IDX GW Monitoring Report Oct 1999 (BF)-OCR

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GROUNDWATER MONITORING REPORT
FOR OCTOBER 1999
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
Prepared for:
Hamilton Beach<>Proctor-Silex, Inc .
4421 Waterfront Drove
Glen Allen, Virginia 23060
Prepared by:
Radian International
P.O. Box 13000
Research Triangle Park, North Carolina 27709
November 1999
• TABLE OF CONTENTS
C .fi . p .. ert1 icat1on age ................................................................................................................ 11
List of Figures .................................................................................................................... iv
List of Tables .......................................... ; ........................................................................... v
1.0 INTRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS .......................................................................................................... 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3 .1 Water Level Measurements ................................................................................. 3-1
3.2 Analytical Results ................................................................................................ 3-1
APPENDIX A GROUNDWATER SAMPLING ANALYTICAL REPORTS
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650138.090 I OctGW _ Rpt.doc ( 11129/99) 11l
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1-1
2-1
3-1
3-2
3-3
LIST OF FIGURES
Topographic Map, Hamilton Beach<>Proctor-Silex, Inc.
Site Map, Washington Facility, Hamilton Beach<>Proctor-Silex, Inc.
Generalized Groundwater Flow Direction for Hydrogeologic Unit A,
Washington Facility
Generalized Groundwater Flow Direction for Hydrogeologic Unit B,
Washington Facility
Location of Surrounding Water Supply Wells, Hamilton Beach<> Proctor-Silex, Inc. . '
650138.0901 OctGW _Rpt.doc (11/29/99) lV
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2-1
3-1
3-2
. 3-3
3-4
3-5
LIST OF TABLES
Monitoring Well Construction Data for Sampled Wells
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Water Level Measurements and Elevations, October 20, 1999
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-6 Historical Water Level Elevations at MW-226
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-7 Historical Water Level Elevations at MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-8 Historical Water Level Elevations at MW-234
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-9 Field Measurements, October 20, 1999
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-10 Qualified Analytical Results, Volatile Organic Compounds by Method 8260B,
October 1999, Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-11 Historical Analytical Results for MW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-12 Historical Analytical Results for MW-222
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-13 Historical Analytical Results for MW-224
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
650138.0901 OctGW _Rpt.doc (I 1/29/99) v
• LIST OF TABLES (Continued)
3-14 Historical Analytical Results for MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-15 Historical Analytical Results for MW-226
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-16 · Historical Analytical Results for MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-17 Historical Analytical Results for MW-234
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
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650138.090 I OctGW _Rpt.doc (11/29/99) Vl
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1.0 INTRODUCTION
The Hamilton BeachOProctor-Silex (HBOPS) facility is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HBO PS since 1990 and previously leased by predecessor companies. The facility is involved
in the final assembly, packaging, and warehousing of small electrical household appliances.
Since 1992, when organic compounds were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
assessment (CSA). The results of the CSA indicated that a plume of organic compounds is
present in groundwater underlying the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer used at the facility.
A plan for corrective action at the site has been proposed.,Until corrective action l
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to.l
a monitoring program requested and approved by the North Carolina Department of f
Environment and Natural Resources, Groundwater Section. fhe purpose of the monitoring
program is to sample selected downgradient monitoring wells to detect potential migration of the
plume.
Radian International (Radian) conducted groundwater sampling at the facility in
October 1999. The sampling event included the measurement of water levels, temperature, pH,
and specific conductance; and the collection and analysis of samples from seven monitoring
wells. This report describes the sampling methods and presents the results for the second
quarterly sampling event.
650138.0901 OctGW _Rpt.doc (11/29/99) 1-1
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2.0 FIELD METHODS
Groundwater was sampled on October 20, 1999, in general accordance with the
methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for this site.
Seven monitoring wells were sampled. They included MW-220, MW-222,
MW-224 through MW-226, MW-230, and MW-234. The locations of the seven monitoring
wells are shown in Figure 2-1. Details of well construction are provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using dedicated inertial foot-valve pumps.
