5803_MadisonCountyCDLF_GWMR_DIN27932_20161018

February 2017
Madison County Operating Solid Waste Facility, Permit No. 58-03
Fall 2016
Semiannual Water Quality Monitoring Report
Prepared for Madison County, North Carolina

Fall 2016 Semiannual Water Quality Monitoring Report 1 February 2017
TABLE OF CONTENTS
1 Introduction ................................................................................................................................ 2
2 Methods ....................................................................................................................................... 3
2.1 Groundwater Purging and Sampling Methods ....................................................................................... 3
2.2 Surface Water Sampling Methods ................................................................................................................ 3
2.3 Leachate Sampling Methods .......................................................................................................................... 4
2.4 Sample Handling, Documentation, and Analysis .................................................................................... 4
3 Findings ........................................................................................................................................ 5
3.1 Analytical Results ................................................................................................................................................. 5
3.1.1 Groundwater Monitoring Wells ..................................................................................................... 6
3.1.2 Surface Water ........................................................................................................................................ 6
3.1.3 Leachate .................................................................................................................................................. 7
4 Hydrogeology ............................................................................................................................. 8
5 Summary ...................................................................................................................................... 9
5.1 Future Activities ................................................................................................................................................... 9
6 References ................................................................................................................................. 10

TABLES
Table 1 Well Construction Details and Corresponding Elevations
Table 2 Summary of Laboratory Analyses Performed on Samples
Table 3 Groundwater and Surface Water Summary of Analytical Results
Table 4 Leachate Summary of Analytical Results
FIGURES
Figure 1 Site Location Map
Figure 2 Sample Locations
Figure 3 Generalized Groundwater Flow
APPENDICES
Appendix A Sampling Logs and Equipment Documentation and Instrument Calibration Data
Sheets
Appendix B Report of Laboratory Analysis and Chain-of-Custody Documentation

Fall 2016 Semiannual Water Quality Monitoring Report 2 February 2017
1 Introduction
Anchor QEA of North Carolina, PLLC (Anchor QEA) is pleased to present the results of semiannual fall
2016 water quality monitoring at the Madison County Operating Solid Waste facility.
The Madison County Solid Waste Department operates a solid waste facility (Operating Landfill)
located on Craig Rudisill Road, west of U.S. Highway 25/70 near Marshall, North Carolina. A site
location map is included as Figure 1. The Operating Landfill includes the following permitted
components:
 Operating Construction and Demolition Debris (C&D) landfill cell (Permit No. 58-03)
 Operating Transfer Station (Permit No. 58-03T)
 Closed C&D landfill cell (Permit No. 58-03)
 Closed Municipal Solid Waste (MSW) landfill cell (Permit No. 58-03)
The Operating Landfill also contains a leachate underground holding tank that was installed in
August 2011. Previously, the leachate was stored in a lined leachate basin that is no longer in use.
State regulations applicable to landfills are enforced by the North Carolina Department of
Environmental Quality (DEQ), Division of Waste Management (DWM). This solid waste facility is
permitted by the DEQ DWM under Permit No. 58-03. The permit requires semiannual monitoring of
groundwater, surface water, and leachate quality.
This report documents the second semiannual groundwater, surface water, and leachate monitoring
event for 2016 and is being submitted in accordance with requirements stipulated in the DEQ Solid
Waste Management Rules, Title 15A, North Carolina Administrative Code (NCAC), Subchapter 13B
(15A NCAC 13B).
This semiannual report provides an evaluation of groundwater, surface water, and leachate quality
for the solid waste facility.
The water quality monitoring network for the Operating Landfill consists of nine compliance
monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05, MW-06R, MW-07R, MW-08, and MW-
09); two surface water sample locations (SW-01 and SW-02R) located along a tributary to Walnut
Creek; and a leachate sample (LT-01) collected from the fill port on the underground holding tank.
Monitoring well construction details are summarized in Table 1.

Fall 2016 Semiannual Water Quality Monitoring Report 3 February 2017
2 Methods
On October 18 and 19, 2016, Altamont Environmental, Inc. (Altamont, who became Anchor QEA of
North Carolina, PLLC [Anchor QEA] on December 29, 2016) collected nine groundwater samples from
monitoring wells, two surface water samples from a tributary to Walnut Creek, and one aqueous
sample from the leachate underground holding tank located at the Operating Landfill. One of the
monitoring wells sampled, MW-06R, is upgradient from the landfill. Groundwater collected from this
well is assumed to represent background groundwater quality at the site. This monitoring well was
installed on September 30, 2008 as a replacement for the pre-existing background monitoring well,
MW-06, which had historically been dry. Sampling locations are shown on Figures 2 and 3.
2.1 Groundwater Purging and Sampling Methods
Prior to collecting groundwater samples from the monitoring wells, the static water level was
measured and recorded for each well. The monitoring wells were purged and sampled using low-
flow techniques in accordance with the procedures described in Low-Flow (Minimal Drawdown)
Ground-Water Sampling Procedures, United States Environmental Protection Agency (EPA),
Groundwater Issues (Puls and Barcelona, 1996). During purging, pH, specific conductivity (SC),
dissolved oxygen (DO), oxidation-reduction potential (ORP), turbidity, and temperature were
measured and recorded approximately every 3 minutes. Well purging continued until these
parameters stabilized for three consecutive readings. The required stabilization criteria are as follows:
 pH values within +/- 0.1 pH unit
 SC values within +/- 3 percent
 Temperature, DO, and turbidity values within +/- 10 percent
 ORP values within +/- 10 millivolts
Following stabilization of these parameters, a groundwater sample was collected by a technician
wearing a new pair of non-reactive nitrile gloves. Each sample was placed directly into laboratory-
supplied sample containers. Low-flow sampling logs are included in Appendix A.
2.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02R were collected at designated locations from an unnamed
tributary to Walnut Creek that flows in a northerly direction adjacent to the western border of the
Operating Landfill (Figure 2). Sample SW-01 is considered representative of surface water quality
upstream of the Operating Landfill, while sample SW-02R is considered representative of surface
water quality downstream from the facility. Surface water sample SW-01 was collected further
downstream than during prior sampling events, due to a lack of surface water flow in the usual
sample collection location. Refer to Figure 2 for the adjusted sample location. Surface water samples
were collected in laboratory-supplied sample containers by a technician wearing a new pair of non-

Fall 2016 Semiannual Water Quality Monitoring Report 4 February 2017
reactive nitrile gloves. As with groundwater sampling, temperature, pH, SC, DO, ORP, and turbidity
were measured and recorded at each surface water sampling location prior to sample collection.
Field parameters and observations pertaining to surface water quality are provided on sampling logs
included in Appendix A.
2.3 Leachate Sampling Methods
One aqueous sample was collected from the leachate underground holding tank, designated as
LT-01. Historically leachate was collected from a lined storage basin. On August 12, 2011, a leachate
underground holding tank was installed and connected to the leachate collection piping associated
with the closed MSW landfill cell. Shortly thereafter, the lined leachate basin was closed. Sample
LT-01 was collected on October 18, 2016 from one of the tank’s fill ports using a new disposable
polyethylene bailer. One round of field parameters (as described above) was measured and recorded
for sample LT-01 (see Appendix A). Leachate collected in the holding tank at the site is trucked, as
needed, to the Metropolitan Sewerage District (MSD) treatment facility for the town of Marshall,
North Carolina.
2.4 Sample Handling, Documentation, and Analysis
Field parameters for groundwater and surface water were measured, and the results are provided on
the sampling logs provided in Appendix A. Following sample collection, each sample was
immediately placed on ice in a sample cooler for transport to TestAmerica Laboratories, Inc.
(TestAmerica), a North Carolina-certified laboratory located in Nashville, Tennessee. Altamont
submitted the groundwater, surface water, and leachate samples for the required analyses
summarized in Table 2.
Proper chain-of-custody documentation procedures were followed during collection and transport of
each sample. Three trip blanks provided by the laboratory, each stored in a separate sample cooler,
were analyzed for Appendix I volatile organic compounds (VOCs). The reports of laboratory analysis
and chain-of-custody documentation are provided in Appendix B.

Fall 2016 Semiannual Water Quality Monitoring Report 5 February 2017
3 Findings
3.1 Analytical Results
The field parameter data and laboratory analytical results for groundwater, surface water, the
leachate sample collected at the Operating Landfill, and the trip blanks are included in Appendices A
and B and also submitted separately to the DEQ Solid Waste Section (SWS) of the DWM in the
Electronic Data Deliverable (EDD) format (a format most recently updated on May 5, 2010).
As stipulated in the May 2010 DWM documents, non-detections were reported at the laboratory-
specific method detection limit (MDL), and all concentrations exceeding the MDL were reported and
appropriately qualified (see Tables 3 and 4). The MDL is the minimum concentration of a substance
that can be measured and reported by a laboratory with 99 percent confidence that the analyte
concentration is greater than zero. The laboratory’s method reporting limit (MRL) is the minimum
concentration of a target analyte that can be accurately determined by the referenced method. MRL
is listed as the “Report Limit” (RL) column in the TestAmerica report of laboratory analysis (see
Appendix B). All detections were compared to analyte-specific Solid Waste Section Limits (SWSLs)
established by the SWS. The SWSL is the lowest concentration, determined by the SWS, of an analyte
in a sample that can be quantitatively determined with suitable precision and accuracy. If the
reported concentration is greater than the laboratory MRL and less than the SWSL, the analytical
result is qualified as estimated and is flagged with a “J” qualifier (italicized J-flag) by Altamont per the
DEQ requirement. A “J” qualifier (non-italicized) is assigned by the laboratory and is used for
parameters detected at estimated concentrations greater than the MDL but less than the MRL.
Detected concentrations of constituents below the applicable SWSLs are not discussed in the text of
this report unless they exceed their applicable North Carolina water quality standard.
Detected concentrations of analytes in groundwater samples were compared to the values specified
in the 15A NCAC 2L.0202 groundwater quality standard (2L standard). Detected concentrations of
analytes in groundwater with no established 2L standard were compared to an updated list of the
interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]). Detections of analytes in surface water samples were
compared to the 15A NCAC 2B.0200 surface water quality standard (2B standard) established for
class C waters.
Table 3 presents the summary of detected compounds and outlines concentrations of analytes that
were above the applicable SWSLs, as well as concentrations of analytes that exceed their respective
2L standard, IMAC, or 2B standard.

Fall 2016 Semiannual Water Quality Monitoring Report 6 February 2017
3.1.1 Groundwater Monitoring Wells
The following sections summarize the results of laboratory and field parameter analyses of
groundwater samples.
3.1.1.1 Appendix I Metals
Nine metals were detected above their respective MDLs in one or more of the monitoring wells (see
Table 3). Five metals (barium, cadmium, chromium, cobalt, and zinc) were detected above their
SWSLs in one or more of the samples collected from the monitoring wells (see Table 3). Cadmium
was detected above its 2L standard in the samples collected from monitoring wells MW-03 and
MW-07R. Chromium was detected above the applicable 2L standard in the sample collected from
monitoring well MW-07R. Cobalt was detected above the applicable IMAC in the samples collected
from monitoring wells MW-02, MW-03, MW-05, MW-07R, and MW-08 (see Table 3). Vanadium was
detected above the applicable IMAC standard in the samples collected from all site monitoring wells
(see Table 3). All vanadium concentration were below the SWSL. Vanadium concentrations are
believed to be naturally occurring.
3.1.1.2 Appendix I VOCs
One VOC, xylene, was detected in the sample collected from monitoring well MW-05. The
concentration of this VOC was below the MRL and well below the 2L standard established for xylene.
Acetone was detected in the trip blank associated with the monitoring wells, at a concentration
below the MRL. Detection of this VOC is likely attributable to laboratory contamination.
3.1.1.3 Field Parameters
Field parameters were recorded during sampling activities on October 18 and 19, 2016. Measured pH
values for all samples collected from monitoring wells were slightly below the 2L standard pH range
of 6.5 to 8.5 Standard Units (SU) (see Table 3). Turbidity values for samples collected from the
monitoring wells ranged from 4.89 Nephelometric Turbidity Units (NTUs) to 179 NTUs.
3.1.2 Surface Water
The following sections summarize the results of laboratory and field parameter analyses of surface
water samples SW-01 and SW-02R.
3.1.2.1 Appendix I Metals
Three metals (barium, cobalt, and vanadium) were detected in both surface water samples below
their respective SWSLs. No metals were detected above applicable 2B standards (see Table 3).

Fall 2016 Semiannual Water Quality Monitoring Report 7 February 2017
3.1.2.2 Appendix I VOCs
No VOCs were detected in either of the surface water samples collected from the Operating Landfill.
Acetone was detected in the trip blank associated with the surface water samples at a concentration
below the method report limit. The detection of this VOC is likely due to laboratory contamination.
3.1.2.3 Field Parameters
The pH values recorded for surface water samples SW-01 and SW-02R were recorded as 6.87 SU and
6.52 SU, respectively. Both values were within the 2B standard pH range of 6.0 to 9.0 SU (see Table 3).
The measured turbidity value for the upstream surface water sample (SW-01) was recorded at 97.1
NTUs, which is outside of the 2B standard for turbidity established at 25 NTUs (Table 3). Due to dry
conditions, this surface water sample had to be collected from stagnant, turbid water. DO was
recorded at 6.98 milligrams per liter (mg/L) and 8.74 mg/L for surface water samples SW-01 and SW-
02R, respectively. These concentrations are within the 2B standard established at “equal or greater
than” 6.0 mg/L.
3.1.3 Leachate
Analytical results for the leachate sample (LT-01) collected from the leachate underground holding
tank are summarized in Table 4 and discussed below.
3.1.3.1 Appendix I Metals
Nine metals were detected in the aqueous sample collected from the leachate storage tank. Of these
metals, seven of them were detected above their respective SWSLs (see Table 4).
3.1.3.2 Appendix I VOCs
No VOCs were detected in the leachate sample or in the trip blank associated with the leachate
sample.
3.1.3.3 Inorganics
LT-01 was also analyzed for biological oxygen demand (BOD), chemical oxygen demand (COD),
nitrate, phosphorus, and sulfate. The analytical results for detected parameters are summarized in
Table 4. Nitrate was detected at a concentration in excess of the SWSL (see Table 4). All other
parameters, with the exception of sulfate, do not have established SWSLs. Sulfate was detected well
below its SWSL.
3.1.3.4 Field Parameters
Field parameters were measured and recorded for the leachate sample on October 18, 2016.
Dissolved oxygen, pH, and turbidity results are summarized in Table 4. No standards exist for
leachate; therefore, the recorded results are not evaluated.

Fall 2016 Semiannual Water Quality Monitoring Report 8 February 2017
4 Hydrogeology
The predominant groundwater flow direction within the regolith overlying the bedrock at the
Operating Landfill appears to be west-northwest, toward an unnamed tributary of Walnut Creek.
Figure 3 depicts the generalized groundwater flow direction based on groundwater measurements
taken by Altamont on October 18 and 19, 2016. Water level data are summarized on Table 1.

Fall 2016 Semiannual Water Quality Monitoring Report 9 February 2017
5 Summary
Altamont completed the second semiannual water quality monitoring event of 2016 at the Operating
Landfill on October 18 and 19, 2016.
Tables 3 and 4 of this report, sampling logs (see Appendix A), and the TestAmerica Reports of
Laboratory Analysis (see Appendix B) provide detailed analytical results and field data used to
interpret groundwater and surface water quality at the Operating Landfill.
5.1 Future Activities
Anchor QEA has discussed the exceedances of applicable water quality standards with Madison
County. Anchor QEA will continue to measure field parameters and collect water quality samples
from groundwater, surface water, and leachate monitoring points associated with the Operating
Landfill. Water quality samples will be submitted to a North Carolina-certified laboratory for analysis
for Appendix I metals and VOCs on a semiannual basis. The next sampling event is scheduled for
April 2017.

Fall 2016 Semiannual Water Quality Monitoring Report 10 February 2017
6 References
DENR DWM SWS, 2006. New Guidelines for Electronic Submittal of Environmental Monitoring Data.
October 27, 2006
DENR DWM SWS, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding New
Guidelines for Electronic Submittal of Environmental Data. February 23, 2007
Puls, R.W., and M. J. Barcelona, 1996. Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures, U.S. Environmental Protection Agency, OSWER, EPA/540/S-95/504.

Tables

Table 1
Well Construction Details and Corresponding Elevations
58-03 MW-01 1,859.04 1,857.04 6.46 1,852.58 7 1,850.0 2 to 17 1,855.04
58-03 MW-02 1,898.94 1,895.94 5.20 1,893.74 6 1,889.9 1 to 16 1,892.94
58-03 MW-03 1,932.96 1,929.46 25.16 1,907.80 NA NA 15.5 to 25.5 1,913.96
58-03 MW-04 1,935.64 1,932.04 29.33 1,906.31 35.2 1,896.8 70.7 to 80.7 1,861.34
58-03 MW-05 1,972.76 1,969.26 47.03 1,925.73 NA NA 46.5 to 61.5 1,922.76
58-03 MW-06 2,082.87 2,081.87 NA NA 28 2,053.9 80 to 100 2,001.87
58-03 MW-06R 1,942.19 1,942.19 10.72 1,931.47 NA NA 10 to 25 1,932.19
58-03 MW-07R 1,919.34 1,916.64 30.33 1,889.01 NA NA 26 to 41 1,890.64
58-03 MW-08 1,899.92 1,896.92 20.18 1,879.74 NA NA 16 to 26 1,880.92
58-03 MW-09 1,949.43 1,946.43 7.80 1,941.63 NA NA 12.4 to 22.4 1,934.03
Notes:
Elevations are in feet, based on the NAVD 88 datum.
Top of casing
Not Applicable
Calculated based on TOC elevations and field measurements.
Depth-to-water measurements were obtained in the field on October 18 and 19, 2016.
Installed during closure of MSW cell.
Elevations
TOC
NA
Ground Elevations
Facility
Permit Well ID
Depth to
Bedrock
Top of Bedrock
Elevation
Ground
Elevation
Depth to
Water from
TOC
Depths are measured in feet below ground surface. Data was taken from boring logs completed on September 26, 27, 28, and 29, 1992 by
Metro Drill, Inc. and April 12, 1995 by Engineering Tectonics.
Screened
Interval
Top of Screen
Elevation
TOC
Elevation
Groundwater
Elevation
Included on the Closure Plan drawing generated by McGill Associates on January 4, 2007. Adjusted "Depth to Bedrock" and "Screened Interval" elevations
were calculated using original data from September 1992 boring logs and new data from the December 14, 2006 survey.
Depth to Water
Depth to Bedrock &
Screened Interval
TOC Elevations
MW-03 and MW-04
MW-06
Ground survey data
For MW-01, MW-02, MW-05, and MW-06, TOC elevations are based on the report, Transition Plan Application (Law Engineering, April 1994). For MW-03
and MW-04, elevations are from the survey performed on December 14, 2006 by McGill Associates staff (J. Dallas Gordon, PLS). For MW-07R and MW-08,
elevations were taken from survey data included on boring logs completed by Bunnell-Lammons Engineering, Inc. on July 28, 29, and 30, 2003. For MW-09,
elevation was taken from survey data included on boring log completed by Bunnell-Lammons Engineering, Inc. on October 13, 2006.
Monitoring of background well MW-06 was terminated in Fall 2008 because the well was dry. MW-06R was installed on September 27, 2008 to replace
MW-06. Survey data for MW-06R are based on a survey conducted on April 16, 2009 by Wes Cole Land Surveying, PA. MW-06 was gauged and recorded if
water was present, but not sampled.
Fall 2016 Semiannual Water Quality Monitoring Report
Madison County Operating Solid Waste Facility
Page 1 of 1
Februray 2017
Table 2
Summary of Laboratory Analyses Performed on Samples
Groundwater Samples Surface Water Samples
Metals VOCs Metals VOCs
EPA 6010D
EPA 6020B
EPA 7470A EPA 8260B
EPA 6010D
EPA 6020B
EPA 7470A EPA 8260B
MW-01 10/18/2016 X X SW-01 10/19/2016 X X
MW-02 10/19/2016 X X SW-02R 10/18/2016 X X
MW-03 10/19/2016 X X
MW-04 10/19/2016 X X Quality Control Sample
MW-05 10/19/2016 X X VOCs
MW-06R 10/18/2016 X X EPA 8260B
MW-07R 10/18/2016 X X TRIP BLANK (LT-01)10/18/2016 X
MW-08 10/18/2016 X X TRIP BLANK (MW)10/19/2016 X
MW-09 10/19/2016 X X TRIP BLANK (SW)10/19/2016 X
Leachate Sample
Metals VOCs
Biochemical
Oxygen Demand
(BOD)
Chemical Oxygen
Demand
(COD) Nitrate as N
Total
Phosphorus Sulfate
EPA 6010D
EPA 6020B
EPA 7470A EPA 8260B SM 5210B SM 5220D
Nitrate by
calc EPA 365.4 EPA 300.0
LT-01 10/18/2016 X X X X X X X
Analyses
VOCs Volatile organic compounds
LT-01 Leachate sample, collected from the leachate underground holding tank.
Metals and VOCs analyses include Appendix I metals per 40 CFR Part 258 "Appendix I Constituents for Detection Monitoring". Metals
analyses also includes mercury.
Notes:
Sample
Name Collect Date Sample Name Collect Date
Sample Name Collect Date
Sample
Name Collect Date
Fall 2016 Semiannual Water Quality Monitoring Report
Madison County Operating Solid Waste Facility
Page 1 of 1
February 2017
Table 3
Groundwater and Surface Water Summary of Analytical Results
Metals VOCs Field Parameters
Lab Certification 387 387 5445 (pH only)
Lab Method EPA 6010D, 6020B EPA 8260B
Parameter Arsenic Barium Beryllium Cadmium Chromium Cobalt Lead Nickel Vanadium Zinc Acetone
Xylene
(total)
Dissolved
Oxygen pH Turbidity
CAS Number 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7439-92-1 7440-02-0 7440-62-2 7440-66-6 67-64-1 1330-20-7 7782-44-7 SW320 SW330
SWS ID 14 15 23 34 51 53 131 152 209 213 3 346 356 320 330
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L SU NTU
Sample Name Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Monitoring Well Samples
MW-01 10/18/2016 8.60 U 106 0.100 U 0.500 U 4.30 J 0.662 J 2.00 U 3.00 U 1.73 J, B 5.20 U 2.66 U 0.580 U 2.80 5.92 6.00
MW-02 10/19/2016 8.60 U 97.8 J 0.100 U 0.500 U 3.40 J 7.64 J 4.30 J 3.00 U 9.01 J, B 5.20 U 2.66 U 0.580 U 3.62 6.14 54.8
MW-03 10/19/2016 8.60 U 218 0.100 U 5.90 3.60 J 85.7 2.00 U 3.00 U 1.41 J, B 5.20 U 2.66 U 0.580 U 0.52 6.26 99.8
MW-04 10/19/2016 8.60 U 146 0.100 U 0.500 U 3.00 U 0.100 U 2.10 J 3.00 U 5.98 J, B 5.20 U 2.66 U 0.580 U 3.01 6.33 6.01
MW-05 10/19/2016 8.60 U 135 0.100 U 0.800 J 3.20 J 1.27 J 2.10 J 6.50 J 7.51 J, B 79.5 2.66 U 1.06 J 1.61 5.81 22.2
MW-06R 10/18/2016 8.60 U 28.4 J 0.100 U 0.500 U 3.00 U 0.159 J 2.00 U 3.00 U 2.59 J, B 5.20 U 2.66 U 0.580 U 5.42 6.35 6.77
MW-07R 10/18/2016 9.00 J 242 0.506 J 6.50 14.2 4.06 J 5.80 J 6.90 J 20.3 J, B 44.1 2.66 U 0.580 U 6.40 5.94 179
MW-08 10/18/2016 8.60 U 33.5 J 0.100 U 0.500 U 3.00 U 1.14 J 2.70 J 3.00 U 6.54 J, B 5.20 U 2.66 U 0.580 U 6.17 6.23 9.31
MW-09 10/19/2016 8.60 U 146 0.100 U 0.500 U 3.00 U 0.235 J 2.20 J 3.00 U 2.65 J , B 5.20 U 2.66 U 0.580 U 1.62 6.32 4.89
Surface Water Samples
SW-01 10/19/2016 8.60 U 48.0 J 0.100 U 0.500 U 3.00 U 2.22 J 2.00 U 3.00 U 3.54 J, B 5.20 U 2.66 U 0.580 U 6.98 6.87 97.1
SW-02R 10/18/2016 8.60 U 53.9 J 0.100 U 0.500 U 3.00 U 0.357 J 2.00 U 3.00 U 3.02 J, B 5.20 U 2.66 U 0.580 U 8.74 6.52 11.0
Quality Control Samples
TRIPBLANK (MW)10/19/2016 NA NA NA NA NA NA NA NA NA NA 11.0 J 0.580 U NA NA NA
TRIPBLANK (SW)10/18/2016 NA NA NA NA NA NA NA NA NA NA 4.03 J 0.580 U NA NA NA
MDL 8.60 5.00 0.100 0.500 3.00 0.100 2.00 3.00 0.700 5.20 2.66 0.580 NA NA NA
MRL 10.0 10.0 2.0 1.0 5.0 2.0 5.0 10.0 2.0 25.0 25.0 3.0 NA NA NA
SWSL 10 100 1 1 10 10 10 50 25 10 100 5 NE NE NE
2L 10 700 NE 2 10 NE 15 100 NE 1,000 6,000 500 NE 6.5-8.5 NE
IMAC NE NE 4 NE NE 1 NE NE 0.3 NE NE NE NE NE NE
GWPS NE NE 4 NE NE 1 NE NE 0.3 NE NE NE NE NE NE
2B 150 200,000 6.5 0.15 35 4 0.54 16 NE 36 2,000 670 > 5.0 6.0-9.0 25
Notes:
Detections Only detected constituents are listed on this table. Please refer to TestAmerica Laboratories, Inc. Report of Laboratory Analysis for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID The Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, milligrams per liter (mg/L) for dissolved oxygen, Standard Units (SU) for pH, and nephelometric turbidity units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in both the laboratory blank and the sample.
2L Groundwater standards from North Carolina Administrative Code (NCAC), Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards, DEQ (Amended April 1, 2013).
IMAC Interim Maximum Allowable Concentration. An IMAC is applied to a constituent if there is not a 2L standard established. Standards are from NCAC 15A 02L .0202.
GWPS
2B
NE Not Established
NA Not Applicable
106 Indicates a result in exceedance of the SWSL.
5.92 Indicates a result in exceedance of the 2L, IMAC, or 2B (surface water) standards, or greater than or equal to the GWPS (if no 2L or IMAC exist).
The Groundwater Protection Standard pursuant to 15A NCAC 13B .1634, DEQ. Current standards were obtained from http://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-
section/environmental-monitoring/environmental-monitoring-list.
"2B" indicates surface water standard per North Carolina Administrative Code, Title 15A: Department of Environment and Natural Resources, Subchapter 2B - Surface Water and Wetland Standards, (last amended on May 1, 2007).
For compounds with no 2B standard established, the Environmental Protection Agency (EPA) National Criteria Table (current as of May 15, 2013) was used for the most stringent of fresh water and human health.
Fall 2016 Semiannual Water Quality Monitoring Report
Madison County Operating Solid Waste Facility
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February 2017
Table 4
Leachate Summary of Analytical Results
Metals
Lab Certification 387
Lab Method EPA 6010D & 6020B
Parameter Barium Beryllium Chromium Cobalt Copper Nickel Selenium Vanadium Zinc
CAS Number 7440-39-3 7440-41-7 7440-47-3 7440-48-4 7440-50-8 7440-02-0 7782-49-2 7440-62-2 7440-66-6
SWS ID 15 23 51 53 54 152 183 209 213
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Sample Name Collect Date Result Result Result Result Result Result Result Result Result
LT-01 10/18/2016 793 1.13 J 24.9 83.2 10.6 62.4 9.00 J 100 B 402
TRIPBLANK (LT-01)10/18/2016 NA NA NA NA NA NA NA NA NA
MDL 5.00 0.500 3.00 0.500 5.00 3.00 5.00 3.50 26.0
MRL 10.0 10.0 5.0 10.0 10.0 10.0 10.0 10.0 125
SWSL 100 1 10 10 10 50 10 25 10
General Chemistry Field Parameters
Lab Certification 387 5445 (pH only)
Lab Method SM5210B SM 5220D Nitrate by calc EPA 365.4 EPA 300.0
Parameter BOD COD Nitrate as N
Total
Phosphorus Sulfate
Dissolved
Oxygen pH Turbidity
CAS Number SW316 SW317 14797-55-8 7723-14-0 14808-79-8 7782-44-7 SW320 SW330
SWS ID 316 317 303 412 315 356 320 330
Units µg/L µg/L µg/L µg/L µg/L mg/L SU NTU
Sample Name Collect Date Result Result Result Result Result Result Result Result
LT-01 10/18/2016 4,510 117,000 42,000 664 133,000 J 7.53 7.10 35.8
TRIPBLANK (LT-01)10/18/2016 NA NA NA NA NA NA NA NA
MDL 2,000 4,000 40.0 50.0 6,000 NA NA NA
MRL 2,000 20,000 100 100 10,000 NA NA NA
SWSL NE NE 10,000 NE 250,000 NE NE NE
Notes:
Detections Only detected constituents are listed on this table. Please refer to the TestAmerica Report of Laboratory Analysis for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID The Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, milligrams per liter (mg/L) for dissolved oxygen, Standard Units (SU) for pH, and Nephelometric Turbidity Units (NTU) for turbidity.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Altamont.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL and SWSL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B A laboratory data qualifier used for parameters that were detected in both the laboratory blank and the sample.
VOCs Volatile organic compounds
BOD Biological oxygen demand
COD Chemical oxygen demand
NE Not Established
793 Indicates a result in exceedance of the SWSL.
Fall 2016 Semiannual Water Quality Monitoring Report
Madison County Operating Solid Waste Facility
Page 1 of 1
February 2017

