6401_NashCoMSWLF_GWMR_DIN27997_20161107

11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]

Explanatory Text for Notification Table
Nash County Municipal Solid Waste Landfill, Permit # 64-01
Nashville, Nash County, NC
November 2016 Assessment Monitoring

The results of the November 2016 assessment monitoring are generally consistent with the
results from the previous assessment monitoring results. The concentrations of VOCs in
groundwater at down gradient monitoring wells MW-7s and MW-8s have shown significant
reductions since the inception of assessment monitoring and none were detected in samples
collected from those wells in November 2016. The concentrations of VOCs reported in the
groundwater samples collected from down gradient Type III monitoring wells MW-7d and MW-8d
in November 2016 showed slight increases compared with recent sampling results. However,
the increase in concentrations may be associated with the extended period of dry weather
conditions leading up to the November 2016 monitoring, which tend to promote increased
concentrations of monitoring constituents. It is anticipated that the concentrations of VOCs in
groundwater at MW-7d and MW-8d will show decreases when a more normal rainfall pattern is
re-established.

Cadmium was reported at a concentration exceeding the 15A NCAC 2L groundwater quality
standard (2 µg/L) in the groundwater sample collected from monitoring well MW-4 (2.60 µg/L).
Cobalt was reported at concentrations exceeding the Groundwater Interim Maximum Allowable
Concentration (1 µg/L) effective October 1, 2010 in the groundwater samples collected from
monitoring wells MW-2R (1.7 µg/L), MW-3 (59 µg/L), and MW-4 (51 µg/L). Vanadium was
reported at an estimated concentration exceeding the October 1, 2010 IMAC (0.3 µg/L) in the
groundwater sample collected from monitoring well MW-7s (3.2 µg/L). Inasmuch as vanadium
has been historically reported at background monitoring well MW-1 at similar concentrations to
that reported at MW-7s (see Table 4), it is concluded that the concentrations of vanadium
measured in groundwater at the site are naturally occurring. Zinc was reported at a
concentration exceeding the 15A NCAC 2L groundwater quality standard (1,000 µg/L) in the
groundwater sample collected from monitoring well MW-7s (1,400 µg/L). The elevated
concentration of zinc reported in groundwater at GW-7s for the November 2016 monitoring
event is attributed to the elevated turbidity of the groundwater sample collected from that
location (24.5 NTUs). None of the other metals detected in the groundwater or surface water
samples collected from the site November 2016 were reported at concentrations that exceed
the applicable water quality standards.

– 2 – December 9, 2016
11112 BRANDING IRON PLACE, WENDELL, NC 27591 919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
Pig Basket Creek is classified as Class C surface water by the NCDENR. No metals were
reported in the surface water samples collected from the site at concentrations that exceed
applicable surface water quality standards for Class C surface waters.

Based on the results of the November 2016 assessment monitoring event, it is recommended
that semi-annual monitoring of groundwater and surface water be continued without
modification. The results of the semi-annual monitoring will be evaluated for any changes in
conditions that would indicate a sustained increase in dissolved contaminant concentrations and
the likelihood that the groundwater quality standards will be consistently exceeded at the
compliance boundary. If such conditions arise, Nash County will propose additional assessment
and/or corrective actions to address the situation.

11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]

December 9, 2016

Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
P. O. Box 27687
Raleigh, NC 27611-7687

RE: Report of Results
Appendix II Assessment Monitoring: November 2016
Nash County Municipal Solid Waste Landfill (Closed)
Nashville, Nash County, NC
Permit # 64-01

Dear Ms. Drummond:

This report presents the results of Appendix II assessment monitoring conducted at the landfill
site referenced above (Figure 1) in November 2016 in accordance with North Carolina Solid
Waste Management Rule 15A NCAC 13B .1634 (Rule .1634). The assessment monitoring was
a continuation of monitoring initiated in May 2007 during which four Appendix I constituents
(methylene chloride, trichloroethene, tetrachloroethene and vinyl chloride) were detected in
groundwater at the site at concentrations in excess of the 15A NCAC 2L .0202 Class GA
groundwater quality standards (2L standards). In a letter dated February 17, 2015 to Nash
County, the NCDEQ granted a request by the county to reduce the frequency of monitoring
groundwater for pesticides, fluoride, and phenol based on a lack of detection of these
constituents in groundwater since 2010. The NCDEQ granted a reduction in the monitoring
frequency for pesticides, fluoride, and phenol from semiannual to every five years.

The scope of work performed during November 2016 included sampling and laboratory analysis
of groundwater from 10 groundwater monitoring wells and surface water samples from two
surface water sampling locations. The groundwater and surface water samples were collected
in accordance with the NCDEQ, Division of Waste Management (DWM), Solid Waste Section
(SWS) Groundwater Monitoring Guidance Document and the facility Water Quality Monitoring
Plan. The groundwater and surface water sampling and data collection methods, as well as the
results of field and laboratory testing of the groundwater and surface water samples, are
presented in the following sections.

– 2 – December 9, 2016
11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]

1.0 GROUNDWATER GAUGING AND WATER SAMPLE COLLECTION
Groundwater levels were gauged in the site monitoring wells on November 7, 2016 as part of
assessment monitoring. Depths to groundwater were measured using an electronic water-level
meter that was thoroughly decontaminated between wells with a non-phosphate soap and water
wash followed in order by multiple rinses with distilled water, an isopropyl alcohol rinse, and
multiple distilled water rinses. Depth-to-water measurements were made after the wells were
opened for sufficient periods of time to allow water levels to equilibrate with atmospheric
pressure. The locations of the site monitoring wells are depicted in Figure 2. Groundwater
elevation data collected at the monitoring wells on November 7, 2016 are presented in Table 1.

Groundwater and surface water samples were collected for laboratory analysis on November 7
and 8, 2016 to monitor water quality at the site. The samples were analyzed for Appendix I
volatile organic compounds (VOCs) by SW 846 Method 8260B, and Appendix I metals plus
mercury by the EPA 6000/7000 Series Methods. The groundwater and surface water samples
were collected and handled in accordance with the sampling protocols included in the site Water
Quality Monitoring Plan as well as the SWS Groundwater Monitoring Guidance Document. It is
noted that monitoring well MW-1 serves as the upgradient, natural background well for the
facility, and monitoring wells MW-2R through MW-6, MW-7s, MW-7d, MW-8s and MW-8d serve
as the downgradient monitoring wells. It is further noted that MW-6, MW-7d and MW-8d are
deep Type III groundwater monitoring wells that monitor the deeper zone of the shallow aquifer
at the site. All reusable sampling equipment was properly decontaminated between sampling
locations with a non-phosphate soap and water wash, followed by multiple rinses with distilled
water. New disposable nitrile or latex gloves were worn during all sampling activities.
Disposable sampling equipment/material was discarded after each use.

Prior to groundwater sampling, all monitoring wells were purged of stagnant water using pre-
cleaned Teflon-lined disposable polyethylene tubing connected to a peristaltic pump under low
flow (≤ 200 ml/min) conditions. During purging, measurements were made in the field of the pH,
temperature, specific conductance and turbidity of the groundwater collected from the
monitoring wells, in accordance with SWS requirements. The results of the field analyses for
these parameters are presented in Table 1. Copies of Groundwater Sampling Forms containing
pertinent information recorded in the field during purging and sampling at each groundwater
monitoring well are presented in Appendix A.

The results of the field-measured water-quality parameters indicate that the values measured in
groundwater collected from the site monitoring wells were generally within applicable
stabilization criteria (see Groundwater Sampling Forms), except for elevated turbidity at
monitoring wells MW-7s, and MW-8s. Groundwater at the site is slightly acidic based on the pH
values measured in the field (4.85 to 6.07). Specific conductance values ranged from 38 (MW-
– 3 – December 9, 2016
11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
1) to 214 (MW-4) µS/cm in groundwater at the monitoring wells. Turbidity values ranged from
2.1 (MW-1) to 49.3 (MW-7s) NTUs. After field parameters had stabilized over three consecutive
recording intervals, groundwater samples were collected using the same tubing that was used
to purge the well. The samples were pumped directly into laboratory prepared containers,
which were then placed into ice-filled coolers and shipped under proper chain-of-custody to
Prism Laboratories, Inc. (Prism) for analysis.

Surface water samples were collected from sampling locations SW-1 and SW-2 (Figure 2).
SW-1 is located approximately 50-feet east of the MSW Landfill along a tributary of Pig Basket
Creek. SW-2 is located down gradient and due south of the MSW Landfill along the same
tributary of Pig Basket Creek. New disposable nitrile or latex gloves were worn during all
sampling activities. All surface water samples were collected in accordance with the protocol
presented in the SWS Groundwater Monitoring Guidance Document. Following collection, the
samples were placed into ice-filled coolers and shipped under proper chain-of-custody to Prism
for analysis.

2.0 RESULTS OF GROUNDWATER AND SURFACE WATER SAMPLING AND
ANALYSIS
Groundwater flow direction, average hydraulic gradient, and average interstitial flow velocity
were derived from water-level measurements recorded during the sampling event. A water-
table elevation contour map derived from the groundwater elevation measurements recorded on
November 7, 2016 is presented as Figure 3. The water-table elevation contours in Figure 3
indicate that the direction of shallow groundwater flow is generally to the southwest with an
average hydraulic gradient of approximately 0.014 ft./ft. This is consistent with the general flow
direction observed during previous monitoring events.

The hydraulic gradient in the vicinity of each well was derived by dividing the elevation
difference between water table elevations measured at the monitoring wells and proximal water-
table elevation contour lines, by the perpendicular horizontal distance between the wells and
contours (Figure 3 and Table 2). Results of in-situ slug testing performed by others between
February 4, 1999 and October 1, 1999, as well as the results of slug tests conducted in
November 2007, indicate hydraulic conductivity values in the shallow surficial aquifer ranging
from 6.0 x 10-5 cm/s to 1.3 x 10-3 cm/s (approximately 0.17 ft/day to 3.7 ft/day). Using the
horizontal hydraulic gradient measurements, the individual estimates of hydraulic conductivity,
and an assumed effective porosity of 0.15, the range of average interstitial groundwater flow
velocities for the shallow surficial aquifer was calculated using the following formula:

vx = (K/ne) dl
dh×
Where:
– 4 – December 9, 2016
11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
vx = average interstitial groundwater flow velocity
K = hydraulic conductivity
ne = effective porosity
dh/dl = horizontal hydraulic gradient

Average linear flow velocities are estimated to range between approximately 0.016 to 0.47
feet/day. Table 2 summarizes the data used to calculate the average interstitial groundwater
flow velocity in the vicinity of each Type II monitoring well.

Summarized results of laboratory analyses for groundwater and surface water samples
collected from the site on November 7 and 8, 2016 are presented in Table 3. Historical results
of Appendix II assessment monitoring conducted at the site since May 2007 are presented in
Table 4. Copies of the original laboratory reports are included in Appendix B.

The laboratory analytical results for the November 2016 sampling event indicate that benzene
(1.6 µg/L) was reported at a concentration in excess of the 15A NCAC 2L groundwater quality
standard at monitoring well MW-6. In addition, benzene (1.6 ug/L), 1,1-dichloroethane (6.1
ug/L), methylene chloride (9.5 ug/L), tetrachloroethene (2.0 µg/L), and trichloroethene (4.4 ug/L)
were reported at concentrations in excess of the corresponding 15A NCAC 2L groundwater
quality standards at monitoring well MW-7d.

Various other VOCs, including chlorobenzene, 1,4-dichlorobenzene, cis-1,2-dichloroethene,
ethylbenzene, tetrahydrofuran, and total xylenes were reported in groundwater samples
collected from several monitoring wells at concentrations well below the applicable 15A NCAC
2L groundwater quality standards. No VOCs were reported in surface water samples SW-1 and
SW-2.

The results of the metals analyses of the groundwater and surface water samples indicate that
barium, beryllium, cadmium, chromium, cobalt, lead, nickel, silver, thallium, and zinc were
reported in all of the samples. Antimony, arsenic, copper, mercury, and vanadium were reported
in 1 to 11 of the samples tested. Selenium was not detected in any of the samples tested.
Cadmium was reported at a concentration exceeding the 15A NCAC 2L groundwater quality
standard (2 µg/L) in the groundwater sample collected from monitoring well MW-4 (2.60 µg/L).
Cobalt was reported at concentrations exceeding the Groundwater Interim Maximum Allowable
Concentration (1 µg/L) effective October 1, 2010 in the groundwater samples collected from
monitoring wells MW-2R (1.7 µg/L), MW-3 (59 µg/L), and MW-4 (51 µg/L). Vanadium was
reported at an estimated concentration exceeding the October 1, 2010 IMAC (0.3 µg/L) in the
groundwater sample collected from monitoring well MW-7s (3.2 µg/L). Inasmuch as vanadium
has been historically reported at background monitoring well MW-1 at similar concentrations to
that reported at MW-7s (see Table 4), it is concluded that the concentrations of vanadium
– 5 – December 9, 2016
11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
measured in groundwater at the site are naturally occurring. Zinc was reported at a
concentration exceeding the 15A NCAC 2L groundwater quality standard (1,000 µg/L) in the
groundwater sample collected from monitoring well MW-7s (1,400 µg/L). The elevated
concentration of zinc reported in groundwater at GW-7s for the November 2016 monitoring
event is attributed to the elevated turbidity of the groundwater sample collected from that
location (24.5 NTUs). None of the other metals detected in the groundwater or surface water
samples collected from the site November 2016 were reported at concentrations that exceed
the applicable water quality standards.

Pig Basket Creek is classified as Class C surface water by the NCDENR. No metals were
reported in the surface water samples collected from the site at concentrations that exceed
applicable surface water quality standards for Class C surface waters.

3.0 CONCLUSIONS AND RECOMMENDATIONS
The results of the November 2016 assessment monitoring are generally consistent with the
results from the previous assessment monitoring results. The concentrations of VOCs in
groundwater at down gradient monitoring wells MW-7s and MW-8s have shown significant
reductions since the inception of assessment monitoring and none were detected in samples
collected from those wells in November 2016. The concentrations of VOCs reported in the
groundwater samples collected from down gradient Type III monitoring wells MW-7d and MW-8d
in November 2016 showed slight increases compared with recent sampling results. However,
the increase in concentrations may be associated with the extended period of dry weather
conditions leading up to the November 2016 monitoring, which tend to promote increased
concentrations of monitoring constituents. It is anticipated that the concentrations of VOCs in
groundwater at MW-7d and MW-8d will show decreases when a more normal rainfall pattern is
re-established.

Cadmium was reported at a concentration exceeding the 15A NCAC 2L groundwater quality
standard (2 µg/L) in the groundwater sample collected from monitoring well MW-4 (2.60 µg/L).
Cobalt was reported at concentrations exceeding the Groundwater Interim Maximum Allowable
Concentration (1 µg/L) effective October 1, 2010 in the groundwater samples collected from
monitoring wells MW-2R (1.7 µg/L), MW-3 (59 µg/L), and MW-4 (51 µg/L). Vanadium was
reported at an estimated concentration exceeding the October 1, 2010 IMAC (0.3 µg/L) in the
groundwater sample collected from monitoring well MW-7s (3.2 µg/L). Inasmuch as vanadium
has been historically reported at background monitoring well MW-1 at similar concentrations to
that reported at MW-7s (see Table 4), it is concluded that the concentrations of vanadium
measured in groundwater at the site are naturally occurring. Zinc was reported at a
concentration exceeding the 15A NCAC 2L groundwater quality standard (1,000 µg/L) in the
groundwater sample collected from monitoring well MW-7s (1,400 µg/L). The elevated
concentration of zinc reported in groundwater at GW-7s for the November 2016 monitoring
– 6 – December 9, 2016
11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
event is attributed to the elevated turbidity of the groundwater sample collected from that
location (24.5 NTUs). None of the other metals detected in the groundwater or surface water
samples collected from the site November 2016 were reported at concentrations that exceed
the applicable water quality standards.

Pig Basket Creek is classified as Class C surface water by the NCDENR. No metals were
reported in the surface water samples collected from the site at concentrations that exceed
applicable surface water quality standards for Class C surface waters.

Based on the results of the November 2016 assessment monitoring event, it is recommended
that semi-annual monitoring of groundwater and surface water be continued without
modification. The results of the semi-annual monitoring will be evaluated for any changes in
conditions that would indicate a sustained increase in dissolved contaminant concentrations and
the likelihood that the groundwater quality standards will be consistently exceeded at the
compliance boundary. If such conditions arise, Nash County will propose additional assessment
and/or corrective actions to address the situation. The next semi-annual assessment monitoring
event will be conducted in May 2017.

If you have any questions or require further assistance regarding this report, please call me at
919-995-0363.