Temperature, pH, and specific conductance were measured and the data were recorded in a field
notebook. Purging continued until temperature, pH, and specific conductance stabilized; a
minimum of three well volumes was extracted; or the well was pumped dry. Each of the wells
· was then sampled immediately following well purging using the dedicated inertial foot-valve
pump.
The groundwater samples were sent by overnight courier to Radian Analytical
Services in Austin, Texas, for analysis of volatile organic compounds by EPA Method 8260B.
650138.0901 OctGW _Rpt.doc (11/29/99) 2-1
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3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the seven wells sampled and eight additional wells. Maps showing the generalized
direction of groundwater flow in hydrogeologic units A and B are included as Figures 3-1 and
3-2, respectively. Historical water-level elevations in sampled wells are included in Tables 3-2
to 3-8.
3.2 Analytical Results
Measurements of water temperature, pH, and specific conductance recorded in the
field are summarized in Table 3-9.
A summary of qualified analytical results is presented in Table 3-10. No analytes
were detected above the groundwater standards in any sample. Qualified data sheets and
laboratory reports are included in Appendix A.
Historical analytical results for the sampled wells are presented in Tables 3-11 to
3-17. A comparison of the latest results with earlier results suggests that the plume remains on-
site, at least 200 feet, or approximately ten years time-of-travel, from the potential receptors
located north of Spring Road (Figure 3-3). In addition, the results indicate that no vertical
migration into the Limestone Aquifer has occurred .
650138.0901 OctGW _Rpt.doc (ll/29/99) 3-1
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Table 3-1
Water Level Measurements and Elevations
October 20; 1999
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Measuring Point Water Level
Elevation Elevation
Well (ft above msl)) Depth to Water (ft) (ft above msl)
MW-201S 29.74 1.68 28.06
MW-208 32.11 5.17 26.94
MW-217 32.75 7.21 25.54
MW-219 31.83 6.61 25.22
MW-220 31.50 5.87 25.63
MW-221 31.39 7.04 24.35
MW-222 35.11 10.89 24.22
MW-223 35.15 7.17 27.98
MW-224 33.43 6.55 26.88
MW-225 33.43 6.19 27.24
MW-226 28.46 17.35 11.11
MW-227 28.47 2.65 25.82
MW-230 33.47 5.76 27.71
MW-233 34.55 9.59 24.96
MW-234 35.03 9.32 25.71
msl = mean sea level
650138.0901 OctGW _Rpt.doc (11/29/99)
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Table 3-2
Historical Water Level Elevations at MW-220
Hamilton BeachO Proctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 25.13
November 16, 1998 20.55
Julv 1, 1999 21.50
October 20, 1999 25.63
msl = mean sea level
650138.090 I OctGW _ Rpt.doc ( 11/29/99)
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Table 3-3
Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 22.34
November 16, 1998 19.99
July 1, 1999 20.61
October 20, 1999 24.22
msl = mean sea level
650138.0901 OctGW _Rpt.doc (11/29/99)
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Table 3-4
Historical Water Level Elevations at MW-224
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
msl = mean sea level
NM =Not measured
650138.0901 OctGW _Rpt.doc (11/29/99)
Water Level Elevation
(ft. above msl)
NM
23.64
24.39
26.88
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Table 3-5
Historical Water Level Elevations at MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
Julv 1, 1999
October 20, 1999
msl = mean sea level
NM = Not measured
650138.0901 OctGW _Rpt.doc (11129/99)
Water Level Elevation
(ft. above msl)
NM
24.36
24.50
27.24
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Table 3-6
Historical Water Level Elevations at MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
Julv 1, 1999
October 20, 1999
msl = mean sea level
NM =Not measured
650138.0901 OctGW _Rpt.doc (11/29/99)
Water Level Elevation
(ft. above msl)
NM
8.43
8.54
11.11
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Table 3-7
Historical Water Level Elevations at MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
Julv 1, 1999
October 20, 1999
ms! = mean sea level
NM =Not measured
650138.090 I OctGW _ Rpt.doc ( 11129/99)
Water Level Elevation
(ft. above msl)
NM
21.14
21.80
27.71
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Table 3-8
Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
msl = mean sea level
NM =Not measured
650138.0901 OctGW _Rpt.doc (11/29/99)
Water Level Elevation
(ft. above msl)
NM
NM
23.24
25.71
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Introduction
Radian International collected seven groundwater samples (1099HBWW-220, -222, -224-226, -230, and -
234) at the Hamilton Beach<> Proctor Silex facility in Washington, NC. The samples were submitted to
Radian's Analytical Services (RAS) laboratory in Austin, Texas for the determination of volatile organic
compounds (VOC) by SW-846 Method 8260B. A trip blank was included in the shipment of samples to
the laboratory for the analysis of voe.
