 188 0.000
0.000 ND 19.5 0.000 ND 780 0.000
0.000 ND 2.94 0.000 ND 117 0.000
0.000 ND 4.60 0.000 ND 184 0.000
0.000 ND 2.96 0.000 ND 118 0.000
0.000 ND 5.65 0.000 ND 226 0.000
0.000 1340 2.44 0.000 11900 .. 97.4 0.000
0.000 ND 2.50 0.000 ND 99.8 0.000
0.000 249 3.48 0.000 31200 139 0.000
0.000 211 3.02 0.000 2380 121 0.000
0.000 ND 4.06 0.000 ND 163 0.000
0.000 ND 3.35 0.000 ND 134 0.000
0.000 ND 2.26 0.000 ND 90.2 0.000
0.000 ND 3.57 0.000 ND 143 0.000
0.000 ND 2.32 0.000 ND 92.8 0.000
0.000 ND 1.83 0.000 ND 73.2 0.000
0.000 ND 3.29 0.000 ND 132 0.000
0.000 ND 3.24 0.000 ND 129 0.000
0.000 ND 2.76 0.000 506 J 110 0.000
0.000 ND B 10.6 0.000 ND B 424 0.000
0.000 ND 8.35 0.000 ND 334 0.000
Page 10 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-I sooroov Ito luene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanen itrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1 1.2-Tetrachloroethane 630-20-6
I 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
1 2 4-Trichlorobenzene 120-82-1
1 1 I-Trichloroethane 71-55-6
1, 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1,2 3-Trichloroorooane 96-18-4
I .1 2-Trichlorotrifluoroethane 76-13-1
1 2.4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWW215
2000903503
Cone Flaa DL
! ND 0.0616
' ND 0.0474
ND 0.0452
ND 0.114
0.937 j 0.0469
ND 0.0845
ND B 0.0796
'ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
12.2 0.402
ND 0.0680
ND B 0.467
ND B 0.118
ND 0.0331
ND 0.0952
0.116 j 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0900HBWW227 0900HBWW228
2000903504 2000903505
Cone Flaa DL RL Cone Flaa DL RL
ND 3.08 0.000 ND 123 0.000
ND 2.37 0.000 ND 94.8 0.000
ND 2.26 0.000 ND 90.4 0.000
ND 5.70 0.000 ND 228 0.000
ND 2.34 0.000 ND 93.8 0.000
ND 4.22 0.000 ND 169 0.000
2.20 UB 3.98 0.000 280 JB 159 0.000
ND 5.30 0.000 ND 212 0.000
ND 34.4 0.000 ND 1380 0.000
ND 4.43 0.000 ND 177 0.000
ND 3.61 0.000 ND 144 0.000
ND 4.74 0.000 ND 190 0.000
ND 3.96 0.000 ND 158 0.000
ND 2.84 0.000 ND 114 0.000
ND 20.1 0.000 ND 804 0.000
8.92 j 3.40 0.000 1340 136 0.000
ND B 23.4 0.000 ND B 934 0.000
ND B 5.90 0.000 ND B 236 0.000
1220 1.66 0.000 64400 66.2 0.000
ND 4.76 0.000 ND 190 0.000
36.9 4.52 0.000 11500 181 0.000
ND 10.4 0.000 ND 416 0.000
ND 2.72 0.000 ND 109 0.000
ND 3.83 0.000 ND 153 0.000
ND 3.74 0.000 933 j 150 0.000
ND 2.18 0.000 ND 87.2 0.000
ND 2.19 0.000 ND 87.6 0.000
ND 2.87 0.000 ND 115 0.000
Page 11 of 34
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
p-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:58
0900HBWW215
2000903503
I Cone Flaa DL
ND 0.137
ND 0.0713
LJMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0900HBWW227 0900HBWW228
2000903504 2000903505
Cone Flaa DL RL ·cone Flaa DL RL
ND 6.85 0.000 1520 J 274 0.000
ND 3.56 0.000 1240 143 0.000
Page 12 of 34
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepar~d
Date/Time Analyz~d
Dilution Factor I
Instrument ·
Units
Surroaate Compound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -09/I 8/2000 I 9:58
0900HBWW215
2000903503
Aqueous
Received
NA
09/07/2000 09:35
09/08/2000 23:29
09/08/2000 23:29
1.0000
MSDA
U!!/L
o/o Recoverv Limits
99 77-117
98 61-143
93 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
F
0900HBWW227 0900HBWW228
2000903504 .. 2000903505
Aqueous Aqueous
Received Received
NA NA
09/07/2000 09:55 09/07 /2000 I 0: I 0
09/09/2000 0 I :24 09/08/2000 23:57
09/09/2000 01 :24 09/08/2000 23:57
50.0000 2000.0000
MSDA MSDA
ug/L ug/L
% Recovery Limits F % Recoverv Limits F