Figures
[0 2,0001,000
Feet
LEGEND:
LANDFILL PARCEL BOUNDARY
Publish Date: 2017/01/18, 3:08 PM | User: alesueurFilepath: P:\Projects\Madison County\Figures\GIS\GIS User\MXDs\2016\AQ Template\5803Apr Figure 1-Site Location Map Operating AQ.mxd
Figure 1Site Location MapMadison County Operating Landfill Water Quality ReportMadison County Operating Solid Waste Facility, Permit #58-03, Marshall, NC
SOURCE(S):Basemap: USGS 1:24,000 Scale Topo Maps, MarshallQuadrangle, 1990.Parcels: Madison County GIS
Anchor QEA of North Carolina, PLLC
#
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MW-05
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CRAIG
R
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[
0 500250
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LEGEND:
@A MONITORING WELL LOCATION
#
I
SURFACE WATER SAMPLE LOCATION
UNNAMED TRIBUTARY
ELEVATION CONTOURS (10 FEET)
ROADS
CELL BOUNDARY LOCATIONS
!(LEACHATE HOLDING TANK
Publish Date: 2017/02/08, 9:14 AM | User: alesueurFilepath: \\Asheville1\Asheville\Projects\Madison County\Figures\GIS\GIS User\MXDs\2016\AQ Template\5803Oct Figure 2-Sample Location Map Operating AQ.mxd
Figure 2Sample Location MapMadison County Operating Landfill Water Quality ReportMadison County Operating Solid Waste Facility, Permit #58-03, Marshall, NC
SOURCE(S):Basemap: NC OneMap 2010Roads and Streams: MadisonCounty GIS 2006
#
I
#
I
!(
@A
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Former Leachate
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
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Closed
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Groundwater
Flow
Direction
SW-01
SW-02R
202
5201
5
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51995198519751965
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R
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D
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MW-07R(1,889.01)
MW-02(1,893.74)
MW-08(1,879.74)
MW-03(1,907.80)
MW-04(1,906.31)
MW-09(1,941.63)
MW-06R(1,931.47)
MW-01(1,852.58)
[
0 500 1,000250
Feet
NOTE(S):1. (1,907.80) = Groundwater Elevation2. Groundwater (GW) flow directionbased on GW elevations in water tablewells MW-02, MW-03, MW-05, MW-06R, MW-07R, and MW-08.3. GW elevations based on depth towater measurements collected onOctober 18 and 19, 2016.
LEGEND:
@A MONITORING WELL LOCATION
#
I
SURFACE WATER SAMPLE LOCATION
UNNAMED TRIBUTARY
ELEVATION CONTOURS (10 FEET)
ROADS
CELL BOUNDARY LOCATIONS
!(LEACHATE HOLDING TANK
Publish Date: 2017/01/18, 3:30 PM | User: alesueurFilepath: P:\Projects\Madison County\Figures\GIS\GIS User\MXDs\2016\AQ Template\5803Oct Figure 3-Groundwater Flow AQ.mxd
Figure 3Generalized Groundwater FlowMadison County Operating Landfill Water Quality ReportMadison County Operating Solid Waste Facility, Permit #58-03, Marshall, NC
SOURCE(S):Basemap: NC OneMap 2010Roads and Streams: MadisonCounty GIS 2006
Anchor QEA of North Carolina, PLLC

Appendix A
Sampling Logs and Equipment
Documentation and Instrument
Calibration Data Sheets