Radian reviewed the analytical results, which were reported by the laboratory under work order number
9910408. The data evaluation was modeled after the National Functional Guidelines for Organic Data
Review (EPA, February 1994). Accuracy was determined from the review of holding times, spike
recoveries, initial and continuing calibration, and blank contamination. Precision was based on the
evaluation oflaboratory duplicate results. Sample results, presented in the Results Summary, have been
appropriately qualified based on criteria of the review process. The results of the data evaluation are
summarized below.
Sample Condition upon Receipt and Holdfug Times
All samples were received intact and in good condition by RAS laboratory on October 21, 1999. The
temperature of the sample containers was within laboratory specification limits of2-6°C upon receipt. A
small air bubble (4 millimeters in diameter) was observed in one of the volatile organic analysis (VOA)
vials that were received by the laboratory for the trip blank. Qualification of the trip blank results is not
required since vials were available for the VOA that did not contain air bubbles greater than 6 millimeters
in size.
Technical hold times were assessed by comparing the sampling dates with that of the analysis date .
Samples were analyzed within EPA-established holding times of seven days for unpreserved samples.
Calibration
Control limits for initial and continuing instrument calibrations are established to ensure that the instrument
is capable of producing accurate quantitative and qualitative data at the beginning and throughout each of
the analyses.
Laboratory specifications were met during volatile organic initial and continuing calibrations. Except for a
few analytes, project1 specifications were also met during the· calibration of the instrument. During the
initial calibration of October 18 on instrument MSDC, the response factor for acrolein (0.0282) and
acetonitrile (0.0234) was less than 0.05. Non-detect sample results for these two VOC were qualified as
unusable (R) because of poor instrument sensitivity.
Blank Contamination
Laboratory blanks are clean liquid and/or solid matrix samples prepared by the analytical laboratory and
analyzed in the same manner as the field samples. Laboratory blanks are used to ensure that the field
samples are not contaminated during the sample preparation, sample analysis, or from previous sample
(instrument carry-over). Trip blanks are analyte-free water samples that accompany volatile investigative
samples during all stages of shipment, storage, and analysis. The trip blanks are used to assess the potential
for artificial introduction of volatile compounds into the investigative samples during the transportation and
sample handling processes.
Methylene chloride, a common blank contaminant, was detected at a concentration of0.0297 J ppb and
0.120 parts per billion (ppb) in the laboratory and trip blanks, respectively. The trip blank also contained
1 Response factor is greater than or equal to 0.05 and the percent relative standard deviation is less than or equal to 30
for all target analytes durins the initial calibration. The recovery of the continuing calibration verification standard is
within 80-120% of the true value during the continuing calibration.
1099 HB-PS DE.doc
Page I of2
I Ill 0199
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toluene at a concentration of0.0974 ppb. The result for methylene chloride in sample 1099HBWW230 is
not significantly greater than that detected in the blanks; therefore, it has been flagged "ND" and the
detection limit elevated to the amount present in the sample and flagged with a "U". Further qualification
of data due to blank contamination is not required since methylene chloride and toluene were not detected
in any other samples.
