5803_MadisonCountyCDLF_GWMR_DIN27934_20160412

Prepared for
Madison County, North Carolina
Project Number 2313.1302

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Spring 2016 Semiannual
Water Quality Monitoring Report
Madison County Operating
Solid Waste Facility
Madison County, North Carolina
Permit No. 58-03
July 6, 2016

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-03, Madison County, North Carolina Page ii
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Spring 2016 Semiannual
Water Quality Monitoring Report
Madison County Operating
Solid Waste Facility
Madison County, North Carolina
Permit No. 58-03
July 6, 2016

Spring 2016 Semiannual Water Quality Monitoring Report July 6, 2016
Permit No. 58-03, Madison County, North Carolina Page iii
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Table of Contents
1.0 Introduction .................................................................................................................... 1
2.0 Methods ......................................................................................................................... 2
2.1 Groundwater Purging and Sampling Methods ..............................................................2
2.2 Surface Water Sampling Methods .................................................................................2
2.3 Leachate Sampling Methods .........................................................................................2
2.4 Sample Handling, Documentation, and Analysis...........................................................3
3.0 Findings .......................................................................................................................... 4
3.1 Analytical Results ..........................................................................................................4
3.1.1 Groundwater Monitoring Wells .........................................................................4
3.1.2 Surface Water ...................................................................................................5
3.1.3 Leachate ...........................................................................................................5
4.0 Hydrogeology .................................................................................................................. 7
5.0 Summary ........................................................................................................................ 8
5.1 Future Activities .............................................................................................................8
6.0 References ..................................................................................................................... 9

Figures
1. Site Location Map
2. Sample Locations
3. Generalized Groundwater Flow
Tables
1. Well Construction Details and Corresponding Elevations
2. Summary of Laboratory Analyses Performed on Samples
3. Groundwater and Surface Water Summary of Analytical Results
4. Leachate Summary of Analytical Results
Appendices
A. Sampling Logs and Equipment Documentation and Instrument Calibration Data Sheets
B. Reports of Laboratory Analysis and Chain-of-Custody Documentation
C. Environmental Monitoring Reporting Form and Electronic Submittal of Environmental Monitoring
Data 5803Apr2016 (Electronic Only)
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1.0 Introduction
The Madison County Solid Waste Department operates a solid waste facility (Operating Landfill) located on
Craig Rudisill Road, west of U.S. Highway 25/70 near Marshall, North Carolina. A site location map is
included as Figure 1. The Operating Landfill includes the following permitted components:
 Operating Construction and Demolition Debris (C&D) landfill cell (Permit No. 58-03)
 Operating Transfer Station (Permit No. 58-03T)
 Closed C&D landfill cell (Permit No. 58-03)
 Closed Municipal Solid Waste (MSW) landfill cell (Permit No. 58-03)
The Operating Landfill also contains a leachate underground holding tank that was installed in August 2011.
Previously, the leachate was stored in a lined leachate basin that is no longer in use.
State regulations applicable to landfills are enforced by the North Carolina Department of Environmental
Quality (DEQ), Division of Waste Management (DWM). This solid waste facility is permitted by the DEQ DWM
under Permit No. 58-03. The permit requires semiannual monitoring of groundwater, surface water, and
leachate quality.
This report documents the first semiannual groundwater, surface water, and leachate monitoring event for
2016 and is being submitted in accordance with requirements stipulated in the DEQ Solid Waste
Management Rules, Title 15A, North Carolina Administrative Code (NCAC), Subchapter 13B (15A NCAC 13B).
This semiannual report provides an evaluation of groundwater, surface water, and leachate quality for the
solid waste facility.
The water quality monitoring network for the Operating Landfill consists of nine compliance monitoring wells (MW-
01, MW-02, MW-03, MW-04, MW-05, MW-06R, MW-07R, MW-08, and MW-09); two surface water sample locations
(SW-01 and SW-02R) located along a tributary to Walnut Creek; and a leachate sample (LT-01) collected from the fill
port on the underground holding tank. Monitoring well construction details are summarized in Table 1.
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2.0 Methods
On April 12 and 13, 2016, Altamont Environmental, Inc. (Altamont) collected nine groundwater samples from
monitoring wells, two surface water samples from a tributary to Walnut Creek, and one aqueous sample
from the leachate underground holding tank located at the Operating Landfill. One of the monitoring wells
sampled, MW-06R, is upgradient from the landfill. Groundwater collected from this well is assumed to
represent background groundwater quality at the site. This monitoring well was installed on September 30,
2008 as a replacement for the pre-existing background monitoring well, MW-06, which had historically been
dry. Sampling locations are shown on Figures 2 and 3.
2.1 Groundwater Purging and Sampling Methods
Prior to collecting groundwater samples from the monitoring wells, the static water level was measured and
recorded for each well. The monitoring wells were purged and sampled using low-flow techniques in
accordance with the procedures described in Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures, United States Environmental Protection Agency (EPA), Groundwater Issues (Puls and Barcelona,
1996). During purging, pH, specific conductivity (SC), dissolved oxygen (DO), oxidation-reduction potential
(ORP), turbidity, and temperature were measured and recorded approximately every 3 minutes. Well purging
continued until these parameters stabilized for three consecutive readings. The required stabilization criteria
are as follows:
 pH values within +/- 0.1 pH unit
 SC values within +/- 3 percent
 Temperature, DO, and turbidity values within +/- 10 percent
 ORP values within +/- 10 millivolts
Following stabilization of these parameters, a groundwater sample was collected by a technician wearing a
new pair of non-reactive nitrile gloves. Each sample was placed directly into laboratory-supplied sample
containers. Low-flow sampling logs are included in Appendix A.
2.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02R were collected at designated locations from an unnamed
tributary to Walnut Creek that flows in a northerly direction adjacent to the western border of the Operating
Landfill (Figure 2). Sample SW-01 is considered representative of surface water quality upstream of the
Operating Landfill, while sample SW-02R is considered representative of surface water quality downstream
from the facility. Surface water samples were collected in laboratory-supplied sample containers by a
technician wearing a new pair of non-reactive nitrile gloves. As with groundwater sampling, temperature, pH,
SC, DO, ORP, and turbidity were measured and recorded at each surface water sampling location prior to
sample collection. Field parameters and observations pertaining to surface water quality are provided on
sampling logs included in Appendix A.
2.3 Leachate Sampling Methods
One aqueous sample was collected from the leachate underground holding tank, designated as LT-01.
Historically leachate was collected from a lined storage basin. On August 12, 2011, a leachate underground
holding tank was installed and connected to the leachate collection piping associated with the closed MSW
landfill cell. Shortly thereafter, the lined leachate basin was closed. Sample LT-01 was collected on April 13,
2016 from one of the tank’s fill ports using a new disposable polyethylene bailer. One round of field
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parameters (as described above) was measured and recorded for sample LT-01 (see Appendix A). Leachate
collected in the holding tank at the site is trucked, as needed, to the Metropolitan Sewerage District (MSD)
treatment facility for the town of Marshall, North Carolina.
2.4 Sample Handling, Documentation, and Analysis
Field parameters for groundwater and surface water were measured, and the results are provided on the
sampling logs provided in Appendix A. Following sample collection, each sample was immediately placed on
ice in a sample cooler for transport to TestAmerica Laboratories, Inc. (TestAmerica), a North Carolina-
certified laboratory located in Nashville, Tennessee. Altamont submitted the groundwater, surface water,
and leachate samples for the required analyses summarized in Table 2.
Proper chain-of-custody documentation procedures were followed during collection and transport of each
sample. Two trip blanks provided by the laboratory, each stored in a separate sample cooler, were analyzed
for Appendix I volatile organic compounds (VOCs). The reports of laboratory analysis and chain-of-custody
documentation are provided in Appendix B.
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3.0 Findings
3.1 Analytical Results
The field parameter data and laboratory analytical results for groundwater, surface water, the leachate
sample collected at the Operating Landfill, and the trip blanks are included in Appendices A and B and also
in Appendix C in the Electronic Data Deliverable (EDD) format specified by the DEQ Solid Waste Section
(SWS) of the DWM (a format most recently updated on May 5, 2010).
As stipulated in the May 2010 DWM documents, non-detections were reported at the laboratory-specific
method detection limit (MDL), and all concentrations exceeding the MDL were reported and appropriately
qualified (see Tables 3 and 4). The MDL is the minimum concentration of a substance that can be measured
and reported by a laboratory with 99 percent confidence that the analyte concentration is greater than zero.
The laboratory’s method reporting limit (MRL) is the minimum concentration of a target analyte that can be
accurately determined by the referenced method. MRL is listed as the “Report Limit” (RL) column in the
TestAmerica report of laboratory analysis (see Appendix B). All detections were compared to analyte-specific
Solid Waste Section Limits (SWSLs) established by the SWS. The SWSL is the lowest concentration,
determined by the SWS, of an analyte in a sample that can be quantitatively determined with suitable
precision and accuracy. If the reported concentration is greater than the laboratory MRL and less than the
SWSL, the analytical result is qualified as estimated and is flagged with a “J” qualifier (italicized J-flag) by
Altamont per the DEQ requirement. A “J” qualifier (non-italicized) is assigned by the laboratory and is used
for parameters detected at estimated concentrations greater than the MDL but less than the MRL. Detected
concentrations of constituents below the applicable SWSLs are not discussed in the text of this report unless
they exceed their applicable North Carolina water quality standard.
Detected concentrations of analytes in groundwater samples were compared to the values specified in the
15A NCAC 2L.0202 groundwater quality standard (2L standard). Detected concentrations of analytes in
groundwater with no established 2L standard were compared to an updated list of the interim maximum
allowable concentrations (IMACs) for Class GA and GSA groundwater (in accordance with 15A NCAC 02L
.0202 [c]). Detections of analytes in surface water samples were compared to the 15A NCAC 2B.0200
surface water quality standard (2B standard) established for class C waters.
Table 3 presents the summary of detected compounds and outlines concentrations of analytes that were above the
applicable SWSLs, as well as concentrations of analytes that exceed their respective 2L standard, IMAC, or 2B
standard.
In the EDD (Appendix C), the identification of a well (“WELL ID”) consists of the name of the well prefaced by
the un-hyphenated permit number for the facility. For example, monitoring well MW-01 is identified on the
EDD as 5803-MW01. In the tables, figures, and text of this report, however, the identification of a well
consists only of the name of the well (MW-01) and does not include the permit number for the facility.
3.1.1 Groundwater Monitoring Wells
The following sections summarize the results of laboratory and field parameter analyses of groundwater
samples.
3.1.1.1 Appendix I Metals
Nine metals were detected above their respective MDLs in one or more of the monitoring wells (see Table 3).
Four metals (barium, cadmium, cobalt, and zinc) were detected above their SWSLs in one or more of the
monitoring wells (see Table 3). Cadmium was detected above its 2L standard in monitoring well MW-03.
Cobalt was detected above the applicable IMAC in monitoring wells MW-02, MW-03, and MW-07R (see Table
3). Vanadium was detected above the applicable IMAC standard in all of the samples collected from the
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monitoring wells (see Table 3). All of the concentrations of the vanadium exceedances are reported below
the SWSL. Vanadium concentrations are believed to be naturally occurring.
3.1.1.2 Appendix I VOCs
Two VOCs were detected in samples collected from one or more monitoring wells. All detected VOC
concentrations were reported below the SWSL (see Table 3). Acetone was detected in multiple monitoring
wells as well as in the trip blank. Due to the trip-blank detection, detection of this VOC is likely due to
laboratory contamination. Tetrachloroethene was detected in monitoring well MW-05 below its SWSL. Trans-
1,2-dichloroethene was also detected in the trip blank, at a concentration below the MRL.
3.1.1.3 Field Parameters
Field parameters were recorded during sampling activities on April 12 and 13, 2016. Measured pH values
for all samples collected from monitoring wells were slightly below the 2L standard pH range of 6.5 to 8.5
Standard Units (SU) (see Table 3). Turbidity values for samples collected from the monitoring wells ranged
from 2.81 nephelometric turbidity units (NTUs) to 145 NTUs.
3.1.2 Surface Water
The following sections summarize the results of laboratory and field parameter analyses of surface water
samples SW-01 and SW-02R.
3.1.2.1 Appendix I Metals
Four metals were detected in both surface water samples below their respective SWSLs. No metals were
detected above applicable 2B standards (see Table 3).
3.1.2.2 Appendix I VOCs
Ethylbenzene and xylene (total) were detected in both the upstream and the downstream surface water
samples collected from the landfill. Both detections are reported at concentrations below their respective
SWSLs and well below the 2B standard. According to historical data, this sampling event is the first in which
these VOCs have been detected. Acetone was detected in the downstream surface water sample (SW-02R)
at a concentration below the SWSL. Acetone was also detected in the trip blank; therefore, detection of this
VOC is likely due to laboratory contamination.
3.1.2.3 Field Parameters
The pH values recorded for surface water samples SW-01 and SW-02R were recorded as 6.48 SU and 6.97
SU, respectively. Both values were within the 2B standard pH range of 6.0 to 9.0 SU (see Table 3). The
measured turbidity values for the surface water samples were within the 2B standard for turbidity,
established at 25 NTUs. DO was recorded at 3.47 milligrams per liter (mg/L) for surface water sample
SW-01 and was below the 2B standard. The 2B standard for DO is established at greater than 5.0 mg/L.
3.1.3 Leachate
Analytical results for the leachate sample (LT-01) collected from the leachate underground holding tank are
summarized in Table 4 and discussed below.

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3.1.3.1 Appendix I Metals
Twelve metals were detected in the aqueous sample collected from the leachate storage tank. Of these
metals, 10 of them were detected above their respective SWSLs (see Table 4).
3.1.3.2 Appendix I VOCs
Three VOCs were detected in the sampled collected from the leachate storage tank. All VOCs detected were
below their respective SWSLs (see Table 4). Trans-1,2-dichloroethene was detected in the trip blank
associated with this sample.
3.1.3.3 Inorganics
LT-01 was also analyzed for biological oxygen demand (BOD), chemical oxygen demand (COD), nitrate,
phosphorus, and sulfate. The analytical results for detected parameters are summarized in Table 4.
Nitrogen/nitrate was detected at a concentration in excess of the SWSL (see Table 4). All other parameters,
with the exception of sulfate, do not have established SWSLs. Sulfate was detected well below its SWSL.
3.1.3.4 Field Parameters
Field parameters were measured and recorded for the leachate sample on April 13, 2016. Dissolved oxygen,
pH, and turbidity results are summarized in Table 4. No standards exist for leachate; therefore, the recorded
results are not evaluated.
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4.0 Hydrogeology
The predominant groundwater flow direction within the regolith overlying the bedrock at the Operating
Landfill appears to be west-northwest, toward an unnamed tributary of Walnut Creek. Figure 3 depicts the
generalized groundwater flow direction based on groundwater measurements taken by Altamont on April 12
and 13, 2016. Water level data are summarized on Table 1.
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5.0 Summary
Altamont completed the first semiannual water quality monitoring event of 2016 at the Operating Landfill on April
12 and 13, 2016.
Tables 3 and 4 of this report, sampling logs (see Appendix A), the TestAmerica Reports of Laboratory Analysis (see
Appendix B), and the EDD (see Appendix C) provide detailed analytical results and field data used to interpret
groundwater and surface water quality at the Operating Landfill.
5.1 Future Activities
Altamont has discussed the exceedances of applicable water quality standards with Madison County. Altamont will
continue to measure field parameters and collect water quality samples from groundwater, surface water, and
leachate monitoring points associated with the Operating Landfill. Water quality samples will be submitted to a
North Carolina-certified laboratory for analysis for Appendix I metals and VOCs on a semiannual basis. The next
sampling event is scheduled for October 2016.
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6.0 References
DENR DWM SWS, October 27, 2006. New Guidelines for Electronic Submittal of Environmental Monitoring
Data.
DENR DWM SWS, February 23, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding
New Guidelines for Electronic Submittal of Environmental Data.
Puls, R.W., and M. J. Barcelona. 1996. Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures,
U.S. Environmental Protection Agency, OSWER, EPA/540/S-95/504.