Appendix B
Report of Laboratory Analysis and
Chain-of-Custody Documentation
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-114461-1
Client Project/Site: Madison Co Operating Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
11/4/2016 2:42:02 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
TestAmerica Job ID: 490-114461-1
Page 2 of 47 TestAmerica Nashville11/4/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
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Sample Summary
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-114461-1 MW-01 Water 10/18/16 11:15 10/20/16 09:20
490-114461-2 MW-02 Water 10/19/16 12:56 10/20/16 09:20
490-114461-3 MW-03 Water 10/19/16 11:19 10/20/16 09:20
490-114461-4 MW-04 Water 10/19/16 11:51 10/20/16 09:20
490-114461-5 MW-05 Water 10/19/16 10:18 10/20/16 09:20
490-114461-6 MW-06R Water 10/18/16 14:42 10/20/16 09:20
490-114461-7 MW-07R Water 10/18/16 13:15 10/20/16 09:20
490-114461-8 MW-08 Water 10/18/16 12:29 10/20/16 09:20
490-114461-9 MW-09 Water 10/19/16 13:36 10/20/16 09:20
490-114461-10 Trip Blank Water 10/19/16 01:01 10/20/16 09:20
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114461-1
Project/Site: Madison Co Operating Landfill
Job ID: 490-114461-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-114461-1
Comments
No additional comments.
Receipt
The samples were received on 10/20/2016 9:20 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 1.3º C.
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
Method 6020B: The method blank for preparation batch 490-381203 and analytical batch 490-383075 contained Vanadium above the
method detection limit (MDL). Associated samples were not re-analyzed because results were less than the reporting limit (RL) OR
practical quantitation limit (PQL).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-1Client Sample ID: MW-01
Matrix: WaterDate Collected: 10/18/16 11:15
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 17:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 17:51 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 17:51 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 17:51 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 17:51 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 17:51 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 17:51 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 17:51 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 17:51 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 17:51 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 17:51 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 17:51 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 17:51 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 17:51 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 17:51 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 17:51 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 17:51 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 17:51 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 17:51 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 17:51 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 17:51 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 17:51 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 17:51 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 17:51 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 17:51 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 17:51 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 17:51 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 17:51 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 17:51 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 17:51 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 17:51 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 17:51 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 17:51 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 17:51 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 17:51 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 17:51 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 17:51 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 17:51 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 17:51 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 17:51 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 17:51 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 17:51 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 17:51 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 17:51 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 17:51 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 17:51 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 17:51 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 17:51 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-1Client Sample ID: MW-01
Matrix: WaterDate Collected: 10/18/16 11:15
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)107 70-130 10/29/16 17:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 10/29/16 17:51 170-130
1,2-Dichloroethane-d4 (Surr)98 10/29/16 17:51 170-130
Toluene-d8 (Surr)98 10/29/16 17:51 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 20:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:10 1Barium0.106
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 20:10 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:06 1Chromium0.00430 J
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:10 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 20:10 1Lead<0.00200
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 20:10 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:10 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:06 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:43 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:43 1Cobalt0.662 J
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:43 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 04:43 1Vanadium1.73 J B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 04:43 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-2Client Sample ID: MW-02
Matrix: WaterDate Collected: 10/19/16 12:56
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 18:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 18:18 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 18:18 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 18:18 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 18:18 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 18:18 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 18:18 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 18:18 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 18:18 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 18:18 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 18:18 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 18:18 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 18:18 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 18:18 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 18:18 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 18:18 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 18:18 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 18:18 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 18:18 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 18:18 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 18:18 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 18:18 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 18:18 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 18:18 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 18:18 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 18:18 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 18:18 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 18:18 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 18:18 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 18:18 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 18:18 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 18:18 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 18:18 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 18:18 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 18:18 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 18:18 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 18:18 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 18:18 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 18:18 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 18:18 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 18:18 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 18:18 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 18:18 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 18:18 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 18:18 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 18:18 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 18:18 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 18:18 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-2Client Sample ID: MW-02
Matrix: WaterDate Collected: 10/19/16 12:56
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)111 70-130 10/29/16 18:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 10/29/16 18:18 170-130
1,2-Dichloroethane-d4 (Surr)97 10/29/16 18:18 170-130
Toluene-d8 (Surr)99 10/29/16 18:18 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 20:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:52 1Barium0.0978
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 20:52 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:37 1Chromium0.00340 J
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:52 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 20:52 1Lead0.00430 J
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 20:52 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:52 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:37 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:49 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:49 1Cobalt7.64
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:49 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 04:49 1Vanadium9.01 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 04:49 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-3Client Sample ID: MW-03
Matrix: WaterDate Collected: 10/19/16 11:19
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 18:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 18:45 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 18:45 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 18:45 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 18:45 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 18:45 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 18:45 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 18:45 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 18:45 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 18:45 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 18:45 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 18:45 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 18:45 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 18:45 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 18:45 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 18:45 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 18:45 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 18:45 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 18:45 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 18:45 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 18:45 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 18:45 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 18:45 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 18:45 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 18:45 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 18:45 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 18:45 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 18:45 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 18:45 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 18:45 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 18:45 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 18:45 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 18:45 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 18:45 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 18:45 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 18:45 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 18:45 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 18:45 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 18:45 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 18:45 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 18:45 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 18:45 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 18:45 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 18:45 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 18:45 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 18:45 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 18:45 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 18:45 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-3Client Sample ID: MW-03
Matrix: WaterDate Collected: 10/19/16 11:19
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)105 70-130 10/29/16 18:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)99 10/29/16 18:45 170-130
1,2-Dichloroethane-d4 (Surr)101 10/29/16 18:45 170-130
Toluene-d8 (Surr)99 10/29/16 18:45 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 20:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:57 1Barium0.218
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 20:57 1Cadmium0.00590
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:52 1Chromium0.00360 J
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:57 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 20:57 1Lead<0.00200
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 20:57 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:57 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:52 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:54 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:54 1Cobalt85.7
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:54 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 04:54 1Vanadium1.41 J B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 04:54 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-4Client Sample ID: MW-04
Matrix: WaterDate Collected: 10/19/16 11:51
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 19:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 19:12 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 19:12 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 19:12 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 19:12 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 19:12 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 19:12 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 19:12 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 19:12 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 19:12 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 19:12 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 19:12 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 19:12 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 19:12 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 19:12 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 19:12 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 19:12 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 19:12 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 19:12 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 19:12 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 19:12 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 19:12 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 19:12 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 19:12 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 19:12 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 19:12 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 19:12 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 19:12 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 19:12 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 19:12 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 19:12 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 19:12 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 19:12 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 19:12 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 19:12 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 19:12 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 19:12 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 19:12 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 19:12 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 19:12 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 19:12 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 19:12 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 19:12 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 19:12 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 19:12 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 19:12 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 19:12 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 19:12 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-4Client Sample ID: MW-04
Matrix: WaterDate Collected: 10/19/16 11:51
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)108 70-130 10/29/16 19:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 10/29/16 19:12 170-130
1,2-Dichloroethane-d4 (Surr)100 10/29/16 19:12 170-130
Toluene-d8 (Surr)100 10/29/16 19:12 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 20:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:36 1Barium0.146
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 20:36 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:32 1Chromium<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:36 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 20:36 1Lead0.00210 J
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 20:36 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 20:36 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:32 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:16 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 04:16 1Cobalt<0.100
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:16 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 04:16 1Vanadium5.98 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 04:16 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-5Client Sample ID: MW-05
Matrix: WaterDate Collected: 10/19/16 10:18
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 19:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 19:39 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 19:39 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 19:39 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 19:39 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 19:39 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 19:39 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 19:39 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 19:39 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 19:39 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 19:39 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 19:39 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 19:39 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 19:39 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 19:39 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 19:39 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 19:39 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 19:39 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 19:39 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 19:39 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 19:39 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 19:39 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 19:39 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 19:39 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 19:39 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 19:39 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 19:39 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 19:39 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 19:39 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 19:39 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 19:39 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 19:39 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 19:39 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 19:39 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 19:39 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 19:39 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 19:39 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 19:39 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 19:39 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 19:39 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 19:39 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 19:39 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 19:39 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 19:39 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 19:39 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 19:39 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 19:39 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 19:39 1Xylenes, Total 1.06 J
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-5Client Sample ID: MW-05
Matrix: WaterDate Collected: 10/19/16 10:18
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)105 70-130 10/29/16 19:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)95 10/29/16 19:39 170-130
1,2-Dichloroethane-d4 (Surr)102 10/29/16 19:39 170-130
Toluene-d8 (Surr)102 10/29/16 19:39 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 21:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:02 1Barium0.135
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 21:02 1Cadmium0.000800 J
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:57 1Chromium0.00320 J
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:02 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 21:02 1Lead0.00210 J
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 21:02 1Nickel0.00650 J
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:02 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 20:57 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:10 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:10 1Cobalt1.27 J
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:10 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 05:10 1Vanadium7.51 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 05:10 1Zinc79.5
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-6Client Sample ID: MW-06R
Matrix: WaterDate Collected: 10/18/16 14:42
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 20:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 20:06 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 20:06 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 20:06 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 20:06 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 20:06 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 20:06 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 20:06 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 20:06 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 20:06 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 20:06 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 20:06 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 20:06 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 20:06 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 20:06 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 20:06 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 20:06 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 20:06 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 20:06 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 20:06 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 20:06 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 20:06 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 20:06 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 20:06 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 20:06 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 20:06 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 20:06 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 20:06 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 20:06 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 20:06 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 20:06 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 20:06 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 20:06 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 20:06 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 20:06 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 20:06 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 20:06 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 20:06 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 20:06 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 20:06 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 20:06 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 20:06 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 20:06 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 20:06 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 20:06 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 20:06 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 20:06 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 20:06 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-6Client Sample ID: MW-06R
Matrix: WaterDate Collected: 10/18/16 14:42
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)103 70-130 10/29/16 20:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)99 10/29/16 20:06 170-130
1,2-Dichloroethane-d4 (Surr)100 10/29/16 20:06 170-130
Toluene-d8 (Surr)99 10/29/16 20:06 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 21:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:07 1Barium0.0284
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 21:07 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:03 1Chromium<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:07 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 21:07 1Lead<0.00200
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 21:07 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:07 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:03 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:16 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:16 1Cobalt0.159 J
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:16 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 05:16 1Vanadium2.59 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 05:16 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-7Client Sample ID: MW-07R
Matrix: WaterDate Collected: 10/18/16 13:15
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 20:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 20:33 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 20:33 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 20:33 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 20:33 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 20:33 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 20:33 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 20:33 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 20:33 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 20:33 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 20:33 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 20:33 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 20:33 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 20:33 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 20:33 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 20:33 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 20:33 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 20:33 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 20:33 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 20:33 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 20:33 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 20:33 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 20:33 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 20:33 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 20:33 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 20:33 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 20:33 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 20:33 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 20:33 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 20:33 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 20:33 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 20:33 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 20:33 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 20:33 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 20:33 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 20:33 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 20:33 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 20:33 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 20:33 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 20:33 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 20:33 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 20:33 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 20:33 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 20:33 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 20:33 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 20:33 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 20:33 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 20:33 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-7Client Sample ID: MW-07R
Matrix: WaterDate Collected: 10/18/16 13:15
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)103 70-130 10/29/16 20:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)99 10/29/16 20:33 170-130
1,2-Dichloroethane-d4 (Surr)101 10/29/16 20:33 170-130
Toluene-d8 (Surr)100 10/29/16 20:33 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 0.00900 J 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 21:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:13 1Barium0.242