98 77-117 99 77-117
IOI 61-143 99 61-143
94 87-113 93 87-113
Page 13 of 34
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Brornobenzene
Brornochlorornethane
Brornodichlorornethane
Brornoforrn
Brornornethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Cljent Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collect~d
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
·74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
' 98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -09/18/2000 19:58
TRIP BLANK2
2000903507
Aaueous
Received
NA
09/07/2000 08:55
09/08/2000 23:01
09/08/2000 23:01
1.0000
MSDA
ug/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Li!tle Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
RL Cone Flag DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 14 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1,2-Dichloroorooane 78-87-5
1 3-Dichloroprooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
i :
cis-1.3-Dichlorooropene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -09/18/2000 19:58
I TRIP BLANK 2
2000903507
Cone Flaa DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND . 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND B 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 15 of 34
-·------------------
-------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Jodomethane 74-88-4
lsoorooylbenzene 98-82-8
4-lsoorooYltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Prooylbenzene 103-65-1
Styrene 100-42-5
LI 1 2-Tetrachloroethane 630-20-6
I, I 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
. 1 2.3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
I I.I-Trichloroethane 71-55-6
1 1,2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2 3-Trichloroorooane 96-18-4
1 I 2-Trichlorotrifluoroethane 76-13-1
1,2 4-Trimethvlbenzene 95-63-6
1.3 5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinyl chloride .. 75-01-4
SECTION IV -Analytical Results -09/18/2000 19:58
I TRIP BLANK 2
2000903507
! Cone Flag DL
ND 0.0616
! ND 0.0474 ! . ND 0.0452
I ND 0.114
ND 0.0469
ND 0.0845
ND B 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND B 0.467
ND B 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Lillle Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flag DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000 -
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -··-..
0.000 --
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 16 of 34
-.
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -09/18/2000 19:58
I TRIP BLANK 2
2000903507
I Cone Flaa DL I
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
Page 17 or 34
- - - - -·-- - - -·-- - - - - - - -
- - - -------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
l-Bromo-4-fluorobenzene
I .2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyz~d
Dilution Factor 1
Instrument
Units
SECTION IV -Analytical Results -09/18/2000 19:58
TRIP BLANK2
2000903507
Aaueous
Received
NA
09/07/2000 08:55
09/08/2000 23:01
09/08/2000 23:01
1.0000
MSDA
ug/L
% Recoverv Limits
95 77-117
100 61-143
92 87-113
LJMS Workordcr: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
F % Recoverv Limits F % Recoverv
- - -
Limits F
Page 18 of 34
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 8021 Instrument Data File: A0908002.D
Instrument ID: MSDA Analyst: JEC
Parameter Reference Value Measured Cone
Acetone 20 15.5
Acetonitrile 100 87.5
Acrolein 100 44.5
Acrvlonitrile 20 17.2
Benzene 20 19.6
Bromobenzene 20 20.l