FIGURES

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



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



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


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



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
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MW-01
(1,853.64)
MW-08
(1,883.69)
MW-07R
(1,893.14)
MW-05
(1,927.66)
MW-09
(1,944.05)
MW-06R
(1,936.38)
MW-04
(1,908.19)
MW-03
(1,911.33)MW-02
(1,894.65)








SW-01
SW-02R
3
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
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TABLES

Table 1
Well Construction Details and Corresponding Elevations
Madison County Operating Solid Waste Facility, Madison County, North Carolina
Depth to
Water
(from TOC)
58-03 MW-01 1,859.04 1,857.04 5.40 1,853.64 7 1,850.0 2 to 17 1,855.04
58-03 MW-02 1,898.94 1,895.94 4.29 1,894.65 6 1,889.9 1 to 16 1,892.94
58-03 MW-03 1,932.96 1,929.46 21.63 1,911.33 NA NA 15.5 to 25.5 1,913.96
58-03 MW-04 1,935.64 1,932.04 27.45 1,908.19 35.2 1,896.8 70.7 to 80.7 1,861.34
58-03 MW-05 1,972.76 1,969.26 45.10 1,927.66 NA NA 46.5 to 61.5 1,922.76
58-03 MW-06 2,082.87 2,081.87 NA NA 28 2,053.9 80 to 100 2,001.87
58-03 MW-06R 1,942.19 1,942.19 5.81 1,936.38 NA NA 10 to 25 1,932.19
58-03 MW-07R 1,919.34 1,916.64 26.20 1,893.14 NA NA 26 to 41 1,890.64
58-03 MW-08 1,899.92 1,896.92 16.23 1,883.69 NA NA 16 to 26 1,880.92
58-03 MW-09 1,949.43 1,946.43 5.38 1,944.05 NA NA 12.4 to 22.4 1,934.03
Notes:
Elevations Elevations are in feet, based on the NAVD 88 datum.
TOC Top of casing
NA Not Applicable
Depth to Bedrock &
Screened Interval
TOC Elevations
MW-06
Ground Elevations Calculated based on TOC elevations and field measurements.
Depth to Water Depth to water measurements were obtained in the field on April 12 and 13, 2016.
MW-03 and MW-04 Installed during closure of MSW cell.
Ground survey data
Facility Permit Well ID TOC
Elevation
Groundwater
Elevation
Depth to
Bedrock
Top of Bedrock
Elevation
Ground
Elevation
Depths are measured in feet below ground surface. Data was taken from boring logs completed on September 26, 27, 28, and 29, 1992 by Metro Drill, Inc. and
April 12, 1995 by Engineering Tectonics.
For MW-01, MW-02, MW-05, and MW-06, TOC elevations are based on the report, Transition Plan Application (Law Engineering, April 1994). For MW-03 and MW-
04, elevations are from the survey performed on December 14, 2006 by McGill Associates staff (J. Dallas Gordon, PLS). For MW-07R and MW-08, elevations were
taken from survey data included on boring logs completed by Bunnell-Lammons Engineering, Inc. on July 28, 29, and 30, 2003. For MW-09, elevation was taken
from survey data included on boring log completed by Bunnell-Lammons Engineering, Inc. on October 13, 2006.
Monitoring of background well MW-06 was terminated in Fall 2008 because the well was dry. MW-06R was installed on September 27, 2008 to replace MW-06.
Survey data for MW-06R are based on a survey conducted on April 16, 2009 by Wes Cole Land Surveying, PA. MW-06 was gauged and recorded if water was
present, but not sampled.
Included on the Closure Plan drawing generated by McGill Associates on January 4, 2007. Adjusted "Depth to Bedrock" and "Screened Interval" elevations were
calculated using original data from September 1992 boring logs and new data from the December 14, 2006 survey.
Screened
Interval
Top of Screen
Elevation
P:\Madison County\Analytical & Data\Water\2016\58-03 Operating\Tables\5803_April2016 T1-Well Construction Details Page 1 of 1
Table 2
Summary of Laboratory Analyses Performed on Samples
Madison County Operating Solid Waste Facility, Madison County, North Carolina
Groundwater Samples Surface Water Samples
Metals VOCs Metals VOCs
EPA 6010D
EPA 6020B
EPA 7470A
EPA 8260B
EPA 6010D
EPA 6020B
EPA 7470A
EPA 8260B
MW-01 4/13/2016 X X SW-01 4/12/2016 X X
MW-02 4/12/2016 X X SW-02R 4/12/2016 X X
MW-03 4/13/2016 X X
MW-04 4/13/2016 X X Quality Control Sample
MW-05 4/12/2016 X X VOCs
MW-06R 4/12/2016 X X EPA 8260B
MW-07R 4/12/2016 X X TRIP BLANK 4/12/2016 X
MW-08 4/12/2016 X X TRIP BLANK (LT-01)4/13/2016 X
MW-09 4/13/2016 X X
Leachate Sample `
Metals VOCs
Biochemical
Oxygen Demand
(BOD)
Chemical Oxygen
Demand (COD) Nitrate as N Total
Phosphorus Sulfate
EPA 6010D
EPA 6020B
EPA 7470A
EPA 8260B SM 5210B SM 5220D Nitrate by
calc EPA 365.4 EPA 300.0
LT-01 4/13/2016 X X X X X X X
Analyses Metals and VOCs analyses include Appendix I metals per 40 CFR Part 258 "Appendix I Constituents for Detection Monitoring". Metals analyses also includes mercury.
VOCs Volatile organic compounds
LT-1 Leachate sample, collected from the leachate underground holding tank.
Notes:
Sample
Name Collect Date Sample Name Collect Date
Sample Name Collect Date
Sample
Name Collect Date
P:\Madison County\Analytical & Data\Water\2016\58-03 Operating\Tables\5803Apil2016 Tables Page 1 of 1
Table 3
Groundwater and Surface Water Summary of Analytical Results
Madison County Operating Solid Waste Facility, Madison County, North Carolina
Metals VOCs Field Parameters
Lab Certification 387 387 5445 (pH only)
Lab Method EPA 6010D, 6020B EPA 8260B
Parameter Barium Cadmium Chromium Cobalt Copper Lead Nickel Vanadium Zinc Acetone Ethyl-
benzene
Tetrachloro-
ethene
trans-1,2-
dichloro-
ethene
Xylene
(total)
Dissolved
Oxygen pH Turbidity
CAS Number 7440-39-3 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7440-62-2 7440-66-6 67-64-1 100-41-4 127-18-4 156-60-5 1330-20-7 7782-44-7 SW320 SW330
SWS ID 15 34 51 53 54 131 152 209 213 3 110 192 79 346 356 320 330
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L SU NTU
Sample Name Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Monitoring Well Samples
MW-01 4/13/2016 110 0.500 U 3.00 U 0.561 J 5.00 U 2.00 U 3.00 U 4.15 J, B 10.0 U 4.20 J 0.190 U 0.140 U 0.230 U 0.580 U 1.47 5.42 5.93
MW-02 4/12/2016 124 0.500 U 3.00 U 3.65 J 5.4 J, B 2.00 U 3.00 U 5.57 J, B 10.0 U 4.19 J 0.190 U 0.140 U 0.230 U 0.580 U 1.25 5.96 17.8
MW-03 4/13/2016 233 2.30 3.00 U 92.6 5.00 U 2.00 U 4.60 J 3.17 J, B 10.0 U 5.07 J 0.190 U 0.140 U 0.230 U 0.580 U 0.82 6.10 9.07
MW-04 4/13/2016 151 0.500 U 3.00 U 0.500 U 5.00 U 2.90 J 3.00 U 8.08 J, B 10.0 U 2.66 U 0.190 U 0.140 U 0.230 U 0.580 U 2.59 6.30 5.28
MW-05 4/12/2016 132 0.900 J 3.00 U 0.824 J 5.00 U 3.30 J 4.50 J 7.69 J, B 10.7 J 4.37 J 0.190 U 0.163 J 0.230 U 0.580 U 1.45 5.86 4.31
MW-06R 4/12/2016 26.8 J 0.500 U 3.00 U 0.500 U 5.00 U 2.00 U 3.00 U 4.66 J, B 10.0 U 5.16 J 0.190 U 0.140 U 0.230 U 0.580 U 3.77 6.28 4.95
MW-07R 4/12/2016 167 1.60 6.40 J 1.90 J 7.3 J, B 3.60 J 3.00 U 11.7 J, B 23.2 J 2.66 U 0.190 U 0.140 U 0.230 U 0.580 U 7.19 5.56 145
MW-08 4/12/2016 31 J 0.500 U 3.00 U 0.500 U 5.00 U 2.30 J 3.00 U 7.48 J, B 10.0 U 2.66 U 0.190 U 0.140 U 0.230 U 0.580 U 5.16 6.24 2.81
MW-09 4/13/2016 170 0.500 U 3.00 U 0.500 U 6.7 J, B 2.60 J 3.00 U 6.42 J, B 10.0 U 2.66 U 0.190 U 0.140 U 0.230 U 0.580 U 2.17 6.31 4.23
Surface Water Samples
SW-01 4/12/2016 50.3 J 0.500 U 3.00 U 2.24 J 5.8 J, B 2.00 U 3.00 U 6.01 J, B 10.0 U 2.66 U 0.203 J 0.140 U 0.230 U 1.45 J 3.47 6.48 10.2
SW-02R 4/12/2016 54.3 J 0.500 U 3.00 U 0.761 J 6.5 J, B 2.00 U 3.00 U 5.24 J, B 10.0 U 2.76 J 0.361 J 0.140 U 0.230 U 2.50 J 5.75 6.97 6.37
Quality Control Samples
TRIPBLANK 4/12/2016 NA NA NA NA NA NA NA NA NA 11.2 J 0.190 U 0.140 U 0.578 J 0.580 U NA NA NA
MDL 5.00 0.500 3.00 0.500 5.0 2.00 3.00 2.10 10.0 2.66 0.190 0.140 0.230 0.580 NA NA NA
MRL 10.0 1.0 5.0 2.0 10 5.0 10.0 4.0 25.0 25.0 1.0 1.0 1.0 3.0 NA NA NA
SWSL 100 1 10 10 10 10 50 25 10 100 1 1 5 5 NE NE NE
2L 700 2 10 NE 1000 15 100 NE 1,000 6,000 600 1 100 500 NE 6.5-8.5 NE
IMAC NE NE NE 1 NE NE NE 0.3 NE NE NE NE NE NE NE NE NE
GWPS NE NE NE 1 NE NE NE 0.3 NE NE NE NE NE NE NE NE NE
2B 200,000 0.15 35 4 2.7 0.54 16 NE 36 2,000 97 3.3 10,000 670 > 5.0 6.0-9.0 25
Notes:
Detections Only detected constituents are listed on this table. Please refer to TestAmerica Laboratories, Inc. Report of Laboratory Analysis for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID The Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, milligrams per liter (mg/L) for dissolved oxygen, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in both the laboratory blank and the sample.
2L Groundwater standards from North Carolina Administrative Code (NCAC), Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards, DEQ (Amended April 1, 2013).
IMAC Interim Maximum Allowable Concentration. An IMAC is applied to a constituent if there is not a 2L standard established. Standards are from NCAC 15A 02L .0202.
GWPS
2B
NE Not Established
NA Not Applicable
110 Indicate a result in exceedance of the SWSL.
5.42 Indicate a result in exceedance of the 2L, IMAC, or 2B (surface water) standards, or greater than or equal to the GWPS (if no 2L or IMAC exist).
The Groundwater Protection Standard pursuant to 15A NCAC 13B .1634, DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-
section/environmental-monitoring/environmental-monitoring-list.
"2B" indicates surface water standard per North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water and Wetland Standards, (last amended on May 1,
2007). For compounds with no 2B standard established, the Environmental Protection Agency (EPA) National Criteria Table (current as of May 15, 2013) was used for the most stringent of fresh water and human health.
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Table 4
Leachate Summary of Analytical Results
Madison County Operating Solid Waste Facility, Madison County, North Carolina
Metals
Lab Certification 387
Lab Method EPA 6010D & 6020B
Parameter Antimony Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Thallium Vanadium Zinc
CAS Number 7440-36-0 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7440-02-0 7440-28-0 7440-62-2 7440-66-6
SWS ID 13 15 23 34 51 53 54 131 152 194 209 213
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Sample Name Collect Date Result Result Result Result Result Result Result Result Result Result Result Result
LT-01 04/13/2016 1.55 J 3,100 11.1 38.4 101 482 442 55.9 129 1.61 J 674 B 3,200
TRIPBLANK (LT-01)04/13/2016 NA NA NA NA NA NA NA NA NA NA NA NA
MDL 0.500 25.0 5.00 0.500 3.00 2.50 50.0 2.00 3.00 0.500 10.5 200
MRL 2.0 50.0 10.0 1.0 5.0 10.0 100 5.0 10.0 2.0 20.0 500
SWSL 6 100 1 1 10 10 10 10 50 5.5 25 10
VOCs General Chemistry Field Parameters
Lab Certification 387 387 5445 (pH only)
Lab Method EPA 8260B SM5210B SM 5220D Nitrate by calc EPA 365.4 EPA 300.0
Parameter Acetone Iodo-
methane
Trans-1,2-
dichloro-
ethene
Trichloro-
fluoro-
methane
BOD COD Nitrate as N Total
Phosphorus Sulfate Dissolved
Oxygen pH Turbidity
CAS Number 67-64-1 74-88-4 156-60-5 75-69-4 SW316 SW317 14797-55-8 7723-14-0 14808-79-8 7782-44-7 SW320 SW330
SWS ID 3 142 79 203 316 317 303 412 315 356 320 330
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L SU NTU
Sample Name Collect Date Result Result Result Result Result Result Result Result Result Result Result Result
LT-01 04/13/2016 9.14 J 2.17 J 0.230 U 0.481 J 17,900 176,000 23,400 44,800 113,000 J 6.44 7.40 Out of Range
TRIPBLANK (LT-01)04/13/2016 2.66 U 1.50 U 0.958 J 0.210 U NA NA NA NA NA NA NA NA
MDL 2.66 1.50 0.230 0.210 10,000 8,000 40.0 1,000 600 NA NA NA
MRL 25.0 10.0 1.0 1.00 10,000 40,000 100 2,000 1,000 NA NA NA
SWSL 100 10 1 1 NE NE 10,000 NE 250,000 NE NE NE
Notes:
Detections Only detected constituents are listed on this table. Please refer to the TestAmerica Report of Laboratory Analysis for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID The Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, milligrams per liter (mg/L) for dissolved oxygen, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Altamont to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in both the laboratory blank and the sample.
VOCs Volatile organic compounds
BOD Biological oxygen demand
COD Chemical oxygen demand
NE Not Established
23,400 Indicates a result in exceedance of the SWSL.
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APPENDICES