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 21:13 1Cadmium0.00650
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:08 1Chromium0.0142
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:13 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 21:13 1Lead0.00580
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 21:13 1Nickel0.00690 J
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:13 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:08 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:21 1Beryllium0.506 J
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:21 1Cobalt4.06
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:21 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 05:21 1Vanadium20.3 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 05:21 1Zinc44.1
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-8Client Sample ID: MW-08
Matrix: WaterDate Collected: 10/18/16 12:29
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 21:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 21:00 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 21:00 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 21:00 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 21:00 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 21:00 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 21:00 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 21:00 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 21:00 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 21:00 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 21:00 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 21:00 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 21:00 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 21:00 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 21:00 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 21:00 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 21:00 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 21:00 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 21:00 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 21:00 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 21:00 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 21:00 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 21:00 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 21:00 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 21:00 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 21:00 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 21:00 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 21:00 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 21:00 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 21:00 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 21:00 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 21:00 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 21:00 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 21:00 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 21:00 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 21:00 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 21:00 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 21:00 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 21:00 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 21:00 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 21:00 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 21:00 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 21:00 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 21:00 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 21:00 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 21:00 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 21:00 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 21:00 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-8Client Sample ID: MW-08
Matrix: WaterDate Collected: 10/18/16 12:29
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)104 70-130 10/29/16 21:00 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)96 10/29/16 21:00 170-130
1,2-Dichloroethane-d4 (Surr)103 10/29/16 21:00 170-130
Toluene-d8 (Surr)99 10/29/16 21:00 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 21:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:18 1Barium0.0335
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 21:18 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:13 1Chromium<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:18 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 21:18 1Lead0.00270 J
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 21:18 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:18 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:13 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:27 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:27 1Cobalt1.14 J
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:27 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 05:27 1Vanadium6.54 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 05:27 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-9Client Sample ID: MW-09
Matrix: WaterDate Collected: 10/19/16 13:36
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 21:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 21:27 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 21:27 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 21:27 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 21:27 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 21:27 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 21:27 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 21:27 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 21:27 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 21:27 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 21:27 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 21:27 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 21:27 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 21:27 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 21:27 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 21:27 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 21:27 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 21:27 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 21:27 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 21:27 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 21:27 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 21:27 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 21:27 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 21:27 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 21:27 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 21:27 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 21:27 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 21:27 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 21:27 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 21:27 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 21:27 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 21:27 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 21:27 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 21:27 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 21:27 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 21:27 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 21:27 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 21:27 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 21:27 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 21:27 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 21:27 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 21:27 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 21:27 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 21:27 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 21:27 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 21:27 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 21:27 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 21:27 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-9Client Sample ID: MW-09
Matrix: WaterDate Collected: 10/19/16 13:36
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)105 70-130 10/29/16 21:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)98 10/29/16 21:27 170-130
1,2-Dichloroethane-d4 (Surr)102 10/29/16 21:27 170-130
Toluene-d8 (Surr)99 10/29/16 21:27 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 21:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:23 1Barium0.146
0.00100 0.000500 mg/L 10/26/16 08:42 10/31/16 21:23 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:18 1Chromium<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:23 1Copper<0.00500
0.00500 0.00200 mg/L 10/26/16 08:42 10/31/16 21:23 1Lead0.00220 J
0.0100 0.00300 mg/L 10/26/16 08:42 10/31/16 21:23 1Nickel<0.00300
0.0100 0.00500 mg/L 10/26/16 08:42 10/31/16 21:23 1Selenium<0.00500
0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 21:18 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:32 1Beryllium<0.100
2.00 0.100 ug/L 10/26/16 08:45 11/01/16 05:32 1Cobalt0.235 J
2.00 0.800 ug/L 10/26/16 08:45 11/01/16 05:32 1Thallium<0.800
2.00 0.700 ug/L 10/26/16 08:45 11/01/16 05:32 1Vanadium2.65 B
25.0 5.20 ug/L 10/26/16 08:45 11/01/16 05:32 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 16:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/19/16 01:01
Date Received: 10/20/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 11.0 J 25.0 2.66 ug/L 10/29/16 17:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/29/16 17:23 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/29/16 17:23 1Benzene<0.200
1.00 0.150 ug/L 10/29/16 17:23 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/29/16 17:23 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/29/16 17:23 1Bromoform<0.290
1.00 0.350 ug/L 10/29/16 17:23 1Bromomethane<0.350
50.0 2.64 ug/L 10/29/16 17:23 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/29/16 17:23 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/29/16 17:23 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/29/16 17:23 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/29/16 17:23 1Chloroethane<0.360
1.00 0.230 ug/L 10/29/16 17:23 1Chloroform<0.230
1.00 0.360 ug/L 10/29/16 17:23 1Chloromethane<0.360
1.00 0.210 ug/L 10/29/16 17:23 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/29/16 17:23 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/29/16 17:23 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/29/16 17:23 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/29/16 17:23 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/29/16 17:23 1Dibromomethane<0.450
1.00 0.190 ug/L 10/29/16 17:23 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/29/16 17:23 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/29/16 17:23 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/29/16 17:23 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/29/16 17:23 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/29/16 17:23 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/29/16 17:23 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/29/16 17:23 12-Hexanone <1.28
10.0 1.50 ug/L 10/29/16 17:23 1Iodomethane<1.50
5.00 1.00 ug/L 10/29/16 17:23 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/29/16 17:23 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/29/16 17:23 1Styrene<0.280
1.00 0.150 ug/L 10/29/16 17:23 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/29/16 17:23 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/29/16 17:23 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/29/16 17:23 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/29/16 17:23 1Toluene<0.170
5.00 0.460 ug/L 10/29/16 17:23 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/29/16 17:23 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/29/16 17:23 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/29/16 17:23 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/29/16 17:23 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/29/16 17:23 1Trichloroethene<0.200
1.00 0.210 ug/L 10/29/16 17:23 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/29/16 17:23 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/29/16 17:23 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/29/16 17:23 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/29/16 17:23 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114461-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/19/16 01:01
Date Received: 10/20/16 09:20
4-Bromofluorobenzene (Surr)107 70-130 10/29/16 17:23 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)96 10/29/16 17:23 170-130
1,2-Dichloroethane-d4 (Surr)98 10/29/16 17:23 170-130
Toluene-d8 (Surr)102 10/29/16 17:23 170-130
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-382382/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/29/16 13:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 10/29/16 13:39 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/29/16 13:39 1Benzene
<0.150 0.1501.00 ug/L 10/29/16 13:39 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/29/16 13:39 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/29/16 13:39 1Bromoform
<0.350 0.3501.00 ug/L 10/29/16 13:39 1Bromomethane
<2.64 2.6450.0 ug/L 10/29/16 13:39 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/29/16 13:39 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/29/16 13:39 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/29/16 13:39 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/29/16 13:39 1Chloroethane
<0.230 0.2301.00 ug/L 10/29/16 13:39 1Chloroform
<0.360 0.3601.00 ug/L 10/29/16 13:39 1Chloromethane
<0.210 0.2101.00 ug/L 10/29/16 13:39 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/29/16 13:39 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/29/16 13:39 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/29/16 13:39 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/29/16 13:39 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/29/16 13:39 1Dibromomethane
<0.190 0.1901.00 ug/L 10/29/16 13:39 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/29/16 13:39 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/29/16 13:39 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/29/16 13:39 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/29/16 13:39 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/29/16 13:39 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/29/16 13:39 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/29/16 13:39 12-Hexanone
<1.50 1.5010.0 ug/L 10/29/16 13:39 1Iodomethane
<1.00 1.005.00 ug/L 10/29/16 13:39 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/29/16 13:39 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/29/16 13:39 1Styrene
<0.150 0.1501.00 ug/L 10/29/16 13:39 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/29/16 13:39 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/29/16 13:39 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/29/16 13:39 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/29/16 13:39 1Toluene
<0.460 0.4605.00 ug/L 10/29/16 13:39 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/29/16 13:39 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/29/16 13:39 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/29/16 13:39 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/29/16 13:39 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/29/16 13:39 1Trichloroethene
<0.210 0.2101.00 ug/L 10/29/16 13:39 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/29/16 13:39 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/29/16 13:39 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/29/16 13:39 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/29/16 13:39 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
4-Bromofluorobenzene (Surr)108 70-130 10/29/16 13:39 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
98 10/29/16 13:39 1Dibromofluoromethane (Surr)70-130
96 10/29/16 13:39 11,2-Dichloroethane-d4 (Surr)70-130
100 10/29/16 13:39 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-382382/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
Acetone 100 125.4 ug/L 125 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 224.4 ug/L 112 63-135
Benzene 20.0 20.74 ug/L 104 70-130
Bromochloromethane 20.0 19.74 ug/L 99 70-130
Bromodichloromethane 20.0 19.26 ug/L 96 70-130
Bromoform 20.0 17.57 ug/L 88 70-137
Bromomethane 20.0 23.75 ug/L 119 53-150
2-Butanone (MEK)100 114.1 ug/L 114 55-143
Carbon disulfide 20.0 20.85 ug/L 104 64-135
Carbon tetrachloride 20.0 17.80 ug/L 89 70-147
Chlorobenzene 20.0 19.80 ug/L 99 70-130
Chloroethane 20.0 20.94 ug/L 105 60-138
Chloroform 20.0 19.34 ug/L 97 70-130
Chloromethane 20.0 20.94 ug/L 105 33-150
cis-1,2-Dichloroethene 20.0 21.50 ug/L 107 70-130
cis-1,3-Dichloropropene 20.0 20.50 ug/L 102 70-133
Dibromochloromethane 20.0 18.53 ug/L 93 70-133
1,2-Dibromo-3-Chloropropane 20.0 16.66 ug/L 83 45-138
1,2-Dibromoethane (EDB)20.0 19.54 ug/L 98 70-130
Dibromomethane 20.0 19.15 ug/L 96 70-130
1,2-Dichlorobenzene 20.0 20.80 ug/L 104 70-130
1,4-Dichlorobenzene 20.0 21.20 ug/L 106 70-130
1,1-Dichloroethane 20.0 20.45 ug/L 102 70-130
1,2-Dichloroethane 20.0 19.56 ug/L 98 70-130
1,1-Dichloroethene 20.0 21.27 ug/L 106 70-132
1,2-Dichloropropane 20.0 21.54 ug/L 108 70-130
Ethylbenzene 20.0 20.21 ug/L 101 70-130
2-Hexanone 100 114.3 ug/L 114 54-142
Iodomethane 20.0 17.05 ug/L 85 40-150
Methylene Chloride 20.0 21.47 ug/L 107 70-130
4-Methyl-2-pentanone (MIBK)100 111.0 ug/L 111 60-137
Styrene 20.0 19.30 ug/L 96 70-130
1,1,1,2-Tetrachloroethane 20.0 18.71 ug/L 94 70-130
1,1,2,2-Tetrachloroethane 20.0 21.91 ug/L 110 69-131
Tetrachloroethene 20.0 19.47 ug/L 97 70-130
Tetrahydrofuran 40.0 47.27 ug/L 118 51-136
Toluene 20.0 21.02 ug/L 105 70-130
trans-1,4-Dichloro-2-butene 20.0 18.09 ug/L 90 41-150
trans-1,2-Dichloroethene 20.0 20.28 ug/L 101 70-130
trans-1,3-Dichloropropene 20.0 19.57 ug/L 98 63-142
1,1,1-Trichloroethane 20.0 18.77 ug/L 94 70-135
1,1,2-Trichloroethane 20.0 21.08 ug/L 105 70-130
Trichloroethene 20.0 19.66 ug/L 98 70-130
Trichlorofluoromethane 20.0 21.17 ug/L 106 59-150
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-382382/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
1,2,3-Trichloropropane 20.0 20.22 ug/L 101 70-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 40.0 44.88 ug/L 112 54-146
Vinyl chloride 20.0 21.95 ug/L 110 57-137
Xylenes, Total 40.0 39.74 ug/L 99 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
107
LCS LCS
Qualifier Limits%Recovery
94Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-382382/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
Acetone 100 126.7 ug/L 127 39-150 1 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 229.8 ug/L 115 63-135 2 16
Benzene 20.0 20.84 ug/L 104 70-130 0 12
Bromochloromethane 20.0 18.50 ug/L 93 70-130 6 16
Bromodichloromethane 20.0 19.16 ug/L 96 70-130 1 14
Bromoform 20.0 18.38 ug/L 92 70-137 4 14
Bromomethane 20.0 23.69 ug/L 118 53-150 0 19
2-Butanone (MEK)100 115.4 ug/L 115 55-143 1 19
Carbon disulfide 20.0 20.82 ug/L 104 64-135 0 16
Carbon tetrachloride 20.0 18.31 ug/L 92 70-147 3 16
Chlorobenzene 20.0 19.71 ug/L 99 70-130 0 12
Chloroethane 20.0 20.74 ug/L 104 60-138 1 15
Chloroform 20.0 18.98 ug/L 95 70-130 2 14
Chloromethane 20.0 21.56 ug/L 108 33-150 3 20
cis-1,2-Dichloroethene 20.0 20.60 ug/L 103 70-130 4 15
cis-1,3-Dichloropropene 20.0 19.37 ug/L 97 70-133 6 15
Dibromochloromethane 20.0 17.85 ug/L 89 70-133 4 13
1,2-Dibromo-3-Chloropropane 20.0 15.51 ug/L 78 45-138 7 19
1,2-Dibromoethane (EDB)20.0 18.88 ug/L 94 70-130 3 13
Dibromomethane 20.0 19.37 ug/L 97 70-130 1 14
1,2-Dichlorobenzene 20.0 20.02 ug/L 100 70-130 4 12
1,4-Dichlorobenzene 20.0 19.88 ug/L 99 70-130 6 12
1,1-Dichloroethane 20.0 20.43 ug/L 102 70-130 0 17
1,2-Dichloroethane 20.0 19.68 ug/L 98 70-130 1 13
1,1-Dichloroethene 20.0 20.70 ug/L 103 70-132 3 20
1,2-Dichloropropane 20.0 21.19 ug/L 106 70-130 2 15
Ethylbenzene 20.0 19.91 ug/L 100 70-130 1 12
2-Hexanone 100 113.2 ug/L 113 54-142 1 17
Iodomethane 20.0 15.94 ug/L 80 40-150 7 20
Methylene Chloride 20.0 20.87 ug/L 104 70-130 3 15
4-Methyl-2-pentanone (MIBK)100 109.6 ug/L 110 60-137 1 21
Styrene 20.0 19.20 ug/L 96 70-130 1 12
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-382382/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
1,1,1,2-Tetrachloroethane 20.0 18.14 ug/L 91 70-130 3 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 20.0 21.43 ug/L 107 69-131 2 15
Tetrachloroethene 20.0 19.39 ug/L 97 70-130 0 17
Tetrahydrofuran 40.0 49.19 ug/L 123 51-136 4 20
Toluene 20.0 20.42 ug/L 102 70-130 3 13
trans-1,4-Dichloro-2-butene 20.0 18.67 ug/L 93 41-150 3 20
trans-1,2-Dichloroethene 20.0 20.56 ug/L 103 70-130 1 15
trans-1,3-Dichloropropene 20.0 18.64 ug/L 93 63-142 5 13
1,1,1-Trichloroethane 20.0 18.76 ug/L 94 70-135 0 15
1,1,2-Trichloroethane 20.0 20.04 ug/L 100 70-130 5 13
Trichloroethene 20.0 19.37 ug/L 97 70-130 2 14
Trichlorofluoromethane 20.0 21.36 ug/L 107 59-150 1 22
1,2,3-Trichloropropane 20.0 19.80 ug/L 99 70-131 2 14
Vinyl acetate 40.0 45.35 ug/L 113 54-146 1 20
Vinyl chloride 20.0 21.98 ug/L 110 57-137 0 15
Xylenes, Total 40.0 38.63 ug/L 97 70-132 3 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
106
LCSD LCSD
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
Acetone <2.66 100 113.8 ug/L 114 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 200.7 ug/L 100 50-135
Benzene <0.200 20.0 19.11 ug/L 96 55-147
Bromochloromethane <0.150 20.0 18.09 ug/L 90 59-132
Bromodichloromethane <0.170 20.0 18.53 ug/L 93 70-140
Bromoform <0.290 20.0 16.58 ug/L 83 53-150
Bromomethane <0.350 20.0 23.61 ug/L 118 30-150
2-Butanone (MEK)<2.64 100 95.71 ug/L 96 50-143
Carbon disulfide <0.220 20.0 19.52 ug/L 98 35-150
Carbon tetrachloride <0.180 20.0 18.54 ug/L 93 56-150
Chlorobenzene <0.180 20.0 17.70 ug/L 89 70-130
Chloroethane <0.360 20.0 19.92 ug/L 100 58-141
Chloroform <0.230 20.0 18.75 ug/L 94 66-138
Chloromethane <0.360 20.0 21.63 ug/L 108 10-150
cis-1,2-Dichloroethene <0.210 20.0 19.71 ug/L 99 68-131
cis-1,3-Dichloropropene <0.170 20.0 18.37 ug/L 92 70-133
Dibromochloromethane <0.250 20.0 17.74 ug/L 89 66-140
1,2-Dibromo-3-Chloropropane <0.940 20.0 13.55 ug/L 68 38-138
1,2-Dibromoethane (EDB)<0.210 20.0 16.86 ug/L 84 65-137
Dibromomethane <0.450 20.0 18.45 ug/L 92 70-130
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
1,2-Dichlorobenzene <0.190 20.0 17.18 ug/L 86 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 20.0 16.67 ug/L 83 70-130
1,1-Dichloroethane <0.240 20.0 19.51 ug/L 98 61-139
1,2-Dichloroethane <0.200 20.0 19.44 ug/L 97 64-136
1,1-Dichloroethene <0.250 20.0 20.59 ug/L 103 54-150
1,2-Dichloropropane <0.250 20.0 19.39 ug/L 97 67-130
Ethylbenzene <0.190 20.0 17.87 ug/L 89 65-139
2-Hexanone <1.28 100 94.57 ug/L 95 44-150
Iodomethane <1.50 20.0 17.27 ug/L 86 34-150
Methylene Chloride <1.00 20.0 19.04 ug/L 95 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 91.66 ug/L 92 50-140
Styrene <0.280 20.0 17.31 ug/L 87 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 16.93 ug/L 85 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 18.62 ug/L 93 56-145
Tetrachloroethene <0.140 20.0 18.01 ug/L 90 57-138
Tetrahydrofuran <0.820 40.0 38.33 ug/L 96 40-136
Toluene <0.170 20.0 18.70 ug/L 94 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 15.68 ug/L 78 39-150
trans-1,2-Dichloroethene <0.230 20.0 19.81 ug/L 99 59-143
trans-1,3-Dichloropropene <0.170 20.0 17.57 ug/L 88 63-142
1,1,1-Trichloroethane <0.190 20.0 18.66 ug/L 93 68-144
1,1,2-Trichloroethane <0.190 20.0 17.65 ug/L 88 70-130
Trichloroethene <0.200 20.0 18.55 ug/L 93 63-135
Trichlorofluoromethane <0.210 20.0 21.27 ug/L 106 44-150
1,2,3-Trichloropropane <0.230 20.0 16.92 ug/L 85 65-131
Vinyl acetate <1.71 40.0 38.71 ug/L 97 43-146
Vinyl chloride <0.180 20.0 21.40 ug/L 107 57-150
Xylenes, Total <0.580 40.0 35.11 ug/L 88 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
MS MS
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
1021,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
Acetone <2.66 100 114.2 ug/L 114 39-150 0 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 224.3 ug/L 112 50-135 11 23
Benzene <0.200 20.0 20.99 ug/L 105 55-147 9 22
Bromochloromethane <0.150 20.0 20.65 ug/L 103 59-132 13 21
Bromodichloromethane <0.170 20.0 20.49 ug/L 102 70-140 10 196
Bromoform <0.290 20.0 17.36 ug/L 87 53-150 5 20
Bromomethane <0.350 20.0 28.25 ug/L 141 30-150 18 44
2-Butanone (MEK)<2.64 100 106.2 ug/L 106 50-143 10 28
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382382
Carbon disulfide <0.220 20.0 21.59 ug/L 108 35-150 10 34
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 20.0 20.38 ug/L 102 56-150 9 18
Chlorobenzene <0.180 20.0 19.20 ug/L 96 70-130 8 15
Chloroethane <0.360 20.0 22.33 ug/L 112 58-141 11 31
Chloroform <0.230 20.0 20.87 ug/L 104 66 -138 11 21
Chloromethane <0.360 20.0 23.77 ug/L 119 10 -150 9 43
cis-1,2-Dichloroethene <0.210 20.0 21.20 ug/L 106 68 -131 7 21
cis-1,3-Dichloropropene <0.170 20.0 20.23 ug/L 101 70 -133 10 19
Dibromochloromethane <0.250 20.0 18.64 ug/L 93 66 -140 5 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 15.43 ug/L 77 38 -138 13 26
1,2-Dibromoethane (EDB)<0.210 20.0 18.71 ug/L 94 65 -137 10 21
Dibromomethane <0.450 20.0 19.63 ug/L 98 70 -130 6 19
1,2-Dichlorobenzene <0.190 20.0 19.47 ug/L 97 70 -130 13 15
1,4-Dichlorobenzene <0.170 20.0 18.87 ug/L 94 70 -130 12 14
1,1-Dichloroethane <0.240 20.0 22.09 ug/L 110 61 -139 12 23
1,2-Dichloroethane <0.200 20.0 22.07 ug/L 110 64 -136 13 22
1,1-Dichloroethene <0.250 20.0 22.76 ug/L 114 54 -150 10 24
1,2-Dichloropropane <0.250 20.0 22.08 ug/L 110 67 -130 13 19
Ethylbenzene <0.190 20.0 18.92 ug/L 95 65 -139 6 18
2-Hexanone <1.28 100 106.7 ug/L 107 44 -150 12 21
Iodomethane <1.50 20.0 19.94 ug/L 100 34 -150 14 37
Methylene Chloride <1.00 20.0 20.96 ug/L 105 64 -130 10 22
4-Methyl-2-pentanone (MIBK)<0.810 100 101.6 ug/L 102 50 -140 10 24
Styrene <0.280 20.0 18.74 ug/L 94 70 -130 8 16
1,1,1,2-Tetrachloroethane <0.150 20.0 17.93 ug/L 90 70 -131 6 16
1,1,2,2-Tetrachloroethane <0.190 20.0 21.25 ug/L 106 56 -145 13 19
Tetrachloroethene <0.140 20.0 18.43 ug/L 92 57 -138 2 17
Tetrahydrofuran <0.820 40.0 49.60 ug/L 124 40 -136 26 27
Toluene <0.170 20.0 20.00 ug/L 100 64 -136 7 18
trans-1,4-Dichloro-2-butene <0.460 20.0 19.01 ug/L 95 39 -150 19 28
trans-1,2-Dichloroethene <0.230 20.0 21.98 ug/L 110 59 -143 10 25
trans-1,3-Dichloropropene <0.170 20.0 19.78 ug/L 99 63 -142 12 18
1,1,1-Trichloroethane <0.190 20.0 21.08 ug/L 105 68 -144 12 17
1,1,2-Trichloroethane <0.190 20.0 19.97 ug/L 100 70 -130 12 18
Trichloroethene <0.200 20.0 20.15 ug/L 101 63-135 8 17
Trichlorofluoromethane <0.210 20.0 23.21 ug/L 116 44-150 9 32
1,2,3-Trichloropropane <0.230 20.0 19.27 ug/L 96 65-131 13 19
Vinyl acetate <1.71 40.0 43.56 ug/L 109 43-146 12 20
Vinyl chloride <0.180 20.0 23.89 ug/L 119 57 -150 11 37
Xylenes, Total <0.580 40.0 37.45 ug/L 94 69 -132 6 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
107
MSD MSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1011,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-381196/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383018 Prep Batch: 381196
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/26/16 08:42 10/31/16 19:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 10/26/16 08:42 10/31/16 19:54 1Barium
<0.000500 0.0005000.00100 mg/L 10/26/16 08:42 10/31/16 19:54 1Cadmium
<0.00500 0.005000.0100 mg/L 10/26/16 08:42 10/31/16 19:54 1Copper
<0.00200 0.002000.00500 mg/L 10/26/16 08:42 10/31/16 19:54 1Lead
<0.00300 0.003000.0100 mg/L 10/26/16 08:42 10/31/16 19:54 1Nickel
<0.00500 0.005000.0100 mg/L 10/26/16 08:42 10/31/16 19:54 1Selenium
Client Sample ID: Method BlankLab Sample ID: MB 490-381196/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383318 Prep Batch: 381196
RL MDL
Chromium <0.00300 0.00500 0.00300 mg/L 10/26/16 08:42 11/01/16 19:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00300 0.003000.00500 mg/L 10/26/16 08:42 11/01/16 19:51 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381196/25-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383318 Prep Batch: 381196
Silver 0.0500 0.04760 mg/L 95 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381196/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383018 Prep Batch: 381196
Arsenic 0.0500 0.04710 mg/L 94 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.027 mg/L 101 80-120
Cadmium 0.0500 0.05030 mg/L 101 80-120
Copper 0.250 0.2491 mg/L 100 80-120
Lead 0.0500 0.04850 mg/L 97 80-120
Nickel 0.500 0.4939 mg/L 99 80-120
Selenium 0.0500 0.05110 mg/L 102 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381196/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383318 Prep Batch: 381196
Chromium 0.200 0.2041 mg/L 102 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383018 Prep Batch: 381196
Arsenic <0.00860 0.0500 0.04740 mg/L 95 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383018 Prep Batch: 381196
Barium 0.106 2.00 2.141 mg/L 102 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Cadmium <0.000500 0.0500 0.05050 mg/L 101 75-125
Copper <0.00500 0.250 0.2515 mg/L 101 75-125
Lead <0.00200 0.0500 0.05010 mg/L 100 75-125
Nickel <0.00300 0.500 0.4940 mg/L 99 75-125
Selenium <0.00500 0.0500 0.05150 mg/L 103 75-125
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383318 Prep Batch: 381196
Chromium 0.00430 J 0.200 0.2105 mg/L 103 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Silver <0.00300 0.0500 0.03900 mg/L 78 75-125
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383018 Prep Batch: 381196
Arsenic <0.00860 0.0500 0.04790 mg/L 96 75-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.106 2.00 2.122 mg/L 101 75-125 1 20
Cadmium <0.000500 0.0500 0.05020 mg/L 100 75-125 1 20
Copper <0.00500 0.250 0.2489 mg/L 100 75-125 1 20
Lead <0.00200 0.0500 0.04910 mg/L 98 75-125 2 20
Nickel <0.00300 0.500 0.4895 mg/L 98 75-125 1 20
Selenium <0.00500 0.0500 0.05060 mg/L 101 75-125 2 20
Client Sample ID: MW-01Lab Sample ID: 490-114461-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383318 Prep Batch: 381196
Chromium 0.00430 J 0.200 0.2116 mg/L 104 75-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Silver <0.00300 0.0500 0.03850 mg/L 77 75-125 1 20
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-381203/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383075 Prep Batch: 381203
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/26/16 08:45 11/01/16 04:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.100 0.1002.00 ug/L 10/26/16 08:45 11/01/16 04:05 1Beryllium
<0.100 0.1002.00 ug/L 10/26/16 08:45 11/01/16 04:05 1Cobalt
<0.800 0.8002.00 ug/L 10/26/16 08:45 11/01/16 04:05 1Thallium
1.558 J 0.7002.00 ug/L 10/26/16 08:45 11/01/16 04:05 1Vanadium
<5.20 5.2025.0 ug/L 10/26/16 08:45 11/01/16 04:05 1Zinc