Sincerely,
Brian S. Boutin, P.G.
Consulting Geologist

Cc: William W. Hill, Jr., M.P.H., Health Director, Nash County Health Department
Ben Barnes, Solid Waste Manager, Nash County Solid Waste Department
Vance Moore, Garrett and Moore, Inc.
Craig Fortner, Garrett and Moore, Inc.
Garrett and Moore, Inc.
Engineering Consulting Services
1428 Aversboro Rd., Suite D, Garner, NC 27529
Tel: [phone] Fax: [phone]
Drawn by:Reviewed by:Drawing #:
Drawing Date:1
SITE LOCATION MAP
Nash County Municipal Solid Waste Landfill
SR 1411 (Duke Rd.)
Nashville, Nash County, North Carolina
Source: USGS 7.5’ Topographic Quadrangle Series
Castalia, North Carolina 1993
Figure No.Project #:
Scale:USGS USGS
1:24,000 7/19/07
NCMSW0707
N
SCALE
020001000 1000 2000
1
9
1
19
3
1
9
3
195
1
9
5
19
7
1
9
7
199
1
9
9
201
2
0
1
203
2
0
3
20
5
20
7
20
9
(216.08)
(193.87)
(193.64)
(193.06)
(193.58)
(191.72)
(190.26)
Latitude
(deg. dec min.)
Longitude
(deg. dec min.)
MW-1 44.5 2.0 36º 3.73366'77º 59.58531'34.5 - 44.5 27.88 243.96 216.08 15.9 5.04 38 2.1
MW-2R 23.0 2.0 36º 3.58734'77º 59.92608'13.0 - 23.0 9.94 203.81 193.87 19.7 4.85 47 2.2
MW-3 15.0 2.0 36º 3.49902''77º 59.81363'5.0 - 15.0 11.37 205.01 193.64 14.1 5.85 166 6.9
MW-4 25.0 2.0 36º 3.37664'77º 59.67142'5.0 - 25.0 8.75 201.81 193.06 18.4 5.84 214 6.2
MW-5 29.0 2.0 36º 3.65441'77º 59.9778''9.0 - 29.0 13.57 207.15 193.58 19.0 5.46 52 5.1
MW-6 50.0 2.0 36º 3.46888'77º 59.81451'40.0 - 50.0 12.32 206.07 193.75 15.2 5.73 86 2.8
MW-7s 20.0 2.0 36º 3.58989'77º 59.93535'5.0 - 20.0 8.58 200.30 191.72 19.7 6.07 60 49.3
MW-7d 42.5 2.0 36º 3.57918'77º 59.95242'37.5 - 42.5 8.15 199.94 191.79 19.4 5.66 57 2.3
MW-8s 20.0 2.0 36º 3.46856'77º 59.81381'5.0 - 20.0 6.54 196.80 190.26 17.8 5.85 50 25.1
MW-8d 39.0 2.0 36º 3.45172'77º 59.84358'34.0 - 39.0 6.42 196.95 190.53 17.7 5.98 59 4.4
Notes:
MSL = Mean Sea Level
BTOC = Below Top of Casing
Monitoring well construction data for MW-1 through MW-6 taken from April-June 2006 Sampling Event Monitoring Report prepared by Withers & Ravenel.
BGS = Below Ground Surface
NM = Not Measured
November 7 and 8, 2016
pH S.C.
umhos/cm
S.C. = Specific Conductance
Permit # 64-01
Monitoring Well and Groundwater Data
Table 1
Water Quality Assessment Monitoring
Nash County Municipal Solid Waste Landfill
Nashville, Nash County, North Carolina
Well
Identity
ntu = Nephelometric Turbidity Units
Temp. Co
Elevation
Top of PVC
Well Casing
(Feet MSL)
Well Diameter
(Inches)
Field Parameters
Turbidity
(ntu)
Screen
Interval
(Feet BGS)
Groundwater
Elevation
(Feet MSL)
Depth to
Groundwater
(Feet BTOC)
Well Depth
(Feet BGS)
Water Table Hydraulic Effective Average Average
Well Elevation Conductivity Porosity Hydraulic Linear Flow
Identity (ft MSL)(ft/day)Gradient Velocity
(ft/ft)(ft/day)
MW-1 216.08 0.17 0.15 0.014 0.016
MW-2R 193.87 3.70 0.15 0.019 0.47
MW-3 193.64 0.52 0.15 0.018 0.062
MW-4 193.06 1.12 0.15 0.010 0.078
MW-5 193.58 0.47 0.15 0.012 0.037
MW-7s 191.72 2.04 0.15 0.006 0.076
MW-8s 190.26 0.80 0.15 0.017 0.091
Notes:1) ft MSL = feet above mean sea level.
2) Hydraulic Conductivity from slug testing performed by G.N. Richardson and Associates, Inc.
and Brian S. Boutin, P.G.
3) Effective porosity value approximated based on published values for similar materials.
4) Average gradient obtained by dividing water-table elevation difference by horizontal distance
between contour lines in the vicinity of each well (See Figure 3).
5) Average Linear Velocity calculated by the following formula:
Vx = (K/ne)*(dh/dl)
Where:
Nash County Municipal Solid Waste Landfill
Table 2
Groundwater Flow Data
Water-Quality Assessment Monitoring
November 7 and 8, 2016
Nashville, Nash County, North Carolina
Permit # 64-01
Vx = average linear flow velocity (ft/day)
K = hydraulic conductivity (ft/day)
dh/dl = average hydraulic gradient (ft/ft)
ne = effective porosity (unitless)
VOLATILE ORGANIC CONSTITUENTS GWP Std NCAC 2L STD
SW 846 8260 (µg/L)(ug/L)(ug/L)
Acetone ND ND ND ND ND ND ND ND ND ND ND ND NE 6000
Benzene ND ND ND ND ND 1.6 ND 1.6 ND ND ND ND NE 1
Bromomethane ND ND ND ND ND ND ND ND ND ND ND ND NE 10
Chlorobenzene ND ND ND ND ND 3.3 ND ND ND ND ND ND NE 50
Chloroethane (Ethyl Chloride)ND ND ND ND ND ND ND ND ND ND ND ND NE 3000
Chloroform (Trichloromethane)ND ND ND ND ND ND ND ND ND ND ND ND NE 70
Chloromethane ND ND ND ND ND ND ND ND ND ND ND ND NE 3
1,4-Dichlorobenzene ND ND ND ND ND 3 ND 0.91 ND ND ND ND NE 6
Dichlorodifluoromethane (Freon-12; Halon)ND ND ND ND ND ND ND ND ND ND ND ND NE 1000
1,1-Dichloroethane ND ND ND ND ND 1.3 ND 6.1 ND 3.4 ND ND NE 6
1,1-Dichloroethene (Vinylidene Chloride)ND ND ND ND ND ND ND ND ND ND ND ND NE 7
1,2-Dichloroethene (Cis and Trans isomers)ND ND ND ND ND 3.3 ND 9 ND 3 ND ND 60 60
Ethylbenzene ND ND 0.98 ND ND ND ND ND ND ND ND ND NE 600
Methylene Chloride (Dichloromethane)ND ND ND ND ND 1.2 ND 9.5 ND 4.4 ND ND NE 5
Methyl Ethyl Ketone (2-butanone)ND ND ND ND ND ND ND ND ND ND ND ND NE 4000
Styrene ND ND ND ND ND ND ND ND ND ND ND ND NE 70
Tetrachloroethene (Tetrachloroethylene), (PCE)ND ND ND ND ND ND ND 2 ND ND ND ND NE 0.7
Tetrahydrofuran ND ND 60 ND ND ND ND ND ND ND ND ND NE NE
Toluene ND ND ND ND ND ND ND ND ND ND ND ND NE 600
1,1,1-Trichloroethane (Methylchloroform)ND ND ND ND ND ND ND ND ND ND ND ND NE 200
Trichloroethene (Trichloroethylene), (TCE)ND ND ND ND ND 0.56 ND 4.4 ND 2 ND ND NE 3
Trichlorofluoromethane (CFC-11) ND ND ND ND ND ND ND ND ND ND ND ND NE 2000
Vinyl Chloride ND ND ND ND ND ND ND ND ND ND ND ND NE 0.03
Total Xylenes ND ND ND ND ND 1.2 ND ND ND ND ND ND NE 500
PESTICIDES GWP Std NCAC 2L STD
EPA 8081 (µg/L)(ug/L)(ug/L)
alpha-BHC NA NA NA NA NA NA NA NA NA NA NA NA 0.006 NE
beta-BHC NA NA NA NA NA NA NA NA NA NA NA NA 0.019 NE
delta-BHC NA NA NA NA NA NA NA NA NA NA NA NA 0.019 NE
gamma-BHC NA NA NA NA NA NA NA NA NA NA NA NA NE 0.03
Aldrin NA NA NA NA NA NA NA NA NA NA NA NA 0.002 NE
Endrin (total)NA NA NA NA NA NA NA NA NA NA NA NA NE 2
Methoxychlor NA NA NA NA NA NA NA NA NA NA NA NA NE 40
4,4'-DDD NA NA NA NA NA NA NA NA NA NA NA NA NE 0.1
4,4'-DDT NA NA NA NA NA NA NA NA NA NA NA NA NE 0.1
MISCELLANEOUS GWP STD NCAC 2L STD
(µg/L)(ug/L)(ug/L)
Fluoride NA NA NA NA NA NA NA NA NA NA NA NA NE 2000
Phenol NA NA NA NA NA NA NA NA NA NA NA NA NE 30
METALS GWP Std NCAC 2L STD
(in ug/L)(ug/L)(ug/L)
Antimony ND 0.089 J 0.19 J ND 0.19 J 0.095 J 0.15 J 0.23 J 0.091 J 0.071 J 0.25 J 0.45 J 1 1
Arsenic ND ND 0.57 J 0.31 J ND ND 0.88 J 0.49 J ND ND 0.44 J 0.52 J NE 10
Barium 24 20 55 150 6.3 57 10 3.9 J 8.3 5.4 28 26 NE 700
Beryllium 0.060 J 0.35 J 0.091 J 0.18 J 0.30 J 0.051 J 0.21 J 0.054 J 0.062 J ND 0.081 J 0.092 J 4 4
Cadmium 0.091 J 0.92 J 0.10 J 2.60 0.11 J 0.12 J 0.63 J 0.42 J 0.38 J 0.22 J 0.065 J 0.073 J NE 2
Chromium 1.4 JB 1.5 JB 0.97 JB 1.6 JB 1.3 JB 1.3 JB 2.6 JB 1.1 JB 3.4 JB 1.3 JB 1.2 JB 1.2 JB NE 10
Cobalt 0.55 J 1.7 59 51 0.18 J 0.26 J 0.54 J 0.22 J 0.41 J 0.037 J 0.70 J 0.38 J NE 1
Copper 0.59 JB 1.7 J 1.6 JB 1.9 JB 1.5 JB 1.3 JB 6.9 0.48 J 1.5 JB ND 0.68 JB 0.90 JB NE 1000
Lead 0.17 JB 0.33 J 0.48 JB 0.95 JB 0.54 JB 2.1 B 1.7 JB 0.33 J 1.1 JB 0.14 JB 0.40 JB 0.40 JB NE 15
Mercury ND 0.097 J ND ND ND ND ND 0.050 J ND ND ND ND NE 1
Nickel 2.2 4.9 2.8 3.50 1.1 J 1.5 J 4.6 1.4 J 1.4 J 0.56 J 0.82 J 0.75 J NE 100
Selenium ND ND ND ND ND ND ND ND ND ND ND ND NE 20
Silver 0.012 J 0.13 J 0.034 J 0.036 J 0.041 J 0.040 J 0.041 J 0.055 J 0.048 J 0.017 J 0.046 J 0.058 J NE 20
Thallium 0.056 J 0.24 J 0.074 J 0.033 J 0.045 J 0.037 J 0.051 J 0.23 J 0.031 J 0.022 J 0.055 J 0.069 J 0.28 0.2
Vanadium ND ND ND ND ND ND 3.2 J ND ND ND ND ND 0.3 0.3
Zinc 22 44 26 42 23 24 1400 19 24 18 18 19 NE 1000
Notes:
Values in boldface exceed the corresponding 15A NCAC 2L .0202 groundwater quality standard for Class GA groundwater.GWP Std = Solid Waste Section Groundwater Protection Standard
NCAC 2L STD = North Carolina Groundwater Standard established in Title 15A of North Carolina Administrative Code Subchapter 2L
J = Estimated value above laboratory method detection limit and below SWSL or reporting limit.
B = Analyte found in associated field and/or laboratory blank.NA = Not Analyzed NE = Not Established
NS = Not Sampled, No sample exists for this sampling period ND = None detected above laboratory method detection limit.
Table 3
MW-1
Nashville, Nash County, North Carolina
MW-5
Nash County Municipal Solid Waste Landfill
MW-7d
Summarized Laboratory Analytical Results for Groundwater and Surface Water Samples
MW-8s
Permit # 64-01
November 7 and 8, 2016Water Quality Assessment Monitoring
MW-8d SW-2SW-1MW-6 MW-7sMW-2R MW-4MW-3
Page 1 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
MW-1 Antimony 1 NS ND ND ND ND ND ND 0.16 J 0.63 J ND ND ND ND ND ND ND ND ND ND ND
Arsenic 10 NS ND ND 2.86 J ND ND ND ND ND 0.26 J 0.24 J 0.40 J 0.38 J ND ND ND ND ND ND ND
Barium 700 NS 29.8 JB 43.2 JB 28.0 JB 17.7 J 28.4 JB 24 19 22 20 25 20 21 21 23 22 20 25 21 24
Beryllium 4 NS 7.55 JB 1.67 B ND ND ND ND ND ND ND ND ND ND 0.055 J 0.055 J ND 0.082 J 0.14 J 0.055 J 0.060 JCadmium2NSNDNDNDNDNDNDNDNDNDNDND0.11 J 0.044 J 0.048 J ND 0.062 J 0.11 J 0.80 J 0.091 J
Chromium 10 NS 2.84 JB 6.26 JB 4.89 JB 3.49 JB 3.51 J 1.2 J 1.4 1.6 2.7 B 0.20 J 3.2 0.26 J 0.87 J ND 0.93 J ND 3.5 B ND 1.4 JB
Cobalt 1 NS ND ND ND ND 2.05 J 0.64 J 0.72 J 0.90 J 0.66 J 1.1 0.81 J 0.61 J 0.60 J 1.1 0.70 J 0.66 J 1.2 0.62 J 0.55 J
Copper 1000 NS 4.27 JB 9.02 JB 4.31 JB 3.96 JB 2.39 JB ND ND 0.93 J 1.0 J 1.2 J 2.0 J 0.63 J ND ND 1.4 J 0.54 J 1.8 J 1.4 J 0.59 JB
Lead 15 NS 5.54 J 3.91 JB 5.27 JB ND ND 0.7 J ND 0.32 J 0.13 J 0.89 J 0.55 J 0.19 J 0.29 J ND ND 0.060 J 0.69 J 0.27 J 0.17 JB
Mercury 1 NS ND ND ND ND ND ND ND ND 0.032 J ND ND ND ND ND ND ND ND ND ND
Nickel 100 NS ND 6.50 J 7.02 J ND 3.76 J ND 1.6 J 2.0 2.3 2.1 1.7 J 1.6 J 1.8 J 1.8 J 2.0 1.7 J 2.6 2.3 2.2
Selenium 20 NS ND ND ND ND ND ND ND ND ND 0.67 J ND ND ND ND ND ND ND ND ND
Silver 20 NS ND 3.49 JB 4.21 JB 0.800 JB ND ND ND ND ND 0.14 J ND 0.082 J ND ND ND ND ND 0.013 J 0.012 J
Thallium 0.2 NS ND ND ND ND ND ND ND ND ND 0.22 J ND 0.35 J 0.032 J 0.20 J ND 0.058 J 0.061 J 0.039 J 0.056 J
Vanadium 0.3 NS ND ND ND 0.910 J ND 0.7 J 4.3 J 3.7 J 3.2 J ND ND 5.8 B 2.9 J 1.5 J ND ND ND ND ND
Zinc 1000 NS 5.50 J 9.45 J 10.7 J 2.94 J 3.83 JB 9.1 J 6.3 J 19 B 22 27 B 11 9.6 J 15 6.8 7.6 J 18 9.3 J 19 22Acetone6000NSND4.60 J ND ND ND ND ND ND ND ND ND ND 18 ND ND ND ND ND ND
Bromomethane 10 ND ND ND ND ND 0.49 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 NS ND 1.8 B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methyl Tertiary-Butyl Ether 20 ND ND ND ND ND 5.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Tetrahydrofuran NE NA NA NA NA NA NA ND 1.6 J 2.2 J ND ND ND ND 1.5 J 9.6 J 3.7 J ND ND ND ND
Toluene 600 NS ND 0.290 JB ND ND ND ND ND ND ND ND ND ND ND 0.76 ND ND ND ND ND
Total Xylenes 500 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.67 J ND ND ND ND ND
Fluoride 2000 ND ND ND ND ND ND ND ND 58 J ND 37 J 48 J ND ND ND ND NA NA NA NA
Phenol 30 NS 7 7 2 4 ND ND 36 J ND ND ND ND ND ND ND ND NA NA NA NA
MW-2R Antimony 1 5.73 ND ND ND ND ND ND 0.14 J 4.80 ND 0.14 J ND ND ND ND ND 0.069 J ND ND 0.089 J
Arsenic 10 2.06 ND ND ND ND ND ND ND 1.00 ND 0.19 J ND 0.45 J ND ND ND ND 0.33 J ND ND
Barium 700 21.7 B 22.2 JB 29.5 JB 23.5 JB 10.8 J 20.3 JB 84 14 15 14 16 14 49 16 17 17 17 16 19 20
Beryllium 4 ND 4.97 JB 4.53 B 5.91 ND ND ND ND 0.16 J 0.17 J ND 0.25 J 0.22 J 0.20 J 0.19 J 0.26 J 0.29 J 0.33 J 0.32 J 0.35 J