Surrogate Spikes and Jnternal Standards
System monitoring compounds (surrogates) are those compounds that are not expected to be detected in the
field samples, but which are chemically similar to the analytes of interest. Surrogate compound percent
recoveries are used to assess extraction efficiencies, possible matrix effects, and overall analytical
accuracy. Internal standards are analytes of interest that are added to each sample prior to analysis to
ensure that GC/MS sensitivity and responses remain stable.
Surrogate and internal standard results met laboratory specification limits for all samples.
Laboratory Control Samples
Laboratory control samples (LCS) are blank samples fortified (spiked) with known concentrations of
analyte of interest. The percent recoveries and/or duplicate results of the LCS and their duplicates are used
to assess extraction efficiencies arid overall analytical accuracy and precision.
Laboratory and project2 specifications were met during the LCS VOA.
Matrix Spikes
Matrix spikes are samples spiked with known concentrations of analytes of interest. MS percent recoveries
and duplicate results are used to assess extraction efficiencies, possible matrix effects, and overall
analytical accuracy and precision.
Accuracy and precision criteria were met during the matrix spike (MS) and MS duplicate analysis of the
batch sample for voe .
2 The recovery of either the LCS or LCSD must be within 60-140%.
1099 HB-PS DE.doc
Page 2of2
11/10/99
• 11/03/99 13:58:32
Report RADIAN INTERNATIONAL
To 3200-E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _--!:R:!:a::;d~i~a:.!.n~I,_,n!!t:.::e:..:r..:.n~a!!t'-'io::o~n~a~l~,_.L~L~C'""­
By _ _.l;.;:4:.::0;.:.4:.::6:.....:;S::;u,,,m:::m:..:i:.::t.__.D:..:ro..;.'"'-"B'-'l'-'d°"q'"'._.B,_
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1099HBWW224
1099HBWW225
1099HBWW226
1099H8WW234
1099H8WW222
1099HBWW230
1099HBWW220
TRIP BLANK
ID/
• II 0 R IC 0 R D E R SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID VOLATILES
Case II ~N:.:.A:..._ _______ _
SDG II ,,N,_,A _______ _
RAS II 91014AJAL
Lab Sample ID Test Code(s)
OlA 826SWACM
OlB SPAREBOO
OlC SPARE800
02A 826SWACM
028 SPAREBOO
02C SPAREBOO
03A 826SWACM
038 SPARE800
03C SPAREBOO
04A 826SWACM
048 SPAREBOO
04C SPARE800
05A 826SWACM
05B SPAREBOO
05C SPAREBOO
06A 826SWACM
06B ; SPAREBOO
06C SPARE800
07A 826SWACM
07B SPAREBOO
07C SPARE800
OBA 826SWACM
08B SPARE800
Work Order # 9910408
Page _1_
RCN 80396901.01
New York ELAP ID#: 10915
Method Desciption
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
•
• 11/03/99 13:58:32 • If 0 R II: 0 R D B R C 0 M M B R T S
The standard Method 8260A surrogate tolerances are laboratory derived from
historical data. Project specific tolerances may differ.
• Work Order # 9910408
Page _2_
• 11/03/99 13:58:32
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIFICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9910408
Page _3_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
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• • 11/03/99 13:58:32 ANALYTICAL PROTOCOL SUMMARY
F L A G D B F I N I T I 0 N S
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A
B
c
Presence of hydrocarbon mix eluting'in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identifica~ion suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation.