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381203/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383075 Prep Batch: 381203
Antimony 100 99.21 ug/L 99 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 97.24 ug/L 97 80-120
Cobalt 100 105.0 ug/L 105 80-120
Thallium 100 96.05 ug/L 96 80-120
Vanadium 100 104.0 ug/L 104 80-120
Zinc 100 80.94 ug/L 81 80-120
Client Sample ID: MW-04Lab Sample ID: 490-114461-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383075 Prep Batch: 381203
Antimony <0.800 100 97.99 ug/L 98 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <0.100 100 95.22 ug/L 95 75-125
Cobalt <0.100 100 102.2 ug/L 102 75-125
Thallium <0.800 100 93.92 ug/L 94 75-125
Vanadium 5.98 B 100 105.6 ug/L 100 75-125
Zinc <5.20 100 81.40 ug/L 81 75-125
Client Sample ID: MW-04Lab Sample ID: 490-114461-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383075 Prep Batch: 381203
Antimony <0.800 100 100.0 ug/L 100 75-125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.100 100 96.14 ug/L 96 75-125 1 20
Cobalt <0.100 100 101.9 ug/L 102 75-125 0 20
Thallium <0.800 100 94.05 ug/L 94 75-125 0 20
Vanadium 5.98 B 100 104.6 ug/L 99 75-125 1 20
Zinc <5.20 100 80.98 ug/L 81 75-125 1 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-380816/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380816
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:08 10/25/16 15:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380816/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380816
Mercury 1.00 1.035 ug/L 104 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380816/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380816
Mercury 1.00 0.9830 ug/L 98 80-120 5 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-114460-G-5-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380816
Mercury <0.100 1.00 1.076 ug/L 108 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114460-G-5-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380816
Mercury <0.100 1.00 0.9736 ug/L 97 75-125 10 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
GC/MS VOA
Analysis Batch: 382382
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-114461-1 MW-01 Total/NA
Water 8260B490-114461-2 MW-02 Total/NA
Water 8260B490-114461-3 MW-03 Total/NA
Water 8260B490-114461-4 MW-04 Total/NA
Water 8260B490-114461-5 MW-05 Total/NA
Water 8260B490-114461-6 MW-06R Total/NA
Water 8260B490-114461-7 MW-07R Total/NA
Water 8260B490-114461-8 MW-08 Total/NA
Water 8260B490-114461-9 MW-09 Total/NA
Water 8260B490-114461-10 Trip Blank Total/NA
Water 8260BMB 490-382382/7 Method Blank Total/NA
Water 8260BLCS 490-382382/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-382382/4 Lab Control Sample Dup Total/NA
Water 8260B490-114461-1 MS MW-01 Total/NA
Water 8260B490-114461-1 MSD MW-01 Total/NA
Metals
Prep Batch: 380816
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-114461-1 MW-01 Total/NA
Water 7470A490-114461-2 MW-02 Total/NA
Water 7470A490-114461-3 MW-03 Total/NA
Water 7470A490-114461-4 MW-04 Total/NA
Water 7470A490-114461-5 MW-05 Total/NA
Water 7470A490-114461-6 MW-06R Total/NA
Water 7470A490-114461-7 MW-07R Total/NA
Water 7470A490-114461-8 MW-08 Total/NA
Water 7470A490-114461-9 MW-09 Total/NA
Water 7470AMB 490-380816/1-A Method Blank Total/NA
Water 7470ALCS 490-380816/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-380816/3-A Lab Control Sample Dup Total/NA
Water 7470A490-114460-G-5-C MS Matrix Spike Total/NA
Water 7470A490-114460-G-5-D MSD Matrix Spike Duplicate Total/NA
Prep Batch: 381196
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114461-1 MW-01 Total/NA
Water 3010A490-114461-2 MW-02 Total/NA
Water 3010A490-114461-3 MW-03 Total/NA
Water 3010A490-114461-4 MW-04 Total/NA
Water 3010A490-114461-5 MW-05 Total/NA
Water 3010A490-114461-6 MW-06R Total/NA
Water 3010A490-114461-7 MW-07R Total/NA
Water 3010A490-114461-8 MW-08 Total/NA
Water 3010A490-114461-9 MW-09 Total/NA
Water 3010AMB 490-381196/1-A Method Blank Total/NA
Water 3010ALCS 490-381196/25-A Lab Control Sample Total/NA
Water 3010ALCS 490-381196/2-A Lab Control Sample Total/NA
Water 3010A490-114461-1 MS MW-01 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Metals (Continued)
Prep Batch: 381196 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114461-1 MSD MW-01 Total/NA
Prep Batch: 381203
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114461-1 MW-01 Total/NA
Water 3010A490-114461-2 MW-02 Total/NA
Water 3010A490-114461-3 MW-03 Total/NA
Water 3010A490-114461-4 MW-04 Total/NA
Water 3010A490-114461-5 MW-05 Total/NA
Water 3010A490-114461-6 MW-06R Total/NA
Water 3010A490-114461-7 MW-07R Total/NA
Water 3010A490-114461-8 MW-08 Total/NA
Water 3010A490-114461-9 MW-09 Total/NA
Water 3010AMB 490-381203/1-A Method Blank Total/NA
Water 3010ALCS 490-381203/2-A Lab Control Sample Total/NA
Water 3010A490-114461-4 MS MW-04 Total/NA
Water 3010A490-114461-4 MSD MW-04 Total/NA
Analysis Batch: 381453
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 380816490-114461-1 MW-01 Total/NA
Water 7470A 380816490-114461-2 MW-02 Total/NA
Water 7470A 380816490-114461-3 MW-03 Total/NA
Water 7470A 380816490-114461-4 MW-04 Total/NA
Water 7470A 380816490-114461-5 MW-05 Total/NA
Water 7470A 380816490-114461-6 MW-06R Total/NA
Water 7470A 380816490-114461-7 MW-07R Total/NA
Water 7470A 380816490-114461-8 MW-08 Total/NA
Water 7470A 380816490-114461-9 MW-09 Total/NA
Water 7470A 380816MB 490-380816/1-A Method Blank Total/NA
Water 7470A 380816LCS 490-380816/2-A Lab Control Sample Total/NA
Water 7470A 380816LCSD 490-380816/3-A Lab Control Sample Dup Total/NA
Water 7470A 380816490-114460-G-5-C MS Matrix Spike Total/NA
Water 7470A 380816490-114460-G-5-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 383018
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 381196490-114461-1 MW-01 Total/NA
Water 6010D 381196490-114461-2 MW-02 Total/NA
Water 6010D 381196490-114461-3 MW-03 Total/NA
Water 6010D 381196490-114461-4 MW-04 Total/NA
Water 6010D 381196490-114461-5 MW-05 Total/NA
Water 6010D 381196490-114461-6 MW-06R Total/NA
Water 6010D 381196490-114461-7 MW-07R Total/NA
Water 6010D 381196490-114461-8 MW-08 Total/NA
Water 6010D 381196490-114461-9 MW-09 Total/NA
Water 6010D 381196MB 490-381196/1-A Method Blank Total/NA
Water 6010D 381196LCS 490-381196/2-A Lab Control Sample Total/NA
Water 6010D 381196490-114461-1 MS MW-01 Total/NA
Water 6010D 381196490-114461-1 MSD MW-01 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Metals (Continued)
Analysis Batch: 383075
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 381203490-114461-1 MW-01 Total/NA
Water 6020B 381203490-114461-2 MW-02 Total/NA
Water 6020B 381203490-114461-3 MW-03 Total/NA
Water 6020B 381203490-114461-4 MW-04 Total/NA
Water 6020B 381203490-114461-5 MW-05 Total/NA
Water 6020B 381203490-114461-6 MW-06R Total/NA
Water 6020B 381203490-114461-7 MW-07R Total/NA
Water 6020B 381203490-114461-8 MW-08 Total/NA
Water 6020B 381203490-114461-9 MW-09 Total/NA
Water 6020B 381203MB 490-381203/1-A Method Blank Total/NA
Water 6020B 381203LCS 490-381203/2-A Lab Control Sample Total/NA
Water 6020B 381203490-114461-4 MS MW-04 Total/NA
Water 6020B 381203490-114461-4 MSD MW-04 Total/NA
Analysis Batch: 383318
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 381196490-114461-1 MW-01 Total/NA
Water 6010D 381196490-114461-2 MW-02 Total/NA
Water 6010D 381196490-114461-3 MW-03 Total/NA
Water 6010D 381196490-114461-4 MW-04 Total/NA
Water 6010D 381196490-114461-5 MW-05 Total/NA
Water 6010D 381196490-114461-6 MW-06R Total/NA
Water 6010D 381196490-114461-7 MW-07R Total/NA
Water 6010D 381196490-114461-8 MW-08 Total/NA
Water 6010D 381196490-114461-9 MW-09 Total/NA
Water 6010D 381196MB 490-381196/1-A Method Blank Total/NA
Water 6010D 381196LCS 490-381196/25-A Lab Control Sample Total/NA
Water 6010D 381196LCS 490-381196/2-A Lab Control Sample Total/NA
Water 6010D 381196490-114461-1 MS MW-01 Total/NA
Water 6010D 381196490-114461-1 MSD MW-01 Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114461-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-01 Lab Sample ID: 490-114461-1
Matrix: WaterDate Collected: 10/18/16 11:15
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 17:511 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 20:10 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 20:06 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 04:43 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:12 LCS TAL NSHTotal/NA
Client Sample ID: MW-02 Lab Sample ID: 490-114461-2
Matrix: WaterDate Collected: 10/19/16 12:56
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 18:181 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 20:52 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 20:37 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 04:49 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:16 LCS TAL NSHTotal/NA
Client Sample ID: MW-03 Lab Sample ID: 490-114461-3
Matrix: WaterDate Collected: 10/19/16 11:19
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 18:451 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 20:57 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 20:52 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 04:54 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:25 LCS TAL NSHTotal/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114461-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-04 Lab Sample ID: 490-114461-4
Matrix: WaterDate Collected: 10/19/16 11:51
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 19:121 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 20:36 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 20:32 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 04:16 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:29 LCS TAL NSHTotal/NA
Client Sample ID: MW-05 Lab Sample ID: 490-114461-5
Matrix: WaterDate Collected: 10/19/16 10:18
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 19:391 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 21:02 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 20:57 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 05:10 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:32 LCS TAL NSHTotal/NA
Client Sample ID: MW-06R Lab Sample ID: 490-114461-6
Matrix: WaterDate Collected: 10/18/16 14:42
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 20:061 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 21:07 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 21:03 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 05:16 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:35 LCS TAL NSHTotal/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114461-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: MW-07R Lab Sample ID: 490-114461-7
Matrix: WaterDate Collected: 10/18/16 13:15
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 20:331 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 21:13 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 21:08 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 05:21 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:38 LCS TAL NSHTotal/NA
Client Sample ID: MW-08 Lab Sample ID: 490-114461-8
Matrix: WaterDate Collected: 10/18/16 12:29
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 21:001 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 21:18 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 21:13 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 05:27 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:42 LCS TAL NSHTotal/NA
Client Sample ID: MW-09 Lab Sample ID: 490-114461-9
Matrix: WaterDate Collected: 10/19/16 13:36
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 21:271 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383018 10/31/16 21:23 RDF TAL NSHTotal/NA
Prep 3010A 381196 10/26/16 08:42 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 383318 11/01/16 21:18 BLG TAL NSHTotal/NA
Prep 3010A 381203 10/26/16 08:45 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 383075 11/01/16 05:32 KKK TAL NSHTotal/NA
Prep 7470A 380816 10/25/16 09:08 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/25/16 16:45 LCS TAL NSHTotal/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114461-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: Trip Blank Lab Sample ID: 490-114461-10
Matrix: WaterDate Collected: 10/19/16 01:01
Date Received: 10/20/16 09:20
Analysis 8260B NC10/29/16 17:231 TAL NSH382382
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-114461-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114461-1
Project/Site: Madison Co Operating Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16 *
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-114461-1
SDG Number:
Login Number: 114461
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-114453-1
Client Project/Site: Madison Co. Operating Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
11/3/2016 2:44:49 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
TestAmerica Job ID: 490-114453-1
Page 2 of 34 TestAmerica Nashville11/3/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
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Sample Summary
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-114453-1 SW-01 Water 10/19/16 13:55 10/20/16 16:39
490-114453-2 SW-02R Water 10/18/16 11:35 10/20/16 16:39
490-114453-3 Trip Blank Water 10/19/16 00:01 10/20/16 16:39
TestAmerica Nashville
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114453-1
Project/Site: Madison Co. Operating Landfill
Job ID: 490-114453-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-114453-1
Comments
No additional comments.
Receipt
The samples were received on 10/20/2016 4:39 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 0.7º C.
GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch
490-382617 recovered outside control limits for the following analytes: Bromomethane. These analytes were biased high in the LCS and
were not detected in the associated samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 6020B: The method blank for preparation batch 490-381692 and analytical batch 490-382571 contained Vanadium above the
method detection limit (MDL). Associated samples were not re-analyzed because results were less than the reporting limit (RL) OR
practical quantitation limit (PQL).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Qualifiers
GC/MS VOA
Qualifier Description
E Result exceeded calibration range.
Qualifier
F1 MS and/or MSD Recovery is outside acceptance limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
*LCS or LCSD is outside acceptance limits.
Metals
Qualifier Description
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
Qualifier
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID: 490-114453-1Client Sample ID: SW-01
Matrix: WaterDate Collected: 10/19/16 13:55
Date Received: 10/20/16 16:39
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/30/16 23:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/30/16 23:03 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/30/16 23:03 1Benzene<0.200
1.00 0.150 ug/L 10/30/16 23:03 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/30/16 23:03 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/30/16 23:03 1Bromoform<0.290
1.00 0.350 ug/L 10/30/16 23:03 1Bromomethane<0.350
50.0 2.64 ug/L 10/30/16 23:03 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/30/16 23:03 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/30/16 23:03 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/30/16 23:03 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/30/16 23:03 1Chloroethane<0.360
1.00 0.230 ug/L 10/30/16 23:03 1Chloroform<0.230
1.00 0.360 ug/L 10/30/16 23:03 1Chloromethane<0.360
1.00 0.210 ug/L 10/30/16 23:03 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/30/16 23:03 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/30/16 23:03 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/30/16 23:03 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/30/16 23:03 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/30/16 23:03 1Dibromomethane<0.450
1.00 0.190 ug/L 10/30/16 23:03 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/30/16 23:03 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/30/16 23:03 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/30/16 23:03 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/30/16 23:03 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/30/16 23:03 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/30/16 23:03 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/30/16 23:03 12-Hexanone <1.28
10.0 1.50 ug/L 10/30/16 23:03 1Iodomethane<1.50
5.00 1.00 ug/L 10/30/16 23:03 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/30/16 23:03 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/30/16 23:03 1Styrene<0.280
1.00 0.150 ug/L 10/30/16 23:03 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/30/16 23:03 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/30/16 23:03 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/30/16 23:03 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/30/16 23:03 1Toluene<0.170
5.00 0.460 ug/L 10/30/16 23:03 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/30/16 23:03 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/30/16 23:03 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/30/16 23:03 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/30/16 23:03 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/30/16 23:03 1Trichloroethene<0.200
1.00 0.210 ug/L 10/30/16 23:03 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/30/16 23:03 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/30/16 23:03 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/30/16 23:03 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/30/16 23:03 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID: 490-114453-1Client Sample ID: SW-01
Matrix: WaterDate Collected: 10/19/16 13:55
Date Received: 10/20/16 16:39
4-Bromofluorobenzene (Surr)103 70-130 10/30/16 23:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)95 10/30/16 23:03 170-130
1,2-Dichloroethane-d4 (Surr)94 10/30/16 23:03 170-130
Toluene-d8 (Surr)99 10/30/16 23:03 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 ^0.0100 0.00860 mg/L 10/27/16 10:24 10/30/16 05:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/27/16 10:24 10/30/16 05:56 1Barium0.0480
0.00100 0.000500 mg/L 10/27/16 10:24 10/30/16 05:56 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/27/16 10:24 10/30/16 05:56 1Chromium<0.00300
0.0100 0.00500 mg/L 10/27/16 10:24 10/30/16 05:56 1Copper<0.00500
0.00500 0.00200 mg/L 10/27/16 10:24 10/30/16 05:56 1Lead<0.00200
0.0100 0.00300 mg/L 10/27/16 10:24 10/30/16 05:56 1Nickel<0.00300
0.0100 0.00500 mg/L 10/27/16 10:24 10/30/16 05:56 1Selenium<0.00500
0.00500 0.00300 mg/L 10/27/16 10:24 10/30/16 05:56 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/27/16 10:27 10/30/16 22:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/27/16 10:27 10/30/16 22:07 1Beryllium<0.100
2.00 0.100 ug/L 10/27/16 10:27 10/30/16 22:07 1Cobalt2.22
2.00 0.800 ug/L 10/27/16 10:27 10/30/16 22:07 1Thallium<0.800
2.00 0.700 ug/L 10/27/16 10:27 10/30/16 22:07 1Vanadium3.54 B
25.0 5.20 ug/L 10/27/16 10:27 10/30/16 22:07 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:15 10/26/16 08:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID: 490-114453-2Client Sample ID: SW-02R
Matrix: WaterDate Collected: 10/18/16 11:35
Date Received: 10/20/16 16:39
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/30/16 22:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/30/16 22:33 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/30/16 22:33 1Benzene<0.200
1.00 0.150 ug/L 10/30/16 22:33 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/30/16 22:33 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/30/16 22:33 1Bromoform<0.290
1.00 0.350 ug/L 10/30/16 22:33 1Bromomethane<0.350
50.0 2.64 ug/L 10/30/16 22:33 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/30/16 22:33 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/30/16 22:33 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/30/16 22:33 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/30/16 22:33 1Chloroethane<0.360
1.00 0.230 ug/L 10/30/16 22:33 1Chloroform<0.230
1.00 0.360 ug/L 10/30/16 22:33 1Chloromethane<0.360
1.00 0.210 ug/L 10/30/16 22:33 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/30/16 22:33 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/30/16 22:33 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/30/16 22:33 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/30/16 22:33 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/30/16 22:33 1Dibromomethane<0.450
1.00 0.190 ug/L 10/30/16 22:33 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/30/16 22:33 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/30/16 22:33 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/30/16 22:33 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/30/16 22:33 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/30/16 22:33 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/30/16 22:33 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/30/16 22:33 12-Hexanone <1.28
10.0 1.50 ug/L 10/30/16 22:33 1Iodomethane<1.50
5.00 1.00 ug/L 10/30/16 22:33 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/30/16 22:33 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/30/16 22:33 1Styrene<0.280
1.00 0.150 ug/L 10/30/16 22:33 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/30/16 22:33 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/30/16 22:33 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/30/16 22:33 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/30/16 22:33 1Toluene<0.170
5.00 0.460 ug/L 10/30/16 22:33 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/30/16 22:33 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/30/16 22:33 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/30/16 22:33 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/30/16 22:33 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/30/16 22:33 1Trichloroethene<0.200
1.00 0.210 ug/L 10/30/16 22:33 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/30/16 22:33 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/30/16 22:33 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/30/16 22:33 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/30/16 22:33 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID: 490-114453-2Client Sample ID: SW-02R
Matrix: WaterDate Collected: 10/18/16 11:35
Date Received: 10/20/16 16:39
4-Bromofluorobenzene (Surr)110 70-130 10/30/16 22:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 10/30/16 22:33 170-130
1,2-Dichloroethane-d4 (Surr)123 10/30/16 22:33 170-130
Toluene-d8 (Surr)98 10/30/16 22:33 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 ^0.0100 0.00860 mg/L 10/27/16 10:24 10/30/16 06:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/27/16 10:24 10/30/16 06:21 1Barium0.0539
0.00100 0.000500 mg/L 10/27/16 10:24 10/30/16 06:21 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/27/16 10:24 10/30/16 06:21 1Chromium<0.00300
0.0100 0.00500 mg/L 10/27/16 10:24 10/30/16 06:21 1Copper<0.00500
0.00500 0.00200 mg/L 10/27/16 10:24 10/30/16 06:21 1Lead<0.00200
0.0100 0.00300 mg/L 10/27/16 10:24 10/30/16 06:21 1Nickel<0.00300
0.0100 0.00500 mg/L 10/27/16 10:24 10/30/16 06:21 1Selenium<0.00500
0.00500 0.00300 mg/L 10/27/16 10:24 10/30/16 06:21 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/27/16 10:27 10/30/16 21:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.00 0.100 ug/L 10/27/16 10:27 10/30/16 21:40 1Beryllium<0.100
2.00 0.100 ug/L 10/27/16 10:27 10/30/16 21:40 1Cobalt0.357 J
2.00 0.800 ug/L 10/27/16 10:27 10/30/16 21:40 1Thallium<0.800
2.00 0.700 ug/L 10/27/16 10:27 10/30/16 21:40 1Vanadium3.02 B
25.0 5.20 ug/L 10/27/16 10:27 10/30/16 21:40 1Zinc<5.20
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:15 10/26/16 08:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID: 490-114453-3Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/19/16 00:01
Date Received: 10/20/16 16:39
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 4.03 J 25.0 2.66 ug/L 10/31/16 15:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/31/16 15:30 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/31/16 15:30 1Benzene<0.200
1.00 0.150 ug/L 10/31/16 15:30 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/31/16 15:30 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/31/16 15:30 1Bromoform<0.290
1.00 0.350 ug/L 10/31/16 15:30 1Bromomethane<0.350 *
50.0 2.64 ug/L 10/31/16 15:30 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/31/16 15:30 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/31/16 15:30 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/31/16 15:30 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/31/16 15:30 1Chloroethane<0.360
1.00 0.230 ug/L 10/31/16 15:30 1Chloroform<0.230
1.00 0.360 ug/L 10/31/16 15:30 1Chloromethane<0.360
1.00 0.210 ug/L 10/31/16 15:30 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/31/16 15:30 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/31/16 15:30 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/31/16 15:30 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/31/16 15:30 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/31/16 15:30 1Dibromomethane<0.450
1.00 0.190 ug/L 10/31/16 15:30 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/31/16 15:30 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/31/16 15:30 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/31/16 15:30 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/31/16 15:30 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/31/16 15:30 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/31/16 15:30 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/31/16 15:30 12-Hexanone <1.28
10.0 1.50 ug/L 10/31/16 15:30 1Iodomethane<1.50
5.00 1.00 ug/L 10/31/16 15:30 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/31/16 15:30 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/31/16 15:30 1Styrene<0.280
1.00 0.150 ug/L 10/31/16 15:30 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/31/16 15:30 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/31/16 15:30 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/31/16 15:30 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/31/16 15:30 1Toluene<0.170
5.00 0.460 ug/L 10/31/16 15:30 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/31/16 15:30 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/31/16 15:30 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/31/16 15:30 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/31/16 15:30 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/31/16 15:30 1Trichloroethene<0.200
1.00 0.210 ug/L 10/31/16 15:30 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/31/16 15:30 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/31/16 15:30 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/31/16 15:30 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/31/16 15:30 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Lab Sample ID: 490-114453-3Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/19/16 00:01
Date Received: 10/20/16 16:39
4-Bromofluorobenzene (Surr)104 70-130 10/31/16 15:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)96 10/31/16 15:30 170-130
1,2-Dichloroethane-d4 (Surr)95 10/31/16 15:30 170-130
Toluene-d8 (Surr)101 10/31/16 15:30 170-130
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-382479/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/30/16 20:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 10/30/16 20:06 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/30/16 20:06 1Benzene
<0.150 0.1501.00 ug/L 10/30/16 20:06 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/30/16 20:06 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/30/16 20:06 1Bromoform
<0.350 0.3501.00 ug/L 10/30/16 20:06 1Bromomethane
<2.64 2.6450.0 ug/L 10/30/16 20:06 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/30/16 20:06 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/30/16 20:06 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/30/16 20:06 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/30/16 20:06 1Chloroethane
<0.230 0.2301.00 ug/L 10/30/16 20:06 1Chloroform
<0.360 0.3601.00 ug/L 10/30/16 20:06 1Chloromethane
<0.210 0.2101.00 ug/L 10/30/16 20:06 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/30/16 20:06 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/30/16 20:06 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/30/16 20:06 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/30/16 20:06 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/30/16 20:06 1Dibromomethane
<0.190 0.1901.00 ug/L 10/30/16 20:06 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/30/16 20:06 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/30/16 20:06 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/30/16 20:06 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/30/16 20:06 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/30/16 20:06 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/30/16 20:06 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/30/16 20:06 12-Hexanone
<1.50 1.5010.0 ug/L 10/30/16 20:06 1Iodomethane
<1.00 1.005.00 ug/L 10/30/16 20:06 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/30/16 20:06 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/30/16 20:06 1Styrene
<0.150 0.1501.00 ug/L 10/30/16 20:06 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/30/16 20:06 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/30/16 20:06 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/30/16 20:06 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/30/16 20:06 1Toluene
<0.460 0.4605.00 ug/L 10/30/16 20:06 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/30/16 20:06 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/30/16 20:06 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/30/16 20:06 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/30/16 20:06 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/30/16 20:06 1Trichloroethene
<0.210 0.2101.00 ug/L 10/30/16 20:06 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/30/16 20:06 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/30/16 20:06 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/30/16 20:06 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/30/16 20:06 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
4-Bromofluorobenzene (Surr)102 70-130 10/30/16 20:06 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
96 10/30/16 20:06 1Dibromofluoromethane (Surr)70-130
94 10/30/16 20:06 11,2-Dichloroethane-d4 (Surr)70-130
100 10/30/16 20:06 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-382479/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