Cadmium 2 6.05 B ND ND ND ND ND 0.56 J 0.45 J ND ND 0.20 J ND 0.23 J 0.086 J 0.049 J ND 0.11 J 0.11 J 0.29 J 0.92 J
Chromium 10 4.16 B 1.84 JB 3.77 JB 4.00 JB 2.63 JB 2.82 J ND 1.5 1.4 J 1.7 JB ND 1.6 ND 3.3 ND 0.62 J ND 1.3 JB 0.58 J 1.5 JB
Cobalt 1 ND ND 3.67 J ND 2.05 J 5.06 J 150 2.1 3.6 6.8 2.0 2.0 4.3 1.3 1.2 1.2 1.1 3.2 1.3 1.7Copper10008.74 B 4.15 JB 6.56 JB 4.72 JB 3.89 JB 3.07 JB 2.8 J 0.82 J 1.2 J 1.3 J 2.0 J 1.2 J 1.6 J 0.98 J ND 1.5 J ND 1.2 J 1.5 J 1.7 J
Lead 15 13.3 B ND ND 4.65 JB ND ND ND ND 0.31 J 0.19 J 0.14 J ND 0.40 J 0.32 J 0.18 J ND 0.078 J 0.30 J 0.15 J 0.33 J
Mercury 1 0.350 B 0.054 J 0.31 0.055 J 0.096 J 0.047 J ND 0.13 J 0.14 J 0.51 0.16 J 0.19 J 0.078 J ND 0.15 J 0.094 J 0.070 J 0.16 J 0.11 J 0.097 J
Nickel 100 6.91 B ND ND 5.29 J ND 3.87 J 46 2.8 3.30 3.50 3.10 2.70 4.40 5.70 3.20 3.30 3.3 3.3 4.4 4.9
Selenium 20 13.8 B ND ND ND ND ND ND ND 0.97 J ND ND ND ND ND ND ND ND ND ND ND
Silver 20 ND ND 3.53 JB 4.83 JB 0.700 JB ND ND ND ND ND ND ND 0.041 J ND ND ND ND ND 0.023 J 0.13 J
Thallium 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.019 J ND ND 0.011 J 0.024 J 0.24 J
Vanadium 0.3 ND ND ND ND 2.39 J ND ND 5 10 B 2.8 J 0.24 J 0.41 J 2.0 JB 2.8 J 2.3 J ND ND ND ND ND
Zinc 1000 23.2 B 19.4 22.2 20.3 14.8 19.7 B 54 23 30 37 47 B 26 12 31 24 23 40 23 31 44
Benzene 1 0.390 J 0.490 J 0.400 J 0.300 J ND 0.43 J 4.2 0.79 0.68 ND 0.83 0.72 0.96 1.2 1.3 1.4 1.8 0.96 1.4 ND
Chlorobenzene 50 ND ND ND ND ND ND 3.1 ND ND ND ND ND ND ND ND ND ND ND ND ND
1,4-Dichlorobenzene 6 ND ND ND ND ND ND 2.7 ND ND ND ND ND ND ND ND ND 0.56 0.56 0.6 ND
1,1-Dichloroethane 6 6.98 7.05 7.07 5.33 6.19 6 4.6 7.2 7.2 5.8 6.8 5.6 6.5 6.6 7.8 6.8 7.6 6 6.8 ND1,1-Dichloroethene
(Vinylidene Chloride)7 0.620 J ND 0.100 J ND ND ND ND ND ND ND ND ND ND ND ND 0.86 ND ND ND ND
Cis-1,2-Dichloroethene
(Cis-1,2-Dichloroethylene)60 6.03 6.77 6.08 5.64 6.6 6.3 5.4 1.2 7.9 6.1 8.7 7.3 8.5 9.0 9.8 9.3 11 7 9 ND
Dichlorodifluoromethane (CFC-12)1000 4.7 ND ND ND ND ND 2 ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 5.55 6.5 4.14 JB 4.00 5.09 8.40 19.0 8.3 6.4 3.6 B 7.1 5.0 7.4 7.4 ND 9.6 10 5 9 ND
Styrene 70 ND ND ND ND ND ND 0.54 J ND ND ND ND ND ND ND ND ND ND ND ND ND
Tetrachloroethene
(Tetrachloroethylene), (PCE)0.7 1.51 0.980 J 1 0.940 J 0.920 J 0.71 J 0.63 J 1.1 1.2 1.1 1.5 1.8 1.6 1.6 1.6 1.5 1.8 1.4 1.8 ND
Toluene 600 0.620 J 0.210 J 0.120 JB 0.190 J ND 0.42 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Trichloroethene(Trichloroethylene), (TCE)3 5.15 4.77 4.74 3.65 4.28 4.2 1.5 J 5.1 5.1 4.4 5 4.7 4.5 4.9 4.8 4.4 5.6 3.7 4.4 ND
Trichlorofluoromethane (CFC-11) 2000 1.2 0.35 0.620 J ND ND 0.33 J 1.2 J ND 0.69 ND 1.9 0.53 ND 0.81 0.52 ND ND 0.74 2.2 ND
Vinyl Chloride 0.03 ND ND ND ND ND ND 1.0 J ND ND ND ND ND ND ND ND ND ND ND ND ND
Total Xylenes 500 1.79 J 0.37 0.100 J 0.440 J ND ND 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
Fluoride 2000 ND ND ND ND ND ND 76 J ND ND ND 29 J 51 J ND 32 J ND 18 J NA NA NA ND
Phenol 30 14 9 6 4 ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA ND
Sampling Date
Analytical Results (µg/L)
Table 4
Historical Results of Appendix II Assessment Monitoring
Nash County Municipal Solid Waste Landfill
Nashville, Nash County, North Carolina
Permit # 64-01
Page 2 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
Sampling Date
Analytical Results (µg/L)
MW-3 Antimony 1 5.89 ND ND ND ND ND 1.5 J 0.22 J 0.70 J 0.33 J 0.28 J ND ND ND ND ND ND ND ND 0.19 J
Arsenic 10 4.65 ND ND 2.27 J ND ND 2.6 J ND 0.60 J ND ND 0.46 J 1..3 0.72 J 0.52 J ND 0.78 J 0.61 J 0.56 J 0.57 J
Barium 700 68.3 B 76.9 JB 85.8 JB 113 B 86.3 J 109 B 99 120 110 110 130 120 29 99 45 46 110 75 39 55
Beryllium 4 2.28 4.33 JB 9.29 B ND ND ND ND ND 0.29 J 0.16 J ND ND ND 0.054 J 0.073 J ND 0.047 J 0.11 J ND 0.091 JCadmium25.77 B ND ND ND ND ND ND 0.21 J 0.28 J ND 0.21 J ND 0.051 J 0.044 J 0.091 J ND 0.046 J 0.29 J 0.11 J 0.10 J
Chromium 10 4.03 B 2.00 JB 7.21 JB 5.38 JB 6.38 JB 5.15 J ND 1.6 0.79 J 2.8 B ND 0.66 J ND ND ND 0.26 J ND 1.5 JB ND 0.97 JB
Cobalt 1 42 26.7 116 95 133 118 150 95 150 200 170 140 1.9 71 120 71 140 110 51 59
Copper 1000 9.06 B 4.05 JB 8.84 JB 7.00 JB 5.69 JB 4.31 JB 5.6 J 0.92 J 1.3 J 1.0 J 0.80 J 1.5 J 0.74 J ND 1.6 J 1.5 J 0.90 J 2.6 J 3.3 J 1.6 JB
Lead 15 14.2 B ND 7.12 JB 7.62 JB ND 8.98 J ND ND 0.63 J 0.25 J 0.18 J 0.16 J 1 1.2 0.48 J 0.43 J 0.15 J 0.53 J 0.68 J 0.48 JB
Mercury 1 0.116 B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Nickel 100 6.13 B ND 8.79 J 9.14 J 7.00 J 7.95 J 6.7 J 10 11 16 9.8 6.7 0.60 J 17 4.6 2.7 2.5 15 1.8 J 2.8
Selenium 20 15.7 B ND 15.7 ND 7.91 J 11.7 14 J ND 0.86 J ND ND ND 0.20 J ND 0.16 J ND ND 0.59 J ND ND
Silver 20 ND ND 3.71 JB 5.57 JB 1.66 JB 1.96 JB ND ND 0.25 J 0.12 J ND ND 0.032 J ND ND ND ND 0.028 J 0.026 J 0.034 J
Thallium 0.2 ND ND 5.29 J 8.1 ND ND ND 0.18 J 1.3 0.53 J ND 0.17 J ND 0.023 J 0.22 J ND 0.038 J 0.22 J 0.019 J 0.074 J
Vanadium 0.3 8.49 ND ND ND 2.90 J ND ND 6.4 3.3 J 1.0 J 0.16 J ND 6.7 JB 2.3 J 4.1 J 2.5 J ND ND 3.4 J ND
Zinc 1000 35.4 B 27.4 8.93 J 11.8 3.04 J 10.4 B ND 23 14 B 31 30 B 15 4.1 J 9.6 J 6.5 J 5.2 J 14 25 5.9 26
Acetone 6000 ND 4.63 J 12.6 J ND 23.5 J 26.1 ND ND 3.7 J 8.0 B 5.6 ND 2.7 J 1.5 J 14 6.9 3.0 J 29 38 38Benzene1ND0.350 J 0.140 J 0.210 J ND 0.32 J ND 0.72 ND 1.7 0.44 J 0.55 ND ND ND ND ND ND ND ND
Chlrobenzene 50 ND ND ND ND ND ND ND ND ND 0.78 ND ND ND ND ND ND ND ND ND ND
Chloroethane (Ethyl Chloride)3000 0.730 J ND 0.340 J ND ND ND 0.88 J ND 0.59 1.7 2.3 0.85 ND ND ND ND ND ND ND ND
Chloromethane 3 ND 0.230 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1,1-Dichloroethane 6 0.730 J 0.670 J 0.120 J ND ND 0.65 J ND 0.71 ND 1.4 0.28 J ND ND ND ND ND ND ND ND ND
1,1-Dichloroethene
(Vinylidene Chloride)7 0.490 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
cis-1,2-Dichloroethene
(Cis-1,2-Dichloroethylene)60 0.270 J 0.730 J ND 0.490 J ND 0.97 J ND 1.2 0.74 1.1 0.66 0.94 ND ND ND ND ND ND ND ND
Dichlorodifluoromethane 1000 1.47 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 600 0.720 J 0.120 J ND 0.290 J ND ND ND ND ND ND ND ND ND ND ND ND 0.64 ND ND 0.98 J
Methylene Chloride(Dichloromethane)5 ND 0.640 J ND 0.420 J ND ND ND 0.76 J ND ND ND ND ND ND ND ND ND ND ND ND
Methyl Ethy Ketone
(2-butanone)4000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.3 J ND
Styrene 70 0.750 J 0.310 J ND ND ND 0.58 J 0.55 J 1.2 ND ND 0.59 0.5 0.54 0.85 ND 1.6 ND ND ND ND
Tetrachloroethene
(Tetrachloroethylene), (PCE)0.7 0.710 J 0.180 J ND ND ND ND ND ND ND ND 0.28 J ND ND ND ND ND ND ND ND ND
Tetrahydrofuran NE NA NA NA NA NA NA NA 51 95 49 120 220 110 210 14 67 170 ND 28 60
Toluene 600 ND 0.370 J 0.200 JB 0.970 J 1.81 0.57 JB ND 0.93 ND ND ND ND ND ND ND ND ND ND ND ND
Trichloroethene
(Trichloroethylene), (TCE)3 ND 0.330 J ND ND ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ND ND ND
Vinyl Chloride 0.03 5.05 1.41 4.45 J 1.29 J 1.86 1.6 1.7 J 1.1 1.9 3.8 1.5 1.6 0.89 1.8 0.55 ND ND ND ND ND
Total Xylenes 500 1.74 J 0.660 J 0.180 J 1.45 J 1.15 J 0.86 J ND 0.69 J ND ND ND ND ND ND ND ND ND ND ND ND
Methoxychlor 40 ND ND ND ND 0.106 J ND ND ND ND ND ND ND ND ND ND ND NA NA ND ND4,4'-DDD 0.1 ND ND ND ND ND 0.0198 ND ND ND ND ND ND ND ND ND ND NA NA ND ND
Phenol 30 5 8 11 13 4 ND ND 49 J ND ND ND ND ND ND ND ND NA NA NA NA
Fluoride 2000 ND ND ND 100 ND ND 100 ND 38 J ND 90 J 74 J 41 J 69 J 61 J 35 J NA NA NA NA
Page 3 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
Sampling Date
Analytical Results (µg/L)
MW-4 Antimony 1 5.73 ND ND ND ND ND ND 0.16 J 0.52 J 0.14 J 0.19 J 0.33 J ND ND ND ND ND ND ND ND
Arsenic 10 2.06 ND 4.82 J 6.54 J ND ND ND 1.1 1.1 ND 0.69 J 0.41 J 0.84 J ND ND ND 0.48 J ND 0.42 J 0.31 J
Barium 700 21.7 B 44.7 JB 111 B 66.2 JB 62.0 J 82.3 JB 98 93 110 81 83 210 3.8 J 150 62 180 88 37 30 150
Beryllium 4 ND 4.67 JB 4.97 B ND ND ND ND ND 0.40 J ND ND ND ND ND 0.094 J ND 0.13 J 0.19 J 0.15 J 0.18 JCadmium26.05 B ND ND ND ND ND ND ND 0.30 J ND ND ND 0.095 J 0.046 J 0.38 J 0.23 J 0.39 J 3.10 3.10 2.60
Chromium 10 4.16 B 2.51 JB 7.62 JB 5.26 JB 3.88 JB 4.57 J ND 1.8 0.99 J 2.4 B ND ND ND ND ND 1.4 ND 1.3 JB 1.1 1.6 JB
Cobalt 1 ND ND 35.8 18.7 20.4 21.5 20 36 48 23 15 40 0.06 J 30 22 56 28 11 12 51
Copper 1000 8.74 B 3.34 JB 10.9 B 6.66 JB 4.60 JB 5.36 JB 3.1 J 0.53 J 1.3 J 1.6 J 1.7 J 2.0 J 0.55 J 0.85 J 1.7 J 0.58 J 1.4 J 2.7 J 2.9 J 1.9 JB
Lead 15 13.3 B 5.23 J 8.65 JB 10.8 B ND 8.42 J ND 0.52 J 0.76 J 0.52 J 0.48 J 0.29 J ND 0.33 J 0.50 J 0.21 J 0.48 J 0.64 J 0.97 J 0.95 JB
Mercury 1 0.350 B ND ND ND ND ND ND ND ND 0.041 J ND ND ND ND ND ND ND 0.011 J ND ND
Nickel 100 6.91 B ND ND ND ND ND ND 3.40 1.0 J 1.7 J 1.3 J 2.10 0.93 J 1.5 J 2.30 2.50 1.9 J 1.4 J 2.80 3.50
Selenium 20 13.8 B ND ND ND 3.29 J 5.11 J 7.4 J ND 0.93 J ND 0.57 J 1.10 ND ND 0.33 J ND 0.62 J ND ND ND
Silver 20 ND ND 3.22 JB 4.84 JB 1.22 JB 0.8 JB ND ND 0.32 J ND ND ND 0.026 J ND ND ND 0.048 J ND 0.033 J 0.036 J
Thallium 0.2 ND ND ND ND ND ND ND ND 0.65 J ND ND ND ND ND 0.033 J 0.12 J 0.14 J 0.017 J 0.046 J 0.033 J
Vanadium 0.3 ND ND ND ND 4.30 J ND 0.98 J 6.0 3.9 J 3.3 J 3.1 J 0.76 J 3.1 JB 2.7 J 3.7 J 1.7 J ND ND ND ND
Zinc 1000 23.2 B 8.95 J 40.3 20.3 6.71 J 20.6 B 17 J 54 22 B 15 30 B 18 11 9.1 J 18 3.8 J 22 9.3 J 58 42
Acetone 6000 ND ND 4.02 J ND ND ND ND ND ND ND 4.8 J ND ND ND ND ND ND 8.8 ND NDBenzene1ND0.110 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Chloroform (Trichloromethane)70 0.210 J 0.240 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 600 ND 0.210 J ND 0.120 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 ND 0.220 J 0.250 JB ND ND 3.4 ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 0.580 J 0.790 J 0.160 JB 0.420 J 0.940 J 0.64 JB 1.7 0.5 0.86 0.89 0.30 J ND ND ND ND 0.83 ND ND ND ND
Total Xylenes 500 1.78 J 1.05 J ND 0.770 J 0.430 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
alpha-BHC NE 0.026 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
beta-BHC NE ND ND ND ND 0.0143 J ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
delta-BHC NE ND ND ND ND ND 0.0101 JD ND ND ND ND ND ND ND ND ND ND NA NA NA NA
4,4'-DDD 0.1 ND ND ND ND 0.0098 J ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
4,4'-DDT 0.1 ND ND ND 0.0203 ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NAEndrin2ND0.0624 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
Endrin Aldehyde 2 ND 0.0876 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
Fluoride 2000 100 ND ND ND ND ND 47 J ND 120 140 51 J 79 J 13 J 75 J 40 J 55 J NA NA NA NA
Phenol 30 5 5 6 2 ND ND 25 J 49 J ND ND ND ND ND ND ND ND NA NA NA NA
MW-5 Antimony 1 ND ND ND ND ND ND ND 0.13 J 0.32 J 0.19 J ND ND ND 0.21 J ND ND ND ND ND 0.19 JArsenic105.29 ND 4.44 J ND ND ND ND 0.48 J 0.30 J 0.94 J 0.48 J ND 0.50 J ND ND ND ND ND ND ND
Barium 700 17.0 B 13.5 JB 23.2 JB 16.4 JB 3.86 J 13.6 JB 5.7 J 5.1 6.9 6.7 7.0 6.1 6.9 7.2 8.0 6.2 5.3 4.3 J 6.6 6.3
Beryllium 4 2.28 5.60 JB ND ND ND ND ND 0.15 J 0.38 J 0.31 J 0.31 J 0.36 J 0.25 J 0.23 J 0.27 J 0.32 J 0.25 J 0.14 J 0.33 J 0.30 J
Cadmium 2 5.11 B ND ND ND ND ND ND ND 0.22 J ND 0.50 J ND 0.071 J ND ND 0.45 J 0.046 J 0.035 J 0.12 J 0.11 J
Chromium 10 4.56 B 2.34 JB 4.59 JB 4.00 JB 2.33 JB 1.95 J 0.6 J 1.7 1.3 2.5 B ND 1.1 ND ND ND 3.1 J ND 1.6 JB ND 1.3 JB
Cobalt 1 ND ND ND ND ND ND ND ND 0.25 J ND 0.35 J 0.13 J 0.079 J 0.055 J 0.16 J 0.86 J ND 0.052 J 0.040 J 0.18 J