APPENDIX A

Sampling Logs and
Equipment Documentation
and Instrument Calibration Data Sheets

APPENDIX B

Reports of Laboratory Analysis
and Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-101708-1
Client Project/Site: Madison Co Operating Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
4/27/2016 3:07:52 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
TestAmerica Job ID: 490-101708-1
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
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Sample Summary
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-101708-1 MW-01 Water 04/13/16 10:03 04/14/16 09:45
490-101708-2 MW-02 Water 04/12/16 12:55 04/14/16 09:45
490-101708-3 MW-03 Water 04/13/16 11:04 04/14/16 09:45
490-101708-4 MW-04 Water 04/13/16 11:53 04/14/16 09:45
490-101708-5 MW-05 Water 04/12/16 14:04 04/14/16 09:45
490-101708-6 MW-06 Water 04/12/16 15:06 04/14/16 09:45
490-101708-7 MW-07 Water 04/12/16 10:11 04/14/16 09:45
490-101708-8 MW-08 Water 04/12/16 11:15 04/14/16 09:45
490-101708-9 MW-09 Water 04/13/16 14:00 04/14/16 09:45
490-101708-10 SW-01 Water 04/12/16 15:25 04/14/16 09:45
490-101708-11 SW-02R Water 04/12/16 11:40 04/14/16 09:45
490-101708-12 Trip Blanks Water 04/12/16 00:01 04/14/16 09:45
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101708-1
Project/Site: Madison Co Operating Landfill
Job ID: 490-101708-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-101708-1
Comments
No additional comments.
Receipt
The samples were received on 4/14/2016 9:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 0.4º C.
GC/MS VOA
Method(s) 8260B: The method blank for analytical batch 490-333272 contained Chloroform above the method detection limit. This target
analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 6010D: The method blank for preparation batch 490-333099 and analytical batch 490-333826 contained Copper (Cu) above the
method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis
of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F2 MS/MSD RPD exceeds control limits
E Result exceeded calibration range.
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
B Compound was found in the blank and sample.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-1Client Sample ID: MW-01
Matrix: WaterDate Collected: 04/13/16 10:03
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 4.20 J 25.0 2.66 ug/L 04/21/16 09:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 09:44 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 09:44 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 09:44 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 09:44 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 09:44 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 09:44 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 09:44 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 09:44 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 09:44 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 09:44 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 09:44 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 09:44 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 09:44 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 09:44 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 09:44 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 09:44 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 09:44 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 09:44 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 09:44 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 09:44 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 09:44 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 09:44 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 09:44 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 09:44 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 09:44 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 09:44 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 09:44 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 09:44 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 09:44 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 09:44 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 09:44 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 09:44 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 09:44 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 09:44 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 09:44 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 09:44 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 09:44 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 09:44 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 09:44 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 09:44 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 09:44 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 09:44 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 09:44 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 09:44 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 09:44 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 09:44 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 09:44 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-1Client Sample ID: MW-01
Matrix: WaterDate Collected: 04/13/16 10:03
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)111 70-130 04/21/16 09:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)103 04/21/16 09:44 170-130
1,2-Dichloroethane-d4 (Surr)115 04/21/16 09:44 170-130
Toluene-d8 (Surr)102 04/21/16 09:44 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:06 1Barium0.110
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:06 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:06 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:06 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:06 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:06 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:06 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:06 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 17:46 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:46 1Cobalt0.561 J
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:46 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 17:46 1Vanadium4.15 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 17:46 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 15:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-2Client Sample ID: MW-02
Matrix: WaterDate Collected: 04/12/16 12:55
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 4.19 J 25.0 2.66 ug/L 04/21/16 10:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 10:12 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 10:12 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 10:12 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 10:12 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 10:12 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 10:12 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 10:12 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 10:12 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 10:12 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 10:12 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 10:12 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 10:12 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 10:12 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 10:12 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 10:12 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 10:12 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 10:12 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 10:12 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 10:12 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 10:12 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 10:12 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 10:12 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 10:12 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 10:12 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 10:12 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 10:12 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 10:12 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 10:12 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 10:12 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 10:12 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 10:12 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 10:12 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 10:12 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 10:12 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 10:12 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 10:12 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 10:12 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 10:12 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 10:12 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 10:12 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 10:12 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 10:12 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 10:12 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 10:12 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 10:12 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 10:12 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 10:12 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-2Client Sample ID: MW-02
Matrix: WaterDate Collected: 04/12/16 12:55
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)103 70-130 04/21/16 10:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)110 04/21/16 10:12 170-130
1,2-Dichloroethane-d4 (Surr)118 04/21/16 10:12 170-130
Toluene-d8 (Surr)103 04/21/16 10:12 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:27 1Barium0.124
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:27 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:27 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:27 1Copper0.00540 J B
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:27 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:27 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:27 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:27 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 17:18 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:18 1Cobalt3.65
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:18 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 17:18 1Vanadium5.57 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 17:18 1Zinc<10.0 F1
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-3Client Sample ID: MW-03
Matrix: WaterDate Collected: 04/13/16 11:04
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.07 J 25.0 2.66 ug/L 04/21/16 10:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 10:40 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 10:40 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 10:40 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 10:40 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 10:40 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 10:40 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 10:40 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 10:40 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 10:40 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 10:40 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 10:40 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 10:40 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 10:40 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 10:40 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 10:40 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 10:40 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 10:40 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 10:40 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 10:40 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 10:40 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 10:40 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 10:40 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 10:40 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 10:40 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 10:40 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 10:40 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 10:40 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 10:40 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 10:40 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 10:40 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 10:40 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 10:40 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 10:40 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 10:40 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 10:40 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 10:40 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 10:40 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 10:40 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 10:40 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 10:40 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 10:40 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 10:40 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 10:40 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 10:40 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 10:40 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 10:40 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 10:40 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-3Client Sample ID: MW-03
Matrix: WaterDate Collected: 04/13/16 11:04
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)107 70-130 04/21/16 10:40 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)108 04/21/16 10:40 170-130
1,2-Dichloroethane-d4 (Surr)118 04/21/16 10:40 170-130
Toluene-d8 (Surr)102 04/21/16 10:40 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:32 1Barium0.233
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:32 1Cadmium0.00230
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:32 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:32 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:32 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:32 1Nickel0.00460 J
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:32 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:32 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 17:51 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:51 1Cobalt92.6
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:51 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 17:51 1Vanadium3.17 J B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 17:51 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-4Client Sample ID: MW-04
Matrix: WaterDate Collected: 04/13/16 11:53
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 11:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 11:09 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 11:09 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 11:09 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 11:09 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 11:09 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 11:09 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 11:09 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 11:09 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 11:09 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 11:09 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 11:09 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 11:09 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 11:09 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 11:09 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 11:09 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 11:09 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 11:09 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 11:09 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 11:09 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 11:09 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 11:09 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 11:09 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 11:09 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 11:09 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 11:09 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 11:09 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 11:09 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 11:09 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 11:09 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 11:09 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 11:09 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 11:09 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 11:09 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 11:09 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 11:09 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 11:09 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 11:09 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 11:09 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 11:09 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 11:09 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 11:09 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 11:09 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 11:09 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 11:09 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 11:09 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 11:09 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 11:09 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-4Client Sample ID: MW-04
Matrix: WaterDate Collected: 04/13/16 11:53
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)102 70-130 04/21/16 11:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)112 04/21/16 11:09 170-130
1,2-Dichloroethane-d4 (Surr)119 04/21/16 11:09 170-130
Toluene-d8 (Surr)101 04/21/16 11:09 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:45 1Barium0.151
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:45 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:45 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:45 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:45 1Lead0.00290 J
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:45 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:45 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:45 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 17:57 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:57 1Cobalt<0.500
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:57 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 17:57 1Vanadium8.08 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 17:57 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-5Client Sample ID: MW-05
Matrix: WaterDate Collected: 04/12/16 14:04
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 4.37 J 25.0 2.66 ug/L 04/21/16 11:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 11:37 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 11:37 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 11:37 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 11:37 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 11:37 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 11:37 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 11:37 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 11:37 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 11:37 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 11:37 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 11:37 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 11:37 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 11:37 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 11:37 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 11:37 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 11:37 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 11:37 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 11:37 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 11:37 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 11:37 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 11:37 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 11:37 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 11:37 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 11:37 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 11:37 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 11:37 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 11:37 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 11:37 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 11:37 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 11:37 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 11:37 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 11:37 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 11:37 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 11:37 1Tetrachloroethene0.163 J
10.0 0.820 ug/L 04/21/16 11:37 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 11:37 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 11:37 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 11:37 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 11:37 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 11:37 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 11:37 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 11:37 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 11:37 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 11:37 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 11:37 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 11:37 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 11:37 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-5Client Sample ID: MW-05
Matrix: WaterDate Collected: 04/12/16 14:04
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)108 70-130 04/21/16 11:37 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)106 04/21/16 11:37 170-130
1,2-Dichloroethane-d4 (Surr)116 04/21/16 11:37 170-130
Toluene-d8 (Surr)101 04/21/16 11:37 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:50 1Barium0.132
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:50 1Cadmium0.000900 J
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:50 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:50 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:50 1Lead0.00330 J
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:50 1Nickel0.00450 J
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:50 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:50 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:14 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:14 1Cobalt0.824 J
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:14 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:14 1Vanadium7.69 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:14 1Zinc10.7 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-6Client Sample ID: MW-06
Matrix: WaterDate Collected: 04/12/16 15:06