Acetone 100 105.9 ug/L 106 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 204.6 ug/L 102 63-135
Benzene 20.0 19.78 ug/L 99 70-130
Bromochloromethane 20.0 19.58 ug/L 98 70-130
Bromodichloromethane 20.0 19.65 ug/L 98 70-130
Bromoform 20.0 20.21 ug/L 101 70-137
Bromomethane 20.0 28.68 ug/L 143 53-150
2-Butanone (MEK)100 98.47 ug/L 98 55-143
Carbon disulfide 20.0 21.45 ug/L 107 64-135
Carbon tetrachloride 20.0 19.21 ug/L 96 70-147
Chlorobenzene 20.0 19.68 ug/L 98 70-130
Chloroethane 20.0 20.59 ug/L 103 60-138
Chloroform 20.0 20.06 ug/L 100 70-130
Chloromethane 20.0 18.40 ug/L 92 33-150
cis-1,2-Dichloroethene 20.0 19.24 ug/L 96 70-130
cis-1,3-Dichloropropene 20.0 20.12 ug/L 101 70-133
Dibromochloromethane 20.0 19.86 ug/L 99 70-133
1,2-Dibromo-3-Chloropropane 20.0 21.00 ug/L 105 45-138
1,2-Dibromoethane (EDB)20.0 20.75 ug/L 104 70-130
Dibromomethane 20.0 20.92 ug/L 105 70-130
1,2-Dichlorobenzene 20.0 20.63 ug/L 103 70-130
1,4-Dichlorobenzene 20.0 19.93 ug/L 100 70-130
1,1-Dichloroethane 20.0 19.72 ug/L 99 70-130
1,2-Dichloroethane 20.0 20.17 ug/L 101 70-130
1,1-Dichloroethene 20.0 20.71 ug/L 104 70-132
1,2-Dichloropropane 20.0 19.42 ug/L 97 70-130
Ethylbenzene 20.0 19.39 ug/L 97 70-130
2-Hexanone 100 113.1 ug/L 113 54-142
Iodomethane 20.0 24.47 ug/L 122 40-150
Methylene Chloride 20.0 20.80 ug/L 104 70-130
4-Methyl-2-pentanone (MIBK)100 110.2 ug/L 110 60-137
Styrene 20.0 19.62 ug/L 98 70-130
1,1,1,2-Tetrachloroethane 20.0 18.64 ug/L 93 70-130
1,1,2,2-Tetrachloroethane 20.0 20.24 ug/L 101 69-131
Tetrachloroethene 20.0 20.12 ug/L 101 70-130
Tetrahydrofuran 40.0 42.19 ug/L 105 51-136
Toluene 20.0 20.14 ug/L 101 70-130
trans-1,4-Dichloro-2-butene 20.0 20.38 ug/L 102 41-150
trans-1,2-Dichloroethene 20.0 19.81 ug/L 99 70-130
trans-1,3-Dichloropropene 20.0 21.06 ug/L 105 63-142
1,1,1-Trichloroethane 20.0 19.66 ug/L 98 70-135
1,1,2-Trichloroethane 20.0 20.87 ug/L 104 70-130
Trichloroethene 20.0 19.74 ug/L 99 70-130
Trichlorofluoromethane 20.0 20.75 ug/L 104 59-150
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-382479/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
1,2,3-Trichloropropane 20.0 18.54 ug/L 93 70-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 40.0 41.81 ug/L 105 54-146
Vinyl chloride 20.0 22.04 ug/L 110 57-137
Xylenes, Total 40.0 38.42 ug/L 96 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-382479/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
Acetone 100 115.6 ug/L 116 39-150 9 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 216.6 ug/L 108 63-135 6 16
Benzene 20.0 19.31 ug/L 97 70-130 2 12
Bromochloromethane 20.0 19.46 ug/L 97 70-130 1 16
Bromodichloromethane 20.0 19.84 ug/L 99 70-130 1 14
Bromoform 20.0 20.33 ug/L 102 70-137 1 14
Bromomethane 20.0 27.77 ug/L 139 53-150 3 19
2-Butanone (MEK)100 108.5 ug/L 108 55-143 10 19
Carbon disulfide 20.0 21.04 ug/L 105 64-135 2 16
Carbon tetrachloride 20.0 18.73 ug/L 94 70-147 2 16
Chlorobenzene 20.0 19.72 ug/L 99 70-130 0 12
Chloroethane 20.0 20.31 ug/L 102 60-138 1 15
Chloroform 20.0 19.38 ug/L 97 70-130 3 14
Chloromethane 20.0 18.86 ug/L 94 33-150 2 20
cis-1,2-Dichloroethene 20.0 19.17 ug/L 96 70-130 0 15
cis-1,3-Dichloropropene 20.0 20.36 ug/L 102 70-133 1 15
Dibromochloromethane 20.0 20.01 ug/L 100 70-133 1 13
1,2-Dibromo-3-Chloropropane 20.0 21.22 ug/L 106 45-138 1 19
1,2-Dibromoethane (EDB)20.0 21.01 ug/L 105 70-130 1 13
Dibromomethane 20.0 20.90 ug/L 105 70-130 0 14
1,2-Dichlorobenzene 20.0 20.26 ug/L 101 70-130 2 12
1,4-Dichlorobenzene 20.0 19.70 ug/L 98 70-130 1 12
1,1-Dichloroethane 20.0 19.28 ug/L 96 70-130 2 17
1,2-Dichloroethane 20.0 20.47 ug/L 102 70-130 1 13
1,1-Dichloroethene 20.0 19.40 ug/L 97 70-132 7 20
1,2-Dichloropropane 20.0 18.80 ug/L 94 70-130 3 15
Ethylbenzene 20.0 19.38 ug/L 97 70-130 0 12
2-Hexanone 100 118.2 ug/L 118 54-142 4 17
Iodomethane 20.0 23.61 ug/L 118 40-150 4 20
Methylene Chloride 20.0 20.90 ug/L 105 70-130 1 15
4-Methyl-2-pentanone (MIBK)100 111.7 ug/L 112 60-137 1 21
Styrene 20.0 19.61 ug/L 98 70-130 0 12
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-382479/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
1,1,1,2-Tetrachloroethane 20.0 18.72 ug/L 94 70-130 0 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 20.0 20.28 ug/L 101 69-131 0 15
Tetrachloroethene 20.0 19.97 ug/L 100 70-130 1 17
Tetrahydrofuran 40.0 45.52 ug/L 114 51-136 8 20
Toluene 20.0 19.82 ug/L 99 70-130 2 13
trans-1,4-Dichloro-2-butene 20.0 20.03 ug/L 100 41-150 2 20
trans-1,2-Dichloroethene 20.0 19.13 ug/L 96 70-130 3 15
trans-1,3-Dichloropropene 20.0 21.09 ug/L 105 63-142 0 13
1,1,1-Trichloroethane 20.0 19.61 ug/L 98 70-135 0 15
1,1,2-Trichloroethane 20.0 20.64 ug/L 103 70-130 1 13
Trichloroethene 20.0 19.64 ug/L 98 70-130 0 14
Trichlorofluoromethane 20.0 20.39 ug/L 102 59-150 2 22
1,2,3-Trichloropropane 20.0 19.71 ug/L 99 70-131 6 14
Vinyl acetate 40.0 44.75 ug/L 112 54-146 7 20
Vinyl chloride 20.0 22.17 ug/L 111 57-137 1 15
Xylenes, Total 40.0 38.07 ug/L 95 70-132 1 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
981,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 500-118785-B-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
Acetone <133 12500 11950 ug/L 96 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <25.0 25000 23390 ug/L 94 50-135
Benzene 74.3 2500 2489 ug/L 97 55-147
Bromochloromethane <7.50 2500 2381 ug/L 95 59-132
Bromodichloromethane <8.50 2500 2364 ug/L 95 70-140
Bromoform <14.5 2500 2361 ug/L 94 53-150
Bromomethane <17.5 F1 2500 4695 F1 ug/L 188 30-150
2-Butanone (MEK)<132 12500 11190 ug/L 89 50-143
Carbon disulfide <11.0 2500 2280 ug/L 91 35-150
Carbon tetrachloride <9.00 2500 2340 ug/L 94 56-150
Chlorobenzene <9.00 2500 2403 ug/L 96 70-130
Chloroethane <18.0 2500 2355 ug/L 94 58-141
Chloroform <11.5 2500 2361 ug/L 94 66-138
Chloromethane <18.0 2500 2103 ug/L 84 10-150
cis-1,2-Dichloroethene <10.5 2500 2245 ug/L 90 68-131
cis-1,3-Dichloropropene <8.50 2500 2098 ug/L 84 70-133
Dibromochloromethane <12.5 2500 2342 ug/L 94 66-140
1,2-Dibromo-3-Chloropropane <47.0 2500 2553 ug/L 102 38-138
1,2-Dibromoethane (EDB)<10.5 2500 2492 ug/L 100 65-137
Dibromomethane <22.5 2500 2456 ug/L 98 70-130
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 500-118785-B-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
1,2-Dichlorobenzene <9.50 2500 2478 ug/L 99 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <8.50 2500 2393 ug/L 96 70-130
1,1-Dichloroethane <12.0 2500 2275 ug/L 91 61-139
1,2-Dichloroethane <10.0 2500 2362 ug/L 94 64-136
1,1-Dichloroethene <12.5 2500 2501 ug/L 100 54-150
1,2-Dichloropropane <12.5 2500 2318 ug/L 93 67-130
Ethylbenzene 619 2500 3382 ug/L 111 65-139
2-Hexanone <64.0 12500 12170 ug/L 97 44-150
Iodomethane <75.0 2500 2565 ug/L 103 34-150
Methylene Chloride <50.0 2500 2496 ug/L 100 64-130
4-Methyl-2-pentanone (MIBK)<40.5 12500 12120 ug/L 97 50-140
Styrene <14.0 2500 2325 ug/L 93 70-130
1,1,1,2-Tetrachloroethane <7.50 2500 2284 ug/L 91 70-131
1,1,2,2-Tetrachloroethane <9.50 2500 2423 ug/L 97 56-145
Tetrachloroethene <7.00 2500 2385 ug/L 95 57-138
Tetrahydrofuran <41.0 5000 3254 ug/L 65 40-136
Toluene 354 2500 2933 ug/L 103 64-136
trans-1,4-Dichloro-2-butene <23.0 2500 1935 ug/L 77 39-150
trans-1,2-Dichloroethene <11.5 2500 2167 ug/L 87 59-143
trans-1,3-Dichloropropene <8.50 2500 2187 ug/L 87 63-142
1,1,1-Trichloroethane <9.50 2500 2418 ug/L 97 68-144
1,1,2-Trichloroethane <9.50 2500 2382 ug/L 95 70-130
Trichloroethene <10.0 2500 2408 ug/L 96 63-135
Trichlorofluoromethane <10.5 2500 2427 ug/L 97 44-150
1,2,3-Trichloropropane <11.5 2500 2446 ug/L 98 65-131
Vinyl acetate <85.5 5000 4617 ug/L 92 43-146
Vinyl chloride <9.00 2500 2437 ug/L 97 57-150
Xylenes, Total 1460 5000 6876 ug/L 108 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
105
MS MS
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
981,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 500-118785-B-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
Acetone <133 12500 12000 ug/L 96 39-150 0 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <25.0 25000 23420 ug/L 94 50-135 0 23
Benzene 74.3 2500 2520 ug/L 98 55-147 1 22
Bromochloromethane <7.50 2500 2428 ug/L 97 59-132 2 21
Bromodichloromethane <8.50 2500 2425 ug/L 97 70-140 3 196
Bromoform <14.5 2500 2373 ug/L 95 53-150 1 20
Bromomethane <17.5 F1 2500 5274 F1 ug/L 211 30-150 12 44
2-Butanone (MEK)<132 12500 11040 ug/L 88 50-143 1 28
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 500-118785-B-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382479
Carbon disulfide <11.0 2500 2330 ug/L 93 35-150 2 34
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <9.00 2500 2401 ug/L 96 56-150 3 18
Chlorobenzene <9.00 2500 2459 ug/L 98 70-130 2 15
Chloroethane <18.0 2500 2382 ug/L 95 58-141 1 31
Chloroform <11.5 2500 2428 ug/L 97 66-138 3 21
Chloromethane <18.0 2500 2514 ug/L 101 10-150 18 43
cis-1,2-Dichloroethene <10.5 2500 2290 ug/L 92 68-131 2 21
cis-1,3-Dichloropropene <8.50 2500 2108 ug/L 84 70-133 1 19
Dibromochloromethane <12.5 2500 2360 ug/L 94 66-140 1 19
1,2-Dibromo-3-Chloropropane <47.0 2500 2446 ug/L 98 38-138 4 26
1,2-Dibromoethane (EDB)<10.5 2500 2505 ug/L 100 65-137 1 21
Dibromomethane <22.5 2500 2547 ug/L 102 70-130 4 19
1,2-Dichlorobenzene <9.50 2500 2484 ug/L 99 70-130 0 15
1,4-Dichlorobenzene <8.50 2500 2409 ug/L 96 70-130 1 14
1,1-Dichloroethane <12.0 2500 2307 ug/L 92 61-139 1 23
1,2-Dichloroethane <10.0 2500 2425 ug/L 97 64-136 3 22
1,1-Dichloroethene <12.5 2500 2513 ug/L 101 54-150 0 24
1,2-Dichloropropane <12.5 2500 2339 ug/L 94 67-130 1 19
Ethylbenzene 619 2500 3403 ug/L 111 65-139 1 18
2-Hexanone <64.0 12500 12220 ug/L 98 44-150 0 21
Iodomethane <75.0 2500 2834 ug/L 113 34-150 10 37
Methylene Chloride <50.0 2500 2538 ug/L 102 64 -130 2 22
4-Methyl-2-pentanone (MIBK)<40.5 12500 12260 ug/L 98 50 -140 1 24
Styrene <14.0 2500 2354 ug/L 94 70 -130 1 16
1,1,1,2-Tetrachloroethane <7.50 2500 2331 ug/L 93 70 -131 2 16
1,1,2,2-Tetrachloroethane <9.50 2500 2453 ug/L 98 56 -145 1 19
Tetrachloroethene <7.00 2500 2436 ug/L 97 57 -138 2 17
Tetrahydrofuran <41.0 5000 4227 ug/L 85 40 -136 26 27
Toluene 354 2500 2964 ug/L 104 64 -136 1 18
trans-1,4-Dichloro-2-butene <23.0 2500 2016 ug/L 81 39 -150 4 28
trans-1,2-Dichloroethene <11.5 2500 2263 ug/L 91 59 -143 4 25
trans-1,3-Dichloropropene <8.50 2500 2241 ug/L 90 63 -142 2 18
1,1,1-Trichloroethane <9.50 2500 2504 ug/L 100 68 -144 4 17
1,1,2-Trichloroethane <9.50 2500 2471 ug/L 99 70 -130 4 18
Trichloroethene <10.0 2500 2474 ug/L 99 63-135 3 17
Trichlorofluoromethane <10.5 2500 2439 ug/L 98 44-150 0 32
1,2,3-Trichloropropane <11.5 2500 2468 ug/L 99 65-131 1 19
Vinyl acetate <85.5 5000 4889 ug/L 98 43-146 6 20
Vinyl chloride <9.00 2500 2492 ug/L 100 57-150 2 37
Xylenes, Total 1460 5000 6899 ug/L 109 69-132 0 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
105
MSD MSD
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
981,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-382617/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/31/16 13:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 10/31/16 13:33 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/31/16 13:33 1Benzene
<0.150 0.1501.00 ug/L 10/31/16 13:33 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/31/16 13:33 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/31/16 13:33 1Bromoform
<0.350 0.3501.00 ug/L 10/31/16 13:33 1Bromomethane
<2.64 2.6450.0 ug/L 10/31/16 13:33 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/31/16 13:33 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/31/16 13:33 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/31/16 13:33 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/31/16 13:33 1Chloroethane
<0.230 0.2301.00 ug/L 10/31/16 13:33 1Chloroform
<0.360 0.3601.00 ug/L 10/31/16 13:33 1Chloromethane
<0.210 0.2101.00 ug/L 10/31/16 13:33 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/31/16 13:33 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/31/16 13:33 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/31/16 13:33 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/31/16 13:33 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/31/16 13:33 1Dibromomethane
<0.190 0.1901.00 ug/L 10/31/16 13:33 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/31/16 13:33 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/31/16 13:33 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/31/16 13:33 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/31/16 13:33 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/31/16 13:33 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/31/16 13:33 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/31/16 13:33 12-Hexanone
<1.50 1.5010.0 ug/L 10/31/16 13:33 1Iodomethane
<1.00 1.005.00 ug/L 10/31/16 13:33 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/31/16 13:33 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/31/16 13:33 1Styrene
<0.150 0.1501.00 ug/L 10/31/16 13:33 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/31/16 13:33 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/31/16 13:33 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/31/16 13:33 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/31/16 13:33 1Toluene
<0.460 0.4605.00 ug/L 10/31/16 13:33 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/31/16 13:33 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/31/16 13:33 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/31/16 13:33 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/31/16 13:33 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/31/16 13:33 1Trichloroethene
<0.210 0.2101.00 ug/L 10/31/16 13:33 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/31/16 13:33 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/31/16 13:33 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/31/16 13:33 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/31/16 13:33 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
4-Bromofluorobenzene (Surr)101 70-130 10/31/16 13:33 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
99 10/31/16 13:33 1Dibromofluoromethane (Surr)70-130
92 10/31/16 13:33 11,2-Dichloroethane-d4 (Surr)70-130
100 10/31/16 13:33 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-382617/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
Acetone 100 102.0 ug/L 102 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 210.8 ug/L 105 63-135
Benzene 20.0 19.88 ug/L 99 70-130
Bromochloromethane 20.0 20.35 ug/L 102 70-130
Bromodichloromethane 20.0 16.71 ug/L 84 70-130
Bromoform 20.0 19.99 ug/L 100 70-137
Bromomethane 20.0 37.68 E * ug/L 188 53-150
2-Butanone (MEK)100 100.5 ug/L 100 55-143
Carbon disulfide 20.0 20.11 ug/L 101 64-135
Carbon tetrachloride 20.0 18.85 ug/L 94 70-147
Chlorobenzene 20.0 19.99 ug/L 100 70-130
Chloroethane 20.0 19.31 ug/L 97 60-138
Chloroform 20.0 19.60 ug/L 98 70-130
Chloromethane 20.0 17.70 ug/L 89 33-150
cis-1,2-Dichloroethene 20.0 19.43 ug/L 97 70-130
cis-1,3-Dichloropropene 20.0 20.13 ug/L 101 70-133
Dibromochloromethane 20.0 19.90 ug/L 99 70-133
1,2-Dibromo-3-Chloropropane 20.0 21.47 ug/L 107 45-138
1,2-Dibromoethane (EDB)20.0 21.04 ug/L 105 70-130
Dibromomethane 20.0 20.53 ug/L 103 70-130
1,2-Dichlorobenzene 20.0 21.30 ug/L 107 70-130
1,4-Dichlorobenzene 20.0 20.32 ug/L 102 70-130
1,1-Dichloroethane 20.0 18.84 ug/L 94 70-130
1,2-Dichloroethane 20.0 19.98 ug/L 100 70-130
1,1-Dichloroethene 20.0 20.21 ug/L 101 70-132
1,2-Dichloropropane 20.0 19.74 ug/L 99 70-130
Ethylbenzene 20.0 19.69 ug/L 98 70-130
2-Hexanone 100 110.3 ug/L 110 54-142
Iodomethane 20.0 22.58 ug/L 113 40-150
Methylene Chloride 20.0 19.88 ug/L 99 70-130
4-Methyl-2-pentanone (MIBK)100 107.1 ug/L 107 60-137
Styrene 20.0 19.71 ug/L 99 70-130
1,1,1,2-Tetrachloroethane 20.0 19.09 ug/L 95 70-130
1,1,2,2-Tetrachloroethane 20.0 21.11 ug/L 106 69-131
Tetrachloroethene 20.0 20.23 ug/L 101 70-130
Tetrahydrofuran 40.0 42.30 ug/L 106 51-136
Toluene 20.0 20.30 ug/L 102 70-130
trans-1,4-Dichloro-2-butene 20.0 20.78 ug/L 104 41-150
trans-1,2-Dichloroethene 20.0 18.66 ug/L 93 70-130
trans-1,3-Dichloropropene 20.0 21.05 ug/L 105 63-142
1,1,1-Trichloroethane 20.0 19.82 ug/L 99 70-135
1,1,2-Trichloroethane 20.0 21.11 ug/L 106 70-130
Trichloroethene 20.0 19.84 ug/L 99 70-130
Trichlorofluoromethane 20.0 17.46 ug/L 87 59-150
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-382617/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
1,2,3-Trichloropropane 20.0 19.89 ug/L 99 70-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 40.0 42.49 ug/L 106 54-146
Vinyl chloride 20.0 20.01 ug/L 100 57-137
Xylenes, Total 40.0 39.19 ug/L 98 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-382617/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
Acetone 100 117.1 ug/L 117 39-150 14 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 204.7 ug/L 102 63-135 3 16
Benzene 20.0 19.61 ug/L 98 70-130 1 12
Bromochloromethane 20.0 19.88 ug/L 99 70-130 2 16
Bromodichloromethane 20.0 18.19 ug/L 91 70-130 8 14
Bromoform 20.0 19.56 ug/L 98 70-137 2 14
Bromomethane 20.0 37.23 * E ug/L 186 53-150 1 19
2-Butanone (MEK)100 103.0 ug/L 103 55-143 2 19
Carbon disulfide 20.0 19.53 ug/L 98 64-135 3 16
Carbon tetrachloride 20.0 18.38 ug/L 92 70-147 3 16
Chlorobenzene 20.0 19.84 ug/L 99 70-130 1 12
Chloroethane 20.0 18.63 ug/L 93 60-138 4 15
Chloroform 20.0 19.37 ug/L 97 70-130 1 14
Chloromethane 20.0 16.02 ug/L 80 33-150 10 20
cis-1,2-Dichloroethene 20.0 18.98 ug/L 95 70-130 2 15
cis-1,3-Dichloropropene 20.0 19.53 ug/L 98 70-133 3 15
Dibromochloromethane 20.0 19.48 ug/L 97 70-133 2 13
1,2-Dibromo-3-Chloropropane 20.0 21.82 ug/L 109 45-138 2 19
1,2-Dibromoethane (EDB)20.0 21.08 ug/L 105 70-130 0 13
Dibromomethane 20.0 20.88 ug/L 104 70-130 2 14
1,2-Dichlorobenzene 20.0 20.56 ug/L 103 70-130 4 12
1,4-Dichlorobenzene 20.0 19.50 ug/L 98 70-130 4 12
1,1-Dichloroethane 20.0 18.53 ug/L 93 70-130 2 17
1,2-Dichloroethane 20.0 20.37 ug/L 102 70-130 2 13
1,1-Dichloroethene 20.0 18.78 ug/L 94 70-132 7 20
1,2-Dichloropropane 20.0 18.96 ug/L 95 70-130 4 15
Ethylbenzene 20.0 19.02 ug/L 95 70-130 3 12
2-Hexanone 100 111.9 ug/L 112 54-142 1 17
Iodomethane 20.0 23.13 ug/L 116 40-150 2 20
Methylene Chloride 20.0 19.57 ug/L 98 70-130 2 15
4-Methyl-2-pentanone (MIBK)100 106.4 ug/L 106 60-137 1 21
Styrene 20.0 19.16 ug/L 96 70-130 3 12
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-382617/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
1,1,1,2-Tetrachloroethane 20.0 18.53 ug/L 93 70-130 3 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 20.0 20.27 ug/L 101 69-131 4 15
Tetrachloroethene 20.0 19.62 ug/L 98 70-130 3 17
Tetrahydrofuran 40.0 43.07 ug/L 108 51-136 2 20
Toluene 20.0 19.81 ug/L 99 70-130 2 13
trans-1,4-Dichloro-2-butene 20.0 19.85 ug/L 99 41-150 5 20
trans-1,2-Dichloroethene 20.0 18.43 ug/L 92 70-130 1 15
trans-1,3-Dichloropropene 20.0 20.45 ug/L 102 63-142 3 13
1,1,1-Trichloroethane 20.0 19.12 ug/L 96 70-135 4 15
1,1,2-Trichloroethane 20.0 20.95 ug/L 105 70-130 1 13
Trichloroethene 20.0 19.92 ug/L 100 70-130 0 14
Trichlorofluoromethane 20.0 17.38 ug/L 87 59-150 0 22
1,2,3-Trichloropropane 20.0 19.72 ug/L 99 70-131 1 14
Vinyl acetate 40.0 39.65 ug/L 99 54-146 7 20
Vinyl chloride 20.0 19.39 ug/L 97 57-137 3 15
Xylenes, Total 40.0 37.98 ug/L 95 70-132 3 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 280-90009-B-18 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
Acetone <13.3 1250 1302 ug/L 104 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <2.50 2500 2684 ug/L 107 50-135
Benzene 322 250 562.2 ug/L 96 55-147
Bromochloromethane <0.750 250 235.6 ug/L 94 59-132
Bromodichloromethane <0.850 250 234.8 ug/L 94 70-140
Bromoform <1.45 250 219.6 ug/L 88 53-150
Bromomethane <1.75 * F1 250 580.5 E F1 ug/L 232 30-150
2-Butanone (MEK)<13.2 1250 1217 ug/L 97 50-143
Carbon disulfide <1.10 250 253.1 ug/L 101 35-150
Carbon tetrachloride <0.900 250 251.7 ug/L 101 56-150
Chlorobenzene <0.900 250 240.0 ug/L 96 70-130
Chloroethane <1.80 250 283.3 ug/L 113 58-141
Chloroform <1.15 250 254.6 ug/L 102 66-138
Chloromethane <1.80 250 342.1 ug/L 137 10-150
cis-1,2-Dichloroethene <1.05 250 284.6 ug/L 114 68-131
cis-1,3-Dichloropropene <0.850 250 228.2 ug/L 91 70-133
Dibromochloromethane <1.25 250 225.6 ug/L 90 66-140
1,2-Dibromo-3-Chloropropane <4.70 250 218.0 ug/L 87 38-138
1,2-Dibromoethane (EDB)<1.05 250 229.8 ug/L 92 65-137
Dibromomethane <2.25 250 233.9 ug/L 94 70-130
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 280-90009-B-18 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
1,2-Dichlorobenzene <0.950 250 236.1 ug/L 94 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.850 250 236.2 ug/L 94 70-130
1,1-Dichloroethane <1.20 250 302.6 ug/L 121 61-139
1,2-Dichloroethane <1.00 250 245.1 ug/L 98 64-136
1,1-Dichloroethene <1.25 250 293.9 ug/L 118 54-150
1,2-Dichloropropane <1.25 250 227.8 ug/L 91 67-130
Ethylbenzene 213 250 462.0 ug/L 100 65-139
2-Hexanone <6.40 1250 1079 ug/L 86 44-150
Iodomethane <7.50 250 312.2 ug/L 125 34-150
Methylene Chloride <5.00 250 306.3 ug/L 123 64-130
4-Methyl-2-pentanone (MIBK)<4.05 1250 1071 ug/L 86 50-140
Styrene <1.40 250 232.9 ug/L 93 70-130
1,1,1,2-Tetrachloroethane <0.750 250 227.8 ug/L 91 70-131
1,1,2,2-Tetrachloroethane <0.950 250 217.7 ug/L 87 56-145
Tetrachloroethene <0.700 250 243.6 ug/L 97 57-138
Tetrahydrofuran <4.10 500 445.5 ug/L 89 40-136
Toluene 82.3 250 333.9 ug/L 101 64-136
trans-1,4-Dichloro-2-butene <2.30 250 228.8 ug/L 92 39-150
trans-1,2-Dichloroethene <1.15 250 274.2 ug/L 110 59-143
trans-1,3-Dichloropropene <0.850 250 237.4 ug/L 95 63-142
1,1,1-Trichloroethane <0.950 250 262.7 ug/L 105 68-144
1,1,2-Trichloroethane <0.950 250 228.0 ug/L 91 70-130
Trichloroethene <1.00 250 241.6 ug/L 97 63-135
Trichlorofluoromethane <1.05 250 304.4 ug/L 122 44-150
1,2,3-Trichloropropane <1.15 F2 F1 250 212.4 ug/L 85 65-131
Vinyl acetate <8.55 500 533.7 ug/L 107 43-146
Vinyl chloride <0.900 250 306.9 ug/L 123 57-150
Xylenes, Total 432 500 904.1 ug/L 95 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
MS MS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-90009-B-18 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
Acetone <13.3 1250 1329 ug/L 106 39-150 2 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <2.50 2500 2747 ug/L 110 50-135 2 23
Benzene 322 250 568.3 ug/L 98 55-147 1 22
Bromochloromethane <0.750 250 245.3 ug/L 98 59-132 4 21
Bromodichloromethane <0.850 250 244.2 ug/L 98 70-140 4 196
Bromoform <1.45 250 226.5 ug/L 91 53-150 3 20
Bromomethane <1.75 * F1 250 638.6 E F1 ug/L 255 30-150 10 44
2-Butanone (MEK)<13.2 1250 1205 ug/L 96 50-143 1 28
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-90009-B-18 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382617
Carbon disulfide <1.10 250 260.4 ug/L 104 35-150 3 34
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.900 250 255.8 ug/L 102 56-150 2 18
Chlorobenzene <0.900 250 241.3 ug/L 97 70-130 1 15
Chloroethane <1.80 250 288.0 ug/L 115 58-141 2 31
Chloroform <1.15 250 259.7 ug/L 104 66-138 2 21
Chloromethane <1.80 250 349.5 ug/L 140 10-150 2 43
cis-1,2-Dichloroethene <1.05 250 278.2 ug/L 111 68-131 2 21
cis-1,3-Dichloropropene <0.850 250 234.6 ug/L 94 70-133 3 19
Dibromochloromethane <1.25 250 235.8 ug/L 94 66-140 4 19
1,2-Dibromo-3-Chloropropane <4.70 250 235.9 ug/L 94 38-138 8 26
1,2-Dibromoethane (EDB)<1.05 250 235.8 ug/L 94 65-137 3 21
Dibromomethane <2.25 250 246.5 ug/L 99 70-130 5 19
1,2-Dichlorobenzene <0.950 250 244.7 ug/L 98 70-130 4 15
1,4-Dichlorobenzene <0.850 250 244.8 ug/L 98 70-130 4 14
1,1-Dichloroethane <1.20 250 313.8 ug/L 126 61-139 4 23
1,2-Dichloroethane <1.00 250 257.7 ug/L 103 64-136 5 22
1,1-Dichloroethene <1.25 250 305.2 ug/L 122 54-150 4 24
1,2-Dichloropropane <1.25 250 232.6 ug/L 93 67-130 2 19
Ethylbenzene 213 250 460.9 ug/L 99 65-139 0 18
2-Hexanone <6.40 1250 1112 ug/L 89 44-150 3 21
Iodomethane <7.50 250 349.2 ug/L 140 34-150 11 37
Methylene Chloride <5.00 250 311.5 ug/L 125 64-130 2 22
4-Methyl-2-pentanone (MIBK)<4.05 1250 1096 ug/L 88 50-140 2 24
Styrene <1.40 250 235.3 ug/L 94 70-130 1 16
1,1,1,2-Tetrachloroethane <0.750 250 234.6 ug/L 94 70-131 3 16
1,1,2,2-Tetrachloroethane <0.950 250 226.6 ug/L 91 56-145 4 19
Tetrachloroethene <0.700 250 249.1 ug/L 100 57-138 2 17
Tetrahydrofuran <4.10 500 538.5 ug/L 108 40-136 19 27
Toluene 82.3 250 333.1 ug/L 100 64-136 0 18
trans-1,4-Dichloro-2-butene <2.30 250 236.0 ug/L 94 39-150 3 28
trans-1,2-Dichloroethene <1.15 250 281.6 ug/L 113 59-143 3 25
trans-1,3-Dichloropropene <0.850 250 242.3 ug/L 97 63-142 2 18
1,1,1-Trichloroethane <0.950 250 269.7 ug/L 108 68-144 3 17
1,1,2-Trichloroethane <0.950 250 241.2 ug/L 96 70-130 6 18
Trichloroethene <1.00 250 252.3 ug/L 101 63-135 4 17
Trichlorofluoromethane <1.05 250 312.5 ug/L 125 44-150 3 32
1,2,3-Trichloropropane <1.15 F2 F1 250 224.7 ug/L 90 65-131 6 19
Vinyl acetate <8.55 500 547.2 ug/L 109 43-146 2 20
Vinyl chloride <0.900 250 310.8 ug/L 124 57-150 1 37
Xylenes, Total 432 500 909.5 ug/L 96 69-132 1 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
991,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-381681/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382504 Prep Batch: 381681
RL MDL
Arsenic <0.00860 ^0.0100 0.00860 mg/L 10/27/16 10:24 10/30/16 05:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 10/27/16 10:24 10/30/16 05:41 1Barium
<0.000500 0.0005000.00100 mg/L 10/27/16 10:24 10/30/16 05:41 1Cadmium
<0.00300 0.003000.00500 mg/L 10/27/16 10:24 10/30/16 05:41 1Chromium
<0.00500 0.005000.0100 mg/L 10/27/16 10:24 10/30/16 05:41 1Copper
<0.00200 0.002000.00500 mg/L 10/27/16 10:24 10/30/16 05:41 1Lead
<0.00300 0.003000.0100 mg/L 10/27/16 10:24 10/30/16 05:41 1Nickel
<0.00500 0.005000.0100 mg/L 10/27/16 10:24 10/30/16 05:41 1Selenium
<0.00300 0.003000.00500 mg/L 10/27/16 10:24 10/30/16 05:41 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381681/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382504 Prep Batch: 381681
Arsenic 0.0500 0.04520 ^ mg/L 90 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 1.924 mg/L 96 80-120
Cadmium 0.0500 0.05030 mg/L 101 80-120
Chromium 0.200 0.2132 mg/L 107 80-120
Copper 0.250 0.2368 mg/L 95 80-120
Lead 0.0500 0.04880 mg/L 98 80-120
Nickel 0.500 0.5101 mg/L 102 80-120
Selenium 0.0500 0.04750 mg/L 95 80-120
Silver 0.0500 0.05560 mg/L 111 80-120
Client Sample ID: SW-01Lab Sample ID: 490-114453-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382504 Prep Batch: 381681
Arsenic <0.00860 ^0.0500 0.04890 ^ mg/L 98 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0480 2.00 2.008 mg/L 98 75-125
Cadmium <0.000500 0.0500 0.05120 mg/L 102 75-125
Chromium <0.00300 0.200 0.2150 mg/L 108 75-125
Copper <0.00500 0.250 0.2399 mg/L 96 75-125
Lead <0.00200 0.0500 0.05030 mg/L 101 75-125
Nickel <0.00300 0.500 0.5156 mg/L 103 75-125
Selenium <0.00500 0.0500 0.04840 mg/L 97 75-125
Silver <0.00300 0.0500 0.05550 mg/L 111 75-125
Client Sample ID: SW-01Lab Sample ID: 490-114453-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382504 Prep Batch: 381681
Arsenic <0.00860 ^0.0500 0.04820 ^ mg/L 96 75-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0480 2.00 2.036 mg/L 99 75-125 1 20
Cadmium <0.000500 0.0500 0.05190 mg/L 104 75-125 1 20
Chromium <0.00300 0.200 0.2196 mg/L 110 75-125 2 20
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: SW-01Lab Sample ID: 490-114453-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382504 Prep Batch: 381681
Copper <0.00500 0.250 0.2434 mg/L 97 75-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Lead <0.00200 0.0500 0.05180 mg/L 104 75-125 3 20
Nickel <0.00300 0.500 0.5230 mg/L 105 75-125 1 20
Selenium <0.00500 0.0500 0.04690 mg/L 94 75-125 3 20
Silver <0.00300 0.0500 0.05660 mg/L 113 75-125 2 20
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-381692/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382571 Prep Batch: 381692
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/27/16 10:27 10/30/16 21:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.100 0.1002.00 ug/L 10/27/16 10:27 10/30/16 21:29 1Beryllium
<0.100 0.1002.00 ug/L 10/27/16 10:27 10/30/16 21:29 1Cobalt
<0.800 0.8002.00 ug/L 10/27/16 10:27 10/30/16 21:29 1Thallium
1.516 J 0.7002.00 ug/L 10/27/16 10:27 10/30/16 21:29 1Vanadium
<5.20 5.2025.0 ug/L 10/27/16 10:27 10/30/16 21:29 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381692/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382571 Prep Batch: 381692
Antimony 100 104.9 ug/L 105 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 101.6 ug/L 102 80-120
Cobalt 100 107.6 ug/L 108 80-120
Thallium 100 98.25 ug/L 98 80-120
Vanadium 100 108.0 ug/L 108 80-120
Zinc 100 94.18 ug/L 94 80-120
Client Sample ID: SW-02RLab Sample ID: 490-114453-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382571 Prep Batch: 381692
Antimony <0.800 100 106.1 ug/L 106 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <0.100 100 100.8 ug/L 101 75-125
Cobalt 0.357 J 100 109.4 ug/L 109 75-125
Thallium <0.800 100 97.14 ug/L 97 75-125
Vanadium 3.02 B 100 111.9 ug/L 109 75-125
Zinc <5.20 100 99.95 ug/L 100 75-125
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QC Sample Results
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: SW-02RLab Sample ID: 490-114453-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382571 Prep Batch: 381692
Antimony <0.800 100 105.1 ug/L 105 75-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.100 100 99.56 ug/L 100 75-125 1 20
Cobalt 0.357 J 100 105.3 ug/L 105 75-125 4 20
Thallium <0.800 100 98.42 ug/L 98 75-125 1 20
Vanadium 3.02 B 100 107.4 ug/L 104 75-125 4 20
Zinc <5.20 100 95.17 ug/L 95 75-125 5 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-380824/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380824
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/25/16 09:15 10/26/16 07:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380824/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380824
Mercury 1.00 1.130 ug/L 113 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380824/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380824
Mercury 1.00 1.002 ug/L 100 80-120 12 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-114437-A-3-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380824
Mercury <0.100 1.00 0.9938 ug/L 99 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114437-A-3-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381453 Prep Batch: 380824
Mercury <0.100 1.00 0.9605 ug/L 96 75-125 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
GC/MS VOA
Analysis Batch: 382479
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-114453-1 SW-01 Total/NA
Water 8260B490-114453-2 SW-02R Total/NA
Water 8260BMB 490-382479/7 Method Blank Total/NA
Water 8260BLCS 490-382479/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-382479/4 Lab Control Sample Dup Total/NA
Water 8260B500-118785-B-11 MS Matrix Spike Total/NA
Water 8260B500-118785-B-11 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 382617