Copper 1000 9.79 B 3.44 JB 7.40 JB 4.13 JB 3.11 JB 3.43 JB ND ND 0.90 J 0.73 J 1.2 J 1.0 J 1.0 J ND 1.1 J 0.46 J ND 0.45 J 0.77 J 1.5 JB
Lead 15 8.50 B 9.00 J ND 8.46 JB ND ND ND ND 0.43 J 0.15 J 0.67 J ND 0.20 J 0.35 J 0.21 J ND 0.065 J 0.13 J 0.25 J 0.54 JB
Mercury 1 0.085 B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Nickel 100 ND ND ND ND ND ND ND ND 1.1 J 1.1 J 1.3 J 0.97 J 0.86 J 0.76 J 1.0 J 2.00 0.80 J 1.2 J 0.98 J 1.1 J
Selenium 20 15.0 B ND ND ND ND ND ND ND 0.54 J ND 1.4 J 0.75 J 0.28 J ND ND ND ND ND ND ND
Silver 20 ND ND 3.21 JB 4.41 JB ND ND ND ND 0.12 J ND 0.48 J ND 0.042 J ND ND ND ND ND 0.026 J 0.041 JThallium0.2 ND ND 5.27 J ND ND ND ND ND 0.28 J ND 2.9 J ND ND 0.017 J 0.019 J ND ND 0.013 J 0.039 J 0.045 J
Vanadium 0.3 ND ND ND ND 3.12 J ND ND 5.5 3.7 J 2.8 J 0.44 J ND 3.6 JB 1.4 J 1.3 J ND ND ND ND ND
Zinc 1000 9.09 B ND 5.78 J 5.45 J 7.61 J 4.53 JB 6.2 J 4.7 J 8.2 JB 18.00 27 B 11.00 8.1 J 12.00 5.0 J 3.8 J 16 2.6 J 7.0 J 23
Acetone 6000 ND ND 2.61 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 600 ND 0.210 J ND 0.130 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 ND ND 0.210 J ND ND ND ND ND ND ND ND ND ND ND ND 1.1 ND ND ND ND
Toluene 600 0.580 J 0.810 J 0.120 JB 0.500 J 0.770 J 0.32 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Total Xylenes 500 ND 0.800 J ND 0.880 J 0.410 J 0.70 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Fluoride 2000 ND ND ND ND ND ND 110 ND ND ND 30 J 55 J ND 37 J ND 22 J NA NA NA NA
Phenol 30 9 5 7 2 ND ND ND 30 J ND ND ND ND ND ND ND ND NA NA NA NA
Page 4 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
Sampling Date
Analytical Results (µg/L)
MW-6 Antimony 1 8.49 ND ND ND ND ND ND 0.14 J 0.28 J 0.13 J ND 0.16 J ND ND ND ND ND ND 0.098 J 0.095 J
Arsenic 10 2.35 ND 6.79 J ND ND ND ND ND ND 0.27 J ND 0.24 J 0.73 J ND 0.50 J ND ND ND ND ND
Barium 700 76.2 B 44.9 JB 64.4 JB 53.9 JB 52.7 J 57.1 JB 47 51 41 46 44 46 44 43 52 51 51 51 54 57
Beryllium 4 ND 7.55 JB 2.11 B 7.89 ND ND ND ND ND ND ND 0.15 J ND ND ND ND ND ND ND 0.051 JCadmium24.81 B ND ND ND ND 0.54 J ND ND ND ND ND ND 0.10 J 0.65 J 0.038 J ND 0.043 J 0.029 J 0.048 J 0.12 J
Chromium 10 8.37 B 3.34 JB 5.01 JB 2.99 JB 4.59 JB 3.02 J 0.71 J 1.8 1.6 1.8 JB 0.98 J 1.0 ND 0.39 J ND 0.61 J 0.64 J 1.8 JB ND 1.3 JB
Cobalt 1 ND ND ND ND 2.11 J 2.16 J ND 0.71 J 0.076 J 0.23 J 0.10 J 0.28 J 0.059 J 0.10 J 0.15 J 0.17 J 0.048 J 0.19 J 0.040 J 0.26 J
Copper 1000 12.8 B 3.90 JB 8.13 JB 4.75 JB 4.75 JB 4.33 JB ND 0.58 J 0.59 J 0.69 J 0.85 J 0.69 J 0.37 J ND ND 0.16 J 2.2 J ND 0.44 J 1.3 JB
Lead 15 14.8 B ND 5.06 JB 7.02 JB ND ND ND 0.20 J 0.23 J 0.15 J 0.16 J 0.22 J ND 0.28 J ND ND 0.073 J 0.089 J 0.084 J 2.1 B
Mercury 1 0.105 B ND ND ND ND ND ND ND ND 0.053 J ND ND ND ND 0.033 J 0.045 J 0.049 J 0.11 J ND ND
Nickel 100 6.85 B ND 5.56 J ND ND 2.83 J ND 1.2 J ND 1.7 J 1.6 J ND 0.49 J 0.77 J 0.66 J 1.8 J 2.9 1.0 J 1.5 J 1.5 J
Selenium 20 17.0 B ND ND ND ND ND ND ND ND ND 0.71 J 0.61 J 0.22 J ND ND ND ND ND ND ND
Silver 20 ND ND 3.39 JB 4.41 JB 0.78 JB ND ND ND ND 0.061 J 0.095 J 0.15 J 0.052 J ND ND ND ND 0.011 J 0.015 J 0.040 J
Thallium 0.2 ND ND ND ND ND ND ND ND 0.14 J ND ND 0.81 J ND ND 0.093 J ND 0.023 J 0.017 J 0.0093 J 0.037 J
Vanadium 0.3 18.3 ND ND ND 11.0 J ND 0.65 J 8.3 5.4 2.7 J 0.46 J 0.22 J 4.9 JB 2.4 J 2.0 J ND ND ND ND ND
Zinc 1000 34.0 B 50.2 25 7.38 J 15.3 11.3 B 9.1 J 13 8.6 JB 23 25 B 8.5 J 10 J 12 6.1 J 5.9 J 20 7.6 J 11 24
Acetone 6000 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.3 J ND ND ND ND ND NDBenzene1ND0.160 J ND 0.140 J 0.190 J 0.30 J ND 0.57 ND 1.3 ND 0.6 ND 0.96 0.81 1.4 ND 1.6 ND 1.6
Chlorobenzene 50 ND 0.0800 J ND 0.130 J ND 0.31 J ND 0.53 ND 0.65 ND 0.91 ND 1.4 1.2 2 ND 2.5 ND 3.3
Chloroethane (Ethyl Chloride)3000 ND ND ND ND ND 0.18 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Chloroform (Trichloromethane)70 ND 0.160J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1,4-Dichlorobenzene 6 ND 0.260 J ND ND ND 0.44 J ND 0.58 ND 0.72 0.41 J 0.7 0.53 1.1 1.2 1.5 1.2 1.8 1.7 3
Dichlorodifluoromethane (CFC-12)1000 ND ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND ND ND ND ND ND
1,1-Dichloroethane 6 1.23 0.910 J 0.370 J 0.650 J 0.760 J 1 0.83 J 1.2 0.53 1.9 0.49 J 1.1 0.54 1.2 1.4 1.4 0.88 1.5 0.9 1.3
cis-1,2-Dichloroethene
(Cis-1,2-Dichloroethylene)60 0.840 J 1.22 J 0.540 J 1.15 J 1.10 J 1.5 1.3 2 0.86 2 0.78 2.2 0.9 2.6 2.8 3.3 1.5 3.6 1.4 3.3
Ethylbenzene 600 ND 0.150 J ND 0.190 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 ND 0.420 J ND ND ND ND ND 0.87 J ND 0.71 JB ND ND ND 0.58 J ND 1.8 ND 1.4 ND 1.2Methyl Ethy Ketone
(2-butanone)4000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.73 J ND ND
Tetrachloroethene
(Tetrachloroethylene), (PCE)0.7 0.720 J 0.230 J ND 0.250 J ND ND ND ND ND 1.5 0.35 J ND ND ND ND 2.3 ND 0.63 ND ND
Toluene 600 0.710 J 0.670 J 0.190 JB 0.720 J 0.880 J 0.46 JB ND 0.67 ND ND ND ND ND ND ND ND ND ND ND ND
1,1,1-Trichloroethane
(Methylchloroform)200 0.630 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Trichloroethene
(Trichloroethylene), (TCE)3 0.330 J 0.400 J ND 0.160 J ND ND ND ND ND ND ND ND ND ND 0.59 2.3 ND 0.53 ND 0.56
Trichlorofluoromethane (CFC-11) 2000 1.1 ND 0.360 J ND ND ND ND ND ND ND ND ND ND 0.55 ND ND ND 0.74 ND ND
Total Xylenes 530 ND 0.850 J 0.160 J 1.33 J 0.450 J 1.0 J ND 0.59 J ND ND ND ND ND 0.53 J ND 0.7 J ND 0.86 J ND 1.2
Aldrin NE ND ND ND ND ND 0.0116 J ND ND ND ND ND ND ND ND ND ND NA NA NA NA
4,4'-DDT 0.1 ND ND 0.0291 J ND ND 0.0256 J ND ND ND ND ND ND ND ND ND ND NA NA NA NAFluoride2000ND0.1 ND ND ND ND 110 ND ND ND 42 J 52 J ND 33 J ND 17 J NA NA NA NA
Phenol 30 8 4 5 2 ND ND ND 55 ND ND ND ND ND ND ND ND NA NA NA NA
Page 5 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
Sampling Date
Analytical Results (µg/L)
MW-7s Antimony 1 ----ND ND ND ND ND ND 0.47 J 0.79 J 1.40 1.20 0.59 J ND 0.17 J 0.15 J 0.12 J 0.12 J ND 0.096 J 0.15 J
Arsenic 10 ----ND 7.38 J 5.17 J ND ND 6.6 J 1.0 J 1.40 1.2 J 2.80 1.10 ND 2.40 1.40 ND 0.80 J 0.37 J 0.55 J 0.88 J
Barium 700 ----20.0 JB 97.0 JB 83.2 JB 101 57.4 JB 110 84 79 43 53 32 13 17 23 10 16 9 11 10
Beryllium 4 ----5.94 JB 4.57 B 7.37 2.86 J 1.2 2.5 2.10 2.20 1.80 1.50 1.60 ND 0.34 J 0.74 J 0.25 J 0.34 J 0.17 J 0.18 J 0.21 JCadmium2----0.210 J 0.54 J 0.65 J 0.66 J 0.43 J ND 0.54 J 0.36 J 0.6 J 1.20 1.70 0.51 J 0.69 J 0.32 J 0.29 J 0.26 J 0.30 J 0.53 J 0.63 J
Chromium 10 ----3.01 JB 11.4 B 11.2 B 14.9 B 6.14 J 15 1.9 J 3.9 5.3 B 2.1 1.5 ND 1.6 5.1 2.10 3.2 2.3 B 1.4 2.6 JB
Cobalt 1 ----ND 8.26 J 4.98 J 9.42 J 4.95 J 6.6 2.6 J 3.80 3.30 3.40 8.00 0.072 J 3.80 2.80 0.58 1.4 0.35 J 1.3 0.54 J
Copper 1000 ----3.82 JB 30.7 B 30.8 B 50 B 19.8 B 61 10 J 14 12 14 14 3.9 J 11 22 10 14 7.6 10.0 6.9
Lead 15 ----3.69 J 15.4 B 19.6 B 19.9 11.7 18 15 17 13 15 10 0.51 J 4 8 1.9 3.8 1.5 2.0 1.7 JB
Mercury 1 ----ND ND ND ND ND ND ND ND 0.014 J ND ND ND ND ND ND ND ND ND ND
Nickel 100 ----ND 18.2 J 15.8 J 22.9 J 11.2 27 10 10 9 12 13 5 6 7 4.2 5.1 4.8 5.7 4.6
Selenium 20 ----ND ND 11 8.47 J ND 11 J ND ND ND 1.8 J 0.88 J ND 0.19 J 0.28 J ND ND 0.37 J ND ND
Silver 20 ----ND 3.59 JB 4.08 JB ND ND ND ND 0.13 J 0.47 J 0.67 J 0.15 J 0.034 J 0.042 J 0.16 J 0.053 J 0.074 J 0.030 J 0.093 J 0.041 J
Thallium 0.2 ----ND ND ND ND ND ND ND ND 0.43 J 4.10 ND ND 0.064 J 0.11 J 0.084 J 0.068 J 0.044 J 0.082 J 0.051 J
Vanadium 0.3 ----ND 14.3 J 13.6 19.3 J 2.48 J 25 4.6 J 8.6 3.2 J 2.1 J 2.5 J 3.2 JB 8.1 15.0 5.1 8.2 ND 3.9 J 3.2 J
Zinc 1000 ----6.79 J 406 677 694 647 730 960 660 B 1500 1500 B 1400 20 1300 2500 1300 1400 1700 2100 1400
Acetone 6000 ----ND ND ND ND 2.2 J ND ND ND ND ND ND ND ND ND ND ND 8.6 ND ND1,1-Dichloroethane 6 ----3.92 J 0.360 J ND 0.240 J ND 0.52 J ND ND ND ND ND ND ND ND ND ND ND ND ND
cis-1,2-Dichloroethene
(Cis-1,2-Dichloroethylene)70 ----1.17 J 0.120 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 600 ----ND ND 0.130 J 0.140 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ----ND 0.150 JB 0.430 J 0.960 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Trichloroethene
(Trichloroethylene), (TCE)3 ----1.02 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Total Xylenes 500 ----ND 0.100 J 0.800 J 0.810 J 0.77 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND
beta-BHC 0.019 ----ND 0.0506 J ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
delta-BHC 0.19*----ND ND ND ND 0.0172 J ND ND ND ND ND ND ND ND ND ND NA NA NA NA
Fluoride 2000 ----ND 100 100 100 134 80 J 160 100 120 92 J 90 J 49 J 100 62 J 40 J NA NA NA NA
Phenol 30 ----6 6 3 4 ND ND 72 ND ND ND ND ND ND ND ND NA NA NA NA
MW-7d Antimony 1 ----ND ND ND ND ND ND 0.15 J 0.24 J 0.26 J 0.22 J ND ND ND ND ND ND ND ND 0.23 J
Arsenic 10 ----ND 3.99 J 3.87 J ND ND ND 0.45 J ND 0.31 J 0.49 J 0.31 J 0.67 J ND ND ND ND 0.33 J 0.37 J 0.49 J
Barium 700 ----14.3 JB 22.0 JB 15.0 JB 3.12 J 17.7 JB 3.3 J 3.6 J 4.9 J 3.7 J 4.2 J 3.7 J 69.0 18.0 3.6 J 3.8 J 3.6 J 3.3 J 3.9 J 3.9 J
Beryllium 4 ----2.43 JB 1.16 B ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.11 J 0.054 J
Cadmium 2 ----0.210 J ND ND ND ND ND 1.6 ND ND ND ND 0.075 J 0.088 J 0.032 J 0.56 J 0.093 J 0.045 J 0.87 J 0.42 JChromium10----4.09 JB 4.87 JB 3.74 JB 3.57 JB 5.26 J ND 1.7 1.4 1.9 B ND 1.1 ND ND ND 0.59 J ND 1.4 JB ND 1.1 JB
Cobalt 1 ----ND ND ND ND 3.4 J ND 0.11 J 0.42 J 0.069 J 0.11 J 0.092 J 8.20 0.16 J 0.13 J 0.22 J 0.12 J 0.16 J 0.12 J 0.22 J
Copper 1000 ----4.15 JB 7.99 JB 4.31 JB 4.12 JB 7.02 JB ND ND 1.1 J 0.69 J 0.61 J 0.81 J 2.6 J ND ND 0.30 J 1.9 J ND 0.53 J 0.48 J
Lead 15 ----7.27 J 7.16 JB 7.60 JB ND ND ND 0.18 J 0.96 J 0.14 J 0.19 J 0.13 J 1.1 0.35 J 0.068 J ND 0.066 J 0.059 J 0.19 J 0.33 J
Mercury 1 ----ND ND ND ND ND ND ND ND ND ND ND ND ND 0.033 J 0.083 J ND 0.23 0.034 J 0.050 J
Nickel 100 ----ND 7.44 J ND ND 5.27 J ND 1.2 J 1.6 J 2.30 1.3 J 0.93 J 1.3 J 1.1 J 0.81 J 1.3 J 3.4 1.1 J 1.3 J 1.4 J
Selenium 20 ----ND ND ND ND ND ND ND ND ND 0.48 J 0.63 J 5.80 ND ND ND ND ND ND ND
Silver 20 ----ND 3.82 JB 4.63 JB 0.730 JB ND ND ND ND ND ND ND 0.024 J ND ND ND ND ND 0.11 J 0.055 J
Thallium 0.2 ----5.53 ND ND ND ND ND ND ND ND ND ND ND ND 0.027 J ND 0.011 J 0.012 J 0.15 J 0.23 J
Vanadium 0.3 ----ND ND ND 3.00 J ND ND 5.5 5.6 4.1 J ND ND 4.2 JB 3.7 J 1.6 J ND ND ND ND ND
Zinc 1000 ----19.3 14.6 9.56 J 6.16 J 23.6 B 9.2 J 11 20 B 21 43 B 12 4.8 J 14 6.3 J 5.5 J 20 5.3 J 10 19
Benzene 1 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.6Chloroform (Trichloromethane)70 ----1.00 J 0.140 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1,4-Dichlorobenzene 6 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3
Dichlorodifluoromethane (CFC-12)1000 ----ND ND ND ND ND 2.4 ND ND ND ND ND ND ND ND ND ND ND ND ND
1,1-Dichloroethane 6 ----2.39 J 2.74 J 2.17 J 2.72 J 2.5 2.7 2.8 3.5 3.2 3.4 3.2 3.8 3.4 4 3.6 4 3.8 3.9 J 6.1
cis-1,2-Dichloroethene
(Cis-1,2-Dichloroethylene)60 ----1.63 J 1.98 J 1.76 J 2.18 J 2 2.3 2.3 2.8 2.7 3.2 3.1 3.7 3.2 4 3.5 4 3.6 3.4 9
Methylene Chloride
(Dichloromethane)5 ----0.490 J ND 0.310 J ND 6.3 ND ND ND ND ND ND 1.3 1.4 1.4 4.6 3.7 4.1 3.6 9.5
Tetrachloroethene
(Tetrachloroethylene), (PCE)0.7 ----0.140 J 0.310 J 0.370 J ND ND ND ND 0.58 0.54 0.7 0.78 0.73 0.74 0.76 0.69 0.75 0.99 0.74 2
Toluene 600 ----ND 0.160 JB 0.250 J 0.350 J 0.61 B ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Trichloroethene
(Trichloroethylene), (TCE)3 ----0.990 J 1.32 1.11 1.4 1.2 1.3 1.3 1.7 1.8 1.8 2 2.1 2.1 2.2 2 2.5 2.3 2.4 4.4Trichlorofluoromethane (CFC-11) 2000 ----ND 0.390 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.63 ND ND