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.16 J 25.0 2.66 ug/L 04/21/16 12:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 12:06 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 12:06 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 12:06 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 12:06 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 12:06 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 12:06 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 12:06 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 12:06 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 12:06 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 12:06 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 12:06 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 12:06 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 12:06 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 12:06 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 12:06 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 12:06 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 12:06 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 12:06 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 12:06 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 12:06 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 12:06 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 12:06 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 12:06 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 12:06 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 12:06 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 12:06 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 12:06 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 12:06 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 12:06 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 12:06 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 12:06 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 12:06 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 12:06 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 12:06 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 12:06 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 12:06 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 12:06 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 12:06 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 12:06 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 12:06 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 12:06 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 12:06 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 12:06 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 12:06 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 12:06 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 12:06 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 12:06 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-6Client Sample ID: MW-06
Matrix: WaterDate Collected: 04/12/16 15:06
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)109 70-130 04/21/16 12:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)109 04/21/16 12:06 170-130
1,2-Dichloroethane-d4 (Surr)124 04/21/16 12:06 170-130
Toluene-d8 (Surr)100 04/21/16 12:06 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:54 1Barium0.0268
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:54 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:54 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:54 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:54 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:54 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:54 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:54 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:20 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:20 1Cobalt<0.500
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:20 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:20 1Vanadium4.66 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:20 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-7Client Sample ID: MW-07
Matrix: WaterDate Collected: 04/12/16 10:11
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 12:34 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 12:34 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 12:34 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 12:34 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 12:34 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 12:34 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 12:34 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 12:34 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 12:34 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 12:34 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 12:34 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 12:34 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 12:34 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 12:34 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 12:34 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 12:34 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 12:34 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 12:34 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 12:34 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 12:34 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 12:34 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 12:34 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 12:34 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 12:34 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 12:34 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 12:34 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 12:34 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 12:34 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 12:34 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 12:34 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 12:34 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 12:34 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 12:34 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 12:34 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 12:34 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 12:34 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 12:34 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 12:34 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 12:34 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 12:34 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 12:34 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 12:34 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 12:34 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 12:34 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 12:34 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 12:34 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 12:34 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-7Client Sample ID: MW-07
Matrix: WaterDate Collected: 04/12/16 10:11
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)102 70-130 04/21/16 12:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)109 04/21/16 12:34 170-130
1,2-Dichloroethane-d4 (Surr)124 04/21/16 12:34 170-130
Toluene-d8 (Surr)99 04/21/16 12:34 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 10:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:58 1Barium0.167
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 10:58 1Cadmium0.00160
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:58 1Chromium0.00640
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:58 1Copper0.00730 J B
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 10:58 1Lead0.00360 J
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 10:58 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 10:58 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 10:58 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:25 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:25 1Cobalt1.90 J
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:25 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:25 1Vanadium11.7 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:25 1Zinc23.2 J
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-8Client Sample ID: MW-08
Matrix: WaterDate Collected: 04/12/16 11:15
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 13:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 13:03 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 13:03 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 13:03 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 13:03 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 13:03 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 13:03 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 13:03 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 13:03 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 13:03 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 13:03 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 13:03 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 13:03 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 13:03 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 13:03 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 13:03 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 13:03 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 13:03 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 13:03 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 13:03 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 13:03 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 13:03 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 13:03 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 13:03 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 13:03 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 13:03 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 13:03 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 13:03 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 13:03 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 13:03 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 13:03 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 13:03 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 13:03 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 13:03 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 13:03 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 13:03 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 13:03 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 13:03 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 13:03 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 13:03 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 13:03 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 13:03 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 13:03 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 13:03 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 13:03 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 13:03 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 13:03 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 13:03 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-8Client Sample ID: MW-08
Matrix: WaterDate Collected: 04/12/16 11:15
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)109 70-130 04/21/16 13:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)108 04/21/16 13:03 170-130
1,2-Dichloroethane-d4 (Surr)118 04/21/16 13:03 170-130
Toluene-d8 (Surr)100 04/21/16 13:03 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 11:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:03 1Barium0.0310
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 11:03 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:03 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:03 1Copper<0.00500
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 11:03 1Lead0.00230 J
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 11:03 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:03 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:03 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:31 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:31 1Cobalt<0.500
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:31 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:31 1Vanadium7.48 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:31 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-9Client Sample ID: MW-09
Matrix: WaterDate Collected: 04/13/16 14:00
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 13:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 13:31 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 13:31 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 13:31 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 13:31 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 13:31 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 13:31 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 13:31 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 13:31 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 13:31 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 13:31 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 13:31 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 13:31 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 13:31 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 13:31 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 13:31 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 13:31 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 13:31 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 13:31 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 13:31 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 13:31 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 13:31 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 13:31 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 13:31 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 13:31 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 13:31 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 13:31 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 13:31 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 13:31 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 13:31 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 13:31 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 13:31 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 13:31 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 13:31 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 13:31 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 13:31 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 13:31 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 13:31 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 13:31 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 13:31 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 13:31 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 13:31 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 13:31 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 13:31 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 13:31 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 13:31 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 13:31 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 13:31 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-9Client Sample ID: MW-09
Matrix: WaterDate Collected: 04/13/16 14:00
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)106 70-130 04/21/16 13:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)109 04/21/16 13:31 170-130
1,2-Dichloroethane-d4 (Surr)121 04/21/16 13:31 170-130
Toluene-d8 (Surr)100 04/21/16 13:31 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 11:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:07 1Barium0.170
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 11:07 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:07 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:07 1Copper0.00670 J B
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 11:07 1Lead0.00260 J
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 11:07 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:07 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:07 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:36 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:36 1Cobalt<0.500
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:36 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:36 1Vanadium6.42 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:36 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-10Client Sample ID: SW-01
Matrix: WaterDate Collected: 04/12/16 15:25
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 13:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 13:59 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 13:59 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 13:59 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 13:59 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 13:59 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 13:59 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 13:59 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 13:59 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 13:59 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 13:59 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 13:59 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 13:59 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 13:59 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 13:59 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 13:59 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 13:59 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 13:59 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 13:59 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 13:59 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 13:59 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 13:59 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 13:59 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 13:59 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 13:59 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 13:59 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 13:59 1Ethylbenzene0.203 J
10.0 1.28 ug/L 04/21/16 13:59 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 13:59 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 13:59 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 13:59 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 13:59 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 13:59 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 13:59 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 13:59 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 13:59 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 13:59 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 13:59 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 13:59 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 13:59 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 13:59 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 13:59 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 13:59 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 13:59 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 13:59 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 13:59 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 13:59 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 13:59 1Xylenes, Total 1.45 J
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-10Client Sample ID: SW-01
Matrix: WaterDate Collected: 04/12/16 15:25
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)104 70-130 04/21/16 13:59 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)109 04/21/16 13:59 170-130
1,2-Dichloroethane-d4 (Surr)117 04/21/16 13:59 170-130
Toluene-d8 (Surr)101 04/21/16 13:59 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 11:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:11 1Barium0.0503
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 11:11 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:11 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:11 1Copper0.00580 J B
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 11:11 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 11:11 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:11 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:11 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:42 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:42 1Cobalt2.24
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:42 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:42 1Vanadium6.01 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:42 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-11Client Sample ID: SW-02R
Matrix: WaterDate Collected: 04/12/16 11:40
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 2.76 J 25.0 2.66 ug/L 04/21/16 14:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 14:28 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 14:28 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 14:28 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 14:28 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 14:28 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 14:28 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 14:28 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 14:28 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 14:28 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 14:28 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 14:28 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 14:28 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 14:28 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 14:28 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 14:28 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 14:28 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 14:28 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 14:28 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 14:28 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 14:28 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 14:28 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 14:28 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 14:28 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 14:28 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 14:28 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 14:28 1Ethylbenzene0.361 J
10.0 1.28 ug/L 04/21/16 14:28 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 14:28 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 14:28 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 14:28 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 14:28 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 14:28 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 14:28 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 14:28 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 14:28 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 14:28 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 14:28 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 14:28 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/21/16 14:28 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 14:28 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 14:28 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 14:28 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 14:28 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 14:28 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 14:28 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 14:28 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 14:28 1Xylenes, Total 2.50 J
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-11Client Sample ID: SW-02R
Matrix: WaterDate Collected: 04/12/16 11:40
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)107 70-130 04/21/16 14:28 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)113 04/21/16 14:28 170-130