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-114453-3 Trip Blank Total/NA
Water 8260BMB 490-382617/7 Method Blank Total/NA
Water 8260BLCS 490-382617/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-382617/4 Lab Control Sample Dup Total/NA
Water 8260B280-90009-B-18 MS Matrix Spike Total/NA
Water 8260B280-90009-B-18 MSD Matrix Spike Duplicate Total/NA
Metals
Prep Batch: 380824
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-114453-1 SW-01 Total/NA
Water 7470A490-114453-2 SW-02R Total/NA
Water 7470AMB 490-380824/1-A Method Blank Total/NA
Water 7470ALCS 490-380824/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-380824/3-A Lab Control Sample Dup Total/NA
Water 7470A490-114437-A-3-B MS Matrix Spike Total/NA
Water 7470A490-114437-A-3-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 381453
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 380824490-114453-1 SW-01 Total/NA
Water 7470A 380824490-114453-2 SW-02R Total/NA
Water 7470A 380824MB 490-380824/1-A Method Blank Total/NA
Water 7470A 380824LCS 490-380824/2-A Lab Control Sample Total/NA
Water 7470A 380824LCSD 490-380824/3-A Lab Control Sample Dup Total/NA
Water 7470A 380824490-114437-A-3-B MS Matrix Spike Total/NA
Water 7470A 380824490-114437-A-3-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 381681
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114453-1 SW-01 Total/NA
Water 3010A490-114453-2 SW-02R Total/NA
Water 3010AMB 490-381681/1-A Method Blank Total/NA
Water 3010ALCS 490-381681/2-A Lab Control Sample Total/NA
Water 3010A490-114453-1 MS SW-01 Total/NA
Water 3010A490-114453-1 MSD SW-01 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Metals (Continued)
Prep Batch: 381692
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114453-1 SW-01 Total/NA
Water 3010A490-114453-2 SW-02R Total/NA
Water 3010AMB 490-381692/1-A Method Blank Total/NA
Water 3010ALCS 490-381692/2-A Lab Control Sample Total/NA
Water 3010A490-114453-2 MS SW-02R Total/NA
Water 3010A490-114453-2 MSD SW-02R Total/NA
Analysis Batch: 382504
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 381681490-114453-1 SW-01 Total/NA
Water 6010D 381681490-114453-2 SW-02R Total/NA
Water 6010D 381681MB 490-381681/1-A Method Blank Total/NA
Water 6010D 381681LCS 490-381681/2-A Lab Control Sample Total/NA
Water 6010D 381681490-114453-1 MS SW-01 Total/NA
Water 6010D 381681490-114453-1 MSD SW-01 Total/NA
Analysis Batch: 382571
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 381692490-114453-1 SW-01 Total/NA
Water 6020B 381692490-114453-2 SW-02R Total/NA
Water 6020B 381692MB 490-381692/1-A Method Blank Total/NA
Water 6020B 381692LCS 490-381692/2-A Lab Control Sample Total/NA
Water 6020B 381692490-114453-2 MS SW-02R Total/NA
Water 6020B 381692490-114453-2 MSD SW-02R Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114453-1
Project/Site: Madison Co. Operating Landfill
Client Sample ID: SW-01 Lab Sample ID: 490-114453-1
Matrix: WaterDate Collected: 10/19/16 13:55
Date Received: 10/20/16 16:39
Analysis 8260B AK110/30/16 23:031 TAL NSH382479
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 381681 10/27/16 10:24 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 382504 10/30/16 05:56 BLG TAL NSHTotal/NA
Prep 3010A 381692 10/27/16 10:27 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 382571 10/30/16 22:07 KKK TAL NSHTotal/NA
Prep 7470A 380824 10/25/16 09:15 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/26/16 08:19 LCS TAL NSHTotal/NA
Client Sample ID: SW-02R Lab Sample ID: 490-114453-2
Matrix: WaterDate Collected: 10/18/16 11:35
Date Received: 10/20/16 16:39
Analysis 8260B AK110/30/16 22:331 TAL NSH382479
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 381681 10/27/16 10:24 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 382504 10/30/16 06:21 BLG TAL NSHTotal/NA
Prep 3010A 381692 10/27/16 10:27 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 1 382571 10/30/16 21:40 KKK TAL NSHTotal/NA
Prep 7470A 380824 10/25/16 09:15 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 381453 10/26/16 08:22 LCS TAL NSHTotal/NA
Client Sample ID: Trip Blank Lab Sample ID: 490-114453-3
Matrix: WaterDate Collected: 10/19/16 00:01
Date Received: 10/20/16 16:39
Analysis 8260B BBR10/31/16 15:301 TAL NSH382617
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-114453-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co. Operating Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114453-1
Project/Site: Madison Co. Operating Landfill
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16 *
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-114453-1
Login Number: 114453
Question Answer Comment
Creator: Ngo, Phiet
List Source: TestAmerica Nashville
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel:[phone]
TestAmerica Job ID: 490-114300-1
Client Project/Site: Madison Co Operating Landfill
For:
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
Attn: Mr. Brian Gant
Authorized for release by:
11/4/2016 5:30:09 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
TestAmerica Job ID: 490-114300-1
Page 2 of 36 TestAmerica Nashville11/4/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
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Sample Summary
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-114300-1 LT-01 Water 10/18/16 13:45 10/19/16 09:20
490-114300-2 Trip Blank Water 10/18/16 01:01 10/19/16 09:20
TestAmerica Nashville
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Case Narrative
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114300-1
Project/Site: Madison Co Operating Landfill
Job ID: 490-114300-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-114300-1
Comments
No additional comments.
Receipt
The samples were received on 10/19/2016 9:20 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 1.3º C.
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
HPLC/IC
Method 300.0, 9056: The following sample was diluted due to the nature of the sample matrix: LT-01 (490-114300-1). Elevated reporting
limits (RLs) are provided.
Method 300.0, 9056: Due to sample matrix, matrix spike/ matrix spike duplicate (MS/MSD) was not analyzed with batch 490-380814.
However, the laboratory control sample/ laboratory control sample duplicate (LCS/LCSD) recoveries were within acceptance limits. (LCS
490-380814/4) and (LCSD 490-380814/5)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method SM 5220D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 490-381445#381445 were outside
control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample
(LCS) recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Qualifiers
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
F2 MS/MSD RPD exceeds control limits
General Chemistry
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114300-1Client Sample ID: LT-01
Matrix: WaterDate Collected: 10/18/16 13:45
Date Received: 10/19/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/25/16 19:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/25/16 19:22 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/25/16 19:22 1Benzene<0.200
1.00 0.150 ug/L 10/25/16 19:22 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/25/16 19:22 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/25/16 19:22 1Bromoform<0.290
1.00 0.350 ug/L 10/25/16 19:22 1Bromomethane<0.350
50.0 2.64 ug/L 10/25/16 19:22 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/25/16 19:22 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/25/16 19:22 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/25/16 19:22 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/25/16 19:22 1Chloroethane<0.360
1.00 0.230 ug/L 10/25/16 19:22 1Chloroform<0.230
1.00 0.360 ug/L 10/25/16 19:22 1Chloromethane<0.360
1.00 0.210 ug/L 10/25/16 19:22 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/25/16 19:22 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/25/16 19:22 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/25/16 19:22 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/25/16 19:22 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/25/16 19:22 1Dibromomethane<0.450
1.00 0.190 ug/L 10/25/16 19:22 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/25/16 19:22 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/25/16 19:22 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/25/16 19:22 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/25/16 19:22 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/25/16 19:22 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/25/16 19:22 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/25/16 19:22 12-Hexanone <1.28
10.0 1.50 ug/L 10/25/16 19:22 1Iodomethane<1.50
5.00 1.00 ug/L 10/25/16 19:22 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/25/16 19:22 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/25/16 19:22 1Styrene<0.280
1.00 0.150 ug/L 10/25/16 19:22 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/25/16 19:22 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/25/16 19:22 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/25/16 19:22 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/25/16 19:22 1Toluene<0.170
5.00 0.460 ug/L 10/25/16 19:22 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/25/16 19:22 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/25/16 19:22 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/25/16 19:22 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/25/16 19:22 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/25/16 19:22 1Trichloroethene<0.200
1.00 0.210 ug/L 10/25/16 19:22 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/25/16 19:22 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/25/16 19:22 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/25/16 19:22 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/25/16 19:22 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114300-1Client Sample ID: LT-01
Matrix: WaterDate Collected: 10/18/16 13:45
Date Received: 10/19/16 09:20
4-Bromofluorobenzene (Surr)88 70-130 10/25/16 19:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 10/25/16 19:22 170-130
1,2-Dichloroethane-d4 (Surr)102 10/25/16 19:22 170-130
Toluene-d8 (Surr)98 10/25/16 19:22 170-130
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Sulfate 133 10.0 6.00 mg/L 10/22/16 18:39 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/25/16 10:57 10/30/16 10:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00500 mg/L 10/25/16 10:57 10/30/16 10:38 1Barium0.793
0.00100 0.000500 mg/L 10/25/16 10:57 10/30/16 10:38 1Cadmium<0.000500
0.00500 0.00300 mg/L 10/25/16 10:57 10/30/16 10:38 1Chromium0.0249
0.0100 0.00500 mg/L 10/25/16 10:57 10/30/16 10:38 1Copper0.0106
0.00500 0.00200 mg/L 10/25/16 10:57 10/30/16 10:38 1Lead<0.00200
0.0100 0.00300 mg/L 10/25/16 10:57 10/30/16 10:38 1Nickel0.0624
0.0100 0.00500 mg/L 10/25/16 10:57 10/30/16 10:38 1Selenium0.00900 J
0.00500 0.00300 mg/L 10/25/16 10:57 10/30/16 10:38 1Silver<0.00300
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony <4.00 10.0 4.00 ug/L 10/25/16 11:03 10/31/16 22:09 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/25/16 11:03 10/31/16 22:09 5Beryllium1.13 J
10.0 0.500 ug/L 10/25/16 11:03 10/31/16 22:09 5Cobalt83.2
10.0 4.00 ug/L 10/25/16 11:03 10/31/16 22:09 5Thallium<4.00
10.0 3.50 ug/L 10/25/16 11:03 10/31/16 22:09 5Vanadium100 B
125 26.0 ug/L 10/25/16 11:03 11/03/16 20:50 5Zinc402
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/21/16 08:31 10/21/16 17:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Phosphorus, Total 0.664 0.100 0.0500 mg/L 10/26/16 14:09 10/26/16 18:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.100 0.0400 mg/L 10/19/16 13:11 1Nitrate as N 42.0
20.0 4.00 mg/L 10/26/16 15:02 1Chemical Oxygen Demand 117
RL RL
Biochemical Oxygen Demand 4.51 2.00 2.00 mg/L 10/19/16 18:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114300-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/18/16 01:01
Date Received: 10/19/16 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/26/16 03:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10.0 0.500 ug/L 10/26/16 03:57 1Acrylonitrile<0.500
1.00 0.200 ug/L 10/26/16 03:57 1Benzene<0.200
1.00 0.150 ug/L 10/26/16 03:57 1Bromochloromethane<0.150
1.00 0.170 ug/L 10/26/16 03:57 1Bromodichloromethane<0.170
1.00 0.290 ug/L 10/26/16 03:57 1Bromoform<0.290
1.00 0.350 ug/L 10/26/16 03:57 1Bromomethane<0.350
50.0 2.64 ug/L 10/26/16 03:57 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 10/26/16 03:57 1Carbon disulfide <0.220
1.00 0.180 ug/L 10/26/16 03:57 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 10/26/16 03:57 1Chlorobenzene<0.180
1.00 0.360 ug/L 10/26/16 03:57 1Chloroethane<0.360
1.00 0.230 ug/L 10/26/16 03:57 1Chloroform<0.230
1.00 0.360 ug/L 10/26/16 03:57 1Chloromethane<0.360
1.00 0.210 ug/L 10/26/16 03:57 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 10/26/16 03:57 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 10/26/16 03:57 1Dibromochloromethane<0.250
10.0 0.940 ug/L 10/26/16 03:57 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 10/26/16 03:57 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 10/26/16 03:57 1Dibromomethane<0.450
1.00 0.190 ug/L 10/26/16 03:57 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 10/26/16 03:57 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 10/26/16 03:57 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 10/26/16 03:57 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 10/26/16 03:57 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 10/26/16 03:57 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 10/26/16 03:57 1Ethylbenzene<0.190
10.0 1.28 ug/L 10/26/16 03:57 12-Hexanone <1.28
10.0 1.50 ug/L 10/26/16 03:57 1Iodomethane<1.50
5.00 1.00 ug/L 10/26/16 03:57 1Methylene Chloride <1.00
10.0 0.810 ug/L 10/26/16 03:57 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 10/26/16 03:57 1Styrene<0.280
1.00 0.150 ug/L 10/26/16 03:57 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 10/26/16 03:57 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 10/26/16 03:57 1Tetrachloroethene<0.140
10.0 0.820 ug/L 10/26/16 03:57 1Tetrahydrofuran<0.820
1.00 0.170 ug/L 10/26/16 03:57 1Toluene<0.170
5.00 0.460 ug/L 10/26/16 03:57 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 10/26/16 03:57 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 10/26/16 03:57 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 10/26/16 03:57 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 10/26/16 03:57 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 10/26/16 03:57 1Trichloroethene<0.200
1.00 0.210 ug/L 10/26/16 03:57 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 10/26/16 03:57 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 10/26/16 03:57 1Vinyl acetate <1.71
1.00 0.180 ug/L 10/26/16 03:57 1Vinyl chloride <0.180
3.00 0.580 ug/L 10/26/16 03:57 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Lab Sample ID: 490-114300-2Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/18/16 01:01
Date Received: 10/19/16 09:20
4-Bromofluorobenzene (Surr)89 70-130 10/26/16 03:57 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 10/26/16 03:57 170-130
1,2-Dichloroethane-d4 (Surr)103 10/26/16 03:57 170-130
Toluene-d8 (Surr)96 10/26/16 03:57 170-130
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-380978/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/25/16 15:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 10/25/16 15:05 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/25/16 15:05 1Benzene
<0.150 0.1501.00 ug/L 10/25/16 15:05 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/25/16 15:05 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/25/16 15:05 1Bromoform
<0.350 0.3501.00 ug/L 10/25/16 15:05 1Bromomethane
<2.64 2.6450.0 ug/L 10/25/16 15:05 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/25/16 15:05 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/25/16 15:05 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/25/16 15:05 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/25/16 15:05 1Chloroethane
<0.230 0.2301.00 ug/L 10/25/16 15:05 1Chloroform
<0.360 0.3601.00 ug/L 10/25/16 15:05 1Chloromethane
<0.210 0.2101.00 ug/L 10/25/16 15:05 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/25/16 15:05 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/25/16 15:05 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/25/16 15:05 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/25/16 15:05 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/25/16 15:05 1Dibromomethane
<0.190 0.1901.00 ug/L 10/25/16 15:05 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/25/16 15:05 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/25/16 15:05 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/25/16 15:05 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/25/16 15:05 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/25/16 15:05 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/25/16 15:05 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/25/16 15:05 12-Hexanone
<1.50 1.5010.0 ug/L 10/25/16 15:05 1Iodomethane
<1.00 1.005.00 ug/L 10/25/16 15:05 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/25/16 15:05 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/25/16 15:05 1Styrene
<0.150 0.1501.00 ug/L 10/25/16 15:05 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/25/16 15:05 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/25/16 15:05 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/25/16 15:05 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/25/16 15:05 1Toluene
<0.460 0.4605.00 ug/L 10/25/16 15:05 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/25/16 15:05 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/25/16 15:05 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/25/16 15:05 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/25/16 15:05 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/25/16 15:05 1Trichloroethene
<0.210 0.2101.00 ug/L 10/25/16 15:05 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/25/16 15:05 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/25/16 15:05 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/25/16 15:05 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/25/16 15:05 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
4-Bromofluorobenzene (Surr)89 70-130 10/25/16 15:05 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
99 10/25/16 15:05 1Dibromofluoromethane (Surr)70-130
104 10/25/16 15:05 11,2-Dichloroethane-d4 (Surr)70-130
96 10/25/16 15:05 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380978/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
Acetone 100 90.37 ug/L 90 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 181.7 ug/L 91 63-135
Benzene 20.0 18.84 ug/L 94 70-130
Bromochloromethane 20.0 20.75 ug/L 104 70-130
Bromodichloromethane 20.0 18.86 ug/L 94 70-130
Bromoform 20.0 19.09 ug/L 95 70-137
Bromomethane 20.0 22.16 ug/L 111 53-150
2-Butanone (MEK)100 95.62 ug/L 96 55-143
Carbon disulfide 20.0 18.68 ug/L 93 64-135
Carbon tetrachloride 20.0 19.59 ug/L 98 70-147
Chlorobenzene 20.0 20.15 ug/L 101 70-130
Chloroethane 20.0 18.52 ug/L 93 60-138
Chloroform 20.0 20.57 ug/L 103 70-130
Chloromethane 20.0 16.50 ug/L 83 33-150
cis-1,2-Dichloroethene 20.0 19.58 ug/L 98 70-130
cis-1,3-Dichloropropene 20.0 18.18 ug/L 91 70-133
Dibromochloromethane 20.0 19.63 ug/L 98 70-133
1,2-Dibromo-3-Chloropropane 20.0 17.56 ug/L 88 45-138
1,2-Dibromoethane (EDB)20.0 19.48 ug/L 97 70-130
Dibromomethane 20.0 19.98 ug/L 100 70-130
1,2-Dichlorobenzene 20.0 20.78 ug/L 104 70-130
1,4-Dichlorobenzene 20.0 20.12 ug/L 101 70-130
1,1-Dichloroethane 20.0 20.50 ug/L 103 70-130
1,2-Dichloroethane 20.0 21.34 ug/L 107 70-130
1,1-Dichloroethene 20.0 21.13 ug/L 106 70-132
1,2-Dichloropropane 20.0 17.89 ug/L 89 70-130
Ethylbenzene 20.0 18.39 ug/L 92 70-130
2-Hexanone 100 83.47 ug/L 83 54-142
Iodomethane 20.0 21.71 ug/L 109 40-150
Methylene Chloride 20.0 20.03 ug/L 100 70-130
4-Methyl-2-pentanone (MIBK)100 88.02 ug/L 88 60-137
Styrene 20.0 19.72 ug/L 99 70-130
1,1,1,2-Tetrachloroethane 20.0 20.27 ug/L 101 70-130
1,1,2,2-Tetrachloroethane 20.0 17.70 ug/L 89 69-131
Tetrachloroethene 20.0 20.08 ug/L 100 70-130
Tetrahydrofuran 40.0 37.26 ug/L 93 51-136
Toluene 20.0 18.24 ug/L 91 70-130
trans-1,4-Dichloro-2-butene 20.0 17.95 ug/L 90 41-150
trans-1,2-Dichloroethene 20.0 19.66 ug/L 98 70-130
trans-1,3-Dichloropropene 20.0 19.11 ug/L 96 63-142
1,1,1-Trichloroethane 20.0 19.20 ug/L 96 70-135
1,1,2-Trichloroethane 20.0 18.59 ug/L 93 70-130
Trichloroethene 20.0 19.30 ug/L 96 70-130
Trichlorofluoromethane 20.0 22.26 ug/L 111 59-150
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380978/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
1,2,3-Trichloropropane 20.0 19.84 ug/L 99 70-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 40.0 42.39 ug/L 106 54-146
Vinyl chloride 20.0 19.08 ug/L 95 57-137
Xylenes, Total 40.0 39.07 ug/L 98 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1041,2-Dichloroethane-d4 (Surr)70 -130
91Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380978/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
Acetone 100 84.51 ug/L 85 39-150 7 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 178.7 ug/L 89 63-135 2 16
Benzene 20.0 18.38 ug/L 92 70-130 2 12
Bromochloromethane 20.0 20.19 ug/L 101 70-130 3 16
Bromodichloromethane 20.0 18.21 ug/L 91 70-130 3 14
Bromoform 20.0 18.88 ug/L 94 70-137 1 14
Bromomethane 20.0 21.64 ug/L 108 53-150 2 19
2-Butanone (MEK)100 93.60 ug/L 94 55-143 2 19
Carbon disulfide 20.0 17.54 ug/L 88 64-135 6 16
Carbon tetrachloride 20.0 18.74 ug/L 94 70-147 4 16
Chlorobenzene 20.0 19.69 ug/L 98 70-130 2 12
Chloroethane 20.0 17.65 ug/L 88 60-138 5 15
Chloroform 20.0 19.99 ug/L 100 70-130 3 14
Chloromethane 20.0 15.06 ug/L 75 33-150 9 20
cis-1,2-Dichloroethene 20.0 18.98 ug/L 95 70-130 3 15
cis-1,3-Dichloropropene 20.0 18.54 ug/L 93 70-133 2 15
Dibromochloromethane 20.0 19.41 ug/L 97 70-133 1 13
1,2-Dibromo-3-Chloropropane 20.0 17.04 ug/L 85 45-138 3 19
1,2-Dibromoethane (EDB)20.0 19.63 ug/L 98 70-130 1 13
Dibromomethane 20.0 19.41 ug/L 97 70-130 3 14
1,2-Dichlorobenzene 20.0 20.47 ug/L 102 70-130 2 12
1,4-Dichlorobenzene 20.0 19.82 ug/L 99 70-130 1 12
1,1-Dichloroethane 20.0 19.41 ug/L 97 70-130 5 17
1,2-Dichloroethane 20.0 20.76 ug/L 104 70-130 3 13
1,1-Dichloroethene 20.0 18.90 ug/L 94 70-132 11 20
1,2-Dichloropropane 20.0 17.35 ug/L 87 70-130 3 15
Ethylbenzene 20.0 18.19 ug/L 91 70-130 1 12
2-Hexanone 100 81.26 ug/L 81 54-142 3 17
Iodomethane 20.0 21.37 ug/L 107 40-150 2 20
Methylene Chloride 20.0 18.99 ug/L 95 70-130 5 15
4-Methyl-2-pentanone (MIBK)100 88.50 ug/L 88 60-137 1 21
Styrene 20.0 19.37 ug/L 97 70-130 2 12
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380978/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
1,1,1,2-Tetrachloroethane 20.0 19.84 ug/L 99 70-130 2 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 20.0 17.55 ug/L 88 69-131 1 15
Tetrachloroethene 20.0 20.03 ug/L 100 70-130 0 17
Tetrahydrofuran 40.0 32.21 ug/L 81 51-136 15 20
Toluene 20.0 18.09 ug/L 90 70-130 1 13
trans-1,4-Dichloro-2-butene 20.0 16.93 ug/L 85 41-150 6 20
trans-1,2-Dichloroethene 20.0 19.04 ug/L 95 70-130 3 15
trans-1,3-Dichloropropene 20.0 19.67 ug/L 98 63-142 3 13
1,1,1-Trichloroethane 20.0 18.40 ug/L 92 70-135 4 15
1,1,2-Trichloroethane 20.0 18.96 ug/L 95 70-130 2 13
Trichloroethene 20.0 19.25 ug/L 96 70-130 0 14
Trichlorofluoromethane 20.0 21.55 ug/L 108 59-150 3 22
1,2,3-Trichloropropane 20.0 18.96 ug/L 95 70-131 5 14
Vinyl acetate 40.0 40.28 ug/L 101 54-146 5 20
Vinyl chloride 20.0 18.01 ug/L 90 57-137 6 15
Xylenes, Total 40.0 38.53 ug/L 96 70-132 1 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
90
LCSD LCSD
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Client Sample ID: LT-01Lab Sample ID: 490-114300-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
Acetone <2.66 100 83.06 ug/L 83 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 173.8 ug/L 87 50-135
Benzene <0.200 20.0 19.68 ug/L 98 55-147
Bromochloromethane <0.150 20.0 21.28 ug/L 106 59-132
Bromodichloromethane <0.170 20.0 19.08 ug/L 95 70-140
Bromoform <0.290 20.0 18.31 ug/L 92 53-150
Bromomethane <0.350 20.0 21.70 ug/L 109 30-150
2-Butanone (MEK)<2.64 100 89.51 ug/L 90 50-143
Carbon disulfide <0.220 20.0 19.11 ug/L 96 35-150
Carbon tetrachloride <0.180 20.0 21.62 ug/L 108 56-150
Chlorobenzene <0.180 20.0 20.53 ug/L 103 70-130
Chloroethane <0.360 20.0 18.66 ug/L 93 58-141
Chloroform <0.230 20.0 21.52 ug/L 108 66-138
Chloromethane <0.360 20.0 16.30 ug/L 81 10-150
cis-1,2-Dichloroethene <0.210 20.0 20.09 ug/L 100 68-131
cis-1,3-Dichloropropene <0.170 20.0 18.35 ug/L 92 70-133
Dibromochloromethane <0.250 20.0 19.07 ug/L 95 66-140
1,2-Dibromo-3-Chloropropane <0.940 20.0 16.55 ug/L 83 38-138
1,2-Dibromoethane (EDB)<0.210 20.0 18.78 ug/L 94 65-137
Dibromomethane <0.450 20.0 19.98 ug/L 100 70-130
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: LT-01Lab Sample ID: 490-114300-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
1,2-Dichlorobenzene <0.190 20.0 20.59 ug/L 103 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 20.0 20.10 ug/L 100 70-130
1,1-Dichloroethane <0.240 20.0 21.06 ug/L 105 61-139
1,2-Dichloroethane <0.200 20.0 21.68 ug/L 108 64-136
1,1-Dichloroethene <0.250 20.0 22.57 ug/L 113 54-150
1,2-Dichloropropane <0.250 20.0 18.48 ug/L 92 67-130
Ethylbenzene <0.190 20.0 18.91 ug/L 95 65-139
2-Hexanone <1.28 100 80.88 ug/L 81 44-150
Iodomethane <1.50 20.0 22.45 ug/L 112 34-150
Methylene Chloride <1.00 20.0 19.47 ug/L 97 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 86.11 ug/L 86 50-140
Styrene <0.280 20.0 20.09 ug/L 100 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 20.50 ug/L 103 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 17.33 ug/L 87 56-145
Tetrachloroethene <0.140 20.0 21.05 ug/L 105 57-138
Tetrahydrofuran <0.820 40.0 36.29 ug/L 91 40-136
Toluene <0.170 20.0 19.03 ug/L 95 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 17.56 ug/L 88 39-150
trans-1,2-Dichloroethene <0.230 20.0 20.59 ug/L 103 59-143
trans-1,3-Dichloropropene <0.170 20.0 18.91 ug/L 95 63-142
1,1,1-Trichloroethane <0.190 20.0 20.51 ug/L 103 68-144
1,1,2-Trichloroethane <0.190 20.0 18.01 ug/L 90 70-130
Trichloroethene <0.200 20.0 20.70 ug/L 104 63-135
Trichlorofluoromethane <0.210 20.0 24.99 ug/L 125 44-150
1,2,3-Trichloropropane <0.230 20.0 19.61 ug/L 98 65-131
Vinyl acetate <1.71 40.0 40.00 ug/L 100 43-146
Vinyl chloride <0.180 20.0 19.38 ug/L 97 57-150
Xylenes, Total <0.580 40.0 39.98 ug/L 100 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
MS MS
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
1021,2-Dichloroethane-d4 (Surr)70 -130
92Toluene-d8 (Surr)70 -130
Client Sample ID: LT-01Lab Sample ID: 490-114300-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
Acetone <2.66 100 87.65 ug/L 88 39-150 5 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 183.1 ug/L 92 50-135 5 23
Benzene <0.200 20.0 20.77 ug/L 104 55-147 5 22
Bromochloromethane <0.150 20.0 21.84 ug/L 109 59-132 3 21
Bromodichloromethane <0.170 20.0 20.31 ug/L 102 70-140 6 196
Bromoform <0.290 20.0 20.02 ug/L 100 53-150 9 20
Bromomethane <0.350 20.0 24.28 ug/L 121 30-150 11 44
2-Butanone (MEK)<2.64 100 93.32 ug/L 93 50-143 4 28
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: LT-01Lab Sample ID: 490-114300-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380978
Carbon disulfide <0.220 20.0 21.21 ug/L 106 35-150 10 34
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 20.0 22.40 ug/L 112 56-150 4 18
Chlorobenzene <0.180 20.0 22.25 ug/L 111 70-130 8 15
Chloroethane <0.360 20.0 20.30 ug/L 101 58-141 8 31
Chloroform <0.230 20.0 23.00 ug/L 115 66-138 7 21
Chloromethane <0.360 20.0 17.75 ug/L 89 10-150 9 43
cis-1,2-Dichloroethene <0.210 20.0 21.47 ug/L 107 68-131 7 21
cis-1,3-Dichloropropene <0.170 20.0 20.31 ug/L 102 70-133 10 19
Dibromochloromethane <0.250 20.0 20.83 ug/L 104 66 -140 9 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 18.40 ug/L 92 38 -138 11 26
1,2-Dibromoethane (EDB)<0.210 20.0 20.48 ug/L 102 65 -137 9 21
Dibromomethane <0.450 20.0 21.52 ug/L 108 70 -130 7 19
1,2-Dichlorobenzene <0.190 20.0 22.38 ug/L 112 70 -130 8 15
1,4-Dichlorobenzene <0.170 20.0 21.56 ug/L 108 70 -130 7 14
1,1-Dichloroethane <0.240 20.0 22.41 ug/L 112 61 -139 6 23
1,2-Dichloroethane <0.200 20.0 22.63 ug/L 113 64 -136 4 22
1,1-Dichloroethene <0.250 20.0 24.25 ug/L 121 54 -150 7 24
1,2-Dichloropropane <0.250 20.0 19.22 ug/L 96 67 -130 4 19
Ethylbenzene <0.190 20.0 20.69 ug/L 103 65 -139 9 18
2-Hexanone <1.28 100 86.05 ug/L 86 44 -150 6 21
Iodomethane <1.50 20.0 23.97 ug/L 120 34 -150 7 37
Methylene Chloride <1.00 20.0 20.66 ug/L 103 64 -130 6 22
4-Methyl-2-pentanone (MIBK)<0.810 100 91.20 ug/L 91 50 -140 6 24
Styrene <0.280 20.0 21.51 ug/L 108 70 -130 7 16
1,1,1,2-Tetrachloroethane <0.150 20.0 22.62 ug/L 113 70 -131 10 16
1,1,2,2-Tetrachloroethane <0.190 20.0 18.43 ug/L 92 56 -145 6 19
Tetrachloroethene <0.140 20.0 22.71 ug/L 114 57 -138 8 17
Tetrahydrofuran <0.820 40.0 41.69 ug/L 104 40 -136 14 27
Toluene <0.170 20.0 20.66 ug/L 103 64 -136 8 18
trans-1,4-Dichloro-2-butene <0.460 20.0 18.35 ug/L 92 39 -150 4 28
trans-1,2-Dichloroethene <0.230 20.0 21.94 ug/L 110 59 -143 6 25
trans-1,3-Dichloropropene <0.170 20.0 20.70 ug/L 104 63 -142 9 18
1,1,1-Trichloroethane <0.190 20.0 21.95 ug/L 110 68 -144 7 17
1,1,2-Trichloroethane <0.190 20.0 19.58 ug/L 98 70 -130 8 18
Trichloroethene <0.200 20.0 22.01 ug/L 110 63-135 6 17
Trichlorofluoromethane <0.210 20.0 26.69 ug/L 133 44-150 7 32
1,2,3-Trichloropropane <0.230 20.0 20.26 ug/L 101 65-131 3 19
Vinyl acetate <1.71 40.0 42.38 ug/L 106 43-146 6 20
Vinyl chloride <0.180 20.0 21.42 ug/L 107 57-150 10 37
Xylenes, Total <0.580 40.0 43.53 ug/L 109 69-132 9 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
89
MSD MSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
92Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-381094/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
RL MDL
Acetone <2.66 25.0 2.66 ug/L 10/26/16 03:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.500 0.50010.0 ug/L 10/26/16 03:28 1Acrylonitrile
<0.200 0.2001.00 ug/L 10/26/16 03:28 1Benzene
<0.150 0.1501.00 ug/L 10/26/16 03:28 1Bromochloromethane
<0.170 0.1701.00 ug/L 10/26/16 03:28 1Bromodichloromethane
<0.290 0.2901.00 ug/L 10/26/16 03:28 1Bromoform
<0.350 0.3501.00 ug/L 10/26/16 03:28 1Bromomethane
<2.64 2.6450.0 ug/L 10/26/16 03:28 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 10/26/16 03:28 1Carbon disulfide
<0.180 0.1801.00 ug/L 10/26/16 03:28 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 10/26/16 03:28 1Chlorobenzene
<0.360 0.3601.00 ug/L 10/26/16 03:28 1Chloroethane
<0.230 0.2301.00 ug/L 10/26/16 03:28 1Chloroform
<0.360 0.3601.00 ug/L 10/26/16 03:28 1Chloromethane