Total Xylenes 500 ----ND 0.130 J 0.480 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Fluoride 2000 ----0.1 ND ND ND ND 34 J ND ND ND 35 J 57 J ND 37 J 26 J 19 J NA NA NA NA
Phenol 30 ----6 5 3 4 ND ND 30 J ND ND ND ND ND ND ND ND NA NA NA NA
Page 6 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
Sampling Date
Analytical Results (µg/L)
MW-8s Antimony 1 ----ND ND ND ND ND ND 0.21 J 0.23 J 0.72 J 0.14 J ND ND ND ND ND ND ND ND 0.091 J
Arsenic 10 ----ND 5.33 J 6.07 J ND ND ND ND 0.36 J 1.3 J ND ND ND ND ND ND ND 1.00 ND ND
Barium 700 ----45.4 JB 31.4 JB 86.0 JB 80.3 J 84.7 JB 120 26 10 18 8 7 6 8 5 7.1 5.4 9.0 6.6 8.3
Beryllium 4 ----5.60 JB ND 7.89 ND 1.59 ND ND ND ND ND ND ND 0.057 J ND ND ND 0.20 J 0.071 J 0.062 JCadmium2----0.200 J ND 0.19 J ND 0.22 J ND ND ND ND 2.00 ND 0.045 J 0.096 J ND ND 0.12 J 0.18 J 0.11 J 0.38 J
Chromium 10 ----3.84 JB 8.47 JB 12.7 B 5.84 JB 9.93 J 4.4 J 1.9 3.0 2.0 B 2.0 3.9 2.5 3.3 3.4 4.6 4.3 3.3 B 3.8 3.4 JB
Cobalt 1 ----4.02 J ND 6.66 J ND 6.33 J ND 1.3 0.32 J 1.2 J 0.31 J 0.19 J 0.065 J 0.22 J 0.072 J 0.18 J 0.15 J 5.3 0.33 J 0.41 J
Copper 1000 ----7.65 JB 7.93 JB 22.2 B 3.60 JB 19.3 B ND 1.7 J 0.78 J 3.4 J 0.76 J 1.0 J 0.37 J 1.2 J 1.8 J 0.55 J ND 5.90 0.66 J 1.5 JB
Lead 15 ----8.96 J 8.38 JB 35.8 B ND 36.2 2.1 J 6.7 1.3 3.6 0.71 J 0.63 J 0.27 J 1.2 0.17 J 0.62 J 0.45 J 3.0 0.50 J 1.1 JB
Mercury 1 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.14 J ND ND
Nickel 100 ----ND ND 13.4 J ND 12.0 J ND 1.5 J ND 2.7 J ND ND 0.38 J 0.64 J 1.3 J 0.44 J 0.54 J 4.80 0.65 J 1.4 J
Selenium 20 ----ND ND 10.5 ND 2.91 J ND ND ND ND 0.85 J 0.54 J ND 0.30 J ND ND ND 0.83 J ND ND
Silver 20 ----ND 3.28 JB 3.57 JB 0.73 JB ND ND ND ND ND ND 0.063 J ND ND ND ND ND 0.044 J 0.049J 0.048 J
Thallium 0.2 ----ND ND 5.22 J ND ND ND ND ND ND ND 0.26 J ND 0.014 J 0.063 J ND 0.016 J 0.056 J 0.15 J 0.031 J
Vanadium 0.3 ----11.4 J 2.03 J 32.9 5.37 J 31.6 3.1 J 9.2 5.6 4.8 J 1.1 J 0.85 J 2.7 JB 5.8 2.4 J 2.2 J ND 6.0 ND ND
Zinc 1000 ----24.9 13.6 318 9.59 J 609 B 25 J 160 63 190 49 B 18 11 20 4.7 J 5.7 J 17 20 6.1 J 24
Acetone 6000 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND 16 ND ND ND NDChloroform (Trichloromethane)70 ----0.200 J 0.280 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Chloromethane 3 ----0.230 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 600 ----ND ND 0.140 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride 5 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.8 ND ND ND ND
Toluene 600 ----ND 0.110 JB 0.480 J 0.770 J 0.43 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Total Xylenes 500 ----ND ND 0.850 J 0.290 J 0.89 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Fluoride 2000 ----0.1 ND ND ND 107 120 130 ND ND 30 J 54 J ND 33 J ND 18 J NA NA NA NA
Phenol 30 ----5 6 3 4 ND ND 49 J ND ND ND ND ND ND ND ND NA NA NA NA
MW-8d Antimony 1 ----ND ND ND ND ND 1.5 J 0.23 J 0.19 J 0.30 J 0.31 J 0.23 J ND ND ND ND ND ND 0.079 J 0.071 J
Arsenic 10 ----ND 5.27 J ND ND ND ND ND ND 0.65 J 0.14 J 0.35 J 0.38 J ND ND ND ND 0.48 J ND ND
Barium 700 ----37.6 JB 30.1 JB 18.2 JB 6.17 J 15.1 JB 5.1 J 4.9 J 5.2 5.8 5.9 5.0 5.3 5.2 5.1 4.8 J 5.2 6.2 5.6 5.4
Beryllium 4 ----2.09 JB 8.34 B 4.96 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Cadmium 2 ----0.200 J ND ND ND ND ND ND ND ND 0.25 J ND 0.089 J ND ND ND 0.084 J 0.045 J 0.29 J 0.22 J
Chromium 10 ----8.03 JB 6.95 JB 5.64 JB 4.20 JB 3.8 J 1.5 J 1.9 2.5 2.9 B ND 1.3 ND 1.2 ND 1.0 1.2 2.3 B 0.85 J 1.3 JB
Cobalt 1 ----ND 3.97 J ND ND ND ND ND ND ND ND ND 0.066 J 0.015 J 0.022 J ND 0.054 J 0.12 J 0.088 J 0.037 J
Copper 1000 ----7.10 JB 6.97 JB 4.99 JB 3.11 JB 3.63 JB ND ND ND 0.62 J ND ND 0.35 J ND ND 0.34 J 0.59 J ND 0.48 J ND
Lead 15 ----9.97 J 8.54 JB 6.22 JB ND ND ND ND 0.16 J 0.30 J 0.15 J ND 0.17 J 0.28 J ND ND 0.078 J 0.15 J 0.16 J 0.14 JBMercury1----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Nickel 100 ----ND 7.48 J ND ND ND ND ND ND ND ND ND 0.23 J 0.67 J ND 0.83 J 0.66 J 0.39 J 0.41 J 0.56 J
Selenium 20 ----ND ND ND ND ND ND ND ND ND 0.53 J 0.71 J ND 0.41 J ND ND ND ND ND ND
Silver 20 ----ND 3.26 JB 4.51 JB ND ND ND ND ND ND ND ND 0.079 J ND ND ND 0.018 J 0.019 J 0.056 J 0.017 J
Thallium 0.2 ----ND ND ND ND ND ND ND ND ND 0.14 J ND 0.18 J ND 0.043 J ND 0.016 J 0.032 J 0.16 J 0.022 J
Vanadium 0.3 ----14.1 J 3.50 J ND 4.00 J ND 1.2 J 3.4 J 5.60 3.4 J 0.97 J 1.8 J 3.8 JB 4.0 J 3.3 J ND 2.5 J ND ND ND
Zinc 1000 ----55.1 8.69 J 6.03 J ND 4.14 JB 8.7 JB 2.1 J 7.1 JB 20.0 20 B 6.5 J 2.9 J 8.2 J 1.3 J 2.0 J 14 1.7 J 4.5 J 18
Acetone 6000 ----2.84 J ND ND ND ND ND ND ND ND ND ND ND ND ND 9.3 ND ND ND ND
Chloroform (Trichloromethane)70 ----0.900 J 0.280 J 0.140 J ND 0.33 J ND ND ND ND 0.31 J ND ND ND ND ND ND ND ND ND
cis-1,2-Dichloroethene
(Cis-1,2-Dichloroethylene)6 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3
1,1-Dichloroethane 6 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3.4Ethylbenzene600----ND ND 0.220 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 ----ND 0.550 JB ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 4.4
Tetrachloroethene
(Tetrachloroethylene), (PCE)0.7 ----ND ND ND ND ND ND ND ND ND 0.31 J ND ND ND ND ND ND ND ND ND
Trichloroethene
(Trichloroethylene), (TCE)3 ----ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2
Toluene 600 ----ND 0.140 JB 0.840 J 0.790 J 0.40 JB ND 0.65 ND ND ND ND ND ND ND ND ND ND ND ND
Total Xylenes 500 ----ND ND 1.34 J 0.380 J 0.81 J ND 0.60 J ND ND ND ND ND ND ND ND ND ND ND ND
Fluoride 1000 ----ND ND ND ND ND 120 ND ND ND 31 J 53 J ND 33 J ND 18 J NA NA NA NA
Phenol 30 ----4 7 10 ND ND ND 36 J ND ND ND ND ND ND ND ND NA NA NA NA
Page 7 of 7
Sample ID
Appendix II
Constituent
NCAC 2L
Standard
(µg/L)5/17/07 11/5-6/2007 5/13-14/2008 11/20-21/2008 5/19-20/2009 11/18-19/2009 5/6/10 11/29/10 5/9/11 11/14/11 5/3/12 11/8/12 5/9/13 10/31/13 5/1/14 11/5-6/2014 5/18-19/2015 11/5/15 5/5-6/16 11/7-8/16
Sampling Date
Analytical Results (µg/L)
SW-1 Antimony 1 ----ND ND ND ND ND ND 0.63 J 4.50 0.23 J 0.19 J ND ND ND 0.31 J ND 0.076 J ND 0.33 J 0.25 J
Arsenic 10 ----ND 5.59 J 3.01 J ND ND ND 0.77 J 1.40 0.99 J 1.10 0.31 J 0.44 J ND 0.83 J ND 0.98 J 0.53 J 0.99 J 0.44 J
Barium 700 ----49.1 JB 42.4 JB 53.1 JB 24.9 J 46.2 JB 39 24 31 24 37 25 75 24 23 27 24 34 26 28
Beryllium 4 ----6.87 JB ND 8.84 ND ND ND 0.20 J ND ND ND ND ND ND 0.031 J ND 0.071 J 0.099 J 0.11 J 0.081 JCadmium2----0.270 J ND ND ND ND ND 0.26 J ND ND ND ND 0.26 J 0.039 J ND 2.90 0.067 J 0.30 J 0.090 J 0.065 J
Chromium 10 ----2.50 JB 4.87 JB 3.99 JB 2.87 JB 3.02 J 1.4 J 2.30 1.9 J 2.7 B ND 1.00 ND 0.45 J 0.15 J 0.81 J 0.58 J 1.8 JB 1.50 1.2 JB
Cobalt 1 ----ND ND ND 2.02 J 2.57 J 2.8 J 0.79 J 1.80 1.60 2.60 1.40 89.0 0.57 J 0.94 J 1.2 0.15 J 0.84 J 0.82 J 0.70 J
Copper 1000 ----4.75 JB 7.37 JB 4.86 JB 14.7 B 3.82 JB 4.0 J 0.70 J 1.1 J 1.4 J 1.4 J 1.2 J 0.66 J ND 2.5 J 0.74 J 0.81 J 1.4 J 4.4 J 0.68 JB
Lead 15 ----ND ND 4.99 JB ND ND 1.3 J 0.69 J 0.93 J 0.8 J 1.10 0.60 J 0.21 J 0.45 J 1.50 0.39 J 1.20 0.48 J 1.80 0.40 JB
Mercury 1 ----ND ND ND ND ND ND ND ND 0.040 J ND ND ND ND ND ND ND 0.018 J ND ND
Nickel 100 ----ND ND ND ND 2.40 J 2.3 J 1.2 J 1.5 J 1.5 J 1.5 J ND 3.40 0.64 J 0.68 J 0.72 J 0.53 J 1.1 J 1.5 J 0.82 J
Selenium 20 ----ND ND ND ND ND 3.7 J ND 3.00 ND 1.1 J 0.63 J 0.26 J 0.18 J ND ND ND ND ND ND
Silver 20 ----ND 3.13 JB 4.54 JB 0.930 JB ND ND 0.22 J ND 0.12 J 0.18 J ND ND ND ND ND ND ND 0.030 J 0.046 J
Thallium 0.2 ----ND ND ND ND ND ND 0.76 J ND 0.14 J 0.49 J ND ND ND 0.046 J 0.24 J 0.053 J 0.034 J 0.051 J 0.055 J
Vanadium 0.3 ----ND ND ND 8.19 J ND 6.8 7.30 12 B 5.30 4.1 J 1.3 J 2.9 JB 3.0 J 6.20 ND 2.8 J ND 4.6 J ND
Zinc 1000 ----9.05 J 6.31 J 11.5 2.19 J 11.9 B 21 J 5.4 J 9.1 J 19.00 31 B 9.5 J 11.00 9.8 J 5.0 J 6.2 J 15 7.5 J 9.8 J 18
Acetone 6000 8.11 J 5.57 J ND ND ND ND ND ND ND ND 5 ND 1.9 J ND 9.8 ND ND ND NDMethylene Chloride
(Dichloromethane)5 ----5.93 0.400 JB 0.290 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
delta-BHC NE ----ND ND ND ND 0.0197 JD ND ND ND ND ND ND ND ND ND ND NA NA NA NA
gamma-BHC 0.03 ----ND ND ND 0.0233 J ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
Toluene 1000 ----0.270 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
Fluoride 1000 ----ND ND ND ND ND 69 J ND 78 J 90 100 80 J 56 J 82 J 60 J 43 J NA NA NA NA
Phenol 30 ----10 6 2 4 ND 40 J 30 J ND ND ND ND ND ND ND ND NA NA NA NA
SW-2 Antimony 1 ----ND ND ND ND ND ND 0.31 J 7.10 0.44 J 0.25 J ND ND ND 0.17 J ND 0.080 J ND 0.48 J 0.45 J
Arsenic 10 ----ND 6.72 J ND ND ND ND 0.40 J 3.20 0.22 J 0.59 J 0.89 J 1.10 ND 0.97 J ND 0.78 J 0.68 J 0.77 J 0.52 J
Barium 700 ----64.7 JB 43.0 JB 50.6 JB 27.1 J 46.8 JB 37 23 34 24 35 21 30 24 24 24 25 34 27 26
Beryllium 4 ----6.18 JB ND 4.52 ND ND ND ND ND ND ND ND ND 0.040 J 0.037 J ND ND 0.049 J 0.15 J 0.092 J
Cadmium 2 ----0.140 J ND ND ND ND ND ND ND ND ND ND 0.13 J 0.036 J ND ND 0.063 J 0.15 J 0.093 J 0.073 J
Chromium 10 ----2.92 JB 5.83 JB 4.25 JB 2.87 JB 3.21 J 1.1 J 2.00 2.00 2.5 B ND 1.70 ND ND 0.16 J 0.57 J 0.60 J 1.7 JB 1.80 1.2 JB
Cobalt 1 ----7.34 J 3.57 J 3.57 J 1.81 J 2.25 J 1.9 J 0.69 J 2.60 1.10 1.90 0.73 J 1.80 0.37 J 0.93 J 0.61 J 0.81 J 0.85 J 0.85 J 0.38 J
Copper 1000 ----6.24 JB 7.42 JB 5.03 JB 3.53 JB 3.78 JB 1.7 J 0.66 J 1.3 J 1.5 J 1.5 J 0.73 J 1.0 J ND 2.0 J 0.42 J 1.2 J 1.4 J 3.0 J 0.90 JB
Lead 15 ----ND ND 6.93 JB ND ND ND 0.41 J 1.00 1.00 0.77 J 0.62 J 1.20 0.48 J 1.40 0.26 J 1.10 0.60 J 1.70 0.40 JB
Mercury 1 ----ND ND ND ND ND ND ND ND 0.040 J ND ND ND ND ND ND ND ND ND NDNickel100----ND ND ND ND 3.13 J ND 0.92 J 1.3J 2.30 1.3 J ND 0.72 J 0.38 J 0.79 J 0.73 J 1.0 J 1.0 J 1.2 J 0.75 J
Selenium 20 ----ND ND ND ND ND ND ND 2.10 ND 0.85 J 0.93 J 0.37 J ND ND ND ND ND ND ND
Silver 20 ----ND 3.39 JB 4.61 JB ND ND ND ND ND 0.080 J ND ND 0.093 J ND ND ND 0.11 J ND 0.074 J 0.058 J
Thallium 0.2 ----ND ND ND ND ND ND 0.16 J ND ND ND ND 0.40 J 0.19 J 0.036 J 0.20 J 0.073 J 0.031 J 0.056 J 0.069 J
Vanadium 0.3 ----5.61 J ND ND 7.90 J ND 5.6 8.2 13 B 3.2 J 3.6 J 1.4 J 6.9 B 3.5 J 7.4 1.6 J ND ND 4.7 J ND
Zinc 1000 ----30.1 8.96 J 9.56 J ND 14.4 B 3.7 J 3.8 J 7.2 J 18.0 22 B 5.9 J 6.3 J 10.0 5.1 J 3.6 J 16 8.9J 9.6 J 19
Acetone 6000 ----6.08 J 6.67 J ND ND ND ND ND ND 2.6 JB ND 14 ND 1.4 J ND ND ND ND ND ND
Methylene Chloride
(Dichloromethane)5 ----0.600 J 0.210 JB 0.430 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 600 ----ND 0.180 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
alpha-BHC NE ----ND ND ND ND 0.0109 JD ND ND ND ND ND ND ND ND ND ND NA NA NA NA
beta-BHC NE ----ND 0.136 JD ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NAdelta -BHC NE ----ND ND ND 0.0124 J 0.0198 JD ND ND ND ND ND ND ND ND ND ND NA NA NA NA
Fluoride 1000 ----ND ND ND ND ND 130 ND 49 J ND 87 80 J 53 J 93 J 57 J 45 J NA NA NA NA
Phenol 30 ----7 10 2 ND ND 47 J 74 ND ND ND ND ND ND ND ND NA NA NA NA
Notes:NCAC 2L STD = Groundwater Quality Standard under Title 15A of North Carolina Administrative
Code Subchapter 2L
* - Solid Waste Section Groundwater Protection Standard (SWS GWP Standard)
Laboratory results in bold exceed 15A NCAC 2L or 3B Standard or SWS GWP Standard
ND - Not Detected above the Laboratory Reporting Limit
NA = Not analyzed
NE - Not Established
NS = Not sampled
J = Estimated value above laboratory method detection limit and below SWSL or reporting limit.
D = Detected, but RPD is >40% between results in dual column method.