1,2-Dichloroethane-d4 (Surr)121 04/21/16 14:28 170-130
Toluene-d8 (Surr)100 04/21/16 14:28 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 11:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:16 1Barium0.0543
0.00100 0.000500 mg/L 04/20/16 12:07 04/22/16 11:16 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:16 1Chromium<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:16 1Copper0.00650 J B
0.00500 0.00200 mg/L 04/20/16 12:07 04/22/16 11:16 1Lead<0.00200
0.0100 0.00300 mg/L 04/20/16 12:07 04/22/16 11:16 1Nickel<0.00300
0.0100 0.00500 mg/L 04/20/16 12:07 04/22/16 11:16 1Selenium<0.00500
0.00500 0.00300 mg/L 04/20/16 12:07 04/22/16 11:16 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 1.00 ug/L 04/20/16 12:07 04/21/16 18:48 1Beryllium<1.00
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:48 1Cobalt0.761 J
2.00 0.500 ug/L 04/20/16 12:07 04/21/16 18:48 1Thallium<0.500
4.00 2.10 ug/L 04/20/16 12:07 04/21/16 18:48 1Vanadium5.24 B
25.0 10.0 ug/L 04/20/16 12:07 04/21/16 18:48 1Zinc<10.0
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 16:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-12Client Sample ID: Trip Blanks
Matrix: WaterDate Collected: 04/12/16 00:01
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 11.2 J 25.0 2.66 ug/L 04/21/16 07:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 04/21/16 07:21 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/21/16 07:21 1Benzene<0.200
1.00 0.150 ug/L 04/21/16 07:21 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/21/16 07:21 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/21/16 07:21 1Bromoform<0.290
1.00 0.350 ug/L 04/21/16 07:21 1Bromomethane<0.350
50.0 2.64 ug/L 04/21/16 07:21 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/21/16 07:21 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/21/16 07:21 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/21/16 07:21 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/21/16 07:21 1Chloroethane<0.360
1.00 0.230 ug/L 04/21/16 07:21 1Chloroform<0.230
1.00 0.360 ug/L 04/21/16 07:21 1Chloromethane<0.360
1.00 0.210 ug/L 04/21/16 07:21 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/21/16 07:21 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/21/16 07:21 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/21/16 07:21 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/21/16 07:21 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/21/16 07:21 1Dibromomethane<0.450
1.00 0.190 ug/L 04/21/16 07:21 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/21/16 07:21 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/21/16 07:21 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/21/16 07:21 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/21/16 07:21 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/21/16 07:21 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/21/16 07:21 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/21/16 07:21 12-Hexanone <1.28
10.0 1.50 ug/L 04/21/16 07:21 1Iodomethane<1.50
5.00 1.00 ug/L 04/21/16 07:21 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/21/16 07:21 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/21/16 07:21 1Styrene<0.280
1.00 0.150 ug/L 04/21/16 07:21 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/21/16 07:21 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/21/16 07:21 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/21/16 07:21 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/21/16 07:21 1Toluene<0.170
5.00 0.460 ug/L 04/21/16 07:21 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/21/16 07:21 1trans-1,2-Dichloroethene 0.578 J
1.00 0.170 ug/L 04/21/16 07:21 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/21/16 07:21 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/21/16 07:21 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/21/16 07:21 1Trichloroethene<0.200
1.00 0.210 ug/L 04/21/16 07:21 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/21/16 07:21 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/21/16 07:21 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/21/16 07:21 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/21/16 07:21 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-101708-12Client Sample ID: Trip Blanks
Matrix: WaterDate Collected: 04/12/16 00:01
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)100 70-130 04/21/16 07:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)104 04/21/16 07:21 170-130
1,2-Dichloroethane-d4 (Surr)114 04/21/16 07:21 170-130
Toluene-d8 (Surr)101 04/21/16 07:21 170-130
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-333272/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/21/16 06:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 04/21/16 06:53 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/21/16 06:53 1Benzene
<0.150 0.1501.00 ug/L 04/21/16 06:53 1Bromochloromethane
<0.170 0.1701.00 ug/L 04/21/16 06:53 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/21/16 06:53 1Bromoform
<0.350 0.3501.00 ug/L 04/21/16 06:53 1Bromomethane
<2.64 2.6450.0 ug/L 04/21/16 06:53 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 04/21/16 06:53 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/21/16 06:53 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/21/16 06:53 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/21/16 06:53 1Chloroethane
0.2447 J 0.2301.00 ug/L 04/21/16 06:53 1Chloroform
<0.360 0.3601.00 ug/L 04/21/16 06:53 1Chloromethane
<0.210 0.2101.00 ug/L 04/21/16 06:53 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/21/16 06:53 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/21/16 06:53 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/21/16 06:53 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/21/16 06:53 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/21/16 06:53 1Dibromomethane
<0.190 0.1901.00 ug/L 04/21/16 06:53 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/21/16 06:53 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/21/16 06:53 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/21/16 06:53 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/21/16 06:53 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/21/16 06:53 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/21/16 06:53 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/21/16 06:53 12-Hexanone
<1.50 1.5010.0 ug/L 04/21/16 06:53 1Iodomethane
<1.00 1.005.00 ug/L 04/21/16 06:53 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/21/16 06:53 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/21/16 06:53 1Styrene
<0.150 0.1501.00 ug/L 04/21/16 06:53 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/21/16 06:53 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/21/16 06:53 1Tetrachloroethene
<0.820 0.82010.0 ug/L 04/21/16 06:53 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 04/21/16 06:53 1Toluene
<0.460 0.4605.00 ug/L 04/21/16 06:53 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/21/16 06:53 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/21/16 06:53 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 04/21/16 06:53 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/21/16 06:53 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/21/16 06:53 1Trichloroethene
<0.210 0.2101.00 ug/L 04/21/16 06:53 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/21/16 06:53 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/21/16 06:53 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/21/16 06:53 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/21/16 06:53 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
4-Bromofluorobenzene (Surr)105 70-130 04/21/16 06:53 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
109 04/21/16 06:53 1Dibromofluoromethane (Surr)70-130
114 04/21/16 06:53 11,2-Dichloroethane-d4 (Surr)70-130
101 04/21/16 06:53 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333272/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
Acetone 250 335.9 ug/L 134 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 624.9 ug/L 125 63-135
Benzene 50.0 52.15 ug/L 104 70-130
Bromochloromethane 50.0 57.36 ug/L 115 70-130
Bromodichloromethane 50.0 57.82 ug/L 116 70-130
Bromoform 50.0 56.45 ug/L 113 70-137
Bromomethane 50.0 50.81 E ug/L 102 53-150
2-Butanone (MEK)250 312.9 ug/L 125 55-143
Carbon disulfide 50.0 54.09 ug/L 108 64-135
Carbon tetrachloride 50.0 55.43 ug/L 111 70-147
Chlorobenzene 50.0 53.36 ug/L 107 70-130
Chloroethane 50.0 52.02 ug/L 104 60-138
Chloroform 50.0 57.09 ug/L 114 70-130
Chloromethane 50.0 51.30 ug/L 103 33-150
cis-1,2-Dichloroethene 50.0 59.86 ug/L 120 70-130
cis-1,3-Dichloropropene 50.0 57.70 ug/L 115 70-133
Dibromochloromethane 50.0 56.62 ug/L 113 70-133
1,2-Dibromo-3-Chloropropane 50.0 52.25 ug/L 104 45-138
1,2-Dibromoethane (EDB)50.0 55.83 ug/L 112 70-130
Dibromomethane 50.0 57.13 ug/L 114 70-130
1,2-Dichlorobenzene 50.0 54.20 ug/L 108 70-130
1,4-Dichlorobenzene 50.0 54.06 ug/L 108 70-130
1,1-Dichloroethane 50.0 60.79 ug/L 122 70-130
1,2-Dichloroethane 50.0 64.08 ug/L 128 70-130
1,1-Dichloroethene 50.0 55.90 ug/L 112 70-132
1,2-Dichloropropane 50.0 53.72 ug/L 107 70-130
Ethylbenzene 50.0 56.35 ug/L 113 70-130
2-Hexanone 250 310.6 ug/L 124 54-142
Iodomethane 50.0 64.61 ug/L 129 40-150
Methylene Chloride 50.0 54.95 ug/L 110 70-130
4-Methyl-2-pentanone (MIBK)250 309.7 ug/L 124 60-137
Styrene 50.0 59.81 ug/L 120 70-130
1,1,1,2-Tetrachloroethane 50.0 54.11 ug/L 108 70-130
1,1,2,2-Tetrachloroethane 50.0 50.93 ug/L 102 69-131
Tetrachloroethene 50.0 52.22 ug/L 104 70-130
Tetrahydrofuran 100 122.9 ug/L 123 51-136
Toluene 50.0 54.68 ug/L 109 70-130
trans-1,4-Dichloro-2-butene 50.0 53.60 ug/L 107 41-150
trans-1,2-Dichloroethene 50.0 60.99 ug/L 122 70-130
trans-1,3-Dichloropropene 50.0 61.05 ug/L 122 63-142
1,1,1-Trichloroethane 50.0 56.75 ug/L 113 70-135
1,1,2-Trichloroethane 50.0 55.26 ug/L 111 70-130
Trichloroethene 50.0 55.82 ug/L 112 70-130
Trichlorofluoromethane 50.0 60.89 ug/L 122 59-150
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333272/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
1,2,3-Trichloropropane 50.0 56.58 ug/L 113 70-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 100 84.00 ug/L 84 54-146
Vinyl chloride 50.0 54.46 ug/L 109 57-137
Xylenes, Total 100 116.2 ug/L 116 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1111,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-333272/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
Acetone 250 316.1 ug/L 126 39-150 6 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 596.9 ug/L 119 63-135 5 16
Benzene 50.0 50.63 ug/L 101 70-130 3 12
Bromochloromethane 50.0 55.36 ug/L 111 70-130 4 16
Bromodichloromethane 50.0 56.26 ug/L 113 70-130 3 14
Bromoform 50.0 54.32 ug/L 109 70-137 4 14
Bromomethane 50.0 50.04 E ug/L 100 53-150 2 19
2-Butanone (MEK)250 305.8 ug/L 122 55-143 2 19
Carbon disulfide 50.0 52.22 ug/L 104 64-135 4 16
Carbon tetrachloride 50.0 52.27 ug/L 105 70-147 6 16
Chlorobenzene 50.0 51.97 ug/L 104 70-130 3 12
Chloroethane 50.0 50.27 ug/L 101 60-138 3 15
Chloroform 50.0 55.26 ug/L 111 70-130 3 14
Chloromethane 50.0 48.89 ug/L 98 33-150 5 20
cis-1,2-Dichloroethene 50.0 58.21 ug/L 116 70-130 3 15
cis-1,3-Dichloropropene 50.0 57.00 ug/L 114 70-133 1 15
Dibromochloromethane 50.0 55.57 ug/L 111 70-133 2 13
1,2-Dibromo-3-Chloropropane 50.0 50.00 ug/L 100 45-138 4 19
1,2-Dibromoethane (EDB)50.0 54.43 ug/L 109 70-130 3 13
Dibromomethane 50.0 53.99 ug/L 108 70-130 6 14
1,2-Dichlorobenzene 50.0 53.89 ug/L 108 70-130 1 12
1,4-Dichlorobenzene 50.0 53.31 ug/L 107 70-130 1 12
1,1-Dichloroethane 50.0 58.46 ug/L 117 70-130 4 17
1,2-Dichloroethane 50.0 60.90 ug/L 122 70-130 5 13
1,1-Dichloroethene 50.0 52.14 ug/L 104 70-132 7 20
1,2-Dichloropropane 50.0 51.68 ug/L 103 70-130 4 15
Ethylbenzene 50.0 55.06 ug/L 110 70-130 2 12
2-Hexanone 250 299.8 ug/L 120 54-142 4 17
Iodomethane 50.0 62.99 ug/L 126 40-150 3 20
Methylene Chloride 50.0 52.87 ug/L 106 70-130 4 15
4-Methyl-2-pentanone (MIBK)250 302.0 ug/L 121 60-137 3 21
Styrene 50.0 58.37 ug/L 117 70-130 2 12
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-333272/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
1,1,1,2-Tetrachloroethane 50.0 52.33 ug/L 105 70-130 3 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 50.0 51.16 ug/L 102 69-131 0 15
Tetrachloroethene 50.0 50.93 ug/L 102 70-130 2 17
Tetrahydrofuran 100 100.1 ug/L 100 51-136 20 20
Toluene 50.0 53.36 ug/L 107 70-130 2 13
trans-1,4-Dichloro-2-butene 50.0 51.27 ug/L 103 41-150 4 20
trans-1,2-Dichloroethene 50.0 58.48 ug/L 117 70-130 4 15
trans-1,3-Dichloropropene 50.0 59.68 ug/L 119 63-142 2 13
1,1,1-Trichloroethane 50.0 53.55 ug/L 107 70-135 6 15
1,1,2-Trichloroethane 50.0 54.15 ug/L 108 70-130 2 13
Trichloroethene 50.0 52.83 ug/L 106 70-130 6 14
Trichlorofluoromethane 50.0 57.49 ug/L 115 59-150 6 22
1,2,3-Trichloropropane 50.0 54.79 ug/L 110 70-131 3 14
Vinyl acetate 100 99.07 ug/L 99 54-146 16 20
Vinyl chloride 50.0 52.04 ug/L 104 57-137 5 15
Xylenes, Total 100 114.2 ug/L 114 70-132 2 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
1091,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-101842-D-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
Acetone 4.09 J 250 322.9 ug/L 128 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 599.1 ug/L 120 50-135
Benzene <0.200 50.0 50.55 ug/L 101 55-147
Bromochloromethane <0.150 50.0 57.52 ug/L 115 59-132
Bromodichloromethane <0.170 50.0 57.61 ug/L 115 70-140
Bromoform <0.290 50.0 54.14 ug/L 108 53-150
Bromomethane <0.350 50.0 46.91 ug/L 94 30-150
2-Butanone (MEK)<2.64 250 307.8 ug/L 123 50-143
Carbon disulfide <0.220 50.0 51.63 ug/L 103 35-150
Carbon tetrachloride <0.180 50.0 58.56 ug/L 117 56-150
Chlorobenzene <0.180 50.0 50.83 ug/L 102 70-130
Chloroethane <0.360 50.0 53.19 ug/L 106 58-141
Chloroform <0.230 50.0 57.00 ug/L 114 66-138
Chloromethane <0.360 50.0 48.71 ug/L 97 10-150
cis-1,2-Dichloroethene <0.210 50.0 57.28 ug/L 115 68-131
cis-1,3-Dichloropropene <0.170 50.0 53.50 ug/L 107 70-133
Dibromochloromethane <0.250 50.0 54.52 ug/L 109 66-140
1,2-Dibromo-3-Chloropropane <0.940 50.0 47.85 ug/L 96 38-138
1,2-Dibromoethane (EDB)<0.210 50.0 52.16 ug/L 104 65-137
Dibromomethane <0.450 50.0 57.39 ug/L 115 70-130
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-101842-D-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
1,2-Dichlorobenzene <0.190 50.0 51.93 ug/L 104 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 50.0 50.58 ug/L 101 70-130
1,1-Dichloroethane <0.240 50.0 59.68 ug/L 119 61-139
1,2-Dichloroethane <0.200 50.0 64.62 ug/L 129 64-136
1,1-Dichloroethene <0.250 50.0 54.68 ug/L 109 54-150
1,2-Dichloropropane <0.250 50.0 52.00 ug/L 104 67-130
Ethylbenzene <0.190 50.0 53.77 ug/L 108 65-139
2-Hexanone <1.28 250 288.4 ug/L 115 44-150
Iodomethane <1.50 50.0 61.58 ug/L 123 34-150
Methylene Chloride <1.00 50.0 53.99 ug/L 108 64-130
4-Methyl-2-pentanone (MIBK)<0.810 250 295.4 ug/L 118 50-140
Styrene <0.280 50.0 55.67 ug/L 111 70-130
1,1,1,2-Tetrachloroethane <0.150 50.0 51.71 ug/L 103 70-130
1,1,2,2-Tetrachloroethane <0.190 50.0 52.00 ug/L 104 56-145
Tetrachloroethene <0.140 50.0 50.88 ug/L 102 57-138
Tetrahydrofuran <0.820 100 114.6 ug/L 115 40-136
Toluene <0.170 50.0 51.31 ug/L 103 64-136
trans-1,4-Dichloro-2-butene <0.460 50.0 47.62 ug/L 95 39-150
trans-1,2-Dichloroethene <0.230 50.0 59.81 ug/L 120 59-143
trans-1,3-Dichloropropene <0.170 50.0 55.89 ug/L 112 63-142
1,1,1-Trichloroethane <0.190 50.0 57.84 ug/L 116 68-144
1,1,2-Trichloroethane <0.190 50.0 52.90 ug/L 106 70-130
Trichloroethene <0.200 50.0 51.34 ug/L 103 63-135
Trichlorofluoromethane <0.210 F2 50.0 63.42 ug/L 127 44-150
1,2,3-Trichloropropane <0.230 50.0 52.38 ug/L 105 65-131
Vinyl acetate <1.71 100 101.6 ug/L 102 43-146
Vinyl chloride <0.180 50.0 55.06 ug/L 110 57-150
Xylenes, Total <0.580 100 111.1 ug/L 111 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
MS MS
Qualifier Limits%Recovery
109Dibromofluoromethane (Surr)70 -130
1201,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101842-E-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
Acetone 4.09 J 250 286.1 ug/L 113 39-150 12 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 575.7 ug/L 115 50-135 4 17
Benzene <0.200 50.0 50.47 ug/L 101 55-147 0 50
Bromochloromethane <0.150 50.0 54.95 ug/L 110 59-132 5 17
Bromodichloromethane <0.170 50.0 56.07 ug/L 112 70-140 3 18
Bromoform <0.290 50.0 52.40 ug/L 105 53-150 3 30
Bromomethane <0.350 50.0 48.84 ug/L 98 30-150 4
2-Butanone (MEK)<2.64 250 298.7 ug/L 119 50-143 3 19
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101842-E-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333272
Carbon disulfide <0.220 50.0 51.32 ug/L 103 35-150 1 21
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 50.0 54.96 ug/L 110 56-150 6 19
Chlorobenzene <0.180 50.0 50.52 ug/L 101 70-130 1 14
Chloroethane <0.360 50.0 53.86 ug/L 108 58-141 1 20
Chloroform <0.230 50.0 54.62 ug/L 109 66-138 4 18
Chloromethane <0.360 50.0 49.70 ug/L 99 10-150 2 31
cis-1,2-Dichloroethene <0.210 50.0 56.70 ug/L 113 68-131 1 17
cis-1,3-Dichloropropene <0.170 50.0 53.55 ug/L 107 70-133 0 15
Dibromochloromethane <0.250 50.0 53.98 ug/L 108 66-140 1 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 48.28 ug/L 97 38-138 1 24
1,2-Dibromoethane (EDB)<0.210 50.0 52.38 ug/L 105 65-137 0 15
Dibromomethane <0.450 50.0 53.09 ug/L 106 70-130 8 16
1,2-Dichlorobenzene <0.190 50.0 52.36 ug/L 105 70-130 1 15
1,4-Dichlorobenzene <0.170 50.0 50.58 ug/L 101 70-130 0 15
1,1-Dichloroethane <0.240 50.0 58.08 ug/L 116 61-139 3 17
1,2-Dichloroethane <0.200 50.0 61.21 ug/L 122 64-136 5 17
1,1-Dichloroethene <0.250 50.0 54.45 ug/L 109 54-150 0 20
1,2-Dichloropropane <0.250 50.0 51.24 ug/L 102 67-130 1 17
Ethylbenzene <0.190 50.0 53.61 ug/L 107 65-139 0 15
2-Hexanone <1.28 250 282.4 ug/L 113 44-150 2 17
Iodomethane <1.50 50.0 62.05 ug/L 124 34-150 1 23
Methylene Chloride <1.00 50.0 51.75 ug/L 104 64-130 4 17
4-Methyl-2-pentanone (MIBK)<0.810 250 291.9 ug/L 117 50-140 1 21
Styrene <0.280 50.0 55.38 ug/L 111 70-130 1 24
1,1,1,2-Tetrachloroethane <0.150 50.0 51.20 ug/L 102 70-130 1 16
1,1,2,2-Tetrachloroethane <0.190 50.0 52.25 ug/L 105 56-145 0 20
Tetrachloroethene <0.140 50.0 50.02 ug/L 100 57-138 2 17
Tetrahydrofuran <0.820 100 108.9 ug/L 109 40-136 5 20
Toluene <0.170 50.0 52.14 ug/L 104 64-136 2 15
trans-1,4-Dichloro-2-butene <0.460 50.0 49.44 ug/L 99 39-150 4 26
trans-1,2-Dichloroethene <0.230 50.0 57.99 ug/L 116 59-143 3 16
trans-1,3-Dichloropropene <0.170 50.0 56.21 ug/L 112 63-142 1 14
1,1,1-Trichloroethane <0.190 50.0 56.52 ug/L 113 68-144 2 17
1,1,2-Trichloroethane <0.190 50.0 52.75 ug/L 106 70-130 0 15
Trichloroethene <0.200 50.0 50.77 ug/L 102 63-135 1 17
Trichlorofluoromethane <0.210 F2 50.0 49.53 F2 ug/L 99 44-150 25 22
1,2,3-Trichloropropane <0.230 50.0 52.35 ug/L 105 65-131 0 19
Vinyl acetate <1.71 100 100.5 ug/L 101 43-146 1 21
Vinyl chloride <0.180 50.0 55.82 ug/L 112 57-150 1 17
Xylenes, Total <0.580 100 110.0 ug/L 110 69-132 1 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
1091,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-333099/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333826 Prep Batch: 333099
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/20/16 12:07 04/22/16 09:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 04/20/16 12:07 04/22/16 09:53 1Barium
<0.000500 0.0005000.00100 mg/L 04/20/16 12:07 04/22/16 09:53 1Cadmium
<0.00300 0.003000.00500 mg/L 04/20/16 12:07 04/22/16 09:53 1Chromium
0.007200 J 0.005000.0100 mg/L 04/20/16 12:07 04/22/16 09:53 1Copper
<0.00200 0.002000.00500 mg/L 04/20/16 12:07 04/22/16 09:53 1Lead
<0.00300 0.003000.0100 mg/L 04/20/16 12:07 04/22/16 09:53 1Nickel
<0.00500 0.005000.0100 mg/L 04/20/16 12:07 04/22/16 09:53 1Selenium
<0.00300 0.003000.00500 mg/L 04/20/16 12:07 04/22/16 09:53 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333099/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333826 Prep Batch: 333099
Arsenic 0.0500 0.04580 mg/L 92 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 1.995 mg/L 100 80-120
Cadmium 0.0500 0.04900 mg/L 98 80-120
Chromium 0.200 0.1888 mg/L 94 80-120
Copper 0.250 0.2406 mg/L 96 80-120
Lead 0.0500 0.04960 mg/L 99 80-120
Nickel 0.500 0.5069 mg/L 101 80-120
Selenium 0.0500 0.04610 mg/L 92 80-120
Silver 0.0500 0.04960 mg/L 99 80-120
Client Sample ID: MW-01Lab Sample ID: 490-101708-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333826 Prep Batch: 333099
Arsenic <0.00860 0.0500 0.04740 mg/L 95 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.110 2.00 2.132 mg/L 101 75-125
Cadmium <0.000500 0.0500 0.04960 mg/L 99 75-125
Chromium <0.00300 0.200 0.1893 mg/L 95 75-125
Copper <0.00500 0.250 0.2421 mg/L 97 75-125
Lead <0.00200 0.0500 0.04990 mg/L 100 75-125
Nickel <0.00300 0.500 0.5132 mg/L 103 75-125
Selenium <0.00500 0.0500 0.04880 mg/L 98 75-125
Silver <0.00300 0.0500 0.05010 mg/L 100 75-125
Client Sample ID: MW-01Lab Sample ID: 490-101708-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333826 Prep Batch: 333099
Arsenic <0.00860 0.0500 0.04510 mg/L 90 75-125 5 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.110 2.00 2.128 mg/L 101 75-125 0 20
Cadmium <0.000500 0.0500 0.04920 mg/L 98 75-125 1 20
Chromium <0.00300 0.200 0.1905 mg/L 95 75-125 1 20
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: MW-01Lab Sample ID: 490-101708-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333826 Prep Batch: 333099
Copper <0.00500 0.250 0.2425 mg/L 97 75-125 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Lead <0.00200 0.0500 0.05080 mg/L 102 75-125 2 20
Nickel <0.00300 0.500 0.5099 mg/L 102 75-125 1 20
Selenium <0.00500 0.0500 0.04920 mg/L 98 75-125 1 20
Silver <0.00300 0.0500 0.04990 mg/L 100 75-125 0 20
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-333101/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333787 Prep Batch: 333101
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/20/16 12:07 04/21/16 17:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.00 1.002.00 ug/L 04/20/16 12:07 04/21/16 17:07 1Beryllium
<0.500 0.5002.00 ug/L 04/20/16 12:07 04/21/16 17:07 1Cobalt
<0.500 0.5002.00 ug/L 04/20/16 12:07 04/21/16 17:07 1Thallium
3.628 J 2.104.00 ug/L 04/20/16 12:07 04/21/16 17:07 1Vanadium
<10.0 10.025.0 ug/L 04/20/16 12:07 04/21/16 17:07 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333101/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333787 Prep Batch: 333101
Antimony 100 90.70 ug/L 91 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 100.5 ug/L 101 80-120
Cobalt 100 88.45 ug/L 88 80-120
Thallium 100 94.78 ug/L 95 80-120
Vanadium 100 98.99 ug/L 99 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-333101/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334350 Prep Batch: 333101
Zinc 100 93.71 ug/L 94 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-02Lab Sample ID: 490-101708-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333787 Prep Batch: 333101
Antimony <0.500 100 82.24 ug/L 82 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <1.00 100 95.13 ug/L 95 75-125
Cobalt 3.65 100 86.73 ug/L 83 75-125
Thallium <0.500 100 95.86 ug/L 96 75-125
Vanadium 5.57 B 100 95.32 ug/L 90 75-125
Zinc <10.0 F1 100 71.65 F1 ug/L 72 75-125
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QC Sample Results
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-02Lab Sample ID: 490-101708-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 333787 Prep Batch: 333101
Antimony <0.500 100 81.74 ug/L 82 75-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <1.00 100 93.42 ug/L 93 75-125 2 20
Cobalt 3.65 100 86.18 ug/L 83 75-125 1 20
Thallium <0.500 100 95.83 ug/L 96 75-125 0 20
Vanadium 5.57 B 100 95.61 ug/L 90 75-125 0 20
Zinc <10.0 F1 100 70.38 F1 ug/L 70 75-125 2 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-332333/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332700 Prep Batch: 332333