Bromoch loromethane 20 23.5
Bromodichloromethane 20 16.8
Bromoform 20 18.2
Bromomethane 20 13.1
2-Butanone (MEK) 20 19.0
n-Butvlbenzene 20 19.4
sec-Butvlbenzene 20 19.8
tert-Butv I benzene 20 19.2
Carbon disulfide 20 14.3
Carbon tetrachloride 20 14.8
2-Chloro-1 3-butadiene 20 20.4
Chlorobenzene 20 21.5
Chloroethane 20 18.3
Chloroform 20 20.6
1-Chlorohexane 20 22.7
Chloromethane 20 13.9
3-Chloroorooene 20 12.7
2-Chlorotoluene 20 19.9
4-Chlorotoluene 20 19.7
1.2-Dibromo-3-chloroorooane 20 20.2
SECTION V -Calibration and QC Information -09/18/2000 19:58
LIMS Workorder: 756200.UA-Lillle Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:09/08/2000 14:09
Units: ug/L
%Recoveni Flag QC Limits %Recoverv
77
87
44
86
98
101
118
84
91
66
95
97
99
96
72
74
102
108
91
103 80-120
114
70
63
99
98
IOI
Page 19
-----------------
of 34
- -
----------------·---
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibrati~m Check
Analysis Batch ID: 8021 · ' Instrument Data File:
Instrument ID: MSDA Analyst:
Continued
Parameter Reference: Value Measured Cone
Dibromochloromethane 20 I 17.8
1 2-Dibro'moethane 20 I 19.7
Dibromomethane 20 I 18.7 I
trans-I 4-Dichloro-2-buten.e 20 I 9.68
I 4-Dichlorobenzene 20 18.8
1,2-Dichlorobenzene 20 19.3
I 3-Dichlorobenzene 20 19.0
Dichlorodifluoromethane 20 9.55
1 1-Dichloroethane 20 19.4
I 2-Dichloroethane 20 18.7
I 1-Dichloroethene 20 16.9
cis-1 2-Dichloroethene 20 22.5
trans-1.2-Dichloroethene 20 19.4
1 2-Dichloroorooane 20 18.9
1.3-Dichloroorooane 20 19.3
2.2-Dichloroorooane 20 21.1
1, 1-Dichloropropene 20 18.9
cis-1 3-Dichloroorooene 20 17.1
trans-I 3-Dichloroorooene 20 16.4
Ethvl methacrvlate 20 19.1
Ethvlbenzene 20 21.0
Hexachloro-1 3-butadiene 20 26.6
2-Hexanone 20 17.2
lodomethane 20 14.6
lsooroovlbenzene 20 20.9
4-Isopropyltoluene 20 19.7
SECTION V -Calibration and QC Information -09/18/2000 19:58
LIMS Workordcr: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
.
A0908002.D
JEC
Flaa %Recoverv
89
99
93
48
94
97
95
48
97
93
84
113
97
95
97
105
94
85
82
96
105
133
86
73
105
99
Date/Time Analyzed:09/08/2000 14:09
Units: ug/L
Flag QC Limits %Recoverv
80-120
80-120
80-120
Page 20 of 34
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 8021 Instrument Data File: A0908002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Methvl methacrvlate 20 18.7
Methvl tert-butyl ether (MTBE) 20 19.2
4-Methvl-2-oentanone (MJBK) 20 18.8
Methylene chloride 20 18.6
Naohthalene 20 24.9
Propanenitrile 100 96.1
n-Prooylbenzene 20 20.4
Styrene 20 21.2
1.1 1.2-Tetrachloroethane 20 20.1
I, 1 2 2-Tetrachloroethane 20 20.5
Tetrachloroethene 20 . 22.4
Tetrahvdrofuran 20 21.2
Toluene 20 20.4
1.2 3-Trich lorobenzene 20 31.8
J ,2 4-Trichlorobenzene 20 26.9
I I. I -Trichloroethane 20 20.8
I 1,2-Trichloroethane 20 20.7
Trichloroethene 20 21.8
Trichlorofluoromethane 20 21.2
1.2 3-Trich loroorooane 20 18.9
I, 1 2-Trich lorotrifluoroethane 20 14.2
1.2 4-Trimethylbenzene 20 18.8
1,3 5-Trimethvlbenzene 20 18.7
Vinyl acetate 20 19.8
Vinvl chloride 20 16.6
o-Xylene/m-Xvlene 40 42.9
SECTION V -Calibration and QC Information -09/18/2000 19:58
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Dateffime Analyzed:09/08/2000 14:09
Units: ug/L
%Recoverv Flaa QC Limits %Recovery
93
96
94
93
125
96
102
106
101
1.02
112
106
102 80-120
159
135
104
104
109
106
95
71
94
94
99
83 80-120
107
Page 21
- - - ---------------
of 34
- -
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 8021
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
l
!
i
!
