5603I_IAC_EMR_DIN27948_2015924

Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]
Pinckney, MI 48169 FAX: [phone]

ABF Environmental
28200 Orchard Lake Rd.
Farmington Hills, MI 48322
RE: Project Name:Old Fort Landfill
Project No:14-1547
Submit Date:9/24/2015
LLL Project Number: 10707-101491
Dear Bob Nawakowski
Enclosed are the results for sample(s) submitted for the above referenced project. Also enclosed are
an invoice and a quality control report.
I certify that the data presented in this report meets both the minimum quality assurance standards
specified in the referenced analytical methodology and the standards established by this laboratory.
I believe the information submitted is true, accurate and complete.
Please contact me directly should you have further questions regarding this analytical. Be advised the
samples will be disposed 60 days from the date of this report. If you would like the samples to be
retained for a longer period of time, please call the office. All data associated with this report will be
retained for five (5) years.
Lakeland Laboratories, Inc. appreciates the opportunity to provide you with quality analytical services.
Sincerely,
Lorri White
President
September 29, 2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101491
Collection Date:9/21/2015
Sample ID:MW-1
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium ND 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101492
Collection Date:9/21/2015
Sample ID:MW-1A
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium ND 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101493
Collection Date:9/21/2015
Sample ID:MW-4
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium 0.3 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101494
Collection Date:9/21/2015
Sample ID:MW-3
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium 0.4 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101495
Collection Date:9/21/2015
Sample ID:MW-2
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium ND 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101496
Collection Date:9/21/2015
Sample ID:SW-1
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium ND 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101497
Collection Date:9/21/2015
Sample ID:SW-2
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium 0.1 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
8290 Pettysville Road Phone: [phone]Pinckney, MI 48169 FAX: [phone]
Certificate of Analysis
Date: September 29, 2015 Customer:ABF Environmental
28200 Orchard Lake Rd.
Project Name:Old Fort Landfill Farmington Hills, MI 48322
Project Number:14-1547
Submit Date:9/24/2015 Lab Sample ID:10707-101498
Collection Date:9/21/2015
Sample ID:SW-4
Method Analysis
Parameters Result LRL Units Reference Date Analyst
Metals Analysis
Digestion QC Batch ID:092415M-1W KEW
Arsenic ND 0.005 mg/L SW846 7060 9/25/2015 LLW
Barium ND 0.1 mg/L SW846 7081 9/25/2015 LLW
Cadmium ND 0.001 mg/L SW846 7131 9/25/2015 LLW
Chromium ND 0.01 mg/L SW846 7190 9/25/2015 LLW
Lead ND 0.003 mg/L SW846 7421 9/25/2015 LLW
Mercury ND 0.001 mg/L SW846 7470 9/26/2015 LLW
Selenium ND 0.005 mg/L SW846 7740 9/25/2015 LLW
Silver ND 0.0002 mg/L SW846 7760 9/28/2015 LLW
Parameter- Analysis performed or the name of the chemical analyzed.
Result- The reported concentration in the sample
Analysis Date- Date the analysis was performed
LRL- Lower Reporting Limit- the LRL is based on MDEQ TDL, dilutions may affect the LRL.
Analyst- Initials of the analyst performing the analysis
Units- The unit which corresponds to the reported concentration
ND- Parameter not detected above the reported LRL
Reviewed By:
Date:9/29/2015
Lorri White
Lakeland Laboratories, Inc.
Metals Batch Quality Control Report
Batch ID:030614M-1X
Metals Batch Quality Control Fortified Sample ID:95354
Method Standard Matrix Spike/Matrix Spike Duplicate
Metal MBlk Spk Conc Conc %Rec.Spk Conc Smp Conc MS MSD
Arsenic ND 50 52.2 104 50 0 52.2 52.6
Barium ND 250 238 95.2 250 41.8 301.4 301.8
Cadmium ND 2.5 2.55 102.0 2.5 0 2.35 2.32
Chromium ND 25 21.8 87.2 20 0 18.7 19
Copper ND NA NA NA
Lead ND 25 21.4 85.6 25 0 24.9 21
Mercury ND 5 4.73 95 5 0 4.11 4.03
Selenium ND 25 21.8 87.2 25 0 28 25.5
Silver ND 1 0.988 98.8 0.75 0 0.757 0.754
Zinc ND NA NA NA
Iron ND NA NA NA
Manganese ND NA NA NA
ND NA NA NA
ND NA NA NA
ND NA NA NA
Note: NA-Not Applicable, spike not required for QC sample batch 1
Note: All Concentrations expressed as mg/L
Accuracy Precision
QA/QC Limits MS MSD Pass QC Limit Pass
Metals Lower Upper %Rec %Rec Fail Upper %RD Fail
Arsenic 80 120 104 105 Pass 20 0.8 Pass
Barium 80 120 103.8 104.0 Pass 20 0.1 Pass
Cadmium 80 120 94.0 92.8 Pass 20 1.3 Pass
Chromium 80 120 93.5 95.0 Pass 20 1.6 Pass
Copper 80 120 20
Lead 80 120 100 84 Pass 20 17.0 Pass
Mercury 80 120 82.2 80.6 Pass 20 2.0 Pass
Selenium 80 120 112.0 102.0 Pass 20 9.3 Pass
Silver 80 120 100.9 100.5 Pass 20 0.4 Pass
Zinc 80 120 20
Iron 80 120 20
Manganese 80 120 20
MBlk Method Blank Percent Recovery/%Rec =MStd*100/Spk Conc
MStd Method Standard Percent Relative Deviation =200(MS-MSD)/(MS+MDS)
MS Matrix Spike (%RD)
MSD Matrix Spike Duplicate Note: Sample Conc. reported as "0" if below DL

Property Lines Shown are Approximate
SITE LOCATION MAP
Figure 1
SOURCE: USGS Delorme 2008
SCALE: 1” = 1,000 Feet Approx
CLIENT: IAC GROUP NA

SITE: OLD FORT LANDFILL

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