11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
APPENDIX A

Groundwater Sampling Forms

11112 BRANDING IRON PLACE, WENDELL, NC 27591
919-366-3663 Office ● 919-995-0363 Cell ● [e-mail]
APPENDIX B

Laboratory Reports
And
Chain-of-Custody Records

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
12/06/2016
Nautilus Geologic Consulting, PLLC
Brian S. Boutin
11112 Branding Iron Place
Wendell, NC 27591
Project: Nash County MSW Landfill
Project No.: 64-01
Lab Submittal Date: 11/09/2016
Prism Work Order: 6110189
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A Reporting limit raised to 2 ug/L on samples associated with this batch.
Aa Reporting limit raised to 2 ug/L on the samples associated with this batch
Ab Reporting limit raised to 5 ug/L on samples associated with this batch.
B Analyte is found in the associated blank at a concentration >1/2 RL.
E Estimated concentration above the calibration range
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 56
Sample Receipt Summary
12/06/2016
Prism Work Order: 6110189
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6110189-01 11/07/166401-Trip Blank 11/09/16Water
6110189-02 11/07/166401-MW1 11/09/16Water
6110189-03 11/07/166401-MW4 11/09/16Water
6110189-04 11/07/166401-SW2 11/09/16Water
6110189-05 11/07/166401-SW1 11/09/16Water
6110189-06 11/07/166401-MW5 11/09/16Water
6110189-07 11/08/166401-3 11/09/16Water
6110189-08 11/08/166401-6 11/09/16Water
6110189-09 11/08/166401-8S 11/09/16Water
6110189-10 11/08/166401-8D 11/09/16Water
6110189-11 11/08/166401-MW7S 11/09/16Water
6110189-12 11/08/166401-MW7D 11/09/16Water
6110189-13 11/08/166401-MW2R 11/09/16Water
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 56
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6110189
12/06/2016
Summary of Detections
24 ug/L6110189-02 6401-MW1 Barium 6020B
0.060 J ug/L6110189-02 6401-MW1 Beryllium 6020B
0.091 J ug/L6110189-02 6401-MW1 Cadmium 6020B
1.4 J, B ug/L6110189-02 6401-MW1 Chromium 6020B
0.55 J ug/L6110189-02 6401-MW1 Cobalt 6020B
0.59 J, B ug/L6110189-02 6401-MW1 Copper 6020B
0.17 J, B ug/L6110189-02 6401-MW1 Lead 6020B
2.2 ug/L6110189-02 6401-MW1 Nickel 6020B
0.012 J ug/L6110189-02 6401-MW1 Silver 6020B
0.056 J ug/L6110189-02 6401-MW1 Thallium 6020B
22 ug/L6110189-02RE1 6401-MW1 Zinc 6020B
0.31 J ug/L6110189-03 6401-MW4 Arsenic 6020B
150 ug/L6110189-03 6401-MW4 Barium 6020B
0.18 J ug/L6110189-03 6401-MW4 Beryllium 6020B
2.6 ug/L6110189-03 6401-MW4 Cadmium 6020B
1.6 J, B ug/L6110189-03 6401-MW4 Chromium 6020B
51 ug/L6110189-03 6401-MW4 Cobalt 6020B
1.9 J, B ug/L6110189-03 6401-MW4 Copper 6020B
0.95 J, B ug/L6110189-03 6401-MW4 Lead 6020B
3.5 ug/L6110189-03 6401-MW4 Nickel 6020B
0.036 J ug/L6110189-03 6401-MW4 Silver 6020B
0.033 J ug/L6110189-03 6401-MW4 Thallium 6020B
42 ug/L6110189-03RE1 6401-MW4 Zinc 6020B
0.45 J ug/L6110189-04 6401-SW2 Antimony 6020B
0.52 J ug/L6110189-04 6401-SW2 Arsenic 6020B
26 ug/L6110189-04 6401-SW2 Barium 6020B
0.092 J ug/L6110189-04 6401-SW2 Beryllium 6020B
0.073 J ug/L6110189-04 6401-SW2 Cadmium 6020B
1.2 J, B ug/L6110189-04 6401-SW2 Chromium 6020B
0.38 J ug/L6110189-04 6401-SW2 Cobalt 6020B
0.90 J, B ug/L6110189-04 6401-SW2 Copper 6020B
0.40 J, B ug/L6110189-04 6401-SW2 Lead 6020B
0.75 J ug/L6110189-04 6401-SW2 Nickel 6020B
0.058 J ug/L6110189-04 6401-SW2 Silver 6020B
0.069 J ug/L6110189-04 6401-SW2 Thallium 6020B
19 ug/L6110189-04RE1 6401-SW2 Zinc 6020B
0.25 J ug/L6110189-05 6401-SW1 Antimony 6020B
0.44 J ug/L6110189-05 6401-SW1 Arsenic 6020B
28 ug/L6110189-05 6401-SW1 Barium 6020B
0.081 J ug/L6110189-05 6401-SW1 Beryllium 6020B
0.065 J ug/L6110189-05 6401-SW1 Cadmium 6020B
1.2 J, B ug/L6110189-05 6401-SW1 Chromium 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 56
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6110189
12/06/2016
Summary of Detections
0.70 J ug/L6110189-05 6401-SW1 Cobalt 6020B
0.68 J, B ug/L6110189-05 6401-SW1 Copper 6020B
0.40 J, B ug/L6110189-05 6401-SW1 Lead 6020B
0.82 J ug/L6110189-05 6401-SW1 Nickel 6020B
0.046 J ug/L6110189-05 6401-SW1 Silver 6020B
0.055 J ug/L6110189-05 6401-SW1 Thallium 6020B
18 ug/L6110189-05RE1 6401-SW1 Zinc 6020B
0.19 J ug/L6110189-06 6401-MW5 Antimony 6020B
6.3 ug/L6110189-06 6401-MW5 Barium 6020B
0.30 J ug/L6110189-06 6401-MW5 Beryllium 6020B
0.11 J ug/L6110189-06 6401-MW5 Cadmium 6020B
1.3 J, B ug/L6110189-06 6401-MW5 Chromium 6020B
0.18 J ug/L6110189-06 6401-MW5 Cobalt 6020B
1.5 J, B ug/L6110189-06 6401-MW5 Copper 6020B
0.54 J, B ug/L6110189-06 6401-MW5 Lead 6020B
1.1 J ug/L6110189-06 6401-MW5 Nickel 6020B
0.041 J ug/L6110189-06 6401-MW5 Silver 6020B
0.045 J ug/L6110189-06 6401-MW5 Thallium 6020B
23 ug/L6110189-06RE1 6401-MW5 Zinc 6020B
0.19 J ug/L6110189-07 6401-3 Antimony 6020B
0.57 J ug/L6110189-07 6401-3 Arsenic 6020B
55 ug/L6110189-07 6401-3 Barium 6020B
0.091 J ug/L6110189-07 6401-3 Beryllium 6020B
0.10 J ug/L6110189-07 6401-3 Cadmium 6020B
0.97 J, B ug/L6110189-07 6401-3 Chromium 6020B
59 ug/L6110189-07 6401-3 Cobalt 6020B
1.6 J, B ug/L6110189-07 6401-3 Copper 6020B
0.48 J, B ug/L6110189-07 6401-3 Lead 6020B
2.8 ug/L6110189-07 6401-3 Nickel 6020B
0.034 J ug/L6110189-07 6401-3 Silver 6020B
0.074 J ug/L6110189-07 6401-3 Thallium 6020B
0.98 ug/L6110189-07 6401-3 Ethylbenzene 8260B
60 ug/L6110189-07 6401-3 Tetrahydrofuran 8260B
26 ug/L6110189-07RE1 6401-3 Zinc 6020B
0.095 J ug/L6110189-08 6401-6 Antimony 6020B
57 ug/L6110189-08 6401-6 Barium 6020B
0.051 J ug/L6110189-08 6401-6 Beryllium 6020B
0.12 J ug/L6110189-08 6401-6 Cadmium 6020B
1.3 J, B ug/L6110189-08 6401-6 Chromium 6020B
0.26 J ug/L6110189-08 6401-6 Cobalt 6020B
1.3 J, B ug/L6110189-08 6401-6 Copper 6020B
2.1 B ug/L6110189-08 6401-6 Lead 6020B
1.5 J ug/L6110189-08 6401-6 Nickel 6020B
0.040 J ug/L6110189-08 6401-6 Silver 6020B
0.037 J ug/L6110189-08 6401-6 Thallium 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 56
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6110189
12/06/2016
Summary of Detections
1.3 ug/L6110189-08 6401-6 1,1-Dichloroethane 8260B
3.0 ug/L6110189-08 6401-6 1,4-Dichlorobenzene 8260B
1.6 ug/L6110189-08 6401-6 Benzene 8260B
3.3 ug/L6110189-08 6401-6 Chlorobenzene 8260B
3.3 ug/L6110189-08 6401-6 cis-1,2-Dichloroethylene 8260B
1.2 ug/L6110189-08 6401-6 Methylene Chloride 8260B
1.2 ug/L6110189-08 6401-6 o-Xylene 8260B
0.56 ug/L6110189-08 6401-6 Trichloroethylene 8260B
1.2 J ug/L6110189-08 6401-6 Xylenes, total 8260B
24 ug/L6110189-08RE1 6401-6 Zinc 6020B
0.091 J ug/L6110189-09 6401-8S Antimony 6020B
8.3 ug/L6110189-09 6401-8S Barium 6020B
0.062 J ug/L6110189-09 6401-8S Beryllium 6020B
0.38 J ug/L6110189-09 6401-8S Cadmium 6020B
3.4 J, B ug/L6110189-09 6401-8S Chromium 6020B
0.41 J ug/L6110189-09 6401-8S Cobalt 6020B
1.5 J, B ug/L6110189-09 6401-8S Copper 6020B
1.1 J, B ug/L6110189-09 6401-8S Lead 6020B
1.4 J ug/L6110189-09 6401-8S Nickel 6020B
0.048 J ug/L6110189-09 6401-8S Silver 6020B
0.031 J ug/L6110189-09 6401-8S Thallium 6020B
3.2 J ug/L6110189-09 6401-8S Vanadium 6020B
24 ug/L6110189-09RE1 6401-8S Zinc 6020B
0.071 J ug/L6110189-10 6401-8D Antimony 6020B
5.4 ug/L6110189-10 6401-8D Barium 6020B
0.22 J ug/L6110189-10 6401-8D Cadmium 6020B
1.3 J, B ug/L6110189-10 6401-8D Chromium 6020B
0.037 J ug/L6110189-10 6401-8D Cobalt 6020B
0.14 J, B ug/L6110189-10 6401-8D Lead 6020B
0.56 J ug/L6110189-10 6401-8D Nickel 6020B
0.017 J ug/L6110189-10 6401-8D Silver 6020B
0.022 J ug/L6110189-10 6401-8D Thallium 6020B
3.4 ug/L6110189-10 6401-8D 1,1-Dichloroethane 8260B
3.0 ug/L6110189-10 6401-8D cis-1,2-Dichloroethylene 8260B
4.4 ug/L6110189-10 6401-8D Methylene Chloride 8260B
2.0 ug/L6110189-10 6401-8D Trichloroethylene 8260B
18 ug/L6110189-10RE1 6401-8D Zinc 6020B
0.15 J ug/L6110189-11 6401-MW7S Antimony 6020B
0.88 J ug/L6110189-11 6401-MW7S Arsenic 6020B
10 ug/L6110189-11 6401-MW7S Barium 6020B
0.21 J ug/L6110189-11 6401-MW7S Beryllium 6020B
0.63 J ug/L6110189-11 6401-MW7S Cadmium 6020B
2.6 J, B ug/L6110189-11 6401-MW7S Chromium 6020B
0.54 J ug/L6110189-11 6401-MW7S Cobalt 6020B
6.9 ug/L6110189-11 6401-MW7S Copper 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 56
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6110189
12/06/2016
Summary of Detections
1.7 J, B ug/L6110189-11 6401-MW7S Lead 6020B
4.6 ug/L6110189-11 6401-MW7S Nickel 6020B
0.041 J ug/L6110189-11 6401-MW7S Silver 6020B
0.051 J ug/L6110189-11 6401-MW7S Thallium 6020B
3.2 J ug/L6110189-11 6401-MW7S Vanadium 6020B
1400 E ug/L6110189-11RE1 6401-MW7S Zinc 6020B
0.050 J ug/L6110189-12 6401-MW7D Mercury 7470A
0.23 J ug/L6110189-12 6401-MW7D Antimony 6020B
0.49 J ug/L6110189-12 6401-MW7D Arsenic 6020B
3.9 J ug/L6110189-12 6401-MW7D Barium 6020B
0.054 J ug/L6110189-12 6401-MW7D Beryllium 6020B
0.42 J ug/L6110189-12 6401-MW7D Cadmium 6020B
1.1 J, B ug/L6110189-12 6401-MW7D Chromium 6020B
0.22 J ug/L6110189-12 6401-MW7D Cobalt 6020B
0.48 J ug/L6110189-12 6401-MW7D Copper 6020B
0.33 J ug/L6110189-12 6401-MW7D Lead 6020B
1.4 J ug/L6110189-12 6401-MW7D Nickel 6020B
0.055 J ug/L6110189-12 6401-MW7D Silver 6020B
0.23 J ug/L6110189-12 6401-MW7D Thallium 6020B
6.1 ug/L6110189-12 6401-MW7D 1,1-Dichloroethane 8260B
0.91 ug/L6110189-12 6401-MW7D 1,4-Dichlorobenzene 8260B
1.6 ug/L6110189-12 6401-MW7D Benzene 8260B
9.0 ug/L6110189-12 6401-MW7D cis-1,2-Dichloroethylene 8260B
9.5 ug/L6110189-12 6401-MW7D Methylene Chloride 8260B
2.0 ug/L6110189-12 6401-MW7D Tetrachloroethylene 8260B
4.4 ug/L6110189-12 6401-MW7D Trichloroethylene 8260B
19 ug/L6110189-12RE1 6401-MW7D Zinc 6020B
0.097 J ug/L6110189-13 6401-MW2R Mercury 7470A
0.089 J ug/L6110189-13 6401-MW2R Antimony 6020B
20 ug/L6110189-13 6401-MW2R Barium 6020B
0.35 J ug/L6110189-13 6401-MW2R Beryllium 6020B
0.92 J ug/L6110189-13 6401-MW2R Cadmium 6020B
1.5 J, B ug/L6110189-13 6401-MW2R Chromium 6020B
1.7 ug/L6110189-13 6401-MW2R Cobalt 6020B
1.7 J ug/L6110189-13 6401-MW2R Copper 6020B
0.33 J ug/L6110189-13 6401-MW2R Lead 6020B
4.9 ug/L6110189-13 6401-MW2R Nickel 6020B
0.13 J ug/L6110189-13 6401-MW2R Silver 6020B
0.24 J ug/L6110189-13 6401-MW2R Thallium 6020B
44 ug/L6110189-13RE1 6401-MW2R Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-01
Prism Work Order: 6110189
Time Collected: 11/07/16 00:00
Time Submitted: 11/09/16 07:40
6401-Trip Blank
64-01
SWSL
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/17/16 22:29KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/17/16 22:29KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/17/16 22:29KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/17/16 22:29KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/17/16 22:29KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/17/16 22:29KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/17/16 22:29KDMug/L 0.075Carbon disulfide 100<0.075
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/17/16 22:29KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/17/16 22:29KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/17/16 22:29KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/17/16 22:29KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/17/16 22:29KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-01
Prism Work Order: 6110189
Time Collected: 11/07/16 00:00
Time Submitted: 11/09/16 07:40
6401-Trip Blank
64-01
SWSL
8260B P6K043011.0 11/17/16 22:29KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/17/16 22:29KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/17/16 22:29KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/17/16 22:29KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/17/16 22:29KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/17/16 22:29KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124101 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123114 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-02
Prism Work Order: 6110189
Time Collected: 11/07/16 09:40
Time Submitted: 11/09/16 07:40
6401-MW1
64-01
SWSL
Total Metals
7470A P6K043810.20 11/18/16 13:45JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:04bgmug/L 0.069Antimony6<0.069
6020B P6K023411.0 11/15/16 22:04bgmug/L 0.29Arsenic10<0.29
6020B P6K023415.0 11/15/16 22:04 bgmug/L 0.041Barium10024
6020B P6K023411.0 11/15/16 22:04 bgmJug/L 0.047Beryllium10.060
6020B P6K023411.0 11/15/16 22:04 bgmJug/L 0.019Cadmium10.091
6020B P6K023415.0 11/15/16 22:04 bgmJ, B ug/L 0.51Chromium101.4
6020B P6K023411.0 11/15/16 22:04 bgmJug/L 0.013Cobalt100.55
6020B P6K023415.0 11/15/16 22:04 bgmJ, B ug/L 0.44Copper100.59
6020B P6K023412.0 11/15/16 22:04 bgmJ, B ug/L 0.020Lead100.17
6020B P6K023412.0 11/15/16 22:04 bgmug/L 0.053Nickel502.2
6020B P6K023411.0 11/15/16 22:04bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:04 bgmJug/L 0.011Silver100.012
6020B P6K023411.0 11/15/16 22:04 bgmJug/L 0.0093Thallium5.50.056
6020B P6K023415.0 11/15/16 22:04bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/17/16 23:03KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/17/16 23:03KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/17/16 23:03KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/17/16 23:03KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/17/16 23:03KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/17/16 23:03KDMug/L 0.18Bromomethane10<0.18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-02
Prism Work Order: 6110189
Time Collected: 11/07/16 09:40
Time Submitted: 11/09/16 07:40
6401-MW1
64-01
SWSL
8260B P6K043015.0 11/17/16 23:03KDMug/L 0.075Carbon disulfide 100<0.075
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/17/16 23:03KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/17/16 23:03KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/17/16 23:03KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/17/16 23:03KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/17/16 23:03KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/17/16 23:03KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/17/16 23:03KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/17/16 23:03KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/17/16 23:03KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/17/16 23:03KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/17/16 23:03KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124102 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123114 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-02RE1
Prism Work Order: 6110189
Time Collected: 11/07/16 09:40
Time Submitted: 11/09/16 07:40
6401-MW1
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:01 bgmug/L 0.98Zinc1022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-03
Prism Work Order: 6110189
Time Collected: 11/07/16 14:55
Time Submitted: 11/09/16 07:40
6401-MW4
64-01
SWSL
Total Metals
7470A P6K043810.20 11/18/16 13:49JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:08bgmug/L 0.069Antimony6<0.069
6020B P6K023411.0 11/15/16 22:08 bgmJug/L 0.29Arsenic100.31
6020B P6K023415.0 11/15/16 22:08 bgmug/L 0.041Barium100150
6020B P6K023411.0 11/15/16 22:08 bgmJug/L 0.047Beryllium10.18
6020B P6K023411.0 11/15/16 22:08 bgmug/L 0.019Cadmium12.6
6020B P6K023415.0 11/15/16 22:08 bgmJ, B ug/L 0.51Chromium101.6
6020B P6K023411.0 11/15/16 22:08 bgmug/L 0.013Cobalt1051
6020B P6K023415.0 11/15/16 22:08 bgmJ, B ug/L 0.44Copper101.9
6020B P6K023412.0 11/15/16 22:08 bgmJ, B ug/L 0.020Lead100.95
6020B P6K023412.0 11/15/16 22:08 bgmug/L 0.053Nickel503.5
6020B P6K023411.0 11/15/16 22:08bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:08 bgmJug/L 0.011Silver100.036
6020B P6K023411.0 11/15/16 22:08 bgmJug/L 0.0093Thallium5.50.033
6020B P6K023415.0 11/15/16 22:08bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/17/16 23:37KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/17/16 23:37KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/17/16 23:37KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/17/16 23:37KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/17/16 23:37KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/17/16 23:37KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/17/16 23:37KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-03
Prism Work Order: 6110189
Time Collected: 11/07/16 14:55
Time Submitted: 11/09/16 07:40
6401-MW4
64-01
SWSL
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/17/16 23:37KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/17/16 23:37KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/17/16 23:37KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/17/16 23:37KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/17/16 23:37KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/17/16 23:37KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/17/16 23:37KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/17/16 23:37KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/17/16 23:37KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/17/16 23:37KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/17/16 23:37KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124102 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-03RE1
Prism Work Order: 6110189
Time Collected: 11/07/16 14:55
Time Submitted: 11/09/16 07:40
6401-MW4
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:15 bgmug/L 0.98Zinc1042
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-04
Prism Work Order: 6110189
Time Collected: 11/07/16 15:10
Time Submitted: 11/09/16 07:40
6401-SW2
64-01
SWSL
Total Metals
7470A P6K043810.20 11/18/16 13:53JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.069Antimony60.45
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.29Arsenic100.52
6020B P6K023415.0 11/15/16 22:21 bgmug/L 0.041Barium10026
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.047Beryllium10.092
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.019Cadmium10.073
6020B P6K023415.0 11/15/16 22:21 bgmJ, B ug/L 0.51Chromium101.2
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.013Cobalt100.38
6020B P6K023415.0 11/15/16 22:21 bgmJ, B ug/L 0.44Copper100.90
6020B P6K023412.0 11/15/16 22:21 bgmJ, B ug/L 0.020Lead100.40
6020B P6K023412.0 11/15/16 22:21 bgmJug/L 0.053Nickel500.75
6020B P6K023411.0 11/15/16 22:21bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.011Silver100.058
6020B P6K023411.0 11/15/16 22:21 bgmJug/L 0.0093Thallium5.50.069
6020B P6K023415.0 11/15/16 22:21bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 0:11 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 0:11 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 0:11 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 0:11 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 0:11 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 0:11 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 0:11 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-04