Work Order # 9910408
Page _4_
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Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Volatile Organics SW8260B
Project Sample ID/Description
1099HBWW220
1099HBWW222
1099HBWW224
l.099HBWW225
1099HBWW226
1099HBWW230
1099HBWW234
TRIP BLANK
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch II
9910408-0?A 826SWACM NA
9910408-0SA 826SWACM NA
9910408-0lA 826SWACM NA
9910408-02A 826SWACM NA
9910408-03A 826SWACM NA
9910408-06A 826SWACM NA
9910408-04A 826SWACM NA
9910408-0BA 826SWACM NA
Work Order II 9910408
Page _s_
Analysis Batch II
MSMSDC91021172601
MSMSDC91021172601
MSMSDC91021172601
MSMSDC91021172601
MSMSDC91021172601
MSMSDC91021172601
MSMSDC91021172601
MSMSDC91021172601
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
1-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
1099HBWW220
9910408-07A
C1021914
10/20/99 11:45
00:00:00
10/21/99 22:38:00
1
Water
ug/L
rece'ived
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.162
ND
ND
ND
ND
DL
1. 04
3.79
3. 71
0.305
0.0469
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0.0744
0.0619
0.0493
0.0778
0.0836
0.0527
0.0819
• RESULTS SUMMARY
1099HBWW222
9910408-05A
Cl021912
10/20/99 11: 05
00:00:00
10/21/99 21:41:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0944
ND
ND
ND
ND
DL
1. 04
3.79
3. 71
0.305
0. 0469
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0.0744
0.0619
0.0493
0. 0778
0.0836
0.0527
0.0819
1099HBWW224
9910408-0lA
C1021908
10/20/99 09:40
00:00:00
10/21/99 19:48:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2. 72
ND
ND
ND
ND
DL
1. 04
3.79
3. 71
0.305
0. 04 6 9
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0. 0744
0.0619
0. 04 93
0.0778
0.0836
0.0527
0.0819
Work Order # 9910408
Page _6_
1099HBWW225
9910408-02A
Cl021909
10/20/99 09:25
00:00:00
10/21/99 20:16:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0691
ND
ND
ND
ND
DL
1. 04
3.79
3.71
0.305
0.0469
0.0507
0.0566
0.0990
0.0619
0.0756
0. 0962
0.179
0.0655
0.0744
0.0619
0.0493
0. 0778
0.0836
0.0527
0.0819
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1099HBWW220
9910408-07A
Cl021914
10/20/99 11:45
00:00:00
10/21/99 22:38:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0.0454
0.0556
0 .. 0651
0.270
0.0588
0.0408
0.0819
0.0407
0.0422
• RESULTS S UM MAR Y (Cont'd)
1099HBWW222
9910408-05A
C1021912
10/20/99 11:05
00:00:00
10/21/99 21:41:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0. 04 54
0.0556
0.0651
0.270
0.0588
0.0408
0.0819
0. 04 07
0.0422
1099HBWW224
9910408-0lA
Cl021908
10/20/99 09:40
00:00:00
10/21/99 19:48:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0. 0454
0.0556
0.0651
0.270
0.0588
0. 04 08
0.0819
0.0407
0.0422
Work Order # 9910408
Page _7_
1099HBWW225
99104 08-02A
Cl021909
10/20/99 09:25
00:00:00
10/21/99 20:16:00
1
Water
ug/L
received
Cone.
0 .171
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0.0454
0.0556
0.0651
0.270
0.0588
0.0408
0.0819
0.0407
0.0422
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1, 3-Dichloroprop'ane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
1099HBWW220
9910408-07A
Cl021914
10/20/99 11:45
00:00:00
10/21/99 22:38:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0. 0712
0.0375
0.0430
0.0412
0.0563
0.0763
0.144
0.0436
0.0815
0.0662
0.0916
0.0512
0.0775
0.0607
0.0576
0.408
0.0558
• RBSULTS S UM MAR Y (Cont'd)
1099HBWW222
9910408-05A
Cl021912
10/20/99 11:05
00:00:00
10/21/99 21:41:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0. 0712
0.0375
0.0430
0. 0412
0.0563
0.0763
0.144
0.0436
0.0815
0.0662
0.0916
0.0512
0. 0775
0.0607
0.0576
0.408
0.0558
1099HBWW224
9910408-0lA
Cl021908
10/20/99 09:40
00:00:00
10/21/99 19:48:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0. 0712
0.0375
0. 0430
0.0412
0.0563
0.0763
0.144
0.0436
0.0815
0.0662
0.0916
0.0512
0.0775
0.0607
0.0576
0.408
O.Cf558
Work Order # 9910408
Page _8_
1099HBWW225
9910408-02A
Cl021909
10/20/99 09:25
00:00:00
10/21/99 20:16:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0.0712
0.0375
0.0430
0. 0412
0.0563
0.0763
0.144
0.0436
0.0815
0.0662
0.0916
0.0512
0.0775
0.0607
0.0576
0.408
0.0558
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
1099HBWW220
9910408-07A
C1021914
10/20/99 11 :45
00:00:00
10/21/99 22:38:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0.0728.