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/18/16 06:10 04/18/16 15:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332333/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332700 Prep Batch: 332333
Mercury 1.00 0.8618 ug/L 86 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-101617-A-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332700 Prep Batch: 332333
Mercury <0.100 F1 1.00 0.8034 ug/L 80 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101617-A-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332700 Prep Batch: 332333
Mercury <0.100 F1 1.00 0.7421 F1 ug/L 74 75-125 8 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
GC/MS VOA
Analysis Batch: 333272
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-101708-1 MW-01 Total/NA
Water 8260B490-101708-2 MW-02 Total/NA
Water 8260B490-101708-3 MW-03 Total/NA
Water 8260B490-101708-4 MW-04 Total/NA
Water 8260B490-101708-5 MW-05 Total/NA
Water 8260B490-101708-6 MW-06 Total/NA
Water 8260B490-101708-7 MW-07 Total/NA
Water 8260B490-101708-8 MW-08 Total/NA
Water 8260B490-101708-9 MW-09 Total/NA
Water 8260B490-101708-10 SW-01 Total/NA
Water 8260B490-101708-11 SW-02R Total/NA
Water 8260B490-101708-12 Trip Blanks Total/NA
Water 8260B490-101842-D-1 MS Matrix Spike Total/NA
Water 8260B490-101842-E-1 MSD Matrix Spike Duplicate Total/NA
Water 8260BLCS 490-333272/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-333272/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-333272/7 Method Blank Total/NA
Metals
Prep Batch: 332333
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-101617-A-1-B MS Matrix Spike Total/NA
Water 7470A490-101617-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 7470A490-101708-1 MW-01 Total/NA
Water 7470A490-101708-2 MW-02 Total/NA
Water 7470A490-101708-3 MW-03 Total/NA
Water 7470A490-101708-4 MW-04 Total/NA
Water 7470A490-101708-5 MW-05 Total/NA
Water 7470A490-101708-6 MW-06 Total/NA
Water 7470A490-101708-7 MW-07 Total/NA
Water 7470A490-101708-8 MW-08 Total/NA
Water 7470A490-101708-9 MW-09 Total/NA
Water 7470A490-101708-10 SW-01 Total/NA
Water 7470A490-101708-11 SW-02R Total/NA
Water 7470ALCS 490-332333/2-A Lab Control Sample Total/NA
Water 7470AMB 490-332333/1-A Method Blank Total/NA
Analysis Batch: 332700
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 332333490-101617-A-1-B MS Matrix Spike Total/NA
Water 7470A 332333490-101617-A-1-C MSD Matrix Spike Duplicate Total/NA
Water 7470A 332333490-101708-1 MW-01 Total/NA
Water 7470A 332333490-101708-2 MW-02 Total/NA
Water 7470A 332333490-101708-3 MW-03 Total/NA
Water 7470A 332333490-101708-4 MW-04 Total/NA
Water 7470A 332333490-101708-5 MW-05 Total/NA
Water 7470A 332333490-101708-6 MW-06 Total/NA
Water 7470A 332333490-101708-7 MW-07 Total/NA
Water 7470A 332333490-101708-8 MW-08 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Metals (Continued)
Analysis Batch: 332700 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 332333490-101708-9 MW-09 Total/NA
Water 7470A 332333490-101708-10 SW-01 Total/NA
Water 7470A 332333490-101708-11 SW-02R Total/NA
Water 7470A 332333LCS 490-332333/2-A Lab Control Sample Total/NA
Water 7470A 332333MB 490-332333/1-A Method Blank Total/NA
Prep Batch: 333099
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-101708-1 MW-01 Total/NA
Water 3010A490-101708-1 MS MW-01 Total/NA
Water 3010A490-101708-1 MSD MW-01 Total/NA
Water 3010A490-101708-2 MW-02 Total/NA
Water 3010A490-101708-3 MW-03 Total/NA
Water 3010A490-101708-4 MW-04 Total/NA
Water 3010A490-101708-5 MW-05 Total/NA
Water 3010A490-101708-6 MW-06 Total/NA
Water 3010A490-101708-7 MW-07 Total/NA
Water 3010A490-101708-8 MW-08 Total/NA
Water 3010A490-101708-9 MW-09 Total/NA
Water 3010A490-101708-10 SW-01 Total/NA
Water 3010A490-101708-11 SW-02R Total/NA
Water 3010ALCS 490-333099/2-A Lab Control Sample Total/NA
Water 3010AMB 490-333099/1-A Method Blank Total/NA
Prep Batch: 333101
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-101708-1 MW-01 Total/NA
Water 3010A490-101708-2 MW-02 Total/NA
Water 3010A490-101708-2 MS MW-02 Total/NA
Water 3010A490-101708-2 MSD MW-02 Total/NA
Water 3010A490-101708-3 MW-03 Total/NA
Water 3010A490-101708-4 MW-04 Total/NA
Water 3010A490-101708-5 MW-05 Total/NA
Water 3010A490-101708-6 MW-06 Total/NA
Water 3010A490-101708-7 MW-07 Total/NA
Water 3010A490-101708-8 MW-08 Total/NA
Water 3010A490-101708-9 MW-09 Total/NA
Water 3010A490-101708-10 SW-01 Total/NA
Water 3010A490-101708-11 SW-02R Total/NA
Water 3010ALCS 490-333101/2-A Lab Control Sample Total/NA
Water 3010AMB 490-333101/1-A Method Blank Total/NA
Analysis Batch: 333787
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 333101490-101708-1 MW-01 Total/NA
Water 6020B 333101490-101708-2 MW-02 Total/NA
Water 6020B 333101490-101708-2 MS MW-02 Total/NA
Water 6020B 333101490-101708-2 MSD MW-02 Total/NA
Water 6020B 333101490-101708-3 MW-03 Total/NA
Water 6020B 333101490-101708-4 MW-04 Total/NA
Water 6020B 333101490-101708-5 MW-05 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Metals (Continued)
Analysis Batch: 333787 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 333101490-101708-6 MW-06 Total/NA
Water 6020B 333101490-101708-7 MW-07 Total/NA
Water 6020B 333101490-101708-8 MW-08 Total/NA
Water 6020B 333101490-101708-9 MW-09 Total/NA
Water 6020B 333101490-101708-10 SW-01 Total/NA
Water 6020B 333101490-101708-11 SW-02R Total/NA
Water 6020B 333101LCS 490-333101/2-A Lab Control Sample Total/NA
Water 6020B 333101MB 490-333101/1-A Method Blank Total/NA
Analysis Batch: 333826
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 333099490-101708-1 MW-01 Total/NA
Water 6010D 333099490-101708-1 MS MW-01 Total/NA
Water 6010D 333099490-101708-1 MSD MW-01 Total/NA
Water 6010D 333099490-101708-2 MW-02 Total/NA
Water 6010D 333099490-101708-3 MW-03 Total/NA
Water 6010D 333099490-101708-4 MW-04 Total/NA
Water 6010D 333099490-101708-5 MW-05 Total/NA
Water 6010D 333099490-101708-6 MW-06 Total/NA
Water 6010D 333099490-101708-7 MW-07 Total/NA
Water 6010D 333099490-101708-8 MW-08 Total/NA
Water 6010D 333099490-101708-9 MW-09 Total/NA
Water 6010D 333099490-101708-10 SW-01 Total/NA
Water 6010D 333099490-101708-11 SW-02R Total/NA
Water 6010D 333099LCS 490-333099/2-A Lab Control Sample Total/NA
Water 6010D 333099MB 490-333099/1-A Method Blank Total/NA
Analysis Batch: 334350
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 333101LCS 490-333101/2-A Lab Control Sample Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101708-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-01 Lab Sample ID: 490-101708-1
Matrix: WaterDate Collected: 04/13/16 10:03
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 09:441 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:06 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 17:46 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 15:57 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-02 Lab Sample ID: 490-101708-2
Matrix: WaterDate Collected: 04/12/16 12:55
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 10:121 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:27 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 17:18 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:00 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-03 Lab Sample ID: 490-101708-3
Matrix: WaterDate Collected: 04/13/16 11:04
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 10:401 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:32 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 17:51 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:02 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-04 Lab Sample ID: 490-101708-4
Matrix: WaterDate Collected: 04/13/16 11:53
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 11:091 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:45 ADN TAL NSHTotal/NA 50 mL 50 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101708-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-04 Lab Sample ID: 490-101708-4
Matrix: WaterDate Collected: 04/13/16 11:53
Date Received: 04/14/16 09:45
Prep 3010A KMS04/20/16 12:07 TAL NSH333101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 17:57 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:04 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-05 Lab Sample ID: 490-101708-5
Matrix: WaterDate Collected: 04/12/16 14:04
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 11:371 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:50 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 18:14 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:07 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-06 Lab Sample ID: 490-101708-6
Matrix: WaterDate Collected: 04/12/16 15:06
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 12:061 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:54 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 18:20 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:09 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-07 Lab Sample ID: 490-101708-7
Matrix: WaterDate Collected: 04/12/16 10:11
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 12:341 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 10:58 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 18:25 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:11 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101708-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-08 Lab Sample ID: 490-101708-8
Matrix: WaterDate Collected: 04/12/16 11:15
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 13:031 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 11:03 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 18:31 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:14 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: MW-09 Lab Sample ID: 490-101708-9
Matrix: WaterDate Collected: 04/13/16 14:00
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 13:311 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 11:07 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 18:36 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:16 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: SW-01 Lab Sample ID: 490-101708-10
Matrix: WaterDate Collected: 04/12/16 15:25
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 13:591 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 11:11 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 333787 04/21/16 18:42 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:18 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: SW-02R Lab Sample ID: 490-101708-11
Matrix: WaterDate Collected: 04/12/16 11:40
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 14:281 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 333099 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 333826 04/22/16 11:16 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 333101 04/20/16 12:07 KMS TAL NSHTotal/NA 50 mL 50 mL
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101708-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: SW-02R Lab Sample ID: 490-101708-11
Matrix: WaterDate Collected: 04/12/16 11:40
Date Received: 04/14/16 09:45
Analysis 6020B KKK04/21/16 18:481 TAL NSH333787
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Prep 7470A 332333 04/18/16 06:10 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 332700 04/18/16 16:25 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Client Sample ID: Trip Blanks Lab Sample ID: 490-101708-12
Matrix: WaterDate Collected: 04/12/16 00:01
Date Received: 04/14/16 09:45
Analysis 8260B NC04/21/16 07:211 TAL NSH333272
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-101708-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101708-1
Project/Site: Madison Co Operating Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-101708-1
Login Number: 101708
Question Answer Comment
Creator: Stvartak, Anthony Q
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-101527-1
Client Project/Site: Madison Co Operating Landfill-Leachate
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
5/2/2016 9:36:48 AM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
TestAmerica Job ID: 490-101527-1
Page 2 of 37 TestAmerica Nashville5/2/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37
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Sample Summary
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-101527-1 LT-01 Water 04/13/16 12:38 04/14/16 09:45
490-101527-2 Trip Blank Water 04/13/16 00:01 04/14/16 09:45
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101527-1
Project/Site: Madison Co Operating Landfill-Leachate
Job ID: 490-101527-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-101527-1
Comments
No additional comments.
Receipt
The samples were received on 4/14/2016 9:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.0º C.
GC/MS VOA
Method(s) 8260B: The following volatile samples were received and analyzed from a vial containing headspace. Trip Blank
(490-101527-2)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
HPLC/IC
Method(s) 300.0: The following sample was diluted due to the nature of the sample matrix: LT-01 (490-101527-1). Elevated reporting
limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 6020B: The method blank for 490-335080 contained Vanadium above the method detection limit (MDL). Associated samples
were not re-analyzed because results were less than the reporting limit (RL) OR practical quantitation limit (PQL).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method(s) 353.2, SM 4500 NO3 F: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 490-332145 were
outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control
sample (LCS) recovery was within acceptance limits.
Method(s) 365.4: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 490-334638 and analytical batch
490-334795 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits.
Method(s) 365.2/365.3/365: The following sample was distilled at a reduced volume due to matrix: LT-01 (490-101527-1). Elevated
reporting limits are provided.
Method(s) SM 5220D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 490-332870 were outside control
limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS)
recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
E Result exceeded calibration range.
HPLC/IC
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Metals
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Lab Sample ID: 490-101527-1Client Sample ID: LT-01
Matrix: WaterDate Collected: 04/13/16 12:38
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 9.14 J 25.0 2.66 ug/L 04/16/16 05:54 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/16/16 05:54 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/16/16 05:54 1Benzene<0.200
1.00 0.150 ug/L 04/16/16 05:54 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/16/16 05:54 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/16/16 05:54 1Bromoform<0.290
1.00 0.350 ug/L 04/16/16 05:54 1Bromomethane<0.350
50.0 2.64 ug/L 04/16/16 05:54 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/16/16 05:54 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/16/16 05:54 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/16/16 05:54 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/16/16 05:54 1Chloroethane<0.360
1.00 0.230 ug/L 04/16/16 05:54 1Chloroform<0.230
1.00 0.360 ug/L 04/16/16 05:54 1Chloromethane<0.360
1.00 0.210 ug/L 04/16/16 05:54 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/16/16 05:54 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/16/16 05:54 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/16/16 05:54 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/16/16 05:54 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/16/16 05:54 1Dibromomethane<0.450
1.00 0.190 ug/L 04/16/16 05:54 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/16/16 05:54 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/16/16 05:54 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/16/16 05:54 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/16/16 05:54 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/16/16 05:54 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/16/16 05:54 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/16/16 05:54 12-Hexanone <1.28
10.0 1.50 ug/L 04/16/16 05:54 1Iodomethane2.17 J
5.00 1.00 ug/L 04/16/16 05:54 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/16/16 05:54 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/16/16 05:54 1Styrene<0.280
1.00 0.150 ug/L 04/16/16 05:54 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/16/16 05:54 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/16/16 05:54 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/16/16 05:54 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/16/16 05:54 1Toluene<0.170
5.00 0.460 ug/L 04/16/16 05:54 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/16/16 05:54 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/16/16 05:54 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/16/16 05:54 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/16/16 05:54 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/16/16 05:54 1Trichloroethene<0.200
1.00 0.210 ug/L 04/16/16 05:54 1Trichlorofluoromethane0.481 J
1.00 0.230 ug/L 04/16/16 05:54 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/16/16 05:54 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/16/16 05:54 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/16/16 05:54 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Lab Sample ID: 490-101527-1Client Sample ID: LT-01
Matrix: WaterDate Collected: 04/13/16 12:38
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)101 70-130 04/16/16 05:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 04/16/16 05:54 170-130
1,2-Dichloroethane-d4 (Surr)94 04/16/16 05:54 170-130
Toluene-d8 (Surr)95 04/16/16 05:54 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Sulfate 113 1.00 0.600 mg/L 04/15/16 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/27/16 14:29 04/28/16 11:26 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.0100 0.00500 mg/L 04/27/16 14:29 04/28/16 11:26 1Barium3.10
0.00100 0.000500 mg/L 04/27/16 14:29 04/28/16 11:26 1Cadmium0.0384
0.00500 0.00300 mg/L 04/27/16 14:29 04/28/16 11:26 1Chromium0.101
0.100 0.0500 mg/L 04/27/16 14:29 04/29/16 11:57 10Copper0.442
0.00500 0.00200 mg/L 04/27/16 14:29 04/28/16 11:26 1Lead0.0559
0.0100 0.00300 mg/L 04/27/16 14:29 04/28/16 11:26 1Nickel0.129
0.0500 0.0250 mg/L 04/27/16 14:29 04/28/16 18:12 5Selenium<0.0250
0.0250 0.0150 mg/L 04/27/16 14:29 04/28/16 18:12 5Silver<0.0150
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 1.55 J 2.00 0.500 ug/L 04/27/16 14:35 04/29/16 14:56 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 5.00 ug/L 04/27/16 14:35 04/29/16 08:22 5Beryllium11.1
10.0 2.50 ug/L 04/27/16 14:35 04/29/16 08:22 5Cobalt482
2.00 0.500 ug/L 04/27/16 14:35 04/29/16 14:56 1Thallium1.61 J
20.0 10.5 ug/L 04/27/16 14:35 04/29/16 08:22 5Vanadium674 B
500 200 ug/L 04/27/16 14:35 04/29/16 15:36 20Zinc3200
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/27/16 13:52 04/27/16 16:07 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
General Chemistry
RL MDL
Phosphorus, Total 44.8 2.00 1.00 mg/L 04/26/16 11:36 04/26/16 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.100 0.0400 mg/L 04/14/16 16:20 1Nitrate as N 23.4
40.0 8.00 mg/L 04/19/16 16:36 2Chemical Oxygen Demand 176
RL RL
Biochemical Oxygen Demand 17.9 10.0 10.0 mg/L 04/14/16 18:43 5
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Lab Sample ID: 490-101527-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/13/16 00:01
Date Received: 04/14/16 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/16/16 05:24 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 0.500 ug/L 04/16/16 05:24 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/16/16 05:24 1Benzene<0.200
1.00 0.150 ug/L 04/16/16 05:24 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/16/16 05:24 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/16/16 05:24 1Bromoform<0.290
1.00 0.350 ug/L 04/16/16 05:24 1Bromomethane<0.350
50.0 2.64 ug/L 04/16/16 05:24 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/16/16 05:24 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/16/16 05:24 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/16/16 05:24 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/16/16 05:24 1Chloroethane<0.360
1.00 0.230 ug/L 04/16/16 05:24 1Chloroform<0.230
1.00 0.360 ug/L 04/16/16 05:24 1Chloromethane<0.360
1.00 0.210 ug/L 04/16/16 05:24 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/16/16 05:24 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/16/16 05:24 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/16/16 05:24 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/16/16 05:24 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/16/16 05:24 1Dibromomethane<0.450
1.00 0.190 ug/L 04/16/16 05:24 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/16/16 05:24 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/16/16 05:24 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/16/16 05:24 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/16/16 05:24 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/16/16 05:24 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/16/16 05:24 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/16/16 05:24 12-Hexanone <1.28
10.0 1.50 ug/L 04/16/16 05:24 1Iodomethane<1.50
5.00 1.00 ug/L 04/16/16 05:24 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/16/16 05:24 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/16/16 05:24 1Styrene<0.280
1.00 0.150 ug/L 04/16/16 05:24 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/16/16 05:24 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/16/16 05:24 1Tetrachloroethene<0.140
10.0 0.820 ug/L 04/16/16 05:24 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 04/16/16 05:24 1Toluene<0.170
5.00 0.460 ug/L 04/16/16 05:24 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/20/16 15:11 1trans-1,2-Dichloroethene 0.958 J
1.00 0.170 ug/L 04/16/16 05:24 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/16/16 05:24 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/16/16 05:24 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/16/16 05:24 1Trichloroethene<0.200
1.00 0.210 ug/L 04/16/16 05:24 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/16/16 05:24 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/16/16 05:24 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/16/16 05:24 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/16/16 05:24 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Lab Sample ID: 490-101527-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/13/16 00:01
Date Received: 04/14/16 09:45
4-Bromofluorobenzene (Surr)101 70-130 04/16/16 05:24 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr)99 04/20/16 15:11 170-130
Dibromofluoromethane (Surr)98 04/16/16 05:24 170-130
Dibromofluoromethane (Surr)99 04/20/16 15:11 170-130
1,2-Dichloroethane-d4 (Surr)94 04/16/16 05:24 170-130
1,2-Dichloroethane-d4 (Surr)96 04/20/16 15:11 170-130
Toluene-d8 (Surr)95 04/16/16 05:24 170-130
Toluene-d8 (Surr)98 04/20/16 15:11 170-130
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-332090/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/16/16 04:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 04/16/16 04:24 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/16/16 04:24 1Benzene
<0.150 0.1501.00 ug/L 04/16/16 04:24 1Bromochloromethane
<0.170 0.1701.00 ug/L 04/16/16 04:24 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/16/16 04:24 1Bromoform
<0.350 0.3501.00 ug/L 04/16/16 04:24 1Bromomethane