Prism Work Order: 6110189
Time Collected: 11/07/16 15:10
Time Submitted: 11/09/16 07:40
6401-SW2
64-01
SWSL
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 0:11 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 0:11 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 0:11 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 0:11 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 0:11 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 0:11 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 0:11 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 0:11 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 0:11 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 0:11 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 0:11 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123116 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-04RE1
Prism Work Order: 6110189
Time Collected: 11/07/16 15:10
Time Submitted: 11/09/16 07:40
6401-SW2
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:19 bgmug/L 0.98Zinc1019
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-05
Prism Work Order: 6110189
Time Collected: 11/07/16 15:20
Time Submitted: 11/09/16 07:40
6401-SW1
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:12JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.069Antimony60.25
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.29Arsenic100.44
6020B P6K023415.0 11/15/16 22:25 bgmug/L 0.041Barium10028
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.047Beryllium10.081
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.019Cadmium10.065
6020B P6K023415.0 11/15/16 22:25 bgmJ, B ug/L 0.51Chromium101.2
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.013Cobalt100.70
6020B P6K023415.0 11/15/16 22:25 bgmJ, B ug/L 0.44Copper100.68
6020B P6K023412.0 11/15/16 22:25 bgmJ, B ug/L 0.020Lead100.40
6020B P6K023412.0 11/15/16 22:25 bgmJug/L 0.053Nickel500.82
6020B P6K023411.0 11/15/16 22:25bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.011Silver100.046
6020B P6K023411.0 11/15/16 22:25 bgmJug/L 0.0093Thallium5.50.055
6020B P6K023415.0 11/15/16 22:25bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 0:45 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 0:45 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 0:45 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 0:45 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 0:45 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 0:45 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 0:45 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-05
Prism Work Order: 6110189
Time Collected: 11/07/16 15:20
Time Submitted: 11/09/16 07:40
6401-SW1
64-01
SWSL
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 0:45 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 0:45 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 0:45 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 0:45 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 0:45 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 0:45 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 0:45 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 0:45 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 0:45 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 0:45 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 0:45 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124101 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-05RE1
Prism Work Order: 6110189
Time Collected: 11/07/16 15:20
Time Submitted: 11/09/16 07:40
6401-SW1
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:22 bgmug/L 0.98Zinc1018
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-06
Prism Work Order: 6110189
Time Collected: 11/07/16 15:55
Time Submitted: 11/09/16 07:40
6401-MW5
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:23JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:28 bgmJug/L 0.069Antimony60.19
6020B P6K023411.0 11/15/16 22:28bgmug/L 0.29Arsenic10<0.29
6020B P6K023415.0 11/15/16 22:28 bgmug/L 0.041Barium1006.3
6020B P6K023411.0 11/15/16 22:28 bgmJug/L 0.047Beryllium10.30
6020B P6K023411.0 11/15/16 22:28 bgmJug/L 0.019Cadmium10.11
6020B P6K023415.0 11/15/16 22:28 bgmJ, B ug/L 0.51Chromium101.3
6020B P6K023411.0 11/15/16 22:28 bgmJug/L 0.013Cobalt100.18
6020B P6K023415.0 11/15/16 22:28 bgmJ, B ug/L 0.44Copper101.5
6020B P6K023412.0 11/15/16 22:28 bgmJ, B ug/L 0.020Lead100.54
6020B P6K023412.0 11/15/16 22:28 bgmJug/L 0.053Nickel501.1
6020B P6K023411.0 11/15/16 22:28bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:28 bgmJug/L 0.011Silver100.041
6020B P6K023411.0 11/15/16 22:28 bgmJug/L 0.0093Thallium5.50.045
6020B P6K023415.0 11/15/16 22:28bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 1:19 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 1:19 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 1:19 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 1:19 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 1:19 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 1:19 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 1:19 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-06
Prism Work Order: 6110189
Time Collected: 11/07/16 15:55
Time Submitted: 11/09/16 07:40
6401-MW5
64-01
SWSL
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 1:19 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 1:19 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 1:19 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 1:19 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 1:19 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 1:19 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 1:19 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 1:19 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 1:19 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 1:19 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 1:19 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124100 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-06RE1
Prism Work Order: 6110189
Time Collected: 11/07/16 15:55
Time Submitted: 11/09/16 07:40
6401-MW5
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:26 bgmug/L 0.98Zinc1023
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-07
Prism Work Order: 6110189
Time Collected: 11/08/16 08:45
Time Submitted: 11/09/16 07:40
6401-3
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:27JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:32 bgmJug/L 0.069Antimony60.19
6020B P6K023411.0 11/15/16 22:32 bgmJug/L 0.29Arsenic100.57
6020B P6K023415.0 11/15/16 22:32 bgmug/L 0.041Barium10055
6020B P6K023411.0 11/15/16 22:32 bgmJug/L 0.047Beryllium10.091
6020B P6K023411.0 11/15/16 22:32 bgmJug/L 0.019Cadmium10.10
6020B P6K023415.0 11/15/16 22:32 bgmJ, B ug/L 0.51Chromium100.97
6020B P6K023411.0 11/15/16 22:32 bgmug/L 0.013Cobalt1059
6020B P6K023415.0 11/15/16 22:32 bgmJ, B ug/L 0.44Copper101.6
6020B P6K023412.0 11/15/16 22:32 bgmJ, B ug/L 0.020Lead100.48
6020B P6K023412.0 11/15/16 22:32 bgmug/L 0.053Nickel502.8
6020B P6K023411.0 11/15/16 22:32bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:32 bgmJug/L 0.011Silver100.034
6020B P6K023411.0 11/15/16 22:32 bgmJug/L 0.0093Thallium5.50.074
6020B P6K023415.0 11/15/16 22:32bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 1:53 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 1:53 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 1:53 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 1:53 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 1:53 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 1:53 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 1:53 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-07
Prism Work Order: 6110189
Time Collected: 11/08/16 08:45
Time Submitted: 11/09/16 07:40
6401-3
64-01
SWSL
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.061Ethylbenzene10.98
8260B P6K043011.0 11/18/16 1:53 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 1:53 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 1:53 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 1:53 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 1:53 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 1:53 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 1:53 KDMug/L 0.16TetrahydrofuranNE60
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 1:53 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 1:53 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 1:53 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 1:53 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129105 %Dibromofluoromethane
77-123115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-07RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 08:45
Time Submitted: 11/09/16 07:40
6401-3
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:41 bgmug/L 0.98Zinc1026
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-08
Prism Work Order: 6110189
Time Collected: 11/08/16 09:25
Time Submitted: 11/09/16 07:40
6401-6
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:31JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:35 bgmJug/L 0.069Antimony60.095
6020B P6K023411.0 11/15/16 22:35bgmug/L 0.29Arsenic10<0.29
6020B P6K023415.0 11/15/16 22:35 bgmug/L 0.041Barium10057
6020B P6K023411.0 11/15/16 22:35 bgmJug/L 0.047Beryllium10.051
6020B P6K023411.0 11/15/16 22:35 bgmJug/L 0.019Cadmium10.12
6020B P6K023415.0 11/15/16 22:35 bgmJ, B ug/L 0.51Chromium101.3
6020B P6K023411.0 11/15/16 22:35 bgmJug/L 0.013Cobalt100.26
6020B P6K023415.0 11/15/16 22:35 bgmJ, B ug/L 0.44Copper101.3
6020B P6K023412.0 11/15/16 22:35 bgmBug/L 0.020Lead102.1
6020B P6K023412.0 11/15/16 22:35 bgmJug/L 0.053Nickel501.5
6020B P6K023411.0 11/15/16 22:35bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:35 bgmJug/L 0.011Silver100.040
6020B P6K023411.0 11/15/16 22:35 bgmJug/L 0.0093Thallium5.50.037
6020B P6K023415.0 11/15/16 22:35bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0831,1-Dichloroethane 51.3
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 2:27 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 2:27 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.0501,4-Dichlorobenzene 13.0
8260B P6K043015.0 11/18/16 2:27 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 2:27 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.048Benzene11.6
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 2:27 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 2:27 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 2:27 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-08
Prism Work Order: 6110189
Time Collected: 11/08/16 09:25
Time Submitted: 11/09/16 07:40
6401-6
64-01
SWSL
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.062Chlorobenzene33.3
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.056cis-1,2-Dichloroethylene 53.3
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 2:27 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 2:27 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 2:27 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 2:27 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 2:27 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 2:27 KDMug/L 0.083Methylene Chloride 11.2
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.044o-Xylene NE1.2
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 2:27 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 2:27 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.078Trichloroethylene10.56
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 2:27 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 2:27 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 2:27 KDMJug/L 0.15Xylenes, total 51.2
Surrogate Recovery Control Limits
80-124101 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123116 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-08RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 09:25
Time Submitted: 11/09/16 07:40
6401-6
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:45 bgmug/L 0.98Zinc1024
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-09
Prism Work Order: 6110189
Time Collected: 11/08/16 10:35
Time Submitted: 11/09/16 07:40
6401-8S
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:35JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:39 bgmJug/L 0.069Antimony60.091
6020B P6K023411.0 11/15/16 22:39bgmug/L 0.29Arsenic10<0.29
6020B P6K023415.0 11/15/16 22:39 bgmug/L 0.041Barium1008.3
6020B P6K023411.0 11/15/16 22:39 bgmJug/L 0.047Beryllium10.062
6020B P6K023411.0 11/15/16 22:39 bgmJug/L 0.019Cadmium10.38
6020B P6K023415.0 11/15/16 22:39 bgmJ, B ug/L 0.51Chromium103.4
6020B P6K023411.0 11/15/16 22:39 bgmJug/L 0.013Cobalt100.41
6020B P6K023415.0 11/15/16 22:39 bgmJ, B ug/L 0.44Copper101.5
6020B P6K023412.0 11/15/16 22:39 bgmJ, B ug/L 0.020Lead101.1
6020B P6K023412.0 11/15/16 22:39 bgmJug/L 0.053Nickel501.4
6020B P6K023411.0 11/15/16 22:39bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:39 bgmJug/L 0.011Silver100.048
6020B P6K023411.0 11/15/16 22:39 bgmJug/L 0.0093Thallium5.50.031
6020B P6K023415.0 11/15/16 22:39 bgmJug/L 2.5Vanadium253.2
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 3:01 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 3:01 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 3:01 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 3:01 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 3:01 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 3:01 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 3:01 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-09
Prism Work Order: 6110189
Time Collected: 11/08/16 10:35
Time Submitted: 11/09/16 07:40
6401-8S
64-01
SWSL
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 3:01 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 3:01 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 3:01 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 3:01 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 3:01 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 3:01 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 3:01 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 3:01 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 3:01 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 3:01 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 3:01 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-09RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 10:35
Time Submitted: 11/09/16 07:40
6401-8S
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:48 bgmug/L 0.98Zinc1024
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-10
Prism Work Order: 6110189
Time Collected: 11/08/16 11:15
Time Submitted: 11/09/16 07:40
6401-8D
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:39JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:43 bgmJug/L 0.069Antimony60.071
6020B P6K023411.0 11/15/16 22:43bgmug/L 0.29Arsenic10<0.29
6020B P6K023415.0 11/15/16 22:43 bgmug/L 0.041Barium1005.4
6020B P6K023411.0 11/15/16 22:43bgmug/L 0.047Beryllium1<0.047
6020B P6K023411.0 11/15/16 22:43 bgmJug/L 0.019Cadmium10.22
6020B P6K023415.0 11/15/16 22:43 bgmJ, B ug/L 0.51Chromium101.3
6020B P6K023411.0 11/15/16 22:43 bgmJug/L 0.013Cobalt100.037
6020B P6K023415.0 11/15/16 22:43bgmug/L 0.44Copper10<0.44
6020B P6K023412.0 11/15/16 22:43 bgmJ, B ug/L 0.020Lead100.14
6020B P6K023412.0 11/15/16 22:43 bgmJug/L 0.053Nickel500.56
6020B P6K023411.0 11/15/16 22:43bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:43 bgmJug/L 0.011Silver100.017
6020B P6K023411.0 11/15/16 22:43 bgmJug/L 0.0093Thallium5.50.022
6020B P6K023415.0 11/15/16 22:43bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0831,1-Dichloroethane 53.4
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 3:35 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 3:35 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 3:35 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 3:35 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 3:35 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 3:35 KDMug/L 0.18Bromomethane10<0.18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-10
Prism Work Order: 6110189
Time Collected: 11/08/16 11:15
Time Submitted: 11/09/16 07:40
6401-8D
64-01
SWSL
8260B P6K043015.0 11/18/16 3:35 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.056cis-1,2-Dichloroethylene 53.0
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 3:35 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 3:35 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 3:35 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 3:35 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 3:35 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 3:35 KDMug/L 0.083Methylene Chloride 14.4
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 3:35 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 3:35 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.078Trichloroethylene12.0
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 3:35 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 3:35 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 3:35 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123114 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-10RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 11:15
Time Submitted: 11/09/16 07:40
6401-8D
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:51 bgmug/L 0.98Zinc1018
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-11
Prism Work Order: 6110189
Time Collected: 11/08/16 12:30
Time Submitted: 11/09/16 07:40
6401-MW7S
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:42JABug/L 0.030Mercury0.2<0.030
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.069Antimony60.15
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.29Arsenic100.88
6020B P6K023415.0 11/15/16 22:46 bgmug/L 0.041Barium10010
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.047Beryllium10.21
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.019Cadmium10.63
6020B P6K023415.0 11/15/16 22:46 bgmJ, B ug/L 0.51Chromium102.6
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.013Cobalt100.54
6020B P6K044315.0 11/18/16 20:58 gmartug/L 0.44Copper106.9
6020B P6K023412.0 11/15/16 22:46 bgmJ, B ug/L 0.020Lead101.7
6020B P6K023412.0 11/15/16 22:46 bgmug/L 0.053Nickel504.6
6020B P6K023411.0 11/15/16 22:46bgmug/L 0.35Selenium10<0.35
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.011Silver100.041
6020B P6K023411.0 11/15/16 22:46 bgmJug/L 0.0093Thallium5.50.051