I
Instrument Data File: A0908002.D
Injection Time: 09/08/2000 14:09
Ion Abundance Criteria
Lower limit Unner Limit
15 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -09/18/2000 19:58
LJMS Workorder: 756200.UA-Little Washington, N [20009035) Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 09/08/2000 14:09
Analyst: JEC
% Relative Abundance
21.7
39
100
6
0
73.7
6.5
98.6
6.3
Page 23 or 34
- - --· -·--·-- - - - - - - - - - -
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/T~me PreparEid
Date/Time Analyzed I Instrument
Units
CAS I I
67-64-1 :
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
SECTION V -Calibration and QC Information -09/18/2000 19:58
1014308
Method Blank
Aqueous
09/08/2000 15:33
09/08/2000 15:33
MSDA
u!!IL
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
·o.ooo
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 24 of 34
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
l 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
l .2-Dichlorobenzene 95-50-1
I J-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l, 1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
l 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
I 2-Dichloroprooane 78-87-5
I 3-Dichloropropane 142-28-9
2,2-Dichloroorooane 594-20-7
I 1-Dichloroprooene 563-58-6
cis-1,3-Dichloroorooene I 0061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsoproovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether <MTBE) 1634-04-4
SECTION V -Calibration and QC Information -09/18/2000 19:58
1014308
Cone Flaa DL
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND .0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
0.326 J 0.212
ND 0.167
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
LIMS Workordcr: 756200.UA-Littlc Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flan DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 25 or 34
- - - - - - - - - - - -·-- - - - - -
-----------------!--
SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
4-Methyl-2-pentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Propanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
I I 1.2-Tetrachloroethane 630-20-6
I I 2.2-Tetrachloroethane 79-34-5
. Tetrach loroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-l
I I, I-Trichloroethane 71-55-6
I 1.2-Trich loroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trich loroorooane 96-18-4
1 1,2-Trichlorotrifluoroethane 76-13-1
1 2.4-Trimethy I benzene 95-63-6
I 3.5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinyl chloride 75-01-4
o-Xylene/m-Xylene 106-42-3
o-Xylene 95-47-6
' I I
I
!
SECTION V -Calibration and QC Information -09/18/2000 19:58
1014308
Cone Flaa DL
ND 0.0845
2.27 0 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
0.902 J 0.467
0.425 J 0.118
ND 0.0331
ND 0.0952
0.0894 u 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
ND 0.137
ND 0.0713
UMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STL Austin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000 --.
0.000 ...
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -
Page 26 of 34
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Surroaate Comoound
1-Bromo-4-fluorobenzene
I ,2-Dichloroethane-d4
Toluene-d8
Method Blank ID
Sample Type
Matrix
Date/Time Prepar~d
Date/Time Analyz~d
Instrument
Units
'
SECTION V -Calibration and QC Information -09118/2000 19:58
1014308
Method Blank
Aaueous
09/08/2000 15:33
09/08/2000 15:33
MSDA
ug/L
% Recovery Limits
98 77-117
103 61-143
92 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
F % Recoverv Limits F % Recovery Limits F
Page 27 of 34
---·---------·---·--·--
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Client Sample ID:
Prep Batch ID:
LCS for HBN 8021 [MSV/1313]
8021
Analysis Batch ID: 8021
I
Parameter I