<2.64 2.6450.0 ug/L 04/16/16 04:24 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 04/16/16 04:24 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/16/16 04:24 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/16/16 04:24 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/16/16 04:24 1Chloroethane
<0.230 0.2301.00 ug/L 04/16/16 04:24 1Chloroform
<0.360 0.3601.00 ug/L 04/16/16 04:24 1Chloromethane
<0.210 0.2101.00 ug/L 04/16/16 04:24 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/16/16 04:24 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/16/16 04:24 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/16/16 04:24 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/16/16 04:24 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/16/16 04:24 1Dibromomethane
<0.190 0.1901.00 ug/L 04/16/16 04:24 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/16/16 04:24 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/16/16 04:24 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/16/16 04:24 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/16/16 04:24 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/16/16 04:24 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/16/16 04:24 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/16/16 04:24 12-Hexanone
<1.50 1.5010.0 ug/L 04/16/16 04:24 1Iodomethane
<1.00 1.005.00 ug/L 04/16/16 04:24 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/16/16 04:24 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/16/16 04:24 1Styrene
<0.150 0.1501.00 ug/L 04/16/16 04:24 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/16/16 04:24 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/16/16 04:24 1Tetrachloroethene
<0.820 0.82010.0 ug/L 04/16/16 04:24 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 04/16/16 04:24 1Toluene
<0.460 0.4605.00 ug/L 04/16/16 04:24 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/16/16 04:24 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/16/16 04:24 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 04/16/16 04:24 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/16/16 04:24 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/16/16 04:24 1Trichloroethene
<0.210 0.2101.00 ug/L 04/16/16 04:24 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/16/16 04:24 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/16/16 04:24 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/16/16 04:24 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/16/16 04:24 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
4-Bromofluorobenzene (Surr)103 70-130 04/16/16 04:24 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
101 04/16/16 04:24 1Dibromofluoromethane (Surr)70 -130
98 04/16/16 04:24 11,2-Dichloroethane-d4 (Surr)70 -130
93 04/16/16 04:24 1Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332090/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
Acetone 250 254.6 ug/L 102 39 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 486.6 ug/L 97 63 -135
Benzene 50.0 53.81 ug/L 108 70 -130
Bromochloromethane 50.0 53.10 ug/L 106 70 -130
Bromodichloromethane 50.0 49.90 ug/L 100 70 -130
Bromoform 50.0 47.15 ug/L 94 70 -137
Bromomethane 50.0 52.12 ug/L 104 53 -150
2-Butanone (MEK)250 232.3 ug/L 93 55 -143
Carbon disulfide 50.0 50.76 ug/L 102 64 -135
Carbon tetrachloride 50.0 53.17 ug/L 106 70 -147
Chlorobenzene 50.0 44.64 ug/L 89 70 -130
Chloroethane 50.0 50.19 ug/L 100 60 -138
Chloroform 50.0 54.74 ug/L 109 70 -130
Chloromethane 50.0 49.78 ug/L 100 33 -150
cis-1,2-Dichloroethene 50.0 52.66 ug/L 105 70 -130
cis-1,3-Dichloropropene 50.0 41.94 ug/L 84 70 -133
Dibromochloromethane 50.0 49.07 ug/L 98 70 -133
1,2-Dibromo-3-Chloropropane 50.0 49.38 ug/L 99 45 -138
1,2-Dibromoethane (EDB)50.0 42.79 ug/L 86 70 -130
Dibromomethane 50.0 49.46 ug/L 99 70 -130
1,2-Dichlorobenzene 50.0 44.62 ug/L 89 70 -130
1,4-Dichlorobenzene 50.0 44.84 ug/L 90 70 -130
1,1-Dichloroethane 50.0 51.47 ug/L 103 70 -130
1,2-Dichloroethane 50.0 51.18 ug/L 102 70 -130
1,1-Dichloroethene 50.0 52.90 ug/L 106 70 -132
1,2-Dichloropropane 50.0 49.03 ug/L 98 70 -130
Ethylbenzene 50.0 49.71 ug/L 99 70 -130
2-Hexanone 250 202.3 ug/L 81 54 -142
Iodomethane 50.0 49.97 ug/L 100 40 -150
Methylene Chloride 50.0 53.57 ug/L 107 70 -130
4-Methyl-2-pentanone (MIBK)250 203.9 ug/L 82 60 -137
Styrene 50.0 45.21 ug/L 90 70 -130
1,1,1,2-Tetrachloroethane 50.0 45.84 ug/L 92 70 -130
1,1,2,2-Tetrachloroethane 50.0 46.45 ug/L 93 69 -131
Tetrachloroethene 50.0 46.85 ug/L 94 70 -130
Tetrahydrofuran 100 94.16 ug/L 94 51 -136
Toluene 50.0 47.22 ug/L 94 70 -130
trans-1,4-Dichloro-2-butene 50.0 39.72 ug/L 79 41 -150
trans-1,2-Dichloroethene 50.0 50.24 ug/L 100 70 -130
trans-1,3-Dichloropropene 50.0 43.59 ug/L 87 63 -142
1,1,1-Trichloroethane 50.0 51.68 ug/L 103 70 -135
1,1,2-Trichloroethane 50.0 43.52 ug/L 87 70 -130
Trichloroethene 50.0 50.94 ug/L 102 70 -130
Trichlorofluoromethane 50.0 52.53 ug/L 105 59 -150
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332090/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
1,2,3-Trichloropropane 50.0 42.71 ug/L 85 70 -131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 100 103.7 ug/L 104 54 -146
Vinyl chloride 50.0 48.99 ug/L 98 57 -137
Xylenes, Total 100 92.57 ug/L 93 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-332090/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
Acetone 250 288.8 ug/L 116 39 -150 13 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 532.4 ug/L 106 63 -135 9 16
Benzene 50.0 58.29 ug/L 117 70 -130 8 12
Bromochloromethane 50.0 57.80 ug/L 116 70 -130 8 16
Bromodichloromethane 50.0 54.22 ug/L 108 70 -130 8 14
Bromoform 50.0 50.94 E ug/L 102 70 -137 8 14
Bromomethane 50.0 55.68 ug/L 111 53 -150 7 19
2-Butanone (MEK)250 256.6 ug/L 103 55 -143 10 19
Carbon disulfide 50.0 53.42 ug/L 107 64 -135 5 16
Carbon tetrachloride 50.0 56.63 ug/L 113 70 -147 6 16
Chlorobenzene 50.0 47.52 ug/L 95 70 -130 6 12
Chloroethane 50.0 52.91 ug/L 106 60 -138 5 15
Chloroform 50.0 58.90 ug/L 118 70 -130 7 14
Chloromethane 50.0 51.88 ug/L 104 33 -150 4 20
cis-1,2-Dichloroethene 50.0 56.47 ug/L 113 70 -130 7 15
cis-1,3-Dichloropropene 50.0 45.31 ug/L 91 70 -133 8 15
Dibromochloromethane 50.0 53.37 E ug/L 107 70 -133 8 13
1,2-Dibromo-3-Chloropropane 50.0 53.40 ug/L 107 45 -138 8 19
1,2-Dibromoethane (EDB)50.0 46.54 ug/L 93 70 -130 8 13
Dibromomethane 50.0 54.59 ug/L 109 70 -130 10 14
1,2-Dichlorobenzene 50.0 48.10 ug/L 96 70 -130 8 12
1,4-Dichlorobenzene 50.0 48.85 ug/L 98 70 -130 9 12
1,1-Dichloroethane 50.0 55.00 ug/L 110 70 -130 7 17
1,2-Dichloroethane 50.0 56.37 ug/L 113 70 -130 10 13
1,1-Dichloroethene 50.0 56.09 ug/L 112 70 -132 6 20
1,2-Dichloropropane 50.0 52.84 ug/L 106 70 -130 7 15
Ethylbenzene 50.0 52.53 ug/L 105 70 -130 6 12
2-Hexanone 250 221.9 ug/L 89 54 -142 9 17
Iodomethane 50.0 54.03 ug/L 108 40 -150 8 20
Methylene Chloride 50.0 58.16 ug/L 116 70 -130 8 15
4-Methyl-2-pentanone (MIBK)250 224.6 ug/L 90 60 -137 10 21
Styrene 50.0 48.25 ug/L 97 70 -130 7 12
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-332090/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
1,1,1,2-Tetrachloroethane 50.0 49.30 ug/L 99 70 -130 7 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 50.0 51.78 ug/L 104 69 -131 11 15
Tetrachloroethene 50.0 48.45 ug/L 97 70 -130 3 17
Tetrahydrofuran 100 103.9 ug/L 104 51 -136 10 20
Toluene 50.0 50.43 ug/L 101 70 -130 7 13
trans-1,4-Dichloro-2-butene 50.0 43.56 ug/L 87 41 -150 9 20
trans-1,2-Dichloroethene 50.0 53.46 ug/L 107 70 -130 6 15
trans-1,3-Dichloropropene 50.0 47.88 ug/L 96 63 -142 9 13
1,1,1-Trichloroethane 50.0 55.63 ug/L 111 70 -135 7 15
1,1,2-Trichloroethane 50.0 48.10 ug/L 96 70 -130 10 13
Trichloroethene 50.0 55.67 ug/L 111 70 -130 9 14
Trichlorofluoromethane 50.0 55.84 ug/L 112 59 -150 6 22
1,2,3-Trichloropropane 50.0 47.15 ug/L 94 70 -131 10 14
Vinyl acetate 100 106.3 ug/L 106 54 -146 2 20
Vinyl chloride 50.0 51.69 ug/L 103 57 -137 5 15
Xylenes, Total 100 97.63 ug/L 98 70 -132 5 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-101280-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
Acetone <2.66 250 223.6 ug/L 89 39 -150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 506.0 ug/L 101 50 -135
Benzene <0.200 50.0 57.66 ug/L 115 55 -147
Bromochloromethane <0.150 50.0 55.33 ug/L 111 59 -132
Bromodichloromethane <0.170 50.0 51.29 ug/L 103 70 -140
Bromoform <0.290 50.0 45.76 ug/L 92 53 -150
Bromomethane <0.350 50.0 50.23 ug/L 100 30 -150
2-Butanone (MEK)<2.64 250 229.2 ug/L 92 50 -143
Carbon disulfide <0.220 50.0 56.84 ug/L 114 35 -150
Carbon tetrachloride <0.180 50.0 57.98 ug/L 116 56 -150
Chlorobenzene <0.180 50.0 44.72 ug/L 89 70 -130
Chloroethane <0.360 50.0 54.00 ug/L 108 58 -141
Chloroform <0.230 50.0 57.76 ug/L 116 66 -138
Chloromethane <0.360 50.0 53.45 ug/L 107 10 -150
cis-1,2-Dichloroethene <0.210 50.0 55.45 ug/L 111 68 -131
cis-1,3-Dichloropropene <0.170 50.0 41.74 ug/L 83 70 -133
Dibromochloromethane <0.250 50.0 48.69 ug/L 97 66 -140
1,2-Dibromo-3-Chloropropane <0.940 50.0 36.33 ug/L 73 38 -138
1,2-Dibromoethane (EDB)<0.210 50.0 43.17 ug/L 86 65 -137
Dibromomethane <0.450 50.0 52.38 ug/L 105 70 -130
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-101280-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
1,2-Dichlorobenzene <0.190 50.0 43.58 ug/L 87 70 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 50.0 44.81 ug/L 90 70 -130
1,1-Dichloroethane <0.240 50.0 54.95 ug/L 110 61 -139
1,2-Dichloroethane <0.200 50.0 54.41 ug/L 109 64 -136
1,1-Dichloroethene <0.250 50.0 59.94 ug/L 120 54 -150
1,2-Dichloropropane <0.250 50.0 51.90 ug/L 104 67 -130
Ethylbenzene <0.190 50.0 49.96 ug/L 100 65 -139
2-Hexanone <1.28 250 196.2 ug/L 78 44 -150
Iodomethane <1.50 50.0 52.37 ug/L 105 34 -150
Methylene Chloride <1.00 50.0 57.29 ug/L 115 64 -130
4-Methyl-2-pentanone (MIBK)<0.810 250 204.6 ug/L 82 50 -140
Styrene <0.280 50.0 45.08 ug/L 90 70 -130
1,1,1,2-Tetrachloroethane <0.150 50.0 46.14 ug/L 92 70 -130
1,1,2,2-Tetrachloroethane <0.190 50.0 47.30 ug/L 95 56 -145
Tetrachloroethene <0.140 50.0 47.85 ug/L 96 57 -138
Tetrahydrofuran <0.820 100 93.26 ug/L 93 40 -136
Toluene <0.170 50.0 48.37 ug/L 97 64 -136
trans-1,4-Dichloro-2-butene <0.460 50.0 38.27 ug/L 77 39 -150
trans-1,2-Dichloroethene <0.230 50.0 54.87 ug/L 110 59 -143
trans-1,3-Dichloropropene <0.170 50.0 43.79 ug/L 88 63 -142
1,1,1-Trichloroethane <0.190 50.0 57.42 ug/L 115 68 -144
1,1,2-Trichloroethane <0.190 50.0 44.87 ug/L 90 70 -130
Trichloroethene <0.200 50.0 55.30 ug/L 111 63 -135
Trichlorofluoromethane <0.210 50.0 57.99 ug/L 116 44 -150
1,2,3-Trichloropropane <0.230 50.0 42.86 ug/L 86 65 -131
Vinyl acetate <1.71 100 103.9 ug/L 104 43 -146
Vinyl chloride <0.180 50.0 54.52 ug/L 109 57 -150
Xylenes, Total <0.580 100 92.47 ug/L 92 69 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MS MS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101280-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
Acetone <2.66 250 233.9 ug/L 94 39 -150 4 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 491.8 ug/L 98 50 -135 3 17
Benzene <0.200 50.0 57.35 ug/L 115 55 -147 1 50
Bromochloromethane <0.150 50.0 54.30 ug/L 109 59 -132 2 17
Bromodichloromethane <0.170 50.0 51.56 ug/L 103 70 -140 1 18
Bromoform <0.290 50.0 45.37 ug/L 91 53 -150 1 30
Bromomethane <0.350 50.0 51.62 ug/L 103 30 -150 3
2-Butanone (MEK)<2.64 250 231.9 ug/L 93 50 -143 1 19
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101280-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332090
Carbon disulfide <0.220 50.0 56.53 ug/L 113 35 -150 1 21
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 50.0 57.72 ug/L 115 56 -150 0 19
Chlorobenzene <0.180 50.0 45.43 ug/L 91 70 -130 2 14
Chloroethane <0.360 50.0 53.50 ug/L 107 58 -141 1 20
Chloroform <0.230 50.0 56.90 ug/L 114 66 -138 2 18
Chloromethane <0.360 50.0 50.34 ug/L 101 10 -150 6 31
cis-1,2-Dichloroethene <0.210 50.0 55.13 ug/L 110 68 -131 1 17
cis-1,3-Dichloropropene <0.170 50.0 42.13 ug/L 84 70 -133 1 15
Dibromochloromethane <0.250 50.0 49.29 ug/L 99 66 -140 1 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 44.27 ug/L 89 38 -138 20 24
1,2-Dibromoethane (EDB)<0.210 50.0 42.85 ug/L 86 65 -137 1 15
Dibromomethane <0.450 50.0 51.00 ug/L 102 70 -130 3 16
1,2-Dichlorobenzene <0.190 50.0 44.10 ug/L 88 70 -130 1 15
1,4-Dichlorobenzene <0.170 50.0 44.46 ug/L 89 70 -130 1 15
1,1-Dichloroethane <0.240 50.0 54.56 ug/L 109 61 -139 1 17
1,2-Dichloroethane <0.200 50.0 53.95 ug/L 108 64 -136 1 17
1,1-Dichloroethene <0.250 50.0 58.17 ug/L 116 54 -150 3 20
1,2-Dichloropropane <0.250 50.0 51.40 ug/L 103 67 -130 1 17
Ethylbenzene <0.190 50.0 51.01 ug/L 102 65 -139 2 15
2-Hexanone <1.28 250 193.4 ug/L 77 44 -150 1 17
Iodomethane <1.50 50.0 51.60 ug/L 103 34 -150 1 23
Methylene Chloride <1.00 50.0 56.54 ug/L 113 64 -130 1 17
4-Methyl-2-pentanone (MIBK)<0.810 250 197.8 ug/L 79 50 -140 3 21
Styrene <0.280 50.0 45.53 ug/L 91 70 -130 1 24
1,1,1,2-Tetrachloroethane <0.150 50.0 46.35 ug/L 93 70 -130 0 16
1,1,2,2-Tetrachloroethane <0.190 50.0 47.22 ug/L 94 56 -145 0 20
Tetrachloroethene <0.140 50.0 49.23 ug/L 98 57 -138 3 17
Tetrahydrofuran <0.820 100 92.89 ug/L 93 40 -136 0 20
Toluene <0.170 50.0 49.18 ug/L 98 64 -136 2 15
trans-1,4-Dichloro-2-butene <0.460 50.0 38.40 ug/L 77 39 -150 0 26
trans-1,2-Dichloroethene <0.230 50.0 54.11 ug/L 108 59 -143 1 16
trans-1,3-Dichloropropene <0.170 50.0 43.93 ug/L 88 63 -142 0 14
1,1,1-Trichloroethane <0.190 50.0 57.28 ug/L 115 68 -144 0 17
1,1,2-Trichloroethane <0.190 50.0 44.74 ug/L 89 70 -130 0 15
Trichloroethene <0.200 50.0 55.13 ug/L 110 63 -135 0 17
Trichlorofluoromethane <0.210 50.0 56.05 ug/L 112 44 -150 3 22
1,2,3-Trichloropropane <0.230 50.0 41.92 ug/L 84 65 -131 2 19
Vinyl acetate <1.71 100 100.1 ug/L 100 43 -146 4 21
Vinyl chloride <0.180 50.0 53.75 ug/L 107 57 -150 1 17
Xylenes, Total <0.580 100 93.62 ug/L 94 69 -132 1 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MSD MSD
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
991,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-332936/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/20/16 12:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 04/20/16 12:22 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/20/16 12:22 1Benzene
<0.150 0.1501.00 ug/L 04/20/16 12:22 1Bromochloromethane
<0.170 0.1701.00 ug/L 04/20/16 12:22 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/20/16 12:22 1Bromoform
<0.350 0.3501.00 ug/L 04/20/16 12:22 1Bromomethane
<2.64 2.6450.0 ug/L 04/20/16 12:22 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 04/20/16 12:22 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/20/16 12:22 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/20/16 12:22 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/20/16 12:22 1Chloroethane
<0.230 0.2301.00 ug/L 04/20/16 12:22 1Chloroform
<0.360 0.3601.00 ug/L 04/20/16 12:22 1Chloromethane
<0.210 0.2101.00 ug/L 04/20/16 12:22 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/20/16 12:22 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/20/16 12:22 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/20/16 12:22 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/20/16 12:22 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/20/16 12:22 1Dibromomethane
<0.190 0.1901.00 ug/L 04/20/16 12:22 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/20/16 12:22 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/20/16 12:22 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/20/16 12:22 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/20/16 12:22 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/20/16 12:22 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/20/16 12:22 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/20/16 12:22 12-Hexanone
<1.50 1.5010.0 ug/L 04/20/16 12:22 1Iodomethane
<1.00 1.005.00 ug/L 04/20/16 12:22 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/20/16 12:22 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/20/16 12:22 1Styrene
<0.150 0.1501.00 ug/L 04/20/16 12:22 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/20/16 12:22 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/20/16 12:22 1Tetrachloroethene
<0.820 0.82010.0 ug/L 04/20/16 12:22 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 04/20/16 12:22 1Toluene
<0.460 0.4605.00 ug/L 04/20/16 12:22 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/20/16 12:22 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/20/16 12:22 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 04/20/16 12:22 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/20/16 12:22 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/20/16 12:22 1Trichloroethene
<0.210 0.2101.00 ug/L 04/20/16 12:22 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/20/16 12:22 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/20/16 12:22 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/20/16 12:22 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/20/16 12:22 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
4-Bromofluorobenzene (Surr)98 70-130 04/20/16 12:22 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
86 04/20/16 12:22 1Dibromofluoromethane (Surr)70-130
98 04/20/16 12:22 11,2-Dichloroethane-d4 (Surr)70 -130
100 04/20/16 12:22 1Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332936/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
Acetone 250 271.4 ug/L 109 39 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 500 492.6 ug/L 99 63 -135
Benzene 50.0 42.90 ug/L 86 70 -130
Bromochloromethane 50.0 47.46 ug/L 95 70 -130
Bromodichloromethane 50.0 51.43 ug/L 103 70 -130
Bromoform 50.0 53.20 E ug/L 106 70 -137
Bromomethane 50.0 47.21 ug/L 94 53 -150
2-Butanone (MEK)250 241.8 ug/L 97 55 -143
Carbon disulfide 50.0 45.99 ug/L 92 64 -135
Carbon tetrachloride 50.0 48.40 ug/L 97 70 -147
Chlorobenzene 50.0 49.64 ug/L 99 70 -130
Chloroethane 50.0 45.62 ug/L 91 60 -138
Chloroform 50.0 45.48 ug/L 91 70 -130
Chloromethane 50.0 41.98 ug/L 84 33 -150
cis-1,2-Dichloroethene 50.0 46.92 ug/L 94 70 -130
cis-1,3-Dichloropropene 50.0 49.89 ug/L 100 70 -133
Dibromochloromethane 50.0 51.07 E ug/L 102 70 -133
1,2-Dibromo-3-Chloropropane 50.0 51.60 ug/L 103 45 -138
1,2-Dibromoethane (EDB)50.0 53.30 ug/L 107 70 -130
Dibromomethane 50.0 49.11 ug/L 98 70 -130
1,2-Dichlorobenzene 50.0 51.04 ug/L 102 70 -130
1,4-Dichlorobenzene 50.0 49.28 ug/L 99 70 -130
1,1-Dichloroethane 50.0 45.74 ug/L 91 70 -130
1,2-Dichloroethane 50.0 46.64 ug/L 93 70 -130
1,1-Dichloroethene 50.0 46.83 ug/L 94 70 -132
1,2-Dichloropropane 50.0 45.88 ug/L 92 70 -130
Ethylbenzene 50.0 46.78 ug/L 94 70 -130
2-Hexanone 250 256.9 ug/L 103 54 -142
Iodomethane 50.0 41.68 ug/L 83 40 -150
Methylene Chloride 50.0 48.56 ug/L 97 70 -130
4-Methyl-2-pentanone (MIBK)250 246.5 ug/L 99 60 -137
Styrene 50.0 51.35 ug/L 103 70 -130
1,1,1,2-Tetrachloroethane 50.0 52.26 ug/L 105 70 -130
1,1,2,2-Tetrachloroethane 50.0 52.84 ug/L 106 69 -131
Tetrachloroethene 50.0 46.29 ug/L 93 70 -130
Tetrahydrofuran 100 98.16 ug/L 98 51 -136
Toluene 50.0 46.09 ug/L 92 70 -130
trans-1,4-Dichloro-2-butene 50.0 49.37 ug/L 99 41 -150
trans-1,2-Dichloroethene 50.0 45.04 ug/L 90 70 -130
trans-1,3-Dichloropropene 50.0 47.28 ug/L 95 63 -142
1,1,1-Trichloroethane 50.0 46.65 ug/L 93 70 -135
1,1,2-Trichloroethane 50.0 51.01 ug/L 102 70 -130
Trichloroethene 50.0 47.26 ug/L 95 70 -130
Trichlorofluoromethane 50.0 44.67 ug/L 89 59 -150
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332936/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
1,2,3-Trichloropropane 50.0 50.25 ug/L 101 70 -131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 100 100.9 ug/L 101 54 -146
Vinyl chloride 50.0 46.93 ug/L 94 57 -137
Xylenes, Total 100 97.41 ug/L 97 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
1071,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-332936/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
Acetone 250 254.6 ug/L 102 39 -150 6 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 500 483.9 ug/L 97 63 -135 2 16
Benzene 50.0 41.41 ug/L 83 70 -130 4 12
Bromochloromethane 50.0 49.03 ug/L 98 70 -130 3 16
Bromodichloromethane 50.0 49.70 ug/L 99 70 -130 3 14
Bromoform 50.0 52.02 E ug/L 104 70 -137 2 14
Bromomethane 50.0 50.19 E ug/L 100 53 -150 6 19
2-Butanone (MEK)250 236.6 ug/L 95 55 -143 2 19
Carbon disulfide 50.0 43.49 ug/L 87 64 -135 6 16
Carbon tetrachloride 50.0 46.31 ug/L 93 70 -147 4 16
Chlorobenzene 50.0 47.69 ug/L 95 70 -130 4 12
Chloroethane 50.0 43.33 ug/L 87 60 -138 5 15
Chloroform 50.0 43.63 ug/L 87 70 -130 4 14
Chloromethane 50.0 48.98 ug/L 98 33 -150 15 20
cis-1,2-Dichloroethene 50.0 45.25 ug/L 90 70 -130 4 15
cis-1,3-Dichloropropene 50.0 48.15 ug/L 96 70 -133 4 15
Dibromochloromethane 50.0 50.38 E ug/L 101 70 -133 1 13
1,2-Dibromo-3-Chloropropane 50.0 51.14 ug/L 102 45 -138 1 19
1,2-Dibromoethane (EDB)50.0 51.49 ug/L 103 70 -130 3 13
Dibromomethane 50.0 50.17 ug/L 100 70 -130 2 14
1,2-Dichlorobenzene 50.0 50.11 ug/L 100 70 -130 2 12
1,4-Dichlorobenzene 50.0 48.25 ug/L 97 70 -130 2 12
1,1-Dichloroethane 50.0 41.83 ug/L 84 70 -130 9 17
1,2-Dichloroethane 50.0 46.07 ug/L 92 70 -130 1 13
1,1-Dichloroethene 50.0 44.66 ug/L 89 70 -132 5 20
1,2-Dichloropropane 50.0 44.21 ug/L 88 70 -130 4 15
Ethylbenzene 50.0 44.85 ug/L 90 70 -130 4 12
2-Hexanone 250 247.7 ug/L 99 54 -142 4 17
Iodomethane 50.0 44.87 ug/L 90 40 -150 7 20
Methylene Chloride 50.0 47.41 ug/L 95 70 -130 2 15
4-Methyl-2-pentanone (MIBK)250 251.2 ug/L 100 60 -137 2 21
Styrene 50.0 49.46 ug/L 99 70 -130 4 12
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-332936/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
1,1,1,2-Tetrachloroethane 50.0 50.25 ug/L 100 70 -130 4 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 50.0 51.93 ug/L 104 69 -131 2 15
Tetrachloroethene 50.0 44.90 ug/L 90 70 -130 3 17
Tetrahydrofuran 100 91.25 ug/L 91 51 -136 7 20
Toluene 50.0 44.19 ug/L 88 70 -130 4 13
trans-1,4-Dichloro-2-butene 50.0 50.42 ug/L 101 41 -150 2 20
trans-1,2-Dichloroethene 50.0 44.10 ug/L 88 70 -130 2 15
trans-1,3-Dichloropropene 50.0 46.58 ug/L 93 63 -142 1 13
1,1,1-Trichloroethane 50.0 44.42 ug/L 89 70 -135 5 15
1,1,2-Trichloroethane 50.0 49.73 ug/L 99 70 -130 3 13
Trichloroethene 50.0 45.69 ug/L 91 70 -130 3 14
Trichlorofluoromethane 50.0 43.76 ug/L 88 59 -150 2 22
1,2,3-Trichloropropane 50.0 48.68 ug/L 97 70 -131 3 14
Vinyl acetate 100 100.9 ug/L 101 54 -146 0 20
Vinyl chloride 50.0 45.66 ug/L 91 57 -137 3 15
Xylenes, Total 100 93.86 ug/L 94 70 -132 4 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
93Dibromofluoromethane (Surr)70 -130
1091,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-101703-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
Acetone <2.66 250 220.7 ug/L 88 39 -150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 500 459.5 ug/L 92 50 -135
Benzene <0.200 50.0 40.54 ug/L 81 55 -147
Bromochloromethane <0.150 50.0 46.94 ug/L 94 59 -132
Bromodichloromethane <0.170 50.0 46.89 ug/L 94 70 -140
Bromoform <0.290 50.0 48.18 ug/L 96 53 -150
Bromomethane <0.350 50.0 47.40 ug/L 95 30 -150
2-Butanone (MEK)<2.64 250 216.9 ug/L 87 50 -143
Carbon disulfide <0.220 50.0 43.60 ug/L 87 35 -150
Carbon tetrachloride 0.819 J 50.0 47.80 ug/L 94 56 -150
Chlorobenzene <0.180 50.0 46.57 ug/L 93 70 -130
Chloroethane <0.360 50.0 42.97 ug/L 86 58 -141
Chloroform 0.238 J 50.0 42.87 ug/L 85 66 -138
Chloromethane <0.360 50.0 49.21 ug/L 98 10 -150
cis-1,2-Dichloroethene <0.210 50.0 44.05 ug/L 88 68 -131
cis-1,3-Dichloropropene <0.170 50.0 45.04 ug/L 90 70 -133
Dibromochloromethane <0.250 50.0 47.57 ug/L 95 66 -140
1,2-Dibromo-3-Chloropropane <0.940 50.0 45.44 ug/L 91 38 -138
1,2-Dibromoethane (EDB)<0.210 50.0 48.48 ug/L 97 65 -137
Dibromomethane <0.450 50.0 46.95 ug/L 94 70 -130
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-101703-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
1,2-Dichlorobenzene <0.190 50.0 47.08 ug/L 94 70 -130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 50.0 46.43 ug/L 93 70 -130