6020B P6K023415.0 11/15/16 22:46 bgmJug/L 2.5Vanadium253.2
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 4:43 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 4:43 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 4:43 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 4:43 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 4:43 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 4:43 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 4:43 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-11
Prism Work Order: 6110189
Time Collected: 11/08/16 12:30
Time Submitted: 11/09/16 07:40
6401-MW7S
64-01
SWSL
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 4:43 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 4:43 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 4:43 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 4:43 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 4:43 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 4:43 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 4:43 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 4:43 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 4:43 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 4:43 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 4:43 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124100 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-11RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 12:30
Time Submitted: 11/09/16 07:40
6401-MW7S
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:55 bgmEug/L 0.98Zinc101400
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-12
Prism Work Order: 6110189
Time Collected: 11/08/16 13:10
Time Submitted: 11/09/16 07:40
6401-MW7D
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:46 JABJug/L 0.030Mercury0.20.050
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.069Antimony60.23
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.29Arsenic100.49
6020B P6K026215.0 11/16/16 18:06 bgmJug/L 0.041Barium1003.9
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.047Beryllium10.054
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.019Cadmium10.42
6020B P6K026212.0 11/16/16 18:06 bgmJ, B ug/L 0.51Chromium101.1
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.013Cobalt100.22
6020B P6K026215.0 11/16/16 18:06 bgmJug/L 0.44Copper100.48
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.020Lead100.33
6020B P6K026212.0 11/16/16 18:06 bgmJug/L 0.053Nickel501.4
6020B P6K026211.0 11/16/16 18:06bgmug/L 0.35Selenium10<0.35
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.011Silver100.055
6020B P6K026211.0 11/16/16 18:06 bgmJug/L 0.0093Thallium5.50.23
6020B P6K026215.0 11/16/16 18:06bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0831,1-Dichloroethane 56.1
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 4:09 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 4:09 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.0501,4-Dichlorobenzene 10.91
8260B P6K043015.0 11/18/16 4:09 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 4:09 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.048Benzene11.6
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 4:09 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 4:09 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 4:09 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-12
Prism Work Order: 6110189
Time Collected: 11/08/16 13:10
Time Submitted: 11/09/16 07:40
6401-MW7D
64-01
SWSL
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.056cis-1,2-Dichloroethylene 59.0
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 4:09 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 4:09 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 4:09 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 4:09 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 4:09 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 4:09 KDMug/L 0.083Methylene Chloride 19.5
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.098Tetrachloroethylene12.0
8260B P6K043011011/18/16 4:09 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 4:09 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.078Trichloroethylene14.4
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 4:09 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 4:09 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 4:09 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124103 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123113 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-12RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 13:10
Time Submitted: 11/09/16 07:40
6401-MW7D
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 18:58 bgmug/L 0.98Zinc1019
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-13
Prism Work Order: 6110189
Time Collected: 11/08/16 13:50
Time Submitted: 11/09/16 07:40
6401-MW2R
64-01
SWSL
Total Metals
7470A P6K043910.20 11/18/16 14:50 JABJug/L 0.030Mercury0.20.097
6020B P6K026211.0 11/16/16 18:18 bgmJug/L 0.069Antimony60.089
6020B P6K026211.0 11/16/16 18:18bgmug/L 0.29Arsenic10<0.29
6020B P6K026215.0 11/16/16 18:18 bgmug/L 0.041Barium10020
6020B P6K026211.0 11/16/16 18:18 bgmJug/L 0.047Beryllium10.35
6020B P6K026211.0 11/16/16 18:18 bgmJug/L 0.019Cadmium10.92
6020B P6K026212.0 11/16/16 18:18 bgmJ, B ug/L 0.51Chromium101.5
6020B P6K026211.0 11/16/16 18:18 bgmug/L 0.013Cobalt101.7
6020B P6K026215.0 11/16/16 18:18 bgmJug/L 0.44Copper101.7
6020B P6K026211.0 11/16/16 18:18 bgmJug/L 0.020Lead100.33
6020B P6K026212.0 11/16/16 18:18 bgmug/L 0.053Nickel504.9
6020B P6K026211.0 11/16/16 18:18bgmug/L 0.35Selenium10<0.35
6020B P6K026211.0 11/16/16 18:18 bgmJug/L 0.011Silver100.13
6020B P6K026211.0 11/16/16 18:18 bgmJug/L 0.0093Thallium5.50.24
6020B P6K026215.0 11/16/16 18:18bgmug/L 2.5Vanadium25<2.5
Volatile Organic Compounds by GC/MS
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P6K043011.0 11/18/16 5:17 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P6K043012.0 11/18/16 5:17 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P6K043015.0 11/18/16 5:17 KDMug/L 0.31Acetone100<0.31
8260B P6K043012011/18/16 5:17 KDMug/L 0.20Acrylonitrile200<0.20
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.048Benzene1<0.048
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.14Bromochloromethane3<0.14
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P6K043011.0 11/18/16 5:17 KDMug/L 0.040Bromoform3<0.040
8260B P6K043011.0 11/18/16 5:17 KDMug/L 0.18Bromomethane10<0.18
8260B P6K043015.0 11/18/16 5:17 KDMug/L 0.075Carbon disulfide 100<0.075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-13
Prism Work Order: 6110189
Time Collected: 11/08/16 13:50
Time Submitted: 11/09/16 07:40
6401-MW2R
64-01
SWSL
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.062Chlorobenzene3<0.062
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.22Chloroethane10<0.22
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.076Chloroform5<0.076
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.079Chloromethane1<0.079
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.065Dibromomethane10<0.065
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.061Ethylbenzene1<0.061
8260B P6K043011.0 11/18/16 5:17 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P6K043015.0 11/18/16 5:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P6K043015.0 11/18/16 5:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P6K043015.0 11/18/16 5:17 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P6K043015.0 11/18/16 5:17 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P6K043011.0 11/18/16 5:17 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.044o-Xylene NE<0.044
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.047Styrene1<0.047
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P6K043011011/18/16 5:17 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.044Toluene1<0.044
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P6K043011011/18/16 5:17 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.078Trichloroethylene1<0.078
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P6K043012.0 11/18/16 5:17 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P6K043010.50 11/18/16 5:17 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P6K043013.0 11/18/16 5:17 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124105 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123114 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 56
Laboratory Report
12/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
11112 Branding Iron Place Project No.:
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 6110189-13RE1
Prism Work Order: 6110189
Time Collected: 11/08/16 13:50
Time Submitted: 11/09/16 07:40
6401-MW2R
64-01
SWSL
Total Metals
6020B P6K054911011/28/16 19:02 bgmug/L 0.98Zinc1044
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6K0430 - 5030B
Blank (P6K0430-BLK1)Prepared & Analyzed: 11/17/16
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6K0430 - 5030B
Blank (P6K0430-BLK1)Prepared & Analyzed: 11/17/16
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10050.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10552.6
ug/L 50.00 77-123Surrogate: Toluene-d8 11457.2
LCS (P6K0430-BS1)Prepared & Analyzed: 11/17/16
1,1-Dichloroethylene ug/L17.3 0.50 20.00 70-15487
Benzene ug/L16.3 0.50 20.00 77-12881
Chlorobenzene ug/L19.7 0.50 20.00 78-11998
Tetrahydrofuran ug/L17.4 10 20.00 70-13087
Toluene ug/L16.2 0.50 20.00 76-13181
Trichloroethylene ug/L16.3 0.50 20.00 77-13381
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10150.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 77-123Surrogate: Toluene-d8 11658.0
LCS Dup (P6K0430-BSD1)Prepared & Analyzed: 11/17/16
1,1-Dichloroethylene ug/L21.1 0.50 20.00 2070-154106 20
Benzene ug/L18.6 0.50 20.00 2077-12893 13
Chlorobenzene ug/L23.2 0.50 20.00 2078-119116 16
Tetrahydrofuran ug/L18.9 10 20.00 2070-13095 9
Toluene ug/L18.7 0.50 20.00 2076-13194 14
Trichloroethylene ug/L18.9 0.50 20.00 2077-13395 15
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 77-123Surrogate: Toluene-d8 11858.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6K0234 - 3005A
Blank (P6K0234-BLK1)Prepared: 11/10/16 Analyzed: 11/15/16
Antimony ug/L0.400 1.0 J
Arsenic ug/L0.304 1.0 J
Barium ug/L1.48 5.0 J
Beryllium ug/L0.0583 1.0 J
Cadmium ug/L0.0990 1.0 J
Chromium ug/L1.22 1.0 Ab
Cobalt ug/L0.0473 1.0 J
Copper ug/L8.17 5.0 Ab
Lead ug/L0.990 1.0 A, J
Nickel ug/L0.338 2.0 J
Selenium ug/LBRL1.0
Silver ug/L0.0910 1.0 J
Thallium ug/L0.0640 1.0 J
Vanadium ug/LBRL5.0
LCS (P6K0234-BS1)Prepared: 11/10/16 Analyzed: 11/15/16
Antimony ug/L91.2 1.0 100.0 80-12091
Arsenic ug/L87.5 1.0 100.0 80-12087
Barium ug/L92.8 5.0 100.0 80-12093
Beryllium ug/L91.2 1.0 100.0 80-12091
Cadmium ug/L90.5 1.0 100.0 80-12091
Chromium ug/L91.2 1.0 100.0 B80-12091
Cobalt ug/L91.4 1.0 100.0 80-12091
Copper ug/L92.8 5.0 100.0 B80-12093
Lead ug/L93.1 1.0 100.0 B80-12093
Nickel ug/L92.1 2.0 100.0 80-12092
Selenium ug/L87.7 1.0 100.0 80-12088
Silver ug/L93.3 1.0 100.0 80-12093
Thallium ug/L92.1 1.0 100.0 80-12092
Vanadium ug/L90.1 5.0 100.0 80-12090
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6K0262 - 3005A
Blank (P6K0262-BLK1)Prepared: 11/11/16 Analyzed: 11/16/16
Antimony ug/L0.436 1.0 J
Arsenic ug/LBRL1.0
Barium ug/L0.504 5.0 J
Beryllium ug/L0.0547 1.0 J
Cadmium ug/L0.107 1.0 J
Chromium ug/L0.721 1.0 Aa, J
Cobalt ug/L0.0627 1.0 J
Copper ug/LBRL5.0
Lead ug/L0.347 1.0 J
Nickel ug/L0.496 2.0 J
Selenium ug/LBRL1.0
Silver ug/L0.0653 1.0 J
Thallium ug/L0.0823 1.0 J
Vanadium ug/LBRL5.0
LCS (P6K0262-BS1)Prepared: 11/11/16 Analyzed: 11/16/16
Antimony ug/L99.9 1.0 100.0 80-120100
Arsenic ug/L95.7 1.0 100.0 80-12096
Barium ug/L1015.0 100.0 80-120101
Beryllium ug/L97.5 1.0 100.0 80-12097
Cadmium ug/L99.4 1.0 100.0 80-12099
Chromium ug/L99.3 1.0 100.0 B80-12099
Cobalt ug/L99.6 1.0 100.0 80-120100
Copper ug/L1015.0 100.0 80-120101
Lead ug/L1011.0 100.0 80-120101
Nickel ug/L1012.0 100.0 80-120101
Selenium ug/L93.7 1.0 100.0 80-12094
Silver ug/L1021.0 100.0 80-120102
Thallium ug/L99.3 1.0 100.0 80-12099
Vanadium ug/L98.0 5.0 100.0 80-12098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6K0262 - 3005A
Matrix Spike (P6K0262-MS1)Prepared: 11/11/16 Analyzed: 11/16/16 Source: 6110189-12
Antimony ug/L97.7 1.0 100.0 0.226 75-12597
Arsenic ug/L94.7 1.0 100.0 0.491 75-12594
Barium ug/L1045.0 100.0 3.92 75-125100
Beryllium ug/L96.4 1.0 100.0 0.0543 75-12596
Cadmium ug/L97.7 1.0 100.0 0.422 75-12597
Chromium ug/L98.1 1.0 100.0 1.14 B75-12597
Cobalt ug/L99.1 1.0 100.0 0.225 75-12599
Copper ug/L99.6 5.0 100.0 0.481 75-12599
Lead ug/L99.0 1.0 100.0 0.331 75-12599
Nickel ug/L99.9 2.0 100.0 1.36 75-12599
Selenium ug/L92.8 1.0 100.0 BRL 75-12593
Silver ug/L1011.0 100.0 0.0547 75-125101
Thallium ug/L98.0 1.0 100.0 0.228 75-12598
Vanadium ug/L98.0 5.0 100.0 BRL 75-12598
Matrix Spike Dup (P6K0262-MSD1)Prepared: 11/11/16 Analyzed: 11/16/16 Source: 6110189-12
Antimony ug/L96.0 1.0 100.0 0.226 2075-12596 2
Arsenic ug/L93.4 1.0 100.0 0.491 2075-12593 1
Barium ug/L1015.0 100.0 3.92 2075-12597 2
Beryllium ug/L95.8 1.0 100.0 0.0543 2075-12596 0.6
Cadmium ug/L95.9 1.0 100.0 0.422 2075-12596 2
Chromium ug/L96.2 1.0 100.0 1.14 20 B75-12595 2
Cobalt ug/L97.0 1.0 100.0 0.225 2075-12597 2
Copper ug/L98.5 5.0 100.0 0.481 2075-12598 1
Lead ug/L96.2 1.0 100.0 0.331 2075-12596 3
Nickel ug/L98.5 2.0 100.0 1.36 2075-12597 1
Selenium ug/L91.2 1.0 100.0 BRL 2075-12591 2
Silver ug/L98.2 1.0 100.0 0.0547 2075-12598 3
Thallium ug/L95.4 1.0 100.0 0.228 2075-12595 3
Vanadium ug/L96.0 5.0 100.0 BRL 2075-12596 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6K0262 - 3005A
Post Spike (P6K0262-PS1)Prepared: 11/11/16 Analyzed: 11/16/16 Source: 6110189-12
Antimony ug/L93.8 100.0 0.226 80-12094
Arsenic ug/L92.8 100.0 0.491 80-12092
Barium ug/L100 100.0 3.92 80-12096
Beryllium ug/L94.2 100.0 0.0543 80-12094
Cadmium ug/L96.4 100.0 0.422 80-12096
Chromium ug/L95.1 100.0 1.14 B80-12094
Cobalt ug/L95.6 100.0 0.225 80-12095
Copper ug/L95.7 100.0 0.481 80-12095
Lead ug/L95.6 100.0 0.331 80-12095
Nickel ug/L97.0 100.0 1.36 80-12096
Selenium ug/L91.7 100.0 0.0820 80-12092
Silver ug/L93.5 100.0 0.0547 80-12093
Thallium ug/L95.0 100.0 0.228 80-12095
Vanadium ug/L93.5 100.0 0.359 80-12093
Batch P6K0438 - 7470A
Blank (P6K0438-BLK1)Prepared & Analyzed: 11/18/16
Mercury ug/LBRL0.20
LCS (P6K0438-BS1)Prepared & Analyzed: 11/18/16
Mercury ug/L9.44 0.20 9.375 80-120101
Batch P6K0439 - 7470A
Blank (P6K0439-BLK1)Prepared & Analyzed: 11/18/16
Mercury ug/LBRL0.20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6K0439 - 7470A
LCS (P6K0439-BS1)Prepared & Analyzed: 11/18/16
Mercury ug/L9.16 0.20 9.375 80-12098
Matrix Spike (P6K0439-MS1)Prepared & Analyzed: 11/18/16 Source: 6110189-05
Mercury ug/L9.62 0.20 9.375 BRL 80-120103
Matrix Spike Dup (P6K0439-MSD1)Prepared & Analyzed: 11/18/16 Source: 6110189-05
Mercury ug/L9.61 0.20 9.375 BRL 2080-120102 0.2
Batch P6K0443 - 3005A
Blank (P6K0443-BLK1)Prepared & Analyzed: 11/18/16
Copper ug/L0.602 5.0 J
LCS (P6K0443-BS1)Prepared & Analyzed: 11/18/16
Copper ug/L95.8 5.0 100.0 80-12096
Batch P6K0549 - 3005A
Blank (P6K0549-BLK1)Prepared: 11/23/16 Analyzed: 11/28/16
Zinc ug/L1.47 10 J
LCS (P6K0549-BS1)Prepared: 11/23/16 Analyzed: 11/28/16
Zinc ug/L99.7 10 100.0 80-120100
Matrix Spike (P6K0549-MS1)Prepared: 11/23/16 Analyzed: 11/28/16 Source: 6110189-02RE1
Zinc ug/L117 10 100.0 21.8 75-12595
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 56
12/6/16
Level II QC Report
11112 Branding Iron Place Project No: 64-01
Project: Nash County MSW LandfillNautilus Geologic Consulting, PLLC
Wendell, NC 27591
Attn: Brian S. Boutin
Prism Work Order: 6110189
Time Submitted: 11/9/2016 7:40:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6K0549 - 3005A
Matrix Spike Dup (P6K0549-MSD1)Prepared: 11/23/16 Analyzed: 11/28/16 Source: 6110189-02RE1
Zinc ug/L118 10 100.0 21.8 2075-12596 0.9
Post Spike (P6K0549-PS1)Prepared: 11/23/16 Analyzed: 11/28/16 Source: 6110189-02RE1
Zinc ug/L117 100.0 21.8 80-12096
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 56
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P6K02346110189-02 11/10/16 14:5650 50mL mL
P6K05496110189-02RE1 11/23/16 8:1050 50mL mL
P6K02346110189-03 11/10/16 14:5650 50mL mL
P6K05496110189-03RE1 11/23/16 8:1050 50mL mL
P6K02346110189-04 11/10/16 14:5650 50mL mL
P6K05496110189-04RE1 11/23/16 8:1050 50mL mL
P6K02346110189-05 11/10/16 14:5650 50mL mL
P6K05496110189-05RE1 11/23/16 8:1050 50mL mL
P6K02346110189-06 11/10/16 14:5650 50mL mL
P6K05496110189-06RE1 11/23/16 8:1050 50mL mL
P6K02346110189-07 11/10/16 14:5650 50mL mL
P6K05496110189-07RE1 11/23/16 8:1050 50mL mL
P6K02346110189-08 11/10/16 14:5650 50mL mL
P6K05496110189-08RE1 11/23/16 8:1050 50mL mL
P6K02346110189-09 11/10/16 14:5650 50mL mL
P6K05496110189-09RE1 11/23/16 8:1050 50mL mL
P6K02346110189-10 11/10/16 14:5650 50mL mL
P6K05496110189-10RE1 11/23/16 8:1050 50mL mL
P6K04436110189-11 11/18/16 9:5550 50mL mL
P6K02346110189-11 11/10/16 14:5650 50mL mL
P6K05496110189-11RE1 11/23/16 8:1050 50mL mL
P6K02626110189-12 11/11/16 8:3050 50mL mL
P6K05496110189-12RE1 11/23/16 8:1050 50mL mL
P6K02626110189-13 11/11/16 8:3050 50mL mL
P6K05496110189-13RE1 11/23/16 8:1050 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P6K04386110189-02 11/18/16 8:5020 30mL mL
P6K04386110189-03 11/18/16 8:5020 30mL mL
P6K04386110189-04 11/18/16 8:5020 30mL mL
P6K04396110189-05 11/18/16 8:5020 30mL mL
P6K04396110189-06 11/18/16 8:5020 30mL mL
P6K04396110189-07 11/18/16 8:5020 30mL mL
P6K04396110189-08 11/18/16 8:5020 30mL mL
P6K04396110189-09 11/18/16 8:5020 30mL mL
P6K04396110189-10 11/18/16 8:5020 30mL mL
P6K04396110189-11 11/18/16 8:5020 30mL mL
P6K04396110189-12 11/18/16 8:5020 30mL mL
P6K04396110189-13 11/18/16 8:5020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P6K04306110189-01 11/17/16 17:1910 10mL mL
P6K04306110189-02 11/17/16 17:1910 10mL mL
P6K04306110189-03 11/17/16 17:1910 10mL mL
P6K04306110189-04 11/17/16 17:1910 10mL mL
P6K04306110189-05 11/17/16 17:1910 10mL mL
P6K04306110189-06 11/17/16 17:1910 10mL mL
P6K04306110189-07 11/17/16 17:1910 10mL mL
P6K04306110189-08 11/17/16 17:1910 10mL mL
P6K04306110189-09 11/17/16 17:1910 10mL mL
P6K04306110189-10 11/17/16 17:1910 10mL mL
P6K04306110189-11 11/17/16 17:1910 10mL mL
P6K04306110189-12 11/17/16 17:1910 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 56
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P6K04306110189-13 11/17/16 17:1910 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 56
Page 55 of 56
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