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Ch loromethane
2-Chlorotoluene
4-Chlorotoluene
I 2-Dibromo-3-chloroorooane
Dibromochloromethane
1.2-Dibromoethane
Dibromomethane
1.4-Dichlorobenzene
SECTION V -Calibration and QC Information -09/18/2000 19:58
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
c ontrol s amnle
LablO: 1014306
FilelO: A0908003.D
Sok Amt Cone %Rec Fla
20 15.4 77
20 18.2 91
20 19.2 96
20 22.4 112
20 16.5 82
20 18.l 90
20 12.5 63
20 20.6 103
20 19.0 95
20 20.0 100
20 18.5 93
20 15.0 75
20 14.4 72
20 20.5 102
20 16.4 82
20 19.7 98
20 I 1.5 57
20 19.5 97
20 19.0 95
20 19.1 95
20 18.1 90
20 19.9 100
20 17.7 89
20 18.2 91
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
Lab ID:
FilelO:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
JEC Analyst:
Control Sample D I' up 1cate
1014307
A0908004.D
Cone %Rec Fla
15.0 75
18.4 92
19.0 95
22.7 113
16.6 83
17.6 88
12.9 65
18.2 91
18.6 93
19.7 99
18.2 91
15.9 79
14.5 73
20.2 IOI
16.9 84
19.9 99
11.9 60
19.0 95
18.9 94
18.7 93
I 8.2 91
19.3 97
17.9 89
18.I 91
QC Limits
RPO Fla %Rec RPO
2.6 0.1-240 71
I. I 71-133 17
I 67-127 12
0.9 61-145 21
1.2 57-135 19
2.2 23-151 17
3.1 34-128 25
12 0.1-214 39
2.1 28-184 30
1 45-160 31 ---2.2 65-148 27
5.2 29-223 23
1.4 46~150 23
I 77-129 14
2.4 39-133 27
I 64-146 16
5.1 18-140 26
2.1 70-136 24
I.I 74-132 23
2.1 39-171 25
I.I 45-137 15
3 19-187 19
0 52-138 21
0 70-132 13
Page 28 of 34
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Lab ID:
c ontrol s amole contmued
1014306
File ID: A0908003.D
Parameter ' Sok Amt Cone
1 2-Dichlorobenzene 20 19.0
I 3-Dichlorobenzene 20 18.2
Dichlorodifluoromethane 20 9.54
I 1-Dichloroethane 20 18.4
I 2-Dichloroethane I 20 17.8
I 1-Dich loroethene I• 20 16.1
cis-1.2-Dichloroethene : 20 20.9
trans-1.2-Dichloroethene 20 18.7
1.2-Dichloroorooane 20 18.6
1,3-Dichloroorooane 20 15.3
2.2-Dich Ioroorooane 20 20.6
I, 1-Dichloroorooene 20 17.3
cis-1 3-Dichloroorooene 20 16.4
trans-I 3-Dichloroorooene 20 15.6
Ethvlbenzene 20 20.4
Hexachloro-1 3-butadiene 20 26.4
2-Hexanone 20 17.8
Iodomethane 20 15.2
lsooroovlbenzene 20 20.7
4-lsooroovltoluene 20 18.9
4-Methvl-2-oentanone (MIBK) 20 17.9
Methvlene chloride 20 17.7
Naphthalene 20 26.4
n-Proovlbenzene 20 20.4
Styrene 20 21.2
1 I 1.2-Tetrachloroethane 20 19.7
1 I 2.2-Tetrachloroethane 20 20.4
Tetrachloroethene 20 22.4
Toluene 20 19.5
1.2 3-Trichlorobenzene 20 33.8
1,2 4-Trichlorobenzene .. 20 27.5
SECTION V -Calibration and QC Information -09/18/2000 19:58
LIMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
95
91
48
92
89
80
105
93
93
76
103
86
82
78
102
132
89
76
103
94
90
89
132
102
106
99
102
112
97
169 0
137
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Control Samole D uolicate contmue d
1014307
A0908004.D QC Limits
Cone %Rec Fig RPO Fla %Rec RPO
18.7 94 I. I 67-135 14
18.0 90 I.I 68-134 14
9.79 49 2.1 0.1-166 26
18.4 92 0 66-138 19
18.0 90 I. I 48-152 23
16.5 82 2.5 47-175 25
21.8 109 3.7 66-144 18
19.I 96 3.2 62-146 22
18.2 91 2.2 61-133 17
18.3 91 18 0 70-128 16
20.7 103 0 40-168 30
17.2 86 0 71-155 31
17.I 86 4.8 36-142 16
15.9 79 1.3 34-138 21
20.9 104 1.9 75-131 14
25.7 128 3.1 46-150 34
18.0 90 I.I 22-164 34
16.1 81 6.4
20.3 101 2 54-152 26
18.7 93 I. I 41-165 28
18.I 91 I. I 27-149 36
17.9 90 I. I 36-166 23
26.5 132 0 32-172 22
19.8 99 3 61-143 28
20.6 103 2.9 68-136 14
19.4 97 2 63-141 20
19.9 100 2 47-143 20
21.0 105 6.5 69-137 16
19.4 97 0 70-132 17
33.9 170 0 0.6 66-140 20
27.8 139 1.4 66-144 22
Page 29 of 34 ___ , _____ , ___ . _______ _
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Lab ID:
C t IS on ro amp e contmue
1014306
I File ID: A0908003.D
Parameter Sok Amt Cone
1 1 I-Trichloroethane 20 19.9
I 1 2-Trichloroethane I 20 19.4
Tri ch Ioroethene I 20 20.8
Trichlorofluoromethane I 20 17.3 !