0.0785
0.0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0.0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
• RESULTS SUMMARY (Cont'd)
1099HBWW222
9910408-05A
C1021912
10/20/99 11: 05
00:00:00
10/21/99 21:41:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0.0728
0.0785
0.0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0. 0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
1099HBWW224
9910408-0lA
C1021908
10/20/99 09:40
00:00:00
10/21/99 19:48:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
,0.0728
0.0785
0.0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0.0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
Work Order # 9910408
Page _9_
1099HBWW225
9910408-02A
Cl021909
10/20/99 09:25
00:00:00
10/21/99 20:16:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0. 0728
0. 0785
0.0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0.0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0 .112
0.0732
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
1099HBWW220
9910408-07A
Cl021914
10/20/99 11:45
00:00:00
10/21/99 22:38:00 ' 1
Water
ug/L
received
Cone. DL
Recovery
\
. 97
107
102
• RB s·u LT s S UM MAR Y (Cont'd)
1099HBWW222 1099HBWW224
9910408-05A 9910408-0lA
C1021912 C1021908
10/20/99 11:05 10/20/99 09 :40
00:00:00 00:00:00
10/21/99 21:41:00 10/21/99 19:48:00
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
Recovery Recovery
\ %
98 99
104 100
102 102
Work Order # 9910408
Page lQ_
1099HBWW225
9910408-02A
Cl021909
10/20/99 09:25
00:00:00
10/21/99 20:16:00
1
Water
ug/L
received
Cone. DL
Recovery
%
99
99
102
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Aero le in
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
1099HBWW226
9910408-03A
Cl021910
10/20/99 10:20
00:00:00
10/21/99 20:44:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0950
ND
ND
ND
ND
DL
1. 04
3.79
3. 71
0.305
0.0469
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0.0744
0.0619
0. 0493
0.0778
0.0836
0.0527
0.0819
• Rll:SUl.TS SUMMAR Y (Cont'd)
1099HBWW230
9910408-06A
Cl021913
10/20/99 11: 25
00:00:00
10/21/99 22:09:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
1. 04
3.79
3.7i
0.305
0.0469
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0.0744
0.0Ql9
0.0493
0. 0778
0.0836
0.0527
0.0819
1099HBWW234
9910408-04A
Cl021911
10/20/99 10:40
00:00:00
10/21/99 21:13:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0600
ND
ND
ND
ND
DL
1. 04
3.79
3. 71
0.305
0. 0469
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0.0744
0.0619
0. 04 93
0. 0778
0.0836
0.0527
0.0819
Work Order # 9910408
Page 11._
TRIP BLANK
9910408-08A
Cl021907
10/20/99
00:00:00
10/21/99 19:19:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
1. 04
3.79
3. 71
0.305
0. 0469
0.0507
0.0566
0.0990
0.0619
0.0756
0.0962
0.179
0.0655
0.0744
0.0619
0. 04 93
0.0778
0.0836
0.0527
0.0819
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1099HBWW226
9910408-03A
C1021910
10/20/99 10:20
00:00:00
10/21/99 20:44:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0.0454
0.0556
0.0651
0.270
0.0588
0. 04 08
0.0819
0.0407
0.0422
• RBSULTS S UM M AR Y (Cont'd)
1099HBWW230
9910408-06A
C1021913
10/20/99 11: 25
00:00:00
10/21/99 22:09:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.265