<0.210 0.2101.00 ug/L 10/26/16 03:28 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/26/16 03:28 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 10/26/16 03:28 1Dibromochloromethane
<0.940 0.94010.0 ug/L 10/26/16 03:28 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 10/26/16 03:28 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 10/26/16 03:28 1Dibromomethane
<0.190 0.1901.00 ug/L 10/26/16 03:28 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 10/26/16 03:28 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 10/26/16 03:28 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 10/26/16 03:28 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 10/26/16 03:28 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 10/26/16 03:28 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 10/26/16 03:28 1Ethylbenzene
<1.28 1.2810.0 ug/L 10/26/16 03:28 12-Hexanone
<1.50 1.5010.0 ug/L 10/26/16 03:28 1Iodomethane
<1.00 1.005.00 ug/L 10/26/16 03:28 1Methylene Chloride
<0.810 0.81010.0 ug/L 10/26/16 03:28 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 10/26/16 03:28 1Styrene
<0.150 0.1501.00 ug/L 10/26/16 03:28 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 10/26/16 03:28 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 10/26/16 03:28 1Tetrachloroethene
<0.820 0.82010.0 ug/L 10/26/16 03:28 1Tetrahydrofuran
<0.170 0.1701.00 ug/L 10/26/16 03:28 1Toluene
<0.460 0.4605.00 ug/L 10/26/16 03:28 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 10/26/16 03:28 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 10/26/16 03:28 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 10/26/16 03:28 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 10/26/16 03:28 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 10/26/16 03:28 1Trichloroethene
<0.210 0.2101.00 ug/L 10/26/16 03:28 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 10/26/16 03:28 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 10/26/16 03:28 1Vinyl acetate
<0.180 0.1801.00 ug/L 10/26/16 03:28 1Vinyl chloride
<0.580 0.5803.00 ug/L 10/26/16 03:28 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
4-Bromofluorobenzene (Surr)89 70-130 10/26/16 03:28 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
98 10/26/16 03:28 1Dibromofluoromethane (Surr)70-130
97 10/26/16 03:28 11,2-Dichloroethane-d4 (Surr)70-130
94 10/26/16 03:28 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381094/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
Acetone 100 84.66 ug/L 85 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 181.8 ug/L 91 63-135
Benzene 20.0 18.91 ug/L 95 70-130
Bromochloromethane 20.0 20.81 ug/L 104 70-130
Bromodichloromethane 20.0 18.45 ug/L 92 70-130
Bromoform 20.0 18.99 ug/L 95 70-137
Bromomethane 20.0 22.12 ug/L 111 53-150
2-Butanone (MEK)100 92.98 ug/L 93 55-143
Carbon disulfide 20.0 18.77 ug/L 94 64-135
Carbon tetrachloride 20.0 19.74 ug/L 99 70-147
Chlorobenzene 20.0 19.88 ug/L 99 70-130
Chloroethane 20.0 18.04 ug/L 90 60-138
Chloroform 20.0 20.72 ug/L 104 70-130
Chloromethane 20.0 15.84 ug/L 79 33-150
cis-1,2-Dichloroethene 20.0 19.81 ug/L 99 70-130
cis-1,3-Dichloropropene 20.0 18.47 ug/L 92 70-133
Dibromochloromethane 20.0 19.50 ug/L 98 70-133
1,2-Dibromo-3-Chloropropane 20.0 18.37 ug/L 92 45-138
1,2-Dibromoethane (EDB)20.0 19.40 ug/L 97 70-130
Dibromomethane 20.0 19.97 ug/L 100 70-130
1,2-Dichlorobenzene 20.0 20.47 ug/L 102 70-130
1,4-Dichlorobenzene 20.0 19.88 ug/L 99 70-130
1,1-Dichloroethane 20.0 20.10 ug/L 100 70-130
1,2-Dichloroethane 20.0 21.80 ug/L 109 70-130
1,1-Dichloroethene 20.0 20.78 ug/L 104 70-132
1,2-Dichloropropane 20.0 17.95 ug/L 90 70-130
Ethylbenzene 20.0 18.61 ug/L 93 70-130
2-Hexanone 100 84.98 ug/L 85 54-142
Iodomethane 20.0 22.15 ug/L 111 40-150
Methylene Chloride 20.0 20.14 ug/L 101 70-130
4-Methyl-2-pentanone (MIBK)100 88.53 ug/L 89 60-137
Styrene 20.0 19.80 ug/L 99 70-130
1,1,1,2-Tetrachloroethane 20.0 20.07 ug/L 100 70-130
1,1,2,2-Tetrachloroethane 20.0 17.61 ug/L 88 69-131
Tetrachloroethene 20.0 19.83 ug/L 99 70-130
Tetrahydrofuran 40.0 38.90 ug/L 97 51-136
Toluene 20.0 18.51 ug/L 93 70-130
trans-1,4-Dichloro-2-butene 20.0 16.98 ug/L 85 41-150
trans-1,2-Dichloroethene 20.0 19.56 ug/L 98 70-130
trans-1,3-Dichloropropene 20.0 18.92 ug/L 95 63-142
1,1,1-Trichloroethane 20.0 19.06 ug/L 95 70-135
1,1,2-Trichloroethane 20.0 18.28 ug/L 91 70-130
Trichloroethene 20.0 19.47 ug/L 97 70-130
Trichlorofluoromethane 20.0 22.26 ug/L 111 59-150
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381094/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
1,2,3-Trichloropropane 20.0 19.82 ug/L 99 70-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 40.0 40.60 ug/L 101 54-146
Vinyl chloride 20.0 18.92 ug/L 95 57-137
Xylenes, Total 40.0 39.81 ug/L 100 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1041,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-381094/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
Acetone 100 84.28 ug/L 84 39-150 0 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 180.0 ug/L 90 63-135 1 16
Benzene 20.0 18.71 ug/L 94 70-130 1 12
Bromochloromethane 20.0 20.38 ug/L 102 70-130 2 16
Bromodichloromethane 20.0 18.64 ug/L 93 70-130 1 14
Bromoform 20.0 18.84 ug/L 94 70-137 1 14
Bromomethane 20.0 21.97 ug/L 110 53-150 1 19
2-Butanone (MEK)100 96.90 ug/L 97 55-143 4 19
Carbon disulfide 20.0 18.06 ug/L 90 64-135 4 16
Carbon tetrachloride 20.0 19.28 ug/L 96 70-147 2 16
Chlorobenzene 20.0 19.66 ug/L 98 70-130 1 12
Chloroethane 20.0 18.06 ug/L 90 60-138 0 15
Chloroform 20.0 20.61 ug/L 103 70-130 1 14
Chloromethane 20.0 15.51 ug/L 78 33-150 2 20
cis-1,2-Dichloroethene 20.0 19.40 ug/L 97 70-130 2 15
cis-1,3-Dichloropropene 20.0 18.24 ug/L 91 70-133 1 15
Dibromochloromethane 20.0 19.00 ug/L 95 70-133 3 13
1,2-Dibromo-3-Chloropropane 20.0 17.19 ug/L 86 45-138 7 19
1,2-Dibromoethane (EDB)20.0 19.25 ug/L 96 70-130 1 13
Dibromomethane 20.0 19.75 ug/L 99 70-130 1 14
1,2-Dichlorobenzene 20.0 20.54 ug/L 103 70-130 0 12
1,4-Dichlorobenzene 20.0 19.53 ug/L 98 70-130 2 12
1,1-Dichloroethane 20.0 19.91 ug/L 100 70-130 1 17
1,2-Dichloroethane 20.0 21.37 ug/L 107 70-130 2 13
1,1-Dichloroethene 20.0 20.21 ug/L 101 70-132 3 20
1,2-Dichloropropane 20.0 18.00 ug/L 90 70-130 0 15
Ethylbenzene 20.0 18.57 ug/L 93 70-130 0 12
2-Hexanone 100 82.40 ug/L 82 54-142 3 17
Iodomethane 20.0 21.34 ug/L 107 40-150 4 20
Methylene Chloride 20.0 19.53 ug/L 98 70-130 3 15
4-Methyl-2-pentanone (MIBK)100 87.50 ug/L 88 60-137 1 21
Styrene 20.0 19.56 ug/L 98 70-130 1 12
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-381094/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
1,1,1,2-Tetrachloroethane 20.0 19.57 ug/L 98 70-130 3 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 20.0 17.54 ug/L 88 69-131 0 15
Tetrachloroethene 20.0 19.82 ug/L 99 70-130 0 17
Tetrahydrofuran 40.0 41.87 ug/L 105 51-136 7 20
Toluene 20.0 18.45 ug/L 92 70-130 0 13
trans-1,4-Dichloro-2-butene 20.0 17.27 ug/L 86 41-150 2 20
trans-1,2-Dichloroethene 20.0 19.47 ug/L 97 70-130 0 15
trans-1,3-Dichloropropene 20.0 19.06 ug/L 95 63-142 1 13
1,1,1-Trichloroethane 20.0 19.14 ug/L 96 70-135 0 15
1,1,2-Trichloroethane 20.0 18.66 ug/L 93 70-130 2 13
Trichloroethene 20.0 19.70 ug/L 98 70-130 1 14
Trichlorofluoromethane 20.0 22.58 ug/L 113 59-150 1 22
1,2,3-Trichloropropane 20.0 19.55 ug/L 98 70-131 1 14
Vinyl acetate 40.0 40.54 ug/L 101 54-146 0 20
Vinyl chloride 20.0 18.17 ug/L 91 57-137 4 15
Xylenes, Total 40.0 39.06 ug/L 98 70-132 2 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
91
LCSD LCSD
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
92Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-114602-C-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
Acetone <2.66 100 90.22 ug/L 90 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 180.0 ug/L 90 50-135
Benzene <0.200 20.0 20.25 ug/L 101 55-147
Bromochloromethane <0.150 20.0 21.37 ug/L 107 59-132
Bromodichloromethane <0.170 20.0 19.03 ug/L 95 70-140
Bromoform <0.290 20.0 18.19 ug/L 91 53-150
Bromomethane <0.350 20.0 21.51 ug/L 108 30-150
2-Butanone (MEK)<2.64 100 91.92 ug/L 92 50-143
Carbon disulfide <0.220 20.0 19.24 ug/L 96 35-150
Carbon tetrachloride <0.180 20.0 21.11 ug/L 106 56-150
Chlorobenzene <0.180 20.0 20.31 ug/L 102 70-130
Chloroethane <0.360 20.0 19.17 ug/L 96 58-141
Chloroform <0.230 20.0 21.50 ug/L 107 66-138
Chloromethane <0.360 20.0 17.60 ug/L 88 10-150
cis-1,2-Dichloroethene <0.210 20.0 20.85 ug/L 104 68-131
cis-1,3-Dichloropropene <0.170 20.0 18.69 ug/L 93 70-133
Dibromochloromethane <0.250 20.0 19.83 ug/L 99 66-140
1,2-Dibromo-3-Chloropropane <0.940 20.0 17.36 ug/L 87 38-138
1,2-Dibromoethane (EDB)<0.210 20.0 19.57 ug/L 98 65-137
Dibromomethane <0.450 20.0 20.35 ug/L 102 70-130
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-114602-C-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
1,2-Dichlorobenzene <0.190 20.0 20.59 ug/L 103 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,4-Dichlorobenzene <0.170 20.0 20.07 ug/L 100 70-130
1,1-Dichloroethane <0.240 20.0 21.44 ug/L 107 61-139
1,2-Dichloroethane <0.200 20.0 21.54 ug/L 108 64-136
1,1-Dichloroethene <0.250 20.0 22.40 ug/L 112 54-150
1,2-Dichloropropane <0.250 20.0 18.18 ug/L 91 67-130
Ethylbenzene <0.190 20.0 19.47 ug/L 97 65-139
2-Hexanone <1.28 100 83.32 ug/L 83 44-150
Iodomethane <1.50 20.0 22.47 ug/L 112 34-150
Methylene Chloride <1.00 20.0 19.84 ug/L 99 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 89.89 ug/L 90 50-140
Styrene <0.280 20.0 20.00 ug/L 100 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 20.08 ug/L 100 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 17.58 ug/L 88 56-145
Tetrachloroethene <0.140 20.0 20.51 ug/L 103 57-138
Tetrahydrofuran <0.820 40.0 36.96 ug/L 92 40-136
Toluene <0.170 20.0 19.49 ug/L 97 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 16.17 ug/L 81 39-150
trans-1,2-Dichloroethene <0.230 20.0 21.02 ug/L 105 59-143
trans-1,3-Dichloropropene <0.170 20.0 19.09 ug/L 95 63-142
1,1,1-Trichloroethane <0.190 20.0 20.65 ug/L 103 68-144
1,1,2-Trichloroethane <0.190 20.0 18.71 ug/L 94 70-130
Trichloroethene <0.200 20.0 20.92 ug/L 105 63-135
Trichlorofluoromethane <0.210 20.0 23.85 ug/L 119 44-150
1,2,3-Trichloropropane <0.230 20.0 19.73 ug/L 99 65-131
Vinyl acetate <1.71 40.0 30.41 ug/L 76 43-146
Vinyl chloride <0.180 20.0 19.84 ug/L 99 57-150
Xylenes, Total <0.580 40.0 40.32 ug/L 101 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
91
MS MS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
981,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114602-D-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
Acetone <2.66 100 79.96 ug/L 80 39-150 12 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 163.9 ug/L 82 50-135 9 23
Benzene <0.200 20.0 19.30 ug/L 96 55-147 5 22
Bromochloromethane <0.150 20.0 19.78 ug/L 99 59-132 8 21
Bromodichloromethane <0.170 20.0 18.15 ug/L 91 70-140 5 196
Bromoform <0.290 20.0 17.64 ug/L 88 53-150 3 20
Bromomethane <0.350 20.0 21.01 ug/L 105 30-150 2 44
2-Butanone (MEK)<2.64 100 84.30 ug/L 84 50-143 9 28
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114602-D-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381094
Carbon disulfide <0.220 20.0 18.33 ug/L 92 35-150 5 34
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride <0.180 20.0 19.86 ug/L 99 56-150 6 18
Chlorobenzene <0.180 20.0 20.68 ug/L 103 70-130 2 15
Chloroethane <0.360 20.0 17.68 ug/L 88 58-141 8 31
Chloroform <0.230 20.0 20.36 ug/L 102 66-138 5 21
Chloromethane <0.360 20.0 15.12 ug/L 76 10-150 15 43
cis-1,2-Dichloroethene <0.210 20.0 19.64 ug/L 98 68-131 6 21
cis-1,3-Dichloropropene <0.170 20.0 18.76 ug/L 94 70-133 0 19
Dibromochloromethane <0.250 20.0 19.55 ug/L 98 66-140 1 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 16.40 ug/L 82 38-138 6 26
1,2-Dibromoethane (EDB)<0.210 20.0 19.28 ug/L 96 65-137 1 21
Dibromomethane <0.450 20.0 18.85 ug/L 94 70-130 8 19
1,2-Dichlorobenzene <0.190 20.0 20.30 ug/L 102 70-130 1 15
1,4-Dichlorobenzene <0.170 20.0 19.90 ug/L 99 70-130 1 14
1,1-Dichloroethane <0.240 20.0 19.62 ug/L 98 61-139 9 23
1,2-Dichloroethane <0.200 20.0 20.17 ug/L 101 64-136 7 22
1,1-Dichloroethene <0.250 20.0 20.80 ug/L 104 54-150 7 24
1,2-Dichloropropane <0.250 20.0 17.43 ug/L 87 67-130 4 19
Ethylbenzene <0.190 20.0 19.35 ug/L 97 65-139 1 18
2-Hexanone <1.28 100 82.48 ug/L 82 44-150 1 21
Iodomethane <1.50 20.0 20.84 ug/L 104 34-150 7 37
Methylene Chloride <1.00 20.0 18.57 ug/L 93 64-130 7 22
4-Methyl-2-pentanone (MIBK)<0.810 100 87.68 ug/L 88 50-140 2 24
Styrene <0.280 20.0 19.85 ug/L 99 70-130 1 16
1,1,1,2-Tetrachloroethane <0.150 20.0 20.56 ug/L 103 70-131 2 16
1,1,2,2-Tetrachloroethane <0.190 20.0 17.05 ug/L 85 56-145 3 19
Tetrachloroethene <0.140 20.0 21.11 ug/L 106 57-138 3 17
Tetrahydrofuran <0.820 40.0 32.50 ug/L 81 40-136 13 27
Toluene <0.170 20.0 19.59 ug/L 98 64-136 1 18
trans-1,4-Dichloro-2-butene <0.460 20.0 16.20 ug/L 81 39-150 0 28
trans-1,2-Dichloroethene <0.230 20.0 19.37 ug/L 97 59-143 8 25
trans-1,3-Dichloropropene <0.170 20.0 19.23 ug/L 96 63-142 1 18
1,1,1-Trichloroethane <0.190 20.0 18.98 ug/L 95 68-144 8 17
1,1,2-Trichloroethane <0.190 20.0 18.85 ug/L 94 70-130 1 18
Trichloroethene <0.200 20.0 20.36 ug/L 102 63-135 3 17
Trichlorofluoromethane <0.210 20.0 22.90 ug/L 114 44-150 4 32
1,2,3-Trichloropropane <0.230 20.0 18.86 ug/L 94 65-131 5 19
Vinyl acetate <1.71 40.0 32.01 ug/L 80 43-146 5 20
Vinyl chloride <0.180 20.0 18.58 ug/L 93 57-150 7 37
Xylenes, Total <0.580 40.0 40.39 ug/L 101 69-132 0 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
90
MSD MSD
Qualifier Limits%Recovery
95Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 490-380814/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380814
RL MDL
Sulfate <0.600 1.00 0.600 mg/L 10/22/16 16:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380814/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380814
Sulfate 10.0 9.971 mg/L 100 90-110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380814/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380814
Sulfate 10.0 10.01 mg/L 100 90-110 0 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-380927/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382503 Prep Batch: 380927
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 10/25/16 10:57 10/30/16 09:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.00500 0.005000.0100 mg/L 10/25/16 10:57 10/30/16 09:33 1Barium
<0.000500 0.0005000.00100 mg/L 10/25/16 10:57 10/30/16 09:33 1Cadmium
<0.00300 0.003000.00500 mg/L 10/25/16 10:57 10/30/16 09:33 1Chromium
<0.00500 0.005000.0100 mg/L 10/25/16 10:57 10/30/16 09:33 1Copper
<0.00200 0.002000.00500 mg/L 10/25/16 10:57 10/30/16 09:33 1Lead
<0.00300 0.003000.0100 mg/L 10/25/16 10:57 10/30/16 09:33 1Nickel
<0.00500 0.005000.0100 mg/L 10/25/16 10:57 10/30/16 09:33 1Selenium
<0.00300 0.003000.00500 mg/L 10/25/16 10:57 10/30/16 09:33 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380927/25-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382503 Prep Batch: 380927
Silver 0.0500 0.04570 mg/L 91 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380927/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382503 Prep Batch: 380927
Arsenic 0.0500 0.04930 mg/L 99 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.119 mg/L 106 80-120
Cadmium 0.0500 0.05080 mg/L 102 80-120
Chromium 0.200 0.2235 mg/L 112 80-120
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380927/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382503 Prep Batch: 380927
Copper 0.250 0.2581 mg/L 103 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Lead 0.0500 0.05040 mg/L 101 80-120
Nickel 0.500 0.5147 mg/L 103 80-120
Selenium 0.0500 0.05750 mg/L 115 80-120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114525-F-2-A MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382503 Prep Batch: 380927
Arsenic <0.00860 0.0500 0.05640 mg/L 113 75-125 7 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0173 2.00 2.033 mg/L 101 75-125 1 20
Cadmium <0.000500 0.0500 0.03920 mg/L 78 75-125 2 20
Chromium <0.00300 0.200 0.2040 mg/L 102 75-125 0 20
Copper <0.00500 0.250 0.2584 mg/L 103 75-125 0 20
Lead <0.00200 0.0500 0.04080 mg/L 82 75-125 3 20
Nickel <0.00300 0.500 0.4670 mg/L 93 75-125 1 20
Selenium 0.00990 J F2 0.0500 0.06630 F2 mg/L 113 75-125 21 20
Silver <0.00300 0.0500 0.04150 mg/L 83 75-125 0 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-114525-H-2-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382503 Prep Batch: 380927
Arsenic <0.00860 0.0500 0.05240 mg/L 105 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0173 2.00 2.053 mg/L 102 75-125
Cadmium <0.000500 0.0500 0.03840 mg/L 77 75-125
Chromium <0.00300 0.200 0.2032 mg/L 102 75-125
Copper <0.00500 0.250 0.2596 mg/L 104 75-125
Lead <0.00200 0.0500 0.03970 mg/L 79 75-125
Nickel <0.00300 0.500 0.4695 mg/L 94 75-125
Selenium 0.00990 J F2 0.0500 0.05360 mg/L 87 75-125
Silver <0.00300 0.0500 0.04140 mg/L 83 75-125
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-380936/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382907 Prep Batch: 380936
RL MDL
Antimony <0.800 2.00 0.800 ug/L 10/25/16 11:03 10/31/16 21:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.100 0.1002.00 ug/L 10/25/16 11:03 10/31/16 21:29 1Beryllium
<0.100 0.1002.00 ug/L 10/25/16 11:03 10/31/16 21:29 1Cobalt
<0.800 0.8002.00 ug/L 10/25/16 11:03 10/31/16 21:29 1Thallium
1.049 J 0.7002.00 ug/L 10/25/16 11:03 10/31/16 21:29 1Vanadium
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-380936/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384117 Prep Batch: 380936
RL MDL
Zinc <5.20 25.0 5.20 ug/L 10/25/16 11:03 11/03/16 19:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380936/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382907 Prep Batch: 380936
Antimony 100 91.75 ug/L 92 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Beryllium 100 88.01 ug/L 88 80-120
Cobalt 100 101.6 ug/L 102 80-120
Thallium 100 97.38 ug/L 97 80-120
Vanadium 100 100.7 ug/L 101 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380936/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384117 Prep Batch: 380936
Zinc 100 88.90 J ug/L 89 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114525-F-2-B MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382907 Prep Batch: 380936
Antimony <4.00 100 98.70 ug/L 99 75-125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.500 100 84.75 ug/L 85 75-125 1 20
Cobalt 2.67 J 100 99.40 ug/L 97 75-125 2 20
Thallium <4.00 100 90.05 ug/L 90 75-125 0 20
Vanadium <3.50 100 101.4 ug/L 101 75-125 7 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-114525-H-2-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382907 Prep Batch: 380936
Antimony <4.00 100 100.4 ug/L 100 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Beryllium <0.500 100 84.05 ug/L 84 75-125
Cobalt 2.67 J 100 101.9 ug/L 99 75-125
Thallium <4.00 100 89.70 ug/L 90 75-125
Vanadium <3.50 100 108.4 ug/L 108 75-125
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-380048/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380514 Prep Batch: 380048
RL MDL
Mercury <0.100 0.200 0.100 ug/L 10/21/16 08:31 10/21/16 16:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380048/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380514 Prep Batch: 380048
Mercury 1.00 0.9823 ug/L 98 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-114145-D-1-E MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380514 Prep Batch: 380048
Mercury <0.100 1.00 0.9382 ug/L 94 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114145-D-1-F MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380514 Prep Batch: 380048
Mercury <0.100 1.00 0.8793 ug/L 88 75-125 6 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 365.4 - Phosphorus, Total
Client Sample ID: Method BlankLab Sample ID: MB 490-381417/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381569 Prep Batch: 381417
RL MDL
Phosphorus, Total <0.0500 0.100 0.0500 mg/L 10/26/16 14:09 10/26/16 18:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381417/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381569 Prep Batch: 381417
Phosphorus, Total 2.00 2.029 mg/L 101 90-110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-381417/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381569 Prep Batch: 381417
Phosphorus, Total 2.00 2.022 mg/L 101 90-110 0 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: 365.4 - Phosphorus, Total (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 580-63494-D-2-H MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381569 Prep Batch: 381417
Phosphorus, Total 0.333 2.00 2.307 mg/L 99 73-119
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 580-63494-D-2-I MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381569 Prep Batch: 381417
Phosphorus, Total 0.333 2.00 2.292 mg/L 98 73-119 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: SM 5220D - COD
Client Sample ID: Method BlankLab Sample ID: MB 490-381445/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
RL MDL
Chemical Oxygen Demand <4.00 20.0 4.00 mg/L 10/26/16 15:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381445/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 50.0 48.59 mg/L 97 95-105
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-381445/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 50.0 48.47 mg/L 97 95-105 0 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-114484-A-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 52.3 F1 50.0 98.76 F1 mg/L 93 95-105
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114484-A-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 52.3 F1 50.0 96.73 F1 mg/L 89 95-105 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method: SM 5220D - COD (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 580-63307-E-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 93.1 50.0 144.3 mg/L 102 95-105
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 580-63307-E-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 93.1 50.0 145.7 mg/L 105 95-105 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 580-63307-E-2 DU ^2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381445
Chemical Oxygen Demand 190 190.2 mg/L 0.1 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM5210B - BOD, 5 Day
Client Sample ID: Method BlankLab Sample ID: USB 490-381875/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381875
RL RL
Biochemical Oxygen Demand <2.00 2.00 2.00 mg/L 10/19/16 18:24 1
USB USB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-381875/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381875
Biochemical Oxygen Demand 3.96 4.027 mg/L 102 85-115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: DuplicateLab Sample ID: 490-114298-C-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381875
Biochemical Oxygen Demand 14.4 11.77 mg/L 20 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
GC/MS VOA
Analysis Batch: 380978
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-114300-1 LT-01 Total/NA
Water 8260BMB 490-380978/7 Method Blank Total/NA
Water 8260BLCS 490-380978/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-380978/4 Lab Control Sample Dup Total/NA
Water 8260B490-114300-1 MS LT-01 Total/NA
Water 8260B490-114300-1 MSD LT-01 Total/NA
Analysis Batch: 381094
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-114300-2 Trip Blank Total/NA
Water 8260BMB 490-381094/7 Method Blank Total/NA
Water 8260BLCS 490-381094/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-381094/4 Lab Control Sample Dup Total/NA
Water 8260B490-114602-C-2 MS Matrix Spike Total/NA
Water 8260B490-114602-D-2 MSD Matrix Spike Duplicate Total/NA
HPLC/IC
Analysis Batch: 380814
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0490-114300-1 LT-01 Total/NA
Water 300.0MB 490-380814/3 Method Blank Total/NA
Water 300.0LCS 490-380814/4 Lab Control Sample Total/NA
Water 300.0LCSD 490-380814/5 Lab Control Sample Dup Total/NA
Metals
Prep Batch: 380048
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-114300-1 LT-01 Total/NA
Water 7470AMB 490-380048/1-A Method Blank Total/NA
Water 7470ALCS 490-380048/2-A Lab Control Sample Total/NA
Water 7470A490-114145-D-1-E MS Matrix Spike Total/NA
Water 7470A490-114145-D-1-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 380514
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 380048490-114300-1 LT-01 Total/NA
Water 7470A 380048MB 490-380048/1-A Method Blank Total/NA
Water 7470A 380048LCS 490-380048/2-A Lab Control Sample Total/NA
Water 7470A 380048490-114145-D-1-E MS Matrix Spike Total/NA
Water 7470A 380048490-114145-D-1-F MSD Matrix Spike Duplicate Total/NA
Prep Batch: 380927
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114300-1 LT-01 Total/NA
Water 3010AMB 490-380927/1-A Method Blank Total/NA
Water 3010ALCS 490-380927/25-A Lab Control Sample Total/NA
Water 3010ALCS 490-380927/2-A Lab Control Sample Total/NA
Water 3010A490-114525-F-2-A MSD Matrix Spike Duplicate Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Metals (Continued)
Prep Batch: 380927 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114525-H-2-A MS Matrix Spike Total/NA
Prep Batch: 380936
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-114300-1 LT-01 Total/NA
Water 3010AMB 490-380936/1-A Method Blank Total/NA
Water 3010ALCS 490-380936/2-A Lab Control Sample Total/NA
Water 3010A490-114525-F-2-B MSD Matrix Spike Duplicate Total/NA
Water 3010A490-114525-H-2-B MS Matrix Spike Total/NA
Analysis Batch: 382503
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 380927490-114300-1 LT-01 Total/NA
Water 6010D 380927MB 490-380927/1-A Method Blank Total/NA
Water 6010D 380927LCS 490-380927/25-A Lab Control Sample Total/NA
Water 6010D 380927LCS 490-380927/2-A Lab Control Sample Total/NA
Water 6010D 380927490-114525-F-2-A MSD Matrix Spike Duplicate Total/NA
Water 6010D 380927490-114525-H-2-A MS Matrix Spike Total/NA
Analysis Batch: 382907
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 380936490-114300-1 LT-01 Total/NA
Water 6020B 380936MB 490-380936/1-A Method Blank Total/NA
Water 6020B 380936LCS 490-380936/2-A Lab Control Sample Total/NA
Water 6020B 380936490-114525-F-2-B MSD Matrix Spike Duplicate Total/NA
Water 6020B 380936490-114525-H-2-B MS Matrix Spike Total/NA
Analysis Batch: 384117
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 380936490-114300-1 LT-01 Total/NA
Water 6020B 380936MB 490-380936/1-A Method Blank Total/NA
Water 6020B 380936LCS 490-380936/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 381004
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Nitrate by calc490-114300-1 LT-01 Total/NA
Prep Batch: 381417
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 365.2/365.3/365490-114300-1 LT-01 Total/NA
Water 365.2/365.3/365MB 490-381417/1-A Method Blank Total/NA
Water 365.2/365.3/365LCS 490-381417/2-A Lab Control Sample Total/NA
Water 365.2/365.3/365LCSD 490-381417/3-A Lab Control Sample Dup Total/NA
Water 365.2/365.3/365580-63494-D-2-H MS Matrix Spike Total/NA
Water 365.2/365.3/365580-63494-D-2-I MSD Matrix Spike Duplicate Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
General Chemistry (Continued)
Analysis Batch: 381445
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 5220D490-114300-1 LT-01 Total/NA
Water SM 5220DMB 490-381445/3 Method Blank Total/NA
Water SM 5220DLCS 490-381445/4 Lab Control Sample Total/NA
Water SM 5220DLCSD 490-381445/5 Lab Control Sample Dup Total/NA
Water SM 5220D490-114484-A-1 MS Matrix Spike Total/NA
Water SM 5220D490-114484-A-1 MSD Matrix Spike Duplicate Total/NA
Water SM 5220D580-63307-E-1 MS Matrix Spike Total/NA
Water SM 5220D580-63307-E-1 MSD Matrix Spike Duplicate Total/NA
Water SM 5220D580-63307-E-2 DU ^2 Duplicate Total/NA
Analysis Batch: 381569
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 365.4 381417490-114300-1 LT-01 Total/NA
Water 365.4 381417MB 490-381417/1-A Method Blank Total/NA
Water 365.4 381417LCS 490-381417/2-A Lab Control Sample Total/NA
Water 365.4 381417LCSD 490-381417/3-A Lab Control Sample Dup Total/NA
Water 365.4 381417580-63494-D-2-H MS Matrix Spike Total/NA
Water 365.4 381417580-63494-D-2-I MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 381875
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM5210B490-114300-1 LT-01 Total/NA
Water SM5210BUSB 490-381875/1 Method Blank Total/NA
Water SM5210BLCS 490-381875/2 Lab Control Sample Total/NA
Water SM5210B490-114298-C-1 DU Duplicate Total/NA
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Lab Chronicle
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114300-1
Project/Site: Madison Co Operating Landfill
Client Sample ID: LT-01 Lab Sample ID: 490-114300-1
Matrix: WaterDate Collected: 10/18/16 13:45
Date Received: 10/19/16 09:20
Analysis 8260B RP10/25/16 19:221 TAL NSH380978
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Analysis 300.0 10 380814 10/22/16 18:39 NC TAL NSHTotal/NA
Prep 3010A 380927 10/25/16 10:57 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 382503 10/30/16 10:38 BLG TAL NSHTotal/NA
Prep 3010A 380936 10/25/16 11:03 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 5 382907 10/31/16 22:09 KKK TAL NSHTotal/NA
Prep 3010A 380936 10/25/16 11:03 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6020B 5 384117 11/03/16 20:50 KKK TAL NSHTotal/NA
Prep 7470A 380048 10/21/16 08:31 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 380514 10/21/16 17:41 LCS TAL NSHTotal/NA
Prep 365.2/365.3/365 381417 10/26/16 14:09 LDT TAL NSHTotal/NA 20 mL 20 mL
Analysis 365.4 1 381569 10/26/16 18:16 SDL TAL NSHTotal/NA 20 mL 20 mL
Analysis Nitrate by calc 1 381004 10/19/16 13:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis SM 5220D 1 381445 10/26/16 15:02 MSJ TAL NSHTotal/NA 2 mL 2 mL
Analysis SM5210B 1 381875 SD TAL NSHTotal/NA
10/19/16 18:24
10/24/16 13:30
(Start)
(End)
Client Sample ID: Trip Blank Lab Sample ID: 490-114300-2
Matrix: WaterDate Collected: 10/18/16 01:01
Date Received: 10/19/16 09:20
Analysis 8260B RP10/26/16 03:571 TAL NSH381094
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-114300-1Client: Altamont Environmental, Inc.
Project/Site: Madison Co Operating Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
MCAWW300.0 Anions, Ion Chromatography TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
EPA365.4 Phosphorus, Total TAL NSH
SMNitrate by calc Nitrogen, Nitrate-Nitrite TAL NSH
SMSM 5220D COD TAL NSH
SMSM5210B BOD, 5 Day TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Altamont Environmental, Inc.TestAmerica Job ID: 490-114300-1
Project/Site: Madison Co Operating Landfill
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Nitrate by calc Water Nitrate as N
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Altamont Environmental, Inc.Job Number: 490-114300-1
SDG Number:
Login Number: 114300
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueResidual Chlorine Checked.
TestAmerica Nashville
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