I 2 3-Trichloropropane I 20 18.8
1 2 4-Trimethvlbenzene I 20 18.2
1,3 5-Trimethvlbenzene I 20 18.7
Vinvl acetate I 20 16.4
Vinvl chloride ' 20 14.7
o-Xvlene/m-Xvlene ' 40 41.6
o-Xvlene 20 20.6
SECTION V -Calibration and QC Information -09/18/2000 19:58
LIMS Workorder: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
100
97
104
86
94
91
93
82
74
104
103
d
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
40
20
C t IS on ro amoe uo tea e con mue I D r t f d
1014307
A0908004.D QC Limits
Cone %Rec Fig RPO Fla %Rec RPO
19.9 99 1 49-155 24
19.4 97 0 67-135 17
20.8 104 0 71-129 17
18.l 90 4.5 39-147 29
18.7 93 1.1 64-140 18
17.7 88 3.4 54-156 25
18.1 90 3.3 62-144 25
15.1 75 8.9 0.1-164 31
14.9 75 1.3 24-138 27
40.5 101 2.9 "'"' 76-134 15
20.3 102 I 77-131 15
.-
Page 30 of 34
SECTIONV
Calibratio1,1 and QC Information
Control Sample Results
MS-VOA
SW8260B
Surroaate Comoounds
J-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -09/18/2000 19:58
Lab ID: 1014306
o/oRecoverv
99
98
92
LIMS Workordcr: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
Fla as
Lab ID: 1014307
o/oRecoverv Flags QC Recoverv Limits
98 77-117
JOO 61-143
94 87-113
Page 31 of 34
-----------------·--
-------·------------
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 8021
Client Samole ID
INSTRUMENT QC
INSTRUMENT QC
LCSforHBN 8021 fMSV/13131
LCSD for HBN 8021 fMSV/13131.
MB for HBN 8021 fMSV/13131 zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz
zzzzzzzzzz zzzzzzzzzz I
TRIP BLANK2
0900HBWW215
0900HBWW228
0900HBWW213
0900HBWW214
0900HBWW227
0900HBWD999
SECTION VI -Batch Summaries -09/18/2000 19:58
i Lab Samole ID
1000:
1406'
1014306
1014307
1014308
2000902401
1014309
1014310
2000903801
2000903802
2000903803
2000902402
2000902403
2000902404
2000902405
2000902406
2000902407
2000902408
2000902409
2000902410
2000903507
2000903503
2000903505
2000903501
2000903502
2000903504
2000903506
Start Date/Time: 09/08/2000 14:09
Stop· Dateffime: 09/09/2000 01 :54
Sample Type Matrix
GC/MS Tune Aaueous
Continuine: Calibration Check Aqueous
Lab Control Sample Aaueous
Lab Control Sample Duolicate Aqueous
Method Blank Aqueous
Field Sample Aaueous
Matrix Soike Aqueous
Matrix Spike Duplicate Aaueous
Field Samole Aqueous
Field Sample Aaueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
Field Samole Aqueous
Field Sample Aqueous
Field Samole Aaueous
Field Sample Aqueous
Field Samole Aaueous
LIMS Workordcr: 756200.UA-Little Washington, N (20009035] Hamilton Beach-Proctor Silex
STL Austin
Analyst: JEC
Sample Size
Initial Final Preoaration Method
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW82608
15 mL 15 mL SW82608
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL-15 mL SW8260B
15 mL 15 mL SW8260B -
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW82608
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
Page 32 or 34
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 8021 Instrument ID: MSDA
Seauence Client Samole ID I Lab Sample ID
I INSTRUMENT QC 1000
2 INSTRUMENT OC ' 1406
3 LCS for HBN 8021 fMSV /13 I 31' 1014306
4 LCSD for HBN 802 I fMSV /I 3 I 31 1014307
5 MB for HBN 8021 fMSV/13131: 1014308
6 zzzzzzzzzz 2000902401
7 zzzzzzzzzz 1014309
8 zzzzzzzzzz 10143 JO
9 zzzzzzzzzz 2000903801
JO zzzzzzzzzz 2000903802
1 I zzzzzzzzzz 2000903803
12 zzzzzzzzzz 2000902402
13 zzzzzzzzzz 2000902403
14 zzzzzzzzzz 2000902404
15 zzzzzzzzzz 2000902405