ND
0 .133
0.304
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0.0454
0.0556
0.0651
0.270
0.0588
0.0408
0.0819
0. 04 07
0.0422
1099HBWW234
9910408-04A
Cl021911
10/20/99 10:40
00:00:00
10/21/99 21:13:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0.0454
0.0556
0.0651
0.270
0.0588
0.0408
0.0819
o·. 0407
0.0422
Work Order # 9910408
Page lL
TRIP BLANK
9910408-08A
Cl021907
10/20/99
00:00:00
10/21/99 19:19:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0600
0.0586
0.109
0.0693
0.0581
0.0733
0.266
0.0665
0.0782
0.0300
0.264
0.0454
0.0556
0.0651
0.270
0.0588
0.0408
0.0819
0.0407
0. 0422
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
1099HBWW226
9910408-03A
Cl021910
10/20/99 10:20
00:00:00
10/21/99 20:44:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0.0712
0.0375
0. 0430
0. 0412
0.0563
0.0763
0.144
0.0436
0.0815
0.0662
0. 0916
0.0512
0. 0775
0.0607
0.0576
0 .408
0.0558
• RESULTS S 0 MM ARY (Cont'd)
1099HBWW230
9910408-06A
Cl021913
10/20/99 11:25
00:00:00
10/21/99 22:09:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0.0712
0.0375
0.0430
0. 0412
0.0563
0.0763
0.144
0.0436
0.0815
0.0662
0. 0916
0.0512
0. 0775
0.0607
0.0576
0 .408
0.0558
1099HBWW234
9910408-04A
Cl0219ll
10/20/99 10:40
00:00:00
10/21/99 21:13:00
1
Water
u;i/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0527
0.0591
0.0903
0. 0712
0.0375
0.0430
0. 0412
0.0563
0.0763
0 .144
0. 0436
0.0815
0.0662
0.0916
0.0512
0. 0775
0.0607
0.0576
0.408
0.0558
Work Order U 9910408
Page 11_
TRIP BLANK
9910408-08A
Cl021907
10/20/99
00:00:00
10/21/99 19:19:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.120 B
ND
ND
ND
DL
0.0527
0.0591
0.0903
0. 0712
0.0375
0.0430
0.0412
0.0563
0.0763
0.144
0. 0436
0.0815
0.0662
0. 0916
0.0512
0.0775
0.0607
0.0576
0. 408
0.0558
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
1099HBWW226
9910408-03A
C1021910
10/20/99 10:20
00:00:00
10/21/99 20:44:00
1
Water
ug/L
rece'ived
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0. 0728
0.0785
0.0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0. 0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
• RESULTS S UM MARY (Cont'd)
1099HBWW230
9910408-06A
C1021913
10/20/99 11:25
00:00:00
10/21/99 22:09:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
0.309
ND
ND
ND
ND
0.921
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0. 0728
0.0785
0. 0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0.0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
1099HBWW234
9910408-04A
C1021911
10/20/99 10:40
00:00:00
10/21/99 21:13:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0.0728
0. 0785
0.0591
0.527
0. 0645
0.0682
0.0512
0.0631
0.0576
0.0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
Work Order # 9910408
Page ll_
TRIP BLANK
9910408-08A
Cl021907
10/20/99
00:00:00
10/21/99 19:19:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
0.0974
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0500
0. 0728
0. 0785
0.0591
0.527
0.0645
0.0682
0.0512
0.0631
0.0576
0.0499
0.0632
0.0795
0.0599
0.0590
0.0668
0.0512
0.0957
0.112
0.0732
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
1099HBWW226
9910408-03A
Cl021910
10/20/99 10:20
00:00:00
10/21/99 20:44:00
1
Water
ug/L
received
Cone.