1,1-Dichloroethane <0.240 50.0 42.44 ug/L 85 61 -139
1,2-Dichloroethane <0.200 50.0 43.64 ug/L 87 64 -136
1,1-Dichloroethene <0.250 50.0 47.09 ug/L 94 54 -150
1,2-Dichloropropane <0.250 50.0 42.03 ug/L 84 67 -130
Ethylbenzene <0.190 50.0 44.61 ug/L 89 65 -139
2-Hexanone <1.28 250 230.6 ug/L 92 44 -150
Iodomethane <1.50 50.0 44.89 ug/L 90 34 -150
Methylene Chloride <1.00 50.0 45.12 ug/L 90 64 -130
4-Methyl-2-pentanone (MIBK)<0.810 250 233.7 ug/L 93 50 -140
Styrene <0.280 50.0 47.53 ug/L 95 70 -130
1,1,1,2-Tetrachloroethane <0.150 50.0 48.60 ug/L 97 70 -130
1,1,2,2-Tetrachloroethane <0.190 50.0 48.06 ug/L 96 56 -145
Tetrachloroethene <0.140 50.0 45.63 ug/L 91 57 -138
Tetrahydrofuran <0.820 100 88.68 ug/L 89 40 -136
Toluene <0.170 50.0 43.93 ug/L 88 64 -136
trans-1,4-Dichloro-2-butene <0.460 50.0 43.14 ug/L 86 39 -150
trans-1,2-Dichloroethene <0.230 50.0 43.61 ug/L 87 59 -143
trans-1,3-Dichloropropene <0.170 50.0 41.90 ug/L 84 63 -142
1,1,1-Trichloroethane <0.190 50.0 44.85 ug/L 90 68 -144
1,1,2-Trichloroethane <0.190 50.0 47.71 ug/L 95 70 -130
Trichloroethene <0.200 50.0 45.13 ug/L 90 63 -135
Trichlorofluoromethane <0.210 50.0 37.67 ug/L 75 44 -150
1,2,3-Trichloropropane <0.230 50.0 46.79 ug/L 94 65 -131
Vinyl acetate <1.71 100 88.29 ug/L 88 43 -146
Vinyl chloride <0.180 50.0 46.17 ug/L 92 57 -150
Xylenes, Total <0.580 100 91.44 ug/L 91 69 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
MS MS
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
1071,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101703-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
Acetone <2.66 250 234.0 ug/L 94 39 -150 6 50
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 500 460.1 ug/L 92 50 -135 0 17
Benzene <0.200 50.0 42.14 ug/L 84 55 -147 4 50
Bromochloromethane <0.150 50.0 48.74 ug/L 97 59 -132 4 17
Bromodichloromethane <0.170 50.0 49.50 ug/L 99 70 -140 5 18
Bromoform <0.290 50.0 50.90 E ug/L 102 53 -150 5 30
Bromomethane <0.350 50.0 50.86 E ug/L 102 30 -150 7
2-Butanone (MEK)<2.64 250 227.2 ug/L 91 50 -143 5 19
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101703-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332936
Carbon disulfide <0.220 50.0 44.39 ug/L 89 35 -150 2 21
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride 0.819 J 50.0 49.88 ug/L 98 56 -150 4 19
Chlorobenzene <0.180 50.0 48.20 ug/L 96 70 -130 3 14
Chloroethane <0.360 50.0 44.98 ug/L 90 58 -141 5 20
Chloroform 0.238 J 50.0 44.47 ug/L 88 66 -138 4 18
Chloromethane <0.360 50.0 49.78 ug/L 100 10 -150 1 31
cis-1,2-Dichloroethene <0.210 50.0 44.87 ug/L 90 68 -131 2 17
cis-1,3-Dichloropropene <0.170 50.0 46.67 ug/L 93 70 -133 4 15
Dibromochloromethane <0.250 50.0 49.58 ug/L 99 66 -140 4 15
1,2-Dibromo-3-Chloropropane <0.940 50.0 49.95 ug/L 100 38 -138 9 24
1,2-Dibromoethane (EDB)<0.210 50.0 50.98 ug/L 102 65 -137 5 15
Dibromomethane <0.450 50.0 49.05 ug/L 98 70 -130 4 16
1,2-Dichlorobenzene <0.190 50.0 50.19 ug/L 100 70 -130 6 15
1,4-Dichlorobenzene <0.170 50.0 48.98 ug/L 98 70 -130 5 15
1,1-Dichloroethane <0.240 50.0 44.99 ug/L 90 61 -139 6 17
1,2-Dichloroethane <0.200 50.0 45.03 ug/L 90 64 -136 3 17
1,1-Dichloroethene <0.250 50.0 48.30 ug/L 97 54 -150 3 20
1,2-Dichloropropane <0.250 50.0 43.73 ug/L 87 67 -130 4 17
Ethylbenzene <0.190 50.0 46.22 ug/L 92 65 -139 4 15
2-Hexanone <1.28 250 241.1 ug/L 96 44 -150 4 17
Iodomethane <1.50 50.0 46.89 ug/L 94 34 -150 4 23
Methylene Chloride <1.00 50.0 46.21 ug/L 92 64 -130 2 17
4-Methyl-2-pentanone (MIBK)<0.810 250 245.0 ug/L 98 50 -140 5 21
Styrene <0.280 50.0 49.35 ug/L 99 70 -130 4 24
1,1,1,2-Tetrachloroethane <0.150 50.0 50.00 ug/L 100 70 -130 3 16
1,1,2,2-Tetrachloroethane <0.190 50.0 51.57 ug/L 103 56 -145 7 20
Tetrachloroethene <0.140 50.0 46.12 ug/L 92 57 -138 1 17
Tetrahydrofuran <0.820 100 91.29 ug/L 91 40 -136 3 20
Toluene <0.170 50.0 45.36 ug/L 91 64 -136 3 15
trans-1,4-Dichloro-2-butene <0.460 50.0 47.18 ug/L 94 39 -150 9 26
trans-1,2-Dichloroethene <0.230 50.0 45.59 ug/L 91 59 -143 4 16
trans-1,3-Dichloropropene <0.170 50.0 44.99 ug/L 90 63 -142 7 14
1,1,1-Trichloroethane <0.190 50.0 46.30 ug/L 93 68 -144 3 17
1,1,2-Trichloroethane <0.190 50.0 49.45 ug/L 99 70 -130 4 15
Trichloroethene <0.200 50.0 46.46 ug/L 93 63 -135 3 17
Trichlorofluoromethane <0.210 50.0 46.83 ug/L 94 44 -150 22 22
1,2,3-Trichloropropane <0.230 50.0 48.25 ug/L 96 65 -131 3 19
Vinyl acetate <1.71 100 91.53 ug/L 92 43 -146 4 21
Vinyl chloride <0.180 50.0 46.52 ug/L 93 57 -150 1 17
Xylenes, Total <0.580 100 94.53 ug/L 95 69 -132 3 15
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MSD MSD
Qualifier Limits%Recovery
90Dibromofluoromethane (Surr)70 -130
1081,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 490-331914/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331914
RL MDL
Sulfate <0.600 1.00 0.600 mg/L 04/15/16 11:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-331914/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331914
Sulfate 100 96.88 mg/L 97 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-99810-B-16 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331914
Sulfate 118 F1 100 195.0 F1 mg/L 77 80 -120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-99810-B-16 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331914
Sulfate 118 F1 100 195.7 F1 mg/L 77 80 -120 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-335077/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335464 Prep Batch: 335077
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/27/16 14:29 04/28/16 10:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 04/27/16 14:29 04/28/16 10:48 1Barium
<0.000500 0.0005000.00100 mg/L 04/27/16 14:29 04/28/16 10:48 1Cadmium
<0.00300 0.003000.00500 mg/L 04/27/16 14:29 04/28/16 10:48 1Chromium
<0.00200 0.002000.00500 mg/L 04/27/16 14:29 04/28/16 10:48 1Lead
<0.00300 0.003000.0100 mg/L 04/27/16 14:29 04/28/16 10:48 1Nickel
<0.00500 0.005000.0100 mg/L 04/27/16 14:29 04/28/16 10:48 1Selenium
<0.00300 0.003000.00500 mg/L 04/27/16 14:29 04/28/16 10:48 1Silver
Client Sample ID: Method BlankLab Sample ID: MB 490-335077/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335601 Prep Batch: 335077
RL MDL
Copper <0.00500 0.0100 0.00500 mg/L 04/27/16 14:29 04/28/16 17:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-335077/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335464 Prep Batch: 335077
Arsenic 0.0500 0.04810 mg/L 96 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.029 mg/L 101 80 -120
Cadmium 0.0500 0.04980 mg/L 100 80 -120
Chromium 0.200 0.1952 mg/L 98 80 -120
Lead 0.0500 0.05040 mg/L 101 80 -120
Nickel 0.500 0.5140 mg/L 103 80 -120
Selenium 0.0500 0.04740 mg/L 95 80 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-335077/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335601 Prep Batch: 335077
Copper 0.250 0.2430 mg/L 97 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-335077/8-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335464 Prep Batch: 335077
Silver 0.0500 0.05230 mg/L 105 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-102378-C-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335464 Prep Batch: 335077
Arsenic <0.00860 0.0500 0.04780 mg/L 96 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0943 2.00 2.066 mg/L 99 75 -125
Cadmium <0.000500 0.0500 0.04840 mg/L 97 75 -125
Chromium <0.00300 0.200 0.1878 mg/L 94 75 -125
Lead 0.00260 J 0.0500 0.05100 mg/L 97 75 -125
Nickel <0.00300 0.500 0.4923 mg/L 98 75 -125
Selenium 0.00530 J 0.0500 0.05530 mg/L 100 75 -125
Silver <0.00300 0.0500 0.03840 mg/L 77 75 -125
Client Sample ID: Matrix SpikeLab Sample ID: 490-102378-C-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335601 Prep Batch: 335077
Copper <0.00500 0.250 0.2410 mg/L 96 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-102378-C-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335464 Prep Batch: 335077
Arsenic <0.00860 0.0500 0.04860 mg/L 97 75 -125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-102378-C-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335464 Prep Batch: 335077
Barium 0.0943 2.00 2.071 mg/L 99 75 -125 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Cadmium <0.000500 0.0500 0.04840 mg/L 97 75 -125 0 20
Chromium <0.00300 0.200 0.1879 mg/L 94 75 -125 0 20
Lead 0.00260 J 0.0500 0.05100 mg/L 97 75 -125 0 20
Nickel <0.00300 0.500 0.4923 mg/L 98 75 -125 0 20
Selenium 0.00530 J 0.0500 0.05400 mg/L 97 75 -125 2 20
Silver <0.00300 0.0500 0.03880 mg/L 78 75 -125 1 20
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-102378-C-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335601 Prep Batch: 335077
Copper <0.00500 0.250 0.2422 mg/L 97 75 -125 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-335080/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335692 Prep Batch: 335080
RL MDL
Antimony <0.500 2.00 0.500 ug/L 04/27/16 14:35 04/29/16 07:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.00 1.002.00 ug/L 04/27/16 14:35 04/29/16 07:36 1Beryllium
<0.500 0.5002.00 ug/L 04/27/16 14:35 04/29/16 07:36 1Cobalt
<0.500 0.5002.00 ug/L 04/27/16 14:35 04/29/16 07:36 1Thallium
2.544 J 2.104.00 ug/L 04/27/16 14:35 04/29/16 07:36 1Vanadium
Client Sample ID: Method BlankLab Sample ID: MB 490-335080/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335987 Prep Batch: 335080
RL MDL
Zinc <10.0 25.0 10.0 ug/L 04/27/16 14:35 04/29/16 14:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-335080/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335692 Prep Batch: 335080
Antimony 100 97.02 ug/L 97 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 91.57 ug/L 92 80 -120
Cobalt 100 88.37 ug/L 88 80 -120
Thallium 100 91.76 ug/L 92 80 -120
Vanadium 100 94.64 ug/L 95 80 -120
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-335080/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335987 Prep Batch: 335080
Zinc 100 88.26 ug/L 88 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-102378-F-2-D MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335692 Prep Batch: 335080
Antimony <0.500 100 102.0 ug/L 102 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <1.00 100 93.57 ug/L 94 75 -125
Cobalt 5.54 100 94.82 ug/L 89 75 -125
Thallium <0.500 100 95.92 ug/L 96 75 -125
Vanadium 3.33 J B 100 93.25 ug/L 90 75 -125
Client Sample ID: Matrix SpikeLab Sample ID: 490-102378-F-2-D MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335987 Prep Batch: 335080
Zinc <10.0 100 92.38 ug/L 92 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-102378-F-2-E MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335692 Prep Batch: 335080
Antimony <0.500 100 101.1 ug/L 101 75 -125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <1.00 100 93.97 ug/L 94 75 -125 0 20
Cobalt 5.54 100 97.76 ug/L 92 75 -125 3 20
Thallium <0.500 100 95.74 ug/L 96 75 -125 0 20
Vanadium 3.33 J B 100 97.43 ug/L 94 75 -125 4 20
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-102378-F-2-E MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335987 Prep Batch: 335080
Zinc <10.0 100 90.76 ug/L 91 75 -125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-334871/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335131 Prep Batch: 334871
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/27/16 05:19 04/27/16 09:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-334871/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335131 Prep Batch: 334871
Mercury 1.00 0.9543 ug/L 95 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-102334-D-5-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335131 Prep Batch: 334871
Mercury <0.100 1.00 0.9166 ug/L 92 75 -125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-102334-D-5-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 335131 Prep Batch: 334871
Mercury <0.100 1.00 0.8732 ug/L 87 75 -125 5 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 365.4 - Phosphorus, Total
Client Sample ID: Method BlankLab Sample ID: MB 490-334638/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334795 Prep Batch: 334638
RL MDL
Phosphorus, Total <0.0500 0.100 0.0500 mg/L 04/26/16 11:36 04/26/16 16:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-334638/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334795 Prep Batch: 334638
Phosphorus, Total 2.00 1.809 mg/L 90 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-101529-B-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334795 Prep Batch: 334638
Phosphorus, Total 0.0550 J F1 2.00 3.497 F1 mg/L 172 73 -119
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-101529-B-3-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 334795 Prep Batch: 334638
Phosphorus, Total 0.0550 J F1 2.00 3.414 F1 mg/L 168 73 -119 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: SM 5220D - COD
Client Sample ID: Method BlankLab Sample ID: MB 490-332870/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332870
RL MDL
Chemical Oxygen Demand <4.00 20.0 4.00 mg/L 04/19/16 16:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332870/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332870
Chemical Oxygen Demand 50.0 52.13 mg/L 104 95 -105
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-332870/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332870
Chemical Oxygen Demand 50.0 51.61 mg/L 103 95 -105 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 580-58650-D-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332870
Chemical Oxygen Demand 56.1 F1 50.0 100.3 F1 mg/L 88 95 -105
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 580-58650-D-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332870
Chemical Oxygen Demand 56.1 F1 50.0 93.56 F1 mg/L 75 95 -105 7 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 490-101763-B-10 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332870
Chemical Oxygen Demand 19.5 J 20.74 mg/L 6 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM5210B - BOD, 5 Day
Client Sample ID: Method BlankLab Sample ID: USB 490-332917/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332917
RL RL
Biochemical Oxygen Demand <2.00 2.00 2.00 mg/L 04/14/16 18:43 1
USB USB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample Results
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method: SM5210B - BOD, 5 Day (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-332917/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332917
Biochemical Oxygen Demand 3.96 3.391 mg/L 86 85 -115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: LT-01Lab Sample ID: 490-101527-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 332917
Biochemical Oxygen Demand 17.9 18.93 mg/L 6 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
GC/MS VOA
Analysis Batch: 332090
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-101280-B-1 MS Matrix Spike Total/NA
Water 8260B490-101280-C-1 MSD Matrix Spike Duplicate Total/NA
Water 8260B490-101527-1 LT-01 Total/NA
Water 8260B490-101527-2 Trip Blank Total/NA
Water 8260BLCS 490-332090/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-332090/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-332090/8 Method Blank Total/NA
Analysis Batch: 332936
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-101527-2 Trip Blank Total/NA
Water 8260B490-101703-B-1 MS Matrix Spike Total/NA
Water 8260B490-101703-C-1 MSD Matrix Spike Duplicate Total/NA
Water 8260BLCS 490-332936/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-332936/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-332936/10 Method Blank Total/NA
HPLC/IC
Analysis Batch: 331914
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0490-99810-B-16 MS Matrix Spike Total/NA
Water 300.0490-99810-B-16 MSD Matrix Spike Duplicate Total/NA
Water 300.0490-101527-1 LT-01 Total/NA
Water 300.0LCS 490-331914/5 Lab Control Sample Total/NA
Water 300.0MB 490-331914/4 Method Blank Total/NA
Metals
Prep Batch: 334871
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-101527-1 LT-01 Total/NA
Water 7470A490-102334-D-5-B MS Matrix Spike Total/NA
Water 7470A490-102334-D-5-C MSD Matrix Spike Duplicate Total/NA
Water 7470ALCS 490-334871/2-A Lab Control Sample Total/NA
Water 7470AMB 490-334871/1-A Method Blank Total/NA
Prep Batch: 335077
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-101527-1 LT-01 Total/NA
Water 3010A490-102378-C-1-B MS Matrix Spike Total/NA
Water 3010A490-102378-C-1-C MSD Matrix Spike Duplicate Total/NA
Water 3010ALCS 490-335077/2-A Lab Control Sample Total/NA
Water 3010ALCS 490-335077/8-A Lab Control Sample Total/NA
Water 3010AMB 490-335077/1-A Method Blank Total/NA
Prep Batch: 335080
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-101527-1 LT-01 Total/NA
Water 3010A490-102378-F-2-D MS Matrix Spike Total/NA
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QC Association Summary
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Metals (Continued)
Prep Batch: 335080 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-102378-F-2-E MSD Matrix Spike Duplicate Total/NA
Water 3010ALCS 490-335080/2-A Lab Control Sample Total/NA
Water 3010AMB 490-335080/1-A Method Blank Total/NA
Analysis Batch: 335131
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 334871490-101527-1 LT-01 Total/NA
Water 7470A 334871490-102334-D-5-B MS Matrix Spike Total/NA
Water 7470A 334871490-102334-D-5-C MSD Matrix Spike Duplicate Total/NA
Water 7470A 334871LCS 490-334871/2-A Lab Control Sample Total/NA
Water 7470A 334871MB 490-334871/1-A Method Blank Total/NA
Analysis Batch: 335464
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 335077490-101527-1 LT-01 Total/NA
Water 6010D 335077490-102378-C-1-B MS Matrix Spike Total/NA
Water 6010D 335077490-102378-C-1-C MSD Matrix Spike Duplicate Total/NA
Water 6010D 335077LCS 490-335077/2-A Lab Control Sample Total/NA
Water 6010D 335077LCS 490-335077/8-A Lab Control Sample Total/NA
Water 6010D 335077MB 490-335077/1-A Method Blank Total/NA
Analysis Batch: 335601
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 335077490-101527-1 LT-01 Total/NA
Water 6010D 335077490-102378-C-1-B MS Matrix Spike Total/NA
Water 6010D 335077490-102378-C-1-C MSD Matrix Spike Duplicate Total/NA
Water 6010D 335077LCS 490-335077/2-A Lab Control Sample Total/NA
Water 6010D 335077MB 490-335077/1-A Method Blank Total/NA
Analysis Batch: 335692
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 335080490-101527-1 LT-01 Total/NA
Water 6020B 335080490-102378-F-2-D MS Matrix Spike Total/NA
Water 6020B 335080490-102378-F-2-E MSD Matrix Spike Duplicate Total/NA
Water 6020B 335080LCS 490-335080/2-A Lab Control Sample Total/NA
Water 6020B 335080MB 490-335080/1-A Method Blank Total/NA
Analysis Batch: 335772
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 335077490-101527-1 LT-01 Total/NA
Analysis Batch: 335987
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 335080490-101527-1 LT-01 Total/NA
Water 6020B 335080490-101527-1 LT-01 Total/NA
Water 6020B 335080490-102378-F-2-D MS Matrix Spike Total/NA
Water 6020B 335080490-102378-F-2-E MSD Matrix Spike Duplicate Total/NA
Water 6020B 335080LCS 490-335080/2-A Lab Control Sample Total/NA
Water 6020B 335080MB 490-335080/1-A Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
General Chemistry
Analysis Batch: 332870
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 5220D490-101527-1 LT-01 Total/NA
Water SM 5220D490-101763-B-10 DU Duplicate Total/NA
Water SM 5220D580-58650-D-1 MS Matrix Spike Total/NA
Water SM 5220D580-58650-D-1 MSD Matrix Spike Duplicate Total/NA
Water SM 5220DLCS 490-332870/4 Lab Control Sample Total/NA
Water SM 5220DLCSD 490-332870/5 Lab Control Sample Dup Total/NA
Water SM 5220DMB 490-332870/3 Method Blank Total/NA
Analysis Batch: 332917
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM5210B490-101527-1 LT-01 Total/NA
Water SM5210B490-101527-1 DU LT-01 Total/NA
Water SM5210BLCS 490-332917/2 Lab Control Sample Total/NA
Water SM5210BUSB 490-332917/1 Method Blank Total/NA
Prep Batch: 334638
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 365.2/365.3/365490-101527-1 LT-01 Total/NA
Water 365.2/365.3/365490-101529-B-3-B MS Matrix Spike Total/NA
Water 365.2/365.3/365490-101529-B-3-C MSD Matrix Spike Duplicate Total/NA
Water 365.2/365.3/365LCS 490-334638/2-A Lab Control Sample Total/NA
Water 365.2/365.3/365MB 490-334638/1-A Method Blank Total/NA
Analysis Batch: 334780
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Nitrate by calc490-101527-1 LT-01 Total/NA
Analysis Batch: 334795
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 365.4 334638490-101527-1 LT-01 Total/NA
Water 365.4 334638490-101529-B-3-B MS Matrix Spike Total/NA
Water 365.4 334638490-101529-B-3-C MSD Matrix Spike Duplicate Total/NA
Water 365.4 334638LCS 490-334638/2-A Lab Control Sample Total/NA
Water 365.4 334638MB 490-334638/1-A Method Blank Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101527-1
Project/Site: Madison Co Operating Landfill-Leachate
Client Sample ID: LT-01 Lab Sample ID: 490-101527-1
Matrix: WaterDate Collected: 04/13/16 12:38
Date Received: 04/14/16 09:45
Analysis 8260B NC04/16/16 05:541 TAL NSH332090
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Analysis 300.0 1 331914 04/15/16 16:00 JHS TAL NSHTotal/NA 10 mL
Prep 3010A 335077 04/27/16 14:29 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 335464 04/28/16 11:26 ADN TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 335077 04/27/16 14:29 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 5 335601 04/28/16 18:12 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 335077 04/27/16 14:29 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 10 335772 04/29/16 11:57 TSC TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 335080 04/27/16 14:35 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 5 335692 04/29/16 08:22 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 335080 04/27/16 14:35 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 335987 04/29/16 14:56 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 3010A 335080 04/27/16 14:35 KMS TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 20 335987 04/29/16 15:36 KKK TAL NSHTotal/NA 50 mL 50 mL
Prep 7470A 334871 04/27/16 13:52 BLG TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 335131 04/27/16 16:07 RDF TAL NSHTotal/NA 30.0 mL 30.0 mL
Prep 365.2/365.3/365 334638 04/26/16 11:36 LDT TAL NSHTotal/NA 1 mL 20 mL
Analysis 365.4 1 334795 04/26/16 16:48 SDL TAL NSHTotal/NA 1 mL 20 mL
Analysis Nitrate by calc 1 334780 04/14/16 16:20 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis SM 5220D 2 332870 04/19/16 16:36 MSJ TAL NSHTotal/NA 2 mL 2 mL
Analysis SM5210B 5 332917 YSJ TAL NSHTotal/NA 300 mL
04/14/16 18:43
04/19/16 13:20
(Start)
(End)
Client Sample ID: Trip Blank Lab Sample ID: 490-101527-2
Matrix: WaterDate Collected: 04/13/16 00:01
Date Received: 04/14/16 09:45
Analysis 8260B KS04/20/16 15:111 TAL NSH332936
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Analysis 8260B 1 332090 04/16/16 05:24 NC TAL NSHTotal/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-101527-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill-Leachate
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
MCAWW300.0 Anions, Ion Chromatography TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
EPA365.4 Phosphorus, Total TAL NSH
SMNitrate by calc Nitrogen, Nitrate-Nitrite TAL NSH
SMSM 5220D COD TAL NSH
SMSM5210BBOD, 5 Day TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-101527-1
Project/Site: Madison Co Operating Landfill-Leachate
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Nitrate by calc Water Nitrate as N
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-101527-1
Login Number: 101527
Question Answer Comment
Creator: Huskey, Adam
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueResidual Chlorine Checked.
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APPENDIX C

Environmental Monitoring Reporting Form
and
Electronic Submittal of Environmental
Monitoring Data
5803Apr2016 (Electronic Only)