16 zzzzzzzzzz 2000902406
17 zzzzzzzzzz 2000902407
18 zzzzzzzzzz 2000902408
19 zzzzzzzzzz 2000902409
20 zzzzzzzzzz 2000902410
21 TRIPBLANK2 2000903507
22 0900HBWW215 2000903503
23 0900HBWW228 2000903505
24 0900HBWW213 2000903501
25 0900HBWW214 2000903502
26 0900HBWW227 2000903504
27 0900HBWD999 2000903506
SECTION VI -Batch Summaries -09/18/2000 19:58
LIMS Workordcr: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STLAustin
Analysis
Date Time
09/08/2000 14:09:00
09/08/2000 14:09:00
09/08/2000 14:37:00
09/08/2000 15:05:00
09/08/2000 I 5:33:00
09/08/2000 16:01:00
09/08/2000 16:29:00
09/08/2000 16:57:00
09/08/2000 17:25:00
09/08/2000 17:53:00
09/08/2000 18:21:00
09/08/2000 18:49:00
09/08/2000 19:17:00
09/08/2000 19:45:00
09/08/2000 20:13:00
09/08/2000 20:41:00
09/08/2000 21:09:00
. 09/08/2000 21:37:00
09/08/2000 22:05:00
09/08/2000 22:33:00
09/08/2000 23:01:00
09/08/2000 23:29:00
09/08/2000 23:57:00
0910912000 00:26:00
0910912000 00:54:00
09/09/2000 01:24:00
0910912000 01:54:00
Analyst: JEC
SampleTvpe Analysis File ID Sub-Batch ID
GC/MS Tune A0908002.D 0
Continuing Calibration Check A0908002.D 0
Lab Control Samole A0908003.D 0
Lab Control Sample Duplicate A0908004.D 0
Method Blank A0908005.D 0
Field Sample A0908006.D 0
Matrix Soike A0908007.D 0
Matrix Spike Duplicate A0908008.D 0
Field Samole A0908009.D 0
Field Samole A0908010.D 0
Field Sample A090801 l.D 0.
Field Samole A0908012.D 0
Field Sample A0908013.D 0
Field Sample A0908014.D 0
Field Samole A0908015.D 0
Field Sample A0908016.D 0
Field Samole A0908017.D 0
Field Samole A0908018.D 0
Field Sample A0908019.D 0
Field Samole A0908020.D 0
Field Sample A0908021.D 0
Field Samole A0908022.D 0
Field Samole A0908023.D 0
Field Sample A0908024.D 0
Field Sample A0908025.D 0
Field Samole A0908026.D 0
Field Samole A0908027.D 0
Page 33 of 34
-------------------
- -
SECTION VII
Certifications
State/Aaencv
----
!
Arkansas Department of Pollution Control and Ecology
- -- -
California Environmental Laboratorv Accreditation Program I Waste Water/Hazardous Waste
Kansas Department of Health and Environment J, Solid and Hazardous Waste/Di-inking Water
- - - -
ID#
2257
E-10165
Louisiana Department of Environmental Oualitv~ ELAP I Waste Water/Hazardous Waste/ Air/Emissions
New Jersev Deoartment of Environmental Protection
New York State Department of Health I Waste Water/Hazardous Waste
North Carolina Dept. of Natural Resources & Communitv Develooment I Waste Water
Oklahoma Water Resources Board I Waste Wate'r
South Carolina Dept. of Health & Environmentai Control '
Utah Deoartment of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources I
US Air Force/AFCEE
US Armv Corps of Engineers (ACE)
US Department of Agriculture I Restricted Soils Permit
SECTION VII -Certifications -09/18/2000 19:58
LIMS Workorder: 756200.UA-Little Washington, N [20009035] Hamilton Beach-Proctor Silex
STL Austin
82005
10915
302
8720
82003002
RADC
999885260
Participating Laboratorv
S-42350
- ----
Page 34 of 34
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
APPENDIXB
CONTAMINANT CONCENTRATIONS VERSUS TIME
MW-213
1000 -;
900
800
700
:::r -. 600 C> ::::J -c 0 ~ 500 I! ....
-~
~ -~
-~ --'.
--+-1, 1-Dichloroethene
-Tetrachloroethene
--*-Trichloroethene c G> (,) c 400 0
--~"'£ . T
-*-Vinyl chloride
(.)
300
200
100 -
: ----,.. "' ..,
0 ., ..
Nov-98 Feb-99 May-99 Aug-99 Dec-99 Mar-00 Jun-00 Oct-00
Sample Date
-------------------