Recovery
%
98
103
102
DL
• RBSULTS S UM MARY (Cont'd)
1099HBWW230
9910408-0GA
C1021913
10/20/99 11: 25
00:00:00
10/21/99 22:09:00
l
Water
ug/L
received
Cone.
Recovery
%
97
104
100
DL
1099HBWW234
9910408-04A
C1021911
10/20/99 10:40
00:00:00
10/21/99 21:13:00
1
Water
ug/L
received
Cone. DL
Recovery
%
97
104
101
Work Order # 9910408
Page 12.._
TRIP BLANK
9910408-08A
Cl021907
10/20/99
00:00:00
10/21/99 19:19:00
1
Water
ug/L
received
Cone. DL
Recovery
%
98
99
101
•
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDC991018000000
Calibration Date ~l~O-/wl~8-/~9~9~~~~-
Sequence/Analysis Time
1 10/21/99 16:28:00
2 10/21/99 16:57:00
3 10/21/99 17:26:00
4 10/21/99 17:26:00
5 10/21/99 17:54:00
6 10/21/99 18:23:00
7 10/21/99 18:51:00
8 10/21/99 19:19:00
9 10/21/99 19:48:00
10 10/21/99 20:16:00
11 10/21/99 20:44:00
12 10/21/99 21:13:00
13 10/21/99 21:41:00
14 10/21/99 22:09:00
15 10/21/99 22:38:00
16 10/21/99 23:06:00
17 10/21/99 23:35:00
18 10/22/99 00:03:00
19 10/22/99 00:31:00
20 10/22/99 01:00:00
21 10/22/99 01:28:00
22 10/22/99 01:56:00
23 10/22/99 02:25:00
24 10/22/99 02:53:00
25 10/22/99 03:23:00
26 10/22/99 03:53:00
27 10/22/99 04:23:00
28 10/22/99 04:53:00
• ANALYSIS BATCH SUMMARY
Analysis Batch# MSMSDC91021172601
Analysis Start Date/Time 10/21/99 17:26:00
Analysis Stop Date/Time 10/22/99 04:53:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
SB Blank, System
BFB GC/MS tune files
VSTDCAL Continuing Calibration
LCS994409 Lab Control Sample
Work Order # 9910408
Page .!..§._
Instrument MSDC
Analyst !':1!IB.
Reviewer -~T_L_A~~~~~~~~-
Analysis File #
Cl021901
C1021902
Cl021903
Verification C1021903
C1021904
LCSD994410 Lab Control Sample Duplicate Cl021905
BLK992783 Blank, Method Cl02l906
TRIP BLANK 9910408-0SA Sample Cl021907
1099HBWW224 9910408-0lA Sample C1021908
1099HBWW225 9910408-02A Sample Cl021909
1099HBWW226 9910408-03A Sample Cl021910
1099HBWW234 9910408-04A Sample Cl021911
1099HBWW222 9910408-05A Sample Cl021912
1099HBWW230 9910408-06A Sample Cl021913
1099HBWW220 9910408-07A Sample C1021914
9910310-06A Sample C1021915
9910310-12A Matrix Spike Cl021916
9910310-13A Matrix Spike Duplicate Cl0219l7
9910310-07A Sample Cl021918
9910310-08A Sample Cl021919
9910310-09A Sample Cl021920
9910310-llA Sample C1021921
9910393-04A Sample Cl021922
9910393-0SA Sample C1021923
9910310-lOA Sample Cl021924
9910393-0lA Sample C1021925
9910393-02A Sample C1021926
9910393-03A Sample C1021927
•
I
• 11/03/99 13:58:32
Method Volatile Organics SW8260B
Lab Sample ID
File ID
Project Sample
ID/Description
Specification#
Analyte
• ANALYTICAL PROTOCOL SUMMARY
COMMBNTS/NARRATIVB
Flag Comment/Narrative Corrective Action
• Work Order # 9910408
Page 12.._